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HomeMy WebLinkAboutWQ0004122_Monitoring - 09-2020_20201104Cameron Testing Services, Inc. Laboratory Report Client: Jordan Lake SRA CTS Proj. Project: Sept. 2020 Poplar Point MWs Regulatory s- Sample Information Sampled C. Cameron = D$t 09/22/20 Received Analyses and Results NC DENR #654 NC PHHS #37799 US EPA #NC01918 2009-195 Yes Page 1 of 3 S. Puckett Date j 09/22/20 Lab ID Sample ID y e Analyte Result C d E a M 2009-195 01 MW-1 cW cr Chloride 1.97 mgl 001 09/28/20 o TDS 34.0 mg/L 25 09/22/20 (V o N-NH3 <0.100 #N/A 0.1 09/24/20 _ c--1 N-NO3 <0.050 mg/L 0.05 09/29/20 o Fec. Coliform-W <1 cFU 1 09/22/20 Z /100mt. TOC <1.00 mg/L 1 09/28/20 VOC Attached 02 MW-2 cW cr Chloride 50.3 mg/L 0.01 09/28/20 TDS 457 mg/L 25 09/22/20 N-NH3 <0.100 #N/A 0.1 09/24/20 N-NO3 0.118 mg/L 0.05 09/29/20 Fec. Coliform-W <1 cFU 1 09/22/20 /100mL TOC 7.13 mg/L 1 09/28/20 VOC Attached 03 MW-3 GW cr Chloride 4.93 mg/L 0.01 09/28/20 TDS 805 mg/L 25 09/22/20 �3 N-NH3 <0.100 #N/A 0.1 09/24/20 N-NO3 <0.050 mg/L 0.05 09/29/20 c<i c CD T7J Fec. Coliform-W <1 cFu 1 09/22/20 /100mL p TOC 1.90 mg/L 1 09/28/20 +A ►� VOC Attached N � `-= VO& analyzed by Environmental Chemists, Wilmington, NC; report 219 S. Steele Str. Sanford NC 27330 `m E Std, Methods Reference 4500 Cl- D 2540 C - TDS 4500 NH3 - D 4500 NO3 - E 9222 D - MF 5310 B2000 4500 Cl- D 2540 C - TDS 4500 NH3 - D 4500 NO3 - E 9222 D - MF 5310 B2000 4500 Cl- D 2540 C - TDS 4500 NH3 - D 4500 NO3 - E 9222 D - MF 5310 B2000 919-721-4067 919-208-4240 chris a camerontesting.coin Cameron Testing Services, Inc. Laboratory Report NCDENR#654 NC PHHS #37799 Client: Jordan Lake SRA CTS Proj. 2009-195 US EPA #NC01918 Project: Sept. 2020 Poplar Point MWs Regulatory Yes Page 2 of 3 Sample Information Sampled ail Q,f *� p C. Cameron a 09/22/20 „¢@d S. Puckett Date 09/22/20 Analyses and Results Lab ID Sample ID M o �° Analyte Result E N T E Std. Methods Reference Q C7 2009-195 04 MW-4 Gw Gr Chloride 108 mg/L 0.01 09/28/20 4500 Cl-'D TDS 447 mg/L 25 09/22/20 2540 C - TDS N-NH3 <0.100 #N/A 0.1 09/24/20 4500 NH3 - D N-NO3 <0.050 mg/L 0.05 09/29/20 4500 NO3 - E Fec. Coliform-W <1 CFU /100mL 1 09/22/20 9222 D - MF TOC 3.59 mg/L 1 09/28/20 5310 B2000 VOC Attached 05 MW-5 Gw Gr Chloride 8.37 mg/L 0.01 09/28/20 4500 Cl- D TDS 150 mg/L 25 09/22/20 2540 C - TDS N-NH3 <0.100 #N/A 0.1 09/24/20 4500 NH3 - D N-NO3 0.240 mg/L 0.05 09/29/20 4500 NO3 - E Fec. Coliform-W <1 CFU 1 09/22/20 9222 D - MF /t TOC 1.35 mg/L 1 09/28/20 5310 B2000 VOC Attached 06 MW-6 Gw Gr Chloride 19.2 mg/L 0.01 09/28/20 4500 Cl- D TDS 113 mg/L 25 09/22/20 2540 C - TDS N-NH3 <0.100 #N/A 0.1 09/24/20 4500 NH3 - D N-NO3 <0.050 mg/L 0.05 09/29/20 4500 NO3 - E Fec. Coliform-W <1 CFU 1 09/22/20 9222 D - MF /100mL TOC 1.44 mg/L 1 09/28/20 5310 B2000 VOC Attached VOCs analyzed by Environmental Chemists, Wilmington, NC; report 219 S. Steele Str. 919-721-40679t9-208-4240 Sanford NC 27330 civis@camerontesting.com Cameron Testing Services, Inc. Laboratory Report NC DENR #654 NC PHHS #37799 Client, Jordan Lake SRA CTS Proj. 2009-195 US EPA #NCO1918 Project: Sept. 2020 Poplar Point MWs Regulatory Yes Page 3 of 3 Sample Information :sampled C. Cameron '" Dat 09/22/20 Ftec i esl S. Puckett Date.? 09/22/20 Analyses and Results Lab ID Sample ID E 2Analyte Result .E `E Std. Methods ULL :J o Reference < a 2009-195 07 MW-7 cw Gr Chloride 18.0 mg/L 0.01 09/28/20 4500 Cl- D TDS 211 mg/L 25 09/22/20 2540 C - TDS N-NH3 <O.100 #N/A 0.1 09/24/20 4500 NH3 - D N-NO3 0.088 mg/L 0.05 09/29/20 4500 NO3 - E Fec. Coliform-W <1 /1oomL 1 09/22/20 9222 D - MF TOC 2.16 mg/L 1 09/28/20 5310 B2000 VOC Attached VOCs analyzed by Environmental Chemists, Wilmington, NC; report Report Review Project Manager Date 219 S. Steele Str. 919-721-4067919-208-4240 Sanford NC 27330 chris@camerontesting.com Environmental Chemists, Inc. envircochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-41798 Site: 01 9/24/2020 1:15 PM Water Client Test Method Results Date Analyzed 1, 1, 1,2-Tetrachloroethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 8260815030B <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1-Dichloroethane SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 1,1-Dichloroethene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1,2,3-Trichlorobenzene SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 846 method 8260BI5030B <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 8280B15030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 82808/5030B <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 848 method 02608/5030B <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 846 method 82808/5030B <0.5 pg/L 09/29/2020 1,3-Dichlorobenzene SW 848 method 8260B/50308 <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 8280B15030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Reportk: 2020-16323 Page 1 of 21 :envirochem ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 646 method 8260B/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloroform SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 cis-1,2-Dichloroethene SW 846 method 8280B150306 <0.5 pg/L 09/29/2020 cis- 1,3-Dichloropropene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 8260815030B <0.5 pg/L 09/29/2020 Isopropylbenzene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 8260B/50308 <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 sec-Butylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 tert-B utyl benzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 2 of 21 Environmental Chemists, Inc. it 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax �' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Trans- 1,2-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans-1,3-dichloropropene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Report V 2020-16323 Page 3 of 21 F77— � 7771 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 " 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-41799 Site: 02 9/24/2020 11:58 AM Water Client Test Method Results Date Analyzed 1, 1, 1,2-Tetrachloroethane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 845 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 8260815030B <0.5 pg/L 09/29/2020 1, 1 -Dichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1, 1 -Dichloroethene SW 846 method 82608150308 <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2, 3-Trichlorobenzene SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 646 method 8260B/50308 <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 6260B/50308 <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 6260B/5030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 846 method 6260B/5030B <0.5 pg/L 09/29/2020 1,3-Dichlorobenzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1, 3-Dichloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 646 method 826013/50308 <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 4 of 21 L rochem ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8280B15030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Chloroform SW 846 method 8280B15030B <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 cis-1,2-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 cis-1,3-Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1 sopropyl benzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 8260B15030B <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 8260815030E <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 82808/5030B <0.5 pg/L 09/29/2020 sec -Butyl benzene SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 Styrene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 tert-Butylbenzene SW 646 method 826013/50308 <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 5 of 21 [envi7roehie]m ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Toluene SW 848 method 8280B/5030B <0.5 pg/L 09/29/2020 Trans-1,2-Dichloroethene SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 Trans-1,3-dichloropropene SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 8260015030E <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 6 of 21 enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-41800 Site: 03 9/24/2020 12:11 PM Water Client Test Method Results Date Analyzed 1,1,1,2-Tetrachloroethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 1,1-Dichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 1,2,3-Trichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 848 method 8280E/5030B <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 848 method 8280B/5030B <0.5 pg/L 09/29/2020 1, 3-Dichlorobenzene SW 848 method 8260B15030B <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 82BOB/50308 <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 6260815030B <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Report k: 2020-16323 Page 7 of 21 Environmental Chemists, Inc. enviro6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab " 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax v 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 646 method 8260B15030B <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 8260815030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 848 method 826013/503013 <0.5 pg/L 09/29/2020 Chloroform SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 cis-1,2-Dichloroethene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 cis-1,3-Dichloropropene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 8260815030E <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Ethylbenzene SW 848 method 8260B/5030B <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 646 method 8260B/5030B <0.5 pg/L 09/29/2020 Isopropylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 M+P Xylene SW 646 method 8260B/5030B <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 sec-Butylbenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 tert-Butylbenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 8 of 21 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Trans- 1,2-Dichloroethene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Trans- 1, 3-d ich loropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 8260B/503DB <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 8260Bt5O3OB <0.5 pg/L 09/29/2020 Report V 2020-16323 Page 9 of 21 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-41801 Site: 04 9/24/2020 12:40 PM Water Client Test Method Results Date Analyzed 1,1,1,2-Tetrachloroethane SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 1, 1 -Dichloroethane SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 1,1-Dichloroethene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 1,2,3-Trichlorobenzene SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 848 method 826OB/5030B <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,4-Trimethyl benzene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 828OB/5030B <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 828OB/5030B <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 62608/5030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1, 3-Dichlorobenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 646 method 82606/50308 <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 828OB15030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 8260E/5030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 10 of 21 :envirper-hem'. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 Chloroform SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 cis-1,2-Dichloroethene SW 848 method 8260B/5030B <0.5 pg/L 09/29/2020 cis- 1,3-Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Dich lorodifl uoro methane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Isopropyl benzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 8260B/5030B <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 848 method 82608/5030B <0.5 pg/L 09/29/2020 sec-Butylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 ten`-Butylbenzene SW 846 method 8260B/50306 <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 11 of 21 C�rocheIF-07, ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans- 1,2-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans- l,3-dichloropropene SW 846 method 8280B/50308 <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Report #., 2020-16323 Page 12 of 21 001�- envirochem ANALYTICAL $ CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: 20-41802 Site: 05 Test Collect DatelTime 9/24/2020 2:07 PM Method Matrix Sampled by Water Client Results Date Analyzed 1, 1, 1,2-Tetrachloroethane SW 846 method82BOB/5030B <0.5pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 1,1-Dichloroethane SW 846 method 8260615030E <0.5 pg/L 09/29/2020 1, 1 -Dichloroethene SW B46 method 82BOB/5030B <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 1,2,3-Trichlorobenzene SW B46 method 8280B/5030B <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 848 method 826OB/5030B <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,3-Dichlorobenzene SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 846 method 826OB/50308 <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 82608/5030B <0,5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 8260815030B <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 82808/5030B <0.5 pg/L 09/29/2020 Report #.: 2020.16323 Page 13 of 21 [envii-rochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 82508/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 Chloroform SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 cis-1,2-Dichloroethene SW 846 method 826OB150308 <0.5 pg/L 09/29/2020 cis- 1,3-Dichloropropene SW 846 method 8260E/5030B <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 826OB150308 <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 826013/50306 <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 Isopropyl benzene SW 846 method 82608150308 <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 82608/5030B <1.0 pg/L 09/29/2020 Methylene chloride SW 848 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 sec -Butyl benzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 8260B150308 <0.5 pg/L 09/29/2020 tert-Butyl benzene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Report #: 2020-16323 Page 14 of 21 Environmental Chemists, Inc. 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax `M 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Trans-1,2-Dichloroethene SW 846 method 82808/5030B <0.5 pg/L 09/29/2020 Trans- 1,3-dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 8260BI5030B <0.5 pg/L 09/29/2020 Report #- 2020-16323 Page 15 of 21 6:zvir'oehem' ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Lab ID Sample ID: 20-41803 Site: 06 Test Collect DaterTime 9/24/2020 1:52 PM Method Matrix Sampled by Water Client Results Date Analyzed 1,1,1,2-Tetrachloroethane SW 846 method8260B/5030B <0.5pg/L 09/29/2020 1, 1, 1 -Trichloroethane SW 846 method 8250B15030B <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 846 method 8260815030E <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,1-Dichloroethane SW 846 method 8280B/50308 <0.5 pg/L 09/29/2020 1,1-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1, 1 -Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2, 3-Trichlorobenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2,3-Trichloropropane SW 846 method 8280B/50308 <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 848 method 8260B/5030B <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 646 method 8260B/5030B <0.5 pg/L 09/29/2020 1,3-Dichlorobenzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 8260815030E <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 16 of 21 Environmental Chemists, Inc, i 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 Chloroform SW 846 method 8280BI5030B 3.23 pg/L 09/29/2020 Ch loromethane SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 cis- 1,2-Dichloroethene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 cis- 1,3-Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 82606/50308 <0.5 pg/L 09/29/2020 Dibromomethane SW 845 method 8260B/5030B <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Isopropylbenzene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 8260815030B <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 826013/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 sec-Butylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 826013/5030B <0.5 pg/L 09/29/2020 tert-Butyl benzene SW 846 method 82BOB15030B <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 8260815030E <0.5 pg/L 09/29/2020 Report C 2020-16323 Page 17 of 21 6envirocheF 7 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 826OB/5030B <0.5 pg/L 09/29/2020 Trans- 1,2-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans-1,3-dichloropropene SW 846 method 82BOB/50308 <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 8260815030E <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 18 of 21 envirochem ANALYTICAL & CONSULTING CHEMISTS Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Lao lu Sample ID: 20-41804 Site:07 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Collect Date/Time Matrix Sampled by 9/24/2020 2:25 PM Water Client Test Method Results Date Analyzed 1, 1, 1,2-Tetrachloroethane SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 1,1,1-Trichloroethane SW 846 method 8260815030E <0.5 pg/L 09/29/2020 1,1,2,2-Tetrachloroethane SW 646 method 82808/50308 <0.5 pg/L 09/29/2020 1,1,2-Trichloroethane SW 84e method 826013/503013 <0.5 pg/L 09/29/2020 1,1-Dichloroethane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1, 1 -Dichloroethene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 1,1-Dichloropropene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2,3-Trichlorobenzene SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 1,2, 3-Trichloropropane SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,2,4-Trichlorobenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 1,2,4-Trimethylbenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,2-Dibromo-3-Chloropropane SW 846 method 8280B/50308 <0.5 pg/L 09/29/2020 1,2-Dibromoethane SW 846 method 82BOB/5030B <0.5 pg/L 09/29/2020 1,2-Dichlorobenzene SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 1,2-Dichloroethane SW 846 method 82608/503013 <0.5 pg/L 09/29/2020 1,2-Dichloropropane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,3,5-Trimethylbenzene SW 846 method 826013I5030B <0.5 pg/L 09/29/2020 1,3-Dichlorobenzene SW 846 method 62608/50308 <0.5 pg/L 09/29/2020 1,3-Dichloropropane SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 1,4-Dichlorobenzene SW 846 method 8260B150308 <0.5 pg/L 09/29/2020 2,2-Dichloropropane SW 846 method 826013/503013 <0.5 pg/L 09/29/2020 2-Chlorotoluene SW 846 method 8260B150308 <0.5 pg/L 09/29/2020 4-Chlorotoluene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Benzene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Bromobenzene SW 846 method 82606/503013 <0.5 pg/L 09/29/2020 Report #:: 2020-18323 Page 19 of 21 Fool", Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. 219 South Steele St. Sanford NC 27330 Attention: Date of Report: Oct 05, 2020 Customer PO #: Customer ID: 12090010 Report #: 2020-16323 Project ID: 2009-195 Bromochloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromodichloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromoform SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Bromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Carbon tetrachloride SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Chlorobenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Chloroethane SW 846 method 82608/50308 <0.5 pg/L 09/29/2020 Chloroform SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Chloromethane SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 cis- 1,2-Dichloroethene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 cis-1, 3-Dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromochloromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dibromomethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Dichlorodifluoromethane SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Ethylbenzene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Hexachlorobutadiene SW 846 method 8260B15030B <0.5 pg/L 09/29/2020 Isopropylbenzene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 M+P Xylene SW 846 method 8260B/5030B <1.0 pg/L 09/29/2020 Methylene chloride SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Naphthalene SW 846 method 826OB15030B <0.5 pg/L 09/29/2020 n-Butylbenzene SW 846 method 82609/5030B <0.5 pg/L 09/29/2020 n-Propylbenzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 ortho-Xylene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 p-Isopropyltoluene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 sec -Butyl benzene SW 846 method 8280B/5030B <0.5 pg/L 09/29/2020 Styrene SW 846 method 826013/50308 <0.5 pg/L 09/29/2020 tert-B utyl benzene SW 845 method 826OB15030B <0.5 pg/L 09/29/2020 Tetrachloroethene SW 846 method 8260B/50308 <0.5 pg/L 09/29/2020 Report #:: 2020-16323 Page 20 of 21 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Cameron Testing Services, Inc. Date of Report: Oct 05, 2020 219 South Steele St. Customer PO #: Sanford NC 27330 Customer ID: 12090010 Attention: Report #: 2020-16323 Project ID: 2009-195 Toluene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans-1,2-Dichloroethene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trans-1,3-dichloropropene SW 846 method 8260B/5030B <0.5 pg/L 09/29/2020 Trichloroethene SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Trichlorofluoromethane SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Vinyl chloride SW 846 method 82608/5030B <0.5 pg/L 09/29/2020 Comment: Reviewed by: Report #:: 2020-16323 Page 21 of 21 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.3S2.0223 Sample( Receipt Checklist Client: �W TE:f l ( N 6— Date: ` `( U Report Number:Q Receipt of sample: Delivered UPS ❑ FeclEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES 113 NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES I0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES 113 NO 4. Were proper custody procedures (relinquished/received) followed? YES ID NO 5. Were sample ID's listed on the COC? YES 113 NO 1 6. Were samples ID's listed on sample containers? YES ❑ NO 1 7. Were collection date and time listed on the COC? JZ YES 10 NO 1 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? tX YES 10 NO 10. Did samples arrive in good condition for each test? 5? YES 10 NO 11. Was adequate sample volume available?' 4d YE S 10 NO 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES 10 NO 14. Were cyanide samples received at a pH >12? ❑ YES I ❑ NO 115. Were sulfide samples received at a pH >9? ❑ YES 101 ❑ YES ❑ NO 116. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *' NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. * * Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): HzSO, HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediate!y for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: Dnr nA nm 4M Analytical & Consulting Chemists CLIENT: Cameron Testing Services ADDRESS: 219 S. Steele St. Sanford NC, 27330 Sampled Bv: ENVIRONMENTALCHEMISTS, INC OFFICE: 910I392-0 23FAX910-3 9-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME: o�OO�I- �7� REPORT NO:� ` �3 CONTACT NAME: PO NO: REPORT TO: Chris Cameron PHONE/FAX: SAMPLE TYPE: 1 = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil SL = Sludge Other: Sample Identification Collection a f' n. E W a O E ° cD ° _ C C7 _ ° 0 4 L C J L E " a W a E � n z PRESERVATION ANALYSIS REQUESTED Date Time Temp - p x o' $ Z _ = O `_ o W x o ro. /9� ` / /S C P ���g EPi# CVAS/0d -P9-4.5"--oa c P c P c P c P p1� �� 9 i9s446 - C PS 3 ZS- c P dK . / ' -� � ©M Transfer Rel quished By: Date/Time eceived By: Date/Time 1. L 1 2. Temperature when Received: Accepted: Rejected: Resample Requested: Delivered By: ,� Received B r Y _- Date Comments: Time: ILG� TURNAROUND: 219 S. Steele Str- Sanford, NC 27330 Cameron Testing Services, Inc. Chain of Custody Phone: 919-208-4240 NC WW/GW Cert. #654 INC PHHS Cert # 37799 US EPA NC01918 Page of Company: ; J-ordan Lake SRA Email: william.baker@ncparks.gov CTS lab use — - Office-919-362-0586/Cell-919-218-0117 °"°t= William Baker ,Phone: -- ---- Sample Temp i f (C) Lab ID i Address (City,280 State Parks Road Fax: Ice (Y/N) State, Zip), Apex, NC 27523 Notes: Permit (Y/N) 111 — Project: MWS - IMF Tl�� ^L ----- Rush ii (Y/N) Due: Collected: Name: Signature: Sample Information Number of bottles Requested Analysis Sample ID o 4) E o- E� x .� I Z >- m o `° I o i a� a I L Preservatives: U n reserved, H(C)I, O p CTS Lab V N ICl) C' I 1 O I O H2(S)04, H(N)03, (Na)Thiosulfate, Na(0)H, ID a i m > I Other (X), Indicate Chloride, TOS, NO2 i ; NH3, NO3 1S 1 Z if 1 Na _ Fec-W - Z4 I 113 I TOC --- -- 8260 (Sept only) 0 5 fi---- Field pH, temp, water level 0-7 MWs sampled Mar. June, Sept. Reli ais- „ Received: Date/Time Z,Z 94-14S O Rush work will require prior approval. Additional charges will apply GW-59A COMPLIANCE REPORT FORM Permit # 129 (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. ( ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NSY IF the answer to question f or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES N If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby ac nowledge that the above information was evaluated and the information submitted in this repo (Co pliance Report GW-59A) is true and complete to the best of my knowledge. I R y i s , Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: �1617 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004122 Expiration Date: June 2020 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC June 2020 Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex NC 27523 County Chatham ❑ Lagoon g El Remediation: Infiltration Gallery .,,evsrta; - ❑� Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ❑ Rotary Distributor ElLand Application of Sludge Well Location/Site Name: Poplar Point No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 09/22/2020 FIELD ANALYSES: WAS Well Depth: 23.0 ft. Well Diameter: 2 in. pH 00400: 4.58 units Temp. 000lo: 17.3 °C DRY at Depth to Water Level 82546: 19.0 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 2.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ■❑ NO and field acidified: ❑ YES ■❑ NO LABORATORY INFORMATION Date sample analyzed: 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.050 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 34.0 mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC om8o <1.00 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 1.97 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia 0o6lo <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH. as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: � � - DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM �1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00004122 Expiration Date: June 2020 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC June 2020 Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex NC 27523 County Chatham ❑ Lagoon g ❑Remediation: Infiltration Gallery 11ej ❑■ Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Poplar Point No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 09/22/2020 FIELD ANALYSES: WAS Well Depth: 22.2 ft. Well Diameter: 2 in. pH 00000: 6.72 units Temp. 000lo: 20.5 °C DRY at Depth to Water Level 82546: 5.0 p ft. below measuring point Screened Interval: ft. to _ft. Spec. Cond. 000sa: µ Mhos time of sampling, Measuring Point is 2•5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 9 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed: 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N o0620 0.118 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 457 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 7.13 mg/L Ca - Calcium 00916 mg/L Chloride 00940 50.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia oo6lo <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 uglL , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00004122 Expiration Date: June 2020 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC June 2020 Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex NC 27523 County Chatham ❑ Lagoon g El Remediation: Infiltration Gallery ty�+=�e; _ IN Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: Poplar Point No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 09/22/2020 FIELD ANALYSES: WAS Well Depth: 36 ft. p Well Diameter: 2 in. pH ooaoo: 6.29 units Temp. 00010: 16.3 °C DRY at Depth to Water Level 82546: 20.3 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 7.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES K NO LABORATORY INFORMATION Date sample analyzed. 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.050 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 805 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.90 mg/L Ca - Calcium 00916 mg/L Chloride 00940 4.93 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia oo610 <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total) Mn - Manganese oloss ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly orType PERMIT Number: W00004122 Expiration Date: June 2020 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC June 2020 Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex "" NC 27523 County Chatham ❑ Lagoon ❑ Remediation: Infiltration Gallery _. ) s," e' ❑■ Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: Poplar Point No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: (from Pemrt SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 09/22/2020 FIELD ANALYSES: WAS Well Depth: 53.5 ft. Well Diameter: 2 in. pH 00000: 7.26 units Temp. 000lo: 16.8 °C DRY at Depth to Water Level 82546: 27.6 ft. below measuring point Screened Interval: ft. to — ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 5.25 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES K NO LABORATORY INFORMATION Date sample analyzed: 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.050 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 447 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC omm 3.59 mg/L Ca - Calcium 00916 mg/L Chloride 00940 108 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? W Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia 000lo <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • _EWE DEPARTMENT OF ENVIRONMENT &NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0004122 Expiration Date: June 2020 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC June 2020 Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex "" NC 27523 County Chatham ❑ Lagoon g El Remediation: Infiltration Gallery �c,v) `�t���" ` ❑■ Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: Poplar Point No. of wells to be sampled: 7 ❑ Water Source Heat Pump ❑ Other: from Perrnit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-5 Date sample collected: 09/22/2020 FIELD ANALYSES: WAS Well Depth: 49.0 ft. Well Diameter: 2 in. pH oo400: 6.63 units Temp. 000lo: 16.8 °C DRY at Depth to Water Level 82546: 39.3 p ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 0009a: µ Mhos time of sampling, Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 1.75 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed: 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.240 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 150 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.35 mg/L Ca - Calcium 00916 mg/L Chloride 00940 8.37 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? A Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia oo610 <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3asN. Ammonia Nitrogen, Total) Mn -Manganese oloss ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Jordan Lake State Recreational Area Permit Name (if different): Facility Address: 280 State Parks Road Apex Contact Person: William Baker Well Location/Site Name: NC 27523 County Chatham Poplar Point Telephone#: 919-362-0586 No. of wells to be sampled: 7 PARTMENT OF ENVIRONMENT & NATURAL RESOURCES VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 07 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 ERMIT Number: W00004122 Expiration Date: June 2020 on -Discharge UIC June 2020 PDES Other YPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-6 Date sample collected: 09/22/2020 Well Depth: 38.0 ft. Well Diameter: 2 in. Depth to Water Level 82546: 27.0 ft. below measuring point Screened Interval: ft. to ft. Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 6 gallons Samples for metals were collected unfiltered: El YES ■❑ NO and field acidified: ❑ YES © NO FIELD ANALYSES: pH 0040o: 5.74 units Temp. 000lo: 17.3 °C Spec. Cond. 00094: µMhos Odor 00085: Appearance If WELL WAS DRY at time of sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: 09/22-29/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.050 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 113 mg/L AI - Aluminum oil o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.44 mg/L Ca - Calcium 00916 mg/L Chloride 00940 19.2 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia oo610 <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY WAS DRY at time of sampling, check here: OUNDWATER QUALITY MONITORING: MPLIANCE REPORT FORM Name: Jordan Lake State Recreational Area Name (if different): Address: 280 State Parks Road Apex IContact Person: William Baker Well Location/Site Name: NC 27523 Poplar Point or Type County Chatham Telephone#: 919-362-0586 No. of wells to be sampled: 7 SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-7 Date sample collected: 09/22/20220 Well Depth: 26.5 ft. Well Diameter: 3 in. Depth to Water Level 82546: 19.0 ft. below measuring point Screened Interval: ft. Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 3.75 gallons DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 PERMIT Number: W00004122 Expiration Date: June 2020 Non -Discharge UIC June 2020 NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge to _ ft. ft. Samples for metals were collected unfiltered: ❑ YES K NO and field acidified: ❑ YES ■❑ NO ❑ Water Source Heat Pump ❑ Other FIELD ANALYSES: pH 000lo: 6.37 units Spec. Cond. 00094: Odor 00085: Appearance Temp. 000lo: 17.3 °C uMhos ite sample analyzed: 09/22/2020 Laboratory Name: Cameron Testing Services/Environmental Chemists Certification No. #654 1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.088 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 70300 211 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 2.16 mg/L Ca - Calcium 00916 mg/L Chloride 00940 18.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (1) ❑ No (0) ecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # 8260B Total Ammonia oo610 <0.100 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH, as N. Ammonia Nitrogen, Total) Mn - Manganese oloss ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Baker, Authorized Agent Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010