NCG030056_2020 DMR_20201221 (3)

i
O
Q
OC
w
�i
O
O
2
Q)
tv
L
m
zN
M
a
0
41
++ Q
Z
0 H
N
f6
�
Q
a
0
O
O
El 3
Z
(7
O
{A
4- L
O a)
O
CD
N>
O N O
❑❑�
H
w
7
Q 7
';gig
i V)W
G
U
W
w
0 ®
®
LU
W 0
O
F-
H
W
�
O
z
Ja
�
O uj
a-
J J
Q
=
Ca CCL
V1 �
O
Z
D
O
U
Y
CD
0
H
W
J
a
Q
z
U
W
J
J
O
U
Z
O
N
w
W
a
U m
,p
❑
�E
2
41-
w
w
w
w
0 O
C7 E In
06 O C
N O
J
0 O 0
V
N
Lo
O
O
O
O
O
O
a° a o
,n
o
LO
V
LO
V
LO
V
C ;@+ T
0 =
Z
U
C_
N
J
to
E
O
0O
O
O
N
O
aN-I
O
O
O
~
O
.a
N
J
OA
E
�I
J
Ln
O0
oo
O
o
0
�I
O
O
O
V
O
V
H
0
v
a
CL
0)
co
(D
N
U
OE
-1
O
O
o
Y
C
p
O
O
O
O
H
p
Y
C
O
O
2
Qj
I
O
*
co
N
CO
Iz m
O
00
r
O
V)
C
tD
m
c%
to
�
�
J
Ln
v
w
CD
C
L
O
M
MO
O
ch
N
C
U
tw
Vf
E
m
CD
O
O
4T
c
•i
3 Ol
°1
N
0
co
0
0
0
M
` O v
30 E C
tLn
a
O
O
O
s � —
N
N
D
O
O
O
N \
N
N
N
f0 U m
Vf N
I
N
N
�
N
w O
o U E
O
Z
p
U
wt3+��
0
o
CD
0
CD
0
O
u
E
a
m
a°
C d
0000
L
N W O N
(U -0
Em
O
a) U
\
C 0 U
CO CT Q
4�-,
a) L
v
N Cai •U
C O
N y(o E 4-
�^
a E L
(n O N
Y
L- LO
1 c U C) U N
n
co M
Co N U O `� N
V1' O
N lD
N ,-I
N +' > o i� M
C
C 4- U �
� N
w
L U
N a
cY1 a"i
(o w N , N co U O
O- U •� L t O J.
E
`} C C 3
N O 0
41 4! (C6 Lo
Q. -a Y v)
Eo
4- i) :M L) U (o C
N v
0] i — C o
U W a) s C:p o +�
c •c N 3 0 +� c
6 O V) coo (6 C
CU
Q)) c f° o v o v-0
U O E P O ♦- "a 0)
a
N U bA o f +'
C C ++ 0)
(o h :Eo =
N
E m a c6 ,N_ ++ N
U U c c L
u
_0 to +, (o N
.�
C
4C y=
c E '= E
L
N ..Q N o s 0) f6
h0 C
L
O _ pp SZ T O
a C v t= U
U Y U
C +J (6' 4-- N '
n o
= a) c 3
o
E N
vw N V) M u
o S� O 41
t A O _
a) 4- C O
M
3 E o o o E N
C O N O LL r{ m
•� 0 Q1 't
+ cm + U
N 'N Y U-
txo O
� U
c c c d
E C Q) O E O
C
a-+ M O U a 3
C tw 'a rl U L N a
•Q
co o a) CO-0 c 40
t U:E IZ U :3 O C
E U N co m0J `^ `~ O
Ln
0) -0 N F- v1 +�, m +�
N
4-- -0 m wC C
0
O
0 ,F, C C �o U O
-a c Ln m
N
O
c\I
Ln
3 c cn ° E 4"a,
o
oA O U C C
+1 •�
o
C L vl (U +� N
_ L
N
\
S? Q '� � im •= N
.O
M C Q M u U a)
r-I
Q (6 C O U (7 ate, c
�
E +� a, F- c +� u m
o O 4- E
o
Y
C�
O + C
2 N `6
U-cn Fo
N m a In N W E Y
a)I
2

40 L
O
L —
0
•t2 (6 v
L U C
O a) c c
(6
E a) La O 4-
41 p
0 C7 O O v
Q1 U_ � �
X O
cl- In
m v '>
i 4, O
O a)
a) N L Co
E - a) 4 V
L
4 —
aa) � v 3 a)
s m E o
E — a, m +,
L (D tw
0 6 L
v
aa)) E
41
ca O +_ a)
L v 3 E
tU r.
(U -0W O o.LA
U c c E
�'3 t_' a)_
� a 0 E '
� U
> N — a) o m
n3 O 0 n = N
C t Y U 41
o (o
c o..5 3 �9
0 0 — u o
a) U t cu u
_U N XO
E L Q 41
O tlbA � 0
LO (o U
O U U aci —
=5 X N b0 U i C
O a (D c p (a
_� a) Ou O_ a
L -J ..0 �' E O O
a) L w
N C: w — O
O >
E _0
O 0 p n.
bA c
v) k c Q o E o
_ •� c a)
a3 O v n
O -0 0 u a.
7 CO u L L
U E L O O
C O O v c n3
m co 3
n o bnv E
++ t (U v( 'p t LO
c N a L a) bA a) v N
E n3 > o v
a) Q. O Y 4=
m C E O >, u •O
(co a) a) L E r
E (u o Q a
ito L N i U
c
O E a) >, .c O
a) a) 0 O = C:+ > � a)
M 0 Oc N
n. (U o E o
o H v o v
c o Q u cu E
6 L -O — 3
+� +J v
(o > L - 0 , >
'co o Co o 0
3 L. - n 0
V -
(IJ a)
+� E
U > L
(o
E a
a)
E
C
a)
E
Z
I
J
a�
a)
7
4-
c
as
in
c
O
U
u
U �
L }+
a) a)
E
a)
1
c �-
O O O
> O
N L
(U
a)
o � a s a
0 = (n C U
O
•J v( E 'Q
Z V) L O
�X o �z
') a ❑
a) a) p
7 a) L
c= M 3
o 3 L a)
Z � O
I�
J J L O
d o
a E b�0
0 v Ln
Ln
co ~ n
+_% ++ bA
E Cl C
5- iz bA
C O .4,
O i
4�
a) ;
U +s+ fC
a) • a)
Q
3 a)
i it U
O O
m a) L
L
O O O 4-
a) � C
L 3 i O
a
°c E (�
O a)75
a CA
+' N a)
(o
E c E- i
4� 0 0
tn
U U V
a) a v
E Q-
c () a)
Q) L
J 3
a) _O bA V
+' E v r_
L a)
0 -0 E a C
CL a)a) (n C
O f0
i
O oA O U
(u 5
� L t
0 t o a)0 >
�Co
Q1 C i- 4 L
O i E O f6
Z _ z C.
vJ
E
W (n
Lm
o
N. M
L
rn
Vf (Ln
n
J
\
O
v
m
op
E
~
O
r-I
— c
Y O
F- m
\ U
(7 OL13
J
O >'
v�i
m E
�
o
0 3
a
c 0
o
z y
a
L W
O M
O
L —
�
o p
1O
o u
Z
i
N
Z =
4�
C
7
O
E
m a)
O
N
Ln
U
m c
lD
�
O
s
N
N
a
a,
U
a)
O
U O
a) \
EO
m E
En
w
(C
o
z
0
L
L
45
z
�
e
w
m
O
a
m
a°
00
li
0
N
c\-I
N
ice. '>
a)
^FZ L
L @ M
aLn o
d N
N
I @
Q) V) a
CD
a)
H

a
§
§
/
\
>
5
LuLLI
\ �
/ 2
§ /
§
/ z
o
z }
§ <
L
/ /
w >
<
� <
� >
\ J
LLJ
\El
�
<LL- 0
\ 2
0/r
\ \ LLI
§�LU
\
\ LLLL
\
2Lu z0
0
} j Lu
w
o
/
< = G
® o 0 0
$ # $ /
<®©
/ _ § /
$ \ b z
2 < \ <
/ E /
\ \
j < §
/ ®aEL
3 E LLA %
w p 5 /
f
}
�
�
@
�/
a°ƒ
2 { §
\\
2 = V;
_0_
cc
\ k \�
/@G/
m E CU Q \
= o 3 7
\ \ / \
S
c 0
\CL\\
2 G 2 E
® 'o # a
§ » » _
yaR=
2 °°
m t 5 Q
/ \ E )
G g 0 c
c=4z
g£»%
\
o
>°°'
E\\/
CL
c 41
\ / \ E
Et7\
& E ° —
m/§/
am=
(� (/
a \ / E
In0 0
\ \CD w
/
\ v
�y23
3 ®
e»Ea
J t i °
o m / /
�\4-1
M
(Cu,
/\G
//\\
¥\\¥
\ \ \
k\/
5 » S o
0- y 5 =
5 § n
__\/
4&\
e
\ ( \ (
K
G
S
\
\
/ m
a0
\ t
y =
m
°1
\ �
/
\\
�
0
�
�

(�IaneAnalyficale
www.pacelabs.com
December 08, 2020
John Burke
Gilbarco
7300 West Friendly Ave.
Greensboro, NC 27410
RE: Project: Stormwater Sampler
Pace Project No.: 92508405
Dear John Burke:
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
NI I 1 I"171
Stephanie Knott
[e-mail]
336-996-2841
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

laceAnalyfical"
www.pacelabs.com
Project: Stormwater Sampler
Pace Project No.: 92508405
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

(�15'xAnalj&al"
www.pacelabs.com
Project: Stormwater Sampler
Pace Project No.: 92508405
Lab ID Sample ID
92508405001 001 Outlet
92508405002 002 Outlet
92508405003 003 Outlet
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 11/26/20 06:10 11/30/20 11:18
Water 11/26/20 06:00 11/30/20 11:18
Water 11/26/20 05:50 11/30/20 11:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytical
www.pacolabs.com
SAMPLE ANALYTE COUNT
Project: Stormwater Sampler
Pace Project No.: 92508405
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
92508405001
001 Outlet
SM 2540D-2011
MLS1
1
EPA1664B
CJM
1
EPA 200.7 Rev 4.4 1994
IDS
3
92608405002
002 Outlet
SM 2540D-2011
MLS1
1
EPA1664B
CJM
1
EPA 200.7 Rev 4.4 1994
IDS
3
92508405003
003 Outlet
SM 2540D-2011
MLS1
1
EPA1664B
CJM
1
EPA 200.7 Rev 4.4 1994
IDS
3
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

(�15'cieAnalytica(
www.pecolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Project: Stormwater Sampler
Pace Project No.: 92508405
Sample: 001 Outlet Lab ID: 92508405001 Collected: 11/26/20 06:10 Received: 11/30/20 11:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Eden
Total Suspended Solids
136 mg/L
5.3
1
12/01/20 08:27
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
12/08/20 08:35
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
0.013 mg/L
0.0050
1
12/05/20 01:37 12/06/20 17:18 7440-50-8
Lead
0.0050 mg/L
0.0050
1
12/05/20 01:37 12/06/20 17:18 7439-92-1
Zinc
0.077 mg/L
0.010
1
12/05/20 01:37 12/06/20 17:18 7440-66-6
Date: 12/08/2020 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

(�IaceAnalXicalo
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Project: Stormwater Sampler
Pace Project No.: 92508405
Sample: 002 Outlet Lab ID: 92508405002 Collected: 11/26/20 06:00 Received: 11/30/20 11:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Eden
Total Suspended Solids
8.4 mg/L
3.2
1
12/01/20 08:27
1664 SGT-HEM, TPH
Analytical Method: EPA 1664E
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
12/08/20 08:35
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
0.0058 mg/L
0.0050
1
12/05/20 01:37 12/06/20 17:21 7440-50-8
Lead
ND mg/L
0.0050
1
12/05/20 01:37 12/06/20 17:21 7439-92-1
Zinc
0.075 mg/L
0.010
1
12/05/20 01:37 12/06/20 17:21 7440-66-6
Date: 12/08/2020 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

(�15'ne Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Stormwater Sampler
Pace Project No.: 92508405
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Sample: 003 Outlet Lab ID: 92508405003 Collected: 11/26/20 05:50 Received: 11/30/20 11:18 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Eden
Total Suspended Solids
17.7 mg/L
3.4 1
12/01/20 08:27
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L
5.0 1
12/08/20 08:35
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Copper
0.012 mg/L
0.0050 1
12/05/20 01:37 12/06/20 17:37 7440-50-8
Lead
ND mg/L
0.0050 1
12/05/20 01:37 12/06/20 17:37 7439-92-1
Zinc
0.12 mg/L
0.010 1
12/05/20 01:37 12/06/20 17:37 7440-66-6
Date: 12/08/2020 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

(�15'neAnalytical'
www.pacelabs.com
QUALITY CONTROL DATA
Project: Stormwater Sampler
Pace Project No.: 92508405
QC Batch: 583485 Analysis Method: SM 254OD-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92508405001, 92508405002, 92508405003
METHOD BLANK: 3084976 Matrix: Water
Associated Lab Samples: 92508405001, 92508405002, 92508405003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/01/20 08:26
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
LABORATORY CONTROL SAMPLE: 3084977
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 242 97 90-110
SAMPLE DUPLICATE: 3085030
92508454001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 381 411 8 25
SAMPLE DUPLICATE: 3085031
92508461001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 405 370 9 25
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13

aceAnaiXical
www.pacolabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Project: Stormwater Sampler
Pace Project No.: 92508405
QC Batch: 585226
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 SGT-HEM, TPH
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92508405001, 92508405002, 92508405003
LABORATORY CONTROL SAMPLE:
3093376
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 13.5
68 64-132
MATRIX SPIKE SAMPLE:
3093377
92509161001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND 20
ND 2 64-132 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 13

aceAnalytical
www.paceiabs.com
QUALITY CONTROL DATA
Project: Stormwater Sampler
Pace Project No.: 92508405
QC Batch: 584771 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92508405001, 92508405002, 92508405003
METHOD BLANK: 3091372 Matrix: Water
Associated Lab Samples: 92508405001, 92508405002, 92508405003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper mg/L ND 0.0050 12/06/2016:35
Lead mg/L ND 0.0050 12106/2016:35
Zinc mg/L ND 0.010 12/06/2016:35
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
LABORATORY CONTROL SAMPLE:
3091373
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Copper
mg/L
0.25 0.26
103 85-115
Lead
mg/L
0.25 0.25
101 85-115
Zinc
mg/L
0.25 0.25
98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3091374
3091375
MS
MSD
92507513001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qua]
Copper mg/L
212 ug/L
0.25
0.25
0.48
0.48
109
109
70-130
0 20
Lead mg/L
ND
0.25
0.25
0.26
0.26
104
104
70-130
0 20
Zinc mg/L
61.0 ug/L
0.25
0.25
0.33
0.33
109
108
70-130
1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3091376
3091377
MS
MSD
92508491001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qua]
Copper mg/L
0.014
0.25
0.25
0.29
0.28
109
108
70-130
1 20
Lead mg/L
0.0052
0.25
0.25
0.27
0.27
105
105
70-130
0 20
Zinc mg/L
0.038
0.25
0.25
0.31
0.31
107
107
70-130
0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

aceAnalXical
www.pacelabs.cem
QUALIFIERS
Project: Stormwater Sampler
Pace Project No.: 92508405
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 13

(�Ia'ceAnalXical'
www.pacelabs.cem
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Project:
Pace Project No.:
Stormwater Sampler
92508405
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92508405001
001 Outlet
SM 2540D-2011
583485
92508405002
002 Outlet
SM 2540D-2011
583485
92508405003
003 Outlet
SM 2540D-2011
583485
92508405001
001 Outlet
EPA 1664B
585226
92508405002
002 Outlet
EPA 1664B
585226
92508405003
003 Outlet
EPA 1664B
585226
92508405001
001 Outlet
EPA 200.7 Rev 4.4 1994
584771
EPA 200.7 Rev 4.4 1994
584807
92508405002
002 Outlet
EPA 200.7 Rev 4.4 1994
584771
EPA 200.7 Rev 4.4 1994
584807
92508405003
003 Outlet
EPA 200.7 Rev 4.4 1994
584771
EPA 200.7 Rev 4.4 1994
584807
Date: 12/08/2020 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 13

\�_ m
�l
D
1 n
V/ O
O
-1
-C
to
O
D
cn
_
m
me
=1
{�Di
J D
D
Z
W�
m
N
f..j m
\� J
7
U Co cf)
nh
m
L M
n
n
J
o
s
m
s
VI)
%
m
m
m
o
J
�m
6�
m
m
r�
`
eI.
o s
?on
C
rl
N�
D
}
I
j
O
C
c
C,
z
C:
cn ;u
>
r
r
D
C��l
m
mCn
�"
',
C
�rn
mm
m
7I
D
_
�
SJ
m
m
C)
m
-C
NO. OF CONTAINERS
u
--I
2 /6
9oiri Nq
y�'rb
n
?So Via/
�ij s 2 ip
p (i
C'
1-3
G O So
�� ((e Qcss
7p G (O o/
4
p e�di J eJ J
S
re . G(Cy s y�r yS0 y`SO
4ie
p gNiO a�eSs q
G (OoioJNdoy ytio
f
I0
�-
m
..
cn
cn
-0 DD;0
O Ol m
CD V1
�0 O y
CD� r
cc) n O i
N U
GlJ -
p ? (/�
z D
C_
c-t
ct I
O
O
Cf] l J
D
Page 13 of 13

- GVR-226
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 8l3 / 0/ D / 6 / 6/
Facility Name: G i \ kjc(--Lz
County: Gu. � ��— Phone No. 33 6 — S'cj % —
Inspector: = Vr-w ,A' t,
Date of Inspection: i 1 , 6
Time of Inspection:
Total Event Precipitation (inches): (), 3 O
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
1. Outfall Description:
Outfall No. O d Structure (pipe, ditch, etc.): 071T 4-
Receiving Stream:
j �L
Describe the industrial activities that occur within the outfall drainage area:
Q AA, ►cZ;J1—. 0L0-f=rt1 A STVVC�S I Ik✓A-C— . mr=A-4L Sul-" ST4--A-6-E- , CWfi�
Page 1 of 2
SWU-242, Last modified 06/01/2018

7. Is there any foam in the stormwater discharge? o Yes
8. Is there an oil sheen in the stormwater discharge? oYes
9. Is there evidence of erosion or deposition at the outfall?
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: !_ LK O'Vf'V C'C
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 0 o,^1r,-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
I 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
2 3 4 5
XNo.
X No.
Yes o No
n.L 1
i -
1'm-t' s
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

r,. GVR-226
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ e3/.3 / v/ 6 / 6 / 6/
Facility Name: i bc-ru� h t-
County: Gu- �— Phone No. 33 6 S"Ln — roa©
Inspector:
Date of Inspection: t1i I
Time of Inspection: (D a
Total Event Precipitation (inches): Q, 3 D
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signa ure, T =4iA�-t t4h! rPnDA�is accurate and complete to the best of my knowledge:
of Permittee or Designee)
1. Outfall Description:
Outfall No. © 0 Z Structure (pipe, ditch, etc.): D ►ETC-l�r'
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: L-Z
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 (D 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
l 1 2 3 4 5
7.
8.
9.
10.
Is there any foam in the stormwater discharge? 9 Yes
Is there an oil sheen in the stormwater discharge? C>Yes
Is there evidence of erosion or deposition at the outfall? O Yes
Other Obvious Indicators of Stormwater Pollution:
List and describe
No.
XNo.
XNo.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

GVR-226
JM.-
Cnvironmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https:Hdeq.ne.gov/aboutidivisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ C)/3 / 01' c3 / 6 % 6/
Facility Name: i �jC�C-t a L-
County: Gui �— Phone No. 33 h ",5L % — Joao
Inspector: n7w E ?W c r.-
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): Q,3 0
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
U(Signatur of Permittee or Designee)
1. Outfall Description: �
Outfall No. O O Structure (pipe, ditch, etc.):/ � "-Gk-
Receiving Stream:
Vk1wS
Describe the industrial activities that occur within the outfall drainage area:
-7&4c L- P ,U, ilk (� , (fir- �� N -c J s �L-s .
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: LT�'6*-V—
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 1y-` G--
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 � 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
(0 2 3 4 5
7. Is there any foam in the stormwater discharge? o Yes X No.
8. Is there an oil sheen in the stormwater discharge? 9Yes X-No.
9. Is there evidence of erosion or deposition at the outfall? O Yes X No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

GVR-226
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 8/3/ 6/.6 / 6 / 6/
Facility Name: Gi bclZ,,� T_^ t.
County: Gu _ Phone No. 3 3 b 57S o a d
Inspector:7}
Date of Inspection:
Time of Inspection: ` .-2-z A
Total Event Precipitation (inches): 0,3 D
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this sigpature, I certify that this report is accurate and complete to the best of my knowledge:
(Sig ature of ermittee or Designee)
1. Out 11 Description:
outfa11 No. OU LA Structure (pipe, ditch, etc.): Q .] TZAA—
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: 0 JQG a-✓`-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): P'jw1�-'r
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
el) 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
oil 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
01 2 3 4 5
7.
8.
9.
10
Is there any foam in the stormwater discharge? o Yes
Is there an oil sheen in the stormwater discharge? 0Yes
Is there evidence of erosion or deposition at the outfall? O Yes
Other Obvious Indicators of Stormwater Pollution:
List and describe
X No.
No.
No.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.ne.gov/about/divisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 8/,3 / 6/` b / J / 6/
Facility Name: G A bC--(U�- T—✓L C—
County:yV-1 k�V�— Phone No. 33h 7(- % S uLd
Inspector: wo
Date of Inspection: I t 1 � b ) 2-,D
Time of Inspection: � �'Lc 1A�
Total Event Precipitation (inches): ON 0
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By thisA.'gaaturo4Ge a+ tb_ 's port is accurate and complete to the best of my knowledge:
( ignature f Permittee or Designee)
1. Outfall Description:
Outfall No. 00 Structure (pipe, ditch, etc.): PT- z-�
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: C'i.✓L
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals
chlorine odor, etc.): (y ��-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? o Yes
8. Is there an oil sheen in the stormwater discharge? OYes
No.
No.
9. Is there evidence of erosion or deposition at the outfall? o Yes No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018

GVR-226
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deq.ne.gov/aboutidivisions/energy-mineral-land-resources/
npdes-stormwater-gps
Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 8/.3 / 61, 6 / J / 6/
Facility Name: G A bC�,-u- T-^ t_
County: Gvi � �Y�- Phone No. 3U - S"(-j 7 -- road
Inspector: ,o V"') on! i t
Date of Inspection: I 0 I � L
Time of Inspection: 6 � 3 J ►t3 y�
Total Event Precipitation (inches): 0, J 0
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By thi, signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or
1. I-'Outfall Description:
Outfall No. © O -6 Structure (pipe, ditch, etc.): DrA-Z-kA—
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 06/01/2018

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: L-T—�
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 02) 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 02' 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
10.
2 3 4 5
No.
No.
Is there evidence of erosion or deposition at the outfall? O Yes No.
Is there any foam in the stormwater discharge? O Yes
Is there an oil sheen in the stormwater discharge? 9Yes
Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 06/01/2018