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WQ0001863_Regional Office Historical File Pre 2018 (14)
Schutte, Maria From: Schutte, Maria Sent: Thursday, April 05, 2018 10:40 AM To: 'Adam Brigman' Cc: 'david Johnson@mtholly.us'; 'doug.shoutd@mtholly.us'; Gregory, Sonia Subject: RE: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Adam, Thank you for the additional information in this and the March 29th, 2018 email. I have no further questions. Sincerely, Maria Schutte From: Adam Brigman [mailto:abrigman@SYNAGRO.com] Sent: Wednesday, April 04, 2018 5:25 PM To: Schutte, Maria <maria.schutte@ncdenr.gov>; david.johnson@mtholly.us Cc: doug.shoutd@mtholly.us; Gregory, Sonia <Sonia.Gregory@ncdenr.gov>; Pitner, Andrew <andrew.pitner@ncdenr.gov>; Robert Roth <rroth@SYNAGRO.com> Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request � i;$ Y= r7 {G �rtrl rfM1 ✓ ri';, . :;r..,l<<;: .: a i •.i r # c iie 2 5 21'li.. J C� p4. ,tol _ nA _ n , ©�e 11rN EG t n,:: t. f` 1 I {[ t f E] A Par labs just sent me the additional page to the 30-Day Bench Test report, it is attached. If you have any more questions just let me know. From: Schutte, Maria[mailto:maria.schutteCCncdenr.gov] Sent: Tuesday, March 27, 2018 6:52 PM To: david.johnson@mtholly.us Cc: doug.shoutd(a)mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Mr. Johnson, This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A report copy was received in the Mooresville office on March 51h, 2018. Upon review, the following additional information is requested: • Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable Sodium Percentage (ESP) parameter in accordance with permit condition IV.S. of your permit (copied below for your convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was brought to your attention last year (see attached email) and needs to be corrected now and for future reports. • The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing page, showing the "extended aeration" testing. Please email the requested information to me or contact me with any questions. Sincerely, Maria 5. ii annuil repre5eritative oils. anal}his (i.c:, 81an6rd Soil Fertility A-natysis} s lill b'd 66nducted'on. each land application site=_listed-in Alta-Biller-t 13 nil' kylilich a r�.sidgals limit applica,tior c4citt`.will. occur in the ycear T6 is. nill.yrsis shall be in, accordance with ti e-*!G. tidattce on SoiiI S.anlpfjng'' loc4tod sri the-Sait�Pling-litstruetions sr�etion-ef tile. NC Delrarwic-iit of Aaricuktivic Consumer Services' �.vebs.ire (lttt� r'��tw�t+.ttta�,r:�ovfa�ran�Tttia'pii.bs.ht1�1}. The Perniiitee ataintain their ctsul s and =r descriptipq of it-c saniplidg methodologie-k used to defertitntc,sotl fc tility; fora peridd at': lest, tlian frvc� �srs,:aitd: siral3 he tttade. -t�ailohle to file DFvrs on.t.ppi regtt�t., Af a-. ininistitini, the: Standard Sk')R Fertility a-nalysis shall include the following psIralnctc rs: . ,acidity. � E.r•.chattgeable Saidiutt .Vercent> t;e ; ,Pltn�liarus I 13asc Saluratio.n (bycal;c;illminl) Magnesium � Potss;iutat r C ICditil] lv ail tli 5 Siai3ittnx, Cation Exdl1 nge Capacity Percent Humid ,Witer 11t1C- pH Maria Schutte Environmental Specialist Water Quality Regional Operations Section Division of Water Resources North Carolina Department of Environmental Quality 704 663 1699 office 704 235 2184 direct Maria. schutte(a-)ncdenr.gov 610 East Center Avenue Suite 301 Mooresville, NC 28115 -:�>-'Nothing Compares. - Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. 0 Schutte, Maria From: Schutte, Maria Sent: Thursday, April 05, 2018 10:40 AM To: 'Adam Brigman' Cc: 'david Johnson@mtholly.us'; 'doug.shoutd@mtholly.us'; Gregory, Sonia Subject: RE: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Adam, Thank you for the additional information in this and the March 29th, 2018 email. I have no further questions. Sincerely, Maria Schutte From: Adam Brigman [mailto:abrigman@SYNAGRO.com] Sent: Wednesday, April 04, 2018 5:25 PM To: Schutte, Maria <maria.schutte@ncdenr.gov>; david.johnson@mtholly.us Cc: doug.shoutd@mtholly.us; Gregory, Sonia <Sonia.Gregory@ncdenr.gov>; Pitner, Andrew <andrew.pitner@ncdenr.gov>; Robert Roth <rroth@SYNAGRO.com> Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request CAUTION: Par labs just sent me the additional page to the 30-Day Bench Test report, it is attached. If you have any more questions just let me know. From: Schutte, Maria fmailto:maria.schutte@ncdenr.gov] Sent: Tuesday, March 27, 2018 6:52 PM To: david.johnson@mtholly.us Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Mr. Johnson, This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A report copy was received in the Mooresville office on March 51h, 2018. Upon -review, the following additional information is requested: • Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable Sodium Percentage (ESP) parameter in accordance with permit condition IV.S. of your permit (copied below for your convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was brought to your attention last year (see attached email) and needs to be corrected now and for future reports. • The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing page, showing the "extended aeration" testing. Please email the requested information to me or contact me with any questions. Sincerely, Maria 1 5. An annual representative soils analysis (i.e.. Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment S on which a residuals land application evert will occur in the respective calcndar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture 8c Consumer Services' website(littp:ll«,rvw.nc<7gr.,govlagronoml;pubs.htm). 'Ric Pertninee shall maintain these results and a description of the sampling methodologies used to determine soil fertility fora period of no.less than rive years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include [lie following parameters, Acidity Exchangeable Sodium Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH ! - Maria Schutte Environmental Specialist Water Quality Regional Operations Section Division of Water Resources North Carolina Department of Environmental Quality 704 663 1699 office 704 235 2184 direct Maria. schutte(a-ncdenr.gov 610 East Center Avenue Suite 301 Mooresville, NC 28115 -::�:"othing Compares -,-,- Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Schutte, Maria From: Adam Brigman <abrigman@SYNAGRO.com> Sent: Thursday, March 29, 2018 7:29 AM To: Schutte, Maria Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Robert Roth; david.johnson@mtholly.us Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Attachments: ESP Soil samples.pdf CAUTION: I'm still waiting on the lab to get me the missing page of the 30-Day bench, but I wanted to go ahead and send you this document that shows the ESP values for the soil reports done through waypoint. Waypoint does not include ESP on the report since it is considered the same as the Percent Sodium found in the Base Saturation. I will get the missing 30-Day Bench test page to you as soon as the lab gets it to me. From: Schutte, Maria [mailto:maria.schutte@ncdenr.gov] Sent: Tuesday, March 27, 2018 6:52 PM To: david.johnson@mtholly.us Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request Mr. Johnson, This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A report copy was received in the Mooresville office on March 5th, 2018. Upon review, the following additional information is requested: • Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable Sodium Percentage (ESP) parameter in accordance with permit condition IV.5. of your permit (copied below for your convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was brought to your attention last year (see attached email) and needs to be corrected now and for future reports • The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing page, showing the "extended aeration" testing. Please email the requested information to me or contact me with any questions. Sincerely, Maria ,5, An annual representative soils ;analysis (i.e.. Standard Soil Fertility Analysis) shall be conducted on each land application site: listed in Attachment R on which to residuals land application eveltt will oecur in the respective calendar year. This analysts shall be in aceordancc wilh the "Guidance on Soil Sampling" located in the Sampling Instructions seetion of the NC nepnrtnaeni of Agriculture Consumer Services' website(lit tp:tlww%%,.nc:agr.goviagronomi1pubs.hiIn). The Permiuce shall maintain these results and a du%cription of the: sampling nwihodologics used to detennine sail fertility for a period of no leis than five year,, and shall be made (avail-nhic to the Di%�sion upon request, At a mininiurn, the Swndard Sail fertility ,Analysis shrill include elie following pan, meters, Acidity E;elttangeahic sodituni.I'et-centoge Phosphorus Hasc Sniuratiola (by calculation) Magnesium � Potassivait Calcium Manganese Sodiuni Cation Exchange Capacity � Percent l-littntiC Mahe;, � Fine Copper PH �a Maria Schutte Environmental Specialist Water Quality Regional Operations Section Division of Water Resources North Carolina Department of Environmental Quality 704 663 1699 office 704 235 2184 direct Maria. schutteCaD-ncdenr.gov 610 East Center Avenue Suite 301 Mooresville, NC 28115 ----"Nothing Compares.,-,-,_. Ik Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. PA PROMPT•ACCU RATE- RELIABLE LABORATORIES, INC WWW.PARLABS.COM Crucible Tare Wt (g) Sample(g) Dried Wt(g) Burned Wt(g) TS% VS% 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO ■ CITY OF MT HOLLY 1ST EVENT 126327 ■ • 01/17/17 ■ ■ • 02/14/17 As Received Day 0 Day 7 Day 14 Day 21 Day 28 01/17/18 01/17/17 01/24/17 01131 /17 02/07/17 02/14/17 X10 X10 X2 X10 X2 X10 22.7037 22.7037 25.0632 22.7043 25.0655 22.7064 37.0990 37.0990 36.4780 36.4427 39.0083 36.5308 22.9513 22.9513 25.2550 22.9420 25.3039 22.9469 22.7636 25.1111 22.7646 25.1267 22.7683 1.72% 1.72% 1.68% 1.73% 1.71 % 1.74% 75.81 % 75.03% 74.63% 74.33% 74.26% 0.005059436 x 0.001614599 TS 0.2476 VS 0.1877 Volatile Fraction In 0.44074 t P.O. Box 411483 ■ Charlotte, NC 28241-1483 Phone: (704) 588.83330 Fax: (704) 588-S335 0.004889025 x 0.001694461 TS 0.2405 VS 0.1786 Volatile Fraction Out: 0.42687 RAF;Z RROMRT•ACCU RATE- RGLIA9 LE I.AB®RATORIES, II C WWW. PARLASS. COM 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO CITY OF MT HOLLY 1ST EVENT 126327 01/17/17 02/14/17 Start: End: TS g 0.2476 0.2405 TS% 1.72% 1.74% VS (g) 0.1877 0.1786 VS% 75.81 % 74.26% yIN 0.005059 yOUT 0.00488903 FSVR (Mass Balance) 3.37% FSVR (Van Kleeck) 7.92% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box 411483 • Charlotte, NC 28241.1483 Phone: (704) 588.8333 a Fax: (704) 588-8335 1WA�, Page 1 of 1 Report Number: 17-340-0506 Account Number: 46441 Send To: Synagro Central LLC/ Charlotte Adain Brigman 12701 Lancaster Hwy Pineville NC 28134 c 0 Waypognt. ANALYTICAL 'Every acre... Every year. SOIL ANALYSIS REPORT nata Rarnivnri. igiris/?nm7 Data OfAnalvsis' 12/07/2017 Date Of Renort: 12107/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Tony Jones City of Mt Holly Analytical Mothod(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH OM WIV ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Soil Ibs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate pprn Rate ppm Rate ppm Rate ppm Rate pH Index meg1100g meg1100g 46-02 12318 5,5 150 4 VL 48 VL 177 H 853 M 28 VL 6.0 6.82 1.1 7.1 H NC = 3 NC = 25 MIN 46-04 12319 5.8 150 2 VL 40 VL 165 H 787 M 45 L 6.1 6.84 0.9 6.5 H M1N NC = 2 NC = 20 46-05 12320 5.7 150 2 VL 38 VL 172 H 823 M 42 L 6.0 6.82 1.1 6.9 H NC = 2 NC = 19 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble salts Sample ID E K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS Field ID % % % % % m Rate ppm m Rate ppm Pp m Rate Pp m Rate m Rate ppm pp m Rate PP m Rate mslcm Rate 46-02 1.7 20.8 60.1 1.7 15.5 34 H 0.6 VL 46 H 50 H 1.8 H 0.3 VL e NC=71 NC=15.0 NC=288 NC=90.Q 46.04 1.6 21.2 60.5 3.0 13.8 69 VH 0.7 VL 41 H 47 H 1.3 M 0.3 VL 2 NC=144 NC=17:5 NC=256 NC=65.0 J O 46-05 1.4 20.8 59.6 2.6 1 15.9 76 VH 0.6 VL 36 H 58 VH 1.1 M 0.3 VL , NC = 158 NC = 15.0 NC = 226 NC = 55,0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to somple(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (nlili-mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: pprn x 2 = Ibs1A, Soluble Analysis prepared by: waypohN Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by ?of;,, lnc �1 Pauric McGroary r Page 1 of 1 Report Number: 17-073-0791 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 3 Waypoint ANALYTICAL "Every acre...Every year. ",M Date Received: 03/14/2017 Date Of Analvsis: 03/16/2017 Farm ID: NC-MG-37 SOIL ANALYSIS REPORT Date Of Resort: 03/16/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Dale Connell Mt Holly 50-1701 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On ignition Water pH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number % Soil Ibs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 01 03535 5.4 150 29 L 74 L 185 VH 602 M 4 VL 6.2 0.7 5.5 H NC = 24 NC = 36 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Sample ID S K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS Field ID % % % % a/a RR m Rate Rp m Rate RR m Rate m Rate ppm m Rate ppm pp m Rate ppm Rate ms/cm Rate .01 3A 28.0 54.7 0.3 12.7 7 VL 5.9 H 54 VH 93 VH 3.1 VH 0.3 VL NC = 15 NC = 147.5 NC = 338 NC = 155.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), IbsJA This report applies to sample(&) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (mild -mhos per centimeter), meg1100g maximum of thirty days after testing. by ��`c G H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 Report Number: 17-073-0790 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 Date Received: 03/14/2017 Date Of Analvsis: 03/15/2017 Farm ID: NC-LT-46 SOIL ANALYSIS REPORT Date Of Report: 03/15/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Tony Jones Mt Holly 50-1701 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH OM WfV ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E,C Sample ID Field ID Lab Number % Soil IbslA M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg11009 megl.100g 01 03532 6.5 150 91 H 62 L 127 M 1009 M 8 VL 6.1 6.83 1.0 7.3 I MIN H NC=76 NC=32 03 03533 7.1 150 36 M 55 VL 148 H 833 M 13 VL 6.1 6.84 0.9 6.5 VH MIN NC = 30 NC = 28 08 03534 6.1 150 86 H 51 VL 167 H 750 M 10 VL 6.3 , 0.6 - 5.9 H MIN NO = 72 NO = 26 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron. Soluble Salts Sample ID ES K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS Field ID % % % % °lo pp m Rate pp m Rate pp m Rate pp m Rate pp m Rate pp m Rate pp m Rate ms/cm Rate 01 2.2 14.6 69.1 0.5 13.7 4 VL 8.4 VH 20 M 127 VH 6.6 VH 0.5 L O 5 NC=8 NC=210.0 NC=125 NC=330.0 ' 03 2.2 19.0 64.1 0.9 13.8 15 L 4.7 H 41 H 62 VH 3.5 VH 0.4 L 1 NC=256 NC=175.0 t/• f NC=31 NC=117.5 08 2.2 23.6 63.6 0.7 10.2 13 L 9.5 VH 23 H 76 VH 4.9 VH 0.5 L ' NC = 27 NC = 237.5 NO = 144 NO = 245.0 Values on this report represent the plant available nutrients In the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This repod applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), megf100g maximum of thirty days after testing. by H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs1A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts mslcm x 640 = ppm. Pauric McGroary Charlotte Water 2016 Soil ESP Field Na (PPM) Na (meq/100g) CEC (meq/100g) ESP LT-46-02 28 0.122 7.1. 1.7 LT-46-04 45 0.196 6.5 3.0 LT-46-05 42 0.183 6.9 2.7 LT-46-01 8 0.035 7.3 0.5 LT-46-03 13 0.056 6.5 0.9 LT-46-08 10 0.044 5.9. 0.7 MG-37-01 4 0.017 5.5 0.3 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIVIO! #DIV/0! #DIV/0! #DIV/0! Equations: Na (meq/100g)= (Na PPM x 2)/460 ESP=((Na meq/100g)/CEC) x 100 "��-cam? � i r -ter° ���''�` •" � l .> REc�+ti'=�i�c�ElvRrnw hil,hl� � zmg WQROS OFFICE MOORESVILLE REGIO►� RECEIVEDINCCEP1RfD F° 1VIAR. � 201�' W()ROS MOORESV ILLS REGIONAL OFFICE City of Mount Holly, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0001863 2017 ANNUAL REPORT City of Mount Holly, NC Residuals Land Application Program 2017 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis, 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00001863 County Gaston Year 2017 Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NCO021156 & 01-36-020 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summarv: Total number of application fields in the permit: 21 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 252.66 Total number of acres utilized for land application during the year: 157.1 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. . 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under.penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting fals nformation, including the psibility of fines and imprisonment for knowing violations." a 111 Dannv Jackson City Manager A . �-�7-/d Per iitte Name and Title (type or print) Si atu of PU` ttee Date AbAre of P eparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION MOUNT HOLLY, NC MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID MONTHNEAR AMOUNT UNIT DRY TONS UNIT February 2017 353,400.00 G 24.91 D March 2017 297,600.00 G 20.97 D June 2017 638,600.00 G 60.97 D July 2017 682,000.00 G 52.33 D October 2017 675,800.00 G 56.08 D December 2017 700,600.00 G 37.40 D YEARLY TOTAL 3,348,000.00 G 252.66 D DRY METRIC TONS 22.59 19.01 55.29 47.46 50.87 33.90 229.12 2/1 /2018 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001863 Facility Name: MOUNT HOLLY, NC NPDES# : NCO021166 or WQ# (residual only) WWTP Name: MOUNT HOLLY WWTP Residuals Analysis Data a Product Type AEDLIQ AEDLIQ AEDLIQ Date Sampled (grab) or 01/17/17 05/08/17 06/15/17 Date Composited Percent Solids 1.69 2.29 1.84 PARAMETERS (mg/kg dry weight) Arsenic Cadmium Mercury Chromium Copper Lead Molybdenum Nickel Selenium Zinc Total Phosphorus TK17 Ammonia -Nitrogen Nitrate and Nitrite Laboratory Waypoint Analytical Virginia Inc. AEDLIQ AEDLIQ 09/06/17 10/31/17 1.99 1.28 <3 4.5 <3 <3 3.39 <2 <2 <2 <2 <2 1.48 0.481 0.433 0.54 <0.4 289 236 207 175 157 453 418 497 483 402 35.1 26.4 22.2 18.5 16.1 <5 5.02 <5 <5 <5 21.4 15 14 15.2 17.1 <5 5.2 <5 <5 5.23 730 672 773 758 692 13800 12900 13100 11100 10800 68800 7b900 70300 65000 56600 26500 16500 15100 13500 12400 259 114 859 328 2760 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen_ajties�for submittt-qfalse information, including the possibility of fines and imprisonment for knowing violations." Date DENR FORM RSSF (6/2003) Printed: Tuesday - February 13, 201B at 08:53:56 for: 1701 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001863 Laboratory Facility Name: MOUNT HOLLY, NC Waypoint Analytical Virginia Inc. NPDES# : NCO021156 or WQ# (residual only) WWTP Name: MOUNT HOLLY WWTP Residuals Analysis Data Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ Ar! Q Date Sampled (grab) or 01/17/17 05/08/17 06/15/17 09/06/17 10/31/17 Date Composited Percent Solids 1.69 2.29 1.84 1.99 1.28 PARAMETERS (mglkg dry weight) Aluminum 21000 11000 8810 7490 8320 Calcium 9920 9690 12100 10500 10300 Magnesium 2430 2100 2440 2420 2280 pH 7.28 7.49 7.68 7.69 7.62 Potassium 2680 2700 2490 2170 2260 Sodium 7340 6030 6300 6570 6600 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � Date 6 IV NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (712002) Printed: Tuesday- February 13, 2018 at 08:54:19 for: 1701 01 Page: 1 of 2 Report Number: 17-019-0213 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 61783 Sample Id : Mt Hollyl st event Waypoint(D ANALYTICAL Project : Mt Holly NC Cert#257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/17/2017 10:20:00 Date Received: 01/19/2017 00:00 Date Reported: 01/26/2017 Total Solids * 1.69 16900 100.0 JM 01/19/2017 17:00 SM-2540G Moisture ` 98.30 100.0 JM 01/19/2017 17:00 SM-2540G Total Kjeldahl Nitrogen 6.88 68800 10.0 JM 01/20/2017 08:55 SM-4500-NH3C-TKN Total Phosphorus 1.38 13800 100 JTR 01/24/2017 03:44 6010C Total Potassium 0.27 2680 1000 JTR 01/24/2017 03:48 6010C Total Sulfur 1.28 12800 100 JTR 01/24/2017 03:44 6010C Total Calcium 0.99 9920 100 JTR 01/24/2017 03:44 6010C Total Magnesium 0.24 2430 100 JTR 01/24/2017 03:44 6010C Total Sodium 0.73 7340 100 JTR 01/24/2017 03:44 6010C Total Iron 14400 100 JTR 01/24/2017 03:44 6010C Total Aluminum 21000 100 JTR 01/24/2017 03:44 6010C Total Manganese 444 5.00 JTR 01/24/2017 03:44 6010C Total Copper 453 5.00 JTR 01/24/2017 03:44 6010C Total Zinc 730 5.00 JTR 01/24/2017 03:44 6010C Ammonia Nitrogen 2.65 26500 10.0 JM 01/20/2017 08:55 SM-4500-NH3C Organic N 4.23 42300 10.0 01/20/2017 08:55 CALCULATION Nitrate+Nitrite-N 259 2.28 SJB 01/23/201713:11 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 17-019-0213 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 61783 Sample Id : Mt Holly1st event D Waypoin(t.� ANALYTICAL Project : Mt Holly NC Cert#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/17/2017 10:20:00 Date Received: 01/19/2017 00:00 Date Reported: 01/26/2017 Total Cadmium <2.00 2.00 JTR 01/24/2017 03:44 6010C Total Chromium 289 5.00 JTR 01/24/2017 03:44 6010C Total Nickel 21.4 5.00 JTR 01/24/2017 03:44 6010C Total Lead 35.1 5.00 JTR 01/24/2017 03:44 6010C Total Arsenic <3.00 3.00 JTR 01/24/2017 03:44 6010C Total Mercury 1.48 0.400 JM 01/25/2017 15:50 SW-7471B Total Selenium <5.00 5.00 JTR 01/24/2017 03:44 6010C pH (Standard Units) * 7.28 1.00 JM 01/20/2017 08:55 SW-9045D Total Molybdenum <5.00 5.00 JTR 01/24/2017 03:44 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , ftLI to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 1/17/2017 11112017-3/31/2017 2.2200 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (7340 x 1.6900) _ 100 = 124.046 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (9920 x 1,6900) = 100 = 167.648 Mg mg/I = (mg mg/kg x % Solids) : 100 = (2430 x 1.6900) _ 100 = 41.067 Na meq = Na mg/I _ Molec.Wgt.Na = 124.046 + 23 = 5.3933 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 167.648 _ 20 = 8.3824 Mg meq = Mg mg/I = Molec.Wgt.Mg = 41.067 _ 12 = 3.42225 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.3933 _ SgrRoot[0.5(8.3824+3.42225)] = 2.21995 Printed: 2/1/2018 Page 1 - 13:03 Page: 1 of 2 Report Number: 17-129-0208 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 63800 Sample Id : Mt Holly 2nd Event 2017 (2) Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: Mt Holly 50-1701 REPORT OFANALYSIS Date Sampled: 5/8/2017 09:40:00 Date Received: 05/09/2017 00:00 Date Reported: 05/16/2017 Total Solids * 2.29 22900 100.0 R D 05/09/2017 15:30 SM-2540G Moisture * 97.70 100.0 R D 05/09/2017 15:30 SM-2540G Total Kjeldahl Nitrogen 7.09 70900 50.0 R D 05/10/2017 08:45 SM-4500-NH3C-TKN Total Phosphorus 1.29 12900 100 JTR 05/12/2017 23:26 6010C Total Potassium 0.27 2700 1000 JTR 05/12/2017 23:31 6010C Total Sulfur 0.96 9570 100 JTR 05/12/2017 23:26 6010C Total Calcium 0.97 9690 100 JTR 05/12/2017 23:26 6010C Total Magnesium 0.21 2100 100 JTR 05/12/2017 23:26 6010C Total Sodium 0.60 6030 100 JTR 05/12/2017 23:26 6010C Total Iron 9810 100 JTR 05/12/2017 23:26 6010C Total Aluminum 11000 100 JTR 05/12/2017 23:26 6010C Total Manganese 355 5.00 JTR 05/12/2017 23:26 6010C Total Copper 418 5.00 JTR 05/12/2017 23:26 6010C Total Zinc 672 5.00 JTR 05/12/2017 23:26 6010C Ammonia Nitrogen 1.65 16500 50.0 R D 05/10/2017 08:45 SM-4500-NH3C Organic N 5.44 54400 50.0 05/10/2017 08:45 CALCULATION Nitrate+Nitrite-N 114 2.23 SJB 05/10/201714:16 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Gewr Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 17-129-0208 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 63800 Sample Id : Mt Holly 2nd Event 2017 WaypigintAYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Mt Holly 50-1701 REPORT OF ANALYSIS Date Sampled: 5/8/2017 09:40:00 Date Received: 05/09/2017 00:00 Date Reported: 05/16/2017 Total Cadmium <2.00 2.00 JTR 05/12/2017 23:26 6010C Total Chromium 236 5.00 JTR 05/12/2017 23:26 6010C Total Nickel 15.0 5.00 JTR 05/12/2017 23:26 6010C Total Lead 26.4 5.00 JTR 05/12/2017 23:26 6010C Total Arsenic 4.50 3.00 JTR 05/12/2017 23:26 6010C Total Mercury 0.481 0.400 SJB 05/11/2017 12:40 SW-7471B Total Selenium 5.20 5.00 JTR 05/12/2017 23:26 6010C pH (Standard Units) * 7.49 1.00 R D 05/10/2017 08:45 SW-9045D Total Molybdenum 5.02 5.00 JTR 05/12/2017 23:26 6010C Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. pwc-4 P 61ewr Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 5/8/2017 511/2017-613012017 2.1848 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (6030 x 2.2900) _ 100 = 138.087 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (9690 x 2.2900) + 100 = 221.901 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2100 x 2.2900) = 100 = 48.09 Na meq = Na mg/I _ Molec.Wgt.Na = 138.087 _ 23 = 6.00378 Ca meq = Ca mg/I = Molec.Wgt.Ca = 221.901 = 20 = 11.095 Mg meq = Mg mg/I = Molec.Wgt.Mg = 48.09 _ 12 = 4.0075 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.00378 _ SgrRoot[0.5(11.095+4.0075)] = 2.18482 Printed: 2/1 /2018 Page 1 13:03 Page: 1 of 2 Report Number: 17-167-0206 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 64394 Sample Id : Mt Holly 3rd Event • WayPAoint,M NALYTICAL Project : Mt Holly REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 6115/2017 10:15:00 Date Received: 06/16/2017 00:00 Date Reported: 06/23/2017 Total Solids * 1.84 18400 100.0 JM 06/16/2017 15:25 SM-2540G Moisture * 98.15 100.0 JM 06/16/2017 15:25 SM-2540G Total Kjeldahl Nitrogen 7.03 70300 50.0 JM 06/20/2017 08:30 SM-4500-NH3C-TKN Total Phosphorus 1.31 13100 100 MOS 06/22/2017 13:46 6010C Total Potassium 0.25 2490 100 MOS 06/22/2017 13:46 6010C Total Sulfur 1.15 11500 100 MOS 06/22/2017 13:46 6010C Total Calcium 1.21 12100 100 MOS 06/22/2017 13:46 6010C Total Magnesium 0.24 2440 100 MOS 06/22/2017 13:46 6010C Total Sodium 0.63 6300 100 MOS 06/22/2017 13:46 6010C Total Iron 7890 100 MOS 06/22/2017 13:46 6010C Total Aluminum 8810 100 MOS 06/22/2017 13:46 6010C Total Manganese 320 . 5.00 MOS 06/22/2017 13:46 6010C Total Copper 497 5.00 MOS 06/22/2017 13:46 6010C Total Zinc 773 5.00 MOS 06/22/2017 13:46 6010C Ammonia Nitrogen 1.51 15100 50.0 R D 06/20/2017 08:30 SM-4500-NI3C Organic N 5.52 55200 50.0 06/20/2017 08:30 CALCULATION Nitrate+Nitrite-N 859 2.3d SJB 06/21/201713:08 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the wotff, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 17-167-0206 Account Number: 00015 Submitted By: Clay Fisackerly Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 64394 Sample Id : Mt Holly 3rd Event Waypoint(z) ANALYTICAL Project : Mt Holly REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 6/15/2017 10:15:00 Date Received: 06/16/2017 00:00 Date Reported: 06/23/2017 Total Cadmium <2,00 2.00 MOS 06/22/2017 13:46 6010C Total Chromium 207 5.00 MOS 06/22/2017 13:46 6010C Total Nickel 14.0 5.00 MOS 06/22/2017 13:46 6010C Total Lead 22.2 5.00 MOS 06/22/2017 13:46 6010C Total Arsenic <3.00 3.00 MOS 06/22/2017 17:00 6010C Total Mercury 0.433 0.400 SJB 06/21/201715:57 SW-7471B Total Selenium <5.00 5.00 MOS 06/22/2017 13:46 6010C pH (Standard Units) * 7.68 1.00 R D 06/19/2017 09:00 SW-9045D Total Molybdenum <5.00 5.00 MOS 06/22/2017 13:46 6010C Comments: NC CERT#257, SC CERT#9300 7001 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference he made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (sAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 6/15/2017 7/1/2017-9/30/2017 1.8482 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (6300 x 1.8400) = 100 = 115.92 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (12100 x 1,8400) + 100 = 222.64 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2440 x 1.8400) + 100 = 44.896 Na meq = Na mg/I = Molec.Wgt.Na = 115.92 _ 23 = 5.04 Ca meq = Ca mg/I - Molec.Wgt.Ca = 222.64 = 20 = 11.132 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 44.896 + 12 = 3.74133 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.04 = SgrRoot[0.5(11.132+3.74133)] = 1.84817 Printed: 2/1 /2018 Page 1 13:04 Page: 1 of 2 Report Number: 17-250-0210 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 55999 Sample Id : Mt Holly 4th Event '(D Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 / www.waypointanalytical.com Project : Mt Holly 4th Event REPORT OF ANALYSIS Date Sampled: 9/6/2017 09:42:00 Date Received: 09/07/2017 00:00 Date Reported: 09/14/2017 Total Solids * 1.99 19900 100.0 JM 09/07/2017 16:30 SM-2540G Moisture * 98.00 100.0 JM 09/07/2017 16:30 SM-2540G Total Kjeldahl Nitrogen 6.50 65000 50.0 R D 09/08/2017 08:45 SM-4500-NH3C-TKN Total Phosphorus 1.11 11100 100 MOS 09/12/2017 14:51 6010C Total Potassium 0.22 2170 100 MOS 09/12/2017 14:51 6010C Total Sulfur 1.31 13100 100 MOS 09/12/2017 14:51 6010C Total Calcium 1.05 10500 100 MOS 09/12/2017 14:51 6010C Total Magnesium 0.24 2420 100 MOS 09/12/2017 14:51 6010C Total Sodium 0.66 6570 100 MOS 09/12/2017 14:51 6010C Total Iron 8870 100 MOS 09/12/2017 14:51 6010C Total Aluminum 7490 100 MOS 09/12/2017 14:51 6010C Total Manganese 359 5.00 MOS 09/12/2017 14:51 6010C Total Copper 483 5.00 MOS 09/12/2017 14:51 6010C Total Zinc 758 5.00 MOS 09/12/2017 14:51 6010C Ammonia Nitrogen 1.35 13500 50.0 R D 09/08/2017 09:30 SM-4500-NH3C Organic N 5.15 51500 50.0 09/08/2017 08:45 CALCULATION Nitrate+Nitrite-N 328 2.25 SJB 09/13/201712:46 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 17-250-0210 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 55999 Sample Id : Mt Holly 4th Event (2) Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project : Mt Holly 4th Event REPORT OF ANALYSIS Date Sampled: 9/6/2017 09:42:00 Date Received: 09/07/2017 00:00 Date Reported: 09/14/2017 Total Cadmium <2.00 2.00 MOS 09/12/2017 14:51 6010C Total Chromium 175 5.00 MOS 09/12/2017 14:51 6010C Total Nickel 15.2 5.00 MOS 09/12/2017 14:51 6010C Total Lead 18.5 5.00 MOS 09/12/2017 14:51 6010C Total Arsenic <3.00 3.00 MOS 09/12/2017 14:51 6010C Total Mercury 0.540 0.400 SJB 09/11/2017 15:32 SW-7471B Total Selenium <5.00 5.00 SJB 09/14/2017 12:02 6010C pH* 7.69 1.00 R D 09/08/2017 09:30 SW-9045D Total Molybdenum <5.00 5.00 MOS 09/12/2017 14:51 6010C Comments: NC CERT#257, SC CERT#9300 7001 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ? ram« mC Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 9/6/2017 101112017-11130/2017 2.1140 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (6570 x 1.9900) + 100 = 130.743 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (10500 x 1.9900) = 100 = 208.95 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2420 x 1.9900) _ 100 = 48.158 Na meq = Na mg/I + Molec.Wgt.Na = 130.743 _ 23 = 5.68448 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 208.95 = 20 = 10.4475 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 48.158 -= 12 = 4.01317 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.68448 = SgrRoot[0.5(10.4475+4.01317)] = 2.11403 Printed: 2/1 /2018 Page 1 13:04 Page: 1 of 2 Report Number: 17-305-0201 Account Number: 00015 Submitted By: Adam Brigman Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 56945 Sample Id : Mt. Holly 5th Event N + M O Waypoint" ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Mt. Holly 50-1701 REPORT OF ANALYSIS Date Sampled: 10/31/2017 07:45:00 Date Received: 11/01/2017 00:00 Data Reported: 11/08/2017 Total Solids * 1.28 12800 100.0 R D 11/01/2017 14:00 SM-2540G Moisture * 98.71 100.0 R D 11/01/2017 14:00 SM-254OG Total Kjeldahl Nitrogen 5.66 56600 50.0 R D 11/02/2017 08:30 SM-4500-NH3C-TKN Total Phosphorus 1.08 10800 100 MOS 11/07/2017 13:45 6010C Total Potassium 0.23 2260 100 MOS 11/07/2017 13:45 6010C Total Sulfur 1.24 12400 100 MOS 11/07/2017 13:45 6010C Total Calcium 1.03 10300 100 MOS 11/07/2017 13:45 6010C Total Magnesium 0.23 2280 100 MOS 11/07/2017 13:45 6010C Total Sodium 0.66 6600 100 MOS 11/07/2017 13:45 6010C Total Iron 8400 100 MOS 11/07/2017 13:45 6010C Total Aluminum 8320 100 MOS 11/07/2017 13:45 6010C Total Manganese 370 5.00 MOS 11/07/2017 13:45 6010C Total Copper 402 5.00 MOS 11/07/2017 13:45 6010C Total Zinc 692 5.00 MOS 11/07/2017 13:45 6010C Ammonia Nitrogen 1.24 12400 50.0 R D 11/02/2017 08:30 SM-4500-NH3C Organic N 4.42 44200 50.0 11/02/2017 08:30 CALCULATION Nitrate+Nitrite-N 2760 2.02 SJB 11/b6/201712:54 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 0��a rr Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 17-305-0201 Account Number: 00015 Submitted By: Adam Brigman Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 56945 Sample Id : Mt. Holly 5th Event N + M • Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Mt. Holly 50-1701 REPORT OFANALYSIS Date Sampled: 10/31/2017 07:45:00 Date Received: 11/01/2017 00:00 Date Reported: 11/08/2017 Total Cadmium <2.00 2.00 MOS 11/07/2017 13:45 6010C Total Chromium 157 5.00 MOS 11/07/2017 13:45 6010C Total Nickel 17.1 5.00 MOS 11/08/2017 12:21 6010C Total Lead 16.1 5.00 MOS 11/07/2017 16:39 6010C Total Arsenic 3.39 3.00 MOS 11/07/2017 13:45 6010C Total Mercury <0.400 0.400 SJB 11/06/2017 10:56 SW-7471B Total Selenium 5.23 5.00 MOS 11/07/2017 16:39 6010C pH * 7.62 1.00 JM 11/02/2017 08:30 SW-9045D Total Molybdenum <5.00 5.00 MOS 11/07/2017 13:45 6010C Comments: NC CERT#257, SC CERT#9300 7001 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 10/31/2017 1211/2017-1213112017 1.7292 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (6600 x 1.2800) = 100 = 84.48 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10300 x 1.2800) _ 100 = 131.84 Mg mg/I = (mg mg/kg x % Solids) - 100 = (2280 x 1.2800) = 100 = 29.184 Na meq = Na mg/I _ Molec.Wgt.Na = 84.48 _ 23 = 3.67304 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 131.84 _ 20 = 6.592 Mg meq = Mg mg/I + Molec.Wgt.Mg = 29.184 = 12 = 2.432 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.67304 _ SgrRoot[0.5(6.592+2.432)] = 1.72919 Printed: 2/1/2018 Page 1 13:05 FACILITY NAME: MOUNT HOLLY, NC OWNER: GREG SPRINGS SITE #: NC GA 00041 FIELD# : GA 00041 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: MADISON PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 5.23 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation T N Nitrogen and (pptn) Crop Total Per Acre 7/26/17 68,200.00 (G) 20058.824 1.84 1.539 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 15,100.00 p 859.00 p 24969 FESCUE Jul-17 68,200.00 (G) 20,058.824 [7,300.p 1 1 Total Gallons/Ac: 20,058.82 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 77 0.009 0.006 0.637 1.530 0.068 0.001 0.015 0.043 0.015 2.379 40.32 Cumulative lbs/acre 0.009 0.006 0.637 1.530 0.068 0.001 0.015 0.043 0.015 2.379 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 167 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID 6 ' XCL (SIGN LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, InjectionAncorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 FACILITY NAME: MOUNT HOLLY, NC DWNER: GREG SPRINGS SITE #: NC GA 00041 FIELD# : GA 00041 0006 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 14.75 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90 Page: 1 Lane Applied *** Date:4 Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) pro Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre MONTH 7/25/17 124,000.00 (G) 13932.584 1.84 1.069 MHAEDL DRY 0- 1/2" SUR 0.5 0.30 70,300. p 15,100.00 p 859.00 p 24969 I FESCUE 7/26/17 68,200.00 (G) 7662.9211 1.84 0.588 MHAEDL DRY 0- 1/2" SUR 0.5 0.30 70,300. p 15,100.00 p 859.00 p 24969 FESCUE Jul-17 1 192,200.00 (G) 21,595.505 1 Total Gallons/Ac: 21,595.51 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 83 0.010 0,007 0.686 1.647 0.074 0.001 0.017 0.046 0.017 2.562 43.41 Cumulative lbs/acre 0.061 1 0.039 5.386 1 10.728 1 0.653 0.023 0.145 1 0.530 0.103 15.881 ?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 187 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 i 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID X /2 /�//2 ;//xe�_ (SI O AND APPLIER) DAE "leer�� r penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 FACILITY NAME: MOUNT HOLLY, NC OWNER: GREG SPRINGS SITE #: NC GA 00041 FIELD# : GA 00041 0014 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 10.47 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop Total Per Acre 7/26/17 136,400.00 (G) 20058.824 1.84 1.539 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,300.p 15,100.00 p 859.00 p Jul-17 136A .00 (G) 20,058.824 7[��FESCUE Total Gallons/Ac: 2U,058.82 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 77 0.009 0.006 0.637 1.530 0.068 0.001 0.015 0.043 0.015 2.379 40.32 Cumulative lbs/acre 0.045 0.030 4.346 8.568 0.516 0.017 0.115 0.414 0.079 12.751 Permit PAN Limit (Ibs/acre) Ist Crop/21id Crop 190 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID X 2Xl4 (AATUREOF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD JWNER: DAVID ALLEN PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 48.12 iITE #: NC GA 00045 FIELD# : GA 00045 0001 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Total Per Acre 7/20/17 49,600.00 (G) 2917.647 1.84 0.224 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,300. p 15,100.00 p 859.00 p 24969 I FESCUE 7/21/17 86,800.00 (G) 5105,882 1.84 0.392 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,300. p 15,100.00 p 859.00 p 24969 I FESCUE 7/24/17 130,200.00 (G) 7658.824 1.84 0.588 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,300. p 15,100.00 p 859.00 p 24969 I FESCUE 7/25/17 18,600.00 (G) 1094.118 1.84 0.084 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,300.p 15,100.00 p 859.00 p 24969 FESCUE Jul-17 285,200.00 (G) 16,776.471 10/16/17 74,400.00 (G) 4376.471 1.99 0.363 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 65,000. p 13,500.00 p 328.00 p 22528 I FESCUE 10/17/17 124,000.00 (G) 7294.118 1.99 0.605 MHAEDL DRY 0-<1/2" SUR I 0.5 0.30 65,000. p 13,500.00 p 328.00 p 22528 I FESCUE 10/18/17 117,800.00 (G) 6929.412 1.99 0.575 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 65,000. p 13,500.00 p 328.00 p 22528 FESCUE Oct-17 316,200.00 (G) 18,600.001 1 ,AGILITY NAME: MOUNT HOLLY, NC )WNER: DAVID ALLEN !ITE #: NC GA 00045 FIELD# : GA 00045 0001 ZESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 48.12 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page Lime Applied *** Date LWAc allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Total Per Acre Solids PerResidual Dry, Wet, Past 24 Method zation zation TIN Nitrogen and (ppm) Crop Total Gallons/Ac: 35,376.47 TOTALS: As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN Annual lbs/acre 134 0.017 0.011 1.073 2.771 0.114 0.003 0.028 0.083 0.028 4.330 67.99 Cumulative lbs/acre 0.034 0.023 2.694 5.912 0.338 0.009 0.061 0.223 0.057 9.245 'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 194 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 M AEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID 4 X / 5 la ("SI ueOF LAND APPLIER) DATE ,drenalty, of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 32.05 SITE #: NC LT 00046 FIELD# : LT 00046 0001 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches A It Vola- Miner - DATE or % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN 'Total Per Acre MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop 3/1/17 43,400.00 (G) 3677.966 1.69 0.259 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 68,800.p 26,500.00 p 259.00 p 26199 FESCUE 3/3/17 142,600.00 (G) 12084,746 1.69 0.852 MI-IAEDL MOIST 0-<1/2" SUR 0.5 0.30 68,800. p 26,500.00 p 259.00 p 26199 FESCUE Mar-17 186,000.00 (G) 15,762.712 6/3/17 62,000.00 (G) 5254.237 2.29 0.502 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 I FESCUE 6/7/17 31,000.00 (G) 2627.119 2.29 0.251 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 I FESCUE 6/8/17 105,400.00 (G) 8932.203 2.29 0.853 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,900.p 16,500.00 p 114.00 p 24684 FESCUE Jun-17 198,400.00 (G) 16,813.559 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 137 0.021 0.011 1.400 2.349 0.163 0.005 0.027 0.096 0.028 3.780 72.08 Cumulative Ibs/acre 0.062 0.038 4.836 8.634 0.613 0.018 0.097 0.413 0.096 13.279 Peanut PAN Limit (lbs/acre) 1st Crop/2nd Crop 173 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 s 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID x�� (*/REOF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 26.14 SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20 Page Lune Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp-) Crop Total Per Acre 12/4/17 49,600.00 (G) 1097.345 1.28 0.059 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 22220 I FESCUE 12/5/17 74,400.00 (G) 1646.018 1.28 0.088 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 22220 FESCUE 12/6/17 117,800.00 (G) 2606.195 1.28 0.139 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 56,600.p 12,400.00 p 2,760.00 p 22220 Ij I FESCUE 12/7/17 136,400.00 (G) 3017.699 1.28 0.161 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 22220 I FESCUE 12/12/17 43,400.00 (G) 960.177 1.28 0.051 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 22220 I FESCUE 12/13/17 68,200.00 (G) 1508.850 1.28 0.081 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 1-2220 FESCUE Dec-17 489,800.00 (G) 1 10,836.284 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 26 0.004 0.002 0.182 0.465 0.019 <.001 0.006 0.020 0.006 0.801 12.49 Cumulative Ibs/acre 0.362 1 0.074 1 6.016 30.628 2.068 0.065 0.341 1.383 0.162 37.543 'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 149 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 i 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID X 2 � d l (SKIN URE OF LAND APPLIER) DATE "I cert fy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL DWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 26.19 SITE #: NC LT 00046 FIELD# : LT 00046 0003 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Total Per Acre 2/28/17 105,400.00 (G) 10646.465 1.69 0.750 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 68,800. p 26,500.00 p 259.00 p 26199 FESCUE Feb-17 105,400.00 (G) 10,646:465 3/1/17 31,000.00 (G) 3131.313 1.69 0.221 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 68,800. p 26,500.00 p 259.00 p 26199 FESCUE Mar-17 31,000.00 (G) 3,131.313 6/3/17 18,600.00 (G) 1878.788 2.29 0.179 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 I FESCUE 6/7/17 93,000.00 (G) 9393.939 2.29 0,897 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 I FESCUE 6/8/17 62,000.00 (G) 6262.626 2.29 0.598 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 FESCUE Jun-17 173,600.00 (G) 17,535.353 i orai Cialions/Ac: 31,313.13 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 134 0.021 0.011 1.352 2.280 0.157 0.004 0.027 0.092 0.027 3.668 70.00 Cumulative lbs/acre 0.069 0.042 5.316 9.518 0.669 0.021 0.108 0.464 0.107 14.528 ?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 171 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 i 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID X �' G (SI OF LAND APPLIER) DATE "I c ify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 FACILITY NAME: MOUNT HOLLY, NC DWNER: TONY JONES 3ITE #: NC LT 00046 FIELD# : LT 00046 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 11.25 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40 Page Lune Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre 12/11/17 148,800.00 (G) 7670.103 1.28 0.409 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p F 22220 I FESCUE 12/12/17 62,000.00 (G) 3195.8761 1.28 0.171 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 56,600. p 12,400.00 p 2,760.00 p 22220 FESCUE Dec-17 210,800.00 (G) 10,865.979 Total Gallons/Ac: 10,865.98 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 26 0.004 0.002 0.182 0.466 0.019 <.001 0.006 0.020 0.006 0.803 12.53 Cumulative Ibs/acre 0.137 0.073 4.579 40.511 1.667 0.085 0.457 1.551 0.158 37.036 'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 148 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) . 36.6 34.8 1 i 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID X �L (SIGV&<0F LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pptm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 K Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM 'ACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD )WNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 15.99 :ITE #: NC LT 00046 FIELD# : LT 00046 0005 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page Lune Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre 6/8/17 12,400.00 (G) 1569.620 2.29 0.150 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 70,900.p 16,500.00 p 114.00 p 1 24684 (FESCUE 6/9/17 155,000.00 (G) 19620.253 2.29 1.874 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 FESCUE Jun-17 167,400.00 (G) 21,189.873 A ULQl Uallu11b/Hu: 41,16Y.51 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 100 0.018 0.008 0.955 1.692 0.167 0.002 0.020 0.061 0.021 2.720 52.21 Cumulative lbs/acre 0.037 0.019 2.388 4.099 0.281 0.008 0.048 0.191 0.049 6.169 'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 209 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 11339.0 267.9 15.0 375.0 89.0 2500.0 VIHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID x (SIfURF OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or tng/lcg * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 15.15 ;ITE #: NC LT 00046 FIELD# : LT 00046 0008 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): 2ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60 Page Lune Applied *** Date F LbdAc allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - DATE or % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total Per Acre MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop 3/1/17 80,600.00 (G) 12212.121 1.69 0.861 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 68,800. p 26,500.00 p 259.00 p 26199 FESCUE Mar-17 80,600.00 (G) 12,212.121 1 1 6/3/17 93,000.00 (G) 14090.909 2.29 1.346 MHAEDL MOIST 0-<1/2" SUR 0.5 0.30 70,900.p 16,500.00 p 114.00 p 24684 I FESCUE 6/7/17 6,200.00 (G) 939.394 2.29 0.090 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 70,900. p 16,500.00 p 114.00 p 24684 FESCUE Jun-17 99,200.00 (G) 15,030.303 A.1a, Ua IUII /tW. 4I'L4L.46 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 116 0.018 0.009 1.175 1.980 0.136 0.004 0.023 0.080 0.024 3.186 60.78 Cumulative lbs/acre 0.066 0.041 5.169 9.269 0.652 0.020 0.106 0.455 0.104 14.083 'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop 171 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 s 1339.0 267.9 15.0 375.0 89.0 2500.0 VIHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID x 11 (SIOF LAND APPLIER) DATE "I ce fy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg r* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 FACILITY NAME: MOUNT HOLLY, NC OWNER: DEAN S. CONNELL SITE #: NC MG 00037 FIELD# : MG 00037 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 47.32 OPERATOR: DEAN S. CONNELL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.20 ACRES PERMITTED: 20.20 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - DATE or % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate p,e,N Total Per Acre MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop 2/27/17 248,000.00 (G) 12277.228 1.69 0.865 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 68,800. p 26,500.00 p 259.00 p 26199 FESCUE Feb-17 248,000.00 (G) 12,277.228 10/19/17 248,000.00 (G) - 12277.228 1.99 1.019 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 65,000. p 13,500.00 p 328.00 p 22528 I FESCUE 10/20/17 111,600.00 (G) 5524.752 1.99 0.458 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 65,000. p 13,500.00 p 328.00 p 22528 FESCUE Oct-17 359,600.00 (G) 17,801.980 Total Gallons/Ac: 30,079.21 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 112 0.014 0.009 1.017 2.211 0.115 0.004 0.023 0.082 0.023 3.503 56.68 Cumulative lbs/acre 0.105 0.037 4.524 8.672 0.539 0.019 0.106 0.424 0.090 12.592 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 147 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 I i 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID X (SIG TURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018 Summit Environmental Technologies, Inc. N InSUMMIT 3310 Win St. ��5� Narrative €NVIROFIME14-Ir L iEr-Hhl0LDGIES, V11C. Cuyahoga Falls, Ohio 44223 WO#: 17010901 Ana.'giffcEi Lebad8F-Pr;e= TEL: (330) 253-8211 FAX.- (330) 253-4485 Website: htto:11i9ivi9.settekcorr Date: 2/10/2017 CLIENT: Synagro, NC 28134 Project: Mt.Holly 50-1701 WorkOrder Narrative: 17010901: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Teclurologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any continents or problems with the analytical events associated with this report are noted below. Analytical Sequence QC Comments: 40 ug/mL CCV 1067889: Analytical Comments for svoc-MSTR NPW(8270), Sample 40 ug/mL CCV, Batch ID R64812 : The SVOC CCV (Batch R64812) exhibited high recovery for 2,4,5-Trichlorophenol; All reported samples are ND. lcs-25177 1075432: Analytical Comments for tclp-svoc-herb tclp(8151), Sample lcs-25177, Batch ID 25177 : The TCLP Pest LCS (25177/R65243) exhibited low recovery for Analyte: 2,4,5-TP; Possible low bias for Analyte:2,4,5-TP in associated samples; Original Page 2 of 29 Page 2 of 35 Summit Environmental Technologies, In Qualifiers and Acronyms summirt 3310 Win E F71iNIR0Wm1EhaT,aL7EC. IOLDC-IEs, r4c. Cuyahoga Falls, Ohio442.' WO#: 17010901 Anatyt:esi LFbor„&w.1i= TEL: (330) 253-8211 FAX: (330) 253-44� Website: htto://www.settek.co Date: 2/10/2017 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. x The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). s The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 29 Page 3 of 35 ffflsummlat , bn a.lyiAez .�FY30 T�1''11t=T . CLIENT: Synagro, NC 28134 Project: Mt.Holly 50-1701 Lab SampleID Client Sample ID 17010901-001 Mt.Holly 50-1701 Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4485 Website: http://www.settek.corr. Tag No Date Collected 1/17/2017 10:25:00 AM Workorder Sample Summary WO#: 17010901 10-Feb-17 Date Received Matrix 1/19/201710:00:00 AM Sludge Page 4 of 29 Page 4 of 35 Summit Environmental Technologies, Inc. SUMMI;T DATES REPORT 3310 Win St. , Cuyahoga Falls, Ohio 44223 f1nnlyidoal LaLapriitoria.� TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http://www.settelccom 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 Sample ID Client Sample ID Collection Date 1 Matrix Test Name Leachate Date Prep Date Analysis Date 17010901-OOIA Mt.Holly 50-1701 1/17/2017 10:25:00 AM Sludge Flashpoint Determination (1010) 1/24/2017 10:37:31 AM Ignitability of Solids (SW-846: 1030) 2/9/2017 7:00:00 AM pH (SW9045D) 1/23/2017 3:46:00 PM Reactive Cyanide (9014/7.3.3.2) 1/27/2017 3:04:00 PM Reactive Sulfide (9034) 1/27/2017 3:04:00 PM SVOC 8270 TCLP BNA List 1/24/2017 4:02:06 PM 1/26/2017 9:30:00 AM 1/26/2017 5:28:00 PM SVOC SW-846: 8081-TCLP Pesticide! 1/24/2017 4:02:06 PM 1/26/2017 8:30:00 AM 1/26/2017 6:22:00 PM SVOC SW-846: 8151 Herbicides-TCL 1/24/2017 4:02:06 PM 1/27/2017 5:00:25 PM 2/7/2017 4:53:00 PM SVOC SW-846: 8151 Herbicides-TCL 1/24/2017 4:02:06 PM 1/27/2017 5:00:25 PM 2/7/2017 4:53:00 PM TCLP Mercury Analysis (1311/7470) 1/24/2017 4:02:06 PM 1/25/2017 10:00:00 AM 1/25/2017 4:18:00 PM TCLP Metals Analysis (6010) 1/24/2017 4:02:06 PM 1/25/2017 9:52:01 AM 1/26/2017 11:53:56 AM VOC by GUMS (8260)-TCLP 1/27/2017 4:07:00 PM Original Page 5 of 29 Page 5 of 35 Summit Environmental Technologies, Inc. EMSUMMAT 3310 Win St. EtIVIFON&IENT LIEt.HNOLDCIES_.ac-4c_ Cuyahoga Falls, Ohio44223 .4n31yb'c aU-4-baraipda'i TEL: (330) 253-8211 FAX: (330) 253-4485 Website: http://www.settekcorr, Analytical Report (base report) WO#: 17010901 Date Reported: 2/10/2017 CLIENT: Synagro, NC 28134 Tag Number: Matrix: SLUDGE Collection Date: 1/17/2017 10:25:00 AM Lab ID: 17010901-001A Project: Mt.Holly 50-1701 Client Sample ED Mt.Holly 50-1701 Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: ALJ TCLP MERCURY ANALYSIS (1311/7470) TCLP Mercury ND 0.00200 mg/L 1 1/25/2017 4:18:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010C SW3010A Analyst: VVK TCLP METALS ANALYSIS (6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/26/2017 11:53:56 AM TCLP Barium(Ba) ND 5.00 mg/L 1 1/26/2017 11:53:56 AM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/26/2017 11:53:56 AM TCLP Chromium(Cr) ND 0.200 mg/L 1 1/26/2017 11:53:56 AM TCLP Lead(Pb) ND 0.500 mg/L 1 1/26/2017 11:53:56 AM TCLP Selenium(Se) ND 0.500 mg/L 1 1/26/2017 11:53:56 AM TCLP Silver(Ag) ND 0.500 mg/L 1 1/26/2017 11:53:56 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW3510C Analyst: MSM SVOC 8270 TCLP BNA LIST 1,4-Dichlorobenzene ND 0.0800 mg/L 2 1/26/2017 5:28:00 PM 2,4,5-Trichlorophenol ND 0.200 QC+ mg/L 2 1/26/2017 5:28:00 PM 2,4,6-Trichlorophenol ND 0.200 mg/L 2 1/26/2017 5:28:00 PM 2,4-Dinitrotoluene ND 0.100 mg/L 2 1/26/2017 5:28:00 PM Cresols, Total ND 4.00 mg/L 2 1/26/2017 5:28:00 PM Hexachloro-1,3-butadiene ND 0.100 mg/L 2 1/26/2017 5:28:00 PM Hexachlorobenzene ND 0.100 mg/L 2 1/26/2017 5:28:00 PM Hexachloroethane ND 0.0800 . mg/L 2 1/26/2017 5:28:00 PM Nitrobenzene ND 0.0800 mg/L 2 1/26/2017 5:28:00 PM Pentachlorophenol ND 0.200 mg/L 2 1/26/2017 5:28:00 PM Pyridine ND 0.200 mg/L 2 1/26/2017 5:28:00 PM Surr: 2-Fluorophenol 49.3 10 - 109 %Rec 2 1/26/2017 5:28:00 PM Surr: Phenol-d6 49.9 10 - 109 %Rec 2 1/26/2017 5:28:00 PM Surr: Nitrobenzene-d5 65.5 19 - 120 %Rec 2 1/26/2017 5:28:00 PM Surr: 2,4,6-Tribromophenol 51.2 10 - 120 %Rec 2 1/26/2017 5:28:00 PM Surr: 2-Fluorobiphenyl 65.6 22 - 117 %Rec 2 1/26/2017 5:28:00 PM Surr: p-Terphenyl-d14 70.6 34 - 116 %Rec 2 1/26/2017 5:28:00 PM Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response ND Not Detected at the Reporting Limit PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit W Sample container temperature is out of limit as specified at testcode Original Page 6 of 29 Page 6 of 35 Summit Environmental Technologies, Inc. Analytical Report ffISUMM3310 Win St. €t�JV1R(*Ni fo%L7ECIANOLDGltS,INC. Cuyahoga Falls, Ohio44223 (base report) 4na;y?r�ai a �aa-�dy ig TEL: (330) 253-8211 FAX. (330) 253-4485 WO#: 17010901 Website: hay.-Iltviviv.settekcorr Date Reported: 2/10/2017 CLIENT: Synagro, NC 28134 Tag Number: Matrix: SLUDGE Collection Date: 1/17/2017 10:25:00 AM Lab ID: 17010901-OOIA Project: Mt.Holly 50-1701 Client Sample ID Mt.Holly 50-1701 Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SVOC SW-846: 8081-TCLP PESTICIDES SW8081A SW3510C Analyst: JBN Chlordane, total ND 0.0100 mg/L 1 1/26/2017 6:22:00 PM Toxaphene ND 0.0200 mg/L 1 1/26/2017 6:22:00 PM Endrin ND 0.00100 mg/L 1 1126/2017 6:22:00 PM gamma-BHC ND 0.00100 mg/L 1 1/26/2017 6:22:00 PM Heptachlor ND 0.00100 mg/L 1 1/26/2017 6:22:00 PM Heptachlor epoxide ND 0.00100 mg/L 1 1/26/2017 6:22:00 PM Methoxychlor ND 0.00100 mg/L 1 1/26/2017 6:22:00 PM Surr: Tetrachloro-m-xylene 70.6 10 - 119 %Rec 1 1/26/2017 6:22:00 PM TCLP HERBICIDES ANALYSIS (SW846 131118151) SW8151A SW8151A Analyst: JBN SVOC SW-846: 8151 HERBICIDES-TCLP 2,4-D ND 1.00 mg/L 1 2/7/2017 4:53:00 PM 2,4,5-TP ND 0.500 mg/L 1 2/7/2017 4:53:00 PM Surr: DCAA 85.6 20 - 140 %Rec 1 2/7/2017 4:53:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B Analyst: MES VOC BY GC/MS (8260)-TCLP 1,1-Dichloroethene ND 0.100 mg/L 1 1127/2017 4:07:00 PM 1,2-Dichloroethane ND 0.100 mg/L 1 1127/2017 4:07:00 PM MEK ND 2.00 mg/L 1 1/27/2017 4:07:00 PM Benzene ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Carbon tetrachloride ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Chlorobenzene ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Chloroform ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Tetrachloroethene ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Trichloroethene ND 0.100 mg/L 1 1/27/2017 4:07:00 PM Vinyl chloride ND 0.200 mg/L 1 1/27/2017 4:07:00 PM Surr: 4-Bromofluorobenzene 98.2 70 - 130 %Rec 1 1/27/2017 4:07:00 PM Surr: Dibromofluoromethane 100 70 - 130 %Rec 1 1/27/2017 4:07:00 PM Surr: Toluene-d8 100 70 - 130 %Rec 1 1/27/2017 4:07:00 PM RCI REACTIVE CYANIDE (9014/7.3.3.2) Qualifiers: H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode SW9014 Analyst: MS M Manual Integration used to determine area response PL Permit Limit RL Reporting Detection Limit Original Page 7 of 29 Page 7 of 35 MSUMMSummit Environmental Technologies, Inc. Analytical Report IT 3310 Win St. Fl•lirlRONMEFa'P.aL 1'ECHNOLDCIES, J BG_ Cuyahoga Falls, Ohio 44223 (base report) t Ftrli�rl,reHi �?e3drrtC?fi?4 TEL: (330) 253-8211 FAX.- (330) 253-4485 W04: 17010901 Website: htttwIliviviv.settek.corr, Date Reported: 2/10/2017 CLIENT: Synagro, NC 28134 Tag Number: Matrix: SLUDGE Collection Date: 1/17/2017 10:25:00 AM Lab ID: 17010901-001A Project: Mt.Holly 50-1701 Client Sample ID Mt.Holly 50-1701 Analyses Result PQL Qual Units DF Date Analyzed RCI SW9014 Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2) Cyanide, Reactive ND 0.500 mg/Kg 1 1/27/2017 3:04:00 PM IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: RMT Ignitability Non-flammable. 1 2/9/2017 7:00:00 AM RCI SW9045D Analyst: DHC PH (SW9045D) pH 6.85 s.u.@21.00 1 1/23/2017 3:46:00 PM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034) Sulfide, Reactive ND 25.0 mg/Kg 1 1/27/2017 3:04:00 PM Qualitlers: H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits W Sample container temperature is out of limit as specified at testcode M Manual Integration used to determine area response PL Permit Limit RL Reporting Detection Limit Original Page 8 of 29 Page 8 of 35 "'MIT�. Summit Environmental Technologies, Inc.M5 Sul 3310 Win St. QC SUMMARY REPORT rraLlBtorrr!9Bnl�a1� PttlHpJ+iL•cG1[S ]�9i Cuyahoga Falls, Ohio44223 WO#: 17010901 r'dnBlysic a,,1 LohDr„ mrie5 TEL: (330) 253-8211 FAX: (330) 253-4489 Website: http://`wivw.settek,com 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 2SI33 Sample ID: MB-25133 SampType: MBLK TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 1/25/2017 RunNo: 64742 Nent ID: PBW Batch ID: 25133 TestNo: SW6010C SW3010A Analysis Date: ' 1/25/2017 SegNo: 1066749 analyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) ND 0.500 TCLP Barium(Ba) ND 5.00 TCLP Cadmium(Cd) ND 0.100 TCLP Chromium(Cr) ND 0.200 TCLP Lead(Pb) ND 0.500 TCLP Selenium(Se) ND 0.500 TCLP Silver(Ag) ND 0.500 Sample ID: LCS-25133 SampType: LCS TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 1/25/2017 RunNo: 64742 client ID: LCSW Batch ID: 25133 TestNo: SW6010C SW3010A Analysis Date: 1/25/2017 SegNo: 1066750 4nalyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.01 0.500 2.000 0 101 80 120 TCLP Barium(Ba) ND 5.00 2.000 0 98.5 80 120 TCLP Cadmium(Cd) 1.98 0.100 2.000 0 99.0 80 120 TCLP Chromium(Cr) 2.00 0.200 2.000 0 100 80 120 TCLP Lead(Pb) 1.98 0.500 2.000 0 99.0 80 120 TCLP Selenium(Se) 1.97 0.500 2.000 0 98.5 80 120 TCLP Silver(Ag) 0.980 0.500 1.000 0 98.0 80 120 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 9 of 29 Page 9 of 35 Summit Environmental Technologies, Inc. ^r SUMMARY REPORT ffJ Sul mmiar 3310 Win St. l� 1. r7 �J lV� i REPORT 1 LI.NllRrJ,'JngEt-l"S.,L'tf=rHtJ0GDti1L5',]t9G Cuyahoga Falls, Ohio44223 d#nalyircr�l-d: l3s�r e rrr�.�, TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: httb://wivw.settek.co7n 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID• 25139 Sample ID: MB-25139 SampType: MBLK TestCode: HG TCLP(74 Units: PPM Prep Date: 1/25/2017 RunNo: 64750 Client ID: PBW Batch ID: 25139 TestNo: SW7470A SW7470A Analysis Date: 112512017 SegNo: 1066822 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 0.00200 Sample ID: LCS-25139 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/25/2017 RunNo: 64750 Client ID: LCSW Batch ID: 25139 TestNo: SW7470A SW7470A Analysis Date: 1/25/2017 SegNo: 1066823 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] TCLP Mercury 0.00393 0.00200 0.00400 0 98.2 80 120 Sample ID: 17010901-001AMS SampType: MS TestCode: HG TCLP(74 Units: PPM Prep Date: 1/25/2017 RunNo: 64750 Client ID: Mt.Holly 50-1701 Batch ID: 25139 TestNo: SW7470A SW7470A Analysis Date: 1/25/2017 SegNo: 1066836 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ TCLP Mercury 0.00394 0.00200 0.00400 0 98.5 75 125 Sample ID: 17010901-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/25/2017 RunNo: 64750 Client ID: Mt.Holly 50-1701 Batch ID: 25139 TestNo: SW7470A SW7470A Analysis Date: 1/25/2017 SegNo: 1066837 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua] TCLP Mercury 0.00391 0.00200 0.00400 0 97.8 75 125 0.00394 0.764 20 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 10 of 29 Page 10 of 35 iS U ir Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT ENVIRCIPM01 Ef1TAL TFaIHNOLoc'nis, .*ic Cuyahoga Falls, Ohio 44223 WO#: 17010901 �1,n�drtt�co,' Lrbaf-arari TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto://wii,iv.sett6k.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25139 Sample ID: 17010901-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/25/2017 RunNo: 64750 Client ID: Mt.Holly 50-1701 Batch ID: 25139 TestNo: SW7470A SW7470A Analysis Date: 1/26/2017 SegNo: 1066837 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 11 of 29 Page 11 of 35 3310 Win St. Summit Environmental Technologies, Inc.EJ C SUMMARSumm''l-Wr REPORT QC SUMMARY Csf;iPl'I tiL`fP��HCIflLW�IES,tt9, Cuyahoga Falls, Ohio44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: htW.-1Av14,w.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25164 Sample ID: MB-25164 SampType: MBLK TestCode: svoc-BNA T Units: mg/L Prep Date: 1/26/2017 RunNo: 64812 client ID: PBW Batch ID: 25164 TestNo: SW8270C SW3510C Analysis Date: 1/26/2017 SegNo: 1067890 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene ND 0.0200 2,4,5-Trichlorophenol ND 0.0500 2,4,6-Trichlorophenol ND 0.0500 2,4-Dinitrotoluene ND 0.0100 Cresols, Total ND 1.00 Hexachloro-1,3-butadiene ND 0.00400 Hexachlorobenzene ND 0.0100 Hexachloroethane ND 0.0200 Nitrobenzene ND 0.0200 Pentachlorophenol ND 0.0500 Pyridine ND 0.0500 Surr: 2-Fluorophenol 0.240 Surr: Phenol-d6 0.241 Surr: Nitrobenzene-d5 0.309 Surr: 2,4,6-Tribromophenol 0.263 Surr: 2-Fluorobiphenyl 0.314 Surr: p-Terphenyl-d14 0.360 0.5000 47.9 10 109 0.5000 48.1 10 109 0.5000 61.7 19 120 0.5000 52.6 10 120 0.5000 62.8 22 117 0.5000 72.0 34 116 QC+ 'ample ID: LCS-25164 SampType: LCS TestCode: svoc-BNA_T Units: mg/L Prep Date: 1/26/2017 RunNo: 64812 Nent ID: LCSW Batch ID: 25164 TestNo: SW8270C SW3510C Analysis Date: 1/26[2017 SegNo: 1067891 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 29 Page 12 of 35 Summit Environmental Technologies, Inc. QC SUMMARY REPORT ffJ Summ-ur 3310 Win St. �N� IRC:Pip.9El'I'��L'PEdH1�CG�GIES,.a6*9 Cuyahoga Falls, Ohio44223 �7.a�ly:aa�Ad�:a€ntor,3e9ri�5 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: httD://www.settek.com 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25164 Sample ID: LCS-25164 SampType: LCS TestCode: svoc-BNA T Units: mg/L Prep Date: 1/26/2017 RunNo: 64812 client ID: LCSW Batch ID: 25164 TestNo: SW8270C SW3510C Analysis Date: 1/26/2017 SegNo: 1067891 �nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene 0.135 0.0200 0.2000 0 67.3 19.1 126 2,4,5-Trichlorophenol 0.154 0.0500 0.2000 0 77.2 11.7 151 2,4,6-Trichlorophenol 0.148 0.0500 0.2000 0 73.8 12.4 150 2,4-Dinitrotoluene 0.133 0.0100 0.2000 0 66.3 20.6 140 Cresols, Total ND 1.00 0.4000 0 63.2 10 129 Hexachloro-1,3-butadiene 0.135 0.00400 0.2000 0 67.7 14.7 137 Hexachlorobenzene 0.120 0.0100 0.2000 0 60.2 12 139 Hexachloroethane 0.124 0.0200 0.2000 0 61.8 14.8 132 Nitrobenzene 0.128 0.0200 0.2000 0 63.8 15.6 138 Pentachlorophenol 0.136 0.0500 0.2000 0 67.8 10 156 Pyridine ND 0.0500 0.2000 0 13.1 10 126 Surr: 2-Fluorophenol 0.308 0.5000 61.5 10 147 Surr: Phenol-d6 0.314 0.5000 62.8 1 D 140 Surr: Nitrobenzene-d5 0.401 0.5000 80.2 10 169 Surr: 2,4,6-Tribromophenol 0.335 0.5000 67.0 10 185 Surr: 2-Fluorobiphenyl 0.369 0.5000 73.9 10 169 Surr: p-Terphenyl-d14 0.424 0.5000 84.7 10 179 QC+ m Sample ID: 17010934-006AMS SampType: MS TestCode: svoc-BNA T Units: mg/L Prep Date: 1/26/2017 RunNo: 64812 Client ID: BatchQC Batch ID: 25164 TestNo: SW8270C SW3510C Analysis Date: 1/26/2017 SegNo: 1067892 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Perm it Limit' E Value above'quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 13 of 29 Page 13 of 35 Summit Environmental Technologies, Inc.ffl, S rr 3310 Win St. SUM 1 K r, Y M V� �� SUMMARY T�-���m O C-,td'11,,90N11!Qr=Y1TAL TEU H NO LOGIE% lm.t Cuyahoga Falls, Ohio44223 nn,flrido,,W-LabDrarorres-- TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: hQ.-II-v!vw.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25164 Sample ID: 17010934-006AMSD SampType: MSD TestCode: svoc-BNA T Units: mg/L Prep Date: 1/26/2017 RunNo: 64812 Client ID: BatchQC Batch ID: 25164 TestNo: SW8270C SW3510C Analysis Date: 1/26/2017 SegNo: 1067893 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua] 1,4-Dichlorobenzene 0.289 0.0800 0.4000 0 72.2 29 112 0.2680 7.47 30 2,4,5-Trichlorophenol 0.463 0.200 0.4000 0 116 53 123 0.4216 9.40 30 QC+ 2,4,6-Trichlorophenol 0.458 0.200 0.4000 0 115 50 125 0.4180 9.22 30 2,4-Dinitrotoluene 0.277 0.0400 0.4000 0 69.3 57 128 0.2572 7.49 30 Cresols, Total ND 4.00 0.8000 0 75.6 20 125 0 0 30 R Hexachloro-1,3-butadiene 0.396 0.0160 0.4000 0 99.0 22 124 0.3564 10.5 30 Hexachlorobenzene 0.294 0.0400 0.4000 0 73.5 53 125 0.2752 6.61 30 Hexachloroethane 0.262 0.0800 0.4000 0 65.4 21 115 0.2432 7.29 30 Nitrobenzene 0.371 0.0800 0.4000 0 92.8 45 121 0.2620 34.5 30 R a, Pentachlorophenol 0.364 0.200 0.4000 0 91.0 35 138 0.3572 1.89 30 Pyridine ND 0.200 0.4000 0 35.4 10 126 0 0 30 Rm Surr: 2-Fluorophenol 0.659 1.000 65.9 10 147 0 m Surr: Phenol-d6 0.656 1.000 65.6 10 140 0 m Surr: Nitrobenzene-d5 0.870 1.000 87.0 10 169 0 Surr: 2,4,6-Tribromophenol 0.664 1.000 66.4 10 185 0 Surr: 2-Fluorobiphenyl 0.874 1.000 87.4 10 169 0 Surr: p-Terphenyl-d14 0.886 1.000 88.6 10 179 0 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 15 of 29 Page 15 of 35 l' t Summit Environmental Technologies, Inc.Sum 3310 Win St. QC SUMMARY REPORT Csfl:'b�i h5D,7lPhi,^,L'I'Er;HhJ�L��lea,m9�, 71w�dyEia.a�i FJA Lr3f677ies. Cuyahoga Falls, Ohio44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: httn:/Avmw.sette%co1n 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25166 Sample ID: mb-25166 SampType: mblk TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 1/26/2017 RunNo: 64828 client ID: PBW Batch ID: 25166 TestNo: SW8081A SW3510C Analysis Date: 112612017 SegNo: 1068224 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Chlordane, total ND 0.00500 Toxaphene ND 0.0100 Endrin ND 0.000500 gamma-BHC ND 0.000500 Heptachlor ND 0.000500 Heptachlor epoxide ND 0.000500 Methoxychlor ND 6.000500 d Surr: TCMX 5.63 10.00 56.3 10 119 Surr: DCB 6.87 10.00 68.7 10 119 Sample ID: Ics-25166 SampType: Ics TestCode: telp-svoc-cpe Units: mg/L Prep Date: 1/26/2017 RunNo: 64828 :Iient ID: LCSW Batch ID: 25166 TestNo: SW8081A SW3510C Analysis Date: 1/26/2017 SegNo: 1068225 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] cnunn U.U0494 0.000500 0.00500 0 98.8 20 157 gamma-BHC 0.00450 0.000500 0.00500 0 90.0 22 137 Heptachlor 0.00478 0.000500 0.00500 0 95.7 24 121 Heptachlor epoxide 0.00448 0.000500 0.00500 0 89.5 27 152 Methoxychlor 0.00581 0.000500 0.00500 0 116 10 199 Surr: TCMX 6.69 10.00 66.9 10 119 Surr: DCB 7.95 10.00 79.5 10 119 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 16 of 29 Page 16 of 35 Summit Environmental Technologies, Inc.M5 S U tom 1, or 3310 Win St. QC SUMMARY REPORT GrdJINCrCBP)1�r1 Y� `Pt'_:HPJ LuGIES, WP , Cuyahoga Falls, Ohio 44223 .�ln,nJipaJ4a,� Lsu�,r�fori�$ WO#: 17010901 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: ht(D://wia)w.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25166 Sample ID: 17010934-006ams SampType: ms TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 112612017 RunNo: 64828 Client ID: BatchQC Batch ID: 25166 TestNo: SW8081A SW3510C Analysis Date: 112612017 SegNo: 1068226 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDL]mit Qua[ Endrin 0.00578 0.00100 0.0100 0 57.8 20 157 QMR gamma-BHC 0.00494 0.00100 0.0100 0 49.4 22 137 QMR Heptachlor 0.00551 0.00100 0.0100 0 55.1 24 121 QMR Heptachlor epoxide 0.00555 0.00100 0.0100 0 55.5 27 152 QMR Methoxychlor 0.00628 0.00100 0.0100 0 62.8 10 199 mQMR Surr: TCMX 8.17 20.00 40.9 10 119 Surr: DCB 10.5 20.00 52.7 10 119 Sample ID: 17010934-006amsd SampType: msd TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 1/26/2017 RunNo: 64828 Client ID: BatchQC Batch ID: 25166 TestNo: SW8081A SW3510C Analysis Date: 1/26/2017 SegNo: 1068227 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Endrin 0.00978 0.00100 0.0100 0 97.8 20 157 0.00578 51.4 gamma-BHC 0.00852 0.00100 0.0100 0 85.2 22 137 0.00494 53.3 Heptachlor 0.00901 0.00100 0.0100 0 90.1 24 121 0.00551 48.3 Heptachlor epoxide 0.00954 0.00100 0,0100 0 95.4 27 152 0.00555 52.9 Methoxychlor 0.0113 0.00100 0.0100 0 113 10 199 0.00628 57.0 Surr: TCMX 13.9 20.00 69.4 10 119 0 Surr: DCB 18.1 20.00 90.6 10 119 0 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits 30 R 30 R 30 Rm 30 R 30 Rm Original Page 17 of 29 Page 17 of 35 Summit Environmental Technologies, Inc. Sumfo, ' v 3310 Win St. V1r1 �� SUMMARY REPORT RNVIHrM11.ltN CH I:S,_Jut Cuyahoga Falls, Ohio44223 An.ad;TEL: (330) 253-8211 FA- (330) 253-4489Ia�WO#: 17010901 Website: http://wmnv.settek.com 10-Feh-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: 25212 mple ID: mb-25212 SampType: mblk TestCode: tclp�svoc-her Units: mg/L Prep Date: 1/27/2017 RunNo: 65243 ent ID: PBW Batch ID: 25212 TestNo: SW8151A SW8151A Analysis Date: 2/7/2017 SegNo: 1075436 alyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D ND 1.00 0 0 2,4,5-TP ND 0.500 0 0 Surr: DCAA 423 500.0 84.6 20 140 Sample ID: Ics-25212 SampType: Ics TestCode: telp-svoc-her Units: mg/L Prep Date: 1/27/2017 RunNo: 65243 Client ID: LCSW Batch ID: 25212 TestNo: SW8151A SW8151A Analysis Date: 2/7/2017 SegNo: 1075437 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D ND 1.00 0.500 0 99.3 62.6 125 2,4,5-TP ND 0.500 0.500 0 67.3 52.5 128 Surr: DCAA 405 500.0 81.1 20 140 mple ID: 17010714-001ams SampType: ms TestCode: telp-svoc-her Units: mg1L Prep Date: 1/27/2017 RunNo: 65243 ent ID: BatchQC Batch ID: 25212 TestNo: SW8151A SW8151A Analysis Date: 2/7/2017 SegNo: 1075438 alyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D ND 1.00 0.500 0 128 37 105 SQMR 2,4,5-TP ND 0.500 0.500 0 85.4 38 106 Surr: DCAA 639 500.0 128 20 140 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 18 of 35 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 18 of 29 ffJ S umfarr Summit Environmental Technologies, 172c. 3310 Win St. QC SUMMARY REPORT rdPd'1�,IRrrP,bfl,gENT.^,L'I'EOHt,JCLO,GIES,.INC f1r10IJ#V00J 0:,9fvear3,r WO& Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 17010901 Website: _http://wivw.settekeom 10-Feb-17 Client: Synagro, NC 28134 Project: MtRolly 50-1701 BatchID: 25212 Sample ID: 17010714-001amsd SampType: msd TestCode: telp-svoc-her Units: mg/L Prep Date: 112712017 RunNo: 65243 client ID: BatchQC Batch ID: 25212 TestNo: SW8151A SW8151A Analysis Date: 2/7/2017 SegNo: 1075439 %nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDUrnit Qua] 2,4-D 1.27 1.00 0.500 0 255 37 105 0.638 66.5 30 RS 2,4,5-TP ND 0.500 0.500 0 89.8 38 106 0 0 30 Surr: DCAA 744 500.0 149 20 140 0 S Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded J- Analyte detected below quantitation limits MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit P Second column confirmation exceeds PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 19 of 29 Page 19 of 35 i SunsnaitEnvironmental Technologies, Inc.M9 QC SUMMARY REPORTSlor 3310 Win St. Gft4ir�J•cSIr�BPa1 ,1 'PE�HtdmL•�GIE�,7��C Cuyahoga Falls, Ohio44223 =�l��dlr�ead•I:t�f�.ur3r•�rrP�.K TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http:Uwiviv.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64598 Sample ID: LCS-R64598 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@21.5C Prep Date: RunNo: 64598 client ID: LCSW Batch ID: R64598 TestNo: SW9045D Analysis Date: 1/23/2017 SegNo: 1064310 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual PH 6.99 7.000 0 99.9 98.6 101.4 Qualifiers: * Value exceeds Maximum Contaminant Level. H IIolding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 20 of 29 Page 20 of 35 SUM. SunsmitEnvironmental Technologies, Inc. QC CTTMM�� T T,-,T®�r�, �. 3310 Win St. C SUMMARY Y REPORT 1 2114111P, o-U9 kMf-1'r,6.L TFCHWLO`IES, 7P9G Cuyahoga Falls, Ohio 44223 :1,nody r�rA,!:sJ�vr3r?ri TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http://www.settekcoin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64634 Sample ID: LCS-R64634 SampType: LCS TestCode: FlashPt S(10 Units: °F Prep Date: RunNo: 64634 client ID: LCSS Batch ID: R64634 TestNo: SW1010 Analysis Date: 1/24/2017 SegNo: 1065062 Nnalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua] Flashpoint (140°F) 84.0 77.00 0 109 100 110 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 21 of 29 Page 21 of 35 Sul mm'Jor 3310 Win St. SunimitEnvironnientaZTechnologies, Inc.ffl, QC SUMMARY REPORT Cw.'laCrrhft`i�hlorL'I'6t;`F1PJ�t�cfi�,,,etJ .L�otlesfeaJ l:+�LrFeTr.+s Cuyahoga Falls, Ohio44223 TEL: (330) 253-8211 FAX- (330) 253-4489 WO#: 17010901 Website: http:lAvij,iv.settek.coni 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchlD: R64863 mple ID: 17010805-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 64863 ent ID: BatchQC Batch ID: R64863 TestNo: SW9014 Analysis Date: 112712017 SegNo: 1068975 alyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ snide, Reactive 0.990 0.500 1.000 0.1070 88.3 81.6 122 mple ID: 17010805-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 64863 ent ID: BatchQC Batch ID: R64863 TestNo: SW9014 Analysis Date: 1/2712017 SegNo: 1068976 alyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Cyanide, Reactive 0.981 0.500 1.000 0.1070 87.4 81.6 122 0.9900 0.913 5 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 22 of 35 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 22 of 29 siulmmAr Suminit Environrnental Technologies, Inc. 3310 Win St. Q1SUMMARY U lilY REPORT TP®`T �Aa�,�I�OCSP,9PP5'A,L'I'Er;`HPd�[ J.�IL5',.7j9 Cuyahoga Falls, Ohio 44223 +=!n.uSyvirml! Lalaerzjtaries TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: httn:/Mvivw.sette%com 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64863 Sample ID: MB-R64863 SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 64863 ;lient ID: PBW Batch ID: R64863 TestNo: SW9014 Analysis Date: 1/27/2017 SegNo: 1068972 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] �yarnde, Reactive ND 0.500 Sample ID: LCS-R64863 SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 64863 client ID: LCSW Batch ID: R64863 TestNo: SW9014 Analysis Date: 1/27/2017 SegNo: 1068973 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] :yanide, Reactive 1.02 0.500 1.000 0 102 85 115 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 23 of 29 Page 23 of 35 i umm Summit Environmental Technologies, Inc.S 3310 Win St. QC SUMMARY "PORT rtNVIR1'1AM1IEI'IULTECHNda]GIB0$,1M Cuyahoga Falls, Ohio44223 Anafyifo-� �LgbDrarcrries TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http://Wi4�w.settek.cmii 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID' R64864 Sample ID: 17010805-001AMS SampType: MS TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 64864 Client ID: BatchQC Batch ID: R64864 TestNo: SW9034 Analysis Date: 112712017 SegNo: 1068989 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Sulfide, Reactive 2700 25.0 2800 0 96.4 80 120 mple ID: 17010805-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 64864 ent ID: BatchQC Batch ID: R64864 TestNo: SW9034 Analysis Date: 1/27/2017 SegNo: 1068990 alyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Ifide, Reactive 2840 25.0 2800 0 101 80 120 2700 5.05 30 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte, detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 24 of 35 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 24 of 29 Summit Environmental Technologies, Inc. QC SUMMARY REPORT sumow"i-Ir 3310 Win St. �f�'dlR rP�I,uSh1Y�,�'I'OCHtdd LOGICS, I* Cuyahoga Falls, Ohio 44223 WO#: 17010901 nahe.rsca/ I_aborata ie4 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http://ivivw.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64864 Sample ID: MB-R64864 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 64864 Client ID: PBW Batch ID: R64864 TestNo: SW9034 Analysis Date: 1/27/2017 SegNo: 1068987 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Sulfide, Reactive ND 25.0 Sample ID: LCS-R64864 SampType: LCS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 64864 Client ID: LCSW Batch ID: R64864 TestNo: SW9034 Analysis Date: 1/2712017 SegNo: 1068988 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 2740 25.0 2800 0 97.9 85 115 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit Page 25 of 35 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit Original R RPD outside accepted recovery limits Page 25 of 29 R5 NtSummi SunamitEnvironmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT UNIRCIN) ; EPITAL TECHN,0LD,t31re, mic .1.,aa,llagi�a,� LAdawraro�rir:5 Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http:/hvww.settek.coin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchlD: R64876 Sample ID: 17011296-001ams SampType: MS TestCode: telp-voc-mstr Units: mg/L Prep Date: RunNo: 65045 Iient ID: BatchQC Batch ID: R64876 TestNo: SW8260B Analysis Date: 1/31/2017 SegNo: 1071977 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.208 0.0200 0.200 0 104 39.9 160 1,2-Dichloroethane 0.208 0.0200 0.200 0 104 42.5 157 MEK 1.18 0.100 1.00 0.0206 116 16.6 227 Benzene 0.226 0.0200 0.200 0 113 38.1 155 Carbon tetrachloride 0.215 0.0200 0.200 0 108 40.8 162 Chlorobenzene 0.216 0.0200 0.200 0 108 35.7 168 Chloroform -0.217 D.0200 0.200 0 109 18.3 199 Tetrachloroethene 0.236 0.0200 0.200 0 118 10 261 Trichloroethene 0.199 0.0200 0.200 0 99.4 23.8 175 Vinyl chloride 0.158 0.0200 0.200 0 79.2 10 165 Surr:4-Bromofluorobenzene 1030 1000 103 84.6 130 Surr: Dibromofluoromethane 945 1000 94.5 71.4 127 Surr: Toluene-d8 967 1000 96.7 74.6 127 Sample ID: 17011296-001amsd SampType: MSD TestCode: tclp-voc-mstr Units: mg/L Prep Date: RunNo: 65045 ;lient ID: BatchQC Batch ID: R64876 TestNo: SW8260B Analysis Date: 1/31/2017 SegNo: 1071978 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1-Dichloroethene 0.198 0.0200 1,2-Dichloroethane 0.207 0.0200 MEK 1.21 0.100 Benzene 0.220 0.0200 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds 0.200 0 99.2 39.9 0.200 0 103 42.5 1.00 0.0206 119 16.6 0.200 0 110 38.1 B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit 160 0.208 4.53 157 0.208 0.483 227 1.18 3.20 155 0.226 2.60 E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits 25 25 25 25 Original Page 26 of 29 Page 26 of 35 In'SUPAIWI-T Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT ENVIRG-MVIEVIT LTErHPJOC. -DIES, Dfq, e2,nalyyir-q1 L'c.giv�a s raigr Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 Website: http:/hvww.settelf.com 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchlD: R64876 Sample ID: 17011296-001amsd SampType: MSD TestCode: tclp-voc-mstr Units: mg/L Prep Date: RunNo: 65045 client ID: BatchQC Batch ID: R64876 TestNo: SW8260B Analysis Date: 1/31/2017 SegNo: 1071978 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ Carbon tetrachloride 0.210 0.0200 0.200 0 105 40.8 162 0.215 2.26 25 Chlorobenzene 0.212 0.0200 0.200 0 106 35.7 168 0.216 1.97 25 Chloroform 0.217 0.0200 0.200 0 108 18.3 199 0.217 0.369 25 Tetrachloroethene 0.231 0.0200 0.200 0 116 ID 261 0.236 2.23 25 Trichloroethene 0.194 0.0200 0.200 0 96.8 23.8 175 0.199 2.65 25 Vinyl chloride 0.159 0.0200 0.200 0 79.4 10 165 0.158 0.252 25 Surr:4-Bromofluorobenzene 1030 1000 103 84.6 130 0 25 Surr: Dibromofluoromethane 937 1000 93.7 71.4 127 0 25 Surr: Toluene-d8 966 1000 96.6 74.6 127 0 25 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 27 of 29 Page 27 of 35 Summit Environmental Technologies, Inc.M5 QC SUMMARY REPORT svmm�lrr 3310 Win St. BhttlR�:rt�ItlCt9�s�`I'k�'HPJOSLz�le5fnjk; Cuyahoga Falls, Ohio44223 WO#: 17010901 "1nijJldaea<<LaLvoratel.riE.s TEL:(330) 253-8211 FAX.- (330) 253-4489 Tfehsite: http:11wi4m,.settekcom 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64876 Sample ID: les 10ppb L0123/ SampType: LCS TestCode: telp-voc-mstr Units: mg/L Prep Date: RunNo: 64876 Client ID: LCSW Batch ID: R64876 TestNo: SWB260B Analysis Date: 112712017 SegNo: 1069233 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1-Dichloroethene 0.0110 0.00500 0.0100 0 110 79.4 131 1,2-Dichloroethane 0.0107 0.00500 0.0100 0 107 73.6 137 MEK 0.0580 0.0250 0.0500 0 116 55.1 163 Benzene 0.0108 0.00500 0.0100 0 108 73.1 132 Carbon tetrachloride 0.00992 0.00500 0.0100 0 99.2 63.7 139 Chlorobenzene 0.0104 0.00500 0.0100 0 104 72.3 139 Chloroform 0.0108 0.00500 0.0100 0 108 79.3 129 Tetra chloroethene 0.0106 0.00500 0.0100 0 106 56.2 187 Trichloroethene 0.00932 0.00500 0.0100 0 93.2 64.1 138 Vinyl chloride 0.00902 0.00500 0.0100 0 90.2 22.1 147 Surr:4-Bromofluorobenzene 52.7 50.00 105 80.4 126 Surr: Dibromofluoromethane 47.3 50.00 94.5 70.3 125 Surr: Toluene-d8 49.9 50.00 99.9 82 117 Sample ID: mblk SampType: MBLK TestCode: tclp-voc-mstr Units: mg/L Prep Date: RunNo: 64876 -lient ID: PBW Batch ID: R64876 TestNo: SW8260B Analysis Date: 1/27/2017 SegNo: 1069234 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1-Dichloroethene ND 0.100 1,2-Dichloroethane ND 0.100 MEK ND 2.00 Benzene ND 0.100 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 28 of 29 Page 28 of 35 msummlor Sun:mitEnvironmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT CuPd7.'1RirC8P4iLPa� ,L'I'B HPJ4]L�rilE5,.RiJt Cuyahoga Falls, Ohio44223 !areed LsbDrrstario& TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901 . nwa i Website: htta://ivwiv.settelccoin 10-Feb-17 Client: Synagro, NC 28134 Project: Mt.Holly 50-1701 BatchID: R64876 Sample ID: mblk SampType: MBLK TestCode: tclp-voc-mstr Units: mg/L Prep Date: RunNo: 64876 :lient ID: PBW Batch ID: R64876 TestNo: SW8260B Analysis Date: 1/27/2017 SegNo: 1069234 >nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Carbon tetrachloride ND 0.100 Chlorobenzene ND 0.100 Chloroform ND 0.100 Tetrachloroethene ND 0.100 Trichloroethene ND 0.100 Vinyl chloride ND 0.200 Surr: 4-Bromofluorobenzene 47.9 Surr: Dibromofluoromethane 51.2 Surr: Toluene-d8 48.4 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding tines for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds 50.00 95.9 70 50.00 102 70 50.00 96.8 70 B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit 130 130 130 E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Original Page 29 of 29 Page 29 of 35 summit. Environni.cutal `Qechnoliaiggics, Inc. 33 10 Win Strecl Cliyalkaglk Falls, Ohio 44223 v rQ CD W 0 0 h w cn A n lysis Request/Oall n of CustOdY I-br Sumillit I':fIVk6Y191111�631a1 Fechi Oogics, Iskc. use iksal.y jlkjga till.' - oc-' Jzs-'. 1 _ Summit Environmental Technologies, Inc. Cooler Receipt Form Initials cf per<_:nn inspecting tooter and samples: �A Client, -1'1 (r r'J y Older Numbe: _. > > rl � i Q� � ttaio Recel:cd: 1-1 i`t lime Reccived:� � Dail; coote-rgsf opened and samples inspected: Nlurnber of cooler5.'soxes: _ NIA Shipper' ry Ups U}-It ,4irt;ome Us Postal %galtc-in pickup - Other: Packaging: Peanuts B •ri,5 Paper Foam Mc)re tcE--:: Tape on c*oterPoox: N NIA €;ustoiy Seals intact r N r: C-O-C in plas°:c N r'j.' lc�- slue .Ce �_ Pd eft / absent r msneq MIA % S�•t'irls 7en:peraiuro iP, GJ%: n"tu2tl45a Cyr (.i. `% �'l',' 6.0 � °s WA Radiological Testing IT'W.1meni serial 7,'354271 y U 141A (see rage 2 for eaan results} '*Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiclog:cal Safety Officer must be notiiled immediately G-D-C filled out prep rly t:1y N W11"k Samp'es ;n separate U•ats r=y M NIA sample rontai-Ws intact' N P:;A 'If no, listhreken Samp` 12b61{gt ccn5l_•iet (IQ, �dBt�„ e>c.) M NIA l 5 cVsj agr :e With //(f K WA cc-ne7 convriners °,sad {y N i)YA Si,fficent simple receit ed � c N WA Samplc; received .within hotdtno time i M Bobbies absent frorn 4G nil- vials" y N P,lffR " Serrip"es ewitn bear eE <6mm are acceptable. Indicate buLWo snz:' it y6rrm. VVasclientcontacied_bDutsamples y M VJill client send ncr: samples y N Client coniact: Logged in Page 1 of 9 Page 31 of 35 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL. QUALITY RESOURCES WWA LAB4.®I ATO CE'I TI'F'I.0 TI N '®, NCH In accordeninvWth the provisions of M.C.G " ' (1J,• 143-215.3 (a)(f0) and MCAC 214.0800: Summ. it Environmental Technologies., Inc. Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data tO.DEQ for compCance with NPDES effluent, surface water, groundwater, and pretreatment regulations. By reference 15A NCAC 2H-0800 is made apart of this certificate. This certificate does not guarantee valldityofdaia generated, butiridldates the methodology, equipment, qualitycontrol procedures, records, and proficiency ofthe laboratoryhave been 0amined and found to be. acceptable. This cerfificate shall be valid until, 12131/20�_.7 Certificate No. 631 N� Dana'B. Sett-;' 4� "D v cc (D IV O North Carolina Wastewater/Groundwater Laboratory Certification Certified Parameters Listing Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631 Address: 3310 Win Street Effective Date: 1/1/2017 Cuyahoga Falls, DH "223- Expiration Date: 12/31/2017 Date of Last Amendment: 1/5/2016 The above he mod laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby cer5fied for the measurement of the parameters listed below. CERTIFIED PARAMETERS INORGANIC SILICA BOD EPA 200.7, Rev. 4.4, 1994 (Aqueous) SM 5210 B-2001 (Aqueous) SW-846 6010 D (Aqueous) CHLORIDE SULFATE SW-846 9056 A (Aqueous) EPA 300.0, Rev. 2.1, 1993 (Aqueous) COD sW-846 9056 A (Aqueous) SM 5220 C-1997 (Aqueous) SULFIDE FLUORIDE SW-846 9034 (Aqueous) EPA 300.0, Rev. 2.1, 1993 (Aqueous) METAL SW-846 9056 A (Aqueous) TCLP METALS INORGANIC PHENOLS SW-8461311 (Aqueous) EPA420.1, Rev. 1978 (Aqueous) ALUMINUM NITROGEN, NITRATE EPA 200.7, Rev. 4.4,1994(Aqueous) EPA 300.0, Rev. 2.1, 1993 (Aqueous) SW-846 6010 D (Aqueous) SW-846 9055 A (Aqueous) EPA 200.8, Rev. 6.4, 1994 (Aqueous) NITROGEN, NITRITE SW-946 6020 B (Aqueous) EPA 300.0,. Rev. 2.1, 1993 (Aqueous) ANTIMONY SW-846 9056 A (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) NITROGEN, NO3 + NO2 SW-846 6010 D (Aqueous) EPA 300.0, Rev. 2.1, 1993 (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 9056 A (Aqueous) SW-846 6020 B (Aqueous) NITROGEN, TOTAL KJELDAHL ARSENIC SM 4500 Norg B-1997 (SM 4500 NH3 D-1997) (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) OIL & GREASE SW-846 601 D D (Aqueous) EPA 1664 Rev. B (Aqueous) EPA 20D.8, Rev. 5.4, 1994 (Aqueous) SW-846 9071 B (Non -Aqueous) SW-846 6020 B (Aqueous) PHOSPHORUS, TOTAL BARIUM EPA 200.7, Rev. 4.4 (1094) (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6010 D (Aqueous) RESIDUE, DISSOLVED 180 C EPA 200.8, Rev. 5.4, 1994 (Aqueous) SM 2540 C-1997 (Aqueous) SW-846 6020 B (Aqueous) RESIDUE, SUSPENDED BERYLLIUM SM 2540 D-1997 (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) RESIDUE, TOTAL SW-846 6020 B (Aqueous) SM 2540 B-1927 (Aqueous) BORON This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penaltL*s �nna.4t1 rlrtitrv�r °u"arIfFGS SaYJs as set forth In 15A NCAC 21-1.08D7. _U O (D co O —n .P North Carolina Wastewater/Groundwater Laboratory Certification Certified Parameters Listing Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631 Address: 3310 Win Street Effective Date: 1/1/2017 Cuyahoga Falls, OH 44223- Expiration Date: 12/31/2017 Date of Last Amendment: 1/5/2016 The above named laboratory, having duly met the requirements of 15A NCAC 2H.0aoo, is hereby certified for the measurement of the parameters listed below CERTIFIED PARAMETERS EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-84e 6020 B (Aqueous) MAGNESIUM CADMIUM EPA 200.7, Rev. 4.4, 1994 (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 5010 D (Aqueous) SW-846 6IJ10 D (Aqueous) MANGANESE EPA 200.8, Rev. 5.4, 1994 (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 6D20 B (Aqueous) SW-846 5010 D (Aqueous) CALCIUM EPA 200.8, Rev. 5.4, 1994 (Aqueous) EPA 2017, Rev. 4.4, 1994 (Aqueous) SW-846 5020 B (Aqueous) SW-846 6010 D (Aqueous) MERCURY CHROMIUM TOTAL EPA 245.1, Rev. 3.0, 1994 (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 7470 A (Aqueous) SW-846 6010 D (Aqueous) EPA 1631 E (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) MOLYBDENUM SW-846 6020 B (Aqueous) EPA 200.7, Rev. 4.4, 1904 (Aqueous) COBALT SW-846 6010 D (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) EPA 20D.8, Rev. 5.4, 19D4 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6020 B (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) NICKEL SW-846 6020 B (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) COPPER SW-846 6010 D (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) EPA 20D.8, Rev. 6.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-846 6020 B (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) POTASSIUM SW-846 6020 B (Aqueous) EPA 200,7, Rev. 4.4, 1994 (Aqueous) IRON SW-846 6010 D (Aqueous) EPA 200.7, Rev, 4.4, 1904 (Aqueous) SELENIUM SW-846 6010 D (Aqueous) EPA 20D,7, Rev. 4.4, 1994 (Aqueous) LEAD SW-846 6010 D (Aqueous) EPA 200.7, Rev. 4.4. 1994 (Aqueous) EPA 20D.8, Rev. 5.4, 1994 (Aqueous) SW-846 6010 D (Aqueous) SW-848 6020 8 (Aqueous) EPA 200.8, Rev, 5.4, 1994 (Aqueous) SILVER SW-845 6D20 B (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) LITHIUM SW-846 6010 D (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) EPA 200.8, Rev. 6A, 1994 (Aqueous) This certification requires malntance of an acceptable quality assurance as set forth In 15A NCAC 2H,0807. program, use of approved methodology, and aetlsfactory performance on evaluation samples. Laboratories are subject to civil penalties a�6ror=u3d Beal �n fUrJnP.aePr�P9 '0 O W 01 O W 01 North Carolina Wastewater/Groundwater Laboratory Certification Certified Parameters Listing Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631 Address: 3310 Win Street Effective Date: 1/1/2017 Cuyahoga Falls, OH 44223- Expiration Date: 12/31/2017 Date of Last Amendment: 1/5/2016 The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below. r CERTIFIED PARAMETERS SW-846 6020 B (Aqueous) CHLORINATED PHENOLICS SODIUM EPA 1653, Rev. A, 1997 (Aqueous) EPA 200.7, Rev, 4.4, 1994 (Aqueous) EXTRACTABLE PETROLEUM HYDROCARBONS SW-846 8010 D (Aqueous) MADEP, May 2004, Rev. 1.1 (Aqueous) STRONTIUM NONHALOGENATED VOLATILE, ORGANICS EPA 200.7, Rev. 4.4, 1994 (Aqueous) SW-846 801B C (Aqueous) SW-846 8010 D (Aqueous) PESTICIDES, ORGANOCHLORINE EPA 200.8, Rev. 5.4, 1994 (Aqueous) EPA 808 (Aqueous) SW-846 6020 B (Aqueous) SW-846 8081 B (Aqueous) THALLIUM POLYCHLORINATED BIPHENYLS (PCBs) EPA 200.7, Rev. 4.4, 1994 (Aqueous) EPA 608 (Aqueous) SW-846 6010 D (Aqueous) SW-846 8082 A (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) PURGEABLE, ORGANICS SW-846 5020 B (Aqueous) EPA 624 (Aqueous) TIN SW-846 B260 B (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) TOTAL ORGANIC HALIDES SW-846 6D10 D (Aqueous) SW-846 9020 B (Aqueous) VANADIUM TPH DIESEL RANGE, ORGANICS EPA 200.8, Rev. 6.4, 1994 (Aqueous) SW-846 8015 C (Aqueous) SW-846 6020 B (Aqueous) TPH GASOLINE RANGE, ORGANICS ZINC SW-846 8015 C (Aqueous) EPA 200.7, Rev. 4.4, 1994 (Aqueous) VOLATILE PETROLEUM HYDROCARBONS SW-846 6D10 D (Aqueous) MADEP, May 2004, Rev. 1.1 (Aqueous) EPA 200.8, Rev. 5.4, 1994 (Aqueous) SW-846 6020 B (Aqueous) ORGANIC TCLP ORGANICS SW-846 1311 (Aqueous) ADSORBABLE ORGANIC HALIDES EPA 1650, Rev. C, 1997 (Aqueous) BASE NEUTRAUACID, ORGANICS EPA 625 (Aqueous) SW-846 8270 D (Aqueous) a CHLORINATED ACID HERBICIDES SW-846 8151 A (Aqueous) This certification requires maintenes of an acceptable quality assurance program, use of approved methodology, and satisfactoryperformance on evaluation samples. Laboratories are subject to civil penalties w4,br deca,,d,'m qn Par h11==j:k asset forth In 15A NCAC 2H,0807. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 01/01/17 To 03/31/17 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative perlormed Mass A or Mass 13 corn fete the ionowing momtorm aata: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 th Coliform power per gram MPN MPN/g event sludge SM9221E of total solids CFU 57,000 88,376 1,000,000 CFU/g Event sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Mt. 5 Option/Alt. 6 Option/Alt. 7 Option/Mt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying - Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification i c udinE5:4Laqq fine and imprisonment." Doug Shoutd / ORC g5 Pre er me d Title pe or print) Land p r N�d Title (if applicable) (type or print) 11 �UFl S ature fPrep arer* Date Si antDated`Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Case Narrative ' •_=''_:: ,, NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 01/19/2017 M I Environmental Solutions SC Certification No. 99012 BORATORIES, INC. Synagro Clay Fisackerly 12701 Lancaster Hwy. Pineville, NC 28134 Project: 2017 Production Lab Submittal Date: 01/17/2017 Prism Work Order: 7010215 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative dotes: This report contains a total of 4 pages. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Sample Receipt Summary Full -Service Analytical & !� S Environmental Solutions 01/19/2017 YY ORATORIE$ ING Prism Work Order: 7010215 Client Sample iD Lab Sample ID (Matrix Date Sampled Date Received Mt. Holly 50-1701 7010215-01 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-02 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-03 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-04 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-05 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-06 Solid 01/17/17 01/17/17 Mt. Holly 50-1701 7010215-07 Solid 01/17/17 01/17/17 Samples were received at 13.9 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number. 1-8001529-6364 - Fax: 7041525-0409 r: r , M LABORATORIES, INC. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Client Name: Synagro Sample DatelTime Collected: Sample Date/Time Submitted: Full -Service Analytical & Environmental Solutions 449 Springbrook Rd. P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 Fax: 704/525-0409 Project Name: Mt. dolly 50-1701 1/17/17 10:15 Project ID: Mt. Holly 50-1701 1st Event 1/17/17 12:20 COC Group: 7010215 Prism Sample ID Client Sample ID Fecal Coliforifi ifi Sollds(cfulg) SM9222 D Reporting Limit % Solids SM2640 G Analysis DatelTime 7010215-01 Clariant Corp. 61000 A 61000 1.65 1/17/17 12:25 7010215-02 Clariant Corp. 1000.000 57000 1.74 1117/17 12:25 7010215-03 Clariant Corp. 58000 A 58000 1.73 1117/17 12:25 7010215-04 Clariant Corp. 60000 A 60000 1.66 1117117 12:25 7010215-05 Clariant Corp. 57000 A 57000 1.76 1117/17 12:25 7010215-06 Clariant Corp. 60000 A 60000 1.66 1117117 12:25 7010215-07 Clariant Corp. 58000 A 58000 1.73 1117/17 12:25 WiN[�Tl Prism Sample ID: 7010216 Note: All results are reported on a dry -weight basis. Geometric Mean: 88376 cfu/g Reporting Limit: 58696 A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting lin 12 Data Reviewed By: � r, '�/�j?'rr� �(`Project Manager: C. Rusmisell Review Date: 1-19-17 Approval Date: 1-19-17 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. ,) 07 Full -Service Analytical & Environmental Solutions LA130RATORIES, INC. 449 Springbrook Road - Charlot4e, NC 28217 Phone 7041529-6364 n Fax: 704/525-0409 Client Company Name: S_'c��•fi veJ Deport To/Contact Name: Roiling Address: ((ne'yitif, a Phone. til' --LI- ,29t Fax (Yes) h9a Ernail Address: EDD Type: PDF r�EXcel_Other Site Location Name: Site Location Physical Address: TIME MATRIX CLIENT DATE COLLECTED (SOIL, SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR HOURS SLUDGE) PAGE �A, ou: L nuo-rE a To ENSURE PROPER BILLING- ProjectName: Wlt %ADV�m 5 ,—�'U 31 Short Hold Analysis: (Yes) (N®) UST Project: (Yes) (NO) *Please ATTACH any project specific reporting (QC LEVEL 1 I1 11I IV) provisions and/or QC Requirements Invoice To: Address. Purchase Order Mo./Billing Reference C1 ��=I 1'tt TO OBE FILLED IN EV CLIENT/SAMPLENG PERSONNEL Requested Due Date ® 1 Day 0 2 Days ® 3 Days ® 4 Days E3 5 Days Certification: NELAC Doa FL IBC A "Working Days" 0 6-9 Days ® Standard 10 days ® Rush ork dust Be Sc OTHER NIA Samples received after 14:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO `ij (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection. YES �L MO SAMPLE CONTAINER • ANALYSIS REQUEST�D PRISM PRESERVA- *TYPE NO. SIZE TIVES SEE BELOW �1 4 .1- U Sampler's Signature 'UM. + • �. U °P ) � Sampled By (Print Name) L.VW 11 c;-� ' Itt Affiliation s . Upon relinquishing, this Chain of Custody is your A thoriaation for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSTJOeUNTIL RECEIVED AT THE LABORATORY. D Fed Ex ❑ UPS ❑ Hand -delivered O Prism Field Service O Other IOUTER IATER E1NC ®SLANDFILL ® NC ® SC El NC ® SC © NC ® SC ® NC D SC ® NC ® SC2 ®SCNCC I ® N® SCI ® NC ® SC ® -I ® *CCNTa rYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined /OA = Volatile Organics Analysis (Zero Head Space) REMARKS LAD ID NO. Additional Comments: 0,fy� 'Ur1—e ,t Site ]je ° partUrw T11Ylp I' � C)RICINAI_ PA PRO mPT- Ao:u,ame.szAecE LABOP—A-TORIES,INC W� N : R! : s 0,*%l 2722R2 2y awAE23Es Attn: c2 FISACKERLY SYRAc 0 127e1 LANCASTER HWY 2IR IEEE, K2 28134- >. ! T K»2E: JAN l; TE: 02Z22Z17 S 2c2 MATRIX- scSE NUMBER- 2e32 _DA7E S242cz»- 01/17/17 . TIRESAMPLED- 1030 .m2 zs7N p- 01/17/ 7 Kyt32 C1 RECETV - DJ I:Mz RECEIVED- 1242 DETTv22ED BY- 2a PE SAMPLE- Grp Page l o£ 1 ANALYSIS to DAY BENCH SCALE ?Es 2KatYSis K y 2r 1 TI2E BY RESc1T UNITS R 01/17z17 RE ATTACHED LABORATORY DIRECIPOR�� \� & •�. P.O. Box $lga•Cbr.t NC226Q 483 ebw:(m%588 2.Fax: E+12&g RALF:Z PROMPT•ACOU RATE•RE LIABLE LABORAT®R.IES, INC WWW.RARLABS.COM 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO ■ CITY OF MT HOLLY 1ST EVENT • 126327 • ■ • 01/17/17 ■ ■ • 02/14/17 Start: End: TS (9) 0.2476 0.2405 TS% 1.72% 1.74% VS () 0.1877 0.1786 VS% 75.81% 74.26% I N 0.005059 OUT 0.00488903 FSVR Mass Balance) 3.37% FSVR (Van Kleeck) 7.92% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 0 Fax: (704) 588-8335 PAR L4BORATORIES, INC. www.pariabs.com , Shipping: 2217 Graham Park Drive Charlotte, NC 28273 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc, and the North -..11.... n.......i........ -1 C...d...n......,1..t —A KI-i I Dunn . Company Name (billing) SYNAGRO CENTRAL Comments/ Special Instructions 6'Rcl u _to, dgl i"A�u e\xn" ,<` ca v 7" �ICRS �c�k � be C�4��d to , 9620 Address 12701 LANCASTER HWY City, State Et zip code PINEVILLE NC 28134 Point of Contact Et Telephone Number Claq FISQcwL Sample Taken By: SIGNATURE a�L� PRINTED NAME CIG �'i�`� ARE SAMPLES FOR STATE or EPA REPORTING? YES (ENO '`Sample Type: DW ww GWMW HW Soil Other Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C "Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a Residual Chlorine checked at time of sampling (YIN): Oechlorination Necessary (Y/N): Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Datemme Collection DateMme Analyses Requested CIN ac W. HD114 14814ffa 403(DI� �eocj� Scale-u es;h®n ReligQylshed by: uate! 1 ime rcecenrea ate/ i ime Relinquish by: J Daterrime Received by: Daterrime " C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste —See Other Side ANNUAL .PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 04/O1/17 To 06/30/17 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion lI appiicaDie ro atternauve periormea l.lass A or t-iass 15 com lere Lne ionowing monnOrm aaia: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 Coliform power per gram NUN MPN/g event sludge SM9221E of total solids CFU 420,000 439,869 450,000 CFU/g Event sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) Option/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Mt. 6 (Alk Stabilization) Option/Mt. 10 (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) X Option/Alt. 7 (Drying —Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction . X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statem ent attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the informatiori used to determine that the ppathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification*cludin fine and imprisonment." DougShoutd / ORC I �/� y�MAM Prep er N. me Title e o mt) Land rier Naml6and Title (if applicable) (type or print) Si re of reparer* Date Si of Land Applier (if applicable) ate *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) A RR� S M LABORATORIES, INQ Synagro Clay Fisackerly 12701 Lancaster Hwy. Pineville, NC 28134 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 Environmental Solutions SC Certification No. 99012 Project: 2017 Production Lab Submittal Date: 05/08/2017 Prism Work Order. 7050126 0511012017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: This report contains a total of 4 pages. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 AFull-Sti � S Environmenvicetal Analytical s ,ARM Environmental Solutions ✓r L aowom Es, WC. Sample Receipt Summary 05/1012017 Prism Work Order: 7050126 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Mt Holly 2nd Event - 1 7050126-01 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 2 7050126-02 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 3 7050126-03 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 4 7050126-04 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 5 7050126-05 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 6 7050126-06 Solid 05/08/17 05/08/17 Mt Holly 2nd Event - 7 7050126-07 Solid 05/08/17 05/08/17 Samples were received in good condition at 5.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364-Toll Free Number. 1-800/529-6364 -Fax: 7041525-0409 QM BORATORIES, INC. . . . . . . . . . . . . . . . . NC Certification No. 402 SO Certification No. 99012 NO Drinking Water Cart. No. 37735 Client Name: Synagro Sample Date/Time Collected: Sample Date/Time Submitted: Full -Service Analytical & Environmental Solutions 449 Springbrook Rd. P.O. Box 240543 Charlotte, NO 28224-0543 Phone: 7041529-6364 Fax: 704/525-0409 Project Name: City of Mt. Holly 5-8-17 09:20 Project ID: Mt. Holly 2nd Event 5-8-17 10:10 COC Group: 7050126 - Prism Sample ID Client Sample ID Fecal iff oliform in Sollds(cfulg) SM9222 D Reporting Limit % Solids SM2540 G Analysis Date/Time 7050126-01 MtHolly 2nd Even i 420000 A 420000 2.40 5-8-17 12:00 7050126-02 Mt Holly 2nd Event 450000 A 450000 2.24 5-8-17 12:00 7050126-03 Mt Holly 2nd Even 430000 A 430000 2.30 5-8-17 12:00 7050126-04 Mt Holly 2nd Event 440000 A 440000 2.28 5-8-17 12:00 7050126-05 IMt Holly 2nd Event 450000 A 450000 2.23 5-8-17 12:00 7050126-06 IVIL Holly 2nd Event 440000 A 440000 2.26 5-8-17 12-00 7050126-07 Mt. Holly 2nd Even 450000 A 450000 2.23 5-8-17 12:00 Geometric Mean Calculation: Prism Sample ID.- 7050126 Geometric Mean: 439889 A cf u/g Reporting Limit: 439869 Note: All results are reported on a dry -weight basis. A: The result is less than the reportiV0, limit. At the request of the client, the value reported equals the value of the reporting limit. Data Reviewed By: e. Project Manager: C. Rusmisell Review Date: 5-10-17 Approval Date: 5-10-17 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. r;q•,trr�•; ,'C "'•'r' .'I{; @r HARN OF CUSTOW®Y RECORD :•I; I Full -Service Analytical & Environmental Solutions �t LABORATORIES, INC. iS' 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 • Fax: 7041525-0409 Client Company Name: C")- i%�r4.) Reporrd To/Contact Narrte: Report! ng� Address: v--1 I CR-0 z_,t u• r _ P106Q i, U-e_ 00,:2,0 PAGE 0 OF _ QUOTE 9 TO ENSURE PROPER BILLING: Project Name:0AL 4i W 6—HdO Short Hold Analysis) (Yes) (Noy' -1JST Project: (Yes) (NO) *Please ATTACH any Oroject specific reporting (QC LEVEL 1 1l I11 IV) provisions and/or QC Requirements Invoice To: Address: Phone: .,- 1r ax (Yes) Purchase Order No./Billing Reference TO BE FILLED IN BY CLIEN ISAMP@ LNG PERSONNEL (Email Address: n J r G�6$�r Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days O 5 Days Certification: N�L�yC ®®® FL NC EDO Type: PDF k Excel ® r yp _ —, Rush Work Must Be "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ pp SC OTHER Pre -Approved NIA �/.I �,� p Site (Location Name: . 9�r 1'� o-_I¢ rQ Y% d i Samples received after 14:00 will be processed next business day. NO Slte Location Physical Ad ess: �— Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YESlj'` //��� NO RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) — TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTS® (SOIL, PRE' REMARKS LAB SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIVE5 NO. SIZE ID NO. HOURS SLUDGE) SEE BELOW y y I CIE F--ece C,jN-Cvv 9Vl_0 ' Li Oki o 1✓�cr�.r � L Ing 9- a �_- �p S fa Sampler's Signature ei pled By (Print Name) 6-,.N la Affiliation ward' Upon relinquishing, this Chain 9f Custody is your aut rization for Prism to proceed wlth06e analyses as reque ed above. Any changes must I o submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. a Rel'rt�uj hed By: (Sign re) Received B Si nature Date Military/Hours y: (Signature) ) Additional Comments: ' Stt�Airhial Tltiie I `, ' Rellnq fished : (Signature) Received By: (Signature) Dale I 7 ( rjr r 5ttefp�pdrture-Tlrn"d - `"'=° Relinquished By: (Signature) Received ForPrism�L bdraidrle,, Data FIEfdTeC(1 F}3e rr rr ' t 01y111eao Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUS� Y SEALS FOR TRANSPORTATIONTO THE LABORATORY. COG Group No. r ,r SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. ❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ OtherNPDES: UST: DRINKING CERCLA ILL OTHER: ASC E. PO C®SCI ®NC ®SC ❑ NC ❑ SC 9 ❑ NC-0 SC 1 ®S4ICUATER. I NC ®LID NC I fRC ®SC I NC SC SC NC ®SC ®NC ® AI *CONW TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined /OA = Volatile Organics Analysis (Zero Head Space) p &ANK PROM PT•ACCLIRATE• RELIABLE 11A33(:)3ZA-F0P,I:ES, IWC WW%V.PARLABS.CU1Ni REPORT OF ANALYSES Attn: CLAY FISACKERLY SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: MAR 17 DATE: 05/01/17 SAMPLE NUMBER- 127107 SAMPLE ID- MT. HOLLY SAMPLE MATRIX- SO DATE SAMPLED- 03/29/17 TIME SAMPLED- 1030 DATE RECEIVED- 03/29/17 SAMPLER- CF RECEIVED BY- DJ TIME RECEIVED- 1213 DELIVERED BY- CF TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 03/29/17 RE ATTACHED LA30RATORY DIRECTOR-- P.O. Box 411483 • Charlotte, NC 28241-1483 Phoric: (704) 588-8333 a Fax: (704) 588-8335 PAAF;Z PROM PT•ACCU RATE•RELIAOLE LABORATORIES, INC WWW.PARLABS.COM 30 ®ay Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO MOUNT HOLLY 127107 • 03/29/17 l a • 04/26/17 Start: End: TS g 0.2120 0.2117 TS% 1.83% 1.83% VS g) 0.1655 0.1613 VS% 78.07% 76.19% N 0.005064 yOUT 0-00493843 FSVR (Mass Balance) 2.48% FSVR Van Kleeck) 10.08% FSVR Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box 411483 • Charlotte, NC 28241-1483 Phone; (704) 588-8333 • Fax:(704):88-8335 P Am, AR PROMPT•ACCU RATE• RELIABLE LABORATORIES, INC W W W.PARLABS.COM Crucible Tare Wt (g) Sample(g) Dried Wt(g) Burned Wt(g) TS% VS% 30 ®ay Bench Scale Extended Aeration Vest Percent Volatile Solids Reduction SYNAGRO ■ MOUNT HOLLY 127107 ■ • 03/29/17 ■ ■ • 04/26/17 As Received Day 0 Day 7 Day 14 Day 21 Day 28 nz»0117 nA1n-117 nd/12117 nd/19/17 04/26/17 X28 X28 X24 X29 X30 X28 - 21.0947 21.0947 21.2216 28.7940 32.4196 21.0948 32.1745 32.6814 32.8792 39.1226 43.8166 32.6622 21.3853 21.3067 21.4338 28.9809 32.6293 21.3065 21.1412 21.2708 28.8374 32,4687 21.1452 2.62% 1.83% 1.82% 1.81 % 1.84% 1.83% 78.07% 1, 76.81%1 76.78%1 76.59%1 76.19% 0.005064043 x 0.001422828 TS ) 0.212 VS 0.1655 Volatile Fraction In: 0.42666 P.O. Box 411483 s Charlotte, NC 28241.1483 Phone: (704) 588-8333 a Fax- (704) 588.8335 0.00493843 x 0.001543068 TS 0.2117 VS ( 0.1613 Volatile Fraction Out: 0.41632 Shipping: 2217 Graham Park Drive Charlotte, NC 28273 DRAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704).588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Company Name (bitting) Comments/ Special Instructions ?CM 182& °�z Soles oe1 4V\11 2--�'v r'r Sh\Ojka \:�k SYNAGRO CENTRAL Address 12701 LANCASTER HWY City, State Et zip code PINEVILLE NC 28134 Point of Contact @ Telephone Number CLAY FISACKERLY 704-574-5291 Sample Taken By: SIGNATURE PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? Y,ES NO *Sample Type: DW Wyy GWMW HW Soil other 131&kl Sample Temp at time of sampling: 0 C Sample Temp upon receipt: ° C **Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN): Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up DatelTime Collection Date/Time Analyses Requested "tY1�, t-lolly ,� 3-a9 _/ 3a Kei Rel 0 Received by: Date(fime —Zy l * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 07/01/17 To 09/30/17 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitorinjZ data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 Coliform power per gram MPN MPN/g event sludge SM9221E of total solids CFU 560,000 628,770 700,000 CFU/g Event sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) 0ption/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) X Option/Alt. 7 (Drying —Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certificati ' chiding ine and imprisonment." -DougShoutd / ORC �� Pre er ame Tit type or print) Land ,�pl' r Name dZd Title (if applicable) (type or print) 2-J% giKature f reparer* Date Si o and Applier (if applicable) date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) NC Certification No. 402 Case Narrative IFull Service Analytical & NC Drinking Water Carl No. 37735 06/19/2017 Environmental Solutions SC Certification No.99012 MORATORIES,II\O. Synagro Clay Fisackerly 12701 Lancaster Hwy. Pineville, NC 28134 Project: 2017 Production Lab Submittal Date: 06/15/2017 Prism Work Order: 7060323 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: This report contains a total of 4 pages. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 _ Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 E IS I Fullironmee Analytical s Environmental Solutions Sample Receipt Summary 06/19/2017 r_ Prism Work Order: 7060323 Client. Sample ID Lab Sample ID Matrix Date Sampled Date Received Mt Holly 3rd Event - 1 7060323-01 Solid 06/15/17 06/16/17 Mt Holly 3rd Event - 2 7060323-02 Solid 06/15/17 06/15/17 Mt Holly 3rd Event - 3 7060323-03 Solid 06/15/17 06/15/17 Mt Holly 3rd Event-4 7060323-04 Solid 06/15/17 06/15/17 Mt Holly 3rd Event - 5 7060323-05 Solid 06/15/17 06/15/17 Mt Holly 3rd Event - 6 7060323-06 Solid 06/15/17 06/15/17 Mt Holly 3rd Event - 7 7060323-07 Solid 06/15/17 06/15/17 Samples were received in good condition at 3.6 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 ..._<....41'.'-•.__-- '-'] v--..--�:._._... ��-.o-+--�.ec-_-.:e'.' - t._ti'+_.__:'.-�_�.:«e »C:e'..am,:v:'i.R� _„_•-d w_ n-.... ^.. ..-_.-v .._ .. ..... aaa_.�-- _. Y-�.-.... , . � - - •-__^nw •....t .. AI I AR0RAT0RIE S, INC. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Client Name: Synagro Sample Date/Time Collected: Sample Date/Time Submitted: Full -Service Analytical & Environmental Solutions 449 Springbrook Rd. P..O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 Far,: 704/525-0409 Project Name: City of Mt. Holly 6-15-17 10:01 Project ID: lint. Holly 3rd Event 6-15-17 11:10 COC Group: 7060323 rBsi Sample ID Client Sample ID eca C®i orm In Solids(cfu/g) SM9222 D Reporting Limit % Solids SM2540 G Analysis Date/Time 0323-01 Mt Holly 3rd Event 560000 A 560000 1.80 6-15-17 15:08 0323-0 L Mt. Holly 3rd Event 610000 A 610000 1.65 6-15-17 15:08 7060323-03 Mt. Holly 3rd Event 620000 A 620000 1.60 6-15-17 15:08 7060323-04 Mt. Holly 3rd Event 630000 A 630000 1.59 6-15-17 15:08 7060323-05 Mt. Holly 3rd Event 650000 A 650000 1.53 6-15-17 15:08 7060323-06 Mt. Holly 3rd Event 700000 A 700000 1.42 6-15-17 16:08 7060323-07 Mt Holly 3rd Event 640000 A 640000 1.57 6-15-17 15:08 Geometric Mean Calculation: Prism Sample ID: 7060323 Geometric Mean: 628770 A cfu/g Reporting Limit: 628770 Note: All results are reported on a dry -weight basis. A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting limit. ; Y B Data Reviewed By: t?I'ojectManager: C. Rusmisell Review Date: 6-19-17 Approval Date: 6-19-17 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, lne. .. � �`.i'1!,_fJ:1:r:r.:l:lYi•rv...r:J:!:...,.J....-....J.J.rJJ.J.1.L._J.. JJ�J.......v_...r�......._._.�......_.._....................�,_u+..u�v.w...u.a�.u�.u.u.ulr.w_rJJ..ul.,.r.ua.f.�u�_,..,���i,��_r.r���.�.r_riw��.ria��,�.u��.r��.u.r.r���siui.u.�..rye.r_..y..,_�..._�y..--_r_�W..�...J .+.�ri.r_�...LL��ur—..r_ r Full -Service Analytic al & Solutions Environmental n � ��IY ��'ti ',.r''LA130RATOnIrS,1INC. 449 Sgringbr•ook Road ^ Charlotte, NC 282.17 Phone 704/529-6364 ° Pax: 704/525-0409 Client Company Name: � dL Report To/Contact Name: Reporting Address: _ , � a;IL-ke p 1011152512111 II S+.., alp • �'ee�� ski w. PAGE OF _L QUOTE IfTO ENSURE PROPER 131ILLIe NG Project Namne: WW ail V U Short Hold Analysis: (Yes) o) UST Project: (Yes) (NO) *Please ATTACH any project specific reporting (QC LEVEL 111 111 lV) provisions and/or QC Requirements Invoice To: Address: Plane afl 11ll Fax (Yes) : Purchase OrderNo.1SII1ing Reference TO BE FILLED IN BY CLBE1e9TISAMPLING PERSONNEL Email Address: L���'� ���� � a ��-� -�---�'�' ' � �'° Requested Due Date ® 1 Day ® 2 Days D 3 Days ® 4 Days ® 5 Days Certification: NELAC ®®® VcL It9C EDD Type: PDF�Excel Othper "Working Days" ® 6-9 Days ® Standard 10 days ® RushrWork Mdust Be Sc OTHER MIA Site Location Name: W±1 W011 l Samples received after 14:00 will be processed next business day. Site Location Physical Address' Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO_. Z. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES CC,,,,�� Sample Iced Upon C®Ilecti®n: YES Y- NO RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- REMARKS LAB *TYPE NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES N ID NO. HOURS SLUDGE) SEE BELOW p i �y �o ppp m U b c, � Ijf{ 0 �rL Eispr Sampler's Signature ��✓ Sampled By (Print Name) a£ f iP es�(— Affiliation Upon relinquishing, dais Chain Af Custody is your a rizatlon for Prisms to proceed with the analyses as requested above. Any change?muskad; for r 11 submitted in Writing to the PrismProject Manager. There wiil be charges any Changes after analyses have been Initialized. 11Li uP� J�rs� Relinquished B':Vii", ture) H Received By: (Signature) Date Military/Hours1r❑ Additional Comments: 51§�%AtFival Time Relinquished By: (Signs re) Received By: (Signature) Date SI{(3 )o�arfll)(jfitrp�,¢ r I r NMI Relinquished By: (Signature) Received For Is Lab o des By: Date J' r Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT IN T LS STODY SEAFOR TRANSPORTATION TO THE LABORATORY. COC Gr up No. i- t - -� SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST Cbd UNTIL RECEIVED AT THE LABORATORY. 0 "°��� � �• O Fed F�c Q UPS ❑ Hand -delivered ❑Prism Field Service ❑Other NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: C%CLA LANDFILL OTHER: ❑NCQS.0 ®NC ®SC ®NC ©SC ®NC ®SC ANC ®SC ®NC®SCI ANC 35C ®NC ®SC ®NC ®SC ' rrlrtrat *CONTAI YPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined C DA = Volatile Organics Analysis (Zero Head Space) PAR PROMPT•ACOU RATE- RELIABLE IAgORA'I'ORIRS' Il`TC WWW.PARLABS.COM REPORT OF ANALYSES Attn: CLAY FISACKERLY SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: JUN 17 DATE: 07/18/17 SAMPLE NUMBER- 127966 SAMPLE ID- MT. HOLLY 3RD EVENT DATE `SAMPLED- 06/15/17 DATE RECEIVED- 06/15/17 SAMPLER- CF TIME RECEIVED- 1138 DELIVERED BY- CF Page 1 of 1 ANALYSIS 30 DAY BENCH SCALE TEST ANALYSIS METHOD DATE TIME BY SAMPLE MATRIX- SO TIME SAMPLER- 1012 RECEIVED BY- DJ TYPE SAMPLE- Pumped RESULT UNITS VAR. 06/15/17 1315 RE ATTACHED LABORATORY DIRECTOR r_. =fir •� - C�., _ g P.O. Box 411483 e Charlotte, NC 28241-1483 Phone: (704) 588-8333 - Fax: (704) 588-8335 pb- L PROM PT-A000 RATE. RELIAB L-E: I,ABOPCXCIPCEES, UITC WWW.PAR!_ASS.COM 30 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction N F S1]���t14��1ppPWE Ili � � � � �z � � �MT HOLLYR D EVENT Start: End: TS (9) 0.2096 0.2062 TS% 1.95% 1.94% VS (g) 0.1624 0.1561 VS% 77.48% 75.70% ylN 0.005039 yOUT 19.00486191 FSVR (Mass Balance) 3.51 % FSVR (Van Kleeck) 9.45% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <16% YES 1?o. Box411483 * charlotte,NC28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 r ." PL.),k PROMPT•AGCi] RATE- R ELIA81-E 1,ABORATORIES, INC W W W.PARLABS.COM Crucible Tare Wt (g) Sample(g) Dried Wt(g) Burned Wt(g) TS% VS% 34 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO SAMP1 E 1D :MT HOLLY SAiVIPL.E # � i� 3M �STAfLT DATA � � As Received Day 0 Day 7 Day 14 Day 21 Day 28 AaMGl.97 na/11114 7 nA19Q147 07/06147 07/13/17 X9 X26 X15 X24 X9 21.4804 20.8652 21.9479 22.0096 21.4798 32.2307 31.8612 33.9042 33.0071 32.1067 21.6900 21,0818 22.1763 22.2252 21.6860 _ . _ 21.5276 20.9163 22,0025 22.0617 21.5299 ##DIV101 1.95% 1.97% 1.91% 1.96% 1.94% 77.48%1 76.41%1 76.09%1 75.83%1 75.70% 0.005038674 x 0.001464442 TS ) 0.2096 VS ( 0.1624 Volatile Fraction In: 0.39733 P.O. Box411483 • Charlotte, NC 28241-1483 Phone: (704.) 588-8333 • Fax: (704) 588-8335 gftG22mg 0.004861914 x 0.001560422 TS 0.2062 VS 0.1561 Volatile Fraction Out: 0.39021 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704),588-8335 Shipping-, Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Environmental and Natural Resources. Company Name (bitting) Comments/ Special Instructions SYNAGRO CENTRAL Address 12701 LANCASTER HWY City, State if zip code Q, S('}' j�� �� ek, PINEVILLE NC 28134 Ao Cedl}c-,& b-doio Point of Contact Et Telephone Number CLAY FISACKERLY 704-574-5291���� Sample Taken By: SIGNATURE PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? YES �/ NO *Sample Type: Dw Ww GWMW HW Soil Other ► Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C *"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No nla Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N): Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Daterf rime Collection Date/Time Analyses Requested iY1�. l olly 30-.I)CXL) fan ' t �i ! 0 -WA3 &0 V11 Kelln i eo py: uatel I ime Recelvea by'! f' j uate/ I Ime 466 Relinquish d y: Date/Time Received by: y ( DateMme * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWIAW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 10/01/17 To 11/30/17 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. I/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment ThermophiIic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf annlirnhir to altPrnnfiva narfnrmPA Wlgcc A nr C'Incc R) rmm�ia+a +ha f.U.- — m ,+nri I. +.,- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 ffi Coliform power per gram MPN MPN/g event sludge SM9221E of total solids 430,000 536,950 610,000 CFU/g Event sludge SM92221) CFU 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 NTN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: Ation/Alt. 1 Option/Alt.2 Option/Alt 3 Option/Alt.4 reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying— Stable) (Drying— Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." T "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an _ explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Doug Shoutd / ORC Preparerilame an -Title (type or print) 4igenaturoffreparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26) �.P'11�72-_;I .e-� BORATORIES, INC. Synagro Adam Brigman 12701 Lancaster Hwy. Pineville, NC 28134 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cart No. 37735 Environmental Solutions SC Certification No. 99012 Project: 2017 Production Lab Submittal Date: 09/06/2017 Prism Work Order: 7090068 Case Narrative 09/08/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Marrative Notes: This report contains a total of 4 pages. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Ivey Reference: Reviewed By Cara C. Rusmisell Project Manager BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 7 B S Full -Service Analytical & Environmental Solutions ` =1'L ..Mxcmm INC. Sample Receipt Summary 09/08/2017 Prism Work Order: 7090068 Client Sample I® Lab Sample ID Matrix Date Sampled Date Received Mt Holly 4th Event -1 7090068-01 Solid 09/06/17 09/06/17 Mt Holly 4th Event - 2 7090068-02 Solid 09/06/17 09/06/17 Mt Holly 4th Event - 3 7090068-03 Solid 09/06/17 09/06/17 Mt Holly 4th Event - 4 7090068-04 Solid 09/06/17 09/06/17 Mt Holly 4th Event - 5 7090068-05 Solid 09/06/17 09/06/17 ' Mt Holly 4th Event - 6 7090068-06 Solid 09/06/17 09/06/17 Mt Holly 4th Event - 7 7090068-07 Solid 09/06117 09/06/17 Samples were received in good condition at 5.3 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7041529-6364 - To 11 Free Number: 1-800/529-6364 - Far.: 7041525-0409 'M . � A=s! 1 ..� f _ `jLABORATORIES, INC. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Client Name: Synagro Sample Date/Time Collected: Sample Date/Time Submitted: 449 Springbrook Rd. P.O. Box 240543 Full -Service Analytical & Charlotte, NC 28224-0543 Environmental Solutions Phone: 704/529-6364 Fax: 704/525-0409 Project Name: obit. Holly 9-6-17 09:42 Project ID: Mt. Golly 4th Event 9-6-17 10:45 C®C Group: 709006E Prism Sample ID Client Sample ID Fecal Co Q orm in Solids(cfulg) SM9222 D Reporting Limit % Solids SM2640 G Analysis Date/Time 7060068-01 1 Mt Holly4th Event 610000 A 610000 1.64 9-6-17 12:02 7060068-02 Mt. Holly4th Event 560000 A 560000 1.77 9-6-17 12:02 7060068-03 Mt. Holly 4th Event 570000 A 570000 1.76 9-6-17 12:02 7060068-04 Mt Holly 4th Event 530000 A 530000 1.90 9-6-17 12:02 7060068-05 Mt Holly 4th Event 500000 A 500000 2.01 9-6-17 12:02 7060068-06 Mt. Holly 4th Event 430000 A 430000 2.30 6-17 12:02 7060068-07 Mt Holly 4th Event 580000 A 580000 1.73 if9-:6:-712:02 Geometric Mean Calculation: Prism Sample ID: 7090068 Geometric Mean: 536950 A cfu/g Deporting Limit: 536950 Note: All results are reported on a dry -weight basis. A: The result is less than the reporting Jimit. At the request of the client, the value reported equals the value of the reporting h r limit.- f Data Reviewed By: Poject Manager: C. RUsmisell Review Date: 9-8-17 ,approval Date: 9-8-17 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. I ,r FullService Analytical p �i W i �.� v Environmental Solutions '1 LABORATORIES, INC. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 Fax: 7041525-0409 Client Company Mame: � d tCi G r J (Report To/Contact Nang 4,1t1 ✓y) Errs m'ta'ti Reporting Address: L),ieyal'1.2 All.. Lli�S Y VAGE___L_ OF _ QU07E # 40 E'pNSUIl PROPER SOLU.11MG: Project Name: JV i ' I I`! ) o l ly Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) *Please ATTACH any project specific reporting (QC LEVEL I II III IV) provisions and/or QC Requirements Invoice To: split i;-f-0 Address: Phone: 70LI '- - ) - ° 6s�l I Fax (Yes) (6): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: 0 r <radvrclan � SY� sty .: CG�rn — ,�—� Requested Due Date ❑ 1 Day ® 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification. NELAC DOD FL NC EDD Type: PDF }C Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days Q Rush Worlc Must Be Pre -Approved SC OTHER NIA Site Location Name: A/Va No II Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. Water ChlorlInated: YES_ NO N (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES ,>\' NO — TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- REMARKS LAB *TYPE NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES ID NO. HOURS SLUDGE) SEE BELOW eI- G ev (),` Of j J 7 o! Sampled By Name) ! aRJ2 f', E t �t A'! Affiliation Sampler's Signature (Print Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be f submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. }' Relinquished r�r Received By: (Signature) D e Military Hours Additional Comments: ' ' f Site �pnv !I Ytme R ,l Relinquished e : (Signature) Received By: Date - Site Pgpartufe,T!ntb' - �., .; Relinquished By: (Signature) "�' Received F r Prls Labo ries By: 4 per^ pate ; FIe1d TeclrFec ,.� � _ ; Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUST DY SEALS FOR TRANSPO.RTATIOWTO THE LABORATORY. COC Group No. SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC UNTI ECEIVED AT THE LABO TORY. t) }( v (.�u �� ❑ Fed Ex ❑ UPS ❑ Hand-derivered ❑ Prism Field Service ❑ Other U NPOES: I UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: RCLA LAN®FILL OTHER: CENC ' ❑NC❑SC ❑NC ©SC ❑NC ❑SC ❑NC ❑SC I ❑NC ®SC ®NC❑5C ❑®SC ❑NC El 0NC Ell SC r r-O —1 ❑ ❑ ❑ ❑ ❑ ❑ ❑ ,onlnlAl *CONTA TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined IOA = Volatile Organics Analysis (Zero Head Space) I\Rn—, ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 11/01/17 To 12/31/17 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air.Drying Composting Aerobic Digestion Anaerobic Digestion it appucaDie to airernauve periormea t- ass A or mass is corn fete ine ionowing monitoring aata: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 Coliform power per gram MPN MPN/g event sludge SM9221E of total solids CFU 1,000,000 1,152,409 1,300,000 CFU/g Event sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) OptioriWt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Mt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) X Option/Mt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including P e and imprisonment." Doug Shoutd / ORC a � ?�1 �� 55 Prepa e d Titl (type or print) Land p ier Name and Title (if applicable) (type or print) r ignature o Prepare Date Sigdg, r Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) C %M Ta :> ��-e�.,-s��: IABORA70RIES INC, Synagro Adam Brigman 12701 Lancaster Hwy. Pineville, NC 28134 NO Certification No. 402 Full -Service Analytical & NO Drinking Water Cert No. 37735 Environmental Solutions SO Certification No. 99012 Project: 2017 Production Lab Submittal Date: 10/31/2017 Prism Work Order: 7100541 �3 t' t Case Narrative 11 /02/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: This report contains a total of 4 pages. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. 6. -� Cara C. Rusmisell Project Manager Reviewed By Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-0543 Phone: 704/529-6364 -Toll Free Number 1-800/529-6364 - Fax: 7041525-0409 Sample RecMpt Summat F ll-Se�l.e Analytical& PRISM I Environmental Solutions 11/0212017 Prism Work Order: 7100541 Client Sample ID Lob Sample ID Matrix Date Sampled Date Received 5th Event 1 7100541-01 Solid 10/31/17 10/31/17 5th Event 2 7100541-02 'Solid 10/31/17 10/31117 5th Event 3 7100541-03 Solid 10131/17 10/31/17 5th Event 4 7100541-04 Solid 10/31117 10131117 5th Event 5 7100541-05 Solid 10/31/17 10/31/17 5th Event 6 7100541-06 Solid 10/31/17 10131/17 5th Event 7 7100541-07 Solid 10/31/17 10131117 Samples were received in good condition at 4.8 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.D. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 ..... ........ ..... VEm.- BORATORIES, INC. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert. No. 37735 Client Name: Synagro Sample Date/Time Collected: Sample Date/Time Submitted: Full -Service Analytical & Environmental Solutions 449 Springbrook Rd. P.O. Box 240543 Charlotte, NC 28224-0543 Phone: 704/529-6364 Fax: 7041525-0409 Project Name: Mt. Dolly 10-31-17 07:45 Project ID: 5th Event 10-31-17 09:00 CGC Group: 7100541 rlsrra Sample ID Client Sample ID 'eea C®I orsxa in Solids(ctu/g) SM9222 D Reporting Limit % Solids SM2540 G Analysis Date/Time. 7100541-01 Mt. Holly 5th Event 1200000 A 1200000 0.830 10-31-17 10:45 7100541 02 Mt. Holly 5th Event 1100000 A 1100000 0.940 10-31-17 10:45 7100541-03 Mt. Holly 5th Event — 1100000 A _[ 1100000 — 0.910 10-31-17 10:45 7100541-04 Mt Holly5th Event 1000000 A 1000000 0.970 10-31-17 10:45 7100541-05 Mt. Holly5th Event 1100000 A 1 100000 0.890 10-31-17 10:45 Mt. Holly 5th Event 1300000 A 1300000 0.790 10-31-17 10:45 E Mt Holly 5th Event 1300000 A 1300000 0.750 10-31-17 10:45 Geometric Mean CalcuIR166i: Prism Sample ID: 7100541 Geometric Mean: 1152409 A cfu/g Reporting Limit: 1152409 Note: All results are reported on a dry -weight basis. A: The result is less than the report g limit. At the request of the client, the value reported equals the value of the reporting limit. /I ; � Data Reviewed By:; yf '�Zl ' Y t'roject Manager: C. Rusmisell Review Date: 11-2-17 Approval Date: 11-2-17 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. i. f. i , �" ,.� rrr,,,u......,.�., rra. r.car.�rrr..,.e.u.u.,.....�,.ii}Y:__�..... d.irr..._.r.,.%55$:i: .. 7S5i:.w....._.�:i:'_...._ r...r . .. .0 .�_ - sr• ...,r.e.... .,rs+_ _s, r __r.c.._ ,.0 ..._us._i�u��_J.w�.,.r_.s_i.,....,..ua...,.,sr'uT'i,�`•r•,'�•;•:'%rmmm:...'rc,am�r CHAIN OF CUSTODY RECORD r o r r Full -service Anal rtleal w' � +4 t pp g p' '} ��� iI rrR i c y , }; y Environmental Solutions PAGt of l QUO'TE0TOENSUREPROPER0116ILINGa ,�F�1 t= «.4 '��AsoaA7oRiES tnia /#f g r SatTfp�e$7hLTF1 T 4PO�t rplyalrl r f{ x y r i I f fir f9 :rrf 'Sr n5 � •ai: 44.9 Sprincdbrook Road > Charlotte, HC 28217 Project Name: Phone 704/529-6364 Fax: 7041525-0409 Short Hold Analysis: (Yes) j o) UST Project: (Yes) (NO) "Please ATTACH any project specific reporting [QC LEVEL 1 li III IV) Client Company Name: �yg!�4'—v —���' provisions and/or QC Requirements Report To/Contact Name: r9q i3ri',2-?k6 -) Invoice To: Reporting Address: 12.70+ Q tatCrd.m- •Nlrwt. Address: Phone:701 6, 0G 1' 1( Fax (Yes)W): �, PlarchaBe �Irder N®.!Filling Reference C• kA4 ( 4_,0a4lr,0 TO SE FILLED IN EY CLIENT/SAMPLING PERSONNIEL / Email Address: ,'4c1°' . ,ce.,71 � EDD Type: PDP' ?,/ Excel Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days m 4 Days 05 Days RushBe "Working h Work Certification: NELAC ®®® FL NO ar ' _Other' Days" ❑ 6-9 Days ® Standard 10 days ❑ Site Location Name: 1144 e 4e�t+!# Iy --s o — I s 0 tf dust re Samples received after 14:00 will be processed next business day. SC OTHER NIA Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ N® v (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES r' Sample Iced Upon Collection: YES V NO RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- at' REMARKS LAB *TYPE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR NO. SIZE TIMES A10011" ID NO. HOURS SLUDGE) SEE BELOW I `w f 1:3� tnd. .0 Y �Z,> ry Y � iJ� '�11Lar`'E�✓i t t� NrJ,FU-e14- Vt yri1 F'" 4 a� ,vlctl �•Tg' �iY�I V:••�/d'd`� � t t L�jp 9 �`t r4 ✓ g/ t/ W "1i ti8� 5 0.1 l Al �,r lit Sampler's Signature dJ�(7 Sampler's Sampled By (Print Name) ,�1^f64? r!Gr y dl1i Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes roust be submitted in writing to the Prison Project Manager, There will be charges for any changes after analyses have been initialized. ° Relinquished By: (Signature) , Received By: (Signature) Date qq 1 �y Military/Hours �a Additional Comments: 1,Sit�/�f•t'Ivaf,,;�jm�. ,' l, +t Relinquished By: (Signature) d Received By: (Signature) Date OlemrlI T(1no + ('$� Relinquished By: (Signature) Receiy or Prism Laboratories By: Date c g '°� — I y �i ,'°jj°'� 1 `"' �J 1 1 d 4:+'"d.°' Method of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No. t 9 J SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY. { �I 10 CT 1 O Fed Ex ❑ UPS ® Hand -delivered ❑ Prism Field Service O Other NPDES, UST. GROUNDWATER:DRINKING WATER:' SOLID WASTE: RCRA. CERCLA LANDFILL OTHER: ❑NC❑SC ❑NC ®SC ❑NC ❑SC ❑NC El I ❑NC El SC ❑NC❑SC El ®SC ❑NC ❑SC I ' ©NC ®SC ❑ ❑ ❑ ❑ ❑ c ❑ ❑ - ❑ !r^1n;t11 *CONTJ TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined VOA = Volatile Organics Analysis (Zero Head Space) 0 Am P PROMPT-ACCURATE' yR,E[+LIAVB�LE: T t,-� \VNN'N'.PARLABS.('0Nl REPOR': OF AtiA_Y: ES Attn: ADAM BRIG -MAN SYNAGRO 12701 LANCASTER HWY PINEVILLE, N_' 28134- PROJECT NAME: SEP 17 DATE: 10/10/17 SAMPLE NUMBER- 129036 SAMPLE ID- MT. y' LLY 4TH EVENT SAMPLE MATRIX- SO DATE SAMPLED- 09/06/17 TIME SAMPLED- 0942 DATE RECEIVED- 09/06/17 SAMPLER- AB RECEIVED BY- DJ TIME' RECEIVED 1111 DELIVERED BY -CAB TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS METHOD -DA` E' TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 09/06/17 RE ATTACHED LABORATORY DIRECT,):-. 11.0. Box 411443 ° Charlotte. INC 2S'241-14,N } Phone: (/04) 588 33 - Fay: (704) 58845335 s P PROM PT•ACCU RATE• RELIA9 LE I..ABORA-FORTES, INC WWW. RARLAE3S. COM 30 ®ay Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAGRO r MT. HOLLY 4TH EVENT 129036 09/06/17 • 10/05/17 Start: End: TS () 0.1963 0.1808 TS% 1.66% 1.63% VS () 0.1523 0.1371 VS% 77.59% 75.83% I N 0.00437 OUT 0.00401875 FSVR (Mass Balance) 8.04% FSVR (Van Kleeck) 9.38% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 0 Fax: (704) 588-8335 P Am PRO MPT•ACCU RATE -RELIABLE LABORATORIES, INC W W W.PARI-ABS.COM Crucible Tare Wt (g) Sample(g) Dried Wt(g) Burned Wt(g) TS% VS% 3.0 Day Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SYNAG RO MT. HOLLY 4TH EVENT 129036 09/06/17 s • 10/05/17 As Received Day 0 09/06/17 09/07/17 Day 7 Day 14 Day 21 Day 28 09/14/17 09121/17 09/28/17 10/05/17 X15 X18 X5 X18 X22 X18 21.9490 23.0242 20.5204 23.0241 22.3086 23.0250 35.2112 34.8509 32.3846 34.4477 33.4244 34.1151 22,2421 23.2205 20.7114 23.2126 22,4909 23.2058 23.0682 20.5638 23.0671 22.3508 23.0687 2.21 % 1.66% 1.61 % 1.65% 1.64% 1.63% 77.59%1 77.28%1 77.19%1 76.85%1 75.83% 0.004370045 x 0.001262521 TS () 0.1963 VS () 0.1523 Volatile Fraction In: 0.46741 P.O. Box411483 • Charlotte, NC 28241-1483 Phone: (704)SSS•8333 • Fax: (704)5SS-8335 0.004018748 x 0.001280968 TS { 0.1808 VS ) 0.1371 Volatile Fraction Out: 1 0.46521 L RALABORATORIES, , INC. www.pariabs.com CHA ®F CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carnlina Denartment of Environmental and Natural Resources. Company Name (billing) Comments/ Special Instructions SYNAGRO CENTRAL Address 12701 LANCASTER HWY l !17 y I Ae (� V el 1J`` 'I �GoL i' e J Q �,Jf e Ne edS 40 b e City, State Et zip code PINEVILLE NC 28134 �e �t('c l d. d �8 below e ow ZG/ Point of Contact iY Telephone Number }/ Z __n �/EI9A ril DIV .ac}�pj �`} -) — 650 .Lu L/ _ v I l r Sample Taken By SIGNATURE PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? YES NO "Sample Type: DW Ww GWMW HW Soil Other r'o Sample Temp at time of sampling: ° C Sample Temp upon receipt: 0 C "Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N): Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Daterrime Collection Datef rime Analyses (Requested ffi , HollY 30- aY e1,101 113 L ven'r X q � �7 ` ' `IZl%r sQ- dtifU eh�h C)P I Relinquished by: Dgte ime Received by: Dateffime �i',w✓_`Cr G' -C'4 Relinquis ed by: D&e/Time Received by: Date/Time C=Composite G=Grab DW=Drinking Water W1N=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side Agricultural Lime Application Log 2017 Project: City of Mt Holly Field (state -county -site -field) Grower Soil pH Lime Requirement (from soil analysis) Tons/Acre Applied Date Applied Total Acres NC-GA-41-01 Greg Springs 6.3 0.0 0.0 NC-GA-41-06 Greg Springs 6.3 0.0 0.0 NC-GA-41-14 Greg Springs 6.4 0.0 0.0 NC-GA-45-01 David Allen 6.1 0 0.0 NC-LT-46-01 Ton Jones 6.1 0 0.0 NC-LT-46-02 Ton Jones 6 0 0.0 NC-LT-46-03 Tony Jones 6.1 0 0.0 NC-LT-46-04 Tony Jones 6.1 0 0 NC-LT-46-05 Ton Jones 6 0 0 NC-LT-46-08 Tony Jones 6.3 0 0 NC-MG-37-01 Dale Connell 6.2 0 0 * lime has been ordered but not spread NCDA&CS Ai mic Division Phone: (919) 733-2655 Website: www.nc-,..y.)v/agronomi/ Report No. FY18-�,�i.2239 Greg Springs �y <-�m•_••„•• g Advisor: Synagro Predictive 410 West Catawba Ave 12701 Lancaster H wy Mount Holly, NC 28120 Pineville, NC 28134 i=. Soil Report Mehlich-3 Extraction 4 r••>� .' Sampled County :Gaston Links to Helpful Information Client ID: 452256 Advisor ID: 449334 Sampled: Received: 08/11/2017 completed: 09/01/2017 Farm: NC-GA-41 Agronomist's Comments: This report provides Test Results and Recommendations for each sample submitted for testing. Look for Lime Recommendations and N-P-K Fertilizer Recommendations. The lime recommendation is always listed next to the first crop and will be based on the higher target pH if the pH targets for crop 1 and crop 2 differ. Application at the indicated rate will raise soil pH to the optimal level for the plant you specified and should be sufficient for 2 to 3 years, depending on soil type. Common target pH values are as follows: 5.0 for azalea, camellia, rhododendron and mt. laurel; 5.5 for centipedegrass; 6.0 for other lawn grasses, shrubbery, and; flowering plants; and 6.5 for vegetable gardens. N-P-K Recommendations are based on the nitrogen (N) needs of the plants being grown and the soil test results for phosphorus (P-1) and potassium (K-1); a 50 to 70 index for either is optimum. If the exact fertilizer cannot be found, find the closest match and ad'ust the rate accordin I . Refer to "Understanding the Soil Report" last page of this report) for additional explanation and links to helpful information. Sample ID: 41-06 Recommendations: Lime . Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 70 90 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.91 9.4 92 0.8 6.3 29 26 63 27 60 224 146 208 208 400 0.1 1 Sample ID: 41-01 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.41 0.93 15.2 93 1.1 6.3 67 143 59 29 65 272 176 370 370 180 0.2 1 Iorth Carolina ' �i�IY:�CyiP �141SL 1�111rL1 C1a111hIc5}li>IA Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner ofAciriculture NCDA&CS A ------ mic Division Phone: (919) 733-2655 Website: www.nLay,.yov/agronomi/ Report No. FY18-bLUu2239 Greg Springs Page 2 of 3 Sample ID: 41-14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 100 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cnn ; CEC and Na in meq/100 cm3; NO3-N in mg/dnr ]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 0.82 12.5 94 0.8 6.4 98 19 67 27 83 195 129 448 448 485 0.2 2 NCDA&CS A_ mic Division Phone: (919) 733-2655 Website: www.n( ov/agronomi/ Report No. FY1E, __j2239 Greg Springs Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat( is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncacrr.gov/agronomi/obpart4.html fsFind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize) Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, CA, S-I, SS-1, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrpov/agronomi/uvrst.htm Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS -I soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS / r omic Division Phone: (919) 733-2655 Website: www.n _ jov/agronomi/ Report No. FY10-0L-Lj01248 L l.lpq .. : a �� tli Client: David Allen Advisor: Synagro Predictive 110 Helton Rd 12701 Lancaster Hwy k ra wu� fit~I Cherryville, NC 28021 Pineville, NC 28134 Soil Report Mehlich-3 Extraction Sampled County: Gaston Links to Helpful Information Client ID: 452255 Advisor ID: 449334 Sampled: Received: 0712712017 Completed: 08/04/2017 Farm: NC-GA-45 Sample ID: 45-01 Recommendations. Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, E 1.2 50-70 90 60 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 80 90 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cn-P; NO3-N in mg/dnr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.05 7.6 80 1.5 6.1 24 23 58 21 37 1601 970 976 102 102 118 0.1 1 North Carolina is+It;i4,�ia°Jnlwf I�i.nul�'i��ItirCi55141� Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS A _ imic Division Phone: (919) 733-2655 Website: www.n". u..uov/agronomi/ Report No. FY1b-oL_uJ1248 David Allen Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg/ % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not M-0 N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Na sodium NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmVl#sFind information that P-I phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS -I soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uvrst.htm Page 1 of 1 Report Number: 17-073-0790 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 Waypoint ANALYTICAL "Every acre... Every year.'4M Date Received: 03/14/2017 Date Of Analysis: 03/15/2017 Farm ID: NC-LT-46 SOIL ANALYSIS REPORT Date Of Report: 03/15/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Tony Jones Mt Holly 50-1701 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 %, Rate Soil Class Ib/A s M3 .. ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g meq/100g 01 03532 .6.5 H 150 91 H NC = 76 62 L NC = 32 127 M 1009 M 8 VL 6.1 6.83 1.0 7.3 MIN 03 03533 7.1 VH 150 36 MT NC = 30 55 VL NC = 28 148 H 833 M 13 VL 6.1 6.84 0.9 6.5 MIN 08 03534 6.1 H 150 86 H NC = 72 51 VL NC = 26 167 H 750 M 10 VL 6.3 0.6 5.9 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K % Mg % Ca % Na % H % NON ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 01 2.2 14.5 69.1 0.5 13.7 4 VL NC=8 8.4 VH NC=210.0 20 M NC=125 127 VH 6.6 VH NC=330.0 0.5 L 03 2.2 19.0 64.1 0.9 13.8 15 L NC=31 4.7 H NC=117.5 41 H NC=256 62 VH 3.5 VH NC=175.0 1.4 L 08 2.2 23.6 63.6 0.7 10.2 13 L NC=27 9.5 VH NC=237.5 23 H NC=144 76 VH 4.9 VH NC=245.0 0.5 L values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested, samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: P z` C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric McGroary Page 1 of 1 Report Number: 17-340-0506 Account Number:46441 Send To: Synagro Central LLC/ Charlotte Adam Brigman 12701 Lancaster Hwy Pineville NC 28134 e Waypoint ANALYTICAL "Every acre... Every year. "rn+ SOIL ANALYSIS REPORT Date Received: 12/06/2017 Date Of Analysis: 12/07/2017 Date Of Report: 12/07/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Tony Jones City of Mt Holly Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number ° �° Rate Soil Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g meq/100g 46-02 12318 5.5 H 150 4 VL NC=3 48 VL NC=25 177 H 853 M 28 VL 6.0 6.82 1.1 7.1 MIN 46-04 12319 5.8 HH 150 2 VL NC = 2 40 VL NC = 20 165 H 787 M 45 L 6.1 6.84 0.9 6.5 46-05 12320 5.7 H 150 2 VL NC = 2 38 VL NC = 19 172 H 823 M 42 L 6.0 6.82 1.1 6.9 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Sample ID Field ID K % Mg % Ca % Na % H % NO,N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 46-02 1.7 20.8 60.1 1.7 15.5 34 H NC=71 0.6 VL NC=15.0 46 H NC=288 50 H 1.8 H NC=90.0 0.3 VL 46-04 1.6 21.2 60.5 3.0 13.8 69 VH NC=144 0.7 VL- NC=17.5 41 H NC=256 47 H 1.3 M NC=65.0 0.3 VL 46-05 1.4 20.8 59.6 2.6 15.9 76 VH NC=158 0.6 VL NC=15.0 36 H NC=225 58 VH 1.1 M NC=55.0 0.3 VL Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �aµri� C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypolntMalytical Virginia, Inc. Pauric McGroary Page 1 of 1 Report Number: 17-073-0791 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 Waypoint A NALYTICAL "Every acre... Every year."Tu no4o ao..oi —4- nR/1A/7n17 nat. rlf Annlvcic- mvi';;/7nl7 Farm ID: NC-MG-37 SOIL ANALYSIS REPORT Date Of Renort: 03/16/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: Dale Connell Mt Holly 50-1701 Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH OM wN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil M3 K Mg Ca Na Soil Buffer H Field ID Number Rate Class Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 01 03535 5.4 150 29 L 74 L 185 VH 602 M 4 VL 5.2 0.7 5.5 H I NC = 24 NC = 38 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS Field ID % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 01 3.4 28.0 54.7 0.3 12.7 7 VL 5.9 H 54 VH 93 VH 3.1 VH 0.3 VL NC=15 N6=147.5 NC=338 NC=155.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), los/A i nis report appnes to sampiets) testeu. aampies soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by: ?W11 m'` 6001 Pauric McGroary Schutte, Maria From: Schutte, Maria Sent: Tuesday, April 11, 2017 5:56 PM To: 'david Johnson@mtholly.us' Cc: Jonathan Jordan@mtholly.us'; 'ray.clemmer@mtholly.us'; 'Clay Fisackerly'; Gregory, Sonia Subject: WQ0001863 Mt. Holly 2016 Annual Report Receipt and Additional Information Request Mr. Johnson, This.email will serve as the Acknowledgement of Receipt of the 2016 Annual Report for the referenced residuals permit. A report copy was received in the Mooresville office on March 6th, 2017. My comments and additional information requests are noted below and were discussed with Jonathan Jordan during the March 28th inspection. Waypoint labs does not include the Exchangeable Sodium Percentage (ESP) calculations in their soil reports. The missing information needs to be submitted for each field (a table with field ID and calculated ESP is acceptable), per Permit Condition IV.5. • Verify contract lab is performing the 30day bench in accordance with the procedure. The dates displayed on the Sept/Oct PAR labs report appear to be <30days. There is often an additional lab bench sheet that shows readings overtime and that should be included with the report. • A 3.01 % solids is recorded for the first quarter (2/18/16); however, the lab results show a 1.96% .solids. This will affect all parameter calculations for the fields applied during the first quarter. The resulting PAN and total metals data will actually be lower not greater, so there is no concern of an over application, but the "Application Field Summary" forms need to be corrected for accurate cumulative totals going forward. Please contact me with any questions and email your response with the requested additional information. Thank You! Maria Maria Schutte Environmental Specialist Water Quality Regional Operations Section Division of Water Resources North Carolina Department of Environmental Quality 704 663 1699 office 704 235 2184 direct Maria. schutte(aD_ncdenr.gov 610 East Center Avenue Suite 301 Mooresville, NC 28115 Err,ad ccrrospomdonce to aria ro;aa this address is subject to the North Carolina Public Records Law and may be disclosed to third parries. - 71� REcmVLD/NCDENR10WR WQROS MOORESVILLE REGIONAL OFFICE rj FEB 2 7 2017 City of Mount Holly, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0001863 2016 ANNUAL REPORT City of Mount Holly, NC Residuals Land Application Program 2016 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms and SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00001863 County Gaston Year 2016 Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NC0021156 & 01-36-020 Land Application Operator Synna ro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 21 Total number of fields utilized for land application during the year: 10 Total amount of dry tons applied during the year for all application sites: 198.46 Total number of acres utilized for land application during the year: 140.5 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. Allother monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification:. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting fal information, ' clud' g the possibility of fines and imprisonment for knowing violations." Danny Jackson, City Manager b ^ 1 l Permittee Name and Title (type or print) i pg Date FEDy F'V AA 201 Ygnature of eparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION -,'iVIOUNT HOLLY, NC MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS March 2016 527,000.00 G 66.14 D 59.99 June 2016 657,200.00 G 57.27 D 51.94 September 2016 471,200.00 G 37.31 D 33.86 November 2016 620,000.00 G 37.74 D 34.24 YEARLY TOTAL 2,275,400.00 G 198.46 D 180.03 1 /25/2017 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001863 Facility Name: MOUNT HOLLY, NC NPDES# : NCO021156 or WQ# (residual only) WWTP Name: MOUNT HOLLY W/WTP Residuals Analysis Data / Product Type AEDLIQ Date Sampled (grab) or 02/18/16 Date Composited Percent Solids PARAMETERS (mg/kg dry weight) Arsenic Cadmium Mercury Chromium Copper Lead Molybdenum Nickel Selenium Zinc Total Phosphorus TKN Ammonia -Nitrogen Nitrate and Nitrite Laboratory WAYPOINT ANALYTICAL Waypoint Analytical Virginia Inc. AEDLIQ AEDLIQ AEDLIQ *.. 04/19/1607/28/16� 09/26/16' 2.09 1.90 1.46 3 <3 3 <3 <2 <2 <2 <2 1.1 1 1.7 1.2 257, 258 298 328 476 516 548 578 37 36 38 50.7 <5 6 7 <5 22 24 34 26 <5 <5 <5 <5 768 857 881 898 14500 15400 13500 13500 52600 56500 50000 50300 4590 7660 10500 9520 <2 <2 <2 <5.42 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." JURE OF' PREPARER) :SSF (5/2003) Date-2-44 7 Printed: Wednesday - January 25 2017 at 11:56:37 for: 1701 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001863 Facility Name: MOUNT HOLLY, NC NPDES# : NCO021156 or WQ# (residual only) WWTP Name: MOUNT HOLLY WWTP Residuals Analysis Data Product Type Date Sampled (grab) or Date Composited Percent Solids AEDLIQ 02/18/16 PARAMETERS (mg/kg dry weight) Aluminum Calcium Magnesium pH Potassium Sodium Laboratory WAYPOINT ANALYTICAL Waypoint Analytical Virginia Inc. i f AEDLIQ AEDLIQ AEDLIQ 04/19/16 07/28/16 09/26/16 3.01 2.09 1.90 1.46 24100 23000 28700 20200 11100 11700 10900 13400 2470 2640 2490 2940 7.33 7.37 7.39 7.51 2610 2830 1860 2200 5830 7040 6010 9110 I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X M111 NR - Data Not Reported or Data Not Required Date 2`ce : t7 DENR FORM RSSF-B (7/2002) Printed: Wednesday - January 25, 2017 at 11:57:04 for: 1701 01 Page: 1 of 2 Report Number: 16-050-0202 Account Number: 00015 Send To: SYNAGRO CENTRAL/MT HOLLY WAYNE BRADY 12701 LANCASTER HWY PINEVILLE , NC 28134 (2) Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: MT HOLLY WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/18/2016 14:00:00 Lab Number: 55117 Date Received: 02/19/2016 00:00 Sample Id : MY HOLLY WWTP 50-1701 1ST EVENT Date Reported: 02/24/2016 Total Solids Moisture * Total Kjeldahl Nitrogen Total Phosphorus Total Potassium Total Sulfur Total Calcium Total Magnesium Total Sodium Total Iron Total Aluminum Total Manganese Total Copper Total Zinc Ammonia Nitrogen Organic N Nitrate+ N itrite-N 98.04 5.26 1.45 0.26 1.38 1.11 0.25 0.58 0.46 4.80 52600 14500 2610 13800 11100 2470 5830 14900 24100 437 476 768 4590 48010 <2.00 <2.0 100.0 RD 02119/201614:30 SM-254OG 100.0 RD 02/19/201614:30 SM-2540G 10.0 JM 02/22/2016 08:44 SM-4500-NH3C-TKN 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 100 KM 02/22/2016 10:46 SW 6010C 5 KM 02/22/2016 10:46 SW 6010C 5 KM 02/22/2016 10:46 SW 6010C 5 KM 02/22/2016 10:46 SW 6010C 10.0 JM 02/22/2016 08:44 SM-4500-NH3C 10.0 02/22/2016 08:44 CALCULATION 2.00 JM 02/22/2016 08:45 SM-450ONO3F 2.0 KM 02/22/2016 10:46 SW 6010C on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made hpany in any advertising, news release, or other public announcements without obtaining our prior written authorization. 0091910 f•7C Page: 2 of 2 Report Number: 16-050-0202 Account Number: 00015 Send To: SYNAGRO CENTRAL/MT HOLLY WAYNE BRADY 12701 LANCASTER HWY PINEVILLE , NC 28134 0 Waypoin,(Zt ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: MT HOLLY WWTP NC CERT#257 REPORT" OF ANALYSIS Date Sampled: 2/18/2016 14:00:00 Lab Number: 55117 Date Received: 02/19/2016 00:00 Sample Id : MY HOLLY WWTP 50-1701 1ST EVENT Date Reported: 02/24/2016 �PARAMETtR RESULT RESULT QUANTITATION METHOD Total Chromium 257 5 KM 02/22/2016 10:46 SW 6010C Total Nickel 22 5 KM 02/22/2016 10:46 SW 6010C Total Lead 37 5 KM 02/22/2016 10:46 SW 6010C Total Arsenic 3.0 3.0 KM 02/22/2016 10:46 SW 6010C Total Mercury 1.1 0.4 KM 02/23/2016 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 02/22/2016 10:46 SW 6010C pH (Standard Units) * 7.33 2.00 JM 02/22/2016 08:44 SW-9045D Total Molybdenum <5 5 KM 02/22/2016 10:46 SW 6010C Comments: QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: John Culp Project Name: City of Mt. Holly WWTP Biosolids Project Number:50-1701 Lot Number:RC16061 Date Completed:03/1712016 Lucas Odom Project Manager LABORATORY_ ACCREDITATION ION I. BUREAU ���• ACCREDITEO roue roza This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist. Shealy Environmental Services, Inc. Page: 1 of 5 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: RC16061 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page Shealy Environmental Services, Inc. Page: 2 of 5 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Synagro Lot Number: RC16061 Sample Number Sample ID Matrix Date Sampled Date Received 001 CITY OF MT HOLLY WWTP % SOLID 1ST EVENT Solid 03/16/2016 0805 03/16/2016 (1 sample) Shealy Environmental Services, Inc. Page: 3 of 5 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com SHEALY ENVIRONMENTAL SERVICES, INC. Executive Summary Synagro Lot Number: RC16061 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 CITY OF MT HOLLY VWVfP % SOLID Solid % Solids SM 2540G 3.01 % 5 (1 detection) Shealy Environmental Services, Inc. Page: 4 of 5 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Client:Synagro Laboratory ID:RC16061-001 Description: CITY OF MT HOLLY WWTP % SOLID 1ST EVENT Matrix: Solid Date Sampled:03/16/2016 0805 % Solids: 3.01 03/17/2016 0111 r1ate Received: 03/1612016 Inorganic non-metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 03/17/2016 0111 HMA 98618 CAS Analytical Parameter Number Method Result Q PQL Units Run % Solids SM 254OG 3.01 % 1 PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time ND = Not detected at or above the PQL J = Estimated result < PQL and > M DL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria ,sere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W' ealy Environmental Services, Inc. Page: 5 of 5 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Chain of Custody ..�k Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com ' SHEALY ENVIRONMENTAL SERVICES, INC. ean3-7Faxluaobaa��7Za172I` , Telephone No. 71-9D 1~ vAv.sheslyllab.com Number 4 45 8 8 Gti°mr 3+rpc [ ro Cc100 Tc*v?rrnO r4V Fnwk QW(a vp, Adt>W I A 7 01 "7� I SaroiW$ St MTWX X— - ,UMfYVS (AUARV 8'st+f AM spa^4'rt,7e.GaWJ' I Fx5�7a (I)TJ Ar1,g,L4-11e SUGc ZO Cad N. FirvivA %7jW ,Pieve&Mx RM Ma Ppv b �atnfr3 �r sergns a'ay Ly ewoom Ow W j i — 7 R—__,._._. 7irrrrfirautrdUlu"RaquLwd(Martabs�vavalrawuanf&aear�a�7tm�9�� ❑SrAndar4r oshfsa '7) Imo• .'i 13 sa�rpte�7i�� pdga l&HSsvdMalmk-13A ggovo iv L70f bi'4ab Non-l!mrd ❑Hwonahlo ❑8!girINwik OPolsoh ❑ftnoµrr acRequim enfe,j5��c ) �. itis;ie 6� Darc i.Re Jby T-ffmr-l" DDM& p Tynvs r1 {� 2 �F'iaP,RgttiShe�M by Dare + . a ia5 a, ,+ 'ARM3. RaR quishadby x �yGe 3. AECIMPI � r7}' .Lwa .�'aw 41 hl2fmPU'shad bP' date g aG+a roun'ucd b_ as '�4 Mkp Tyra ,rote. AN r,m*s am, r-Wafywdfor four wmeks frofta Temps r_.apusEora,r on,1e6 o0ar atrangamenfg arg made. AnSINdwrrtso,fGY *) cyc * a:�- P,r.Er I RUMf WSMIUVEM: WHI-M& YELLOW-flebm 0 Wmrory rM Gavy di=mi?,gMYLm6ar:;---A0.7J3 fSacnW IMfer 06,"W14 cn 2 z TC N z ic M z v) /M MrA U) SHEALY ENVIRONMENTAL SERVICES, INC. -11u3)!?F,nAror)mw1113 Service;, 11w- Fake i of L 330vurratni Nitmb= Elkalve Vau-! rR103,12036 Sample &�Qeipt Cheeldist (SRQ) Coolcr lnsper,tr4 byldaw \—.r,s Lot Means of receipt. 'ES1 Ujmt lEl UPS [] FMEx El Other VWE] 11 No 1Z 1, weTe cufuody seals present on the cookT? Yes U JELJLJ NA L-�T 2. If wstvdy seaTs were resent, we . pH strip TD, cl scrip 11): Cooler ID/01riginal tewpaatare upon rwcjpt'T)t"4ved (conected) temp-7aturcupon receipt "C Oc IZC—thalk, [aTemperatur- Blank E.] Against Bottles IRGun. lD-.. S- JP, Gun Correc9on Factor: 2Qt=,_:°Q Method of roolant., wet ice ❑ R1 Ue Ire EJ Dryloe. ❑ N-Ma 3. If lerrip1mture of any cooler cumded 6,011(%,was 11rcftet klanaggr nedifficd? pM to X:itti' ma W-raee� (CirvIe One). fled hy: hone I - -- it i faw - Yes El No ❑ -,NAFZ 4, 19 lie. commerciil courier's packinig slip atuachod to this form? NaFos El 5, Wcrv, piftper eustody_p 'A --Z �qcedurts (relinquishe Ire eive foil nvcd? M3 ❑ P 16, Wcre %ample [IN listed on the COC? Y,. -3 No C1 17, Were gample 1D.% listed on all saMlc <;ontaiaers? Yes Ler NoEl 8. Was oulledion date be time fisted an the COC? Yes No 9, Was Im elistedonalls YCS No EJ— .1 10- Did all container label itifo=ation (iD, date; (imp) air with the HOC? Yes No F1 11. lk"tere tesis to bo pCeLormi;d liste4 on the Coe'? Y�A- [2�' No El 12. Did all sample arrivu- in the pCoper containers fbr carh tm( antYar in good oondirion ken, lids 014 ew)? y YeS N0 13. Was adequate 5 a to volu ale al-aflable? 7- - di-e holding time or 48 hu=, whkhever come; first? 14� Were all sampics rcceiwil within J,,' Yes El No 15. Were any samples containers missia_Wexr=s& (v,11rcl t; one) =Vles not listicd on COC? 16- Werebubble-s present>"pea-sip'' 4'or 6Dun in diaoveow) in any VOA vials? ties _ NGEJ IV" all las received at: a pH -of <,2?'L-- Yes F❑— I -W- clo NA 19. Wwo all rw4nide and'ar sulfide samples ro=-o--d aL a pH > 111 Yes ❑No 1. 9- Were all applivable NHITIC-Mleyaniddphenol (-'Urngfr );5aTnpte& rree of msidual Yrs Ala OfNti L far I ? ed -3n the COC 0 C Sa!R11 CS Yes wc, [37 NAU 2 1, Ware client remarkshequests rcquesttd dilixtians, MS(NISD designations, utc--) correctly transcribed frorA else COO into ffie commcut wulion in 77 17- No [0' the quote number used I Rkcn kont thrw- Container label'? SamploPmervation (Must be mmpleed, for any sample(s) inwrmadypr�ievved or with headspace.) ;wro recciNrcut -1111;VITeL�JL[y pi-eseived and tJ 3ovore-filgly in sample rweiving with M7SOA, iUO!, U-6U05R4 sampic(k) wvrc =cuivud with bubbles >6 nini In diameter. saniples(s) wtye received vAth TRO >02-1 mg (lf 921 is No) and :47-7r, adjwqted. accordingly in satngle rooeiving- ".%rith sodium thiostilfine (Na7.9;,,Oi) with Shealy ID: SO DrinkIng Watcr Project Sample(s) pEl wrific-d to bu ` 2 by Datec Sato wcrcnot rqcrived ata PN of.<2 and wore aLsted accardingty using SR4 Sample labels applied by-. Verified by:- Date QqMgLelits: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 2/18/2016 111/2016-3/3112016 2.2547 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) — 100 = (5830 x 3.0100) _ 100 = 175.483 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (11100 x 3.0100) _ 100 = 334.11 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2470 x 3.0100) _ 100 = 74.347 Na meq = Na mg/I = Molec.Wgt.Na = 175.483 _ 23 = 7.6297 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 334.11 = 20 = 16.7055 Mg meq = Mg mg/1= Molec.Wgt.Mg = 74.347 _ 12 = 6.19558 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.6297 + SgrRoot[0.5(16.7055+6.19558)] = 2.25473 Printed: 1/25/2017 Page 1 11:59 Page: 1 of 2 Report Number: 16-111-0203 Account Number: 00015 Submitted By: DREW CULP Send To: SYNAGRO CENTRAL/MT HOLLY WAYNE BRADY 12701 LANCASTER HWY PINEVILLE , NC 28134 Lab Number: 56806 Sample Id: 2ND EVENT D Waypoint( ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: MT HOLLY WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/19/2016 09:30:00 Date Received: 04/20/2016 00:00 Date Reported: 04/22/2016 Total Solids * 2.09 20900 100.0 JM 04/20/2016 13:45 SM-2540G Moisture * 97.91 -100.0 JM 04/20/2016 13:45 SM-254OG Total Kjeldahl Nitrogen 5.65 56500 10.0 JM 04/21/2016 09:20 SM-4500-NH3C-TKN Total Phosphorus 1.54 15400 100 KM 04/21/2016 11:14 SW 6010C Total Potassium 0.28 2830 100 KM 04/21/2016 11:14 SW 6010C Total Sulfur 1.42 14200 100 KM 04/21/2016 11:14 SW 6010C Total Calcium 1.17 11700 100 KM 04/21/2016 11:14 SW 6010C Total Magnesium 0.26 2640 100 KM 04/21/2016 11:14 SW 6010C Total Sodium 0.70 7040 100 KM 04/21/2016 11:14 SW 6010C Total Iron - 15100 100 KM 04/21/2016 11:14 SW 6010C Total Aluminum 23000 100 KM 04/21/2016 11:14 SW 6010C Total Manganese 430 5 KM 04/21/2016 11:14 SW 6010C Total Copper 516 5 KM 04/21/2016 11:14 SW 6010C Total Zinc 857 5 KM 04/21/2016 11:14 SW 6010C Ammonia Nitrogen 0.77 7660 10.0 JM 04/21/2016 09:20 SM-4500-NH3C Organic N 4.88 48840 10.0 04/21/2016 09:20 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 04/21/2016 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 04/21/2016 11:14 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made (� to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 16-111-0203 Account Number: 00015 Submitted By: DREW CULP Send To: SYNAGRO CENTRAL/MT HOLLY WAYNE BRADY 12701 LANCASTER HWY PINEVILLE , NC 28134 Lab Number: 56806 Sample Id: 2ND EVENT Waypointo ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: MT HOLLY WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/19/2016 09:30:00 Date Received: 04/20/2016 00:00 Date Reported: 04/22/2016 Total Chromium 258 5 KM 04/21/2016 11:14 SW 6010C Total Nickel 24 5 KM 04/21/2016 11:14 SW 6010C Total Lead 36 5 KM 04/21/2016 11:14 SW 6010C Total Arsenic <3.0 3.0 KM 04/21/2016 11:14 SW 6010C Total Mercury 1.0 0.4 KM 04/21/2016 09:00 SW-7471B Total Selenium <5.0 5.0 KM 04/21/2016 11:14 SW 6010C pH (Standard Units) * 7.37 2.00 JM 04/21/2016 09:29 SW-9045D Total Molybdenum 6 5 KM 04/21/2016 11:14 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "As", "Cr", "Fe", "Pb", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 4/19/2016 41112016-7/31/2016 2.2056 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (7040 x 2.0900) = 100 = 147.136 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11700 x 2.0900) = 100 = 244.53 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2640 x 2.0900) = 100 = 55.176 Na meq = Na mg/I = Molec.Wgt.Na = 147.136 _ 23 = 6.39722 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 244.53 _ 20 = 12.2265 Mg meq = Mg mg/I = Molec.Wgt.Mg = 55.176 _ 12 = 4.598 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.39722 _ SgrRoot[0.5(12.2265+4.598)] = 2.20564 Printed: 1/25/2017 Page 1 11:59 Page: 1 of 2 Report Number: 16-211-0218 Account Number: 00015 Submitted By: Drew Culp Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 58651 Sample Id : 3rd event • Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: Mt Holly WWTP NC Cert#257 REPORT OF ANALYSIS Date Sampled: 7/28/2016 09:00:00 Date Received: 07/29/2016 00:00 Date Reported: 08/05/2016 Total Solids * 1.90 19000 100.0 JM 07/29/2016 14:15 SM-2540G Moisture * 98.10 100.0 JM 07/29/2016 14:15 SM-2540G Total Kjeldahl Nitrogen 5.00 50000 10.0 JM 08/02/2016 09:35 SM-4500-NH3C-TKN Total Phosphorus 1.35 13500 100 km 08/01/2016 13:27 SW 6010C Total Potassium 0.19 1860 100 km 08/01/2016 13:27 SW 6010C Total Sulfur 1.52 15200 100 km 08/01/2016 13:27 SW 6010C Total Calcium 1.09 10900 100 km 08/01/2016 13:27 SW 6010C Total Magnesium 0.25 2490 100 km 08/01/2016 13:27 SW 6010C Total Sodium 0.60 6010 100 km 08/01/2016 13:27 SW 6010C Total Iron 15600 100 km 08/01/2016 13:27 SW 6010C Total Aluminum 28700 100 km 08/01/2016 13:27 SW 6010C Total Manganese 439 5 km 08/01/2016 13:27 SW 6010C Total Copper 548 5 km 08/01/2016 13:27 SW 6010C Total Zinc 881 5 km 08/01/2016 13:27 SW 6010C Ammonia Nitrogen 1.05 10500 10.0 JM 08/02/2016 09:35 SM-4500-NH3C Organic N 3.95 39500 10.0 08/02/2016 09:35 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 08/01/2016 08:50 SM-450ONO3F All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 6wm 4LOur reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , to the work, the results, or the company In any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-211-0218 Account Number: 00015 Submitted By: Drew Culp Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 D Waypoin(t," ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Mt Holly WWTP NC Cert#257 REPORT OF ANALYSIS Date Sampled: 7/28/2016 09:00:00 Lab Number: 58651 Date Received: 07/29/2016 00:00 Sample Id : 3rd event Date Reported: 08/05/2016 PARAMETER RESULT RESULT QUANTITATION METHOD Total Cadmium <2.0 2.0 km 08/01/2016 13:27 SW 6010C Total Chromium 298 5 km 08/01/2016 13:27 SW 6010C Total Nickel 34 5 km 08/01/2016 13:27 SW 6010C Total Lead 38 5 km 08/01/2016 13:27 SW 6010C Total Arsenic 3.0 3.0 km 08/01/2016 13:27 SW 6010C Total Mercury 1.7 0.4 CC 08/02/2016 16:05 SW-7471 B Total Selenium <5.0 5.0 km 08/01/2016 13:27 SW 6010C pH (Standard Units) * 7.39 2.00 JM 08/01/2016 08:44 SW-9045D Total Molybdenum 7 5 km 08/01/2016 13:27 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Cr", "Mo", "Na", AND "Ni". THE LCS WAS OUT OF LIMITS FOR "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "N031NO2-N", "AI", "P", "Se", "S", AND "Zn". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 7/28/2016 811/2016-9130/2016 1.8569 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (6010 x 1.9000) = 100 = 114.19 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10900 x 1.9000) _ 100 = 207.1 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2490 x 1.9000) = 100 = 47.31 Na meq = Na mg/I = Molec.Wgt.Na = 114.19 = 23 = 4.96478 Ca meq = Ca mg/I t- Molec.Wgt.Ca = 207.1 = 20 = 10.355 Mg meq = Mg mg/I = Molec.Wgt.Mg = 47.31 = 12 = 3.9425 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.96478 _ SgrRoot[0.5(10.355+3.9425)] = 1.85689 Printed: 1/25/2017 Page 1 11:59 Page: 1 of 2 Report Number: 16-273-0203 ' • Account Number: 00015 7621 Whitepine Road, Richmond, VA 23237 Submitted By: Marshall Puryear Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: Synagro Central LLC/ MT Holly Project : Mt Holly Wayne Brady NC Cert#257 12701 Lancaster Highway Pineville, NC 28134 REPORT OFANALYSIS Date Sampled: 9/26/2016 10:00:00 Lab Number: 59991 Date Received: 09/29/2016 00:00 Sample Id : Mt Holly Date Reported: 10/06/2016 PARAMETER RESULT RESULT QUANTITATION METHOD Total Solids * 1.46 14600 100.0 R D 09/29/2016 15:20 SM-2540G Moisture * 98.53 100.0 R D 09/29/2016 15:20 SM-2540G Total Kjeldahl Nitrogen 5.03 50300 10.0 JM 09/30/2016 08:50 SM-4500-NH3C-TKN Total Phosphorus 1.35 13500 100 MOS 10/03/2016 11:51 6010C Total Potassium 0.22 2200 100 MOS 10/03/2016 11:51 6010C Total Sulfur 1.65 16500 100 MOS 10/03/2016 11:51 6010C Total Calcium 1.34 13400 100 MOS 10/03/2016 11:51 6010C Total Magnesium 0.29 2940 100 MOS 10/03/2016 11:51 6010C Total Sodium 0.91 9110 100 MOS 10/03/2016 11:51 6010C Total Iron 16300 100 MOS 10/03/2016 11:51 6010C Total Aluminum 20200 100 MOS 10/03/2016 11:51 6010C Total Manganese 510 5.00 MOS 10/03/2016 11:51 6010C Total Copper 578 5.00 MOS 10/03/2016 11:51 6010C Total Zinc 898 5.00 MOS 10/03/2016 11:51 6010C Ammonia Nitrogen 0.95 9520 10.0 JM 09/30/2016 08:50 SM-4500-NH3C Organic N 4.08 40780 10.0 09/30/2016 08:50 CALCULATION Nitrate+Nitrite-N <5.42 5.42 SJB 09/30/201614:17 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , me'� to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-273-0203 Account Number: 00015 Submitted By: Marshall Puryear Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville, NC 28134 Lab Number: 59991 Sample Id : Mt Holly o Waypoint.� ANALYTICAL Project : Mt Holly NC Cert#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 9/26/2016 10:00:00 Date Received: 09/29/2016 00:00 Date Reported: 10/06/2016 Total Cadmium <2.00 2.00 MOS 10/03/2016 11:51 6010C Total Chromium 328 5.00 MOS 10/03/2016 11:51 6010C Total Nickel 26.0 5.00 MOS 10/03/2016 11:51 6010C Total Lead 50.7 5.00 MOS 10/03/2016 11:51 6010C Total Arsenic <3.00 3.00 MOS 10/03/2016 11:51 6010C Total Mercury 1.20 0.400 JM 10/03/2016 12:00 SW-7471B Total Selenium <5.00 5.00 MOS 10/03/2016 11:51 6010C pH (Standard Units) * 7.51 JM 09/30/2016 09:25 SW-9045D Total Molybdenum <5.00 5.00 MOS 10/03/2016 11:51 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 9/26/2016 1011/2016-1213112016 2.2375 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (9110 x 1.4600) - 100 = 133.006 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (13400 x 1.4600) _ 100 = 195.64 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2940 x 1.4600) _ 100 = 42.924. Na meq = Na mg/I _ Molec.Wgt.Na = 133.006 _ 23 = 5.78287 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 195.64 _ 20 = 9.782 Mg meq = Mg mg/I + Molec.Wgt.Mg = 42.924 _ 12 = 3.577 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.78287 _ SgrRoot[0.5(9.782+3.577)] = 2.23754 Printed: 1/25/2017 Page 1 11:59 FACILITY NAME: MOUNT HOLLY, NC OWNER: GREG SPRINGS SITE #: NC GA 00041 FIELD# : GA 00041 0006 RESIDUAL SOURCE(S):* See list at bottom of report _]ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 16.70 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90 Page: 1 Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 A li cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN m (pp ) Crop Total Per Acre 9/12/16 124,000.00 (G) 13932.584 1.90 1.104 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 17102 I FESCUE 9/13/16 74,400.00 (G) 8359.551 1.90 0.662 MIIAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p p 2.00 17102 I FESCUE 9/15/16 12,400.00 (G) 1393.258 1.90 0.110 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p p 2.00 p 17102 FESCUE Sep-16 1 210,800.00 (G) 23,685.393 Total Gallons/Ac: 23,685.39 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 64 0.011 0.008 1.118 2.057 0.143 0.006 0.026 0.128 0.019 3.307 50.67 Cumulative Ibs/acre 0.051 0.032 4.700 9.081 0.579 0.021 0.128 0.484 0.087 13.319 Permit PAN Limit (lbs/acre) lst Crop/2nd Crop i , i 1 r, s is t �1 z s° f sr s t + i 209 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1 1339.0 267.9 15.0 ' ` l 375.0 89.0 2500.0 i s MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID . &M 9"�" V - - a- (0- 9,01-4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: GREG SPRINGS PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 9.83 SITE #: NC GA 00041 FIELD# : GA 00041 0010 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page : 1 Lane Applied *** Date +_Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Solid s Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKI�I Ammonia Nitrogen Nitrate and PAN (ppm ) Crop p Total Per Acre 9/13/16 31,000.00 (G) 3924.051 1.90 0.311 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p F 17102 I FESCUE 9/14/16 68,200.00 (G) 8632.911 1.90 0.684 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p 17102 FESCUE 9/15/16 24,800.00 (G) 3139.241 1.90 0.249 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p 17102 FESCUE Sep-16 1 124,000.00 (G) 15,696.203 brat uauonsiac: 1S,696.111 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 43 0.007 0.005 0.741 1.363 0.095 0.004 0.017 0.085 0.012 2.191 33.58 Cumulative lbs/acre 0.033 0.022 3.339 6.504 0.404 0.014 0.092 0.335 0.059 9.397 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop q i 209 t FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 (, 375.0 89.0 2500 0 f 9 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID x &A qL 2t" Lq- IF - 1 -4 (SIGNATURE OF LAND APPLIER) V DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, IN7 -Injection, SUR1N -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: GREG SPRINGS PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 10.81 SITE #: NC GA 00041 FIELD# : GA 00041 0014 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80 Page Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Solids Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN m (pp ) Crop p Total Per Acre 9/13/16 37,200.00 • (G) 5470.588 1.90 0.433 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p 17102 I FESCUE 9/14/16 74,400.00 (G) 10941.176 1.90 0.867 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p 17102 I FESCUE 9115116 24,800.00 (G) 3647.059 1.90 0.289 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,000. p 10,500.00 p 2.00 p 17102 FESCUE Sep-16 1 136,400.00 (G) 20,058.823 iotat vauons/Ac: zu,u.smu TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Anttuallbs/acre 54 0.010 0.006 0.947 1.742 0.121 0.005 0.022 0.108 0.016 2.800 42.91 Cumulative lbs/acre 0.036 0.023 3.709 7.038 0.448 0.016 0.100 0.371 0.063 10.372' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop e p� �� } �' i C '� f °'i 209 ! FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 I15.0 1339.0 267.9 375.0 89.0 I c ,LLy 4, MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID X ok qo(,"f,�4 9_-(,0-r4 (SIGNATURE OF LAND APPLIER) T DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD OWNER: DAVID ALLEN PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 28.64 SITE #: NC GA 00045 FIELD# : GA 00045 0001 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page Lane Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre 6/13/16 105,400.00 (G) 6200.000 2.09 0.540 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 I FESCUE 6/14/16 86,800.00 (G) 5105.882 2.09 0,445 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 Ij FESCUE 6/16/16 136,400.00 (G) 8023.529 2.09 0.699 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18414 FESCUE Jun-16 1 328,600.00 (G) 1 19,329.411 1 1 otai liaisons/Ac: 19,SLY.41 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 62 0.010 0.007 0.869 1.739 0.121 0.003 0.020 0.081 0.017 2.887 51.89 Cumulative Ibs/acre 71, 0.017 0.012 1.621 3.142 0.224 0.007 0.032 0.140 0.029 4.915 t — Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop _ 4��' .-, ' �� I :� J 216 ri FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 tI MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID X9-(0-r-7 (SIGNATURE OF LAND APPLIER) 61 DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 35.41 SITE #: NC LT 00046 FIELD# : LT 00046 0001 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % . ons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Solids P r Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm ) Crop p Total 3/ Per Acre MONTH 3/24/16 31,000.00 (G) 26 1 9 3.01 0 30 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 I FESCUE 3/25/16 148,800.00 (G) 12610.1 9 3.01 .583 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 I FESCUE 3/29/16 24,800.00 (G) 210 .6 5 3.01 0.264 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16100 FESCUE Mar-16 204,600.00 (G) 17,338.98 6/17/16 12,400.00 (G) 1050.847 2.09 0.092 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 I FESCUE 6/20/16 99,200.00 (G) 8406.780 2.09 0.733 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 FESCUE Jun-16 111,600.00 (G) 9,457.627 I otal Gallons/Ac: 26,796.61 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 103 0.018 0.012 1.544 2.923 0.220 0.006 0.032 0.135 0.030 4.756 88.50 Cumulative Ibs/acre 0.041 0.027 3.436 6.285 0.450 0.014 0.070 0.317 0.068 9.500 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 17 t T'Ik 209 yti FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0it MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID \R OF r.ANn APPLIER) DATE f law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." - Not Required % = percent p = ppm or mg/kg NJ - Injection, SURIN - Incorporation ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 23.03 SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20 Page Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN m (pp ) Crop p Total Per Acre 11/15/16 111,600.00 (G) 2469.027 1.46 0.150 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,300.p 9,520.00 p 5.42 p 16999 I FESCUE 11/16/16 155,000.00 (G) 3429.204 1.46 0.209 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,300.p - 9,520.00 p 5.42 p 16999 FESCUE 11/17/16 111,600.00 (G) 2469.027 1.46 0.150 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,300.p 9,520.00 p 5.42 p 16999 FESCUE Nov-16 378,200.00 (G) 8,367.258 1 ULUI UdIlUllb/11 . 0,JU-/.Lb TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 17 0.003 0.002 0.334 0.589 0.052 0.001 0.005 0.027 0.005 0.915 13.75 Cumulative lbs/acre 0.358 0.071 5.834 30.163 2.049 0.064 0.335 1.363 0.156 36.742 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop; r R -'� 7,77 1` 209 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 ' ' 15 0 375.0 89.0 2500.0 ,. MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID x &8 (SIGNATURE Oq LAND APPLIER) 4f DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 30.80 SITE #: NC LT 00046 FIELD# : LT 00046 0003 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - Tons Cond. Precip. cation tilt- ali- Ammonia Nitrate PAN DATE or MONTH SoiidS Pb Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Total Per Acre 3/23/16 124,000.00 (G) 12525. 3 3.01 1.5172 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 FESCUE 3/24/16 31,000.00 (G) 3131 13 3.01 9293 MHAEDL DRY 0-<I/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 FESCUE Mar-16 ' 155,000.00 (G) 15,656. 6 6/17/16 86,800.00 (G) 8767.677 2.09 0.764 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 I FESCUE 6/20/16 43,400.00 (G) 4383.838 2.09 0.382 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18414 FESCUE Jun-16 130,200.00 (G) 13,151.515 total tJanons/Ac: L2i,bus.ub TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 108 0.019 0.012 1.602 3.054 0.228 0.007 0.033 0.141 0.031 4.983 92.29 Cumulative lbs/acre 0.048 0.032 3.964 7.238 0.513 0.016 0.082 0.372 0.080 10.860 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop ;. 2 09 lay' FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 ' 15 0 `i 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID 11 q -7 X ',IGNATURYOF LAND APPLIER) U DATE -1-tify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and ated the information submitted. I am aware that there are significant penalties for submitting false infornation, including the possibility of fines and imprisonment for Icnowing violations." )rted or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ace, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 14.72 SITE #: NC LT 00046 FIELD# : LT 00046 0004 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):"` See list at bottom of report ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Total Per Acre Solids Per Residual Dry, Wet, Past 24 Method zation zation TI{N Nitrogen and (pprn ) Crop p i�io.»i 1.4b U•U16 1VIMAU LKx U-11/L" JUK u.c u.su cusuu.p y,JLU.UU p 5.42 p 16999 FESCUE 11/18/16 124,000.00 (G) 6391.753 1.46 0.389 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,300. p 9,520.00 p 5.42 p 16999 I FESCUE 11/21/16 93,000.00 (G) 4793.814 1.46 0.292 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 50,300. p 9,520.00 p 5.42 p 16999 FESCUE Nov-16 241,800.00 (G) 12,463.918 Total Gallons/Ac: 12,463.92 TOTALS: As Cd Cr Cu Ph Hg Mo Ni Se Zn P PAN Annual lbs/acre 26 0.005 0.003 0.498 0.877 0.077 0.002 0.008 0.039 0.008 1.363 20.49 Cumulative Ibs/acre 0.133 0.070 4.397 40.045 1.649 0.084 0.451 1.531 0.152 36.233 ::. f :! Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop " 1 1 s 209 J FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89:0 2500.0 MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID X Q1-4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 FACILITY NAME: MOUNT HOLLY, NC OWNER: TONY JONES SITE #: NC LT 00046 FIELD# : LT 00046 0007 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: PACOLET PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 8.56 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 7.00 ACRES PERMITTED: 7.00 Page 'Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - DATE or o Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total Per Acre/ MONTH ! -� SolI ss per Residual Dry, Wet, Past 24 Method zation zation TKN Nitro en g and m (pp ) Crop \ 3/29/16 68,200.00 (G) 9742� 57 3.01 1.21 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 52,600.p 4,590.00 p 2.00 p 16700 FESCUE Mar-16 68,200.00 (G) 9,742.857 iuLal vaucus/tic. Y,/ JL.bU TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Za P PAN Annuallbs/acre 41 0.007 0.005 0.629 1.164 0.090 0.003 0.012 0.054 0.012 1.878 35.46 Cumulative lbs/acre 0.030 0.020 2.436 4.364 0.309 0.009 0.050 0.229 0.050 6.257 J -,' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop it 188 ic T" FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 ;; 1 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "T - "Ify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and d the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = N-' Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 20.02 SITE #: NC LT 00046 FIELD# : LT 00046 0008 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or MONTH Total Per Acr/ s j er Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop 3/24/16 62,000.00 (G) 9393.939 3.01 1.179 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 I FESCUE 3/25/16 37,200.00 (G) 5636.36 3.01 0.707 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 52,600. p 4,590.00 p 2.00 p 16700 FESCUE Mar-16 99,200.00 (G) 15,030.30 , _ 6/17/16 43,400.00 (G) 6575,758 2.09 0.573 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 I FESCUE 6/20/16 43,400.00 (G) 6575.758 2.09 0.573 MHAEDL DRY 0-<1/2" SUR 0.5 0.30 56,500. p 7,660.00 p 2.00 p 18484 FESCUE Jun-16 86,800.00 (G) 13,151.516 1 ULal vallonS/Ac: AZs,-L6i.6Z TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 105 0.018 0.012 1.561 2.979 0.222 0.006 0.033 0.138 0.030 4.862 90.01 Cumulative lbs/acre 0.048 0.032 3.994 7.289 0.516 0.016 0.083 0.375 0.080 10.898 s, Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ' y I = s 209 { 4 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID 'LAND APPLIER) DATE alty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and �tion submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." t or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017 Summit Environmental Technologies, Inc. JO 3310 Win St. f--UVlR0t4folP,'TALTF:CHNOLOGIEs;,Yy Cuyahoga Falls, Ohio44223 Arralyrcal Lsbarainaaa, TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httn://www.settek.com May 03, 2016 Drew Culp/Reports&Invoices Synagro, NC 28134 12701 Lancaster Hwy Pineville, NC 28134 TEL: 704-752-8673 FAX: (704) 752-8736 RE: MT Holly WWTP Dear Drew Culp/Reports&Invoices: Order No.: 16021266 Summit Environmental Technologies, Inc. received 1 sample(s) on 2/19/2016 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Bachar Najm Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Region 8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 30 Summit Environmental Technologies, Inc. Case Narrative summrr 3310 Win St. FUVIRONNIEt,!tALIECW40LaG,155: utc. Cuyahoga Falls, Ohio 44223 WO#: 16021266 Ara;,ftir_a1 L:yi eraiur+e TEL: (330) 253-8211 FAX: (330) 253-4489 Website: htty.-1Avivw.settek.com Date: 5/3/2016 CLIENT: Synagro, NC 28134 Project: MT Holly WWTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway Haddock, GA 31033 All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. The information contained in,this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency. Any comments or problems with the analytical events associated with this report are noted below. Analytical Comments for SVOC-BNA TCLP(8270), Sample LCS-18991, Batch ID 18991 : The TCLP SVOC LCS (Batch 18991) exhibited high recovery for Surrogate: 2,4,6-Tribromophenol; All other Revision v2 Page 2 of 30 Summit Environmental Technologies, Inc. Case Narrative SUMMAIT 3310 Win St. MVIzOMMEXIMLIECSNOLOG1ES,W(7. Cuyahoga Falls, Ohio44223 WO#: 16021266 Anai,.tii7al Ln1' araT"Or1eq TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hyp:Uwww.settekcom Date: 5/3/2016 CLIENT: Synagro, NC 28134 Project: MT Holly WWTP surrogates exhibited recoveries within Acceptance Limits. Analytical Comments for tclp-svoc-herb_tclp(8151), Sample les-19008, Batch ID 19008 : The TCLP Herbicides LCS (Batch 19008) exhibited high recovery for 2,4-D; All samples were ND. Analytical Comments for TCLP-SVOC-Herb_TCLP(8321), Sample LCSD-R50514, Batch ID R50514 : The TCLP Herbicides LCSD (Batch 50514) exhibited outlying recoveries and RPDs; Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCSD-R50630, Batch ID R50630 : The TCLP Herbicides LCSD (Batch R50630) exhibited high recoveries; All samples were ND. Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCS-R50630, Batch ID R50630: The TCLP Herbicides LCS (Batch R50630) exhibited high recoveries; All samples were ND. Revision v2 Page 3 of 30 Summit Environmental Technologies, In Qualifiers and Acronyms fT sumMIT 3310 Win 5 UAI ROWENTAL IZ'-H IOLO Tics, INC. Cuyahoga Falls, Ohio 442� WO#: 16021266 Angly cal Lzboratorlez. TEL: (330) 253-8211 FAX.- (330) 253-446 Website: htto://wivw.settekco. Date: 5/3/2016 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GUMS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL ' Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Revision v2 Page 4 of 30 Summit Environmental Technologies, Inc. Workorder S IF 3310 Win St. FIRVIR010,1E11,JYi13_r cir]La�;_s; ;pt�. Cuyahoga Falls, Ohio 44223 Sample Summary l'ir,.afyticsf LEbaraform". TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 16021266 Website: hgpa/www.settekcom 03 May-16 CLIENT: Synagro, NC 28134 Project: MT Holly WWTP Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix 16021266-001 MT. Holly WWTP 2/18/2016 2/19/2016 9:30:00 AM Sludge Page 5 of 30 fr!SUMMIT Summit Enviroi7mental Technologies, Inc. Analytical Report 3310 Win St. `VIFONMENTALT_CIt OLaml :wi,-_ Cuyahoga Falls, Ohio44223 (base report) Arralvtri73i Laf orafones TEL: (330) 253-8211 FAX.' (330) 253-4489 WO#: 16021266 Website: hyp.-11wiv19.settek.com Date Reported: 5/3/2016 CLIENT: Synagro, NC 28134 Tag Number: Matrix: SLUDGE Collection Date: 2/18/2016 Lab ID: 16021266-001A Project: MT Holly WWTP Client Sample ID MT. Holly WWTP Analyses Result RL Qual Units DF Date Analyzed RCI SW9045D Analyst: DHC PH (SW9045D) pH 6.77 s.u.@20.3C 1 2/26/2016 3:59:00 PM Qualifiers: ` Value exceeds Maximum Contaminant Level. E Value above quamitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Revision v2 R RPD outside accepted recovery limits RL Reporting Detection Limit U Samples with CalcVal <MDL Page 6 of 30 summloff- Summit Environmental Technologies, Inc. WO#: 16021266 rNVIR7NhIENIAL1.2cW40LZG;=5,zht: 3310 Win St. Cuyahoga Falls, Ohio44223 Date Reported: 5/3/2016 I.r:alvtir-sl Laboratories TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro, NC 28134 Website: htto:/hmwiv.settek.com Address: 12701 Lancaster Hwy Pineville NC 28134 Received: 2/19/2016 Project#: MT Holly WWT TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 TCLP Arsenic(As) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Barium(Ba) 5.00 ND mg/L Sludge EPA 6010 C 1 100 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Cadmium(Cd) 0.100 ND mg/L Sludge EPA 6010 C 1 1.00 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Chromium(Cr) 0.200 ND mg/L Sludge EPA 6010 C 1 5.00 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Lead(Pb) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Selenium(Se) 0.500 ND mg/L Sludge EPA 6010 C 1 1.00 2/29/2016 VVK MT. Holly WWTP 001 2/18/2016 TCLP Silver(Ag) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 2/29/2016 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 TCLP Mercury 0.00200 ND mg/L Sludge EPA 7470 A 1 0.200 2/29/2016 MFW SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 Chlordane, total 0.0250 ND mg/L Sludge EPA 8081 B 1 0.0300 2/29/2016 JBN MT. Holly WWTP 001 2/1812016 Toxaphene 0.0500 ND mg/L Sludge EPA 8081 B 1 0.500 2/29/2016 JBN MT. Holly WWTP 001 2/18/2016 Endrin 0.00250 ND mg/L Sludge EPA 8081 B 1 0.0200 2/29/2016 JBN MT. Holly WWTP 001 2/18/2016 gamma-BHC 0.00250 ND mg/L Sludge EPA 8081 B 1 0.400 2/29/2016 JBN MT. Holly WWTP 001 2/18/2016 Heptachlor 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/29/2016 JBN MT. Holly WWTP 001 2/18/2016 Heptachlor epoxide 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 2/29/2016 JBN MT. Holly WWTP 001 2/18/2016 Methoxychlor 0.00250 ND mg/L Sludge EPA 8081 B 1 10.0 2/29/2016 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 1,1-Dichloroethene 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 1,2-Dichloroethane 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 MEK 2.00 ND mg/L MT. Holly WWTP 001 2/18/2016 Benzene 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Carbon tetrachloride 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Chlorobenzene 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Chloroform 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Tetrachloroethene 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Trichloroethene 0.100 ND mg/L MT. Holly WWTP 001 2/18/2016 Vinyl chloride 0.200 ND mg/L Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 0.700 2/26/2016 MES 0.500 2/26/2016 MES 200 2/26/2016 MES 0.500 2/26/2016 MES 0.500 2/26/2016 , MES 100 2/26/2016 MES 6.00 2/26/2016 MES 0.700 2/26/2016 MES 0.500 2/26/2016 MES 0.200 2/26/2016 MES Page 7 of 30 � - Summit Environmental Technologies, Inc. 3310 Win St. WO#: 16021266 P,IVIRONMEW6iLIECHNOLGGES. ;NtM Cuyahoga Falls, Ohio44223 Date Reported: 5/3/2016 etr H ytlr_at Laboratories TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro, NC 28134 Website: httP.-hivww.settek.com Address: 12701 Lancaster Hwy Pineville NC 28134 Received: 2/19/2016 Project#: MT Holly WWT SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 1,4-Dichlorobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 7.50 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 2,4,5-Trichlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 400 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 2,4,6-Trichlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 2.00 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 2,4-Dinitrotoluene 0.100 ND, mg/L Sludge EPA 8270 C 2 0.130 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Cresols, Total 10.0 ND mg/L Sludge EPA 8270 C 2 200 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Hexachloro-1,3- 0.100 ND mg/L Sludge EPA 8270 C 2 0.500 2/29/2016 CxA butadiene MT. Holly WWTP 001 2/18/2016 Hexachlorobenzene 0.100 ND mg/L Sludge EPA 8270 C 2 0.130 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Hexachloroethane 0.200 ND mg/L Sludge EPA 8270 C 2 3.00 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Nitrobenzene 0.200 ND mg/L Sludge EPA 8270 C 2 2.00 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Pentachlorophenol 0.500 ND mg/L Sludge EPA 8270 C 2 100 2/29/2016 CxA MT. Holly WWTP 001 2/18/2016 Pyridine 0.500 ND mg/L Sludge EPA 8270 C 2 5.00 2/29/2016 CxA SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst MT. Holly WWTP 001 2/18/2016 2,4-D 5.00 ND mg/L Sludge EPA 8321 A 1 10.0 3/4/2016 BJH MT. Holly WWTP 001 2/18/2016 2,4,5-TP 0.500 ND mg/L Sludge EPA 8321 A 1 1.00 3/4/2016 BJH Page 8 of 30 Summit Environmental Technologies, Inc. WO#: 16021266 WJ -, 3310 Win St. FES* y RNIVRONMENShLIEC-8W)LbutES,JNr, Cuyahoga Falls, Ohio44223 Date Reported: 5/3/2016 Arar f.cal Lzilorarorles TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro, NC 28134 Website: htto://1vww.settek.com Address: 12701 Lancaster Hwy Pineville NC 28134 Received: 2/19/2016 Project#: MT Holly WWT Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst MT. Holly VVWTP 001 MT. Holly WVVTP 001 MT. Holly WVVTP 001 2/18/2016 Flashpoint (140°F) 2/18/2016 Cyanide, Reactive 2/18/2016 Sulfide, Reactive >140 °F Sludge EPA 1010 1 2/22/2016 TAH ND mg/Kg Sludge EPA 9014 1 0.500 2/26/2016 MS ND mg/Kg Sludge EPA 9034 1 25.0 2/26/2016 MS Page 9 of 30 Summit Environmental Technologies, Inc. 14"oftolhirt 3310Win St. QC SUMMARY REPORT E:-NNI UNPUNIP,l. I I.i.3 ?&1L(t1J1!z'a.ING, Cuyahoga Falls, Ohio44223 WO#: 16021266 Anattdl.cai Laborwurie� TEL: (330) 253-8211 FAX- (330) 253-4489 Website: hUp:/hvww.sette1ccom 03 May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18975 Sample ID MB-18975 SampType: MBLK TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 212912016 RunNo: 50370 client ID: PBW Batch ID: 18975 TestNo: SW6010C SW3010A Analysis Date: 2/2912016 SegNo: 790118 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) ND 0.500 TCLP Barium(Ba) ND 5.00 TCLP Cadmium(Cd) ND 0.100 TCLP Chromium(Cr) ND 0.200 TCLP Lead(Pb) ND 0.500 TCLP Selenium(Se) ND 0.500 TCLP Silver(Ag) ND 0.500 Sample ID LCS-18975 SampType: LCS TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 212912016 RunNo: 50370 'lient ID: LCSW Batch ID: 18975 TestNo: SW6010C SW3010A Analysis Date: 212912016 SegNo: 790119 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.10 0.500 2.000 0 105 80 120 TCLP Barium(Ba) ND 5.00 2.000 0 105 80 120 TCLP Cadmium(Cd) 2.06 0.100 2.000 0 103 80 120 TCLP Chromium(Cr) 2.01 0.200 2.000 0 101 80 120 TCLP Lead(Pb) 2.10 0.500 2.000 0 105 80 120 - TCLP Selenium(Se) 2.10 0.500 2.000 0 105 80 120 TCLP Silver(Ag) 0.920 0.500 1.000 0 92.0 80 120 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 10 of 30 Sununit Environmental Technologies, Inc. C SUMMARY REPORT 3310 Win St. `� �:wlHarar+naNl+�J. wa:r.a�€attLu�tl a; Inr.ti. Cuyahoga Falls, Ohio44223 WO#: 16021266 ff1summm l.�ai1 fi.caf Lab r so,rtt�s TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto:/hvtvw.settefc.coni 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18981 Sample ID 16021355-001AMS SampType: MS TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/29/2016 RunNo: 50368 Client ID: BatchQC Batch ID: 18981 TestNo: SW7470A SW7470A Analysis Date: 2/2912016 SegNo: 790066 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ TCLP Mercury 0.00419 0.00200 0.00400 0 105 75 125 Sample ID 16021355-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/2912016 RunNo: 50368 Client ID: BatchQC Batch ID: 18981 TestNo: SW7470A SW7470A Analysis Date: 2/29/2016 SegNo: 790067 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00415 0.00200 0.00400 0 104 75 125 0.00419 0.959 20 Sample ID MB-18980 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/29/2016 RunNo: 50368 Client ID: PBW Batch ID: 18981 TestNo: SW7470A SW7470A Analysis Date: 2/2912016 SegNo: 790128 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ TCLP Mercury ND 0.00200 Sample ID LCS-18980 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/29/2016 RunNo: 50368 Client ID: LCSW Batch ID: 18981 TestNo: SW7470A SW7470A Analysis Date: 2/29/2016 SegNo: 790129 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00403 0.00200 0.00400 0 101 80 120 Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit P Second column confirmation exceeds PL Permit Limit E Value above quantitation range M Manual Integration used to determine Revision V2 O RSD is greater than RSDlimit R RPD outside accepted recovery limits Page 11 of 30 Summit Environmental Technologies, Inc. QC SUMMARY REPORT 1; JM , 3310 Win St. IHV'Nrrn,N I RL 91-.CIl-la-dULSJJItti,, INC Cuyahoga Falls, Ohio 44223 WO#: 16021266 Ana.tvUraf l ,Thorato,rir=s TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto://wivw.setteh.com 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18981 Sample ID LCS-18980 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/29/2016 RunNo: 50368 DI]ent ID: LCSW Batch ID: 18981 TestNo: SW7470A SW7470A Analysis Date: 2/29/2016 SegNo: 790129 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighUrnit RPD Ref Val %RPD RPDLimit Qua] Qualifiers: " Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 12 of 30 i 1 Sumnsit Environmental Technolo res, Inc. 3310 Win St. QC SUMMARY REPORT LMYIH.0 Nb71; P, L.N. d d.C.` TAJLWJI1 :Si, JPtC. Cuyahoga Falls, Ohio 44223 WO#: 16021266 k, t rtlril.cai L;Tbo,rsto�Fe.. TEL: (330) 253-82I J FAX.(330) 253-4489 Website: htm:/hvwiv.setlek.conz 03-May-16 Client: Synagro, NC 28134 Projeet: MT Holly WWTP BatehID: 18984 Sample ID mb-18984 SampType: mblk TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 2/29/2016 RunNo: 50380 I Client ID: PBW Batch ID: 18984 TestNo: SW8081A SW3610C Analysis Date: 2/2912016 SegNo: 790297 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Chlordane, total ND 0.0250 Toxaphene ND 0.0500 Endrin ND 0.00250 gamma-BHC ND 0.00250 eptachlor ND 0.00250 Heptachlor epoxide ND 0.00250 Methoxychlor ND 0.00250 Sample ID Ics-18984 SampType: Ics TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 2/29/2016 RunNo: 50380 Client ID: LCSW Batch ID: 18984 TestNo: SW8081A SW3510C Analysis Date: 2/29/2016 SegNo: 790298 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 0.0286 0.00250 0.0250 0 115 20 157 C 0.0223 0.00250 0.0250 0 89.4 22 137 0.0257 0.00250 0.0250 0 103 24 121 epoxide 0.0259 0.00250 0.0250 0 104 27 152 or 0.0303 0.00250 0.0250 0 121 1 199 * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine Revision v2 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Page 13 of 30 F� wd Summit Environmental Technologies, Inc. QC SUMMARY REPORT MIT 3310 Win St. e ra:ulH,4aaru;r i.al. r:a�nar�auU rts; IRC Cuyahoga Falls, Ohio 44223 WO#: 16021266 naayrth.,z L baratrarte� TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hgp.-Iliviv3v.settelf.com 03-11ay-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18984 Sample ID 16021331-001ams SampType: ms TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 212912016 RunNo: 50380 :lient ID: BatchQC Batch ID: 18984 TestNo: SW8081A SW3510C Analysis Date: 2/2912016 SegNo: 790299 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Endrin 0.0278 0.00250 0.0250 0 ill 20 157 gamma-BHC 0.0214 0.00250 0.0250 0 85.5 22 137 Heptachlor 0.0212 0.00260 0.0250 0 84.9 24 121 Heptachlor epoxide 0.0246 0.00250 0.0250 0 98.5 27 152 Methoxychlor 0.0274 0.00250 0.0250 0 110 1 199 'ample ID 16021331-001amsd SampType: msd TestCode: telp-svoc-cpe Units: mg/L Prep Date: 2/29/2016 RunNo: 50380 'lient ID: BatchQC Batch ID: 18984 TestNo: SW8081A SW3510C Analysis Date: 212912016 SegNo: 790300 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Endrin 0.0218 0.00250 0.0250 0 87.1 20 157 0.0278 24.2 30 gamma-BHC 0.0179 0.00250 0.0250 0 71.4 22 137 0.0214 17.9 30 Heptachlor 0.0173 0.00250 0.0250 0 69.2 24 121 0.0212 20.3 30 Heptachlor epoxide 0.0195 0.00250 0.0250 0 77.9 27 152 0.0246 23.4 30 Methoxychlor 0.0212 0.00250 0.0250 0 84.6 1 199 0.0274 25.7 30 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 14 of 30 -7�,:Zr. pw Summit Environmental Technologies, Inc. C SUMMARY REPORT 3310 Win ,St. er<: INV P•ann:N J,AJ, 4 1atPNUL.r1J1t51 lh: Cuyahoga Falls, Ohio 44223 WO#: 16021266 Anal 1Phw-i1 L7boratarke:� TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htm✓/wwiv.setteh.com 03-May-I6 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18991 Sample ID MB-18991 SampType: MBLK TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50394 client ID: PBW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790622 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDL]mit Qua[ 1,4-Dichlorobenzene ND 0.100 2,4,5-Trichlorophenol ND 0.250 2,4,6-Trichlorophenol ND 0.250 2,4-Dinitrotoluene ND 0.0200 Cresols, Total ND 5.00 Hexachloro-1,3-butadiene ND 0.0200 Hexachlorobenzene ND 0.0200 Hexachloroethane ND 0.100 Nitrobenzene ND 0.100 Pentachlorophenol ND 0.250 Pyridine ND 0.250 Sample ID LCS-18991 SampType: LCS TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50394 'Iient ID: LCSW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790623 knalyte, Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,4-Dichlorobenzene 0.745 0.100 1.000 0 74.5 10 134 2,4,5-Trichlorophenol 0.992 0.250 1.000 0 99.2 27 154 2,4,6-Trichlorophenol 1.01 0.250 1.000 0 101 27 154 2,4-Dinitrotoluene 0.942 0.0200 1.000 0 94.2 29 149 Cresols, Total ND 5.00 3.000 0 55.2 20 125 Hexachloro-1,3-butadiene 0.849 0.0200 1.000 0 84.9 14 126 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine ReVIS10ri V2 MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 15 of 30 _ Summit Environmental Technologies, bzc. n ���� //�� ,�� 77�� 7� L 3310 Win St. QC SU1�11�1-tS.itY REPORT L-NNIk4"rabiwr4l.IsVLLtIH ULUUJLS,;NS::. Cuyahoga Falls, Ohio44223 WO#: 16021266 I. � 6nali Wcwf Laborworip: r TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httv:/hviviv.settek.com 03-May-I6 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID• 18991 iample ID LCS-18991 SampType: LCS TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50394 ;lient ID: LCSW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790623 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Hexachlorobenzene 0.986 0.0200 1.000 0 98.6 1 162 Hexachloroethane 0.764 0.100 1.000 0 76.4 30 123 Nitrobenzene 0.887 0.100 1.000 0 88.7 25 190 Pentachlorophenol 0.777 0.250 1.000 0 77.7 4 186 Pyridine ND 0.250 1.000 0 22.2 5 130 Sample ID 16021356-003AMS SampType: MS TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50394 :;lient ID: BatchQC Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790626 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene 0.818 0.200 1.000 D 81.8 10 134 2,4,5-Trichlorophenol ND 0.500 1.000 0 0 27 154 S 2,4,6-Trichlorophenol ND 0.500 1.000 0 0 27 154 S 2,4-Dinitrotoluene 0.987 0.0400 1.000 0 98.7 29 149 Cresols, Total ND 10.0 3.000 0 58.9 20 125 Hexachloro-1,3-butadiene 0.947 0.0400 1.000 0 94.7 14 126 Hexachlorobenzene 1.08 0.0400 1.000 0 108 1 162 Hexachloroethane 0.832 0.200 1.000 0 83.2 30 123 Nitrobenzene 0.961 0.200 1.000 0 96.1 25 190 Pentachlorophenol 0.719 0.500 1.000 0 71.9 4 186 Pyridine ND 0.500 1.000 0 43.2 5 130 QMR Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision V2 P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 16 of 30 Summit Environmental Technologies, Inc. mmsuI g QC SUMMARY REPORT 3310 Win St. L:r,A-1K,carT,1P;NIfM, 0'+:ch9Y•dauJS3tza.!NC Cuyahoga Falls, Ohio44223 WO#: 16021266 +I.rtatrti.c�i L:7Morar❑ri TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htto://www.sette%com 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18991 Sample ID 16021356-003AMSD SampType: MSD TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/2912016 RunNo: 50394 -lient ID: BatchQC Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790627 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ 1,4-Dichlorobenzene 0.722 0.200 1.000 0 72.2 10 134 0.8180 12.5 30 2,4,5-Trichlorophenol ND 0.500 1.000 0 0 27 154 0 0 30 S 2,4,6-Trichlorophenol ND 0.500 1.000 0 0 27 154 0 0 30 S 2,4-Dinitrotoluene 0.874 0.0400 1.000 0 87.4 29 149 0.9870 12.1 30 Cresols, Total ND 10.0 3.000 0 51.9 20 125 0 0 30 Hexachloro-1,3-butadiene 0.853 0.0400 1.000 0 85.3 14 126 0.9470 10.4 30 Hexachlorobenzene 0.935 0.0400 1.000 0 93.5 1 162 1.082 14.6 30 Hexachloroethane 0.749 0.200 1.000 0 74.9 30 123 0.8320 10.5 30 Nitrobenzene . 0.859 0.200 1.000 0 85.9 25 190 0.9610 11.2 30 Pentachlorophenol 0.641 0.500 1.000 0 64.1 4 186 0.7190 11.5 30 Pyridine ND 0.500 1.000 0 30.9 5 130 0 0 30 R Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine O RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 17 of 30 Summit Environmental Technologies, Inc. QC SUMMARY REPORT sumnin 3310 Win St. LMVIH)NNII;hi:u- a �a ea taLU�i�s; WC Cuyahoga Falls, Ohio44223 WO#: 16021266 ; nzaltq?-ml i_abo:rarvfies TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httU:/Avww.settelc.com 03 May-16 Client: Synagro, NC 28134 Project: NIT Holly WWTP BatchID: 18991 Sample ID LCS-18991 SampType: LCS TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50371 client ID: LCSW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790126 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 1,4-Dichlorobenzene 0.713 0.100 1.000 0 71.3 10 134 m 2,4,5-Trichlorophenol 0.996 0.250 1.000 0 99.6 27 154 2,4,6-Trichlorophenol 1.03 0.250 1.000 0 103 27 154 2,4-Dinitrotoluene 0.940 0.0200 1.000 0 94.0 29 149 Cresols, Total ND 5.00 3.000 0 55.4 20 125 Hexachloro-1,3-butadiene 0.848 0.0200 1.000 0 84.9 14 126 Hexachlorobenzene 0.986 0.0200 1.000 0 98.6 1 162 Hexachloroethane 0.764 0.100 1.000 0 76.5 30 123 m Nitrobenzene 0.887 0.100 1.000 0 88.7 25 190 Pentachlorophenol 0.790 0.250 1.000 0 79.0 4 186 Pyridine ND 0.250 1.000 0 22.2 5 130 Sample ID MB-18991 SampType: MBLK TestCode: SVOC-BNA T Units: mg/L Prep Date: 212912016 RunNo: 50371 :lient ID: PBW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790127 %nalyte Result PQL SPK value SPK Ref Val %REC LowUrnit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene ND 0.100 2,4,5-Trichlorophenol ND 0.250 2,4,6-Trichlorophenol ND 0.250 2,4-Dinitrotoluene ND 0.0200 Cresols, Total ND 5.00 Hexachloro-1,3-butadiene ND 0.0200 Qualifiers: k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision v2 P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 18 of 30 r - Summit Environmental Technologies, Inc. QC SUMMARY REPORT I , 3310 Win St. r <' Ix. rtrnav i ah I i:C,MilULQilI`S; !NiC. Cuyahoga Falls, Ohio 44223 WO#: 16021266 ArTztilrticRf La bor rwhr f TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://wtvw.settelr.cont 03 May-l6 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: 18991 Sample ID MB-18991 SampType: MBLK TestCode: SVOC-BNA T Units: mg/L Prep Date: 2/29/2016 RunNo: 50371 Client ID: PBW Batch ID: 18991 TestNo: SW8270C SW3510C Analysis Date: 2/29/2016 SegNo: 790127 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Hexachlorobenzene ND 0.0200 Hexachloroethane ND 0.100 Nitrobenzene ND 0.100 Pentachlorophenol ND 0.250 Pyridine ND 0,250 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 19 of 30 �-r-^ Summit Environmental Technologies, Inc. �a ,yAMRIWAhox I T 3310 win St. QC SUMMARY REPORT tc�rarnrnaiPk a i.� wtiuw�r,�s,.irtr�. Cuyahoga Falls, Ohio44223 WO#: 16021266 !1 rafiaErRf L 7uorwtorle5 TEL: (330) 253-8211 FAX.- (330) 253-4489 website: http:/hvrvw.settek.conz 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50088 Sample ID LCS-R50088 SampType: LCS TestCode: FlashPt_S(10 Units: °F Prep Date: RunNo: 50088 'lient ID: LCSS Batch ID: R50088 TestNo: SW1010 Analysis Date: 2/22/2016 SegNo: 784873 knalyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qual Flashpoint (140°F) 83.0 77.00 0 108 100 110 Qualifiers: r Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to detennine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 20 of 30 Summit Environmental Technologies,Inc. QC SUMMARY REPORT U M f, ni 3310 Win St. LMVIKU NMUN i Al. a t;�r:rur,�uutrs�i�es; INC. Cuyahoga Falls, Ohio 44223 WO#: 16021266 r?aildl.aaf Lzbo,rgioriF�4 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://ivlvw.settek.coni 03 May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50283 Sample ID MB-R50283 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 50283 Client ID: PBW Batch ID: R50283 TestNo: SW9034 Analysis Date: 212612016 SegNo: 788524 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Sulfide, Reactive ND 25.0 Sample ID LCS-R50283 SampType: LCS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 50283 Client ID: LCSW Batch ID: R50283 TestNo: SW9034 Analysis Date: 2/26/2016 SegNo: 788525 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 81.8 25.0 86.00 0 95.1 85 115 Sample ID 16021626-001AMS SampType: MS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 50283 Client ID: BatchQC Batch ID: R50283 TestNo: SW9034 Analysis Date: 2/26/2016 SegNo: 788526 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 84.6 25.0 86.00 0 98.4 75 125 Sample ID 16021626-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 50283 Client ID: BatchQC Batch ID: R50283 TestNo: SW9034 Analysis Date: 212612016 SegNo: 788527 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 82.6 25.0 86.00 0 96.0 75 125 84.60 2.39 30 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision v2 P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 21 of 30 Summit Environmental Technologies, Inc.IT 3310 Win St. QC SUMMARY REPORT r lkc ramti:r Ifu, a r.� �r uLUt�a; artc Cuyahoga Falls, Ohio 44223 WO#: 16021266 f!.rr<ttl,rtl.raP TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hqp.-1 www.settek.cotn 03-May-I6 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50283 Sample ID 16021626-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 50283 Client ID: BatchQC Batch ID: R50283 TestNo: SW9034 Analysis Date: 2/2612016 SegNo: 788527 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision V2 P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 30 Summit Environmental Technolo es, Inc. ��, F: 3310WinSt. QC SUMMARY REPORT crovlrrr-"Nru:NM, a i:r atdUl_v+;i. s; irrc. Cuyahoga Falls, Ohio44223 WO#: 16021266 ;1,,r,y1_,�L'.cal LaboyworFP6 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httn://ivivii,.settelc.coni 03 May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID• R50284 Sample ID MB-R50284 SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 50284 Client ID: PBW Batch ID: R50284 TestNo: SW9014 Analysis Date: 2/2612016 SegNo: 788536 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Cyanide, Reactive ND 0.500 Sample ID LCS-R50284 SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 50284 Client ID: LCSW Batch ID: R50234 TestNo: SW9014 Analysis Date: 2/26/2016 SegNo: 788537 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 1.04 0.500 1.000 0 104 85 110 Sample ID 16021626-OD1AMS SampType: MS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 50284 Client ID: BatchQC Batch ID: R50284 TestNo: SW9014 Analysis Date: 2/26/2016 SegNo: 788539 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110 Sample ID 16021626-OOIAMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 50284 Client ID: BatchQC Batch ID: R50284 TestNo: SW9014 Analysis Date: 2/26/2016 SegNo: 788540 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Cyanide, Reactive 0.965 0.500 1.000 0 96.5 85 110 1.010 4.56 20 Qualifiers: :k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit P Second column confirmation exceeds PL Permit Limit E Value above quantitation range M Manual Integration used to determine Revision V2 O RSD is greater than RSDlimit R RPD outside accepted recovery limits Page 23 of 30 Summit Environmental Technologies, Inc. �C SUMMARY REPORT' p � �v 3310 Win St. r_c.,airc r�rnr;n i. h a i.� rtt ciL[t 3r�s; ;r Cuyahoga Falls, Ohio 44223 _ _ pk.naairidc��i L.Ti?nr9ro,��e� TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 16021266 Website: http://wiviv.settelr com 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50284 Sample ID 16021626-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 50284 Client ID: BatchQC Batch ID: R50284 TestNo: SW9014 Analysis Date: 2/2612016 SegNo: 788540 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua] Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 24 of 30 SUMIAIT Summit Environmental Technologies, Inc. 3310Win St. QC SUMMARY REPORT tri'AlIKU NMUN I A6 A 1A:NWUL4i:i1:-S: NC Cuyahoga Falls, Ohio 44223 WO#: 16021266 a Lxibrp -8211 FAX (330) 253-4489natVUmfP Website: hitp://ivivw.settek.com 03-May-I6 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50317 Sample ID LCS 20PPB ABS022 SampType: LCS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 ,lient ID: LCSW Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789008 %nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ M-Dichloroethene 0.223 0.100 0.200 0 112 79.4 131 1,2-Dichloroethane 0.210 0.100 0.200 0 105 73.6 137 MEK ND 2.00 1.00 0 104 55.1 163 Benzene 0.204 0.100 0.200 0 102 73.1 132 Carbon tetrachloride 0.215 0.100 0.200 0 107 63.7 139 Chlorobenzene 0.196 0.100 0.200 0 98.0 72.3 139 Chloroform 0.206 0.100 0.200 0 103 79.3 129 Tetrachloroethene 0.185 0.100 0.200 0 92.5 56.2 187 Trichloroethene 0.214 0.100 0.200 0 107 64.1 138 Vinyl chloride - ND 0.200 0.200 0 95.3 22.1 147 Sample ID LCSD 20PPB ABS02 SampType: LCSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 ;lient ID: LCSS02 Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789009 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1-Dichloroethene 0.227 0.100 0.200 0 114 79.4 131 0.223 1.64 25 1,2-Dichloroethane 0.206 0.100 0.200 0 103 73.6 137 0.210 2.36 25 MEK ND 2.00 1.00 0 95.2 55.1 163 0 0 25 Benzene 0.211 0.100 0.200 0 106 73.1 132 0.204 3.37 25 Carbon tetrachloride 0.222 0.100 0.200 0 ill 63.7 139 0.215 3.07 25 Chlorobenzene 0.200 0.100 0.200 0 100 72.3 139 0.196 2.22 25 Chloroform 0.206 0.100 0.200 0 103 79.3 129 0.206 0.146 25 Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Revision V2 MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 25 of 30 s Summit Environmental Technologies, Inc. umftn3310 Wit St. QC SUMMARY REPORT L!91HQrarv;N1Al. ,JNC; Cuyahoga Falls, Ohio44223 WO#: 16021266 A.,at4,tf.caf L bo,raior er TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http:/hvivw.settekcom 03 May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50317 Sample ID LCSD 20PP13 ABS02 SampType: LCSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 'lient ID: LCSS02 Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789009 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Tetrachloroethene 0.193 0.100 0.200 0 96.3 56.2 187 0.185 4.03 25 Trichloroethene 0.216 0.100 0.200 0 108 64.1 138 0.214 1.07 25 Vinyl chloride ND 0.200 0.200 0 95.4 22.1 147 0 0 25 Sample ID MBLK SampType: MBLK TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 ,lient ID: PBW Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789010 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene ND 0.100 1,2-Dichloroethane ND 0.100 MEK ND 2.00 Benzene ND 0.100 Carbon tetrachloride ND 0.100 Chlorobenzene ND 0.100 Chloroform ND 0.100 Tetrachloroethene ND 0.100 Trichloroethene ND 0.100 Vinyl chloride ND 0.200 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit B Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 26 of 30 t` Summit Environmental TechnoloWrac. 331OWininSt. QC SUMMARY REPORT era IIKV'Nmur%,uki- R ia;MNULUC]I-'b,.INC. Cuyahoga Falls, Ohio 44223 WO#: 16021266 _ Ai a( fla'if Laborstorir:� TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httl2:llwwiv.sett6lc.coni 03 May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID• RS0317 Sample ID 16021599-001ams SampType: MS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 client ID: BatchQC Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/2612016 SegNo: 789025 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.209 0.100 0.200 0 104 39.9 160 1,2-Dichloroethane 0.190 0.100 0.200 0 94.8 42.5 157 MEK ND 2.00 1.00 0 102 16.6 227 Benzene 0.192 0.100 0.200 0 96.2 38.1 155 Carbon tetrachloride 0.201 0.100 0.200 0 101 40.8 162 Chlorobenzene 0.182 0.100 0.200 0 90.8 35.7 168 Chloroform 0.187 0.100 0.200 0 93.4 18.3 199 Tetrachloroethene 0.185 0.100 0.200 0 92.4 10 261 Tiichooroethene 0.231 0.100 0.200 0 115 23.8 175 Vinyl chloride ND 0.200 0.200 0 80.1 10 165 Sample ID 16021599-001amsd SampType: MSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 client ID: BatchQC Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789026 �nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.210 0.100 0.200 0 105 39.9 160 0.209 0.526 25 1,2-Dichloroethane 0.199 0.100 0.200 0 99.6 42.5 157 0.190 4.89 25 MEK ND 2.00 1.00 0 97.5 16.6 227 0 0 25 Benzene 0.198 0.100 0.200 0 99.1 38.1 155 0.192 2.97 25 Carbon tetrachloride 0.206 0.100 0.200 0 103 40.8 162 0.201 2.16 25 Chlorobenzene 0.193 0.100 0.200 0 96.5 35.7 168 0.182 6.03 25 Chloroform 0.199 0.100 0.200 0 99.6 18.3 199 0.187 6.32 25 Qualifiers: * Value exceeds Maximum Contaminant Level, B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Revision V2 P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 27 of 30 S Summit Environmental Technolo ies, Inc. U M m 3310 Win St. QC SUMMARY REPORT LNNIH:UNM1;rJirtl. A I;C"NULUJH:s, VC Cuyahoga Falls, Ohio44223 WO#: 16021266 y_ !4 zr(4-, ; rRf Lzbor.9lorrca TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://lvivw.settelc.com 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50317 Sample ID 16021599-001amsd SampType: MSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 50317 client ID: BatchQC Batch ID: R50317 TestNo: SW8260B Analysis Date: 2/26/2016 SegNo: 789026 4nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Tetra chloroethene 0.190 0.100 0.200 0 95.2 10 261 0.185 2.99 25 Trichloroethene 0.212 0.100 0.200 0 106 23.8 175 0.231 8.59 25 Vinyl chloride ND 0.200 0.200 0 84.0 10 165 0 0 25 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Revision v2 Page 28 of 30 Et Summit Environmental Technologies, Inc. (� r SUMMARY 771tr nTnORr�, 3310 Win St. QC S l.J 1V11�' AR i REPORT tNVIrtar•1rnlaNIPI,91;CHNULrJ'jK:S;1N'C Cuyahoga Falls, Ohio44223 WO#: 16021266 ?1,.r:-tf4�2�'.cr7f C:Tia��.r9ro,rrr� r TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hU12.-1 vivtiv.sette&cont 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID• R50630 Sample ID 16021626-001AMS SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 50630 Client ID: BatchQC Batch ID: R50630 TestNo: SW8321A Analysis Date: 3/4/2016 SegNo: 798230 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 2,4-D 57.6 5.00 50.00 0 115 37 105 S 2,4,5-TP 61.8 0.500 50.00 0 124 38 106 S Sample ID 16021626-001AMSD SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 50630 Client ID: BatchQC Batch ID: R50630 TestNo: SW8321A Analysis Date: 3/4/2016 SegNo: 798231 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D 57.1 5.00 50.00 0 114 10 150 57.56 0.855 30 2,4,5-TP 61.7 0.500 50.00 0 123 10 150 61.78 0.190 30 Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. P Second column confirmation exceeds B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit PL Permit Limit E Value above quantitation range M Manual Integration used to determine R0V1SlOri V2 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits Page 29 of 30 Summit Environmental Technologies, Inc. QC SUMMARY REPORT j' 3310 Win St. er:;v�rs�aNPUNIRI.0J.i-- N1JL41J1_1S:M Cuyahoga Falls, Ohio44223 WO#: 16021266 aina(vtlu3f L.Tbar.gtu.6eF TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http://iviviv.settelc.coni 03-May-16 Client: Synagro, NC 28134 Project: MT Holly WWTP BatchID: R50630 Sample ID MB-R50630 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 50630 Client ID: PBW Batch ID: R50630 TestNo: SW8321A Analysis Date: 3/4/2016 SegNo: 795495 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D ND 5.00 2,4,5-TP ND 0.500 Sample ID LCS-R50630 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 50630 Client ID: LCSW Batch ID: R50630 TestNo: SW8321A Analysis Date: 3/4/2016 SegNo: 795496 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 2,4-D 56.9 5.00 50.00 0 114 37 105 S 2,4,5-TP 59.2 0.500 50.00 0 118 38 106 S Sample ID LCSD-R50630 SampType: LCSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 50630 Client ID: LCSS02 Batch ID: R50630 TestNo: SW8321A Analysis Date: 3/4/2016 SegNo: 795497 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 2,4-D 56.4 5.00 50.00 0 113 37 105 56.92 0.912 30 S 2,4,5-TP 62.0 0.500 50.00 0 124 38 106 59.23 4.61 30 S Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine Revision v2 MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 30 of 30 =r-r-11SUMMIT CNVIR0Mmt:N'rAL 'i EQHN0L0GI ES. iNr-, 33Yfl WJtn Street Analysis Request f Chain of Custody For Sumutit 13aviroYtmental Technologies,1w. use only Page- f of f SI=ENE - CSicin Nanrc S na ro Certtra4 Prr�jty t Ittt ntiticatian i 77. f OL-L t( UW7p Address 92 � t h• Q fl 1z fl II i � � Anal PAramet.m andM1tid5 Client Address y Pinov111e NC, 28134 12701 Lancswr 4w 1, • Client Phone 704-752-8673 Report 1b DREW Cllen[ Fax No, / In Receive Ilccults by Fax ; 704-762 srsso Pb NUMIler 1 d Con Iar.1 P n nn GiL' Quu1r Noinbur &,mVled Byf.V OMW L.LW,,y if Ohio VAP Samples Sample Ideatitientiai Date :cam dr "' -led a G. o -170 of t7d-f$- SL r x l i . Re11tt ubbad b 1%tc Time Received by -.)Ale Thne Notes, I Comment$: Received in >i ab by. I Date Time Rush Regnestedt _ Day(s) lotus[ be ap roved h+ Lab majulger U D47 Rev. 1s Summit Environmental Technologies, Inc. Cooler Receipt Form 04H6rtr. Initials of person inspecfing cooler and samples: � Client Order €Number, ! a 2.i,e U Date Received: /fF Time Received: '7 Date coolers) opened and samples Inspected: Number of CoolerslBoxes: NIA Shipper: D�C UPS DHL Airborne US Postal Walk-in Pickup Other. Packaging: Peanuts bl Paper Foam None Other. Tape on coolerlbox: N NIA Custody Seals Intact Y dp N/A C-O-C in pl tj N NIA ice t/ l3tue ice present / absent I melted NIA Sample Temperature IR Gun 916020469 CF L °C y 'C N/A Radiofogicai Testing Instrument serial #35127 Y N (see page 2 for scan results) —Use 4 sheet per sample for Radiological Testing. Ifsample is HOT, the Radlological Safety Officer mast be natilled Immediately. C Q C filled out properly N NIA Samples in separate bags N NIA Sample containers intact` Y,�/ N NIA *If no, list broken sarnple(s): Sample label(s).complete (ID. date, etc.) 6 N N/A Labet(s) agree with C-O-C e N N/A Correct containers used N NIA Sufficient sample received N NIA Samples receFvsd within holding time G/ N Bubbles absent from 40 mL vials" Y N NIA "Samples with bubbles <6mm are accr..piable. Indicate bubble size i€>6mm. Was client contacted about samples Y N Will client send new samples Y N Client contact Datemme: Logged in by: Comments: Page 1 of 2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WWTP Name: Mt Holly WWTP NPDES Number: Monitoring Period: From 01/01/16 To 04/30/16 WQ 0001863 NCO021156 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion H nnnlienhle to niternntive nP.rfnrmerl Wines A nr C19QQ Rl rmmn1PtP fhP fallnwina mnnifnrina dhfa- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6th Coliform power per gram MPN 157,342 161,435 163,349 MPN/g 0 event sludge SM9221E of total solids CFU CFU/g quarterly sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an _ explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jonathan Jordan / ORC Prep r Name and Tit (type or print) ignature o r er* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) PRO h4PT•ACCLI RATE• REUTAE3L.E LABORATORIES, INC WN"N'TAR LARS.COM REPORT OF ANALYSES Attri: DREW CULP SYNAGRO PROJECT NAME: FEB 16 12701 LANCASTER HWY DATE: 03/17/16 PINEVILLE, NC 28134- SAMPLE NUMBER- 122363 SAMPLE ID- MT. HOILY 50-1701 1ST EVENT SAMPLE MATRIX•- SO DATE SAMPLED- 02/18/16 TIME SAMPLED- 0815 DATE RECEIVED- 02/18/16 SAMPLER- DC RECEIVED BY- DJ TIME RECEIVED 0927 DELIVERED BY- DC TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 02/18/16 1500 RE 161,435 MPN/g LABORATORY DIRECTOR �i.r 7_.r-•"Z�-�"' P.O. Box 411483 • Charlotte, NC 28241-1483 Plione: (704) 588-8333 , Ftex: (704) 588-8335 PA PROMPT -ACCURATE- RELIABLE LEiBOItATORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NO Cert # 20; SC Cert # 99003001 �LIENT NAME SAMP,�LE DATE MOM RNALYSIS .� �, � AN,i4LYSiS METN�DDMRI � � - • - + A, •` 122363 1 4,066 2.55% 159,539.39 2 4,084 2.50% 163,348.65 3 4,116 2.52% 163,321.84 4 4,141 2.65% 162,383.79 5 4,066 2.49% 1 163 277.53 6 3,949 2.51% 167,341.95 7 4.088 2.54% 160,934.52 PFftbi Coljfdrm W L5. -f Geotnetr�e I1lieara • PAR CHAIN OF CUSTODY ueaRaro»,as uva PAR Laboratories, Inc Phone (704) 588-8333 www.parlabs.com Fax (704) 588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It Is essential that all Information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North Company Name (billing) Comments/ SYNAGRO CENTRAL Address 12701 LANCASTER HWY City, State & zip code €'INEVILLE NC 28134 Point of Contact It Telephone Number DREW r-uLP 7ot4-57'f-52Q j taken By: SIGNATURE ft PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? YES k NO *Sample Type: DW WW GWMW HW Soil Other Sample Temp at time of sampling: a C Sample Temp upon receipt: 0 C "Field Preserved: Yes _No _Teflon Liner/Zero Headspace: Yes No _ nla Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN): (lent Sample I.D. (Sample Location I Number) Camp Grab Prasew. set Up Date/Time Collection Date/Time Analyses Requested m , L Z o/ X 02-I t3 -I(o 09 : 5' C44- Goy �t}`fi AST i' .2.0 W /77f !Yi -3 S aF nnIuiyuiz+unu u vaiei I lit It: Uarer I Ime oa-W-IG40q; 2 Relinquished by. Datemme Received by: Datemme "C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste -See Outer Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 05/01/16 To 06/30/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf annlicahle to alternative nerformed (Class A or Class M comnlete the following, monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal th 2x10 to the 6 Coliform power per gram MPN 381,219 386,385 389,848 MPN/g 0 event sludge SM9221E of total solids CFU CFU/g quarterly sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Mt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jonathan Jordan / ORC Pre er Name and T' le (type or print) ignature of rep er* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) P AA11 R PROM PT•ACCU RATE -RE LIABLE LABORATORIES, INC WNVMV PARLABS.COM R EPORT OF ANALYSES Attn: DREW CULP SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: APR 16 DATE: 05/31/16 SAMPLE NUMBER- 122988 SAMPLE ID- CITY OF MT. HOLLY 2ND EVENT SAMPLE MATRIX- SO DATE SAMPLED- 04/19/16 TIME SAMPLED- 0940 DATE RECEIVED- 04/19/16 SAMPLER- DC RECEIVED BY- DJ TIME RECEIVED- 1145 DELIVERED BY- DC TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS FECAL COLIFORM (GEOM. MEAN) ANALYSIS METHOD DATE TIME BY RESULT UNITS SM 9221 E 04/19/16 RE 386,385 MPN/g LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PAF;Z PROMFT•ADC;URATE• RELIABLE I.ABOIZATO.RIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 SYNAGRO CITY OF MT. HOLLY 2ND EVENT 04/19/16 FECAL COLIFORM, GEOMETRIC MEAN • • SM 9221 E 10122988 1 . 8,077 2.08% 389,058.75 2 7,995 2.07% 385,825.85 3 7,987 2.08% 383,975.43 4 8,031 2.06% 389,848.93 5 7,929 2.08% 381,219.07 6 8,089 2.09% 387,021.30 7 8,028 2.07% 387,815.06 Fecal Coliform Geometric Mean= _; • LLAF? CHAIN ®F CUSTODY OORATOMEs,rNc. PAR Laboratories, Inc Phone (704) 588-8333 www.partabs.com Fax (704) 588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR laboratories, Inc. and the North t,aronna Ue arrment or tnYlronmental ana Natural Kesources. Company Name (billing) Comments/ Special Instructions SYNAGRO CENTRAL Address 12701 LANCASTER HWY City, State Et zip code PINEVILLE NC 28134 Point of Contact Et Telephone Number D99W CUL_P 704-5711-5-2?1 Sample Taken By: SIGNATURE PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO *Sample Type: DW WW GWMW HW Soil other Sample Temp at time of sampling: 0 C Sample Temp upon receipt: ° C "Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN): (lent Sample I.D. Sample Location / Number) Comp Grab Preserv. Set Up Date/rime Collection Dateri-ime Analyses Requested G/ OF N7 h- & X o •qo � � Coc�Fc, ,01(o Cse- oy: uatei 11 rtecely )y: DatelTime by: Datelftime Received by: Date/Time C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt Holly WQ Permit Number: WQ 0001863 WWTP Name: Mt Holly WWTP NPDES Number: NCO021156 Monitoring Period: From 07/01/16 To 09/30/16 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf a,.,,l—hlo 4n al*orna4ivn nnrf--A !('lace A nr ('lace R) rmmnlrte thr fnllnwinv mnnitnrina rlatn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency' Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6t Coliform power per gram MPN 249,517 302,287 354,440 MPN/g 0 event sludge SM9221B of total solids CFU CFU/g quarterly sludge SM9222D 1000 MPN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1.106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jonathan Jordan / ORC Prep r Name and Title (type or print) a�6 17 (5Z of P e er* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) RA R PRO h7PT•ACCURATE• RELIABLE LABORATORIES, INC 1YWWPARLA6S.CON1 Attn: DREW CULP SYNAGRO 12701 LANCASTER HWY PINEYIL•LE, NC 2.8134- REPORT OF ANALYSES. PROJECT NAME: JUL 16 DATE: 08/19/16 SAMPLE NUMBER- 124172 SAMPLE ID- MT. HOLLY WWTP 50-1701 3RD EV SAMPLE MATRIX- SO DATE SAMPLED- 07/28/16 TIME SAMPLED- 0930 MATE RECEIVED- 07/28/16 SAMPLER- DC RECEIVED BY- CT TIME RECEIVED- 1011 DELIVERED SY- DC TYPE SAMPLE- Grab Page 1 or 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORI✓ (GEOM. MEAN) SM 9221 E 07/28/16 1550 RE 302,287 MPN/g LABORATORY DIRECTOR `is -r_,- P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PAFZ PROMPT•ACCU RATE- RELIABLE LABORATORIES INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 SYNAGRO MT. HOLLY WWTP 60-1701 3RD EVENT 07/28/16 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E 1 6,734 1.90% 354,440.08 124172 2 4,969 1.91 % 260,450.29 3 5,907 1.91% 309,256.74 4 5,832 1.91 % 305,359.23 5 6,602 1.90% 347,449.03 6 4,741 1.90% 249,517.60 7 5,859 1.92% 305,175.78 -- - - -- -- ---'-' --I Fecal Coliform Geometric Mean= _j >� GRAIN! OF CUSTODY PAA Phone (704) 588-8333 PROMPT'ACCUR4TE*RELfABLE Fax (704) 588-8335 LABOR.ATORIES, INC Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 it is essential that all information be recorded on this Chain of Custody document for acceptance by PAR taboratoriPs_ Inn nnrr rha M—fh yarouna ue arunenr or cnvrronmemar r mpany Name (billing) Address ,270/ City, State Et zip code Point of Contact & Telephone Number f�22r.� G4 0 ?° `l - S7,1 - S zy/ Comments/ Special Instructions sampie Taken By: SIGNATURE PRINTED NAME !i Cu ARE SAMPLES FOR STATE or EPA REPORTING? YES NO *Sample Type: Dw ww GVVMW HW Soil other Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C **Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N): tientSample I.D.Setp Sample Location / Number) Italy Cotle;'ibn ", Preserv. Date -rime Datefi-ime aif ec Yrest ii"" jLLn/ WW 1Up i_tL%-'j� ��co.� GO��ir✓h 3a (r w4 j M ry 2 wl Relinquished by: Datemme * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Mt WWTP Name: Mt Monitoring Period: Holly WQ Permit Number: FIolly WWTP NPDES Number: From 10/01/16 To 12/31/16 VQ 0001863 NCO021156 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf nnnlirnhle to niternative nerfnrmed (( ncc A nr Class R) rmmnlete the fnllnwino mnnitnrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 Coliform power per gram NUN 341,941 346,491 350,020 MPN/g 0 event sludge SM9221E of total solids CFU CFU/g quarterly sludge SM9222D 1000 NUN per gram of total solids (dry weight) MPN/g Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Mt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt: 5 Optiori.Wt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jonathan Jordan / ORC Preparer ame and Title (type or print) S' ature of P er* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Late *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) PAR PROM PT-ACCU RATE -RE LlASLE LABORATORIES, INC W WW.PARLABS.00M REPORT OF ANALYSES Attn: DREW CULP SYNAGRO 12701 LANCASTER HWY PINEVILLE, NC 28134- PROJECT NAME: SEP 16 DATE: 11/01/16 SAMPLE NUMBER- 124968 SAMPLE ID- MT HOLLY SAMPLE MATRIX- SO DATE SAMPLED- 09/26/16 TIME SAMPLED- 1100 DATE RECEIVED- 09/26/16 SAMPLER- MP RECEIVED BY- DJ TIME RECEIVED- 1210 DELIVERED BY- MP TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 09/26/16 RE ATTACHED FECAL COLIFORM (GEOM. MEAN) SM 9221 E 09/26/16 1600 RE 346,491 MPN/g '-'� •� f f_^,%yam LABORATORY DIRECTOR P.O. Box 411483 - Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 AM RAA R PROMPT•ACCURATE•RELIA9 LE I.ABORATORSES, INC WWW. PARLABS. COM 30 Day Bench Scale Extended Aeration Test Percent !Volatile Solids Reduction CLIENT NAME: - �SA�MPLE ��SAMPLE # a. * ; START DATE: i • M.. Start: End: TS () 0.2035 0.1941 TS% . 1.51 % 1.49% VS () 0.1447 0.1346 VS% 71.11% 69.35% IN 0,004214 OUT 0.00397164 FSVR (Mass Balance) 5.74% FSVR (Van Kleeck) 8.07% FSVR (Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES P.O. Box411483 ® Charlotte, NC 28241-1483 Phone: (704) 588-833 3 0 Fax: (704) 588-8335 RA PROMPT' ACCURATE- RELIABLE LABOPUNTOP-MSS INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert# 20; SC Cert # 99003001 WENT NAMEc• ` - • tSAMPLE ID ° SAMPLE. DATE: { ANALYSIS- I&YAWN • GEOMETRIC FECAL COLIFORM, "LYjMt-TjHQP,,4wn"wM • � o e e e • 124968 1 5,237 1.51 % 346,799.82 2 5,176 1.50% 345,082.57 3 5,202 1.49% 349,128.28 4 5,250 1.50% 350,020.35 5 5,224 1.50% 348,263.52 6 1 5,199 1 1.51 % 344, 274.17 7 1 5,198 1 1.52% 341, 941.13 Feeal_Coliform �Geoti%etric Mepn= 1 • • CHAIN OF CUSTODY Phone (704) 588-8333 P R r3 M tyP•AQCLIRaT Fax (704) 588-8335 L-A-BORATORiES, I1%TC Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custndv dnaumanr fnr --+— — h„ oe o I — t:am"na uepartment of Lnvironmentai and Natural Resources C�any Nam (billing) U Add s� /-/ 'a Z: City, State rt zip code IN06 -2) 7 Point of Contact $ Telep one Number Comments/ Special Instructions aafnple Taken By: SIGNATURE PRINTED NAME ARE SAMPLES FOR STATE or EPA REPORTING? YES NO `Sample Type: DW ww GWtVW Nw Soil other v Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C "Field Preserved: Yes No _Teflon LinerlZero Neadspace: Yes No _ nla Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN): Iient Sample'D. Sample Loca#]ott /Number) ."CarA 7 '.GiaE3 -R�esety: Set f7: ll'ateliJme Calleciio6' aateTmie ReRa�st'ech j ;` : ' -fry f..• r ,'of/y 20 � /., (; lJ i y D telTime Heceived by: uatei i ime R linauished bv.— Datefr-ime Received by: Date/Time C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=hazardous Waste Agricultural Lime Application Log 2016 Project: Mt. Holly 50-1701 * lime has been ordered Field Grower Soil Lime Requirement Tons/Acre Date (state -county -site -field) pH (from soil analysis) Applied Applied [Total Acres NU-CAA-41-Ub vreg Springs 6./ 1 0 tons/acre N/A N/A NC-GA-41-10 Greg Springs 6.4 0 tons/acre N/A N/A NC-GA-41-14 Greg Springs 6.3 0 tons/acre N/A N/A NC-GA-45-01 David Allen 5.9 0 tons/acre N/A N/A NC-LT-46-01 Tony Jones 6.2 0 tons/acre N/A N/A NC-LT-46-02 Tony Jones 6.0 0 tons/acre N/A N/A NC-LT-46-03 Tony Jones 6.3 0 tons/acre N/A N/A NC-LT-46-04 Tony Jones 6.3 0 tons/acre N/A N/A NC-LT-46-07 Tony Jones 6.4 0 tons/acre N/A N/A NC-LT-46-08 Tony Jones 6.1 0 tons/acre N/A N/A TOTAL 1 0.0 Page 1 of 2 Report Number: 17-003-0913 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 Waypointo ANALYTICAL "Every acre... Every year."rM Date Received: 01/03/2017 Date Of Analysis: 01/04/2017 Farm ID: NC-GA-41 SOIL ANALYSIS REPORT Date Of Report: 01/06/2017 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com Grower: Greg Springs Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Sample ID OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Field ID Lab Number % Rate Soil Class Ib/A s M3 ppm Rate ppm Rate ppm Rate K ppm Rate Mg ppm Rate Ca ppm Rate Na ppm Rate Soil pH Buffer Index H meq/100g megl100g 06 05850 5.4 H 146 51 H NC = 42 37 VL NC = 19 270 VH 1088 M 43 L 6.7 0.4 8.4 MIN 10 05851 8.7 VH 150 91 H NC = 76 45 VL NC = 23 343 VH 1268 M 36 VL 6.4 0.9 10.4 MIN 14 05852 7.4 VH 150 82 H NC = 68 30 VL NC = 15 350 VH 12116 M 39 VL 6.3 1.1 10.7 MIN Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Sample ID Field ID K % Mg % Ca % Na % H % NO,N ppm Rate S ppm Rate Zn ppm Rate Mn ppm Rate Fe ppm Rate Cu ppm Rate B ppm Rate SS ms/cm Rate 06 1.1 26.8 64.8 2.2 4.8 14 L NC=29 8.6 VH NC=215.0 39 H NC=244 77 VH 4.8 VH NC=240.0 0.5 L 10 1.1 27.5 61.0 F.5 8.7 16 M NC=33 14.8 VH NC=370.0 33 H NC=2)6 79 VH 5.3 VH NC=265.0 0.8 M 14 0.7 27.3 60.1 1.6 [10.3 16 M NC=33 15.1 VH NC=377.5 31 H NC=194 90 VH 5.9 VH NC=295.0 0.7 M values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. me GCoivy/ H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: " o C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypolntAnalytical Virginia, Inc. Pauric McGroary Page 2 of 2 Report Number: 17-003-0913 Account Number: 00015 Send To: Synagro Central LLC/ MT Holly Wayne Brady 12701 Lancaster Highway Pineville NC 28134 Date Received: 01/03/2017 Date Of Report: 01/06/2017 o Waypoint," ANALYTICAL "Every acre... Every year. "TM Farm ID: NC-GA-41 SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Greg Springs Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Field ID Intended Crop Tons Tons/A N P205 K20 Mg S Zn Mn Fe Cu B Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 06 Fescue Hay 4 0.0 50 30 250 0 15 0 0 0 0 0 10 Fescue Hay 4 0.0 50 30 250 0 13 0 0 0 0 0 14 Fescue Hay 4 0.0 50 30 250 0 13 0 0 0 0 0 Comments: Sample(s) : 10,14 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary NCDA&CS i— ___omic Division Phone: (919) 733-2655 Predictive }t Soil Report VVeosite: wwW.n....y..,jov/agronomi/ Report No. FYT.---30494 Client: David Allen Advisor: Synagro 110 Helton Rd 12701 Lancaster Hwy Cherryville, NC 28021 Pineville, NC 28134 Mehlich-3 Extraction Sampled County : Gaston Sampled: Received: 07/12/2016 completed: 07/20/2016 Fans: NC-GA-45 Links to Helpful Information Sample ID: 01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 80 60 0 0 0 0 0 0 Note: 12 1.00 tons/acre; 10/2015 2- Test Results [units - W[V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.04 8.6 86 1.2 5.9 25 37 59 24 36 888 550 97 97 109 0.1 1 North Carolina �iiN;it�i�:r Jn»c Fi�mcl �Gn�ntuirs:;lc�io Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS / _..omic Division Phone: (919) 733-2655 Website: www.r _ jov/agronomi/ Report No. FY1 , -oL-uD0494 David Allen Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi16bpart4.htmY sFind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei Test Results The first seven values [soil class, HM%, W/V, CEC, BS%o, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomiluyrst.htm Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index Page 1 of 1 Report Number: 16-084-0666 Account Number: 00015 Send To: SYNAGRO CENTRAL/MT HOLLY WAYNE BRADY 12701 LANCASTER HWY PINEVILLE NC 28134 Waypoint0 ANALYTICAL "Every acre... Every year. SOIL ANALYSIS REPORT Date Received: 03/24/2016 Date Of Analysis: 03/25/2016 Date Of Report: 03/25/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: TONY JONES NC-LT-46 MT HOLLY 50-1701 Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition Water pH Sample ID Lab OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Field ID Number % Soil Ibs/A M3 K Mg Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g 01 24652 6.8 150 194 VH 90 L 177 M 1604 H 20 VL 6.2 1.4 11.2 MIN H NO = 162 NO = 46 03 24653 8.0 150 83 H 137 M 206 H 1437 M 26 VL 6.3 1.1 10.5 MIN VH NO = 69 NC = 70 07 F6,4 7'5 150 95 H 53 VL 168 H 1359 H 18 VL 6.4 0.8 9.2 MIN VH NO = 79 NO= 27 08 24656 8'6 150 192 VH 116 M 283 H 1239 M 27 VL 6.1 6.79 1.4 10.4 MIN VH NO = 160 NO = 59 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NC N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 01 13 L 15.2 VH 58 VH 12.4 VH 2.1 13.2 71.6 0.8 12.5 171 VH 1.0 M 0.27 VL NC=27 NC=380.0 NC=363 NC=620.0 03 12 L 8.0 H 77 VH 5.5 VH 3.3 16.3 68.4 1.1 10.5 104 VH 0.8 M 0.27 VL NC=25 NC=200.0 NC=481 NC=275.0 07 13 L 8.4 VH 39 H 4.8 VH 1.5 15.2 73.9 0.9 8.7 108 VH 0.9 M 0.13 VL NO = 27 NO = 210.0 NO = 244 NO = 240.0 08 18 M 16.8 VH 38 H 8.4 VH 2.9 22.7 59.6 1.1 13.5 132 VH 1.0 M 0.22 VL NO = 37 NC = 420.0 NO = 238 NO = 420.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. to G�N� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc. Pauric McGroary NCDA&CS.L.y.—..omicDivision Phone: (919)733-2655 Website: www.n„aU,..gov/agronomi/ Report No. FY1',�,'u16999 Client: Tony Jones Advisor: Synagro Predictive ':. 1418 Nature Preserve Trl. Denver, NC 28037 12701 Lancaster Hwy Pineville, NC 28134 � Soil Report Mehlich-3 Extraction r #' Sampled County: Lincoln Sampled: Received: 11/21/2016 Completed: 12/20/2016 Farm: NC-LT-46 Links to Helpful Information Sample ID: 02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/cn•r3; CEC and Na in meq/100 crrr3; NO3-N in mg/drn3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.01 13.2 90 1.3 6.0 73 107 62 24 56 179 124 315 315 550 0.1 1 Sample ID: 04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 50 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/dn�]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.32 1.04 13.2 93 0.9 6.3 38 138 63 25 54 362 230 215 215 406 0.1 1 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS / r omic Division Phone: (919) 733-2655 Website: www.n__,..gov/agronomi/ ReportNo. FYI —_ 16999 Tony Jones Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I. and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagrgovlagronomilobpart4.htmy sFind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize] Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine, available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrqov/agronomiluvrst.htm Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN. mineral soil class Mn manganese Mn-All Mn-availability index for crop I Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P206 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index