WI0400176_Monitoring (Report)_20140310

MUNICIPAL ENGINEERING SERVICES CO., P.A.
Post Office Box 97
Garner, N.C. 27529
[phone]
FAX [phone]
TO: Ms. Shuying Wang
Aquifer Protection Section
NCDENR
Please find enclosed:
Post Office Box 349
Boone, N.C. 28607
[phone]
FAX [phone]
TRANSMITTAL
Corporate License#: C-0281
DATE- 315114 PROJ, G 13032.0
NO -
ATTENTION: Ms. Wang
RE: Semi -Annual Water Qualify Monitoring
Report
Surry County Closed Landfill -Mt. Airy
Permit: W10400176
COPIES
DATE
DESCRIPTION
1
3/5114
Semi -Annual Water Quality Monitoring Report for latest event October 29, 2013
(A copy of this report has also been emailed to shuying.wang[a)ncdenr.gov and a hard
copy & email to Mr. Slusser/ Raleigh office
Dear Ms. Knight;
Enclosed is a Semi -Annual Water Quality Monitoring for the latest event performed at the
Surry County Closed Landfill -Mt. Airy on October 29, 2013. We have also sent an
electronic and hard copy to Mr. Slusser at the Raleigh office.
Thank You.
J na han Pfoh!
If enclosures are not as noted, kindly notify us at once.

Semi -Annual Water Quality Monitoring Report
Prepared for
Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
October 2013
01FCFIVCa�c7
ELF .
Pq�alsr
UIC Permit Number:WI0400175
SWS Facility Permit Number: 86-02
MESC❑ Project Number: G13032.0
Submitted: March 5, 2434
� 11Slmiripal !J W � �PgInCC!'itl�
C—,, wC
P.O. Box 97 Municipal Engineering 5cnicv% Company, P.A.
Gamer, NC 27529 Gamer and Boone. North Carolina
License No. C-0281

SECTION
TABLE OF CONTENTS
m..___.m__._m____m_.___ _._.m _ _mm..m. Page I
Sampling Procedure_..,W _ _
Page 2
Field Parameter Data__,_,--
_ _--Page 2
Laboratory Results_ _ _ __.
_ W _ _.._._...__ Page 2
Groundwater Samples _ ___----------- _W...W.._._.__.__._W__
...__.__._ .___— _Page 3
Groundwater Characterization——- � _ Page 3
3
Closing--- � �.� m_ _ m _m m.. � � _ _ � � � � -- Page 4
FIGURES
Topographic Map with Site Location 1 figure I
Potentiometric Map of Uppermost Aquifer wl VOCs Detected Above 2L Standards.,,,,__, _µ,_ —«�_ Figure 2
Total Cumulative VOC Concentrations Pre/Post Injection Comparison.,.. .,-,-..__,-,___,, _„-. ,._Figure 3
Bromide Tracer Concentrations Time Series Graph and Table _ w Figure 4
TABLES
Sampling and Analysis Summary ------ _._. .._.__. .._�w .. _ Table l
Detections that Attain or are Above SWSL or 2L Standard Table 2
Field Parameter Data Summary-, ......... ..._W. _w.W._.... _.W..._..W... .W__.... ._. _._...WTable 3
Hydrologic Properties at Monitoring Wells ,. _.. _. ._ . ,...,.,,..., -------- ,..,,....,,..,.,.__-Table 4
APPENDICIES
Laboratory Analysis Report and Chains of Custody,_ _ W,Appendix A
r1 ECE
Water Qt+alily

License Nc C-028'
ti
CIVIL SAN(TARYIENVIRONMENTAL ENGINEERS
Municipal
Services
SITE PLANNING7SUBOWISION1S
Mr. Thomas Slusser, P.G.
Aquifer Protection Section -Underground Injection Control Program
Division of Water Quality
North Carolina Department of Environment and Natural Resources
1636 Mail Service Center
Raleigh, NC 27699-1636
Re: Semi Annual Water Quality Monitoring Report
Surry County Closed C&D and Closed MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 27030
SWS Permit No. 86-02
UIC Permit No. W10400176
MESCO Project No. G13032.0
Event Date(s) October 29 - 31, 2013
Dear Mr. Slusser:
Introduction
SOLID WASTE MANAGEMENT
Engineering
Company, P.A.
SUBSURFACE UTILITY ENGINEERING (SUE)
March 5, 2014
Municipal Engineering Services Company, PA (MESCO), on behalf of Surry County, appreciates the opportunity to
present this brief Semi Annual Water Quality Report that details a water quality monitoring event performed at the
Surry County Closed C&D and Closed Unlined Municipal Solid Waste Landfill (MSWLF) Facility (Permit # 86-02)
on October 29-31, 2013. The Injection Well Permit .application and Well Permit No. W10400176 (4/15/13) requires
that Surry County provide this report to the Underground Injection Control (UIC) program on a semi-annual basis.
Laboratory analytical results indicate volatile organic compounds (VOCs) attributed to landfill activities continue to
persist in levels above 2L Standards at eight wells that monitor the uppermost aquifer downgradient of five injection
points. However, total VOC concentrations have decreased at all locations compared to their respective baseline
averages established during the five events prior to the first injection event performed in November 2011.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Figure 1. Prior to becoming a C&D landfill
the subject area operated as a MSW unlined sanitary landfill that stopped receiving waste prior to January 1, 1999.
The MSWLF was closed with a low permeability cohesive soil cap per the Transition Plan. The top portion of the
southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed
with another cohesive soil cap in accordance with the Closure Plan.
Per the SWS approved Corrective .fiction Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection 11ell Permit
Application and Well Permit No, W10400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards.
On November 2-3, 2011 an EOS-water emulsion with sodium bromide tracer was injected into three wells ( IW-2,
IW-3 and IW-5). Injection was attempted into IW-I during this same event but due to the tightness of the formation
an insignificant amount (< 3 gallons of slurry) entered the uppermost aquifer. For all intents and purposes IW-I
injection did not occur nor ever will be able to in the future. Monitoring of wells downgradient of this location will
continue to be monitored semi-annually as required by the NC Solid Waste Section (SWS). Any observed changes
in geochemistry downgradient of IW-1 is not attributed to the unsuccessful injection event. Details of the premier
injection event are provided in the Injection Event Record dated November 4, 2010.
PG 6c • 97 Gamer. North Carolina 27529 (919 177 2,5393 PD Sox 349 Bone. NC 2W7 (8281'262 ' 787

On October 24-25. 2012 similar substrates were injected into monitoring wells MW-4lIW-4 and MW-BIIW-6 in
fulfillment of Phase 2 of Corrective Action. Details of the second injection events is provided in the Injeefion Event
Recordsubmitted January 10, 2013.
The UIC Injection Well Permil was renewed on April 15, 2013 which reduced monitoring frequency from
quarterly to semi-annually and the prescribed constituents listed in the approved application was also reduced
and vague.
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available
since 1994. This is the sixth post -injection water quality monitoring event with previous events performed on
February 9, 2012, May 30. 2012. August 20, 2012. October 23. 2012 and May 29. 2013. Previous event reports
have already been submitted to the UIC and SWS.
This report contains sampling procedures, field and laboratory results, groundwater characterisation, and findings.
A potentiometric map of the uppermost aquifer, time -series graphs of select constituents, a table of detections
compared to Standards, field data results table, groundwater flow directions/rates table and laboratory analytical
data results are also enclosed.
Sampling Procedure
MESCO personnel performed this sampling event targeting the parameters outlined in the Water QualitV Sampling
and Analysis Flan (SAP) (DIN:]8936) dated April 30, 2013 and approved by the SWS (DIN: 18938) on May 10,
2013. Monitored locations were consistent with the renewed Well Permit (4/15/13).
Groundwater samples were collected and analyzed from fourteen wells which includes MW-3R, MW-7, MW-9,
MW-125, MW-13, MW-14, MW-16, MW-17. MW-18, MW-19, MW-20, MW-22, MW-23 and upgradient
background well MW-I. Additionally, water within all six injection wells were measured and visually evaluated in
an effort to determine the amount of residual organic substrate remaining in the wells which may help evaluate the
viability of these wells to be used for future water quality analysis. Monitoring locations are depicted on Figure 2.
Sampling was performed per the protocols outlined in the SWS approved Groundwater and Surface Water Sampling
and Analysis Plan which was submitted with the Corrective Action Plan (CAP) revision 2 dated December 10, 2010.
The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation.
Low -flow pumping methodology or bailing was utilized to adequately purge the wells a minimum of three well
volumes or until dry. During purging the stabilized field parameters were recorded. The samples were then placed
into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were kept on
ice, and transported within hold -times to a NC -certified laboratory under proper chain of custody (C-O-C) protocols.
Field Parameter Data
Field parameters recorded included depth to water, pH, specific conductance, temperature, dissolved oxygen (DO),
oxidating reduction potential (ORP), total dissolved solids (TDS) and turbidity. A summary of the field parameter
data since injection is presented in Table 3.
Laboratory Results
Pace Analytical Laboratories (PACE) of Huntersville and Asheville, NC performed the majority of the laboratory
analysis. Groundwater samples were analyzed for all the parameters requested by the SWS which includes
constituents listed in Appendix II of 40 CFR 258. Environmental Conservation Laboratories (ENCO) of Cary, NC
analyzed select samples for the bromide tracer. A sampling and analysis table summarizing the locations, target
parameters and laboratory methods is presented as Table 1. Water samples were reported at the laboratory specific
Method Detection Limits (MDL), which are quantifiable at or below the current Solid Waste Section Limits
(SWSL). Laboratory results and C-Q-Cs are presented in Appendix A.

Groundwater Samples
The wells with Appendix 1 VOCs detected in concentrations in exceedance of their respective 2L Standard during
this event include MW-9 (1,4-dichlorobenzene, benzene, vinyl chloride), MW-13 (1,2-DCA, 1,1-DCA), MW-14
(PCE), MW-15 (TCE, 1,2-DCA, 1,1-DCA, benzene, vinyl chloride), MW-16 (1.4-dichlorobenzene, 1,2-DCP, 1,2-
DCA, benzene, vinyl chloride), MW-17 (vinyl chloride), MW-21 (1,2-DCA, 1,1-DCA) and MW-22 (1,2-DCA).
Table 2 summarizes Appendix li constituents detected in groundwater samples in concentrations above the current
SWSL or North Carolina Groundwater Standards (2L).
A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard
during this event is presented on Figure 2,
Groundwater Characterization
A potentiometric map of the uppermost aquifer created from static groundwater elevations recorded during the
October 2013 event is included as Figure 2. Groundwater flow rates and directions were calculated via modified
Darcy's equation and are included in Table 4. Groundwater flows in the unconfined and upper bedrock water -
bearing zones in a general southwesterly direction away from the waste limits. Calculated groundwater velocities
were variable but consistent compared to historical observations.
Findings
The laboratory results indicate that dissolved phase VOCs consisting primarily of chlorinated hydrocarbons continue
to be detected in groundwater samples collected from nine wells. All VOCs detected in concentrations above the
2L Standard during this event remain within their own respective historically identified range. Total cumulative
VOC concentrations were lower during this event compared to their own respective five event averages established
prior to injection in all locations as shown on Figure 3.
Evaluation of the injection wells (IW-1,1W-2, IW-3, 1W-4, 1W-5 and IW-6) continues to indicate that a considerable
amount of residual organic substrate remain in each of these wells rendering them unsuitable for representative
water quality analysis. The viscosity of the water in the injection wells precludes sample collection as either a
bailer would not descend or the check valve failed.
In an attempt to track migration of injectants bromide was targeted at MW-I4, MW-I5, MW-16 and background
well MW-1. The bromide tracer was only detected in low non -quantifiable "j-qualified" concentration in sample
MW-16 during this event. MW-16, located 86 feet downgradient of IW-3, is the only location exhibiting tracer
levels which may potentially indicate injectant migration. Based on the average linear velocity rates of IW-3 and
MW-16 reported since injection the injectant was expected to reach MW-16 on May 25, 2011 Bromide
concentrations exhibited a consistent increasing trend in MW-16 the first year following injection then has decreased
the last year (Figure 4). Calculations performed following injection indicates that reported levels of bromide that
was injected was insufficient to ever provide clear evidence of communication within the uppermost aquifer.

Closing
Water quality monitoring is planned to continue with the next event scheduled for May 2014. No further injections
are planned at this time but if they do Permr1 conditions will be met including giving the UIC advance notice prior to
installation or injection of any additional well(s).
If you have any questions or comments regarding this report, please contact us at [phone] or by email at
[e-mail].
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
�j�
Jonathan Pfohl
Environmental Specialist
Enclosures
CC' Mr. Dennis Bledsoe
Surry County
Ms. Jaclynne Drummond (Electronic Copy Only)
SWS-Compliance Branch
Ms. Shuying Wang (Electronic Copy Only)
UIC
4

Figures

Topographic Map with Site Location
Surry County Closed Unlined C&❑ and Closed Unlined MSWLF, Mt. Airy
237 Landfill Road
Mount Airy, NC 28621
Lat:36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
I MILE
ROAD CLASSIFICATION
Primary highway, Ught-duty road, hard or
hard surface. improved Surface
Secondary highway,
hard Surface Unimproved road -------
0 Interstate Route C U. S. Route Q Slate Route
Closed Unlined C&❑ Landfill
Closed Unlined Sanitary Landfill
FIGURE 1

LANDFILL RDA
W is
L y �
NOW OR FORMERLY F ,'`,
OWNED BY
ww
JOHNN Y COX
!
1 �
1 i
raw r:
• i
ti_
I � i
1
1
1
1
Mfap
1 � 1
! 1
f
1
!
!
I 1
fir'
f T[�
i !
'II I y
-AKZ WATER KWftY WELL SERVES FACK"
+I
I
}
0
WWI
I -
OWNED BY
SURRY COUNTY
:�.as
IIMJ
fMil
NOW OR FORMERLY O WNF() BY
SHA WNA SUMMERS
IMP
EkfS IMO TOPOGRAPk1C CP4TOUR5
�i EwS+ANG ROADS
•�L
ESTIMATED WA57E LIMf75 UNLINED US* k/OR C&D
LINER LIMITS OF SLfBrTLE D LINED MSRLF (MONOtORED SEPERATELY)
EXTENT OF CONESI VE CLAY CLOSURE UPON CLRSED MSW AMD CAA
1
PROPERTY ONE EXTRAPOLATED FROM SURVEY AND Cf5
1
- COMPLrANCE BOUNDARY (250- FRDM EOW - -SO' FRO/ PROPERTr LINE)
—
EXTENT OF VO"(0 DETECrM A60W 5115L & 2L STANDARD BEYLYyD COMPLIANCE BOUN!
LIM
FmuffI
IDW— ECOJIF07IM71AL UPPERMOST GROUNDWAMRR CONTOURS
j •-�
STREFAf/d7E(1[%RlVE7P
} ��
WATER SUPPLY WELL (F•ACAJ TY CONSIDERS fT NON -POTABLE)
_ r
S"4 SURFACE WATER MOWTORnM PCWT
WAM YORTORW6 HELL
W41D W.ECTfON WELL NOT SALIPLED OURIK THIS EVENT)
j
2mm 4RO6NDWATER PaTENIrOwmic ECEVAA(W (AAfSL)
--' M-
NOTE-ELEVA nON NOT USED FOR CONTOLWS
�J
SEDWEMT BASIN
Dw
SURRY COUNTY
\
1
I
GRAPHIC SCALE
I
FIGURE 2
"
CLOSED C&D LANDFILL and -.
• •
CL05ED MSWLF FACILITY
—
IfniCipai Engineering
COMPMny, P.A.
PQTf K6X,- C, YAP CF tFPDW—Wr AMM
SURRY COUNTY
�rvrces f�
.ewe. 1� f �y /Pl wlprwt k0.iM>
Itfilf WL5 DMIM APOW ZL STAWOW
MT. AIRY, NORTH CAROLINA

Figure 3
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
October 22, 2009 - October 31, 2013
DW+wo�upKw* C�.F.i �todi c.,..wm.. HOC Ce-n'Mntle�w f.}a xw1�47
o0v�.�6aAdENt Of iwa �Ton�cww�nr. HOC cenexa.eon... �oL e. �Yn�l
W:
•
8
�
�'
� � �
�] f � 3 k 4 � �
i
� M � ! 3 it
OOWNOIIIL�HR 0� M4 ReW Cv..uyne. VOC Cerc.mn�ww a. qL w fW�Li
Wvrtiv.Goi[xi v� rWa ITwi C�m�MW.vOe corc.iwa�wn .. WL w xrli�
W •
•
s
S s
Average of
first Five
Corrective
Oct May Oct May Oct Action Oct Statistical Trend"`
2009 2010 2010 2011 2011 Events 2013 Difference Difference Between Oct
Well ID (uglL) (uglL) (ug/L) (uglL) [ugfL] (ug1L) (uglL) (ug1L) N 2009-May 2013
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION 50 DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S, MW-13_&_M_ W_-1_8
IMW-12S
0.00 0.00 0.00 I 0.00 5.40
1.08
0.40 -1.08
-100 No Trend
MW-13
61-00 50.60 74.20 87.30 72.50
69.12
32.92 -36.20
-53 i Downward
?MW-18
0.00 0.00 0.00 0.00 0.00
0.00
0.00 ❑-00
❑ No Trend
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW 16
NW-3R 0.00 1 0.00 0.0D 0.00 0.00 r 0.00 0.0y J .00 0
IMW-16 137.90 1 113.60i 135.70! 121.20j 116.30 124.94 102.70-❑22.24�- --18
__ INJECTION WELL (1W-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14 15.20 ? 15.60 15.60 8.20 17.00 14.32 11.90 -2.42 l -17 No Trend
MW-21 52.10 50.70� 5_1.38 39.10 32AI 45.14 35.42 -9.72_ -22 No Trend
MW-23 4.30 0.00 0-00 0.00 0.00 0.86 0.00 -0.86 -100 No Tread
_ INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MWA9
MW-15 96.13 63.89 55.00 78.10 64.06 71.44 58.99�_2A5 -17
+11 is F 0.00 0.00 0-00 0.00 0.00 0.00 0.00 0.00 - 0
No Trend
No Trend
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE_
= Statistical Trend analysis via 5en's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Figure 4
Bromide Tracer Concentrations Time Series Graph and Table
February 9, 2012 - October 31, 2013
Bromide Tracer Levels in MW-16
Located 87 feet Downgradient of IW-3 Injected on November 2, 2011
0.3000
0.2500
0.2000
0.150071
0.1000
0.0500
y
0.0000
Date
♦ iNW-16
Date
MW-16
2/9/2012
0.03800)
5/30/2012
0.1300 0)
8/20/2012
0.26000)
10/23/2012
0.28000)
5/30/2013
0.14000)
10/31 /2013
0.1100 0)
(j] = The reported value is between the laboratory method detection limit [MIL] and the laboratory method reporting limit (MRL),
= May 25. 2012 Calculated date injectant expected to reach MW-16 using average Flow rates of IW-3 and MW-16 (155 ft)yrj since injection occurred.
Surry County Closed C&❑ and Closed MSWLF, Mt. Airy Page 1 of 1

Tables

Table 1
Sampling and Analysis Summary
October 29 — 31, 2013
App.
II
Field
Parameter
Tracer
CL
0
U
Q
❑
-
W
t�
(L
a
a
m
o
w
a
m
7
Q
m
0]
l4
L)
m
[�
m
H
CI
ti
U
[6
_
E
0
m
'�—�
H
e
`�
E
0
Is-
T
N
[i
rn
O
x
Q
-_
m
o
a
a
19
m_
g
ma
GD
m
�
Nr
rn
a
n-
w
a
m
m@
m
0
m
m
iu
m
a�
d?
m
—3
4
'J
J
—i
ii
ii
ii
u_
U-
U-
U-
w
_
I W-1
x
MW-1
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
Iw-2
x
MW 3R
x
x
x
x
x
x
x
x
x
x
x
x
x
x
IW--3
x
1W-4
x
IW 5
x
MW7
x
x
x
x
x
x
x
x
x
x
x
x
x
x
1W-6
x
MVIr-9
x
x
x
x i x
x
x
x
x
x
x
x
x
x
MW-12S
x
x
x
x; x
x
x
x
x
x
x
x
x
x
MW-13
x
x
x
x: x
x
x
x
x
x
x
x
x
x
MW-14
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-15
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-16
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-17
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-18
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-19
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-20
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-21
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-22
x
x
x
x
x
x
x
x
x
x
x
x
x
x
MW-23
x
x
x
x
x
x
x
x
x
x
x
x
x
x
EB
x
x
x
x
x
x
x
FB
x
x
TB
x
App I & II = Appendix I & it List from current 40 CFR 258
Surry County Closed CRD and Closed MSWLF, Mt. Airy Page 1 of 1

Table 2
Detections in Water Samples above SWS or 2L Standard
October 29-31 & November 4, 2013
Sample
Parameter Name-
Sample
Result
Unit
MDL2
SWSL 3
2L•
MCL a
2L Exceedance
ID
Date
Amount
MW-7
_
1,4-Uchlorobenzene
10/30/13
2.9
uglL
0.33
1
6
5
MW-7
Cobalt, total
10130/13
64.6
uglL
5
10
NE
NE
MW-7
Chlorobenzene
10130/13
5.8
uglL
0.23
3
50
100
MW-7
Cyanide, total
10/30/13
10.6
uglL
5
10
70
MW-9
1,4-Dichlorobenzene
10/31/13
7.6
uglL
0.33
1
6
76
1.6
MW-9
Benzene
10131/13
2.8
ug1L
0.25
1
1
6
1.8
MW-9
Vinyl chloride
10/31/13
6.8
ug1L
0.62
1
0.03
5
6.77
MW-9
Cobalt, total
10/31/13
195
uglL
5
10
NE
NE
MW-9
cis-1,2-Dichloroethene
10/31/13
5.2
uglL
0.19
5
70
70
MW-13
1,1-Dichloroethane
10/30/13
6.1
uglL
0.32
5
6
7
0.1
MW-13
1,2-Dichloroethane
10130/13
0.72 j
uglL
0.12
1
0.4
5
0.32
MW-13
cis-1,2-Dichloroethene
10/30/13
24.1
uglL
0,19
5
70
70
MW-13
Trichloroethene
10/30/13
1.1
uglL
0.47
1
3
5
MW-13
1,4-Dichlorobenzene
10/30/13
2
ug1L
0.33
1
6
5
MW-13
Cobalt, total
10/30/13
10.1
uglL
5
10
NE
NE
MWA4
Tetrachloroethene
10129113
1.2
ug1L
0.46
1
0.7
5
0.5
MW-14
1,1-Dichloroethane
10/29/13
5.5
uglL
0.32
5
6
7
MW-14
cis-1,2-Dichloroethene
10/29/13
6.4
uglL
0.19
5
70
70
MW-15
1,2-Dichloroethane
10/31113
0.59 j
ug1L
0.12
1
0.4
5
0.19
MW-15
Trichloroethene
10/31113
3.2
ug1L
0.47
1
3
5
0.2
MW-15
Benzene
10/31113
1.3
ug1L
0.25
1
1
5
0.3
MW-15
Vinyl chloride
10/31113
0.84 j
uglL
0.62
1
0.03
5
0.81
MW-15
1,1-Dichloroethane
10/31/13
16.3
uglL
0-32
5
6
7
10.3
MW-15
cis-1,2-Dichloroethene
10/31/13
37
uglL
0.19
5
70
70
MW-15
1,4-Dirhlorobenzene
10/31/13
3.8
uglL
0.33
1
6
5
MW-15
Cobalt, total
10/31/13
14.4
uglL
5
10
NE
NE
MW-16
Benzene
10/31/13
1.9
uglL
0.25
1
1
5
0.9
MW-16
1,2-Dichloroethane
10/31113
3.4
uglL
0.12
1
0.4
5
3
MW-16
1,2-Dichioropropane
10/31113
4.1
ug1L
0.27
1
0.6
5
3.6
MW-16
Vinyl chloride
10131/13
6.6
uglL
0.62
1
0.03
6
6.57
MW-16
1,4-Dichlorobenzens
10131113
23.3
ug1L
0.33
1
6
76
17.3
MW 16
Cobalt, total
10/31/13
361
ug/t_
5
10
NE
NE
291
MW-16
,Zinc, total
10131/13
13.1
ug1L
10
10
1000
5000
MW-16
Chlorobenzene
10/31/13
7.7
uglL
0.23
3
50
100
MW-16
cis-1,2-Dichloroethene
10/31/13
62.3
uglL
0,19
5
70
70
MW-16
Cyanide, total
10/31/13
71.3
uglL
5
10
70'
MW-17
Vinyl chloride
10/30/13
0.72 j
uglL
0.62
1
0.03
5
0.69
MW-17
Cobalt, total
10/30/13
38.5
uglL
5
10
NE
NE
MW-17
1,4-Dichlorobenzene
10/30/13
4.7
uglL
0.33
1
5
75
MW-17
Chlorobenzene
10/30/13
3.8
uglL
0.23
3
50
100
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 2

Sample Parameter Name, Sample Result Unit MDL' SWSL 3 2L-
ID Date
MCL s 2L Exceedance
Amount
MW-20
Vanadium, total
10/30/13
5.1 j
ug1L
5
25
NE
NE
MW-20
Cobalt, total
10130/13
27.7
ug1L
5
10
NE
NE
MW-20
Zinc, total
10/30113
22.4
uglL
10
10
1000
5000
MW-21
1,2-Dichloroethane
10/30/13
0.52 j
ugIL
0.12
1
0.4
5 0.12
MW-21
1,1-Dichloroethane
10/30/13
8.3
ug/L
0.32
5
6
7 2.3
MW-21
cis-1,2-❑ichforoethene
10/30/13
25.5
ug/L
0.19
5
70
70
MW-21
14-Dichlorobenzene
10/30/13
1.1
ug1L
0.33
1
6
5
MW-21
Trichloroethene
10/30/13
1.5
ug/L
0.47
1
3
5
MW-22
1,2-Dichloroethane
10/30/13
0.771
uglL
0.12
1
0.4
5 0.37
MW-22
Cyanide, total
10/30/13
10.3
ug/L
5
10
70
MW-22
Cobalt, total
10/30/13
110
ug1L
5
10
NE
NE
MW-22
1,4-Dichlorobenzene
10/30113
5.6
ug/L
0.33
1
6
75
E6
Cyanide, total
1114113
5.4 j
ug1L
5
10
70
1 Table contains Appendix 11 constituents detected at or above SWSL, 2L or 213
2 MDL = Method Detection Limit
;SWSL = Solid Waste Section Reporting Limit
4 2L = North Carolina 15A NCAC 2L Groundwater Quality Standard
s MCL = Maximum Contaminant Level (Drinking Water Standard) not applicable regulatory Standard but shown for comparison purposes
j =The reported value is between the laboratory method detection Iimil (M0Q and the laboratory method reporting limit (MRQ.
adjusted for actual sample preparation data and moisture content, where app)icable. (Value maybe considered estimated)
= 2L Standard is assigned to 'free cyanide" not total cyanide so not considered a regulatory exceed ance
SOLD = Concentration > 2L Standard
5urry County Closed C&D and Closed MSWLF, Mt Airy Page 2 of 2

Table 3
Field Parameter Data Summary
October 29-31, 2013
Depth to
Water
TOG
Specific
Parameter
Water'
Elevation_
Elevation
Temp_.
ORP___
i]O
pH
Conductance
TDS
Turbidity_
Units
ft (btoc)
ft (amsl)
ft (amsl)
C
mV
mglL
SU
umhoslcm
mg1L
Visual or NTU
MW-1
25.92
1108.43
1134.35
16.6
193
2.8
5.99
290
140
18.1
IW-2
39.91
1028.95
1068.86
NR
NR
NR
NR
NR
NR
>1000
MW-3R
42.34
975A 6
1017.50
15.5
121
0.5
7.68
210
100
Clear
1W-3
33.36
987.21
1020,57
NR
NR
NR
NR
NR
NR
>1000
IW-4
35.05
991.21
1026,26
NR
NR
NR
NR
NR
NR
>1000
IW-5
40.38
1039.80
1080.18
NR
NR
NR
NR
NR
NR
>1000
MW-7
12.65
1060.85
1073.50
16.1
201
2.8
5.82
300
140
Clear
IW-6
41.81
1046,64
1088,45
NR
NR
NR
NR
NR
NR
>1000
MW-9
33.35
1060.72
1094.07
15.4
-55
0.8
5.06
440
210
Clear
MW-12S
13.68
1012.12
1025.80
15.1
142
4.3
6.78
390
190
Slight
MW-13
25.93
982.55
1008.48
14.2
301
0.8
5.81
280
130
Slight
MW-14
37.87
980.93
1018.80
14.8
173
2.1
5.45
120
50
Moderate
MW-15
50.14
1025.82
1075.96
14.1
181
0.2
5.22
90
40
Clear
MW-16
27.11
972.43
999.54
14A
134
0.5
5.59
380
160
Slight
MW 17
8.71
956.72
965.43
15.3
192
2.3
5.82
520
250
Clear
MW-18
9.12
973.88
983.00
15.5
291
4.5
6.53
20
0
Clear
MW-19
10.39
935.88
946.27
15,1
302
4.6
5.37
20
0
Slight
MW-20
19.61
1062.58
1082.19
16.1
181
1.9
6.21
60
20
Slight
MW-21
5.97
959.39
965.36
15.2
303
3.1
5.92
180
80
Slight
MW-22
5.55
947.85
953.40
14.4
138
1A
5.75
220
100
Clear
MW-23
7.35
947.96
955.31
14.9
432
3.5
5.53
50
20
Clear
Minimum
5.55
935.88
946.27
14.1
-55
0.2
5.06
20
0
18.10
Average
25.06
1002.72
1027.78
15.2
202
2.2
5.91
223
102
Slight
Maximum
50.14
1108A3
1134.35
16.6
432
4.6
7.68
520
250
>1000
btoc = Below top of casing
amsl = Above mean sea level
NR = No reading attempted
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Table 4
Hydrologic Properties at Monitoring Well Locations
October 30-31, 2013
Groundwater
Average
Hydraulic
Effective
hydraulic
Linear
Monitoring
Conductivity
Porosity
Gradient
Velocity Rate
Flow
Well
(cm/second)
[°Iof
(feet/feet)
(feettyear)
-
Direction_
MW-1
4.30E-05
15
0.083
25
S18W
IW-2
4,30E-05
15
0.021
6
S61 E
MW-7
8,10E-04
15
0.161
898
N84W
IW-6
4.40E-04
15
0.150
454
S34W
MW-9
1.90E-04
15
0.026
33
S53E
MW-13
2.06E-04
23
0,050
46
S36E
MW-18
2.04E-03
15
0,116
no
S39E
MW-19
1.10E-03
3
0.052
1,954
S13W
MW-21
1.28E-03
3
0.068
2,992
S55E
MW-22
9.88E-04
15
0.142
970
S29W
MW-23
3.04E-04
15
0.151
317
S40E
Minimum
4.30E-05
3
0.021
6
-
Average
6.77E-04
14
0.093
770
-
Maximum
2.04E-03
23
0.161
2.992
-
MW-3R
2.40E-04
5
na
na
na
I W-3
2.40E-05
5
0.201
100
S41 W
IW-4
1.10E-04
5
0.107
243
S41 E
IW-5
1.50E-05
5
0.154
48
S63W
MW-11
3.10E-04
5
0.086
549
S15W
MW-12S
na
3
0.091
no
SO4W
MW-14
7.45E-03
3
0.083
21,392
S72E
MW-15
7.21 E-05
3
0.292
726
S01 W
MW-16
2.82&05
3
0.193
188
S43W
MW-17
2.94E-04
3
0.100
1,016
S66W
MW-20
1,92E-04
3
0.099
657
S03E
Minimum
1.50E-05
3
0.083
48� ��
-
Average
8.74E-04
4
0.141
441
-
Maximum
7.45E-03
5
0.292
1.016
-
Groundwater
Groundwater
Potentiometric
Depth
Elevation
Screened Interval
(feet btoc)
(feet amsl)
Lithology
25.92
1108.43
Clay
39.91
1028.95
Clay
12.65
1060.85
PWRIFractured Rock
41.81
1046.64
PWRIFractured Rock
33.35
1060.72
Sandy Silt
25.93
982.55
Saprolite
9.12
973.88
Saprolite
10.39
935.88
PWR
5.97
959.39
Saprolite/PWR
5.55
947.85
Saprobte
7,35
947.9E
Sandy Silt
5.55
935.88
-
19.81
1004.83
-
41.81
1108.43
-
42.34
33.3E
35.05
40.38
23.46
13.68
37.87
50.14
27.11
8.71
19.61
8.71
30.16
50.14
975A 6
987.21
991.21
1039,80
1128,34
1012.12
980.93
1025.82
972.43
956.72
1062.58
95632
1012.03
1128.34
NOTE; Valdes Tor hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Hydrologic gradient from water levels recorded on October 30-31, 2013.
Wells screened entirely in rock were not utilized for flow directianslgradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
no = Not availablelapplicable
Average Linear Velocity (Q) is defined by modified Darcy's equation
K A K= hydraulic conductivity
where Q = - M dl ne= effective porosity
e dh= head difference
dh-- horizontal distance
Fractured Rack
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Fractured Rock
Rock
Rock
Surry County Closed C&D and Closed MSWE_F, Mt. Airy Page 1 of 1

Appendix A
Laboratory Analysis Reports
Chains of Custody

.PaceAna)Wical'
• wv. Pa.Yi1 m.
Novefber 13, 2013
P. Anrlylly.l a.rrl.... in..
Po.d
E4- NC VAR
Mr. Jonathan Pfohl
Municipal Engineering Services
PO Box 97
Garner, NC 27529
P.a. An.r211u1 N.M.... IRS
Pa.. Arlalydu a.Mw., IM-
1.. AReve.n
ear.la.., Ine.
P.- An.l Mal e...l" , I.e.
P... An.1y7.11 eanf..a, hrP.
222 pr. W.O�
A.n.4i. NC, 2"0a
9afJnw .rl .. 9JN I
rA. .4. Nclwa
/nn �1n `�+ r� '.SOS E.µ e1..-A-Rc.d-I—A
rI _. �G�r��J `r�Q� '-R.M1 ?M.
!�]5+f-r. Rr
AY`72 fK i6B0�
9flW Kac.r Ay. 5u 100
MwN.rwW.NL M070
fa2e1251 7170
17Naws-OW2
^+'x'w1 �41
133a162)402
fA7fl121. 7176
lroyals-ium
CERTIFICATIONS
r4nfect: BURRY CLOSED - MT AIRY (UIC)
paea Project No.: R2177MA
Charictle Ca riificallnn l0.
91f00 Kv"y RYe. sN 100, Eamter�Yrre- Nc 23070
Fl.,W.FNELAP C.MR-U.. 1. EA1827
Hnr1h CRraSna DrfRklrlp Water certileatim ■: 37706
Keflluc ky UST Cerl[RCerl.R 6.44
Noah caralne Field senores CerliRcual l 5342
Yves) V.O.. C.rul"f IF 157
NPrlf CwcAne Wula"lar CecG6ce= a: Y2
V'0 laNE1.AP cwIllc"" /: 460221
soup c.relne cerkflc-ilon r: 9ea19001
Aehav4 le CertHkallan 10e
2225 Rr"FaWde Dr., Ami—ille, NC 28ew
N.IM C"IARII Wunwner C.rM.N.n e: eo
Fl.rld►WNE !` Cer0c.11m a: Ee764
ewth C.M n. C.ra11-11- ■: 99030001
kleue ch"I" C..aaC-Z I. M'40030
M11 wpine Car111kaeal a: 316
Npr4i Cµpin. DfWki.g 4lller Cenft-ben e: 3T712
W%ORI.NELAP Cerllee. lion e: 460222
RE- Project SURRY CLOSED - MT, AIRY (UiC)
Pace Project No.: 921 T7964
Dear Mr Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2013.
The results relate only to the samples included in this report. Results reported hereln conform to the
most current TN standards and the Iaboratorys 0ualiIV Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed al the Pace Analytical Services location indicated on the sample analyse
page for analysis unless otherwise faatrlosad.
If you have any questions concerning this report, please feel free to conlacl me
Sincerely,
Kevin Godwin
kevi n.9 odwi n@ pacelabs.co m
Project Manager
EI16D-r.I
"+ REPORT OF LABORATORY ANALYSIS
TN. raP4A oRPJ mf b. nprpduc.A...c.pt n IA.
tr v.Mc.Ir"-Hal —I F—ARalyYws.f.rr...I-
P.O. 1 91 79
REPORT OF LABORATORY ANALYSIS
TN sport Y,Y rat b. r.prcwMcM,..C.p
.A. 'th.-14"Pm 1of Par. AR.Fe-a S.Rw...Iz..
Pepe 2 01 19

Pee. Arreryllear auvr.e., Ine.
Pec. Amelpl
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IkmYrevlle. NC 7607E
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t7D4 H1'r9002
SAMPLE SUMMARY
Prdad.
SORRY CLMED - M7. AIRY (IJICJ
Pace Pr5)4d No.
92177164
Lab ID
Sample 10
M.Wr
Ow ro11C11d
Da11 R411i91d
N177164001
VW-1
yVeler
Iorm1313:30
11001113121.15
12177194002
MWSR
vy. ter
IM01130030
11MU1312110
921771140W
MW-7
Y4.ter
1MfAqw1115:40
1116111I111S
12177464004
MW.4
W.I.,
1U3111310:30
T117111312;11
Q 77114009
A1YM-fI4
W.I.,
IMIWI316:05
11101,1312:15
121779140"
MWt3
W.I.,
1W3011316: 30
11A7I11312AS
6277T164007
MW-14
WAIe,
IW21N317:40
1100112 12: 15
52177164001
MW16
WMw
1W3111306:40
WWII 12:11
63177164001
MIN-16
We1cr
1111111309-40
110DIA112115
13177644610
MW11
YP.Ier
1013u1312,00
$1 M III 312:15
32177944011
MW-11
Waler
IW2W014:30
1110N131215
12177H4012
MW-11
W.ter
IW2101317;D0
11MV1312:15
021770440"
MW-20
Weler
IWWI $4105
1too 111317:15
62177564014
MW41
VYater
I03011717:30
1N0111312111$
12177614016
MV"2
VOW
1013011311.05
1110111312:15
12177114016
Mwv
VAN,
Tw3w%31020
11MM11131215
REPORT OF LABORATORY ANALYSIS
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_e , a'..e.Yn rsn 0 Feu An41y1ee1 Se "., Inc. Peye 3 aT 79
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aceMalyticaJR No E.�i M..dw nn.d E:. A 7373 Rrv...M. c 46p0 Ax+c.1 Ar. SuG
Ed , N. 271EE AI+.r6.. NL 7Ee04 F,,, N.. NC 26t175
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SAMPLE ANALYTE COUNT
Plo2ecL
SLRRY CLOSED -MT. AIRY(WC)
P4c4 Pr.pd No.:
PW7964
Amyl"
L.610
sample 17
Method
Amaiple
Ropert•d
Laboratory
92I77144091
I4W-1
EPAWID
JMW
15
PASI.A
EPA 1410
MTS
I
PASI-A
EPA4200
MCK
57
PASI-C
SM 4500.9W
SAE
+
PA$t.A
0M 4500-CWC
JDA
1
PA$I A
17177014052
MW4R
EPAW10
JMW
16
PA$I•A
EPA 7470
MTS
I
PAST -A
EPA 1260
MCK
67
PASI-C
$M 4W-1920
EW$
1
PA$I-A
SM 4500•CN-E
JDA
1
PASI•A
U1779H003
MW.7
CPA so$0
JMW
16
PAM-A
EPA 7470
MTS
I
PASI A
EPA62W
MCK
67
PAS1-C
SM 4500SM
EWS
I
PASI-A
SM 4500'"
JDA
I
PAST -A
1vl17714AD94
MWJ
CPA 60I0
JMW
1fl
PASI-A
CPA 7470
M75
T
PASI-A
EPA 9260
MC,K
61
PASI-C
SM 450GS2D
SAE
I
PASI-A
$M 450&CN-C
JDA
I
PASI-A
12177114001
MW-Us
EPA5010
JMW
I
PAS1 A
EPA 7470
MTS
1
PASI•A
EPA 1200
MCK
57
PA$I.0
SM 4500•S27D
$AE
I
PASI•A
SM 4500-CN E
JDA
1
PA51-A
12177144006
MW-13
EPA 0010
JMW
16
PASI A
EPA7470
MTS
I
PAS1•,6
EPA 62a0
MCI(
67
PA51-C
$M 4500-$20
EYWS
1
PA$I-A
SM 450M-CN-E
JDA
1
PASI-A
121T7164007
MAW
EPA 6M$0
JMW
16
PASI A
EPA 7470
MTS
t
PASI-A
EM6260
MCK
67
PASI C
SM 4500420
SAE
I
PASI-A
SM4WI)-CN•E
JOA
1
PASI-A
12177164005
MW-11
EPA 6010
N.1Yy
16
PASI•A
EPA7470
MTS
I
PASI-A
REPORT OF L.ABORATORYANALYSIS
T W, n Pee.NP1 e.1 w npr .d. pinhN.
w4wur bn .re`n wn..nl or Paw Iwlreefl 8ahrc.. Mc
Page 4 of 71

P.ea AnM y6r.l a.nl en, Me. Pae. A-1vu .l /.rvVr.s, in.. Parr AM.lyec.l 6rrrlo.., Mc
aceAnalytica! • 706 E..I M..4 . Rn.d • 3u1.A 7775 R—wU a 96D0 kl— Ayr 3.1. IM
E4.n. NC 777a. A.-A.NC 79901 IFr,I.rw4.. NC M71
C828ON-71M 1704/875,6
I
SAMPLE ANALYTE COUNT
Propct SIJRRY CLOSED - MT. AIRY (0C)
Pic. Propcl No.: 92177864
P... RnNydul s.rvkn, In.. Pc. An.lyUW 1.M—. Ina P— Andy9a.l
CCNial ICaJ, E..l M..dew Ford - swe.A ME RN. wd. w ON ✓Jr A.. Sur IDO
Ed— NC 27M A.h. ". Nc 766W IlunrrWM.. NC 7W7A
..r pk.`Crmt {8.761620dY71 la281754 7176 [70116754M
SAMPLE AN ALYTE COUNT
Pr4lecl: S1IRRY CLOSED -MT -AIRY ILICI
Pic6 P10�6ct No.: 92177964
A nalyh.
An.lyr.r
La610
OAI11pl6 ID
Molhod
Aaalyws
R.pon.d
L..,
Lb In Sample M M.Ihcd
An.lylU
Reporlod
Lahar l-y
EPA6260
MCK
67
PASI-C
SM 6500.CN.E
JDA
1
PASI•A
SM 450"ZO
SAE
1
PASI•A
1717795401E MY�172 EPA 6010
JDA
16
?Asp -A
SM 4500.CN•E
JDA
1
PASI•A
EPA7470
MTS
1
PASI-A
1217711406E
MWA16
EPA9d}0
JMW
16
PAS -A
EPA 6290
MCK
S7
PASI-C
EPA 7470
MTS
I
PASI-A
SM 4500S20
EWS
I
PASI-A
EPA 1260
MCK
87
PASI-C
SM 4SDG-CN-E
JDA
I
PASI-A
SM 4500SM
SAE
1
PA51-A
SM 4500•CN•E
JDA
1
PAS1-A
91177664010
MW.47
EPAW10
JMVY
16
PASI-A
EPA 7►79
MTS
I
PASI-A
EPA 6760
MCI(
67
PASI-C
SM 4500�S2D
EWS
1
PASI•A
SM 4WO-CN-C
JDA
1
PASI•A
01177144011
MWM6
EPA6D10
JMW
16
PAS•A
EPA 7470
MTS
$
PAS•A
EPA3260
MCK
67
PASI•C
am 4500-S20
SAE
1
PASI•A
SM 4500�CN E
JOA
I
PASV-A
12177164612
MW-11
EPA6610
JMW
16
PASI-A
EPA 1470
Mrs
1
PASI-A
EPA 6260
MCK
67
PAS-C
SM AW-820
SAE
1
PASI-A
SM 4Sd0. CIV E
JdA
I
PASI-A
12177l1491a
61 Wh20
EPA 6010
JMyy
16
PAS -A
EPA7470
MTS
I
PA514
EPA 8260
MCI(
07
PASI-C
SM 45DDS2D
EVVS
I
PAS! -A
SM 4500-CWE
JDA
1
PASI-A
12177164114
MWII
EPA 6010
JM4V
16
PAS•A
EPA 7470
Mrs
I
PASI-A
EPA6760
MCK
67
PASI-C
SM 4500-22D
EWS
I
PASI,A
SM 4SDd-CN•E
JDA
I
PASI•A
12177544016
MW22
EPA8010
]DA
1a
PASI-A
EPA 7479
Mrs
1
PASI-A
E PA 1260
MCK
67
PA51•C
SM 4500-S20
EWs
1
PASi-A
REPORT OF LA130RATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
TM r.W N.1 ml to r.yr.4—d. —pl h &0.
TIN. I.IM Y o -1 W P—A n V,
.I.wM M. MAYneon..M.4 P.. An•wa 5—"., inc
P.qe 5 M 79
Ivw4 wrnrn mnwnl.l Prc. An.goctl 3.—. irc
Pepe 6 of 79

P.p. A� "cal
elm c..• �..
P... Anayddrl6.m..., Im.. P.r..m.lyu..1 errelwr, k,..
Pre. Amq ypvN
erM.vo, In..
Pre.
Analptl•N e.M.n, loll
Fr -A m Oyu." Nrvla r, Im.
aceAr�alytical4
ZOfi E.n M..daw Rv.d • ewr A
E d.e. NL 277ae
,An R ..dd.9. "W �� .., $,Ar ,OD
a.h..w.. NC 2a404 Il,x.r.a.Jr. NC 75T4
n �/}� y•
ace P nrI�Ilf�' •
7v6 E.. *..av a." • 5� 4.A
4d.n NC 7tlaa
3m R....a. or
AW.w., NL HaO.
A&W tee, Aw 5.% 100
Wn1u.rM- NC 7801E
a'.wyurCr re.
I
1
Ia3fi Ifi7]a97n
[ea5N34•il i6 ITIMNiS Wag
' "'^'Pt'�fe1^'
137E1a73-0921
{E]aj234•tl to
[7p4IaY5.4PP2
ANALYTICAL
RESULTS
ANALYTICAL
RESULTS
PrnJa�r SI1RRy CLOSER - MT Al RV {i11C1
Pro)W: SORRY CLOSED • MT. NRV (WO)Pace
Prvleel Ne' 22177964
Pace Pre091 N9,: 921779E4
ammpl.: M69-,
Lab 101 921771104001 CoRacu d: 10129f1313:30
Re""d: iI M Ill 112:15 MaV1k-W4tar
Samplw MIN-1
Lab 10: 1217TH4001 C06.91•4.
IW2B11313]0 Recm.d IU0I 1131216 Mcbtr MW
Report
Repvn
Pmremelx.
Reaulla Llr41m Lknll
MOL
OF
PRpmred Arfatyzed CAS Nv 0",
Pmr.nn4lwa
Raaytl. IJrNY Llml
MOL
OF Prep....I
Mmiy.ed CAS Mo. O..r
9010 10 P Qmw dwdtr
AnelyWol Ma9lod: EPA 6010 Propmailm Method; EPA 3Q10
8240 MSV Low L4-I Landfl9
And,IkM MaNwd: EPA a200
Anumvny
NO ug4,
6.0
6.0
1
1NOVI310:30 11AW1320,07 7440-36-0
kmla•1,4.OiCllkla 2•binane
NO u9R
10O
fA
1
11105113052E 110.57-6
A--
NO ug&
$0.0
S.0
1
11102f1310:30 1110571320; 17 74463'8.2
Okhkmd9umamalnane
NO °q&
5-0
021
1
11105113 05 20 75-71.8
13.0-1
381J ugVL
100
S.0
1
11102`13 IM30 IIMW1320r17 7440-39.3
1,1.Okldorwlhcn.
NO ug1L
5.0
0.32
1
11N61130Y2e 75-34.3
Beryllium
NO ua&
1.0
IA
1
11N211310t30 11105fi320:11 7440.41-7
!2-0IcNaoplun.
NO ug1L
12
0.12
1
11m5ft3052E 103-0tl.2
CadrNum
NO uglL
1-0
1.a
1
1110211310:30 JIM"120:17 744043.9
1,1-0kMoroWrane
NO -j;&
60
0.5E
1
11/05/13 0526 75.35.4
ChrenOPm
NO ugA
10.0
6.0
1
11A21131010 11 ?out 320:17 744047-3
d8-12.01ahlm oath one
NO uq+L
6.0
0.19
1
111051t305:28 150.59.2
CabmM
NO ugll
100
5.0
1
1IAW131014 11106f132017 74404a4
1tm1a•12-dddoromlMne
NO aq4
5.0
0.49
1
UM5413052E 156665
Lopper
NO upA
100
5.0
1
111021131030 tIMoll 320:17 1440.50-6
12.O1chkxuprop.na
NO uqL
1.0
0.27
1
11m511305;24 ?W-5
Load
NO uUJL
100
5-0
1
11621131P:n t1 moll 320;17 1430.22.1
1,3-01chl.rWr pane
NO ug&
14
0.20
1
11 MWI305:24 T42-24-9
Nickel
NO ug1L
10.0
5.0
1
11m2113 ta:30 11 MWI320:17 744042.O
22-Okhlumpropmne
NO ugA
15.0
0.13
1
11 m571305:24 594-204
SNuNum
NO NFL
Ip p
10.0
1
TIW1310!M 1110511320-17 7782-4114
1,I Okhlar opropane
k0 uA
5.0
0.49
f
11m571305211 763-SdB
H6yar
NO uprL
10.0
5.0
1
S11ON5310:30 11111611320:11 2440424
do- 1.3• okNaeprnp.na
NO ugiL
1-0
0.13
t
II?owl 30525 10061.01.5
TkmlAun.
NO-OA
55
5-4
1
17 M21t3 tOJPD t110311320:11 7M634p
u.n.•1•]•dddorvproPane
NO r^
1.0
0-26
I
V1m57t305:2e 10051-02-0
Tun
NO ug1L
100
1.p
1
11MRA310;30 1VOW 132017 7440.St.6
ENrylbrnt.n.
NO uA
1.0
0.30
I
111a61130526 100.41-4
vommum
Np UA
25.0
1.0
1
11NL1310:30 11m511320,11 744042/-2
Eoyl mathauylele
NO u91L
10-0
030
1
t11061130525 97-012
A-
NO UOR.
100
10.0
I
11m211310;30 1ImV F]2037 7440-66411
Ne.erJ-0wo•5 }wledlene
NO +,yL
10.0
0-71
t
11 MVI105;2E 0746.3
Z+1.a Anona
NO u07L
"10
9.46
1
11 m511305:26 591.78E
1410 M.Kury
An•tymal Mt". EPA 7470 Pn eparaNm Melhod; EPA 7470
IDdemedmm�e
NO ug1L
10-0
0.32
}
11 Osf 13 054E 74-06-4
Mwn y
NO ugk
020
0.10
1
1110411313:15 1IA111316A5 743"74
I.vlrutanul
NO uy1L
100
35.0
1
11105113952E 7S•83.1
M.1h crylv.euR.
NO uq6.
100
0.93
I
111061130520 125.91-7
Saco MaV E t-1 L-dfm
MNyueal Mmlhud: EPA 1260
M.91yr.ne Lhrulda
NO uylL
1.0
0-97
1
11105113 0526 75-09-2
Aulm•
NO ug1L
too
10.0
1
I1IO6111063E tl1414.1
M."I mevlamylmle
NO Lqg&
VA
2.0
1
I M""1 5:26 a0-02-0
ACelvnkrA.
NO uyi
55.0
22
t
i1mSh30S7E 75458
4•MmNg4.2•pwanane IMIBK}
NO rp4
109
0.33
1
111p5153 p5 106-10-1
A.Weln
NO ug&
53.0
16
1
11 m61130520 107.02.E
N4prdhmlmne
NO uyi
10.0
0.24
1
11 M5113053a 91.20.3
An:rylvnlu4m
NO ug&
200
1-1
f
f1mSry30530 107-fY1
Pr9I4m me
Nb uyi
ISO
36
1
1V051130524 107.12.0
Amyl Chlpuda
NO p9R
70.0
1.5
1
f170W1305:2: 107-05.1
law"
NO up4
1.0
0.26
1
11m51130520 10842•5
B-T-
NO uUfL
1 0
0.26
t
11105713052E itJ3-7
1,1,t,bT trmchlvmeRune
NO ugiL
&0
0-11
I
tImN13 052: 630 xMb
Hrvnivctnlwoma Elan•
NO ug1L
1.0
0.17
t
1}1051131352 E 74.07.5
1,12.2•Tmtrmdllvrvrt.
NO ug0
3-0
0.40
1
51 M5NSOST6 79-045
BrvmvdlcMwvm.0lmn►
NO ug&
1.0
8.1E
1
111051133053E 75.274
Tawomwomm.rir
NO ug11
1-0
0-40
1
t11rr51130526 127-l"
grvmv}wm
NO uyL
3.0
0.2E
1
1110011a 053a 7fr26-2
TaNa0d
NO uck
1-0
0-24
1
17105113051E 1046E-3
&omwnehmne
NO uqR
}0.0
0'a
1
I1AM"1 a,28 14-S19
1,2.4-TOWvrvL.pm-
NO ug1L
10-0
alai
t
Itm51130526 t20-
2 But-m. {MEK)
ND ug1L
100
0.9E
1
11/05113 0520 78.933
1,1,1-TFICN rar4na
NO ug1L
1A
0.4E
t
S
1S105t13052E 71-55•S
C.l"n ".khd.
NO u91L
100
12
1
11105f1305.6 75.15-0
1,1240CW.rveth-
NO ug1L
1.a
029
1
1110511705:2E I9-0RS
Lmuvn Iotw1u .rde
NO ug1L
1.0
0.25
1
1065113 0525 65-23-6
Trkh1«o.Vren.
NO ug4
!.11
0.47
1
flIp51,3 p5:26 72-01-0
Chl-bonrme
NO ug1L
3,p
0-2]
1
11105113052E 106.947
TrkhlaraRw,omelh.na
NO nw1L
I.0
0.4
I
1110511305.2a 75419-4
Chkxa.aiana
Np ua
10.0
0-E4
1
11f0511a 054E 7590-3
12,1TnMlvrvprvpmn.
Nb U2&
I,0
0.41
I
11106113953E 9bf6-4
Chlvrvkrm
NO ugJL
50
0-14
1
11105113052E 67-06]
vhA mc.l.l.
NO -A
60.0
035
I
11107151111215 f06-0}i
ChkrvrlNfnm.
Np ug1L
1,0
0.11
1
R1m5r130526 74-07.2
Vkny1 chlplde
NO uA
10
OA2
I
11 m515] 052E 754TA
Lnl9rgprene
NO ug&
20.4
0.21
1
11MS/1305lo 126-99-6
xy1•ne lTPl.q
NO rPi
50
0.6E
1
I1m61t305:28 1J]0-20-7
1 7 Obrvmv-0-nhlDrvaop eRm
NO uqL
130
2-5
1
Amu 30520 9612.E
5ulrapmf.m
4-aromawuaraa.nx-d4IS;
96 %
7613a
}
11+0511306;2: 46060-0
OOromocnwiam.m.na
N❑ ugA
3.0
021
1
1}m511305-26 12444t
1,2 Okh4vrvOu n.-04 IS;
iO4 %
76100
t
1N1%51130526 f7060-07-0
1.2 p4xemvIhmnm IEOBJ
NO uq4
I,0
027
1
111cw 50510 1ob-n34
Tvluen.•da IS;
97 ![
min
1
1. '5052 2037. 11,5
Olbromamedlan4
NO ug1L
10.0
021
1
11105113052E 7495.3
1,2-f]Ir:Nmlv6enlan.
ND uok
5.0
tl,30
1
1110511 ] 05:20 DS•50.1
4500520 SuIrwo Water
An.lylkal 6}.111P4
HM 4500-S70
1,3-Okhlwvbehzam
r40 ug1L
5.0
024
1
1110611305:2a K1-7}1
1 a-plehlorvEenrene
NO udL
1.0
0-33
1
111051t3 06.26 $06.46-7
31AE4e
NO WL
1000
100
!
11 Moll11020 18495.25.8
REPORT
OF LABORATORY ANALYSIS
REPORT OF LABORATORY ANALYSIS
rr....pan.n.r nut W
..Pro K.d ....im h
m.l
rN. ,.port .mar mf r. r.poa.:wn .-P.
n M.
Oslo 1111117D13 0212 PM
Mh- lh. -,n wer.nl er
Pr.. Av.ryuc.n
S.rvwf..
Inc Pogo 1 01 79
Om1e. 1 t11 3120t3 02:31 PM
,rcT•N er. A.nr.f-qn....l ul Pr A yrj" S. k... 1.
Page 6 e110

Pa.. An.lyaeal Same.., In,. Pace Analyd
ul demur. Me,
Pau Andylkal aenlw., im.
I 1A� A,�^y 'na!
P4 iuk7i r�
205 E.W M.edew R-0 • State A
4an. ML naee
122S 19-W. D.
Aan.wl.. N� JAW
Le00 Wneer Me. awl. I00
�Ar p9a- NC JmM
r n1,. ptxWr w.r
In 67SE971
18761754-7176
176116752002
ANALYTICAL RESULTS
ProJecl: SORRY CypSEU - MT. AIRY (UIC)
Pace Projacl No.: 92177964
Samph: MI.F1
Lab 10. 221771144"1 C.pecled tORu13 13:30
Repaired: 11001113 57:15 Maklt v4kEar
Report
paramelsn
Rau" Walk LIm6 MOL OF
Meparsd
Analyzed CAS No, Owl
4 E0OCNE Cyanlds, TOW
Anaryllcal Molfod: 6M 450O-ME
Cyuod.
NO u00L 10.0 5-0 5
fl(61113 13i9 V-12.5
REPORT OF LABORATORY ANALYSIS
Trr. npwl .l.N rpl y. r.prPduc.d. drop n ru1.
Dow IT) I W10130232 PIA xrnwtm. w. .c-P.f P.a. A - POW s.rvbe. Inc.
P.n Anal ree.I ea.Vlan, Ine. P.O. Arr"w eaFrk.a, Ina P.n. Anelyg.el Eertile.a, Ine,
aceAnalyticale E..1 A .&. R..d • S. A 2]JS Rrr.r.d. nr A56a K car Ara 51...100
Ed.n. W NMI . NG 7a&N .anN+eMe NC 21tlia
(17eT6f A.h.r?mw, PIAPY-,717n 1704075colll
ANALYTICAL RESULTS
Frt*cL SURRY CL05E0-MT.AIRY(LIIC)
Pace prplael NO.: 02111064
Sample: M,"R
Lab 1O1 92177914002
CoRecled:
ID W11CO-30
Rar:elc.d: 1110111312:15 MNO.: IN816r
Report
Param4lars
Resully Unl4
Limo
MOL
OF
Prepared Malyred CAS No Oulu
1010 1CP Ofolr.dwalor
Anerylleal #laillad. EPA 6010 Prepar40"
Melhed: EPA
3Cl0
Aldlmmy
NO UUJL
6.0
5.0
1
1110VIa 10:30 1iM511120:20 7440.36-0
Arsallo
NO ugA
11) 1)
5.0
1
11A7211310:30 11M51112020 7440-36.2
Bulum
9.0J uA
100
5.0
1
11WI310:30 II M5113 x020 7410-39-3
6efyliium
NO ugA
1.0
1.0
1
1M2f43 N)14 IIMS1132020 744041.7
Cadrnlurn
NO uWL
1.0
i-0
i
11A72f i 210:30 11165113202E 744"3-1
Chramlum
ND uyi
100
SD
1
IVO71131030 111051122070 744047-3
Cobalt
NO ug&
10.0
5-0
4
IV02M310:34 11f051132020 7440.41.4
Capper
NO uplL
TO.O
5.0
1
ll002M 31030 11loul12020 7440.56•E
Load
NO ugJL
100
5A
1
11 00W310;30 11 mul37020 7139.9Q-1
fAckel
NO u0+i
50.0
5.0
1
11f02113 t0'30 it itlul32070 7440-02-0
Sslardum
N0u0A
100
10.0
1
11f021i350:30 1il051132020 771240.2
BiWar
NOVA
100
5-0
1
11102113:1)30 11f fil3202C 7440-V-4
Th41FRn
NO uak
III
SA
1
11102/13 030 151OS1320L20 7140.21-0
Ttn
NO -u&
4p9
5.0
1
11 MZI" 10:30 11 XWJ32020 7440.7t-5
Vanadlum
NO ugA•
25.0
5.o
1
11 f02r1310:30 111OSf132020 744M-2
Zinc
NO ugA
10.0
10.0
1
i1f02113 10:30 WOV1320:20 7440-W41
7470 Mercury
Maf111eal Method: EPA 7470
Preparalm Melhed: EPA
7470
Mowry
NO ug&
020
MID
1
111041313-15 1W1113167011 7439.97-6
■210 M1 V Low L-1 LurdR11
An alydcal Melfwd: EPA 6260
^clime
NO ugJL
100
10.0
I
1110503 05:42 67-04.4
AeelmMm-
NO 41L
55.0
2.2
1
11,05" OSA2 nt"
Acrolam
NO ug1L
53-0
1.6
1
1100543 05:42 107.02.E
Awyoomlrla
NO 41L
200
1.9
1
111051f3 05:42 107.13.1
A1lyI r3l rld.
NO uWL
10.0
1.5
I
111OW$3 05:42 1 -O"
Bsn2ene
NO ugA-
1-0
0-25
1
1100511306:42 71d3.2
91em4ehlmomem.na
NO ugA
3.0
0-17
1
1110"305:4i 714.97.5
Bromadlchlclm olhans
NO uQ&
1.0
0-IB
1
11f0W 1105:42 75.27.4
Bromororm
NO lrµ
3.0
0.26
4
11 M511305A2 75.25.2
Bromomalhsns
NO ug&
10.0
0,29
1
1V0511a 05:42 7443.1
2-BuGnone IMEK)
ND ugA-
100
0-16
1
r1105J1305,42 71-93-3
Calbm disWlde
NO ug4.
100
1-2
$
}1 f0511305A2 75.15.0
Cnhm Ietto h1wlda
NO ugR
1.0
0.2E
1
41 f6S1136SA2 S6-23-5
CM-henxene
NO .Q&
5.0
923
1
11 MWJ30SA2 1069E-7
C4110004* na
NO ugA
10.0
0.54
1
11I=305:42 75-00.1
ChWroform
NO ugd.
$.0
0,14
1
SMNI305:42 67-5&3
Chloromelhehs
ND ugii
1.0
0.11
1
1IMS113 05:42 74a17-3
Chlaroprana
NO.gf1
20.0
0.27
1
1110511305:42 126.99.E
12-Dbramo-]-elMropropsne
NO ug&13.0
2.5
1
11M51f305, 2. W12-6
Dlbromocnloromslhsne
NO ug&
3.0
0.21
1
11 WI6 05:42 12444-1
1,2-Obromoad1w. X08)
NO uo&
"I
02 r
1
114511705:4Q 106.93.4
NO ugfL
11-Ih.m
11-0
1.21
1
111G5113 65'42 74.9E-3
I �•O+cMorabenxena
NO ug1L
E-0
0-30
1
11105f13 050. 0566.1
I ,3•Qichrorobenxene
NO u01L
5.0
024
1
11AWI305,42 541.73-1
1.4-Dichlmohen2Ma
NO ugfL
1.0
0-31
1
11105/13 g5'42 106.4E-7
REPORT OF LABORATORY ANALYSIS
Th. r.MA Mai net br npraduced. nmpl n All.
Page 0 cf 79 O.Ie' 1111312013 02:32 PM w 0-1 as xn.rn a ",i of Pr. A r. Sarrn[a., la
Pape 10 of 71

P.P. A.d yp..l 9.Ma.s, r... Palo Am"" ""lags. lee, Pap A.WyO..l 9.mor, Ina- Pee. A.Rayued aerWrn, Im. R.C. AnalyYwl 6.Mic.e, Inr. P.e. An.fytlal 9.rvlco6, Wt.
2n'. E.0 M..daw Reed anf. A Z226 RN N. 9e 14c.y A�. 9w.. f 00 205 x..r M..dw R..W • &WW A 2= f -eel. Or NN00 lift y A" &.. 1W
accAfWyiiCal ed.. 7r75e ANeWe. NC 20e04 Min.. enr.. NL 2e0 yE ��ace
AnaVical* Ed- MC 37,6E Aw..... K IOWA 14�rMY. NL iW71%
...,.,tee o�
p3616736011 lue)n+ rt7e 17dr l6]&9082 I336K272<901 m7aPY4.7 f 76 I rw lers 903�
ANALYTICAL RESULTS
ProleolSQRRY CLOSED - MT. MRY IUICI
Poo. Pruj..1 No : 921770E4
9ar.lpla! MW-AR
1JhlO: 921779E-0002
COME cted
t071611309.M
Recdred. II MI M3IA: 15 M911k Mier
Report
poromolero
Re"Ire IJnlb
Lint
MOL
13F
Preper.d An*zvd 'e No. Quell
e 210 M6Y Low L-1 L-el Pill
AnNyfl-1 M.tMd: EPA GM
Nor..-I,►-0Id.t0r0-2bul.ne
NO u111L
100
1-0
1
11 M511305A2 150.67.E
DkhWadll-...LP-
NO ugAL
6.0
0.21
1
11 M511305,42 75.71.1
5,1-0icNawlh.n.
NO up1L
5.0
0.32
1
.0NI305:i2 M34.3
l.2-0ktaor..lhene
NO rrpA
1-0
0112
1
1tM611305:42 107-w2
1,t-0kNord.O.ona
NO upL
6.0
0.S6
1
1IM511305AZ 75.35.4
dirf,2a1M1er..M.ne
NO uU&
6-0
0.19
I
111Wf 1305A2 IW51-2
Sam-12•dvhlor.ellrano
NO upR
5.0
0.49
1
11105f1305:42 H4-00.5
1 ,2�khlorvpopano
NO uq4
1..0
027
I
11M5f1305:42 M-87.5
1,3.D"� Woprop.rie
NO UP&
I,0
0.26
1
11='$105:42 142.Ms7r
22.Oknloro1, no
NO upL
16.0
0.17
1
1110511305:42 S94-20-
1,1-1160 opro Pero
NU �pR
510
0-49
1
11M6f1306A2 503.5E-d
p.-s,3-pchloropf opene
NO upL
to
0113
1
111 WI4:5:42 1m1-01-5
fim. 1,3-OIAN..opr.p.n.
NO UOL
1A
P.,
1
41 M51535%06 2 101-0;4
E%Vlh.nzon.
NO u*&
14
0-30
1
tI M511305AZ f00.41.4
E"I melheaylalo
NO ug1L
10A
020
1
'I M511305AZ 97.6362
Nereddoro-1.3 bw.dlene
NO uq+L
10.0
0.11
1
WOW 1305A2 974"
xair..nona
NO..g1L
50.9
0.411
1
1TMS1130SA2 591-70.6
iodomemene
NO uqR
10-0
0.32.
1
HMSN30i:A2 74.56.4
Iec6utmal
NO UA
100
35-0
1
11M6f130S141 76-03-1
IM91.oyl.nlh9e
NO upR
.11
0.91
1
11M5fl30542 12b96-i
M.dryrm. Cmakw
red uok
I'll,0.97
1
IImfl3 OSA2 7S40F2
&Woryl m"W"Aw
NO ug1L
30.0
2A
1
1110503 05AZ 0"24
44ANMYP-2-perftanan'twmI
NO u01L
10033
1
11106f130542 f0610.1
Na".len.
NO u9A
10.0
624
t
11N91130sA2 91.90-1
Proplar'09e
NO u9AL
150
3.6
S
0.11051.42 107.12-0
STNfono
NO -a&
1.0
02e
S
11 M511305AZ IM42.5
t,1,1-Tatr.oMproenane
NO uq+L
SA
0-33
1
11 x5d305A2 630.20.E
1,1,2,2-T u.dYor0a9iano
NO ugk
3-0
4.40
1
11 175f005 A2 79.34•S
Till dddr041nefm
NO upl
L6
0.4E
1
11M6f13GSA2 127-144
Toluene
NO uplL
1.0
021s
1
"to"305:4: 106.6E-3
l JA-TFI.Nc.ohen2.ne
NO upL
i0.0
1.10
1
11N5f1305AZ 120.02.1
1,1,1-TdWoma9f one
NO uq4
1.6
1146
1
Ifl0H130S:aZ 71.65.E
1:1.2.7dcaN, NNnN
NOug&
1,6
0.29
1
11106f130SA2 79-00.S
Trid.IwoeNene
NO upt
I.0
0.47
I
1t10511705�42 79-01.6
TFII. lh olwfomdhMr
NO uq4
SA
020
1
11105"305A2 7""
12.1•Tnchlordpr0pano
NO upL
1.0
a"I
t
11M141306A2 96.16.4
WO ocelue
NO 41L
50.0
0.31
1
IIM511305-42 10 -05-4
VmO cNoride
NO up+L
1-0
0.67.
1
11 MU1305AZ 76-01.4
Xy4.ne(7e1a0
NO uWL
5.0
0.6E
1
1I106113 OS-142 1330.247
Sw galoa
4.Orem.lPorohen=en. 15)
96 %
70.130
1
"Awl303:42 460.00-4
12.01chluoeUvne-04 M
101 %
70.110
1
1110W 105:42 17060-07.0
ToWeee-daM
97 %
70.130
1
1110515305A2 2037.26.5
4 P1M?0 3u01d. Y61.r
An.lyllcW M.lnod 5M 4500-370
Su11de
NO uqA
low
100
1
11 M6113 lU0 16496.25.E
ANALYTICAL RESULTS
Ptol.ct S1IRRY CLOSED -MT-AI RY(411C)
P.- R*d N..' 92127964
6.rnph: MW.7R uh 10: 92177f94003 Cdq d.d. I07011309:10 Revolved: 11 f61 f 1112:15 MGM. Y*Wf
R.P.A
PNNn..1.r. R.-HI LMlih Lrro MOL OF Pfoperod Anowed CAS NO. dual
4600CNE Cy-W., Tvul M.ly1i0.1 Melh.d: SM 4500-CN-E
Cy.nlde NO uq4 10.0 5.0 1 11110113 11:$4 57.12.5
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
t �r. own am em u...P.r.e�c.d -0.n nn rN. aspen ww nel a r.Grodunrd..x-pt n k--
Dota: It113f2013 0212 Plfl N.r.a.r ur w..l.n P oanl of P.es ArWocd SoMmm. h.c. P4ge 11 04 79 O.h: 1111=013 02.32 PM eii-i o.. wnfbn -M of P.P. A...fy►r.l GMc... 1- P.qe 12 o7 70

2ceAnalytical'
Pa.. A natyaeal 6.rv4e.., - Pa.. Aneiyn.M
6anle.r, IM
I,-. A.."..+ S..H..., W..
M6 Ea M.A. rY.w,RnW• 6,.e. A
i22 RFNC .'W. Dr
9100AMeq A.. S,er100
-
Ce_. NL 27�WA
Arh.wl. MN1A�r11rIN1.
Ne 25076
13m)mulml
I003bl7M-71 rg
f70/16iSNo,
ANALYTICAL RESULTS
Pre}eqSIJRRY CLOSED • MT. A1RY [111O)
Pae. P+u}.d He . 9217796a
ear.lpl.; MW7
Lah IO; 9217716400E Co11.0od: 10f30f 134E-40
Recaf.e4: 1100111311; 15
Matrix:VAtter
Pau An.lydr.l &-k -1ne. Petyl ... A.kal Sam...,1n.
aceAna�ytica�' 2o5Cow .1..d.wRo.O-..A 22251E-d.Dr
Ee.rr. ML AM, 2+246 .r.... HC M04
4.1)123a 1 femmI254-717a
ANALYTICAL RESULTS
"act SORRY CLOSED • M7. AIRY OAC}
p.m, Prel.0 Ne-./7177264
E.W0.1 W*7 L.h ID; 91177964003 Col.eled: 101301131S.40 Rdealved 111CIA
Pan A n.lyeul a.nd..., +ne
WWKbW.r Mr 4. ,O0
i.nl.rp,... 4c 2W7e
f7041ef}ppSs
Ml4k:
Rel,arl
Report
peremele.e
Reruns Onln
0ml
MOL
DF
PrePped MOW.* "SNO. 0401
Patometen
R-Ift 11n11.
Llmll
MDL
OF
P1.pmed Analy2ad CIS Ho. Oud
60101CP O.... A aler
AlrafyrleAI Method EPA60IC P1 epere
Um- Ml d: EPA 3010
1260 M SY Lew Level Lmdflp
Ane Vl¢el Me n.a
EPA 6760
Anpn+onr
NO ug+L
5.0
50
1
WOV131030 111061132024 7440.364
Iron. 1,4.OWWO(O.2•E1Man1
ND uW1
100
to
1
1110511305.58 110.57.6
M46r+C
NO ug+L
1D.0
5,0
1
WOVI110:30 11M61132024 7440-38-2
dchwr0dl8uweme/nene
ND UWL
6.0
C.21
i
11105H30536 76.71-a
om-,
if.4J uyL
100
5.0
1
IMV1310;E0 IVM 112024 7440.39.3
1, 1.OkNwaemin9
NO uyL
50
0.12
1
$1105113053a 75.34.3
Bery5lim
NO ug&
1.0
1,0
1
11102f1310:30 111031132U4 744041.7
1,2•Dkhlwoefh.ne
NO Ug&
1.0
0.12
1
1061130510 107-06-2
Cad.rvu�„
NO" A.
1.0
1.0
1
11M21131030 11M6f132024 744041.9
1,1-Dkhlwvelnene
NO UO&
6.0
0.56
1
11✓DW1305M 75.35-4
Clrrornuai
ND �W&
100
S.0
1
11 M211310:36 IIMWI32024 7440-47.3
d1.1,2•DICrlwoelherve
0.41J uyL
5.0
0.14
1
111051130SA1 M-5412
Cobol)
443 u0'L
10.0
1D
1
IWOM31"ll JIM 0132024 7440-41$
tren.4.2 Dludareehene
NO up11
5a
DAS
1
IM15f 1395 t51 158-80-
Copper
ND uC&
T0.0
5.0
1
1$102111 M30 11145113 2024 7440.504
1,2•Okhtnropropane
ND UO&
1.0
0.27
1
WWII 70,47.5
Lend
NO nA.
10.0
6.0
1
1110221310:30 112W11329=74 7439.92.1
1,3-01rh1wopropane
NO UOA-
1.0
6.26
1
1110WI1l DS11 142.2E-1
NIReI
NO ufyL
Soo
5.0
1.
1IM211310:30 1VOW132024 7440.024E
2?•Okhlwvpropxne
NO ugti
15.0
0.13
1
11105430516 554.2Q7
S.Ieruum
NO ug1i
10.0
10.0
1
I110711310:30 111DW320-24 1712-49-7
1,1-D1.h1oropi.pene
ND ug&
5b
0.49
1
1100511305:56 M3-56$
Serer
NO uyi
100
5.0
1
1110711310-30 111M511320:24 7440.22d
d1.1,3 Olehlervplopene
ND uam,
1.0
0.13
1
11105A305:50 1001E-01-5
Th.14um
NO ug&
55
5.4
1
1110211310:30 1110511) H:24 7440-26-D
van.-1,3-Dlchloropropene
NO ug1L
1-0
0.26
1
I110511305111 low 1.02-5
T.
NO eyl
too
5,11
1
1110201310;30 11105032024 7440-31-5
EvWbonew.
NO ugA,
1-0
0.30
1
11 f0S1130516 100414
Von.da+m
NO ug4
25.0
5.0
1
111D211310:30 IIIQW5320i4 7440-OL2
E9.yr melMvyl.le
NO wg&
10.4
0.20
1
1110511305'56 97$3.2
2nc
NO uyi
100
too
1
I1A77113 f73e IV0511320:24 7440363
HrrecNoro 1 lhutedl-
NO u9+L
19.0
0.71
1
110OU1305;56 67-9&3
7-Ne.enone
NO 4&
SO.0
0.46
1
1110511E 0536 $41.1a-6
WO Mercury
Meryllul Method. EPA WO Pr.p.retlon
M.tlwd. EM7470
lod0melrene
NO ug/L
WD
0.32
1
11 mul30536 74-084
Mercury
ND ug -
On
0.19
1
111D4113 13-11 1111111316:10 7432-97.1
I.Ohut.nd
NO uyL
100
ES.o
1
tIM51130536 ia-6E•1
NO uD&
106
0.0.E
1
11low1 05:56 126.91.7
1294 MOV Lew Lorel Lendlll
Awym.4 A..Ihod: EPA 9260
oAeeiaaplonippe
Mr MIA". CNor.&
NO ugll
1.0
00
t
111031E 05.16 75.09.2
Aeet4Pe
NO .,A
100
10.0
1
$11051120551 67.64•t
Meliylmommuylat*
NO uA
30.0
2.0
1
7TMSH305-Sa am1$
AL.M 6m.
NO u9,L
SSA
2-2
1
11 MWI10536 7S-05-6
4•Me0y4-2-penlenw,e lMIOKI
NO UO&
100
0 33
1
111057136S9f6 104.10.1
Acrotekl
NO ug,l
53.0
1.6
1
11 r0511305!56 101-02-8
Naphlh.lene
NO uOL
10.0
0T4
1
$1 mul30516 91-20-3
Auy1e011r4.
NO dgfL
200
1.4
1
1110511E OS-56 107.13•I
P1oplonw4e
NO ug&
ISO
3.6
t
1110511305-56 107,12.0
A111 d0oAde
NO ug+L
10.0
13
1
11 mWI305.56 167.05.E
Slpf
NU UJI&
1.11
026
i
II10M305.58 100-02-5
8-t-
0.44J uglL
1 0
0.26
1
010WI30111 71.43.2
1,1,1,2-Tetwh1o1 eeriane
NO u04
6.0
0,31
1
11 MU 130S.58 630-20,6
9.onwtldor.m.8une
ND ug&30
0.17
1
14wila 05i8 74-07-S
1. 1,2,2•T4eechlor c.l,.,,t
NO ug&
3,0
0.40
1
11 M511305-48 79.34.5
OlzodpAvremem4ne
ND dg1L
1 0
0.16
1
I Im30556 7647d
Tetrachlw9e01ene
ND PAR
$.a
D.A6
1
111051130638 177.16-4
9romnrorm
NO uglL
1.0
0.78
1
11105H305-54 Is2S-2
Towene
ND 00&
lA
0.26
1
111OW130518 IM16.3
1.cmvmellene
ND.0%
TOO
024
1
111M30538 74-83.9
1,2,FTrld11a,0benrena
NO upR
10A
0.35
1
11711§I110918 12 -0-1
2 50-W. tMEK)
NO ug&
1Do
0.9E
1
Illow 3055a 7693-3
1,1,1•TrlMrcre. inane
NO uQ,L
t.0
0.46
1
11N511305 Sa 111 55-0
Carhnndt.dld.
NO uglL
1DO
12
1
1110S11305:58 75.E S•0
1,12-7dChloroc D,.nr
NO uyt
1A
0.29
1
1lim II0S-1a 79-00-5
cet0arr WrowmId.
NO ugfL
$.a
0.25
1
111051E 10S:La 5623.5
T11111"vr6r.'.
ND ugk
1.0
OA7
1
11MSR3 at 9 79-01.6
Chbruhenren.
98 uWL
3.0
023
1
'IMP 31)51A 104.90.7
TrluAoreluwememane
NO uO,L
1.0
D20
1
1'At& 305.54 71$9J
Clrier om6r a
NO uWL
too
0.64
1
111050130531 754X0.3
1,2,3-70oh1wopr0parte
NO uyL
1.0
0.41
1
1114511305:54 96.16.4
Chl-Im.
NO WO&
5.0
0.14
1
1110Li305:51 6746-3
%,W evelate
NO uq&
SOA
0.15
1
1110111305:51 t06-05-4
Chkram.rirle
NO "A
1.0
011
1
11/05/13 O5:51 7447.3
v91yr chimm.
NO 1+0ti
1.0
0.62
1
1170611 E 06:51 7S-01-4
Chnrvpr.M
NO.gA.
20.0
027
1
11103IT305:SO 121-04-8
Xylane(Tool)
NO ugIL
5.0
0.66
1
1Owl' 305156 1330.20.7
1,2•Obrnr-3-w.fvpr.p4ne
NO uDiL
13.0
23
t
11 M5113 05 58 96.92.E
Sunopen.
4-B+emeworehenlene IS}
96 %
7Q130
I
11f05153 05:56 440.0Q4
Dlb, m chlmameman.
NO uIPL
1.0
021
T
I1105113 IS 69 12a44-1
]-Dknwoernins-d4 [51
7Q130
!
11MullI03:S6 170a0-07.0
i-O4rerrq.lNete (EDE)
DaK0m9m.11er1.
NO 4A
14pup+L
10
100
1127
021
f
1
111051t3 05i1 100.4] 4
1110571E05;S6 74.95.E
Toluene-da[5)
97%
7p-130
I
IINNISOSI6 2037.2E-6
1,2•DkhlwaWn2W"
NO ugA.
50
0.30
1
11 M511305:59 I5-50.T
4Wa2081011d. WAI.r
Af Nmcml Method
SM 4500-S2D
1,3-0kNoropmn 5
ND uQA
1-0
0.24
1
11 IOU 1105:51. 541-73-1
1,4-DicMgohenrene
2.a .,yL
10
0.36E
1
11 IOU I105'59 TOS-46.7
SAW.
NO LIPA
1000
IN
1
II NMI 313]0 14648.25.1
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
Th.•. poa Y,N gel e. nprodu-ad...... J n hdl. T., nM� h.. m1 p. nprrdu .. p1.. ".
Oel. 1 N 30013 02:32 PM h..,v„ 1 ems:: P.c. Ar..1,r_.i 5.n . I- Page 13 o2 79 Dote: 111$MCI 101 all PM „, u..,., *. wm.. _a .1 P.. Ar rPcW It-. ore Pogo $4 01 79

Pa.. Amd 0.416. m..., 1.- Pace An.lyt"
6ary1n., 1+a-
Pa.. An+lrea.l 9-k.., Ina.
/�[� dn•�1
7Y� E.N khA�w Ro.4 • Su -A
2M Rkar dv p
WM scat• W. Sil4 IW
�, . �L4rr1 fQi l��1•
Ewv. NI: 777+e
Arir;y- NC 7660e
Nun..r=. NC 7e07a•
I]30 e23a9x1
(626125F717d
jm4l mwu
ANALYTICAL RESULTS
Project: SURRY CLO SED -MT•AI RY (UI C]
P6ce Project No-. 92177964
66mpw+ MW-7
Leh 10: SM796093 0v1ec1.d; 10130013 15%0
Reul-d: 11 M 711312-15
M.brk NJ.Ar
R.Peq
Pelamelere
Randle Ilr61a Lkll MOL OF
pr w-,+ Mely7.d
CA$ No 0u.1
46000NE Cy-kol., Tetal M."k-1 M.9rad: SM 4509-CN-E
cv.mde 10.6 up4 f0A Do 1 1111011111:15 37.12-5
CB, mj, liaW'
. artrptwaoa-
Pau AnJydcar S.rr4r_.., Inc. Pa.. Aal yo .! l.rcic.T, Int Veai Analyaep e6mp., Ina.
M Eau M..dax R:.d Yuraw 27"
Hh.ra.N a Y650lflnt TMa BWIa lm
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1376H n a62 r te2e)254• r 1 re 9N)6?5.@M
ANALYTICAL RESULTS
PruleclSURRY CLOSED • MT. AIRY (UIC)
Pace Ploycl No. 92177964
1+mpl.: MW-9
L661ot 12177914004
C611ede4: 10OW1310:30
Received: IIn11113 1115 Mlkix. W612P
R.poll
P-omeaen
ROOL414 La111.
LkWi
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OF
Prepw.d Malyxed CAS No- Owl
6010ICP 6ewlndw.f+7
An.lylk+l M.Ihed. EPA 0010 Pt.P.n69n
M.dred: EPA
30 t0
Andmony
NO up1L
6,0
5-D
1
1110211310-31) 1MW 1112026 744D-I"
Ar-ork
NO n0A
10.0
5.0
1
711p2111 M30 17JOSII1202: 744D•36-2
garhrm
El.iJ �d2
100
5.Q
1
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NO u01L
1.0
1.1
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1$A711310:30 1110W132021 744D•+1.7
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1.0
1.0
1
11f0211310,30 11roWs1 lose 7a40.13-9
Chromium
NO uplL
70,0
5.0
1
11lp2113 Mn it MSF13 20:24 7a40i7-7
CobaO
1e6 MyL
10.0
5.1)
1
11A2fl3 00:30 ti MS113 2026 744114"
Copper
NO uQ&
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5.0
1
1110211310:30 11 r051132D26 74a0-AOa
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NO "A
10.0
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I
I1r07l1310A0 t11OP13202: 7439.92.1
N:ckN
NO uWL
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1
11J02113 10;30 11ro671] 2026 744042A
Selenium
NO ug&
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10.0
S
VIOLS310;30 1f/o511320:29 776219-2
SINer
NO upR
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5-0
f
11102/13 1010 I1 M5113202: 7440.22d
ThMlum
NO ug&
8.5
5.1
1
I1*1113 f011 t IOU13 ZD27440.26.
Tin
NO ug&
100
50
1
71 OOZ153 5010 11105713 2D•26 7 AG-31-5
y6ead9um
NO ug&
25.0
5.0
1
11ro&131010 11451112024 744042-2
21nc
NO wp+L
10.0
10-0
1
IIPMIa 10'30 1IAMII2D29 7440464
7470 Mercury
Medy111+1 McOmd: EPA
A70 Prepere99n
Mpll d- EPA
7410
Mercury
NO ug1L
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O.fO
1
1110403 Is! IS IUl111310:13 74311474
6219 MSV Low L... l L-41111
Maryllcsl MaOwd. EPA 0260
Acelal.
NO upA
I00
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1
1170i1r700:44 07-04.1
Acelarvhd.
NO uWL
55.0
22
1
1IMW 306:14 75-DS•6
A-1.In
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310
1 A
I
11106113 00:14 107.0P 6
AcryWn11r6.
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200
1_9
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1IMM306:54 107.1]•I
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NO agIL
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1.5
1
1110W13 DOM 107.05.1
9enaen+
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1-0
0111
f
1110511106:14 71.4112
Sr9m9dder9melh+ne
NO uA
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0-17
S
f1f05H300-14 14-97.0
&vmvdldrlorom+9r+M
NC ugti
1.0
0.18
1
"110511300:14 75.27.4
Blomakrm
NO vg/L
3.0
020
1
II Mu1300-14 76-23-2
&omomelrane
NO ug1L
t0,0
029
1
11f0511306:14 744]4
7-gul+non. IMEll1
N01pA
100
0.90
1
1*AWI306-14 7193-3
Carbon mwl6de
ND UD&
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12
1
111MI306-14 MI"
C6rbm le4Achlorlde
ND WA
1.0
0.25
1
111M,109:14 W 3-5
Chlvreb.nx.n.
2.3J uWL
1.0
0.23
1
IIMU1304,14 105.967
Chl6ro.el7
NO uyL
f0.0
0-54
1
1IM5113 D6:f4 7540.3
Chlombrm
NO uQJL
5.0
0-14
I
HIp57f3 M;1{ 57-W3
Chlo-Oh.
NO up4
1.0
0.11
I
:161S11305;14 7447-3
Chlowpren.
NO up4
ZO-0
027
I
1110W1306:14 126.pp•1
12.OIMvmo-1 chlorep owe
NO u0R
13.0
2.5
1
SIMW,"05:14 96-12-6
Olhromo aiw.Pmelhr+e
NO upt
7-0
0.21
f
IMii705:14 124.45-I
1,2-Ohrvma. Man. 1f60}
NO ug&
1-6
1127
1
1110W 306:14 1D0.91J
Dlk-momerh+n.
NO ug1L
II.0
031
1
11NSI13 D6;14 7
1,2-OiCMvfoOMx{nv
2.1J uyl
5.D
0.30
1
11ro5113 06:1 a 96-50.1
I,3-Dkliwopanlene
NO upA
50
0.24
1
111p5113p0;14 547-73.1
I,4.OkMu90entepe
7.1 VWL
1,0
0.33
1
11NW1306:1a 10S.M.7
REPORT OF LABORATORY ANALYSIS REPORT DF LABORATORY ANALYSIS
T r W,, W.. Zvi a. r.P-.d,.t-M YF iW flw r.me aha netb. nped-d..-Na hhy,
Dale, I I I t W013 W:J7 PM rne.an tlu .,nw.. -1 or Fae. MNrww S.mw.. IM P.q. 15 GI 79 DNe' 1111 Ifnl3 02 32 PM erenrd tlr. -. .. mn-dP-Malpc+l 6wvk 6- P+ye 16 of 79

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1 .... p..re..�w
Pe.. A--ro" arrwaPe, mr. Poe. An ykl..1611•.t" 1, I... P.r1An11ynr.1 alnNae, Mr.
703 E..I W.&. R." � S..0 A 2226 Rnxe Dc e600 rl- M1 5� $m
Ew..., NC 272M AY1wM. NC 2eMH 14-11ren1e, RC 2eW16
f13e1621d621 162017E+11fe f Mb75.90e2
ANALYTICAL RESULTS
F1*;l: SORRY CLOSED - MT. AM, (UPC)
P6Pe PC." No.: 02177964
swapta. 911N4
Lab ID: 12IM64004
Celeoad: 100 V 1310'30
Recalved: 1100111312.15 Matrix YN1p1r
R.PPA
Pr.Ineler.
ReeH6e 1)Ne1
011
MOL
DF
Prepped Analyzed CAS No. MW
6260 MSV I- Law at Land1111
A"y1kal MCN.vd- EPA 1240
Orr. -IA Okl,16 -2 b.A-
NO ugk
1DO
10
1
l%XlWI30614 110•S7$
Dw+navw6w.ramell..nr
NO LKA
5.0
0.21
1
1VOW 13PIS: 14 7541-4
1,1 OkNorwlMne
uu uQR
5.0
0.32
1
1110501506:14 76.34.3
1c1401
I26w11yne
NO uryi
1.0
0-12
1
IVW1306:116 107-06.2
1,7 01chow. r.enc
NO u04
5.0
0.56
1
1Imo 1306:t4 75.35.4
w-I,2 OIcNoIoem-
1.2 Volt-
50
0-11
1
111pui1 t> M 136-5C2
Clans 1,2 Olchler 0.ene
ND uq&
5-0
D.A9
1
I Ifo 173 06114 156410.5
1-7-L)klJowP,004nc
No �gk
1 0
a]7
1
17/05Ha 06:1e T6->I7-s
t ]-OlehlmoploP.ne
NO ugR
1 0
0.21
1
$1 WIN 106A4 $42.284
x,z•Okhla Nolm's
NO u91L
15.0
0.13
1
1110511106:14 514.247
1,1-Oknloroproperr.
NO u91L
5.0
0.40
1
11"1306:14 513.51.E
at,4.3 DICId91Ppfopene
NO ug4
1.0
0.13
1
1N05f 1306;14 10D61.01.5
It n 1,1 DI["mpkow.e
NO uWL
t.0
0.26
1
111651176E-14 16061.02.E
Elhvll--e
ND uWk-
PAN
0.10
1
11f0511106:14 100-41.4
Elhyl melr. ylme
ND uNjA
100
020
1
111W2011A 1743.2
nel.cnu•iv-1 S WI.d.ene
NO u04
100
071
1
111051t301:74 17ib3
NO uWi
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046
1
11109130E-14 311.79.E
IWemral.ne
NO kq4
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0-32
t
II1M511316;14 74.6E-4
Iaah l.n.d
No uµ
1W
35.0
1
tim&1306:14 71a3.1
u.Ih.crHmnNr
NO ugtL
100
0.93
1
1110511306:14 121I-W?
Methrlena Chwwe
No u91L
1.0
0.97
1
limu 30674 MM2
Me tho PlalheuYl.t.
NO u9lL
30.0
2.0
1
1N0811306-14 80-12.6
4 M.9.y[-x•prni.nwe (INCE0 k
NO u91L
100
0.]1
1
I$MW 006'14 IN-10-1
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NO uyt
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0.24
1
111051110014 9t•20.3
PFQPIP11f9e
ND up
t50
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1
JVW13 DINA4 107.12.0
&Won*
NO u0A-
1.0
0.16
1
1110311306:14 10D•42.5
1,1,1,2•TeY.dilwoetllene
NO uA
S.0
0.11
1
11104"3 D6'Ia 630-20-0
t,1,2,2 Teu.dnu mm-
NO 1.W1
3.0
0.40
1
1110511304.14 70-34-5
T.s pa.Ik.oe Y.nir
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10
044
1
1IMDA3 Da 14 127•1a-4
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1
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035
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INOU1306:$A 120.92.1
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$110u13up: 14 71.56•S
1,1-TIItl11.1valh ane
140 uWi
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No u0ti
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047
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fIX1823 ml j67a175.1• Y 116
ANALYTICAL RESULTS
Prol.cl SORRY CLOSED - MT. AIRY 1UC1
Pa.. Plopct No. 92177964
Pa- A.Wynrrl a.meef, Nr.
9e00 Nkery Aw Su111,w
t4.r,MrwNe. NC 2e07e
ONIe7seoe7
$WWI@; MW-1 Lab ID: 11171164004 Cvlknumcl. W3111110:30 Received 11A31115095 Makkc:11kifir
RcpoM
Pwiontoen Rep4u Lwu Lk IQ MIL OF PI.Prcd Ahalyaed CAS N11- Owl
46000 NE Cyanide, Total An41N Iil Method. SM 4500.CN•E
CY.Mde ND u0& Ma 50 1 1111W1311:34 $7.124
REPORT OF LABORATORY ANALYSIS
Tlw erprrt M,11 not be leproeucad..... P. 1. eJ,
Del« t111117 n1•l n2 17 PA W..•1t 4•..wk1e•. o1no-.1 Pr "I v- 6.= In< Page 17.179 Dole till ZR013 02-32 PM
REPORT OF LABORATORY ANALYSIS
rM1 •pe.. •I�H ror a rrO�oPucrd .aup n h..
w mnul mr rrin.n r.rnrnl of a.cr AneNhcd Srrro e. I•c
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ANALYTICAL RESULTS
P,crj-L. SU RRY CL DSED- MT AIRY (U,C)
Pete Prv1.0 No 92177964
Peu AnYylrral 9enrnr, 1,m Pao AnalyCaal SaMam, Ina- P.-Aruly4W 1"'-, Inc
BafA Ke�crr A.e SON Ip0 201 E.at "N's w Reed huh A 22]5 II -eh Dr
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17g41ars9W3 1 '^ ate r3361673-Mi (6215)MA 7171
ANALYTICAL RESULTS
P,nkcl !jURRY CLOSED - MT AIRY [UICI
PA" P,01.Ct No 92177994
3.mp1.: M9Y-1]6
P.-@14r,
Lah10; 12177664004
Reewlr LWIS
Ca6eC1,241: ICM03 W05
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3010
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5 0
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1142113 I0-30 11M6117 20:13 7440-36-0
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NO up+L
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5.0
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114ZM31030 11 MVI320:33 771242.2
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REPORT OF LABORATORY ANALYSIS
TH.nW M..a -- Noe reProdur4d, eaq(a n TUI.
V.I. 111112013 02 12 PM .eeww e.. wrie.v eem.nr er Pwa A,>,lreeal 9.Ntera Ina. Page 19 of 79
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0.42
1
1WWI 30634 %7-1554
cl4-t,3�ictdwvprvp.n.
NO uWL
l.0
0-13
I
11lOSH]06:]0 1OD61.01.5
Ire--1,7-01.MWopF0pen4
NO ugli
1.0
028
I
I1M511] 06:30 1D061.02.6
Ed1y6e-.ne
NO uWL
}.0
0-30
1
11M511 ] 01130 100-41.4
E Nyl melnawl.I.
ND -A
10.0
0.20
I
11=1,,, 97.13.2
Hex. N-1,}hut.dl. ne
NO up4
100
0.75
I
110
11M 101.30 5 G -3
2•Mr.6nontl
ND oyL
50.0
0.41
1
11M51}]0620 591-765
Iodvm.meve
NO ryL
10.0
0.12
1
I'MS113171:]0 74.9 .4
I401xjw,,p,
MD.0&
100
15.0
1
[I165/1306:3D 76.1]-1
Mem.Or 1Wuu1le
ND up1
100
0.43
I
11105/i3 p6:30 ;zS 91.7
McMO.-CNwId.
NO N9R
1.0
0.l7
}
11 M5/1106'30 5-00-1
Ma7ryl melhaaylatr
NO u9&
70.0
2-0
1
11M51130830 604.24
4-Methyl-2 y.M.non.[MIBK)
NO ug1L
100
0.33
4
117051+306:30 +06+0-+
N.phd,.Iena
NO u0&
10.4
OL24
1
IIMSl1306-30 91.20.3
Pivplanl9lle
NO u97L
150
1.
1
11105H30 ,30 107.12.0
6ret".
NO nk
IA
0.26
1
117051130E-30 106.42.5
1,1,1,2.7e9edioroallane
NO u0h
5.0
0.31
1
111g511709�70 630.204E
1,1,2,2-T60acMw0efiene
NO uO+L
7.0
0.40
1
11fO511306:70 71-343
To9acht9r0a11ane
NO uOIL
1.0
0.4E
I
11105r1706:a0 127. 16-4
Toluene
NO uqL
1.0
0.26
I
11r051f706:34 106.16.3
1 Z,4-TrknWfdhen6ene
NO UPC
10.0
0.3E
I
I1r65713 DI X 120.12.1
1,1,5 Td0hlaoHhelw
ND UWL
1.0
AS
I
IIAW 3 D6 3D 11-55-6
1.1 ,2-Trknlaoenane
Mp uqR
f.0
029
1
11ro671306:w 79-DO-6
Tlkfilor"Ihm
NO up+L
10
0.41
[
11MS1130930 79-01-9
Trkhm&k.or0ete61ene
NO -OIL
1.0
1120
a
11M511]176-30 7539.4
12,7-Trkf" praip-
NO uu1L
1.0
041
1
1IM5113 01:10 96-16-4
wql 6c6We
NO uy&
50-0
0-35
1
+1M571306-3O t06-054
vino 0NWWe
Np VD&
I ID
0.62
1
11/05/13 06.30 75 01.4
](yleM {Tai.r}
NO vVL
E0
0.0E
1
11105013Gum 1330-20-2
Sumop.He
4-9,WnP9uero6enaene [SI
9T %
M130
1
IIM511301130 4a0-M
1,2•dchlorwulenetl4 [S}
103 %
70-100
+
1110671] 06:74 1706O. 07•0
Toluenis,cM M
29%
W130
1
I'MU1306;50 203726-5
4100S209u9ld. Mb.r
Anelylrcu Methw: 8 M 4500• S20
Sul&&
NO IrglL
low
100
1
}IFW131029 11416-25 6
REPORT OF LABORATORY
ANALYSIS
Tin m-ri
vier mi 1w iepea ..-W n M.
p4n- I 10 1 In 01102: 32 PfA
•rawer lM -W,
[_M., Paer
Anar/ee.l "mica. Ina
Page 20 H 79

P.[s Ar,slytl[.I e.rKl.l, Irv[, Ples Aturye[sl Svrlcss, Inc
PaceArraly[ical' >� �k Mr.do. pew - 5�.,
Edon, NC 772Se hRw.l. 1N: xe5Q1
4.ie)e]]+79:I !n7611s+. 717a
ANALYTICAL RESULTS
P.pso SUR RY CLOSED - MC AIRY (I11C)
Pace Project No. 02177964
P.[. RnHyesal asnlH., Ins.
01.901Qn[ar,w. SJM tp0
~W,"NA HC 26076
rm4p759m
6ampla; Y9V.126 LAIR ID: E21T7Ei406E Collecled: 10/211/13 16:6S Repdred: 11091R3 12.15 Maud' Valer
Reporl
P.remelar. R "'Its UNIS Lkwl MDL OF Prepared Anaryxed CAS No. Oct k
46WNE Cyanld., Total A ,sW kel Mothad: SM 4500•CN•E
Cyamdo NO ugIL 100 50 1 L111N1310:55 57.12.5
REPORT OF LABORATORY ANALYSIS
T10 r.pen.ho nets rapt .d. -,A In e11.
DelaIV W20130272 PM rrVN rh.-ft, vxr...er 0 P.r,. A-Y" Srn .. pc. Page 21 at 79
P.a. Anal ylk sl %ml[r r, I- P,.. AmryYe.1 E.nkw,, Me. P... RnMyllval aankH, Me.
dCBAIia1 1Cr31 ' 2351: M u..mw Read 5.4.A 7225 RIwn1M ar 9ew lurc.r M: 9u 1P7
Ed.�. NC ]7ia6 AYyrf. w ]1601 H-Mr . NC P6076
mrrRr. .- f13aM7]agxt t6P6j254 717E 170116T6406x
ANALYTICAL RESULTS
Prated 5URRV CLOSED - MT. AIRY NrCj
Pace Prapcl Np. 92177964
Swnpl.: NW-12
Lab ED: 7117796100E
Cvll.ctad: 1DWI 3 16,30
Rocel9ed 11 M Iit 112:15 McRN' VAler
R.P.d
pwomelere
R.-H. klnld
Liz
MOL
W
Prepared Akt*W CAS No. Owl
6010 ICP 0romdwalar
AnelyHeel Me1Rpd' EPA 6R 10 P-pop.um
Melhed EPA
3010
AntlmmV
NO uA
6.0
5.0
1
11102013 10:30 11 M511320A6 1140.1E-0
Are.r4e
NO vOA.
102
S.0
I
11 MIA 1 t0:30 11 IOU 132046 7440.36.2
Baoum
63.9J ugk
100
5.0
1
1110L+110,30 1V051IS 20.46 7440.3E-3
BwyWum
ND uq&
1,11
f-0
1
I1 M211111130 11M51132OA: 744011-7
Cadmlum
NO GO&
I.0
1.0
1
1110N5] 10:30 11 M511320:A6 7440.4 .9
Chrvw-
NO u001-
$0.0
50
1
11 M211110:30 11M611320:40 7440.47.3
Cobalt
10A uA
10.0
5.0
1
11M771319:30 IIlftl320:i0 7440-44-4
Copper
ND uqA-
10.0
S.6
1
$1M2r131010 11M511310:40 7440-50-6
Le.d
ND Ujp&
10.11
6.0
1
11M21131it3O 1IM511320:16 143e•92.1
M06
NO dg&
60.0
5.0
1
1tM21131030 1SM511320'I5 7440�2-0
Se4enWm
NO Uo&
10.0
10.0
1
11M211310:30 11M511320:46 7762.49.2
SArer
NO pg14
10.0
5.0
1
11M211S 10:24 1IM511120:46 7440-22-4
Th4l9um
NO uQA-
4A
5.4
1
1110211 1 1 0'30 11 M611120:46 7140.26L0
T k,
NO UP&
100
5.0
1
11Mi11310;30 11Mj713 z0:46 7440a1-5
uan.mum
NO ugd_
25.0
5.0
11 t21k3 5010 11 M511320 A6 744042-2
2nc
NO ug2
10.0
10.0
5
41102111}0:30 11M6ry520:4a 74AC45-5
7 An M9-4ry
000711cd Me010d EPA 1470 Prepare46d
Malhod: EPA TANI
Mercury
ND vlpt
020
0.50
1
11 MU1313-15 1111111315:16 7431k-f7-0
E 210 M9V Lnw Lent Landl to
Anelytiebi Method: EPA V150
ACe1WIe
NDugA-
100
19-0
1
11IDS);306'47 67.04.1
Acts .".
NO tM?L
SSA
22
1
+1m611SOW IF""
A-leln
NO LKVL
53.1
1.8
1
t1 M511306,47 107.02.5
AcrykONOk
NO u91L
200
1.0
+
}I00511306r47 107-ml
AIM chlorlda
NO ug1L
10-0
1.3
+
11 M9H366A7 107-05-I
Benign.
NG HPIL
1-0
1125
1
I1N511306:47 7t Y13-2
&emechlprpnulh.ne
NO uplL
S.0
0.17
1
11M611S 06-47 74-Ei-5
&prrlodleruvremelhene
NO VIA-
I.0
0.1a
1
11 M611306.f1 1527.4
grolnohrm
ND uDt
3.0
0.26
1
"M511306-47 73-I6.2
Br PlnomelRene
NO ugR
$0.0
0.29
1
1}AIN 309-11 74-13-6
2-6...=(MEK1
NO uOIL
$00
0A6
1
I Ift 306:47 78.933
Carlwry dl ""1
MD uqA.
100
12
I
11M5113 O6A7 7i-15-0
Cerbpn t.bachko 1d.
NO uqA
1.0
0.25
I
111*W 3 04:17 56-23.5
CRbiObanxene
0404 ugrL
3.0
023
1
1110571306.A 106-90-7
ChWrv.lhm.
NO uS&
10-0
0.54
1
If 103113 kM:47 75.00-1
Guor9hrm
ND ugIt
5-0
0.f4
I
11 M6113004:47 E1-6&3
ChkromeFane
NO ugA
1-0
0.11
I
I IM5713116:47 74-67-1
Chloroplene
NO uIk
206
027
I
1110511305AT 12G96-6
1,2 Oita. :,S.dloMpr0pene
ND uA
13.0
25
k
11M511306.47 96.12.E
D-bromQ=k)melllarn
NO uWL
3.0
021
1
11 MSI I106.AT 1244E-1
1,2-Dlblomoe61.ne (E De)
ND uglL
1,0
11.11
1
14MShS 06:A7 106.91.4
4lbromamemane
NO ug4
t6.0
0.21
1
11 M3113 06 A;71.95.3
1,2-0ichloroh eneene
NO uglL
59
0.511
1
11M511306:47 95.50-1
k,101rn1waeenxene
NO uO+L
50
0.24
1
11M511306:47 541-73.1
1,4-Dkhlafohms-
2.0 ugtL
I,a
0.33
1
1VDVI306'47 106467
REPORT OF LABORATORY ANALYSIS
TN.» d Y d rot as rapredue».. -pt h ".
Dale 11113,201302.32PM Mimvi " -M6 eo.lnra.r Pw An.h11c.161.rw.. I- pagan o}79

Par,. AnNMaAl I.Mc.1. Ies. Faaa AnatyMa41
lavInt, Ink
Pas. Artdytlual f.rylc.r, Ina.
•
PS Eau M.aeaw Real - 6,ela A
#Z4 R-0clo Dr.
9WQ u r., 4r. 9u . I W
--. aceAnalytical
Elan. rvc 7i266
Aahavea, NC 2ef64
H�nMrnriAa, NG 2e019
I
i336f67]E971
1626)264.TTT6
I7Mq]5.60M
ANALYTICAL RESULTS
P(okeL SORRY CLOSED - MT. AMY (lll C)
Peet Pmyect No.: 92177954
9.mp4: MW-I)
Lab 1p: 92177944006 CoOaded: IW30Np Id:M
Recelv.d: IUp 101312:15
M4ft: MW
P-ater.
Raeulh Lkrh
Reyorl
LUM
MDL
OF
Reparad MfYjmd CATS No. Oual
E260 MSV Law Lots LandRR
AnO&ml MaTod: EPA 6260
trine-1,4-0Ipdore-2-butane
NO u91L
Im
1.0
1
11 WI!106A7 11"74
DkhHerod6unmm eltmne
NO u94
&0
0.21
1
1IMUT306s? 76.7"
1,1-Dknlmv vinene
6.1 aWL
S.0
0.12
1
.0W7306Y7 75.34-3
1 ¢•O4c Moroethane
0.724 Dg&
1.0
0.17
1
11106f1104 A7 107-062
1.14xoMvrve[herw
NO up&
5.0
0.516
1
111OUT306:47 75.31.4
ch-1,2-DICN01001hene
24.1 uWL
5.0
O.T9
1
1110"0441 IWW2
hire- 1,2•Didtlaloe0tene
NO uOR
SA
0.49
1
1V011130E'47 1S54"
1.2-01,11-propene
NO u94
1.0
0.27
1
111OS1$106:47 M871.5
1 ,3-0kNprppropme
RD u9R
1.0
0.26
1
1,051110EAl 142-M-9
2,2•DkMoropropule
NO u9&
15.0
0.13
1
11005013 M-47 SBA-20-7
1,1-mmoTwopene
NO uWL
S.D
DAR
1
1110511 MAT 56166.E
d.- 1,34MAW, opropene
N0 u94
1.0
0.t1
I
11,05"a 06A7 l0061.01.5
rene-1,1OIWaropr0pene
NO u0&
t.0
0.2E
1
11101411::47 10061-024
E9glreneene
NOupR
1.0
0.30
I
11MV1308Ai 100.41.4
Ed+yl melhecrylete
HD u9A
70.0
0.20
1
1IM511306:47 97-03.2
He. adNara•1-3•wlamen4
NO u9&
10,0
0.71
1
11 mwl:t 06A7 67.6E-3
2-H-me
NO u91L
50,0
0.4E
1
11 MWI106:47 591.76.E
I dvmerhane
ND u9HL
$0.0
0.12
!
11 M51130547 74-M-4
l soiutsmA
NO 4pAL
100
35.0
I
11105l I308A7 T6d11
Ma6+acrylonigiHe
ND up+L
S0011105l1306A7
126.9E-7
Me6g44ne C61N We
NO -A
1.0
0.97
t
1IM5113"--47 76-0¢2
IA."metheCrylNe
NO apk
30A
2.0
I
11 f05113 WAY 004216
41Mfthv1-2•penrAnone(MIaK)
NO upiL
1DO
0.33
1
;M511306,47 IM10.1
Nephmte --
ND nyi
10.0
0.24
1
11 Ml3 COAT 91.20-3
Prvplp.a61r4
NO uu&
150
36
t
1110611106A7 107.12-0
styrene
NO uA
t.0
0.2E
t
1t10511106A7 100.42.E
2-T6Yed+broao+ene
NO uyL
E.0
0.3]
t
1f&W 30E:47 630-2"
1,1,2.2-TeracT.lvrve6+...
ND uyL
3.0
OAO
t
11105ry30E:41 7sF3f-5
Te#acAloroe6ler+e
ND upot
1.9
0.4E
t
11705r130E:47 127.1E-4
Tolwna
NO -A
1.0
0.2E
1
111061f]0E•A7 10"6.3
1$,e-Tnenlerohenlme
ND u0&
10-0
0.75
1
lllm$306,47 12042-1
1,1,T-Tr1cf1W eh-
NO ug&
1.0
0.4E
1
1VOW 30E:47 71.554
1,1.2-Trlchlarve9tene
NDuOHL
1.0
0.29
1
IItawl300141 79-00.5
THoMaovthenv
1.1 uj'l
1,0
0.47
1
11l051120d A7 79.01.E
Tlknlwoluorema�hane
Na upIL
I.0
D.2D
1
1110511306'47 75-094
1.2,3-Tnchluroprop an a
ND up1L
1.0
0.41
1
I1lO5113 MAT 96-16A
Vrtyl acetate
NO up1L
60.0
0.35
I
1IH05113 06:47 106.05.4
IfYx„ chloride
NO u91L
1,0
0.62
1
1110511106,47 7541.4
Xylene(T.1.1)
NO n&
5.0
6.6E
1
1N0611306A7 f330.20-7
s�n•npir.a
491 omo1uvrahen tune(S)
91%
70.110
I
111051110E47 460.00-4
1,2 DId4orovlhene d4 (5)
10. %
M130
1
1110611]06AT 17040-07.0
Toluene-d6(5)
97 %
70-110
+
11 foul 3"AT 2D37-25.5
4600S I 9.If1d+ Weler Anelyllul Method! SM 4500-SW
Svllde ND uWL 1000 100 1 11MWO 13-,U 164W2"
REPORT OF LABORATORY ANALYSIS
Tres nMn 40 ncrW N p-ou d..L.0n M.
Dare 11M U2013 0232 PM P...A IVMM S.-C me Pegs 23 of 10
Paw A"VMCA1■.Mc.r,Iz. P-AMlMa.l 6.Mc.a lne.
P.-An Y711eat I..-,. Inr.
�+p
_ . alit �'17 i�1 �4Lr1'
xis AW M-oaw Raae . 8 . A
f�fan. RC 2i�ee
7M RN.ra Dr
M.M . Nc I8E(H
ppDD A-, &. S.I. 1w
HunYrwla., NC 2W15
_
'^+viYOf m`
[33616?]E931
162e1xs.•1r re
17 Wsgm
ANALYTICAL RESULTS
PmyecL SORRY CLOSET] - MT AIRY (111C)
Pace Proyec1 No : 921779E4
Sampis: MW-13
L.h16: 921"1144001 CoHed.d: 1013011016:30
R-6-d1110111312:15
M.DM Wafer
Repon
pa-aw.
Resu6f thdti LIMIt MDL 11F
Prepared
An*20d CAS NO. Du.1
4EOOCNE Cymnlde, Tot61
AnetyOk 14elhod: SM 4500-CN•E
CyanW6
NO u94 10.0 50 t
1111E11311:16 57-17-5
REPORT OF LABORATORY ANALYSIS
lTH naw1"-t1 npiodus.d..,..A. W.
Mm!I V1 WM 302:32 PM ..Haut eH wrlwn -send Pau A--Vem 9emaA rnv
Pape 24 M 79

Pa.. A"yd.Al
u.rrlP.., Ire.
Par. Atilyea.l
■wOcs., Ins. P.- AnYyu. umlen, Ina.
Pan Anwydud
Asrv1.a., Ina.
Paw
Analyelwl A.mp., Ma
P.s. A.My".l lwlw 1, M.-
/gyp .+,.,,.I
i115 �a.i Maadow Road SwAA
2725 Rr..r.Ma G BaW P.w} Ara SuN 1W
n p A ^.�
]66 E.m M..dc a R..d - WNA
2325 R-uso Dc
s000 %awry Ma Sue. Ipe
�Lfi �/l ICi1 lC�I
Ed -NC 2129E
AMrrea NG .nr 11 NC 71HIM
.• p�L il�iQ I�I
Etlan. Ni -91"
Aiia4ca. HC m6111
Rwl calla. NC 2wya
.rs ..e. fav
I376]47]�B7i
Ia7A176. T17a I1DaIa75 p.702
^`'s *m"
{S3E1127d 71
1a7a 173a-7116
11Oa la liiiAl
ANALYTICAL
RESULTS
ANALYTICAL
RESULTS
Preinr. BURRY CLOSES - MT NRY I111C1
Pln3nd. SORRY CLOSED- MT-NRV [111C)
Pe Pcgecl No : 92117994
Pace Prated Ns.: 02117964
snmpl.: MW-14
Lsh 1D: N21771164007 Ceueofed +WMI11740
RecNwd 1IM1113 T2:15 M41rta' Mtar
Semple: WK1614
Lab ID: 62177964007 Cone cred-
TW 2113 17 40 Reeved: It 001113 12 T5 Mauk' yWw.
Report
R.poa
Parawaurs
Reswis IJrWh LrM
MIL OF
Prcpved Ancgnd CAS No 0u11
Pusmelers
Rasults t"111 LMr1
MOL
Df Praimed
AnrAy7en CAS No. Oust
6010 ICP OIe11Pdwal41c
Analtrkw Method: EPA Rot Preper.Aon
Method EPA 3D10
1290 MAV Lew L...1 Laa d110
AnWy6o.l Method:
EPA 6260
Ane.nonr
NO u04
60
SG +
11ASj 131 D.30 IW0511320:50 7440-36-0
It"-1,4-plplioro-2-bulene
NO "A
100
1-0
I
111p541307:01 140-97-6
kseirw
NO uV&
r0.(t
5-0 1
11 P02M310.10 111051f 32030 7440.36.2
Dlcm.dk... WeRlane
NO uQA
5-0
011
1
11105N307.03 75.71-a
Sulu.,
2E-11 u97L
100
$.0 1
11AYT310:30 i110S1132030 7440.39-)
1,1-0kNornelMne
6Jl uwt
5.D
032
T
11 A57+30703 7544.3
aae76Mni
NOu0A
I0
1-0 1
IND2151SD:30 1l106w::'D 74404"
1,2-OIGllaoelh.ne
NOp1Yi
1-D
6-12
7
TI16571307fl3 1m-06.2
C.rnium
ND ug&
1 0
1.0 1
11A215310:30 "A51132050 7140.13.1
1,1-0IaHa}oelhene
NO ugiL
5.0
O.S6
!
I oou 3079] 75-35-4
Chrwpkun
No ug&
100
50 1
11 N715310:30 $110511120 L50 7440.47.7
da•1.2-DoNoroc11wne
4A uyL
5.0
0-19
1
11 foul 307:03 151-59.2
Cohan
NO ug1L
to 0
5.0 1
11 N7113+0:30 II MOW 1320:50 7440.4"
6H1rIF1,2,CW1hh3 o therle
NO uok
5.0
ode
1
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REPORT
OF LABORATORY ANALYSIS
REPORT OF LABORATORY
ANALYSIS
TN.
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ANALYTICAL RESULTS
Prej"t: Sl1RRY CLOSED . h17. AIRY (l)IC}
Pan Pr0*1 No: 92171994
Sample! MVV-14 Look w! 02177fi6007 CWIacMd. 1W911317:40 Recolved! I1N 111312!15 hla0fr, Vhler
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PrOict. SORRY CLOSED • MT. AIRY (UIC)
Pan pmod No. 92171901
Simple: MW16
Law ID: 1211'7964004 Colfoled: 1N311130040
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REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
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]a5 Eeel+M.daw nvAd - S�io- R 2225 Rn o Or 2e K.ce. Are 5w. 1w
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IMBAT3 2t {em175.1-7174 17w)e1Sida]
ANALYTICAL RESULTS
PfoleclSURAY CLOSED - MT, AIRY (tllC)
ilea* Project No. 92177064
SAmple: MVY-16
Leh ID: 92177964005
C.A.eed: 10)31f13 06:40
R-1ved' tllD111312:15 Menl.' YAK,,
Repwl
Petompid.
Result. LPN%
LIMI MOL DF
Ple -d Anklyfod CAS Nn. Oual
4600CNE Cyanide, Total
A4101Y11CS1 Mvlhod. SM 4500 CN E
Cyanid*
6.3J uq+L
10.0 50 1
11ry011311 35 57.12-5
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
TN. r.pM ... -, a r.pmdlud...c.p n f 1 TI.R r.pod Nee rpl u. n dyad...
D.I. 1III 3an 13 02:32 A45 ,+e-I.I.w ' --I of pace' n_'V t.i $.,-. Inc P.pe 29 vl 79 Date: 11113r1013 02,32 PM •..ran 1n..xAyn con.enl w P.. 5.I.tce. Inc Paoe 10.179

Pa[. A nN ybm
al l4rvkef,ln[.
Paca And71Na18""",
In[.
P.C. An.Iyuaai Sarvlcaa inc.
Pap AnMytle.l
e.rri[.a, ine
P[..
A n.lyllni 5.rvin.-W[.
Pac. analytlul 64rvle.l, Ine.
ay{rvA(3 ica1•
11!EJ.n.
7P3EakM.PdwRo.d Eun.A
77J5ReaneaOr
9eW•+[.yA.. a-i[x
!Jr�^,JJ,
2Eaf[M..W Rn.-l-A i••
221 Rr.• .IN
00100un ayAa S...1W
+1 �r�kkl ia.
NC 7176E
1330y02-M1
A .rrla. NC :0e04
467a 1734-717d
HM rn.f. HC 7W11
(70418759092
•i.a4Lru+atyrrcal'
J ^' '�'�
E,N� f+.: ]rlee
(336)67'ii1971
AN•.rna NG :690[
lax NS4-l1le
IaanVr-P NC ]sore
170g875 DOBT
ANALYTICAL
RESULTS
ANALYTICAL
RESULTS
Prgad SORRY CtOSEO - MT. AIRY (UIC)
Proye[1' 9URRY CL OSEO - MT AIRY (UIC)
P.c. PfDlecl No.: 92117954
PIW Pfoped No 02177064
Sk 10: MW-11
L.bID[ 9211104009 CR114 .W 1QMW0940
R.C9hro,! W111I1312:15 M.hp. VYYt.r
Sampl.: MWAS
LsbiO: 12IT7944001 Cek.dW: UV31130940 R.c1IV/d I1M1111312:16 MIW: V,4ww
Report
RCWI
Fra 1-
Re. A. VN4 UrrO
M➢L OF
Prepared
An*r.d CAS No. QU.l
pwameldn
ft..uM9yMIII LMOII
MDL
OF Plaparad
AnalyrM CAC NO. pup
$010 ICP 4rnundwal9r
Ahalyll[al MaM+6d: EPA 6010 Prapora0on M.Owd: EPA 1010
6219 MSV Low Lda 91 Landfill
An/Iy110A1 M.d 4 EPA 0200
A.Mtl y
NO ugll
6.0
5.0 1
111050 13 011. 30
1110511100.07 7440.38.0
ttW9.1!-D1dNe1e•2-blden9
ND uVk
100
1-0
1
117Q6r1707:76 110-073
Ar9.Mc
NO ug&
10.0
5.0 1
111115111WM
I111W1I OD:01 74411.1:4
Dictwor0A140l omelmene
NO
5-0
0.21
1
11M151130135 I5-71-8
9wk-
13AJ uW1,
100
50 1
1110511309'.30
1110611300317 744VA 3
I,1-Olc•14oroedrne
nl&
3.11 uOIL
5.0
0.3i
1
1V0&15071 75.34.3
emrylklull
NO u9+L
1.0
$0 1
1110 01309-30
111D111300.0 7440-41-7
12-O+cNcrwlhllA
SA uOeL
1.0
0.12
1
11 r05f1]07:75 f07-06-2
Cadmium
NO ug1L
1A
i.0 f
11103V1709-10
111p611700A7 7L40.43-9
I,I Ime oroekhm..
NO u0yi
6.0
9.SC
1
11M75l1307:35 75.31F4
Chromum
ND uq&
10.0
5.0 f
1110N1701-M
1V001I700.07 7440j7-]
d.-1,2-Dldalore.th.n.
i2-] ugrL
1.11
9�A9
1
11IM301:33 A66.69.2
C.b.9
361 uVL
10.0
50 1
1lA3511309:30
111OU1300A7 7440-48J
d.n1-1,2-DICNPfo1M.n9
0.661 ugiL
S-0
0.40
1
1110611707;75 1504ws
Capper
NO up+t
10-0
S-0 f
11(05, 0113E
111p111300A7 7440•SO.6
1)•61ct4moprepone
4.1 uDIL
1.0
027
1
iV A307;36 76-{73
L49d
NO UWL
III
6A 1
111111" 02:30
111007A30Do.01' 7431-92-1
1,3-Dlchlnoprop.ne
NO u9iL
I.0
021
1
11rO5R307:15 142.26.9
NIckN
13.1J vgii-
50.0
5It 1
11iMl, 0930
11106113 00'07 144Q-02-0
22-0ICNropopl^e
NO upIL
1 0
11.13
I
11M511307:SS 594.20.7
S.I.,VU.
NO uV&
10.0
10.0 1
1VDWI309�70
11 MM1130007 776242.2
1.1.OkMPropapine
NO UA
5.0
0.41
1
1VO51130,:1S 663-N45
SIN1.
NO ujat
10.0
5-0 1
1Mul3011,10
1IAWI30QA7 7440.22.4
Cll•1,3.O1cidar0prop1nl
NO [g&
1.0
0.11
1
111Q511307-3fi 10p61.01-6
Th.[kum
NO Uq+t
51
54 1
11+p611a M30
11W67A100-07 7440.26-0
kwn9.1,]•peNvropeaPen9
No WR
1.0
0.29
1
I:1002 o7:16 10061-02-6
TM
Np uqA
100
5-0 1
11pL1701-30
IUM1300A7 744441-5
E6,y6ent.n.
NO "k
t.0
0.70
1
1VW: 307335 100-41.4
V-dt-
NO ug1L
25.0
50 1
1VM309-30
11106A130007 744M-2
Ethyl fnamwylat.
NO upM
10.0020
1
'lift 30735 97-03.2
2FIc
13-1 ugrL
10-0
100 1
11OD501309:30
1 NMI3 11103117 7440484
Hea6d". 1,3db f4dkn.
NO"k
10.0
0.71
1
1Mm1307:35 67-00.7
2 NeaanO^s
NO flpll
50.0
0.4E
1
IApy 13 07'36 5PI.7"
1410 M.reufy
Ah.lylkd Me O,od. EPA 7470 Pr.paf46on
Method: EPA 7470
I0d0"IPMA
NO 'MA
10.9
032
1
1AMsf1307:35 74-18-4
Mew wry
W upL
02D
11.10 f
11"13 MIS
(111V13 M32 7430-97-0
nobuanN
NO PA
100
25.0
A
111p5r13 P7.3S 1543-1
M.6,.crylvnrod.
P1D ugIL
100
Q-93
1
nros+s30, 126.6E-1
1240 M1V Law L-4 L.ndne
Apatybcal Me.wd' EPA 4260
M.el -. CKI-d.
NO ugti
1.0
0.97
1
11/63/13 or76 7l41F2
ACHa.e
ND u0ti
too
1tl 0 1
11 MISN30735 67.64-1
M." m.[hepylale
NO ugti
00.0
20
1
11165l13 07:75 6087fi
Ace1PMYM.
NO U0ti
33.0
22 1
"A151110715 75AS6
4-Me01yi-2-pemanon. (M10K]
NO ugti
100
0.77
I
11103r17 07:76 106.10.1
Acmlem
NO ugti
57.Q
1-d 1
II M161130735 1Q7.02.6
Nophlhalane
NO uyL
10.0
024
1
f1 MM71107116 Pl•20.3
Aay10n11rR.
NO uqa
20D
1-1 1
11MIN13117]6 101.13.1
prupl-M.06
NO ugti
16o
2.1
1
Il ym571107 75 107.12.0
A1114 Wall
NO uqR
100
1-5 I
ItA61130715 107.05�1,
Slyr.n.
ND ugti
1.0
026
I
1110671307:35 10a42•S
:11mu130713:
C9neel,e
1,1 vQ&
1,0
D26 1
11M1511307 15 71-47.2
1,1,5,2.7aVIWorvallan.
NO ugti
5A
0-M
1
63D•2QC
grofnchlorome0,.ne
NO u04,
3.0
0.fi 1
f1M16115 Q7.30 7497.E
1,1,2, 2-T.t. d4 oelh.h.
NO ugti
3A
X1
1
11 M161130736 79.34.5
CromodlWwom.gnn.
NO ugti
I.0
0.1E 1
11MF3l1307:56 75.27,4
T.9acMwwlh.^•
NO v0ti
1.0
048
S
111.1107.3E 127-16-4
&omahrm
NO uq+L
].0
0Y6 1
1V05l1307:75 75.25-2
TaiUma
NO.9&
1.0
029
1
31 MSM307.35 IMM-3
&vinnm9lnene
NO uqR
1DD
D11 1
1SMHi 130735 7"3-a
11yFTd[Nw9heruena
Np up4•
f0A
0.7E
1
AIrp51130735 120•b2.1
2-6ui.non. {MEK}
MD uqR
100
0.9E 1
11105lI7 W:SS 18.93.3
1.1.1•TMdRrv.05.n.
NO ugA-
IA
0.48
1
1WoSf1307']5 Ir""
Carbon d.,49d.
HD uek
100
11 1
11105!l707:35 i5•fi-0
1,1,2•Tflq,lorosYllne
NO uO�L
1.0
Q.29
1
1170511307:75 7 40-9
Carbon NV-N-W.
ND u%I-
1 0
0.2E 1
1'Awl307:SS 56-23.5
TIIdMorw019n9
0.9iJ uprL
1-0
0.67
1
1V051130I15 19-61.6
Chro.ob.^c.Ae
7.7 uyL
30
0.21 1
1VP511301;31 10490.7
TIk4Mrokiaromelh.ne
NOV&
1-0
020
1
1I105113 of 35 7549.4
ChgrPkglan.
MD qg&
10.0
0.54 1
1V0511701M 754W3
1],34,10 1mw-p.ne
NO vyl
1-0
0-41
1
11MI51130735 98-18-4
Chlero6im
NO upli
5-0
0,14 1
11mS1p307:35 67-W3
VROsc11k19
ND uVr
60.0
035
1
1t10511301-]5 106.0E-4
Chkxom.Wen.
ND uyL
1,0
0-" 1
11MI6113 07:35 74-07.3
IM1ryl cNadde
lb uNit.
1 0
OAf2
1
1Vrn511307-35 I5-01.4
Chkxopren.
HD u0ti
ZO-0
027 1
1VD511307SS 176.91.E
1[ylene {iofap
ND uqA-
S.0
0.0E
1
11MYSII707:Si 1}3040-7
1.2-OMKomv-]-uHvropropl no
NO u0ti
TS.D
2.S 1
1VD571307�35 16.12-8
Sunpp.r..
0�. wflad,lnwnenan.
ND upl
2.
371 1
11105130735 1244F1
4-6rvmv6uw9ben7en. 151
95 %
7G130
1
1I7061133 MI5 41*00-4
O9a-Ifi.ne iEDC1
D
0
1
111513075 10S412
1,2.OfcNuP9lrMna•da f$1
102 x
0130
1
A6071317OW07 -0
OiWomom.tlun.
ND up1L
10.0
021 1
M1611aMS 744!1.5
Tol,,.ne-d0(S)
997E
Mi"
1
I IffiW$ 3 07:35 2037.20-fi
}1•D1cNpai1�071n9
2-1J ugvt
5.1
0.30 I
11M15W307]6 9MOt-1
4wosxD Spend. W.E.r
APwy11C.i Med+Gd'
SM 4500-820
1.3-Okhlorohennn.
0.JIJ uqk
6.0
624 I
11106713070E 541.7311
1,4-010, orWenc.n.
241 UpL
10
0.33 1
1IM76130715 IM4d7
SulA de
NO WA-
i000
1Q0
1
Ill071131031 1a49&2Se
REPORT OF LABORATORY ANALYSIS
REPORT
OF LABORATORY
ANALYSIS
TNa r9peK N.1 not k. i.OfeWr[ed. 4a e4rH �^
ul.
T.w h.l ne wCe ft Iw npeW[b. -" n Tw.
pate. 1111/02013 02:12 PM
ren.aAe,.
wtlYn .anfaM of P.p An.hkcv Swvk.. Im
pd31 of lip
p6
Dote. 1 NIwo" 02-32 PM
M.nN el.. M ean..rM 01 P.O.
Af IV*40 e.nluf. Inr
pg. 32 of IN

Pot m AnYymeml"Vi-C Ind. P.ee,.nmrlhMaervlua, ln.
Pr ea A nalyeuVad.vleed, 1".
2m E.om ml.*&C.d - � A
2m R,.ar.tdd tlr
amo9 H �., •.. sue. ,m
aceAna�yticala
Eden. NC 272aa
Aw.raf. xc 75e04
r+,..Ir,.,,n.. xc 7evle
e...P..aer�.
{3361a734W21
nllusw-l+Ts
170.ne75.yw;
ANALYTICAL RESULTS
9u.1-1 SVRRY CLOSED - MT. AIRY (ILK I
Pm" Pl 000. Na 92177954
S.mpl.: MW-le
Lab 10: 0177964006 Collrclad. IOr311 k30940
Recewed: IV31111$2;$5 Malw*vwler
Row
Pmrmr. Mr.
Raaulk IFt1k LkWl MOL DF
Prepmmd
Analymad CAS No. G"I
4 e00C NE Cym lda, Tu1e1
A wo..I Wliivd SM 4500-CH-E
Crmnide
71.3 u%fL 10.0 5.9 1
111101131199 67.12-s
P..r An yeu.I e.rrw.e- k.c. reed A m"w mmml, In.. Pau AMAI rmu1 aeblree, Inr.
aceAr�a)ytrcal • 205 5eN Meenvr KwM A zm RIP rmN w e p w�x+r C -1
Eden. NC 2:2as Aari..a.- Nc 7tlew 1wni.n.n.. N[ z4o7e
i "�•^�^*",.°'� rnal627aai1 (eael3u•717e I704i473.9(ta7
ANALYTICAL RESULTS
polocI. SUARY CLOSED - MT. AIRY I=l
Pace Prvlecs No.: 92177964
Semple: MWd7
Lab ID: 52177594011)
Coached 10r30013 1200
Rat:awad; IMI113 12:15 Mmtrlr: Yy4eer
Ropan
Permm.lere
Fl.-H. J.1b,
LIInd
MDL
OF
Preparod Am"ad CAS No. 61ta1
$4101CP Omundwaloe
Arlalylieef Method- EPA61110 Prrp...
don M.Ihod: Ep
3010
At41many
NO u(yL
60
5.0
1
1M5AI100:30 11 AM11300:12 7440-36-0
A"onic
ND uwk
t0.0
50
S
11165/17 tiv:70 i110611300:12 7140-Se-2
17erium
51-11 uWL
100
sea
1
lIAt1611309:30 1170W+s 99-12 7440.39•S
Baryelum
ND con,
!.0
1.0
1
1 MIW1309:30 N106N30012 7440-41-7
C.dmhtm
NO upR
1 0
1.0
1
11A0511309: 30 1t10611300:12 7440J3.0
Cht"mw
ND uq&
t0A
So
1
11AOS11309:30 t1+061110012 7440�7-3
CPNO
38-5 uyL
10.0
5.0
1
[phone]:30 11f66A1300: 12 7440-46.4
Copp4r
NO uqR
10-0
5-0
1
11A511309-30 1110611300.12 7440.504
Lead
NO ugAL
104
1.0
1
11"1309:30 11f WII 00:12 741v.92.1
Nickel
9.1J uyL
li,0
5.0
1
11Im,1%09:30 1110511300:12 7440424
SNentum
NO d AL
100
100
1
111051309:30 1110611300:12 776249•i
Shyer
ND I- AI,
10-6
SA
I
IIMNa 09:30 4110611300-12 74410,224
TheI1Pm
NO A
5.5
$-4
1
11Owl a0v:30 11f09l1300:12 7440-25-0
71n
NO I+gR
100
5-0
1
1110511309:30 11 ml,300,12 7440.31.5
Vanneitrm
ND vg&
25.0
50
1
11 A05f1309:30 1l1061300:12 ",)" 4Tint=
NO uu&
10.0
f00
1
If A0511109:10 11IOBf13(0;12 744'.4
7470 klarculy
Anmlylkal Malhvd. EPA 7470
Provaro0on Method: EPA 7470
Mercury
NO ug&
020
0 0
1
1IM411313-15 111111319r34 743"7-0
1 Zoe MSV Lvw Levm1 Lr d011
AAAWW111 Wove EPA v260
Aufune
NO upR
100
10.0
I
110611a 0711 67-64.1
A,.I.r."I.
NO -A
5"1
12
I
i"asfl307l1 7&M-41
Aualeln
NO upR
53.0
CA
1
1116511507:51 10 -02•0
Acrylanimid
NO uyL
200
1-9
1
11105+1307:61 107.13,,
A"ohidAde
NO I+qR
I0.0
1-5
1
11MW130751 107-05.1
samr.ne
a.rw .ofL
1 d
0.25
1
1110511307:51 7143-2
&vmoChlDrvmrtl+.ne
NO uyL
1.0
0.17
1
11l0611307:51 74.97-b
&vmDNUllaromeat►rf
NO "YAL
1.0
I1.16
I
11105A130751 75-27.4
&.ZIDIm
NO uyL
3.0
ORO
1
1t105/! ] 07:51 75.25.2
8rvmam Awe
ND KA1-
10.0
0.79
I
110DS 117:S1 74-a3-v
2-Bulmrwn. IMEK)
NO ugR
100
0-0
I
11105/10 071 7y9}�
Cmrbm dkwilde,
NO ugR
100
1-2
1
1110511307:31 7`s1b0
Cemwt lekarhlprlde
NO uyL
1.0
0 21
1
11105113 07.31 56.23.5
Chlorobenren4
a$ uyL
o.0
0.21
1
1f7951130151 106.90.7
ChAaroadla"
ND "at
10.0
0.54
1
100617307;41 7dlI_w3
Chloroform
ND ug4
5.0
0,11
1
1110511a 07:S1 l37.66.3
Chlorpmethmne
NO uq&
1.0
0.11
1
IVO5A f307;51 74-67.3
Chhroprana
NO u9+L
20.0
0.27
1
"tosA3 o731 I249F5
1]-Omeomo-3-phtprvpropana
NO upR
1.
1.5
1
1110N1307.5 96-12•a
OroleRtOcW&&mefhmne
NO uyL
3.0
0.21
I
11A0N13:7i1 124i6-S
1,2-Dlhrvmve ho- fEDO)
NO 410L
1.0
0 27
1
11f05d13071 f0693-4
Oitr0m 4hene
NO uyL
10-0
0.21
1
11*5`1307-51 74.95-3
1 ,2•DIchimoban2ene
2.9J upt
5.0
030
1
1110511307 d11 151-51H
1,3 Pkldorabencenm
ND upR
5,1,
0.24
1
1110511307'S1 541.73-1
1,4-0"lWalbon -ne
4.7 uyt
1.0
0,33
1
11A'05f139T:51 1M46.7
REPORT OF LABORATORY ANALYSI5 REPORT OF LABORATORY ANALYSIS
71 rmvan ma nvtw uaeacn...eep n to TI.. operr mm velw npio . dredr4 M w.
Dot I I o i 3A2o1] 02 32 PiA ..Ii uA m. -flan rar,.da et need An.Irew 5--,. Inr Pogo 31 of 79 bale: r1n312013 a232 pm a.owul n. wnnn --to P_ wiww wnnn., I- Page 34 6170

Pa ea AnY711sa1 Se,vlee., Ine Pa[e Al.lyllul aervl[aIne.
'_'~J"�'• i05 EeN.A.. der, Pe5vn.A :725A W.d ;BW,
.n.-r. _ Eer+2128a .wurw.�eeoa
I330M73d97, (678)25471f6
ANALYTICAL RESULTS
PI.J. t: SURRY CkOSEO -MT. AIRY (01 C)
P e.e pl9jaet Na.: 021112"
Pam AnAlyWcal 0-tca D. Me Pa.e Anal yM[Y %. eaa, M[. Pa.a Amlyc4 1erv1[aa, Ini
eemw.,ay Ara 5...,W �j,.,�+ j + W5 E..1 Me.newp W -S.I.A 22A Arwa.e 61
.Wnl.,wl.a, NC 2w?a ace i171L1iytICa1 F_ M HL 212e6 Aaherpe. NL 2aew
(lwj6Tyg7p2 ' ""�"b'cv1e 137ej07]dFri {67a175a•7,M
ANALYTICAL RESULTS
P..jece SORRY CLOSED - MT. AIRY (UI C)
Pm" Pr.jeu No ! 02177OU
S.mPle: MW47
Lab 0: 92177964010
CoNeeled: 1010W31200 R4cefrad. ItIOT11312-15 Motrb-;Ml.r
sample: MW17
ftep.rl
puomele+e
ReeMle Omit
Llmll
MOL
OF Papered
Anayeed CAS No Oue1
P.,amelefe
9260 MSV L.. L-i L-,IFHI
Ana100.e1 Method. EPA 626D
4600C NE CyaN". Total
U.n[-1,4.drhlor.-2-huWne
NO "wt.
100
1-0
t
1501wil307:61 110-57b
Cyowde
DI[hleroalworemerhe n.
NO uA
SA
0.21
I
1rf0S111073& 75.71-0
1,/-Dbhl.r.slhene
1.1J wWL
5.0
O.S2
1
1N051130"1 75,.34.3
I �•Olr]vwoefh.n.
NO upk
IS
0.12
1
1Imsii307,51 167-00-2
I,S•01[1dor.elnene
NO uOIL
5.0
0.58
t
1$70511307iI 76-15,4
da-1-2-Dlchtoroelhene
3.9J uDIL
5-0
0.19
S
1IM5f1707it 150.50-2
1,­ 1,2-DI.hl.rnethene
NO upii
5.0
0.49
1
1IMN 1307151 15,148.5
1,2-DchlorOP,Rp&"
ND.pIL
1.0
0.27
1
1IM501307:61 76.67-5
1.3.O,chler.prop.ne
NO u"
1.0
0.26
1
IIm?1301:61 14L26-%
2,I-Oichlm.popene
ND uyL
1l.0
0.11
1
111051130751 594.20.7
1.1-0wh,_pmpe.n.
NO upR
5.0
8.e9
1
1110i11307;51 663-wo
c.-1-] 1, "ropr9p.ne
NO uyi
1.11
D.13
1
1i10511]0751 low,-DI-1
vem-,,3-Dl0-pr. pens
NO uplL
1.0
0.20
1
151OS11307:51 10061.0,41
E:111ypenam.
NO w0 -
1,0
0.30
1
1110511307:61 100-414
EOlyl melMcrylele
NO 4&
10.D
D.20
1
11M6113075, 57.53-2
,.a.ude.o- l-3•Euleawne
NO uok
10.0
0.71
1
IVnII3 D731 67�6.1
2-Hemenorle
NO uyi
60.0
0.40
I
iIAW130731 591.70.E
l.d.me lhene
NO ug&
100
D.32
1
J AW30,:51 744164
I.ohulenW
ND vgIL
1Do
35.D
1
1110015307:61 76.03.1
Mekt,owWrOe
NO wa&
100
0.92
1
11105I1207:61 126-ee•t
Melhyl.ne Chi. W.
NO WIL
1.0
0.97
1
11006f130751 70.11"
Melhyl mell.aQylele
NO 4&
30.0
2.D
I
'IMP$30731 50-62-6
4-MOOVl 2-panla wa 11401L)
NO 01;&
100
0.33
1
I11pw13073i }00.10-t
N.phthelene
NO w0A
10.0
024
1
11 F051110731 91.20.3
p,.pig.160e
NO ugk
IN
3.0
1
11M5I1a 0731 107.12.0
slylehe
NO ugA
1.0I1
M5H107251 100.42.5
1,1.,1,2-1.tracM.r.enene
NO u2k
5.0
0.33
I
11 Mw13075 530-20-6
1,1.,2,2•T.tra.Ndoe0lene
NO n&
3.0
0.i0
1
I1I067110731 79-34-5
Atrachloaw9,em
NO up+L
4.0
0-46
I
IIm f130711 127.1&
Aluene
NO W&
S.0
"1
1
sl10w1307751 106•!6-]
I,z,4-i,iMlorohenlene
NO uplL
I0.0
0.35
1
s110sfI30731 I20•e2.1
1,1,1-trlchiW.elhene
NO "&
1.0
0.ea
I
Ilmw13071 71-65-6
I,r,2-TFichl.tc.lt.
NO uyL
L0
I,.29
1
11 A&I307-51 79-00•s
TrhAlorneN.n.
NO ug&
1A
0.47
1
1#OOf1307:51 79-01-6
TrlchloroWwan+alhAae
ND udl
1.0
0.20
5
11fOW110731 76469.4
I r2,3-TtivMwopvpul.
NO u0R
1A
0A1
1
IIM51130731 96-I e-♦
V9pe eaeldle
NO MU&
50.0
0..
I
11M5f1307.51 100.05.4
WO ehTplda
072J uyL
1.0
052
1
11 WI307!51 75-01-e
xvi.ne(7c;W)
ND wpR
5.0
016
1
1IM&I30731 I330.20.7
Slrr.c0ares
4-gromo0upr.heneene 19)
90 %
M130
1
11M5713 D731 4WW-4
1,2-0101.9.010 14 (S)
104 %
70.130
1
1IMV307;51 17Do0-0 -0
Toluene-d61S)
67 %
70430
1
11M57130731 2037$6.5
4690320 9.01de mtes
AndyWW MOM& SM 45DD-=
SIAe¢.
NO up,l
I000
100
I
114403 1310 $1490-26.6
REPORT OF LABORATORY
ANALYSIS
TM.r.p.n
h.e net b.
r.yivdyr:W.. jA-U.
i7U.:IIII U201302:12PM
MT[IrTl1.•.n`.IoccuMOI
Papa Am"W6alrleae.1rc
Plot 35of79
Pete:11113l20t302!32PM
P..a Analya[al a.nlu., i,p.
*+eDF lu..wr'w. sw tm
H W,r.Y[. NC 7e07a
(7M16r&om2
Lib 10: 12 17 7% 4010 CaN"ied; I1)tN?13 12:00 11eeNyed: i 110 1113 12.15 Maw, WIINI
Repm1
110.0. Lhim Limn VIOL OF prepared Anelyme CAS Np. Q0.1
ApwOeml Mall.cd SM 4500-CN-E
NO uWL 10.0 5.0 1 110001311: 19 5712-5
REPORT OF LABORATORY ANA LYS 13
TNa won m" nw be mP.dl,rad, -pi h AA.
,n.lela M A.fl.n _.ere el P- mal W W G_ry .. hrz
Poo. 38 of 19

Rau Anxymc.l i..Nc.., ler. Pa e. AnkNrP.l
i.rvic.., me
P... An xyd•.r 4-1 n., In..
I f_Af`[y�r�f[
GeAnaryr
205 cw)A..d RoW 6yiyA
:1J5 Rh.'H 17,
96op v.ir.C..T n.a Su41�4
L� i
En.n Nc 71 ]i6
AN.re.. NC 2810.
Nunarrvil.. Nc Im?n
f1Mp21-0071
1%23264-711a
17041675 1X91
ANALYTICAL RESULTS
Propel- BURRY CLOSED - MT. AIRY 1LHC1
Pace Propel No. 92$77964
3-pl.: M3y16
Le610: 92117244011 C.IMc16d: tOr29113 1430
R-6.641 II0G1113 13:15
MAilt. VYata1
P[r.mal.ra
Reeu14 Unto
R41m
LI-m
MOL
OF
Pfepamd Anmyl'ed CAS No Owl
6010 ICp 0-de'al.r
An.hueat Mernod: EPA 5010 Pt.pAr
Aflen Mauled. EFA 31010
Arwmmy
RD up4
60
50
t
11 f05rt309:30 tlroa1130O 15 7440-364
A--
NO upA
100
50
t
11MV120930 I1AM1300'.16 A4C-38-2
BOW.
13-0.1 uyt
100
50
1
110051$109: 30 11IMI100.10 744049-3
Barylllum
ND upA
1.0
10
1
$110511309:30 1170611300.16 7440.41.7
t;eplrur,r
ND vy+L
1.0
10
1
"AW1309.30 I?MW 1300:16 74404M
Chromium
ND U9A
".0
50
1
11 105fl 3 09:30 1N001130015 744047-3
Cubd1
ND uA
10.0
5.0
1
1116SI130910 1110111100:1A 74464a4
Copper
NO "Q&
10.0
5.0
I
1$10501309]0 11106f I10010 7440.50.1
Laed
NO uyt
10-0
5.0
1
1110SN30010 1110011I MAG 7439.97-1
NIck.1
N13"g&
500
5.0
1
1110511309:30 111OI100010 7440-07.0
56.n ,m
NO uA
10.0
10.0
1
111061 3 09:30 11/00/13 00:16 7712-+9-2
Sarar
ND uoA-
10-0
5.0
1
IIAMI309:30 I1owa300.t5 744022-4
T11wum
NO uok
5S
54
t
IImul30E30 1110611300: to 7440-?6-0
TIn
ND P0A
100
50
1
IMN1309:30 11r0011300:t0 7440-31-5
V.n1dum
NO uqA
MI)
50
1
1110511300:30 11r0611300:14 744047-2
2m.
NO uqA
too
Ilk
1
11106M1 lW30 I1r0611300 Is 7440464
7470 Ma.aury
M ivk"I U.919d EPA 7470 P-mmlron
M.riod: EPA 147E
Merwlly
NO u01t
020
6.10
1
111041131316 111110P $437 Y439-0-6
400 MSV Low L.a.l 4-"Wl
M.lyoc.l M.fiod. EPA 0260
Aral. 6
ND ug&
100
r6.6
I
1low 304 1.07 61.114.1
Acelpldabe
N13 uqA
550
72
1
1Mall 306.07 75.06.E
APfu1Nn
NO uGA-
53.0
1 6
1
11105rt3 Do 07 107-02-6
Aulph-11m.
NO..GOL
200
1.0
1
111051t301:07 107.13•1
Aryl chl-dn
ND uq4-
10.0
4.5
I
1170503 06:07 107.0'r1
Banitrle
NO uOrL
10
025
1
1110517108.07 7143-2
El-dol.6-tlen.
NO uqk
3.0
CAT
I
110011$301;01 74107-5
9rornpdd4W4n1a Y10.A
ND uWt
10
9 to
T
II001f1706:07 10.27-4
Ellomelorm
ND Ok
3 0
026
t
t1 foul 09:07 70.26.2
9rpmerneln.fle
f4D upA
10.0
0.29
1
11 foul 205107 74-113-9
26.d.nale tM EX)
ND uy.L
100
0.9E
1
t1 M511301:07 71.93-3
Cerbal dlwok"
NO uq,L
160
12
1
1110611301:07 76-15-0
Carton 1.0-M.1te
ND yglL
1.0
025
1
11 foul 308.07 56,23.5
CnkaobeMbne
ND uqA
3.0
0.23
1
11 Mail 306:07 106-907
Chic'""we
NO uoli
$0.0
0.54
1
Wftl30/A7 76.00-3
CN. M.-
ND uqA
5.0
0.14
1
IIMW1308E7 67 66.1
ChPa-than.
ND PyL
I 1
0.11
1
111o5113 OR A7 74-07.3
Chrorepren.
N0 rryL
20.0
0.27
1
1f745f I301`07 128-I&S
1:1pweme•YonlarPpropan4
NO ug1L
13.0
2.S
I
1110511306A1 11.12.4
D.n.omocnwromen.ne
NO Ppi
30
021
1
1710S1$101d7 124-40.1
12Oldnm-an.(EDH7
NO uA
10
0.27
I
II'05M30697 f06.193.4
Dd+r p..wm461.n.
NO.rp6
100
021
1
111051130E-07 74.95.3
1,2-glcnlrvobuuena
NO OWL
4.9
0.30
1
11105111 W07 WWI
I,3-D..IAoroben4erle
NDW&
5.0
024
4
11MW1306:07 541-73.1
1 A omm.oh.t'rana
ND uq&
1 0
0.33
1
41105/13 06!07 106.46-7
PAee A�.Italta16.ry1[fl, M4. P.C. An."-l.WlS[s,
M[.
•
795 E.x Meede� Rees s .. n
IL Nrv. W4 d
aceAnaloicai
F don. HC 7T2a0
AM.ra.. 1.0 26601
• "�"��"'^'"
f136H274925
[a 71I1154.117a
ANALYTICAL RESULTS
Propel S11RRY CLOSED - MT. AIRY (111C1
Pace Prvpd NP : 92177964
P.q Arylydur Mrylree. In[.
96001[xrurAw 5uw 100
rWnMrefYe. NC 79674
I fOt y1T5-061R
Sempl.: MIN-16
LAb ID: 12177964011
C.H.dad1012993 14'30
R"iWod 11101113 12 15 M"b, VYa3H
R.Porl
PO.rneler3
R.10% 111d%
Ulna
MOL
DF
RIIJ ad Mely-d CAS Np (WW
0280 IM 9V Lew Level Landfl ll
M6yTrrar M.1hod. EPA 6760
Ir Oa-1
ND u0A
too
1.0
1
1170511309.07 f10-57-6
00I.rnd6unrvmemane
f4D uyL
50
021
1
11105113CAW 7671 a
1,1 pichimoalhane
NO uO&
5.0
037
1
11MVIs06fl7 15.04-)
0-0khi-wh.na
ND u0R
1.0
012
1
1110511306.07 f07-06-2
I,I-pknlwuelhene
NO ORA
5.0
056
1
11105111 as 07 7&154
pa•12-0chtnrparhane
NO OPM1
5.1)
01111
1
1IlOSn30"7 IWW2
4ena-1,2-L3lcldorP.9pn.
NO uWL
5.0
049
1
111owlsa@07 165-565
I,2.Okhlprppfppan6
NO upA
1.0
0.17
t
t11051130807 78.87.5
I,]•Dkllroruproparp
NO uqA
1 0
0.20
1
111ftIs 01:07 142-70.0
2,2-0.dllpr.propane
NO uq,L
$6.0
0.13
I
IImi130E:01 504-207
1, 1 •pkhlpfopr0pan.
ND uqA
S.0
0.49
I
111010106:07 5634"
01.11,3•DkMoo¢ Pp.n.
ND uqA.
IA
0.11
I
11foul a06.07 10061-01-5
Or-1,3-01eld... prepene
ND uq,l
t 0
025
1
11106N30107 10061-07.6
E41Y910174r1.
NO uqA
$.0
0.10
1
1110511106.97 100-41-4
E1hy1 melh.uypre
ND uqA
f00
0.20
1
011051114"7 91.61-2
N9.6d1Wra•t-1•Wlad.ne
NO u0A
100
0.71
I
II70611308.07 874E-1
2-H.a.none
ND upA
50.0
0.4E
1
111051130A 07 591.7E-6
Indvm9man.
NO L*k
10.0
032
1
1T10511301147 74 W4
IaeGrmnd
NO uOIL
100
35.0
1
WON 1304d7 74434
M.M.ery1mN1.
ND "Oh-
100
0.a3
f
11105/1104 p7 1211-0-Y
L141h "d CN010
ND uWL
1.0
0 97
1
1110M10407 76-W2
M46g4 meYlommil
NO uµL
30.0
2-0
1
111051130887 40$23
4-A1.irtyl.Z-p.11regma(M111K)
ND uyi
100
C-13
1
1TM6013 do 07 106-tb1
NAphlnalAne
ND UP&
f0.9
024
1
WM0130007 01.20.1
PrePIWLNM-
ND upA
ISO
3.6
1
1110511301:07 107.12-0
Wong
NO utpi
1.0
0.26
1
1Iml301.07 100-42-5
1,1.1.2•TekadNaraarhane
NOu01L
60
0-33
1
1110511301U7 aao-2o-a
l,s,2,2•Tatracnlw6elhen.
ND uyl
3.0
0.40
1
1110a1130197 79.34.6
Ta IrmcfINaelhmre
ND tOeL
1.0
0.40
1
1110511306A7 t27-16.4
T.IWne
ND uoA
t 0
016
1
11 m5113 0697 lca-ml
12,4.7danlapbsnlene
NO u9'L
10.0
0.35
1
11ID51110907 12092•I
1,1,1-THchl-kh-A
ND u91L
1.0
0.46
1
11/05113 01'O7 71-354
1,1,2-7rIphNNoaM4I1e
NO 40A
19
020
1
11N51t30601 70.00-5
ldNmu 0- 7r
NO u0t
1.0
0.61
T
1110&ta O8.07 7ml-m
T-1100 r 11 o omalh.ne
NO u1yL
1.0
020
1
tI M511306.97 IF 19-4
1.2.371Id11ordprod.n9
NO UO&
1.0
041
1
11105f130807 96.18-4
V.0 .-W.
NO uyt
50 0
0 35
t
IIIt" 3 03.07 101-05-4
V..0 dAWAS
NO OWL
1.0
6.62
1
1111oull 0607 75414
Xv%ns (ropy
ND "CA
so
a m
1
1510aH 3 0a97 1330-20-7
4 &omoAVannmx.ne (S]
96 %
70-130
1
11f0UO 3a.97 460.00.4
1,2-plcl+lofae}h.na-d415!
104 %
70-T30
1
11105113 CAW 11060-07-0
Toluene-d6(5)
95 %
70 $30
1
111061130607 m7-26-5
450052D 5u1111. Walar AANM.c6 M.QNd. SM 4300-520
Sunda NO 00A Iwo 100 1 11=111020 11409,25.9
REPORT OF LABORATORY ANALYSIS
I rf. �.roA A,.. nar a r.p.oe..rw ..nr• n fw.
Owe 11111r201 S o2.37 AM rr0u1 ar erirn ran..nt 14rr.u. Mc P.p9 31 Of 76 Onto 1111102013 02:32 PM
R E PO RT OF LABORATO RY A NALYSI S
Taw r.Pln.nw -I a,.O-k[ed. e.uor r. ko
.xnaw Au -M%. ra k or Para M.fy.rx S....0.. rn<
P.qe 36.170

Pave A n.lrtle.l emwu,Inc. Paw AnalyOen Eenlw., Inc. Pi n Analrun l eanlaee, Ina.
aeeRnalytrcal • 7G� Faa Mwww SVIN A ZZ S Rw.c 2 9801.E y M. SuN
[wn. HC 7:7aa Ad..riN, H,: aeep. Ih,.d.r..w.. NC tag+e
�6a]dH21 Io2at25.-717o Ii0i1E7 S0092
ANALYTGAL RESULTS
ProJect: BURRY CLOSED -MT. AIRY IV IC}
Peca Pryrcl No . V2117984
SNnplr: MW-1e Lab ID: i2177f64011 CWkctad- IDQ911314:30 Received: 1110111312:15 Math: Mi.,
Report
P.1Am.ten Re outs U,Id Limit MOL OF Prepped Awdyaad CAS W Q.W
460pCNE Cyanide, Told Andylkd Mett.od. GM 4500-CN-E
Cyeldde ND ugh 100 5o t Tf1701131058 57-17-5
REPORT OF LABORATORY ANALYSIS
i lr. •.wn.nu n:, r. irre..c.e...-.A Hr
Cie 1, 1111 N201.30232 PM .nFmAine-% wnaent ar P.c..•...iyc 9.naP.r. 1. P.pe 390179
PAC
e A"ytivel ernine. Ine. P.n A"yuval Hrvlaw- Inc. Pa.. AnN yuul�.JceAnaVical • M E.w i4w&. Re.e - SuN A 22] RrnNe. Wp0 , A }uN r W
Ed.n HC ZZ Zee Aw.d.. HC xeew rrn., HC ]50ia
'^. p.er441 Rm IS]e)621de21 i62e 12aa-i5 i6 E1Q41e7S9092
ANALYTICAL RESULTS
PI.I.n SURRY CLOSED - MT. AIRY MCI
Paco PraJ.H No 92t77964
SamPlr: MW1f
Lahlp: 4217711e40t2
CeN.n.d:
1012911117.00
RecelvrdIIMI113 12.15 Matta: KYler
Repcn
Purmrt-
R... It. Unit.
DOI
MOL
OF
Pr.pmd An.lyted CAS No. 0-1
i0to IGP OMu 41-4t.r
A- yl.o.1 M.IMd: EPA 6010 P.eperaW
Method: EPA 3010
Antimony
NO upi
1.0
SO
1
1f A)57130910 11106f 150019 7440-.
Areerrt
NO ""
10.0
5 0
1
11+037131 9.70 71108+1 ] 00 19 7440.35.2
sedum
]4,7 J uA
100
5 0
1
71 451I ]11+46+T] 00 19 74i0.39•]
Brrythl.m
NO ug+L
1.0
1 0
1
11105/13 0910 11f06i%3 00:f 9 7440-41-7
Catlmlum
NU uA
I0
1.0
1
11fO Sf 1309.30 Ii2a 1300.10 744"3.1
Cin A01
NO ug+L
10.0
50
1
11 M"I S g91C IIZ0 1100IS 7440.473
Cchall
t4O uA
10.0
5 0
1
11005013 09:30 11+06113 00 19 74484E-4
Copp►r
NO uA
10.0
50
1
ttf05+1309'30 I1+p6113 CIO IS 7440-M-8
L.ad
NO up-
10.0
52
1
W05f13 09 30 1/003/13 00:f 9 7439-92-1
Nickel
NO uA
50.0
5.0
1
I71051130930
30930 11106/13 00 19 7440-02-0
Sal.nlum
ND up4
700
t0.0
I
1710$f1309:]0 11/0611300 s9 77E2.a .2
Sihn
NO np-
10.0
6.11
1
1t10j11309.30 11+0611]00.19 iNOd24
Th4luuln
NO upt
SS
5.4
1
I110"1300:30 11+05H1011.t9 74402E-0
7I.I
NO gyti
t00
SA
1
11 A751t]0934 It10611300.19 7640 1•S
V.nrdlum
NO ugA
25.0
50
I
I1dy5+i309:30 i1+0E11300'79 7140622
Zinc
NO �yt
.0.0
t00
I
11 e751$109:30 IImal1300: t9 744066.6
7470 Mercury
Analytical Momod' EPA 7470 Prvparn0
Method EPA 7470
Mercury
NO ugL
0-�0
010
t
111050110:15 1111211176:26 14310-5
a.60 M8V Low L.vat Ondt111
Andyw&I Med d EPA 1260
Aoelw,e
NO upn-
IQO
f0.0
1
111Q5+170827 eid4-1
Argil-14R.
I+O ug•i
S5 Q
2.2
1
111m tie 2S•05 8
Auolain
NO upL
530
1.A
I
11105f130813 IQ1-02-6
"I.Nk'ft
NO ug.4
200
1,v
1
1110:" 11123 707. 1]•1
Anvl40rlda
NO ng&
100
1.5
1
11f051130e27 107-05.7
aenrcne
N4 uu+L
10
0.25
1
11 f051t306:21 7t-47.2
Bromoerllw a me than.
NO upi
3.0
0.11
I
VI+051150923 74-97.5
are roarhto,a,l,en,rna
NOupi
1.0
0.14
I
11101130a 3 7S.27.4
aromotclm
NO up1
1.0
0.28
1
11005010e23 7Sx'.!-2
13ro,rwn'ed+ane
NO MgR
100
0.29
1
I1 f051t1 M213 74.83.9
2-8u1a�0.rr(MEW-)
NO ugti
100
C.96
1
1100511a 0823 1e-91-1
C k'bo+, dlfulede
NO upL
tOp
IT
I
11+051130823 15-13-0
4r.hw+ l.u..1.1.1d.
NO uget-
1 0
❑ 11
1
11105/13 06 23 56.23-5
Chkwhentene
ND upL
30
111
1
11+057110525 toe-9D7
Ct'Z.Wene
NO ugx
10.0
0.54
t
71f051t]Q623 75-00-3
ch.- m
NO -0A
S 0
Q 14
1
IIRM130823 67-68-3
ChloromaE.enr
NO ugfL
1 0
011
1
It A)SH 3 011 2 3 74-871-3
C1+Ioroprene
NO uglL
200
Q.'
1
111p5+130423 126-99.6
I r-0rbrwno-}.4-prcprne
NO uq+L
13 0
2 5
1
1119Sf1 S 0E 23 W-12-5
OlMvmochlo.omvlhenr
NO Lv
30
; I
1
1tN5+130E23 124461
I •OiElomwdlene lEp6J
NO ug1L
1_.0
1).27
1
17105f13061] 106-03-i
tit-inalh.nr
NO ug+L
II .
0.21
I
11105+130.6 74-95-3
1)-f]IcMwoilent.r.e
NO ugti
5.11
0.30
1
17165+Ovil 9350-t
I.yploldu d,e ni.na
NO up1L
5.0
aY4
1
1Tf05+1308:23 541.7y-1
f 4.OicMl+ahenavo.
NO ug&
1 0
0.31
1
1100511300.23 f06-46-7
REPORT OF LABORATORY
ANALYSIS
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..PaceAnalytical'
P4.. Arwyd..l i.me.r, ln. P... Awydwl her .,. M.. law Anelytl[e1 Nn1[eo• Inr-
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I076)m?24W21 I8MNSA-7r16 fINA75-001p
ANALYTICAL RESULT'S
Prejecl: SURRY CLOSED • MT. AIRY MCI
Pa"Plajecl No.: W177M
S.Mp1.; MYy-19
La410: $21779W012
CWl.mml 10Y M31700
Received! 11P011111215 Mom; Wow
A.pw
Premews
Reouke L)"m
LImR
MOL
PF
Replred An*"d CAS No. QV0
62e0 M5V"w L.rol L.ndlpl
Analytical Method EPA IlM
A ane• 1.4-Dlchlwo-24w1ene
NO 0g&
t00
1.0
1
11105r110o23 11p-57a
OlplbrodWvrwn.IMn.
NO"Q&
5.0
0.21
1
111051170627 i& a
I,1-dclilwo.111eM
2-51 -A
S.0
0112
1
I'm al 75.34.3
I,243ichlordedlerl.
NO ug&
1.0
0-12
1
1110 1130023 107.06.2
t,t-OcaAlu'IIwR.
NO n&
5-0
0.56
I
11105f13 08.23 75.3"
4..1,2-Dtchte..tow .
M uWL
5-0
0.19
I
Il l03f110:21 15a54.2
pun•1,2-owilafwmene
NO ugA.
9-0
0-49
1
11l0520211 156-11L5
1247.0-I 1ppalla
NO .90-
1.0
Q 27
1
1100510 0,123 76-67.5
1,3-DlcZaptopena
NO uWL
fA
0-2a
t
MOM 0621 142-Mil
22-Dkmwapr0p"
NO u0R
1"
0 13
1
111054130623 M-20.7
t,1-0Ichi QowcP.n.
NO 404
5Q
Q-49
1
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w-1,347whI.twopene
NO uQiL
1-0
0-13
t
111057t3 all 10p61.01-5
ION,,-02-6
ban.l,3-pnhwopapene
ND uyR
1-0
020
1
Ili0571706:23
Eglylbomone
NO uwt
1.0
0-30
1
1N0wjl30:23 10041-4
E 61y11ee1hedlytAl.
ND ug&
10-0
on
1
f1f0511306:23 074i3.2
Nrxedywo•I,}Weedl.ne
"D R04
10-0
0.71
1
11 M511300:23 61a63
2-He.wlvne
NO u04
10.0
0.46
1
1110511106:23 S9t-76.6
IOdRmrrirna
ND ZL
1020
0.32
1
i1fmla 0623 74•l6.4
111.hulrnp
NO uOIL
100
36.0
1
I lmul1 0023 7b63.1
Melh.cryl-Isk.
NO'OIL
f0o
0.93
1
1N05H30623 126-947
SM01y=(;W.ld.
NO u0tl
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0.97
1
11f051110621 75-09.2
M.1hy1 m.Ih.aytat.
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30.0
2-0
1
1110511306:i3 SM24
4•M4&)l.2•pdntll .IM101q
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100
0.33
1
timsil30521 108.10.1
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00.10
5.24
1
11f061130:23 91.20.3
P,.pknr411.
NO 1,OlL
160
3.6
1
11f05l13023 107.12.0
Sly -one
NO VylL
1.0
1125
1
0-47
Iilmli30623 f0-5
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NO ug&
5.0
0.31
1
$ m513 a623 630-204
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NO wa
3.0
0.40
1
$11051130623 70.34-5
TMt.r711w6mm4rte
NO uQlL
1.0
046
1
111051130623 127•tb4
7olualle
NO 19A.
10
02i
1
1WIWI30623 f06.69.1
I,2,4-irinhWrobenaene
NO ZL
$0,0
0.36
1
11 Mul30623 1M82.1
1,1,t-ideNeaae/14nr
NO u0A
1.0
6.46
1
1t105f130643 71-SS•6
I,t•2• Tllchbluelhenr
ND u0&
1.0
0.26
1
1t1951130823 7F00-
Trkhlao M-
NO ZL
1.0
11.47
1
111061110823 79.01-0
I}kh*011u0r0m.Ihwe
NO 4O&
1.0
020
1
1t10y11300211 7""
I,2,1-Twwwrprcprne
ND ug&
I.0
0.41
1
111QSn30621 W-l"
Vinyl e..Ielr
NO uU?L
50.0
0.35
1
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I
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kylrn.{Yploq
NO uG&
5.0
066
1
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90 %
70.116
1
15N51130623 46040A
1,2-Dichiww0lend-di ISt
100 %
70-130
1
11AW 30623 17000-07-0
T.W.-d8 (9)
96 %
70.130
1
11IM130023 2037.29-5
4600E 21) HOhdo W.I.,
A-yl ,el Method SM A5(l0•S20
Sdidv
NO uUIL
1000
100
I
11M5l13 10,29 16401545-6
REPORT OF LABORATORY ANALYSIS
iHe npert Nrl ml M nproAc.d. rnapl n 1,r.
0m. 11fI 12011 02 32 PM whorl d.. wmon rmunl of P.,. Aryllacol 6.Mre., riot Pogo 41 el 70
P... Aral0.0 NM..., Ier. pees Anely11f.1 3-1[.a, In e. Po[. A..lyi1.[I 6e1vi[.fI in.
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n'ee A -01.. NC 7ee61 winl.+aHf NC 7e076
016)6734021 1e7aIM-t17e (704pli9
ANALYTICAL RESULTS
P'.0.1: SUR RY CLOSED- MT AIRY WIC)
P.Ce PrO�rc{ No: 92177964
Sample: MW-is Lab iD- 12177984012 CoUEled Imv0 t700 Re cowed 11 lD11131215 M&Wc W.ler
Report
paf.melme R.eWIe LMlte L1mN MDL DF PtepMed Anelyled CAS N0 Owl
4600cNE cvA"kd., TetA1 Analylwc 4 Method: SM 450"N-E
Cyentd4 1.4J r,yi 100 $p 1 11110f131059 57•12-6
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
ANALYTICAL RESULTS
ptq*ut: BURRY CLOSED - Mt. A{RY ful Ci
P.A.1 313RRY CLOSED - MT. AIRY (I11C)
Pan Pio)ed No.. 92177044
Paee P..d N. 92177964
brnple: III
Lab 10: 92177994013 Ce9acled: IQW?l314AS Rom"d: 1110111312:15 Motile! View
Sample: MW20
Lob 10: 121171144413 Calleded: 1WSW 1314.05 Racalred: 11 M 1 i111215 Makk: Valor
R494
R.Wrl
Penmafere
flewlla War LLd1
MOL OF
Prepared Annyzed CAS No, Dud
Paramalen
Re.ults QN13 L6mil
MDL
OF Prepued
Analyzed CAS No, Owl
90101CP Oroundwalar
Analylkal Medevd: EPA 5010 Preperellm Malhod: EPA 3010
8210 MSV Lew L.-I L-.nellih
An.lyilcal Wth.d. EPA 4260
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11.0
5.0 1
11,0501309:30 1V06l 7440-36A
uam-f,4•pch4erv.0•b"1.ne
NO ug1L
100
IA
1
I7M611308;40 110.67-6
Area l-
ND ugiL
10.9
6.0 1
11M511309:00 1fI04171 Dp32 7140-7d,2
plehkfvdauvrwnvh.n.
NO uWL
5.0
0.21
1
I IJD5177 0a:40 W71-a
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I110WI 109: 30 11, 117440.41.7
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I1IDWI009:34 Ili"a"IWI2 7440-43.0
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I
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10.0
SA 1
11MW1109A0 111011110032 744047-3
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5.0
0.10
1
1IM51110940 158490-5
Copper
NO VUA-
10.0
5-0 1
11 MW1309:30 11 MW130111 7440.50.9
1.2•01ch1wopropane
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1.0
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1
*1105113 Ill 741.67-5
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NO "lilt
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NIekol
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50.0
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11MN,109:]0 1..30032 7440-0x4
2,2 Dithl.rawcpane
NO u04
15.0
0A
f
11 MU 306-40 594.20.7
SN4nldm
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10-0
10.0 1
IIMY S09;30 flPON 300:3i 779219-2
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1
11 MW110a 40 $0061.01•S
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I1M511308460 9743-2
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0.71
1
IIM51130840 87.68.3
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NO up+L
60.0
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I
3 4
7470 Mercury
Analytical M.Ihnd EPA747p Prepara9dn Method: EPA 7470
Ivdemeinane
NO uy1L
10.0
0.37
1
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11N571311115 1111211378:34 7011-97-0
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100
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1
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100
0.91
1
1,1108111D1'40 121-1b7
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M41n71.n. CNo.ld.
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0.97
I
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Acetone
NO uyi
1DO
10.0 1
11 My11309%0 67.64.1
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111D51130J A0 ifA7-x
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11MSH301:40 74.97.5
1,1,2,2•Te oodllwoe hone
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3.D
0.4D
I
11M611301140 10.34-5
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0.16 1
17M511708,10 75.27.4
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4.44
7
I7MSn3 pe;49 127-15•4
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3,0
0.75 1
11M5i1]08:40 71F2b2
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1.0
O.26
I
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NO upL
10-0
029 I
11104/13 Oa;40 74JlS9
12,4-T1691dwvhanrer.e
Np u4'L
40,0
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7
11M511306:40 720.62.1
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1.1,1-TrKhlavrlh.ne
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LO
0,46
1
11 MWr 309:40 7"S"
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1-2 1
1VOW1306;4a 73.15,9
I,1,2-Tr1c711aroelhana
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029
1
t1M511306:4D 79-00-5
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I.D
0.47
1
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3�0
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11 M511106A0 10a•90.7
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1.0
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1
17M511306:40 75-09.4
cnlwn.m4ne
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0.54 1
11MINI is 06-40 75-00.3
1,2.1 Trltlllvrvpropane
NO uyi
1.0
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1
11MW1306A0 9¢I8-4
ChloraWrm
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5,0
0,14 1
11 M61130aA0 67.44.3
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NO ,plL
50-0
0-35
I
111051:306:{0 I0d-05.1
C11lwana9lane
NO uWi
1,0
0.11 1
11MW1S OaA0 74-67.3
"chlalde
NO Wet
1.0
0.62
1
11M511306-40 76-0I-4
Chl-1 ena
NO'WL
20,p
027 1
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xylene I7vl.lj
N0 uq4
5.0
0.66
1
74rp511S 0e A0 1330.20-7
1,2-Olbrvmo-1 ddvrapreprn.
NO ZI
13.0
2.5 1
11MW1308A0 06.12.9
Snreoga/e4
06 %
70-110
1
11o51110e40 46Q-0D•4
Dh.rna naom.h.ne
kD.pl
3-0
0.21 1
11MWI30a:44 124.481
C10vrvelhene-tl4 [Sj
I2-Qkthk-Lhanr-d4 (S)
105 %
70-130
1
7.0
1V0511] 08:40 170d00.5
1,2 DWomvealen.IEDeI
NO uyi
1.0
0.27 1
11MSiu DIIAD IW%- -o
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9e %
70-13Q
1
11lI18173 05:4Q 2077.26.5
Dab-nn.lh-0
RD u9R
10.0
0,21 I
11M5113 01140 74.95.3
1,2DiC1lw oo.nzene
NO upiL
8,0
0-30 f
11l06753 06;4D 95-50-}
4600S2D Burfld. yWlar
An.tyllul Me4.od 9i: 45Q0.SZp
1 S-DI.W-b ...
ND "lift
5.9
0-74 1
11105/13 DeAO 547.11.1
1 4-D,C?j.*an2.ne
ND ug1L
1.0
0-33 1
11 OD511a 06%0 $06-461
Sulade
NO ug1L
1000
100
I
}1MW1311'30 1a496•tS•a
REPORT
OF LABORATORY ANALYSIS
REPORTOF
LABORATORY
ANALYSIS
rlaa,aPvn.n.r nct ca
r.pr.ducad.., uIA
M VI
rl..,.Pan Maw W
rsped-d..te.pe.1
M.
Dole. 11013120130272PM
.ee.r..ea.wrltbnpy,e.nlWP-Anelraeya-rI-
P.q.43er79
Dale
Page449f79

2cekulytical'
7D5
d- flood S.. 7 ..[ M..A 715 R-x Dr
lid.., MC 211s9 AN wn., HC 78e1N
. •••"�'"�+
111e1erla97r le7e175+•7+1e
ANALYTICAL RESULTS
Pr.J-t STIR RY CLOSED - hit. AIRY (UACI
P.- Profe.l Na 92, 77964
P.e. Ae.lye.4l 9"W.j, Ar4.
SON 1r"Aye &urti }00
i WWA., Nc 28WO
f94A754M
3-4A.: AINf20 Lah1O: 0"77*14013 Couecled jWA(hr1114;i5 RO,calred- 11101f1312.$5 AAwy'Awer
R.por1
Pwm.l.ra R-WM Wke Limn MOL OF PropM.d An6lyted CAS Na. Oual
160001E OyAMd., TWA! An.lylc.l Alelhod: SM A500-CN-E
Cyamd4 NO ugt 100 5-0 1 IUM131}120 157.12.5
0.14: 11113f2013 02.32 PM
REPORT 0F LABORATORY ANALYSIS
TM r.pwl Y.M rwi W r.geOCW,.nvpl n Y
er.._' Na w.uncwrr.nl el Pew A Iyc.I RS+.wr. elc
aceAm)ytiral�
I ..rr�nm
Pae. AnMlnl- H.r.lr.r, [nc. Para An. OW 6.nI..S, I" P..a
705 E..i M..dc. ReW Surer A IRS RnHWa Cn 9e'.]e lunu7lwe Sur. IW
EJ.n, NC 7I78e AYI WM.lrC 76H61 Hunl.rs.il.. NC 2H 7'
I.11M1M7]-0OZI fe261 u-111e I1ti Ie75 om
ANALYTICAL RESULTS
Prnl.cl SIIRRY CLOSED- MT AIRY rI11Cl
Pen prol.ei Na. 92111964
5amp1.! M49-21
Lah1R: 62177e64014
C0.d d. }013011117: 30
R.celred: MU111312:15 Ma11v lelelar
fl.perl
P.r.melera
Re.lAl. 11Nh1
L#Mt
A1OL
Of
Prepued Maly2ad CAS No. Owl
4010 ICp Oroun dwal.r
Ah. ylk.l M."d: EPA 6010 P f pafsWoo
Matnad: EPA
3010
M6meny
NO uO/L
60
5.0
1
15705f1309.30 11f061130-0'3d 7410.34-6
Are. nk
NO u01L
too
5.0
1
11106f1310, 0 1110R11300:3d 744G-36-2
6NWm
619J uprL
}00
SO
1
111151130930 11f06A}300:36 7449-W3
Beryllium
NO W&
1.9
1.0
1
1N0511IN 30 11 f0611100:A 74404,'?
C.drTo-M
NOuAi
1E
1.0
1
11MSH3 DO 3011 MO,130ot l'"0a3-0
CnrQ-
NO uQA-
106
S.B
1
1fAif 13 DO 30 1116613 0016 744"7-1
Cotall
6.4J uyL
100
5.0
1
11f09 1309:30 }I M1611a 00;35 7440.4E-4
Capper
1A uyl
1010
SA
1
100511309;30 11 MM11100:16 7440.56.E
Load
N4 uyt
10-0
5.0
1
11111f13011:30 1:106H300.36 111:-12.1
Nickel
NO uyL
56.0
5.0
1
I110511 ] DIM ,POW am 744E-0z-
SNenyrm
NO u01i
100
10A
}
111P5113 On }IM111300.36 7762.4E-2
SIN.r
N7) u9R
19.0
6.9
1
I1f95f1309:]0 }1*11, 300:06 1440-22-1
Th.ltum
NO u9A-
S.S
SA
1
11f0511309:36 11196f1300:. 7440-26.6
T�
NO up4
100
SA
1
11 A35r1109'36 }1Mv1300:36 7440-31-5
%&..do.
NO uyL
26.0
60
1
}11061130 31) 1570611 100:ae 744062.2
Ikrc
NO 49f1
10.0
10.0
1
11 M1Sf1309:30 1110611300:36 7440456-5
1470 M.icury
M.Iy11e.I Medwd: £PA 7470
Pr.p.nW.d MoMoa: EPA
7470
U.rmry
NO40L
0.20
0.10
1
1}10511314.15 1VIVIIISM 7439.67a
6260 M5V Lew Lrr.I Landflil
An.lylkar M.tlwd. EPA0760
Ac.1rn.
NA NIL
100
1G.0
1
111E5ry306.S0 5 -04-1
Ace1aN0Re
NO uyL
550
22
I
1110511306:56 75-OS•B
Acrel4ln
NO up1L
53.9
1.4
1
11MP,304% 197.02.E
AcrvldWWK.
NO up1L
200
1.6
I
111061130E-56 107.13-I
AV ehieride
NO uok
100
1,6
1
11105113065E 10745.1
BenierH
NO uyL
1 0
a.25
1
111176113063E 71.13-2
HrerrwclNwometh.ne
NO upM1
Oo
0li
1
1}M7W1306.86 74.97.E
910m015dRaoma6lane
NO UA
1.0
0.5E
1
1#96f 13643E 75.27.1
Brame}crm
NO uyL
3.0
0.24
1
1$XW 1504i6 75-25.2
&orn9man.na
NO u04
TOO
0.29
1
1NO5fl3 es'56 74.63.5
2-&d.non.{RACK!
NO uyL
100006
1
11105113003E 7473-]
C.rhan dlulEde
NO u04.
190
12
1
11195ff30E.56 M15.0
Carton i.t.dgwiq.
NO u9&
1.0
6.25
1
11M67130E.So 56Q15
':No.o6anxa no
0,sw vyL
3.0
033
1
1110311306:56 10 ,90.7
C1NOro.ln.n.
NO 69AL
irk 0
0.64
1
11106113 06:56 7500-3
Cdlur.W.
NO upi
50
0.14
1
1110011306:50 W7 Wi
Cllwrom441anr
NO L*t
1.0
0.11
1
11/06/13 06:54 14-E7-1
C111er.pr.n.
NO u04
.00
0-27
I
11 M15111011 }26-99-4
}.2-0luornd-3-dx0roprvpana
NO uyL
17.E
"
I
}IM51130666 96.12.E
Otb'p achloram.lhanr
NO U0A
3-9
0-11
1
111051130E-58 12446.1
12 Oldomo.m6n. 1EOS1
NO uyl
1.0
0.21
1
11 M7N1300-56 100.93.4
DNoMm.1h6n.
NO up0
10.0
011
1
11 MI51130636 74.9513
12-p�chloroh.nien
NO uyL
5.6
016
1
11105f1306:56 95.66.1
1 ]-Ok4lwoL- :
NO uyL
5.0
024
1
1TIM 30646 541.7Y}
1.4 Oknloreten7.n.
1.1 uyL
1.0
0.33
1
111o6f130E.56 06.4S•7
REPORT OF LABORATORY ANALYSIS
ilw rµrert aM1M rW W nryeWnR. wc.p[ h A•.
Palle 45 01 79 Gel. : 11113,7013 02 32 PM .#W rn. wr.elnc.na.n1 el r.o. hrlyAeN U-., or
Page 46 0170

i
I. -2ceArralyticale
Pau A.OW.ar EeMeer, I- Paz. AmaryUcal arrvl r. r, In[. "..r AnYyu..r Servin r, No.
705 e.ai Maado+/ R..d -1P W A Z126 R,-.ds nr am Kvn ' Ar. Sur 100
EdM NC 2i7e6 AJ,.r NC ZS Nunrr.rR.. NC 2907.
ANALYTI CAL RESULTS
Project SORRY CLOSED - MT. 7URY JUIC)
P6 Pf*d Nv-: 92171m
Sample MVY-21
Lab W, 92177e94914
Cotem- 1013W1317r70
R.celred: ri10111312:16 Mon: 9Wtar
Report
Parv"Nora
Rlaolla UrAk
LlnYt
MDL
OF
Prepred Anory"d CAS No. Qu■1
1260 MSV Low Lanai Landrlll
Ans"ol Mo01od: EPA 6260
uana•1.4-DICNWO-2•butena
NO ugli
IOU
1.0
T
I11051130a3e 110-57-4
[xchloredlM1uv+om■Inane
NO ug1L
5.0
031
1
1111611306:56 7'.5-11.6
1.1-Dkhlarvethene
6-3 ug1L
5.0
9.32
}
IIm'i306A6 15.11.3
1 Zokm. o. then.
0-62J ug1L
1.0
0.12
}
1I1WN 06:56 107.06.2
I,e.OkiNaoetnene
ND uak
5.0
0-66
1
II706113 as 75.15-4
pa-1,2-Okldvrvelhene
26-6 ug�L
7.0
0.19
1
I1r0511306:56 156-6&2
uona•1,2.01u+Ivrcelhene
NO pO&
5.a
0-49
1
116WI1 )0e:6e 156-60-5
1,2-mpj.epfepane
NO uryL
1.0
0.27
1
1110611309:50 76.67.5
7,7-Olchlprvprvpane
N❑ uyL
I 0
0.26
1
11@5113>f6:56 147-2e-9
2�-DkMoloprvp4na
Ni)uyi
15.4
0.1]
1
1.Po 106:56 594-20.1
1.1.0W)mN propa.
NO uA
E-0
0.49
1
11/06713 De:56 563.54.E
cia-l3-piclllarvprppane
NO upd.
1.0
0.13
I
II'D371306:5e 10041.01.5
Ir..-
NO NO ua&
1.0
ORB
I
IIl06f1006:56 10001-07-e
Eu Vit-1ene
NO "04.
1.0
0.30
I
111D51$3 06;66 160.41.4
Ethyl melhenylaN
ND WA.
10.0
0"
I
II105fI30 ;56 973}2
F16.4 pofo- 1,3•buudMne
NO u0&
10A
0.71
1
11M511306:% 97.66.3
2-kaaanone
NO ugg.
50.0
0.4E
1
11105113 0e;56 591-76-0
rvdvmelhena
ND uCA
10.0
6.32
1
1110511706.5E f4S6-4
I.vWI.-W
NO W&
100
35.o
I
IIMill 30636 7r"3-1
M.Ih.cry-mm
ND 41L
100
0-93
1
11 f051130:15 126.9E-i
Metlulen. ClJrrlde
ND up+L
1.0
0.97
1
TIf05rI306'S6 75-00.2
Me1h31 m.lh.. A.
NO upIL
30.0
2.0
1
1,low,30635 60412-8
4-mmovA-2•p.M.- tmisiq
No ZL
1v0
0.33
1
11105113 asm IGe-10-1
Nephmelene
NO rruM1
10.0
0.24
I
111051130E-m 91.20.3
oraplonlu9e
NO zL
150
3.S
1
11f05r1306:59 107, 12-0
alyrw
NO ugA-
IA
tlse
1
111051130E:56 100.42.5
1,1,1,2.Tebamlvrvevlane
N0 upL
5.0
0-]3
1
17 rQ5713 Qe3e e10.20�
I,1,2.t•Teuacnlerve1h
NO uP&
3-0
0-40
T
111o51130a-56 79-34.5
70,0lvrvelhene
NO uRR
"a
0-4E
1
1IM130a36 127.0-4
Taafene
NO ull2
1.6
036
I
1 MWI30056 105-66-7
1 ,2,■-TNch]vmhenlene
No "DrL
10.0
0.15
1
1I16MMSOE36 120.62-1
11-7rid+lwve0rane
NO uyl
1-0
0-46
1
1I=306:56 71.55.E
1,1.2•Tr1ohlmavrhana
NO ugx
1-0
0-29
1
1N0511306;5e i9-OOd
7rkt6noelhene
1.6 ugx
1-0
0.47
1
11AWT506:Se 79.01.E
TNehlnveuvrvnbmane
NO ugfL
I A
0.20
I
11=2 06;5! 75�9-4
12.3- Trlrnlvrop.opane
ND v01L
1.0
0.41
I
I1105f130e:5e 96-16-4
Wo OCOW9
ND ua1L
500
0.35
I
IImm30e:se 10d 05-4
y■1yl doerld■
NO uglL
1 Q
11
1
11111-13 Q6:56 75-05.4
Xylem jolo
NO ug&-
5 0
0.66
1
11105r}3 0e:5e 1330-20-7
Scare"sm
f-Eralrle3uuvL4e5Len■ (S)
96 Ku95
1Q-I3300
I
1110055r13 00.4
564s060-07
1,t•Orcl4uaathan■•W (8)
I
0v6:
-0
TDluna d8(5)
97
}0.130
1
%1 mun 06.5E 2637-26 5
4500E 20 Euuid■ Water
Anelylicet Mainod: SM 4500-S20
Sullde
ND u0A
1000
100
1
11 r06r13 1310 16496.25-a
REPORT OF LABORATORY ANALYSIS
rm'.pert a m not W r.2rev.ced. -.P1 ti all.
D■le. 15 e 1 U201302.12 PM +rowutm..e+ll.n wrnens 0 Pat. Ana61.06emne lnc. Pape 470170
Paer A"ytl..l SmAtbi, Inc. Pate Amlyd..I 6.fy1.e Ins
Par. An JyYeal 6ervlee r, lrp.
7Q5 E.aI MP.daw Rv.o-5WAA
7273 F.'r Ir
9W0lGxvr M. 6�N IQp
. • 1�1� 1
Fd.n. N� 772..
Aaov is wL' 7116W
IxmrrNae NC 260721
'
e.ePx.tiF+v..
131op7]a9xr
1e�9135ai11e
S7W 16769W2
ANALYTICAL RESULTS
Pro*l: SORRY CLOSED - MT. AIRY (OIC)
Paco ProAd No.: 92177964
$-Pp.; MY!-I1
Lab 10; 12177944014 CWMc1ad1DWI 1 I7:30
R■c■Had: 1110101412:15 Makk: YWEr
R■porl
Pllrem■IAn
Raumb WS Ifni! hrDL OF
Prepared
Analyzed CA5 No. oval
460OCNE Cyahwa, Tefa1
ApaWv9 Me91ed: SM 4500-CR-E
CyaNdo
1.3J uplL 10.0 5.0 1
1111WI311:20 57.12-5
REPORT OF LABORATORY ANALYSI8
TI.. r.pon r.d . radP1 n h .
Date 1111312013 02 32 Pm .o T..nnrnca,..,..1 el P.p AnaNvc.i S.mcm. ft
Pane 46 of 79

Per. A.Mythel 6."440, Me.
P...An "..i 8rrrc.e, Inc
P.r. h..lyllc.l 11 r 1 .f, 1n .
Pere AnWvmdl 9:1-.Ors.
Pa.. AMPIM A BxHe.., Inc
P.- An nyec.i hen ., Mc.
�A1,^,,,,,��y
205 E.n M..ebW Ro.d - SW4A
7I]5 RMerriSm Dr
BBW KhcryM S,.le 100
•
:r�9 E.rl M.edvw ROW -9WMA
237E Rtr.rude d
9e00 F.,rrery A.. &ul. tA1
: a .�.11na"caI
Eme, NC zyzm
n.ryr4. Nr; 36ev4
Hwier..n.. NC 2e07e
/ .. ' +EtS! kit
Eden, NC 172Ba
AN.rN- NL 76601
lr,lni.rrr,r.. MC 20070
.
mrwP.ni.a.v.
is36Mxeae7/
152eJzn4-717e
r+O+N13-Kq7
f+ ..�P,r.rr. r.,v
[3%]e13d921
Jer6fu�117e
rmaJl7sanv�
ANALYTICAL RESULTS ANALYTICAL RESULTS
P,.Jed BURRY CLOSED - MT. AIRY (UIC)
P.e1ed: SV"Y CLOSEb - MT. AIRY "CI
P." N.Jed N. 92177961
Pace Project Mc. 92t77964
5.mpl.; My9.22
Led IO! i7177044015
Ce6ecled:
IWIW13 It 05
Received: 11 M1113 IT$1 M.Iz r Mter
Sample MW-22
Lab ID: 52171H4o1a
Callecled: t0156113 1}:05 R6 NI& 11191117 12'$5 MaIrk: YMtler
RepcN
R.porl
P..n.eler.
Rem0l. LJWk
Llmll
MOL
OF
Prepped Andyred CAS No Ouei
par"olm
Rea1.116 LMm
Llmll
MOIL
OF Pf"ord
Arralyled GAS No. O9el
6010 IeP Oroundwatmf
An Niy .l Melhvd: EPA 6010 P,.p.retcq.
M.Ihod: EPA3010
1260 MaV Low Level Landfill
Analytkai Motho d: EPA8260
Anumvny
ND uA
is
5.0
1
t1M6M 310:45 TIf011131IL23 7440-38-0
kar-1,4.01Wmo-26rlienr
NO uWL
100
$A
1
IUOU1309A2 11041.E
Ar W.
ND ug4
100
50
1
}110611310A5 IIMV1316'21 7440.36.2
Okhfarodl4uoromelhana
NO "a&
5.0
0.21
}
1110511309,12 75.71-a
RWWm
94AJ ug&
r00
S,0
1
IT10611110!0 11MW1316.23 7440.393
1,1-0RNaeal1r11na
2Ad UA
50
0.32
T
11 M5l5308:12 75-34-3
Barymlum
NO ug,l
1 0
IA
1
11 MW310:45 15M81131823 7440a1.7
1,2.Oichlwoeltune
0-77J uliL
It
032
1
11 M511109;12 107.06.2
Cm,o am
ND ugA
1 0
Ip
1
1110141310:46 11M6f I11623 ?440L43.11
1,1-0lehloraemene
NO ug&
510
0.56
1
11 MSl I309:12 75.;0+4
Chremlum
ND ug&
100
1.0
1
15M6113 ISSAS S1M6f I11623 744047-3
da•1.2-[NGWOPv.Ihane
4.1J ugh
6.0
0,19
1
IIMSM309:12 156.59.2
C0411
110 ugfL
100
6.0
1
1VOW1310r45 117011131822 7440-414
1tan4-1.7-dcMwoeihm.
NO u0R
5.0
0.49
1
1TM54 13(19:12 156-60-5
Copper
ND wwl1
10A
SA
1
0AW13 M.0 IIIW131813 7440.504
1A4 N6AWq r.p.ne
ND ugfL
1.0
027
1
11 tou009:12 79.67.5
Load
NO ug&
100
5.0
1
11M8f 1310-45 SWIM 1222 7439-W2-1
1,3-Dk}Yuopropane
N4 WI;&
1-0
0.2E
1
15M511S 0:12 142.2E-9
NicYel
iA1 r.0t
50 0
5.0
1
I1M1M 3 10 45 11Ma113 19i3 71404Z•D
2,2. Nohloroprolcom
NO ugh
15-0
0,13
1
11M51131":(2 504.20.7
Se1e.4um
NO uU&
10.0
100
}
11NNI] 10A5 11001113 $623 779240.2
1,1•DkNoropropene
NO ugh
50
0.49
1
11136M309:}2 563.58.E
Se..r
NO agfi
Sao
5.0
t
IVW 3 tO:415 IIMill 3 se23 7440.22.4
rh-1,3•gmlrf0prvpane
NO gk
1 0
a.I]
I
IImm Omm 10081-01-5
T114111ym
ND ug&
5-5
6,4
1
11 MBMS tO'45 11M61131921 74140.26.0
Dana-1,3•pd+rornpr0p...
NO uUA-
1.0
016
1
11/115113 09:12 1g061-024
TIn
NO uaR
100
6.0
1
11M61s310;4! 11 MW131623 7440-31-5
Edly4.n7.ne
NO uA
1.0
0-30
1
IIMU1301:12 100.414
Venedlum
NO ug1L
25.0
5-0
1
1110ar13 10:43 11MN111643 7441142.2
SMVI melhecry! ate
No POLL
$0.0
0.20
1
1110511309-12 97-63.Z
Inc
NO ugh
MID
10-0
1
11M10310:45 11AW131623 74404164
Hereohld o 1,3-bul lcm-
NO uUrL
10.0
0.71
$
11 M5113012 874E-3
2-1-lezmnona
NO u0R
50,0
0.4E
1
1SMW 13(19:12 591.79-8
7470 Mercury
Nrmylkal Me6ro4EPA 7470 PfefMlre6gn M*11 0: EPA 7470
IadpmaLhene
40 uWL
10.0
0.32
1
1SMSM 3 09:12 74.69.4
MercurY
NO ug1L
9.2E
0.10
1
11MS1318: 15 W1211315:39 7439.974
Ieobulanvl
NO ug4
100
35-0
1
1110511.19212 7143-1
MefiacrylaNtrlle
NP u9k
109
a"
1
ItM5M3 Ot 12 126.9a-7
0280 MSV Law Level LontRIH
Aneiylfcml Me 6rod: EPA 9260
Meriylene Mortal
No uglL
IA
0.97
1
1100503 00:T2 75-OM
Ace lone
NO I.94
1f10
10.0
T
W0511309:52 6744.1
Me So* melhperylal a
NO nk
30-0
7.0
1
1Sf05M309:12 60.62.5
A"t.wlyde
HA r.WI
550
22
1
IVONT30012 7645.E
4-Melhyt-2-pentenone tMIM
NO oWL
100
0.33
1
1110511309:12 t06.s04
Ac,Ml
NO ugh
53.0
1.6
1
f1M5l1309-12 fo7-02-1
Naphtherenm
NO uWL
10.0
0-24
T
11OU1309:12 91.20.3
furyh.mtnL.
NO ug&
200
ug
1
$1 fOW1309:12 107-$3.1
Prvplenluee
NO uA
160
3A
}
IIMS11309:12 107.12-0
MVI chlende
ND ug&
}0A
1.5
1
11AW30012 107-05-1
Styrene
NO uUIL
1.0
0.20
t
11 M511300:12 10042.5
Samaria
NO ugh
1.0
0.25
1
15M51130912 7143.2
1,1,s,2-7eba6h10ioaarana
NO UA
5.0
0.32
1
IIM5f1300:12 OW204
&.nwdda ORrelrr.na
NO uWL
:SO
0.17
1
Wowla 09.12 74.97.5
1,1,2.2-Tetr.cMwvral w.
NO Pgll
3.0
0.40
1
11 ry15130:;12 70.34-5
Brvmvdicteorom.ln.ne
NO ugk
1-9
0.18
1
11M5f 130912 76.274
T bechlo. coin-
NO Zt
10
0.46
1
11low309;12 121.1E-4
lk-r glcnrl
NO -pA
1.0
071
1
IV0511309:17 75-25-Z
TaM1.ne
ND uyL
7.0
0.26
1
11MS11309:12 101.8E-3
BrrrnrmrFe...
NO.wA
10.0
0.20
1
1110501309:12 74-43-9
1,2,4-TnrTlow6onrene
NO v9fL
10-0
0-35
1
11MSf 13 G9112 120-92.1
2-Butar (MEN)
NO ugiL
100
GIG
1
I11051" 09-12 78.9Y3
l jj Tnchtorommena
NO UA1
0
0 4a
1
11M511309;17 71.5"
Co.b., J.+I9da
NO.^
100
1Y
1
110051130112 75-SS-0
1,1�•Tgphleroelhmne
NO ug1L
1-0
0129
1
11M8M309:12 MOD,5
Carbon Ieuaddoride
ND uA
1.9
O15
}
11 f051130932 56.23.5
Tt"I&O.dr.na
NO 41L
1.0
DAIS
1
11f06113 ON %Z 79-01-8
Chloroh+nrane
1JJ VWL
'10
0.23
1
111o5M3 ON; 12 10640,7
Trkhlmoluoreme0.mne
NO ug1L
11
0.20
t
11105M309:52 7849.4
Chl«R.ihan.
NO uaft.
10.0
0.64
$
$1MNI309:12 75-W3
$2,3-Tllchlorop. opmee
NO ugh
1.0
0.41
1
1110511300:12 M-16.4
Chlm.Irrm
NO uGA,
5.0
054
1
11 Awl 309:1a V-68-3
V"4vol.l.
NO uyL
S0.0
0.35
1
}1M511309,12 lW054
Chlorvmearene
ND ugk
1A
0.11
1
11m5f1309r12 74-97-3
Vfttyl thkv4d#
NO uOIL
1.0
0.62
1
IIM511300-12 7&014
Ct.m7rop..na
NO uyl
2D.0
0.27
1
1}M5M309-12 126.w6
X"Am S70120
"D-Dk
5.0
am
1
11M511302:17 1330-20-1
1,2-OO-omo- 3-drloroprvp.ne
NO ugh
13.0
2.5
1
1110lu 309:12 96-124
$umegeha
4-BtarrmAuorobenxene {Si
96 %
70•f30
1
11lOS11309:12 490,06-4
DlM omovhlorvmeMene
NO ugrt
3.0
0.25
1
11l0511309.12 IZ4.46.1
Igo %
70.130
1
1}MSf1700:12 1707-25-5
1.2 Dlhrr m00tnan. (Eno)
NO uyL
TA
0.27
1
111WM309.12 106.93.1
T-ltma-dl (5hane-d4151
Teh,en a-ei [sy
995L
745m
I
S1M5MS 09:13 ZO77-21-5
D"amametnane
NO ug4
10.0
0.21
1
1JMR 1309:12 74-95-3
52-Orchlvrob.-mvS.
0,13d ut7L
5.0
GAG
1
1110WQON$1 9S•50•I
4500520su IfId. MI.?
Anmlyllcet Malhod. BM 4%0•S20
1 ]-Drcmwcbmr.na
NO ugfL
5.0
024
1
1V05113 69:52 541.73.1
I.A-VJOhia .b-x-
1.6 mok
1.0
0-11
1
11 M611300:12 106404
Suslde
NO uA
1000
too
I
1170E+1] 13.10 1a496 254
REPORT OF LABORATORY
ANALYSIS
REP 0RT0F LABORATORY
ANALYSIS
ltw rp.n.hN
rirf M nrrrd.K.d..rcry n
hi-
*m..ern anal -I b. r.Preuvrd ­0 n "..
0.I.: 11/11/2013 02:32 PM
wl_. Wt -Imer, can..nt nr P.. 6n Imy "-k Mc Page 49 of 79
Dale: 1101372010 92:32 PM
..e,r,,..1nr ann....A r• P.
fwlyr l 54P . ree
Pogo 50 of 70

Pa[a Rnal]al[Y aa1Ne.1, NIC- Paca Anal VUeM as -.Inc.
I .' 444 Mil Mil iCala 205 filet M..d Rees -%J A 2=RwerWe Or
44 1 H �d.n, NC Rim I ah,.," HL Z9E[II
..rp:rYMme ;]3ep7}eP21 (e2e1xS1-1r r9
r
ANALYTICAL RESULTS
Plvyacl SURRY CLDSED • MT. AIRY tlllCl
Pan P,v�.cl 7iv.9Z177964
Ps" MYydsal Semi" 1. In[-
o60a lr rA.. bur lu]
H n11-o NO 2m7a
;7mle75 om
3ampH: MW41 Lab 10: 9217794401E Coaaefad: IOt-WhI II' 3 Reealved: film I11312:15 Maul.: We ter
Report
Pelemelen R... No Will LNriI MOL OF P.PP..d Anllylld CAO No Qual
4WOGNE Cymnld., 7014i Anstymum Me6wd: SM 4500 CN-E
Cyanlue 10.3 VOL $0.0 5.0 I 11110113 11:21 5742.5
011h • f I rl U2013 02:32 PM
REPORT OF LABORATORY ANALYSIS
TNo reed N.m c W eprW,ced-­pH 1, N.
•eaw-1 M nnllln voneenl pl PeN MIIyocal San cle. Inc..
PaceRnalytical�
I
Pap Adalytlaal 6aMen, ka0 Peer Awlyde.l WKYllaa, hit. P. Andyd.ml 6.ryru1, I.W.
XDE..1 M..dw Read - SIAl1A !225 R-,.d. Or. MW Ohay Ave Suim IIX1
Ed-, NO 2726E Aen -NC gum IWnw-le. NO 2W76
P369234m, 16211P54- 176 17 1575 DM
ANALYTICAL RESULTS
proleol: SURRY CLOSED - MT. AIRY (I11CI
P1ce Protect No.'/2177964
lamPlo: mwW v
Lau IO: 12177164016
Gvhdad:
1013W 13
10:20
R49alrad IVDIR3 12:15 Math. Vfubar
flow
Pa1lmalwe
RawM Llrwb
U m
MOIL
DF
Pm"md Arl"d GAS No- Dual
90101CP G-and-lar
Analyllpal lialwd-EPA 5019 P(►pa/a1rlh MaONd=FPA
3019
Anamony
ND ugti
5.0
SA
f
IOwl 3 f0'46 III man 316j6 7440-16-0
Anent[
ND v01{,
10-0
SA
9
119N1310:46 11 00611319:35 7440-3S,2
B4elum
30.7J u01L
100
5.0
1
DA W13 t0:46 51106113 16:36 7440.39.3
0 errakrm
ND uliL
1-0
1-0
1
1,am 3 I1A 11TV 316'36 744041-7
Caddlwm
NO US&
1.0
1-0
1
11411013 fCA 1110W 311�36 1 4"3.0
Clwnmlum
NO ugk
10.9
6.0
1
11AW1310:46 1VOW131836 7449d7.3
Coh.11
ND ugA.
19.0
6-0
1
fl?DSM310:46 IJA61131626 1440-404
Copper
NO uUM,
10-0
6-0
1
If)QW131046 1r1062131&55 7440-50-6
L..d
NO ugk
10.0
5.0
1
;1mW1310,46 IOM1316:36 uw*2.1
NI<ael
NO ugk
50.0
5-0
1
IIIOW1310:45 11A611316:36 744042.0
S.I-rn
NO uglL
190
100
1
IJAW1310%6 111061131E-39 77Q42,2
&We,
NO ug+L
10.0
5-0
1
1191001110:45 Ifm611316:30 7440.22.4
7haOium
NO uyL
5.6
SA
1
1tAW13-I CA111=1318:36 7440.2 -0
In
NO ugIL
100
5-0
1
IIAW1310>46 Illmn I6:36 7440.SI.5
Vaned-m
NO 41L
25.0
5-0
1
IlmW131OM6 1110VI3 18.30 744042.2
ZIPc
NO u04.
10.0
10.0
1
IImW1310:►6 11 MI1 16'36 7440-06-0
7470 Mercury
A.urtnl 440.011- EPA 7470 Prapardarl Ma7wd: EPA 7470
Mercury
NO uyl
020
0.10
1
110OW13 ICis 11102111 tl:42 7419-07-0
02" Msy Low L.ral Luadi III
Malylleel Merced' EPA 6200
A[elone
NO ug&
100
I0-0
1
11mW1309:26 9144-1
A-INAe6.
NO.0.
55.0
22
1
110OW130924 79-054
Aaolcm
NO u04
53.0
16
1
11 035H309:29 107.024
Aerylnnlldle
NO u0L
200
1.9
1
11mwl10926 107.12-1
Ally! chImIda
NO uv&
10.0
1.5
1
f1A6130926 f07.06-I
Oenlene
NO ugl-
IA
025
1
11/Owl309IS 7t•43.2
9rumoonloromenana
HD uq&
3.0
0117
1
I$MNI302:24 74-07.5
HrvmadlalNwoma6+ana
ND ug&
I.0
0-I6
1
11m51I302-6 M2114
6rom0:xm
NO uWl
3-0
026
I
I?X611309IS 75-Zrs2
Ornmome9lene
ND ugA-
10-0
0-29
1
11MM30126 7443.9
2-9ulanona(MErq
NO v94
100
0.11E
1
1Im5113092A 7b-93-3
Carbon doul60
NO ug1L
100
12
1
11m6n3Oil 21 7 %&O
Carbon 114atdlNmWq
NO ug1L
1-0
02E
1
111W1130921 $6.23-6
Chloroh-arena
NO LI;,t
3.0
9.23
1
1119E1130926 101-WI
C1rlor:Mhl a
NO ugIL
10.0
0.54
I
11 06113 DO 7540.3
Clrlwkrm
RD u0R
5.0
0.14
1
1JIDWS3 D129 074W-1
Chfarorne61one
NO ugIL
1.0
0.11
1
11AM130921 74.67.2
CAlvrep m"
NO u11L
20.0
027
1
11105113062E 1 '"A
12-011r,ornoa-d,k""-pane
NO ug4
13.0
2.5
1
11/0311/ 092E 96.12.E
phr0m6d+wramehene
ND uyL
3.0
021
1
I110511a 0926 f24-0-1
1 2-Obromoefh.ne (€O6)
NO ulyL
1.0
0.27
I
11 Moil 30920 1WO314
0lfnem ..Ih.ne
NO ug4
10-0
021
1
11 A51130926 74.95•3
12-DIchlwubar r.ne
NO -A
50
0.30
1
11451130026 9 -50-1
I.3-Okhlpvben3ape
NO uyL
5.0
024
T
11+O5H30 19 541.73.1
14-Drcdorobenre4e
NO u9R
I.0
033
1
IImW 13092E 106.4&7
REPORT OF LABORATORY ANALYSIS
7warey+erl .oM nerd. ...-P h..
Pa04 61 Ell79 Dail, I. III Wal3 in32 PM +nowt a.. cm[wn rn -I .l PK. Analy9[ar 5.= ft.
Pogo 52 0176

Pale Anelytl.el 5-kH, Irk. P.e. A11."tai a.nW..ai 1Z. Pew Anegl.al a.rrS..., * . P.C. Anrly0"I a.ryle.r, InF P4a4And1p..1 S.rrla.e. In.. P.e. Anely4m.l aePde.., lae.
205 Earl M..d.w (few - S. A 2725 fuy. W. Ur 9e00 K Y Ar. 11 a 100 206 F.y1 /Ae.d.w R..d . 5uirr A 2M RI-ade G "M K-ey A: 5rnN 100
aceAnarytrcal Ea . NC 27M Aeh.My- NC 20M4 H1 W-Ale, No 2591E � aceAmiytica)E1-1 NC ". ew.w NC 2009 unWlp a., NC 2WIF
...rwal.e..r 1375]62]d921 t028)214-117m 170/p73i092 l .er n>.0.a m+ IdM16" all (.r)231-71 re t1 ?57som
i I!
ANALYTICAL RESULTS
P1q.c1 Ei7RRY CLOSEO - MT AIRY 010
P4c. 0rapt! Nv . 92177984
Sampl.: MW-23
Lmb1D: 2217TH4015
C.Amd d: 111l30M
V120 R.edYed. }NOf1131Z:15 M.4uVAW
R.P.0
Puamelerm
R'b"A. WIN
LIm9
MOL
OF Prepared
An -Wed CAS No. Dual
a26o MEV Lon L-1 Landfl0
An MI-1 M.1h.d: EPA 87B0
vane-1,4.Olrhlvrv-2bun..
NO uV.
100
1.0
!
11K151f309.Z6 IN-517-4
gchbrvdlluvror0e0r4ne
NO ug1L
6.0
0.21
I
11/05111 0929 75-7-1
I,f-Dlvlawwth4n4
I'di ug&
5.0
0.32
1
1110511309:21 7S41.1
I x•oKMor oelll.n4
NO ug&
1-0
0.12
1
1110501309:28 107.M-2
l,e•OtNol oeH-
NO ugli
6.0
055
1
IVDV13092E 75-55.4
d.-1.2-pk3llvlvnr,ena
04v uwt.
1.11
o19
I
11 MW53092: 155-59-2
van4.1,20knwr0etlis0e
NO uQ&
S.
OAg
I
111051130112 l56-E0-5
I x-0Lchleroprapane
NA uWk
1.0
0-27
1
1V051130929 78.47.5
1,3.Oicidwoprvpane
NO ugA
1.0
"1
1
R10511309:2a 142-234
2$-plc} _Wv p.ne
NO .A
15.0
1-11
1
:1105113092a 594-M7
I.110ichiw dpropen4
NO u04
5-0
a
1
111057130926 507•Sa-6
eY-1,S-Oidlhrep opane
NO uWL
1.0
0.13
1
1I n151130926 }00411-W
h.r1F1,1-aclOoruP.enene
NO u04
1.0
024
1
11A151130020 100a-024
ElryEenpene
NO -A
1-0
0.30
1
11 M51130929 IW41.4
Ewyl m.lh.0 yl.t.
NO Z_
10-0
0.20
f
11 f0511309.2 97.63.2
11. r.Woro-1.3-6uT.Wene
NO ug1L
10-0
0.71
1
1N051130028 174ta-3
2-H44an6ee
NO 1ig+L
60-0
0.4E
1
1tA)SI130978 SIl•7"
IPEP-111 ne
NO uglL
10,0
0.12
f
111051I.1092E 7448-4
y9Mrlulel
HO uylL
100
SS-Q
1
1 MW 30226 76�Y1
Meun Qylontella
NO uglL
100
0.93
1
1}lOSII70948 126-91-7
MHhyl4r.e Cnlmtdo
NO ayi
1.0
0.97
t
11145117092a 76•Q9.2
Me lhyl meth-0.le
NO �gIL
30.0
2.0
1
1170v 30926 a04I2-6
4 Md Lhz-p4ndnon4 (1,411K)
NO ug&
100
0.33
I
11A75i1309-28 106.18.1
N.PIA146 a
NO uA
IDA
121
1
1111*19092: 04W3
Wpplonlvnm
NO uQ&
T50
3.8
1
11105113092107-12.0
spe-0
NO uglL
4A
025
1
11105113092: 100.42-5
1,t.7,2 Ter.wor9ew4n.
NO 1gll
S.0
0,33
1
11.13 M-2 630�20.6
1,t,2,2.7.6.FiluveiN.ne
NO Pok
3-0
0.40
1
I110W$3 W20 79.04-5
Teuavntavalnwla
NO kgQX
TA
0.40
1
WON'30926 127-19.4
T.kw 4
NO uVL
"1
026
1
11105113092: 109.98.3
1Z,4 TAcht:bancena
NO c94
10.0
0,33
1
111051130921 120.62.E
T,1,!•TrxAllma.%.ne
NO uWL
1-0
016
1
1110A71308:2a 71.56.E
} 1,2-Tnchlorve#Wi.
NO uyi
19
1-29
1
11105111062E 79-00.5
Tlkhlale41h.n0
NO UWL
1.0
0.47
1
111057110926 7L01.6
Trkhlao4uo -than.
NO uWt
1.0
02Q
1
II AW,20926 75.6Qd
1,2,3•Trkhwrvprvp.ne
No 00R
1-0
I'll
1
11106113092E 91.105-4
✓►1N.elate
NOug-
50-0
0,3E
1
11709113092E 106.O"
logo cMeeide
NO u0R
1.0
0.52
1
11MU130928 7S•01.4
xyl.n. [ToulJ
NO ug&
s.0
0,01
1
11106113092E 1330-20-7
s,r 9.lem
4 era m.luwahen20110(S)
95 %
70.130
1
111061130:2a 480-WA
I,2•DklJarmanune•d4 M
103 %
10, 110
1
"145113018 17060.07.0
Toh.".•dS LSI
g9 %
10-110
1
1$106 30921 2031-7A-5
450037D Sulfld. Wow
Aalalylk el the lhl d SM 4600520
9vILAe
NO ,WA
loco
100
1
Ilmil313'10 1649E-26-a
REPORT OF LABORATORY
ANALYSIS
True r.p.rt
wrl .nl4r lepl,d.crl .•[apt n en
De10 I1113129f ] 07:37 PM
Mewl an w.rn uen..m of
P.i. M.101.1
Seale. irw
Papa 33 of 79
ANALYTICAL RESULTS
V'cl.cl' SLURRY CLOSED -MT. AIRY;IIICI
Pace Pwjad No : 92177964
Samp v MW-23 Lab 10: 92177164011 CL414 clad. IOfn 1110'20 R4c51y4d: N70111312:15 K1"1V W4ts1
R.Mn
P.-.1ere Readlh Limo Lana MOL OF p1epM4A AA."ad CAS No, Odal
000CNE Cyan l de, Tol.! Anely9mal Method: GM 4500-CN-E
Cyanide ND uqk 10.0 5.0 1 11110111 IL24 57.12.5
REPORT OF LABORATORY ANALYSIS
TN. 1.P h.4 tbt be nPyNrc.O.-pr nam.
Omit; 111132013 n.32 PM .1-1 aH llrl eeewnt 0 P.-A-V tI. l &mks.. InP.
Page 54 pI 79

��-,,CeAnaVkal'
..ejreeWm.
Fen. Anal yll—1 a.rrl..,, rne. Pie. A-ly[leal!,trio,,, M.. Pat. Aeelytl
E6en..l a.rrlc,f, Irw.
z<J5 [..[ H.,dow ria.d - s�i[, A 2225 R.—,c. Dr. 9a06 Xe.cel Aa.. aula 100
. aM8 C 21Ae ml. NC 20004 Hw ren4. NC 24610
i3lfi]6ll�lH: Ism., 117a lTN)D1S9092
QUALITY CONTROL DATA
Prefect. SVRRY CLOS EO • MT. NRY IVICy
Pau ".,I Na : 92177964
OC Belch: MERPt5774 An.lyak Mathod: EPA 7470
00 Balch Mod. EPA 7470 Ana" Desalptlm: 7470 Morcury
AsaodWd Leh Sei.plos: 921779840D1, 92t77HB4002. 02177904 D03, 92177964004, 02177@64005. 02177964006, 92177W4001,
92177964005, 02177964009, 92177964010, 92177N4951
METHOD BLAW: 1075697 Makiml vAlar
Aaa4defod Lab same.: 92177904001. 92177"4002. 02177964ODS. 92IItM4004, 92177%4065, 92117964000, 9x177964007,
92177954M, 92177964009, 92177964010, 9217IN4011
Blwk Reprlklg
Premater I1n9s Maury Limn Anslyiad ouatl9are
M4rnsy uWL NO 020 1111V1313:25
LABORATORY CONTROL SAMPLE: 1070529
SPrk4
Lee
LCS
%Rep
Pram41e1' 19a Lh
Cono.
REPA
'A Rea
Limp C-Aaere
Memo uWL
2A
2A
99
80-120
MA7RA SPINE a MATRIX SPINE DUPLICATE: 1076599
10718H
Ms
US()92117843005
Spike
Spike
As
MSD
MS MSO
%Rea
Mu
Perem.l.r 11r111a R.-It
Con..
c6l1
Rae1A1
R*KM
%Roc %Ron
Uwhw
RPO RPO Qual
Merwry ug& NO
2.5
2.4
1.3
12
51 47
7&$25
S 25 M1
2eAna,&,7l'
I'.. —ga..kbr e:.m
i
P... A nil Vdc el aerHeef, W. Pae. Anaiytf le w., lee. Pee. A.WyIM.14.n1..e, 1rw.
A5 E.alMeadow Ree6 - SJN A 2225 Rrm.n*
d ve09 tUrc4r iw. s,w. 1m
Eden. NC 272H A.h-ft. NC 2a004 ISIPI n-1 e. NC 28070
pmp2.sd991 jus)26411 In 1ru41e1�ao92
QUALITY CONTROL DATA
P,.1.e5: SORRY CLOSED - MT. AIRY ILNCI
Peee Pr.0d No: 92177954
OC Belch: LIERF15760
A7ulyal. Melhed EPA 7470
OC Selch A1elhod: EPA 7470
Mwill's DwAp ion: 7470 Marcury
Auadaled Lab Samploo: 52f77164812, 92f77984013.
921779640fi, 9217796401 i, 9217798401d
METHOD BLANK: 1079520
M.bu, YOU,
Aaeodalea Lea s.mPNe� 92177964 o12, 9x 17796401 s,
9x 1779645rs 4, 9217796401 s. 9x1779040re
Blank R.Paplg
Penmeler 11A9a
Reeutt Llmll M.lyred QwN6an
Martyry u91L
ND 020 11fI27131520
LABORATORY CONTROL SAMPLE: WWI
Spike LCS LCS % Roe
Paramour WKS
Cone. Ra i ll %Rae L.kdM O..Wlen
Merl,,y VA
2.5 2.6 Pm 60-120
MATRIX SPIKE IL MATRIX SPIKE DUPLICATE 1079522
1079523
MS
MS0
92177904017 Spike
Spike
MS
MSD MS MSO
% Rec
Mae
P.—W., UM1. Read Cenc-
Cane.
Ro.rel
Reelrll %Rd. %M.
LAmit.
RPO RFD Owl
Mercury Up4 ND 2-5
2-6
2.7
2.7 101 101
75.125
0 25
REPORT0F LABORATORYANALYSIS REPORT OF LABORATORY ANALYSIS
Tie, r4pM Wd M[be repraducM, .,dal F AA, in, report NN �w[ W r.proeuc.e. ,ru W n fw
Dole: f In32013 02:37 PM wlNart na. and--am.t P.c. A--&.0 S.mpr...c Page 55 of 79 Dare 1111317GI3 5x 32 PM .. n.re In..mmn re....n[er R.I. S.— a, rn< P.O. 56 of 79

n Anp711aa1 S.Mnr, me. Peet Amlyenf aarvleer, me. Pu. An.1y114al fervleu. me-
c�C$ i ICal ]95 f aN M..&Rcad SI.,.A 27M AM—W. INWeX Orr we. adr 100
' n Edtn Nr.7r±ee •N•.v9., NC 2aBD4 lxnWrrrt-uG 2e0Ta
nT`ay,— I.p]3-007, 1a Aa VA il10 170.167541002
OUAL1TY CONTROt DATA
Projepl:
BURRY CLOSED - MT. A1RY CLOG)
Paea Plojeel Ne.
12177964
QC Serch:
MPRPI14580
An@"& Memod.
EPA9010
CC H-1c Method:
£PA7010
Analysis De mWan:
6010 MET NO Orollndwaler
Aeaode[ed tab Sample a: 921779640p1, 9217i994002, 921779&Ipp3- 421771764004, 92177964003, 92177964006, 90177961007
METI40D BLANK-
1076677
Mae1.. 9v1110r
Aeaodeted Leh Sampree- 92177%e00f,9Z177%40pQ, 02177994003, 92177964004, 9217796400i. 921779K40Dfi, 62177964007
Blank Re9onlnq
Parameter Unaa
Rawl IJmll
^-"d Qualtere
Anllmoay
uyL
N❑
610 1Va571316110
Ardent.
uDrl.
ND
10.0 11 MW a 1s:56
Buh,m
uyL
N❑
100 11106J1316:59
13.ylhlm
uyL
ND
1.0 11N0511319:50
cadmium
,prL
ND
1.0 11 MW" I6:59
Chromwm
uyL
NO
10.0 11Noula III:%
COW
uyL
N❑
11).0 11MU1311119
Copper
uyL
ND
$0.0 11705N319109
Lead
uyL
ND
10.0 1110W1319:59
M.LeI
LWL
Np
50.0 1100511316:59
SMenarm
uyL
Np
10.0 11 M51131949
S&IF
U%OL
IJD
10.0 11 M14$1 16;69
Thduum
tlyL
ND
5.6 11105113 It:"
71h
uyL
NO
100 11 Win I6:59
Vmudlun,
ugrL
ND
26.0 11 m611310:59
T"
uyL
NO
10.0 il/WW1315:39
LABORATORY CONTROL SAMPLE:
Paremaler
tWO(I78
UNU
Spoke
Denc
LCS
Ro"R
LCS
SV Rao
% Rec
L"Is queaFen
An6mcuy
uyL
500
476
95
WD n
Amen.
VWL
56D
464
93
ao-12D
:Wwm
OgOL
500
474
91
ao-12p
B.glli—
u{yL
SOD
467
93
a0.120
Carimxrm
ugrL
500
4:1
93
ad-120
ChrolnlYlll
UWL
Soli
457
91
a0.120
coall
Wk.
50D
462
92
66-120
Copper
uyL
500
47$
95
90-120
Lead
uyL
$00
465
93
aD-t20
Ne-pel
I-WL
500
1"
93
10-12D
Selenium
pyL
500
476
96
a0-120
Slrer
ayL
250
234
94
66.120
Thallium
ryL
SOD
465
93
60.120
Tn
uyL
5110
462r
93
50-120
VanadK4m
uyL
SOD
473
96
I10.120
2h,c
uyL
500
453
91
90.120
REPORT OF LARCRATORYANALYSIS
lm rtaan.n.r mrlw repea,.ew, tarp n 1W1.
Pale: Ito I3QD}3 02:32 PM .r,ran 1n...•o.,, uc...., rrl r.r..n.ryx.r s. r.�.. lrr
P.w Arlely0pleerWen,
1M.
Fna
M,pygwl 8-1wa, en .
Pw. AnMy9ael S.M-a, Imo.
`
206 E.q wee—
Road - Swr A
2225
RNar1Ne Dr.
6M lue ay A Susa Wo
' aceAr+alyfical
5eaA. K 272H
AshwaRa, NC 23W
F-A—We.
NO 2107a
t,.. a4[taaruP
i
f1161673-e971
je M12Wile.
004A1154 Yl
QUALITY CONTROL
DATA
Project: SUR RY CLOSED - MT. AIRY IUICj
Pace Pro" No.. 92177964
MATRIX SPIKE Si MATRIX SPINE DUPLICATE' 1076679
1079650
MS
M50
92177955007
Sp%e
Spike
MS
M$D
MS
MSO
%Rae
Max
Parameter
Unit. Re1dl
Cone.
Cone.
Rmil
Rewd
XRec
%Rec
LimYr
RPD
RPO Duel
AlAMMY
uyL
NO
S00
500
501
467
Ida
93
75-125
i
26
Auaeldc
-WL
NO
500
500
496
4112
99
92
75.125
7
25
Barium
uyL
UAJ
5D0
5D0
506
471
Is
92.
76-125
7
25
Baryllum
4L
NO
500
500
411
456
%
91
75.125
6
25
Cadmium
uyL
NO
500
500
479
453
96
91
M125
6
25
Chromium
vyL
ND
S00
Soo
490
445
96
69
7&125
6
26
Cohel
-A
NO
500
w
464
451
97
90
75.125
7
25
Copper
�9JL
NO
500
500
503
iae
1DD
94
75-125
7
25
Lead
uyL
NO
500
500
467
442
93
96
75-M
6
25
Nickel
uyL
NO
500
500
462
451
96
9D
W125
7
25
SerenWm
uyL
No
500
500
46a
467
96
93
76.125
4
25
50-1
uWL
ND
750
750
23a
229
95
91
75.123
A
25
TheWum
uwk
HD
500
500
477
457
65
91
75.125
4
25
Tin
byL
ND
50D
Soo
467
454
97
00
75-125
7
25
vanadium
uyL
N❑
SOp
500
496
463
94
93
75-125
1
25
71nc
uyL
ND
Soo
Slid
475
441
M
27
75.125
7
25
REPORT OF LABORATORY ANALYSIS
frue,eaen Ora ,•al M e9�ed•ie.a...-,A h a,a.
Pace S7 at 79 Dale. 11 IM013 P2 32 PM w,awul n.e wndar• rena..x 0 P.0 ,.,ryW-.II su.i— 1.
Page 5A 070

P.n. Ann Ytlr.1 a.rvr..., ram- P... A..Iyd..r e......I me- rraa Anrlpl.A$ Mama.., In4.
1'r - a�eAnnalytica� • ins Eau h1..ww F c n'7205 nmw NC 2a ❑i ,b00 MY.cq Ara 9�. 1lld
EJ.n. NC 272&e A.nrrll., NC 7eeD4 IArI11.f.M., INC 2a01a
r t 1,M1823a121 ro2a)254 711e 17D4149759092
r
QUALITY CONTROL DATA
Prooct: SUR7tY CL05ED-Bet-ARY(UIC)
Phu PtvJeR 149-= 92177964
OC Ba"- MPRPf14S13 An"ia Mm&wd: EPA90fY
OC ea" Ma"; EPA 3010 Anstp is Deealpllan: 6019 MET NC 6rmnditm
Wevclatad Leh 9ampin: 92t77M4v06, 92177964009, 921779640f0, 92177964011, 92177964012, 9217796i013, 92}77964014
METHOD 6LANK IO N07
mithu:
Waw
Ar.mi.l.d Lab O.mplae:
92177964009, 82117964009, 92177964010, 92f 779F{011,92177964012, 9217796i915, 92177p6401i
Wilm
Repaotba
P6r.m.1e1
unift
Ra"
LiR/l M*nd Ou1N6en
Ant~Y
uyL
NO
610 11 RIS1S322:47
A11eroc
uyL
ND
10.0 1110611122147
Bsltum
uyL
ND
100 1100511322:47
Befyaerm
uyL
ND
1.4 11 MS11321,47
C6dmxrin
uyL
NO
1.0 1110511522:47
Crrcmlum
uyL
NO
S0.0 IVOW15U,47
Cobalt
uyL
ND
$0.0 111p611322A7
Copper
uyL
NO
10.0 11105N322:07
L..d
uyL
ND
10.0 1110511322:17
Nkhe,
uyL
ND
So.O 11MWS 22!47
SaWntum
4yL
ND
10.0 1wom322'17
sh..
uyL
NO
10.0 tVOW 322:47
lbokwm
uyL
ND
63 "M5N322:47
Inn
upL
NO
100 1110SI132247
Ybnsdlum
uyL
NO
2S.0 11705/13 72:41
Eno
uyL
NO
10-0 11l65113 2247
LA6ORATORY CONTROL SAMPLE'
Prtamo"r
1079005
Lira
SOk.
Coma.
LCS
R.eult
LC8
-A Roe
%Rec
Lh.e14 Oumhera
AnilrwY
9rL
600
5156
101
80.120
All.—
uyL
Soo
404
99
of)-12D
13x1um
uyL
No
497
99
60.520
Evryli..m
uyL
600
502
$00
80.120
C4drru­
uyL
Soo
499
96
80.120
Chumlum
uyL
Son
492
9e
60-120
CcU.h
uVL
Soo
491
9M
00-120
Copper
ugfL
500
497
99
10.120
L..d
uyL
500
495
97
8o 170
Nkke1
uyL
500
493
99
80.120
Serenkl
uyL
Ko
401
97
WAN
S0N4r
uyL
750
247
99
90.120
Th►loum
uyL
SDO
481
96
SO.12D
T6,
uprir
SDO
Soo
100
60-120
uprL
i00
Sol
t00
60-120
Zinc
uph
5m
464
97
a0-12o
P.- Anod VW Y 1.Me.., Ina. Pre. A-WW.W 1a 1ma., In..
Pee. maymcm l.nfur, In.-
r � E.N W.derr 14 d - Sms A 2i]S Rl w. EN
OW Kline" Ar. Sr.r 100
aceAr rytirar . Nc
Ed21760 Ad r4l.M94 - NC 28
mun*nwr.- NC M70
xww p..Yr. mn Pm%236921 i42M1254.7176
17D40mom
QUALITY CONTROL DATA
Pr.jW: BURRY CLOSED • MT. AIRY (UiC)
P.Pa Proj4ci No.: 92117964
AWTRIX SPIKE 5 MATRIX SPIKE WPUCATE: 1079009 1079010
Paramalar
92177641006
Wdfa R.eull
M$
6p"
Cone.
MSa
soke
C9nc
M6
Reet4l
u30
PtestA
M9
%Rec
MSD
%Rec
% Roe
1.141911.
Maur
RPD RPD Ou.1
Anamomy
uyL
No
S00
500
SO 1
501
100
101
75-f25
1
25
An 4c
uyL
NO
too
Soo
491
491
9a
98
75.12S
0
26
e.rh.m
PyL
34.s-1
$00
590
12$
533
96
100
75.t25
2
25
13 rY14um
uWL
NO
500
600
IOU
SO4
too
101
7S-126
1
25
C6dnuum
upR
NO
ZOO
Soo
464
482
97
90
75.425
1
26
Ch.vmlum
'sk
NO
500
$40
401
411
91
99
M125
1
25
Cob69
�VL
ND
Soo
500
404
495
91
99
75.125
1
26
Copper
uyL
NO
500
No
493
$02
96
100
75.125
2
25
Lead
uyL
No
SOU
5Do
477
463
95
97
7&125
1
25
N.ck.r
uyL
ND
Soo
SW
491
494
90
99
75.125
1
25
9.tenlum
uprL
ND
500
Soo
492
464
98
97
75-125
2
25
wasp
uyL
ND
250
250
246
249
98
99
75.176
1
25
Th.111um
uyL
ND
600
500
474
in
95
97
7a-125
2
25
Tk1
uyL
ND
500
Soo
491
401
98
99
75.125
1
21,
wI,14um
uyL
ND
$00
W
490
507
100
101
75.125
2
25
Zmc
..y4
ND
$00
500
444
491
96
97
79.125
1
25
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
+awn".a Wnpm*cd..—p1nnil. TMr.wn M.1 not WnP W. we.0.M.
Orle 11+13ri 01]92.72 PLS .1>narte....dn...—..r.luf Paw n.ur7vul srnlnr. I- Prq. 59u119 0.4. 11ri3R01102: 32 PM Mfttf. sm. evwM.l P.. A..W" S.rvq I- Pep. 60 of 79

Pbce An.lytl�el b.rvl[.t- ins. P.ta An41 yllul a.nl.e., Inc- P.[o AnmyS[er 5t
G4`nnryf J�a�� PM Fr,C 14-Ww—d-3.�V.r 7iZS AryerW. Ur MWKk,[, SW4100
7�7ee nr,.w.. rrc:2eew NC7ao7e
1a39Z3 W, 1bi6 4-7176 1704101541M
QUALITY CONTROL DATA
aroJecr:
SURRY CL05CO- MT- AIRY (I)ICI
Anne Protect No:
92177,364
❑C Fmdc
MPRP114016
Anotom Method:
EPA6010
Qc Belch Memad'
EPA 3010
Anah4fa Da 1pmw!
6010 MET NC 0roundwvllu
Ailapdg6d L W S.Ilpko: 9217796401 i, 921779640 f 0
METHOD BLANK
1067403
M51<1e- MNalel
A..odel.d Lah Semp14 [; 921 T796A045, 92177P64016
Blank R.P-Lkg
Ppmmeler UPRA
R4101 Lank
Anw"d OUaNflm
mr.—y
1+07L
NO
6.0 11MOM316,57
Am.N[
lrplL
ND
10.0 11 mm1] 1&17
Harrum
L
NO
100 1111314;17
0m
Eeryaiuin
u0'ug
L
NO
1..0 11106m1]i
C
NO
1.0101617
CN--
NO
100 1VOm1316;17
C.nah
IPWL
ND
10.0 11A611] fa'17
c%M-0
uWL
NO
10-0 Hqm! ] l6:17
Lead
ug'L.
NO
IQ-0 11106713 t6.11
Nlckel
Irpmt
NO
509 11"I7 L6:77
Selonlum
uyi
NO
10.0 111 m13 H;77
Sint
uyL
ND
100 1110m131110
T4mlllr
ZL
ND
5-1 1U0 3T6;17
T�
�9+L
NO
100 111"1318.17
Venadllm
uWL
NO
25-0 111m :116 i7
Il.c
LlVL
NO
19.0 111Nm13 I2V
LABORATORY C ONTROL SAM PLE
Paremelsl
1"140A
Ltnka
Sp+Ice
C.-
LCS
R—At
LCS
%A►[
% Roc
Limb 9lle6lipp
All,—y
uplL
500
469
96
50420
Nwu
ug&
%0
460
06
60.120
,.wt
500
479
9e
30-120
Hery4lun,
AWL
500
.94
09
6 - n
C"nIwl
-WL
000
AUG
9e
69. 120
Char—d—
u0rt
500
514
103
80.120
1%O-R
L41.
500
494
99
60-120
Copp.,
ugR
SOD
471
04
aO-QO
Leed
uVL
500
464
97
80.120
Nlekel
llq+L
500
501
101
to-120
Selenk,m
uymL
500
473
95
ED-120
Slnr
up7L
250
250
100
60.120
Thewunl
upmL
500
469
94
60-120
T.
u0lL
500
494
99
60-120
V4n4dhb.
1eWL
500
496
tog
60-120
Zllu
aWL
500
497
09
60-120
REPORT OF LABORATORY ANALYSIS
rN. --1 en.l ncr W r4preduced...rapl n AA1.
Dote 11113120110212 PM .,,.l N. wnu.n r:.n.—rP. An Wpl S.NIa Irc Papa 01 .179
P.[e AnYy6[.1 b.M[t 1, lu. P.- A nA1y5[el6wlu �, M[. P4[. A-1,d.:I 6ervle. t, M[
aceAnalytical • 705 9.11 N..yow Ru.p • SW I.n 224 ll—r.in. B.p9 klrvwy Are 6W loO
l Fd.n. N4 717a6 AO-1116, tIC 7e604 Vxml.,Wil. NC 70016
r+r.e rnw 5366]0A011 ext]31-717a ruge7svou7
QUALITY CONTROL DATA
O-Jmt:
Pan Ptok91 NO.:
SVRRY CLOSED - MT. AIRY IUI C}
R21 "1164
MATRIX SPIKE ■ MATRIX SPIKE DUPLICATE:
1067A05
f 062406
Ma
MSO
52177964015
Spike
Spike
Ma
MSD
Ma
Mao
%Aec
Mel
Pkr[mel.r Rnitil
RMWI
Con..
C9nc-
R"MI
Aaeh11
%Rep
%Rea
Llwm
APO
RPO 09AI
Anil.mV
ugrL
NO
500
500
490
409
06
100
75-125
2
25 J
Am"c
UVL
NO
500
500
455
492
97
91
75•S25
1
25
Hmium
u9rL
00.0J
500
500
566
$77
94
96
75.125
2
25
E[ry6mm
ugmL
NO
600
500
462
461
96
16
7542S
0
2S
Cadmium
ugrL
ND
S6O
500
477
462
95
16
75-125
1
25
V-0-lum
,giL
NO
500
500
499
501
100
f00
76.125
0
25
Cob.6
ugrL
110
Soo
500
S23
6DO
97
"
IS- 125
1
25
Copper
u0rt
NO
500
500
470
466
P5
97
75425
2
25
Lead
ugr-
NO
5150
50D
465
473
13
9S
76-125
2
25
Nickel
u0R
5.01
Sao
Soo
402
499
97
99
7S•t2S
1
26
Selbnk,m
Vert-
NO
500
500
477
419
95
97
76-Q5
2
25
5"00
W-
NO
2SO
260
2"
250
99
100
75-12S
1
76
Th.11hm
ugn-
Nil
Soo
SEE
454
461
9O
P2
75-125
2
25
in
qot
ND
500
500
419
497
07
M
75-1125
2
23
vankmum
ugiL
NO
500
S00
491
496
98
1OD
7S-125
1
25
Zinc
Yp0.
NO
He
500
461
494
96
99
755,12S
1
25
REPORT OF LA BORATORY ANA LYSI 5
The roW Nal n he mpraduad..xepl ne6.
Dolt 11/1372013 02:32 PM .H ,i me weimrn eeni or Pue Awymm a.nnn., ine Pty. 62 .179

P.a. A..I Val 'A /.rvl[i., "I. P. r,. An.1 yucal een 1 oel, Inc. Pa e. A..lyfkal larvlraa, Ire.
2aceAnaOical* m i..l Meedew Read - SuixA zn Ri..•w . QWO K+n.r Ay.. ll 1
Eoa.. Nc 77. A.n..e.. Nc JIM4 „n...wr.• NC M71
13MA232921 IB2 M4.71r6 (704I675•W92
QUALITY CONTROL DATA
project: SURRY CLOSED - MT. AIRY (ULC)
Pau Prole" Ho.: 92, 771164
OC BOO: M5VAU763 An04lo Method: EPA 92W
GC Belch Meet.d: EPA628O M.Mel4 13-Lpti - 4260 MSV Lm Lw.1 Lendaa
Aaovd.l.d Lab Sompla.- 921779640p1.92777960002, 92177964003, 92177964004, 92177864005, 92177954046, 92177 %4907,
92177964008. 921779640o9, 9i 177964414, 92177954011, 92177964QI2, 92171964013, 92T77964014.
92177964015,92177964016
METHOD BLANK: 1078587 M.61x: V014t
Assodaled Led Somoloo; 921779e4001, 92177954002, 62177954M, 92177664004. 92177954005, 921779640051 92177954007,
22177964005, 9R177964009, 92177%4010,92177%4011, 02177954012, 92177964015, 92177964014,
92177954015,92 177984018
Blond
R4VWInp
P.r.-L.1
I.I.M.
R.-It
Lim![ Mdyr.d 0-111.n
1,1,1,2.Te4achtwoamane
uyL
ND
5-o 11 MN, 301:96
1,1.1-Tdcidofoelh.na
uyL
ND
1.0 11 A6IM'd8
I,1�,2-Teeechkmelhon.
VL
ND
3-0 ITM&,341108
1,1,2-Tfich1weeth.'.
uyL
NO
1-0 1I105N301-04
l,r-0luhlbrnelnene
nVL
ND
5.0 11105713 O19e
$,I•olchloroelh4ne
aWL
NO
5.4 11 M51T301104
1,I.Olchlnropf opens
uyL
ND
5.0 11105157 01;06
1,2,3•Trkhlvwopene
uyL
Ho
1.0 111051130L06
1�,4-Trirh..benaene
uyL
NO
"Is 1100N130196
1.2•Dbroma3•chl9fopr0pen4
uOIL
No
13A 11NN130I:Q6
1,2•Dbmmoelhene(EDO)
upIL
No
IA IIAN1301;06
1�-Dld.rvrvb.neene
uyL
NO
5A 111OSf13QT08
1,2-Dlrflwoe0.ene
uyL
No
IA Wowl301:06
1,2•dd�wroprvpene
uyL
NO
1.0 1FA51t30,-06
1,3-pd.lerebenxene
uyL
NO
5.0 ItM13O1:06
f,3-01d.luvprvpene
uyL
No
fA 1I1067130,-9a
1,4.3ichrorobenten.
uyL
NO
1,4 11MU1301-03
2,2•0immopmpane
uyL
NO
15.0 11A5713 o100
2-8r.1anun. IMM
uyL
NO
100 1110511301;06
2-Hea4n4
uyL
No
So.O 11m5f,101 W
4•Melhyl-2•p.nl.nme(MI81K)
uyL
NO
100 11 tout 30I06
Acolone
uyL
NO
foe 11 ANI101 A6
Ace4onHfi.
VyL
NO
65.0 SSA511301:46
A-Wh
uyL
ND
Silo 11105111 a4ZIS
Acrltonleoo
uWL
No
200 "'VW'30, 106
Aeyl rd.lorld.
uyL
NO
10-0 1110511301-94
Bmsen.
uyL
NO
1.0 11145m301-in
&vmvchlvrvmelhene
u41L
NO
1.0 111050501-06
Brw.mdichlarvmethene
UDrL
NO
1.0 1IIOSN301-06
B-ojvr.e
uyL
NO
3.0 111O57I3 01:011
!1' l melh4ne
uyL
NO
10.0 11 AN1301;06
Carben .laurade
uyL
NO
100 1.611E 11 -06
Cerb9 1e91[Hkr1d4
uyL
NO
SA STAN 139$;06
Chlorc4on2ene
uprL
No
39 ISA511301!00
CNemerhene
uyL
NO
10-0 1110N, 30,-08
ChP.Wo m
up1L
NO
5.0 1IA5f13 Ill pd
Chkromelhone
upfL
No
fA 11ASR301:06
CNv.Oprena
uyL
NO
20.0 livP1301:08
de•1,2 pdn...e .
uyL
No
5.4 II1 wa III-%
P... A.WYlkal 8erv1e., t- Pace An.lylcv S-Itee, Inc.
aceAnadyticad • Ee.i Ne.dew Re.d - 5 u. R Z225 R-Nd. Or eedo R4 [., Rv. Su,. t
Eden Nc n7ee Aeh.w.- NC 26W4 1k~.Aa. Nt 21010
rtwj,I.pw"or. [7701923-0971 (671D)A5 7176 1104)O7S9097
I
QUALITY CONTROL DATA
Pr.lee(: SURRY CLOSED - MT AIRY WIC)
P1e4 Project No: 92177004
METHOD BLANK- 1D71617 Maa1x- Almlar
A.avdered Lab 6ampl.e: 92177964001, 921779e4002, 82177954003, 921779e4004, 92177984005, 92177061006, 92F77964007
9217796404e. 921779W009, 92177961010, 92177964011,02177%0012,921TT854015,821779ee01a-
92177964013,9211796406
K1 Il
R4pwhg
?uornelor
LMr.
RMuI!
Unk Anolynd Ovollm
d.-13-DlaW0pr.p.no
uyL
No
1.0 SIA511301.In
obromodwWomothme
uyL
ND
SA 11 XMI301;06
Diibromvmelhm.
uyL
No
10.4 II&NI101-011
DklllaodlflruoromaYlana
uyL
No
5-0 1Imul3 01.0o
Effho meN.nylera
vyL
NO
10.0 1110571301Q6
El.yken2ene
uyL
NO
1.0 I M5113 a1.06
Necaclaw0-1,3-bWedlene
uyL
NO
l0.0 IIMWI3 U%.06
lvdeme5ran.
uyL
NO
$0.0 11 ANI301 b8
1.ubu1.nv1
upfL
NO
100 1110"'101:06
M6el.oryknWN.
,1yL
ND
I 1f11161130,. 0
M.,,, m.Necryle1.
uyL
No
Solo $$MNI3 Q1 A5
Methyl.'. Chlwtde
uyL
No
1.0 11ASr130I-Do
Naphlh.len.
uyL
No
10.0 11 fow"01;06
ProonnIu4c
.9&
ND
A5
ISO 11113 O1 05
Styrene
uyL
NA
Is1Im"l3 Ot �O
ie4.d1lomchon4
vOrL
NO
IA 1110511301:0:
Tn4uoe4
u41L
NO
1A IIA67T301;06
9an.-1,2-dwaoathene
uVL
No
SA 11AN1301;06
Ir.na 1,3-pchia0prop4n6
UVL
No
1.0 111p51130106
trans-14. Dialvl.-2-0ulene
uyL
NO
100 11N",311;06
rnohloroaahen.
uyL
NO
1.0 11ANt301;08
TdnhkNumgR.ea.anm
uyL
No
1.0 i1A511301:08
Vlnyl.celat.
uyL
ND
so T1ASH301A8
Vinyl chloride
uyL
ND
1.0 $IMW1301-08
"I, -.'Total,
upft
ND
S.O I$Xm 11101:46
1,2-pd.tp.rxe.ane-0i;91
%
101
70.130 It1p6f 1301:0a
.com llumbansen.;8l
%
97
70.134 11A3ArT301-66
Tob.n.-d61S)
%
96
70.130 110D511301-09
LABORATORY CONTROL SAMPLE:
Parameter
1075eE5
Uni(r
Spa
Conc
LCS
Rmll
LCS
% Roo
% Ras
LYNN 0"11114n
1, 1,1,2.7obo chkroolha
up4
50
M.1
112
70-130
I,1.1-Wd0orv.tr.ane
uo4
50
56.6
111
70.130
f r1,2,2-7*V*ChMF 1.h.-
uyL
50
54-4
100
70-130
1,1t-Tr1dllbfeelllane
u0L
50
552
110
70-130
1,1.OIc1ilmo.9 ne
uyL
50
574
HS
70.130
1,140krimo.ihene
uyL
50
6020
120
70.132
I Ndsweprvpe'e
uWL
50
"1
+20
70.130
I,2,1Tdchm.oprvp.ne
uyL
so
59.6
410
70.130
1,2,4•TdoHo+obenden.
uyL
64
54.9
110
70.134
1 ,2•D�rpme-3•v+rGf epwp.ne
upiL
SO
IT 7
103
70.100
7��rbrvmvadrane l EDBI
uyL
5o
555
11l
70-130
l,2•0.chl-bom,w.
uyL
50
57.5
115
70.130
REPORT OF LABORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
Ttn.ep.d cornet h. npnd-dd. gaup n fill. Irw nNft N"-iW nr><ed .napnrut,
DaM; W1 WO 02:32 PM Mdwvt the wdoan -sen! of Pau AnOrecal 6orv4w., Ire.. Pa06113 of T9 D.T.. 11113RDI3 02:32 PM ..t-4 e.. wihen Deno". el Pau A-IyOurl 6amu.. Ins.. pope 54 0179

Aaa. AAN yb.01.M0/[. Ma,
V.=Rase-L.A
A4aa AAM VOW a4rHcs[,
le[.
P.[.Ar,aryyul e.rvl[as, In[.
Pa[a Ae yll.al Yarvle4r, loc. Pac[ A.."W l�
""I"
P.-Anallift, Fary}[as, M[.
f
AnAnapiCal'
706
Er rlM
77M RNarrea 9r
9e!f0 r,n<.rn.. &Ma f0a
CeAlla�f �C�CaI [
x00 E.0 M..ew/ R.re-SwlnA
22M I..W. Or
Uw Knuy H. bun 1N
0, he 712ee
Aah.HM- RC
9ee0.
Ihewr4 T. nC 200te
Ed- NC 272M
Am, %,
NG 206a
tM _*.. Me 24070
PR a. 4
nxxir�as2+
ra26r254.7,74
I7p4)67}-W9x
""P ' ° m*
ta3ala73 i
[ampm-117a
l7Y 61sBo02
QUALITY CONTROL DATA
QUALITY CONTROL DATA
pr0leCl: SORRY CLOSED - MT AIR" (UIC)
"act- SORRY CLOSED • MT. AIRY (VICj
P-. PrO* t N.. 121 i7964
Pace Pryod No.: 92177M
LABORATORY CONTROL SAMPLE'
1018666
LABORATORY CONTROL SAMPLE: 1079511
SPOW
LLS
LCS
%Rae
SA. Les
Let
%Re.
Paromotal
Was Cone.
Result
%Roc
L1r111R OIeLAan
Pu.matar
Untle Cone- Ruu6
%Rao
Llmhe
Ouoklom
1,20chl.-th"o
apfL
5030.1
1fa
70.130
Trid4w0euw a1hane
uprL S6 i9,4
70
IW-03
1,101mw.propan4
uyL
50
51.9
120
70•I30
1Anyl ■cola[.
OWL 100 $21
121
mils?1,34D1.N
.Smr
OWL
SC
S4.6
109
711-136
4lnyr chlmlde
uyL SO 60.2
120
a9-120
1,]•OlcmWoprop4ne
uyL
50
60.4
121
70-110
xylen. (70161]
uyL 150 S6a
IQ70.120
1 ,Qchkw.n.nzona
uyL
50
54.6
T09
10.130
1,2-Orch1P dO,ene-d41S]
%
IN
70.130
2,2-UlehcwW9P4r,e
gWL
K
4a.2
as
58.143
4-&omoh,lorohenrene (S)
%
66
70-136
2-BulAnon.{M EK1
OWL
100
115
135
70-145
Tokrene• gJSI
%
100
10130
2•Howone
uyL
109
127
t27
70.144
4-Metny1-,2-P_tanona [MIBKI
uyL
109
122
57,E
70440
Acoune
uyL
IN
133
133
60175
MATRIX SPIKE E MATRIX SPIKE DUPLICATE' 1071619 f 076690
AcotorwIre/
'WL
600
639
128
MI 30
MS MSD
A..W.
,lyL
250
353
145
70.130 F3,L3
92177964006P Spike Spike MS
MSO
M$ MSO
%Rn
Mali
A ImKA.
uyL
250
291
111
70.141
pvem"t
Uh64 Reou6 COL Conn. Result
Raedl
The %Rot
Llydla
RPO RPD Owl
A6V rN.rld.
uyL
50
57.3
115
70.130
Bens4na
4L
50
544
}69
70-110
1,1-01ahl.roewew
benzene
OWL NO 50 60 54-7
upR }.19 SO 611 19.3
V-0
59"
111
116
114
114
70-16E
70.146
3 30
i 30
Elamad4nrom411ano
,r{IlL
50
53.E
1.
70.130
ChIDrobenzene
62& 7.7 50 60 607
il-B
f06
107
10- 46
0 30
&arlwdlull0r0man4w,a
uyL
56
65.7
1l1
70.130
Tai"na
uyL ND SIt 50 53.7
52.1
107
105
70.156
2 30
61Ongrarm
uyL
60
47.5
15
70139
7dchl0ree1hen4
uyL 0.161 Ib 50 596
57.6
111
114
69-151
3 30
Smmomem.n.
uyL
SO
51.0
102
54-130
1,2-Olchlwoelhane-dl [SI
%
I04
SO1
70.136
C. tm awd do
uyL
50
55 5J
Il1
7b131
4•Brnm06unr0ben2ene jE]
%
97
96
MIX
C.rhan t.1fil r14.
uyL
50
53.0
Ili
10102
7Mwne-dd (S]
%
100
1a
70.13C
ChlaaOenzen.
uyL
SO
64.E
Ica
7b130
Chl. L,ene
uyL
50
3a.8
74
64-134
C40:O'm
uyL
50
$7.5
115
7b130
ChlwomeMane
4L
5D
60.1
120
64-110
Lhlerupiene
UWL
50
44.8
130
70.t30
d.-1,2-0icNwwewene
RyL
50
51.2
}15
70-131
d}plchlw0prapcne
uyL
50
69,6
119
70•T30
DI6r.mO.N. an,.a,ene
uyL
50
49.6
100
7"'
OIOrl.m.m.lh.n.
UyL
50
6e-7
101
70-131
D4Chluodieuwur 0cO'.
UyL
50
6E,I
130
S6.130
EuIH nbNveryLl.
uyL
50
61 2
122
70.'30
EIhyN.m.n4
uyL
50
626
161
16130
Haaecldara•1-3-6uladl.ne
uO+L
50
5215
10
70130
le00 n mrno
uyL
100
125
125
49•}80
Ia.6Wanal
uqR
INN
1260
125
70.13a
Me6lattylpRllfNe
uyL
S00
i16
123
10130
Menlyl mem4cryl4le
uyL
50
53 3
107
10-110
Memylene Lhlmlde
uyL
50
60-4
121
63.130
N.Oft.kne
uyL
50
53-2
170
M138
W.O.Pwwo.
uyL
500
641
121
70.130
5ryl.ne
uyL
50
56-0
110
10-110
7e1r...NOmeU..-
OWL
50
54,2
108
I&.11
luhren4
uyL
50
63.1
106
70.130
uano.l,2•pONuro.ren.
uyL
50
59-6
119
70.130
Yam.l,]•DIWar.plep. ne
uyL
50
!2-Z
114
70.132
e.n.-1,4-CM-M e-2-0uL4r,a
Nyt
50
a5 ,2J
160
74141 L3
TH.hhm.&Ih-.
uyL
50
St?
105
70-130
RE PORT OF LABORATORY ANALYSIS
REPORT0F LABORATORY ANALYSIS
TN. r.WP ..A ear
w,.P•POuc.a..rww kr.
T1r. np.n.hM w1 o...geduc.d...c.P n hr.
pole: I111_W013 02:37 PM
�F.wl aM x Ilmn co-,r.nl'rr Pae. Malvac.l $.rr•ear- me
Pago 65 01 7a
Dare. 11013-1200 0212 PM
.,,r..w..a..ft �enw•w ar pace A Iyww e.r.aa.
..
rLwp 6A 0f 19

P.O:Anal rAcat a.mee., Ina. Pace OL-mydc.I a.rrin., tax.
�
msc ...o—Rom-� A 2nsri . .a.
aceAnalytrcal
EA.n. NG 2 M Ali.Nl., HC 74
I
IM023-e921 (626)25 i TS
QUALITY CONTROL DATA
P.91act. BURRY CL0.SE0 - MT. AIRY X1ACI
Paca PPo)Gd No.. 92177994
P.1. AealMdu.e.rvlsn, ne. P.;. A n.l yU..l e.wlea., Inr. Pa.. A n.lyVnl au.l.a 1.In..
9eW tc.Kn n.. sNu :00 7e>5 E... k....w+Ra.d sNr A 2m R—usw l)t
n .r�.. 2'! aceAna✓ytica� E4.. N� 710ea aNnN., NC 7eea.
i7wb1s9w1 17.tepvae7l Id7a 17S.•itM
OIJALITY CONTROL DATA
P.el.cl BURRY CLOSED -MXT AIRY(UICI
Pace Propel No.: 92177%4
0C Babch: Y&T127942 Am"ki klem9d 5M 4500S2D
OC BakA Meowd: SM 4590-s20 Ankk'als ONwkwon: A OMO SkAm. Wt.
Aued.l.d Lab 9wmPAa: 92177964001, 92t179MOO 5, Q 11710114 007. 921?7994011, 9217761"012
METnO BLANK' 1078542 Matrix: Water
AaeaNatad Lab SamPla9: 92177964001, 921?7964005, SP2177964007. 9217 7264011, 92177%4012
Blank Ra"g
Pereme%F Vnke Reevk Ur.el Analyzed Ow9Aers
Sur"m US& NO 1000 11IQW1310.29
LABORATORY CONTROL SAMPLE; 1076663
Splka LCS LCS % Rea
Pmameler Lk19e Csnc. Result '1L Roe UmIM O1111"m
sinew uyL 500 526J 105 Will)
MATRIX. SPIKE S MATRIX SPIKE DUPLICATE: 1076664 197950
MS MS0
92177769001 Sp1ke Spke MS MSO MS MSD
%Reg Max
Pw%rrLMar U.14 Rea.4( Cwc. Cease. Raso Rasa! -A Rae %Rae
LIR9te RPD RPO Oua1
Wide -01- ND 500 500 509J 509J 107 102
75125 9 20
MATRIX SPIKE A MATRIX. SPIKE WPLICATE: 1076569 1076561
MS MSO
W1779SWO4 epka spike MS MSD MS MSD
%Rac Max
Puemm"t vnfta Ru%AI Cane. Cone. Rdaull Revell %Rao %Roe
LkN1s RPD RPD Owl
Sunda vg& NO SIX) 600 .90J 400J 96 66
75.125 0 20
REPORT OF LABORATORY ANALYSIS
iN. r.port N.1 net h. r.pmAced...eapt N.
Dale. 111 t 3R01302:]2 PM...e.o..1 .h..nb.n ceneNLLar Aau A� 41W S.=4R P.O. 61 e179
naa. Analy%.l e..vlt.., Ins.
9g0%"Aw s-4O0
µ.wrcw._ Rc 7e07a
(70{M6750=
CC Sstch. WET12796Q Anslysl. MM.0" SM 4500-S20
0C Belch Method $M 4500-S20 Analyels OaeMpn9n, 4500S2D Su16de W"
Ayeocloled Leh Semple. 9217704002. 92,77964001, 92177964ON, 92177904Q10. 9217T%4011, 921T7964014, 92117964p16,
92177964016
METHOD BLANK: 101tWZ5 Meyit- WMNr
Aeeed44ed Lab Sathpls M: 92177%4002.92 I t7%4000, 92177964006. 12117 %4010, 9277704015. 0171064014. 971179540115.
Wt77" 016
Blank Repo"
Pww*tw UnkA Revell Link A..ly..d C1.01—
$.aed4 POOL NO lom 11AW1313:00
LABORATORY CONTROL SAMPLE: 1050M
300 LC8 LCS % Rac
P.ram.lar Unma Cane. Raau11 %Rae Uml4 Qum,"
SWed. uWL no 501J 100 00,110
MATRIX SPIKE A MATRIX SPITE MPLICATE: IOM27 IOW26
MS MSO
956 21777001 S*' Splits MS MSD MS MSD %Rae
Mae
PMamat.. Vgl1e Rawll Conc. Cone. RnWt RaauA %Rec. -A Rae Lkota
APO RPD Oua1
some upL NO 500 500 NO NO 0 0 M125
20 Mt
MATRIX SPOKE & MATRIX SPIKE OUPUCAT E: I0M29 I ONO 0
M$ M5O
92177967001 Splke Spx. MS MBO MS LIBD %Rac
M..
Param4W UNq R-WAI co— Cone. RaaW1 Rom* %Rea %Rec LANK
RPO APO 04at
SJede upL NO 500 5W NO ND 11 11 75125
70 Mt
REPORT OF LABORATORY ANA LYS IS
7n...wn aW In­w.....µ MnA
D.te: 1T113RO 1102:32 PM ..14w1 e...n11.n --t Pr Pen mmlvt l 5.—., 1- P00e 66 or 70

/-, ceAnaVical*
P.N An.1 yL..1 Hrvlr.., me Pas. Ar Iyliepl J« Lta., Inc Pit. AemlylYml HIYI4a., 1.0
Ro.a 5r,..A 7775 A".fla. Or 9W0ker4e awe. EPu1102
k den NC I1_+kg AaN.rn.. NC 76g01 IMunYmNe, ryG awn:33e)62)-e 7r '02e1754-711g I7011e754092
QUALITY CONTROL DATA
P-Jed. SLHWY CLOSED - MT Ai RY ILI Ci
P.- Pny.d Me 92177964
Of; 8.10 VYETf2bol4 A—"'. Me7wd SM 45DDS20
OC F-wh Meg..*: SM 45mwv APelymle Dew*W-4500670 S. Wq. YWIn
A..wel.d Lab Sampk. 1121 T79M004. 22177964006, IQ f 77054009
METHOOSLANK- 1061655 MOVA: lryYYr
A.egd.led L" Se mpka 921779M00e, 921719MOOB, 9$177IM4009
Bunk R.Portr,p
Pm,emet.l I1n114 Result Llml( Anelyeed Oualifion
5u" uW1 NO T000 1110711110:31
LABORATORY CONTROL SAMPLE: I W1656
SPIN LCS LCS %Pa.
pu.meser Vnae Cone. Reel/1 %Roc Llml. 0-111 ee
Sulide uMKL 500 5301 106 W110
MATRIX SPIKE A MAT RIK SPIKE DUPLICATE 1011157 1011158
MS MSO
97177964004 elplk. Spike MS MSO MS MW %R.c. Mail
Pa,omel.I LKYt Raddl Cann Cent- Rosin! Ramm %Roc %Rmc unit RPO RPO Duel
Sdkdm YgIL f1D 50o Soo 3371 5371 R07 lot 15125 0 20
REPORT OF LABORATORY ANALYSIS
Tw r w- ehe4 em a r. P'op.cr4..,.1m n '-
Palo: II11 V2013 03:32 FM ..4—"r.nYn meetm+ I Per. J.vy� s.me.. 1.c P.O. 69 nr 7.9
eeAna"icalf
F ass.a
r
Pen AMlytleel urf1u., Inc. Fees AnalyPoi Hryl.al, Me. Pan An.Iytleal aeMuf, Inm.
705 [.0 M..— A.M - S..Y A 2225 Fl w Dr 91100 K—., ! . 6u tm
Ld.n. w 2720 AY -". NC 211104 .w.x.iwe.. NC 2e076
I umn4921 K6761734.7, 76 1164ia,SAp97
PrgpgL SIIRRY CLOSED- MT. ATRV WIC)
P... Frepd No: 021779M
OO Bdrh. WETA117026
OG Belch M.mod: SM 451104N-E
Amagdal.d Lab Serrplea: 92177964001
METNODBLANK 1062311
A—.I.d Lab Se p4— 92177%4001
Pr meter UPha
Cyanlde upL
QUALITY CONTROL DATA
Anatt,4. M.Owd• SM 450D-CN•E
An.". Dm-4sk n: 4UR CNE Cy -Id., Te t.1
Melee• Wear
Blank RepMwlbO
ft.wl urrA Andlrred 0"Kiws
NO 100 11 AWt 1 13:3a
LABORATORY CONTROL SAMPLE: 1=312
Spike
LCS
LCS
%Rae
Parem.t.r Ufa.
Cenc.
Raa,N1
%Rae
LI11We
OuaNare
Cyeldda up4
IOD
fit
112
W120
MATOIN SPIKE 6 MATRIX SPIKE DUPLICATE: 1032111
1062314
MS
MSD
92f7745600f
30ke
90ke
MS
MS0
Ms
MSD
%Reg
Me.
Pe.amau7 Uh6k Remot
Cone.
co".
RH A
Re4.Yl
%Rag
%Reg
LkNti
RPD RFD 0u11
Cy.md. up4. 0.6]
too
$00
614
me
411
-443
75,125
45 20 M1.R1
MWL
MATRIX SPOKE Il MATRIX SPIKE DUPLICATE! 1062]1S
1042310
MS
WD
92I776ium
SP9Ra
soka
MS
MSD
MS
MSD
%Reg
Mae
Palam ler upft Bekull
Conc.
COM.
Rgkull
RmA
%Reg
%Reg
LIMIs
RPO RFD Ouil
Cyaroda log& 5.61
too
100
41.7
42.5
36
37
75-125
2 20 M1
REPORT OF LABORATORY ANALYSIS
TN*-w NM -16. nr.vw.ed. erwl. h.I.
D.1.: 11113RO 13 Ot 32 PM weKKn se.e.YA cme M Pee. A..f10eal y. Ape. Mr
P.g4 70 PT i9

Paao An40..l SoMN., In,
. Peel Amtydul IerNeeo, Ina P.-A.Wyeeel E.rvlu o, Ine.
;aceAnWica)" W5 E.H W.d.. Ro.d • &Wa A a22a R v.rery 9e9a I9 wY Ae. SW.
iCC
Edon NC 277aa A.).WN- W 2aa04 Hun11rw9e, NC 20071
[3381621E92, fe2&pS1-r17e j7o1I87SPo02
QUALITY CONTROL DATA
Propel SORRY CLOSED - MT. FURY {MCI
Pool Prated No.: 9217T1B4
OC Imici, WETAM7060 An."Ia M4Mo,;; SM45H,CN-E
GC Balch M.th d: SM 45W-C*E Ano". 10"Wipit W! 4500CNE Cy.Md., TOM
Aaiocleted Lab Sampi.a: 92177%i009, 92577904007, 92T77%4011, 92177264012
METHOD BLANK: 1003391 Meal.: WYte+
Aeiocumed LW Semptee 012177964005, 921779640D7, 92177964011, 02177964012
Blank ReporOng
ppame,er UnNi RpouK LI1nI A qW.d 0u11Aen
Cy-W44 uprL 14D ItlA 1111(0310.46
LABORATORY CONTROL SAMPLE. M"II2
Splk. LCS LCS % R..
Per Rmm, UnRe Cant Resin, %Reo OrNa 046,11 ro
Cyanide UWL 100 101 101 50.120
MATRIX SPIKE 4 MATRIX SPIRE DUPLICATE- 1063393 10133114
M$ M5D
0217E274003 Spike Spike MS MSD MS MS0 %Rat Mur
Per. —I., UM. Ra.WI Conc. Conc. Result Revell %Reo %Reo Lknlle RPO RPO Dual
Cy.nlde u9t ND 10) 100 1D1 99.9 97 90 70-125 1 20
uATR IA SPIKE L MATRIX 9.PIKE DUPLICATE: 1083395 1053390
M9 MSD
217 97043001 Spike We MS MSO MS M80 %Rao Mao
Par.maler UMn A —At Conc. Conc. Re.uil Futum %Rae %Roc Umk4 RPO RPO Cull
cmicla ND 100 IN 103 1D2 99 07 75-175 1 20
�acemalyfical
e,.Arraa r'.
Pa ee Anal y9[al 9a"Icae, In.. Pr la Amlyee.r 5"101, Irl4- P.M Rn4lYacel 6fnlaaa, Ma.
205 E ee1 Na odow Roed - S. to A 2225 A—cim Or ea00 wrr r A: SN. 1W
Eee�. NC i776a AMMI., NG 2eBW YEnilreHla, HC 78015
t 77aAn 0921 ra26r754,7176 (M-A154r19!
QUALITY CONTRO4 DATA
Prel.ct: SORRY CLOSED - W. AIRY (VICI
Poee Propel No.: 22177*64
OC Botch: WETA117011 Malyalo Method. SM 4500-CN-E
QC Belch Me mod: SM 4100-CN-E tinsel$ Oe$ulp9on. 450OCNE Cyanide, file)
Ao.xiol.d Lot, S.nptea: 92177964002, 92177964DD3-92177064006. 92177964010, 12177064013, 9217796401{, 9217796401S,
021779940W
METHOD BLANK: 10133117 MI14k- 914Mr
Associated Leh SR mpiei: 92,77904002. 92177964697, 92177%4 D(A. 1217T9&1040. 0117 7084013, 921?7004*14, 9217706401 S.
92T77964010
Blink Rem"
Parameter Unka Rae1d1 LIMA Analynd OuelAm
Cyanide UVL NO 10.0 "110013 TIM5
LABORATORY CONTROL SAMPLE IU3198
SPAu LCS Los % Rae
Pramallr UrWm Cent. Rosdt %Reo Umkl OualAre
Cy4nlda uBIL IN 102 102 10.120
MATRIX SPIKE 4 MATRIX SPIKE DUPLICATE: 1083399 1003400
MS MSD
92177WD01 Spike Spike MS MSO MS MSO %Reo Ma.
P.tartlale2 Ur10a R4s it Conc Cont. Realm Raoul, %Rao %Roe Umld VC, RP13 Coal
Cyor4de uBL NO TOO IN 104 104 19 99 M125 0 20
MATRIX SPIKE 9 MATRIX SPWE DUPLICATE: 109HOI
1053403
IRS
Mao
112177964015 Spike
Spike
MS
MSD MB MSD %RW
MRR
Pramelar WAN Raa1At C-6.
Coro
Result
Re ouA %Roc %Roc Urritl
APO RPO Duel
C9er9de u01L 10.3 100
IN
104
06.4 94 6S 75.125
d 20
REPORT OF LASORATORY ANALYSIS REPORT OF LABORATORY ANALYSIS
iM open Nee naive tepmACM. coupt h M.
TN. r.parl Y,el rnl a lepreMrced- nceW n M.
D.I. 11r1 W2013 02:32 PM rtomm"rw1T11n ow,.e.n of P— Arlleral s.lrnle. Inc Pepe 71 11179 Dole: IV117013 02;32 PM —I ar Pon Analyenl sear %.Ine Page 72 uI 711

Pau ArW ylkal 9eMCar, la.- Pace Analyllcar e.rylcea, In.
Ind Ease M..d.w. React ea - S. A 2225 R.RW. br
f aceAna)ytica) E", Nc tr2ae A.n..n.. NC 2ee0+
Ire .w.I��•w.. (] Pd2]-e1R+ lae812.+70s
QUAL$TY CONTROL DATA
pv.l*cl BURRY CLOSED - Mt. AIRY (UICI
Parr Pwpn No.- 021771164
OC a6ull, IfiETAr1 NX12 Ana%... Method SM a500-CH E
OC Basch M.d.ad: SM 4500-CN E MRIraIa D"cavii n +300CNE Cyarwda, 1'olal
Aea.deted Let, Sample, 97I77911e00e, 92177III&Q09, 82t77964000
P— Analrn I !.tyke• Jac- Poo Anelykel MM.q, 1.$. Pao Aeslylleal aar.lp.a, ie..
9aoe Iu.cey A,. S,x. 10P 2[H Eax ware%Road - SuG A i235 R*.Y or
r..y.r.v... HC 1607e _ - aceArlaly[rcai ea.,, W.. ar20n A.howdPe, NC 2ee04
Irw 161S9w2 ' 'e�+'r"' nc" 11Ta1a23-092I faMI&A-717a
QUALIFIERS
Propct SURRY CLOSED - MT. AIRY lUl Cy
Pace POpcl No.. 92177B64
METHOD BLANK 1093406 Mail. Mier
Auwial ad Lab Sw,pkia 9217796e00., 92177964006, 92171964009
&.id fka"Tk,u
Perameim U.N. Resell Lrmll Anelyaed qua1116ers
Cyanide uWL NO 10.0 1111INn T139
LAa0RATORY COWROLSAMPLE. IG93407
SPIR. LGS 1-C9 16 Rec
Petarpeler UnMe Cone Ree1/1 %Rap UmM Quals.,
Cyx,td. u0fL 100 11119 89 50.120
MATRIX SPIKE S MATRIX SPIKE DUPLICATE: 1 D00400 103400
MS MSp
02t77"'W3 Swke sot MS MSO MS MSO %Roc Me.
Param+le, LPdd Res.al Cane cane Raa,d1 Reskm %f7.c %Roc Lknu RPD RPD Over
Cy.nida vyL ND 100 100 sol 107 105 104 7'✓I25 1 20
MATRIX $PIKE A MATRIX SPIK€ DUPLICATE- 10i3s10
t0113AII
MS
MSD
92177092010 Spu
"a
MS Mal)
MS PASO %Rac
Mez
PeramaM VIA. R"W Cane
C—C
Re.Idl R;.un
%Rea %Rea Urnks
RPD RPD Qu.l
CyMilda 494 O.0051 100
100
107 103
102 09 75125
3 20
M9fL
REPOR1 OF LA80RATORY ANALYSIS
Th.,.Me .h%.-- anp.eMrpW...capthN/.
Oste 111f 3OW 3 02 I2 PM ...w I,.. w'"- Co- k.w r Pe"Iyaua i ura. i2
Page 13 el 79
Pau Myypeq 5.rvr.rs, Inr.
Beer)K�.r A.. 15 i 100
I rwt%., HC MOM
li0e)aise097
DEFINITIONS
OF - 01u4- P-40' II repprrad. repro actors the f.Ow .pplled in the reporled d.la due 10 changes in %ample ptepretl0 . dhitlon of.
1h...mple aetpwl, er ma.lur. c.M.M.
ND -NO Dew at w .Cora adpsted Iepwtthg Howl.
J • Esarneled M Cenaeum abwe die 4,1 Pslod merhod detteti" Nmll and bal w the ad)uelfd fepm ling Il and
MOL • Adiusled Malhod Delec9pn Uni.
PRL - Peca R. periv,g LImR
RL - Reowan0 L"
$ - SurtOgAle
1'2-0
1
phenylhydrasln a 16270 Hill"snatyie] decomposes to Azobene.ne.
CPneialCei 1W111 EPA gvkleen es, unrowndad dsla are dleplmved and have been weed la calculate 54 recnw. sod RPD Values
LCS(D) - Labwelpry C.Mr.1 SampN {Dupllcx.)
Ms(D) - M.YIa Spike joupllcare]
DVP • Semple Dupwcne
RPD. Relaft. Aar curl Dltler once
KC - Nd C.Icutahr.
SO - Note Gel • Clean -Lip
U • Induies the cemimmind seas anslyrsd tor, tall nos dniteted
N-Nlbwodlphenyla mine decpmp0en and eanrlpl b0 %epar sued Arm Dlphenylsmine Wing Mail, dd 6270 The re.uK eeprMed for
each aneMr Is s earrw.iad eoneanleallon
Aid peeaarva Yon may not he appmpdato k. 2-Chum a semyiwnyl ad.ar, Styrene, end VmTI dawlde
Pace Ans"Le 1e TM acue died. Cantad yow Pau PM iw OH a rmnl het et eca 061ed evakres.
TM • Tha NELAC IMiltula.
LABORATORIES
PASI A Pat. Mdytkal $".a. - Al he,414
PASI-C Pace Analyrkal Service%-Chadppe
ANA LYTE QUA LWI ERS
F1 Th. r.covery of IN. a.eond %0ww sl and-1 W ad la v 11f, Ih. MeaF WWAMW c . fw IN. anaMyt. N oul.M. 9e.
IabwNorY% —$mL NMI.. The nauX K sa9mdad-
W Analyser covery In die Iabw Rlbry a MFOI as mite ILCS).xeaeded OC Ilmila. AMIIVW presence bdew repwung IImt. in
upd.led setnptn. Rmrw uneX.ged by high bier.
Mt Matni spike rii very aacH dad OC Fin11a llaren apeepled EHad rMt labualary pMlld aarreaa {LCS1 recw cry
Rt RPD Value w culalde Wnhq 11rryra.
REPORT OF LABORATORYANALYSIS
Tie. rapid ah.l a.i be r•W, ....-Pt n ti.
Dais: I1013Q013 02:72 PIA w.i Ih..w.a.n w„euu of e.T. 4rlyar,.I p.r.+w. xc
Pave 74 0 79

Pan Anliy6ee16:,A . I-.
P— Analy�l[il ealrli.a, Inc-
Paw MYyw.l ■mi-k 9w-
Pau Awylb/i S.Mu1- Ms.
P.e. Analydul a.ryln.., Inc
P.W AnMylkal a.rvin�. Inc
I PPnn
• .' �LL f v rr•I+
IIXII •
205 EEC i ffi r React - iuito A
i.hn, hC 0284,
nN Rk.1.M. Dr
AYwrM. NC fLe(tl
om Rine.714a. Su 100
YFwwlnrra, INC ]11176
r� p �Ay/']�
uc`r � alytical
a
Jn
NS E..l Mwdaw Rob � 6uH A
E; NC II ]aa
2325 RlvaiWi a
+�NivN. H[ Tp6pl
9 Nrc.y Ar. 5— 1M
11unMI Ma- rv[ 7eo iE
�"'��
mm
I]1r+167]-097I
1e7e175i-Tf f0
f704W739092
r! ��
�"
13]aIM1T]2921
(lYey75i•717a
f70i167SBW2
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pfo7etl
Sl1RRY CLOSED • MT. WRY ILIC)
PrGje l'
SLURRY CLOSED- MT. AIRY (VIC)
Pace F.*cl N.
1212?9154
P4e< PrMocl No
02177966
AfulyRcai
Ahalyfiul
Lob IO
SamPl. 10
00 SM9h Mwled
OC Batch A..Iyllc.l Math.d Batch
Lab ID
aampl. 10
QC Baich M.y7ud
QC Batch Am"ul Mathod Balch
92177fµ601
MW1
EPA3010
MPRPr14560 EPA6010
ICP111250
12171164016
Mw-22
EPA8260
MSYY247a3
11177f64001
MNf-2R
EPA3010
MPRPr14580 EPA 6010
ICP111250
92177ti Will
MW21
EPA U60
MSW24763
921T7964007
MW1
EPA3p10
MPRP7145a0 EPA6019
1CP713250
92177e64001
MW-1
5M4500-52D
yyET1219u
121779a4004
MW5
EPA 301a
MPRP7145 e0 EPA6D10
tCP113250
021771640ve
MW126
EPA3010
MPAP114510 EPA6010
ICPI13M
92-177164002
ItW3R
SM 4500-82D
WET127960
}217716400B
MV1.17
EPA3010
MPR11450 PA0
ICP11250
7
SM 45•e2
WTW910
MW-14
0
PAP145a0 EPAa❑
MPT01
ICFY 320
l217Y1a4O0o]
W-v
SM 0-5Y0
1977964007
WETf2604
92177664001
MW-ta
EPA3011
MPRPIT4567 EPAeotO
ICPI13257
92$779i4006
MW-115
SM 45W620
WEYVV042
MW-1176
EPA]0L1U
MPRPI1f45aEPA6D
03257
:21794000:
17741
MW-
EPA SOD
MR,5PA0f0
CPI5257
92S779i4D
MY-1y
5M0.520
WET1210W
f
A0
M3
PRPli5a] EPA GO10
CP725
92177964011
MW-19
EPA010
tl
13257
07
M14
Mi5
S00-Wo2
WET2792194
911177964O0t17
MW-220
EPA0110
MPR1114555 EPA 80110
Cp1325
W{
SM 4S00-=
MW1
EA 30
MPRPl43 EPA
a0
CP7325
17
9179g006
W.
SM 4WD-S202Y116{4
WWTjl6014
60
1Y1T796601i
MW22
EPA2010
MPRP114016 EPA6010
PCP113289
17177964910
Mw.17
am 4500-520
VVET1279e0
};1Y716401d
MW13
EPA 3110
MPRP114616 EPA 5010
ICP113269
621179a4ptt
MW16
SM 4500.520
WE T127442
"I779{4001
MW-1
EPA 74 19
MERP15774 EPA 7470
MERC4556e
OZ177064012
MW-11
SM 4510-S2O
WE11279+2
.177l 4002
MW4R
EPA 1410
RPM? 4 EPA 7470
MERCA 568
9217796401]
MW-20
SM 4500-SZO
WETr$7960
121T7164 a03
mW-7
EPA 7470
MERPf5774 EPA 7470
MERC15586
9]f 77f 64014
MW-]T
SM 4500-570
WETf27980
92t77l44004
WIN-9
EPA 741D
Id ERPR774 EPA 74n
MERC/5566
921771:4015
MW22
SM 4500.510
YVETM 10,
92177964f06
Mw-i2S
EPA 747D
MERPIS774 EPA 7470
MERGS5M
92177994006
MW-13
EPA7470
ME4lP1577i EPA 14110
MERC+S5W
92177954016
Mw-27
SM 4500-52f7
VMTr279a0
92177a140"
MW14
EP^7470
MERPPS774 EPA 7470
MERCISSaa
121771,44001
mw•T
SM 4500•CN-E
WETN170Y6
92177164006
MW-7i
EPA7410
MERP13714 EPA7470
MERCM586
w177}G4002
MW7R
5M 4500•CN•E
WE TN17041
92117964001
MW-16
Ef917470
MERP:774 EPA7470
MERC15Sea
171776eiGG,
MW-7
SM 45W-CNE
WETN17051
l21179649tp
.11
EPA7470
MERP15774 EPA7470
MERUSS86
12177184011
6tw-1l
EPA 1470
MERPW74 EPA 7470
MERC15556
97177aMOv4
MW9
SM 4S00-Cry-E
WETN17082
IW77164012
MW-11
EPA 479
MERP1576D EPA 747q
MEPG15591
92t77 aa4006
MW-l23
SM 4500 CN-E
WETAi 060
92577l64013
MW-]0
EPA 74T0
MERPIS700 EPA 7470
MERCM591
52117954006
Mw•11
SM 4500-CN-E
V4ETNS7061
905Y 796i01i
MW-21
EPA 7470
M£RP15760 EPA 7470
MERC1S591
}217713401a
'Iw•27
EPA 7470
MU6115180 EPA T470
MER"591
92177164007
MW-14
SM 4500•CN•E
WETAn 1061)
111779641,16
MW-23
EPA7470
MERP0760 EPA7470
MERC1S591
y2177994006
SM 45 DO-C-E
WETNiTM2
17l22211177777764p0p0t
MW.1
SV2il6]
2164[
I1W1d
50•CNE
WETN7D62
1EPA1e
a
EPA260
46]
MSVY27
7
9279g01u
MWt7
SM 4500-CN-E
YJE TN1?ON i16400
Y3
MW7
A am
SVQ4763
121714404
MW-1
EPA 1260
MSVr24763
9217796ip11
Mw-te
SM 4500CN-E
WE TN 17p60
12117164006
MW12S
EPA a250
MSVr24783
9211796E 012
MW-t1
SM 4304LN-E
VJETflV OM
12177964006
KW-13
EPA 0260
MSVR47a3
91i77f94013
Mw-20
am 4500•Cf4-E
1AETNf7081
92177164007
MW14
EPA 8250
M9Y7247Al
T7177!{4014
MW-YS
SM 4500•CN•E
WETA, 61
11177164006
MW16
EPA 6260
M$V12478]
9]177964015
MW22
SM4500-CN-E
WETAIl7061
921111 w9
Mw-lf
EPA 02a0
MSV24783
92t779l401}
MW21
8M 4"0-CN-E
MtAt D61
121779N070
MW.17
EPA 62So
MSV724713
92177664011
MW16
EPA 6260
MSVr24713
@2177994012
MW-11
EPA82e0
MSV124713
111TN64017
VW-20
EPA82a0
MSVY2475]
li1776640t4
A19Y-21
EPA 8290
MSV124763
REPORT OF LABORATORY
ANALYSIS
REPORT OF LABORATORY ANALYSIS
TrvE lipwt VUE iglq nrpipbeW, tedq it 1J1.
Tr« •a1M M 1. N Wobd.ew....a h W
Data 11113alJ13 02:32 PM
75 Pf 79
Oale
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Corrected Cooler Tam �1,1 i C Biological Tlaauo 1, Fwxan: Y.. No �fL�l'
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Temp Fho,sd 6e sows freaTYp 1d 8'C Lommenia:
qj1� u"d Insist nr peraon...minlna
contenta:[�4� rrlr:'r f _
chain of cuslody Prowl: i ON. DWA
1,
Chnln of Custody Filed W Ud .. U-. 13VA
Chain of Cus RalLaqwspi klsd: Z(v.. Ow. Owe
3,
Sam lar Nonlo A 5 natura on COG: . ONS OW
4.
S arnplo, a Arnvod wirhln Hold Time: f2�.t r)ra OWA
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short Hold This Mal hi 02hr : Ov.. Ufft Owe
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Rush 7um Around 71ms Re anted: ❑v.. rb CIurA
7.
SullkJenl Volume: fya. 0OwA
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Cvtred Canlelners We& //Yn QN0 l7wA
-Paco Comalnen Used: iJr . Dfw LWA
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GoMalnen InlacL dy. Om. ow
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Flkerod volume received for DIssoN*d teats Owl ON.
11,
Semple Labels match COC: Ova fan. OwA
-Indudn,, daleldrl OADAnal is Mtllml:
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Ix. X76 1IYrc•
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Asc .r nu. naedvq peat^.rv.Hm hsre Beon dwcked. AGr Orre OwA
Ae C takw. needing preeervaken .re rwnd la be In Oyy tlM* ♦ lWA
P.mi+e.nce rah EPA rer rrrwldaeon- ,,�J
ate F: VGA, e..r.re., TPC Dab, *143RO twN.r D/ . ow
SoMpPas dmckad ter dochierinueun: Ov" ❑w 96A
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Heads ace in VOA Vials >Srmn Oyu Ud W ❑RYA
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Trip Blank Preapnl: ay.. []Fie U"
Trip Blank Custody Sees Preeenl OYS. Orr. dwA
Paco Trip Blank Lei f!(if rchased
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Client"Iflang unf flesolution: Field Hate RegWr*d'l Y I N
Person Coniouled: Delemine:
Cmnrnenlaf Roaolulion:
SCURF Revlew: oar.:
8RF Rarlew: [ Dar.: n 4
we YA,nwver ■ discrepancy elfec rq Honh Groyne compll.nc.
SWIA", a ropy or eye form will be sea[ b W4 typdh Crdina DEFT NR
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