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RECEIVED I DENR r DWQ
AQUIPcP vPnTrr-T1pN gPUICN
OCT 4 2 2009
c�c Quarterly HiSOC Monitoring Report
Gilbarco
7300 West Friendly Avenue
Greensboro, North Carolina
Kleinfelder Project No. 97746
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('KL EINFEL,DER
Bright People. Hight Solutions.
September 18, 2009
Fife No. 977461 GS009R167
Mr. Qu Qi
Aquifer Protection Section — UIC Staff
❑ENR — Division of Water Quality
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Reference: Quarterly HiSGC Monitoring Report
Gilbarco
7300 West Friendly Avenue
Greensboro, North Carolina
Kleinfelder Project No. 97746 1 GS009R
Dear Mr. Qi:
Kleinfelder is pleased to provide our quarterly monitoring report for the Underground
Injection Control (U1C) Permit for treatment of groundwater with the HiSQC system at
the referenced site. This report summarizes our field activities, observations, and
includes the analytical results of the groundwater samples. Should you have any
questions or require additional information, please do not hesitate to contact Chris Hay
at your convenience.
Very truly yours,
KLEINFELDER SOUTHEAST, INC.
000
�-O
Christopher W. Hay, E.I.
Environmental Group Manager
Gail G. Licayan, P.E.
Project Professional
CWHIGGL:cas
313 Galhmore Dairy Road, Greensboro, NC 27409 p 1 336.668,0093 f 1336 668-3868
GILBARCO
Greensboro, North Carolina
Groundwater Incident Nos. 12960 And 15123
SITE INFORMATION
Address:
Contact:
Telephone:
Latitude and Longitude
Risk Classification:
Land Use Category:
LAND OWNERSHIP
Name:
Address:
Telephone:
Attention:
RELEASE INFORMATION
September 30, 2009
7300 West Friendly Avenue
Greensboro, North Carolina
Ms. Beth Money
336,547.5130
36.0901 ON, 79.9282 °W
Low
Commercial
Gilbarco
7300 West Friendly Avenue
Greensboro, North Carolina 27420
336.547.5130
Ms. Beth Money
RECEIVED ! DENR I DVVR
AOUIF�a 0Rf17f'TInN 0,F(710N
OCT 0 2 2009
Cause of Release: Release from a 1,000-gallon diesel UST and four
550-gallon gasoline USTs was discovered in
November and December 1994. The quantity
released is unknown.
ENVIRONMENTAL CONSULTANT
Name: Kleinfelder Southeast, Inc.
Address: Post Office Box 18846
Greensboro, North Carolina 27419-8846
Telephone: 336.668.0093
Attention: Mr. Christopher W. Hay
Seal and ",g�WjHr,e of Certifying Professional Engineer
�ZH C A R a ��f�
i, Gail Geis�r<q,;��i�ssional Engineer for Kleinfelder do certify that the information
contai aed. his re s�&orrect and accurate to the best of my knowledge.
SEAL
Gail G 4,i�,a
RegisteVll a Engineer No. 031532
I01111$1110\0
97746 i GS009R167 Page i September 30, 2099
Copyright 2009 Kleinfelder
TABLE OF CONTENTS
1.0
INTRODUCTION......................................................................................................1
2.0
GROUNDWATER MONITORING ACTIVITIES........................................................1
3.0
HiSOC INSTALLATION AND MONITORING...........................................................2
4.0
GROUNDWATER ANALYTICAL RESULTS............................................................4
5.0
CONCLUSIONS AND RECOMMENDATIONS... ......................................................
5
TABLES
1 Groundwater Elevation Data
2 Estimated Dissolved Hydrogen Concentrations at Injection Wells
3 Estimated Hydrogen Consumption
4 Aquifer Characteristics Field Analysis Summary
5 Summary of Groundwater Sample Results
6 Historical Summary of Groundwater Sample Results
FIGURES
1 Site Location Map
2 Site Plan
3 Groundwater Potentiometric Surface Map
4 Total VOCs Concentrations
5 Total Chlorinated Hydrocarbons
APPENDICES
A Laboratory Report and Chain -of -Custody Document
B Total VOC Graphs
977461 GS009R167 Page ii September 30, 2009
Capynght 2009 Kleinfeider
1.0 INTRODUCTION
The subject site is located at 7300 West Friendly Avenue in Greensboro, Guilford
County, North Carolina (Figure 1). There are currently two open groundwater incidents
(Incident Nos. 12960 and 15123). The incidents have a commingled plume and are
being treated with the same corrective action plan. A pump and treat system is
operating at the site, The system consists of four recovery wells, an oil -water
separator, and an air stripping system.
In January 2008, Kleinfelder submitted a CAP Addendum recommending the use of
HiSOC and iSOC technology to degrade the chlorinated and petroleum hydrocarbons in
groundwater at the site. This technology will work in concert with the existing
groundwater recovery system and supplement the ability of the system to contain the
contaminant plume within the property limits and reduce contaminant levels. The
HiSOC system was installed in June of 2008 and began operating on June 13, 2008.
The baseline sampling event was conducted on June 5, 2008. The purpose of this
report is to summarize the quarterly monitoring of the HiSOC system performed on
September 2, 2009.
2.0 GROUNDWATER MONITORING ACTIVITIES
Static water levels were measured in the existing monitoring wells on -site on September
2, 2009. Groundwater samples were collected from twelve of the monitoring wells
(MW-7, MW-11, MW-13, MW-13D, MW-14, MW-14D, MW-23D, MW-24, MW-25,
MW-42, MW-43D, and MW-45) and analyzed for VOCs by EPA Methods 601 and 602,
isopropyl ether, methyl tert-butyl ether, ethylene dibromide, and xylenes. Field
parameters including oxidation-reduction potential (ORP), pH, conductivity, dissolved
oxygen, and temperature of representative groundwater samples were also recorded
from each monitoring well sampled. Groundwater elevations in the existing monitoring
wells were used to determine the groundwater flow direction, average hydraulic
gradient, and plume orientation. Table 1 provides a summary of monitoring well
construction details and the groundwater elevations measured on September 2, 2009.
The monitoring well locations are shown on Figure 2. The static water levels measured
between monitoring wells MW-32 and MW-45 indicate a horizontal groundwater flow
977461 GS009R167 Page 1 of 6 September 30, 2009
Copyright 2009 Kleinfelder
gradient of 0.04 feet per foot to the northwest. A groundwater flow map of the shallow
aquifer based on the September 2, 2009 groundwater elevations are shown on Figure
3. Free product was not observed in any of the monitoring wells during the sampling
event.
Based on data provided in the October 1996 Corrective Action Plan, the surficial aquifer
has an average hydraulic conductivity of 0.09 feet per day. The average groundwater
velocity is estimated to be 0.01 feet per day (4 feet per year), based on the average
groundwater gradient from the September 2, 2009 water level measurements and an
estimated effective porosity of thirty percent.
Groundwater samples were collected from monitoring wells MW-7, MW-11, MW-13,
MW-13D, MW-14, MW-14D, MW-23D, MW-24, MW-25, MW-42, MW-43D, and MW-45
using disposable polyethylene bailers. The wells were purged of three well volumes of
water or until they were bailed dry. Groundwater purged from the monitoring wells was
disposed of in the on -site groundwater recovery system. Groundwater samples were
collected and placed in laboratory prepared containers. The samples were maintained
on ice until delivered to Pace Analytical Laboratories in Huntersville, North Carolina.
3.0 HiSOC INSTALLATION AND MONITORING
Kleinfelder applied for a permit from the Underground Injection Control (U1C) Program
for the installation of a hydrogen and oxygen delivery system for remediation of
contaminants in groundwater at the site. A permit dated March 20, 2008 was issued for
the site (Injection Well Permit W10400091). The permit is effective through April 30,
2010.
Installation of the injection equipment was initiated on April 9 through April 11, 2008.
The existing protective casings were removed from monitoring wells MW-7, MW-10,
MW-23D, MW-29, and MW-34. Ten -inch diameter PVC casings were installed to a
depth of five feet below ground surface adjacent to the monitoring well locations to hold
the hydrogen cylinders. Six to ten inches of gravel was placed in the bottom of each
casing. Excavations were completed for installation of 24-inch square, steel well vaults
and the vaults were set in concrete flush with the ground surface. Protective vaults
were also installed adjacent to the existing above grade protective covers for monitoring
977461 GS009R167 Page 2 of 6 September 30, 2009
Copyright 2009 Kleinfe}der
wells MW-14D, MW-15, MW-16, MW-24, and MW-43D. The 15-inch by 24-inch PVC
protective vaults were installed over the cylinder casings. Vents were installed in the
protective vaults to allow hydrogen to be released in the case of a leak from the delivery
system.
The HiSOC equipment from InVentures was installed at the site in ten existing
monitoring wells (MW-7, MW-10, MW-14D, MW-15, MW-16, MW-231D, MW-24, MW-
29, MW-34, and MW-431D) on June 13, 2008. Within each injection well is a HiSOC
unit and filter. Hydrogen is supplied from a compressed gas cylinder with a regulator
and gauge connected to the HiSOC unit by Parflex tubing and a support cable.
Four -foot grounding rods were installed and connected to the regulator assembly of the
gas cylinders. The HiSOC installation locations are shown on the figures in orange.
On May 13, 2009 the HiSOC equipment was removed from monitoring well MW-10 and
installed in monitoring well MW-25. The hydrogen cylinder was placed on the existing
concrete well pad and a protective cover was constructed around the well and above
ground protective well casing. The protective cover includes three sides and a top
made of dimensional lumber, roofing paper, and asphalt shingles. The east side of the
enclosure is open. A new grounding rod was installed. Other details of the HiSOC
installation at MW-25 are substantially the same as described for the initial installation.
In anaerobic bioremediation applications, the HiSOC supersaturates the treatment well
with dissolved hydrogen, typically at a concentration of 1 to 4 parts per million (ppm)
depending on the immersion depth of the HiSOC unit in groundwater. The dissolved
hydrogen concentration achieved in the injection well depends on the height of the
water column in the well. Each atmosphere of pressure allows for a maximum of
approximately 1.6 ppm of dissolved hydrogen. Table 2 estimates the dissolved
hydrogen concentrations in each of the injection wells. These concentrations are
estimated based on the approximate pressure at the installation depth of the HiSOC
based on the depth of the water column in the injection wells. The calculation is made
with the assumption that 1.6 ppm of hydrogen is dissolved in the groundwater per
atmosphere of pressure.
Hydrogen is infused from the HiSOC into the treatment well at a typical rate of 28
standard cubic centimeters per minute or approximately 1.4 cubic feet per day. The
hydrogen consumption in each of the injection wells is tracked to estimate the
977461 GS009R167 Page 3 of 6 September 30, 2009
Copyright 2009 Kleinfelder
remaining service life of the hydrogen cylinders. Table 3 shows the recorded hydrogen
cylinder pressures and estimates a date for each injection well that the cylinder should
be replaced. It is anticipated that the hydrogen cylinders will be replaced prior to the
next quarterly monitoring event scheduled for December 2009.
The HiSOC produces a convection current in the well with a designed release bubble
from the top of the HiSCC to distribute dissolved hydrogen rich water throughout the
screened interval. A curtain of hydrogen rich water disperses around the well into the
adjacent groundwater forming a treatment zone allowing enhanced bioremediation to
degrade the target contaminants.
4.0 GROUNDWATER ANALYTICAL RESULTS
The groundwater field analysis generally indicates that the subsurface environment is
within acceptable limits for biodegradation to occur. The field measurements recorded
on September 2, 2009 are summarized in Table 4, which includes the preferred
conditions for natural biodegradation of chlorinated compounds within the groundwater
plume. Conductivity is recorded for quality control and sampling consistency.
Volatile organic compounds were detected at levels above their respective North
Carolina groundwater quality standards established in 15 NCAC, Subchapter 2L (21-
Standards) in each of the twelve monitoring wells sampled. The analytical results are
summarized in Table 5 and a historical summary of groundwater sampling results is
presented in Table 6. Chain -of -custody documents were maintained throughout the
collection and transportation process and are included in Appendix A with the laboratory
report.
Historical total volatile organic compound concentrations and chlorinated volatile
organic compound concentrations for each monitoring well sampled are shown in
individual graphs included in Appendix B. The individual graphs of the total VOC
concentration for each monitoring well indicate MW-7, MW-13, MW-13D, MW-14, and
MW-42 generally have trends of decreasing contaminant levels. The graphs of MW-11
and MW-43D show a decrease when compared to the previous sampling event but
have previously shown increases. The graphs of MW-14D, MW-23D, and MW-24
appear to have decreasing trends; however, the most recent concentrations showed an
977461 GS009R167 Page 4 of 5 September 30, 2009
Copyright 2009 Kleinfelder
increase. The graph of contaminant concentrations in MW-25 and MW-45 indicates the
total VOCs level to be increasing. The increase in contaminant levels in monitoring
wells MW-23D, MW-24, and MW-25 is impacted by increases in cis-1,2-dichloroethene
and vinyl chloride which are degradation components of tetrachloroethene. Monitoring
well MW-24 also showed a rebound in the tetrachloroethene concentration. Total
VOCs concentrations detected during the September 2009 sampling event are shown
on Figure 4.
The current hydrogen injection phase of the corrective action plan targets the reduction
of chlorinated hydrocarbon contaminant levels in the groundwater. The oxygen
injection phase will target the reduction of petroleum hydrocarbons. The volatile
organic compounds targeted during the hydrogen and oxygen injection phases of the
corrective action plan are separated in Table 6 by a double line. Total chlorinated
hydrocarbons concentrations detected during the September 2009 sampling event are
shown on Figure 5. Historical chlorinated hydrocarbon contaminant levels generally
follow the trends of total VOCs in the wells that are sampled during this hydrogen
phase. The trend of rising tetrachloroethene contaminant concentrations has been of
concern in monitoring well MW-25. However, during this sampling event, the
tetrachloroethene concentration decreased in comparison to the previous sampling
event.
5.0 CONCLUSIONS AND RECOMMENDATIONS
The groundwater potentiometric map indicates that the groundwater flow direction at
the site is from the southeast to the northwest under a gradient of 0.04 feet per foot as
measured between MW-32 and MW-45, Groundwater aquifer characteristics
monitored during the sampling event indicate suitable conditions for biodegradation of
chlorinated hydrocarbons generally exist at the site. Both the total chlorinated
hydrocarbons and total petroleum hydrocarbons contaminant levels in monitoring wells
MW-7, MW-11, MW-13, MW-14, and MW-42 have decreased when compared to the
groundwater contamination levels during the baseline sampling event in June 2008.
Monitoring wells MW-14D and MW-43D were not sampled during the June baseline
sampling event; however, contaminant levels in both wells have decreased since their
most recent sampling in 2006. Groundwater contaminant levels in monitoring wells
MW-13D, MW-23D, MW-24, MW-25, and MW-45 showed an increase. Of these wells,
97746 l GS009R167 Page 5 of 6 September 30, 2009
Copyright 2009 Kleinfelder
only MW-25 and MW-45 show an increase in tetra chloroethene since the baseline
sampling event.
A comparison of total chlorinated hydrocarbons in the ten monitoring wells sampled
since the baseline sampling event in June 2008 and the ,June 2009 event indicated a
reduction by 52 percent. With the rebound of the tetrachloroethene concentration in
MW-24 and the degradation components in MW-23D, MW-24, and MW-25, the
September 2009 reduction in total chlorinated hydrocarbons is 35 percent.
Corrective action monitoring will be conducted on a quarterly schedule and the next
event should be scheduled in December 2009. During the next sampling event, we
recommend the following wells are sampled: MW-7, MW-13, MW-13D, MW-14,
MW-14D, MW-15, MW-23D, MW-24, MW-25, MW-42, MW-43D, and MW-45. Monthly
system checks should also be conducted during the next quarter to monitor the rate of
hydrogen consumption of the HiSOC delivery system.
Copies of this report have been mailed to the Guilford County Department of
Environmental Health in Greensboro, North Carolina and the UIC Program in Raleigh,
North Carolina.
977461 G5009R167 Page 6 of 6 September 30, 2009
Copydght 2009 Kleinfelder
TABLES
TABLE 1: GROUNDWATER ELEVATION DATA
Well ID
Total Depth
(feet TOC)
TOC Elevation
(feet)
Date Water
Level
Measured
Static Water
Level
feet TOC
Groundwater
Elevation
feet
MW-7
29.9
861,19
09/02/09
6.21
854.98
MW-10
33.6
857,68
09/02/09
8.71
848,97
MW-11
25.1
859.26
09/02/09
14.99
844.27
MW-12
16.8
851.50
09/02/09
11.37
840.13
MW-12D
27.0
851.06
09/02/09
11.26
839.80
MW-13
24.2
861.29
09/02/09
16.05
845.24
MW-13D
39.4
860.40
09/02/09
15.49
844.91
MW-14
24.8
859.32
09/02/09
22.31
837.01
MW-14D
41.0
859.26
09/02109
22.51
836.75
MW-15
25.2
857.71
09/02/09
15.65
842.06
MW-16
35.2
863.60
09/02/09
30.26
833.34
MW-23D
57.1
860.90
09/02/09
17.45
843.45
MW-24
58.8
858,81
09/02/09
23.25
835.56
MW-25
168.9
861 A7
09/02/09
25,71
835,76
MW-27
44.0
862.74
09/02/09
12.76
849,98
MW-28
23.8
861.54
09/02/09
7.35
854.19
MW-29
18.8
861.13
09102M9
4.45
856.68
MW-30
73A
862.28
09/02/09
21,58
840.70
MW-31
19.0
861.73
09/02/09
9.91
851.82
MW-32
19.6
861.76
09/02/09
8.86
852.90
MW-33
21.0
861.77
09/02/09
14.28
847.49
MW-34
21.0
860.45
09/02/09
flooded
---
MW-40
29.7
860.62
09/02/09
11.11
849.51
MW-41
20.3
860.52
09/02/09
8.83
851.69
MW-42
35.0
865.32
09/02/09
31.25
834.07
MW-43D
53.0
865.47
09/02/09
32.31
833.16
MW-44
28.5
NM
---
---
---
MW-45
36.2
861.79
09/02/09
29.33
832.46
Notes:
feet TOC = feet below top of well casing
NM = Not measured
977461 GS009R167 Page 1 ❑f 1 September 30, 2009
Copyright 2009 Kleinfelder
TABLE 2: ESTIMATED DISSOLVED HYDROGEN CONCENTRATIONS AT INJECTION WELLS
Well ip
Total Depth
(feet TOC)
TOC Elevation
ftet)
Bottom
Elevation (feet)
pate Water
Level Checked
Level Static Water
Le
(feet vel
Groundwater
Elevation (feet)
Depth of Water
(feet)
Estimated
Dissolved
Hydrogen
Concentration
(ppm)
MW-7
29.9
861.19
831.29
09/02/09
6.21
854.98
23.69
2.7
MW-10
33.6
860.36
826.76
09/02/09
8.71
851.65
24.89
2.8
MW-14D
41.0
859.26
818.26
09/02/09
22.51
836.75
18.49
2.5
MW-15
25.2
857.71
832.51
09102/09
15.65
842.06
9.55
2.1
MW-16
35.2
863.60
828.40
09/02/09
30.26
833.34
4.94
1.8
MW-23D
57.1
860.90
803.80
09/02/09
17.45
843.45
39.65
3.5
MW-24
58.8
858.81
800.01
09/02/09
23.25
835.56
35.55
3.3
MW-29
18.8
861.13
842.33
09/02/09
4.45
856.68
14.35
2.3
MW-34
21.0
860.45
839.45
09/02/09
0.50
859.95
20.50
2.6
MW-43D
53.0
865.47
812.47
09/02/09
32.31
833.16
20.69
2.6
Notes:
feet TOC = feet below top of well casing
ppm = parts per million
Hydrogen concentrations are estimated based on a saturated hydrogen content of 1.6 ppm per atmosphere.
97746 1 GS009R167 Page 1 of 1 September 30, 2009
Copyright 2009 Kleinfelder
TABLE 3: ESTIMATED HYDROGEN CONSUMPTION
Date Water
Original
Cylinder
Estimated Volume
Estimated Date
Injection
Date Hydrogen
Cylinder
Level and
Pressure on
of Hydrogen
Days Elapsed
Average Hydrogen
Cylinder Must be
Cylinder
Cylinder
Since Cylinder
Use per bay
Well I❑
Pressure
9121Q9
Remaining {cubic
Changed Based on
Installed
Pressure
Installation
(psilday)
(psi)
(psi)
feet)
Pressure
Recorded
MW-7
07/28/09
2,000
09/02/09
1,000
96
36
27.8
10/04109
MW-14D
07/28/09
1,900
09/02/09
1.100
111
36
22.2
10/17/09
MW-15
07/28/09
2,000
09/02/09
1,350
129
36
18.1
11/10/09
MW-16
07/28/09
1,900
09/02/09
900
90
36
27.8
09l30109
MW-23D
03/27/09
1,900
09l02109
1.200
121
159
4.4
05/09/10
MW-24
07/28/09
2,000
09/02/09
1,450
138
36
15.3
11/29/09
MW-25
07/28/09
2,100
09/02/09
1,150
105
36
26.4
10/11/09
MW-29
07/28/09
2,200
09/02/09
1,700
148
36
13.9
12/26/09
MW-34
05/13/09
2,000
09/02/09
700
67
112
11.6
10/23/09
MW-43D
05/13/09
1,900
09/02/09
0
0
112
17.0
08/27/09
Notes:
psi = pounds per square inch
All hydrogen cylinders must be replaced prior to the cylinder pressure falling below 50 psi.
97746 1 GS009R167 Page 1 of 1 September 30, 2009
Copyright 2009 Kleinfelder
TABLE 4: AQUIFER CHARACTERISTICS FIELD ANALYSIS SUMMARY
Monitoring Well
Sample
p
Date
Temperature
°
[ C }
pH
Conductivity
{rnSlcm}
Dissolved
Oxygen
m jL
Redox
(mV)
Preferred
Conditions
a 200C
5<pH<9
---
<0.5 mg1L
<50 mV
MW-7
09/02/09
18.50
8.22
0.237
2.03
54.1
MW-11
09/02/09
18.08
6.24
0.232
0.89
164.9
MW-13
09/02/09
19.81
6.19
0.420
3.65
139.5
MW-13❑
09/02/09
18.15
6.25
0.440
1.09
83.0
MW-14
09/02/09
15.88
7.06
0.167
6.77
76.2
MW-14D
09/02/09
16.29
6.71
0.265
1.49
-20.2
MW-23D
09/02/09
18.34
7.15
0.909
0.44
-163.3
MW-24
09/02/09
15.83
6.80
0.538
1.00
-86.6
MW-25
09/02/09
15.91
8.08
0.244
0.92
-100.8
MW-42
09/02/09
14.96
7.27
1.125
7.43
68.6
MW-43❑
09/02/09
15.45
6.99
0.298
0.66
-13.1
MW-45
09/02/09
14.47
7.33
0.467
3.74
22.4
Notes:
Redox = oxidation-reduction potential
°C = degrees Celsius
mSlcm = millisiemens per centimeter
mg/L = milligrams per liter, analogous to parts per million
mV = millivolts
Conductivity is measured for consistency in groundwater sample collection.
97746 1 GS009R167 Page 1 of 1 September 30, 2009
Copyright 2009 Kleinfelder
TABLE 5: SUMMARY OF GROUNDWATER SAMPLE RESULTS
Parameter
NCGS 2L
Standard
Anaiytical Results
Sample ID
MW-7
MW-11
MW-13
MW-13D
MW-14
MW-14D
MW-23D
MW-24
MW-25
MW-42
MW-43D MW-45
Collection Date
09/02/09
09J02/09
09/02109
09/02/09
09/02/09
09/02/09
09/02/09
09/02/09
09/02/09
09M2109
09/02/09 09/02/09
Volatile Organic Compounds by EPA Method 6011602
IL
Tetrachloroothene
0.7
BDL
4.4
BDL
BDL
23.8
27.1
BDL
946
24.8
3.4
337
2.4
Trichloroethene
2.8
BDL
2.3
BDL
BDL
BDL
1.4
BDL
127
7.9
BDL
11.4
1.1
cis- 1,2-Dichlaroethene
70
556
BDL
47.6
16.7
BDL
8.8
140
760
60.1
BDL
99.4
BDL
11-Dichloroethene
7
6.3
BDL
BDL
BDL
BDL
BDL
BDL
9.7
1.6
BDL
119
BDL
Vinyl Chloride
1 0.015
1 27.3
BDL
BDL
5.3
BDL
BDL
23.5
121
BDL
BDL
BDL
BDL
1,1-Dichloroethane
1 70
7.8
BDL _
BDL
BDL
SDL
6DL
BDL
6-2
1.1
BDL
It7t
BDL
Total Chlorinated Hydrocarbons
597
7
48
22
24
37
164
1,970
96
3
466
4
Benzene
1
BDL
BDL
1.2
BDL
BDL
1.8
2.7
537
BDL
BDL
3
BDL
Toluene
1,000
6.1
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Eth ibenzene
550
519
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Total X lenes
530
468
BDL
BDL
BDL
BDL
BDL
BDL
13.7
BDL
BDL
BDL
BDL
MTBE
200
BDL
BDL
3.6
23.1
BDL
1.3
317
77.5
8.9
BDL
16.7
SQL
Diisopropyl ether
70
BDL
BDL
BDL
BDL
BDL
2.9
6.4
165
9.1
BDL
29.9
BDL
Naphthalene
21
288
BDL
BDL
BDL
BDL
BDL
BDL
15.5
BDL
BDL
BDL
BDL
Chloromethane
2.6
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
3.8
BDL
Dichloroditluoromethane
1,400
8.7
BDL
BDL
BDL
BDL
BDL
8DL
BDL
BDL
BDL
BDL
8DL
Trichlorotluoromethane
2,100
8DL
BDL
BDL
BDL
BDL
BDL
BDL
32
BDL
BDL
3.7
BDL
Total Petroleum Hydrocarbons
1,290
0
5
1 23
0
6
325
841
18
0
57
0
Total VOCs
1,887
7
52
1 45
24
43
490
2,811
114
3
523
4
Notes:
NCGS 2L Standard = North Carolina Groundwater Standard
BDL = Below Detection Limits
pg1L = Micrograms per liter, analogous to parts per billion
BOLD = Concentration exceeds the NCGS 2L Standard
MTBE = Methyl -tent -butyl ether
97746 j GS009R167 Page 1 of 1 September 30. 2009
Copyright 2009 Hleinielder
TABLE 6: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated H drocarbana
Total
Chlorinated
Hydrocarbons
Petroleum hydrocarbons
Total
Petroleum
Hydrocarbons
Total VOCs
Cailectlan pate
Tetra chloroethene
Trichloroelhene
cis 12
Oichloroethene
1,1
Dichloraethene
Vinyl Chloride
1,1-
Dkhloroethane
1,2
Dichloroelhane
trans-1,2
pichloroethane
1,1,1-
Trichioroethane
Benzene
Toluene
Ethylhenzene
TotalXylenes MTBE
Diisopropylether
�2�;nj
NCGS 2L Std.
0.7
2.8
70
7
0.015
70
0.38
100
200
i
1,ODD
550
530 200
70
MW-7
09/27/90
790
190
SOL
BDL
SOL
SDL
SDL
BDL
59
1,039
650
5,30D
1,500
5,700
SOL
SDL
BDL
13.150
14,199
01/14/92
SOL
360
SDL
SDL
SOL
8131-
BDL
BDL
BDL
360
480
3,900
2100
7,100
SDL
BDL
SDL
13.580
13.940
owl1198
SOL
SDL
SOL
354
SDL
BDL
BDL
BDL
238
592
468
8.920
21200
8.990
SDL
BDL
SOL
20,578
21.17D
05/25/99
BDL
6DL
SOL
723
SDL
BDL
SOL
SDL
347
1.070
253
2,280
2,290
10.800
BDL
BDL
BDL
15,623
16.693
D412n3
BDL
SAL
BDL
BDL
BDL
SOL
SQL
SOL
86
88
SOL
220
2,400
5,700
SOL
60
BDL
8,380
8.468
M30104
SOL
BDL
2,3D0
BDL
BDL
SOL
SDL
BDL
BDL
2,300
SDL
110
1,800
3,800
BDL
BDL
520
6,230
8,530
08/16/05
BDL
BDL
2,1D0
BDL
BDL
SDL
8DL
BDL
BDL
2.100
SDL
SQL
1,600
3,020
SDL
SDL
1 520
5.140
7,240
D8125106
SDL
BDL
2,000
14
SDL
BDL
SOL
1.5
14
2,030
1.7
23
370
380
11
3.3
82
871
2,901
12114l06
3.6
4
2.100
670
BDL
15
BDL
5.1
13
2,711
4.1
39
1,300
1,660
SOL
SDL
440
3.443
6.154
06/05/08
SDL
SOL
1,750
SDL
BDL
SQL
SDL
SDL
SDL
1.750
SAL
SDL
1,040
1.200
SQL
BDL
401
2,721
4,471
09/04/08
BDL
SDL
1,190
SDL
BDL
BDL
SDL
BDL
BDL
i,190
BDL
SOL
788
en
BDL
BDL
301
1.952
3.152
01105/09
BDL
SDL
798
BDL
BDL
BDL
SDL
BDL
$DL
798
SOL
BDL
643
598
SDL
SDL
30B
1.549
2,347
03/05/09
BQL
SAL
935
BDL
BDL
SDL
SAL
SOL
BDL
935
SDL
SQL
749
723
BDL
SOL
384
1,B55
2.791
OW24109
BDL
BDL
634
BDL
BDL
BDL
BDL
SDL
SDL
631
SDL
SDL
589
526
SOL
SDL
210
1,325
1.956
09102/09
SQL
BDL
556
6-3
27.3
7.0
SAL
BDL
8DL
597
BDL
6-1
519
468
SOL
SOL
1 288
1.290
1.8871
MW-8 (abandoned)
09/27190
SDL
BDL
BDL
SOL
SDL
BDL
SAL
SOL
BDL 0
SOL
SDL
BQL
1
SDL
BOL
BDL
1 1
01/14/92
BDL
BDL
BDL
SOL
BDL
BDL
BDL
SDL
SDL 0
SOL
SDL
SDL
BDL
SOL
BDL
BDL
0 ❑
05/15/42
SOL
BDL
BDL
BDL
SDL
BDL
SOL
SDL
BDL 0
BOL
SOL
BDL
SOL
SDL
SOL
BDL
0 0
MW-9 (abandoned)
09/27/90
10
2
SOL
SOL
BDL
BDL
BDL
SOL
BDL
12 2
SOL
BDL
BDL
BDL
BDL
BDL
2
14
011141W
BDL
BDL
SDL
SOL
SDL
BDL
BDL
SDL
BDL
0 BOL
BDL
BDL
SDL
SDL
BDL
BDL
0
0
0"5/92
SOL
SDL
SDL
SOL
SOL
SDL
SOL
BDL
SDL
❑ SDL
BDL
SDL
BDL
BDL
SOL
BDL
0
0
MW-10
09/27/90
76
140
SOLMSDL
SDL
BDL
SDL
BDL
140
356
2,900
fib
BDL
670
SDL
SOL
BDL
3.636
3,992
01/14/92
BDL
78
SOLSDL
BDL
BDL
BDL
BDL
198
2,900
SOL
SOL
120
SDL
SDL
BDL
3.020
3.218
03J71/98
SDL
SDL
BDLSOL
SOL
SDL
SOL
BDL
14
234
SOL
BDL
BDL
BDL
BDL
SDL
234
248
05126M
BDL
SOL
BDLSDL
BDL
BOL
SDL
BDL
0
36
BQL
SDL
BDL
SOL
BDL
BDL
36
36
SD/10102
5.9
2.3
BDLSDL
SDL
BDL
BDL
7.3
20
220
9.5
16
71
2,200
16
BDL
2,532
2.551
04/22/03
3.2
1.3
BDLBDL
SOL
$DL
SDL
2.6
7
47
SOL
BDL
BDL
1,1Do
2.9
SDL
1.150
1,157
06130/04
BDL
BDL
8.1BDL
BDL
BDL
BDL
BQL
8
22
BDL
2.8
5.8
770
2.8
BQL
803
812
081161❑5
BQL
SDL
SDLBDL
BDL
BDL
BDL
SOL
0
43
BDL
SAL
BDL
680
SDL
BDL
723
723
OEV24106
BDL
BDL
3
BDL
SDL
BDL
BDL
BDL
SAL
3
8A
SDL
SOL
SDL
360
4.3
SOL
372
375
MW-11
06WI04
2.1
3
1.4
SDL
BDL
SOL
SOL
BDL
SOL
7
SOL
SOL
SDL
BDL
4.1
SOL
BDL
4
11
08115.105
5
3.6
9.7
SDL
BDL
SDL
SDL
SDL
BDL
18
SOL
SDL
SDL
BDL
2.2
SOL
SOL
2
21
08/24/06
4.9
2.5
5.2
SOL
BDL
BDL
BDL
SDL
SDL
13
SOL
BDL
SDL
BDL
4.4
BDL
BDL
4
17
W05108
6.8
1.5
5.0
SDL
BDL
BDL
BDL
BDL
SOL
13
SDL
SOL
SOL
BDL
BDL
BDL
BDL
0
13
091D4108
BDL
SDL
SDL
SDL
BDL
BDL
SDL
BDL
SDL
0
BDL
BDL
BDL
BDL
SDL
SOL
SOL
0
0
01/05/09
2.7
1.6
2.6
SpL
SDL
SDL
SDL
BDL
BDL
BDL
BDL
SDL
BDL
1.1
SOL
SDL
1
8
03/MO9
1.3
BDL
1.5
SDL
BDL
BDL
BDL
BDL
BDL
3
SDL
SQL
SOL
BDL
SDL
SDL
BDL
❑
3
06/24/09 1
6.6
1.6
4.7 1
BDL
SOL
BDL
SOL
BDL
SOL
13
BDL
BDL
SDL
SDL
BDL
SAL
SOL
1
14
❑9102109
4.4
2.3
BDL
BDL
BDL
BDL
BDL
BDL
BDL
7
SDL
SDL
SOL
SDL
SDL
SOL
BDL
I 0
7
MW-12
09/27/90
SOL
SOL
BDL
SOL
BDL
BDL
BDL
BDL
BDL
0
BDL
BDL
BDL
BDL
SOL
BDL
BDL
0
0
01/14/92
SDL
BDL
BDL
SOL
BDL
BDL
SAL
SOL
BDL
❑
BDL
SDL
SOL
BDL
SDL
BDL
SOL
0
❑
03/11.'98
SOL
BDL
BDL
SDL
SOL
BDL
SOL
BDL
BDL
0
SOL
BDL
BDL
BDL
BDL
SOL
BDL
0
0
05/26/99
SDL
BDL
BDL
BDL
BDL
SDL
SOL
SDL
BOL
0
SOL
BDL
SDL
SDL
BDL
SOL
SOL
0
❑
DBW04
BDL
BDL
BDL
SOL
BDL
BDL
BDL
SDL
BDL
❑
SDL
BDL
SOL
SDL
SOL
SDL
BDL
0
❑
OB115/05
BDL
BDL
BDL
SOL
SDL
BDL
SOL
SAL
SDL
❑
SDL
SDL
SDL
BDL
SDL
SOL
SDL
❑
0
08/24/06
BDL
SOL
$OL
BDL
SDL
BDL
SOL
BDL
SDL
0
SDL
BDL
BDL
SDL
SOL
BDL
SDL
0
0
Notes:
All units measured In micrograms per liter, pglL
' Total Petroleum Hydrocarbons and Total VOCs include chloromethane, dichlorodMuoromethene, and Vic hloronuoromelhane values (see Table 5).
BDL - Below Detection Limits
NCGS 21- St& - North Carolina Groundwater Standard
BOLD - Concentration exceeds the 21 Groundwater quality Standard
MTBE - Methyl -tart butyl ether
97746 J GS009R167
Copyright 2009 Klein}elder
Page 1 of 5
September 30, 2009
TABLE 6: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated H drocarhons
Total
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petroleum
Hydrocarbons
Total VOCs
Collection Date
Tetrachloroethene
Tnchloreethene
cis 1,2
Dfchloroethene
1,1 Vinyl Chloride
Dichloroethene
Dichichloroethane
=m0larle
1.2-
trans 1,2
Dichloroethane
1,1.1-
Trichloroelthane
Benzene
Toluene
Ethylbenzene
TotalXylene8
MTBE
Diisopropylether
Naphthalene
NCG52LSid,
0.7
2.8
70
7 0.015
70
0,38
100
200
1
1,000
550
530
200
70
21
MW-12D
09/27/90
BDL
SOL
SOL
BDL
SOL
SOL
BDL
BDL
BDL
0
BDL
SOL
SOL
SDL
BDL
BDL
SOL
0
0
01/14/92
BDL
BDL
SOL
BOL
BDL
BDL
SOL
SOL
SOL
0
BDL
SOL
BDL
SOL
BDL
SOL
SOL
0
0
03/11/98
BDL
SOL
BDL
SOL
BDL
SOL
SOL
SOL
BDL
0
BOL
SOL
SOL
SOL
BDL
SOL
SOL
0
0
0512669
BDL
BDL
BDL
SOL
BDL
SOL
SOL
SDL
BDL
0
BDL
SOL
BDL
SDL
BDL
SOL
BDL
0
❑
06/30/04
SOL
BDL
BDL
SOL
SDL
BDL
SOL
SOL
SOL
0
BDL
SOL
SOL
8DL
BDL
BDL
SOL
0
0
08/15105
BDL
BDL
SOL
SOL
BDL
SOL
BE
SOL
SOL
0
8DL
SOL
SOL
8DL
BDL
SOL
SOL
0
0
08/24/06
SOL
BDL
SOL
SOL
BDL
BDL
SOL
BDL
SOL
0
BDL
SOL
BDL
I SOL
BDL
t SOL
I SOL
H 0
H 0
MW-13
09/26/90
2
BDL
BDL
BDL
BDL
SDL
BDL
SOL
SOL
2
SOL
SOL
SOL
BDL
BDL
SOL
SOL
0
2
01I14192
130
36
SOL
BDL
BDL
SOL
BOL
BDL
SOL
166
BDL
SOL
SOL
BDL
BDL
BDL
BDL
0
166
05/15M
130
20
BDL
BDL
BDL
SOL
BOL
BDL
BDL
150
SOL
SOL
SOL
SDL
8DL
BDL
SOL
0
150
03l1148-
2.5
4.7
SDL
BDL
SOL
SOL
BDL
BDL
SOL
7
BDL
SOL
BDL
SDL
BDL
SOL
SOL
0
7
05/26PA
4.2
15
SOL
BDL
SOL
SOL
BDL
BDL
SOL
19
BDL
SOL
BDL
BDL
BDL
SOL
BDL
0
19
06/30/04
BDL
6.5
140
BDL
SOL
SOL
SOL
BOL
BDL
147
SDL
SOL
BDL
SOL
13
BDL
BDL
13
160
08/16/05
BDL
BDL
110
BDL
BDL
SOL
SOL
SDL
BDL
110
SOL
SOL
BDL
SDL
BDL
SDL
SOL
0
110
08/24/06
BDL
2.9
110
SOL
BDL
SOL
SAL
1.1
BDL
114
SDL
BDL
BDL
BDL
5.4
SOL
BDL
5
119
M05/08
BDL
SOL
94.7
SOL
BOL
SOL
SOL
SOL
BDL
95
6.4
SOL
SDL
SOL
SOL
BOL
BDL
6
101
09/04/08
SOL
SOL
67.9
SOL
BOIL
BDL
SOL
SOL
SOL
68
BDL
BDL
BOL
SAL
SOL
BDL
BDL
0
68
01/05/09
SOL
BDL
66.7
SOL
SOL
SOL
SOL
SDL
BDL
69
3.2
SOL
SDL
SOL
52
BDL
BDL
B
77
03105M
BDL
BDL
119
SOL
SDL
BDL
BOL
BDL
SOL
119
SOL
SOL
BDL
SOL
It
SOL
BDL
3
12-2
06/24/69
SDL
BDL
812
SOL
SOL
8DL
BDL
BDL
BDL
69
BDL
BDL
BDL
SOL
SOL
SOL
SOL
0
69
09/02/09
SAL
BOL
47.6
BDL
SOL
BAL
SOL
SOL
BDL
48
1.2
BDL
SDL
BOL
3.6
BDL
BDL
5
52
MW-13D
06/30/04
SAL
BDL
18
SOL
1.5
SDL
SDL
60L
SDL 20
1.1
BDL
BDL
SOL
26
1.1
BDL
28
48
OW15105
SOL
BDL
37
SOL
1.4
BDL
BDL
BDL
SOL 38
SOL
BDL
SDL
SOL
20
1.3
SDL
21
60
08l24106
SOL
BDL
30
SOL
1.3
SOL
BDL
BOL
SOL 31
SAL
BOL
BDL
SOL
19
SOL
BDL
19
50
06I05108
BOL
BDL
21.6
BDL
3.2
SOL
BDL
DDL
SOL 25
SDL
BDL
3.0
3.6
12.5
1.7
SOL
21
46
0910410B
SOL
BDL
15.2
BDL
3.1
BDL
BDL
BDL
BDL 1B
SOL
BDL
BDL
BDL
17.6
BDL
B0L
18
36
01/05/09
BDL
BDL
17.4
BOL
4.2
BDL
SDL
BDL
SOL 22
SOL
BDL
BDL
SOL
16.3
1 A
BDL
17
39
03/05/09
BDL
BDL
14.6
SOL
3.4
SOL
SDL
BDL
SOL 1B
SOL
BDL
SOL
SOL
13.4
BDL
SOL
13
31
❑6124109
BDL
SOL
19.2
9.4
4.1
SOL
SOL
BDL
SOL 33
SOL
BOL
SOL
BDL
20.2
BDL
8DL
20
53
09/02/09
BDL
SOL
16.7
SDL
5.3
SDL
SOL
BDL
BDL 22
SOL
BDL
SOL
SOL
23.1
BDL
BDL
23
45
MW-14
09/26/90
1,300
SOL
BDL
SOL
SDL
BDL
SOL
SOL
BDL
1,300
BDL
SOL
SOL
SOL
BDL
BOL
SOL
0
1,300
01/14/92
1,400
BDL
BDL
SDL
SOL
SOL
18O
SDL
100
1.680
BDL
60
SOL
100
BDL
BDL
SDL
760
1,1140
03111M
80
BDL
BDL
SOL
BDL
SOL
SOL
SDL
BDL
BO
BDL
SOL
SOL
BOL
BDL
BDL
SDL
❑
80
05/25/99
67
BDL
SOL
BDL
SOL
SOL
BDL
SOL
BDL
67
SDL
BDL
BDL
BDL
BDL
BOL
BDL
0
67
04/22/03
110
DDL
BDL
SOL
SOL
BDL
SOL
SOL
SOL
110
1.1
1.7
BDL
1.9
SDL
BDL
BDL
5
115
06/30/04
BO
BDL
SDL
SOL
SOL
SOL
BDL
SOL
SOL
80
BOL
SOL
BDL
BDL
8DL
SDL
BDL
0
80
08/16/05
58
BDL
BDL
BDL
SOL
BDL
BOL
SOL
SOL
58
SDL
SOL
SOL
SOL
SDL
SOL
BDL
0
58
08/24/06
46
BDL
SDL
SOL
BDL
BDL
BDL
BDL
SOL
46
BDL
SOL
BOL
BOL
BOL
SOL
BOL
0
46
06/05/08
54.0
BDL
SDL
BDL
SOL
SOL
BDL
SOL
SDL
54
BDL
BDL
BDL
BDL
SDL
SDL
SDL
0
54
09/04/08
50.0
BOL
SDL
BDL
SOL
SOL
BDL
SDL
SOL
50
SOL
BDL
SDL
SOL
SDL
SOL
BDL
0
50
01/05/09
29.9
BDL
SOL
BDL
SOL
SOL
BDL
SOL
SOL
30
SOL
BDL
SOL
SDL
BDL
SOL
BDL
0
30
03/05/09
32
SDL
BDL
BOL
SOL
BDL
BDL
SOL
SOL
32
SOL
BDL
BDL
BDL
SDL
BDL
SDL
q
32
0&24/09
31.2
SOL
BDL
SDL
SOL
BDL
BDL
BDL
SOL
31
SOL
BOL
BDL
BDL
SOL
SOL
BDL
❑
31
OW02/09
23.8
BOL
BDL
BDL
BDL
SOL
BDL
BDL
SOL
24
SOL
BOL
SDL
EL
BDL
SOL
SOL
0
24
M W-140
09/27/90
110
3
BDL
58
BDL
5
BDL
SDL
20
196
45
1
SOL
5
SOL
SOL
SOL
51
247
01/14/92
200
SOL
SOL
SDL
SOL
SDL
SOL
BDL
BDL
200
65
3
SOL
SOL
SDL
BOL
SOL
68
268
05/15/92
56
BDL
SOL
2.1
BDL
BDL
SOL
BDL
BDL
58
4.7
SDL
SOL
BDL
SOL
SOL
SOL
5
63
09/09/92
210
BDL
SOL
23
BOL
BDL
SOL
BDL
13
246
220
BDL
SOL
SOL
BDL
SOL
BDL
220
466
Notes:
All units measured in micrograms per liter, ggIL
'Total Petroleum Hydrocarbons and Total VOCs include chlommethane. dchlorodifluoromethane, and trichlorofluaromethane values (see Table 5).
SOL - Below Detection Limits
N C G S 2L Sid. - North Carolina Groundwater Standard
SOLD - Concentration exceeds the 21 Groundwater Quality Standard
MTBE - Methyl -tart butyl ether
97746 J G5009R167 Page 2 of 5 September 30. 2009
Copyright 2009 Kleinfelder
TABLE 6: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated H drocar6ens
Total
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petroleum
Hydrocarbons
Total VOCs
Collection Date
Tetrachloroethene
Trichloroethene
rts-1,2
Dichlaroethene
1.1 Vinyl Chloride
Dichloroethene
1,1-
Dichbroethane
1,2-
Dichloroethane
trans-1.2-
Dichloroethane
1,1,1-
Trichbreethane
Benzene
Toluene
Ethylbenzene
Total Xylenes
MTBE
Diisopropyl ether
Naphthalene
NCGS 2L Std.
0.7
2.8
70
7 0.015
70
0.38
100
200
5
1.000
550
530
200
70
21
MW-140 (Continued)
03/11i98
3S.4
BDL
BDL
10.6
SOL
SOL
SOL
BDL
SDL
46
5.8
BDL
BDL
BDL
BDL
BDL
SOL
6
52
05/25/99
201
SOL
BDL
25
SOL
SOL
SOL
SOL
BDL
226
67
BOL
BDL
BDL
BDL
SOL
BDL
67
293
10/10102
79
2.8
BDL
4
BDL
4.2
BDL
SOL
BDL
90
8.3
SOL
SDL
SOL
11
29
SDL
48
138
04/22/03
40
BDL
BDL
1.2
SOL
SOL
SOL
BDL
BOL
41
BDL
SOL
SOL
BDL
SOL
1.8
SOL
2
43
06/30/04
29
BDL
3.0
3.5
SOL
2.2
SOL
BDL
BDL
35
BDL
BDL
SDL
SOL
3.3
BDL
SOL
3
38
08/16/05
55
1.8
15
3.3
SOL
SOL
SOL
BDL
BDL
75
5.4
SOL
SOL
BDL
3.2
7.3
SOL
15
91
08/24/06
47
2
17
1.4
SOL
BDL
BDL
SOL
BDL
67
12
SOL
SOL
SOL
2.4
6.4
BDL
10
78
031271D9
10.6
SOL
1.0
BDL
BDL
BDL
SOL
BDL
BDL
12
BDL
SOL
SOL
BDL
SOL
SOL
SOL
0
12
06/24109
11.7
SDL
BDL
130L
SOL
SOL
SQL
BDL
SOL
12
SOL
SOL
BDL
SOL
SOL
BDL
SOL
0
12
09/02/09
27.1
1.4
8.8
SOL
BDL
SOL
SOL
SOL
BDL
37
1.8
SOL
BDL
BDL
1.3
2.9
BQL
6
43
MW-15
09/27/90
BDL
SOL
SDL
SOL
BDL
SOL
SQL
BDL
BDL
0
SOL
SOL
BDL
SOL
BDL
BDL
SQL
0
0
01/14/92
BDL
BDL
SOL
SOL
SOL
BDL
BDL
SOL
SOL
0
SOL
SOL
SOL
BDL
SOL
BDL
BDL
0
0
03/11/98
SOL
SDL
SDL
SOL
BDL
BDL
BDL
BDL
BDL
0
BDL
SOL
SOL
SOL
SOL
SOL
BDL
0
0
05125/99
4.9
3
SDL
SOL
SOL
BDL
BDL
SDL
BDL
8
BOL
SOL
SOL
SOL
SOL
BDL
SQL
❑
8
10/10/02
13
7.8
SDL
SOL
BOL
1.4
SOL
BDL
BDL
22
BDL
SOL
BDL
SOL
29
SOL
SOL
29
51
04/22/03
11
5
SOL
SOL
SOL
1.4
BDL
BDL
BDL
17
BDL
SOL
BDL
BDL
17
SOL
BDL
17
34
06/30/04
7.5
3.9
Bfi
BDL
SDL
SDL
SOL
BDL
BOL
97
BDL
SDL
BOL
BOL
18
60L
BDL
18
115
06/16/05
6.B
2.3
d7
SOL
SOL
SDL
BDL
SOL
BDL
56
BpL
SOL
BDL
SOL
15
SDL
BDL
15
71
O8/24106
5.5
5
48
BDL
SOL
SOL
SDL
BDL
SOL
59
BDL
SOL
SOL
SOL
a
BDL
SOL
8
U 67
MW-16
09/26/90
BDL
BDL
SOL
BDL
BDL
SOL
BDL
BDL
SOL
0
BDL
SOL
SOL
SOL
SOL
BDL
SDL
0
0
01/14/92
SOL
BDL
SOL
BDL
SOL
SDL
BDL
BDL
BDL
0
SOL
SOL
SOL
SOL
BDL
BDL
SOL
❑
0
03/11/98
1.9
BDL
BDL
BDL
SOL
BDL
SOL
BDL
BDL
2
SOL
SOL
BDL
SOL
SOL
SDL
BDL
❑
2
06/02199
2.4
BDL
SOL
BDL
SDL
SOL
BDL
BDL
SOL
2
SOL
SOL
SOL
SOL
SOL
BDL
SOL
0
2
10/10/02
22
3.8
SQL
1.8
SOL
SDL
SOL
SDL
SOL
26
SDL
SOL
SOL
SDL
SOL
SDL
SDL
0
28
D4/22/03
46
8.6
SOL
3.6
SOL
SOL
SOL
BDL
BDL
58
BDL
SOL
SOL
BDL
SOL
13DL
BDL
❑
58
06/30/04
31
7.fi
24
2.7
SOL
7
SOL
BDL
BDL
66
BDL
BDL
BDL
BOL
SOL
BDL
BDL
❑
66
D8116/05
30
4A
BDL
1.8
BDL
SOL
SDL
SOL
SOL
36
SOL
SOL
SOL
SOL
BDL
17
BDL
17
53
OB125/06
36
7.4
31
2.9
SDL
SDL
BDL
SOL
SDL
77
SOL
SOL
SOL
SOL
BDL
SOL
BOL
0
77
MW-17 (abandoned 01/03106)
OW26190
i
SOL
BDL
BDL
SOL
SOL
SOL
SOL
BDL
1
BDL
SOL
SOL
SOL
SOL
SOL
BDL
0 1
01114/92
SQL
3
SOL
BOL
SOL
SOL
SOL
SOL
SOL
3
BDL
SOL
BDL
SOL
SOL
8DL
BDL
0 3
03/11/98
BDL
BDL
BDL
SDL
BDL
SOL
BDL
BDL
BDL
0
BDL
BDL
SOL
SOL
BDL
SOL
BDL
0 0
❑8102199
SOL
BDL
SOL
SDL
BDL
SOL
SDL
SDL
SOL
❑
BDL
BOL
SOL
SOL
SOL
BDL
SOL
0 0
06130/04
SOL
BDL
BDL
SOL
SOL
SOL
BDL
BDL
SOL
0
BDL
SOL
SOL
SOL
17
SDL
SOL
17 17
MW-23D
09127/90
SOL
2
BDL
SOL
BDL
5
5
SOL
SOL
12
1
SOL
SOL
SOL
SOL
BDL
SOL
1
13
01/14/92
BDL
BDL
BDL
BDL
BDL
BDL
BDL
SDL
BDL
0
BDL
BDL
SOL
BDL
SOL
BDL
BDL
0
0
05/15/92
BDL
2.2
BDL
SOL
SOL
5.3
SOL
SOL
SOL
8
45
BDL
SOL
SOL
BDL
BDL
BDL
45
53
09/09/92
1.9
6.3
BOL
5.4
BOL
6.5
2
SOL
SOL
22
6.3
SOL
BOL
SOL
BDL
SOL
BDL
6
29
03/11/98
2.5
2.5
BDL
1.4
BDL
2.9
SOL
SOL
4
13
7.1
3.7
SOL
SOL
BDL
SOL
BDL
11
24
05/26/99
SOL
4.1
BDL
2.4
BDL
5.7
216
BDL
SOL
15
3.1
SOL
BDL
SOL
SDL
BDL
BDL
3
18
06/301D4
BDL
BDL
20O
SOL
BOL
BDL
SOL
SOL
SOL
20❑
SOL
SOL
BDL
SOL
500
12
SOL
512
712
08/15/05
SQL
BDL
280
SOL
BOL
SOL
SOL
SOL
SDL
280
BDL
BDL
SDL
BDL
31D
BDL
BDL
310
590
OB124106
BDL
1.1
340
SOL
1.9
BDL
BDL
SOL
SDL
343
1.0
SOL
SOL
BDL
310
9.1
BDL
321
66.4
06/05*8
SOL
SOL
166
BDL
SDL
SOL
BDL
SOL
SOL
166
SOL
BDL
20.2
23.6
208
SOL
BDL
252
418
09/04108
BDL
SOL
5.3
BDL
SDL
BDL
SOL
SOL
SOL
5
BDL
BDL
BDL
SOL
19.3
BDL
BDL
19
25
Notes:
All units measured in micrograms per liter, NgIL
' Total Petroleum Hydrocarbons and Total VOCs include chimomethane, dichloroddluorc metha ne, and trichlorolluoromelhane values (See Table 6).
BDL - Below Detection Limits
N C G S 2L Std. - North Carolina Groundwater Standard
BOLD - Concentration exceeds the 2L Groundwater Quality Standard
MTBE - Methyl-tert butyl ether
977461 GS009R1 B7 Page 3 of 5 September 30, 2009
Copyright 2009 Kleinlelder
TABLE 6: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated N drocerbons
Total
Chlorinated
Hydrocarbons
Petroleum Hydrocarbons
Total
Petroleum
hydrocarbons
Total VOCs
Collection Date
Tetrachloroethene
Trichloroethene cis-1,2
Dichloroethene
1.1-
Dichloroethene
vinylCh"e
1,1
Dichloroethane
1,2
Dichloroethane
trans-1,2•
Dichloroethane
1,1,1-
Tdchloroethane
Benzene
Toluene
Ethylbenzene
Total Xylenes
MTBE
Diisopropylether
N;phalene
NCGS 2L Std.
0.7
2,8 70
7
0.015
70
0.38
100
200
1
1,000
550
530
200
70
1
MW-23D (Continued)
01/05/09
BDL
SDL
15.3
BDL
BOL
BDL
BDL
SOL
BDL
15
I BDL
I BDL
SOL
I SOL
1 37.6
SOL
I BDL
1 38
53
03/05109
SOL
SOL
173
SOL
19.4
1 A
BDL
BDL
SOL
194
1.7
BDL
SOL
SOL
194
SOL
SOL
196
389
06/24/09
SOL
SOL
107
BDL
BDL
SOL
SOL
BDL
SOL
107
SOL
BDL
SOL
SOL
331
SOL
SOL
331
438
09/02/09
BOIL
SOL
140
BOL
23.5
SOL
BOL
SOL
BDL
164
2.7
SOL
BDL
BDL
317
6,4
SOL
326
490
MW-24
09/27/90
630
28
BDL
6D
SOL
SOL
BDL
SOL
SOL
718
11500
80
SOL
80
SOL
BDL
SOL
1.660
2,378
01/14/92
3,860
110
BDL
200
SOL
SOL
56
BDL
80
4,246
1,800
260
SOL
340
BDL
BDL
SOL
2,400
6.646
06/15/92
1,400
25
BDL
4,9
SOL
SOL
SOL
SOL
SOL
1,430
1,80D
180
BDL
BDL
BDL
SOL
BDL
1,980
3.410
09109192
2,700
SOL
BDL
BDL
BDL
BDL
BDL
SOL
100
2,800
2,500
150
SOL
150
BDL
SOL
SOL
2.800
5.600
03/11/98
1,230
BDL
SDL
BDL
BDL
SOL
BDL
SOL
BDL
1,230
1,920
SOL
BDL
BDL
SOL
BDL
SOL
1,920
3,150
05/25/99
637
SOL
SOL
SOL
BDL
SOL
BDL
BDL
SOL
637
1,510
SDL
SOL
BDL
BDL
SOL
BDL
1,510
2.147
10/10/02
2,000
68
SOL
31
SOL
11
2.5
BDL
4.9
2,117
1,700
16
1,4
27
180
630
BDL
2,454
4,572
D4122103
640
24
SOL
17
SDL
6A
BDL
BDL
1.8
689
500
6.4
SOL
6,3
81
180
SOL
774
1,463
06/30/44
87D
BDL
370
BDL
BDL
BDL
BDL
BDL
SOL
1,240
280
BDL
SOL
SOL
74
260
SOL
554
1,794
08/16/05
1,3D0
62
570
SDL
BDL
SOL
SDL
BDL
SOL
1,932
420
BDL
SOL
SOL
69
170
SOL
659
2,591
08/24/06
2,200
84
770
15
BDL
6.4
1.2
1.2
5.5
3.083
660
4,8
SOL
10.4
78
160
5.6
919
4,002
06/05/08
1,940
BDL
545
SOL
BDL
BDL
BAL
SOL
SOL
2,385
210
SDL
SOL
SOL
561
140
SOL
405
2,-M
09/04/08
1,430
51.7
349
SOL
BDL
SOL
SOL
SDL
BDL
1,831
253
SOL
SOL
BDL
BOL
60.3
SOL
313
2,144
01/05/09
1,610
78.4
517
SOL
SOL
BDL
BDL
SOL
SOL
2,205
280
BOL
SOL
SOL
70.9
116
BDL
467
2.672
03105/09
11250
BDL
466
BDL
BDL
SDL
BDL
SDL
BDL
1,716
117
BDL
BDL
BDL
8131-
BOL
BDL
117
1,833
06/24/09
484
BDL
119
BDL
BDL
SOL
SOL
SAL
BDL
603
SOL
BDL
BOL
SOL
SDL
BDL
SOL
0
603
091D2109
946
127
760
9.7
121
6.2
BDL
BDL
BDL
1,970
537
BDL
BOL
13,7
77.5
165
15.5
841
2,811
MW-25
03/11/98
8.9
3.5
BDL
BOL
BDL
SOL
BDL
BDL
SDL
12
SOL
SOL
BOL
BDL
SDL
SOL
SOL
0
12
05126199
10
3.6
SOL
BDL
SOL
BDL
BDL
SOL
SOL
14
SOL
SOL
SOL
SOL
SOL
SOL
BDL
0
14
06/30/04
8.1
3.5
92
BDL
SOL
SOL
SOL
BDL
BDL
22
SOL
SOL
SOL
SOL
SDL
4,4
SOL
4
26
0811"5
17
3.9
31
BDL
BDL
BDL
SOL
BDL
SDL
52
SOL
SOL
BDL
SOL
3.6
SOL
SOL
4
56
OW25106
20
4.8
51
SOL
BDL
SOL
SOL
9DL
SOL
76
SOL
BDL
SOL
SOL
1,8
4.3
BDL
6
82
06/05/08
11.7
3.2
23.5
BDL
SOL
SOL
BDL
SOL
GDL
38
SOL
BDL
1.3
SOL
2.2
4.2
BDL
8
46
09/04/08
1&7
5.2
33.2
SOL
SOL
SOL
BDL
BOL
SDL
57
BDL
I SDL
I SOL
SOL
3
4,8
SOL
8
65
01/05109
2M
615
46.6
1.1
SOL
1.1
SOL
BDL
BDL
78
BDL
SDL
SOL
SOL
4,8
6.2
BOL
11
89
03/05/09
24.9
0.3
51
1.1
BDL
BDL
SOL
SDL
BDL
85
SDL
SOL
SOL
BDL
4,8
BDL
SDL
5
90
0&24109
30.8
7.4
54.7
2,4
BDL
BDL
BDL
SOL
SOL
95
SQL
SOL
BDL
BDL
5,9
6.9
BDL
13
108
09/02109
24.0
7.9
60.1
1.6
SOL
1 A
BDL
BDL
SDL
96
SOL
SOL
SOL
SOL
8.9
9.1
SOL
18
114
MW-26 (abandoned 01/03106)
07/01/04
BDL
BDL
SOL
SOL
SOL
SOL
SOL BDL
SOL
0
BOL
SOL SOL
SOL
BDL
SOL
BDL
0
0
OB115105
BDL
SOL
SOL
BDL
BDL
SOL
SOL BDL
I SOL
U 0
BDL
I SOL I BDL
I 8131L
I SOL
I SOL
I SOL
L0
0
MW-27
10/10/02
SDL
BDL
SDL
SDL
BDL
BDL
SOL
I SDL
T BDL
0
2.3
2
1 47
1 18
1 2,3
1 SOL
I BDL
H 72 11
72
07/01/04
OOL
SOL
SOL
BDL
SOL
SOL
BDL
BDL
BDL
0
5.4
2.7
34
7.9
11
BDL
17
78
78
08/16/05
BDL
SOL
SOL
SDL
BDL
SOL
BDL
SDL
SOL
0
12
4.1
180
34
3.5
SOL
30
264
264
11/01/06
BDL
BDL
SDL
SOL
SDL
SOL
SDL
SDL
SOL
❑
5.2
2,4
38
3.1
BDL
SOL
16
66
66
MW-28
10/10/02
SOL
BDL
SDL
BDL
8131
SOL
SOL
SOL
SOL 0
10
2.2
45
22.5
BDL
2,3
BDL
82
82
07/01/04
SOL
SOL
SOL
SOL
SOL
BDL
SOL
SDL
BDL 0
95
51
4,500
1,OE5
BDL
BDL
480
3,191
3.191
08/15/05
BDL
SOL
BDL
SOL
BDL
SOL
SOL
BDL
BDL 0
210
78
2,3D0
750
SOL
SOL
740
4,078
4,076
08/25/06
SOL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
SOL 0
170
56
2,500
1,200
BDL
SOL
800
4.726
4,726
12/14/06
SOL
BDL
BDL
BDL
BOL
SOL
SOL
SOL
SOL 0
100
BDL
2,500
530
SDL
SOL
940
4,070
4,070
MW-29
07/01/04
23
8131-
2110
BDL
BDL
SOL
BDL
BDL
SOL
303
SOL
BDL
21
BDL
SOL
SOL
BDL
21
324
08/15/05
39
4.2
29
SOL
SDL
8DL
SOL
SOL
SOL
72
SOL
SDL
SDL
BDL
SOL
BDL
BDL
0
72
08/25/06
5
2.2
38
BDL
SOL
BDL
SOL A
BDL
BOL H
45
a SOL
I BDL
I SOL
I SOL
BDL
BDL
BDL 11
0
45
Notes:
All units measured in micrograms per liter, u911-
' Total Petroleum Hydrocarbons and Total VOCs include chioromethane, dichloroddluoramethane, and Vic hlorofluoromethane values (see Table 5).
BOL - Below ➢election Limits
NCO 2L Std. - North Carolwla Groundwater Standard
BOLD - Concentration exceeds the 2L Groundwater Quality Standard
MTBE - Methyl -ten butyl ether
97746 1 GS009R167 Page 4 of 5 September 30, 2009
Copyright 2W09 Kleintelder
TABLE B: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS
Sample ID
Chlorinated Hf drocarbona
Total
Chlorinated
Hydrocarbons
Petroleum Hldrocar6ons
Total
Petroleum
Hydrocarbons
Total VOCs
Collecton pate
Tetrachioroethene
Trichloroethene
'2
DichlorWhene
1'1
DrchbMethene
Vinyl Chloride
1,1
Dichloroelhane
1,2
Dichloroethane
trans 1,2
Oichloroethane
7,1,1
Thchl 'roethane
Benzene
Toluene
=E1hy0-nzene Total Xyienes
I
MTBE
I
Diisopropyl other
I
Naphthalene
NCGS 2L Std.
0.7
2.8
70
7
0.015
70
0.38
100
200
1
1.000
550 53D
200
70
21
MW-30
071011❑4
SOL
SOL SOL
BDL
BOL
BDL
BDL
BDL
BDL
0
SOL
SOL
SOL
BDL
2,200
BDL
80L
2,200 2,200
08/16/05
BDL
SOL 200
43
77
BDL
BDL
BDL
BDL
320
74
SOL
58
BDL
510
SOL
SOL
642 962
0B125106
SOL
SAL 23
2.5
i6
BDL
SOL
BDL
SOL
42
23
L SOL
2.6
2
1,500
13
SOL
1,541 1,582
MW-31
1Oil 0/02
SOL
BDL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
0
SOL
320
2,600
7,900
SAL
BDL
8DL
10.820
10,620
D4122JG3
SOL
SOL
SOL
BDL
SOL
SOL
SOL
SOL
SOL
0
SOL
310
1300
4,600
SOL
SOL
SOL
5.710
6,710
07/01/04
SOL
SAL
53
BDL
SOL
BDL
SOL
BDL
BDL
53
18
84
590
1,360
SOL
SOL
400
2.462
2,505
00/15/05
8DL
BDL
48
BDL
SOL
SOL
BDL
SOL
BDL
48
SOL
67
1,100
1,490
SOL
BDL
750
3.407
3,455
11/01/06
SOL
SOL
SOL
SOL
SOL
8DL
SOL
BDL
BDL
0
SOL
BOL
1,700
390
SDL
BDL
720
2.810
2,810
MW-32
07/01/04
BDL
SOL
SOL
BDL
BDL
BDL
SOL
BOL
SOL
0
SOL
SOL
SOL
SOL
290
L BDL
BDL
290
290
08/15/05
SOL
SOL
SOL
$DL
SOL
SOL
SOL
SOL
SOL
0
SOL
SOL
SOL
SOL
1B0
L SOL
SOL
180
180
08/25/06
SOL
SOL
BDL
SOL
SOL
SOL
BOL
SOL
SOL
0
1,400
280
190
600
15,000
32
160
17,662
17.662
1 V01106
SOL
BOL
SOL
SOL
SOL
BDL
SOL
BDL
SOL
0
1,400
320
340
900
20,000
8DL
SOL
22,960
22,980
12l14/06
SOL
SOL
BDL
SOL
SOL
SOL
SOL
SDL
SOL
❑
1.500
3.700
1,700
8,000
16,000
SOL
1,100
32,000
320❑0
M W •33
10/10/02
SOL
SOL
SOL
BDL
SOL
BDL
BDL
SOL
SOL
0
SOL
BDL
BDL
SOL
SOL
SOL
BDL
0
0
06/30/04
BDL
SOL
1.6
BDL
SOL
BOL
SOL
SOL
BDL
2
SOL
BDL
SOL
SOL
SAL
BDL
SOL
0
2
❑6i5/05
SOL
BDL
5.6
SAL
BDL
BDL
BDL
SOL
SAL
6
BDL
SOL
SOL
SAL
BDL
SOL
SOL
0
6
❑8125106
SOL
BDL
5.7
SOL
SOL
BDL
SOL
SOL
BDL
6
SOL
SOL
BDL
SOL
SOL
SOL
BDL
0
6
MW-34
G4122103
SOL
100
BDL
15
SOL
7.2
SOL
SOL
SOL
122
SOL
SOL
BDL
SOL
BDL
SOL
BDL
0
122
07/01/04
BOL
130
63
6.3
SOL
7.4
BDL
SOL
BOL
207
BDL
BDL
BDL
SOL
SOL
SOL
BDL
G
207
❑8116/05
SOL
90
37
SOL
BDL
$DL
SOL
SOL
SOL
127
BDL
BDL
BDL
SAL
SOL
SOL
SOL
0
127
08/25/06
SOL
59
24
4.8
BDL
2.3
SOL
SOL
BDL
90
SOL
SAL
SOL
BDL
SOL
BDL
BDL
0
90
M W -40
11101*6 SOL SOL BOL SOL SOL BDL SOL SOL BDL 0 250 230 280 652 BDL SOL 130 1,442 1.442
MW-41
04)22J03
SOL
SOL
SOL
BDL
SOL
BDL
BDL
SOL
BDL
0
7,200
6,600
2,400
10,800
SOL
SOL
BDL
27,0D0
27.000
07/08/04
SOL
BDL
BDL
BDL
BOL
SOL
SOL
BDL
SOL
0
7,000
6,600
2,600
13,300
SOL
520
770
30,790
30.790
06/16/05
SOL
SAL
SOL
SOL
BDL
SOL
SDL
SOL
SOL
0
6,400
4,900
2,500
9,700
SOL
230
780
23.510
23.510
08/24/06
BDL
SOL
SOL
SOL
SOL
BDL
9DL
BDL
BDL
0
3,100
3.000
1,000
2,900
BDL
6.4
16
10,022
1❑,022
M W -42
011101D6
36.0
SOL
7.5
6.1
BDL
1.6
SOL
BOL
BDL
51
BDL
SOL
SOL
SOL
BDL
SOL
3.2
3
54
08/25/06
27.0
SOL
4.7
3.5
SOL
1.5
BDL
BDL
BDL
37
SOL
BDL
SOL
SOL
SOL
SOL
BDL
0
37
06/05/08
5.3
SOL
BDL
SOL
SOL
SOL
SOL
BDL
SOL
5
SOL
SOL
SOL
SOL
BDL
SOL
BDL
0
5
09/04/08
6.7
SOL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
6
BDL
BDL
SOL
SOL
BDL
SOL
SOL
❑
6
01105/09
5.3
BDL
80L
BDL
SOL
BDL
BDL
BDL
SOL
5
BDL
BOL
SOL
SOL
BDL
SOL
BDL
❑
5
03/05/09
2.7
SOL
SOL
SOL
BDL
B➢L
BDL
SOL
SOL
3
BDL
SOL
BDL
SOL
SOL
SOL
BDL
0
3
06/24/09
3.1
BOL
BOL
SDL
BRL
BDL
SDL
BDL
BDL
3
BDL
BDL
BDL
BDL
SOL
SDL
BDL
Q
3
D9102/09
3.4
BDL
SOL
BDL
BDL
BDL
SOL
SOL
$➢L
3
BDL
BDL
BDL
BOL
BDL
SOL
BDL
0
3
MW-43D
01/10/06
390
12.0
110
42.0
SOL
6.8
BOL I
SDL
f SOL
H 567
1 4.8
1 BDL
I BDL
BOL
1 36.0
1 68.0
1 BOL
109
670
03/27/09
BOL
SOL
BDL
9.3
BDL
BDL
1.6
BDL
1.2
12
9.0
BDL
7.5
SOL
3.6
SOL
4.4
25
37
0674109
381
11A
114
SOL
BDL
BOL
SOL
SOL
SOL
507
BDL
SOL
SOL
SOL
13.6
BDL
SOL
14
520
09/02/09
337
11A
99A
13.9
BDL
3.9
SOL
SOL
SOL
466
3
BOL
SOL
SOL
167
29.9
SOL
57
523
MW-04
04/11/07 BDL 2.1 SOL BOL BDL SOL SOL BOIL SOL 2 SOL SOL SOL BDL BDL SOL BDL ❑ 2
M W -45
09/13/07
SOL
SOL
SOL
SOL
SOL
SOL
BDL
SOL
BDL
0
SOL
BDL
SOL
SOL
SAL
SOL
SOL
❑
0
06/05/08
1.2
SOL
SOL
SOL
BDL
SOL
SOL
SOL
SOL
1
BDL
SOL
8DL
SOL
BDL
SOL
BDL
0
1
09/041❑B
BDL
BDL
BDL
SOL
SOL
SOL
SOL
BDL
SOL
0
SOL
SOL
BDL
SOL
BOL
SOL
SOL
❑
0
01105/69
1.4
1.2
SOL
SOL
SOL
SOL
BDL
BDL
SOL
3
BDL
BDL
BDL
SOL
SOL
SOL
SOL
❑
3
U051❑9
1.3
BDL
BDL
SOL
SOL
BOL
SOL
SOL
SOL
1
BOL
SOL
BOL
SOL
SOL
BDL
SOL
0
1
06/24/09
1.8
SOL
BDL
SOL
SOL
SOL
SOL
SOL
BOL
2
SOL
SOL
BDL
BDL
BDL
SOL
SOL
0
2
❑91021Q9
2A
1.1
BDL
SOL
SOL
SOL
SOL
SOL
SOL
4
BDL
BDL
BDL
8➢L
BDL
BDL
SOL
0
4
Notes:
All units measured in micrograms per liter, pg/L
1 Total Petroleum Hydrocarbons and Total VQCs include chioromethane, dichloroditluoromethane, and trichlorotluoromethane values {see Table 5).
BDL - Below Detection Limits
NCGS 2L Sid. - North Carolina Groundwater Standard
BOLD - Concentration exceeds the 2L Groundwater Quality Standard
MTBE - Methyl-terl bulyl ether
97746 1 GS009R167 Page 5 of 5 September 30, 2009
Copyright 2DD9 Kleintelcor
FIGURES
KL EINFEL DER
Bright People. Right Solutions.
313 GALLIMCRE OA;HY ROM
GREENSBORO, NORTH CAROLINA
PHONE: 336.888.OD93
FIGURE 1
SITE LOCATION MAP
GilbarCO
7300 West Friendly Avenue
Greensboro, North Carolina
DATE: 9-17.2009
USGS 7,5' TOPOGRAPHIC MAP.
APPROVFD BY:
SCALE: V = 2.000'
1�
L_
MW-45
�r
•.$i- MW-42
MW-12b
r - - MW-12
MW-14 SUB
STATIaNJ
RW- WATER
—Y TANK
Syr Y� MW-41 N MW-13b
G
A MW-11 MW-13
MW-qp j'
i RW-3
RW-2
I
EXISTING
PARKING
ISTING
IRKING
EXISTING
PARKING
M W-45
832.46
A�
835
833.34 e�
833.16
MW-42 842.06
834.07
MW-12
835 W-13
837.01 835-76 ~ SUB
835
�Y•' 836.75 Rmac-
TAiJi{
MW-10
8'10 MW-41 F 848-9� MW-130
851.69 N 844.91
y- MW-40 RW-3
1 845 9-51 -2 ❑
1. 98 MW-11
850 gs= $44-27 843.45
858.68 r
M W-28
856 RW-4 864.19
Mw-33
M W-31$. 847.49
851.82 64r,
M W-32
862.90
MW-27 MW-30
849-98 ` 840-70 4
MW-44
855
LEGEND
EXISTING
INJECTION WELL LOCATION AND BUILDNO
r 854.98 GROUNDWATER ELEVATION
MW-14 MONITORING WELL LOCATION AND
837-01 GROUNDWATER ELEVATION
RW-7 RECOVERY WELL LOCATION
M-,- GROUNDWATER CONTOUR LINE
NOTES-
GROUNDWATER ELEVATIONS WERE RECORDED SEPTEMBER 2, 2W9
w
- 839 80
• -1F -1F mac- �- -iF �F �F --AF -JI--
845
J�
MW-13
845.24
856
85a
EXISTING
PARKING
MONITORING WELLS MW-13D, MW-23D, AND MW-25 ARE SCREENED
BELOW THE WATER TABLE AND WERE NOT USED TO GENERATE
THE GROUNDWATER CONTOURS
EXISTING
PARKING
M W-45
4 ,
MW-42
3
2.811
M W-14
24
43
may,.
�W
BOL
LEGEND
r. INJECTION WELL LOCATION
MW-14 MONITORING WELL LOCATION} WITH
31 TOTAL VOCS CONCENTRATION (uq/L)
RW-7 RECOVERY WELL LOCATION
1 D0� TOTAL VOCs ISOCONCENTRATION LINE
NOTE:
SAMPLES COLLECTED ON SEPTEMBER 2. 20M
lT4 4$�MW-120
MW-12
Mr
STATI
WATER
TANK
MW-10
MW-41 ¢ MW-13D
45 fMW-13
RW-3
MW-40 MW-11 SQL •r
�W ]
R W-2 1.887 438
1.000
100
MW-28 BOL
M W-31
RW-4 10.000
MW-27
EfI TNG
BUILDNO
MW-30 `f
MW-44
EY.ISTING
PARKING
r'
�l
MW-45
sr
s MW-42
466 3
�{1() MW-12D
yr MW-14 1,g70
MW-12
24 Sue L
x —� 96 I ATIONJ T
37 R WATER
�w TANK
i3GL
F MW-10 MW-430
MW-41 ¢ 22
�RW-3 c MW-13
-40 MW-11 ■ 48
..., ,i Rw 2 591 7
•� ` 164
MW-28
-RW d
MW-31
MW-32 MW-33
MW-2 �4
i
i
MW-30 41
MW-4
EXISTING
PARKING
EXISTING
PARKING
EXISTING
LEGEND BUILDNG
',. INJECTION WELL LOCATION
MW-14 MONITORING WELL LOCATION WITH
31 TOTAL CHLORINATED HYDROCARBONS CONCENTRATION (ug/L)
0 RW-7 RECOVERY WELL LOCATION
TOTAL CHLORINATED HYDROCARBONS ISOCONCENTRATION LINE
FIGURE 5
TOTAL CHLORINATED HYDROCARBONS
NOTE:
SAMPLES COLLECTED ON SEPTEMBER 2, 2009 JCL EINFEL DER t Frieno
73ee sbor Friendly Avenue
Bright People. Right Solutions. Greensboro, North Carolina
APPROVED By
313 GALLIMORE DAIRY ROM DATE: 7-31-2009 SCALE: 1' = 100'
GREENSBORO. NORTH CAROLINA
PHONE: 336-SG6.0093 (/!6 /�_1^p
DRAWN BY: GGL v y PROJECT NO! 9774fi
APPENDIX A
e
aceAnalylical
www.peCMW&.COM
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 2a804
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
September 14, 2009
Ms. Gail Licayan
Trigon/Kleinfelder, Inc.
313 Galiimore Dairy Rd
Greensboro, NC 27409
RE: Project: GILBARCO 97746
Pace Project No.: 9252397
(828)254--7176
Dear Ms. Licayan:
Enclosed are the analytical results for sample(s) received by the laboratory on September 03, 2009.
The results relate only to the samples included in this report_ Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
bonnie.mckee@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
(704)875-9092
Page 1 of 21
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc..
aceAnalytical.
www.pecelabscarr
t
Project GILBARCC 97746
Pare Project No.: 9252397
Charlotte Certification IDs
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
North Carolina Drinking Water Certification #: 37706
West Virginia Certification #: 357
Pace Analytical Services, Inc.
2225 Riverside Or.
Ashevllle. NC 28804
(828)254-7176
CERTIFICATIONS
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 990060001
South Carolina Drinking Water Cent. #: 990060003
Tennessee Certification #: D4010
Virginia Certification #: 00213
North Carolina Field Services Certification #: 5342
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, ]no.
9800 Kin ceyAve . Suite 100
Huntersville, NC 28078
(704)875-9092
Page 2 of 21
This report shall not he reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
aceAnalytical
2225 Riverside Rr.
www.pacews.eam
Asheville. NC 28804
(82$)254-7176
SAMPLE SUMMARY
Project.
Pace Project No.:
GILBARCO 97746
9252397
Lab lR
Sample ID
Matrix
Date Collected
Rate Received
9252397001
MW-7
Water
09/02/09 1404
M03109 13:38
9252397002
MW-11
Water
09/02/09 09:37
09/03/09 13:38
9252397003
MW-13
Water
09/02/09 09:10
09/03109 13:38
9252397004
MW-131)
Water
09/02/09 09:06
09/03/09 1138
9252397005
MW-14
Water
09/021091120
0910310913:38
9252397006
MW-23❑
Water
09/02/09 09:03
09/03/09 13:38
9252397007
MW-24
Water
09/0210912:56
09103/0913:38
9252397000
MW-25
Water
09/0210913:00
09103/0913:38
9252397009
MW42
Water
09102M914:52
0910310913:38
9252397010
MW-43D
Water
09102/0914:48
09/03/0913:38
9252397011
MW-45
Water
09/02/0915:05
09/03/0913:38
9252397012
MW-14Q
Water
09/02/0913:12
09/03/0913:38
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except in full.
without the written consent of Paacee Analytical Services, Inc..
la t.
Pace Analytical Services, Inc.
9800 Kin cey Ave. Smote 100
Huntersville, MC 28078
(704)875-9092
Page 3 of 21
aceAnalydrcal
wuNpq(" +abs.cam
Project: GILBARCO 97746
Pace Project No-: 9252397
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
(828)254-7176
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
913M Kincey Ave. Suite 100
Huntersville, NC 28078
(7041875-9092
Lab ID
Sample I❑
Method
Analysts
Analytes
Reported
9252397001
MW-7
SM
6200B
MCK
43
9252397002
MW11
SM
6200B
MCK
43
9252397003
MW-13
SM
6200B
MCK
43
9252397004
MW-13❑
SM
6200B
MCK
43
9252397005
MW-14
SM
62008
MCK
43
9252397006
MW-23❑
SM
6200E
MCK
43
9252397007
MW-24
SM
6200B
MCK
43
9252397008
MW-25
SM
6200B
MCK
43
9252397009
MW-42
SM
6200B
MCK
43
9252397010
MW-43D
SM
6200B
MCK
43
9252397011
MW45
SM
6200B
MCK
43
9252397012
MW-14D
SM
62008
MCK
43
REPORT OF LABORATORY ANALYSIS
This report shall act De reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 21
aceAnalytiea!
www.p&ow8b&wM
Pace AnalyticaI Services, Inc.
2225 Riverside ❑r,
Asheville, NC 28804
(828 y254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. suite 100
Huntersville, NC 28078
{7041875-9092
Project: GILBARCO 97746
Pace Project No.: 9252397
Sample: MW-7 Lab ID: 9252397001 Collected: D9102109 14,04 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
601/602 Volatiles by SM 6200 Analytical Method: SM 6200B
Benzene
NO ug/L
5.0
5.0
5
09/10/09 10:24
71-43-2
BromOdiohloromethane
NO uglL
5.0
5.0
5
09/10/09 10:24
75-27-4
Bromoform
NO ug/L
5.0
5.0
5
D9110109 10:24
75-25-2
Bromomethane
NO ugIL
5.0
5.0
5
09/10/09 10:24
74-83-9
Carbon tetrach#oride
N❑ uglL
5.0
5.0
5
09110/09 10.24
56-23-5
Chlorobenzene
NO uglL
5.0
5.0
5
09110109 10:24
108-90-7
Chloroethane
NO uglL
5.0
5.0
5
09/10/09 10:24
75-00-3
Chloroform
ND uglL
5.0
5.0
5
09110/09 10:24
67-66-3
Chloromethane
ND uglL
5.0
5.0
5
09/10/09 10:24
74.87-3
Dibromochloromethane
NO uglL
5.0
5.0
5
09/10/09 10:24
124-48-1
1,2-Dibromoethane (EDB)
NO ug/L
5.0
5.D
5
09/10/09 1D:24
105-93-4
1,2-Dichlorobenzene
NO ug/L
5.0
5.0
5
09/10109 10:24
95-50-1
1,3-Dichlorobenzene
NO ug/L
5.0
5.0
5
09110/0910:24
541-73-1
1,4-Dichlorobenzene
N❑ ug1L
5.0
5.0
5
09110/0910:24
106-46-7
Dichlorodifluoromethane
8.7 ugIL
5.0
5.0
5
09/10/09 10:24
75-71-8
1.1-Dichloreethane
7.8 ug/L
5.0
5.0
5
09/10/09 10:24
75-34-3
1,2-Dichioroethane
NO ugIL
5.0
5.0
5
09/10/09 10:24
107-06-2
1,1-Dichiomethene
6.3 ug1L
5,0
5,0
5
D9110109 10:24
75-35-4
cis-1,2-Dichloroethene
556 ugIL
5.0
5.0
5
09/10/09 10:24
156.59-2
trans-1,2-Dichloroethene
ND uglL
5.0
5.0
5
09/10/09 10:24
156.60-5
1,2-Dichloropropane
NO ug/L
5.0
5.0
5
09/10109 10:24
78-87-5
cis-1,3-Dichloropropene
N❑ ug/L
5.0
5.0
5
09/10/09 10:24
10061-01.5
trans-1,3-Dichloropropene
ND ug/L
5.0
5.0
5
09/10/09 10:24
10061-02-6
Diisopropyl ether
NO ug1L
5.0
5.0
5
09/10/09 10:24
108-20-3
Ethylbenzene
519 ug1L
5.0
5.0
5
0 9110/0 9 1 D: 24
100-41-4
Methylene Chloride
NO uglL
10.0
1 D.0
5
09/10/09 10:24
75-09-2
Methyl-tert-butyl ether
NO ug/L
5.0
5.0
5
09/10/09 10:24
1634-04-4
Naphthalene
288 uglL
10.0
10.0
5
09110/0910:24
91-20-3
1,1,2,2-Tetrachloroethane
NO ugIL
5.0
5.0
5
09/10/09 10:24
79-34-5
Tetrachloroethene
N❑ ugIL
5.D
5.0
5
09/1010910*24
127-18-4
Toluene
6.1 ugJL
5.0
5.0
5
09/10/09 10:24
108-88-3
1.1,1-TrichIoroethane
N❑ uglL
5.0
5.0
5
09/10/0910.24
71-55-6
1,1.2-Trichloroethane
ND uglL
5.0
5.0
5
09/10/09 10:24
79-00-5
Trichloroethene
N❑ ug1L
5.0
5,0
5
09/10/09 10,24
79-01-6
Tri ch lorofluorom ethane
ND ug/L
5.0
5.0
5
09/10/09 10:24
75-69-4
Vnyl chloride
27.3 ugIL
5.0
5.0
5
09/10/09 10:24
75-01-4
Xylene (Total)
468 ug1L
10.0
10.0
5
09/10109 10:24
1330-20-7
m&p-Xylene
447 ug1L
10.0
10.0
5
09110/0910:24
1330-20-7
o-Xylene
21.5 ug1L
5.0
5.0
5
09/10/09 10:24
95-47-6
4-Bromofluorobenzene (S)
100 %
70-130
5
09/10/09 10:24
460-00-4
Dibromofluoromethane (S)
102 %
70-130
5
09/10/09 10:24
1868-53-7
1,2-Dichioroethane-d4 (S)
102 %
70-130
5
D9110109 10:24
17060-07-0
Toluene-d8 (S)
96 %
70-130
5
09/10/09 10:24
2037-26-5
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS Page 5 of 21
This report shall not be reproduced, except in full,
without the written consent of Pace
rAnalytical Services, Inc..
16h11..�
aceAnalytical
www.pecewbscom
I
Project: GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW-11 Lab ID: 9252397002 Collected: 09/02/09 09:37 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
601/602 Volatiles by SM 6200 Analytical Method: SM 6200B
Benzene
NO uglL
1.0
1.0
1
0911110913:26
71-43-2
Bromodichloromethane
NO uglL
1.0
1.0
1
09/11/09 13.26
75-27-4
Bromoform
NO uglL
1.0
1.0
1
09/11/09 13:26
75-25-2
Bromomethane
NO uglL
1.0
1.0
1
09/11/09 13:26
74-83-9
Carbon tetrachloride
NO uglL
1.0
1.0
1
09/11/09 13:26
56-23-5
Chlorobenzene
NO ug1L
1.0
1.0
1
09111/0913:25
108-90-7
Chloroethane
NO uglL
1.0
1.0
1
09/11/09 13:26
75-00-3
Chloroform
ND uglL
1.0
1.0
1
09/11/09 13:26
67-66-3
Chloromethane
NO uglL
1.0
1.0
1
09111/0913:26
74-87-3
Dibromochloromethane
NO uglL
1.0
1.0
1
09/11/0913:26
124-48-1
1,2-Oibromoethane (EDB)
NO uglL
1.0
1.0
1
09/11/09 13:26
106-93-4
1.2-Dichlorobenzene
NO uglL
1.0
1.0
1
09111/0913:26
95-50-1
1.3-Dichlorobenzene
NO uglL
1.0
1.0
1
09/11/09 13:26
541-73-1
1,4-Dichlorobenzene
NO uglL
1.0
1.0
1
09/11/09 13:26
106-46-7
Dichlorodifluoromethane
NO uglL
1.0
1.0
1
09111/0913:26
75-71-8
1,1-Dlchloroethane
NO ug1L
1.0
1.0
1
09/11109 13:26
75-34-3
1,2-Dichlorcethane
NO uglL
1.0
1.0
1
09/11/0913:26
107-06-2
11-Dichloroethene
NO ug1L
1.0
1.0
1
0911110913:26
75-35-4
cis-1,2-Dichloroethene
NO ug1L
1.D
1.0
1
0911110913:26
156-59-2
trans-1,2-Dichforoethene
NO uglL
1.0
1.0
1
09111/0913:26
156-60-5
1,2-Dichloropropane
NO ug1L
1.0
1.0
1
09111/0913:26
78-87-5
cis-1,3-Dichloropropene
ND ug1L
1.0
1.0
1
09/11/09 13:26
10061-01-5
Vans-1,3-Dichloropropene
ND uglL
1.0
1.0
1
09/11/09 13:26
10061-02-6
Diisopropyl ether
NO uglL
1.0
1.0
1
09/11/09 13:26
108-20-3
Ethylbenzene
NO uglL
1.0
1.0
1
09/11109 13:26
100-41-4
Methylene Chloride
NO uglL
2.0
2.0
1
09/11/09 13:26
75-09-2
Methyl-tert-butyl ether
NO ug1L
1.0
1.0
1
09/11/09 13:26
1634-04-4
Naphthalene
NO ug1L
2.0
2.0
1
09/11/0913:26
91-20-3
1,1,2,2-Tetrachlaroethane
NO uglL
1A
1.0
1
09/11/0913,26
79-34-5
Tetrachloroethene
4.4 ug1L
1.0
1.0
1
09/11109 13:26
127-18-4
Toluene
ND uglL
1.0
1.0
1
09/1110913:26
108-88-3
1,11-Trichioroethane
NO uglL
1.0
1.D
1
09/11109 13:26
71-55-6
1,1,2-Trichloroethane
NO ug1L
1.0
1.0
1
09/1110913:26
79-00-5
Trichloroethene
2.3 uglL
1.0
1.0
1
0911110913:26
79-01-6
Tfthlorofluoromethane
ND uglL
1.0
1.0
1
09/1110913:26
75-59-4
Vinyl chloride
ND uglL
1.0
1.0
1
09/11109 13:26
75-01-4
Xylene (Total)
NO uglL
2A
2.0
1
09/11/09 13:26
1330-2D-7
m&p-Xylene
ND uglL
2.0
2.0
1
09/11/09 13:26
1330-20-7
o-Xylene
NO ug1L
1.0
1.0
1
09111/0913:26
95.47-6
4-Bromofluorobenzene (S)
97 %
70-13D
1
09/11109 13:26
460-00-4
Dibromafluoromethane (S)
101 %
70-130
1
09/11/09 13:26
1868-53-7
1,2-DicNoroethane-d4 (S)
103 %
70-130
1
09/11/09 13:26
17060-07-0
Toluene-d8 (S)
98 %
70-130
1
09/11/09 13:26
2037-26-5
Date: 09/14/2009 09:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduewd, except in full,
without the written consent of Race Analytical Services, Inc..
Page 6 of 21
aceAnalWical
wwwpecabbloom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[828]254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
(704)875-9092
Project: GILBARCC 97746
Pace Project No.: 9252397
Sample_ NW-13 Lab ID: 9252397003 Collected: 09/02/09 09:10 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MOIL OF Prepared Analyzed CAS No. Qual
6011602 Volatiles by SM 6200 Analytical Method: SM 6200B
Benzene
1.2 ug/L
1.0
1.0
1
09/10109 11.11
71-43-2
$romodichloromethane
NO ug/L
1.0
1.0
1
09/10109 11A1
75-27-4
Bromoform
NO ug/L
1.0
1.0
1
09110/09 11:11
75-25-2
Bromomethane
NO ug/L
1.0
1.0
1
09/10/09 11:11
74-83.9
Carbon tetrachloride
N❑ ug/L
1.0
1.0
1
09/10/09 11:11
56-23-5
Chlorobenzene
ND ug/L
1.0
1.0
1
09/10/09 11:11
108-90-7
Chloroethane
ND ug/L
1.0
1.0
1
09/10/09 11,11
75-00-3
Chloroform
ND ug/L
1.0
1.0
1
0911010911:11
67-66-3
Chloromethane
NO ug/L
1.0
1.0
1
09110109 11;11
74-87-3
Dibromochloromethane
ND uglL
1.0
1.0
1
0911010911.11
124-48-1
1.2-Dibromoethane (EDB)
ND ug/L
1.0
1.0
1
09/10/09 11:11
106-93-4
1,2-Dichlorobenzene
ND ug/L
1.0
1.0
1
09/10109 11:11
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
1.0
1
091101091111
541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
1.0
1
091101D911.11
106-46-7
Dichlorodifluoromethane
NO ug/L
1.0
1.0
1
09/10/09 11:11
75-71-8
1,1-Dichloroethane
ND ug/L
1.0
I.0
1
09/10/09 11:11
75-34-3
12-Dichloroethane
NO ug/L
1.0
1.0
1
0911D10911:11
107-06.2
11-Dichloroethene
ND ug/L
1.0
1.0
1
09110/09 11:11
75-35-4
cis-1,2-Dichloroethane
47.6 ug/L
1.0
1.0
1
0911010911:11
156-59-2
trans-1,2-Dichloroethane
ND uglL
1.0
1A
1
09/10/0911:11
156-60-5
1,2-Dichloropropane
ND ug/L
1.0
1.0
1
09/10/09 11:11
78-87-5
ds-1,3-DichlorDpropene
N❑ ug/L
1.0
1.0
1
09/1010911:11
10061-01-5
trans-1.3-Dichloropropene
NO ug/L
1.0
1.0
1
09/10/09 11:11
10061-02-6
Diisopropy! ether
ND ug/L
1.0
1.0
1
09/10/09 11:11
108-20-3
Ethylbenzene
N❑ ug1L
1.0
1.0
1
09/10/09 11:11
100-41-4
Methylene Chloride
NO ug/L
2.0
2.0
1
09/10109 11:11
75-09-2
Methyl -tort -butyl ether
3.6 ug/L
1,0
1.0
1
09/10/09 11:11
1634-04-4
Naphthalene
NO ug/L
2.0
2.0
1
09110/0911:11
91-20-3
1,1,2,2-TetrachIoroethane
ND ug/L
1.0
1.0
1
09/1010911:11
79-34-5
Tetrachloraethene
NO ug/L
1.0
1.0
1
09/10/09 11:11
127-18-4
Toluene
NO uglL
1.0
1.0
1
09/10/09 1111
108-88-3
1,1.1-Trichloroethane
NO ug/L
1.0
1.0
1
09/10/09 11:11
71-55-6
1,1.2-Trichloroethane
ND ug/L
1.0
1.0
1
09/10/09 11,11
79-00-5
Trichloroethene
N❑ ug/L
1.0
1.0
1
09/10/09 11:11
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1.0
1
09/10/09 11:11
75-69-4
Vinyl chloride
ND ug/L
1.0
1.0
1
09/10/09 11,11
75-01-4
Xylene (Total)
NO ug/L
2.0
2.0
1
09110/09 11:11
1330-20-7
m&p-Xylene
ND ug/L
2.0
2.0
1
09/1010911:11
1330-20-7
o-Xylene
NO ug/L
1.0
1,0
1
09/10/09 11:11
95-47-6
4-Bromofluorobenzene (S)
92 %
70-130
1
09/10/09 11:11
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
09/10/09 11;11
1868-53-7
1,2-Dichloroethane-d4 (S)
101 %
70-130
1
09/10/09 11:11
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
09/10/09 11:11
2037-26-5
Date: 09/14/2009 09:56AM REPORT OF LABORATORY ANALYSIS Page 7 of 21
This report shall not be reproduced, except in lull.
without the written can sent of Pace Analytical Services, Inc.
:�J .iG10>L.rc
aceAnalytical
wwwpeoele68.WM
Pace Analytical Services, Inc.
2225 Riverside Dr -
As h eyi I to, NC 28804
(B28)254-7175
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kin cey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: GILBARCO 97746
Pace Project No.: 9252397
Sample: MW-13D Lab ID: 9252397004 Collected: 09/02/09 09:06 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. ❑ual
6011602 Volatlles by SM 6200 Analytical Method: 5M 6200B
Benzene
NO ug1L
1.0
1.0
1
09/10/09 11:35
71.43.2
Bromodichloromethane
NO uglL
1.0
1.0
1
09/10109 11:35
75-27-4
Bromoform
ND uglL
1.0
1.0
1
09110/0911:35
75-25-2
Bromomethane
NO uglL
1.0
1.0
1
09/10/09 11:35
74-83-9
Carbon tetrachloride
ND uglL
1.0
1.0
1
09/10/09 11.35
56-23-5
Chlorobenzene
NO uglL
1.0
1.0
1
0911010911:35
108-90-7
Chlomethane
NO uglL
1.0
1.0
1
09/10/0911,35
75-00-3
Chloroform
ND ug1L
1.0
1.0
1
09/10/09 11:35
67-66-3
Chloromethane
NO ug1L
1.0
1.0
1
09/10109 11:35
74-87-3
Dlbromochloromethane
ND ug1L
1.0
1,0
1
0911010911:35
124-48-1
1,2-Dibromoethane (EDS)
ND ug1L
1.0
1.0
1
09/10109 11:35
106-93-4
1,2-Dichlorobenzene
NO ug1L
1.0
1 A
1
0911 D109 11.35
95.50-1
1,3-Dichlorobenzene
NO uglL
1.0
1,0
1
09110/0911:35
541-73-1
1,4-Dichlorobenzene
NO uglL
1.0
1.0
1
09/10/09 11:35
10646-7
Dichierodifluoromethane
NO uglL
1.0
1.0
1
09/10/09 11:35
75.71-8
1,1-Dichloroethane
N❑ uglL
1.0
1.0
1
09/10/09 11:35
75-34-3
1,2-Dichloroethane
N❑ uglL
1.0
1.0
1
09110/0911:36
107-06-2
1,1-Dichloroethene
ND uglL
1.0
1.0
1
09110/0911.35
75-35-4
cis-1,2-Dichloroethene
16.7 uglL
1.0
1.0
1
09/10/0911:36
156-59-2
trans-1,2-Dichloroethene
NO uglL
1.0
1.0
1
09/10109 11.35
156-60-5
1,2-Dichlompropane
NO uglL
1.0
1.0
1
D911010911:35
78-87-5
cis-1,3-Dichloropropene
NO uglL
1.0
1.0
1
09/10/09 11:35
10061-01-5
trans-1,3-Dichloropropene
NO uglL
1.0
1A
1
0911010911:35
10061-02-6
Diisopropyl ether
NO ug1L
1.0
1.0
1
09/10/09 11:35
108-20-3
Ethylbenzene
ND uglL
1.0
1.0
1
09/10/09 11:35
100-41-4
Methylene Chloride
NO uglL
2.0
2.0
1
09/10/09 11:35
75-09-2
Methyl-tert-butyl ether
23.1 uglL
1.0
1.0
1
09/10/09 11:35
1634-04-4
Naphthalene
NO uglL
2.0
2.0
1
0911010911:35
91-20-3
1,1,2,2-Tetrachloroethane
NO ug1L
1.0
1.D
1
09/10/0911:36
79.34-5
Tetrachloroethene
NO uglL
1.0
1.0
1
09/1010911,35
127-18-4
Toluene
NO uglL
1.0
1.0
1
0911 D109 11:35
108-8B-3
1,1,1-Trichloroethane
ND uglL
1.0
1.0
1
09110/0911:35
71-55-6
1,1,2-Trlchloroethane
ND uglL
1.0
1.0
1
09110/0911:35
79-00-5
Trichloroethene
NO uglL
1.0
1.0
1
09/10/09 11:35
79-01-6
Trich{orofluoromethane
NO uglL
1.0
1.0
1
09110/0911:35
75-69-4
Vinyl chloride
5.3 uglL
1.0
1.0
1
09/10/09 11:35
75-01-4
Xylene (Total)
NO uglL
2.D
2.0
1
09/10/09 11:35
1330-20-7
m&p-Xylene
NO ug1L
2.0
2.0
1
09/10/09 11:35
1330-20-7
o-Xylene
ND uglL
1.0
1.0
1
09/10/09 11:35
95-47-6
4-Bromofluorobenzene (S)
95 %
70-130
1
09/10/09 11:35
460-004
Dibromofluoromethane (S)
102 %
70-130
1
09110/09 11:35
1868-53.7
1,24)ichloroethane-d4 (S)
101 %
70-130
1
09110/09 11:35
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
09/10/09 11:35
2037-26-5
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS Page 8 of 21
This report shall not be reproduced, except in full,
without the written wnsent of Pace
+Aria lytical Services, Inc.,
��l .ItGIR1L�
aceAnalytical
w wPecatebamm
Project: GILBARCQ 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
(&28)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinney Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW-14 Lab ID: 9252397005 Collected: 09/02/09 13:20 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6011602 Vvlatiles by SM 6200
Benzene
Bromod ich torometh a n e
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
❑ibmmochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlarobenzene
1,3-Dichimbenzene
1,4-Dichlorobenzene
DI ch 10 rod ifl u0rometh a n e
1,1-Dichloroethane
1,2-Dichloroethane
1.1-Dichloroethane
cis-1 ,2-Dichloroethane
trans- l ,2-Dichloroethene
1,2-Dichlompropane
cis-1,3-Dichloropropene
trans-1,3-DicMoropropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl4ert-butyl ether
Naphthalene
1,1,22-Tetrachloroethane
Tetrachtorcethene
Toluene
1,1.1-Trichloroethane
1,1,2-TOchloroethane
Trichloroethene
Tdchlarofluoromethane
Vinyl chloride
Xyiene (Total)
m&p-Xylene
o-xyiene
4-Bromofluorobenzene (S)
Dibnomofiuoromethane (S)
1,2-Dichloroethane-dill (S)
Toluene-d8 (S)
Date: 09/14/2009 09:56 AM
Analytical Method: 5M 6200B
ND uglL
1.0
1.0
1
09110/09 11.58
71-43-2
NO uglL
1.0
1.0
1
09110/09 11:58
75-27-4
NO ug1L
1.0
1 A
1
D9110/09 11:58
75-25-2
NO ug1L
1.0
1.0
1
09/10/09 11:58
74-83-9
ND ug/L
1.0
1.0
1
09/10/09 11:58
56-23-5
NO ug1L
1.0
1.0
1
09/10109 11:58
108-90-7
ND ug/L
1.0
1.0
1
09/10109 11:58
75-OD-3
ND ug1L
1.0
1.D
1
09/10109 11:58
67-66-3
NO uglL
1.0
1.0
1
09/10/09 11:58
74-87-3
ND ug)L
1.0
1.0
1
09/10/09 11:58
124-48-1
NO uglL
1.0
1.0
1
09/10/09 1158
106.93-4
NO ugJL
1.0
1.0
1
09/10/09 11.58
95-50-1
NO uglL
1.0
1.0
1
09/1D/0911:58
541-73-1
NO ug/L
1.0
1.0
1
09110/09 11:58
106-46-7
NO uglL
1.0
1.0
1
09/1D10911:58
75-71-8
ND ug1L
1.0
1.0
1
09/10/09 11:58
75-34-3
NO uglL
1.0
1.0
1
09/10/09 11:58
107-06-2
ND ug1L
1.0
1.0
1
09/10/09 11:58
75-35-4
ND uglL
1.0
1.0
1
09/10/09 11:59
156-59-2
ND uglL
1.0
1.0
1
D9110109 11:58
156-60-5
ND uglL
1.0
1.0
1
09/10/09 11:58
78-87-5
NO uglL
1.0
1.0
1
09/10/09 11:58
10061-01-5
NO ug1L
1.0
1.0
1
09/10/09 11:58
10061-02-6
NO ugIL
1.0
1.0
1
09/10/09 11:58
108-20.3
NO ug1L
1.0
1.0
1
09/10/09 11:58
100-41-4
NO ug/L
2.0
2.0
1
09/10/09 11:58
75-09-2
NO uglL
1.0
1.0
1
09/10/09 11:58
1634-04-4
NO ug/L
2.0
2.0
1
09/10109 11:58
91-20-3
NO uglL
1.0
1.0
1
09/10/09 11:58
79-34-5
23.8 uglL
1.0
1.0
1
09110109 11:58
127-18-4
NO uglL
1.0
1.0
1
09/10/09 11:58
108-88-3
NO uglL
1 A
I Z
1
0911 D/D9 11:58
71-55-6
ND ug1L
1.0
1.0
1
09110/09 11:58
79-00-5
ND uglL
1.0
1.0
1
09110/09 11:58
79-01-6
ND uglL
1.0
1.0
1
09/10/09 11.58
75-69-4
NO uglL
1.0
1A
1
09110/09 11:58
75-01-4
NO uglL
2.0
2.0
1
0911 D109 11:58
1330-20-7
NO uglL
2.0
2.0
1
09/10/09 11:58
1330-20-7
NO ug1L
1.0
1.0
1
09/10/09 11:58
95-47-6
94 %
70-130
1
09/10/09 11:58
460.00-4
105 %
70-130
1
09110/09 11.58
1868-53-7
105 %
70-130
1
09/10/09 11:58
17060-07-0
99 %
70-130
1
09/10/09 11:58
2037.26-5
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full.
without the written consent of P300 A�naiyticaI Services, Inc,.
Page 9 of 21
aceAnalyticai�
wwwpOuela6s.com
Project: GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services. Inc.
98DO KinoeyAve. Suite 100
Huntersville, NC 28078
(744)875-9092
Sample: MIN-23D Lab ID: 9252397006 Collected: 09/02/09 09:03 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Quaff
6011602 Volatiles by SM 6200 Analytical Method: SM 6200B
Benzene
2.7 ug1L
2.0
2.O
2
09/10/09 12:22
71-43-2
Bromodichioromethane
NO uglL
2.0
2.0
2
09/10/09 12:22
75-27-4
Bromoform
NO uglL
2.0
2.0
2
09/10109 12:22
75-25-2
Bromemethane
NO uglL
2.0
2.0
2
09/1010912:22
74-63-9
Carbon tetrachloride
ND uglL
2.0
2.0
2
09/10/09 12:22
56-23-5
Chlorobenzene
NO uglL
2.0
2.0
2
09/10/09 12:22
108-90-7
Chloroethane
ND uglL
2.0
2.0
2
09/10/09 12:22
75-00-3
Chloroform
NO uglL
2.0
2.0
2
09/10/09 12:22
67-66-3
Chloromethane
NO uglL
2.0
2.0
2
09110/09 12:22
74-87-3
Dibromochioromethane
NO ug&
2.0
2.0
2
09/10/09 12.22
124-48-1
1,2-Dibromoethane (EDB)
ND uglL
2.0
2.0
2
09/10/09 12:22
106-93-4
1,2-Dichlorobenzene
ND uglL
2.0
2.0
2
09/10/09 12:22
95-50.1
1,3-Dichiorobenzene
ND uglL
2.D
2.0
2
09/10/09 12:22
541-73-1
1,4-Dichiorobenzene
ND ug1L
2.o
2.0
2
D911010912:22
106-46-7
Dichlorodifluoromethane
NO uglL
2.0
2.0
2
09/1010912:22
75-71-8
1.1-Dichloroethane
NO uglL
2.0
2.O
2
09/1010912:22
75-34-3
1.2-Dichloroethane
NO uglL
2.0
2.0
2
09/10/09 12:22
107-06-2
1,1-Dichloroethene
NO uglL
2.0
2.0
2
09110/0912:22
75-35-4
cis- 1,2-Dichloroethene
140 uglL
2.0
2.0
2
0911010912:22
156-59-2
trans-1,2-Dichloroethene
ND uglL
2.0
2.0
2
09/10/09 12:22
156-60-5
1,2-Dichloropropane
ND uglL
2.0
2.0
2
09110/091222
78-87-5
cis-1.3-Dichioropropene
ND uglL
2.0
2.0
2
09/10/09 12:22
10061-01-5
trans-1,3-Dichloropropene
ND uglL
2.0
2.0
2
09110/0912:22
10061-02-6
Diisopropyl ether
6.4 uglL
2.0
2.0
2
09/10/09 12:22
106-20-3
Ethylbenzene
NO ug1L
2.0
2.0
2
09/10/09 12:22
100-41-4
Methylene Chlonde
NO uglL
4.0
4.0
2
D9110109 12:22
75-09-2
Methyl -tent -butyl ether
317 uglL
2.0
2.0
2
09/10109 12:22
1634-04-4
Naphthalene
NO uglL
4.0
4.0
2
09/10/09 12:22
91-20-3
1.1,2,2-TetrachIoroethane
NO ug1L
2.0
2.0
2
09/10/09 12:22
79-34-5
Tetrachloroethene
ND uglL
2.0
2.0
2
09/10/09 12:22
127.18-4
Toluene
ND uglL
2.0
2.0
2
09/1010912:22
109-88-3
1.1,1-Tichloroethane
NO ug1L
2.0
2.0
2
09/1010912:22
71-55-6
1,1.2-ThchIoroethane
ND uglL
2.0
2.0
2
09/10/09 12:22
79-00-5
Trichloroethene
ND uglL
2.0
2.0
2
09/10/09 12:22
79-01-6
TnchOrofluoromethane
N❑ uglL
2.0
2.0
2
09/10/09 12:22
75-69-4
Vinyl chloride
23.5 uglL
2.0
2.O
2
09/10109 12:22
75-01-4
Xylene (Total)
ND uglL
4.0
4.0
2
09/10/09 12:22
1330-20-7
m&p-Xylene
ND uglL
4.0
4.0
2
09110/09 12:22
1330-20-7
o-Xylene
NO uglL
2.0
2.0
2
091101D912:22
9547-6
4-Bromefluorobenzene (S)
94 %
70-130
2
09/10/09 12:22
46MO-4
Dibromofluoromethane (S)
100 %
70-130
2
09110/09 12:22
1868-53-7
1,2-Dichloroethane-d4 {Sj
101 %
70-130
2
09/10/09 12:22
17060-07-0
Toluene -dB (S)
100 %
70-130
2
09/10/09 12:22
2037-26-5
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS Page 10 of 21
This report shall not be reproduced, except in full,
without the written can sent of Pace Ana Services, Inc.,
j�
. ditns r
t 6Analytical"
wwwp::csfabs.mm
Project: GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services. Inc.
2225 Riverside Dr -
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Paco Analytical Services, Inc.
9800 Kin cey Ave. Suits 100
Huntersville, NC 28078
(7041075-9092
Sample: MW-24 Lab ID: 9252397007 Coiiected: 09/02/09 12:56 Received: D9103109 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No, Qual
6011602 Volatlles by SM 6200
Benzene
Bromod ich lorometha n e
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichl prod ifl uo rometha n e
11-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethane
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropro pane
cis-1,3-Dichloropropene
trans- 1, 3-Dich lompropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1,1.2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,11-Trichloroethane
1,1,2-Trichloroethene
Tdchloroethene
Trich loroflu orometh a ne
Vnyl chloride
xylene (Total)
m&p-Xylene
o-xylene
4-Bromofluorobenzene (S)
Dibromofluoromethane [S]
1,2-0ichloroethane-d4 (S)
Toluene-d8 {S)
Date: 09/14/2009 09:56 AM
Analytical Method: SM 6200B
537 ug/L
5.0
5.0
5
09/10/09 12:46
71-43-2
ND ug1L
5.0
5.0
5
09/10109 12:46
75-27-4
ND ug)L
5,0
5.0
5
09110109 12:46
75.25-2
NO ug1
5.0
5,0
5
09/10/09 12:46
74-83-9
ND ug/L
5.0
5.0
5
09110/09 12,46
56-23-5
NO ug/L
5.0
5.0
5
09/10/09 12:46
108-90-7
NO ug/L
5.0
5.0
5
09/10/09 12:46
75-00-3
N❑ ug/L
5.0
5.0
5
09/10/09 12.46
67-66-3
ND uglL
5.0
5.0
5
09110/0912:46
74-B7-3
ND uglL
5.0
5.0
5
09/10/091Z46
124-48-1
ND ug/L
5.0
5.0
5
09/10/09 12:46
106-93-4
NO ug/L
5.0
5,0
5
09/10109 12:46
95-50-1
NO ug/L
5.0
5.0
5
D9110109 12:46
541-73-1
NO ug1L
5.0
5.0
5
09/10/09 12,46
106-46-7
ND uglL
5.0
5,0
5
09/10/09 12:46
75-71-8
6.2 ug/L
5.0
5.0
5
09/10/09 12:46
75-34-3
ND ug/L
5.0
5.0
5
09/10/09 12:46
107-06-2
9.7 uglL
5.0
5,0
5
09110/09 12:46
75-35-4
760 uglL
5.0
5.0
5
09/10/09 12:46
156-59-2
NO ug/L
5.0
5.0
5
09/10/09 12:46
156-60-5
NO ug/L
5.0
5.0
5
09/10/09 12:46
78-87-5
ND uglL
5.0
5.0
5
09/10/09 12:46
10061-01-5
ND uglL
5.0
5.0
5
09/10/09 12:46
10061-02-6
165 ugIL
5.0
5.0
5
09/10/09 12.46
108.20-3
NO ugfL
5.0
5.0
5
09/10/09 12,46
100-414
ND uglL
10.0
10.0
5
09/10/09 12.46
15-09-2
77.5 uglL
5.0
5.0
5
09/10/09 12:45
1634-04-4
15.5 uglL
10.0
10.0
5
09/10/09 12:46
91-20-3
NO ug/L
5.0
5.0
5
09/10/09 12:46
79-34-5
946 ug/L
50.D
50.0
50
09/11109 13:50
127-18-4
ND ug/L
5.0
5.0
5
09/10/09 12:46
108-88-3
ND ug/L
5.0
5.0
5
09/10/09 12:46
71-55-6
ND uglL
5.0
5.0
5
09/10/09 12:46
79-00-5
127 uglL
5.0
5.0
5
09/10109 12:46
79-01-6
32.0 uglL
5.0
5.0
5
09/10/09 12:46
75-69-4
121 uglL
5.0
6.0
5
09/10/09 12:46
75-01-4
13.7 uglL
10.0
10.0
5
09/10/09 12:46
1330-20-7
NO uglL
10.0
10.0
5
09/10/09 12:46
1330-2D-7
11.1 uglL
5.0
5.0
5
09/1010912:46
95-47-6
100 %
70-130
5
09/1010912:46
460-00-4
94 %
70-130
5
09/10/09 12:46
1868-53-7
94 %
70-130
5
0911010912:46
17060-07-0
97 %
70-130
5
09/10/09 12:46
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written can sent
�of PPa�ajjce�eAnalytical Services, Inc.
;`:.
Page 11 of 21
ace Analytical
e
ww pacelabs.eam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28004
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services. Inc.
9M Kincey Ave. Suite 100
Huntersvilie, NC 28078
(704)875-9092
Project: GILBARCD 97746
Pace Project No.: 9252397
Sample: MW-25 Lab ID: 9252397008 Collected: 09/02/09 13:00 Received: 09/03/09 13.38 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
601/602 Volatiles by SM 6200
Benzene
Bromodi ch lof o metha n e
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Di bromochl orometh an e
1,2-Dibromoethane (EDB)
1,2-Dichforobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
❑ ichl orodifl u oromethane
1,1-Dichloreethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Diisopropyf ether
Ethylbenzene
Methylene Chloride
Methyl-tert-bury! ether
Naphthalene
1,1,2,2-Tetrachtoroethane
Tetrachloroethene
Toluene
1,1,1-T6chloroethane
1,1,2-Trichtoroethane
Trichloroethene
Tri ch loroflu oromet h ane
Vinyl chloride
Xylene (Totaf)
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (5)
Dibromofluoromethane (S)
1,2-Dichloroethene-d4 (S)
Toluene-d8 (S)
Date: 09/14/2009 09:56 AM
Analytical Method: SM 6200B
ND ug/L
1.0
ND ug/L
1.0
N❑ ug/L
1.0
ND ugIL
1.0
N❑ ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
N ❑ ug/L
1.0
Nil ug/L
1.0
ND ugIL
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
N❑ ug/L
1.0
1.1 ug/L
1.0
N❑ ug/L
1.0
1.6 ugIL
1.0
60.1 ugIL
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1,0
N❑ ug/L
1.0
9.1 ug/L
1.0
ND ug/L
1.0
N❑ ug/L
2,0
8.9 ug/L
1.0
ND ug/L
2.0
ND ug/L
1.0
24.8 ugIL
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
7.9 ug/L
1.0
ND ug/L
1.0
N❑ ug/L
1.0
N❑ ugIL
2.0
ND ug/L
2.0
ND ug/L
1.0
94 %
70-130
103 %
70-13D
102 %
70-130
99 %
70-130
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.D
1.0
1.0
1.0
1.0
1.0
2.0
1.0
2.0
1.0
1.0
I'D
1.0
1.0
1.0
1.0
1.0
2.0
2.0
1.0
i
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.,
09/101091109
7143-2
09/10/0913*09
75-27-4
09110/0913:09
75-25-2
09/1010913.09
74-83-9
09/10/09 13:09
56-23-5
09/10/09 13:09
108-9 0-7
09/10/09 13:09
75-00-3
09/10/09 13:09
67-66-3
09110/0913:09
74-87-3
0 9110109 13:09
124-48 -1
09/10/09 13:09
106-93-4
09/1010913:09
95-50-1
09/10/09 13:09
541-73-1
09110109 13:09
106-46-7
091101D913.09
75-71-8
09/1010913:09
75-34-3
D9110109 13:09
107-06-2
09/10/09 13:09
75-35-4
D9110109 13:09
156-59-2
09/10/09 13:09
156-60-5
09110/0913:09
78-87-5
09110/0913:09
10061-01-5
09/10/09 13:09
10061-D2-6
09/10/09 13:09
108-20-3
09110109 13:09
1 DO-41-4
09/10/0913:09
75-09-2
09/10/09 13:09
1634-04-4
09/10/09 13:09
91-20-3
0911010913:09
79-34-5
09/10/09 13:09
127-1 B-4
09/10/09 13: 09
108-88 -3
09/10/091109
71-55-6
09110/0913:09
79-00-5
09/10109 13: D9
79-01-6
09/1010913:09
75-69-4
091101091109
75-01-4
D9110109 13:09
1330-20-7
09110/0 9 13:09
13 30-2 0-7
09/1010913:09
95-47-6
09/10/0913,09
460-00-4
09110109 13:09
186 8.5 3-7
09/10/09 13:09
17060-07-0
09/10/09 13:09
2037-26-5
Page 12 of 21
aceAnaly4lcal"
wwPwvh ba.00m
Project: GILBARCD 97746
Pace Project No.: 9252397
Pace Analytical Services. Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Knoey Ave. Suite 100
Huntersville, NC 28078
t704j875-9D92
Sample: MW-42 Lab ID: 9252397009 Collected, 09/02/09 14.52 Received: 09/03/09 1138 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
6011602 Volatiles by SM 6200
Benzene
Bromod i ch is ro metha n e
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloraethane
Chloroform
Chloromethane
Di b rom o chl orometh an e
1,2-Dibromoethane (EDB)
12-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
❑i chi orodifl u oromethane
1.I-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichforoethene
1.2-DichIoropropane
cis-1,3-Dichioropropene
trans- 1, 3-Di ch lorop ropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1.1,1-TrichIoroethane
1,1,2-Trichloreethane
Trichloroethene
Trich lorofl uo ro methan e
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
4-Bromoflucrobenzene (S)
Dibromofluaromethane (S)
1.2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/14/2009 09:56 AM
Analytical Method, SM 6200B
NO ug/L
1.0
1.0
1
09/10/09 13.33
7143-2
NO ug[L
1.0
1.0
1
09/10/09 13:33
75-27-4
Na uglL
1.D
1.0
1
09/10/09 13:33
75-25-2
NO ug/L
1.0
1.0
1
09110/09 13:33
74-83-9
NO ug1L
1.0
1.0
1
09/10/09 13:33
56-23-5
NO ug/L
1.0
1.0
1
09110/09 13:33
108-90.7
NO ug/L
1.0
1.0
1
09/10/09 13:33
75-00-3
NO uglL
1.0
1.0
1
09/10/09 13:33
67-66-3
ND uglL
1.0
1.0
1
09/10/09 13:33
74-87-3
NO uglL
1.0
1.0
1
09/10/09 13:33
124.48-1
NO uglL
1,0
1.0
1
09/10/09 13:33
106-93-4
ND uglL
1.0
1.D
1
09/10/09 13:33
95.50-1
ND ug/L
1,0
1.0
1
09/10/09 13:33
541-73-1
NO ug/L
1.0
1.0
1
D9110109 13:33
106-46-7
ND uglL
1.0
1.0
1
09/10/09 13:33
75-71-8
NO uglL
1.0
1.0
1
09/10/09 13:33
75-34-3
ND uglL
1.0
1.0
1
09/10/09 13:33
107-06-2
ND uglL
1.0
1.0
1
09110/09 13:33
75,35-4
ND ug1L
1.0
1.0
1
09/10/09 13:33
156-59-2
NO ug1L
1.0
1.0
1
09110/09 13:33
156-60-5
NO ug/L
1.0
1.0
1
09/10/09 13:33
78-87-5
NO ug/L
1.0
1.0
1
09/10/09 13:33
10061-01-5
NO uglL
1.0
1.0
1
09/10/09 13:33
10061-02-6
NO uglL
1.0
1.0
1
09/10/09 13:33
108-20-3
ND uglL
1.0
1.0
1
09/10/09 13:33
100414
ND uglL
2.0
2.0
1
09/10/09 13.33
75-09-2
ND uglL
1.0
1.0
1
09/10/09 13:33
1634-04-4
NO uglL
2.0
2.0
1
09/10/09 13:33
91-20-3
ND ug1L
1.0
1.0
1
09/10/09 13:33
79-34-5
3.4 ug1L
1.0
1.0
1
09/10/09 13:33
127-18-4
NO ug/L
1.0
1.0
1
09/10109 13:33
108-88-3
NO uglL
1.0
1.0
1
09/10/09 13:33
71-55-6
NO uglL
1.D
1.0
1
D9/10/09 13:33
79-00-5
ND uglL
1.0
1.0
1
09/10/09 13:33
79-01-6
ND uglL
1.0
1.0
1
D9/10/09 13:33
75-69-4
ND ug1L
1.0
1.0
1
09/10/09 13:33
75-01-4
ND ug1L
2.0
2.0
1
09110/09 13:33
1330-20-7
NO ug1L
2.0
2.0
1
09/10/09 13:33
1330-20-7
NO ug/L
1.0
1.0
1
09/10/09 13:33
95-47-6
94 %
70-130
1
09110/091&33
460-00-4
105 %
70-130
1
09/10/09 13:33
1B66-53-7
104 °%
70-130
1
09/10/09 13:33
17060-07-0
100 %
70-130
1
0911D109 13:33
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written ccnsont of Parse Analytical Services, Inc..
Page 13 of 21
e
ace Analjftal
www.pacalebs.00m
Project: GILBARCQ 97746
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
i828y254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
(764)875-9092
Pace Project No.. 9252397
Sample: MW-43D Lab ID: 9252397010 Collected: 09/02/09 14:48 Received: 09/03/09 13:36 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
60111602 Volatlles by SM 6200 Analytical Method: SM 6200B
Benzene
3.0 uglL
2.0
2.0
2
09110109 13:57
71-43-2
Bromodichlaromethane
NO uglL
2.0
2.0
2
09110/09 13:57
76.27-4
Bromoform
ND uglL
2.0
2.0
2
09110/09 13:57
75-25-2
Bromomethane
NO uglL
2.0
2.0
2
09/1010913:57
74-83-9
Carbon tetrachloride
NO uglL
2.0
2.0
2
09110/09 13:57
56-23-5
Chlorobenzene
NO uglL
2.0
2.0
2
09110109 13:57
108-90-7
Chloroethane
NO ug1L
2.0
2.0
2
09/10/09 13:57
75-00-3
Chloroform
ND ug1L
2.0
2.0
2
09/10/09 13:57
67-66-3
Chloromethane
3.8 uglL
2.0
2.0
2
09/10/09 13:57
74-87-3
Dibromochlaromethane
ND ug1L
2.0
2.0
2
09/10/09 13:57
124-48-1
1,2-Dibromoethane (EDB)
ND uglL
2.0
2.0
2
09/10/09 13:57
106-93-4
1,2-Dichiorobenzene
NO uglL
2.0
2.0
2
09/1010913:57
95-50-1
1,3-Dichiorobenzene
NO uglL
2.0
2.0
2
09/1D10913:57
541-73-1
1,4-Dichlorobenzene
NO uglL
2.0
2.0
2
0911010913:57
106-46-7
Dichlarodifluoromethane
ND ug1L
2.0
2.0
2
09/10/09 13:57
75-71-8
1,1-Dichloroethane
3.9 ug1L
2,0
2.0
2
09/10/09 13:57
75-34-3
1,2-Dichloroethane
ND uglL
2.0
2.0
2
09/10/09 13.57
107-06-2
1,1-Dichloroethene
13.9 ug1L
2.0
2.0
2
09/10/09 13:57
75-354
cis-1,2-Dichloroethene
99.4 uglL
2.0
2.0
2
0911010913.57
15&59-2
trans-1,2-Dichloroethene
NO uglL
2A
2.0
2
09/10/09 13:57
156-60-5
1.2-Dichlorapropane
NO uglL
2.0
2.0
2
09/10109 13:57
78-87-5
cis- 1,3-Dichloropropene
NO uglL
2.0
2.0
2
09110/0913:67
10061-01-5
trans-1,3-❑ichforopropene
ND uglL
2.0
2,0
2
0911010913:57
10061-02-6
Diisopropyl ether
29.9 uglL
2.0
2.0
2
09/10/09 13:57
108-20-3
Ethylbenzene
NO uglL
2.0
2.0
2
09/10/09 13:57
100-41-4
Methylene Chloride
ND ug1L
4.0
4.0
2
0911 D109 13:57
75-09-2
Methyl -tent -butyl ether
16.7 uglL
2.0
2.0
2
09/10/09 1157
1634-04-4
Naphthalene
NO uglL
4.0
4,0
2
09/10/09 13:57
91.20-3
1.1.2.2-Tetrachloroethane
NO uglL
2.0
2.0
2
09/10/09 13:57
79-34-5
Tetrachloroethene
337 uglL
2.0
2.0
2
09/10/09 13:57
127-18-4
Toluene
N❑ uglL
2.0
2.0
2
09/10/09 13:57
108-88-3
1, 1,1 -Trichloroethane
ND uglL
2.0
2.0
2
09110/09 13:57
71-55-6
1,1,2-Trichi Oroethane
ND uglL
2.0
2.0
2
09110/09 13:57
79-00-5
Trichloroethene
11.4 uglL
2.0
2.0
2
09110/09 13:57
79-01-6
Trichlorofluoromethane
3.7 uglL
2.0
20
2
09110/09 13:57
75-69-4
Vinyl chloride
ND ug1L
2.0
2A
2
09/10/09 13:57
75-01-4
Xylene (Total)
ND ug1L
4.0
4.0
2
09110/09 13:57
1330-20-7
m&p-Xylene
NO uglL
4.0
4.0
2
09/1010913:57
1330-20-7
0-Xylene
N❑ uglL
2.0
2.0
2
09/10/09 13.57
95-47-6
4-Bromofluorobenzene (S)
95 %
70-130
2
09/10/09 13:57
460.00-4
❑ibromofluoromethane (S)
103 %
70-130
2
09/10/09 13:57
1868-53-7
1,2-Dichloroethene-d4 (S)
102 %
70-130
2
09/10/09 13:57
17060-07-0
Toluene-d8 (S)
101 %
70-130
2
0911 D109 13:57
2037-26-5
❑ate: 09114/2009 09,56 AM REPORT OF LABORATORY ANALYSIS Page 14 of 21
This report shall not be reproduced, except in full,
w the Lit the written consent of PPaaceerAnalyliraI Services. Inc..
aceAnalytical
V, paceiaba.aom
Project: GILBARCO 97746
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
Pace Project No.: 9252397
Sample: MW-45 Lab ID: 9252397011 Collected: 09/02/09 15:05 Received: 09/03/09 13:38 Matrix: Water
(704)975-9092
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
6011602 Volatiles by SM 6200 Anatytical Method' SM 62008
Benzene
ND ug1L
1.0
1.0
1
09/10109 14:20
71-43-2
Bromodichloromethane
ND uglL
1.0
1.0
1
09/10/09 14:20
75-27-4
Bromoform
ND ug1L
1.0
1.0
1
09/10109 14:20
75-25-2
Bromomethane
NO uglL
1.0
1.0
1
09/10/09 14:2D
74-83-9
Carbon tetrachloride
NO ug1L
1.0
1.0
1
09/10/09 14 20
56-23-5
Chlorobenzene
ND ug1L
1.0
1.0
1
09/10/09 14:20
108-90-7
Chloroethane
ND uglL
1.0
1.0
1
09110/09 14:20
75-00-3
Chloroform
ND uglL
1.0
1.0
1
09110/09 14:20
67-66-3
Chloromethane
ND uglL
1.0
1.0
1
09/10/09 14:20
74.87.3
Dibromochloromethane
ND uglL
1.0
1.0
1
09/10/09 14:20
124-48-1
1,2-Dibromoethane (EDB)
NO uglL
1.0
1.0
1
09/10/09 14:20
106-93-4
1,2-Diohlorobenzene
NO uglL
1.0
1.0
1
09110/0914:20
95-50-1
1,3-Dichlorobenzene
NO uglL
1.D
1.0
1
09/10/09 14:20
541-73-1
1,4-Dichlorobenzene
NO uglL
1.0
1.0
1
09/10/09 14:20
106-46-7
Dichlorodifluoromethane
NO uglL
1.0
1.0
1
09110M9 14:20
75-71-8
1,1-Dichloroethane
NO uglL
1.0
1.0
1
09/10/09 14:20
75-34-3
1,2-Oichloroethane
ND uglL
1.0
1.0
1
09/10/09 14:20
107-06-2
1,1-Dichloroethene
ND uglL
1.0
1.0
1
09/10/09 14:20
75-35-4
cis-1,2-Dichtoroethene
ND uglL
1.0
1.0
1
09/10/09 14:20
156-59-2
trans-1,2-Dichloroethene
NO ug1L
1.0
1.0
1
D911010914:20
156-60-5
1,2-Dichloropropane
ND ug1L
1.0
1.0
1
09/10/0914.20
78-87-5
cis-1,3-Dichloropropene
NO uglL
1.0
1.0
1
09110/09 14:20
10061-01-5
trans-1,3-Dichloropropene
ND uglL
1.D
1.0
1
09/10/0914,20
10061-02.6
Diisopropyl ether
ND ug1L
1.0
1.0
1
09/10/09 14:20
108-20-3
Ethylbenzene
NO ug1L
1.0
1.0
1
09/10/09 14:20
100-41-4
Methylene Chloride
NO uglL
2.0
2.0
1
09/10/09 14:20
75-09-2
Methyl-tert-butyl ether
NO uglL
I.0
1.0
1
09/10/09 14;20
1634-04-4
Naphthalene
NO uglL
2.0
2.0
1
09/10/D9 14:20
91-20-3
1,1,2,2-Tetrachloroethane
NO ug/L
1.0
1.0
1
09/10/09 14:20
79-34-5
Tetra ch loroethe n e
2.4 uglL
1.0
1.0
1
09/10109 14:20
127-18-4
Toluene
NO ug1L
1.0
1.0
1
09/10/09 14:20
10"8-3
1,1,1-Trichloroethane
ND uglL
1.0
1,0
1
0911010914:20
71-55-6
1.1.2-Trichloroethane
NO ug1L
1.0
1.0
1
D911010914:20
79-00-5
Trichloroethene
1.1 uglL
1.0
1.0
1
0911010914:20
79-01-6
Trichlorofluoromethane
NO uglL
1.0
1.0
1
09/10/09 14:20
75-69-4
Vinyl chloride
NO uglL
1.0
1.0
1
09/10/09 14:20
75-01-4
Xylene (Total)
ND uglL
2.0
2.0
1
09/10/09 14:20
1330-20-7
m&p-Xylene
NO uglL
2.0
2.0
1
09110/09 14:20
1330-20-7
o-Xylene
ND uglL
1.0
1.0
1
09/10/09 14.20
95-47.6
4-Bromofluorobenzene (S)
90 p%
70-130
1
09/10/09 14:20
460-00-4
Dibromofluoromethane (S)
107 °%
70-130
1
09110/09 14:20
1868-53-7
1,2-Dichloroethane-d4 (S)
106 °fin
70-130
1
09/10/09 14:2D
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
09/10109 14:20
2037-26-5
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS page 15 of 21
This report shall not be reproduced, except in full,
without the written consent of Pace�e+�Analytical Services, Inc..
laceAnalXical"
www.pWalfiftom
i
Project: GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Or -
Asheville. NC 28804
(828)254-7176
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9600 KinceyAve. Suite 100
Huntersville, NC 2807B
(T04)875.9097
Sample: MW-14D Lab ID: 9252397012 Collected: 09/02/09 13:12 Received: 09/03/09 13:38 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No, Qua#
6011602 Volatfles by SM 6200
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
D i brorn ochl orom eth an e
1,2-Dibromoethane (EDB)
1 ,2 -Di ch lofobe n zen e
1,3-Dichlorobenzene
1,4•Dichlorobenzene
Di ch I o rodifl uorometh ane
1,1-Dichloroethane
1,2-Dichloroethane
1, 1 -Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis- 1,3-0ichlorop rope ne
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
1.1,2,2-Tetrachloroethane
Tetrachioroethene
Toluene
1,1,1-TrichIoroethane
1.1,2-TrichIoroethane
Trichloroethene
Tdch lorofl uoromethane
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/14/2009 09:56 AM
Analytical Method: SM 6200B
1.8 ug/L
1.0
1.0
1
09/10/09 14:44
71.43-2
ND ugIL
1.0
1.0
1
09/10/09 14:44
75-27-4
ND ug/L
1.0
1.0
1
09/10/09 14:44
75-25-2
ND ug/L
1.0
1.0
1
09/10/09 14:44
74-83-9
ND ug/L
1.0
1.0
1
09/10/09 14:44
56-23-5
NO ug/L
1.0
1.0
1
09/10/09 14:44
1OB-90-7
ND ug/L
1.0
1.0
1
09/10/09 14:44
75-00-3
ND ug/L
1.0
1.0
1
09/10/09 14:44
67-66-3
ND ugIL
1.0
1.0
1
09/10/09 14:44
74-87-3
ND ugIL
1.0
1.0
1
09/10/09 14:44
124-48-1
N❑ ugIL
1.0
1.0
1
09/10/09 14:44
106-93-4
ND ug/L
1.0
1.D
1
09/10/09 14:44
95-50-1
ND uglL
1.0
1.0
1
09/10/09 14:44
541-73-1
ND ug/L
1.0
1.0
1
09/10/09 14:44
106-46-7
ND ug/L
1.0
1.0
1
09/10/09 14:44
75.71-8
ND ug/L
1.D
1.0
1
09/10/0914:44
75-34-3
ND uglL
1.0
1.0
1
09/10109 14,44
107-06-2
NO ug/L
1.0
1.0
1
09/10/09 14:44
75-35-4
8.8 ug/L
1.0
1.0
1
D9110109 14:44
156-59-2
NO ug1L
1.0
1.0
1
09/10/09 14:44
156-60-5
ND ug/L
1.0
1.0
1
09/10/09 14:44
78-87-5
ND ug/L
1.0
1.0
1
09/10/09 14A4
10061-01-5
ND ug/L
1.0
1.0
1
09/10/09 14:44
10061-02-6
2.9 ug/L
1.0
1.0
1
09/10/09 14:44
108-20-3
ND ug/L
1.0
1.0
1
09/10/09 14:44
100-41-4
NO ug/L
2.0
2.0
1
09110/0914:44
75-09-2
1.3 ug/L
1.0
1.0
1
09/10/09 14:44
1634-04-4
NO ug/L
2.0
2.0
1
09/10/09 14:44
91-20-3
NO ug/L
1.0
1.0
1
09/10/0914:44
79-34-5
27.1 ug/L
ID
1.0
1
09/10109 14:44
127-18-4
ND uglL
1.0
1.0
1
09/10/09 14,44
108-88.3
ND ug/L
1.0
1.0
1
D9I1010914:44
71-55-6
ND ug/L
1.0
1.0
1
09/10/09 14:44
79-00-5
1.4 ug/L
1.0
1.0
1
09/10/09 14,44
79-01-6
NO ug/L
1.0
1.0
1
09/10/09 14:44
75-69-4
NO ug/L
1.0
1.0
1
09110/0914:44
75-01-4
NO ug/L
2.0
2.0
1
09/10/09 14:4.4
1330-20-7
ND ug/L
2.0
2.0
1
09/10/09 14A4
1330-20-7
ND ug/L
1.0
1.0
1
09/10109 14:44
95-47-6
93 °%
70-130
1
09/10109 14.44
460-00-4
105 %
70-130
1
09110/09 14:44
1868-53-7
104 %
70-130
1
09/10/09 14:44
17060-07-0
100 °%
70-130
1
09/10/09 14:44
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shaft not be reproduced, except in lull,
without the written con sent of PPaace
,AnalyticaI Services, Inc..
Ll�lf]11.._
Page 16 of 21
accAnaVical
wr -Vpa[r+faas.cro,r
Project: GILBARCO 97745
Face Project No.: 9252397
Pace Analytical Services, Inc,
2225 Riverside Dr.
Asheville, NC 28804
QUALITY CONTROL DATA
(828)254-7176
Pace Analytical Services, Inc.
9900 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
C1C Batch: MSV18220 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6011602 Volattles by SM 6200
Associated Lab Samples: 9252397001, 9252397002, 9252397003, 9252397004, 9252397005, 9252397006. 9252397007, 9252397008.
9252397009,9252397010,9252397011,9252397012
METHOD BLANK: 332963 Matrix: Water
Associated Lab Samples: 92523 97 001. 9252397002, 9252397003. 92 523 97004. 9252 39 7005. 92 5239 7006, 9252397007, 9252397008,
9252397009,9252397010,9252397011,9252397012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Tdchloroethane
uglL
ND
1.0
09/10/09 10:00
1,1,2,2-Tetrachloroethane
uglL
ND
1.0
09/10/0910:00
1,12-Tdchloroethane
uglL
ND
1.0
0911010910:00
1,1-Dichloroethane
uglL
ND
1.0
09110/0910:00
1,1-Dichloroethene
ug/L
NO
1.0
0911010910:00
1,2-Dibromoethane (EDB)
uglL
ND
1.0
09/10/09 10:00
1,2-Dichlorobenzene
uglL
N❑
1.0
09/10/0910:00
1,2-Dichloroethane
uglL
Nd
1.0
09/10/0910:00
1.2-Dichloropropane
uglL
NO
1.0
09110/09 10 :00
1,3-Dichlorobenzene
uglL
ND
1.0
09110/09 10., 00
1,4-Dichlorobenzene
ug1L
ND
1.0
0911010910:01)
Benzene
ug1L
NO
1.0
09110/0910:00
Bromodichloromethane
uglL
N❑
1.0
09/10/0910:00
Bromoform
ug1L
NO
1.0
09110/0910:00
Bromomethane
uglL
ND
1.0
09/1010910:00
Carbon tetrachloride
uglL
ND
1.0
09/10/0910:00
Chlorobenzene
uglL
ND
1.0
09/10/0910:00
Chloroethane
uglL
ND
1.0
09/10/0910:00
Chloroform
ug1L
ND
1.0
09/1010910:00
Chloromethane
ug/L
ND
1.0
09/10/0910:00
cis-1,2-Dichloroethene
uglL
ND
1.0
09/1010910.00
cis- 1,3-Dichioropropene
ug/L
NO
1.0
09/1010910:00
Dibromochloromethane
uglL
ND
1.0
09/1010910:00
Dichlorodifluoromethane
uglL
NO
1.0
09/1 DI09 10.00
Diisopropyl ether
uglL
NO
1.0
D9110109 10.00
Ethylbenzene
uglL
NO
1.0
0911010910:00
m&p-Xyiene
uglL
ND
2.0
0911010910:00
Methyl-tert-butyl ether
uglL
N❑
1.0
09/10/09 10:00
Methylene Chloride
ugIL
N❑
2.0
09/10/09 10:00
Naphthalene
ug1L
ND
2.0
09110/0910:00
o-Xylene
uglL
NO
1.0
09/10/0910:00
Tetrachtoroethene
ug/L
NO
1.0
09/10/0910:00
Toluene
ug/l_
ND
1.0
09/10/0910:00
trans-1,2-Dichloroetene
uglL
ND
1.0
09/1010910:00
trans-1,3-Dichloropropene
uglL
ND
1.0
09/10/0910:00
Trichloroethene
uglL
ND
1.0
09/1010910:00
Trichlorofluoromethane
uglL
NO
1.0
09/10109 10: 0 D
Vinyl chloride
uglL
NO
1.0
09110109 10:00
Xylene Jotaly
ug1L
NO
2.0
D9110109 10:00
1,2-Dichloroethane-d4 jSj
%
102
70-130
0911010910:00
4-Bromofluorobenzene (S)
%
97
70-130
09110/0910:00
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except +n full.
without the written conseni of Pace
+Analytical Services, Inc..
Page 17 of 21
aceAnalyfr'cal
WKWpacelaucam
Project: GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr -
Asheville. NC 28804
(828)254-7176
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
(704)875.9092
METHOD BLANK. 332963 Matrix: Water
Associated Lab Samples: 9252397001. 9252397002, 9252397003. 9252397004. 9252397005, 9252397DQ6, 9252397007, 9252397008,
9252397009,9252397010,9252397011,9252397012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Dibromofluoromethane (S) %
Toluene -dB (S) %
102 70-130 09/10/0910:00
102 70-130 09/10/0910:00
LABORATORY CONTROL SAMPLE:
Parameter
332964
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,11-Trichlaroethane
ug/L
50
49.6
99
60-140
1,12,2- Tetra chloroethane
ug/L
50
46.4
93
60-140
1,1,2-Trichtoroethane
ug/L
50
51.0
102
60-140
1,1-Dichloroethane
ug/L
50
48.8
98
60-140
1,1-1)ichloroethene
ug/L
50
50.3
101
60-140
1,2-Dibromoethane (EDB)
ug/L
50
55.2
110
60-140
1,2-Dichlorobenzene
ug/L
50
50.2
1 D0
60-140
1,2-Dichloroethane
ugIL
50
46.7
93
60-140
1,2-Dichlorapropans
ug/L
50
53.6
107
60-140
1,3-Dichlorobenzene
ug/L
50
49.7
99
60-140
1,4-Dichlorobenzene
ug/L
50
47.8
96
60-140
Benzene
uglL
50
49.9
100
60-140
Bromcdichloromethane
ug/L
50
49.6
99
60-140
Bromoform
ugIL
50
45.4
91
60-140
Bromomethane
ug/L
50
61.8
124
60-140
Carbon tetrachloride
ug/L
50
56.4
113
60-140
Chlorobenzene
uglL
50
51.7
103
60-140
Chloroethane
ug/L
50
47.5
95
60-140
Chloroform
ug/L
50
47.8
96
60-140
Chloromethane
ug/L
50
45A
92
60-140
cis-1,2-Dichloroethene
ug/L
50
52A
105
60-140
cis- 1,3-Dichloropropene
ug/L
50
55.4
111
60-140
Dibromochloromethane
ug/L
50
52.9
106
60-140
Dichlorodifluoromethane
ug/L
50
46.3
93
60-140
Diisopropyl ether
ug/L
50
48.8
98
60-140
Ethylbenzene
ugIL
50
51.3
103
60-140
m&p-Xylene
ug/L
100
104
104
60-140
Methyl-tert-butyl ether
ug1L
50
46.6
93
60-140
Methylene Chloride
ug/L
50
46.7
93
60-140
Naphthalene
ug/L
50
55.7
111
60-140
o-Xylene
ug/L
50
53A
107
60-140
Tetrachloroethene
ug/L
50
53.6
107
60-140
Toluene
ugIL
50
413.4
97
60-140
trans-1,2-01chloreethene
ug/L
50
47.2
94
60-140
trans-1,3-Dichloropropene
ug/L
50
53.7
107
60-140
Trichloroethene
ug/L
50
56.4
113
60-140
Tdchlorofluoromethane
ug/L
50
38.2
76
60-140
Vinyl chloride
ug/L
50
48.2
96
60-140
Date: 09114120D9 09:56 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 18 of 21
t
aceAnalylical
wwwpecelabs.cam
Project. GILBARCO 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kin coy Ave, Suite too
Huntersvilie, NC 28078
LABORATORY CONTROL SAMPLE'
332964
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Xylene (Total)
ugIL
150 157 105
60-140
12-❑ichtoroethane-d4 (S)
%
87
70-130
4-Bromofluorobenzene (S)
%
108
70-130
Dibromofluoromethane (5)
%
96
70-130
Toluene -dB (S)
%
99
70-130
(704)875-9092
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 332965
9252397011
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
332966
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
Max
RP❑ RPD Qual
1,1,1-Trichioroethane
ug/L
NO
20
20
23.3
23.0
116
115
60-140
1
30
1,1,22-Tetrachloroethane
ugIL
ND
20
20
23.6
22.3
118
112
60-140
5
30
1,1,2-Trichloroethane
ug/L
ND
20
20
23.4
22.8
117
114
60-140
2
30
1,1-Dichloroethane
ugIL
ND
20
20
23.4
22.5
117
112
60-140
4
30
1,1-Dichloroethene
ugIL
N❑
20
20
24.0
21.1
120
105
60-140
13
30
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
24.8
24.1
124
121
60-140
3
30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.9
22.5
110
112
60-140
3
30
12-Dichloroethane
ug/L
ND
20
20
22A
21.9
112
110
60-140
2
30
1,2-Dichloropropane
ug/L
NO
20
20
24.0
23.6
120
118
60-140
1
30
1,3-Dichlorobenzene
ugIL
ND
20
20
21.8
21.9
109
110
60-140
D
30
1,4-Dichlorobenzene
ugIL
NO
20
20
20.9
20.9
104
105
60-140
0
30
Benzene
ug/L
N❑
20
20
23.0
22.7
115
113
60-140
1
30
Bromodichloromethane
ug/L
NO
20
20
21.9
21.5
110
108
60-140
2
30
Bromeform
ug/L
NO
20
20
20.6
20.1
103
100
60-140
3
3D
Bromomethane
ug/L
NO
20
20
23.4
25.8
117
129
60-140
10
3D
Carbon tetrachloride
ug/L
ND
20
20
25.0
24.8
125
124
60-140
1
30
Chlorobenzene
ug/L
NO
20
20
23.0
22.7
115
113
6D-140
1
30
Chloroethane
ug/L
ND
20
20
22.9
23.6
114
118
60-140
3
30
Chloroform
ug/L
NO
20
20
22.5
21.8
113
109
60-140
3
30
Chloromethane
ugIL
ND
20
20
21.5
21.5
107
108
60-140
0
34
cis-1,2-Dichloroethene
ug/L
ND
20
20
25.1
24.9
123
121
60-140
1
30
cis-1,3-Dichloropropene
ug/L
N❑
20
20
21.2
20.8
106
104
60-140
2
30
Dibromochloromethane
ug/L
ND
20
20
23.3
22A
117
112
60-140
4
30
Dichlorodifluoromethane
ugIL
ND
20
20
23.8
23.1
119
116
60-140
3
30
Diisopropyl ether
ug/L
NO
20
20
22.2
21.8
111
109
60-140
2
30
Ethylbenzene
ug/L
ND
20
20
22.5
22.6
113
113
60-140
0
30
m&p-Xylene
ug/L
ND
40
40
42.3
41.8
106
105
60-140
1
30
Methyl-tert-butyl ether
ug/L
ND
20
20
21.6
20.7
108
104
60-140
4
30
Methylene Chloride
ug/L
NO
20
20
20.7
20.0
104
100
60-140
3
30
Naphthalene
ug/L
NO
20
20
21,0
23.7
105
119
60-140
12
30
o-Xylene
ug/L
ND
20
20
22.1
22.3
111
111
60-140
1
30
Tetrachlaroethene
ug/L
2.4
20
20
25.1
25.0
113
113
60-140
0
30
Toluene
ugIL
NO
20
20
22.0
21.7
110
108
60-140
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.7
21.5
108
108
6D-140
1
30
trans-1,3-Dichloropropene
uglL
ND
20
20
20.2
20.3
101
101
60-140
0
30
Trichloroethene
ug/L
1.1
20
20
26.3
25.8
126
124
60-140
2
30
Trichlorofiuoromethane
ug/L
N❑
20
20
21.1
18.6
105
93
60.140
13
30
Date: 09/14/2009 09:56 AM REPORT OF LABORATORY ANALYSIS Page 19 of 21
This report shall not be reproduced, except in full,
without the written consent of�Pace
rAnalytical Services, Inc
aceAnalXical
www.pac+afahs.00m
i
Project: GILBARCC 97746
Pace Project No.: 9252397
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)254-7176
QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 332965
MS
9252397011 Spike
Parameter
Un€ts Result Conc.
Vinyl chforide
ug/L N❑ 20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
Date. 09/14/2009 09:56 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
332966
MSD
Spike MS
MSD MS
MSD
% Rea Max
Conc. Result
Result % Rec
% Rec
Limits RPD RPD Gual
20 23.2
23.7 116
119
60-140 2 30
94
91
70-130
103
105
70-130
101
99
70-130
98
98
70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�fi^aeh
Page 20 of 21
r, Pace Analytical Services, Inc, Pace Analytical Services, Inc.
/1� laceAnayical 2225 Riverside 0r.9800 ICinceyAve. Suite 1D0
www.pacalabs cam Asheville, NC 288D4 Huntersvilie, NC 28078
QUALIFIERS
Project: GtLBARCO 97746
Pace Project No,: 9252397
DEFINITIONS
(828)254-7176
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1.2-❑ipheny1hydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with FPA guidelines, unrounded data are displayed and have been used to calculate Io recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
(704)875-9092
Date: 09/14/2009 09 56 AM REPORT OF LABORATORY ANALYSIS Page 21 of 21
This report shall not be reproduced. except In full,
Without the written consent of Pace Analytical Services, Inc..
cv*��
�'aC2Ark?lyfrra!
Section A
Required Client Information:
Section B
Required Project information
CHAIN -OF -CUSTODY ! Analytical Request Document
The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information:
Pane : 1 Of
Company Klelnfelder
Report To. Gail Lica an
Altenliun Gail Lica an
Address 313 Gallimore Dairy Rd
Copy To
Company Name Kleinfelder
Greensboro, NC 27409
Address. 313 Gallimare Dairy Rd, Greensboro, N
Regulatory A errs
Email To glicayan@kleinfelder.com
Purchase Order No
Pace Quote Reference:
Phone (336) 668.0093 FaX
Client Project I❑ GILBARCO 97746
Pace Project Manager McKee, Bonnie
8feH1 L"N"a
Requesled Due Date1TAT 10 Da Default
Container Order Number
Pace Profile 4
North Carolina
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WT
G
912109
91b
1
3
X
X
4
MW-13D
WT
G
9l2M9
-166
1
3
x
X
6
MW-14
WT
G
912*9
f
3
x
x
6
MVV•14O
WT
G
WM9
3
x
k
7
MW73D
WT
G
912109
3
1
1
1
X
I
I
X
8
MW-24
WT
G
912109 11V5CP
3
x
x
9
MW-25
WT
G
91209
3
x
x
10
MWA2
WTI
G
912109
3
I
I
%
I
I
I
X
11
JMWA3D
WT
G
912109
3
I
I
x
%
12
MWA5
WTI
G
1 912109
1`1,561
1
x1+�fl
](
ADDITIONAL COMMENTS RELINQUISHED BY) AFFtUATION
DATE
TOE
ACCEPTER BY IARFZ♦.IAMON
DATE
TIME
SAMPLE CRNDRIQNS
SAMPLERNAME AND SIGNATURE
`m
x
a
PRINT Name of SAMPLER:
Gail Lica an
11m
w
m d
Fa m
m ?
SIGNATURE of SAMPLER:
DATE Signed (I
tr u
5 w r
rn ?
APPENDIX B
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-7
t Total VOCs
0 Chlorinated VOCs
n
15,000 0
n
10,000 t
m
1-1
1�0 h ao '0 '0 � �0 *Q %0 7b �y
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-11
imc
:ir
600 0
n
ro
m
400
m
- T 7 rl- 0
Llo
7 �s 79 ri'9 �0 %> 7 0 �l0 rl'0 h'0 ri3O r1'0 *� 7o 7 �i�
0 '00 r0
'90 r r' u' s '�s j 8 �9 0 r 2 U' � S g5' � � .9
Data
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-13
m
w
N
r-
400 'Fl
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-13D
--- 1,000
—+ Total VOCs
+ Chlorinated VOCs
Date
m
600 0
n
co
4
w
400 �
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-14
15,000 o
n
m
3
io
io
111
t!0 ` [lq} t/� vlo Jl G/� �!� , v� , t/� t/� ' �� , �� c% v� ` ✓1 , v� s /� cf� t�� Vlo
'0 �i9 'y9 �9 h �� �9 �9 �0 p '�0 �7 h p r1, `i'0 �o �0 r
r 2 � 'fir S `�S � S 9 �D r � � �u S � � S 9 0
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-14D
WE
m
600 q
n
In
CD
m
400
Date
D
N
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-23D
m
600 Q
n
m
s
7
co
400 T
a]
a
v� v� , `'iQ' v�, vl `l` `�Q' `� `��' `lql `iQ' v� ✓1 c% `rQ' `lq `ro'' c% vq s/o v�
�i �g o �9 ri, �0 f!, �9 � '0 h0 �0 70 �i p �0 f!, �D �0 r
`� �' 2 cr `Qsr S `�5' � 8 � � T c� cs� � S �6' � � �i9 D
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-24
1 'TyT,
15,000 0
m
n
m
m
11,
411
191
ri,9 ri,�,� �9 h9 7o '� ADD �0 �i0 'D �o �0Q '�
`9D i tp 19 S E '�9 O ! u� F S Db' Dig D
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-25
— Total VCCs
0 Chlorinated VOCs
+2
Elio]
600 0
n
ca
3
m
0
IA
400
200
F,
L10
�� �9 �,� �s %� �o �a �� 7� po o r
'$� r 2 '�Sz s '�S S °o r 0sr S S 09 a
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-42
m
:m
600 0
3
n
tp
w
O
N
400
C
vQI ✓� J� ✓� v4, v� vpv� v�, v� v� vo 1
1 ✓1 ,P c% v4, vl 110 c%, v1
�0 �o �.0 �0 79 fi, 7.0 fi, �� fi, '}0 ri0 0 o 7o ri' n0 ri' , r
90 r 2 1? Q S � > `Sip �9 0o r 2 0 u S 06 > 0cP 09 0
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-43D
t Total VOCs
+Chlorinated VOCs
Teti
E 1+I0]
600 0
n
m
N
b
7
N
400
A
10f
V91
1/1�
'� �19 �91 90 '9v �'9s `'�, �9j �-9& �`99 °o 'v, '°a �O1p �Cisr °s �°�, �Y7� �1?p �019 '/0
Date
CHLORINATED AND TOTAL VOLATILE ORGANIC COMPOUNDS
VERSUS TIME IN MW-45
ME
rlflf
600 0
n
3
N
0
(n
400
If
I., v� ✓� v4, v� W� v� ' c% , v� v� , v� �� e%y c�� sly v� ✓� ,
�� �� �9�o '0 �o �� �'o �o 'r
'SD r r' u' r s S' ` o r 2 o S 00 � qc9 9 0
Date