Complete File - Historical_MiscSpills

Management - EM43 Reporting
)orting
Taken by:
C Creighton
Reported by:
NRC
County:
Cleveland
Street Address:
135 Old Boiling Springs Rd
Type: HazMat
NCEM Edited:
Yes
Date/Time Reported:
01/24/2020 21:28:27
Agency:
USCG
City:
Shelby
https://www.ncsparta.net/coc7/boards/boarddata.ashx?comman...
EVENT TYPE
Animal Disease Event Type:
Bomb Threat Event Type:
Complaint Event Type:
Fire Event Type:
FNF Event Type:
FNF Class:
HazMat Event Type:
HazMat Class:
Non-LHS
Petroleum
Homeland Security Event:
Non-FNF Event:
Other Event Type:
SAR Type:
Transportation Event Type:
Wastewater Event Type:
Weather Event Type:
Weather Event Name:
State Resource Request
Include in Report:
Yes
Date/Time Occurred:
01 /24/2020 21:00:27
Phone:
800-424-8802
Area:
13
Zip Code:
HazMat Mode:
Other
Non-FNF Event Type:
WMD Event Type:
1 of 1/27/2020, 8:21 AM

Energy, Mineral
and Land Resources
ENVIRONMENTAL QUALITY
,ROY COOPER
Governor
MICHAEL S. REGAN
Secreta,y
WILLIAM E (TOBY) VINSON, JR
Interim Director
July 10, 20,18
NOTICE OF VIOLATIONS OF THE
SEDIMENTATION POLLUTION CONTROL ACT
AND
GENERAL PERMIT - NCG 010000
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT ISCHARGE ELIMINATION SYSTEM
ID
FOR
CONSTRUCTION ACTIVITIES
CERTIFIED MAIL. 7016 1370 0000 2595 8877
RETURN RECEIPT REQUESTED
Maksym A. Stashchak and Marina Stashchack
11 Heritage Acres
Matthews, North Carolina 28104
RE:. Project Name: 4820-4820D Beulah Church Road
Project ID: Not Yet Assigned
County: Cleveland
Compliance Deadlines: 15 days from receipt by certified mail for SPCA violations
15 days from receipt by certified mail for Construction
Stormwater Permit NCG 010000 violations .
Dear Sir or Madame:
On June 28, 2018, personnel of this office inspected a project located on 4820-4820D Beulah
Church Road, Weddington in Union County, North Carolina. This inspection was performed to
determine compliance with the North Carolina Sedimentation Pollution. Control Act (SPCA) of.
1973 and General Permit - NCG 010000 to Discharge Stormwater Under The National Pollutant
Discharge Elimination System for Construction Activities (Construction Stormwater Permit .
NCG 010000). The inspection revealed a land -disturbing activity of approximately 5 acres being
conducted.
lil is our un ers an _ _ ff21Te=re9p0nsi'-th=is=ram _
The purpose of this letter is to inform you that this activity was found to be in violation of the
State of North Carolina I Environmental Quality 1 Energy, Mineral and Land Resources
Mooresville Regional Office 1 610 East Center Ave Ste 301 1 Mooresville, NC 28115
704 663 1699 T

Notice of Violations
Maksym A. Stashchak and Marina Stashchack
July 10, 2018
Page 4 of 4
We solicit your cooperation, and would like to avoid taking further enforcement action. At the
same time, it is your responsibility to understand and comply with the requirements of the SPCA
and Construction Stormwater Permit NCG 010000. Copies of the relevant statute and
administrative rules may be examined at this office or will be sent to you upon request. Should
you have questions concerning this notice or the requirements of the SPCA and Construction
Stormwater- Permit NCG 010000 please contact either Ms. Lily Kay or me at your earliest
convenience.
Sincerely,
Zahid S. Khans/-CPM, CPESC, CPSWQ
Regional Engineer
Land Quality Section
LCK/THE/cys
Enclosures: Sedimentation Inspection Report
Construction Stormwater Permit NCG 010000
Financial Responsibilitrm
Erosion Control Plan Checklist
Resources for Technical Assistance — Erosion and Sediment Control
State Sediment Specialist
ux�er;vrisor Regio-nal,Water�- ualiit5y ®, ��rat�lnns.S_edt orn

of
Land Quality Section: 610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115,
Phone: [phone]
County: Union Project: 4820-4820D Beulah Church Rd. River basin: Catawba
Person Financially Responsible: Maksym A. Stashchak and Marina Stashchack
Project #: Not yet assigned
Address: 1011 Heritage Acres, Matthews, North Carolina 28104
1. Project location:
4820-4820D Beulah Church Road
..........................................
Pictures: No: F Yes: r- Video": F Digital: 17.
Sunny, workable soils
2. Weather & soil conditions: __. .. ...... __ First inspection: Yes: r- No: l
3. Is site currently under notice of violation? Yes: F No: r
4. Is the site in compliance with S.P.C.A. and rules? Yes: [71 No: r If no, check violations below:
5: Violations:
a. No approved plan, G.S. 113A-57 (4) and 15A NCAC 4B.0107(c)
1 b. Failure to follow approved plan, G.S. 113A-57(5)
17. c. Failure to submit revised plan, G.S. I I3A-54.1(b) and
15A NCAC 4B.0118(a)
17 d. Failure to provide adequate groundcover, G.S. 113A-57(3);
15A NCAC 4B.0107(b) or 15A NCAC 4B.0124(e) "
e. Insufficient measures to retain sediment on site, G.S. 113A-57(3)
g. Inadequate buffer zone, G.S. 113A-57(1)
h. Graded slopes and fills too steep,
G.S. 113A-57(2) or 15A NCAC 4B.0124(d)
i. Unprotected exposed slopes, G.S. I I3A-57(2)
j. Failure to maintain measures, 15A NCAC 4B.0113
k. Failure to self -inspect G.S. 113A-54:1(e) and
15A NCAC 4B.0131
F f. Failuretotake all reasonable measures, 15A NCAC 4B.0105 "1. Other describe) ----•- - - -- - - . --........
__ r- XT_- r"' T.T_t .
6. a site m compliance withY000fr? —Yes 1-��� o Appheabl :
If no, check violations below:
U., in.
Failure to manage construction site pollutants, NCG 010000 Sec. II, B.1 17
n. Failure to provide ground stabilization, NCG 010000 Sec. II, B.2
�W o. Failure to maintain rain gauge or record daily rainfall,'
NCG 010000 Sec. II, B.3(a, b)
p. Failure to meet self -inspection and reporting requirements,
NCG 010000 Sec. II, B.3(c4)
q. Failure to dewater sediment basin from surface,
NCG 010000 Sec. II, BA
r7
r. Failure to have approved plan and NPDES
permit on site, NCG 010000 Sec. III, 3(d)
s. Failure to install and maintain BMP's,
NCG 010000 Sec. III, 4
t. Failure to operate and maintain control
measures, NCG 010000 Sec. IV, 1
u. Bypass of stormwater control facilities,
NCG 010000, Sec. IV, 3
v. Other (describe)_........._.._....................__...,..._._....._.......__..........._._...........,
7. Has sedimentation damage occurred: i since last inspection.F at 1st inspection? Yes: 1-1, No: 1
If yes, where? (check all that apply):
Lake/natural watercourse on the tract: 17 Lake/natural watercourse off the tract: 17 Other property: 1-
N/A
Description: .......... .................. ............ ...... . ................ ............. ............ .. ................ ........ ........... . _........... ....................
Stormwater Discharge Outfall with sediment loss N/A
Degree of damage: slight: moderate: r7 severe: F
8. Contact made with. N/A ... .
Date Inspection report sent to financially responsible party With Nov
Report by: Ldy Kay Others present: ... _._.
6/28/2018 11:45 12 00
Date of inspection: -- Time arriving on site. - ----- - Time leaving site: - •..
r, ....r.. ._. r .....- rIeW'111- A 1 paap 1 of')

Land Quality Section: 610 East Center Avenue, Suite.301, Mooresville, North Carolina 28115,
Phone: [phone]
cc:
9. Corrective actions needed
Submit three (3) copies of an approvable sedimentation and erosion control plan and the appropriate
plan review fee to this office. Until the required plan has been. approved, no land -disturbing activity
may be conducted, except that which is necessary to bring the site into compliance. Until an erosion
and sedimentation plan has been approved, any land -disturbing activity, except that which is necessary
to bring the site into compliance, will constitute additional violations of the SPCA and G.S. 143-
215.1(a) and 15A NCAC 02H .0126. Following our review of the plan within 30 days of receipt, this
office will notify you that the plan has been approved, approved with modifications or disapproved.
Following approval of the plan, all land -disturbing activity on the site must be conducted in
accordance with the terms of the approved plan, the SPCA and the implementing rules and
Construction Stormwater Permit NCG 010000.,
10. Comments:
Please give the above your immediate attention.
rl:,v. x f)OfI "YA II Page 2 of 2

Pat McCrory
FiLEI
-&V4
--..^ >r
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
- Thomas A. Reeder John E. Skvarla, III
Governor Acting Director,
July 8, 2013
CERTIFIED MAIL # 7010 0290 0000 4565 1882
RETURN RECEIT REQUESTED
Mr. Gerald Culp, Plant Manager
Buck Eye Fire Equipment
P.O. Box 428
110 Kings Road
Kings Mountain, North Carolina 28086-0428
Subject: Notice of Violation and
Recommendation for Enforcement
Tracking Number NOV-2013-DV-0141
Compliance Evaluation Inspection and
Illegal Discharge
Buck Eye Fire Equipment
COC Number NCG050083
Cleveland County, NC
Dear Mr. Culp:
Secretary
Chapter 143, Article 21 of the North Carolina General Statutes (G.S.) authorizes and
directs the Environmental Management Commission of the Department of Environment and
Natural Resources to protect and preserve the water resources of the State. The Division of
Water Quality (DWQ) has the delegated authority to enforce adopted waste pollution control
rules and regulations.
The Mooresville Regional Office of the Division of Water Quality received a complaint
of foam in a creek through the Division of Environmental Assistance and Outreach (DEAO) on
June 6; 2013. The foam was observed in Long Creek behind,property located at 1005 Serenity
Woods, .Bessemer City. According to the complaint, the foam in Long Creek had been occurring
for several weeks and an Industrial Park off Kings Road was indicated as the area draining to this
creek. Long Creek is part of the watershed drainage area for the drinking water intake to
Bessemer City's potable water supply.
Mooresville Regional Office
Location: 610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone] FAX: [phone]
Internet: http://portal.nedenr.orglweb/wq
An Equal Opportunity 1 Affirmative Action Employer
NorthCarohna
�litllt�l���l, f

Mr. Gerald Culp
July 8, 2013
Page 2 of 3
As a result of the site investigation performed by Ms: Barbara Sifford with this Office
and staff with the City of Kings Mountain (Ms. Kim Moss and Mr. Brian Ramsey) on June 19,
2013, the following violation of G.S. 143-215.1 was observed:
1. There was an unpermitted discharge of wastewater originating from a dike area behind
the plant. This area was noted on the site plan as a concrete containment vessel between
stormwater outfalls 4 and 5. The wastewater in the dike was being discharged by the
siphoning of three garden hoses into a stormwater drainage ditch that flows to. Long
Creek. The unpermitted discharge was creating a white foam in the drainage ditch and in
Long Creek.
Please be advised that pursuant to G. S. 143-215.6A, a civil penalty of not more than
twenty-five thousand dollars($25,000.00) per day, may be assessed against any person who is
required but fails to apply for a permit required by G. S.143-215.1. In addition, pursuant to G. S.
143-215.88A, any person who intentionally or negligently discharges oil or other hazardous
substances shall incur, in addition to any other penalty provided by law, a penalty in an amount
not to exceed five thousand dollars ($5000.00) for each violation. To comply with the
aforementioned general statutes, your facility must cease all unpermitted.'discharges of
wastewater to surface waters of the State of North Carolina.
During the site visit, Ms. Sifford also conducted an inspection of your facility's
stormwater program; including a review of your Stormwater Pollution Prevention Plan (SPPP),
qualitative or analytical monitoring required by the permit, and each of your stormwater outfalls.
Enclosed with this letter is a copy of the Compliance Evaluation Inspection (CEI) report
prepared by Ms. Sifford for her inspection. The site visit and file review revealed that the
subject facility is covered by NPDES Stormwater General Permit NCG050000. The following
observations were noted during the inspection:
1) Stormwater Pollution Prevention Plan (SPPP) Yes X No
A SPPP has been developed and implemented.
2) Qualitative Monitoring Yes X No
Qualitative monitoring has been conducted and is recorded in accordance with permit
requirements. Review pictures on the web site under monitoring guidance for stormwater,
http://portal.ncdenr.org/web/wq/ws/su
3) Analytical Monitoring Yes No. N/A X
Monitoring is not required by NCG050000 permit.

Mr. Gerald Culp
July 8, 2013
Page 3 of 3
It is requested that a written response be submitted to this Office by July 26, 2013,
addressing your facilities actions to eliminate the illegal dike wastewater discharge. Your
response should also include a permanent disposal location of this dike wastewater and whether
or not arrangements can be made to treat this discharge in your pretreatment system prior to
discharge to the City of Kings Mountain sewer system.
Should you have any questions concerning this matter, please do not hesitate to contact
Ms. Sifford or me at [phone], or via email at [e-mail].
Sincerely,
Michael L. Parker
Regional Office Supervisor
Surface Water Protection Section
Enclosure: Compliance Inspection Evaluation
Cc: Cleveland County Department of Environmental Health
Kings Mountain Public Works — Dennis Wells
Bessemer City Public Works — Jamey Ramsey

Permit: NCG050083
SOC:
County: Gaston
Region: Mooresville
Compiiance Inspection Report
Effective: 06/01/13 Expiration: 05/31/18 Owner: Buckeye Fire Equipment
Effective: Expiration: Facility: Buckeye Fire Equipment
102 Industrial Dr
Contact Person: Kevin Bower
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Title:
Inspection Date: 06/19/2013 Entry Time: 02:00 PM
Primary Inspector: Barbara Sifford
Secondary Inspector(s):
Kings Mountain NC 28086
Phone: [phone]
Certification:
Exit Time: 04:00 PM
Phone:
Phone: [phone]
Ext.2196
Reason for Inspection: Complaint Inspection Type: Compliance Evaluation
Permit Inspection Type: Apparel/Printing/Paper/Leather/Rubber Stormwater
Discharge COC
Facility Status: Q Compliant ■ Not Compliant
Question Areas:
■ Storm Water
(See attachment summary)
Page: 1

Permit: NGG050083 Owner - Facility: Buckeye Fire Equipment
Inspection Date: 06/19/2013 • Inspection Type: Compliance Evaluation Reason for visit: Complaint
Inspection Summary:
Intentional illegal discharge from pit behind plant. Three garden hoses were siphoning untreated wastewater from a
process diked area directly to the creek.
Stormwater Pollution Prevention Plan Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan? ■ n n n
# Does the Plan include a General Location (USGS) map?
■
❑ n
n
# Does the Plan include a "Narrative Description of Practices"?
■
n n
n
# Does the Plan include a detailed site map including outfall locations and drainage areas?
■
n n
n
# Does the Plan include a list of significant spills occurring during the past 3 years?
■
n n
n
# Has the facility evaluated feasible alternatives to current practices?
■
n n
n
# Does the facility provide all necessary secondary containment?
■
n n
n
# Does the Plan include a BMP summary?
■
Cl n
n
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
■
n ❑
n
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
n n
n
# Does.the facility provide and document Employee Training?
■
n n
n
# Does the Plan include a list of Responsible Party(s)?
■
n n
n
# Is the Plan reviewed and updated annually?
■
n. n
n
# Does the Plan include a Stormwater Facility Inspection Program?
■
n n
n
Has the Stormwater Pollution Prevention Plan been implemented?
®
n n
n
Comment:
Qualitative Monitoring
Yes
No NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■
n n
n
Comment:
Permit and Outfalls
Yes No NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
# Were all outfalls observed during the inspection?
# If the facility has representative outfall status, is it properly documented by the Division?
# Has the facility evaluated all illicit (non stormwater) discharges?
Comment: Discharge from pit was notina designated outfalI area.
Page: 2

Report to: M Q0 S w P WATER QUALITY SECTION Page _L of
CHAIN OF CUSTODY (COC) RECORD
NC DENR/DWQ LABORATORY (check one): Er/CENTRAL [ ] ARO [ ] WaRO
l nvestigation of:
l
(� •_ _ j_„
ibL\ �Gvwlt'
Sample collector (print name) Q,,
and DM-1 forms completed by: /
C ,1
�r0. 01� U
% ,
Sample collector's signature: (%
Field storage conditi s d locat' n (when applicable):
Lab Use Only
LAB NO.
STATION NO.
STATION LOCATION
A E
SAMPLED
TIME
SAMPLED
NUMBER
OF
CONTAINERS
�1` , 88 . _
UMIS �o$3
� I� - 0 3 501VWA *�
r � �
io S�
�
7
oscx3
ar�
�a
�v '.15 Arc
uiir - gni
OFFICE
Re li uis d b (si e):
D to
Time
3;Is(
Received i atu e
m
:
f 11
Date
11413
Time
0-0
1: _quished by (sign e):
Date
Time
Received by i ature): I
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one): tate Couri Hand -delivered Federal Express UPS
Other:
S
Security Type andConditions:16,
Sealed by:
Broken:by:
M
INTRALABORATORY CHAIN OF CUSTODY - Lab Use Only
'-LAB.NUMBERS :.., -..",NUMBER.
:.:. ANALYSES, . ,
RELINQUISHED,',,
.-RECEIVED .::.. - ;_
DATE :
TIME , -
FROM -. THROUGH:
BOTTLES
i : •REQUESTED .` ,
'BY:
BY-.
:..7 rn
_
QA\Forms\Sample Receiving\COC form WQ 4/10/01dbs

County: CLEVELAND
\NAj
Sample ID:
AB97885
River Basin
{7r ,
Q�
PO Number #
13W5476
Report -To MROSP,
ti4�
Date Received:
07/1712013•
Time Received:
08:00, '
Collector: B SIFFORD
Labworks LoginlD
HMORGAN
Region: MRO
Final ReportDates
7/30/1.3.
Sample Matrix: SURFACEWATER
Final i�'eport'
Report Print Dates
07/30/2013
Loc. Type: RIVERISTREAM
Emergency Yes/No..
VisiflD
CDC. Yes/No YES
Loc.Desen: STINETT FARM
Location ID: NCG650083
Collect Date: 'DM212013
Collect Time: 10:15
Sample'Depth 1.0
IF this report is labeled prellininary report, the results have not been validated. Do not use for Regulatory purposes.
Result/,,
Method
Analysis ; , a , •,
tIM0 ft
r%ndryte Idatrlc:
r�[�
Qualifier
vruca
Reference'
Date.
LAB
Sample temperature at receipt by lab
0.3
°e
7117(3
HMORGAN
WET
Chemical Oxygen Demand in liquid
20,
20 U
mg/L
Hach 8000
711.9/13
CGREEN
NUT
NH3 as N in liquid
0.02
0.03
mg/Las N
Lac107107-06-1-J
7117/13
CGREEN
Total Kjeldahl N as N In liquid
0.2
0.41
mg/L as,N
Lachafl07-06 2-H
7123113
CGREEN
NO2+NO3 as N in liquid
0.02
0A9
mg/Las N
Lac10-107-04A-c
7/1711.3
CGREEN
Phosphorus_ total as P in liquid
0.02
0.14
mg/Las:P
Lac 10-115-01-1EF
7122/13
CGREEN
Laboratory -Section» 1823 Mail service Center,; Raleigh,: NC .27699.1623 [phone]
For a'detailed description otthe qualifier modes ' -refer to ht6Yf i+ a; cc+en:. s'ef v uhdcjia6trtnfl,rNok••thai utRn nx c?uayrte rude w,'p l nn ni,l :a Plwzbf++ratr dr f xi�rfluteefox>ar r>
Page 1 of 1

County*
River Basin
Repo To
CLEVELAND
MROSP
bo(lector:
B SIFFdRD
Regiort:
MRO
Sample Matrix:
S URFACEWATER
Loc. Type:
RIVERATREAM
Emergency Yes/No.
COCYes/No,YES
'A
0" -VI
Final Repoft,
Visitil)
L:qc.,De.scr.; STINiTT FARM
Sample ib:t
PO Number#
Date Re-cOved'
Time Received:
LabWorks Loglh'ID
Firial Report Date:
Report Print Datw,
AB97885
13WS476
071i7%2013v
HMORGAN
7130/13
07/30/2013
:1
Location lb: NCG656083. Collect bate: 67/'12/2'0.13 Collect Timer 10:15 SampleDeph .0
ff.this:rpportislabeled ,preliminary. ,report, the results have not been validated. Do: not use,for Regulatbty purposes..
CAS # Analyte Name
'POL Units
QuIliffe
"'VOP' Validated by
. Date�
LAB.
Sample temperature at r6ceipt b 7/171,3 HMORG:,�N
y lab
WET
Chemi6a[ Oxygen Demand in liquid, 20: 20'U rbg!L Hadh 8000 7/19/13 CGREEN
NUT'
NH3 as. N in liquid
0-02
0.03
mg/Las N
Lac10-101-06-1-4
7/11/13
CGREEN
a
Total . Kjeld hf N as N in liquid
0.,2
0.41
mg/L as
Lachatl 07-06-2-H
7/23/13
CGREEN
NO2+NO3 ap,N in liquid
0.02
0.19
mg&�qs N
LacI0-107-04-1-c
711710,3
'CGREEN
Phosphorus —total as in liquid.
0.102
0.14
mg/L as. P
Lac10-'115-01-1EF
7/22113
CGREEN
LaborAWiV. Sectldh:?> 1623 Mall SeNide Cehtet,;RaI6Igh,:NC 27699.1623 [phone]
Fore ddWiled descripflon of the quafifer'Codes refer to
Page 1 of 1

County: CLEVELAND�
A
Sample ID:
AB97884
River Basin
;
Q�
P.O Number#
13W6475
ReportTo MROSP
Date Received:
07117/2013
Time Received:
08:00
Collector: B SIFFORD•
Labvorks LogihlD
HMORGAN
Regions MRO;
Final Report Rate:
7131/13
Sample. Matrix: SURFACEWATER
Final Report
Report Print Dates
08701/2013
Loc. Type: RI1/ERISTREAM
Emergency Yes/No.
Visi41D
COC`. Yes/No YES
Loc. Descr.: 'SW-03
Location ID: NCG650083
Collect Date: 07/12%2013
Collect Time: 10.56
Sample Depth 1_0
If this -report is labeled preliminary report, the results have not been validated. .Do not use for Regulatory purposes.
Result/`
Method
Analysis flail info i by
VIIV. ffi' (lllWylG 11011ll3 1�%L 'vuias
Qualifier Reference; .Date:
LAB
Sample' temperature at receipt by lab 0.3 oC. 7/17/13 I-iMO..RGAN
WET
Chemical Oxygen Demand in liquid 20 47 mall Hach 8000' 7119/13 CGREEN
NUT
NH.3 as N.in liquid
0.02'
0.02
mg/Las N
Lac10-107-06-1 J
7/17/13
CGREEN
Total Kjeldal l N as N In liquid
0.2
0A9
mg/Las N
Lachat107-06-2-H'
7422/18
CGREEN
NO2+NO3 as N in liquid
0.02
0.10
mg/Las'N
Lad 0A 07-04-1. c
7117/13
CGREEN
Phosphorus_ total as P in liquid
0.02
IX
mg/Las; P
Lac10-115-01-lEF
7/22113
CGREEN
MET
7440-38-2
AsbyICPMS
2 0
2'.0 U
uglL
EPA 200:8
7123/13
ESTAFFORDI
7440-47-3
Cr by _ICPMS
10
1D u
4g/L
EPA200:8
7123/13
ES.TAFFORD1
7440-50-8
Cu by'ICPMS
2:0
4.7
ug/L
EPA200.8
7123/13
ESTAFFORD1
7440-02-0
Ni by-ICPMS
2:0
$;0
U91
EPA200;Z
7/23/13
ESTAFFORDI
7439-92-1
Pb by ICPMS
2.0
2.0 U
ug%L
EPA 200.'8
7123/13
ESTAFFORDI
7440-66-6
Zn by ICP'
10
$$
us1L
EPA200.7
7/23/13
ESTAFFORDI
Laboratory Section» 1623 Mail Service Center;, Raleigh;, NC 27699.1623 [phone]
Fora detailed -description of the quaiiher.,codes reel' IQ'8 t i•.jP,p� rat nai n"r.orq i, pbf�u�1 674 Nrrti (tech'rssict#nSta., ea IRP Csd :,.ct :c-tl rsA' x. n v� r.rlralwrb/ngto-a6/ t fi fiole- Fra {sr>
Page 1 of 1

DWISIO OF WATER QUALITY
/ Chemistry Laboratory Report / Water Quality
COUNTY PRIORITY SAMPLE TYPE
.
RIVER BASIN: AMBIENT VIIAINOFCUSTODY
�TREAM
r rc ❑
REPORT TO anal Office COMPLIANCE LAKE
Other17� ��(� EMERGENCY VISIT
ID ESTUARY
COLLECTOR(S) (A r a I (}wry ,
Estimated BOD Range: Station Location!'��" ' µrwl
Seed: Chlorinated: Remarks:
13W 510__�
El EFFLUENT
❑ INFLUENT
Lab Number`.'
Date Received: ++
Time Received: ' 1 • f3
Received By O D'Irt
Data Released :
Date Reported:
Ibtation Nflpcatiou
VV int/mm/dd)
dd) I Date End (yy/mm/dd) I Time Begin Time End I Depth - DM, DBt�M, I Value Typq- A, H, L Composite-T, S. B Sample Type
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: NIF Feral 31616 /100ml
Coliform: MF Total 31504 /100ml
Coliform: tube Fecal 31615 /100ml
Colifarrn: Fecal Strap 31673 /100ml
Residue: Total 500 mg(L
Volatile 505 mg/L .
Fixed 510 mg(L
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mg/L
pH 403 units
Acidity to pH 4.5 436 mg/L'
Acidity to pH 8.3 435 mg/L
Alkalinity to pH 8.3 415 • mg(L
Alkalinity to pH 4.5 410 mg/L
TOC 680 mg(L
Turbidity 76 NTU
Coliform Total Tube /100 ml
Chlbride 940 mp/L
Chlorophyll a EPA 445.0 modified option • ug/L
Color: Tme 80 c.u.
Color: (pH) 83 pH= C.U.
Color: pH 7.6 a2 C.U.
Cyanide 720 mg/L
Fluoride 951 mg/L
Formaldehyde 71980 mg/L
Grease and Oils 556 mg/L
Hardness Total 900 mg/L
Specific Cond. 95 umhos/cm
MBAS 38260 mg/L
Phenols32730 ug/L
Sulfate 945 mg/L
Sulfide745 mg/L
Boron
Tannin & Lignin ug/L
Hexavalent Chromium ug(L
Bicarbonate mg/L
Carbonate mg/L
Total Dissolved Solids mg/L
NH3 as N 610 - mg(L
an N 625 mg/L
NO2 plus NO3 as N 630 mp/l,
P: Total as P 665 m&L
PO4 as P 70507 mg/L
P: Dissolved as P 666 mg/L
K-Potassium mg(L
Cd- Cadmium 1027 ug/L
Cr-Chromium:Total 1034 ug(L
Cu- Copper 1042 ug/L
Ni-Nickel 1067 ug/L
Pb- Lead 1051 ug/L
Zn- Zinc 1092 ug/L
V-Vanadium ug/L
All- Silver 1077 ug/L
Al- Aluminum 1105 ug/L
Be- Beryllium 1012 - ug/L
Ca- Calcium 916 mg/L
Co- Cobalt 1037 ug/L
Fe- Iron 1045 ug/L
Ma -Molybdenum , ug/L
Sb-Antimony ug/L
Sn-Tin ug/L
TI-Thal Iium ug/L
Ti-Titanium ug/L
Hg-1631 ng/L
ium 1132 ug/L
agnesium 927 mg/L
anganesr1055 ug/L
dium 929 mgJL
jAmenic,.Total
1002 ug/L
lenium 1147 ug/L
Hg- Mercury 71900 ug/L
Ba-Barium ug(L
Organoehlorine. Pesticides
Organophosphorus Pesticides
Organ onitrogea.Pestici d es
Acid Herbicides.
Base(Neutral&Acid Extractable Organics
TPH Diesel Range
Purgeable Organics (VOA bottle req'd)
TPH Gasoline Range
TPH/BTEX Gasoline Range
Phytoplankton
Temperature on arrival (eC): 'L/ f3

Report to: M i2o S Uo p WATER QUALITY SECTION Page _L of
r�1
CHAIN OF CUSTODY (COC) RECORD
NC DENR/DWQ LABORATORY (check one): [j/CENTRAL [ 1 ARO [ I WaRO
ivestigation of:
aample collector (print name) ((
DM-1 forms CA. f G�. ��'Si�p ice}
r
and completed by:
Sample cotlector's signature: (%
Field storaag`i s e cconnditd locat n (when applicable):
%QD
:. LabUse:OnlyMIMI
01NUMBER
IJ A
TIME
OF
LAB NO.`:`: = .`,'
STATION NO.
STATION LOCATION
SAMPLED
SAMPLED
CONTAINERS
& r 4Yr srA'` 'r'Lx
Rel• uisd b (si t e):
D to
Time
Received i natu e :
Date
Time
J�j
" jig
luished by (sign e):
Date
Time
Received by i ature): I
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one): tate Cour' Hand -delivered Federal Express UPS Other:
Security Type
Sea ed by:
Broken:by
and onditions:.��f(1
�?tO
r r {
96
INTRALABORATORY CHAIN OF CUSTODY - Lab Use Only
LAB NUMBERS:::'::i:
r_
NUMB
ANALYSES,:;;:.'
:RELINQUISHED„ :t
RECEIVED.:'`::. -
:DATE"
..T1ME­.:
1FROM r THROUGH _
BOTTLES
—REQUESTED
13. 3r '
BY :.:
> T
'
Elk
�A .� y t&#
d �':V y:
F
6$*."9r
aro
.Xr«•''s
k u�1
..•
,✓'] (a�y�•
�
t jjk�s�
i
Kv
I
�l = r�
sxq
��
!" J
y�j ;rn'j('
._•'•• s
r.
\:
R
�
GCS-
'
�
;
> �
- :;•
S 4"ril`3
., ad
,.
QA\Forms\Sample Receiving\COC form WQ 4/10/01 dbs

- - FIRE 011EQUIPM
July 23, 2013
Mr. Michael L. Parker
Regional Office Supervisor
Surface Water Protection Section
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
E-mail: [e-mail] Internet: http://www.buckeyef.com/fire
Re: Notice of -Violation and Recommendation of Enforcement
Tracking Number NOV-2013-DV-0141
Compliance Evaluation Inspection and Illegal Discharge
Buckeye Fire Equipment Company
COC Number NCG050083
Cleveland County NC
Dear Mr. Parker:
PF:Cys fED
DI VISIOlq CA "-N E'ER Q$.lA,L$ijV
FjUL 2 6 2013
In response to your letter dated July 8, 2013 for a request of a written response to eliminate the illegal
dike wastewater discharge. The procedure listed below will eliminate any further dike discharge.
Our SOP for disposal of the rainwater that has accumulated in that lower containment area has always
been to pump it into 275 gallon totes and treat it through our waste water treatment facility.
Moving forward, this procedure will be followed exactly and closely monitored by senior plant
management.
This material is non -hazardous and can be easily treated by our approved pretreatment system prior to
discharge. Again, this process will be carefully monitored and documented.
It should be noted that the containment area, because of natural evaporation, rarely needs to be
emptied.
If you should have any questions to this procedure please give me a call at 704-739-7415.
Sincerely,
Gerald Gulp
Plant Manger, Buckeye Fire Equipment Company
Buckeye Fire Equipment Company
ISO 90012000 Registered

r,
FOAM BIODEGRADATION IN THE ENVIRONMENT
Because of the widespread use of fire fighting foam con-
centrates, there exists the potential for a large release of
this material into the environment. Although this is a small
risk, it is important to ensure that these products are as
safe for the environment as possible.
With increasing awareness and corporate responsibility
from the Fortune 500 companies, the indiscriminate dis-
charge of fire extinguishing media to the environment has
been greatly reduced. There are however periodic dis-
charges of fire protection systems and these could be
classified, or fall into two (2) categories; accidental and
deliberate. In other words, a system could discharge as a
result of a malfunction, in for example a detection sys-
tem, thus producing an "unwanted" discharge. Then there
is the deliberate or planned activation of a system for test
purposes, or the designed activation in the event of a fire.
The later two examples are "wanted" discharges. In ei-
ther case though, extinguishing media has been dis-
charged into the environment.
Buckeye Foam Concentrate formulations are configured
for as rapid degradation as possible, thereby preventing
surfactant buildup and accumulation in the environment.
Biodegradation is a key element in reducing the environ-
mental load or burden associated with the high volume
use of surfactant chemicals.
There are effectively seven factors when considering the
environmental impact of foam concentrates and all of
these factors are of concern when the end -use foam so-
lutions reach natural or domestic water systems. These
factors are: 1). Fluorochemicals, 2). Fish Toxicity, 3). Bio-
degradability, 4). Sewage Treatment Plant Treatability, 5).
Nitrogen, 6). Phosphates, 7). Heavy Metals. To deter-
mine the effect that the foam concentrates might have on
the environment, they are subjected to a series of tests.
To ensure accurate, repetitive and un=compromised data
for use by commercial & governmental organizations, an
independent laboratory performs the m�jority of these
tests. � .
In the early 1990's a solvent called butyl carbitol (di -
ethylene glycol butyl ether {DGBE)) was used as a
5
TECHNICAL BULLETIN BUCKEYE FIRE FIGHTING
FOAM PRODUCTS AND THE ENVIRONMENT
foam enhancer in most aqueous film forming foam
(A.F.F.F.) concentrates. This material subsequently
found it's way on to the Federal Register of Hazard-
ous Air Pollutants. Thus every time this material was
released to the environment, including that contained
in the A.F.F.F. products, it was necessary to report
that "spill" to the Environmental Protection Agency
(E.RA.). Some of the A.F.F.F. manufacturers responded
by re-formulating their products to remove the butyl
carbitol. Buckeye was one of those manufacturers and
we took a corporate. responsibility to make ourA.F.F.F.
products as "Environmentally Friendly" as possible,
while still maintaining the highest level of fire fight-
ing performance.
FLUOROCHEMICALS
During May of 2000, The 3M Company decided to dis-
continue its A.F.F.F. product line with the effective end of
production occurring sometime around November 2001.
The reason for this withdrawal was based on test results
that determined a base material used in the production
process (perfluorooctyl sulfonate) is considered P-B-T
(Persistent, Bio-accumulative & Toxic) and as such fur-
ther use would be harmful to the environment. It is very
important to state that the major contributor to
fluorochemical build-up in the environment is not by fire
fighting foam concentrates but by the 3M-fabric
protectorant, Scotchgard® and other complimentary prod-
ucts used to protect food -wrapping paper. In fact, fire fight-
ing foam concentrates represent less than 2% of the
fluorochemical use, worldwide. There is no doubt that
these fluorochemicals are long lasting and the announce-
ment by 3M has highlighted this issue. Foam concentrates
manufactured by Buckeye DO NOT CONTAIN (PFOS),
the P-B-T fluorochemical used in manufacturing the 3M
product. For the foreseeable future, we expect A.F.F.F.
concentrates to be freely available, since they are con-
sidered "essential" products for life safety.
Fluorinated Surfactants
All A.F.F.F. fire -fighting agents, (standard and alcohol
resistant), along with the fluoroprotein and film form-
ing fluoroprotein (F.F.F.P.) foam concentrates contain
fluorinated surfactants. They are a key ingredient;
which provides these agents with the required low
110 Kings Road, Kings Mountain, NC 28086-0428 • Tel [phone] • Fax [phone] • www.buckeyef.com

0
surface tension (15 to 17 dynes/cm) and positive
spreading coefficient that enables film formation on top
of most hydrocarbon fuels. The chemicals used to pro-
duce fluorinated surfactants can be manufactured by
different processes and have different chemical struc-
tures. The fluorinated surfactants used in A.F.F.F. are
produced from fluorochemicals manufactured by
two methods: electrochemical fluorination and
telomerization.
Electrochemical Fluorination
The key fluorochemical raw material produced by elec-
trochemical fluorination is perfluorooctane sulfonyl fluo-
ride (POSF). POSF has been produced since the
1950s for the synthesis of fluorochemicals used in
paper and packaging; textile, leather, and carpet treat-
ment; industrial surfactants, additives, and coatings;
and surfactants in fire fighting foam agents such
as A.F.F.F. The degradation of POSF-derived
fluorochemicals as well as the hydrolysis or neut-
ralization of POSF results in the formation of
perfluorooctyl sulfonate (PFOS). PFOS is currently a
major focus of the U.S. EPA's regulatory activities.
PFOS - What are the issues?'
The EPA has published a hazard assessment (not a
risk assessment) that categorizes PFOS as P-B-T:
P = persistent
B = bio-accumulative
T = toxic
PFOS has been found in the blood of workers han-
dling the chemical, the general U.S. population, people
in other developed countries, and in wild birds and fish.
Levels detected in workers were as high as 12 parts
per million (ppm) and levels detected in the general
population were in the 30-50 parts per billion (ppb)
range.
PFOS - How big a risk is it?
The EPA does not believe that the current situation
presents an imminent health risk to the general popu-
lation, but the EPA has concern for potential future risk
if PFOS continues to be produced and released to the
environment. The EPA has questions and concerns
about occupational exposures to PFOS.
PFOS -What is being done?
3M will voluntarily phase out manufacture of POSF-
derived fluorochemicals for use in performance prod-
ucts (which includes Light-WateO A.F.F.F.) by Decem-
ber 31, 2002. (A.F.F.F. concentrate production ceased
prior to this date). The EPA has proposed a Significant
New Use Rule (SNUR) that is intended to "close the
door" on future manufacture and import of POSF-de-
rived fluorochemicals as well as PFOS.
Impact of The EPA's Actions
The EPA's initial actions and 3M's phase out apply only
to PFOS and its derivatives. Telomer-based A.F.F.F.
will continue to be produced and no disruption of sup-
plies will or has been experienced. The EPA is cur-
rently assessing other perfluorinated chemicals like
PFOA and related chemistries such as telomer prod-
ucts (see below). Telomer-based A.F.F.F. does not con-
tain PFOS or any other compound currently consid-
ered by regulatory agencies to be P-B-T. There is no
known biological pathway by which telomer-based
A.F.F.F. can be oxidized or metabolized into PFOS.
Telomer-based A.F.F.F. agents contain 30-60% less
fluorine than A.F.F.F. based on POSF-derived
fluorosurfactants.
Perfluorooctanoic Acid (PFOA)
The predominant production of PFOA is also by the
electrochemical fluorination process. The EPA is cur-
rently assessing the hazard of PFOA and expects to
publish a hazard assessment sometime before mid -
2002. PFOA is known to be persistent, and substan-
tial toxicity data on PFOA exists in public literature and
regulatory agency files. Telomer-based A.F.F.F. is not
made from PFOA-based products.
Telomers
Telomers is a term used to describe the most common
synthetic route for manufacturing perfluoroalkyl com-
pounds that have straight chains of 6-14 carbons. The
fluorochemical portion of telomer molecules is
persistent, but preliminary data on toxicity and
bioaccumulation indicate that telomers are very differ-
ent when compared to PFOS. In order to better under-
stand the potential environmental effects of telomers,
the manufacturers have begun a voluntary research
program, the results of which will be shared with the
EPA and others. The EPA will be assessing the envi-
ronmental hazard presented by telomers over the next
few years based on existing data and new data gener-
ated by the TRP (Telomer Research Program) and
elsewhere.
Telomer Research Program (TRP)
The TRP is a science -focused research consortium
funded by global fluorotelomer manufacturers. The
TRP is conducting a 2-3 year research program on
common raw material: Telomer 8-2 alcohol. The test-
ing program includes studies on pharmacokinetics
(how the compound is metabolized), environmental
fate and effects (what does the compound break down
110 Kings Road, Kings Mountain, NC 28086-0428 • Tel [phone] • Fax [phone] • www.buckeyef.com

into in the environment and what are the. effects) and
toxicity.
A.F.F.F. Manufacturers
What are A.F.F.F. manufacturers doing to address the
environmental concerns aboutA.F.F.F.? A.F.F.F. manu-
facturers, in conjunction with fluorosurfactant manu-
facturers and telomer producers, have formed the Fire
Fighting Foam Coalition (FFFC). The founding mem-
bers of FFFC include, Buckeye, Ato-Fina, Dupont,
Dynax, and other foam concentrate manufacturers.
FFFC was formed to represent the A.F.F.F. industry's
interests on all issues related to the environmental
acceptability of fire fighting foams. The coalition pro-
vides a focal point for industry science reviews, devel-
opment of industry positions, and interactions with the
EPA and other relevant organizations.
FISH TOXICITY
Foam solution "run-off' is always a concern in fire -fight-
ing operations, since that "run-off' could work it's way into
streams, rivers and the ocean. However, it is also impor-
tant to consider the fuel involved in the fire, which when
spilled can also present a potentially larger problem in
terms of aquatic toxicity, than the foam/water solutions.
Fish are relatively sensitive to the presence of pollutants
in the water and as such, foam solutions are tested to
determine fish toxicity. These tests are normally run on
both estuarine and fresh water species, with the two most
common test species being the Killifish and the Rainbow
Trout. The Killifish is tolerant while the Rainbow Trout is
sensitive. The tests on these two species gives an indi-
cation of the broad range over which various fish popula-
tions may be affected. The results are given as the 96-
hour LC/50, a measurement of the concentration lethal to
50 percent of the test population, during a 96-hour pe-
riod. The units of measure are milligrams/liter or parts
per million (ppm). The higher the values on the test, the
greater the tolerance of the fish to the Buckeye Foam
Products. For Rainbow Trout we found that the test 96
LC/50 values range from 4,500 to 7,000 ppm while Killi-
fish have a 96 LC/50 range from 25,000 to 37,000 ppm.
There is some debate as to the exact reason the fish die;
in some cases, it may not be a chemical effect from the
foam concentrate, but rather an inability of the fish to
"breathe" as a result of oxygen depletion in the water.
Based on the test results, fish toxicity is not of particular
concern for the synthetic foam concentrates.
BIODEGRADABILITY
The biodegradability of Buckeye foam solutions is depen-
dent on a number of factors. For example: the amount of
rl
dilution that occurs prior to a release and the area in which
the release occurs. To determine the biodegradability of
these solutions two tests are conducted and a relation-
ship between the two results developed. The two tests
are BOD (Biological Oxygen Demand) (oxygen demand
by the microorganisms) and COD (Chemical Oxygen
Demand) (oxygen used in chemical decomposition). COD
measures how much oxygen would be required to com-
pletely break down the chemicals contained in the foam
solution. BOD then measures how much oxygen the bac-
teria will consume as they use up ("eat") the chemicals
found in a given amount of foam solution. For an A.F.F.F.,
the BOD test is carried out over a 20-day cycle. Since
most foam solutions have a BOD/COD over 0.5 or 50%
they are considered relatively biodegradable.
SEWAGE TREATMENT PLANT TREATABILITY
Buckeye foam products are not particularly toxic to the
ultramicroscopic size organisms found in water treatment
plants. For water treatment plants that use the activated
sludge process for secondary treatment, Buckeye Foam
Concentrates may cause foaming, the foam could then
carry over (and. out of the plant) suspended solids and
consequently, a large amount of the microbial population,
reducing the effectiveness of the plant. Solutions of Buck-
eye foam products, up to 300 ppm can typically be handled
without adverse effects. For the most part, the dilution,
which takes place on the way to the water treatment plant,
brings the concentration down below the 250-ppm level.
If it does not, the use of a de -foaming agent such as
Dimethylpolysiloxane, Dow Corning H-10, DB 110A, 1410
or Henkel WB-209, which are compatible with the treat-
ment plant's flora, may allow handling of concentrations
above the 300-ppm level.
NITROGEN
Some of the surfactants used in synthetic foam concen-
trates may contain small amounts of nitrogen in an or-
ganic form, however, the level is relatively low and little
environmental impact can be expected.
The protein based foam concentrates contain substan-
tially more organic nitrogen than synthetic foam concen-
trates and will act as very effective fertilizers promoting
excessive growth of plants and algae in waterways.
PHOSPHATES
It is remotely possible that some cheaper foam com-
pounds could contain phosphates. Phosphates act as
fertilizers and will promote excessive growth of some
110 Kings Road, Kings Mountain, NC 28086-0428 • Tel [phone] • Fax [phone] • www.b

plants and algae. Discharging phosphates into a body of
water can damage the ecology by,promoting excessive
plant growth along the banks that could block waterways.
Buckeye Fire Fighting Foam Concentrates do not con-
tain phosphates.
HEAVY METALS
Heavy metal ions such as zinc can be found in some pro-
tein foam concentrates and could accumulate in living or-
ganisms, which can be harmful. Releasing heavy metals
to the environment should be avoided whenever possible.
CURRENT POSITION
Early on, Buckeye took a position to produce foam con-
centrates with the lowest possible environmental impact
and the highest possible fire fighting effectiveness. The
world is becoming smaller and more aware of the impact
associated with the chemicals we use in our everyday
operations. Anything not of a naturally occurring sub-
stance, such as man-made chemicals are likely to be
undesirable for the environment and discharges should
be limited.
Buckeye formulates Earth Friendly Foam Concentrates
without DGBE. This decision was based on information
generated from the market place, with origins dating back
to 1993. As a result of a ruling by the E.P.A. (Environmen-
tal Protection Agency) in 1993, A.F.F.F. concentrate or
A.F.F.F. solution discharges became a reportable incident
under EPCRA, (Emergency Planning and Community
Right -to -Know Act), SARA Title III. This was because the
majority of these foam concentrates contained the glycol
ether called butyl carbitol or DGBE. The glycol ether is or
was used as a'foam-enhancer'to improve the foamability,
increase burnback resistance and produce rapid knock-
down capabilities. Once one (1) pound (0.45 kg) of glycol
ether was spilled, (this represents approximately one [1]
gallon or 3.8 litres of foam concentrate), it was consid-
ered a reportable incident, since this material was listed
on the Federal Register as a toxic hazardous material;
specifically a hazardous air pollutant.
In 1996 the reporting procedures for A.F.F.F. foam/water
solution discharges containing glycol etherwere lifted and
now there are no minimum reportable quantities. How-
ever, even though it is not now necessary to report these
discharges, the owner is still responsible for proper clean-
up and disposal of any foam/water solution containing
glycol ether. It therefore makes environmental and com-
mercial sense to use A.F.F.F. concentrates that do not
contain glycol ether.
Thus foam concentrates offering the lowest environmen-
tal impact should be chosen over those with higher envi-
ronmental impact.
To further reduce environmental impact Buckeye offers
an environmentally benign, non -foaming agent that can
be used for testing foam systems. This agent mimics ex-
actly, the "real" foam concentrate and simulates the per-
formance of the system to verify proportioning accuracy.
Additional information on this innovative method is avail-
able from the Buckeye Foam Systems Engineering De-
partment.
Trying to determine the foam concentrate demonstrating
the lowest environmental impact is a difficult task. This is
made more complex due to a lack of complete and accu-
rate information. Any claim that a regular protein based
foam concentrate has lower environmental impact than a
fluorosurfactant based foam concentrate cannot be sub-
stantiated. These two types of foam concentrate affect
the environment in different ways, but neither can be
shown better or worse than the other. Thus proper evalu-
ation of the M.S.D.S. (Material Safety Date Sheet) should
be exercised and the appropriate decision made.
Buckeye has a Technical Support Department that can
provide additional information and updates to these very
important environmental issues.
110 Kings Road; Kings Mountain, NC 28086-0428 • Tel [phone] • Fax [phone] www.buckeyef.com

FIR75.
EQUI
September 26, 2012
Mr. Robert B..Krebs
Regional Supervisor
Surface Water Protection Section
610 East Center Avenue
Suite 300
Mooresville, NC 28115
Dear Mr. Krebs:
Subiect•
Notice of Violation
Compliance Evaluation Inspection
E-mail: [e-mail] • Internet: http://www.buckeyef.com/fire
I
Buckeye Fire Equipment
NPDES Permit No. NCG050000
COC No. G50583 Ate-6 ® y .3
Gaston County, NC
RECEIVED
DIVISION OF WATER QUALITY
SEP 27 2012
SVVP SECTiON
N",OO ESVILLE REGIONAL OFFICE
I have enclosed the Stormwater Pollution Prevention Plan for Buckeye Fire Equipment Company that
was prepared by David D Smith and Company, PLLC. Also is enclosed is the Additional MSGP
Documentation plan.
These plans should meet the requirements of the permit. The company is committed to meet all
requirements that are required by all state and federal agencies. If you have any questions please do not
hesitate to give me a call at 704-739-7415 ext. 3327.
Sincerely,
Barbara McDonald
Human Resources/Safety Manager
Enclosures (2)
Buckeye Fire Equipment, Company
ISO 9001 Registered

Stormwater. Pollution Prevention Plan
prepared for:
Buckeye Fire Equipment Company
110 Kings Road
Kings Mountain, NC 28086
Tel. [phone]
SWPPP Contact:
Buckeye Fire Equipment Company
Gerald Culp, Plant Manager
110 Kings Road
Kings Mountain, NC 28086
[phone]
Fax: [phone]
SWPPP Preparation Date:
09/ 18 / 2012
Revision No.:
RECEIVED
DIVISION OF WATER QUALITY
SEP 2 7 2012
S9./ilp SECTION
MOORESVILLE REGIONAL OFFICE
DAVID D. SMITH AND COMPANY, PLLC
civil and structural engineering consultants
landscape architecture/land planning
1949 Bob's Creek Road Zirconia, NC 28790
Tel: [phone]

Contents
SECTION 1: FACILITY DESCRIPTION AND CONTACT INFORMATION......................................................1
1.1
Facility Information.................................................................................................................1
1.2
Contact Information/Responsible Parties.............:....................................................................2
1.3
Stormwater Pollution Prevention Team..................................................................................... 3
1.4
Activities at the Facility........................................................................................................... 3
1.5
General Location Map............................................................................................................ 3
1.6
Site Map................................................................................................................................ 3
SECTION 2: POTENTIAL POLLUTANT SOURCES.......................................................................................4
2.1
Industrial Activity and Associated Pollutants............................................................................. 4
2.2
Spills and Leaks..................................................................................................................... 4
SECTION 3: STORMWATER CONTROL MEASURES...................................................................................5
3.1
Minimize Exposure................................................................................................................. 5
3.2
Good Housekeeping............................................................................................................... 5
3.3
Maintenance..........................................................................................................................5
3.4
Spill Prevention and Response................................................................................................ 6
3.5
Management of Runoff...........................................................................................................6
3.6
Employee Training................................................................................................................. 6
3.8
Waste, Garbage and Floatable Debris.............................................................................................
7
SECTION5: INSPECTIONS............................................................................................................................
7
SECTION 7: SWPPP CERTIFICATION...........................................................................................................8
SECTION 8: SWPPP MODIFICATIONS..........................................................................................................9
SWPPPATTACHMENTS..............................................................................................................................10
Attachment A — General Location Map (USGS Map)
Attachment B — Site Plan C-1
Attachment C — Web address to the 2008 MSGP
ii

SECTION 1: FACILITY DESCRIPTION AND CONTACT INFORMATION
1.1 Facility Information
Facility Information
Name of Facility: Buckeye Fire Equipment Company
Street: 110 Kings Road
City: Kings Mountain State: NC ZIP Code: 28086
County or Similar Subdivision: Gaston County
Permit Tracking Number: NCG 050083 (if covered under a previous permit)
Latitude/Longitude
Latitude:
1.35 ° 16' 03" N (degrees, minutes, seconds)
Method for determining latitude/longitude (check one):
® USGS topographic map (specify scale: 1:24000
Longitude:
1.81 ° 19' 33" W (degrees, minutes, seconds)
Is the facility located in Indian Country? ❑ Yes ® No
If yes, name of Reservation, or if not part of a Reservation, indicate "not applicable." N/A (not applicable)
Is this facility considered a Federal Facility? ❑ Yes ® No
Estimated area of industrial activity at site exposed to stormwater: 3.10 (acres)
Discharge Information
Does this facility discharge stormwater into an MS4? ❑ Yes ® No
If yes, name of MS4 operator:
Name(s) of water(s) that receive stormwater from your facility Unnamed tributary to Long Creek
Are any of your discharges directly into any segment of an "impaired" water? ❑ Yes ® No
If Yes, identify name of the impaired water (and segment, if applicable): N/A
Identify the pollutant(s) causing the impairment: N/A
For pollutants identified, which do you have reason to believe will be present in your discharge? N/A
1

For pollutants identified, which have a completed TMDL? N/A
Do you discharge into a receiving water designated as a Tier 2 (or Tier 2.5) water? ❑ Yes ® No
Are any of your stormwater discharges subject tq,effluent guidelines? ❑ Yes ® No
If Yes, which guidelines apply? N/A
Primary SIC Code or 2-letter Activity Code: 39 / Y2
Identify your applicable sector and subsector: 3999-15
1.2 Contact Information/Responsible Parties
Facility Operator (s):
Name: Buckeye Fire Equipment Company - Gerald Culp, Plant Manager
Address: 110 Kings Road
City, State, Zip Code: Kings Mountain, NC 28086
Telephone Number: [phone]
Email address: [e-mail]
Fax number: [phone]
Facility Owner (s):
Name: Bower Family Real Estate, LLC
Address: Kings Mountain Industrial Park, 110 Kings Road
City, State, Zip Code: Kings Mountain, NC 28086
Telephone Number: [phone]
Email address: [e-mail] - Kevin Bower, President
Fax number: [phone]
SWPPP 24 Hour Emergency Contact:
Name: Gerald Culp - Plant Manager
Telephone number: [phone]
Email address: [e-mail]
Fax number: [phone]
2

1.3 Stormwater Pollution Prevention Team
Staff Names
Individual Responsibilities
Gerald Culp - Plant Manager
Primary contact; responsible for day to day coordination and
implementation of all activities associated with Stormwater Pollution
Prevention
Barbara McDonald
Secondary contact; team coordinator
Ken Laws
Assist with sampling and monitoring
Tony Daddario
Assist with sampling and monitoring
Charlie Ruff
Assist with sampling and monitoring
Bill Vegso
Assist with sampling and monitoring
1.4 Activities at the Facility
Manufacture, assembly and annodized finishing and painting of fire extinguishing equipment.
1.5 General Location Map
See Attached Drawing (Attachment A)
1.6 Site Map
See Attached Drawing (Attachment B)

SECTION 2: POTENTIAL POLLUTANT SOURCES
2.1 Industrial Activity and Associated Pollutants
Industrial Activity
Associated Pollutants
Non Hazardous Waste Storage
Foam Water Rinse, Used Oil and Water, Phosphate
Sludge, Caustic Sludge, used Vegetable Oil, Oil
Dry, Alkaline Cleaner Sludge, Ferrous & Non
Ferrous Metal Waste
Bulk Product Storage in Tanks or Silos
Glycol, Nitric Acid, Phosphoric Acid, Mono
Ammonium Phosphate MAP
New Product Storage and Unloading
3% AFFF Foam, 1 % AFFF Foam, Fluroprotien,
Heptanes
Ferric Metal Waste Storage
Ferric Metal
Non - Ferric Metal Waste Storage
Non Ferric Metal
Trash Compactor
Oil, Grease, Hydraulic Fluid, Waste/ Floatable
Debris
Routine Equipment Maintenance by others
Oil, Grease, Hydraulic Fluid
Compressors
Oil
2.2 Spills and Leaks
Areas of Site Where Potential Spills/Leaks Could Occur
Location
Outfalls
Tank/silo non hazardous waste storage along north side of building
Outfall #3, Outfall #4
New product storage, near research & development building
Outfall #4, Outfall #5
Trash compactor/dock, east side of facility
Outfall #2
Tank/silo storage adjacent to compactor
Outfall #1, Outfall #2
Loading Docks
Outfall #6 (from underground storm
drain connecting to trench drains
4

. Description of Past Spills/Leaks'
*No significant spills or discharges have occurred since the facility opened in 1984.
Date
Description
Outfalls
Insert date of
spill/leak
Insert description of spill/leak (where it occurred, what
happened, types of pollutants, extent of damage)
Specify which outfall(s)
were affected
SECTION 3: STORMWATER CONTROL MEASURES
3.1 Minimize Exposure
Industrial activities are located within buildings; material is loaded and unloaded at covered docks to minimize
product exposure to rain. Containers are used that are compatible with the product stored.
3.2 Good Housekeeping
Floors and ground surfaces are maintained both inside and outside with brooms, shovels, vacuum cleaners
and cleaning machines. This minimizes exposure, especially with contaminants that may be tracked out by
employees.
Garbage and waste materials are picked up regularly. Equipment is routinely checked and maintained to
ensure proper working condition and minimize the risks of oil and fluid leaks.
A Stormwater Pollution Prevention Team conducts semi annual visual monitoring of all Outfall locations for
signs of pollutants. Routine monitoring is conducted daily during facility operations and material handling.
Containers are regularly checked for leaks and to ensure that container lids are tightly closed.
Forklifts are regularly inspected for leaks and residue from materials being unloaded. If residue is present,
it will be cleaned and disposed of in accordance with Federal Regulations.
3.3 Maintenance
Buckeye has routine inspection programs for equipment and bulk storage tanks. Buckeye contracts with a
third party contractor for routine equipment maintenance and repair which is performed on site.

3.4 Spill Prevention and Response
■ Containers are plainly labeled e.g. "Used Oil". "Nitric Acid", "Phosphoric Acid", in addition to the
other chemicals that could be susceptible to spillage or leakage to encourage proper handling &
facilitate rapid response should spills or leaks occur. Containers used for storing chemicals are
compatible with the product stored.
■ Material Handling functions are monitored by supervisors to insure proper handling procedures and
technicians are used while loading or unloading materials. Visual inspections are made by forklift
drivers to insure that there are no leaks from the material being loaded or unloaded. In the event of
a spill, oil dry will be applied immediately and then disposed of legally in a hazardous landfill.
■ Stored material is kept under cover whenever possible.
■ Secondary containment devices are provided for Bulk storage of Phosphoric and Nitric Acid in the
form of 4 foot tall concrete dikes. The secondary containment devices are not connected directly to
a storm water conveyance system.
■ Oil dry and lime are stored in the stock room for ready access in the event of a spill.
3.5 Management of Runoff
Control measures include a roof drainage system and trench drains that collect, transport and discharge
stormwater to detention basins. The two (2) detention basins are located at the southeast and southwest
corners of the property.
3.6 Employee Training
Annual Training of employees will be conducted covering: contents of the facility SWPPP, control measures
implemented to achieve compliance with the General Permit, spill containment and cleanup proceedures,
maintenance, monitoring, things to look for during inspections, areas and control measures to be inspected,
planning, reporting and documentation requirements. A sign in / sign out sheet should be provided at each
training class to document that employees have participated and kept current with the SWPPP. The
schedule will be determined and posted in advance of the training session.
rel

3.8 Waste, Garbage and Floatable Debris
Trash compactor and baler at southeast corner of facility between loading dock and covered handicap
ramp is utilized for waste paper products. Covered dumpsters are utilized throughout the facility for normal
waste. All waste, garbage and floatable debris are removed regularly from the site by a contracted waste
disposal company.
SECTION 5: INSPECTIONS
For the routine facility inspections and the comprehensive site inspections to be performed at your site:
■ The names of the person(s), or the positions of the person(s), responsible for inspection:
Gerald Culp - Plant Manager
Ken Laws
Charlie Ruff
Bill Vegso
The schedules to be used for conducting inspections:
During the last week of every month, conduct routine facility inspections during normal hours of operation
and
Specific areas of the facility to be inspected:
Bulk container and drum storage areas: waste storage areas: tanks and silo storage tanks:
Dock areas during loading and unloading: maintenance area during and following equipment maintenance.
Outfall #1 through #6 shall be inspected at least once during the year when a stormwater discharge is
occurring
For the Semi-annual visual assessments to be performed at your site:
■ The names of the person(s), or the positions of the person(s), responsible for inspection:
Gerald Culp - Plant Manager
Ken Laws
Charlie Ruff
Bill Vegso
The schedules to be used for conducting inspections:
Semi annually (2 x per year) during spring and fall and
Specific areas of the facility to be inspected:
During normal buisiness hours, inspect Outfall #1 through Outfall #6 within 30 minutes of a representative
storm event (sufficient to allow sampling): prior to semi annual visual assessment, review inspection reports
& spill records for the prior year.
7

SECTION 7: SWPPP CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is, to
the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine and imprisonment for knowing
violations.
Name:
Title:
Signature: Date:

USGS Topographic Map
Buckeye Fire Equipment Co., Kings Mountain, NC
Map Name.- BESSEMER CITY Map Center: 035' 16'03-00" N 081' 19'00.00" W
Print Date: 09/20f12 Horizontal Datum: NAD27
0 Zi
�
%
V- 1,
1� I gv;
2, 7 fZ, e t
IR
X, `:y AV
IV,
A.
h �4 j".
r
Diking.-
V
4fl
00.
M1, Bbckeye Ire, �A
-4 f.
N_ Eq
4". I ipm6�t'Company.
j 7"
C
:K,
N
A
�Jl
r 0.15
3N
4
iA N 6.Z2: W X
SCALE 1:24000
Buckeye Fire Equipment Company
x 4CC11 ECICO Mc,, sccc
110 Kings Road., Gaston Co-, NC
FEET
DAVID D. SMITH AND COMPANY, PLLC
civil and structural engineering consultants
landscape architecture/land planning
1949 Bob's Creek Road Zirconia, NC 28790
Tel: [phone]
ATTACHMENT A

August 17, 2012
Robert B. Krebs
Regional Supervisor
Surface Water Protection Section
610 East Center Ave. Suite 301
Mooresville, NC 28115
Re: Notice of Violation
Compliance Evaluation Inspection
NOV-2012-pc-0253
Buckeye Fire Equipment
NPDES Permit No. NCG050000
COC No. NCG050053
Gaston County, NC
Dear Mr. Krebs:
E-mail: [e-mail] • Internet: http://www.buckeyef.com/fire
RECEIVED
DIVISION OF WATER QUALITY
AUG 2 0 2012
MOORESVILLE REGIONAL OFFICE
In response to your letter dated July 25, 2012 the Company has obtained the services of David
D. Smith & Company. PLLC located in Asheville, NC to assist the Compliance issues as stated in
Samar Bou-Ghazale's report. We regret that permit requirements were not completed as
required by the Division of Water Quality, due to an unexpected death of the person in charge
of this project. The company is working diligently to rectify this problem so that moving forward
the company will be in compliance with the permit requirement. We have secured a company,
Par Laboratories, Inc in Charlotte, NC to do the testing. Our goal is to have everything in place
within the next 30 days.
Thank you for your patience in this matter. If you should need additional information I will be
glad to have Mr. Smith give you a call regarding our progress.
Sincerely,
�.J�
Barbara McDonal
Safety/Environmental Manager
Buckeye Fire Equipment Company
ISO 9001 Registered .

IFV
Cc: Kevin Bower, President Buckeye Fire Equipment
Gerald Culp, Plant Manager, Buckeye Fire Equipment
David D. Smith, David D. Smith Company
Samar Bou-Ghazale, Surface Water Protection Section

August 17, 2012
Robert B. Krebs
Regional Supervisor
Surface Water Protection Section
610 East Center Ave. Suite 301
Mooresville, NC 28115
Re: Notice of Violation
Compliance Evaluation Inspection
NOV-2012-pc-0253
Buckeye Fire Equipment
NPDES Permit No. NCG050000
COC No. NCG050053
Gaston County, NC
Dear Mr. Krebs:
E-mail: [e-mail] • Internet: http:/Iwww.buckeyef.com/fire
RECEIVED
DIVISION OF WATER QUALITY
AUG 2 0 2012
MOORESVILLE REGIONAL OFFICE
In response to your letter dated July 25, 2012 the Company has obtained the services of David
D. Smith & Company. PLLC located in Asheville, NC to assist the Compliance issues as stated in
Samar Bou-Ghazale's report. We regret that permit requirements were not completed as
required by the Division of Water Quality, due to an unexpected death of the person in charge
of this project. The company is working diligently to rectify this problem so that moving forward
the company will be in ,compliance with the permit requirement. We have secured a company,
Par Laboratories, Inc in Charlotte, NC to do the testing. Our goal is to have everything in place
within the next 30 days.
Thank you for your patience in this matter. If you should need additional information I will be
glad to have Mr. Smith give you a call regarding our progress.
Sincerely,
171
Barb ra McDonald
Safety/Environmental Manager
Buckeye Fire Equipment Company
ISO 9001 Registered

Cc: Kevin Bower, Buckeye Fire Equipment
Gerald Culp, Plant Manager, Buckeye Fire Equipment
David D. Smith, David D. Smith Company
Samar'Bou Ghaale u` act WaterProtectio section

Buckeye Fire Equipment Co. FACILITY PERMIT TRACKING NO.: NCG050083
Additional MSGP Documentation
For:
Buckeye Fire Equipment Company
110 Kings Road
Kings Mountain, NC, 28086
RE-C,--IVED
DIVISION OF
WATER QUALITY
SEP 2 7 m2
Si dig SECTION
MOORESVILLE REGIONAL OI=EICE
[phone]
Facility Permit Tracking No. (Certificate of Coverage): NCG050083
General Permit No.: NCG050000
Instructions:
— Keep the following inspection, monitoring, and certification records in the same location that you keep your
SWPPP:
• A copy of 2008 MSGP (you can find an electronic copy at: www.epa.gov/npdes/stormwater/msgp);
• Descriptions and dates of any incidences of significant spills, leaks, or other releases;
• Records of employee training;
• Documentation of maintenance and repairs of control measures;
• All inspection reports;
• Description of any deviations from the schedule for visual assessments and/or monitoring;
• Description of any corrective action taken at your site;
• Documentation to support any determination that pollutants of concern are not expected to be
present above natural background levels, and that such pollutants were not detected in your
discharge or were solely attributable to natural background sources; and
— With the exception of the first 3 items, these are records that you will be updating throughout the permit
term.
— Follow the instructions in Sections A through I of this template to keep your records complete.

Buckeye Fire Equipment Co. FACILITY PERMIT TRACKING NO.: NCG050083
Contents
A. Significant spills, leaks or other releases......................................................................................1
B. Employee training.........................................................................................................................2
C. Routine Facility Inspection Reports..............................................................................................3
D. Semi -Annual Visual Assessment Reports....................................................................................7
E. Comprehensive Site Inspection Reports......................................................................................9
F. Monitoring results.......................................................................................................................10
G. Deviations from assessment or monitoring schedule.................................................................10
H. SWPPP Amendment Log.......................................................................................................11
I. Miscellaneous Documentation...................................................................................... 12
it

Buckeye Fire Equipment Co. FACILITY PERMIT TRACKING NO.: NCG050083
A. Significant spills, leaks or other releases
Instructions:
— Include the descriptions and dates of any incidences of significant spills, leaks, or other releases that
resulted in discharges of pollutants to waters of the U.S., through stormwater or otherwise; the
circumstances leading to the release and actions taken in response to the release; and measures taken to
prevent the recurrence of such releases.
— Provide information, as shown below, for each incident, and attach additional documentation (e.g., photos,
spill cleanup records) as necessary. Repeat as necessary by copying and pasting the fields below.
Date of incident:
Location of incident:
Description of incident:
Circumstances leading to release:
Actions taken in response to release:
Measures taken to prevent recurrence:
Date of incident:
Location of incident:
Description of incident:
Circumstances leading to release:
Actions taken in response to release: _
Measures taken to prevent recurrence:
Date of incident:
Location of incident:
Description of incident:
Circumstances leading to release:
Actions taken in response to release:
Measures taken to prevent recurrence:

Buckeye Fire Equipment Co. FACILITY PERMIT TRACKING NO.: NCG050083
B. Employee training
Instructions:
— Keep records of employee training, including the date of the training.
— For in -person training, consider using the tables below to document your employee trainings. For computer -
based or other types of training, keep similar records on who was trained and the type of training conducted.
— You must train all employees who work in areas where industrial materials or activities are exposed to
stormwater, or who are responsible for implementing activities necessary to meet the conditions of this permit
(e.g., inspectors, maintenance personnel), including all members of your Pollution Prevention Team. Training
must cover monitoring, inspection, planning, reporting, and documentation requirements in other parts of this
permit. EPA recommends training be conducted at least annually (or more often if employee turnover is high).
Training Date:
Training Description:
Trainer:
Employee(s) trained
Employee signature
Training Date:
Training Description:
Trainer:
Employee(s) trained
Employee signature
Training Date:
Training Description:
Trainer:
Employee(s) trained
Employee signature

Buckeye Fire Equipment Co. FACILITY PERMIT TRACKING NO.: NCG050083
C. Routine Facility Inspection Reports
Instructions:
— Include in your records copies of all routine facility inspection reports completed for the facility.
— The sample inspection report is consistent with the requirements in Part 4.1 of the 2008 MSGP relating to
routine facility inspections. Facilities subject to State industrial stormwater permits may also find this form
useful.
Using the Sample Routine Facility Inspection Report
— When conducting the inspection, walk the site by following your site map and numbered control
measures/areas of industrial activity to be inspected. Also note whether the "Areas of Industrial Materials or
Activities exposed to stormwater" have been addressed (customize this list according to the conditions at your
facility). Note any required corrective actions and the date and responsible person for the correction.
Monitoring Procedures for Visual Assessment:
— All required monitoring must be performed on a storm event that results in an actual discharge from
your site ("measurable storm event") that follows the preceding measurable storm event by at least 72
hours (3 days). The 72-hour (3-day) storm interval does not apply if you are able to document that less than a
72-hour (3-day) interval is representative for local storm events during the sampling period. In the case of
snowmelt, the monitoring must be performed at a time when a measurable discharge occurs at your site.
— For each monitoring event, except snowmelt monitoring, you must identify the date and duration (in hours) of
the rainfall event, rainfall total (in inches) for that rainfall event, and time (in days) since the previous
measurable storm event. For snowmelt monitoring, you must identify the date of the sampling event.
— You must take a minimum of one grab sample from a discharge resulting from a measurable storm event as
described above. Samples must be collected within the first 30 minutes of a measurable storm event. If it is
not possible to collect the sample within the first 30 minutes of a measurable storm event, the sample must be
collected as soon as practicable after the first 30 minutes and documentation must be kept with the SWPPP
explaining why it was not possible to take samples within the first 30 minutes. In the case of snowmelt,
samples must be taken during a period with a measurable discharge.

Stormwater Industrial Routine Facility Inspection Report
General Information
Facility Name
Buckeye Fire Equipment Company
NPDES Tracking No.
NCG050083
Date of Inspection
Start/End Time
Inspector's Name(s)
Inspector's Title(s)
Inspector's Contact Information
Inspector's Qualifications
Weather Information
Weather at time of this inspection?
❑ Clear ❑Cloudy ❑ Rain ❑ Sleet ❑ Fog ❑ Snow ❑ High Winds
❑ Other: Temperature:
Have any previously unidentified discharges of pollutants occurred since the last inspection? ❑Yes ❑No
If yes, describe:
Are there any discharges occurring at the time of inspection? ❑Yes ❑No
If yes, describe:
Control Measures
• Number the structural stormwater control measures identified in your SWPPP on your site map and list them below (add as
many control measures as are implemented on -site). Carry a copy of the numbered site map with you during your inspections.
This list will ensure that you are inspecting all required control measures at your facility.
• Describe corrective actions initiated, date co m leted, and note the gerson that completed the work in the Corrective Action Log.
Structural Control
Control
If No, In Need of
Corrective Action Needed and Notes
Measure
Measure is
Maintenance,
(identify needed maintenance and repairs, or any
Operating
Repair, or
failed control measures that need replacement)
Effectively?
Replacement?
1
Detention Basin 1
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
2
Detention Basin 2
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
3
Drainage Swale 1
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
4
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
5
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
6
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
7
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement
8
❑Yes ❑No
❑ Maintenance
❑ Repair
❑ Replacement

Areas of Industrial Materials or Activities exposed to stormwa'ter
Below are some general areas that should be assessed during routine inspections. Customize this list as needed for the specific
types of industrial materials or activities at your facility.
Area/Activity
Inspected?
Controls
Corrective Action Needed and Notes
Adequate
(appropriate,
effective, and
operating)?
1
Raw Material & Finished
❑Yes ❑No ❑ N/A
❑Yes ❑No
Product loading/
unloading and storage
areas
2
Above ground chemical
❑Yes ❑No ❑ N/A
❑Yes ❑No
storage tanks or basins
containing chemicals
3
Waste handling and
❑Yes ❑No ❑ N/A
❑Yes ❑No
disposal areas
4
Empty Tank Storage
❑Yes ❑No ❑ N/A
❑Yes ❑No
5
Stormwater Detention
❑Yes ❑No ❑ N/A
❑Yes ❑No
Basins
6
❑Yes ❑No ❑ N/A
❑Yes ❑No
7
❑Yes ❑No ❑ N/A
❑Yes ❑No
8
❑Yes ❑No ❑ N/A
❑Yes ❑No
9
❑Yes ❑No ❑ N/A
❑Yes ❑No
10
❑Yes ❑No ❑ N/A
❑Yes ❑No
11
❑Yes ❑No ❑ N/A
❑Yes ❑No
12
❑Yes ❑No ❑ N/A
❑Yes ❑No

Describe any incidents of non-compliance observed and not described above:
Additional Control Measures
Describe any additional control measures needed to comply with the permit requirements:
Notes
Use this space for any additional notes or observations from the inspection:
CERTIFICATION STATEMENT
"I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing
violations."
Print name and title:
Signature: Date:

Additional MSGP Documentation
BUCKEYE FIRE EQUIPMENT CO. FACILITY PERMIT TRACKING NO.: NCGO50083
D. Semi -Annual Visual Assessment Reports
Instructions:
— Include in your records copies of all semi-annual visual assessment reports completed for the facility. An
example quarterly visual assessment report can be found on the following page.
EPA Additional MSGP Documentation

MSGP Semi -Annual Visual Assessment Form
(Complete a separate form for each outfall you assess)
Name of Facility: Buckeye Fire Equipment Company NPDES Tracking No. NCGO50083
Outfall Name: "Substantially Identical Outfall"? ❑ No ❑ Yes (identify substantially identical outfalls):
Person(s)/Title(s) collecting sample: Name/Title
Person(s)/Title(s) examining sample: Name/Title
Date & Time Discharge Began: Date & Time Sample Collected: Date & Time Sample Examined:
Substitute Sample? ❑ No ❑ Yes (identify quarter/year when sample was originally scheduled to be collected):
Nature of Discharge: ❑ Rainfall ❑ Snowmelt
If rainfall: Rainfall Amount: Previous Storm Ended > 72 hours ❑ Yes ❑ No' (explain):
inches Before Start of This Storm?
Parameter
Color ❑ None ❑ Other (describe):
Odor ❑ None ❑ Musty ❑ Sewage ❑ Sulfur ❑ Sour ❑ Petroleum/Gas
❑ Solvents ❑ Other (describe):
Clarity ❑ Clear ❑ Slightly Cloudy ❑ Cloudy ❑ Opaque ❑ Other
Floating Solids ❑ No
❑ Yes (describe):
Settled Solids" ❑ No
❑ Yes (describe):
Suspended Solids ❑ No
❑ Yes (describe):
Foam (gently shake sample)
❑ No ❑ Yes (describe): _
Oil Sheen ❑ None ❑ Flecks
❑ Other (describe):
Other Obvious Indicators ❑ No
of Stormwater Pollution
❑ Globs ❑ Sheen ❑ Slick
❑ Yes (describe):
" The 72-hour interval can be waived when the previous storm did not yield a measurable discharge or if you are able to document (attach applicable documentation)
that less than a 72-hour interval is representative of local storm events during the sampling period.
"" Observe for settled solids after allowing the sample to sit for approximately one-half hour.
Detail any concerns, additional comments, descriptions of pictures taken, and any corrective actions taken below (attach additional
sheets as necessary).
Certification by Facility Responsible Official (facility manager or responsible corporate officer)
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
IA. Name:
C. Signature:
B. Title:
D. Date Signed:
8

Additional MSGP Documentation
BUCKEYE FIRE EQUIPMENT CO. FACILITY PERMIT TRACKING NO.: NCGO50083
E. Comprehensive Site Inspection Reports
Instructions:
— Include in your records copies of all comprehensive site inspection reports completed for the facility.
Copies of the comprehensive site inspection report form (also called the Annual Reporting Form) is
included with the SWPPP for your convenience.
— For corrective actions, complete part D (Corrective Actions) of the Annual Reporting Form included with
this SWPPP.

Additional MSGP Documentation
BUCKEYE FIRE EQUIPMENT CO. FACILITY PERMIT TRACKING NO.: NCG050083
F. Monitoring results
Instructions:
— Include in your records copies of all monitoring results for the facility.
G. Deviations from assessment or monitoring schedule
Instructions:
Include in your records:
— A description of any deviations from the schedule you provided in your SWPPP for visual assessments
and/or monitoring, and
— The reason for the deviations (e.g., adverse weather or it was impracticable to collect samples within the
first 30 minutes of a measurable storm event) (see Part C of this document; Routine Facility Inspection
Reports - Monitoring Procedures for Visual Assessment).
Use the fields below to document the deviations. Repeat as necessary for any deviations.
Date:
❑ Visual assessments
Describe deviation from schedule: _
Reason for deviation:
Date:
❑ Visual assessments
Describe deviation from schedule: _
Reason for deviation:
Date:
❑ Visual assessments
Describe deviation from schedule: _
Reason for deviation:
Date:
❑ Visual assessments
Describe deviation from schedule: _
Reason for deviation:
❑ Monitoring
❑ Monitoring
❑ Monitoring
❑ Monitoring
We

Additional MSGP Documentation
BUCKEYE FIRE EQUIPMENT CO. FACILITY PERMIT TRACKING NO.: NCGO50083
H. SWPPP Amendment Log
Instructions:
Include in your records:
— A log of the date and description of any amendments to your SWPPP.
Fill in the appropriate columns of this table for each amendment to your SWPPP. Copy and paste additional rows
into the table as necessary.
Amend.
No.
Description of the Amendment
Date of
Amendment
Amendment Prepared
by [Name(s) and Title]
1
2
3
4
5
6
7
8
9
10
11
IF

Additional MSGP Documentation
BUCKEYE FIRE EQUIPMENT CO. FACILITY PERMIT TRACKING NO.: NCGO50083
I. Miscellaneous Documentation
Instructions:
Use this section to keep records of any additional documentation that relates to your compliance with the permit,
12

Love, Barry F
From: Weaver Keith <[e-mail]>
Sent: Tuesday, December 01, 2015 4:55 PM
To: Love, Barry F
Subject: KSM Castings Spill Report
Attachments: 113015 Incident.odf
Hi Barry,
Please find attached, a summary letter detailling the events of the waste water spill that we discussed
yesterday evening. The original will be sent by US Mail on 12.02.15. Thanks for your help.
Kind regards / Mit freundlichen GrOBen
Keith Weaver
EHS Manager
KSM Castings NC Inc.
120 Blue Brook Drive
Shelby NC 28150
Office Phone: [phone]
Cell Phone: [phone]
Fax: [phone]
Email: Keith. Weaver(aKSMCastings.com
Web: http://www.ksmcastings.com
i
1
This message may contain confidential and privileged information. If it has been sent to you in error,
please reply to advise the sender of the error and then immediately delete it. If you are not the intended
recipient, do not read, copy, disclose or otherwise use this message. The sender disclaims any liability for
such unauthorized use. PLEASE NOTE that all incoming a -mails sent to ksmcastings.com e-mail accounts
will be archived and may be scanned by us and/or by external service providers to detect and prevent
threats to our systems, investigate illegal or! inappropriate behavior, and/or eliminate unsolicited
promotional a -mails (spam). This process could result in deletion of a legitimate e-mail before it is read by
its intended recipient at our organization. Moreover, based on the scanning results, the full text of a -mails
and attachments may be made available to KSM Castings Group security and other personnel for review
and appropriate action. If you have any concerns about this process, please contact us.

i
I
i
MRO Incident / Complaint Report
Investigator: o v_` I Received By: ar r m v�
Contact Date: ,o h Date Received:
Investigated Da e: i Time Received:
Response Date: County: c r-v` ar
r+str-&AY— �. t z ' i �" j Complaint Type: oil
Investigated? ❑ yes ❑ no Incident M (BIMS, RUST, ETC) zit"S o► `r�o8
Violation? ❑ yes ❑ no �—
NOV Sent? ❑ yes ❑ no
Responsible Party: Complainant:
Responsible Party Address / Phone:; Complainant Address / Phone:
?, d , isox .1, Ltd ►+
S 6 I:Al(-- .7- ►s1 - n
70 006 S
�G� 3 Q 6S'6 `t
I
.�✓I?WLI
Nature of Complaint: /
As ✓ �t r • N N Sao rnt o, v-- 7 At n K. Wry 1 c /1 0"I ` s/ S W a ! 1 Q w q �e o^�r o .
d� 1��.... -F�✓ raNA r,.. �oV ., JieiV �10 J/�� �G1!✓P. .A 1d.�o.AJ—w%0 e_�v444
' �woi
C4 to an✓�ron�sr��B %V, �6
Directions to Site:
Ac�ti�ons11Taken/Comme/nts: r
yvo�5-1.. WA�gr ci BSc �1ar
a -W a 5 To4 K e�
1 ® j wat — W C r WcL 9
S f or' " %,,,,c e r^ o V' N/ 6%c- Y S
L
i
I
I �% 1
C (% J i .✓�r o Ivy S iN1 Wl �1 K. I E
ILn f�on/ nW G-odl�A; .� `� Yer.-►bV�
f
Referred to:
❑ UST ❑ LQ ❑ AP ❑ SWP ❑tHaz. Waste ❑ Solid Waste ❑ PWS ❑ County HD
Referred on: Referred by:

- WA
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral, and Land Resources
Land Quality Section
Tracy E. Davis, PE, CPM
Director
March 11, 2614
Rockwood Lithium, Incorporated
Attention: Mr. John Kuhn, Safety, Health, and Environmental Director
348 Holiday Inn Drive
Kings Mountain, North Carolina 28086
RE: Rockwood Lithium Dam (aka Chemetall Foote Dam)
State ID: CLEVE-007
Cleveland County
Dear Mr. Kuhn:
Pat McCrory, Governor
John E. Skvarla,. III, Secretary
Thank you for the letter dated February 24, 2014, and received on February 25, 2014 for
the referenced dam. This letter provided an update on the status of the subject dam as
requested in the Temporary Repair Approval letter issued December 3, 2009 by this
Division.
Your letter detailed the continued use of siphon operation and permitting activities related
to the Approval to Breach issued by this Division on September 16, 2011, and extended by
this Division on September 25, 2012, and September 18, 2013. Please continue to keep
the impoundment level lowered and perform periodic inspections until the dam breach can
be accomplished.
We appreciate the periodic updates as requested in our December 3, 2009 correspondence.
Thank you for your cooperation in maintaining and operating this dam to provide for
public safety. Please contact me at telephone number [phone] should you have
any questions concerning this matter.
Sincerely,
Zahid S. Khan, CPM, CPESC, CPSWQ
Regional Engineer
Land Quality Section
cc: State Dam Safety Engineer
WUMEMP W;,,. �,. ,T
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 a Phone: [phone] / FAX: [phone]
Internet: http://Portal.ncdenr.org/web/Ir/land-quality
An Equal Opportunity \ Affirmative Action Employer — 50% Recycled \ 10% Post Consumer Paper

NCDENR
North Carolina Department of Environment and Natural Resources
_Division of :Energy, Mineral, andLand "Resources
Tracy-E. Davis, PE, CPM
Director
Certificate of Approval
September.24, 2013
CERTIFIED MAIL
RETURN RECEIPT
City of Kings Mountain
Attn: Mr. Dennis Wells
PO Box 429
Kings Mountain, North Carolina 28086
RE: Approval to Repair
Moss Lake Dam
Cleveland County
CLEVE-018
Dear Mr. Wells:
Pat McCrory, Governor
John E. Skvarla, III, Secretary
R[:C:-:gV�D
SEP 3 ® 2013
MC7UR6L L k;E-&O9VAL OFFICE
This is in response to your submission dated September 3, 2013, received on September 18, 2013
of plans, specifications and design data for -repair of the subject dam in compliance with the Dam
Safety Law of 1967. This dam is of high hazard classification. This project involves concrete,
concrete joint, and concrete crack repairs in the spillway as well as a vertical extension of the
south spillway wall. The plans, specifications and.design data submitted were prepared under
the supervision of Mr. Christopher E. Wood, PE and Mr. Wayne H. Mabry, PE.
This letter constitutes approval of the proposal to repair the subject dam according to the plans
and specifications received by this Division on September 18, 2013 with the following
stipulations:
1. Project construction shall be supervised by Mr. Christopher E. Wood, PE and Mr. Wayne H.
Mabry, PE. Mr. Christopher E: Wood, PE and Mr. Wayne H. Mabry, PE shall be
responsible for field observation of construction as necessary to ensure compliance with
approved plans.
2.. During construction, the Division of Energy, Mineral, and Land Resources may require such
progress reports as are deemed necessary
Geological Survey Section • Land'Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-9200 / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://portal.ncdenr.org/web/Ir/
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper

Mr. Dennis Wells
Approval to Repair
September 24, 2013
Page 2 of 2
Moss Lake Dam
CLEVE-018
In accordance with GS 143-215.29 and NCAC 15A-2K .0203, .0212, .0215, and .0216,
within 30 days of completion of the project, Mr. Christopher E. Wood, PE and Mr. Wayne H.
Mabry, PE shall inspect the completed work and upon finding that the work has been done as
specified and the dam is safe, shall file with the Division of Energy, Mineral, and Land
Resources two sets of record drawings and a certificate stating that the work has been
completed in accordance with approved plans, specifications and other requirements.
4. In accordance with GS 143-215.30 and NCAC 15A-2K .0220, final written consent must be
issued by the Director of the Division of Energy, Mineral, and Land Resources for use of this
dam pursuant to these repairs.
5. The O&M plan shall updated to include components of this repair. This updated section of
the O&M Plan must be submitted with the record drawings.
This approval does not convey the right to access the private property of others. Any
required access to perform the approved work must be secured prior to initiation of
construction activities.
7. You must notify Mr. Zahid Khan, Regional Engineer, Land Quality Section, 610 East Center
Avenue, Mooresville, North Carolina 28115, [phone] ten days before the start of
construction.
The Army Corps of Engineers and the Water Quality Section of this Department should be
- contacted to determine if additional permits are required. Also, the erosion and sediment control
program having jurisdiction should be contacted to determine permit requirements. In any case,
sediment must be prevented from entering the waters of the state or flowing onto neighboring
property.
Construction of the repairs must begin within one year of the date of this letter or this approval is
void. For assistance you may contact the Mooresville Regional Office at [phone] or a
staff member of the Dam Safety Program in the Raleigh Central Office at telephone number
[phone].
Sincerely,
Tracy E. avis, PE, CPM
Director
TED/smm
cc: Mr. Christopher E. Wood, PE
Mr. Wayne H. Mabry, PE
Mr. Zahid Khan, Regional Engineer, Land Quality Section
ux�+�t eater P�atect��rn ' �-zori,�-�pe�,r� r
Filename: CLEVE-018 20130924 COAR Moss Lake Dam

MCDN
North Carolina Department of Environment and Natural Resources
Division of Water Infrastructure
Pat McCrory Kim H. Colson, PE John E. Skvarla, III
Governor Acting Director Secretary
E D
September 5, 2013
Mr. Vince Reese, Plant Manager
Clearwater Paper CorporationNAt_ OFt=9CE
671 Washburn Switch Rd.
Shelby, NC 28150
Subject: Clearwater Paper Corporation
Real and Personal Property
Tax Certification Number TCS MV-162
Cleveland County
Dear Mr. Reese:
As per your request, the staff of the Division of Water Infrastructure has completed the review
of the Tax Certification Request for real and personal property.
Please find attached a copy of Tax Certification Number TCS-MV-162 issued by this office to
Clearwater Paper Corp. for the facility located in Cleveland County. A copy of this Certification is
being sent to the Cleveland County Tax Administrator. along with a copy of this letter. For the
record, an earlier tax certification was approved at this facility on September 17, 2012 by the NC
Division of Waste Management for a resource recovery or recycling facilities at this site.
Please note that as part of this Tax Certification process, the DENR staff did not make any
efforts to confirm either the cost of the items certified or the year of their acquisition.
If there is a need for any additional information or clarification, please do not hesitate to contact
either Mr. Gerald Horton of our staff at gerald.horton@ncdenr.g_ov 919 707-9185 or the undersigned
at [e-mail] 919 707-9162.
Si c rely,
7
ar L. Hubbard, PE, Assistant Chief
Infrastructure Finance Section
aINHr,;wh
Attachments
cc: Chris Green, Cleveland County Tax Administrator, PO Box 1210, Shelby, NC 28150
—ike'Pa kMooresville DWQ Regional Office, 610 E. Center Ave., Ste. 301, Mooresville, NC 28115
Infrastructure Finance Section — Gerald W. Horton, PE
Central Files — NPDES Permit NC 002 4538
fns;l}prrC.. i?(?f.iill^ti ;i�:� r..',: �c';t �I ,fu..: ar.i�;ipi :;nor ^�i;� ;_t; ' S;�,i �, U. :.r ..nnr, T..,, �,�•Pi i! '�'� : i•ri�r ;c,n . no
Infrastructure Finance Section
1633 Mail Service Center, Raleigh, North Carolina 27699-1633 One r_
Location: 81h Floor Archdale Building, 512 N. Salisbury St. Raleigh, North Carolina 27604 N®fthtCa.�ol `--
Phone: [phone] FAX: [phone]%r���
Internet: ifs.nc.00v

N QRTH CA+.ROLINA, DEPARTM NTI OF
Ef`i'dh iQVi I'c �7 i;D NATURAL RF50UiRCF S
North Carolina Division of Water Infrastructure
TAX CERTIFICATION NUMBER TCS-MV-162
In accordance with the provisions of the North Carolina General Statutes G.S. 105-275.(8) this
is to certify that:
Clearwater Paper Corporation
671 Washburn Switch Rd.
Shelby, NC 28150
Cleveland County
filed a request for tax certification for real and personal property covered under Shelby
Industrial User Permit CP12 issued by the City of Shelby, under authority of the Division of
Water Quality NPDES Permit NC 002 4538.
On August 29, 2013, staff of the Division of Water Infrastructure inspected these wastewater
facilities and found or observed, based on the information supplied by the applicant, that the
facilities and listed on the attached application meet the following requirements for Tax
Certification:
1. The treatment equipment property has been constructed and is operational;
2. The property complies with, the requirements of the Environmental Management
Commission (EMC);
3. The property is being effectively operated, in accordance with the terms and conditions of
approvals issued by the EMC; and
4. The property has, as its primary rather than incidental purpose, the reduction of water
pollution resulting from the discharge of sewage or waste.
Please note that as part of this Tax Certification process the DENR staff did not make any
efforts to confirm either the cost of the items certified or the year of their acquisition.
DATE TAX CERTIFICATION ISSUED: S p tuber 5, 20 3
Mark L. Hubbard, P.E., Assistant Chief
Infrastructure Finance Section
Attachment
cc: Chris Green, Cleveland County Tax Administrator, PO Box 1210, Shelby, NC 28150
Mike Parker, Mooresville DWQ Regional Office, 610 E. Center Ave., Ste. 301, Mooresville, NC 28115
Infrastructure Finance Section — Gerald W. Horton, PE
Central Files — NPDES Permit NC 002 45388

Tax Certification Inspection Report Determination
Facility: .............................................. Clearwater Paper Corporation
Tax Certification Number: ........................ TCS-MV-162
Inspection Date: .................................... Thursday August 29, 2013
Site contact .......................................... Vince Reese, Plant Manager tele: 704 476-3801
[e-mail]
ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes ❑ No ❑
Gerald Horton of NC DENR Infrastructure Finance Section visited subject facility Thursday
August 29, 2013 for the purpose of a Tax Certification inspection. IFS discussed items in this
report with Mr. Vince Reese, Plant Manager and following a brief discussion viewed and took
photographs of the wastewater treatment equipment in the manufacturing plant. Clearwater
produces towel and tissue paper products. Wastewater is generated in processing the "pulp" to
product.
Mr. Horton checked with the Mooresville Water Quality Regional Office and Mr. David Hux
704 284-2084 with the Shelby Pretreatment program and neither had cause to deny this Tax
Certification at this time. Clearwater Paper's pretreatment facilities are authorized to discharge
to the City of Shelby's wastewater system under the authority of the City of Shelby Industrial
User Permit CP12 Pretreatment program permit. The City of Shelby holds NPDES Permit NC
002 4538. Clearwater Paper Corp. was producing approximately 0.650 MGD and has reduced
this flow to under 0.450 MGD. There is an ongoing program to reduce the loading and/or the
wastewater flow.
0
Effluent Rotary Screen
Comments: see photo 01
Dissolved Air Floatation
Comments: see photo 02
3. Sludge Press
Comments: see photo 03
4. Sludge Thickener
Comments: see photo 04
Qualifies? Ye No
Qualifies? Yesv No
Qualifies? Yee No
Qualifies? Ye No
L `USE" � I ��=i 1:1p41 Ih ltt` ...:,,, ,:r;•,4 6 � �`P i I i? �.1(V
Page No. 1 of 1

g fi'r r^ a 1 t un�i; f �ODYY,�,�Y�•P., TCN:
treatment systems and
Division of Water QualityW (� Q) Rev.. 06/01/2007
DIRECTIONS: Complete and mail signed copies of the application form and all supporting information to both: 1) the County Tax Administrator for the County in which the facility is located (one copy) AND 2)
to the NC Division of Water Quality, Construction Grants and Loans Section, 1633 Mail Service Center, Raleigh, NC 27699-1633 (two copies). Type or print in blue or black ink. A separate application
package is required for each facility where property proposed for tax certification is located.
THIS APPLICATION WILL NOT BE PROCESSED WITHOUT COMPLETE AND ACCURATE INFORMATION. If you have any questions regarding this application, please call the local tax office or the NC
Division of Water Quality at 919/733-6900 or their web site at www.nccol.net for more specific contact information.
Please Note:
a) Tax Certifications will only be processed for facilities under the authority of the DWQ and only if the DWQ has found that the described property:
1. Has been or will be constructed or installed;
2. Complies with or that plans therefore which have been submitted to the DWQ indicate that it will comply with the requirements of the Environmental Management Commission;
3. Is being effectively operated or will, when completed, be required to operate in accordance with the terms and conditions of the permit, certificate of approval, or other document of approval issued by the
DWQ; and
4. Has or, when completed, will have as its PRIMARY rather than incidental purpose the reduction of water pollution.
5). Is being used exclusively (100%) for waste treatment.
b) If approved, the Tax Certification issued will incorporate all requested assets at the facility that meet the criteria for Tax Certification by DWQ. Therefore this application must include any new assets for
which Tax Certification is being requested, as well as any assets previously receiving Tax Certification from DWQ for which Tax Certification is still needed.
A. Applicant (Applicant is the owner of, and taxpayer for, the propeqy described in this a lication for tax certification.
Name of Applicant: Name of Facility:
CLEARWATER PAPER CORPORATION SHELBY CONVERTING PLANT
Address of Applicant, if different from facility where property located: Physical Address of Facility where property located (no P.O. Box):
PO BOX 92108, AUSTIN, TX 78709 (address) 671 WASHBURN SWITCH RD, SHELBY, NC 28150
(city) (zip) (street address)
Business Relationship of Applicant to facility where property located: (city) (Zip)
AGENT FOR PARENT COMPANY County where property located: CLEVELAND
Name of Contact Person at Facility where property located:
JAMES E. GARZA
Does the Applicant hold any NC Division of Water Quality Permits? ❑ Yes ! ® No Title: AGENT Phone Number: [phone]
If yes, please list CITY OF SHELBY WASTEWATER INDUSTRIAL USER PERMIT #CP12
Permit Nos :
If approved, will this be the first Tax Certification issued for this Facility? If no, attach any previously issued tax
❑ Yes I ® No certifications
U. %lullifete N5 Section only If the Operator/User of the facility and equipment is different from the Owner of the facility.
Name of
Operator/User:
Operator/User
Address:
Operator/User Contact
Name:
Relationship between Operator/User of facility and
and applicant:
'ATTACH A PROCESS SCHEMATIC TO YOUR APPLICATION The number of each item for which Tax Certification is being requested must be shown on the schematic *'*
Application Continues on Next Page ->

DIVISION OF WATER QUALITY TAX CERTIFICATION & EXEMPTION APPLICATION
Waste Treatment Systems & Equipment: Waste treatment systems & equipment must be used exclusively for the abatement of water pollution
Was asset listed in IAsset Number,
the permit (Yes/No) I Vehicle Identification
PAGE2
Rev 06/01/2007
of Use for I Is this asset
Pollution Year of I Original Historical I replacing a prior
Nay..„......a,y
If the asset is listed in the DWQ permit, the description must be identical as listed on the current permit If the asset is not specifically listed in the DWQ permit, the applicant must attach detailed information as to why the asset should quality for Tax Certification.
When certifying systems or equipment, DENR is not certifying the cost of the equipment or the year of acquisition.
Facilities: To qualify for tax certification, the building or section of building being applied for, must be used exclusively for water pollution prevention. A sketch of the building, square footage along with
details as to how the building is used for water pollution prevention, is required.
Land: To qualify for tax certification, the land must be used exclusively for water pollution prevention. A schematic diagram of the facility detailing the land being applied for is required. The amount of land
(acreage) is required and how this land is being used to prevent water pollution. For wastewater treatment and irrigation system list separately the acreage used for actual treatment from the acreage required
by the facility s water quality permit for buffers and setbacks.
SIGNATURE:
I hereby certify that the above equipment, facilities and/or land are used for the purpose stated, and that the information presented in this application is accurate. Furthermore, I certify that any portable or
mobile equipment ' e his application w be used exclusively in the state of North Carolina
Applicant
Signature: YVl@ 5 rTitle:
Date:
(print name also) ,
NOTICE: The pena or false statement, represent do or certification Of: 1 ��i VOJLLo fl,�.t/p o i( `c� � � An ew
herein includes imprisonment and / or the assessor of civil penalties. (Name of Applicant Business Entity) <��� V rc-wo

City of Shelby, North Carolina
Industrial User Permit (IUP)
To Discharge Wastewater under the industrial Pretreatment Program
CP12
1UP Number
430.120
40 CFR Category
(If Applicable)
In compliance with the provisions of North Carolina General Statute 143-215.1, any applicable federal categorical
pretreatment regulations, all other lawful standards and regulations promulgated and adopted by the North
Carolina Environmental Management Commission, and the City of Shelby Sewer Use and Industrial Wastewater
Pretreatment Ordinance, the following Industry, hereafter referred to by the name or as the permittee,
Industry Name, permittee:
Clearwater Paper lCorporation
Owner:
Same
Facility located at Street Address:
671 Washburn Switch Road
City:.
Shelby
State, Zip:
North Carolina, 28150
is hereby authorized to discharge wastewater from the facility located at the above listed address into the
sanitary sewer collection system and the wastewater treatment facility of the City of Shelby listed below,
CUP Control Authority VVWTP name:
City of Shelby— First Broad WWTP
NPDES Number:
f11C0024538
WWTP Address:
1940 South Lafayette Street
City, State, Zip:
Shelby, NC 28152
in accordance with effluent limitations, monitoring requirements, and all other conditions set forth in Parts I, 11,
and III of this Industrial User Permit (IUP).
Effective Date: This permit and the authorization to discharge
shalt become effective at 12:01 a.m. on this date:
January 1, 2013
Expiration date: This permit and the authonzatiorrto discharge
shag expire at midnight on this date:
June 30, 2014
AexpA 29 20/ Z Z-A
Date Farad R. Cornwell, PIS
Public Utilities Director
Form: WVVI-5001-CP-12
Effective Date: 01/01/2013

Permit No.CP12
Part I Specific Conditions
IUP, Part 1, Outline_
A. WP Basic Information
B. IUP Modification History
V. Authorization Statement
D. Description of Discharges
E. Schematic and monitoring locations
F. Effluent limits and monitoring requirements
G. Definition and Limits page(s) notes
A. ]UP Basic Information:
Part I — Specific Conditions
ReceivPOTW Name ing —
PoNPDCS d
City of Shelby —First Broad WVVTP
1 C0024538
[UP Name.
[UP Number.
Clearwater Paper Corporation
CP-12.
fUP Effective date: m�
Pipe Numbers: list all regulated pipes:
January 1, 2013
001, 002.
JUP Expiration date:
lUP 40 CFR d (if applicable), or N/A
June 30, 2014 1430.120
Page 2 of 20
Form: %VWT-5001-cP-1.2
Ehective Date:01/01/13
Revision Date: 01/01/2.3
stvi ioi, 4: 0

Permit No.CP12
C. Authorization Statement:
Part I —Specific Conditions
L The permittee is hereby authorized to discharge wastewater in accordance with the., effluent limitations,
monitoring requirements and all other conditions set forth in this Industrial User Permit (1UP) into the
sewer collection system and wastewater treatment facility of the City of Shelby.
L . The permittee is hereby authorized to continue operation of and discharge wastewater from the foliowing
listed treatment or pretreatment facilities. These facilities must correspond to the treatment units listed
on both the permit application and inspection forms.
I1U Treatment Units �I
List all Treatment Units: Descriptions w
Dissolved Air Floatation Pulp/Paper Slurry Recovery
Sludge Tank/Sludge Press '"waste"Product Processing
Effluent screening Discharge. Screening Prior to Equalization Tank
Flow Equalization 25,100 gal flow equalization tank
I. If required by and after receiving Authorization to Construct (A to C) from the City of Shelby, the
permittee shall construct and operate additional. pretreatment units as needed to meet final effluent
limitations.
D. Description of IUP Discharge(s):
Describe the discharge(s) from all regulated pipes..
001 Includes process wastewater from papermaking process and related maintenance
activities, wash -down water and boiler/cooling tower blow -down.
002 Domestic wastewater from warehouse, office and converting operations. Process
water from converting operations and related maintenance activities..
Page 3 of 20
Form: VJwT-5001-CP-12
Effective Date: 01/01/13
Revision Date: 01/01/13
{ir�FiFirsi� fl

Permit No.C.P12
E. Schematic and MonitoringLocations:
Part I — Specific Conditions
r attlalp I: j
•tt !rt'.i. ].F, it t.1/JvUfA^rf�N!iti�
II'I j3� Flii� i�I�Illlt �Fi If r, I"�1 tYi1,-tr 1T
t
Page 4 of 20
form: VV%krl•5001-C:P-12
Gffertive Date: 01/01/13
]revision Date: 01/01./13
Rovisiun 4: 0
t
.E
r.{
f
1
i
a 1
j 'rt i
i
1
yam,,,
�
i.•__\ t
I
�
1 I
•r
Pipe 002 Pipe 001

Vast I — j) eCI?IC (-ol?omons
Part
Permit No. ('p12
Receiving POT' name: First Broad
kU Name: ;
Clearwater
E fipier: Linli 's
and Monitoring Requirements
Receiving POTW NPDtS #: r=24538
Effective date for these limits: 01/01/2013
Ili Number:
Paper
CP12
Pipe
Number:
001
The permlttee may discharge from this specific pipe number
Expiration date for these limits: 06f30/2014 40 CFR Number:
430
according to these specific
dates, effluent limits, and monitoring
The Limits on this page are, {Ch(,ck one below) (if not applicable put N/A)
requirements.
Limits for entire permit period: X
Interim Limits for period #1:
Interim Limits for period #2:
FINAL LIMITS PAGE:
Concentration Limits
Mass -Based Limits NlonitorinFrequency
Sample
Required
Daily Monthly Daily
Units
Monthly
i Collection
Laboratory
Max. Average Max
Avg Units by Industry by POTW
Method
Detection
1. Flowp,7J0a
h9GD
' (C, I, G or R)
Limits
2. Flow
52D GPM
Metered Every Sample
N/A
N/A
3: Flow
700a GPM
Metered Continuous
j R
N/,1
4. PH
GA-10.5 N/A S.U.
Metered Continuous
R
N/A
I 5. 801]
190 nig/L
RecordedSeeG8 Monthly
G
0.10
6. TSS
iG0
Q a tel;r Monthly
C
2.0
7. Am,"nia
20 mg/L
Quarterly Monthly
C
2.5
8. Total.Nitrogen
mg/L
Quarterly Monthly
C
0,10
9. Oil &grease
mgiL
Quarterly Monthly
C
0.10
10.. T-Phenols �
me/L
Quarterly Monthly
G
5.0
11. Cyanide
mg/1
Quarterly Quarterly
G
0.010
12. Zinr,
mg/L
Quarterly Quarterly
G
0.010
13, f Copper
mg/I
Quarterly Quarterly
l C
0.010
14. Chromium
mg/I
Quarterly Quarterly
C
0.002
15. Cadmium
mg/I
Quarterly Quarterly
C
D.005
16. Barium
mg/I
Quarterly Quarterly
C
0.002
17. Arsenic
m ii
Quarterly Quarterly
[ C
0.010
18. Lead
mg/1
Quarterly Quwlterly
C
0.010
_
19. I Mercury
mg/L
Quarterly Quarterly
C
0.010
20. Molybdenum
me/L
Quarterly Quarterly
C
0.0002
21. Nickel
mg/L.
Quarterly Q tattedy
C
0.10 I
222, Selenium
mg[L
Quarterly Quarterly
C
0.010
23, Silver
mgjL
Quarterly Quarterly
C
0.010
PdonryPoS'rutants
Quarterly Quarterly
C
0.005
Annually I 40 CFR Part136
C W Composite; I - Instantaneous, G- G.rab, R - Recorded All metals ore to be analyzed as Total Metals Industry to provide continuous recording of PN
"- flow.
and
Permitter is required to provide adequate f+ow equalization (storage) and shall not exceed an instantaneous flow dischorge of 520 gallons perntlnutc between hours of3am to 9 pm.
°
• Permitree is allowed to exceed the instantaneous flow discharge of 520 gallons perminute between hours of 9 pm to 3 am, however shall not exceed 700 9A"1 ❑t any time. 0, 750• iV GD be
exceeded at any point,
shot!
not:
-nrm: Wk-W-5001-CP12 b� ur cu
Effecgive Date: 03/01/2013
Reiis°an Date: 01/0/2013
Revisj;:n 91. 0

Part i --Specific Condlitions
Permit No. CT12
air-L 1, :-ecliovnl I-
Receiving PGTVV name: First Broad lU Name: i Clearwater
. Paper
R eceiving POTW NPDES #: NCO024538 1U Number, CP12
cxzl
Eilluem", Urnits and Monitoring Requirements
Effective date for these limits: 01/01/2013 Pipe Number: 002
the per;-niftee incy c4jcf?o.j-ge jron this sn ti er p;p'e number
Expiration date.for these limits: 06/30/2014 40 CFR Number 430
-,-�
to hese sperific dOtes, j"fluent Yrnits,.Gnd rmnoringr
The Limits on this page are,
(Check one below} (if no, applicable put N/A)iccor,jlr:c
m puhreenTs.
Limits for entire permit period: X
interim Limits for period 41:
Interim Limits for period #2.*
LENAL LIMITS PAGE:
Concentration Limits
Mass -Based Limits
Monitoring Frequency
Sample
Required
Daily
Monthly
units
Daily
Monthly
Collection
Laboratory
Max.
Average
j
Max
Avg
Units
by Industry
I
byPOTW
Method
Detection
- -
1. Flow
---
I(C,I,Gor
Limits
2. PH
---.....MGD
j
Evezy Sample
Ever1Sarnple
N/A
N/A
3. BOD
GPM,
Quarterly
Quarterly
G
0.10
4. TSS
G P M, i
Quarterly
Quarterly
C
2.0
Quart
Quarterly
Quarter
Quarterly
C
2.5
S. Ammonia
mg/
Quarterly
Quarterly
C
0.10
6 Oil & grease
n s
Quarlerly
QvartQrty
G
5.0
7. T-Phenols
ma/L
Annually
Annually
8
Cyanide
mp/L
,
1/6 months
1/6 months
G
0.010
9.
Zinc
mp,/L
i
1/6 months
1/6 months
C
0.010
10.
Copper
1/6 months
1/6 months
C
I 0.002
11.
Chromium
/6 months
1/6 months
C
0, W S
12�
Cadmium
ME/]
C
0.002
13.
Bar um
mg/l
1I6 rnon.ths
1/6 Months
C
0.010 ---
14.
Arsenic
l
mg/I
1/6 months
1/6 months
C
15.
Lead
mp/I
1/6 months
1/6 months
c
0.010
16,
Mercury
i
mgjl
1/6 months
1/6 months
C
0.0002
17,
Moiybdenum
mg/I
1/6 months
1/,6 months
C
0.10
18.
Nickel
mg/Lmonths
1/6 months
C
0.010
19.
selenium
MWLmonths
1/6 months
C
0.010
20.
Silver
mg/L
1/6 months
1/6 months
C
0.010
t
Form: WIAT-S,�%-CPJZ Page 6 of 20
Ofectlye Date: 01101/20',3
Revision Vake: 01101/2013
Revision 1: 0

Part I — Specific Conditions
Permit No. CP12
G. definitions and Limit Page(s) notes:
In addition to the definitions in the City of Shelby Sewer Use and Industrial Wastewater Pretreatment Ordinance,
tl-re following definitions apply:
3.. Composite Sample
A composite sample for the monitoring requirements of this IUP, is defined as the automatic or manual
collection of one grab sample of constant volume, not less than 100 ml, collected every hour during the
entire Aischarge period on the sampling day. Sampling day shall be a typical production, and discharge
day.
Composite Sample, alternative definition
A composite sample for the monitoring requirements of this IUP is the same as described above unless
specifically defined below as the automatic or manual collection of a constant volume and constant time
grab samples collected. and composited according to the following criteria:
Specific volume of each grab sample= millimeters
Specific time interval between samples= hours
Total duration of sample collection period'= hours
Total number of grab samples to be composited= samples
2. Daily Monitoring Frequency:
Daily Monitoring Frequency as specified in this IUP shall mean each day of discharge.
Grab Sample
Grab sample forthe monitoring requirements of this IUP, is defined as a single "dip and take" sample
collected at a representative point in the discharge stream.
4. Instantaneous measurement:
An Instantaneous measurement for the monitoring requirements of this IUP; is defined as a single
reading, observation or measurement.
5. Ordinance: Refers to the Code of Ordinances for the City of Shelby, as amended from time to time
hereafter.
G. City:
.As used herein, City shall mean City of Shelby
7. Mass Loading:
Where concentration limits and mass loading limits are both listed for the same parameter, only the
concentration limit will be used when. flow is below permit limit. If the flow exceeds the permitted limit,
the mass -loading limit (Ibs./day) will take precedence over the concentration limit. Parameters and
prohibitions not included in this permit shall be regulated and limited in compliance with the Sewer Use
Ordinance. i
g pH Monitoring:
Only pHs analyzed by a certified lab within the 15 minute hold time will be used for compliance
determination (See City of Shelby Sewer Use Ordinance for definition). if a certified lab obtains a result
that is an excursion, in order to show that the excursion did not last more than 15 minutes, that person
Page 7 of 20
Fern: ,nWT-5001.cr:.2
ii Yective. Date: 01/01/2013

Part I — Specific Conditions
Permit No. CP12
may choose to wait up to 15 minutes from the collection of the first sample and obtain an additional pH
sample. in such cases, the 2"d pH will supersede the 1" one and will be utilized. For these lab analyzed pH
readings, excursions of <5 or >12 s.u. will be considered violations. The POTW Director reserves the right
to take enforcement action if he determines or suspects that any excursion has caused or contributed to
inhibition, pass through, or damage to the POTW.
Effluent pH Continuous monitoring and recording system
Permittee continuous effluent pH monitoring and recording systems information will not be used to judge
pH limit compliance, including chronic compliance; however if the continuous monitoring and recording
system indicates a reason for concern, this permit may be revised to require the data's use for pH limit
compliance (Chronic) judgment. The permittee is required to maintain the system to certain standards as
detailed below, Failure to maintain continuous operating efficiency or. failure to notify City of periods of
in -operation or inaccuracy may subject the permittee to enforcement action. The POTW tirector
reserves the right to take enforcement action if he determines that any value indicated by the continuous
pH monitoring and recording system constitutes documentation of a slug load, including those that may
have caused or contributed to inhibition, pass -through or damage to the POTW.
The continuous pH monitoring and recording system shall be maintained in proper operating condition at
all times. All such devices shall be installed, calibrated and maintained to ensure accuracy. Calibration of
the system shall be performed per the manufacturer's recommendations as often as necessary to
maintain correct pH readings at all times, with a minimum calibration frequency of once per month. The
permittee shall keep records to verify the proper maintenance and calibration of the system for a period
of three years. The records shall be made available to City upon request. The permittee will shall keep a
log of the time, date and reason for any "down time" and shall notify the City as soon as possible of any
period when the effluent pH monitoring and recording system is not operational or any ektencled periods
of inaccuracy. The permittee is required to have spare parts on hand in order to limit periods of in -
operation.
9. Toxicity Screening:
Industrial discharges may be monitored for Toxicity. Toxicity screenings will be evaluated on an individual
basis based on flow and treatability concerns. The Pennittee shall be billed for toxicity screening at the
arnount set forth in the City of Shelby Water and Sewer Rate Schedules.
10. Chronic Refractory Toxicity Evaluation: Within one hundred twenty (120) days of the effective date of
this permit, unless all pertinent information has been previously submitted, the Permittee must complete
and submit the following to the City:
a) A detailed evaluation of all water treatment, cleaning, maintenance, and process chemicals used
in quantities over 50 lbs./day that could be discharged to the City. This evaluation shall include, at
a minimum, the specific chemical name and not just the trade name of the materials, available
information on the aquatic toxicity of the materials, and manufacturers or literature data on the
materials.
NOTE: New chemicals which fall under the criteria stated herein used after the detailed evaluation is
completed must also be evaluated and a report submitted to the City, as defined herein, within ten (10)
days afterfirst use by Permittee.
Pape 8 of 20
norm: VVINI-5021-CP12
t_ffective Date: 01/01/ 201�3
.... Uioji Dal r 01/01/2013

I
Part I — Specific Conditions
Permit No. CP12
t LTMP parameters: The Headworks Long Term Monitoring Plan specifies a minimum monitoring
frequency of certain parameters which are pollutants of concern. Such parameters, may or may not be
listed individually on the permit limits page, but shall be monitored as required by the Long Term
Monitoring Plan.
Page 9 of 20
Form: %VWT-SOOT-CP12.
Eifectivaa Date: Cl/Cl/2C13

Part If General Conditions
Outline of PART 11,
1,
Representative Sampling
2.
Reporting
3.
Test Procedures
4.
Additional Monitoring by Permittee
5.
Duty to comply
6..
Duty to Mitigate
7.
Facilities Operation, Bypass
8.
Removed substances
9.
Upset Conditions
"of
10.
RightEntry
11.
Availability of Records
12.
Duty to provide information
1.3.
Signatory Requirements
14.
Toxic Pollutants
15.
Civil and Criminal Liability
16.
Federal and/or State Laws
1. Representative Sampling
General Conditions
Permit No, CP12
17.
Penalties
18.
Need to Halt or Reduce
19.
Transferability
20.
Property Rights
21.
Seve-ability
22.
Modification, Revocation, Termination
23.
Reapplication
24.
Dilution Prohibition
25.
Reports of Changed Conditions
26.
Construction of pretreatment facilities
27.
Reopener
28.
Categorical Reopener
29.
General Prohibitive Standards
30.
Reports of Potential Problems
31.
Surcharges
32.
Samples and measurements taken as requited herein shall be representative of the volume and
nature of the monitored discharge. All samples shall be taken at the monitoring points specified in
this permit and, unless otherwise specified, before theeffluent joins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to, and approval by, the permit issuing authority.
2. Reporting
a.) Monitoring results obtained by the permittee shall be reported on forms specified by the City,
postmarked no later than the twentieth day of the month following the month in which the
samples were taken. If no discharge occurs during a reporting period (herein defined as each
calendar rnonth) in which a sampling event was to have occurred, a form with the phrase "no
discharge" shall be submitted. Copies of these and all other reports required herein shall be
submitted to the City at the following address:
Pretreatment Coordinator
City of Shelby Utilities
P,O. Box 207
Shelby, N.C. 28151-0207
b.j If the sampling performed by the permittee indicates a violation, the permittee shall notify the
City within 24 hours of becoming aware of the violation. The permittee shall also repeat the
sampling and analysis and submit the results of the repeat analysis to the City within 30 days
after becoming aware of the violation.
Pate 10 of 2.0
Farm; W*7-5001-CP12
El.edwc Cate; 01V01/Z013
P,e;•i�;azn (37?[r.: 01/01./ 211..3

General Conditions
Permit No. CP12
c.) if no self -monitoring is required by this IUP, and the sampling performed by the City indicates a
violation, the City shall repeat the sampling and analysis and receive the results of the repeat
analysis within 30 days after becoming aware of the violation.
d.) If the User receives a split of the sample collected by the City, information regarding the sample
must be documented on the Record of Split Sampling Event form. This form must be
postmarked, hand delivered or faxed within seven (7) days of the sample collection. if the User
fails to submit the required form, the results obtained from the sampling event may be excluded
from use for compliance and surcharge purposes
3. Test Procedures
All pollutant analyses must be performed by a laboratory certified by the State o.f North Carolina for
each parameter analyzed and in accordance with the techniques prescribed in 40 CFR Part 136 unless
otherwise specified in an applicable categorical. pretreatment standard. If 40 CFR Part 136 does not
contain analytical techniques for the pollutant in question, analyses must still be performed by a
laboratory. certified by the State of North Carolina for each parameter analyzed. Toxicity testing must
be performed using the protocol for toxicity screening as stated within this permit document.
4. Additional Monitoring -by Permittee
If the permittee monitors any pollutant at the location(s) designated herein more- frequently than
required by this permit, using approved analytical methods as specified above, the results of such
monitoring shall be submitted to .the City of Shelby. The City of Shelby may require more frequent
monitoring or the monitoring of other pollutants not required in this permit by written notification.
Industrial Sampling charges for the monitoring requirements as .stipulated the responsibility by the
City in Section I F are included in the Monthly Pretreatment Fee Charge, with the exception of the
toxicity monitoring and any additional sampling required by the City and/or any additional sampling
events needed for the industry to maintain compliance for the report period. The costs are also
outlined in the City of Shelby Fee Schedule.
5. Duty to Comply
This permit is issued pursuant to the Code of Ordinances of the City. of Shelby and applicable State and
Federal Laws and Regulations as they now exist or as they may hereinafter be modified. The permittee
must comply with all such Ordinances, laws, regulations and conditions of this permit. Any permit
noncompliance constitutes a violation of the Code of Ordinances and is grounds for an enforcement
action.
6. Duty to Mitigate - .Prevention of Adverse Impact
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
permit which has a reasonable likelihood of adversely affecting human health, the POTW,. the waters
receiving the POTW's discharge, or the environment.
P aCe Z 1. of 70
Form: WWr•500.1-CP12
Effective Date: 01/O1/2013
Re*ien Date: 01101/2013

General Conditions
Permit No. CP12
7. Facilities Operation, Bypass
The permittee shall at all times maintain in good working order and operate as efficiently as possible,
all control facilities or systems installed or used by the permittee to achieve compliance with the
terms and conditions of this permit.. Bypass of treatment facilities is prohibited except when approved
in advance by the City. Bypass approval shall be given only when such bypass is in compliance with A0
CFR A03.17,
S. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of
wastewaters shall be disposed of in a manner such as to prevent any pollutants from such materials
from entering the sewer system. The permittee is responsible for assuring its compliance with any
requirements regarding the generation, treatment, storage, and/or disposal of "Hazardous waste" as
defined under the Federal Resource Conservation and Recovery Act.
9. Upset Conditions
An "upset" means an exceptional incident in which there is an unintentional and temporary
noncompliance with the effluent limitations of this permit because of factors beyond the reasonable
control of the permittee.. An upset does riot include noncompliance to the extent caused by
operational error, improperly designed or inadequate treatment facilities, lack of preventative
maintenance, or careless or improper operations.
An upset may constitute an affirmative defense for action brought for the noncompliance. The
permittee has the burden of proof to provide evidence and demonstrate that none of the factors
specifically listed above were responsible for the noncompliance.
10. Right of Entry
The permittee shall allow the staff of the State of North Carolina Department of Environment and
Natural Resources, Division of Water Quality, the Regional Administrator of the Environmental
Protection Agency, the City of Shelby, and/or their authorized representatives, upon the presentation
of credentials:
1. To enter upon the permittee"s premises where a real or potential discharge is located or in
which records are required to be kept under the terms and conditions of this permit; and
2. At reasonable times to have access to and copy records required to be kept under the terms and
conditions of this permit; to inspect any monitoring equipment or monitoring method required
in this permit; and to sample any discharge of pollutants.
3.1. Availability of Records and Reports
The permittee shall retain records of all monitoring information, including all calibration and
maintenance records as well as copies of reports and information used to complete the application, for
this permit for at least three years. All records that pertain to matters that are subject to any type of
enforcement action shall be retained and preserved by the permittee until all enforcement activities
have concluded and all periods of limitation with respect to any and all appeals have expired.
Page 12 of 20
For L+ibVl-h'001-CF17.
Effed ivk Gate: 01/01/2013
nr`visiai JOl£: 01/U2,C%013

General Conditions
Permit No. CP12
Except for data determined to be confidential under the -Sewer Use Ordinance, all reports prepared in
accordance with terms of this permit shall be available for public inspection at the City. As required by
the Sewer Use Ordinance, effluent data shall not be considered confidential.
12. Duty to Provide Information
The permittee shall furnish to the Public Utilities Director or his/'ter designees, within a reasonable
time, any information which the Director, his/her designee, or the Division of Water Quality may
request to determine whether cause exists for modifying, revoking and reissuing, or terminating this
permit or to determine compliance with this permit. The permittee shall also furnish, upon request,
copies of records required to be kept by this permit.
1.3. Signatory Requirements
All reports or information submitted pursuant to the requirements of this permit must be signed and
certified by the Authorized Representative as defined under the Sewer Use Ordinance. If the
designation of an Authorized Representative is no longer accuratee because a different individual or
position has responsibility for the overall operation of the facility, or overall responsibility for
environmental matters for the company, a new authorization satisfying the requirements of this
section must be submitted to the City prior to or together with any reports to be signed by an
authorized representative.
14. Toxic Pollutants
If a toxic effluent standard or prohibition (including any schedule of compliance specified in such
effluent standard or prohibition) is established under Section 307(a) of the Federal Clean Water Act
fora toxic pollutant which is present in the discharge and such standard or prohibition is more
stringent than any limitation for such pollutant in this permit, this permit may be revised or modified
in accordance with the toxic effluent standard or prohibition and the permittee so notified.
15. Civil and Criminal Liability
Nothing in this permit shall be construed to relieve the permittee from civil or criminal penalties for
noncompliance.
16. Federal and/or State Laws
Nothing in this.permit shall be construed to preclude the institution of any legal action or relieve the
permittee from any responsibilities, liabilities, or penalties established pursuant to any applicable
Federal and/or State law or regulation.
17. Penalties
The Sewer Use Ordinance of the City of Shelby provides that any person who violates a permit
condition is .subject to a civil penalty not to exceed$25,000 dollars per day of such violation.
Under state law, (1141CIGJ 143`215.68), under cell-kaitn, circumstances it is a crime 410 violate terms,.
conditions, or requirements of pretreatment .permits. It is a crime to knowingly make any false
statement, representation, or certification in any record or other document submitted or required to
be maintained under this permit, including monitoring reports or reports of compliance or
Page 13 of 20
Form: WWT-5001-CP:12
effective Date: 01/01/2013
Revision Date: 01/01/2013

General Conditions
Permit No. CP12
noncompliance. These crimes are enforced at the prosecutorial discretion of the local District
Attorney.
With respect to wastewater treatment, any user who is found to have violated an Order of the City
Council or who fails to comply with any provisions of this permit or of the Ordinance, and the orders,
rules, regulations, and permits issued pursuant thereto shall be subject to such fines and penalties as
are provided in the Ordinance for each offense. Each day on which a violation shall occur or continue
shall be deemed a separate and distinct offense. In addition to the penalties, the City mayrecover
reasonable attorne.y's fees, court costs, court reporter's fees and other expenses of litigation by
appropriate suit at law against the person found to have violated the Ordinance or the orders, rules,
regulations, and permits issued.
18. need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity to maintain compliance with the conditions of the permit.
19. Transferability
This permit shall not be reassigned or transferred or sold to a new owner, new user, different
premises, or a new or changed operation without approval of the City.
20. Property Rights
This permit does not convey any property rights in either real or personal property, or any exclusive
privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor
any infringement of Federal, State or local laws or regulations.
21. Severability
The provisions of this permit are severable and, if any provision of this permit or the application of any
provision of this permit to any circumstance is held invalid, the application of such provision to other
circumstances and the remainder of this permit shall not be affected thereby.
22. Permit Modification, Revocation, Termination
This permit may be modified, revoked and reissued or terminated with cause in accordance to the
requirements of the City of Shelby Sewer Use Ordinance and North Carolina General Statute or
implementing regulations.
23. Re -Application for Permit Renewal
The permittee is responsible for filing an application for reissuance of this permit.at least 180 days
prior to its expiration date.
24, Dilution Prohibition
The permittee shall not increase the use of potable or process water or in any other way attempt to
dilute the discharge as a partial or complete substitute for adequate treatment to achieve compliance
with the limitations contained in this permit.
Page 14 of 20
rm m� WvVi'-5001.-CP12
F,ffei-.JMD Up: 0]/D1/r,013
Fievi,ion Dote; W01J2013

General Conditions
Permit NO.'CP12
2.5. Reports of Changed Conditions
The permittee shall give notice to the City of Shelby of any planned significant changes to the
permittee's operations or system which might alter the nature, quality, or volume of its wastewater at
least 90 days before the change. The permittee shall not begin the changes until receiving written
approval from the City of Shelby. Also see Part II, 30 below for additional reporting requirements for
spill/slug issues,
Significant changes may include but are not limited to:
(a) increases or decreases to production;
(b) increases in discharge of previously reported pollutants;
(c) discharge of pollutants not previously reported to the City of Shelby;
(d) new or changed product lines;
(e) new or changed manufacturing processes and/or chemistry.
2.6. Construction
No construction of pretreatment facilities or additions thereto shall be .begun until Final Plans and
Specifications have been submitted to the City and written approval and an Authorization to Construct
(A to C) have been issued. This submission and review process shall include:
1. Submission of three (3) copies of the Final Plans and Specifications to the City of Shelby. The City
may require these submissions be signed by a Professional Engineer registered in North Carolina,
2. Construction shall not begin until the permittee receives from the City of Shelby an Authorization
to Construct, including a signed copy of the Final Plans and Specifications.
3. upon completion of the construction and prior to the operation of the facility, the City must
receive written certification from a registered Professional Engineer certifying that the newly
constructed facility has been installed in accordance with the pretreatment permit, the
Authorization to Construct, and the Final Plans and Specifications.
4. At least 48 hours prior to the operation of the facility, the permittee must notify the City and
request a facility inspection.
S. If, after completion of construction, the facility fails to perform satisfactorily, the permittee shall
take immediate corrective action and notify the City of Shelby. Any additional construction will
require a new Authorization to Construct.
6. The Authorization to Construct.shall not, in any way, be construed to constitute approval by the
City of Shelby of the process described in the Final Plans and Specifications, or as a guarantee by
the City that the process will perform as described therein, The responsibility for meeting the
limitations and conditions of the permit and the conditions of the City of Shelby Sewer Use and
industrial Wastewater Pretreatment Ordinance lies solely with the permittee, and nothing in the
Authorization to Construct shall be construed to relieve the permittee of that responsibility.
7. Any construction of pretreatment facilities without prior approval, including an Authorization to
Construct from the City of and a signed set of Final Plans and Specifications, is a violation of the
Page 15 of 20
Fonw WWT-5001-GF12
Effedive Date: 01/01/7013
R,Msion Date: 01/01 f201.3

F
General Conditions
Permit No. CP12
pretreatment permit and will subject the permittee to enforcement action in accordance with the
City of .Shelby Sewer Use and Industrial Wastewater Pretreatment Ordinance.
27. Reopener
The permit shall be modified or, alternatively, revoked and reissued to comply with any applicable
effluent standard or limitation for the control of any pollutant shown to contribute to toxicity of the
WWTP effluent or any pollutant that is otherwise limited by the POTW discharge permit. The permit
as modified or reissued under this paragraph may also contain any other requirements of State or
Federal pretreatment regulations then applicable.
28. Categorical Reopener
This permit shall be modified, or alternatively, revoked and reissued, to comply with any applicable
effluent standard or limitation issued or approved under Sections 302(b)(2)(C) and (D), 304(b)(2), and
307(a)(2) of the Clean Water Act, if the effluent standard or limitation so issued or approved:
1.) Contains different conditions or is otherwise more stringent than any effluent limitation in this
permit; or
2.) Controls any pollutant not limited in this permit.
The permit as modified or reissued under this paragraph shall also contain any other requirements of
the Act then applicable.
29. General Prohibitive Standards
The permittee shall comply with the general prohibitive discharge standards in 40 CFR 403.5 (a) and
(b) of the Federal pretreatment regulations.
30. Potential Problems
The permittee shall provide protection from accidental and slug discharges of prohibited materials and
other substances regulated by this permit. The permittee shall also notify the POTW immediately of
any changes at its facility affecting the potential for spills and other accidental discharge, discharge of
a non -routine, episodic nature, a non -customary batch discharge, or a slug load as defined in the.
Sewer Use Ordinance.
Additionally, the permittee shall notify by telephone the City immediately of all discharges that could
cause problems to the POTW including any slug loadings as defined in the Sewer Use Ordinance. If the
permittee experiences such a discharge, they shall inform the City immediately upon the first
awareness of the commencement of the discharge. Notification shall include location of the
discharge, type of waste, concentration and volume if known and corrective actions taken by the
permittee. A written follow -Lip report thereof shall be filed by the permittee within five (5) days,
unless waived by the City.
1. Surcharges
The character and concentration of the constituents of the wastewater used in determining
surcharges shall be determined by samples collected and analyzed by the City or, with prior.approval
of the POTW Director, collected by the User and analyzed by a laboratory certified by the State of
Page 16 of 20
Form, WWT-500].•4P.;,2
Fletttve Date: 01101./213
Re_visicn Date: 01/01.12.01

General Conditions
Permit No. CP12
North Carolina for those parameters, or both. Samples shall be collected in such a manner as to be
representative of the actual discharge and shall be analyzed using procedures set forth in 40 CFR Part
136 by a State of North Carolina Approval Authority certified laboratory for each parameter analyzed.
Flow must be recorded and adjusted on an Industrial Flow Monitoring Report form, and reported on
the IDMR for surcharge calculations.
Although all data collected will be considered, the determination of the character and concentration
of the constituents of the wastewater discharge by the POTW Director shall be binding as a basis for
charges_ Volume of flow shall be based on the metered water consumption as measured by a City
water meter or other monitoring devices that have been approved for use by the City and meet the
City's calibration requirements. Metered flow readings adjusted to a 24 hour period will be utilized
and will be determined by manual or by electronic reading of the meter(s). If fo.r any reason daily
meter readings are not available, the best available flow data will be utilized to determine surcharges.
32. Legal Requirement to Meet Categorical Standards
The Permittee is required to meet federal categorical standards where applicable. Limits in this
permit are enforceable as local limits, but they do not take the place of categorical standards.
Compliance with local limits does not relieve the legal requirement to be in compliance with the
categorical standard itself.
Page 1.7 of 20
Forst: WWT-5001-C.P32
Effective Date: O1/0!/20!3
Revision hate: 01/01/2013

Special Conditions
Permit No. CP12
Part III Special Conditions
1. Slug/Spill Control Measures
In addition to the requirements in Part 11, 30, the Permittee shall complete installation and/or
commence implementation, operation, and/or maintenance of the following specific protection
Measures, Activities, Plans. Etc. (Items without specific completion dates, or marked as "Continuous."
must be performed for the entire duration of the permit):
The Permittee shall provide updates to the Control Authority as required by Part II, 30, of this IUP.
Modifications to the measures shall be approved by the Control Authority prior to
installation/implementation. If a measure fails, the Control Authority shall be notified within 24
hours.
2. Sludge Management Plan
Ninety days prior to the initial disposal of sludge generated by any pretreatment facility, the permittee
shall submit a sludge management plan to the Control Authority, if not included in the slug/spill
control measures.
3. Flow Measurement Requirements - (For SIUs with discharge flow meters)
The City of Shelby shall use the flows registered on the permittee's final effluent flow meter located at
Pipe 001 for the purpose of sewer billing, surcharge calculation and flow limit compliance. The
permittee will required to submit records of daily wastewater discharge to the Pretreatment Section
no later than the fifteenth (15") day of each month.
The permittee shall maintain appropriate discharge flow measurement devices and methods
consistent with approved scientific practices to ensure the accuracy and reliability of measurements of
the volume of monitored discharges. Devices installed shall be a continuous recording flow meter
Page 7 8 of 20
Form: L4'VJ7'-5001-f.P;12
Effective Date: D1/01/2013
flee: i,!cn o7te:

I
Special Conditions
Permit No. CP12
capable of measuring flows with a maximum deviation of less than 10% from true discharge rates
throughout the range of expected discharge volumes. The devices shall be installed, calibrated, and
maintained by qualified contractor/vendor to ensure accuracy.
Modifications to the flow metering equipment shall be approved by the City prior to installation. If a
required flow measurement device fails, the City shall be notified within 24 hours. The direct
discharge of unmetered effluent flow is strictly prohibited.
SIU to provide 11.0 power and 4-20 ma connection with flow measurement device. SIU will also allow
City to erect SCADA RTU panel and antennae at the facility to be able to transmit instantaneous flow
measurements to the City of Shelby.
4. Certified Laboratory Analysis
Pollutant analysis shall be performed by a North Carolina Division of Water Quality Certified
Laboratory that is certified in the analysis of the pollutant in wastewater.
5. Certified Operator
A certified operator is not required at this time however an operator must be available to manage and
document daily operation and maintenance of the facility. The permittee shall name an
operator/backup operator and notify the City of any personnel changes within 30 days of those
changes occurring.
Ei. Biocide Certification
In lieu of the categorical based limits listed in 40 CFR Part 430.120, the permittee will make the
following certification at permit .issuance and then annually thereafter:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with
the wastewater discharge permit, l certify that, to the best of my knowledge no chlorophenolic
biocides are being used at this facility."
At a minimum, the certification statement is due by January I" of each year.
i. Plant Start-up Interim Limits
In consideration of the issues with the initial start-up operations of the pretreatment facility at
Clearwater; the City of Shelby is including interim Total Suspended Solids (TSS) limits for the Pipe 001
discharge. Limits will be tiered in such a way that they stepped down over a period of months until
Clearwater will be required to meet the final TSS limits stipulated in the permit.
The User hereby is required to:
A. Implement any means necessary to meet interim permit limits established by the POTW.
B. Meet and comply with all terms and conditions of this permit except those outlined in these
special conditions.
Page 19 of 20
Pars:?: V,14VT-5001.CP.12
Ef#ec=.;•;e Gate: 01101/2013
Revi.5lanDater 01/N120j3

Special Conditions
Permit No. CP12
C. The. Permittee will undertake activities necessary to bring the User into compliance with the
following schedule:
I. Prepare a report of process alternatives and/or pollution prevention/waste
minimization alternatives designed to achieve compliance.
2. If required, submit necessary drawings and information to obtain Authorization to
Construct from the City of Shelby.
3. Begin construction and/or implement identified process alternative(s), pollution
prevention and waste minimization alternatives.
4. Complete all necessary changes to bring User in .compliance with final permit limits.
D. The Interim limits will be as follows:
Date initiated
TSS interim Limit
January 15, 2013
1,500 mg/L
February 15, 2013
1,000 mg/L
March 15, 2013
750 mg/L
April 15, 2013
450 mg/L
May 15, 2013
150 mg/L Final Permit Limit Compliance Date
E. City will require permittee to provide a written report within 5 days following each date
specified in the Interim Limit Section above. Each report shall be narrative in form and shall
detail the activities undertaken since the last report to achieve compliance. The report shall
indicate whether the Permittee has met the due date for the activity and include a statement
explaining the cause of not meeting the due date of an activity and probability of meeting the
next activity due date.
F. In addition to the reports required above the permittee shall submit all sampling, monitoring,
and analysis reports for testing conducted on the effluent discharge during the period to
achieve compliance.
G. Once compliance is achieved, the special condition interim limits (Section 7) and requirements
will expire and the permittee shall be subject to all terms of this permit,
Ii. In performance of activities under these special conditions, user must otherwise follow the
procedures, rules, regulations, ordinances and statutes of the City, State and Federal
governments as they apply to the Permittee. Nothing contained herein shall be construed as a
waiver thereof by the City.
I. It is the responsibility of the City to enforce all applicable Federal, State and local
pretreatment regulations. These regulations are outlined in Federal Regulation 40 CFR 403,
State Regulations 15A NCAC 2H .0900 and the local City of Shelby Sewer Use Ordinance. In
the event that progress is not being made or compliance is not achieved by the date of May
15, 2013, the City of Shelby can evaluate the User's performance and act in accordance with
the Pretreatment Enforcement Response Plan and the City of Shelby Sewer Use Ordinance as
necessary.
Page 20 of 20
Fenn: IVIn!T-$QOJ •lPi2
Witt,: 0110.1/7
EI;'ertivc UJ[c: Ol,r()'/7013

April 15, 2013
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Construction Grants and Loans Section
1633 Mail Service Center
Raleigh, NC 27699-1633
Via Certified First Class Mail, Return Receipt #70I2 22I0 0000 5096 6496
RE: APPLICATION FOR TAX CERTIFICATION & EXEMPTION
CLEARWATER PAPER CORPORATION
671 WASHBURN SWITCH ROAD
SHELBY, NC 28150
Dear Sirs:
Please find enclosed the Application for Certification and Exemption for water -cleaning
equipment owned and operated by Clearwater Paper Corporation at 671 Washburn Switch Road
in Shelby, North Carolina. Please review this application and contact our office to schedule an
appointment for inspection. Thank you for your assistance in this matter, and please do not
hesitate to call our offices with any questions or concerns.
2mes
y,
. Garza
Managing Partner, Industrial Valuation Services
Agent, Clearwater Paper Corporation.
[e-mail]
apt:. �

t
OCT I I Z012
TAX C E RT I F I CAT I O IVY
In accordance with the provisions of the General Statutes of North Carolina [G.S. 130A -
294(a)(3); G.S. 105-122(b); G.S. 105-130.10; G.S. 105-130.5(b)(6); and G.S. 105-275(8)],
this is to certify that:
CLEARWATER PAPER CORP - SHELBY CONVERTING PLANT
671 WASHBURN SWITCH ROAD
SHELBY NC 28150
CLEVELAND COUNTY
filed a request for tax certification on resource recovery or recycling facilities and/or
equipment on 8/17/2012. .
The Division of Waste Management of the North Carolina Department of Environment and
Natural Resources inspected or verified these resource recovery or recycling facilities and/or
equipment on 9117/2012, and found that the facilities and/or equipment in Enclosure (1) meet
the requirements of the Standards for Special Tax Treatment of Recycling and Resource
Recovery Equipment and Facilities.
DATE TAX CERTIFICATION APPROVED: 9/20/2012
son Watkins, Environmental Supervisor
Field Operations Branch, Solid Waste Section
Division of Waste Management
Enclosure: Property Listing
cc: Cleveland County Tax Supervisor
Bill Wagner, Environmental Senior Specialist
Jason Watkins, Environmental Supervisor
1646 Mail Service Center, Raleigh, North Carolina 27699-1646 Phone: [phone]
An Equal Opportunity/Affirmative Action Employer

4
CLEARWATER PAPER CORP -y' 4ELB`i CONVERTI
CLEVELAND COUNTY
9/20/2012
Property Type / Description
Year Acquired
Serial/Asset Number
Original Cost
COMPACTOR #1 MDL 7460-2-6
11
AN 506773, SN 101210472
$35,300.00
2 TRIM FANS
11
ASSET #506811
$63,890.00
SHREDDER LOG FEED HOPPER AND FOOD CONVEYOR
11
ASSET #506853
$53,850.00
SHREDDER
11
ASSET #506861
$114,480.00
SHREDDER TRANSFER FAN TCF915 RBP 25HP
11
ASSET #506870
$25,670.00
BALER LOG FEED HOPPER AND FOOD CONVEYOR
11
ASSET #506896
$53,850.00
BALER C+M 6042-AT310
11
ASSET #506909
$167,426.00
TRIM SYSTEM
it
ASSET #506925
$239,020.00 .
Total
$753,486.00
Page 2 of 2

MCDENR
North Carolina Department of Environment and Natura
Division of Water Quality
Pat McCrory Thomas A. Reeder
Governor Acting Director
July 22, 2013
537
Mr. John Kuhn
Rockwood Lithium, Inc
348 Holiday Inn Drive
Kings Mountain, NC 28086
Resources
FILE
Subject: North Carolina Wastewater/Groundwater Laboratory Certification
Dear Mr. Kuhn:
John E. Skvarla, III
Secretary
Per the written request dated July 15, 2013, we are discontinuing the North Carolina
Wastewater/Groundwater Laboratory Certification of ,your laboratory #573 Rockwood Lithium,
Inc. We will proceed with removing your laboratory from the certified list. You are reminded that
it is not legal to analyze environmental samples required by G. S. 143 Article 21 without our
certification.
Do not hesitate to call on us if we can be of assistance in the future. Contact us immediately at
[phone] if this action is incorrect or if you have questions.
Sincerely,
J. Kent Wiggins
Laboratory Section Chief
Laboratory Section
cc: Chet Whiting
Gary Francies
Mooresville Regional Office
DENR DWQ Laboratory Section NC Wastewater/Groundwater Laboratory Certification Branch
1623 Mail Service Center, Raleigh, North Carolina 27699-1623
Location: 4405 Reedy Creek Road. Raleigh, North Carolina 27607-6445
Phone: [phone] i FAX: [phone]
Internet: www.dwQlab.orq
Nne
ordiCarolina
An Equal Opportunity \ Affirmative Action Employer

­07
EMERGENCY SERVICFSdggA
ENVIRONMENTAL
July 17, 2013 Sent Certified Mail 7012 2210 0001 4287 2377
North Carolina Department of Environment and Natural Resources
Mr. Mike Parker RE:CE-111:n
610 East Center Ave. DIVISION OF WATER rLIALI T Y
Mooresville, North Carolina 28115
JUL 2 2 2013
RE: DIESEL FUEL RELEASE — FINAL REPORT I00OP ESViLLIE F;_:G u NAL OFFIv2
GREATWIDE LOGISTICS SERVICES
2354 INTERSTATE 85 NORTHBOUND
GROVER, CLEVELAND COUNTY, NORTH CAROLINA
CES PROJECT NO..
EM130212S3
NRC INCIDENT NO.
1039925
NCDENR REPORT NO.
030313
GREATWIDE CLAIM NO.
30-5693
Mr. Parker;
Please accept this document as the final report detailing the emergency response and corrective actions
taken regarding the diesel fuel release that occurred on March 3, 2013,. at the above -referenced location.
Attached is a copy of 'the Cura Emergency Services, L.C. (CES) hazardous materials incident report
(HMIR), as well as a Professional Geologist report prepared by our subcontractor describing the response
and corrective actions taken regarding the above -referenced incident. As the quantity of diesel fuel
released was above the minimum reportable level of 25 gallons as required by state regulations, the CES
incident manager made verbal notification to the National Response Center (NRC) at approximately 3:17
am CST on March 3, 2013, and report number 1039925 was assigned to the incident. The CES incident
manager also made verbal notification of the release to the North Carolina Department of Environment
and Natural Resources (NCDENR) and report number 030313 was assigned to the incident.
Following remediation operations, no visual or olfactory evidence of diesel fuel existed at the site.
Analytical data shows Gasoline Range Organics (GRO) and Diesel Range Organics (DRO) levels within
acceptable limits per state regulations (see attached Professional Geologist report). Based on these
results, it appears that all corrective actions were successful and no further actions should be required.
CES recommends that the incident be closed at this time.
Greatwide Logistics Services and Cura Emergency Services, L.C. appreciate your assistance during this
incident. Should any questions arise, please feel free to contact us at [phone].

Respectfully,
Cura Emergency Services, L.C.
Brett E. Johnson
Incident Manager
Attachments: CES Hazardous Materials Incident Report
Physical Geologist Report
Site Photos
Waste Disposal Manifest
CC. Greatwide Logistics Services
Mr. Jay Cole
12404 Park Central, Suite 300S
Dallas, TX 75251
[e-mail]

Cura Emergency Services, L.C.
6205 Chapel Hill Boulevard, Suite 100
Plano, Texas 75093
Ph. [phone] Fax [phone]
A. Incident Information:
Client File No.: 30-5693
Incident Manager: Brett Johnson
Project No.: EM13021253 Project Name: Greatwide Logistics Services - Grover - NC
Date of Loss: 3/3/2013 Time Loss Occured: 01:21 AM EST
Date Reported to CES: 3/3/2013 Time Reported to CES: 02:38 AM CST
Person Reporting: Jay Cole Phone: [phone]
Driver: Tractor #: Trailer #:
Incident Location Contact: John Pallent Phone: [phone]
Incident Location: 23 54 Interstate 85 NB
City: Grover County: Cleveland State: NC
Incident Description:
On March 3, 2013, at approximately 1:21 am EST, a tractor -trailer operated by Greatwide Logistics
Services (GLS) was traveling at the above -referenced location when the unit exited the roadway, detroying_
the tractor's cab, and releasing approximately 200 gallons of diesel fuel to the surface of a concrete drainage
gutter and surrounding soil. The diesel fuel further migrated into a nearby creek
Surfaces affected: 0 soil/grass ❑ asphalt V concrete ❑ other
Water affected: V surface ❑ groundwater ❑ none ❑ other creek
Sensitive Receptor Impact:
Creek
Wednesday, July 17, 2013 EM13021253

Incident Report (Cont.)
B. Chemical Information
Project No.: EM13021253
Client File No.: 30-5693
Reportable Reported Actual* Gal/
Quantity Volume Volume Lbs
.Chemical: diesel fuel, 3, 1993 25 200 200 Gals
Chemical:
Chemical:
C. Health & Safety:
Site Monitoring (if applicable): PPE:
❑ Vapor Concentration (ppm): unmetered ❑ Level A ❑ Level C
❑ Available Oxygen (%): ambient ❑ Level B❑ Level D
❑ LEL Exceeded ❑ MSDS Attached
Site Special Precations:
No special precautions were noted for this site.
Site Condition:
No complicating conditions existed at the site during clean up operations
Injuries: Explain:
Yes The driver was transported to the emergency room for treatment.
D. Emergency Response:
Initial Emergency Actions:
On March 3, 3013, Mr. John Pallent and other members of Cleveland County Fire Department (CCFD) arrived
at the site to ensure public safety and provide preliminary response for the diesel fuel release CCFD
-personnel deployed absorbent boom and pads to the diesel fuel -impacted creek to prevent further migration of
diesel fuel from the site.
At approximately 2:38 am CST, a representative from GLS, Mr. Jay Cole, retained Cura Emergency Services,
L.C. (CES) to manage the environmental remediation of the site on their behalf. Based on the available
information. the CES incident manager dispatched a crew from JBR Environmental Services (JBR) to assess
and remediate the site.
*Unless specified in the Incident Description section, the Actual Volume" is an estimate, based on the observations of the CES subcontractor.
Wednesday, July 17, 2013 EM13021253

Incident Report (Cont.)
Project No.: EM13021253
E. Corrective Actions:
Client File No.: 30-5693
Corrective Actions:
On March 3 2013 at approximately 5.30 am EST JBR personnel arrived at the site and performed a walk-
through with Mr. Pallent, assessing the release and devising a remediation plan. Following the initial walk-
through, the JBR crew deployed granular absorbents to the diesel fuel -impacted gutter and worked it in with
hand tools. The spent absorbents were then loaded int6 a lined roll -off box for transport and disposal The
crew then deployed absorbents pads to the creek to collect any diesel fuel from the surface and loaded the spent
pads into the lined roll -off box Once the spent pads were removed, JBR personnel used a vacuum truck to
collect any remaining diesel fuel and impacted water from the creek and pumped it into one (1) 55-gallon drum
for transport and disposal. Following the collection of diesel fuel -impacted water, the crew used an excavator
to remove all diesel fuel -impacted soil from the site Excavation operations continued until no visual or
olfactory evidence of diesel fuel existed at the site. After securing the site JBR personnel demobilized and
would return the following day to backfill and over seed the excavation
See final report for additional details.
On Monday, March 4, 2013, JBR personnel returned to the site with top soil, straw, and grass seed to complete
F. Responsible Party Information:
Responsible Party: Greatwide Logistics Services
Contact: Jay Cole Title: 0 Send report
Address: 12404 Park Central, Suite 300S
City: Dallas
State: TX Zip: 75251-
Phone: [phone]
Fax: [phone]
Wednesday, July 17, 2013 EM13021253

Incident Report (Cont.)
Project.No.: EM130212S3
G. Regulatory Agencies:
Client File No.:30-5693
❑� Reportable Spill (check if yes)
Explain.: Pursuant to North Carolina state regulations, petroleum related releases in excess of 25 gallons
are considered reportable.
National Response Center (U.S. Coast Guard)
Contact Person: Civilian Bennett
Address:
City:
W Report Required
Note:
NCDENR-Mooresville
Contact Person:
State:
Contact Date: 3/3/2013
Phone:[phone] Contact Time: 3:17 AM
Confirmation No.:1039925
Zip: Fax: _
Contact Date: 3/3/2013
Address: 610 East Center Ave. Phone:[phone]
City: Mooresville State: NC Zip: 28115-
W Report Required Confirmation No.: 030313
Note:
Contact Time: 3:30 AM
Fax: [phone]
July 17, 2013 EM130212S3

Incident Report (Cont.) Project No.: EM130212S3
Client File No.:30-5693
H. Disposal Facilities:
Waste Facility: JBR Environmental Services
Contact Person:
Address: 210 Alice Street
City: Spartanburg State: SC Zip: 29303
Phone: [phone] Ext: Fax:
E-mail: Website:
Disposal Date: 3/3/2013 Amount: 4.17 tons Disposal Documents
Waste Facility: Palmetto Landfill
Contact Person:
Address: 251 New Hope Road
City: Wellford State: SC Zip: 29385-
Phone: [phone] Ext: Fax:
E-mail: Website:
Disposal Date: 3/4/2013 Amount: 11'.81 tons
Disposal Documents
Attached
Waste Facility: Palmetto Landfill
Contact Person:
Address: 251 New Hope Road
City: Wellford State: SC Zip: 29385-
Phone: [phone] Ext: Fax:
E-mail: Website:
Disposal Date: 3/7/2013 Amount: 13.70 tons 0 Disposal Documents
July 17, 2013 EM130212S3

Incident Report (Cont.) Project No.: EM13021253
I. Contractors:
Company: JBR Environmental Services
Contact Person : Rex Russell
Address: 210 Alice Stree, P.O. Box 4098 (29305)
City: Spartanburg State: SC Zip: 29303-
E-mail•
Client File No.:30-5693
Phone: [phone]
Fax: [phone]
July 17, 2013 EM13021253

EMROSOUTH
Environmental Consultants
May 28, 2013
JBR Environmental Services
P.O. Box 4098
Spartanburg, SC 29305
Attention: Mr. Steve Rivers
Re: Confirmation Soil Samples
CURA — S-03045010 — DNR
Diesel Fuel Spill Site
1-85 Northbound (Mile Marker 3) Rest Stop
Cleveland County, North Carolina
EnviroSouth Job No. 1697
Dear Mr. Rivers:
EnviroSouth, Inc. is pleased to provide you with this report concerning soil samples collected at the
referenced location. It is our understanding that a diesel fuel spill occurred on March 3, 2013. Diesel -
impacted soils were excavated and removed for disposal immediately following the spill.
At the request of your firm, EnviroSouth personnel mobilized to the site on March 29, 2013 to collect native
soil samples from the upper 6-inches of soil directly below the zone of excavation. The soil samples were
collected with decontaminated sampling tools and placed into laboratory -prepared bottles, then transferred to
an iced cooler for submittal to a North Carolina certified laboratory. Analyses were performed for Gasoline
Range Organics (GRO) per EPA Method SW5035 and for diesel -range organics (DRO) per EPA Method
SW3550C. Among the four (4) samples (S-1, S-2, S-3, and S-4), S-2 and S-3 exceeded the NCDENR clean-
up limit of 10 mg/kg for DRO. No other GRO or DRO analyses reported values exceeding 10 mg/kg.
In response to the elevated concentrations of DRO in the soils at locations S-2 and S-3, JBR and EnviroSouth
personnel re -mobilized to the spill site on May 13, 2013. JBR personnel excavated additional shallow soils in
the general vicinities of samples S-2 and S-3. Following excavation, EnviroSouth personnel collected soil
samples from the upper 6-inches of native soil in those two (2) areas. Laboratory results from the May 13 re -
sampling (samples S-26 and S-313) indicated that no GRO or DRO concentrations were detected at
concentrations exceeding 10 mg/kg.
Based on the laboratory results, it appears that the clean-up standards set forth by NCDENR have been
satisfied and no additional excavation or sampling is necessary.
We have attached copies of the laboratory reports and a site aerial photo showing the soil sample locations.
We appreciate the opportunity to provide you with this report. If you have any questions, please call.
attachments
Sincerely,
EnviroSouth, Inc.
/ 4Li30&U 57, )&m
Thomas F. Donn, P.G.
President
N.C. License No. 1762
phone: [phone] fax: [phone]
3440 Augusta Road 9 Greenville, SC 29605 • www.envirosouth.com

s r `g as
�4
w�
5-4
S-3, S-36
S-2, S-26 1 ,
1
S-1
EXPLANATION
® = SOIL SAMPLE LOCATION

ANALYnCAL FIVVIRONMENTAL SERVICES, INC.
AES
April 17, 2013
Kevin Herrina
Pace Analytical Services, Inc.
9800 Kincev Avenue. Suite 100
Huntersville NC 28078
TEL: [phone]
FAX: [phone]
RE: 92153376
Dear Kevin Herring: I Order No: 1304553
Analytical Environmental Services, Inc. received 4 samples on Ami15. 2013 12:25 am
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative.
AES' certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/12-06/30/13.
-AIHA Certification ID #100671 for Industrial Hygiene samples (Organics, Inorganics),
Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
effective until 09/01/13.
These results relate only to the items tested. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
I'M 4
Larissa Elslev
Project Manager
Revision 4/17/2013
3755 PRPSID[NTIAI. PIRKIVAY - ATIANTA, GF.ORGIA 30340 • Ti--i.: [phone] • FAX: [phone]
Page 1 of 10

N
O
O
Chain ®f Custody
Workorder. 92153376 Workorder Name: DRO/GRO
Results Requested 41tf2M
13 o y�y,
ceiyti+eai®
wAw4wcvIabs.mn
L4 ).9
�-NA! 11 -
Kevin Herring
Pace Analytical Charlotte P.O S ti
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone[phone]
Email: [e-mail]
F1
LAB USE ONLY
-
=Y
"
♦ -
ZD
5
1
S-1
3/29/201311:00
92153376001
Solid
2
S-2
31291201311:30
92153376002
Solid
✓
�/
3
S-3
31291201312:00
92153376003
Solid
4
S-4
3/29/201312:30
92153376004
Solid
5
.. J ;
�.-..,
-;, . �:...<
�s,.'.:t���`��'�.�--=:s"��
r"E�- �,:=.- -t`� z.-:.F>`n.ill
v:.c- A �'.`.`i��
s.�-:�` .--
;1��'?,_�.s
., _a.,,
..�= _ �"
i_ ,,w•,�..r�:
-�.-�±
___
.,�t,�. �,.:zr�""�
'_:�.-.d.�,z -�.:� Tn�,-.ea-�✓
[d. .;,a.•-cxata€n��
,'�
_
r
�y��""�,y
.��-,..t3�-..
a
�gp�G..�'�%`�P•'.
i?�'m.
�''_.
�
- -�
n. wt
.�,-.ate..
$�'�s�r
-
- �•' r �.�.,_
„T. `� �.��`,�--'
Transfers
Released By
Daterrime
Received By
Daterrime
_
/2i2♦
1
2
3
Cooler Tem erature on Receipt °C
CustodySeal Y or N
Received on Ice Y or N
samples Intact Y or N
Wednesday, April 03, 2013 5:30:44 PM FMT-ALL-C-002rev.00 24March2009 Page 1 of 1

Analytical Environmental Services, Inc
Date: 17-Apr-13
Client: Pace Analytical Services, Inc.
Project: 92153376 Case Narrative
Lab ID: 1304553
DRO Analysis by Method 8015C:
Due to sample matrix, sample 1304553-002 required dilution during preparation resulting in elevated reporting limits.
Page 3 of 10

Analytical Environmental Services, Inc
Date: 17-Apr-13
Client:
Pace Analytical Services, Inc.
Client Sample ID:
S-1
Project Name:
92153376
Collection Date:
3/29/2013 11:00:00 AM
Lab ID:
1304553-001
Matrix:
Solid
Analyses Result Qual MDL Reporting Limit Units BatchID DF Date Analyzed Analyst
GASOLINE RANGE ORGANICS SW8015C
TPH (Gasoline Range Organics)
BRL
Surr: a.a.a-trifluorotoluene
94.9
DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)
10
Surr: Dioctylphthalate
79.8
PERCENT MOISTURE D2216
Percent Moisture
20.3
Qualifiers: "
Value exceeds maximum contaminant level
BRL
Not detected at MML
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW5035)
0.18
0.52
mg/Kg-dry 174532 1
04/05/201315:52
JE
0
52.7-141
%REC 174532 1
04/05/201315:52
JE
(SW3550C)
1.9
8.4
mg/Kg-dry 174489 1
04/07/2013 05:57
SH
0
46-123
OAREC 174489 1
04/07/2013 05:57
SH
0 0 wt% R241699 1 04/08/201313:00 AS
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case nanative
Page 4 of 10

Analytical Environmental Services, Inc Date: 17-Apr-13
Client:
Pace Analytical Services, Inc.
Client Sample ID:
S-2
Project Name:
92153376
Collection Date:
3/29/2013 11:30:00 AM
Lab ID:
1304553-002
Matrix:
Solid
Analyses
Result
Qual MDL
Reporting
Units BatchID
DF Date Analyzed Analyst
Limit
GASOLINE RANGE ORGANICS
SW8015C
(SW5035)
TPH (Gasoline Range Organics)
BRL
0.17
0.49
mg/Kg-d'y 174532
1 04/05/2013 15:24
JE
Sun: a.a.a-trifluorotoluene
62.6
0
52.7-141
%REC 174532
1 04/05/2013 15:24
JE
DIESEL RANGE ORGANICS SW8015C
(SW3550C)
TPH (Diesel Range Organics)
54
J 20
86
mg/Kg-dry 174489
1 04/07/2013 06:21
SH
Surr: Dioctylphthalate
278
S 0
46-123
%REC 174489
1 04/07/2013 06:21
SH
PERCENT MOISTURE D2216
Percent Moisture
7.07
0
0
wt% R241699
1 04/08/2013 13:00
AS
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 5 of 10

Analytical Environmental Services, Inc
Date: 17-Apr-13
Client:
Pace Analytical Services, Inc.
Client Sample ID:
S-3
Project Name:
92153376
Collection Date:
3/29/2013 12:00:00 PM
Lab ID:
1304553-003
Matrix:
Solid
Analyses Result Reporting
y Qual MDL Units BatchID DF Date Analyzed Analyst
Limit
GASOLINE RANGE ORGANICS SW8015C
TPH (Gasoline Range Organics) BRL
Surr: a.a.a-trifluorotoluene 84.7
DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics) 13
Surr: Dioctylphthalate 82.1
PERCENT MOISTURE D2216
Percent Moisture 28.5
Qualifiers: •
Value exceeds maximum contaminant level
BRL
Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
(SW5035)
0.22
0.62
mg/Kg-dry 174532 1
04/05/201316:21
JE
0
52.7-141
%REC 174532 1
04/05/201316:21
JE
(SW3550C)
2.2
9.3
mg/Kg-dry 174489 1
04/07/2013 06:44
SH
0
46-123
°/oREC 174489 1
04/07/2013 06:44
SH
0 0 wt% R241699 1 04/08/201313:00 AS
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Narr See case narrative
Page 6 of 10

Analytical Environmental Services, Inc
Date: 17-Apr-13
Client:
Pace Analytical Services, Inc.
Client Sample ID:
S-4
Project Name:
92153376
Collection Date:
3/29/2013 12:30:00 PM
Lab ID:
1304553-004
Matrix:
Solid
Analyses Result Reporting
Y Qual MDL Units BatchID DF Date Analyzed Analyst
Limit
GASOLINE RANGE ORGANICS SW8015C
TPH (Gasoline Range Organics)
BRL
Surr: a.a.a-trifluorotoluene
97.3
DIESEL RANGE ORGANICS SW8015C
TPH (Diesel Range Organics)
6.5
Surr: Dioctylphthalate
86.5
PERCENT MOISTURE D2216
Percent Moisture
13.4
Qualifiers: "
Value exceeds maximum contaminant level
BRL Not detected at MDL
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
NC
Not confirmed
0.18
0
J 1.8
0
0
(SW5035)
0.52
mg/Kg-dry 174532
1 04/05/201316:49
JE
52.7-141
%REC 174532
1 04/05/2013
16:49
JE
(SW3550C)
7.7
mg/Kg-dry 174489
1 04/07/2013
00:30
SH
46-123
%REC 174489
1 04/07/2013
00:30
SH
0 wt% R241699 1 04/08/201313:00 AS
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
J Estimated value detected below Reporting Limit
> Greater than Result value
< Less than Result value
Nair See case narrative
Page 7 of 10

Analytical Environmental Services, Inc.
Sample/Cooler Receipt Checklist
Client Work Order Number
Checklist completed by
Signature Date
Carrier name: FedEx vUPS Courier Client US Mail Other
Shipping container/cooler in good condition? Yes No
Custody seals intact on shipping container/cooler? Yes No _
Custody seals intact on sample bottles? Yes _ No
Container/Temp Blank temperature in compliance? (4°Cf2)* Yes No _
3 �
Not Present
Not Present _
Not Present _
Cooler #1 1Cooler #2 Cooler #3 Cooler #4 Cooler#5
Chain of custody present?
Yes _-�
No _
Chain of custody signed when relinquished and received?
Yes /
No _
Chain of custody agrees with sample labels?
Yes
No _
Samples in proper container/bottle?
Yes
No _
Sample containers intact?
Yes _�
No _
Sufficient sample volume for indicated test?
Yes =
No
All samples received within holding time?
Yes _'�
No
Was TAT marked on the COC?
Yes _
No _
Proceed with Standard TAT as per project history?
Yes _
No _
Water - VOA vials have zero headspace? No VOA vials
submitted _ V
Yes _
Water - pH acceptable upon receipt?
Yes _
No _
Cooler #6
Not Applicable
No _
Not Applicable _
Adjusted? Checked by
Sample Condition: Good /'Other(Explain)
(For diffusive samples or AIHA lead) Is a known blank included? Yes — No
See Case Narrative for resolution of the Non -Conformance.
" Samples do not have to comply with the given range for certain parameters.
\L\Quality Assurance\Checklists Procedures Sign -Off Templates\Checklists\Sample Receipt Checklists\Sample_Cooler Receipt_Checklist
Page 8 of 10

Analytical Environmental Services, Inc
Date: 17-Apr-13
Client: Pace Analytical Services, Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: 92153376
Workorder: 1304553 BatchID: 174489
Sample ID: MB-174489
Client ID:
Units: mg/Kg
Prep Date: 04/05/2013
Run No: 241610
SampleType: MBLK
TestCode: DIESEL RANGE ORGANICS SW8015C
BatchID: 174489
Analysis Date: 04/06/2013
Seq No: 5058745
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Diesel Range Organics) 1.724 6.7 0 0 0 0 0 0 0 0 J
Surr: Dioctylphthalate 2.869 0 3.3 0 86.9 46 123 0 0 0
Sample ID: LCS-174489
Client ID:
Units: mg/Kg
Prep Date: 04/05/2013
Run No: 241610
SampleType: LCS
TestCode: DIESEL RANGE ORGANICS SW8015C
BatchID: 174489
Analysis Date: 04/07/2013
Seq No: 5058751
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Diesel Range Organics) 27.35 6.7 33.3 1.724 76.9 47.9 116 0 0 0
Surr: Dioctylphthalate 2.677 0 3.33 0 80.4 46 123 0 0 0
Sample ID: 1304553-004BMS
Client ID: S-4
Units: mg/Kg-dry Prep Date: 04/05/2013
Run No: 241610
SampleType: MS
TestCode: DIESEL RANGE ORGANICS SW8015C
BatchID: 174489 Analysis Date: 04/07/2013
Seq No: 5058756
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Diesel Range Organics) 37.04 7.7 38.45 6.506 79.4 36.8 120 0 0 0
Surr: Dioctylphthalate 3.154 0 3.845 0 82 46 123 0 0 0
Sample ID: 1304553-004BMSD
Client ID: S-4
Units: mg/Kg-dry Prep Date: 04/05/2013
Run No: 241610
SampleType: MSD
TestCode: DIESEL RANGE ORGANICS SW8015C
BatchID: 174489 Analysis Date: 04/07/2013
Seq No: 5058760
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Diesel Range Organics) 92.64
Surr: Dioctylphthalate 3.116
Qualifiers: > Greater than Result value
BRL Below reporting limit
I Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
7.7 38.33 6.506 225 36.8
0 3.833 0 81.3 46
< Less than Result value
B Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
120 37.04 85.7 30.2 SF
123 3.154 0 0
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 9 of 10

Analytical Environmental Services, Inc Date: 17-Apr-13
Client: Pace Analytical Services, Inc. ANALYTICAL, QC SUMMARY REPORT
Project Name: 92153376
Workorder: 1304553 BatchID: 174532
Sample ID: MB-174532
Client ID:
Units: mg/Kg
Prep Date: 04/05/2013
Run No: 241621
SampleType: MBLK
TestCode: GASOLINE RANGE ORGANICS Sw8015C
BatchID: 174532
Analysis Date: 04/05/2013
Seq No: 5058653
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Gasoline Range Organics) BRL 0.50 0 0 0 0 0 0 0 0.
Surr: a.a.a-trifluorotoluene 0.05154 0 0.05 0 103 52.7 141 0 0 0
Sample ID: LCS-174532
Client ID:
Units: mg/Kg
Prep Date: 04/05/2013
Run No: 241621
SampleType: LCS
TestCode: GASOLINE RANGE ORGANICS Sw8015C
BatchID: 174532
Analysis Date: 04/05/2013
Seq No: 5058694
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Gasoline Range Organics) 0.9006 0.50 1 0 90.1 60.3 135 0 0 0
Surr: a.a.a-trifluorotoluene 0.05579 0 0.05 0 112 52.7 141 0 0 0
Sample ID: 1304553-002AMS
Client ID: S-2
Units: mg/Kg-dry Prep Date: 04/05/2013
Run No: 241621
SampleType: MS
TestCode: GASOLINE RANGE ORGANICS Sw8015C
BatchID: 174532 Analysis Date: 04/05/2013
Seq No: 5058697
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Gasoline Range Organics) 0.8337 0.54 1.076 0 77.5 50.1 134 0 0 0
Surr: a.a.a-trifluorotoluene 0.05748 0 0.0538 0 107 52.7 141 0 0 0
Sample ID: 1304553-002AMSD
Client ID: S-2
Units: mg/Kg-dry Prep Date: 04/05/2013
Run No: 241621
SampleType: MSD
TestCode: GASOLINE RANGE ORGANICS sw8015c
BatchID: 174532 Analysis Date: 04/05/2013
Seq No: 5058701
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
TPH (Gasoline Range Organics) 0.8250
Surr: a.a.a-trifluorotoluene 0.05719
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
0.54 1.076 0 76.7 50.1
0 0.0538 0 106 52.7
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
134 0.8337 1.06 20
141 0.05748 0 0
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 10 of 10

aceAnaljftal
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
May 21, 2013
Tom Donn
EnviroSouth, Inc.
3440 Augusta Rd.
Greenville, SC 29605
RE: Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Dear Tom Donn:
[phone]
[phone]
Enclosed are the analytical, results for sample(s) received by the laboratory on May 15, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated o_ n the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
cc: Ms. Diane Farrugia, EnviroSouth, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
CERTIFICATIONS
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�ac`eAnalytcal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
SAMPLE ANALYTE COUNT
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92158207001 S-2B EPA 8015 Modified
RES
2
PASI-C
EPA 8015 Modified
RGF
2
PASI-C
ASTM D2974-87
TNM
1
PASI-C
92158207002 S-3B EPA 8015 Modified
RES
2
PASI-C
EPA 8015 Modified
RGF
2
PASI-C
ASTM D2974-87
TNM
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 12

aceAnalyiical
www.paMobs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunters,die, NC 28078
[phone]
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Sample: S-213
Lab ID: 92158207001 Collected: 05/1.3/13 09:30
Received: 05/15/13 13:40 Matrix: Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit DF
Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
ND mg/kg 6.0 1
05/16/13 14:00
05/17/13 20:40 68334-30-5
Surrogates
n-Pentacosane (S)
78 % 41-119 1
05/16/13 14:00
05/17/13 20:40 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics
ND mg/kg 7.2 1
05/17/13 17:11
05/18/13 20:47 8006-61-9
Surrogates
4-Bromofluorobenzene (S)
93 % 70-167 1
05/17/13 17:11
05/18/13 20:47 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
17.0 % 0.10 1
05/16/13 14:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2013 07:49 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
ANALYTICAL RESULTS
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Sample: S-3B
Lab ID: 92158207002 Collected: 05/13/13 10:30
Received: 05/15/13 13:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
ND mg/kg 5.6 1
05/16/13 14:00 05/17/13 23:47 68334-30-5
Surrogates
n-Pentacosane (S)
86 % 41-119 1
05/16/13 14:00 05/17/13 23:47 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030B
Gasoline Range Organics
ND mg/kg 6.7 1
05/17/1317:11 05/18/13 21:10 8006-61-9
Surrogates
4-Bromofluorobenzene (S)
90 % 70-167 1
05/17/13 17:11 05/18/13 21:10 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
11.1 % 0.10 1
05/16/13 14:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2013 07:49 AM without the written consent of Pace Analytical Services, Inc..
Page 5 of 12

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
QC Batch: GCV/6898
QC Batch Method: EPA 5035AI5030B
Associated Lab Samples: 92158207001, 921582070.02
METHOD BLANK: 977349
Associated Lab Samples: 92158207001, 92158207002
Parameter Units
Gasoline Range Organics mg/kg
4-Bromofluorobenzene (S) %
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8015 Modified
Analysis Description: Gasoline Range Organics
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 6.0 05/18/1311:57
94 70-167 05/18/1311:57
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 977350
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Gasoline Range Organics mg/kg . 25 27.6 111 70-165
4-Bromofluorobenzene (S) % 96 70-167
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 977351 977352
MS MSD
92157983001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Gasoline Range Organics mg/kg ND 36 36 38.6 39.1 107 108 47-187 1
4-Bromofluorobenzene (S) % 97 91 70-167
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2013 07:49 AM without the written consent of Pace Analytical Services, Inc..
Page 6 of 12

(�55'neAnalytcal
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXT/22129 Analysis Method: EPA 8015 Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92158207001, 92158207002
METHOD BLANK: 975985
Associated Lab Samples: 92158207001, 92158207002
Parameter Units
Diesel Components mg/kg
n-Pentacosane (S) %
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 05/17/1311:39
81 41-119 05/17/1311:39
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 975986
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Diesel Components mg/kg 66.7 55.8 84 49-113
n-Pentacosane (S) % 85 41-119
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 975987
975988
MS
MSD
92158115002
Spike
Spike
MS MSD MS
MSD % Rec
Parameter Units Result
Conc.
Conc.
Result Result % Rec
% Rec Limits RPD Qua]
Diesel Components mg/kg ND
88.8
88.8
74.2 77.2 82
85 10-146 4
n-Pentacosane(S) %
82
93 41-119
Date: 05/21/2013 07:49 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�aneMalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
QC Batch: PMST/5532 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92158207001, 92158207002
SAMPLE DUPLICATE: 975555
92158207001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 17.0 17.2 1
SAMPLE DUPLICATE: 975556
92158074002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 96.2 96.2 0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21 /2013 07:49 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALIFIERS
Project: NC 1-85 Spill Site (mm3)
Pace Project No.: 92158207
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2013 07:49 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12

aceAnalytical
www.pBcelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
NC 1-85 Spill Site (mm3)
92158207
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92168207001
S-213
EPA 3546
OEXT/22129
EPA 8015 Modified
GCSV/14628
92158207002
S-313
EPA 3546
OEXT122129
EPA 8015 Modified
GCSV/14628
92158207001
S-2B
EPA 5035A/5030B
GCV/6898
EPA 8015 Modified
GCV/6899
92158207002
S-313
EPA 5035AI5030B
GCV/6898
EPA 8015 Modified
GCV/6899
92168207001
S-213
ASTM D2974-87
PMST/5532
92158207002
S-313
ASTM D2974-87
PMST/5532
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/21/2013 07:49 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12

Sample Condition Upon Receipt (SCUR Pa e 1 01 z
aceAnaoical' Document Number: Issuing Authority:
I F-CHR-CS-03-rev.10 Pace Huntersville Quality Office
Client Name:
7
Where Received:
Iuntersvill.e ❑ Asheville ❑ Eden ❑ Raleigh
Courier: ❑Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Pac Other f� `iolali:s��'��:'�?
�ilK � N.��G'Ck�i
Custody Seal on Cooler/Box Present: ❑ yes �no Seals intact: ❑ yes ❑ noeY�
Packing Material: ❑ Bubble Wrap ❑ Btfbble gs ❑ None ❑ Other
Thermometer Used: IR Gun T1101 10 Type of IcjW�Wet Blue None [�-3�amples on Ice, cooling process has begun
e__a_. T44A4• Pain (:mmnefinn T2Nn Cnrrection
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes No NIA
Date and Initials of persogexamining
contents: r ryri
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present: Yes '❑No
❑NIA
I.
Chain of Custody Filled Out:
es ❑No
❑N/A
2.
Chain of Custody Relinquished,
Yes ON.
❑NIA
3.
Sampler Name & Signature on COC:
es ❑No
❑NIA
4.
Samples Arrived within Hold Time:
Yes ❑No
❑N/A
5.
Short Hold Time Analysis <72hr):
❑Yes ❑
❑NIA
6.
Rush -Turn -Around Time Requested:-
Sufficient Volume:
es ❑No
o
❑N/A 17.
NiA
8.
V
Correct Containers Used:
'E�Y—es []No
❑N/A
9.
-Pace Containers Used:
Yes ❑No
❑N/A
Containers Intact:
es UNo
❑N/A
10.
Filtered volume received for Dissolved tests
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
❑Yes 2No
es o
❑ IA
1.
1 L J� —3 ,
13. ,
All containers needing preservation have been checked. DYes ❑No .J:Iw
All containers needing preservation are found to be in
compliance with EPA recommendation.
❑Yes ❑No }WK
/
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) .
❑Yes o
Samples checked for dechlorination:
❑Yes ❑No
WA—
14.
.15.
Heads ace in VOA Vials >6mm :
[]Yes ❑No
/A
Trip Blank Present:
❑Yes []No
❑�NIIAA
16.
Trip Blank Custody Seals Present
❑Yes ❑No
E A
Pare Trin Blank Lot # (if Durchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date: 1 5MI15
SRF Review: Date: S 119
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp,
incorrect containers)
Page 11 of 12

CHAIN -OF -CUSTODY / Analytical Request Document
eAnalytical o The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. N
0
www.pacelahs.cum
Page: of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company: ` .I— Report To: �'t� Aftenfion:
�r1V j to 4' y-<-.
1665543
Address:
Copy To:
Company Name:
REGULATORY AGENCY
Address:
F NPDES !— GROUND WATER I~ DRINKING WATER
F UST ' RCRA r OTHER
Email To:
��
Purchase Order No.:
Pace Quote
Reference:
Phone: Fax:
Project Name: p� /' q' !
1 �I l� P�� ,i I
Pace Project
Manager:
Site Location
A —
STATE;
Requested Due DaterrAT: 1
d .
Project Number.
Pace Profile #:
Requested
Analysis
Filtered
(Y/N)
-
Section D Matrix Codes
RequiredClientlnfornation MATRIX I CODE
—
COLLECTED
Preservatives
a
z
r
Drinking Water DW
�^
o
z
0T
Water W
Waste Water WW
S
U
COMPOSITE
COMP¢SLE
W
_
Z
Product P
m
START
END
®
SoiltSolid SL
y
o
rn
�
®
SAMPLE ID oil OL
"
¢
w
c
Wipe
(A-Z. 0-9 / r) Air AR
CI
aW
a
aai
0)
N
Y�
U
��� •�
Sample IDS MUST BE UNIQUE Tissue TS
O
L)
.
w
,
I
_
L 1
Other OT
Ja
~
a
O
w
U
O
?.
tO
O
dO
U
O@
w
1=
¢
<
rn
DATE
TIME
DATE
TIME
¢
3
_
Z
_
=
Z
II
Z
E
'
O
Q
y
Pace Pro ect No./ Lab I.D.
j
- t3
SL
G
s i3
930
S
2
S- 3 3 -
s4
' l3
!3
jo3o
-5
5c
X
x
3
4
6
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINQUISHED BY /' LIATION
DATE
TIME
ACCEPTED BY / AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
8i1 —,
[ W
fS1.
L
`-✓
SAMPLER NAME AND. SIGNATURE
o
m
ORIGINAL
v
E
m i
T
o U Z
C
to Z
PRINT Name of SAMPLER:
��r ar s
tT
m `—'
tr
O)
E V
SIGNATURE of SAMPLER: T/
_DATE Signed S
"
�.,
(MMIDDNY): ��
to _By signing this form you are accepting Paces NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days.
F-ALL-Q-020rev.07, 15-May-2007

"MATERIAL JBR Environmental Services
Manifest Document No. ,
MANIFEST P. O. Box 4098�
Page of ;
Spartanburg, SC-29305
Job No
Emergency Phone Number: 864 583-271 T
,!GENERATOR_ INFQRMATION
Name: P /" / %� .-�-
US EPA ID No.
xj
Street Address
Mailing Address
Phone No.
J1Wj,) "Sic• r�s 7
Contact
DESCRIPTION
OF MATERIALS
HM
USDOT Proper Shipping Name '
Hazard
UNM
Packing
Containers '
Total
Unit
(Complete All Items for Hazardous Materials)'
Class ,-
'A
Group
Quantity
Wt.Nol.
Qty
Type
-... ,"
ID.No.
.
l?[ t'r
b.
C.
c
'i
ADDITIONAL INFORMATION
ERG No.
JBR-Profile Code
Facility -Use
a.
r
jat<�G; ,� ;�':t.�:.i• l 'l' r t'i%ram � 1'..�:c.>C
-.
•��tlt� !�
h[:�,G't ,. = ,
b.
_ _C'
C.-
GENERATORS
CERTIFICATION
This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for ' -
transportation according to the applicable regulations of the Department of Transportation.' 1 further certify that -none of the materials described,above are a
hazardous waste as defined by EPA 40 CPR Part 261 or any applicable'state law, and unless specifically identified above, the materials contain less tha_n+
1,000 ppm total halogens and do not contain quantifiable levels (2 m) of PCBs as defined by EPA 40 CFR. Parts 279 and 761.
Printedrryped Name
Signature. ;%f
+ ,.
Mo.fDay/Yr.,
6'"/ V�i C�i/�}� i;�.n .t1�
{.rY �'; 6/!s�""�'•'U" L, _
i„sfPP w% ` .✓J '_
je- t' TRANSPORTER INFORMATION'
Transporter ces1
JBR Environmental Servi_
hereby acknowledge receipt of the above -described materials for transport from the generator .
site listed above.-
r _
=' "�-
_
Address 210 Alice Street
Spartanburg, SC 29303"
signature-," _`j Shipment Date.-
Transporter or
Unit No.-
1 hereby aVKn—owledgeetha�t,t4q above -described rnarerials were Mceived from.the generatorsite
EPA ID No.. SC R000004358
�..
and were. transported to the facility listed below.
f
,%�/ . <'` _./ ✓ " %
Signature ..- ,.. Delivery Date
Phone -864-583-271.7 - -
FACILITY INFQRMATION'
Facility
1 herebyacknowledge receipt of the materials covered by this manifest except for any ,
JBR, Environmental Services
discrepancy noted below..
Address 210 Alice Street
Spartanburg, SG' 29303
Signature '°""" Receipt Date
>< .
Facility Or
"' 'DlscPepancies Routing Codes -Handling Methods:
EPA ID No. SCR000004358
a
Phone [phone]
b
Contact Rex Russell
"
Original - Facility Retain COPY 2 - Return to Generator
COPY,3 -Transporter Retain
COPY 4 - Generator Retain

� PAL1�/1�7T0. LAI\I®FLLDo ` - .
A WASTE MANAGEiV1ERIT CC�IVIPANY.
,(
Gate. Ticket No.
NON -HAZARDOUS WASTE MANIFEST
S.
Generator JBk Environmental 1Vlailing Address
Sliipping Location (Return ,completed manifest %to;)
Street:210 Alice Street Street or P O. Box. 4048
S rr
City: Spartanburg State:. SC City: .Spartanburg
County: Spartanburg State: SCE"" Zip Code: 29305
Phone: ( 864 583-2717 Phone: 864 ) 583-2717
Description of Profile . Total Unit of Coniianer .
_. uVaste,:MateriAls _. _ -_ t vNumber Quantity Measure Type
? - -
Non Reg4ilated Solid; nos CF321.9
TPH Contaminated S ' CQ6803 }} } {
Construction Debris CQ8252
I hereby,;certify that the above-describ.ed materials are not hazardous wastes as delinediy 40 CFY2, )'art
261 or any applicable` tate law, have been fully. and accurately described, ciassified and packaged, and .
are n r per condition'for transportation according to app icable deg lations..:
Genera o Authorized Agent Name (Print) Signat' Delivery Date
• •P
,iu„ transporter Name JBR Driver Name'(Print)
Address 210 Alice Street Truck Number 9/
P
'S 'artanbur SC 29303..
g T hereby ack`riowledge receiptof the airove described..
I.hereby acknowledge receibCof the above
materials:
described'makerials .for transport from the ite, and Wei, received frgm the generator s
ere
generator site listed above: transported without incident, to the
vie destination as started on th10
is'"form k
' briv Signature Shipment, ate DriveeOIgnature: Deli 'Miry D to
V,
Site Name: Palmetto
Landfill &Recycling Center Phone Number:~($64) 439-8426 • Fax: 439=0047•
Address: 251 New Hope Road, Wellford, South Carolina 29385
": Ds oral Location ' North West Level. t i
P �' s
Ihoc
ereby acknowledge receipt.of the aboye,described materials..
i
Name of Authorized Agent.(Print) Signature Receipt Date,
NOTE: MANIFEST MUST -BE FILLED OUT COMPLETELY BEFORE DISPOSAL
PAL101 WHITE -ORIGINAL • YELLOW -TRANSPORTER RETAIN• PINK - LANDFILL RETAIN GOLD - GENERATOR RETAIN - -

'4Q did" 7b �9fA/ 3 Tm r
+ • Fa E
d tdL �gfys, MIN
#, it r► l
''�`
EMERGENCY SERVICES

1-7
�• $ � � . . ,
a' - 7 phi >.e,�`
w. Q
t rk
yam; •� -'y ` _ � , n} t� � <<�� � ' , i ;'
it �• :.��� .r.. [� "} y�' -:�. },•.t "' J
EMERGENCY SERVICES

EMERGENCY SERVICES

North Carolina Emergency Management - EM43 Reporting
North Carolina Emergency Management - EM43 Reporting
EM Level:
NCEM Edited:
Include in Report:
4
Yes
Yes
Taken by:
Date/Time Reported:
Date/Time Occurred:
R Brown
05/21/2013 10:44:25
05/21/2013 10:44:25
Reported by:
Agency:
Phone:
Jill Klocek
84 Components
412-758-2952
County:
City:
Area:
Cleveland
Kings Mountain
13
Street Address:
Zip Code:
420 Dixon Dairy Rd
EVENT TYPE
Type: HazMat
Animal Disease Event Type: Bomb Threat Event Type:
Complaint Event Type:
Fire Event Type:
FNF Event Type:
FNF Class:
HazMat Event Type:
HazMat Class:
HazMat Mode:
Diesel Fuel
Petroleum
Fixed Facility
Homeland Security Event:
Non-FNF Event:
Non-FNF Event Type:
Other Event Type:
SAR Type:
Transportation Event Type:
Wastewater Event Type:
Weather Event Type:
Weather Event Name:
WMD Event Type:
State Resource Request
Pagel of 3
Event Description:
A truss manufacturing plant reported the release of 100-150 gallons of diesel fuel to the ground due
to operator error during forklift refueling operations. An unknown amount of the product entered a
storm drain. Hepaco conducted cleanup operations and it was believed that all of the product was
removed from the storm drain. No state resources were requested.
Attachment
Filename: NRC.docx
Deaths: Injuries: Evacuation: Radius:
0 0 0 0
Responsible Party: Responsible Party Phone:
Point of Contact:
Latitude:
00.000000
Point of Contact Phone:
Longitude:
-00.000000
https://www.ncsparta.net/eoc7/boards/board.aspx?tableid=275&viewid=l 011 &uvid=1.408... 5/22/2013

North Carolina Emergency Management - EM43 Reporting
Page
of 3
RRT Request: RRT Approved: RRT Team
Number:
RRT Mission
Number:
https://www.nesparta.netleoc7/boardslboard.aspx?tableid=275&viewid=1011 &uvid=l .408... 5/22/2013

North Carolina Emergency Management - EM43 Reporting
Page 3 of 3
NOTIFICATIONS
LEMC:
SO:
PD:
LFD:
CHealth:
Sewer:
PWRK:
Other Local Agencies:
AC:
SHP/SWP:
ENV MGMT:
WATER: DRP:
CAP:
DOT: Other State Agencies:
Notes:
Hepaco POC: Luke Gibson, 704-564-8849
Plant manager: Ed Shaner, 336-552-9411
1054 - J Ramsey, S Lewis emailed - rjb
1055 - J Ramsey read receipt rec'd - rjb
1104 - S Lewis read receipt rec'd - rjb
ATTACHMENTS
Filename:
Filename:
Filename:
Filename:
Filename:
Filename:
Filename:
Filename:
Filename:
https://www.ncsparta.net/eoc7/boards/board.aspx?tableid=275&viewid=1011 &uvid=1.408... 5/22/2013

PV
NATIONAL RESPONSE CENTER 1-800-424-8802
***GOVERNMENT USE ONLY* "GOVERN MENT USE ONLY***
Information released to a third party shall comply with any
applicable federal and/or state Freedom of Information and Privacy Laws
Incident Report # 1047831
INCIDENT DESCRIPTION
*Report taken by: MST3 RUDOLPH GANTHER at 11:15 on 21-MAY-13
Incident Type: MOBILE
Incident Cause: UNKNOWN
Affected Area: STORM DRAIN
Incident occurred on 20-MAY-13 at 20:00 local incident time.
Affected Medium: WATER STORM DRAIN
REPORTING PARTY
Name: JILL KLOCEK
Organization: 84 COMPONENTS
Address: 420 DIXON DAIRY RD
KINGS MOUNTAIN, NC
PRIMARY Phone: [phone]
Type of Organization: PRIVATE ENTERPRISE
SUSPECTED RESPONSIBLE PARTY
Name: JILL KLOCEK
Organization: 84 COMPONENTS
Address: 420 DIXON DAIRY RD
KINGS MOUNTAIN, NC
PRIMARY Phone: [phone]
INCIDENT LOCATION
420 DIXON DAIRY RD County: CLEVELAND
City: KINGS MOUNTAIN State: NC
RELEASED MATERIAL(S)
CHRIS Code: ODS Official Material Name: OIL: DIESEL
Also Known As:
Qty Released: 150 GALLON(S) Qty in Water: 0 UNKNOWN AMOUNT
DESCRIPTION OF INCIDENT
THERE WAS A SPILL OF 100-150 GALLONS OF DIESEL FUEL FROM A FORKLIFT
WHILE THE FORKLIFT WAS BEING FUELED.

Frr
SENSITIVE INFORMATION
ON SCENE POINT OF CONTACT: ED SHANER, PHONE [phone].
INCIDENT DETAILS
Road Mile Marker:
Length of Service Disruption:
Airbag Deployed: UNKNOWN
---WATER INFORMATION ---
Body of Water: STORM DRAIN
Tributary of:
Nearest River Mile Marker:
Water Supply Contaminated: UNKNOWN
---MOBILE INFORMATION ---
Vehicle Type: FORK LIFT
Vehicle Number: UNKNOWN
Trailer/Tanker Number:
Vehicle Fuel Capacity:
Cargo Capacity:
Cargo On Board:
Hazmat Carrier: UNKNOWN
Carrier Licensed: UNKNOWN
Suspected Non Compliance: UNKNOWN
IMPACT
Fire Involved: NO Fire Extinguished: UNKNOWN
INJURIES: NO Hospitalized: Empl/Crew: Passenger:
FATALITIES: NO Empl/Crew: Passenger: Occupant:
EVACUATIONS:NO Who Evacuated: Radius/Area:
Damages: NO
Hours Direction of
Closure Type Description of Closure Closed Closure
N
Air:
N Major
Road: Artery: N
N
Waterway:
N
Track:
Environmental Impact: UNKNOWN
Media Interest: NONE Community Impact due to Material:
REMEDIAL ACTIONS

CONTRACTOR HAS BEEN HIRED, CLEANUP UNDERWAY.
Release Secured: YES
Release Rate:
Estimated Release Duration:
WEATHER
ADDITIONAL AGENCIES NOTIFIED
Federal:
State/Local: NC DNR
State/Local On Scene:
State Agency Number:
NOTIFICATIONS BY NRC
DHS NOC (NOC)
21-MAY-13 11:25 (202)2828114
DHS I&A STATE AND LOCAL PRGM OFFICE (RALEIGH, NC FUSION CENTER)
21-MAY713 11:25 (202)5575179
DHS SOUTH CAROLINA FUSION CENTER (LE SENSITIVE ADVISORS & LIASON PROGRA
21-MAY-13 11:25 (866)4728477
DOT CRISIS MANAGEMENT CENTER (MAIN OFFICE)
21-MAY-13 11:25 (202)3661863
U.S. EPA IV (MAIN OFFICE)
(404)6504955
U.S. EPA IV (NC/SC INCIDENTS)
21-MAY-13 11:25 (404)6504955
NC DEPT OF EMERGENCY MGMT (MAIN OFFICE)
21-MAY-13 11:25 (800)8580368
NC OCCUPATIONAL ENVMTL EPIDEMIOLOGY (COMMAND CENTER)
21-MAY-13 11:25 (919)7075950
NC PUBLIC HEALTH PREPARE AND RESPNS (PHPR COMMAND CENTER)
21-MAY-13 11:25 (919)7150919
NATIONAL INFRASTRUCTURE COORD CTR (MAIN OFFICE)
21-MAY-13 11:25 (202)2829201
NOAA RPTS FOR NC (MAIN OFFICE)
21-MAY-13 11:25 (206)5264911
NATIONAL RESPONSE CENTER HQ (AUTOMATIC REPORTS)
21-MAY-13 11:25 (202)2671136
SC EMERGENCY MANAGEMENT DIVISION (MAIN OFFICE)
21-MAY-13 11:25 (803)7378500
SEAHAWK IOC (INTER -AGENCY OPERATIONS CENTER)
21-MAY-13 11:25 (803)2060971
STATE OF NORTH CAROLINA DENR (MAIN OFFICE)
21-MAY-13 11:25 (919)8076300
SC DEPT OF ENV CNTL ATTN: ERS (MAIN OFFICE)
21-MAY-13 11:25 (803)2536488 1

USCG DISTRICT 5 (D5 DRAT)
21-MAY-13 11:25 (757)3986231
ADDITIONAL INFORMATION
*** END INCIDENT REPORT#1047831 ***
Report any problems by calling 1-800-424-8802
PLEASE VISIT OUR WEB SITE AT http://www.nrc.uscg.mil E-mail correspondence sent to and from
this address may be subject to the provisions of G.S. 132-1, the North Carolina Public Records Law, and
may be subject to monitoring and disclosed to third parties, including law enforcement personnel, by an
authorized state official.

NATIONAL RESPONSE CENTER 1-800-424-8802
***GOVERNMENT USE ONLY***GOVERNMENT USE ONLY***
Information released to a third party shall comply with any
applicable federal and/or state Freedom of Information and Privacy Laws
Incident Report # 937151
INCIDENT DESCRIPTION
*Report taken by: CIV TIMOTHY SMITH at 14:35 on 15-APR-10
Incident Type: MOBILE
Incident Cause: TRANSPORT ACCIDENT
Affected Area: BEASON CREEK
Incident occurred on 15-APR-10 at 09:00 local incident time.
Affected Medium: WATER BEASON CREEK
REPORTING PARTY
Name: NATE WALDEN
Organization: ERTS
Address: 8401 CHARGIN RD
CHAGRIN FALLS, OH 44023
ERTS reported for the responsible party.
PRIMARY Phone: [phone]
Type of Organization: PRIVATE ENTERPRISE
SUSPECTED RESPONSIBLE PARTY
Name: US INTERMODAL CORP
Organization: US INTERMODAL CORP
Address: PO BOX 1202
SAVANNAH, GA
INCIDENT LOCATION
407 S. CANSLER ST. County: CLEVELAND
City: KINGS MOUNTAIN State: NC
PARKING LOT/ROADWAY
RELEASED MATERIALS)
CHRIS Code: ODS Official Material Name: OIL: DIESEL
Also Known As: DIESEL FUEL
Qty Released: 75 GALLON.(S) Qty in Water: 60 GALLON(S)
DESCRIPTION OF INCIDENT
TRACTOR TRAILER SUFFERED A PUNCTURED SADDLE TANK AFTER STRIKING A
CEMENT CURB. THE RELEASED FUEL TRAVELED APPROXIMATELY 15-20 FT.
INTO A NEARBY STORM DRAIN. AFTER ENTERING THE STORM DRAIN THE FUEL
TRAVELED AN ESTIMATED 100 YARDS INTO A NEARBY CREEK (BEASON CREEK).
THE LOCAL FIRE DEPARTMENT CONTAINED THE RELEASED FUEL. AN UNDERFLOW
DAM WAS CREATED 20 FT. FROM THE STORM DRAIN DISCHARGE LOCATION.

SENSITIVE INFORMATION
INCIDENT DETAILS
Road Mile Marker:
Length of Service Disruption:
Airbag Deployed:
---WATER INFORMATION ---
Body of Water: BEASON CREEK
Tributary of:
Nearest River Mile Marker:
Water Supply Contaminated: NO
---MOBILE INFORMATION ---
Vehicle Type: TRACTOR TRAILER
Vehicle Number: 103678-11
Trailer/Tanker Number:
Vehicle Fuel Capacity: 300 GALLON(S)
Cargo Capacity:
Cargo On Board:
Hazmat Carrier: UNKNOWN
Carrier Licensed: UNKNOWN
Suspected Non Compliance: UNKNOWN
IMPACT
Fire Involved: NO Fire Extinguished: UNKNOWN
INJURIES: NO Hospitalized: Empl/Crew: Passenger:
FATALITIES: NO Empl/Crew: Passenger: Occupant:
EVACUATIONS:NO Who Evacuated: Radius/Area:
Damages: NO
Closure Type Description of Closure
N
Air:
N
Road:
N
Waterway:
N
Track:
Hours Direction of
Closed Closure
Environmental Impact: UNKNOWN
Media Interest: NONE Community Impact due to Material:
Major
Artery:N
REMEDIAL ACTIONS
DISPATCHED ENVIRONMENTAL CLEANUP TO THE SITE FOR INITIAL RESPONSE
AND REMEDIATION ACTIVITIES. A VACUUM TRUCK WAS UTILIZED TO REMOVE
THE FUEL FROM THE WATER AND DRAIN LINES.
Release Secured: UNKNOWN
Release Rate:
Estimated Release Duration:

Weather: UNKNOWN, OF
WEATHER
ADDITIONAL AGENCIES NOTIFIED
Federal: N/A
State/Local: NCDNR
State/Local On Scene: N/A
State Agency Number: N/A
NOTIFICATIONS BY NRC
DHS NOC (NOC)
15-APR-10 14:54 (202)2828114
DHS I&A STATE AND LOCAL PRGM OFFICE (RALEIGH, NC FUSION CENTER)
15-APR-10 14:54 (202)5575179
DHS SOUTH CAROLINA FUSION CENTER (LE SENSITIVE ADVISORS & LIASON PROGRA
15-APR-10 14:54 (866)4728477
DOT CRISIS MANAGEMENT CENTER (MAIN OFFICE)
15-APR-10 14:54 (202)3661863
U.S. EPA IV (MAIN OFFICE)
(404)6504955
U.S. EPA IV (NC/SC INCIDENTS)
15-APR-10 14:54 (404)6504955
FEMA REGION 4 (WATCH UNIT)
15-APR-10 14:54 (770)2203158
USCG NATIONAL COMMAND CENTER (MAIN OFFICE)
(202)3722100
NC DEPT OF EMERGENCY MGMT (MAIN OFFICE)
15-APR-10 14:54 (800)8580368
NC OCCUPATIONAL ENVMTL EPIDEMIOLOGY (COMMAND CENTER)
15-APR-10 14:54 (919)7075950
NC PUBLIC HEALTH PREPARE AND RESPNS (PHPR COMMAND CENTER)
15-APR-10 14:54 (919)7150919
NATIONAL INFRASTRUCTURE COORD CTR (MAIN OFFICE)
15-APR-10 14:54 (202)2829201
NOAA RPTS FOR NC (MAIN OFFICE)
15-APR-10 14:54 (206)5264911
SC EMERGENCY MANAGEMENT DIVISION (MAIN OFFICE)
15-APR-10 14:54 (803)7378500
STATE OF NORTH CAROLINA DENR (MAIN OFFICE)
15-APR-10 14:54 (919)7335083
SC DEPT OF ENV CNTL ATTN: ERS (MAIN OFFICE)
15-APR-10 14:54 (803)2536488
TN BUREAU OF INVESTIGATION (TBI)
15-APR-10 14:54 (615)7444318
WEB REPORT (WEB REPORT SUBMITTER)
15-APR-10 14:54
ADDITIONAL INFORMATION
PLACED AN UNDERFLOW DAM APPROXIMATELY 20FT FROM THE DISCHARGE PIPE
PREVENTING ANY FURTHER MIGRATION OF FUEL DOWN STREAM
*** END INCIDENT REPORT #937151 ***

ENVIRONMENTAL
COMPLIANCE SERVICES
of North Carolina, P.C.
May 4, 2010
Ms. Marcia Allocco
NCDENR
Division of Water Quality
Mooresville Regional Office
610 East Center Street, Suite 301
Mooresville, NC 28115
Re: Kings Mountain Emergency Spill Response
407 South Cansler St.
Kings Mountain, NC
ECS Project No. 14-214102
Incident No. 04162010
Dear Ms. Allocco:
This report presents the results of the emergency spill response events documented by Environmental
Compliance Services of NC, PC (ECSNC) at the referenced site (Figure 1). Emergency Response &
Training Solutions (ERTS) called ECSNC on April 15, 2010 and ECSNC was mobilized to 407 South
Cansler St, Kings Mountain, NC to document the cleanup actions by JBR Environmental. The following
report details the activities documented and provides the results of the soil and surface water analytical
testing.
The following Tables, Figures, and Appendices have been attached:
• Table 1: Summary of Surface Water Analytical Data
• Table 2: Summary of Soil Analytical Data
• Figure 1: Site Locus
• Figure 2: Site Map
• Appendix A: Waste Manifests
• Appendix B: Laboratory Report
EMERGENCY SPILL RESPONSE
On April 15, 2010, ECSNC received a phone call from Mr. Nathan Walden at ERTS requesting a
professional engineer be on site to observe and document the activities of a spill of approximately 75
gallons of diesel fuel from a truck's saddle tank.
The accident occurred when a truck pulled out from a loading dock and punctured its diesel tank.
Approximately 75 gallons of diesel fuel was released and ran downhill into an adjacent dock (Dock #5 -
Yard Receiving) and down into a storm drain. The storm drain ran approximately 500 ft west northwest
of Dock #5 and emptied into a creek which travels west. Upon arrival ECSNC's professional engineer
Engineering and Consulting Services
13504 South Point Boulevard, Unit F . Charlotte, NC Tel: [phone] Fax. [phone]

(PE) noted that approximately 4-5 gallons of diesel fuel was contained in a green curb bucket (Serial # 00
004443 - City of Kings Mountain) and oil absorbent material was placed around the dock area and down
around the drain. The oil absorbent material was vacuumed up by JBR and a fresh batch was applied to
the area.
The PE then travelled to the storm water outfall location (Beason Creek) where the Kings Mountain Fire
Department had contained the spill with an earthen dam. Oil absorbent pads and booms were placed
downstream of the storm water outfall to prevent the diesel from impacting the creek further away. JBR
began vacuuming the diesel fuel on the surface of the water as well as diesel contaminated soil contained
within the earthen dam at 1445. Approximately 2 hours later (1645) the vac truck was filled to capacity
with diesel contaminated soil and water. Prior to leaving site it was discussed that a roll off container and
_ an excavator will be brought_ to the site _and used to remove the remaining contaminated soil that was
stockpiled. The 4-5 gallons of diesel fuel that was found in the green bucket at Dock #5 was vacuumed
by JBR and properly disposed of at JBR's receiving facility (See Appendix A for waste manifest). Prior
to leaving site the outfall was secured with caution tape and 6 oil absorbent booms were placed
downstream of the outfall to prevent free floating diesel migration.
On April 16, 2010 ECSNC's PE remobilized to the site to observe and document the excavation of diesel
contaminated soil. Using a mini excavator, JBR removed approximately 6.71 yards of diesel
contaminated soil. The storm water outfall contained a concrete pad which prevented the contamination
from spreading down into the soil immediately at the outfall (Figure 2). The concrete pad was exposed
by removing all diesel contaminated soil on top of it. A location where the concrete stopped and native
soil began was dug down approximately 1.5 to 2 ft below the bottom of the creek. A sample was
collected at this spot (SW-1). After soil excavation seized, a second soil sample (SW-2) was collected
downstream just beyond the concrete pad.
After all excavation activities were complete JBR continued to vacuum the surface of the water to remove
free floating residual diesel fuel that would exit the storm water outfall. JBR called the Kings Mountain
Fire Department and requested that the sewer system be flushed out to remove residual diesel fuel caught
within the sewer system. Flushing of the storm water sewer system began at 1430 by the Kings Mountain
Water District opening up a fire hydrant and allowing several hundred gallons of water to enter the storm
sewer system. JBR and the PE observed the outfall and JBR maintained a vacuum on the surface water to
capture residual diesel fuel. Several new absorbent booms were placed downstream to collect residual
diesel fuel that the vacuum could not get. Flushing of the system lasted for 1 hour (1430 to 1530). After
the flushing period the creek outfall contained a minor sheen on it. Prior to leaving site clean booms were
left at the location where the creek bottle necks beyond the outfall (approximately 10-15 ft away) to
collect the sheen. The PE spoke with Nathan Walden of ERTS prior to leaving site to notify him that the
contaminated soil was removed and oil absorbent booms were left to collect the sheen on the creek's
surface. A surface water sample from the creek (CR-1) was also collected prior to leaving site.
Based on the attached waste manifests approximately 6.71 yards of TPH contaminated soil was removed
from the site and an approximate total of 17.41 tons of diesel/water/soil/debris mixture were removed
during the emergency activities on April 15 and April 16, 2010. The waste manifests are included with
this report as Appendix A.
ANALYTICAL RESULTS
The surface water and soil samples were collected while wearing disposable iutrile gloves, containerized
in laboratory prepared glass bottles, packed on ice, and transported to Pace Analytical Services, Inc.
(Huntersville, NC), a North Carolina certified laboratory. Standard chain -of -custody procedures were
maintained, as documented in the laboratory reports included as Appendix R.

Three samples were collected on April 16, 2010. Two soil samples were collected from two locations;
SW-1 located adjacent to the concrete pad near the outfall and SW-2 located downstream of the outfall
and approximately 4-5 ft from where the concrete pad ends at the outfall. The soil samples were collected
for TPH-DRO using EPA Method 8015 Modified and prepared using the EPA 3546 Preparation Method.
Soil sample SW-1 was reported to contain 198.0 mg/kg of TPH-DRO. Soil sample SW-2 was reported to
contain 81.3 mg/kg of TPH-DRO.
One surface water sample (CR-1) was collected for volatile organic compounds using Standard Method
6200B. Total Xylenes was reported in CR-1 as 2.7 µg/L. Benzene, Toluene, Ethylbenzene, Diisopropyl
Ether, MTBE and Naphthalene were reported to be less than the laboratory's method detection limit.
Analytical results from the 2 soil samples and 1 surface water sample are presented as Table 1 and Table
2. Sample locations are presented in Figure 3.
If you have any questions or require additional information, please contact the undersigned at (704) 583-
2711, or email [e-mail].
Sincerely,
ENVIRONMENTAL COMPLIANCE SERVICES OF NC, PC
Brett G. Schaefer, PE
NC Licensed Engineer #036114
Enclosures
cc: Mr. Nathan Walden, ERTS
File

TABLES

TABLE 1
SUMMARY OF SURFACE WATER ANALYTICAL DATA
April 16, 2014)
Kings Mountain Emergency Spill Response
Well ID
Benzene
Toluene
Ethylbcn
Totalzenc
\ylenes
MTBE
IPE
Naphthalene
()ig/L)
(µg/L)
(pg/L)
(1rg/L)
(!ig/L)
CR-1
<0.5
<0.5
<0.5
2.7
<0.5
<0.5
<2.0
INCGWQS
1
600
600
50,0
Notes:
1. Laboratory analyses for purgeable aromatics by EPA Method 6200B
2. Concentrations in bold face type exceeded the NCGWQS.
3. Less than the reporting limit specified in the laboratory report.
4. North Carolina Groundwater Quality Standard specified in Title 15A NCAC 02L .0202. Revised 1/13/2010
Page 1 01, 1

TABLE 2
SUMMARY OF SOIL ANALYTICAL DATA
April 16, 2010
Kings Mountain Emergency Spill Response
Well H)
TPH-DRO (mg/kg)
SW-1
198.0
SW-2
81.3
Notes:
1. Laboratory analyses for TPH-DRO
Page 1 of 1

FIGURES

Figure 1 Topographic Map
'FIR 78
vw,*
„
•f ; { � t � � ,t � I F
' 1. -�
r i14
� i
- r. ® Outfall Location
u
(Beason Creek)
A t, ,•
Spill Location '
" _
r _
r
_
"e
ry ,
y ,
jai{'" [� • '. L i Y
�..
a
w
Magnetic Declination
Ohn
�17— tf.
�i
�A'°
SCALE 1:4M
0 100 200 300 YARDS
}� 0 1000 FEET
0 100 200 300 METERS
6.91°W '� �' I_ N 1 r
Copyright (C) 2009 MyTopo

Oil Absorbent
Booms
General Notes:
All locations, dimensions, and property lines
depicted on this plan are approximate. This
plan should not be used for construction or
land conveyance purposes.
s . G
cs
588 Silver Street • Agawam, MA 01001
Phone: [phone]= Far: 413-789-P778
PROJECT:
Kings Mountain Spill Response
407 S. Canster Rcl
Kings Mountain, NC
TITLE:
SITE PLAN
CLIENT:
Emergency Response & Environmental Services
GRAPHIC SCALE:
N a
Q N
N
COMPUTER CAOFILE
DRAWN BY:
DESIGNED BY:
CHECKED BY:
APPROVED BY:
BS
BS
BS
SCALE:
DATE:
JOB NO:
FIGURE NO:
N.T.S.
5/4/10
14-214102
2

APPENDIX A

MATEMAL JBR Environmental SorviCOs M rife t DiC`rc4FtTlent Nri
Spartanburg, C 29305 Fags of
' .�an,nre anrvr�r o%trex.%ei Ki khrihAr, `F�.% Af A-2 i
-77
GENERATOR
Name-
stroee AddfeSs MalfI g Ar ms;5 <<
�tir� lac.=.
t
ontaci
Yy
_IKON
OF NIATERLALS
HM
OOT .r r at<fp tg NMMzt
�
'L�h14J �s@kinq
Gontair�rs
i' ►�I
Un0,a{sli6
1rtt3 rr H�zrlt{t}lass
u
Ti`t�
�sr
ter t
s�
f
H
F
e
d a
A,DDMt1NAL !NFQ9 1 A'nG
CA. p •'=,�;,�yrt' d :j j',^ .Sz t y ... _.
„&� a1F ( _.. .
(g� - h
b-.
Oik;sF,UM iT'4 E LtR C� f tFICA 6IGF -
- L�'s1�>� 17-+i a aTv r�j Ciq-'. ifiud, ��r,Rlbifl pdt. kap&d'�, .�'Snr�'ki'=J am v�.3c elf- s`r"J re Sri
fr ''Ip cf Urar 4� o �3bt36' pr7pg
,'w'
PtFi�a� l a er-ding fo tho ? 1 gofq mgulaunns of ft e �nii�t`� ewl Y liampfoTaPoo P turth�� �arn?¢� Maf GIs"Io rh�+;r,�tomi� Oa csibed auoimr' � 6
.AA.,.,
ha Tc�doa 6' ',Rom as doKnot� by EPA 40 C.�R P� 1 or &ny t x t'raNp Ootp :Aw od bT �-! rr' 79efirc4affy kj&.gfhr"I?d 6b+sve, fhl:k .i' a l l"05 corefai'o .ros'-_.. char
I.lam t tof&J hoiO g az dp mat �ihx��f? �R'. b;a feve"t ( m.) o c8s gas i# , and by �� v �4 ;'Fp ¢tea � !� and '� 4.
'rYnkdf9d Opng tn+tcr poll:jT��y.rY'r-,�
da
.,., ..�... kip OR@NI05WgjO N
TrBtifl pp©© T 1' h eiGK r �r to ;l� f of t'�+p Roi t� e rlt7ru� r ithtdti'ul� �r 2' i'.4 rdP$ fr' t�] file g@'riDrov
J Envi �I^rh'ental e`v���t; 't
{�F,Si. Yid �'$,�{}t`E� d � r
r&�+lire 10 AOStreat e
Spa rktirr,SC 2931)3gr�"ur �'I' s hlF rater€ate == '
'Franspurtor Unit N € 1Qmb 3fCr�.{lfik &dVa b�ial'.ri o #3bot L�-Offf t In IN er�Ot171I f r! r'1 +s3 �-GJN� Cj l�ftZT IIhL t��3P]@ r3T3i 's�M
�
lst I[3No. O{�" E i t . wd Ce�i'rs,tz�i
`
phony } l
n+La t Y J a�.: De1l�l`y
_
- -
' FACI t MATIOra _
of ole marm-R s wv6ro4I"Ih;x ManlYQso} 0:. LL ,W:w aay
JB E;f'lvironmeMal erv4r
2 1 0 Alice Strout
Spartanburg, SC 30 wits+e F }; la�.r�l�t �,�r+,
Gl�F1�t= alrir<+ R ukiug ¢9sa11049ftals.
Phone
uiiiarl Rex usel
i ,rlgF#mf-.FactJit}d iotalln SOP' 2 - RuNim t❑ Gertcrat''dr CGPY 3-Trar3spr.,rIK l OVO COPY 4 - Gcnuf*nr RellAn

M .. T E - RIA L JBREnvironmeiUal Services,
MANIFEST P. 0. Box 40;9,8
Spadan4urg, SC 29305 age
fe
Em ,6rgesicy Phone Number- (864),A03-2717
7_77
GENERATOR INFORMA110141
a- PA III No
Mailing AdfjPhone 0a.
J4 'J i,
7_ 7==J_==77�
DESCRIPTtON-OF,,MATE,,Rj,.ALS.
PaOing ogntalmo-r 'MAW
mard VWN unt
A C�&ljp'
ul.n err* for Hazard4*4 *r�alslla
a.
Y'
ADDMIDNAL INFORMAT T§_R. W®R 6, Fam"I'll
4
GENERATORS GEAITPICAMN
�'�b pr,"- try 4r?d jar�kU igp -ill rppo,, , ipA.
me 6A
rmrj,5pqytzt�p_ id "o rhit �app abf6 mjpi��aqs' 0i ma 6ejotffponf L0 trax�jj;,vYattbo, -tfbL above am a
p �%
ljaiv&d3' waste ae der ftecrby EPA 40 C-t4:R Pail Z_ I .
a 6.-'& sfv& 'ta w, 8 (0 Cf wif &SLg 49 &C-dr. 0 lyy ken fl"6' th a
,poir f �Gfl r 'h of confaiit O&A096m �evofs�f 2 a P06-5 do -.wLk 2 Ta7 9 j�4 Teag&n5qmdd6m Aqpd m 40 CFF? F
f3rritffae l fleY signal um
... TRANSPERMAINF, MAT
,rar ol
si?# 6sted ah6v"V.
J
mq sip
"nature 1k Shipfae, D,
A
wafb skg
Um,I4 I hej'yiby aG*n&A'McVe _rA_ �19�0 pb.;�d mqran
EFAJR NQ. j �jid
k; tO
4
P h mgBPS
Dge
FACILRYINFORMATION
Faktff I y nemrfilmsr e'vtapr lu"ar-y
AdOesp� 21 G AJ ice St
Spartanburg, :5C' 29W3
Facility or
EPA, ID No. SCROOODD4358
Phone
Rex Russell.
OT19fiW - f acil0y,R&An COPY 2 Return fij Gemeratof C4:'PY:,' - Transporler Rriahl 4 - GerieratDr Relllh

.AL
,9V1E=F9 j LANDFOLL
, !MY A WqSTE, AAANAGEMENT C.QNAPAPJ'(
0 2
NON-11A ZAR,f)() tit;
1 11 -
G=emera for; 'm 0 1
Shipp n-
— - — --------
tttcsls
... . ... ...
1% (u Wied SoUd, mmi�
Pdmiihri,g -ss
Ail flT0
Ram ro eoqlq-stered, int-mifest, fw)
Srrzwol, Bw,-
I I b U r g,
Up 'Cody 2930
4 5=2717
Pn;Mu loco
Q31 I
500 >1
CQU25,'
4mm M 1 vuakhmm-
iiisi;e f QW
.1 WE, CordlY 41MI Me OWWW"Dwd mmROWS mm 130 ll,gzv(hus wams as &Aoedty 0, CTR, Pwc
20L or any OPPHOOK state hive, bwvv lwm filly Clod aeLljratd.,!� deseribell. 11 P10gmij rl c14
arv, Etl pnP,01, eu adir"dow 111
Tvaoixl�,orter Nn me
Addrns
f hemby aWwwledg, receipt of the aFtove
described matei-jids fOr Irmr6porl 00m Me
genyvajor she I lited above-
-Av
j1,T1w11l::
'Oliver Name (FT1nQ,:
I hereby 3,ektio"Iedgemedgmf tbo aWl"t, qkxriltvil
molork-LIS:
vvc�re received froull the g-VateraLf"r site, tt
wert, m(n%,pparted withiml hiddent, to the
&Sfiffitg 0 as NWRNUI 01t ildN fiJl 1:1 -
0 �V
,40A IN
Delivcr.,
Phu ne N amber: $864) 43 9-8426 - Elm 43 OTUTY
J Lo Novi Dk p#,�:A , v:�n i Woo 1.,!
. .... . ......
1K, 0 N1 A N1 FES-F M L N I B E F R 1. E I C C.- I I L, I P, I y k j I , � 4 A

APPENDIX B

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
AaceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
/ www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
April 28, 2010
Mr. Brett Schaefer
Environmental Compliance Services
13504 South Point Blvd.
---Unit F - -
Charlotte, NC 28273
RE: Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Dear Mr. Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on April 20, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
Page 1 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
hel1Cf

1,.AaceAnalytical
J wwmpacelabs.com
r
i
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Charlotte Certification IDs
9800 Kincey Ave. - Ste 100 Huntersville, NC 28078
Connecticut Certification #: PH-0104
Virginia Certification #: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cert. #: 990060003
South Carolina Certification #: 990060001
Pennsylvania Certification #: 68-00784
- - --North Carolina Wastewater -Certification #: 12 -
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828 )254-7176
CERTIFICATIONS
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
New Jersey Certification #: NCO12
Louisiana/LELAP Certification #: 04034
Kentucky UST Certification #: 84
Florida/NELAP Certification #: E87627
West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
rlela' f
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 18

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytical
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
/
Asheville, NC 28804
Huntersville, NC 28078
www.pacelabs.com
{
f
[phone]
[phone]
SAMPLE SUMMARY
Project:
Kings Mountain Spill Response
Pace Project No.:
9267703
Lab ID
Sample ID
Matrix
Date Collected
Date Received
9267703001
SW-1
Solid
04/16/1011:00
04120/1014:15
9267703002
SW-2
Solid
04/16/1015:15
04/20/1014:15
9267703003
CR-1
Water
04/16/1015:20
04/20/1014:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
2� ��a6C
Page 3 of 18

aceAnalltical
J`
J mimpacelabs.com
1
i
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Lab ID
Sample ID
9267703001
SW-1
9267703002
SW-2
9267703003
CR-1
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 8015 Modified
ASTM D2974-87
EPA 8015 Modified
- - -ASTM D2974-87-- - -
SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.oco`o
neaGf
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Analysts
Reported
Laboratory
RES
2
PASI-C
JEA
1
PASI-C
RES
2
PASI-C
-JEA - - -
- - - - 1 -
----PASI-C- - - - -
AW
64
PASI-C
Page 4 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
( vAm..pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
i
ANALYTICAL RESULTS
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Sample: SW-1
Lab ID: 9267703001 Collected:
04/16/10 11:00
Received: 04/20/10 14:15 Matrix: Solid
Results reported on a "dry -weight" basis
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified
Preparation Method:
EPA 3546
Diesel Components
198 mg/kg 27.5
17.1 1
04/21/10 14:30
04/26/10 21:54 68334-30-5 P3
n-Pentacosane (S)
0 % 50-135
1
04/21/10 14:30
04/26/10 21:54 629-99-2 S4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
9.2 % 0.10
0.10 1
04/26/10 09:06
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�%nelacm=
Page 5 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ll�aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
( mmpacelabs.corn Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
I
ANALYTICAL RESULTS
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Sample: SW-2
Lab ID: 9267703002 Collected:
04/16/10 15:15
Received: 04/20/10 14:15 Matrix: Solid
Results reported on a "dry -weight" basis
Report
Parameters
Results Units Limit
MDL DF
Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015 Modified Preparation Method: EPA 3546
Diesel Components
81.3 mg/kg 32.0
19.9 1
04/21/10 14:30
04/26/10 22:23 68334-30-5 P3
n-Pentacosane (S)
0 % 50-135
1
04/21/10 14:30
04/26/10 22:23 629-99-2 S4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
21.9 % 0.10
0.10 1
04/26/10 09:07
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,,\
ac
Page 6 of 18

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnal ical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
-" vrrowpacelabs.com Asheville, NC 28804 Huntersville, NC 28078
J
[phone] [phone]
1
ANALYTICAL RESULTS
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Sample: CR-1
Lab ID: 9267703003
Collected:
04/16/10
15:20
Received: 04/20/10 14:15 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Benzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
71-43-2
Bromobenzene _
_ _ ND_.ug/L_- _ _
0.-
_ _ 0.50 _
1
_ _ _ _ 04/27/10 17:52
108-86-1___ ._
Bromochloromethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
74-97-5
Bromodichloromethane
2.3 ug/L
0.50
0.50
1
04/27/10 17:52
75-27-4
Bromoform
ND ug/L
0.50
0.50
1
04/27/10 17:52
75-25-2
Bromomethane
ND ug/L
5.0
1.0
1
04/27/10 17:52
74-83-9
n-Butylbenzene
1.4 ug/L
0.50
0.50
1
04/27/10 17:52
104-51-8
sec-Butylbenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
135-98-8
tert-Butylbenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
98-06-6
Carbon tetrachloride
ND ug/L
0.50
0.50
1
04/27/10 17:52
56-23-5
Chlorobenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
108-90-7
Chloroethane
ND ug/L
1.0
1.0
1
04/27/10 17:52
75-00-3
Chloroform
18.9 ug/L
0.50
0.50
1
04/27/10 17:52
67-66-3
Chloromethane
ND ug/L
1.0
1.0
1
04/27/10 17:52
74-87-3
2-Chlorotoluene
0.60 ug/L
0.50
0.50
1
04/27/10 17:52
95-49-8
4-Chlorotoluene
ND ug/L
0.50
0.50
1
04/27/10 17:52
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
1.0
1.0
1
04127/1017:52
96-12-8
Dibromochloromethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
0.50
0.50
1
04/27/10 17:52
106-93-4
Dibromomethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
74-95-3
1,2-Dichlorobenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
95-50-1
1,3-Dichlorobenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
541-73-1
1,4-Dichlorobenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
106-46-7
Dichlorod ifluorom ethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
75-71-8
1,1-Dichloroethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
75-34-3
1,2-Dichloroethane
ND ug/L
0.50
0.50
1
04127/1017:52
107-06-2
1,1-Dichloroethene
ND ug/L
0.50
0.50
1
04/27/10 17:52
75-35-4
cis- 1,2-Dichloroethene
ND ug/L
0.50
0.50
1
04/27/10 17:52
156-59-2
trans-1,2-Dichloroethene
ND ug/L
0.50
0.50
1
04/27/10 17:52
156-60-5
1,2-Dichloropropane
ND ug/L
0.50
0.50
1
04/27/10 17:52
78-87-5
1,3-Dichloropropane
ND ug/L
0.50
0.50
1
04/27/10 17:52
142-28-9
2,2-Dichloropropane
ND ug/L
0.50
0.50
1
04/27/10 17:52
594-20-7
1,1-Dichloropropene
ND ug/L
0.50
0.50
1
04/27/10 17:52
563-58-6
cis- 1,3-Dichloropropene
ND ug/L
0.50
0.50
1
04/27/10 17:52
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
0.50
0.50
1
04/27/10 17:52
10061-02-6
Diisopropyl ether
ND ug/L
0.50
0.50
1
04/27/10 17:52
108-20-3
Ethylbenzene
ND ug/L
0.50
0.50
1
04/27/10 17:52
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
2.0
1
04/27/10 17:52
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
0.50
1
04/27/10 17:52
98-82-8
Methylene Chloride
ND ug/L
2.0
2.0
1
04/27/10 17:52
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
0.50
1
04/27/10 17:52
1634-04-4
Naphthalene
ND ug/L
2.0
2.0
1
04/27/10 17:52
91-20-3
n-Propylbenzene
0.99 ug/L
0.50
0.50
1
04/27/10 17:52
103-65-1
Styrene
ND ug/L
0.50
0.50
1
04/27/10 17:52
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
0.50
1
04/27/10 17:52
79-34-5
Date: 04/28/2010 02:55 PM REPORT OF LABORATORY ANALYSIS Page 7 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Dy
in. elac,=

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
I_AaceAnalXical 2225 Riverside Dr. 9800 KinceyAve. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
mmpacefabs.com
!� (828 )254-7176 (704 )875-9092
I
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Sample: CR-1
Parameters
6200B MSV
Tetrachloroethene
Toluene._
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
1,2-Dichloroethane-d4 (S)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 04/28/2010 02:55 PM
ANALYTICAL RESULTS
Lab ID: 9267703003
Results Units
Collected:
Report
Limit
04/16/10 15:20
MDL DF
Received: 04/20/10 14:15 Matrix: Water
Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
0.85 ug/L
0.50
0.50
1
04/27/10 17:52
127-18-4
_ND ug/L_- _ _._
_ _0.50 ._
0.50
_1_
_ _ 04127/1017:52108-88-3
ND ug/L
2.0
2.0
1
04/27/10 17:52
87-61-6
ND ug/L
2.0
2.0
1
04/27/10 17:52
120-82-1
ND ug/L
0.50
0.50
1
04/2711017:52
71-55-6
ND ug/L
0.50
0.50
1
04/27/10 17:52
79-00-5
ND ug/L
0.50
0.50
1
04/27/10 17:52
79-01-6
ND ug/L .
1.0
1.0
1
04/27/10 17:52
75-69-4
ND ug/L
0.50
0.50
1
04/27/10 17:52
96-18-4
5.6 ug/L
0.50
0.50
1
04/27/10 17:52
95-63-6
ND ug/L
0.50
0.50
1
04/27/10 17:52
108-67-8
ND ug/L
1.0
1.0
1
04/27/10 17:52
75-01-4
1.6 ug/L
1.0
1.0
1
04/27/10 17:52
1330-20-7
1.1 ug/L
0.50
0.50
1
04/27/10 17:52
95-47-6
86 %
70-130
1
04/27/10 17:52
17060-07-0
92 %
70-130
1
04/27/10 17:52
1868-53-7
113 %
70-130
1
04/27/10 17:52
460-00-4
96 %
70-130
1
04/27/10 17:52
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
n'elac,=
Page 8 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1��aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
�--' www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
/
[phone] [phone]
t
QUALITY CONTROL DATA
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
QC Batch: OEXT/9787
Analysis Method: EPA
8015 Modified
QC Batch Method: EPA 3546
Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 9267703001, 9267703002
METHOD BLANK: 431820
Matrix: Solid
Associated Lab Samples: 9267703001, 9267703002
- - - - - --
- Blank _ Reporting -
- - - - -
Parameter Units
Result Limit
Analyzed Qualifiers
Diesel Components mg/kg
ND 5.0
04/26/10 11:32
n-Pentacosane (S) %
82 50-135
04/26/10 11:32
LABORATORY CONTROL SAMPLE: 431821
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Diesel Components mg/kg
167 167
100 50-114
n-Pentacosane(S) %
104 50-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 431822
431823
MS MSD
9267534002
Spike Spike MS
MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD RPD Qual
Diesel Components mg/kg ND
199 199 212
157 106 79
50-107 30 30
n-Pentacosane(S) %
118 84
50-135
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
nelacf
Page 9 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAna1XJca1 2225 Riverside Dr. 9800 KinceyAve. Suite 100
--' wwwpacelabs.com Asheville, NC 28804 Huntersville, NC 28078
(828 )254-7176 (704 )875-9092
i
QUALITY CONTROL DATA
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
QC Batch: MSV/10716 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Associated Lab Samples: 9267703003
METHOD BLANK: 433087
Associated Lab Samples: 9267703003
-
Parameter
Matrix: Water
- -- - - Blank --------- Reporting---
Units Result Limit
-
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
04/23/10 13:05
1,1,1-Trichloroethane
ug/L
ND
0.50
04/23/10 13:05
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/23/10 13:05
1,1,2-Trichloroethane
ug/L
ND
0.50
04/23/10 13:05
1,1-Dichloroethane
ug/L
ND
0.50
04/23/10 13:05
1,1-Dichloroethene
ug/L
ND
0.50
04/23/10 13:05
1,1-Dichloropropene
ug/L
ND
0.50
04/23/10 13:05
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/23/10 13:05
1,2,3-Trichloropropane
ug/L
ND
0.50
04/23/10 13:05
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/23/10 13:05
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/23/10 13:05
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/23/10 13:05
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/23/10 13:05
1,2-Dichlorobenzene
ug/L
ND
0.50
04/23/10 13:05
1,2-Dichloroethane
ug/L
ND
0.50
04/23/10 13:05
1,2-Dichloropropane
ug/L
ND
0.50
04/23/10 13:05
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/23/10 13:05
1,3-Dichlorobenzene
ug/L
ND
0.50
04/23/10 13:05
1,3-Dichloropropane
ug/L
ND
0.50
04/23/10 13:05
1,4-Dichlorobenzene
ug/L
ND
0.50
04/23/10 13:05
2,2-Dichloropropane
ug/L
ND
0.50
04/2311013:05
2-Chlorotoluene
ug/L
ND
0.50
04/23/10 13:05
4-Chlorotoluene
ug/L
ND
0.50
04/23/10 13:05
Benzene
ug/L
ND
0.50
04/23/10 13:05
Bromobenzene
ug/L
ND
0.50
04/23/10 13:05
Bromochlorom ethane
ug/L
ND
0.50
04/23/10 13:05
Bromodichloromethane
ug/L
ND
0.50
04/23/10 13:05
Bromoform
ug/L
ND
0.50
04/23/10 13:05
Bromomethane
ug/L
ND
5.0
04/23/10 13:05
Carbon tetrachloride
ug/L
ND
0.50
04/23/10 13:05
Chlorobenzene
ug/L
ND
0.50
04/23/10 13:05
Chloroethane
ug/L
ND
1.0
04/23/10 13:05
Chloroform
ug/L
ND
0.50
04/23/10 13:05
Chloromethane
ug/L
ND
1.0
04/23/10 13:05
cis- 1,2-Dichloroethene
ug/L
ND
0.50
04/23/10 13:05
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/23/10 13:05
Dibromochloromethane
ug/L
ND
0.50
04/23/10 13:05
Dibromomethane
ug/L
ND
0.50
04/23/10 13:05
Dichlorodifluoromethane
ug/L
ND
0.50
04/23/10 13:05
Diisopropyl ether
ug/L
ND
0.50
04/23/10 13:05
Ethylbenzene
ug/L
ND
0.50
04/23/10 13:05
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/2311013:05
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/23/10 13:05
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
belac=
Qualifiers
Page 10 of 18

IV /® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
_ aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wv w.pacefabs.com Asheville, NC 28804 Huntersville, NC 28078
(828 )254-7176 (704 )875-9092
f
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
METHOD BLANK: 433087
Associated Lab Samples: 9267703003
Parameter
QUALITY CONTROL DATA
Matrix: Water
Blank
Units Result
Reporting
Limit Analyzed Qualifiers
m&p-Xylene
ug/L
ND
Methyl-tert-butyl ether
ug/L
ND
Methylene Chloride - - - -
ug/L - -
- - - -ND - -
n-Butylbenzene
ug/L
ND
n-Propylbenzene
ug/L
ND
Naphthalene
ug/L
ND
o-Xylene
ug/L
ND
sec -Butyl benzene
ug/L
ND
Styrene
ug/L
ND
tert-Butyl benzene
ug/L
ND
Tetrachloroethene
ug/L
ND
Toluene
ug/L
ND
trans-1,2-Dichloroethene
ug/L
ND
trans-1,3-Dichloropropene
ug/L
ND
Trichloroethene
ug/L
ND
Trichlorofluoromethane
ug/L
ND
Vinyl chloride
ug/L
ND
1,2-Dichloroethane-d4 (S)
%
119
4-Bromofluorobenzene (S)
%
87
Dibromofluoromethane (S)
%
113
Toluene-d8 (S)
%
102
METHOD BLANK: 434760 Matrix: Water
Associated Lab Samples: 9267703003
Parameter
Units
Blank
Result
1,1,1,2-Tetrachloroethane
ug/L
ND
1,1,1-Trichloroethane
ug/L
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
1,1,2-Trichloroethane
ug/L
ND
1,1-Dichloroethane
ug/L
ND
1,1-Dichloroethene
ug/L
ND
1,1-Dichloropropene
ug/L
ND
1,2,3-Trichlorobenzene
ug/L
ND
1,2,3-Trichloropropane
ug/L
ND
1,2,4-Trichlorobenzene
ug/L
ND
1,2,4-Trimethylbenzene
ug/L
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
1,2-Dibromoethane (EDB)
ug/L
ND
1,2-Dichlorobenzene
ug/L
ND
1,2-Dichloroethane
ug/L
ND
1,2-Dichloropropane
ug/L
ND
1,3,5-Trimethylbenzene
ug/L
ND
1,3-Dichlorobenzene
ug/L
ND
1,3-Dichloropropane
ug/L
ND
1.0
04123/1013:05
0.50
04/23/1013:05
- 2.0
- 04/23/10 13:05
0.50
04/23/1013:05
0.50
04/23/1013:05
2.0
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
0.50
04/23/1013:05
1.0
04/23/1013:05
1.0
04/23/1013:05
70-130
04/23/1013:05
70-130
04123/1013:05
70-130
04/23/1013:05
70-130
04/23/1013:05
Reporting
Limit
Analyzed
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
2.0
04/27/1017:08
0.50
04/27/1017:08
2.0
04/27/1017:08
0.50
04/27/1017:08
1.0
04/2711017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
Qualifiers
Date: 04/28/2010 02:55 PM REPORT OF LABORATORY ANALYSIS Page 11 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,N �LCpyO
o �
elac=

aceAnalXical
vnmpacelabs.com
i�
i
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
METHOD BLANK: 434760
Associated Lab Samples: 9267703003
Parameter
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Matrix: Water
Blank
Units Result
1,4-Dichlorobenzene
ug/L
2,2-Dichloropropane
ug/L
-2=Chlorotoluene - - - - --
---ug/L-- ----
4-Chlorotoluene
ug/L
Benzene
ug/L
Bromobenzene
ug/L
Bromochlorom ethane
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis-1,2-Dichloroethene
ug/L
cis-1,3-Dichloropropene
ug/L
Dibromochloromethane
ug/L
Dibromomethane
ug/L
Dichlorodifluoromethane
ug/L
Diisopropyl ether
ug/L
Ethylbenzene
ug/L
Hexachloro-1,3-butadiene
ug/L
Isopropylbenzene (Cumene)
ug/L
m&p-Xylene
ug/L
Methyl-tert-butyl ether
ug/L
Methylene Chloride
ug/L
n-Butylbenzene
ug/L
n-Propylbenzene
ug/L
Naphthalene
ug/L
o-Xylene
ug/L
sec-Butylbenzene
ug/L
Styrene
ug/L
tert-Butylbenzene
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Dichloropropene
ug/L
Trichloroethene
ug/L
Trichlorofluorom ethane
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Dibromofluoromethane (S)
%
Toluene-d8 (S)
%
ND
ND
- - - ND -
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
86
112
91
97
Reporting
L
imit Analyzed
0.50
04127/1017:08
0.50
04/27/1017:08
- - -0.50
04/27/10 17:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
5.0
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
1.0
04/27/1017:08
0.50
04/27/1017:08
1.0
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
2.0
04/27/1017:08
0.50
04/27/1017:08
1.0
04/27/1017:08
0.50
04/27/1017:08
2.0
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
2.0
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
0.50
04/27/1017:08
1.0
04/27/1017:08
1.0
04/27/1017:08
70-130
04/27/1017:08
70-130
04/27/1017:08
70-130
04/27/1017:08
70-130
04/27/1017:08
Qualifiers
Date: 04/28/2010 02:55 PM REPORT OF LABORATORY ANALYSIS Page 12 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
melacf =

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 KinceyAve. Suite 100
1�.KaceAnalyticalvnvw.pacelabss.coomAsheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
I
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
LABORATORY CONTROL SAMPLE: 433088
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
__.__l.,1,2-.Trichloroethane____.__
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromoch lorom ethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Dibromochlorom ethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Date: 04/28/2010 02:55 PM
QUALITY CONTROL DATA
Units
Spike
Conc.
LCS
Result
ug/L
50
50.9
ug/L
50
59.2
ug/L
50
54.0
_ ug/L. _ _
50
_ __. 54,1
ug/L
50
65.3
ug/L
50
63.4
ug/L
50
63.4
ug/L
50
44.3
ug/L
50
48.3
ug/L
50
48.2
ug/L
50
56.1
ug/L
50
59.7
ug/L
50
49.8
ug/L
50
50.8
ug/L
50
60.2
ug/L
50
61.3
ug/L
50
57.1
ug/L
50
51.6
ug/L
50
53.8
ug/L
50
52.6
ug/L
50
56.7
ug/L
50
57.6
ug/L
50
56.2
ug/L
50
59.3
ug/L
50
58.5
ug/L
50
53.2
ug/L
50
59.2
ug/L
50
56.1
ug/L
50
52.6
ug/L
50
62.2
ug/L
50
50.7
ug/L
50
47.2
ug/L
50
59.4
ug/L
50
65.9
ug/L
50
63.2
ug/L
50
63.4
ug/L
50
53.3
ug/L
50
47.8
ug/L
50
52.8
ug/L
50
62.5
ug/L
50
52.0
ug/L
50
47.4
ug/L
50
52.2
ug/L
100
106
ug/L
50
61.4
ug/L
50
61.4
ug/L
50
59.6
ug/L
50
59.1
LCS
% Rec
102
118
108
108
131
127
127
89
97
96
112
119
100
102
120
123
114
103
108
105
113
115
112
119
117
106
118
112
105
124
101
94
119
132
126
127
107
96
106
125
104
95
104
106
123
123
119
118
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
¢�r�elacf
% Rec
Limits
60-140
60-140
60-140
60-140
60-140 CL
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
60-140
Qualifiers
Page 13 of 18

a Pace Analytical Services, Inc. Pace Analytical Services, Inc.
AaceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
/ mwi.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
( [phone] [phone]
i
QUALITY CONTROL DATA
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
LABORATORY CONTROL SAMPLE:
433088
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Naphthalene
ug/L
50
48.1
96
60-140
o-Xylene
ug/L
50
51.9
104
60-140
sec-Butylbenzene
ug/L
50
57.8
116
60-140
-Styrene-- ---------___--
---ug/L_-
_ --
-510-
.
51.2---
102
60-140
tert-Butyl benzene
ug/L
50
53.1
106
60-140
Tetrachloroethene
ug/L
50
47.3
95
60-140
Toluene
ug/L
50
55.7
111
60-140
trans-1,2-Dichloroethene
ug/L
50
63.9
128
60-140
trans-1,3-Dichloropropene
ug/L
50
62.2
124
60-140
Trichloroethene
ug/L
50
51.8
104
60-140
Trichlorofluoromethane
ug/L
50
55.7
111
60-140
Vinyl chloride
ug/L
50
57.2
114
60-140
1,2-Dichloroethane-d4 (S)
%
114
70-130
4-Bromofluorobenzene (S)
%
87
70-130
Dibromofluoromethane (S)
%
108
70-130
Toluene-d8 (S)
%
105
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
433089
433090
MS
MSD
9267836008
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
16.2
22.1
81
110
60-140
31
30 R1
1,1,1-Trichloroethane
ug/L
ND
20
20
20.5
27.3
102
137
60-140
29
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
16.9
23.1
84
115
60-140
31
30 R1
1,1,2-Trichloroethane
ug/L
ND
20
20
18.4
24.6
92
123
60-140
29
30
1,1-Dichloroethane
ug/L
ND
20
20
22.1
29.7
111
148
60-140
29
30 MO
1,1-Dichloroethene
ug/L
ND
20
20
21.7
27.8
108
139
60-140
25
30
1,1-Dichloropropene
ug/L
ND
20
20
21.0
27.3 •
105
137
60-140
26
30
1,2,3-Trichlorobenzene
ug/L
ND
20
20
14.0
21.8
70
109
60-140
43
30 R1
1,2,3-Trichloropropane
ug/L
ND
20
20
15.8
21.3
79
107
60-140
30
30
1,2,4-Trichlorobenzene
ug/L
ND
20
20
14.8
21.9
74
110
60-140
39
30 R1
1,2,4-Trimethylbenzene
ug/L
ND
20
20
18.7
25.3
93
126
60-140
30
30
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
16.9
24.6
84
123
60-140
37
30 R1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
15.7
21.3
79
106
60-140
30
30
1,2-Dichlorobenzene
ug/L
ND
20
20
16.7
23.3
84
116
60-140
33
30 R1
1,2-Dichloroethane
ug/L
ND
20
20
20.0
26.8
100
134
60-140
29
30
1,2-Dichloropropane
ug/L
ND
20
20
20.8
28.0
104
140
60-140
30
30
1,3,5-Trimethyl benzene
ug/L
ND
20
20
18.8
25.5
94
128
60-140
31
30 R1
1,3-Dichlorobenzene
ug/L
ND
20
20
16.8
23.1
84
115
60-140
31
30 R1
1,3-Dichloropropane
ug/L
ND
20
20
17.6
24.1
88
120
60-140
31
30 R1
1,4-Dichlorobenzene
ug/L
ND
20
20
17.1
23.1
85
115
60-140
30
30
2,2-Dichloropropane
ug/L
ND
20
20
13.5
21.1
68
105
60-140
44
30 R1
2-Chlorotoluene
ug/L
ND
20
20
19.6
26.5
98
133
60-140
30
30
4-Chlorotoluene
ug/L
ND
20
20
19.6
26.2
98
131
60-140
29
30
Benzene
ug/L
ND
20
20
20.2
26.6
101
133
60-140
27
30
Bromobenzene
ug/L
ND
20
20
20.2
27.7
101
138
60-140
31
30 R1
Bromochloromethane
ug/L
ND
20
20
20.2
27.1
101
136
60-140
29
30
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,,,- . v
`/Clelac=
Page 14 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
_ aceAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
J www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078
t (828 )254-7176 (704 )875-9092
i
QUALITY CONTROL DATA
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
433089
433090
MS
MSD
9267836008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Bromodichloromethane
ug/L
ND
20
20
18.6
24.9
93
125
60-140
29
30
Bromoform
ug/L
ND
20
20
14.4
20.4
72
102
60-140
35
30 R1
____,Bromomethane_
_ ug/L _.
ND_ _
_ _20
__ 20
18.6
_. 24.1 _.
_ 93
120
60-140
26 _
30
Carbon tetrachloride
ug/L
ND
20
20
22.6
30.0
113
150
60-140
28
30 MO
Chlorobenzene
ug/L
ND
20
20
17.3
23.0
87
115
60-140
28
30
Chloroethane
ug/L
ND
20
20
24.4
32.5
122
162
60-140
29
30 MO
Chloroform
ug/L
ND
20
20
19.8
26.2
99
131
60-140
28
30
Chloromethane
ug/L
ND
20
20
20.2
26.8
101
134
60-140
28
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.9
29.1
109
145
60-140
28
30 MO
cis- 1,3-Dichloropropene
ug/L
ND
20
20
14.9
21.6
74
108
60-140
37
30 R1
Dibromochlorom ethane
ug/L
ND
20
20
15.5
21.5
77
108
60-140
33
30 R1
Dibromomethane
ug/L
ND
20
20
16.6
21.9
83
110
60-140
27
30
Dichlorod ifluorom ethane
ug/L
ND
20
20
17.1
22.0
85
110
60-140
25
30
Diisopropyl ether
ug/L
ND
20
20
21.0
28.7
105
143
60-140
31
30 MO,R1
Ethylbenzene
ug/L
ND
20
20
18.3
24.1
91
120
60-140
27
30
Hexachloro-1,3-butadiene
ug/L
ND
20
20
15.1
19.3
75
96
60-140
24
30
Isopropylbenzene (Cumene)
ug/L
ND
20
20
18.4
25.2
92
126
60-140
31
30 R1
m&p-Xylene
ug/L
ND
40
40
37.8
49.8
95
125
60-140
27
30
Methyl-tert-butyl ether
ug/L
ND
20
20
20.2
28.5
100
142
60-140
34
30 MO,R1
Methylene Chloride
ug/L
ND
20
20
20.0
27.1
100
135
60-140
30
30
n-Butylbenzene
ug/L
ND
20
20
19.2
27.4
96
137
60-140
35
30 R1
n-Propylbenzene
ug/L
ND
20
20
21.2
28.8
106
144
60-140
30
30 M0,R1
Naphthalene
ug/L
ND
20
20
14.3
22.3
72
111
60-140
44
30 R1
o-Xylene
ug/L
ND
20
20
18.4
24.9
92
125
60-140
30
30
sec-Butylbenzene
ug/L
ND
20
20
20.0
28.3
100
141
60-140
34
30 MO,R1
Styrene
ug/L
ND
20
20
16.5
21.7
83
108
60-140
27
30
tert-Butylbenzene
ug/L
ND
20
20
18.6
26.3
93
132
60-140
35
30 R1
Tetrachloroethene
ug/L
ND
20
20
15.5
20.4
78
102
60-140
27
30
Toluene
ug/L
ND
20
20
18.8
24.9
94
124
60-140
28
30
trans- 1,2-Dichloroethene
ug/L
ND
20
20
21.6
27.9
108
140
60-140
26
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
13.9
20.4
70
102
60-140
38
30 R1
Trichloroethene
ug/L
ND
20
20
17.4
22.5
87
113
60-140
26
30
Trichlorofluoromethane
ug/L
ND
20
20
22.1
28.2
111
141
60-140
24
30 MO
Vinyl chloride
ug/L
ND
20
20
20.5
25.7
102
129
60-140
23
30
1,2-Dichloroethane-d4 (S)
%
114
113
70-130
4-Bromofluorobenzene (S)
%
88
88
70-130
Dibromofluoromethane (S)
%
109
109
70-130
Toluene-d8 (S)
%
103
103
70-130
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
v ac
Page 15 of 18

�Z
aceAnal�%�Ica!
J `
J vm wpacelabs.com
1
I
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
QC Batch: PMST/3153
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9267703001, 9267703002
SAMPLE DUPLICATE: 433273
Parameter Units
Percent Moisture %
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
9267703001 Dup Max
Result Result RPD RPD Qualifiers
9.2 9.8 7 25
SAMPLE DUPLICATE: 433274
9267980001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 14.4 16.1 11 25
Date: 04/28/2010 02:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 18

_ aceAnal�/�ical
J`
/ wvvipacelabs.com
i
QUALIFIERS
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
Cu The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
R1 RPD value was outside control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
Date: 04/28/2010 02:55 PM REPORT OF LABORATORY ANALYSIS Page 17 of 18
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�heac

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr. 9800 KinceyAve. Suite 100
( www.pacelabs.com
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
1
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Kings Mountain Spill Response
Pace Project No.: 9267703
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
9267703001
SW-1
EPA 3546
OEXT/9787
EPA 8015 Modified
GCSV/7511
9267703002
SW-2
EPA 3546
OEXT/9787
EPA 8015 Modified
GCSV/7511
9267703003
CR-1
SM 6200B
MSV/10716
_92677.03001__ _____
— .SW-1 ____ __--
ASTMD2974-87
_. PMST/3153
9267703002
SW-2
ASTM D2974-87
PMST/3153
Date: 04/28/2010 02:55 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
-(nelac
Page 18 of 18

; ceAnal ical
www.pacela6s.com
i
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Page: / of /
Required Client Information: Required Project Information: Invoice Information:
Company: •
Report To: Attention:
i �%
11
VCIY
i �
19468
Addre;s pf 1
Copy To:
Company Name:
REGULATORY AGENCY'
_
Address:
j— NPDES j— GROUNDWATER r DRINKING WATER
(— UST r RCRA ✓OTHER
Email To:��'"^'
.CS.�C�C�C �'t'SCdI�iK
Purchase Order No. : [/
7 �e�I7 /Qp�
Pace Quote
Reference:
Phone:
_
F (� 'yf
�/
Project Name: //�% n
Pace Project
�!
Site Location
sraE::
Requested Due DaterrAT:
Project Number. Vr, �-
Pace Profile #:
2 9
Requested
Analysis'
-
Filteted
(YIN)
Section D Matrix Codes
�-
z.
Required Client Information MATRIX / CODE
o
O
COLLECTED
Preservatives
%,
Drinking Water DW
V
Z
' Water WT
O
Waste Water WW
v
m
COMPOSITE
COMPOSITE
�
W
Product P
—
START
END/GRAB
Q
Z
Soil/Solid SL
SAMPLE ID Wipe WP
YL
°
CO
/jJt
(A Z, 0-9 1 ,) Air AR
w
a.
W
N
Fy
/y �lV]
//J]�'D
Sample IDS MUST BE UNIQUE Tissue TS
O
D-
�
_Z
Q
o
L
(`'/li ✓ 1 G
st
Other OT
U
X
Lu
rw-
w
Z
O
Z
,
U
w
1
�
i
tL
�'
O
=
O
rn
c
L
a�
m
~
DATE
TIME
DATE
TIME
�
=
2
2
Z
Z
2
O
y.
Pace Project No./ Lab I.D.
2
-a
sc
G
,ors
a
a
3
�d
4
C-
G
rS"aZo
3
3
3
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY PAFFILIATION
DATE
TIME
SAMPLE CONDITIONS
t/�%s'
+PCs
y/6 jig
i7Try
CSdw
, Z
1 ,
2
SAMPLER NAME AND SIGNATURE I,.
ORIGINAL PRINT Name of SAMPLER:
/2
U
l
v}
a o
o0Z
yZ
DATE Si ned
SIGNATURE of SAMPLER: _ __g 41Z Z
E
of —
O m
d
E

-f'aceAraEytical a SZry
Client Name: �,�;,, IQAee Project # 1,4 q-710.3
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ��n
mmercial ,�J Pace Other
OpUonaf
Custody Seal on Cooler/Box Present: 1-1yes o Seals intact: ❑ yes no Prof Due Date N/R {
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑Other
Thermometer Used T060 Type of Ice OVV
Blue None Samples on ice, cooling process has begun
Cooler Temperature Biological Tissue is Frozen: Yes No N/A Date and Initia p5 son fn' g
Temp should be above freezing to 6°C contents: /d
Comments:
Chain of Custody Present. -
Chain of Custody Filled Out. -
Chain -of Custody Relinquished: -
Sampler Name & Signature on COC:
Samples Arrived within Hold Time:
Short Hold Time Analysis (<72hr):
,,L6I
No
❑ N/A
1.
❑No
❑N/A
2.
Yes
❑No
' ❑N/A
3
L?IY
❑No
❑N/A
4.
es
El No
NIA
5.
❑Yes
No ,ON/A
6.
Rush Turn Around Time Requested:
Oyes
12 o
❑N/A 7.
Sufficient Volume:
Yes
❑No
❑N/A g.
Correct Containers Used:
Yes
[INN/A g.
-Pace Containers Used:
❑Ye
;No
❑N/A
Containers Intact:
Yes
❑No
pN/ 10 .
Filtered volume received for Dissolved tests
❑Yes
No
N/A 11
Sample Labels match COC:
Yes
❑No
❑N/A 12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked,
Yes ❑No
❑N/A 13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
Yes
❑No
❑N/A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes
❑No
nitial when completed
Samples checked for dechlorination:
❑Yes
❑No
NIA 14.
Headspace in VOA Vials ( >6mm):
❑Yes
No
❑NIA 15.
Trip Blank Present:
❑Yes
❑No
16.
Trip Blank Custody Seals Present
❑Yes
❑No
N/A
Pace Trip Blank Lot # (if purchased): N/A
Client Notification/ Resolution:
Field Data Required? Y / N / N/A
Person Contacted:
Date/Time:
Comments/ Resolution:
Project Manager Review: W Date: 1,/
lote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
:ertification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containarc)

NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
May 11, 2009 , ,E 5
Mayor Alton Beal
Town of Lattimore
P.O. Box 272
Lattimore, NC 28089
CERTIFIED MAIL
Return Receipt Requested
M, AY 1 3 2009
DM-� . _ . o ..r: n:..I.,
�lu.:v �ison
Subject: Notification of Watershed Program Deficiency
Dear Mayor Beal:
The purpose of this letter is to notify the Town of Lattimore of its program deficiency pursuant
to N.C. General Statute § 143-214.5 for failing to implement a watershed protection ordinance in
the Broad River watershed.
The Water Supply Watershed Protection Act (N.C.G.S § 143-214.5) and Rule 15A NCAC 2B
.0104(b) require that all local governments having land use jurisdiction within a water supply
watershed adopt and implement land use ordinances. The ordinances must meet the minimum
requirements of the Environmental Management Commission's (EMC) rules under 15A NCAC
2B .0200 for the classification assigned to the watershed. Failure by a local government to
adopt land use ordinances after notice of the watershed reclassification can result in assumption
of the local program by the EMC and civil penalties pursuant to N.C.G.S. 143-215.6A(e).
As you are aware, the EMC reclassified a segment of the Broad River and other river sections,
creeks, and lakes in the Town of Lattimore and surrounding areas (Broad River Basin) from
Class C to Class WS-IV and WS-IV-CA. The reclassification became effective on March 1,
2007. , The Town of Lattimore was notified of the reclassification on March 6, 2007 and was
given until December 1, 2007 to comply by adopting a watershed ordinance and map. The town
failed to meet that deadline. DWQ initially informed the town of the deficiency in our letter of
May 19, 2008. To date, we have not received a response.
Pursuant to N.C.G.S. § 143-214.5, the EMC, or its designee, must notify a local government of
program deficiencies and allow a local government a minimum of 120 days and a maximum of
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 One
Phone: [phone] \ FAX: [phone] \ Customer Service:1-877-623-6748 NorthCarolina .
Intemet:.www.ncwaterquality.org ��t�r�'���
An Equal Opportunity \ Affirmative Action Employer 6

365 days to bring its program into compliance. At anytime between 120 days and 365 days
after local government receipt of notice, the EMC may determine that no substantial progress has
been made. At such time that the EMC determines no substantial progress has been made, the
EMC shall order assumption of a local program. Upon assumption of a local program, civil
penalties of up to $10,000 per month may also be assessed pursuant to N.C.G.S §143-215.6A(e).
This letter initiates the statutory notification process for the Town of Lattimore. Your receipt of
this letter establishes the timeframe for compliance of 120 to 365 days. The Town of Lattimore
must address this deficiency by adopting and implementing a watershed ordinance and map for
the Broad River watershed. You may consider seeking assistance from Cleveland County in
completing these actions and administering your watershed protection program.
To avoid further enforcement action, the following actions must be taken:
1. Adopt and implement the appropriate watershed protection ordinance.
2. Submit to DWQ three copies of the town's ordinance for approval by the EMC or its
designee.
3. Submit to DWQ an updated map indicating your local government boundaries (corporate and
ETJ) and the location of the reclassified waters, including critical area and protected area
boundaries within your jurisdiction.
DWQ plans to present an update on the steps that the town has taken to bring its program into
compliance at the July 2009 Water Quality Committee meeting. Please provide this office a
report on the status of the city's compliance efforts by June 26, 2009. Please send this
information to the attention of Julie Ventaloro at'NC DWQ, Wetlands and Storm -water Branch,
1617 Mail Service Center, Raleigh, NC 27604.
Thank you for your prompt attention to this matter. If you need further assistance, please contact
Julie Ventaloro at [phone] or julie.ventalorota'-,ncdenr.gov.
Sincerely,
Matt Matthews
Surface Water Protection Section Chief
cc: Tom Martin, Flowers, Martin, Moore and Ditz, P.A., 212 South Dekalb St., Shelby, NC 28150
John Hennessy, NPS-ACO Unit
Julie Ventaloro, Water Supply Watershed Protection Program
Rob I reb_s;1Vloo er sv :fle-DWQ
Enclosures
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 1�7One 1
Phone: [phone] \ FAX: [phone] \ Customer Service: 1-877-623-6748 i� OTthCCU* Alma
Internet: www.ncwaterquality.org 9,N� //�
Ari Equal Opportunity \ Affirmative Action Employer Natul

UU11115ENGINEERS
April 16, 2007
OFFICE
APR 17 2007
r a•r - '�J tl'
Public Water Supply Section
NC Division of Environmental Health
1634 Mail Service Center
Raleigh, North Carolina 27699-1634
Subject: Water System Improvements
Chestnut Street Area Water Lines
City of Shelby
- Cleveland County - I.D. 0123010
Gentlemen:
925.014 (34)
This letter is to verify that construction of the subject project has been completed in
substantial compliance and intent of the plans and specifications approved under Division
of Environmental Health serial number 06-00707 dated May 19, 2006.
Yours very truly,
WILLIS ENGINEERS
cm, " -t
/'�
C. A. Willis, P.E.
CAW: jcs
cc: Mr. Brad R. Cornwell, PLS
MQoresil e Reg oval -Office->
Cleveland County Health Department
Registration Number 3322
®g�n�fle®ae�os,
SEAL
2 2,
.r, ART"
1520 South Boulevard
Charlotte, North Carolina 28203
704.377.9844 Fax [phone]

EMERGENCY RESPONSE&TRAINING SOLUTIONS
For those 2vho demand results
August 4, 2006
NC Department of Environment and Natural Resources
Mooresville Regional Office
Division of Water Quality
610 East Center Ave.
Mooresville, NC 28115
RE: Corrective Action Final Report
Knight Transportation
Diesel Fuel Release
2081West Dixon Blvd.
Shelby, NC
Cleveland County
ERTS Project # 07252006ShelbyNC
Dear Sirs,
AND HATU' :L RESOURCE„
0300REVU-7, ` '�00NAL OFF1
AUG 1 0 200-1
C '
ON
The following serves as the final report detailing the emergency response and corrective
action taken in response the incident that occurred on July 25, 2006, at the above
referenced location.
Incident Background:
On, July 25, 2006 at approximately 1:00 am. EST, a Knight Transportation tractor -trailer
suffered a diesel fuel release due to impact with a vehicle and brick sign which resulted in
a puncture to the saddle tank. The punctured saddle tank released diesel fuel onto the
lawn area. There was no water impact from the release.
Emergency Response:
On July 25, 2006, Knight Transportation retained Emergency Response and Training
Solutions (ERTS) to manage and oversee environmental operations on their behalf. ERTS
dispatched JBR Environmental to the scene to ensure the site was contained and secured.
JBR Environmental personnel arrived onsite to perform containment operations of the
released diesel.
8401 Chagrin Road, Suite 15B • Chagrin Falls, Ohio 44023
Tel. [phone] • Fax [phone]

Regulatory Notifications:
Pursuant to North Carolina regulations, ERTS notified the North Carolina
Department of Environment and Natural Resources (NCDENR). The NCDENR did
not issue a confirmation number to the report.
Corrective Action:
On July 28, 2006, Protect Environmental performed excavation of the diesel
contaminated soils was completed. All diesel —impacted soils were containerized for
transportation and disposal. The site was back -filled, regraded and reseeded to
complete the remediation and restoration to original conditions.
Waste Disposal:
On July 28, 2005, 41.65 tons of diesel contaminated soil were transported to and
disposed of at Environmental Soils in Lattimore, NC. Attached are the non-
hazardous waste manifests (Appendix 1).
Conclusion and Recommendations:
No evidence was found that suggests any significant environmental impact remains
on the sites following corrective action. ERTS recommends that the incident be
closed and that no further assessment is needed.
ERTS and Knight Transportation appreciate your assistance in this matter. If you
have any questions regarding this project, please do not hesitate to contact me at
[phone] ext 302.
Respectfully,
Emergency Respons :andTraining Solutions
Christine Kovach
Project Manager
CC: Greg Williams — Knight Insurance

Appendix 1
Non -Hazardous Waste Manifests

Environmental Soils Inc.
PO Box 295 - Lattimore, NC 28089
Phone [phone] - Fax [phone]
­7 Ncin­ Hazardous Waste Manifest #
Date U Load Number
22361
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTANT
Contact:
GEXER,4T0R_-
Phone:
Fax:
Address: "Y' 1County:
Contact: I
?
Phone:
WASTE OR[GJ7V,4T10NPOL?VT- omplete Address: _-Z tj
Class &Type of Contaminate in soil K-14 4- .. ­-
SOURCE, OF CONT_4MLV,4TI0N.• (ex. UST or other source)
GENER,4TORS CERTIFIC,4TION OF WASTE CONSTITUEATTS. In lieu of submitting analytical data (methods
8240 and 82 70) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting Certificate of Waste
P tti rtifi as e
Constituents. Icertify that I am familiar with the source of contamination of the soil and further certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signa
Date:
TRdNSPORTER-
Contact:
Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:.
Date:
, 1 4-
TRUCK#:
rT-Ay #: VOLUME:
TRUCK DRIVER SIGNATURE: :"-/; DATE:
DESTTVATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that- the carrier has delivered the materials described above to this facility, and I hereby accept this material
,for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.')
Facility Signature: Date:
Signature:
Date:
Company. Name
Tide:
White/Facility .-yink/Carrier Golden -j�od/G&nerator
Cknary/Invoic.e_

PPP ,
Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 2 2 3 6 2
Date - = 1,'.: Load Number
_(numbered sequentially as trucks are dispatched)
ENURONMENT4L CONSULTANT
Contact: s '.: r' '� -,- ;�-< Phone: Fax: `iI �•,
GENER,4TOR T7 1' i
Address: + J°", F ..r _�,, ' County:
Contact: /" �:. _ x.. c - 1 Phone:
W14STE ORIGIM47YONPOINT Complete Address: A
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION.• (ex. UST or other source)
GENER,ITORS CERTIFICATION OF W,ISTE CONSTITUENTS: In lieu ofsubmitting analytical data methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste
Constituents. I certify thatl am familiar with the source of contamination of the soil and further cert� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: t �:,:;-„_� ,� ��1� _ ..,r„- i- - � �, 'r _. Date: r f<_t ,t
TRANSPORTER: C- 6_1 C )
Contact: _. �;r < • �r Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. - i
Carrier Signature:-`r�r: - r. Date: f
r ', _ �< _�;-�•�
TRUCK #: C� TAG #: VOLUME:
%
TRUCK DRIVER SIGNATURE: DATE:f�-r-
, ` J
DESTIN-ITION,• Environment;all Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038 -
I certify that the carrier has delivered the materials described above_to this facility, and.I hereby accept this material
for treatment and/or disposal, in a manner that has been authorized by the Sate of North Carolina..
Facility Signature:
Signature: _ r?
Company Name
Date:
Title:
Date:
White/Facility . Canary/Invoice Pink/Carrier
G-oldenrod/Generator.

pppppr
Environmental Soils Inc.
_ .. PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 22363
f
Date %r! - _- `f'�j L Load Number
�! (numbered sequentially as trucks -are dispatched)
ENVIRON E : _
1V� NT4L CONSULT4NT .J �"`' �� .. `:: '�- . j � it _�y,�� fit,
Contact: ."a i J f. ' f ., ! Phone: Fax:
GENERATOR- s
Address: �r Y 1 ;Y r t 4iF y i,.. { ` '. f J T'rb r': e! ti 1 County:
�` !
Contact:
Phone:'
W12STE ORIGIN,ITIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MLV,4TI0N (ex. UST or other source)
GENEP,4TORS CERTIFICATION OF WJSTE CONSTITUENTS: In lieu of submitting analytical data methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certificate of Waste
Constituents. I certify thatl am familiar with the source of contamination of the soil and further certify the source; to
the best of my knowledge, contains no contaminants other than that listed above.
GeneratQrsxgnaxure=_ IJate:
TP.ANSPORTER: ;' .... .
Contact:. Y- ,..+, w� ; -= .1G ^ r
- �^:�'' � r i ' iv�� Phone:
As the, carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. '.1i ,
Carrier Signature: ,/ ..� -ti�:�� .- '7, /1 ;.� - Date: <- I "
TRUCK #: �' ;-�-� %�, ..._.,
r TAG #: VOLUME: ,
TRUCK DRIVER SIGNATURE: DATE,: 1 r`
DESTINATION • Environmental Soils Inca 91Q Crowder -Rd, Shelby,ANC 28150 Dedicated Land Application
Site Permit #SR03;00038
I certify that-t.e carrier has. delivered the materials described, above to this facility, and I hereby accept this material
for treatment'and/or disppsal in a manner that has been. authorized by the Sate of North Carolina. .
Facility Signature: f _ - F Date: f `"
/f JR I
Signature: %' r' .t h� is ::': 'r -- :-•Bate:
Company Name
Title:
White/Facility Canary/Invoice :.- Pink. Carrier. Goldenrod/Generator

Fax:
GENER,4TOR-
Address: County: tL-
Contact: Phone: 16' S_ �9
MSTE ORIG17VATIONPOINT. Complete Address,:
Class &-Type of Contaminate in soil
SOURCE OF CONT4MLV,47I0N• (ex. UST or other source)
GENERdTORS CERTIFICATION OF W_4STE CONSTITUENTS. In lieu of submitting analytical data (methods
8240 and 82 70) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Certificate of Waste
Constituents. Icertify thatlainfamiliar with the source of contamination of the soil and further certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: : Date
T10%."SPORTE
Contact: Phone:
As the carrier, I certify that the materials described abova�5eing"' shipped under this non -hazardous materials
manifest
ani est are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
Environrnentad Soils Inc.
PO Box 295 - Lattimore, NC-28089
Phone [phone] - Fax [phone]
Non -Hazardous Waste Man
ifest #22364
Date
Load Number.
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTANT -
Contact:
Phone:
Date: ti 21'r
TRUCK #: TAG #: VOLUME: 10-4
TRUCK DRIVER SIGNATURE:)Xf, /
DATE:
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in '' ' er that has been authorized by the Sate of North Carolina.
Amann
Facility Signature:;
f -Date:
f
Signature: i
Date:
Company Name
Title:
White/Facility
Canary/lnwice...'.. Pink/Carrier Goldenrod/Generator."

aceAnalytical
cvrevpaLWabS-rom
CHAIN -OF -CUSTODY / Analytical' Request Document
The Chain-cf-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A
Required Client Information:
Section B
Required Project Information:
Section C
Invoice Information:
Page:
\ of
Company: PROTECT Environmental Services
Report To: David Hadster
Attention: David Hardister
REGULATORY
Address: 7104 Sandy Pines Or
Copy To:
Company Name:
PROTECT Environmental Services
S r GROUND WATER r- DRINKING WATER
Youngsville, NC 27596
Address:
7104 Sand Pines Dr Youn sviile, NC 27596
r- RCRA
t' OTHER
Email To: ftardister(@wearotect.us
Purchase Order No.:
Pace Quote Reference:
JF11tered
j� GA I- IL r IN I- MI .4;AC
Phone: [phone] Fax: [phone]
Project Name: Cleveland Yutaka
Pace Project Manager.
• j-'- OH j"
SC r WI
j-• OTHER -
Requested Due DatarrAT:
Project Number.
Pace Profile #:
)
Section D Required Client InformationValid
SAMPLE ID
One Character per box.
(XZ, 0-9 / ,-)
WSamplelDsMUST
~
Mix CodesMATRI 0
orsamawnm+ ON
„mow Bwr „,
P
M a—
re
w
x
a
12
0
o
r,
COLLECTED
a
2 o
9
8o
m
Z
Preservatives
Requested
arysls:
cJ
a Pau pm
Lab IJ-tND
m
-
`
CT
_
r
=
d
6
COMPOSITE START
coarosreaaoaRae
DATE
TIME
DATE
TIME
A
P
C
1
2
6
0
1
D
C
SL
G
1 725/06
8:00
725/06
8:05
A
P
C
1
2
6
0
G
C
`SL
G
725/06
8:10
725/06
8:15
�+
A
P
C
1
2
6
0
C
L
SL
G
725/06
15:20
725/06
15:25
Additional Comments:
•
•
•
•
SAMPLE
CONDITIONS
SAMPLER NAME AND SIGNATURE
PRINT N e of SAMPLER;
610NA1-UR of PLEB:
dzO'STE,2
DATE Signed (
DD//�/y)
U
S
r
a�
o
d
o
a
02
S
c
m
E
e-File(ALLQ020rev.3,31 Mar05))22Jun2005

EMERGENCY RESPONSE&TRAINING SOLUTIONS
For those 2vho demand results
August 18, 2006
NC Department of Environment and Natural Resources
Mooresville Regional Office
Division of Water Quality
610 East Center Ave.
Mooresville, NC 28115
RE: Corrective Action Final Report
Knight Transportation
Diesel Fuel Release
2081West Dixon Blvd.
Shelby, NC
Cleveland County
ERTS Project # 07252006ShelbyNC
Dear Sirs,
AND NATURAL RESOURCES
'nOORES` ILLS a ECIC�##� OFFICE
AUG 2 1 2006
The following serves as the amended final report detailing the emergency response and
corrective action taken in response the incident that occurred on July 25, 2006, at the
above referenced location.
Incident Background:
On, July 25, 2006 at approximately 1:00 am. EST, a Knight Transportation tractor -trailer
suffered a diesel fuel release due to impact with a vehicle and brick sign which resulted in
a puncture to the saddle tank. The punctured saddle tank released diesel fuel onto the
lawn area. There was no water impact from the release.
Emergency Response:
On July 25, 2006, Knight Transportation retained Emergency Response and Training
Solutions (ERTS) to manage and oversee environmental operations on their behalf. ERTS
dispatched JBR Environmental to the scene to ensure the site was contained and secured.
JBR Environmental personnel arrived onsite to perform containment operations of the
released diesel.
8401 Chagrin Road, Suite 15B • Chagrin Falls, Ohio 44023
Tel. [phone] • Fax [phone]

Regulatory Notifications:
Pursuant to North Carolina regulations,. ERTS notified the North Carolina Department of
Environment and Natural Resources (NCDENR). The NCDENR did not issue a
confirmation number to the report.
Corrective Action:
On July 28, 2006, Protect Environmental performed excavation of the diesel
contaminated soils. Samples were taken to verify clean closure. The analytical data is
attached as Appendix 1. All diesel —impacted soils were containerized for transportation
and disposal. The site was back -filled, regraded and reseeded to complete the remediation
and restoration to original conditions.
Waste Disposal:
On July 28, 2005, 41.65 tons of diesel contaminated soil were transported to and disposed
of at Environmental Soils in Lattimore, NC. Attached are the non -hazardous waste
manifests (Appendix 2).
Conclusion and Recommendations:
Based on contractor observations and review of analytical results, no evidence was found
that suggests any significant environmental impact remains on the sites following
corrective action. ERTS recommends that the incident be closed and that no further
assessment is needed.
ERTS and Knight Transportation appreciate your assistance in this matter. If you have
any questions regarding this project, please do not hesitate to contact me at (440) 543-
2400 ext 302.
Respectfully,
Emergency Response and Training Solutions
Christine Kovach
Project Manager
CC: Greg Williams — Knight Insurance

Appendix 1
Analytical Data

_ .. aceAnalytical60
www.pacoiabs.com
August 11, 2006
Mr. David Hardister
Protect Environmental
7104 Sandy Pine Drive
Youngsville, NC 27596
RE: Lab Project Number: 92124440
Client Project ID: Cleveland Yutaka
Dear Mr. Hardister:
Pace Analytical Services, Inc.
9800 Kinccy Avenue:, Suite 100
Huntersvillo, NC 26078
Phone; 704.875.9092
Fax: 704, 075.9091
Pace Analytical Services, Inc.
2225 Riverside: Drive
Asheville, NC 28804
Phone. 828,254.7176
Fax, 828.252.4618
Enclosed are the analytical results for sample(s) received by the laboratory on August 2, 2006. Results reported
herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of
the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely.
k I-L ltv
Kate Knauff
[e-mail]
[phone] ext. 236
Project Manager
Enclosures
As Mlle c. tef ificatia REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services. Inc.
so 99030 �r, roh
FL NELAP E87648 ^��
°' f
;Mac
fLariotty Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
Ed Wd06:b6 960E 91 '6nd i36SESISS616: 'ON Xdd SaotnJaS l?1uawu0uinu3 iO3iOLld: WONA

s. ace Analytical o
wwur.pacelabs.conr
Solid results are reported on a dry weight basis
Lab Sample No: 927261693
Client Sample ID: APC1260 DC
Pace Analytical Services, Inc.
9800 Kinney Avenue, Suite 100
Nuntelsvillc, NC 28078
Phone., 704.875.9092
Fier. 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC26804
Phone'826.254.7176
Fax, 826.252.4618
Lab Project Number: 9212444D
Client Project ID: Cleveland Yutaka
Project Sample Number: 92124440-001 Date Collected: 07/25/06 08:05
Matrix: Sail Date Received: 08/02/06 10:45
Parameters Results Units Report Limit Analyzed By CAS No. Qual R,egLmt
Wet Chemistry
Percent Moisture Method: X Moisture
Percent Moisture 17.9 X 08/02/06 17:58 TNM
GC Semivolatiles
TPH in Soil by 3545/8015
Diesel Fuel
n-Pentacosane (S)
Date Extracted
Date: 08/11/06
hevilk Certifiution l9
NC Wastewater 40
NC Drinking Water 37712
5C 99030
FL NELAP E81648
Prep/Method: EPA 3545 / EPA 8015
11000 mg/kg 1200
0
08/03/06
08/07/06 20:31 KBS
08/07/06 20:31 KBS
08/03/06
REPORT OF LABORATORY ANALYSIS
This report shall not be reprudticed, except in full,
withuut the written consent of Pace Analytical Scrvlces. Inc.
pt nccdgai
• et; s
;e hmr-
68334.30-5
629-99-2 1
Page: 1 of a
c4mgte ' qedjration Uh
NO Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
zd Wdlo:b0 900E 9T -6nd 80SE9SS6TG: 'ON Xti.d SaainuaS (eluawuo.alnu0 10910idd: WONJ

_ aceAnalytical °
www. pacclabs. cnm
Lab Sample No: 927261701�
Client Sample ID: APC1260 GC
Pace Analytical Se"Ices, Inc.
9800 Kllle;QV Avenue, Srrite 100
Nuntersvillc, NC 28078
Phone; 704.67,5. y092
Fix: 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NO 26804
Phone: [phone]
Fix.- 828.252,4618
Lab Project Number: 92124440
Client Project I0: Cleveland YuL'aka
Project Sample Number: 92124440-002 Date Collected: 07/25/06 08:15
Matrix: Soil Date Received: 08/02/06 10:45
Parameters .Results Units Report Limit Analyzed By CAS No. Qual Re9Lmt
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 17.2 V 08/D2/06 17:58 TNM
GC Volatiles
GAS. Soil
Gasoline
4-Bromofluorobenzene (S)
Date; 08/11/06
Ashev' CertifiS�a&.IUB
NC Wastewater
40
NC Drinking Water'
37712
SC
99030
FL NELAP
E87648
Method: EPA 8015
NO Ong/kg 7.2 08/07/06 20:14 DHW
90 % 08/07/06 20:14 DHW 460-00-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Paco Analytical Services, Inc.
1� AI: L'OyA
Page: 2 of 8
Chart Certifi n IN
NO Wastewater 12
NC Drinking Water S7706
SC 99006
FL NELAP E87627
bd WdT0:b0 900E 9T '6nd 80SF9SS6T6: 'ON Xdd saOlnJag 121uawu0,A1nu3 10310dd: WONJ

_ . ace Analytical
www.pacelabs.com
Lab Sample No: 927261719
Cl-ient Sample ID: APC1260 CL
Pace Analytical Services, Inc.
9800 ICincey Avenue, Suite 100
Pluntersville, NC 28078
Phone: [phone]
Far:704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
AyhavIlle, NC 28804
Mono: 828.254.7776 .
Pax: 628.252.4618
Lab Project Number: 92124440
Client Project Iu: Cleveland Yutaka
Project Sample Number: 92124440.003 Date Collected. 07/25/06 15:25
Matrix: Soil Date Received: 08/02/06 10:45
Parameters Results Units Report Limit _ Analyzed By CAS No, Qual Re2Lmt
Wet Chemistry
Percent Moisture Method: X Moisture
Percent Moisture 34.6 . % 08/02/06 17:59 TNM
GC Semivolatiles
TPH in Soil by 3545/8015
D'lesel Fuel
n-Pentacosane (S)
Date Extracted
Date: 08/11/05
A ±eville ►tific• 'nn Ift
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
Prep/Method: EPA 3545 / EPA 8015
No mg/kg 7.6
57 X
08/08/06
08/10/06-13:38 KBS 68334-30.5
08/10/06 13:38 KBS 629.99.2
08/08/06
REPORT OF LABORATORY ANALYSIS
This *report sliall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ineiacC ,
Page: 3 of 8
CharlotteCILtIftioatiQLM
NC Wastewater 12
NC Drinking Water 3770B
Sc 99006
FL NELAP E87627
Sd WdT0:vo 900z 9T -6nd 80Sz9SSST6: 'ON XHd saoln, % i21uawueulnu3 1OEIiO'ld: W06A

aceAnalytical
www.pacelabs.com
PARAMETER FOOTNOTES
Paco Analytical Services, Inc.
9800 Kincoy Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax, 704.875.9091
Pace Analytical Services, Inc.
2225 Riversido Drive
Asheville, NC 28804
Phone: 828.254.717E
Fax: [phone]
Lab Project Number: 92124440
Client Project ID: Cleveland Yutaka
Method 9071E modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended iineediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
Ill Surrogate standards were not recovered due to sample dilution.
Date; 08/11/06 Page: a of 8
Ast ille Ge fica-- DLs REPORT OP LABORATORY ANALYSIS NG Wastewaterratio 1 IU,4
NG Wastewater 40 This report shall not qe reproduced, except in full, NG Drinking Water 37706
NG Drinking Wator 37712 without the written consent of Paco Analytical Services, Inr. sC 99006
SG 99030 a %� FL NELAP E87627
FL NELAP E87648 <``', �`•
9d Wd1;0:b0 900E 9T '6nd 80SE9SS6T6: 'ON Xtid s03in. DS 121uawu0.u1nu3 10910Nd: WONA

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kinney Avenue, Suite 100 2225 Riverside- Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical o Phone: [phone] Phone: [phone]
Fax [phone] Fax. [phone]
www.pace►ahs.coin QUALITY CONTROL DATA
Lab Project Number: 92124440
Client Project ID: Cleveland Yutaka
QC Batch: 163980 Analysis Method: EPA 8015
QC Batch Method: EPA 3545 Analysis Description: TPH in Soil by 3545/8015
Associated Lab Samples: 927261693 927261719
METHOD BLANK: 927269159
Associated Lab Samples: 927261693 927261719
Blank Reporting
Parameter Units Result Limit Footnotes
Diesel Fuel mg/kg ND 5.0
n-Pentacosane (S) X 90
LABORATORY CONTROL SAMPLE: 927269167
spike LCS LCS
Parameter Units Conc. Result 9 Rec Footnotes
Diesel Fuel mg/kg 165.70 149.0 89
n-Pentacosane (S) 123
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 927269176 927269183
927267419 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result X Rec X Rec RPD Footnotes
Diesel Fuel mg/kg 3.496 179.80 134.5 132.8 73 72 1
n-Pentacosane (S) 101 103
page: 5 of a
Date: 08/11/96
Asheville C re tifica n Ins REPORT OF LABORATORY ANALYSIS _ Charlotte Ce ' 'c:ation.l >S
NC Wastewater 12
NC Wastewater 40
This report shall no( be reproduced, except in full, NC Drinking Water 37706
NC Drinking Water 37712 wittwuttile written consent of Paco Analytical Services, Inc. SC 99006
SC 99030 wn �x ^�«hFL NELAP E87627
FL NELAP E87648 --- -- — — - - -
Zd WdTO:b0 900E 91 -,6nti 80SESISS616: 'ON Xtid saO'AaaS I21-uawuOui6ud 103-LONd: WOdd

Pace Analytical services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NO 28078
Analytical © Phune: 704.875.909
hux: 704.875.9091
www.pacelabs.com QUALITY CONTROL DATA
Pace Ana►yncei aervjvuas, mu.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92124440
Client Project ID: Cleveland Yutaka
QC Batch: 164298 Analysis Method: EPA 8015
OC Batch Method: EPA B015 Analysis Description: GAS, Soil
Associated Lab Samples: 927261701
METHOD BLANK: 927280834
Associated Lab Samples: 927261701
Blank Reporting
Parameter Units Result Limit Footnotes
Gasoline mg/kg NO 6.0
4-Bromofluorobenzene (S) 9 72
LABORATORY CONTROL SAMPLE: 927280842
Spike LCS LCS
Parameter Units Conc, Result X Rec Footnotes
Gasoline mg/kg 31.25 45.34 145
4-Bromofluorobenzene (S) 71
SAMPLE DUPLICATE: 927280867
Parameter Units
Gasoline mg/kg
4-Bromofluorobenzene (S) X
Date: 08/11/06
927259911 OUP
Result Result RPD Footnotes
NO NO NC
112 82
shevigeC_ertifi tion.Qa REPORT OF LABORATORY ANALYSIS
NG Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical SBrvices, Inc.
$13 99030
FL NELAP E87048 `v
ne�ac
Page: 6 of e
QL01lotte C.Lrfificatlon IDs
NC Wastewater 12
NC Drinking Water 37706
gC 99006
I-L NELAP E87627
8d WdZ0:b0 900e 91 -6nd BOSE9996T6: 'ON XUA S20TAU2S 12TUMUOUtnU3 1031ONd: WONA

Pace Analytical Services, Inc.
9800 Kincey Avenue, Su to 100
Hunlensville, NO 28078
Analytical Phone, 704.875.909
Fax.' 704.875.9091
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside- Drive
Asheville, NO 28804
Phone; 828,254.7176
Fax, 828•P,52.4h18
Lab Project Number: 92124440
Client Project I0: Cleveland Yutaka
QC Batch: 163899 Analysis Method:rX Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated Lab Samples: 927261693 927261701 927261119
SAMPLE DUPLICATE: 927265702
927264697 DUP
Parameter Units Result Result RPD Footnotes
Percent Moisture z 24.80 24,80 0
Bate; 05/11/06
AshGuLe Ge firatiQ( 1Ds
NC Wastewater 40
NC Drinking Water 37712
SC . 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This repoit shalt not be reproduced, except in full,
without the written consent of Paco Analytical Services, Inc.
�N nrcuyn
4i
Page: 7 of 8
Qharlo rtillcdt{on IDS
NC Wastewater - 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627
6d WdZO:b0 900Z 9Z '6n
d 80SZ9SS616 : 'ON XUA s ao ; n,la8 l uluaUJUOU T nu8 10=6d : W06A

ace Analytical O'
www pacoiabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
,9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone; 704.875.9092
Fax., 704.875.9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,054.7176
Fix. 828.252.4618
Lab Project Number:'92124440
Client Project ID: Cleveland Yutaka
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
NU Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MUL Adjusted Method Detection Limit
RPU Relative Percent Difference
(S) Surrogate
Date: 06/11/06
AS ville, rtificd L ID.S
NC Wastewater 40
NC Drinking Water 37712
5C 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ine.
,a �4COgG
°�relc �.
Page: 8 of 8
G • riotte rtlficati�[l IDS
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87527
8Td WdEO:00 900E 9T -6n
ti 80Si?9SSGT6: 'ON Xdd saO1AUag tE;UaWUOJtnUd i33iONd: WOHJ

/ e2eAnd"car
Section A
itequlnd CYmRi lilofi:
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chartwf-CuADdy is a LEGAL DOCUMENT. All r0evard ftelds must De=mpW1ed —rat*-
SOCHon B Section C P d
itewrhod pmisd Irdanvfnn: Irtvdw lnromtadon:
Carps. PROTECT Er>r=mwr t Sarvlcas
Report To: DawW Ha tdw Abwdkirr David HardisW
- NPDES i GROUNDWATER - DRINKW-%YAER
r UST r RCS` uniER_
Addlem: 7104 Sandy Ptws Or
CopyTo: CompeM Name
PROTECT Envirorlmerllal Services
rowgsIlle• NCn"-ss
- 7104 SancjV Pines Or Youngsville, KC 27596
r GA r- 1- IN ,- Mr 441C
�n0i1T« air.-�r�is�r rotz�i:�5
PundLaseorda"O.: Pam
r DH r SC - vw r oTHER-V--
It d Me
Phaa: 5T1o74-M
Fes: 819-M&M
PR�iedNw D>�IdYut&" P— M
R"wetodDoDaUfrAT
PrgeetNimbar_ PaerPmfileg: i a„
SeCtion D q@q*ed Crnotlffxmw6w vceew .
MnTqjcc
f COLLECTED
Fvasma6,vs
SAMPLE ID „:.�,
o
° a
Mrs
bile Chai7dK pBC Dale onaa
K
~
m W J D
•
'1!'
S tArZ.�Dif% WW
q C01906'IE'JfARr �OOu! M.
D
p
Sa gw. IDS wisT 8E UreQue
aD
f
�+
u
C `o PS Mepd
5 tan
r
DATE TOM DATE TIME
i
z`
•
i
'
A
P
C
1
i
6
D
1
01
C I
I
I
SL I
G Ire"
77LSM 8:16 I
A
P
C
1121.6
0
=
G
C i
SL
G7125.Va
B;10
7R51o6 8:15
A
P
C
1
2
5
1.
0
1
C
L
?
SL f G 7J25M
1 1520
7725M
18:25
!
l-
j
1
I
�
.
I
i
t
QAY9" F Co11rn1TIDUS
AditoW Cair ikwi ,
O
3
�11
O
--I
m
n
—1
ITI
c
7
0
7
a
tD
C+
W
N
r0
7
Q
f8
N
lD
F-�
lD
to
LA
9)
19
O
e-Fi*ALLQ020rev_3,3?h1aeO5Y 22JUP2005

Appendix 2
Non -Hazardous Waste Manifests

Environmental Soils Inc.
PO Box 295 - Lattimore, NC 28089
Phone [phone] - Fax [phone]
Nc . in- Hazardous Waste Manifest # 22361
Date Load Number
(numbered sequentially as trucks are dispatched)
EAWIRONMENT4L CONSULT4NT-
Contact:
Fax:
GENEX4TOR_-
Address: County: 0
Contact: 7 7 -
Al
Phone:
WWSTE ORIGLVATIONPOINT- Complete Address:
Phone:
Class &Type of Contaminate in soil k
SOURCE'OF CONT4MINATION. (ex. UST or other source)
GENERATORS CERTIFICWTION OF W,4STE CONSTITUENTS. In lieu ofsubmitting analytical data (methods
8240 and8270) ver�ing that the waste in question does not contain organic constituents other than those wbicb would
normally appear in analysis of virgin petroleum product residue, Iam submitting Certificate of
P tt rt�i Waste
Constituents. Icert� that Iamfamiliar with the source of contamination of the soil and furtber cert� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
TR,4WSPORTER: t :a
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:,,
Date:
TRUCK#: 7-
rT-AG #: VOLUME:
TRUCK DRIVER SIGNATURE:;
DATE:
DESTIN,4710N.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certifythat the carrier has delivered the materials described above to this facility, and I hereby accept this material
for,treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:
if
Signature:
Date:
Company Name
Title:
Date:
White/Facility Canary/Invoice.. .-Pink/Carrier -Goldenrod/Ge'nerator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
r Non -Hazardous Waste Manifest # 2 2 3 6 2
Date ' ' .' ;.;. Load Number
_(numbered sequentially as trucks are dispatched)
ENVIRONMENT4L CONSULTANT -
Contact: f _ �, a Phone: Fax: a .
GENERf4TOR:
Address: <_ f s` = f a ,t.. _ !:4- - - County:
Contact: Phone:
W-4STE ORIGI VATIONPOINT Complete Address: . 2.stj
Class &Type of Contaminate in soil 3`
SOURCE OF CONT4MLM4TION.• (ex. UST or other source)
I
GENER4TORS CERTIFIC,47ION OF W-4STE CONSTITUENTS: In lieu of submitting analytical data methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Certificate of Waste
Constituents. I certify that am familiar with the source of contamination of the soil and further certio the source, to
the best of my knowledge, contains no contaminants other than that listed above.
_ . S _r-Generators Signature:� ���_
`- Date:_
-
'.1
TX 4NSPORTER:
Contact: _ - . , �.., Phone:
r'
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. =' _
r I i
Carrier Signature: _ , Date:
�•�.� <: �_�
-
TRUCK #: TAG #: VOLUME:
TRUCK DRIVER SIGNATURE: _ _r DATE:
DEST VATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038 -
I certify that the carrier has delivered the materials described above to this facility, and.I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:
Signature: ;V ' j
Company Name
Date:
Date:
Title: f
,,White/Facility.,....,Canary/Invoice Pink/Carrier , Goldenrod/Generator.

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 22363
Date / ; -' `' = Load Number
(numbered sequentially as trucks are dispatched)
ENiIIRONENT4L CONSULT4NT
Contact:a,' i iJ i— Phone:
GENERfITOR:
Address:
Contact: i _
WASTE ORIGIN,4TIONP0INT Complete Address
Fax:
L r County: _
w
;Phone:
r
Class &Type of Contaminate in soil —i
SOURCE OF CONT4MINIITION.• (ex. UST or other source)
GENER,4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (metbods
8240 and 8270) ver fving that the waste in question does not contain organic constituents other than those wbicb would
normally appear in analysis of virgin petroleum product residue, I am submitting this Cert yicate of Waste
Constituents. I certio that am familiar with the source of contamination of the soil and furtber certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators, S,igrrature: `.. „ : ' .. _ _
- .-. Date:
TX4NSPORTER:
Contact:. i r, i' Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date: f r'�? (x`.
TRUCK #: TAG #:
VOLUME: •'-
TRUCK DRIVER SIGNATURE: -t ;� DATEf;, `-l�'f`
..< {
f
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that tie carrier has. delivered the materials described above to this facility, and I hereby accept this material
for treatment 'and/or'disp.os
Al_ in a manner that has been authorized by the Sate of North Carolina. .
Facility Signature:f =
D
1 i ate: i
f.
Signature:. c:! , Date:
an �f
Com N(~~
Company Title::
White/Facility.. , Canary/Invoice - Pink/Carrier Goldenrod/Generator.

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
-- Non -Hazardous Waste Manifest # 2 2 3 6 4
�• J 3
Date
1 ei
ENVIRONMENT4L CONSULT4NT 4-'Y w'
Contact: I
Load Number
(numbered sequentially as trucks are _dispatched)
Phone:
Fax:
GENERJTOR:
Address: County: y'y
Contact: i- Phone:
WASTE ORIG1JVATIONPOINT Complete Address: ,' _'i • 1 �
V
Class &Type of Contaminate in soil` = ";
SOURCE OF CONT4MTVATION.• (ex. UST or other source)
GENERJTORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certyicate of Waste
Constituents. I cert f thatl am familiar with the source of contamination of the soil and further certio the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
TR,4NSPORTEJ?:
Contact:
Phone:
As the carrier, I certify that the materials described abovebeing shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: " v - - Date:
TRUCK #: - j I _� TAG #: VOLUME:
TRUCK DRIVER SIGNATURE: E _ DATE: DESTLVATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials .described above to this facility, and I hereby accept this material
for treatment and/or disposal in a' manner that has been authorized by the Sate of North Carolina. f'
Facility Signature: �` - Date:
Signature: D
ate:
Company Name - Title:
Canary/Invoice... Pink/Carrier Goldenrod/Generator:

Appendix 1
Non -Hazardous Waste Manifests

CLEVELAND COUNTY
HEALTH DEPARTMENT1`1�OE OFFICE
MAY 2 5 211)0,',
May 23, 2006
DATER QUA- 1TY SECT ION
Wes Bell
Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Dear Mr. Bell:
On May 2, 2006 Kevin Whetstine, Environmental Health Specialist and Shea Webster,
Environmental Health Program Specialist from the Cleveland County Health Department
made a visit to the property adjacent to 124 Laren Road. The nature of the complaint was
regarding corrugated pipe(s) discharging into a creek at points marked by yellow stakes
driven into the opposite side of creek bank. After evaluation of the creek, no pipe(s) were
found emptying into the creek. Mr. Shawn McNeilly was present, and advised us that he
had installed drainage pipes to drain surface water standing in the low area of his
property. However, no pipe(s) were found going into the creek.
On May 3, 2006 Marty Allen, Environmental Health Director, and Shea Webster made
another visit to 124 Laren Road. Efforts again were made to locate any pipe(s)
discharging into the creek. No malfunction of the septic system was found, and again no
pipe(s) were detected going into the creek.
On May 11, 2006 Marry Allen and Shea Webster met with Mr. Shawn McNeilly, again,
at 124 Laren Road. More evaluation was done, and no pipe(s) were found at that time.
In summary, no illegal activity was found relating to the septic system at 124 Laren
Road. If you have any questions concerning this matter, please feel free to contact the
Cleveland County Health Department at [phone].
Sinc rely,
Marty Allen, R.S., L.S.S.
Shea Webster, R.S.
cc: Shawn McNeilly „yfh,B.-,t.0 U,
315 E. Grover St., Shelby, NC 28150 3,998---(704)-484-5100 - Fax [phone]

6-Q-VdCe'J Co
MEMORANDUM
To:
Through:
From:
Subject:
Background
Division of Water Quality
Biological Assessment Unit
February 8, 2006
Jimmie Overton
Trish Finn MacPherson _�F_
URCESiPL _
FEB 1 3 2006
p^ ,
Eric Fleek '
Biological Monitoring of Potts Creek (BRD Subbasin 05). Cinderella Mills
Tetrachloroethylene Release Study, July 2005 (BAU Memo B-060208).
Staff of the Mooresville Regional Office requested that a macroinvertebrate sample be conducted on Potts
Creek. Potts Creek at SR 1001 is downstream of the former Cinderella Mills (Figure 1) site where a recent
release of Tetrachloroethylene (also know as PERC, PCE, Perch loroethyl ene, and Tetrachloroethene;
ATSDR 1997) was detected. Tetrachloroethylene evaporates readily into the air and microorganisms also
break down some portions of this chemical upon contact with soil or groundwater (ATSDR 1997). The
Tetrachloroethylene was released into several tributaries of Potts Creek and this sample was conducted in
order to determine if there were any deleterious effects on Potts Creek. There have been no previous
biological samples on Potts Creek.
Site Description
Potts Creek, SIR 1001. Cleveland County.
This reach of Potts Creek is approximately six meters in
width and has a drainage area of 9.3 square miles. Most of
this catchment is comprised of scattered residential and
light commercial areas. This catchment also drains portions
of the western edge of the town of Kings Mountain and the
US 74 corridor. Substrate along this reach was a fairly
unembedded mix of boulder (10%), rubble (30%), gravel
(20%), sand (30%), and bedrock (10%). The most notable
habitat problem observed was the lack of well -developed
pool habitat. Conductivity was 70.3 µmhos/cm and the
.habitat received a score of 78.

Figure 1. Potts Creek, Cinderella Mills Tetrachloroethylene Release
-qti Axi Rrnarl n-r ('lAVAlanrl C'ni into

Methods
Benthic macroinvertebrates for this study were collected using the Division of Water Quality's EPT Method.
This collection method is comprised of one leaf -pack sample, one kick net sample, and one sweep net
sample. In addition, each member of the three -person team conducts visual collections. All organisms are
picked in the field.
The purpose of these collections is to inventory the aquatic EPT fauna and produce an indication of the
relative abundance for each taxon. Organisms are classified as Rare (1-2 specimens, denoted by "R" on
taxa tables), Common (3-9 specimens, "C"), or Abundant (>10 specimens, "A").
Several data -analysis summaries (metrics) can be produced from benthos samples to detect water quality
problems. These metrics are based on the fact that unstressed streams and rivers have many invertebrate
taxa and are dominated by intolerant species. Conversely, polluted streams have fewer numbers of
invertebrate taxa and are dominated by tolerant species. The diversity of the invertebrate fauna is evaluated
using EPT taxa richness counts; the tolerance of the stream community is evaluated using a biotic index.
Bioclassifications for EPT samples are based on the total diversity of EPT present in a sample. EPT
abundance (EPT N) calculations also are used to help examine between -site differences in water quality.
Criteria for the Piedmont ecoregion were used.
An assessment of the stream habitat and of the landuse within the catchment is also completed at each
stream sampled. More specifically, these habitat evaluations assess the quality and quantity of instream
habitat, the quality and quantity of the stream's riparian zone, and also evaluate detrimental impacts on
stream habitat such as bank erosion and substrate embeddedness. Habitat evaluations result in a score
between 1 and 100.
Field measurements were taken at the time of sampling such as water temperature, dissolved oxygen,
specific conductance, and pH using an YSI 85 meter and an Accumet pH meter.
Results and Discussion
Table 1 presents the summaries of the biological, physical, and chemical data for the Potts Creek study site.
These data summaries are not used in assigning the bioclassifications, only EPT taxa richness.
Table 1. PottsCreek (BRD 05) Study Site: Taxa richness (by group), summary
parameters and station description, July2005.
Method
EPT
Site
Potts Creek, SR 1001
BIOLOGY
Parameter:
Ephemero tera
11
Plecoptera
3
Trichoptera
12
EPT Richness
26
EPT Biotic Index
4.4
EPT Abundance
121
HABITAT
Width (m)
6
Depth:
Average (m)
0.3
Maximum m
0.6
Canopy %
90
Aufwuchs
No
3

Table 1. PottsCreek (BRD 05) Study Site: Taxa richness (by group), summary
parameters and station description, July 2005—Continued.
Bank Erosion
Moderate
Drainage Area mi
9.3
Substrate %:
Boulder
10
Rubble
30
Gravel
20
Sand
30
Silt
10
Bedrock
0
CHEMISTRY
Field Chemistry:
Temperature C
21.2
Specific Conductance mhos/cm
70
pH
6.6
Habitat Score
78
Bioclassification
Good
Discussion
Potts Creek, SR 1001. The July 14, 2005 EPT sample resulted in an EPT taxa richness of 26, an EPTBI of
4.4, and a Good bioclassification. Based on benthic data, there seem to be no adverse effects on Potts
Creek as a result of the PCE release. Pollution intolerant EPT taxa present from this collection included the
mayflies Acentrella, the stonefly Acroneuria abnormis, and the caddisflies Lepidostoma, Chimarra,
Rhyacophila torva, and R. carolina. In addition, the long-lived, pollution intolerant stonefly Acroneuria
abnormis was common at this location. This taxon requires between two and three years to complete larval
development and its collection suggests generally favorable, long-term water quality at this location.
Conclusions
In 2005, the EPT sample resulted in a Good bioclassification with several pollution intolerant taxa present. Ir
addition, one long-lived, pollution intolerant taxon (the stonefly Acroneuria abnormis) was common at this
location. Based on benthic data, there seem to be no measured adverse effects on Potts Creek as a result
of the Tetrachloroethylene release from Cinderella Mills. This conclusion supports the environmental toxicity
data of this chemical (ATSDR, 1997).
C P� :a orates
0

References
Agency for Toxic Substances and Disease Registry (ATSDR). 1997. Managing Hazardous Materials
Incidents. Volume III — Medical Management Guidelines for Acute Chemical Exposures: Tetrachloroethylene
PERC . Atlanta, GA: U.S. Department of Health and Human Services, Public Health Service.

Appendix 1. BRD 05—Potts Creek; Cinderella Mills Tetrachloroethylene Release Study. July, 2005. A=Abundant,
C=Common, R=Rare. All sites collected with EPT Methodology.
Taxon
POTTS CR
7/14/2005
SR 1001
EPHEMEROPTERA
ACENTRELLA SPP C
PLAUDITUS DUBIUS GP A
BAETIS FLAVISTRIGA C
BAETIS INTERCALARIS R
BAETIS PLUTO A
ISONYCHIA SPP A
PROCLOEON SPP R
STENONEMA MODESTUM A
SERRATELLA DEFICIENS R
STENACRON PALLIDUM C
TRICORYTHODES SPP C
PLECOPTERA
ACRONEURIA ABNORMIS C
LEUCTRA SPP R
PERLESTA SPP A
TRICHOPTERA
CHEUMATOPSYCHE SPP A
CHIMARRA SPP R
DOLOPHILODES SPP A
HYDROPSYCHE BETTENI A
LEPIDOSTOMA SPP R
NEOPHYLAX OLIGIUS C
POLYCENTROPUS SPP R
RHYACOPHILA CAROLINA R
RHYACOPHILA FUSCULA R
RHYACOPHILA TORVA R
SYMPHITOPSYCHE SPARNA C
TRIAENODES IGNITUS A

NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Land Resources
Land Quality Section
James D. Simons, P.G., P.E.
Director and State Geologist
December 11, 2006
Mr. Dennis Wells
Water Resources Director
City of Kings Mountain
Post Office -Box 429
Kings Mountain, North Carolina 28086
RE: Kings Mountain City Lake Dam
State I.D. CLEVE-013
Dear Mr. Wells:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
r;5JUJI Ur t-MU ttk uL94Cc"
t 'J ^; v
i
J& as
pt#W"'E14T OF ENVIRGNM_' ! '
This is to acknowledge receipt on January 11, 2006 of as -repaired drawings and engineer's
certification for the subject dam. The dam will be inspected by staff from the Land Quality
Section Mooresville Regional Office. We endeavor to respond within 60 days of receipt.
Please contact Mr. Zahid Kahn, Regional Engineer, Mr. Clinton Cook, PE, Assistant Regional
Engineer, or Mr. Scott Harrell at telephone number [phone]; or a meinber of the Dam
Safety Program staff in the Central Office at telephone number [phone] if you have
questions concerning this matter.
Sincerely,
Maxwell R. Fowler, PE AtW E } " C DURCES
State Dam Safety Engineer V4O0ti E IAL OFFICE
cc: Mr. J. C. Bumgarner, PE, President, Pinnacle Engineers v
Mr. D. Rex Gleason, PE, Surface Water Protection Regional Supervisor JAN 17 2006
Mr. Zahid Kahn, Regional Engineer ;
Mr. Clinton Cook, PE, Assistant Regional Engineer
1612 Mail Service Center, Raleigh, North Carolina 27699-1612 •919-733-4574/ FAX: [phone]
512 North- Salisbury Street, Raleigh, North Carolina, 27604
An Equal Opportunity 1 Affirmative. Action Employer — 50% Recycled 110% Post Consumer Paper

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Land Resources
Land Quality Section
James D. Simons, P.O., P.E.
Director and State Geologist
November 12, 2005
Mr. Michael P. Tonelius
Plant Manager
Kings Mountain Mining, LLC
Post Office Box 729
Kings Mountain, North Carolina 28086
RE: Proposed Dam
Cleveland County
Dear Mr. Tonelius:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
, lA e�-LMD ftSCf€J`r u
LWQUALITY SECTION
v� €e '
ADV 5 2605
This is to acknowledge receipt of your application dated November 7, 2005 for the jurisdictional
determination of the proposed dam. The application was received in our office on November 9, 2005. A
copy of the submittal has been sent to the Mooresville Regional Office (MRO) for review and a site visit.
A staff member from MRO should contact you within a few days.
Applications for jurisdictional determination of a dam will be reviewed by this office in the order they are
received except that existing high hazard potential dams will be prioritized. We endeavor to respond to
applications within 60 days of receipt of the application.
Please contact Mr. Zahid Kahn, Regional Engineer, or Mr. Clinton Cook, PE, Assistant Regional
Engineer at telephone number [phone]; or a member of the Dam Safety Program staff in the
Central Office at telephone number [phone] if you have questions concerning this matter.
Sincerely,
A; r��r.ol1PCES
.., ; pt"I;ICE
Maxwell R. Fowler, PE
State Dam Safety Engineer
cc: 0—Id-r-D. Rex Gleason, PE, Surface Water Protection Regional Supervisor
Mr. Zahid Kahn, Regional Engineer
Mr. Clinton Cook, PE, Assistant Regional Engineer
1612 Mail Service Center, Raleigh, North Carolina 27699-1612 •919-733-4574 / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina, 27604
An Equal Opportunity 1 Affirmative Action Employer - 50% Recycled 110% Post Consumer Paper

SEP-28-2005 WED 11:04 AM ESA 1
FAX NO, 502 499 6395 P. 01
qP
FAX Transmission
1So0 )Envoy Circle web Site www.ESAI.coln
Suite 1801 Telephone Number [phone]
Louisville, Kentucky 44299 FAX Nuunber (5b2) 499-6395
bate:
September 28, 2005
To;
Open Records f FOIA Officer
Phone:
[phone]
Company:
NCUFNR - ille Regional Office
Fax Number:
8 )-29 -
From
eli�s:�-We
"�Veo
E-Mail:
mweisbard
Prflject #:
SNC2-0028 -
to Vollow.
Parsuant to the State of North Carolina's Pu lie Records Act, please send copies of any records
the Department of Environmental and Natura Resources has on file with the ground water
protection, superfund, UST, _w�#:e ollntica.0 fgc nd hazardous waste divisions concerni"
r idly �RCt1i[,iEW
permits or violations and/or environmental repo s or other information about envira6`5n� e�ppia1'ryry�}}� pp' ®p���+ //fi�ee 33 //�� ��qq
��® �W�{;l ii!^ll_ IfiLt7lJ�J�H)✓v'1.
conditions for the following property (please call fore incurring any expens, ):
r 13! OC)RESViLL iCNAL- ONCE
Site Owner: �:,•,., :. , ' =`i
Prabhuji Investunents, LLC
Site Name; OCT 0 3 200a
Travelodgej�
%,f-7fN--8
ddress:
Fork Road
ings mountain, Cleveland County, NC 28086
'Please reference ESA P0-Protect Nun
1
C2-0028 when Tr�Ea
Meuse copy arnad forivard to offices that regralate f-he f `oll0wilig, topical areas:
4iM, Groundwater Quality, Air Quality, Solid Waste and Iazardous
Waste/Substances, ' n erground Storage Tanks, and Environmental Response
If you have any questions, please contact the sender at the telephone number listed above.
Thank You.
p� [
D
SEP 2 8 2005 rd
i
WATER QUALITY SECTION
ASHEVILLE REGIONAL CF---J10E I
Revised 8/Z2/05

Ava
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Land Resources
Land Quality Section
James D. Simons, P.G., P.E.
Director and State Geologist
September 19, 2005
Mr. Ron Chidester
126 Cedar Lake Farm Road
Cherryville, North Carolina 28021
RE: Cedar Lake Dam
Cleveland County
CLEVE-002
Dear Mr. Chidester:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
r rW� CiF= 61 •' �',
... 4;,r_1N OF f��ft
-. Jx
This is to acknowledge receipt of your application for repair of the subject dam dated August 9,
2005 concerning the subject dam. The application was received in our office on September 14,
2005. Applications will be reviewed by this office in the order they are received except that
existing high hazard potential dams will be prioritized. We endeavor to respond to applications
within 60 days of receipt of the application.
Please contact Mr. Clinton Cook, PE or Mr. Scott Harrell, PE in our Mooresville Regional Office
at telephone number [phone]; or Mr. Max Fowler, PE, State Dam Safety Engineer or me
at telephone number [phone] if you have questions concerning this matter.
Sincerely,
William H. Denton, IV, EIT
Asst. State Dam Safety Engineer
cc: Mr. Johnny H. Denton, PE
Mr. Zahid Khan, PE, Regional Engineer
1612 Mail Service Center, Raleigh, North Carolina 27699-1612 -919-733-4574! FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina, 27604
An Equal Opportunity 1 Affirmative Action Employer— 50% Recycled 110% Post Consumer Paper

EMERGENCY RESPONSE&TRAINING SOLUTIONS
For those wbo demand results
September 2, 2005
North Carolina Department of Environmental and Natural Resources
Mooresville Regional Office
610 East Center Ave
Mooresville, NC. 28115
RE: Corrective Action Final Report
USF Rolland
Diesel Fuel Spill
1818 W. Dixon Blvd.
Shelby, NC
Cleveland County
ERTS Project NO.0825200SHE
Dear Sirs:
eJii ,'iia•r-j
0 NATURAL RE -SOURCES '1
S its r iQL CFF1cz
QUAUTY SHIM
`1
The following serves as the final report detailing the emergency response and corrective actions
taken in response to the incident that occurred on August 25, 2005 at the above referenced
location.
Executive Summary
Incident Background:
On August 25, 2005, a tractor trailer operating at the above referenced location had its saddle
tank punctured after crossing median and running up a bank thru a fence, releasing 100 gallons
of diesel fuel.
Emergency Response:
On August 25, 2005, Shelby Fire Department arrived on scene and assisted EMS with an injury
to the passenger car driver. Soon afterward they checked the damage to the USF Holland tractor -
trailer. One saddle tank was empty from a large hole ripped in it. Shelby Fire Department then
proceeded to remove cross over line from other tank to prevent drainage of second saddle tank.
Wrecker service was called to remove USF Holland truck out of pasture. USF Holland retained
3201 Enterprise Parkway, Suite 330 • Beachwood, Ohio 44122
Tel. [phone] • Fax [phone]

Emergency Response and Training Solutions (ERTS) to manage and oversee environmental
operations. ERTS dispatched Stat, Inc. to the scene to perform environmental restoration.
Regulatory Notifications:
Pursuant to North Carolina State regulations, ERTS notified the North Carolina Department of
Environment and Natural Resources. The NC Department of Environment and Natural
Resources issued 05-0824-0175 as a confirmation number.
Field Activities
Corrective Action:
On August 25, 2005, Stat personnel arrived onsite. The site was secured. Absorbent material
was spread on the shoulder of the road. The spent absorbent material was swept up and
containerized for transportation and disposal. The pasture that was impacted by diesel fuel was
excavated and containerized for transportation and disposal. All remediation activities were
completed that day. All backfill that was used at site was topsoil. This site is secure.
Waste Disposal:
On August 25, 2005 all spent absorbents and contaminated soils were transported to, and
disposed of at, Soil Technologies located in Shelby, NC. Attached are the non -hazardous waste
manifests (Appendix 1).
Conclusions and Recommendations
No evidence was found that suggests any significant environmental impact remains on the site
following corrective action. ERTS recommends that the incident be closed and that no further
assessment is needed.
ERTS and Calhoun Transport Services, Inc. appreciate your assistance in this matter. If you have
any questions regarding this project, please do not hesitate to contact me at [phone].
Respectfully,
Emergency Response & Training Sol!
Brian Lee Cobb
Project Manager
CC: Susan Camara-USF Rolland

APPENDIX 1
NON -HAZARDOUS WASTE 1VIANIFEST

Sir! a: t r-,. :
p ®s}un®eue a s a Xa� U � uoi aa9srp afr o �1 out ` arf c �c art al
,;�l�-- . .,,�.,��,I �,..--:.r-:­" ,-.i, �pi�� .�.- ,­�,-.�-.,,i­-7� -I,r-4,I .�A� A'��.� � , ­,i-.,
fso� ui: Waryev►�c►s hua �o- sous daote o
_'..F1,­: ­t �-t_;.'.,�, l."-�."-��34.o1,1,,.­_..."-,!,.`I-..­""_­`-.,.!_;i:­,, �-,11v,.1­:1,-,�;,-.4.,,_,����i1­�,1 tx.-.iZ .�,.'-:t.h,1�.f-��R�I��;�I�;­,,I"'n,
A.�.It.
3�f1�3�! ;3Wfoa %.- sa_ r... W _u! `sai9' ftf.'al-
S
It
3 5 KII
sti r erpt ," 1
T 1 1
f � �N e
h
it - •' ^
,
"t4 pN,dad p*ads
s lr :�J £ i t«a f .i k :
i _
+ 7 :�4 7 k'{ f v vkt f'�" �fF dry F i7, 4 r-Jkl [ x ,.2 1,7) t x s
I r 3 7 r { Y r. r, { r;J 1'2 t T,- �r 'r.1 ' 3 !. .
' f I - "} 2 Z4 , �' :Llt_ t - ^/1 3} `� �� .ram-. aa.:1DHi:SUej
t , t _ t .. t t 1� .1 r� 1 Txi St1 3` 'Yx<f '(Sviq f t 3t .'w ;a a sf f,j dam, } ?rS ];;; °71
�a r x
,.
F ,. r,!
_ t ;� 'Circe _,z), I. ks2 F.ff �s i [l _ - -
I r it :+ f' c 5 - r r. 5
�{� v + :., 1� r 3 p t +�r4�%,''�z t � - z '�.F t. i:.,�u f{ -7 d p� , r -
_ w.a _l c� , w!° y r4mM k 7 LR� d��,�l����'����� ..7r � 3 �'� ; � � �
I j f irrf I '1 ex n s -r
as. a w 'ac�� �a_ s o d M G' �r
. t a ap��
�'yyC ,
' �] i �. �y�}. J i. d �k£�.41k+/�, C. 5�d'{... Y.+d�l�.g;y,'3),��F'I.Yr/a(l.�
�JriO 'a4 T` 1� } 5- 7'F7'�F }f F � �� iq ��H /►t� . f4 - g "Sys �y /�
s r € t , L -r:.. +SC%' a r1F r w F�1 Tiy,. v, .� .., rtt' i'a`� - [� ? Sr �
aye, wawacc�� ay //��y i .S! as�!7.
.. ..
4 {iY' - "t'Y8 -r us-.15. (.La 'Xci*ha;Y.t�ri { ,�h't.yl+,v�yYF lc#`f:�-f"-.%N�z°'f f ! ,6'ra.�-`.�'Y
y r' / U7 — "� r � : 4 5 ,.0 I rj .t r I ,� ztP `Y Y t?r'!J _ 1 - V'l � .A s , .
ax
r as 4 - I.._ �-" l
i z n ( r
. r
x } 2 r!'7 fw 'attrrj£r } x7yr Sim 1E StrP'ia�r t r
q + s. V
,it" 4$ ,. s rF r + ti .� "t;,dS.pd `S' -
j
Y" + 11 by 1'"+` `r cl'i4 r tc .7 . .
Y # n,-!' 1F4 Y S-1 - YF'
s:r i#tY ¢f'1 J #tt re r a t ar F1us st ,i+,.� �£✓ (y,r j° .
1F v a t 7'
3e i t M
r H F pJ,}x7 t [ a�u aooeauoo
e r t} r" 1!¢ x t% k
7
iI._1 1_ r
"It ,_,,,I.- .-.�1I.., f.�­ - I� b 1.i— .4--r .. .-.-4!.1.­I-.,�,�.L II�;,.-I,, .. I.I .-, --�I .r.'. -:L­ _ ,f, �L �l-. r.., .. I 1.;­- ,-N�',,..�:. ._. .. � ...t.i ..,,,,1� 4 I �,- .. -...,�:"� ' .- ."...-.., ,..I. �,, -.�.., .',.,, ..- . —.. .-. .� L,I, :� Ir, . .II.. 11 ,�.... .I,i .I,,:-..I.i ,I.. � ..� ,7- . ' �. .'. : -i,., _��I-. ,I.L',.. ,...- . : . I "�. .., .
:: F lj A f_ C 4 i r�. } art ltf i
'7-); Y ;1 r -t',)C N £ ) 1 t i .+}{Lets it y, -0 �-n y4 F2. {7 '.. kY
Yssaa a i
_ ...'� .J . C V ra+, f3. t1# i f7i�.:c _;;1 r''+
t �/
T 4 C
- .. , ' `4 v �ueN ao �.�aua
< h J f 5£
S-'�� Yi r {�{y{ F _ �, rls, L.,�.th 4 9:k f L
- - .<` Stl t.Y. t t .
,. j ., s, .,....;.�. ,. s:,, r
r z7 i
. w t ry �,v F i
. r r s - vz °b t �i S Cu t7- -
'' - '�.q �{Q.if,k 1 K i'�7 f ry i .� ^e ." z f A A3 I } NO
r,'
i i v„ dl r 3. - is `,-, r ,U -u L 7{'J L7 .I
aui- 4anf?opd tl P . ' f 1; x ft` �,` {� I� f 1 ' l�l �i 1 Y ur1o5e`t
a.rn� ��++�
1 s (�\ ( Ir �4� OW XJ "^0 is '�'I /`t� Y(i a J S �r� r� �y'� ! . � 7��,j
;. f 6 f x �} 3 ,j• t n f7 ; b S t i P� �'Cw' i3iT.i �lH•1atA.{ ,i
z` � �� � r f( 1o.:adi(1
�yyY:� > t.6hvn fi ,*. KyP 'Yfk4 F.x., y k v;:
��a
)
T I1S
7.
41
oN qr .
FT J t f .
t ,.f ,i`$ ?y�tjl <.t.I }=x r y .d£,� r t I .ty f .
t R itY ( 3
_ v 3 r t n [� (ro£ r. ;t� S a {_+t,, t F-34� s• �.' !{.4,�` S t '�+ p� 1 6 r,,-.
t9g8 4-v£t.bO:L) xe�/,fUjW. £ !i r 't y c r '- ,
{ 'x r , , 4 's f3 P 'x•re ld , I "r r { y , 1 .
, ><69999G 05<4 #pl %ajxaN ..
1. I ; r
d
96£Z'LLb{b01) a1�9oW/u�eW �`i¢ ; ``
:05�8Z�ui�o� � WQN `�gjaq& ► •
peon{ a. . 940 L�b6.. ssaappy:a;is.. ";h ,� a � t

r ,' ,.' f5 st *', Site Address.;947 Crowder f oal
' Shelby, North Carolina 28150
ti
''r IVfa�r�/�ilob�fe (7Q4)'477 2315
+i c� ,x ,, fVete/;td# h50*9�6669*1
k rs
y t f Qf`frce /Fax (704);434-5!884
t k rr 5 ! v % , l�'7,C you 3 s - - tj ; : J Y t
• h t 'V . it k i zU'�,1(i4r 1k fn ski zf ra t
C ..# i- ",1`t ,_11y ski y _ s s t ;NJ� --t I ur , F .:I r'
arP
IN
�� i 1 I 11-.. 5 PRf i Y '; . 3T.- i ! .
­74..t cv,�« itr, P ,5,. �7 l�f! A P^4 t� .dHw 7j tys,,, .. qC ; -rF
I, It' a+ f!, w , i r r
JR.
-.. _ "Wsy k f e,g Ceil P �. 3 St„ .r f `;7
S.T' 1�:ib,k��'tW rr tl t v r) t! kaVit rt Ck3.+T, yir., raii;c i.v] fi�zn c x ^sui t*i i t',Y fin: at.�r d r + lu tf �.y
. 2 cr - �3r,? ss�1 e t r,. a re vi c � 3 x t �R/
x : / i - _' %4 r,�s cy yr^L F, i- Y t a `., .1-0i t 1 ' +llll�
1 �' hY�G" 'k Y t.5 rNl Q i tX riS 7 i�i h�i� �"r i �j, N; tF t I t l 1 11 .j j Y. f
ype of Cor�rrrirl;�k,� t� fy�,ia3(PCiile}�
K t a L
.fir �°Yt�," "" ! T. t •� s Yk ! Ixt ; �t ai r rix s § z+ '
�asol�nI� 79t1`��If {, ,:'L��I yP�uet Line
_- ��Y�4
1 iXC Yi I ram+ t r rt Ii 1,'r` %j p t t r i t t i �N, n " -
,. r ' E'l IIgl. s'Sd 4'�x -. t t .rr 't q- r , t
sir Is �+, Ors ea - r i + a )tiler n yfi = f d }i th Kti Myn t : tt r ros §
e�« .�::. _-._. .. .... �.- a.,, .v� '. t'-';err. t:: d+. ,Lmm:..s .F'_.C.S ��t€ ` ,4]~
_,. .. ...,._.., r,, _r:�
s ar F s ; s tX F,+
k .fit t :1C i, �x r f a f '! ' -
a5 l 1 n i t y ,
. r kY l 'Iv O .11 - t3ft 4>. F t �i !a I Y.' J -K
Generator Name
1 . r - i. x c j - t r' ems' .�,,', ..g }.r.,_.._,..._,,,r P,C.. i-f—
,.,. ��, ,
.;try ..:. [ r:l 't �` , u ` '
1 C,�F, fr` °7 4u liq me- t` , 4 5�`� is .rhd „ .1 rtI iU �r r k C � ! r t } r x }
�J peep'] >t r } i, "tit 5 Yd t _ !"tft.fr?se+e'i'�; _ u t. 'vjd i�✓r GYr Y3 s k_ r,. 32 - - ti
Site Ad'dreS a d.:, w Y 7 ';
h
t f }t Y
r 4a
' 3 c+ j t iif qi'- c r S- S , 4
..,I�l.,� 'I]�:l. ..,,tL,
III
r a
t r. x r a 7 Y`r / r GEC+ 9' ' r t}:R a"^s"i, 7 -� 6� " ar, t t ° r � t
' ti� :i
- ..zu„� Fa . ?' 1 e +h #_g. 4}c �t,,.tft, z,,� t1 t c i� + , -
,+. r }� t x 'F L .t 7 h w Lq '' df P2ti .-'fSL�+YJ x ] S'x 9 s' ;. rX r.
J.o,ntraCtOG NraC;i'1� �t Lx „Ee:a 9 ''�L ,i4% k "f $s Is 1 ^rr i Heil i 4 -PF 1 ^s
... .. M t I �r 'sztr ° . rC �,� 5 n z caws. i. .+r -a rr-r -. ..�.... i -^ Ik r G,'. rx .d l;
_ z 4«�-x" ,E k far'a, f -itar� ..; jl,:- � ,s,. 'rn it r tt xa,rl t t ,,,
. , f T-,.,i 4 rt K'r i �. 9 # T a4 Ib .m..S2`w ttJ{Yr #'�.i°ES,e��zlr:ca 4kf3Fam f,55I-.ri'�,z S at r z -
y. } o .l.r ,--,�34.,.4..nv.,. u+. v + , ... r
A
n 2
' r` h c t 9iY- y f-X,'1. .fa ss. +" '-a« ,r Pr:iFr ,3.c...Ytr,U: frr y&'..�t r'r" i td _ r
y { r PI r to 1 _
rS , r t
�r E m
�J�
is Cd art :.A n. aYF r a 1 3 st e x f �i.n' k"'. „�jr arl, c ,r F" r gc,, tau
.h Yx' ta`i ,, '�. '}d Es k0 ,y iY 'x
.;ii_, 7q4) 4 ✓ �.. , u i"s?L� �, .« ^t t+'G k e4i r�.f r -.I!
�yy� - ,3, a-1 L X- "�` E.y t 1s.3 rrt-v f t I 2 ,r
1` J�T� l I r t$ S{x t ^Y 4i',j t ktdx fig, ;: '" t q
s ahe ts�1�� i' �bd
_,�,trn�sr'�r�� _ r�i� �< �.� � �� 1 « '@u( art✓��f1i3�n^ih�e
etl srt > d - � #f � , � t
u' �� �A���o� tad
Felbr ;s
dew �p�Ly - v� jj// y� {y�y
k`c"' `>r {`^i�c,'l,f tz., r•�,� w�'�' 1 s..�ij kq,F"'"'Ay 4 i F%Ci% z -C r
rfl'r�[r +.f.7'd`_a.i,Xsr„a+y� ..>~r/i `" Yi cc''.-r�F'"ai, c� ter A^i 't [ iI ;I
at +rs }ry' rj-t. c i Veit "r f- it ff Y a' : {' 9? K -t:,, >i \
r r ' If Md4 y'' r t"fU 4y '�s° 7
I,i ,_ �+ ° r y�a > i t
ans n...�
1i li �JI L 'I
''- -'s ' - a tEt .; '.r 5J .i .� E' _„;L i r l xr z2 t
,C t' 1' l /i�i=Stt
iyier�* , ,aa,{ Q,qs` y� iA z � ' s r£k `u' 7T: j� .� i'4'�tf'S. I b't{a rf,li t ,a;. 4if t l4 F ,.::
n i reY r ^4✓ 1r iC--a,�'� r 7- y x
n, r - ,t.
�+ .y�r "++ ``s..'-C',tfu>'aa3, -. 3JT¢ ,r�'3"r,N r"Z'+y:�'j F r
��n5 101 `,�Sp 1, I•-�.$ � Pd'19 s :35},7a7+t'Y'' t'"F '_.r'+ {.�.�r-.: .,x Et �i .f 4s ,t '�`F p ,, t 'x } f
i t, t #a. m ?u a}khF u4i �t / k xi a L
�•r '" e . t far ,t ;H11 rf y �yi?'tia Y+ !q lid t���
s4Jected`7 � 3S iIi T >l t r ; a i :' zi r
p e, u
.i - , :-..
r {
_ i�. jjSti( r
Time i.:
_
-" I - _
�''a N" ' i'' i i"I.it- X r � z h1 l�Ei ,o�` ': i a.' X ;, ' �i�.... '' - '
— �.: - r {
✓:.: .. ,.,, _ w
r., ., Z .
r
Soil TEc>�ruv)�ain xr�uu#l�rr�1 a �Iacce.aanc�f any'�� °�� oil
�Ei.i.jam„.y!� y� T
w! Lffl �!'i t�� si"xaafi r Z .P `'�5 i L "`" .r z ,T St , J %. i; -
t 4i�' fy ,p��!'y }�

C.'licat :
STAT, lnc.
P. O. Box 1443
Lenoir, NC: 28645
Attention:
Mr. 0. Spa.rl<s
Date Received:
9/26/17005
Report Date:
31-Aug-05
Sample Date:
26-Auk;-05
13RL 9:
BRL-2005-0661
Lab SHmpl€ [D:
LSID-2005-03319
Client Sample I D:
LRTS Ino les Shelby
Parameter
Result 1V1<.Ql,
355p
429 5
>p3()
1'3,9 2
Unit
Method
dn• mg/kg
5030/3550 TY
di-y ms;/kg
5030/35.90 TP
Reported BY:
atheson, S..I. Job nson
Concentratiom are below Minimum Quantification Limit except where noted.
NC Laboratory Certificate No. 275
Page I of 1
Analvsis
Analysis
Time
Date. Analy-t
12:54
8/31 /05 KSv1
15:23
8/11/05 KSlvt

Blue Ridge Labs, s, ne.
faU: 'r, 'O. IWx 2940 Ship Tn' - 506 Pine Nftn . R.d-
1,enoir, w' k. 28645
Telegbona (828-) 72S�0149- Fax (828) 72"131
CHAIN CIF C.USTDDY RECORD
i`` PDS Reporbrng _ Az-'MU,7chYater/UST,_ Hez. Waste Industrial lVon State F,eporina
REPORT e O: --- --- 'Eli - l r PRoJ--CT NAVER�P
'�6. �'
� ` or NUMBER:
-- PO # :
.—A
47; fJ
Smple ID
Sample
Type
rltLU
Collection i
Date Time
UA 1 A cin 1 i-, -
Res. CE Field � Preservatives
Temp. Cherked Dealorinaled PH Res. Temp.
YIN Yes i Flo C1 Pf
Sampler
Initials
Requested analysis
r
i
REt3NIQUISHED 'BY" ($19 j i3A'f�SC:FhEz
isf�rr�
DAME
a� 05 /211 i fG
C1 .�T1 ri(y=E@ - 3 :-y-O ^cs are FiI d: he . ime work I4 zcmple'.LG'w_ 1pe aC17-0 -a a.zr. Ml t
i pall 3T, -m : 9 .� ' , ;
.i roc ".i "b:..'.::4v:.i1C� l:l•'(1iC�i .�.c2`�.. 'x �''..:3arcT— .^.a�^.a .... '.•.5$ �fc_ 1:lOT:�t: Wr.J..� DE ....iSC.:✓`Ci3Q+"�. dl'1 a3,3, a5t-C:3a'c3GC:71:^�9. When�_..
__ _ lei i:: Ei:.:6 iS.tC_-C.!a! 'las',"13 {?Rx.1 bllw� 311%:Q„'��ES 3,�;�� MC �7@1-F:7r31i 4P_�V 'C:1E 3.:�e.�V':.' �......_.�::?•�
^psi _4'i:i�rs.nq s -
all, ag_ee� :a 33: :vim) F::: _ _S! 3X :: 3� �5.^.�;+5 3? =2 C 1 �J:Y:L day a� f3E �1i1 1k:X3i . 317_2 �iGlP.1 �.d }� '�49a_i.r'c
_ �.t_"�i '���::!!.�oLi:3':.':LU: `.`.)r 3 �t ;+vOi. S s act been made i,^ �,ffF!Ct: ''endva'.:-U 'rl:d� �dC3
be cif: _ep : 'y any --? r� _,:aC^ U authe, G
Z.%',: ::,a,—;.l ..l_^• )' .. C.f.23�3_
5:'aa c ss:�. .. ,�:o::si'L:__..- �� .: o�t�c
n
n
c
n
a
c
4
c
c
c
c
c
C

_e
Al,
L° 1 by r
NCDENR i v 0ceoa lyrk'm
�
North Carolina Department of Environment and Natural Resources
Division of Land Resources
James D. Simons, PG, PE Michael F. Easley, Governor
Director and State Geologist William G. Ross Jr., Secretary
July 1, 2005
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
7003 1010 0003 5645 1655
Mr. Michael Tonelis
Zemex Industrial Minerals, Inc.
PO Box 729
Kings Mountain, North Carolina 28086
RE: Mining Permit No. 23-03
Moss-Neisler Mine
Cleveland County
Broad River Basin
Dear Mr.- Tonelis:
ri4, 0EPT. OF MN IRQZ�M-IM �
AND 14ATU,RVAf- RESOURCES 1Y'+.
Y
4 .L.
JUL 19 2005
WATER nY; SECTION
Your request to have the corporate name changed on the referenced mining permit from
Oglebay Norton Specialty Minerals to Zemex Industrial Minerals, Inc. is hereby approved. As we
have received the required surety in an amount sufficient to cover this operation, I am enclosing a
new cover sheet for the updated mining permit. The permit number, expiration date and mine
name shall remain the same as before this corporate name change.
Please review the cover sheet carefully and notify this office of any objections, questions or
corrections that may need to be addressed. I have also enclosed surety bond no. 40OKB6879
issued by St. Paul Fire and Marine Insurance Company for your disposal.
Thank you for your cooperation in this matter. If you should have any questions, please
contact Kristin Hicklin, Assistant State Mining Specialist, at [phone].
pniams,PG, CPG, CPESC
State Mining Specialist
Land Quality Section
FRW/kh-
Enclosures: Surety Bond No. 40OKB6879
cc: Mr. Doug Miller, PE, w/permit
Mr. Bradley Bennett-DWQ, w/permit
Ms. Shannon Deaton -WRC, w/permit
Mr. William Gerringer-DOL, Mine and Quarry Bureau, w/o enclosures
Land Quality Section 919-733-4574 \ FAX:[phone] - Geological Survey Section 919-733-2423 \ FAX: [phone]
1612 Mail Service Center, Raleigh, North Carolina 27699-1612
Division of Land Resources 919-733-3833 \ FAX: [phone] Internet: www_dlr.enr- state.nc.us/dlr.htm
An Equal Opportunity \ Affirmative Action Employer— 50% Recycled \ 10% Post Consumer Paper

DEPARTMENT OF ENVIRONMENT
. AND NATURAL RESOURCES
DIVISION OF LAND RESOURCES
LAND QUALITY SECTION
PERMIT
for the operation of a mining activity
In accordance with the provisions of G.S. 74-46 through 68, "The Mining
Act of 1971," Mining Permit Rule 15A NCAC 5 B, and other applicable
laws, rules and regulations
Permission is hereby granted to:
Zemex Industrial Minerals, Inc.
Moss-Neisler Mine
Cleveland County - Permit No. 23-03
for the operation of a
Mica and By -Products Mineral Mine
which shall provide that the usefulness, productivity and scenic values of
all lands and waters affected by this mining operation will receive the
greatest practical degree of protection and restoration.
MINING PERMIT EXPIRATION DATE: April 5 2015

Page 2
In accordance with the application for this mining permit, which is hereby approved by the
Department of Environment and Natural Resources hereinafter referred to as the Department,
and in conformity with the approved Reclamation Plan attached to and incorporated as part_ of
this permit, provisions must be made for the protection of the surrounding environment and for
reclamation of the land and water affected by the permitted mining operation. This permit is
expressly conditioned upon compliance with all the requirements of the approved Reclamation
Plan. However, completed performance of the approved Reclamation Plan is a separable
obligation, secured by the bond or other security on file with the Department, and may survive
the expiration, revocation or suspension of this permit.
This permit is not transferable by the permittee with the following exception: If another
operator succeeds to the interest of the permittee in the permitted mining operation, by virtue
of a sale, lease, assignment or otherwise, the Department may release the permittee from the
duties .imposed upon him by the conditions of his permit and by the Mining Act with reference
to the permitted operation, and transfer the permit to the successor operator, provided that
both operators have complied with the requirements of the Mining Act and that the successor
operator agrees to assume the duties of the permittee with reference to reclamation of the
affected land and posts a suitable bond or other security.
In the event that the Department determines that the permittee or permittee's successor is not
complying with the Reclamation Plan or other terms and conditions of this permit, or is failing
to achieve the purposes and requirements of the Mining Act, the Department may give the
operator written notice of its intent to modify, revoke or suspend the permit, or its intent to .
modify the Reclamation Plan as incorporated in the permit. The operator shall have right to a
hearing at a designated time and place on any proposed modification, revocation or
suspension by the Department. Alternatively and in addition to the above, the Department
may institute other enforcement procedures authorized by law.
Definitions
Wherever used or referred to in this permit, unless the context clearly indicates otherwise,
terms shall have the same meaning as supplied by the Mining Act, N.C.G.S. 74-49.
Modifications
June 12, 1979: This permit has been modified to include an additional 465 acres identified as
the Neisler and U.S. Gypsum Corporation Tracts.
September 20, 1981: This permit has been renewed and transferred from Kings Mountain
Mica Company, Inc. to KMG Minerals, Inc.
May 16, 1994: This permit has been modified to include the changes to the operation as
indicated on the revised mine maps, Sheets 1 through 17 of 17, dated March 9, 1994.
October 14, 1994: This permit has been transferred in its entirety from KMG Minerals, Inc. to
Franklin Industries, Inc.

Page 3
March 10, 1997: This permit has been modified to incorporate Mining Permit No. 23A 0
(Hawks Mine) in its entirety and to add the Archdale Tract as indicated on the mine map last
revised February 11, 1997.
November 19, 1998: This permit has been modified to allow test blasting to be conducted at
the Hawks Mine as indicated on the 8 Y2 by 11 inch section of the mine map received by the
Land Quality Section on October 15, 1998 with stipulations.
May 12, 1999: A partial release has been granted to release Tract No. 1, Tract No. 3, Tract
No. 4, and Tract No. 5 from the permitted and affected acreage at this site. Tract No. 2 was
previously released.
March 6, 2000: This permit, issued to Franklin Industries, Inc., has been transferred in its
entirety to Oglebay Norton Specialty Minerals, Inc.
January 8, 2001: This permit has been modified to increase the permitted acreage to 753.92
acres and increase the affected acreage to 381.03a'creSr as indicated on the Moss Mine's No.-
1 & No. 2 Mine Map last revised November 30, 2000 and the Archdale Mine - East Mine Map
last revised August 21, 2000. This modification includes a 2.0-acre stockpile/excavation area
on the 4.19-acre addition (the McIntosh Addition) and a 1.03-acre mine area that will be
converted to a waste storage area on the 1.03 acre addition (the Landstar Addition).
July 1, 2005: This permit has been modified to have the corporate name changed on the
mining permit from Oglebay Norton Specialty Minerals to Zemex Industrial Minerals, Inc.
Expiration Date
This permit shall be effective from the date of its issuance until April 5,, 2015.
Conditions
This Permit shall be subject to the provisions of the Mining Act, N.C.G.S. 74-46, et. seq., and
to the following conditions and limitations:
OPERATING CONDITIONS:
Wastewater and Quarry Dewatering
A. Any wastewater processing or mine dewatering shall be in accordance with the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission.

Page 4
B. Any storm water runoff from the affected areas at the site shall be in accordance
with any applicable permit requirements and regulations promulgated by the
Environmental Protection Agency and enforced by the N.C. Environmental
Management Commission. It shall be the permittee's responsibility to contact
Division of Water Quality to secure any necessary storm water permits or other
approval documents.
2. Air Quality and Dust Control
A. Any mining related process producing air contaminant emissions including
fugitive dust shall be subject to the requirements and rules promulgated by the
N.C. Environmental Management Commission and enforced by the Division of
Air Quality. -
B. During processing. operation, water trucks or other means that may be necessary
shall be utilized to prevent dust from leaving the permitted area.
3. Buffer Zones
A. Any mining activity affecting waters of the State, waters of the U. S., or wetlands
shall be in accordance with the requirements and regulations promulgated and
enforced by the N. C. Environmental Management Commission.
B. Sufficient buffer (30 foot undisturbed) shall be maintained between any affected
land and any adjoining waterway or wetland to prevent sedimentation of that
waterway or wetland from erosion of the affected land and to preserve the
integrity of the natural watercourse or wetland.
C. All buffer zones shown on the Moss Mine's No. 1 & No. 2 and Overall Property
Map both received by the Land Quality Section on August 1.7, 2004, and the
Archdale Mine — East, Archdale West, Archdale Mine, Hawks Mine, and Neisler
Mine's No. 1, No. 2, & No. 3 mine maps received by the Land Quality Section on
December 13, 2004 shall be maintained to protect adjoining property. These
buffer zones, with the exception of the installation of required sediment control
measures and approved earthen berms, shall remain undisturbed.
D. An undisturbed buffer zone of 25 feet along both sides of the gas line located
near Concept Drive on the Neisler 1 and 2 Tracts shall be maintained. In
addition, all excavated slopes adjacent to the buffer zones along the gas line
shall be maintained at a 2-foot horizontal to 1-foot vertical or flatter slope.

Page 5
4. Erosion and Sediment Control
A. Adequate mechanical barriers including, but not limited to diversions, earthen
dikes, check dams, sediment retarding structures, rip rap pits, or ditches shall be
provided in the initial stages of any land disturbance and maintained to prevent
sediment from discharging onto adjacent surface areas or into any lake, wetland
or natural watercourse in proximity to the affected land.
B. All, -mining activities, including the installation and maintenance of all erosion and
sedimentation control measures, shall be conducted as indicated on the Moss
Mine's No. 1 & No. 2 and Overall Property Map both received by the Land
Quality Section on August 17, 2004, and the Archdale Mine— East, Archdale
West, Archdale Mine, Hawks Mine, and Neisler Mine's No. 1, No. 2, & No. 3
mine maps received by the Land Quality Section on December 13, 2004, and the
Erosion & Sediment Control Details Drawings 1 and 2, dated February 11, 2005.
C. Appropriately designed erosion and sediment control measures shall be installed
and maintained, as necessary, below the previous United States Gypsum plant
area to prevent off -site sedimentation.
D. Appropriately designed diversions and chute spillway shall be provided and
maintained, as necessary, to control surface drainage on the fill area between
the plant area and Interstate 85.
E. An erosion and sediment control plan(s) shall be submitted to the Department for
approval prior to any land disturbing activities not indicated on the revised
erosion control plan or mine maps submitted with the approved application for a
mining permit and any approved revisions to it. Such areas include, but are not
limited to, expansion outside of the approved pit area, creek crossings, or
expansion -of overburden or waste disposal areas.
F. The surface water runoff from the 2.0 acres stockpile/excavation area on the
4.19 acre addition to the Moss Mine's No. 1 & No. 2 tract and the 1.03 acre mine
area that will be converted to a waste storage area on the 1.03 acre addition to
the Archdale Mine —.East tract shall be diverted internal to the mine excavation
or into existing sedimentation and erosion control measures to prevent off site
sedimentation. -
5. Groundwater Protection
Groundwater monitoring wells shall be installed and monitored as deemed appropriate
by the Department.

Page 6
6. Graded Slopes and Fills
A. The angle for graded slopes and fills shall be no greater than the angle which
can be retained by vegetative cover or other adequate erosion control measure,
structure, or device. In any event, exposed slopes or any excavated channels,
the erosion of which may cause off -site damage because of siltation, shall be
planted or otherwise provided with groundcover, devices or structures sufficient
to restrain such erosion.
7. Surface Drainage
The affected land shall be graded so as to prevent collection of pools of water that are,
or likely to become, noxious or foul. Necessary structures -such as drainage ditches or
conduits shall be constructed or installed when required to prevent such conditions.
8. Blastinq
The operator shall monitor each blast with a seismograph located at a distance
no farther than the closest off site regularly occupied structure not owned or
leased by the operator. A seismographic record including peak particle velocity, air
overpressure, and vibration frequency levels shall be kept for each blast (except as
provided under Operating Condition Nos. 8B and 8D of this permit). The following
blasting conditions shall be observed by the mine operator to prevent hazard to persons
and adjacent property from surface blasting:
A. Ground Vibration With Monitoring:
In all blasting operations, the maximum peak particle velocity of any component
of ground motion shall not exceed Figure 1 (below) at the immediate location of
any regularly occupied building outside of the permitted area such as a dwelling
house, church, school, or public, commercial or institutional building.

Page 7
ti
r
Blast Vibration, Frreque'ncy,
e &x n6g / try Cm
I sl aurce. f -n Odirleul from �q�r - ..fix a .T
Ground Vibration Without.Monitoring:
In the event of seismograph malfunction or other condition which prevents
monitoring, blasting shall be conducted in accordance with the following
formulas:
W = (D/DS)2 DS = D
W 1/2
V = 160(DS)-''6
W = Maximum charge weight of explosives per delay period of 8.0 milliseconds
or more (pounds).
D = Distance from the blast site to the nearest inhabited building not owned or
leased by the mine operator (feet).
Ds = Scaled distance factor.
V = Peak Particle Velocity (inches per second).
The peak particle velocity of any component shall not exceed 1.0 inch per
second, for the purposes of this Section.

Page 8
C. Air blast With Monitoring:
Air blast overpressure resulting from surface blasting shall not exceed 129
decibels linear (dBL) as measured at the immediate location of any regularly
occupied building not owned or leased by the operator outside of the permitted
area such as a dwelling house, church, school, or public, commercial or
institutional building, unless an alternate level based on the sensitivity of the
seismograph microphone as specified below is being used:
Lower Frequency Limit of Max Level,
Measuring System, in Hz in dBL
0.1 Hz or lower -flat response 134 peak
2.0 Hz or lower -flat response 133 peak
6.0 Hz or lower -flat response 129 peak
D. Air blast Without Monitoring:
In the event of seismograph malfunction or other condition which prevents
monitoring, blasting shall be conducted in accordance with the following
formulas:
To convert U (psi) to P (dBL):
U = 82 (D/W0.33)-1.2
P = 20 x log (U/2.9x10-9)
Confined Air blast/Overpressure (dBL)
for quarry situation:
A=P-35
U = Unconfined air overpressure (pounds per square inch).
W = Maximum charge weight of explosives per delay period of 8.0 milliseconds
or more (pounds).
D = Distance from the blast site to the nearest inhabited building not owned or
leased by the mine operator (feet).
P = Unconfined air overpressure (decibels).
A = Air blast or air overpressure for typical quarry situations (decibels).
The air blast/overpressure shall not exceed 129 decibels, for the purposes of this
Section.

Page 9
E. - Record Keeping:
The operator shall maintain records on each individual blast describing: the total
number of holes; pattern of holes and delay of intervals; depth and size of holes;
type and total pounds of explosives; maximum pounds per delay interval; amount
of stemming and burden for each hole; blast location; distance from blast to
closest offsite regularly occupied structure; and weather conditions at the time of
the blast. Records shall be maintained at the permittee's mine office and copies
shall be provided to the Department upon request.
F. Excessive Ground Vibration/Air blast Reporting_
If ground vibration or Air blast limits are exceeded, the operator will immediately
report the event with causes and corrective actions to the Department. Use of
explosives at the blast site that produced the excessive reading shall cease until
corrective actions approved by the Department are taken. However, blasting
may occur in other approved areas within the permitted boundary. Authorization
to blast at the blast site may be granted at the time of the verbal reporting of the
high ground vibration or high air blast reading if the circumstances justify verbal
approval. Failure to report will constitute a permit violation.
G. Flyrock Prevention:
The operator shall take all reasonable precautions to ensure that flyrock is not
thrown beyond areas where the access is temporarily or permanently guarded by
the operator. Failure to take corrective measures to prevent flyrock and
repeated instances of flyrock shall be considered a violation of the Mining Permit.
H. Flyrock Reporting:
Should flyrock occur beyond the permitted and guarded areas, the operator shall
immediately report the incident to the Department. Further use of explosives on
the mine site shall be suspended until the following actions have been taken:
1. A thorough investigation -as to the cause(s). of the incident shall be
conducted.
2. A. report detailing the investigation shall be provided to the Department
within 10 days of the incident. The report shall, at a minimum, document
the cause(s) of the incident along with technical and management actions
that will be taken to prevent further incidents. The report shall meet with
the approval of the Department before blasting may resume at the mine
site.

Page 10
I. Studies:
The operator shall provide to the Department a copy of the findings of any
seismic studies conducted at the mine site in response to an exceedence of a
level allowed by these blasting conditions. The operator shall make every
reasonable effort to incorporate the studies' recommendations into the
production blasting program.
J. Notice:
The operator shall, when requested by the Department, give 24-hour advance
notice to the Land Quality Section Regional Office prior to any blast during a .
period for which notice is requested.
K. The test shots in the Hawks Pit shall be conducted as indicated on the 8 Y2 by 11
inch section of the mine map and related correspondence received by the Land
Quality Section on October 15, 1998 with the following stipulations:
1. _the test shall be limited to two shots,
2. the above blasting conditions shall be followed for the test shots, and
3. the blasting consultants shall submit to the Land Quality Section two
copies of the seismograph recordings and blasting records, including -any
conclusions made, shortly after completion of the test.
L. A modification shall be submitted to and approved by the Division of Land
Resources prior to incorporating blasting activities into the routine mining
activities at the site. Prior to submitting the modification request, a meeting shall
be conducted as described in the additional information letter from Ms. Judy
Wehner dated October 19, 1998.
9. High Wall Barrier
.A physical barrier consisting of chain link fencing, vegetated earthen berms, 4-strand
barbed wire fencing (a minimum 4-feet,-high), or large boulders placed end -to -end shall
be maintained at all times along the perimeter of any highwall to prevent inadvertent
public access. In addition, a minimum 10 foot wide horizontal safety bench shall be
provided at the junction between the top of rock and the toe of any overburden cut
slope.
10. Visual Screening
A. _ Existing vegetation shall be maintained between the mine and public
thoroughfares to screen the operation from the public. Additional screening
methods, such as constructing earthen berms, shall be employed as deemed
appropriate by the Department.

Page 11
B. Vegetated earthen berms and other acceptable screening shall be located and
maintained as shown on the Moss Mine's No. 1 & No. 2 and Overall Property
Map both received by the Land Quality Section on August 17, 2004, and the
Archdale Mine — East, Archdale West, Archdale Mine, Hawks Mine, and Neisler
Mine's No. 1, No. 2, & No. 3 mine maps received by the Land Quality Section on
December 13, 2004. Berms shall be constructed a minimum five foot high with a
16 foot top width and a minimum two horizontal to one vertical or flatter side
slopes.
C. In addition to grasses, long leaf and/or Virginia pines or other acceptable
evergreen species shall be planted as deemed appropriate by the -Department to
improve visual and noise buffering.
11. Plan Modification
A. The operator shall notify the Department in writing of the desire to delete, modify
or otherwise change any part of the mining, reclamation, or erosion/sediment
control plan contained in the approved application for a mining permit and any
approved revisions to it. Approval to implement such changes must be obtained
from the Department prior to on -site implementation of the revisions.
B. A modification request shall be submitted to and approved by the Division of
Land Resources prior to incorporating blasting activities into the routine mining
activities at the site. Prior to submitting the modification request, a meeting shall
be conducted as described in the additional information letter from Ms. Judy
Wehner dated October 19, 1998.
12. Refuse Disposal
A. No on -site disposal of refuse or other solid waste that is generated outside of the
mining permit area shall be allowed within the boundaries of the mining permit
area unless authorization to conduct said disposal has first been obtained from
both the Division of Waste Management and the Land Quality Section,
Department of Environment and Natural Resources. The method of disposal
shall be consistent with the approved reclamation plan.
B. Mining refuse as defined. by G.S. 74-49 (14) of The Mining Act of 1971
generated on -site and directly associated with the mining activity may be
disposed of in a designated refuse area. All other waste products must be
disposed of in a disposal facility approved by the Division of Waste
Management. No petroleum products, acids, solvents or their storage containers
or any other material that may be considered hazardous shall be disposed of
within the permitted area.
C. For the purposes of this permit, the Division of Land Resources considers the
following materials to be "mining refuse" (in addition to those specifically listed
under G.S. 74-49 (14) of the N.C. Mining Act of 1971):

Page 12
1. on -site generated land clearing debris
2. conveyor belts
3. wire cables
4. v-belts
5. steel reinforced air hoses
6. drill steel
D. If mining refuse is to be permanently disposed within the mining permit
boundary, the following information must be provided to and approved by the
Division of Land Resources prior to commencement of such disposal:
1. the approximate boundaries and size of the refuse disposal area;
2. a list of refuse items to be disposed;
3. verification that a minimum of 4 feet of cover will be provided over the
refuse;
4. verification that the refuse will be disposed at least 4 feet above the
seasonally high water table; and
5. verification that a permanent vegetative groundcover will be established
13. Annual Reclamation Report
An Annual Reclamation Report shall be submitted on a form supplied by the
Department by February 1 of each year until reclamation is completed and approved..
14. Bonding
The security, which was posted pursuant to N.C.G.S. 74-54 in the form of a
$500,000.00 blanket bond, is sufficient to cover the operation as indicated in the
approved application. This security must remain in force for this permit to be valid. The
total affected land shall not exceed the bonded acreage.
15. Archaeological Resources
Authorized representatives of the Division of Archives and History shall be granted
access to the site to determine the presence of significant archaeological resources.

Page 13
APPROVED RECLAMATION PLAN
The Mining Permit incorporates this Reclamation Plan, the performance of which is a condition
on the continuing. validity of that Mining Permit. Additionally, the Reclamation Plan is a
separable obligation of the permittee, which continues beyond the terms of the Mining Permit.
The approved plan provides:
Minimum Standards As Provided By G S 74-53
1. The final slopes in all excavations in soil, sand, gravel and other unconsolidated
materials shall be at such an angle as to minimize the possibility of slides and be
consistent with the future use of the land. i
2. Provisions for safety to persons and to adjoining property must be providedin all
excavations in rock.
3. All overburden and spoil shall be left in a configuration which is in accordance with
accepted conservation practices and which is suitable for the proposed subsequent use
of the land.
4. No small pools of water shall be allowed to collect or remain on the mined area that are,
or are likely to become noxious, odious or foul.
5. The revegetation plan shall conform to accepted and recommended agronomic and
reforestation practices as established by the North Carolina Agricultural Experiment
Station and the North Carolina Forest Service.
6. Permittee shag conduct reclamation activities pursuant to the Reclamation Plan herein
incorporated. These activities shall be conducted according to the time schedule
included in the plan, which shall to the extent feasible provide reclamation simultaneous
with mining operations and in any event, provide reclamation at the earliest practicable
time after completion or termination of mining on any segment of the permit area and
shall be completed within two years after completion or termination of mining.
RECLAMATION CONDITIONS:
1. Provided further, and subject to the Reclamation Schedule, the planned reclamation
shall be to allow the quarry excavation to fill with water, provide a permanent barricade
(fence) along the top of any high wall, and grade and revegetate any areas in
unconsolidated material.
2. The specifications for surface gradient restoration to a surface suitable for the planned
future use are as follows:

Page 14
A. Overburden shall be used to slope all side .slopes of the mine excavation in
unconsolidated material to a 1 '/Z horizontal to 1 vertical or flatter slope on the
Moss Tract and United States Gypsum Tract and to a 2 horizontal to 1 vertical or
flatter slope on the Neisler, Hawks, and Archdale Tracts.
B. All lakes shall be excavated to maintain a minimum water depth of four feet
measured from the low water table elevation.
C. The side slopes of the lake excavation shall be graded to a 3 horizontal to 1
vertical or flatter above the water level and 1 '/Z horizontal to 1 vertical below the
water level.
D. Any settling ponds and sediment.control basins shall be backfilled, graded, and
stabilized or cleaned out and made into acceptable lake areas.
E. The processing, stockpile, and other disturbed areas neighboring the mine
excavation shall be leveled and smoothed.
F. Compacted surfaces shall be disced, subsoiled or otherwise prepared before
revegetation.
G. No contaminants shall be permanently disposed of at the mine site. On -site
disposal of waste shall be in accordance with Operating. Conditions Nos. 12A
through 12D.
H. The affected land shall be graded to prevent the collection of noxious or foul
water.
3. Revegetation Plan:
Disturbed areas shall be permanently revegetated according to the Revegetation Plan
prepared by Mr. Ben Robinson, NRCS District Conservationist dated April 12, 2004.
Whenever possible, disturbed areas should be vegetated with native warm season
grasses such as switch grass, Indian grass, bluestem and gamma grass.
In addition, the permittee shall consult with a professional wildlife biologist with the N.C.
Wildlife Resources Commission to enhance post -project wildlife habitat at the site..

Page 15
4. Reclamation Plan:
Reclamation shall be conducted simultaneously with mining to the extent feasible. In
any event, reclamation shall be initiated as soon as feasible after completion or
termination of mining of any mine segment under permit. Final reclamation, including
revegetation, shall be completed within two years of completion or termination of
mining.
This permit, issued to Kings Mountain Mica Company, Inc..July 26, 1972, modified June
12, 1979, renewed and transferred in its entirety to KMG Minerals, Inc. September 20,
1981, renewed and modified May 16, 1994, transferred in its entirety to Franklin
Industries, Inc. October 14, 1994, modified March 10, 1997, November 19, 1998, and
May 12, 1999, transferred in its entirety to Oglebay Norton Specialty Minerals, Inc.
March 6, 2000, modified January 8, 2001, and renewed April 5, 2005, is hereby
modified to have the corporate name changed on the mining permit from Oglebay
Norton Specialty Minerals to Zemex Industrial Minerals, Inc. this 1st day of July 2005.
By:
James D. Simons, Director
Division of Land Resources
By Authority of the Secretary
Of the Department of Environment and Natural Resources