WQ0031725_Regional Office Historical File Pre 2018 (2)

a
S Southern
S Soil
$ Builders, Inc.
958 Hoots Road Roaring River, NC 28669
[phone] 9 Fax [phone]
AUG 1 5 20 � 07
Thursday, August 09, 2007
-arotection
Chonticha McDaniel
Land Application Unit
1636 Mail Service Center
Raliegh, NC 27699-1636
Subject: Baxter Healthcare Land Application Permit
Enclosed is the acknowledgement letter that I got from Lincoln County acknowledging
that fields S-1, S-2, and T-1 and T-2 will no longer be in their land application program.
If there are any further questions or concerns, feel free to contact me at any time, at (336)
957-8909 or at [e-mail]
Sincerely,
Zach ey rVI
Southern Soil Builders, Inc. ;� , = '''
w)

To Whom It May Concern:
We acknowledge that Fields S-1, S-2 and T-1, T-2 are being dropped from our land
application program, We only used these fields once and due to the availability of land
closer and more accessible to the waste treatment plants, we will not need these fields for
land application.
(4

e ' AQUIFER PROTECTION Q REGIONAL STAFF REPORT
Date: 08/13/07 i coo py County: Catawba
To: Aquifer Protection Central Office Permittee/Owner: Baxter Healthcare Corp.
Central Office Reviewer: Chonticha McDaniel Application No.: W00031725
L GENERAL INFORMATION
1. This application is (check all that apply): ❑ New ® Renewal ❑ Renewal with mod.
❑ Minor Modification ❑ Major Modification
❑ Surface Irrigation ❑ Reuse ❑ Recycle ❑ High Rate Infiltration ❑ Evaporation/Infiltration Lagoon
® Land Application of Residuals ❑ Attachment B included ❑ 503 regulated ® 503 exempt
❑ Distribution of Residuals ❑ Surface Disposal
❑ Closed -loop Groundwater Remediation ❑ Other Injection Wells (including in situ remediation)
Was a site visit conducted in order to prepare this report? ❑ Yes or ❑ No.
a. Date of site visit: August 1, 2007
b. Person contacted and contact information: Zach Key, 336/957-8909
c. Site visit conducted by: Ellen Huffman
d. Inspection Report Attached: ❑ Yes or ® No.
2. Is the following information entered into the BIMS record for this application correct?
® Yes or ❑ No. If no, please complete the following or indicate that it is correct on the current application.
For Treatment Facilities: NPDES Permit #NC0006564
a. Location: Hwy 221 N, Pitts Station Road. 828/756-6618
b. Driving Directions:
c. USGS Quadrangle Map name and number:
d. Latitude: Longitude:
e. Regulated Activities / Type of Wastes (e.g., subdivision, food processing, municipal wastewater):
For Disposal and Iniection Sites: See application.
a. Location(s):
b. Driving Directions:
c. USGS Quadrangle Map name and number:
d. Latitude: Longitude:
FORM: WQ0031725 Baxter LA 08 2007 1

AQUIFER PROTECTION REGIONAL STAFF REPORT
III. RENEWAL AND MODIFICA77ONAPPLICA77ON
Description Of Waste(S) And Facilities
1. Are there appropriately certified ORCs for the facilities? E Yes or ❑ No.
Operator in Charge: Dennis Key Certificate #: 15704
Backup- Operator in Charge: Zach Key Certificate #: 27660
2. Is the design, maintenance and operation (e.g. adequate aeration, sludge wasting, sludge storage, effluent
storage, etc) of the treatment facilities adequate for the type of waste and disposal system? ❑ Yes or ❑ No.
The wastewater treatment facilities are located in the Asheville Region. The ARO is going to supply compliance
data on the already permitted wastewater treatment plant (NPDES Permit #NCO00656i The application fields
are located in the AMO. The fields are currently permitted for another facility.
3. Are the site conditions (soils, topography, depth to water table, etc) maintained appropriately and adequately
assimilating the waste? ® Yes or ❑ No. If no, please explain:
4. Has the site changed in any way that may affect permit (drainage added, new wells inside the compliance
boundary, new development, etc.)? ❑ Yes or ® No. If yes, please explain:
5. Is the residuals management plan for the facility adequate and/or acceptable to the Division?
® Yes or ❑ No. If no, please explain:
6. Are the existing application rates (hydraulic or nutrient) still acceptable? ® Yes or ❑ No. If no, please
explain:
7. Is the existing groundwater monitoring program (number of wells, frequency of monitoring, monitoring
parameters, etc.) adequate? ❑ Yes ❑ No ® N/A.
8. Will seasonal or other restrictions be required for added sites? ❑ Yes ® No ❑ N/A
9. Are there any buffer conflicts (treatment facilities or disposal sites)? ® Yes or ❑ No. The maps provided
were old and inadequate. New maps were requested and received by AMO. These maps were not much of an
improvement. The new maps will be sent up with this report.
10. Is the description of the facilities, type and/or volume of waste(s) as written in the existing permit correct?
® Yes or ❑ No. If no, please explain:
11. Were monitoring wells properly constructed and located? ❑ Yes or ❑ No ® N/A.
12. Has a review of all self -monitoring data been conducted (GW, NDMR, and NDAR as applicable)? ® Yes or
❑ No ❑ N/A. Please summarize any findings resulting from this review:
13. Check all that apply: ® No compliance issues; ❑ Notice(s) of violation within the last permit cycle; ❑
Current enforcement action(s) ❑ Currently under SOC; ❑ Currently under JOC; ❑ Currently under
moratorium.
14. Have all compliance dates/conditions in the existing permit, (SOC, JOC, etc.) been complied with? ❑ Yes
❑ No ❑ Not Determined ® N/A.. If no, please explain:
FORM: WQ0031725 Baxter LA 08 2007 2

AQUIFER PROTECTION REGIONAL STAFF REPORT
15. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit?
❑ Yes or ® No ❑ N/A. If yes, please explain:
V. EVALUATIONAND RECOMMENDATIONS
1. Provide any additional narrative regarding your review of the application.:
The wastewater treatment facilities are located in the Asheville Region. Keith Haynes with ARO can supply
compliance data on the permitted wastewater treatment plant (NPDES Permit #NC0006564). The application
fields are located in the MRO. The fields are currently permitted for another facility. Documentation was
received (August 10) regarding the transfer to these fields to the proposed Baxter Corp. program, however, it
was not on County letterhead, therefore, no means to confirm the authority of the request. The Central Office
can request another letter to clan fy, if needed. The data submitted by Pace analytical was unclear. I could not
find sour test results, total solids, or calculations for volatile solids reduction, and the TCLP was accompanied
with a letter from the lab that the test was run out of recommended hold time. Please see items], 2, and 3 of
page 29 (of 29) from Pace Analytical located in the original application package. The original application
package did not have adequate maps for the proposed sites. Replacement maps (included with this report)
were received on July 18, 2007.
2. -, Attach Well Construction Data Sheet - if needed information is available
3. Do you foresee any problems with issuance/renewal of this permit? ❑ Yes ® No. If yes, please explain
briefly. see comments in W.
4. List any items that you would like APS Central Office to obtain through an additional information request.
Make sure that you provide a reason for each item: See comments in #1.
None
5. List specific Permit conditions that you recommend to be removed from the permit when issued. Make sure
that you provide a reason for each condition: None.
6. List specific special conditions or compliance schedules that you recommend to be included in the permit when
issued. Make sure that you provide a reason for each special condition: None.
7. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office; ❑ Hold,
pending review of draft permit by regional office; ® Issue upon receipt of needed additional information; ❑
Issue; ❑ Deny. If deny, please state reasons:
8. Signature of report preparer(s):
Signature of APS regional super
Date: Q f - / ( - C) '-�
ADDITIONAL REGIONAL STAFFREVIEWITEMS
None
FORM: WQ0031725 Baxter LA 08 2007

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Baxter 0 D a' ?, Soil
SCALEI" = 1320
CVitCKLUBY ,. Land Application Program Survey
uw�wn' uv BRANCH Derek Teague Farm Vl ap
RTB RESIDUALS
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1 of 1 7/17/2007 11:13 AM

Vd A TF
Michael F. Easley, Governor
O� QG r William G. Ross Jr., Secretary
i DE North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
�r
k1 . ---
Aquifer Protection Section
June 19, 2007
Mr. Zach Key
Southern Soil Builders
958 Hoots Rd.
Roaring River, North Carolina 27604
Subject: Application No. WQ0031725
Baxter Healthcare Corp.
Land Application of Residual Solids
McDowell County
Dear Mr. Key:
In accordance with your permit request received April 19, 2007, the Division is requesting additional
information to complete the review of permit No. WQ0031725, for Baxter Healthcare Corp., Land Application of
Residual Solids.
The following additional information is required before permitting can continue:
1. A delegation letter of signing official for Mr. Gouge. According to 15A NCAC 2T .0106 (b)(1),
the application must be signed by a principal executive officer of at least the level of vice-president, or
his authorized representative.
2. Acknowledgement of field transfer from Permittee relinquishing field.
3. Acknowledgement of field transfer from Land Owner. Fields may not be permitted to multiple Permitees
over the same time period.
After review of the permit package it was noted that the field mapping is inadequate. Please see mapping guidance
and examples of maps to be submitted, enclosed with this additional information request.
Two copies of the required additional information (noted above) shall be submitted to Chonticha McDaniel
at the Divisions' Central Office by July 19, 2007. Two copies of the maps should be submitted to the
Mooresville Regional Office. A land review will be scheduled when the maps are received.
If you need additional information concerning this matter or will be unable to meet the required deadline,
please contact Chonticha Mc Daniel at [phone] or Ellen Huffman at [phone].
Sin rely,
f
Ellen Huffman
Mooresville Regional Office
cc: Stephan Gouge, Baxter Healthcare
Chonticha McDaniel, Central Office
EH
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] NcoxthCarolina
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Internet: www.ncwaterraualitv.org Naturallff

V'LJL-, J
AOUIFER PROTECTION SECTION`( 2 3 20
APPLICATION REV II I
Date: May 22, 2007 U
To: ® Landon Davidson, ARO-APS JUN 18 21U D ay, WaRO-APS
❑ Art Barnhardt, FRO-APS ❑❑ C rlie tehman, WiRO-APS
❑ Andrew Pitner, MRO-APS NC DERi� fv1 rri 'ght, WSRO-APS
❑ Jay Zimmerman, RRO-APS DWQ - Aquifer Protection
From: Chonticha McDaniel, Land Application Unit
Telephone: [phone] Fax: [phone]
E-Mail: [e-mail]
A. Permit Number: W00031725
B. Owner: Baxter Healthcare Corporation
C. Facility/Operation: Baxter Healthcare Corporation
® Proposed ❑ Existing ❑ Facility ® Operation
D. Application:
1. Permit Type: ❑ Animal ❑ Surface Irrigation ❑ Reuse ❑ H-R Infiltration
❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND)
❑ UIC - (5QW) closed loop water only geothermal
For Residuals: ® Land App. ❑ D&M ❑ Surface Disposal
® 503 ❑ 503 Exempt ❑ Animal
2. Project Type: ® New ❑ Major Mod. ❑ Minor Mod. ❑ Renewal ❑ Renewal w/ Mod.
E. Comments/Other Information: ❑ I would like to accompany you on a site visit.
Attached, you will find all information submitted in support of the above -referenced application for your
review, comment, and/or action. Within 30 calendar days, please take the following actions:
Ll
�Ret Coo p etecllForm St--
❑ Attach Well Construction Data Sheet.
❑ Attach Attachment B for Certification by the LAPCU.
❑ Issue an Attachment B Certification from the RO*.
* Remember that you will be responsible for coordinating site visits, reviews, as well as additional
information requests with other RO-APS representatives in order to prepare a complete Attachment B for
certification. Refer to the RPP _SOP for additional detail.
When you receive this request form, please write your name and dates in the spaces below, make a copy
of this sheet, and return it the approprie 9fitral Office -Aquifer Protection Section contact person
listed above.
RO-APS Reviewer: Date: —7
FORM: APSARR 02/06 Page 1 of 1

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
May 15, 2007
Stephen Gouge D
Baxter Healthcare Corporation
PO Box 1390
Marion, NC 28752 JUN 1 8 2007
Subject: Acknowledgement of Application No. WQ0031725
Baxter Healthcare Corporation MC DENR MRO
Land Application of Residual Solids (503) DWQ -A i:ifer Protection
McDowell
Dear Mr. Gouge:
The Aquifer Protection Section of the Division of Water Quality (Division) acknowledges receipt of your permit
application and supporting materials on April 19, 2007. This application package has been assigned the number
listed above and will be reviewed by Chonticha McDaniel.
The reviewer will perform a detailed review and contact you with a request for additional information if necessary.
To ensure the maximum efficiency in processing permit applications, the Division requests your assistance in
providing a timely and complete response to any additional information requests.
Please be aware that the Division's Regional Office, copied below, must provide recommendations prior to final
action by the Division. Please also note at this time, processing permit applications can take as long as 60 - 90 days
after receipt of a complete application. To check on the status of your application, you can visit
hILtp://h2o.enr.state.nc.us/bims/reports/repoitsPerrnits.html.
If you have any questions, please contact Chonticha McDaniel at 919-715-6188, or via e-mail at
[e-mail]. If the reviewer is unavailable, you may leave a message, and they will respond
promptly. Also note that the Division has reorganized. To review our new organizational chart, go to
httn•//h2o.enr.state.nc.us/documents/dwq orgchart.ydf.
PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES ON THIS
PROJECT.
Sincere y,
for Kim Colson, P.E.
Supervisor
cc: Asheviille R giA al C -1173 , Aquifer PT7?ect0 , Sectit5,
Dennis Key, Southern Soil Builders, Inc.
Permit Application File WQ0031725
Aquifer Protection Section 1636 Mail.Service Center . Raleigh, NC 27699-1636
Internet: www.ncwatereuality.orp Location: 2728 Capital Boulevard Raleigh, NC 27604
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper
Noe Carolina
�turdip,
Telephone: [phone]
Fax 1: [phone]
Fax 2: [phone]
Customer Service: [phone]

0- 1 •. N

S
S
B
Southern
Soil
Builders, Inc.
958 Hoots Road Roaring River, NC 28669
[phone] 9 Fax [phone]
DAUG- 62007D
Thursday, August 02, 2007
Ellen Huffman
Mooresville Regional Office
NC Dept. of Environment & Natural Resources
610 East Center Ave, Suite 301
Mooresville, NC 28115
Subject: Update Maps. for Baxter Healthcare
Enclosed are the updated maps for fields S-1 and S-2. I have buffered out the areas
behind the trees in S-2 were I sunk my Jeep. If there are any questions or concerns feel
free to contact me.
_I P "�
Zach Key
Southern Soil -Builders, Inc.

S Southern �
s Soil
BI Builders, Inc. '
M
FILE
958 Hoots Road Roaring River, NC 28669
[phone] • Fax [phone]
Southern Soil Builders, Inc, is under contract to provideMaxtere 1tcCarporation
with land application services. The 4 fields we are going to use for Baxter's land
app ica ion program are ocated in Catawba County. These fields are going to be
transferred from Lincoln County's program. I have enclosed maps of the fields for a
watershed classification. This is will be a new program and does not have a permit
number. I have also enclosed the previous watershed classification for these four fields if
that will be of any assistance to you.
If there is any. questions or concerns, feel free to contact me at anytime.
Zach Key
Southern Soil Builders, Inc.
�srw"9,(7
CCT 1 8 2001

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
WATERSHED CLASSIFICATION ATTACHMENT
FOR RESIDUALS PROGRAMS
(THIS FORMMAY BE PHOTOCOPIED FOR USE ASAN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to follow the instructions or to submit all of the
required items will lead to additional application processing and review time.
For more information or for an electronic version of this form, visit our site at : http:/,,%2o. enr.state. nc. uY/ndpui"
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application
form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare the attachment form with the requested information for each location where the residuals
program activities are planned to occur within a particular regional office county coverage.
✓ Additional copies of Page 2 of 2 of this attachment form may be used if necessary.
✓ Use a portion of an 8.5-inch by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to
identify the location where the residuals program activities are planned to occur as well as the closest
downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and
number, the identified location, and be of clear and reproducible quality.
✓ Latitudes and longitudes must reported as being based on either the NAD 27 or the NAD 83 data systems.
✓ Acceptable methods of determining location latitudes and longitudes and their corresponding codes are as
follows:
♦ Address Matching (ADD) ♦ Digital or Raw Photo Extraction (EXT)
♦ Aerial Photography with Ground Control (AER) ♦ Geodetic Quality GPS Survey (GEO)
♦ Cadastral Survey (SUR) ♦ LORAN-C Navigation Device (LOR)
♦ Conversion from Coordinate Plane (CP) ♦ Navigation Quality GPS (GPS)
♦ Conversion from Township -Section -Range (TSR) ♦ Remote Sensing (RS)
♦ Conversion from Universal Trans Merc (UTM) ♦ Zip Code Centroid (ZIP)
♦ Map Interpretation by Digital or Manual Extraction (MAP)
✓ Location accuracy must be provided to the nearest unit (e.g., nearest second, tenth of a second, etc.).
C. Mail or fax the attachment form and the map portions to the appropriate regional office for review and
to obtain the waterbody and classification information.
✓ A list of the Division's regional offices, their county coverage, and their contact information may be
downloaded from the web site at: http://h2(i.enr.state.nc.us/ndpu/.
✓ The Division will not consider this attachment form to be complete until it is completed by the appropriate
regional office.
To: Regional office: Mooresville Regional Office
Address of regional office: 919 North Main Street
City: Mooresville State: NC Zip: 28115
Facsimile number: (_704_) 663
Please provide me with the waterbody name(s), stream index number(s), and current/proposed
classification(s) of the surface waters that are closest to . and downslope from the location(s) where the
proposed residuals program activities, aKe planned to occur, as identified on the attached map segment.
Signature of regional office staff:-' � Date:
t
FORM: RWSCA 02/02 Page 1 of 2 Attachment Order 3-
a 1 "

Location
ID
County
Latitude
Longitude
Location
Datum
Location
Method
Code
Location
Accuracy
Waterbody Subbasin and
Stream Index No.
(To Be Completed by DWQ)
Current and
Proposed Class
(To Be Completed
by DWQ)
S-1
Catawba
3503759.86"N
81004'26.70"W
NAD27
MAP
± 1"
r-'' c
tJ= 1°C I `
WS-1V
S-2
T-1
Catawba
Catawba
35037'50.04"N
35037'19.21"N
81004'41.69"W
81005'36.83"W
NAD27
NAD27
MAP
MAP
±1"
± 1"
, t'
WS-IV
WS-1v
T-1
Catawba
35037'33.75"N
81005'47.13"W
NAD27
MAP
±1"
WS-IV
FORM: RWSCA 02/02
* * * END OF FORM RWSCA 02/02 * * *
Page 2 of 2
Attachment Order 3-

S Southern
S Soil
g Builders, Inc.
958 Hoots Road Roaring River, NC 28669
[phone] . Fax [phone]
D JUN 1 8 2007 D
March 2, 2007
North Carolina Department of Environmental and Natural Resources
Division of Water Quality
Aquifer Protection Section
Land Application Unit
2728 Capital Boulevard
Raleigh, North Carolina 27604
Reference: APPLICATION FOR LAND APPLICATION PERMIT
Baxter Healthcare Corporation
Residual Solids Management Program
Southern Soil Builders, Inc is under contract with Baxter Healthcare to provide assistance
in the preparation of a land application permit application for Baxter Healthcare
Corporation.
Your attention in the review of this permit application will be greatly appreciated. Please
contact us immediately with any questions, concerns, or additional information.
Sincerely,
f � _
Zach Key
Southern Soil Builders, Inc.
RECEIVED / DENR / DWQ
AQUIFFR-PRnTFrr,naj SECTION
APR 1 ZUUI

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM
(FORM: NDRLAF 10-06)
The Division of Water Quality will not accept this application unless all the instructions are followed. Failure to
submit all of the required items will lead to additional processing and review time.
For more information, visit our web site at: http:1'l12o.enr.state.nc.itsllaithizain.hbrzl
A. Application Form: (All Application Packages):
✓ Submit one original and two copies of the completed application package. Any changes made to this form will result in the
application being returned. The Division of Water Quality will only accept application packages that have been fully
completed and all applicable items are addressed.
✓ Non -dedicated residuals land application programs are ones in which all land application sites do not meet the criteria in
15A NCAC 2T .1102(12). Specifically, a residuals land application program cannot be designated as non -dedicated if any
of the following is applicable:
e Any land application site certified for the residuals land application program that receives residuals at rates or
frequencies greater than agronomic rates.
e Any land application site certified for the residuals land application program that is used primarily for residuals
disposal, and agricultural crop production is of secondary importance.
e Any land application site certified for the residuals land application program that receives residuals through fixed
irrigation facilities or irrigation facilities fed through a fixed supply system.
✓ The signing official must meet the criteria stipulated in 15A NCAC 2T .0106(b). An alternate person may be designated as
the signing official, provided that a delegation letter from a person who meets the referenced criteria is submitted. The
delegation letter does not have to be resubmitted if the signing official has not changed since the last permitting action
associated with this residuals land application program.
✓ If this project involves a modification of an existing permit, submit one copy of the existing permit.
✓ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages):
✓ For new permits submit a check in the amount of $1,090 if over or equal to 300 acres of land required or $675 if less than
300 acres of land required, made payable to: North Carolina Department of Environment and Natural Resources
(NCDENR). Major modification fee are $325 and $205, respectively
C. Cover letter (All Application Packages)
✓ Submit a cover letter, which lists all items and attachments included in the application package as well as a brief project
description.
✓ If necessary for clarity, include attachments to the application form. Such attachments will be considered part of the
application package and should be numbered to correspond to the section to which they refer.
D. Environmental Assessments (Maybe Required— See 15A NCAC 1C .0300):
✓ Submit one copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also,
include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of
the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or
lands are used for the construction of the subject facilities.
E. Submission of Application Packages:
✓ To determine which attachment forms and supplemental attachments are required to make a complete application package,
read the instructions of each attachment form carefully. Application packages should be organized and bound (i.e., stapled,
placed in three-ring binder, etc.) in the following order prior to submission:
® Cover letter and application fee.
® Attachment Order 1: Non -Dedicated Residuals Land Application Programs (FORM: NDRLAP 10-06).
➢ Attachment Order 1-a: Signing official delegation letter.
Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA 10-06).
m Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA 10-06).

✓ The application package should be sent to the address at the end of this application form. Do not submit this application
package to any Division regional office.
i:0-IR is i'dDRLAP 10-06 Pag, sit 6 Attacnment Ordcr L

Sbwte of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAMS
(FORM: NDRLAP 10-06)
(THIS FORMMAYBEPHOTOCOPIED FOR USEASANORIGINAL)
Application Number: (to be completed by DWQ)
RECEIVED / DEAR i DVVQ
L OWNERSHIP INFORMATION: AQUIFER-PRnTF('TI(ln1 SECTION
1. Specify whether the process facility is owned by: APR 19 2007
❑ County; ❑ Federal; ❑ Municipal; ❑ State; ® Non -Government.
IL
tj
Owner's name (please specify the name of the municipality, corporation, individual, etc.)
Baxter Healthcare Corporation
Mailing address: PO Box 1390
City: Marion State: NC Zip: _28752
Physical address: Hwy 221N, Pitts Station Road
City: Marion State: NC Zip: 28752
Telephone number: ( 828_) _756-6618 Facsimile number: ( 828 ) _756-4821
E-mail address: [e-mail]
3. Signing official's name and title: (See Instruction A)
Stephen Gouge, Waste Water Treatment Supervisor
Mailing address: PO Box 1390
City: Marion State: NC
Physical address: Hwy 221N, Pitts Station Road
City: Marion Telephone number: ( 828_) _756-6618
E-mail address: [e-mail]
PERMIT INFORMATION:
Zip: 28752
Facsimile number: ( 828 ) 756-4821
1. Application is for: ® new, ❑ modified, ❑ renewed permit (check all that apply).
2. Fee Submitted: $ 675.00 (See' Instruction B)
3. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number
Most recent issuance date and the expiration date
Date of most -recently certified Attachment A:
Date of most -recently certified Attachment B:
1

4. Check all that apply to the requested permit modification:
❑ INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for existing residuals
source -generating facility(ies) certified.
❑ ADD ❑ DELETE residuals source -generating facility(ies) to/from those certified.
❑ INCREASE ❑ DECREASE the acreage associated with land applications site(s).
D�ADD ❑ DELETE land application site(s) to/from those certified.
�p
❑ OTHER. , Explain:
M. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. County where residuals land application program is headquartered: McDowell
2. County(ies) where residuals source -generating facilities are located:
McDowell
3. County(ies) where land application sites are located: Catawaba
Program contact person and/or consulting firm who prepared application: Southern Soil Builders. Inc.
Mailing address: 958 Hoots Road
City: Roaring River State: NC Zip: 28669
Physical address:
958 Hoots Road
City: Roaring River State: NC Zip
Telephone number: ( 336 ) _957-8909 Facsimile number: ( 336 ) _
E-mail address:
[e-mail]
28669
957-8909
4. Who will be responsible for the day-to-day management of the residuals land application program:
❑ Permittee or ® residuals management firm. If a residuals management firm, complete the
following:
Firm contact person and title: Dennis Key President
Firm name: Southern Soil Builders, Inc.
Mailing address: 958 Hoots Road
City: Roaring River State: NC Zip: 28669
Telephone number: (_336) 957-8909 Facsimile number: ( 336) 957-8940
E-mail address: ssbiA_wilkes.net
FORM: NDRL,1-& 10-06 . Page 4 of 6 Attachment Order, i

5. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application
program, their certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification
Number
ORC
Dennis Key
Southern Soil Builders, Inc.
15704
Back -Up ORC
Zach Key
Southern Soil Builders, Inc.
27660
Additional Back -Up
ORCs
(if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application
program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's
completion of the required training school and certification test:
6. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN)
generated by all residuals source -generating facilities as currently certified and proposed for
certification with this application and list the results in the following table:
Maximum amount of residuals to be certified: 200 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
58.58
67.58
11716
13516
Five -Year Maximum Adjusted
60.38
69.38
12076
13876
b. Land Application Site Use Summary: Summarize information regarding the land application sites as
currently certified and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
Hay
Pasture
80.8
Total:
80.8
Methods
Surface
80.8
Incorporation or
Total:
80.8
Restrictions
Year -Round
80.8
Seasonal
Total:
FORM: NDRLAP W-06 X'age _, .)I c Attachment order 1

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the
residuals as currently certified and proposed for certification assuming the scenarios listed in the
following table:
Assumed
Application Rate
(bs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
234.32
270.32
241.52
277.52
100
117.16
135.16
120.76
138.76
150
78.1
90.1
80.5
92.5
200
58.58
67.58
48.3
69.38
8. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application
of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough
storage, not enough land, vector reduction practices not in place, etc.)
***FORM: NDRLAP 10-06 CONTINUES ON NEXT PAGE***
FORM: NDRLAP 10-06 Page 6 of 6 Aaactiment Order .l

Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater
facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or
abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under
Rule 2T .0105.
❑ Yes ❑ No, Explain;
I, Slwp _,N &,,k , attest that this application for 8ftIP- _ iLrN k K C A Qe-
NOMCNItL,JMIE_ WN & I e eN-1 Pk-\N:" has been reviewed by me and is
accurate and complete to the best of my knowledge. I understand that the Division of Water Quality may not
conduct a technical review of this program and approval does not constitute a variance to any rules or statutes
unless specifically granted in the permit. Further, any discharge: of residuals to surface waters or the land will
result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal
prosecution. I will make no claim against the Division of Water Quality should a condition of this permit be
violated. I also understand that if all required parts of this application are not completed and that if all required
supporting information and attachments are not included, this application package will be returned to me as
incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any
person who knowingly makes any false statement, representation, or certification in any application shall be guilty
of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000
per violation.
Signature: %Date: '11 1pa—
[EDIDENRIDWQ DC� C� a
RECEIVE
AQUIFER; PRQTF('T101 SFCTION J U N 1 8 2007
APR 19 2007
THE COMPLETED APPLICATION PACKAGE, NC DENR MRO
INCLUDING ALL SUPPORTING INFORMATION AND MAT Q - A uifer Prote
SHOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
AQUIFER PROTECTION SECTION
LAND APPLICATION UNIT
By U.S. Postal Service:
1636 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1636
By Courier/Special Delivery:
2725 CAPITAL BOULEVARD
RALEIGH, NORTH CAROLINA 27604
TELEPHONE NUMBER: [phone]
I
FGIZIvI: I':I1iZ1 A:' IG 06 ( age / of 0 Auuvulunent Ordef i

State of North Caroiina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL)
The Division of Water Quality (Division) will not accept this attachment unless all the instructions are
followed. Failure to submit all required items will lead to additional processing and review time.
For more information, visit our web site at: http://it20.enr.state.nc.usllaulmain.html '
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application
form (FORM: NDRLAP 10-06, FORM: DRS 10-06, or FORM: SDRS 10-06).
✓ Any changes to this attachment form will result in the application package being returned.
✓ For new residuals programs or renewed residuals programs, submit a separate attachment form for each
residuals source -generating facility to be certified for this residuals program.
✓ For modified residuals programs in which any modification to the certified residuals -source generating
facilities is proposed, submit a separate attachment form for only those residuals source -generating facilities
that are affected by the proposed modification.
✓ The attachment should be organized prior to submission in the following order (i.e., by facility):
o Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA 10-06).
➢ Attachment Order 2-a: Vicinity map.
➢ Attachment Order 2-b: Process flow diagram and/or narrative.
➢ Attachment Order 2-c: Quantitative justification for residuals production rate.
➢ Attachment Order 2-d: Sampling plan.
➢ Attachment Order 2-e: Laboratory analytical reports and operational data.
B. Residuals Source -Generating Facility Information:
✓ Attach a vicinity map that shows the location of the facility and meets all of the criteria in the latest version
of the document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina
Residuals Permitting Programs."
✓ Attach a detailed narrative and/or process flow diagram that describes how the residuals are to be generated,
treated, processed, and stored at the facility.
✓ Attach a quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals
listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition,
ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or
disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
C. Residuals Quality Information:
✓ Attach a detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In
addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable
pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring
must be completed on the residuals as they are to be land applied, distributed, and/or disposed.
✓ Attach reports for all laboratory analyses used to complete this attachment form. Attach documentation that
the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
✓ Item H. 3. does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only.
rORM: RSCA 10-06 i°age � of 9 Attacru lent Order-')

Applicant's name: Baxter Healthcare Corporation
Check all that apply: RENEWED RENEWED RESIDUALS PROGRAM
❑ INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals source -
generating facility certified for this residuals program.
Current: Dry Tons/yr. And proposed: Dry Tons/yr.
❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this
residuals program.
❑ OTHER Explain:
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Name of facility: Baxter Healthcare Corporation
2. Facility permit holder: Baxter Healthcare Corporation
Facility permit holder is (check one): ❑ federal, ❑ state, ❑ local government, or ® private.
Facility permit number: CS0.0.0.6564 �
Facility permit issued by (check one): ® Div. of Water Quality, ❑ Div. of Environmental Health, or
❑ other (explain:
3
If the facility permit is not issued by the Div. of Water Quality, complete the following:
a. Facility contact person and title:
Facility complete mailing address:
City: State: Zip:
Telephone number: ( ) Facsimile number:
E-mail address:
b. Facility complete location address:
City: State: Zip:
Latitude: and longitude:
4. County where facility is located:
5. Purpose of the facility (check one):
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100%industrial wastewater,
® treatment of industrial wastewater mixed with domestic wastewater, or
(approximate percentages: 81_ % industrial and _19_ % domestic)
6. Does the facility have an approved pretreatment program: ® yes ❑ no
7. Facility permitted/design flow: _1.2_ MGD and facility average daily flow: _0.8 MGD.
8. Average amount of residuals being generated at this facility dry tons per year.

9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 149,000 gallons per day of domestic, 651,000
gallons per day of Industrial through aerobic digesters
Type and volume of residuals storage (i.e., outside of residuals treatment units):
2 digesters- 307,000 gallons
II, RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under (check one): ® 40 CFR Part 503 or ❑ 40 CFR Part 257.
2. Specify if residuals are intended for (check one):
❑ Land Application/Distribution (Class A or Equivalent).
Complete all items EXCEPT Items II. 4b., 7b., and 7c.
® Land Application (Class B or Equivalent).
Complete all items EXCEPT Items II. 4b., 7a., and 7c.
❑ Surface Disposal.
Complete all items EXCEPT Items II. 4a., 5., 7a., 7b., and 8.
***FORM: RSCA 10-06 CONTINUES ON NEXT PAGE***

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-
hazardous under RCRA:
a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
§261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity
characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and
reactivity: laboratory: Pace Analytical and date of analysis: 11-28-2006
Passed corrosivity test: ® yes ❑ no. pH: 5.8-
s.u. (2 < pH < 12.5).
Passed ignitability test: ® yes ❑ no. Flashpoint: _>200_ T (> 140T).
Passed reactivity test: ® yes ❑ no. HCN: <1_ mg/kg (<250) & H2S: _<10 mg/kg
(<500).
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
2.0
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
.01
Lead
5.0
0.050
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
.002
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
.001
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
.002
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the
residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory: A&L Eastern Laboratories, Inc._ and date of analysis: _6-20-2006
Parameter
Ceiling
Concentration Limits
(Class,4 & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(For Class Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
1.4
Cadmium
85
39
2
Copper
4,300
1,500
289
Lead
840
300
31
Mercury
57
17
1.1
Molybdenum
75
n/a
9
Nickel
420
420
41
Selenium
100
100
1.2
Zinc
7,500
2,800
265
c. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory:
and date of analysis:
Closest Distance
to Property Lines
(ineters)
Arsenic
(mg/kg)
Chromium
(mgAk
Nickel
(mg/kg)
> 0 but < 25
30
200
210
> 25 but < 50
34
220
240
> 50 but < 75
39
260
270
> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125 but < 150
62
450
420
> 150
73
600
420

5. Nutrient/Mcronutrient Determination: Complete the following:
a. Total solids: 12.61 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the
following nutrient and micronutrient parameters: laboratory: A&L Eastern Laboratories, Inc.
and date of analysis: 6-20-2006
Parameter
Result
(mg/kg, dry weight)
Aluminum
3310
Ammonia -Nitrogen
9000
Calcium
25100
Magnesium
228
Nitrate -Nitrite Nitrogen
11
pH (Standard Unit)
5
Phosphorus
21400
Potassium
3000
Sodium
3100
Total Kjeldahl Nitrogen
91600
c. Using the results listed in Item H. 5b. above, calculate the sodium adsorption ration (SAR): _1.60_ .
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the
residuals: _30 %. This rate is a ® default value or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or
provide technical justification as to why the selected default value is appropriate to be applied to these
residuals: default rate for aerobic digestion
Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following
table:
Application Method
First Year
Five -Year
PAN
Maximum Adjusted
PAN
(mg/*9)
(mg/W
Surface
29291
30191
Injection/Incorporafion
33791
34691
e. Are the residuals a registered fertilizer with the NC Department of Agriculture and Consumer Services:
❑ yes ® no. If yes, provide date of registration approval:
the current registration number: .

and the fertilizer equivalent: %, %, and %.
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the
residuals and list the results of the latest analyses:
7. Pathogen Reduction Determination: Specify which alternative(s) will be used to meet the pathogen
reduction requirements:
a. For Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry
solids.
OR
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry
solids.
AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed):
❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance.
❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment.
❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric VirusNiable Helminth Ova.
❑ Alternative 4 [40 CFR §503.32 (a)(6)] - No Prior Testing for Enteric VirusNiable Hehninth Ova.
❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation.
❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process.
Explain:
b. For Class B or Equivalent:
® Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [40 CFR §503.32 (b)(3)] - Process to Significantly Reduce Pathogens (PFRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process.
Explain:
❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
c. For Surface Disposal:
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Not :Applicable - Reg - lated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.

8. Vector Attraction Reduction Determination: Specify which alternative(s) will be used to meet the vector
attraction reduction requirements:
❑ Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
® Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 140 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization.
❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [40 CFR §503.33 (b)(9)] - Injection.
❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Alternatives for Animal Processing Residuals Only:
Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10.
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.

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BAXTER NORTHCOVE WASTEWATER TREATMENT PLANT PROCESS
NARRATIVE
The wastewater treatment plant was originally designed to treat a capacity of
600,000 gallons per day. In 1973, due to increased production levels, the wastewater
plants' capacity was doubled to its current 1.2 MGD capacity. Other improvements,
such as the ultraviolet disinfection system, filter press, and solution dump system,
were made throughout the 1970's, 1980's, and 1990's.
Currently, the existing wastewater treatment plant is permitted at 1.2 MGD
capacity. Wastewater is pumped from the manufacturing plant on the east side of the
North Fork Catawba River to the wastewater plant on the west side of the river by the
influent pumping station. Preliminary physical treatment of the wastewater consists of
three static fine screens for the removal of any solid materials received at the plant, _
such as pieces of plastic IV and PD solution bags, paper or plastic products, cafeteria _
scraps, or other large non -degradable objects. Each screen is rated at 450 gallons per
minute capacity, for a total capacity of 1350 gallons per minute. The solid materials
are collected in a trough and removed by the operators into a dumpster for ultimate
disposal at the landfill.
The influent wastewater flows through the static screens and falls into a flow
equalization basin with a capacity of 1,324,000 gallons. At this point, a minimal
amount of air and mixing energy is added by high speed floating surface aerators to
prevent any solids from settling in the basin.
From the flow equalization basin, the influent is pumped to a flow splitter box
that divides flow between the two (2) aeration basins. The aeration basins are
equipped with eight (8) low speed fixed mechanical aerators, four (4) in each basin.
Total design retention time in the aeration basins istap omately8�lrou�s
.� �I�T�u�ients��an:tl'ego_r�o��gz�an��lfe�fi�i�zer�( 4f 0)dare-al�so�adde��at�tlai�.�p�int-to
Hydrated lime is also added to maintain the proper wastewater alkalinity levels, as
well as provide some carbon source for the biological process. Both of the additions
are made by hand and require monitoring by plant staff to maintain appropriate levels
for biological growth.
The aeration process is followed by clarification in four (4) center -feed, suction
header type sludge draw off secondary clarifiers. There are two (2) 32.5-foot
diameter, 8-foot side water depth units rated at 300,000 gallons each, and two (2)
42.5-foot diameter, 10-foot side water depth units rated at 600,000 gallons per day
each, for a total clarification capacity of 1.8 MGD. While modern clarification
equipment is normally designed with deeper side water depths than those found in the
existing clarifiers (normally no less than 12 feet), the existing clarifier performance
has been historically adequate.

Solids captured by the secondary clarifiers are then collected and subsequently
treated in two (2) aerobic digesters with a total volume of approximately 307,000
%Iq in 1J ne oir; N,Cf
The Baxter Wastewater Treatment Facility is also equipped with three (3) tertiary
upflow sand filters; each rated at 425 gpm each, as a final polishing step prior to
disinfection and discharge. Effluent from the secondary clarifiers and autoclave
cooling water excess is mixed together in a holding pond and applied to the filters, as
well as used to provide water for filter backwash operations.
Disinfection is accomplished with two (2) ultraviolet (UV) disinfection units.
These units destroy bacteria in the effluent by exposure to ultraviolet radiation instead
of oxidation by addition of free chlorine ions (chlorination). This creates a less toxic
discharge into the receiving stream and eliminates the need to monitor chlorine
residual in the effluent. Because the receiving stream is classified as designated trout
waters, the facility does have very stringent chlorine limits. A process diagram of the
wastewater treatment facility is included.

10.
-0
PSTEWg7Eq TREATMENT
RLANT EVAWATION:
E ACTHCARE CORPORATION
COUNTY, NORTH CAROLINA
150,000 GALLON WATERFILTER
FILTER SLUDGE BASIN WASHWATER
i�
lo
III
12'CIP TO
i
HOLDING
BASIN
SLUDGE
DRYING BEDS
III
00
III
III
III
TI
ol l
li
rn
I z
IIIZ
Illm
III
III
UNFILTERED
9
12'
BACKWASH LINE
S S 0 C," IA
T E
-
-Pil),A?�T"`7:'
"TTIT A T,7 ('p

JUSTIFICATION FOR RESIDUALS PRODUCTION RATE
The residuals production rate for Baxter Healthcare Corporation has been estimated to be
121.856 dry tons per year. This permit application is for 200 dry tons per year. This
should give ample room for growth and any additional increase in flow of the Waste
Treatment Plant.

SAMPLING PLAN
Prior to application, residual solids samples are collected from the sludge holding tank.
The grab samples that are taken will be composted for nutrient and metal analysis. The
composted sample is mixed to keep the solids suspended and containers filled for the
analysis. Volatile solids are collected from the sludge holding tank and the clarifier for
calculation of volatile reduction.
Annually, if a land application event occurs; a TCLP samples will be taken. This TCLP
will consist of:
Arsenic Hexachlorobenzene Barium
Hexacloro-1,3-Butadiene Benzene Hexachloroethane
Cadmium Lead Carbon Tetrachloride
Lindane Chlordane Mercury
Chlorobenzene Methoxychlor Cholorform
Methyl Ethyl Ketone Chromium Nitrobenzene
m-cresol Pentachlorophenol o-cresol
Pyridine
Cresol
Tetrachloroethylene
1,2-Dichloroethane
2,4, 5 -Trichlorophenol
Endrin
Heptachlor and its Hydroxide
p-Cresol
Silver
1,4-Dichlorobenzene
Trichloroethylene
2,4-Dinitrotoluene
2,4,5-TP(Silvex)
Selenium
2,4-D
Toxaphene
1,1-Dichloroethylene
2,4,6-Trichlorophenol
Vinyl Chloride
Annually or when residuals solids are to be land applied, the residual solids will be
analyzed for: Arsenic, Cadmium, Copper, Mercury, Molybdenum, Nickel, Selenium,
Zinc, Aluminum, Ammonia -Nitrogen, Calcium, Nitrate -Nitrite Nitrogen, Magnesium, %
total solids, pH, Phosphorus, Potassium, TKN, and Sodium. From this information the
Plant Available Nitrogen (PAN) will be calculated.
Volatile solids analysis will be conducted annually, when residuals solids are land
applied. Fecal coliform samples will be collected prior to a land application event to
ensure class B compliance.

F
The Div]
+
U
�! INSTRUCT
A. Attache
✓ Do
�1
ND
✓
An,
✓
For
i f
infc
L
✓
For
i
cert
nem
B. Land Ai
✓
Ada
✓
The
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in It
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✓
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ao
r�iwcncnenr - 7-5--r-a-sits and agronomiic evaluation that meets all of the criteria m the latest version of 4.
the document ntitled "Guidance for the Preparation of Soils and Agronomic Evaluations for North Carolina
Residuals Permitting Programs."
✓ For each land application site with a status code of R, attach the following in the order specified:
♦ Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA 10-06).
➢ By Land Application Site:
■ Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA 09-06).
• Attachment Order 3-d: Buffer Waiver Agreement Attachment (FORM: SWAA 10-06).
• Attachment Order 3-e: An updated vicinity/buffer map (i.e., see above for criteria guidance).
■ Attachment Order 3- : An updated accounting of the land application site's cumulative pollutant loading
rates (CPLRs) that are required by the permit of the residuals land application program from which the s
is being transferred. ite
✓ For each land application site with a status code of g contact the appropriate Division's regional office to determine
attachment requirements.
✓ For each land application site with a status code of T, attach the following in the order specified:
♦ Attachment Order 3 through 3 f Everything required for land application sites with a status code of N.
➢ Attachment Order 3-g: A-n txpd ;-ee acco•� t of rt,,� !'" PT (i.e. see above for ri 't
ena
. aC i en'iC�rc�er

S Southern
S Soil
$ Builders, Inc.
958 Hoots Road Roaring River, NC 28669
[phone] 9 Fax [phone]
Southern Soil Builders, Inc, is under contract to provide Baxter Healthcare Corporation
with land application services. The 4 fields we are going to use for Baxter's land
application program are located in Catawba County. These fields are going to be
transferred from Lincoln County's program. I have enclosed maps of the fields for a
watershed classification. This is will be a new program and does not have a permit
number. I have also enclosed the previous watershed classification for these four fields if
that will be of any assistance to you.
If there is any questions or concerns, feel free to contact me at anytime.
Zach Key
Southern Soil Builders, Inc.

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
WATERSHED CLASSIFICATION ATTACHMENT
FOR RESIDUALS PROGRAMS
(THIS FORM MAY BE PHOTOCOPIED FOR USE ASAN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to follow the instructions or to submit all of the
required items will lead to additional application processing and review time.
For more information or for an electronic version of this form, visit our site at : http � h'v enr state.nc. us iidpu
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application
form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare the attachment form with the requested information for each location where the residuals
program activities are planned to occur within a particular regional office county coverage.
✓ Additional copies of Page 2 of 2 of this attachment form may be used if necessary.
✓ Use a portion of an 8.5-inch by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to
identify the location where the residuals program activities are planned to occur as well as the closest
downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and
number, the identified location, and be of clear and reproducible quality.
✓ Latitudes and longitudes must reported as being based on either the NAD 27 or the NAD 83 data systems.
✓ Acceptable methods of determining location latitudes and longitudes and their corresponding codes are as
follows:
♦ Address Matching (ADD) ♦ Digital or Raw Photo Extraction (EXT)
♦ Aerial Photography with Ground Control (AER) ♦ Geodetic Quality GPS Survey (GEO)
♦ Cadastral Survey (SUR) ♦ LORAN-C Navigation Device (LOR)
♦ Conversion from Coordinate Plane (CP) ♦ Navigation Quality GPS (GPS)
♦ Conversion from Township -Section -Range (TSR) ♦ Remote Sensing (RS)
♦ Conversion from Universal Trans Merc (UTlvl) ♦ Zip Code Centroid (ZIP)
♦ Map Interpretation by Digital or Manual Extraction (MAP)
✓ Location accuracy must be provided to the nearest unit (e.g., nearest second, tenth of a second, etc.).
C. Mail or fax the attachment form and the map portions to the appropriate regional office for review and
to obtain the waterbody and classification information.
✓ A list of the Division's regional offices, their county coverage, and their contact information may be
downloaded from the web site at: http:/ih2b.enr.state.nc.us/ndpu/.
✓ The Division will not consider this attachment form to be complete until it is completed by the appropriate
regional office.
To: Regional office: Mooresville Regional Office
Address of regional office: 919 North Main Street
City: Mooresville State: NC Zip: 28115
Facsimile number: ( _704_ ) 663-6040
Please provide me with the waterbody name(s), stream index number(s), and current/proposed
classification(s) of the surface waters that are closest to and downslope from the location(s) where the
proposed residuals program activiti a e planned to occur, as identified on the attached map segment.
Signature of regional office staff: % Date:
FORM: RWSCA 02/02 Page 1 of 2 Attachment Order 3-
arL�--
�f

Location
ID
County
Catawba
Latitude
3503759.86"N
Longitude
81004'26.70"W
Location
Datum
NAD27
Location
Method
Code
MAP
Location
Accuracy
t 1"
Waterbody Subbasin and
Stream Index No.
(To Be Completed by DWQ)
I,c
N' C; �' � 11 _ y 9 - 6.>
Current and
Proposed Class
(To Be Completed
by DWQ)
WS-N
rS-2E
Catawba
35037'50.04"N
81°04'41.69"W
NAD27
MAP
t 1"
a S
WS-N
T-1
Catawba
35037'19.21"N
81005'36.83"W
NAD27
MAP
WS N
T-1
Catawba
35037'33.75"N
81005'47.13"W
NAD27
MAP
t 1"
, y 74 0,S
WS N
FORM: RWSCA 02/02
*** END OF FORM RWSCA 02/02 ***
Page 2 of 2
Attachment Order 3-

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1 of 1 2/26/2007 430 P1VI

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
COUNTY MANAGER NOTIFICATION ATTACHMENT
(THIS FORMMAYBEPHOTOCOPIED FOR USEASANORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete unless
all the instructions .are followed. Failure to submit all of the required items will lead .
to additional application processing and review time.
For more information or for an electronic version of this form, visit our web site at:
http:llh2o. enr.`state.nc. usllau/applications.htinl
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application
form (FORM: NDRLAP 10-06).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each county in which the land application sites for which the
applicant is seeking certification are located.
C. Mail the attachment form to the appropriate county manager by certified mail with a return receipt
renuested.
✓ The most current publication of the Directory of State and County Officials may be downloaded from the
web site at: http://www.secretary.state.nc.uLpubsweb/direct.asp.
✓ A list of the Division's regional offices, their county coverage, and their contact information may be
downloaded from the web site at: http://www.enr.state.nc.usfhtml/regionalofFices.html
D. Attach an 8.5-inch by 11-inch copy of the return receipt to the back of this attachment form prior to
submission of the application to the Division for review.
To: County where land application sites are located: Catawba
Name and complete address of county manager: Tom Lundy
PO Box 389 100A. South West Blvd.
City: Newton State: NC Zip: 28653
This is to notify you that the applicant listed in Item I(1) of this attachment form will be submitting an
application for the land application of residual solids to land in your county to.. the Division for review.
During this review, the Division will ensure that all federal and state regulations are enforced. Maps of the
land application sites included in this application will be available at the following location no later than the
listed expected application date:
Name and complete address of appropriate regional office: Ashville Regional Office
2090 US Hwy 70
City: Swannanoa State: NC Zip: 28778
Telephone number: ( _828_) 296-4500 Facsimile number: (_828_) 299-7043
Expected date of application submission: 3-5-2007
Actual date of application submission (to be completed by DWQ):
Deadline for county manager response (to be completed by DWQ):
Should you desire to comment on this application as it related to your interests, please do so no later than 30
calendar days following the expected application submission date. If you have any questions or comments
about this notification or if you would like more information, please contact the Aquifer Protection
Supervisor of the appropriate regional office at the telephone number provided above. Thank you in
r04h.,m.ce for 0IhN r+:alte1;.
FORM: CMNA 09-06 rage 1 of 2 Attachment Order 3-b

I. GENERAL INFORMATION:
1. Applicant's name: Baxter Healthcare Corporation
2. Signing official's name and title: Stephen Gouge WWTP Supervisor
3. Complete mailing address of applicant: PO Box 1390
City: Marion State: NC Zip: 28752
Telephone number: (_828_) 756-6618 Facsimile number: ( _828_) 756-4821
E-mail address: Stephen gougebaxter.com
4. Name and complete mailing address of contact person and consulting firm who prepared application:
Zach Key Southern Soil Builders, Inc.
City: Roaring River State: NC Zip: 28669
Telephone number: (_336_) 957-8909 Facsimile number: (_336_) 957-8940
E-mail address: [e-mail]
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ® new, ❑ modified, and/or ❑ renewed permit.
2. If this application is being submitted to renew or modify an existing permit, provide:
the permit number
the most recent issuance date and the expiration date
Date of most -recently certified Attachment A:
Date of most -recently certified Attachment B:
III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION
1. County(ies) where residuals source -generating facilities are located:
McDowell
2. Purpose of the residual source -generating. facilities (check all that apply):
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
® treatment of industrial mixed with domestic wastewater, and/or
(approximate percentages: _81 % industrial and _19_ % domestic)
❑ other (explain: ).
3. Are land application sites currently certified for this residuals land application program in this county:
❑ yes ® no. If yes, provide the total number of acres (i.e., excluding
buffers) that are certified: acres (approximate percentages: % forested, %
agricultural, and % reclamation sites).
4. This application, if approved by the Division, will certify _80.8 additional acres (i.e., excluding
buffers) in this county for this residuals land application program (approximate percentages: %
forested, _100 % agricultural, and __. % reclamation sites).
FORM: CMNA 09-06 Page 2 of 2 Attachment Order 3-b

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
LANDOWNER AGREEMENT ATTACHMENT
(THIS FORMMAY BE PHOTOCOPIED FOR USE ASAN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete unless
all the instructions are followed. Failure to follow the instructions or to submit all of the required
items will lead to additional processing and review time for the application.
For more information or for an electronic version of this form, visit our web site at.
http://h2o. enr.state.nc. us/lazy/applications. html
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (FORM: NDRLAP 10-06).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner
and operated by a lessee/operator (Le., if applicable) other than the applicant.
✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and
the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS
TO PRIVATELY OWNED LAND APPLICATION SITES
The undersigned landowner or his representative hereby permits:
Applicant's name: Baxter Healthcare Corporation
Complete mailing address of applicant: PO Box 1390
City: Marion State: NC Zip: 28752
Telephone number: (_828_) 756-6618 Facsimile number: ( _828_ ) 756-4821
E-mail address: stephen aougenabaxter.com
hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -
generating facility(ies) onto the following land application site(s) (i.e., see attached buffer maps) in
accordance with the stipulations and restrictions as given in this Agreement:
Site/Field ID
Land Use or
Cropping Patterns
Intended Use or
Disposition of Crops
Residuals Source -Generating
Facilities
T-1
Hay Pasture
Baxter Healthcare
T-2
Hay Pasture
Baxter Healthcare
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land application site(s) described
above for the disposal of the residuals.
This Agreement shall remain in effect for the Iength of the Division's permit for the residuals land
application program and shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.

The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.
FORM: LOAA 02/02 Page' of 3 Attachment Order 3-a

L STIPULATIONS:
1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement.
The land application of any additional residuals or waste, other than that generated by the residuals source -generating
facilities specified by the Division's residuals land application program permit, is prohibited.
2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply
with all provisions of this Agreement.
3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third
party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and
conditions of this Agreement.
4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the
subject matter of this Agreement.
5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18
months from the date of the most recent residuals land application event.
6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge
Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land
application site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a
notice shall be given by the current landowner to the new landowner that gives full details of the residuals applied or
incorporated at the land application site(s).
8. The Permittee has provided the landowner or his representative with information and data concerning the residuals land
application program, including an analysis of constituents of the residuals, residuals application methods, schedules for
typical cropping patterns, and a description of the equipment used by the Permittee.
9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program
permit that has been most -recently issued by the Division prior to commencement of any residuals land application
event. This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws
and regulations.
10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The
only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided
that a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least
6.0.
11. The Permittee will Punish the landowner or his representative with a copy of the results of each soil analysis.
12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and
the Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil
samples.
13. The landowner or his representative will fiunish the Permittee with information regarding the amount and analysis of
other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application
site(s).
14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and
cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this
Agreement and schedule residuals land application events at appropriate periods.
15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the
Permittee and/or the landowner or his representative prior to and during a residuals land application event.
16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public
access to the land application site(s) during active use and for the 12-month period following a residuals land
application event. Such controls may include the posting of signs that indicate the activities being conducted at the land
application site(s).
17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application
event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access
during these periods after such residuals land application events.
18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals
land application program permit.
19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their
representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and
to established monitoring facilities on or near the land application site(s) as required by the residuals land application
program permit.
20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter
and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the
purpose of determining compliance with the Division's residuals land application program permit; may inspect or copy
any records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater,
surface water, or leachate.
FORM: IOAA 02/02 Page 3 of 3 Attachrnent Order 3-c

21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives
to take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination
of, this Agreement.
FORM LOAA 02/02 Page � c;f 3 Attachment Urae-- 3-c

IL RESTRICTIONS:
Landowner's Certification:
❑ I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to
make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that
I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding
the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced
land application site(s) are not included in any waste disposal contract or agreement with another
municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations and restrictions, and do hereby grant permission to the Permittee to land apply
residuals to the land application site(s) as specified herein.
Landowner name:
Signature: / G Date:
t
NORTH CAROLINA; COUNTY
I, the undersigned Notary Public do hereby certify that ��^ 1'1 " l Tta I u e
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
WITNESS my hand and official seal this the o?-14
1
day of Jc4 tt
Signature and seal:
My commission eN
Lessee's/Operator's Certification:
❑ I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Lessee/operator
Signature:
Permittee's Certification:
Date: / 2 7" 2
❑ I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Signing official name:
Signature:
Date: c IT 10
FORM: LOAA 02/02 Page 5 of 3 Attachment Ordl:r 3-c

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
LANDOWNER AGREEMENT ATTACHMENT
(THIS FORMMAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete unless
all the instructions are followed. Failure to follow the instructions or to submit all of the required
items will lead to additional processing and review time for the application.
For more information or for an electronic version of this farm, visit our web site at.
http: //h2o. enr. state. nc. us/lay/applications. hhnl
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (FORM: NDRLAP 10-06).
✓ Any changes to this -attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner
and operated by a lessee/operator (i.e., if applicable) other than -the applicant.
✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and
the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS
TO PRIVATELY OWNED LAND APPLICATION SITES
The undersigned landowner or his representative hereby permits:
Applicant's name: Baxter Healthcare Corporation
Complete mailing address of applicant: PO Box 1390
City: Marion State: NC Zip: 28752
Telephone number: (_828_) 756-6618 Facsimile number: ( _828_) 756-4821
E-mail address: stenhen [e-mail]
hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -
generating facility(ies) onto the following land application site(s) (Le., see attached buffer maps) in
accordance with the stipulations and restrictions as given in this Agreement:
Site/Field ID
Land Use or
Cropping Patterns
Intended Use or
Disposition of Crops
Residuals Source -Generating
Facilities
S-1
Hay Pasture
Baxter Healthcare
S-2
Hay Pasture
Baxter Healthcare
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land application site(s) described
above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land
application program and shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.

The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.
FORM: LOAA 02/02 Page 2 of 3 Attachment Order 3-c

L STIPULATIONS:
1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement.
The land application of any additional residuals or waste, other than that generated by the residuals source -generating
facilities specified by the Division's residuals land application program permit, is prohibited.
2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply
with all provisions of this Agreement.
3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third
party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and
conditions of this Agreement.
4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the
subject matter of this Agreement.
5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18
months from the date of the most recent residuals land application event.
6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge
Pernutting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land
application site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a
notice shall be given by the current landowner to the new landowner that gives full details of the residuals applied or
incorporated at the land application site(s).
8. The Permittee has provided the landowner or his representative with information and data concerning the residuals land
application program, including an analysis of constituents of the residuals, residuals application methods, schedules for
typical cropping patterns, and a description of the equipment used by the Permittee.
9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program
permit that has been most -recently issued by the Division prior to commencement of any residuals land application
event. This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws
and regulations.
10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The
only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided
that a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least
6.0.
11. The Permittee will furnish the landowner or his representative with a copy of the results of each soil analysis.
12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and
the Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil
samples.
13. The landowner or his representative will Punish the Permittee with information regarding the amount and analysis of
other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application
site(s).
14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and
cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this
Agreement and schedule residuals land application events at appropriate periods.
15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the
Permittee and/or the landowner or his representative prior to and during a residuals land application event.
16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public
access to the land application site(s) during active use and for the 12-month period following a residuals land
application event. Such controls may include the posting of signs that indicate the activities being conducted at the land
application site(s).
17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application
event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access
during these periods after such residuals land application events.
18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals
land application program permit.
19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their
representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and
to established monitoring facilities on or near the land application site(s) as required by the residuals land application
program permit.
20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter
and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the
purpose of determining compliance with the Division's residuals land application program permit; may inspect or copy
any records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater,
surface wat- , or leachate
FMA: LOAA 02/02 Page 3 of 3 Attachment Order 3-c

21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives
to take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination
of, this Agreement.
FORM: LOAA 02/02 Page 4 of 3 Attachment Orde;

IL RESTRICTIONS:
Landowner's Certification:
❑ I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to
make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that
I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding
the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced
land application site(s) are not included in any waste disposal contract or agreement with another
municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations and restrictions, and do hereby grant permission to the Permittee to land apply
residuals to the land application site(s) as specified herein.
Landowner name:
Signature: ,Z Date:
NORTH CAROLINA, C t a w b COUNTY
I, the undersigned Notary Public do hereby certify that A m
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
t�
WITNESS my hand and official seal this the
day of S{ P'? , bp r 20 0-4
Signature and seal:
Gj aoU� OFFICIAL SEAL
My commission expires: I •mow»
NOTARY I i)BLIC NOflTH CA=H Klee
ROUNIA
Lessee's/Operator's Certification: - COUNTY OF WILKES
❑ I certifythat I have read this Agreement and do herebyagree to abi n" omra s.,in:; Expires �1-9r_vr�
specified herein.
Lessee/operator n +— /ey
Signature: Date:
Permittee's Certification:
❑ I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Signing official name: S e
Signature: 11 Dater
FORM: LOAA 02/02 Page 5 of 3 Attachme iL girder 3-c. ..

*** END OF FORM LOAA 02/02 ***
FORM: LOB 02/02 Page 6 of 3 riiL,,adimz;nt Order 1 r

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DEREK TEAGUE FARM
BAXTER
SOILS AND AGRONOMY REPORT
There are four fields in this tract, Fields S-1, S-2, T-1 and T-2. These fields were previously
permitted in the Lincoln County Permit No. WQ0016922. This farm has two distinct sections. The
first section (Fields S-1 and S-2) is located southeast of the intersection of Old Beatties Ford Road
and Bandy's Cross Road. The second section (Fields T-1 and T-2) is located east of the intersection
of Buffalo Shoals Road and Puddle Path Road. These fields are utilized for fescue pasture but may
receive a cutting of hay in the spring if managed properly. These fields were gently sloping and had
good permanent cover established but were receiving considerable grazing pressure. The quality of
the vegetative cover will be a useful guide for appropriate application rates. Southern Soil Builders
is responsible for the buffer maps but buffers will need to exclude areas of slope, property lines,
houses, creeks, and surface water drainage.
Review of the nutrient and metals data from this residuals source indicate no metals above
regulation limits and no presence of salt or nutrient concerns. Both phosphorus and potassium are
available in this source but additional potassium will likely need to be added to promote good crop
growth. The residual's sample is high in nitrogen fractions and low in percent solids. These two
will determine annual and individual loadings for the sites listed.
Field investigations performed by a BR&S soil scientist concurred with the mapping published in
the Catawba Soil Survey. Field investigations found soils that were identified as Cecil, Hiwassee,
and Madison soils. A map of the sites identified on the soil survey is attached. My investigations
and soil profile descriptions concur with the soil survey. Detailed soil profile descriptions from the
investigation have also been attached. These sites are suitable for year round application. Please
note that areas marked as having D and E slopes were noted in the soil survey but those were not
always observed in the field. Areas of excessive slope adjacent to surface water drainage were
noted and should be buffered from the application area. Some areas of E slopes were mapped not
due to slope, but due to change in erosion class from eroded to severely eroded. It is thought this
map unit was identified to illustrate areas with the potential for greater erosion without the presence
of a suitable permanent cover.

Soil samples were collected and sent to A&L Labs in Richmond, Virginia and North Carolina
Department of Agriculture NCDA. Because of the schedule for NCDA, heavy metal values have
not been completed for this site. As soon as they are ready, they will be forwarded to you. Based
on a review of the soil nutrient and partial metal information from A&L Labs, Field S-2 should have
an application of lime immediately before or after the initial application of residuals from this
source. Potassium levels should be monitored closely for all fields since low amounts are applied
with this source.
Attached is a table with the predominant soil series indicated and the corresponding realistic yield
estimation (RYE) as available from http://www.soil.ncsu.edignmp/ncnmwg/yields/. These fields
should receive nitrogen applications in accordance with the rates specified in this table or in the
standard DWQ permit shell.
Soil Scientist /

Pages 35 and 44 of the Catawba County Soil Survey
SCALE: 1 ° = 1320 Baxter
CHECKED BY: - Land Application Program
DRAWN BY: RTB BRANCH Derek Teamue Farm
Soil
Survey
Map
Feb-07 ! ' & SOILS, LLC i Project No. 1 2007-60

- SOIL EVALUATION FORM
BRANCH RESIDUALS & SOILS, LLC
311 B South Westgate Drive - Greensboro, NC 27407
PHONE [phone] — FAX [phone]
Project Name Baxter Project Number
Owner Derek Teague Tract/Site
Operator Derek Teague Field
Slope 3 - 9 % Sample No. S-1 Crop
boasts teiic::::::::::::::::: Ma
2007-60
S-1
Fescue Pasture
Ap
1 0-4
SCL
1 5 YR 4/4
wk med gr
fr
n/a
Common roots
Btl
4 - 22
CL
2.5 YR 3/6
mod med sbk
fr
n/a
Few roots
Bt2
22 - 32
C
2.5 YR 4/8
mod med sbk
fi
n/a
Few roots
BC
32 - 40+
CL
2.5 YR 4/6
wk med sbk
fr
7.5 YR 4/6 (c)
-
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in.
Depth to Restrictive Horizon (in.) >40+ Type of Restrictive Horizon
Boring needed prior to application: no Attached map with boring location
Most Closely Related Soil Series Cecil
Discussion of Site
Soil mapped is a little redder than a typical cecil.
Good year round site. SOIL
�R�JB
>40+
n/a
no
t9l� 1180
Signed r% Date 1/26/2007

Project Name
Owner
Operator
Slope
SOIL EVALUATION FORM
BRANCH RESIDUALS & SOILS, LLC
S 11 B South Westgate Drive - Greensboro, NC 27407
PHONE [phone] — FAX [phone]
Baxter Project Number
Derek Teague Tract/Site
Derek Teague Field
Sample No. S-2 Crop
2007-60
S-2
Fescue Pasture
.....:.....:.......:.:.:.:.:.:.:.....AV
............:................................................:.:.:.:.:.:.:.:
Ap
0-5
It. CL
5 YR 4/4
wk med gr
fr
n/a
Common roots
BA
5- 12
CL
2.5 YR 3/6
wk med sbk
fi
n/a
Few roots
Btl
12 - 34
134-40+
C
2.5 YR 4/6
1
mod med sbk
fi
n/a
Few roots
I
BC
CL
2.5 YR 4/8
wk med sbk
fi
-
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in. >40+
Depth to Restrictive Horizon (in.) >40+ Type of Restrictive Horizon n/a
Boring needed prior to application: no Attached map with boring location no
Most Closely Related Soil Series Hiwassee
Discussion of Site
Buffer creek and drainage. Chewacla soils excluded in buffereing of the creek.
Good vear round
T.
P
Signed
Date 1/26/2007

Project Name
Owner
Operator
Slope
SOIL EVALUATION FORM
BRANCH RESIDUALS & SOILS, LLC
311 B South Westgate Drive - Greensboro, NC 27407
PHONE [phone] — FAX [phone]
Baxter
Derek Teague
Derek Teague
3 - 9 % Sample No. T-1
Project Number
Tract/Site
Field
Crop
2007-60
T-1
Fescue Pasture
oriti
be 'tlgfiu::.€rr........fire............
tie
Co s
=
Ap
04
1t. CL
5 YR 4/4
wk med gr
fr
n/a
Common roots
Btl
4 - 10
C
2.5 YR 3/6
wk med sbk
fi
n/a
Few roots
Bt2
10 - 26
C
2.5 YR 4/6
mod med sbk
fi
n/a
-
Bt3
26 - 40+
C
2.5 YR 4/6
wk med sbk
f
7.5 YR 4/6
-
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in. >40+
Depth to Restrictive Horizon (in.) >40+ Type of Restrictive Horizon n/a
Boring needed prior to application: no Attached map with boring location no
Most Closely Related Soil Series Hiwassee
Discussion of Site
Buffer drainage and property lines. No sign of E slopes.
fl---A --A -:+e
Date 1/26/2007

SOIL EVALUATION FORM
RANCH RESIDUALS & SOILS, LLC
J1aY✓Vuua •. v.s..bw..v a..iaa.v va��--...��.-..�-��• •-•
PHONE [phone] — FAX [phone]
Project Name Baxter
Owner Derek Teague
Operator Derek Teague
Slope 3 - 9 % Sample No. T-2
Project Number
Tract/Site
Field
Crop
Ap
0-4
gr. Lt SCL
7.5 YR 4/4
wk med gr
fr
n/a
BE
4-9
hvy SCL
7.5 YR 4/6
wk med sbk
fr
n/a
Btl
9 - 17
CL
5 YR 5/8
mo med sbk
fr
n/a
fine mica flakes
Bt2
17 - 24
C
1 2.5 YR 4/8
mo med sbk
fr
n/a
Many fine mica flakes
BC
24 - 33
SCL
7.5YR 4/8
wk med sbk
fr
2.5 YR 4/6
Many coarse mica flakes
C
33 - 40+
SCL
I Mixed
SL MA
v fr
7.5 YR 4/8, 2.5 YR 4/6
Mica schist
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in. >40+
Depth to Restrictive Horizon (in.) >40+ Type of Restrictive Horizon n/a
Boring needed prior to application: no Attached map with boring location no
Most Closely Related Soil Series Madison
Discussion of Site
Slope areas should be buffered and marked prior to application.

Soil Description Explanation
All depths are in inches.
n/a means not encountered or not applicable.
Horizons are depicted in standard soil taxonomy.
Color and mottles refer to Soil Munsell Colors.
Structure refers to the shape and size of the peds or individual soil units.
Consistency refers to the ease of which the soil can be crushed.
Mottles are defined as colors in the soil different from the predominant color matrix.
Horizons
Color
A
Surface Horizon
10 YR 4/4
Dark yellowish brown
E
Zone of leaching
10 YR 4/6
Dark yellowish brown .
B
Subsurface Horizon
7.5 YR 4/4
Dark brown
C
Parent Material Horizon
7.5 YR 4/6
Strong brown
R
Rock
7.5 YR 4/8
Strong brown
BA, BE
Transition Horizons
5 YR 4/4
Reddish brown
BC, CR
Transition Horizons
. 5 YR 4/6
Yellowish red
t
Zone of accumulation of clay
5 YR 4/8
Distinct yellowish red
5 YR 5/8
Distinct yellowish red
2.5 YR 3/6
Dark Red
Texture
2.5 YR 4/6
Red
S
Sand
2.5 YR 4/8
Red
LS
Loamy sand
2.5 YR 5/8
Red
SL
Sandy loam
Multi
Multi -colored
SCL
Sandy clay loam
SC
Sandy clay loam
C
Clay
Structure
L
Loam
wk
weak
CL
Clay loam
mo
moderate
SI
Silt
st
strong
SIL
Silt loam
f
fine
SICL
Silty clay loam
med
medium
SIC
Silty clay
gr
granular
hvy
Heavy texture modifier
sbk
subangular blocky
It
Light texture modifier
sl
structureless
gr
Gravelly
ma
massive
Consistency
vfr
very friable
fr
friable
fi
firm
vfi
very firm
to
loose

Report Number:
R07031-0004 A&L Eastern Laboratories, Inc.
Account Number: 7621 Whitepine Road Richmond, Virginia 23237 [phone]
46368 Fax No. [phone] Email: [e-mail]
Send To: BRANCH RESIDUALS & SOILS LLC Grower: DEREK TEAGUE
311B S WESTGATE DR
GREENSBORO, NC 27407
SOIL ANALYSIS REPORT
Page: 1 Date Received: 1/31/2007 Date of Analysis: 2/1/2007 Date of Report: 2/6/2007
Submitted By: BRANCH RESIDUALS
Analytical Method(s):
f
1.
'1 1�,. ....,.. ...
� ho cts
-':::.. ., .1.
Potassium� ';�
5bdfum
Y,C,.. 4
=«r�..
..:fz
Yt,(t•.�11, antoalYldtter
d: !;.
Nw�ha k
� P �
��
�Ma nest m
. �Caict[
Sam le
p,
Lab
� �, i
Vx •� F
;� I :'. �,
s .;;�, .�
;�
�
'fix
i..
K
iV1G
� CA
NA
. , m
Solt
Butte •
�
,
=E
.�.:,.,.,,
1bslA,,,Rate
, ..`u�43,t:.-
x
.. Rate....
,...P,P�_. -, .c>..
1�A m -,o Rate .,E
ate
E?P.? .tea #� ..�.
m: 'Rate
. ,P ., .,...:rtteq�1.Q�9.f
S-1
15330
3.4 110 M
73 H
65 L
235 VH
620 M
6.3
6.9
0.6
5.8
NC=61
NC=33
5-2
15331
4.3 128 M
30 L
89 M
155 H
530 L
5.4
6.8
1.6
5.8
NC=25
NC=46
T-1
15332
4.8 134 M
40 M
32 VL
215 H
1020 M
6.0
6.8
1.3
8.2
NC=33
NC=16
T-2
15333
4.8 137 M
34 M
91 M
180 H
720 M
6.2
6.9
0.7
6.1
NC=28
NC=47
u, .«,�.
f ., :�.f,.s 0. .ercent.t#asez3atu:a...
.,,...,
..: E > .3•,
t',t
:?. `y-` .,. .& ,.:a... L,
. «
k ..... ..
... ,. `9a& ..... F ,.�,
5o14tktie
,
„x . '.; -f
ChCortde ,-. >
Alufninutn=
.,>
n
€„
�
-f:•,
.1V1
�
r:: �
,Salt$,
� � � .� y
``
zNumber
� ,�£�•::•.
1�� x
-.. „ �..• ,- > -<,v,
+�:
+�:-,.. >'
� ,E: �.x
,«.,
+. ,F,.M
....�,`±�, -'
� � f
4 T�,'
-.�� � ,.� hAL� .Y.'.
. - .,...., .
�'ra �,.,. ;�' ..n�.?.
o.._, m, ,Rate; m R to
t?p , ,. ._. ..,RP..... �,_
,.,,.,>
,, m.,,_Rate
' PP ........
,.,.,
.., rn. ,Rate m- ,Rate
.PP,,, . ,-,e.., • PA, -...,. PPrn:
s
Rafe ; PP...r Rate rnslcrp Rate
'ppm r£ Rate. ,.PP.,m.'Ra{e
S-1
2.9
33.5
53.1
10.6
5-2
3.9
22.2
45.6
28.3
T-1
1.0
21.7
61.9
15.4
T-2
3.8
24.7
59.3
12.1
This report applies to the sample(s) tested. Samples are retained a
Values on this report represent the plant available nutrients in the soil. Explanation of symbols: % (percent), ppm (parts per million), IbslA (pounds per acre), maximum of thirty days after testing. Soil Analysis prepared by:
Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VIA (Very
& L EASTERN LABORATORIES, INC. (Very High). mslcm (milli -mhos per centimeter), meg1100g (milli -equivalent per 100 grams). �� �,
ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Conversions: ppm x 2 = IbsIA, Soluble Salts mslcm x 640 = ppm. by:
Paul Chu, Ph.D.
NC

Report Number:
R07031-0004 A&L Eastern Laboratories Inc.
Account Number: 7
46368 7621 Whitepine Road Richmond, Virginia [phone]
Fax No. [phone] Email: [e-mail]
To: BRANCH RESIDUALS & SOILS LLC For: DEREK TEAGUE Copy To: BRANCH RESIDUALS
311 B S WESTGATE DR
GREENSBORO, NC 27407
Attn: BOB BRANCH
Date Received: 01/31/2007
Date Reported: 02/06/2007
SOIL FERTILITY RECOMMENDATIONS
Page: 1
.,.. tee, .;
y
�y
ek?%N
1 .....
x>,,
r
.. , ......
,. .,
P os ��
ft of
�..
• ,o
P
e•.
:=-Iro ,s
6 _•,
PP
, >�
n..
a
OWE.,^
, , ,
_ _taa
•,
tX ... t:•�t ..
..,. .. r.,.
J
..
v3+ ...... ,
:.Y.. ,
. �. E ....t
•,^.
P205
- �
K20
M eu:sv�.i
._e:.
S
..i::
Zh
d '.�J
Mn,
r,»-k
Fe ,
Cu
4:
Ke,;.
� , �
Ton 1A
- :.
�. ,.• �
� r
w x ,,
S-1
Pasture
3 tons
0.0
50
30
250
0
5-2
Pasture
3 tons
1.3
50
75
235
0
T-1
Pasture
3 tons
0.8
50
60
250
0
T-2
Pasture
3 tons
0.0
50
70
235
0
Samples S-1, 5-2, T-1, T-2: For pasture, apply 30 Ibs of N per acre after pasture down or before regrowth. ALE-R,e
Samples S-1, T-1: The recommended amount of potash is the total amount per acre needed to achieve the yield goal. To prevent salt
injury, single application for K20 should not be over 200 Ibs per acre, split the total amount of K20 into 2 or 3 applications.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." C A f Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made to the t �►it-°
work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Copyright 1977. Paul Chu, Ph.D.

Report Number:
R07031-0004 r=
Acount Number: A& L Eastern La bo rto ri es, Inc.
�F
46368
7621 Whitepine Road Richmond, Virginia 23237 [phone]
Fax No. [phone] Email: [e-mail]
TO: BRANCH RESIDUALS & SOILS LLC RE: DEREK TEAGUE BRANCH RESIDUALS
311 B S WESTGATE DR
GREENSBORO, NC 27407
ATTN: BOB BRANCH
Date Received: 1/31/07 Date Reported: 02/06/2007 REPORT OF ANALYSIS Page: 1
<.. ... '... .... �. ..; ,. .., .. ,... ,... uii
s p... b.. :. 3u •. ".. - .i... .. 1 f„h1:H, ,.u..
1�f,..in ... ..
dE.,
-- '� k -� ,a.R.•'.
?.
3..E xN •. M:. J.: 5 €
-{.. .. ... .�.,:....
E
.,: ., .. -....... .. <x... .. a. .„...,
� ANQI,YSIS x t IESUL,T. MBTH013 �k,E
. .�
� }�
15330
S-1
Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
(Mo)- Mehlich-3
0.4
PPm
NCR-13 No._221, 1998.._.__.
15331
5-2
Mercury - Mehlich-3
< 0.2
mg/kg
_ ........ __
SW 846-7471A
.... ........... ..._._.... _............._Molybdenu... (Mo)_Mehlich-3........._
................. ....................... _..........................._0..3.........._
........ ....... ppm
........................................................................................................................................._................._........_...................................._..._..................................................
NCR-13 No. 221, 1998
15332
T-1
Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
_._.
__ Molybdenum (Mo)- Mehlich-3
�0.3
ppm
NCR-13 No. 221, 1998
15333
T-2
Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
..... .................................
............ .....................................
.................. _......... ....... __..... _..............................._....... Molybdenum (Mo)- Mehlich-3
0.4
ppm
...................................._.......................__..........._.._.._...................._,
NCR-13 No. 221 1998
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made rDAX a —
Paul
the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Paul Chu, Ph.D.

BAXTER
CATAWBA COUNTY
DEREK TEAGUE FARM
fA .
S-1
CmB2 *
CmC2
CmD2
Cecil sandy loam 2 to 6 percent slopes, eroded
Fescue
218
Cecil sandy loam 6 to 10 percent slopes, eroded
Cecil sandy loam 10 to 15 percent slopes, eroded
S-2
HsB2 *
CmB2
CmC2
HsC2
Cw
Hiwassee loam, 2 to 6 percent slopes, eroded
Fescue
218
Cecil sandy loam 2 to 6 percent slopes, eroded
Cecil sandy loam 6 to 10 percent slopes, eroded
Hiwassee loam, 6 to 10 percent slopes, eroded
Chewacla loam
T-1
HsB2 *
HsC2
CmB2
CmC2
CnE3
MgE2
Hiwassee loam, 2 to 6 percent slopes, eroded
Fescue
218
Hiwassee loam, 6 to 10 percent slopes, eroded
Cecil sandy loam 2 to 6 percent slopes, eroded
Cecil sandy loam 6 to 10 percent slopes, eroded
Cecil sandy loam 10 to 25 percent slope, severely eroded
Madison gravelly sand loam 10 to 25 percent slope, eroded
T-2
MgC2 *
MgB2
MgE2
CmC2
Madison gravelly sand loam 6 to 10 percent slope, eroded
Fescue
163
Madison gravelly sand loam 2 to 6 percent slope, eroded
Madison gravelly sand loam 10 to 25 percent slope, eroded
Cecil sandy loam 6 to 10 percent slopes, eroded
* Indicates predominant soil type and basis for realistic yield expectations (RYE)
hftp://www.soil.ncsu.edu/nmp/­ncnmwq/vields/

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PM"ASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK- OR BOX WHEN NOT APPLICABLE.
Facility Na,i,,m.e: Lincoln County Permit #: WQ0016922 . Annual Dry Tons Applied:
Owner. Trilby Setzer Operator: Derek Teague Cation Exchange Capacity (non 503):
Site #: �� S-01 Field #: S-01 Acres Utilized: 19 8 Acres Permitted: 19.8
o=''
Totals
Cond.
Inches
Appli-
Voli-
Miner-
0 S.
�,,,•Yd,
/o
Tons Per
Residual
Preci
cation
tila-
ala-
Y o
Q
a . -,
Re7 ort
Per
Acre
Solids
Acre
Sources
(Summarize)
�3'�
past 24
Meth-
zation
zation
TKN
Hrs.
od*
Rate**
Rate
Moist
5-06
2`7�­_,'00
14116
0.56
0.329640606
WWTP
dry
0
s
0.5
30%
12.14
5-06
21 ` ,':00
10833
5.53
2.4981775
WTP
dry
0
s
0.5
30%
7200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
kmmo-
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Cro 1 or Cro
p p
2
Crop 1 Crop 2
41100
411
5.69266
#######
Fescue
1
700
1
11.4966
#######
Fescue
2
0
0
3
0
0
4
0
1 0
15
0
0
6
0
0
7
0
0
8
0
0
9
0
0
1(
0
0
1]
0
0
1.
TOTAL; 24949 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annual 0.0587042 0.00697 0.38169 0.80735 0.08549 0.00232 0.06175 0.12163 0.01109 0.82999 30.9164 17.1893 0 Date lbs/ac
Current C. :. dative 1bs/ac 0.1114294
4 0.051
78 0.38169 8.43479 1.47135 0.03744 0.
18237 0.46549 0.07903 12.3962
PriorYea; 0 05 e� arnul 27252 0 ative lbs/a 04481 0 C 7.62744 3 1. 8586 0.03512
12 0.11462 0.34386 0.06794 11.5662
>> > ''> 1.
P rmi -
i= :
***
e tt� : .. P. L. R 36 34 NA
1338 6 2 7 15 NA 374 89
2498
Pe t nru P�.� :,..^.m..
it 1 st/2nd Cro
p
P
250
0
"I certif,; , ..g..der penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significarm: penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incornoration -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** IP.Ic , 9SF Data and the Dry Tons Per Acre are to be entered on the WLSF Form. The FSF and NFLSF are mathematically linked so this information needs to be entered
ir:;,, `'';_ same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Pf F SSE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility N...aA2.ne: Lincoln County Permit #: WQ0016922 Annual Dry Tons Applied: 14.09
Owner. Larry Teague Operator
Site #: -01 Field #: T-01
Acres Utilized: 26
Derek Teague Cation Exchange Capacity (non 503):
Acres Permitted: 26
0
0 o
Q
":i
! `' '
Gal.
�; , Yd.
i ,•ort
P;oiaai
Totals
Per
Acre
o
/o
Solids
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
�,
Wet
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo-
ma-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p 2
Crop 1
Crop 2
4-05
33 000
13000
1
0.5421
WWTP
dry
0
s
0.5
30%
91000
22000
150
34.5318
#######
Fescue
1
'f
0
0
0
0
2
0
0
0
0
3
-
0
0
0
0
4
0
0
0
0
15.
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTAL-
13000
::: ::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annual E', y :,,,re
0.004022382
0.00195
0
0.41633
0.04987
0.00186
0
0.02385
0.00679
0.68413
22.7682
34.5318
0
Date
lbs/ac
Current ( _­;.ilative lbs/ac
0.010822382 0.01055 0 1.18633 0.15687 0.00665 0.1447 0.11785 0.01579 1.70413
0.0068 0.0086 0 0.77 0.107 0.00479 0.1447 1 0.094 1 0.009 1.02
36 34 NA 1338 267 15 NA 374 89 2498
250
>
Prior Year., ,= umulative lbs/ac
Permitted f:'. P. L. R.***
Permit PA, a t.inut 1 st/2nd Crop
"I certify: ~der penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed ssure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significat, -nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
V J -c �'
*Application Method: S -Surface, IN -Injection, INC -Incorporation
Signature of and Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
**** T, � , :SF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)

aceAnalytical
www.pacelabs.com
October 09, 2006
Mr. Stephen Gouge
Baxter Healthcare Corporation
P.O. Box 1390
Hwy 221N, Pitts Station Road
Marion, NC 28752
RE: Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Dear Mr. Gouge:
Pace Analytical Ser✓ices, Inc..
9800 Kincey Avenue, Suite 10(1
Huntersville, NC 2807111
Phone: [phone]
Fax: [phone]
Pace ,1 II;'alylical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 21, 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrai:td in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organ-!: testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
2(� - � / r
Annette Scott
[e-mail]
[phone] ext. 233
Project Manager
Enclosures
Asheville Certification IN NC Wastewater 40 REPORT OF LAOORATORI( ANALI(SIS
OrinIdPg ���,.,�... ?77
FL RIELAP E87648
yc
Charlotte C_l.r::ification IDs
Nr •_'VJ �'r,r: 0
99006
FL NELAP E87627

ace Analytical °
www.pacelabs.com
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntelsville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Am Ittical Services, Inc.
'225 Riverside Drive
lsheville, NC 28804
'gone: 828.254.7176
Fax: [phone]
Lab Project Number: c')2128129
Client Project ID: QUARTERLY SLUDGE
Lab Sample No: 927460360 Project Sample Number: 92128129-001. Date Collec-i.ed: 09/21/06 14:10
Client Sample ID: DIGESTER SLUDGE Matrix: Soil Date Recei%gad: 09/21/06 16:30
Parameters Results Units Report Limit Analyzed By CAS No. Quu lRegLmt
Metals
Trace ICP Metals, TCLP Leach. Method: EPA 6010
Date Digested 09/22/06 15:00 09/22/06 15:00
Trace ICP Metals, TCLP Leach.
Prep/Method: EPA 3010
/ EPA 6010
Arsenic
ND
mg/l
0.025
Barium
0.21
mg/l
0.025
Cadmium
ND
mg/l
0.0050
Chromium
ND
mg/l
0.025
Lead
0.050
mg/l
0.025
Selenium
ND
mg/l
0.050
Silver
ND
mg/l
0.025
Date Digested
09/26/06 08:00
Metals, Trace ICP
Prep/Method: EPA 3050
/ EPA 6010
Cadmium
ND
mg/kg
1.4
Calcium
6700
mg/kg
140
Chromium
37.
mg/kg
7.2
Copper
140
mg/kg
7.2
Lead
18.
mg/kg
7.2
Magnesium
1300
mg/kg
140
Nickel
15.
mg/kg
7.2
Potassium
ND
mg/kg
1400
Sodium
4000
mg/kg
1400
Zinc
150
mg/kg
14.
Date Digested
09/27/06 09:30
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Mercury ND mg/l
Wet Chemistry
Percent Moisture
Percent Moisture
Total Percent Solids
Percent Solids
Total Volatile Solids
Date: 10/09/06
Method: % Moisture
93.8 %
Method: EPA 160.3
6.2 %
Method: EPA 160.4
09/26/06 13:29 EWS 7440-38-2
09/26/06 13:29 EWS 7440-39-3
09/26/06 13:29 EWS 7440-43-9
09/26/06 13:29 EWS 7440-47-3
09/26/06 13:29 EWS 7439-92-1
09/26/06 13:29 EWS 7782-49-2
09/26/06 13:29 EWS 7440-22-4
09/26/06 08:00
09/30/06 15:27 JDA1 7440-43-9
09/30/06 15:27 JDA1 7440-70-2
09/30/06 15:27 JDA1 7440-47-3
09/30/06 15:27 JDA1 7440-50-8
09/30/06 15:27 JDA1 7439-92-1
09/30/06 15:27 JDAi 7439-95-4
00/30/06 15:27 JDA1 7440-02-0
09/30/06 15:27 JDA1 i'440-09-7
09/30/06 15:27 JDA1 7440-23-5
09/30/06 15:27 JDA1 7440-66-6
09/27/06 09:30
0.00020 09/25/06 11:15 ALV 7439-97-6
09/22/06 11:54 TNM
09/26/06 TNM
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
DiInking Vlater 7 )
SC J:SU Oliit ou, ilu< x'`V:i' cl Giri ,ii of Pat,c ,.1'Cal
FL NELAP E87648
tFU " • � c
mei c T
Page: 1 of 29
Charlotte (;frtification IDs
aC 99006
FL NELAP E87627

;aneAnalyficaP)
www.pacelahs.com
Lab Sample No: 927460360
Client Sample ID: DIGESTER SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Ana, j�'tical Services, Inc.
?25 Riverside Drive
Asheville, NC 28804
f'Fi one: 828.254.7176
Fax., 828.252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Project Sample Number: 92128129-001 Date Collect,�d: 09/21/06 14:10
Matrix: Soil Date Recefif,,d: 09/21/06 16:30
Parameters
Results
Units Report Limit
Analyzed
By
CAS No. QuiI... RegLmt
Total Volatile Solids
13800
mg/kg
0-100
09/27/06
18:30
JMW
Chloride(Mercuric Nitrate)
Method:
EPA
325.2 Modified
Chloride
4600
mg/kg
800
09/29/06
13:51
JDA1
116887-00-6
Nitrogen, Ammonia
Method:
EPA
350.1 Modified
Nitrogen, Ammonia
ND
mg/kg
160
09/25/06
10:33
JDA1
7727-37-9
Total Kjeldahl Nitrogen, Soil
Method:
EPA
351.2
Nitrogen, Kjeldahl, Total
16000
mg/kg
800
09/27/06
17:45
JMW
Nitrogen, Nitrate plus Nitrite
Method:
EPA
353.2 Modified
Nitrate as N
2700
mg/kg
150
09/22/06
10:25
JDA1
Nitrate -Nitrite (as N)
2700
mg/kg
150
09/22/06
10:25
JDA1
'7727-37-9
Phosphorus, Total, Soil
Method:
EPA
365.2
Phosphorus
NO
mg/kg
6290
10/02/06
16:30
JDA1
7723-14-0
Sulfate, Total, Soil
Method:
EPA
375.4 Modified
Sulfate
NO
mg/kg
8000
09/29/06
14:05
JDA1
pH Method: EPA 9045
pH 5.00 units
Plant Available Nitrogen Method:
Nitrogen 7500 mg/kg
S.O.U.R. Method: Standard Methods
SOUR ND mg/g/hr
GUMS Semivolatiles
Semivolatile Organics, TCLP
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Date: 10/09/06
09/25/06 06:50 TMR
1.0 10/05/06 SHB 7'727-37-9
1 10/04/06 SHB 1
Prep/Method:
EPA 3510
/ EPA 8270
NO
mg/l
0.75
10/03/06
00:52
BET
1.06-46-7
ND
mg/l
0.013
10/03/06
00:52
BET
121-14-2
NO
mg/l
0.050
10/03/06
00:52
BET
617-68-3
NO
mg/l
0.013
10/03/06
00:52
BET
118-74-1
NO
mg/l
0.30
10/03/06
00:52
BET
67-72-1
ND
mg/l
0,050
10/03/06
00:52
BET
95-48-7
NO
mg/l
0.010
10/03/06
00:52
BET
Asheville Certification IDs REPORT OF LARDR�TORY ANAVYSIS
NC lnhsie,n/ater 4^
N!(.- Dwikihq, bVai:n 37,11 i „lIS 1'e.p,
SC the `wi:ldii Gi,i. _-I.: 0I �.� . , i'- IF.a. J • . "1:,.
�x nr. r. olio
FL NELAP E87648
-n =r
Page: 2 of 29
Charlotte Gi:irtification IDs
+I(. `Aa1-j1 06
SC 99006
FL NELAF E87627

;acneAnalyficalo
www.pacelabs.com
Lab Sample No: 927460360
Client Sample ID: DIGESTER SLUDGE
Pace Analytical Services, Inc.
Pace Ana) 1,1ical Services, Inc.
9800 Kincey Avenue, Suite 100
:'.;:25 Riverside Drive
Huntersville, NC 28078
4 3heville, NC 28804
Phone: [phone]
h one: 828.254.7176
Fax: [phone]
Fax: [phone]
Lab Project -Number: S2128129
Client Project ID: QUARTERLY SLUDGE
Project Sample Number: 92128129-001 Date Colleci:i!c: 09/21/06 14:10
Matrix: Soil Date Receiw!c: 09/21/06 16:30
Parameters
Results
Units
Report Limit
Analyzed
By
- CAS No. uzi._. RegLmt
Nitrobenzene
ND
mg/l
0.20
10/03/06
00:52
BET
98-95.3
Pentachlorophenol
NO
mg/l
10.
10/03/06
00:52
BET
87-86-5
Pyridine
ND
mg/l
0.50
10/03/06
00:52
BET
1.10-86-1
2,4,5-Trichlorophenol
NO
mg/l
40.
10/03/06
00:52
BET
95-95-4
2.4,6-Trichlorophenol
NO
mg/l
0.20
10/03/06
00:52
BET
88-06.2
Nitrobenzene-d5 (S)
41
%
10/03/06
00:52
BET
4165-60-0
2-Fluorobiphenyl (S)
44
%
10/03/06
00:52
BET
321-60.8
Terphenyl-d14 (S)
55
%
10/03/06
00:52
BET
1.718-51-0
Phenol-d5 (S)
19
%
10/03/06
00:52
BET
4165-62-2
2-Fluorophenol (S)
28
%
10/03/06
00:52
BET
367-12-4
2,4,6-Tribromophenol (S)
58
%
10/03/06
00:52
BET
118-79-6
Date Extracted
09/29/06
09/29/06
GC Semivolatiles
Pesticides, TCLP Leachate
Prep/Method:
EPA 3535 /
EPA 8081
gamma-BHC (Lindane)
ND
mg/1
0.040
10/04/06
12:02
JEM
58-89-9
Chlordane
ND
mg/1
0.0030
10/04/06
12:02
JEM
57-74.9
Endrin
ND
mg/l
0.0020
10/04/06
12:02
JEM
'72.20.8
Heptachlor
ND
mg/l
0.00080
10/04/06
12:02
JEM
76-44.8
Methoxychlor
ND
mg/l
1.0
10/04/06
12:02
JEM
72-43-5
Toxaphene
ND
mg/l
0.050
10/04/06
12:02
JEM
13001-35.2
Tetrachloro-m-xylene (S)
64
%
10/04/06
12:02
JEM
877.09-8
Decachlorobiphenyl (S)
88
%
10/04/06
12:02
JEM
2051-24-3
Date Extracted
10/03/06
10/03/06
GUMS Vol ati l es
Volatile Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1.4-Dichlorobenzene
1,2-Dichloroethane
1.1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
jT luene-d8 (S)
Date: 10/09/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
Method:
EPA 8260
ND
mg/l
0.0050
10/06/06
18:19
DLK
71-43-2
ND
mg/l
0.10
10/06/06
18:19
DLK
78-93.3
NO
mg/l
0.0050
10/06/06
18:19
DLK
56-23-5
ND
mg/l
0.0050
10/06/06
18:19
DLK
108.90-7
ND
mg/l
0.0050
10/06/06
18:19
DLK
60 -66.3
ND
mg/l
0.0050
10/06/06
18:19
DLK
1.06-46-7
ND
mg/l
0.0050
10/06/06
18:19
DLK
1.07-06.2
ND
mg/l
0.0050
10/06/06
18:19
DLK
75-35.4
ND
mg/l
0.0050
10/06/06
18:19
DLK
1.27.18.4
ND
mg/l
0.0050
10/06/06
18:19
DLK
79-01-6
ND
mg/l
0.0050
10/06/06
18:19
DLK
75.01-4
130
%
10/06/06
18:19
DLK
2037-26-5 2
Page: 3 of 29
REPORT OF LABORATORY ANALYSIS ChaWase..Q.atetf r!cation IDs
12
This report shall not be reproduced, except in full, NC Drink:i-ilj Water 37706
without the written consent of Pace Analytical Services, Inc. Sc 99006
627
FL NELAf E87
W

ace Analytical
www.pacelabs.com
I
Lab Sample No: 927460360
Client Sample ID: DIGESTER SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analy!0al Services, Inc.
' >"5 Riverside Drive
s Neville, NC 28804
PI; o ve: 828.254.7176
Fax: [phone]
Lab Project Number: 92128129
Client Project ID: QLARTERLY SLUDGE
Project Sample Number: 92128129.001 Date Collected: 09/21/06 14:10
Matrix: Soil Date Received: 09/21/06 16:30
Parameters
Results
Units Report Limit Analyzed
By
CAS No. La_.. RegLmt
4-Bromofluorobenzene (S)
98
% 10/06/06
18:19
DLK
I•a50-00-4
Dibromofluoromethane (S)
92
% 10/06/06
18:19
DLK
3.868-53-7
1,2-Dichloroethane-d4 (S)
97
X 10/06/06
18:19
DLK
].7060 07 0 3
Date: 10/09/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
a nccoRn
Page: 4 of 29
CharlottE: (','ertification IDs
NC Wastfiv,ater
12
NC Drinkin) Water
37706
Sc
99006
FL NELAIP
E87627

aceAnalytical0
www.pacelabs.com
PARAMETER FOOTNOTES
Method 9071B modified to use ASE.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 26078
Phone: [phone]
Fax: [phone]
Pace Anal.Vli;al Services, Inc.
2"'15 Riverside Drive
!.sheville, NC 28804
Pt one: 828.254.7176
fax: [phone]
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outs -de of EPA recormn:!nded immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a (J-y weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
Ill % Dry solids = 6.2%
[21 The surrogate recovery was above the QC recovery limit. The sample was not re extracted since no target
analytes were detected in the sample.
[31 Analysis conducted in excess of EPA recommended holding time.
E
Date: 10/09/06 Page: 5 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte..:;.;rtification IDs
NC Wastewater
40
This report shall not be reproduced, except in full,
NC Wast?.tvater
NC Drinki'iij Water
12
37706
NC Drinking Water
37712
without the written consent of Pace Analytical Services, Inc.
Sc
99006
Sc
FL NELAP
99030
E87648
�`'°�� ` "��"y
FL NELAF
E87627
�°�`elac4

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
grip AnaliltiralO Phone: 704.875.909
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 169250
QC Batch Method: EPA 3535
Associated Lab Samples: 927460360
METHOD BLANK: 927506816
Associated Lab Samples: 927460360
Parameter
Units
gamma-BHC (Lindane)
mg/l
Chlordane
mg/1
Endrin
mg/l
Heptachlor
mg/l
Methoxychlor
mg/l
Toxaphene
mg/l
Tetrachloro-m-xylene (S)
X
Decachlorobiphenyl (S)
LABORATORY CONTROL SAMPLE: 927506824
Pace Analytical Services, Inc.
2 "'S Riverside Drive
7 s:heville, NC 28804
PI 'line: 828.254.7176
1 ax.- 828.252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Analysis Method: EPA 8081
Analysis Description: Pesticides, TCLP Leachate
Blank
Reporting
Result
Limit Footnotes
NO
0.040
NO
0.0030
NO
0.0020
NO
0.0008
NO
1.0
ND
0.050
47
74
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
gamma-BHC (Lindane)
mg/l
0.0004
0.0002
50
Endrin
mg/l
0.0004
0.0002
60
Heptachlor
mg/l
0.0004
0.0002
57
Methoxychlor
mg/l
0.0010
0.0009
94
Tetrachloro-m-xylene (S)
48
Decachlorobiphenyl (S)
145
Date: 10/09/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
u nc c0�o
a:
�redac-
Page: 6 of 29
Charlotte Certification IDs
NC Waste\,2iter 12
NC Drinkiry Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100 "'?5 Riverside Drive
Huntersville, NC 28078 7s5;heville, NC 28804
Phone: [phone] Pi one: 828.254.7176
ace Analytical e
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 9z'128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 167375 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: Semivolatile Organics, T(:LP
Associated Lab Samples: 927460360
METHOD BLANK: 927448795
Associated Lab Samples: 927460360
Parameter
Units
1.4-Dichlorobenzene
mg/l
2,4-Dinitrotoluene
mg/l
Hexachloro-1,3-butadiene
mg/l
Hexachlorobenzene
mg/l
Hexachloroethane
mg/l
2-Methylphenol (o-Cresol)
mg/l
3&4-Methylphenol
mg/l
Nitrobenzene
mg/l
Pentachlorophenol
mg/l
Pyridine
mg/l
2,4,5-Trichlorophenol
mg/l
2,4,6-Trichlorophenol
mg/l
Nitrobenzene-d5 (S)
X
2-Fluorobiphenyl (S)
X
Terphenyl-d14 (S)
X
Phenol-d5 (S)
X
2-Fluorophenol (S)
%
2.4.6-Tribromophenol (S)
%
LABORATORY CONTROL SAMPLE: 927416024
Blank
Reporting
Result
Limit Footnotes
NO
0.75
NO
0.013
ND
0.050
ND
0.013
NO
0.30
NO
0.050
NO
0.010
NO
0.20
NO
10.
NO
0.50
NO
40.
NO
0.20
57
60
74
19
30
42
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
1.4-Dichlorobenzene
mg/l
0.0500
0.0274
55
2,4-Dinitrotoluene
mg/l
0.0500
0.0389
78
Hexachloro-1.3-butadiene
mg/l
0.0500
0.0218
44
Hexachlorobenzene
mg/l
0.0500
0.0284
57
Hexachloroethane
mg/l
0.0500
0.0224
45
2-Methylphenol (o-Cresol)
mg/l
0.0500
0.0263
52
3&#4Methylphenol
mg/l
0.0500
0.0264
53
Date: 10/09/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N AIFO�
., F
nelac:
Page: 7 of 29
Charlotte (;ertification IDs
NC Wastewiter 12
NC Drinkircl Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
aceAnalytical ® Phone: 704.875.909
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 927416024
Parameter
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4.6-Tribromophenol (S)
Spike
LCS
LCS
Units
Conc.
Result
% Rec
mg/l
0.0500
0.0331
66
mg/l
0.0500
0.0205
41
mg/l
0.0500
0.0199
40
mg/l
0.0500
0.0260
52
mg/l
0.0500
0.0285
57
62
70
80
27
39
60
LABORATORY CONTROL SAMPLE: 927444372
Pace Analpi'Ical Services, Inc.
2:',?5 Riverside Drive
msheville, NC 28804
F'1,cne: 828.254.7176
lax: 828.252.4618
Lab Project Number: 92/28129
Client Project ID: QUARTERLY SLUDGE
Spike
LCS
LCS
Parameter
Units
Conc.
Result
Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.1542
62
2,4-Dinitrotoluene
mg/l
0.2500
0.2277
91
Hexachloro-1.3-butadiene
mg/l
0.2500
0.1211
48
Hexachlorobenzene
mg/l
0.2500
0.1780
71
Hexachloroethane
mg/l
0.2500
0.1284
51
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1411
56
3&4-Methylphenol
mg/l
0.2500
0.1375
55
Nitrobenzene
mg/l
0.2500
0.1950
78
Pentachlorophenol
mg/l
0.2500
0.0854
34
Pyridine
mg/l
0.2500
0.1107
44
2.4,5-Trichlorophenol
mg/l
0.2500
0.1870
75
2.4,6-Trichlorophenol
mg/l
0.2500
0.1814
73
Nitrobenzene-d5 (S)
71
2-Fluorobiphenyl (S)
76
Terphenyl-d14 (S)
76
Phenol-d5 (S)
29
2-Fluorophenol (S)
40
2.4.6-Tribromophenol (S)
63
Date: 10/09/06
Asheville Certification IDs
NO Wastewater 40
NO Drinking Water 37712
SC 99030
FL NELAP E87648
1
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N AC f.�RG
%neiac ,4
Page: 8 of 29
Charlotte ( artification IDs
NO Wastem-ter
12
NO Drinkirll Water
37706
SC
99006
FL NELAF
E87627

aceAnalytical°
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 927448803
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
1,4-Dichlorobenzene
mg/l
0.2500
0.1278
51
2,4-Dinitrotoluene
mg/l
0.2500
0.2260
90
Hexachloro-1.3-butadiene
mg/l
0.2500
0.1000
40
Hexachlorobenzene
mg/l
0.2500
0.1774
71
Hexachloroethane
mg/l
0.2500
0.1058
42
2-Methylphenol (o-Cresol)
mg/l
0.2500
0.1314
53
3&4-Methylphenol
mg/1
0.2500
0.1267
51
Nitrobenzene
mg/l
0.2500
0.1884
75
Pentachlorophenol
mg/l
0.2500
0.1388
56
Pyridine
mg/1
0.2500
0.0993
40
2.4,5-Trichlorophenol
mg/l
0.2500
0.1828
73
2,4,6-Trichlorophenol
mg/l
0.2500
0.1843
74
Nitrobenzene-d5 (S)
68
2-Fluorobiphenyl (S)
76
Terphenyl-d14 (S)
75
Phenol-d5 (S)
26
2-Fluorophenol (S)
36
2.4.6-Tribromophenol (S)
64
LABORATORY CONTROL SAMPLE:
92.7494682
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
1,4-Dichlorobenzene
mg/l
0.0500
0.0186
37
2,4-Dinitrotoluene
mg/l
0.0500
0.0272
54
Hexachloro-1,3-butadiene
mg/l
0.0500
0.0108
22
Hexachlorobenzene
mg/l
0.0500
0.0295
59
Hexachloroethane
mg/l
0.0500
0.0145
29
2-Methylphenol (o-Cresol)
mg/l
0.0500
0.0248
50
3&4-Methylphenol
mg/l
0.0500
0.0201
40
Nitrobenzene
mg/l
0.0500
0.0243
48
Pentachlorophenol
mg/l
0.0500
0.0223
44
Pyridine
mg/l
0.0500
0.0166
33
2.4.5-Trichlorophenol
mg/l
0.0500
0.0302
60
2.4,6-Trichlorophenol
mg/l
0.0500
0.0275
55
Niprpbenzene-6 (S)
49
2 6l orobiphenyl (S)
59
Terphenyl-d14 (S)
53
Phenol-d5 (S)
21
2-Fluorophenol (S)
33
2,4,6-Tribromophenol (S)
67
Ashevillg,QgrtWgWjQ@
IDs
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
Pace Anallili,al Services, Inc.
"?5 Riverside Drive
sheville, NC 28804
Rorie: 828.254.7176
Fax: [phone]
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Footnotes
Footnotes
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N AC5pRo
-�elac£
Charlotte (:g 'q4 I s
NC Waste%ir:.ter 12
NC Drinking Water 37706
Sc 99006
FL NELAR E87627

Pace Analytical Services, Inc. Pace Anali'Y li„al Services, Inc.
9800 Kincey Avenue, Suite 100 ' "'S Riverside Drive
Huntersville, NC 28078 Is heville, NC 28804
/62ro 4nahitiral' Phone: [phone] Pl:iFax: 828.252.7176
4618
Fax: [phone] Fax: [phone]
www.pacelabs.com
4
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
Charlotte G:irtification IN
NC Wastewater
40
This report shall not be reproduced, except in full,
NC Waste%, .ter
NC Drinkirg Water
12
37706
NC Drinking Water
37712
without the written consent of Pace Analytical Services, Inc.
SC
99006
SC
99030
"°°°
FL NELAP
E87648
'" 'k°'�
, ° :..._...
;slack-
FL NELAF'
E87627

Pace Analytical Services, Inc. Pace Anal ylical Services, Inc.
9800 Kincey Avenue, Suite 100 2?G?5 Riverside Drive
Huntersville, NC 28078 1 sheville, NC 28804
X<Inp. Anal vtir,3l ® Phone: 704.875.909Pt 828.254.7176
Fax: [phone] Fax: [phone]
www pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 92:128129
Client Project ID: QUARTERLY SLUDGE
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 927416032 927416040
927406728
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result %
Rec: %
Rec
RPD Fooiiotes
1,4-Dichlorobenzene
mg/l
0
0.2500
0.1247
0.1298
50
52
4
2.4-Dinitrotoluene
mg/l
0
0.2500
0.1807
0.1895
72,
76
5
Hexachloro-1,3-butadiene
mg/l
0
0.2500
0.0955
0.1038
38
42
8
Hexachlorobenzene
mg/l
0
0.2500
0.1292
0.1391
52.
56
7
Hexachloroethane
mg/l
0
0.2500
0.0941
0.1023
38
41
8
2-Methylphenol (o-Cresol)
mg/l
0
0.2500
0.1227
0.1270
49
51
3
3&4-Methylphenol
mg/l
0
0.2500
0.1245
0.1262
50
50
1
Nitrobenzene
mg/l
0
0.2500
0.1537
0.1644
62'
66
7
Pentachlorophenol
mg/l
0
0.2500
0.1052
0.0825
42
33
24
Pyridine
mg/l
0
0.2500
0.1002
0.1054
40
42
5
2.4,5-Trichlorophenol
mg/l
0
0.2500
0.1193
0.1109
4E;
44
7
2,4,6-Trichlorophenol
mg/l
0
0.2500
0.1326
0.1290
5:-
52
3
Nitrobenzene-d5 (S)
5<.
59
2-Fluorobiphenyl (S)
60
66
Terphenyl-d14 (S)
68
65
Phenol-d5 (S)
2`•.
26
2-Fluorophenol (S)
37
38
2,4.6-Tribromophenol (S)
51.
53
Date: 10/09/06 Page: 10 of 29
Asheville Certification IDs
NO Wastewater 40
NO Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCp
0
O F
u
Charlotte (. rtification IDs
NO Waste�i;Jer 12
NO Drinking Water 37706
SC 99006
FL NELAF E87627

Pace Analytical Services, Inc. Pace AnalY li.;al Services, Inc.
9800 Kincey Avenue, Suite 100 '' ""'5 Riverside Drive
Huntersville, NC 28078 1s Neville, NC 28804
ace Analytical ® Phone: [phone] Pl:ime: 828.254.7176
Fax: [phone] Fax.- 828.252.4618
www.pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 92128129
Client Project ID: QLARTERLY SLUDGE
QC Batch: 169459 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: Volatile Organics, TCLP leach.
Associated Lab Samples: 927460360
METHOD BLANK: 927516641
Associated Lab Samples: 927460360
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzene
mg/l
NO
0.0050
2-Butanone (MEK)
mg/l
NO
0.10
Carbon tetrachloride
mg/1
ND
0.0050
Chlorobenzene
mg/l
NO
0.0050
Chloroform
mg/l
NO
0.0050
1,4-Dichlorobenzene
mg/l
NO
0.0050
1,2-Dichloroethane
mg/l
ND
0.0050
1,1-Dichloroethene
mg/l
ND
0.0050
Tetrachloroethene
mg/l
ND
0.0050
Trichloroethene
mg/l
NO
0.0050
Vinyl chloride
mg/l
NO
0.0050
Toluene-d8 (S)
%
109
4-13romofluorobenzene (S)
X
94
Dibromofluoromethane (S)
%
106
1.2-Dichloroethane-d4 (S)
%
99
LABORATORY CONTROL SAMPLE: 927516658
Spike
LCS
Parameter
Units
Conc.
Result
Benzene
mg/l
0.0500
0.0548
2-Butanone (MEK)
mg/l
0.1000
0.0816
Carbon tetrachloride
mg/l
0.0500
0.0572
Chlorobenzene
mg/l
0.0500
0.0552
Chloroform
mg/l
0.0500
0.0523
1.4-Dichlorobenzene
mg/l
0.0500
0.0522
1,2-Dichloroethane
mg/l
0.0500
0.0508
1,1-Dichloroethene
mg/l
0.0500
0.0588
Tetrachloroethene
mg/l
0.0500
0.0592
T�,nFhloroethene
mg/l
0.0500
0.0554
Date: 10/09/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
LCS
X Rec Footnotes
109
82
114
110
105
104
102
118
118
111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
`N ACOOgO
°r�elac�=
Page: 11 of 29
Charlotte i;(;rtification IN
NC Wastewater 12
NC Drinkir ;I Water 37706
SC 99006
FL NELAP E87627

ace Analytical
www.pacelabs.com
I
LABORATORY CONTROL SAMPLE: 927516658
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Ana.f iffcal Services, Inc.
,,,.25 Riverside Drive
Arheville, NC 28804
P `.1i me: 828.'254.7176
.=ax. 828.252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Vinyl chloride mg/l 0.0500 0.0630 126
Toluene-d8 (S) 94
4-Bromofluorobenzene (S) 98
Dibromofluoromethane (S) 95
1,2-Dichloroethane-d4 (S) 100
Date: 10/09/06 Page: 12 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte il;.tification IDs
NO Wastewater
40
NO Wastew:iler
12
NO Drinking Water
37712
This report shall not be reproduced, except in full,
NO Drinkin ;i Water
37706
SC
99030
without the written consent of Pace Analytical Services, Inc.
SC
99006
FL NELAP
E87648
0 N ACCORD
f
FL NELAP
E87627
W�
e act

Pace Analytical Services, Inc. Pace Anal!ylisal Services, Inc.
9800 Kincey Avenue, Suite 100 Riverside Drive
Huntersville, NC 28078 .1;> Neville, NC 28804
Phone. 704.875.909Pi828.254.7176
Fax[phone] fax: [phone]aceAnalya®ic
www.pace►abs.com QUALITY CONTROL DATA
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168463 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: Mercury, CVAAS, TCLP Leac:hate
Associated Lab Samples: 927460360
METHOD BLANK: 927470799
Associated Lab Samples: 927460360
Blank Reporting
Parameter Units Result Limit Footnotes
Mercury mg/l ND 0.0002
LABORATORY CONTROL SAMPLE: 927470807
Spike LCS LCS
Parameter Units Conc. Result Rec Footnotes
Mercury mg/l 0.0025 0.0024 96
MATRIX SPIKE: 927470815
927464677
Spike
MS
MS
Parameter Units Result
Conc.
Result %
Rec Footnotes..
Mercury mg/l 0.00005
0.0025
0.0034
132 1
SAMPLE DUPLICATE: 927470823
Parameter Units
Mercury mg/l
I
Date: 10/09/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
927445486 DUP
Result Result RPD Footnotes
ND ND NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
`p ACCORp
."hdac
Page: 13 of 29
Charlotte.';!;!rtification IN
NC Wastu,,i.iter
12
NC Drink n(: Water
37706
SC
99006
FL NELAI'
E87627

ace Analytical °
www.pacelahs.com
QC Batch: 168494
QC Batch Method: EPA 3010
Associated Lab Samples: 927460360
METHOD BLANK: 927472308
Associated Lab Samples: 927460360
Parameter
Units
Arsenic
mg/1
Barium
mg/1
Cadmium
mg/1
Chromium
mg/1
Lead
mg/l
Selenium
mg/l
Silver
mg/1
LABORATORY CONTROL SAMPLE: 927472316
Pace Anaiyncaj Services, u,c.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
r aoc nuu I,P a vu. v— - I vv, ..._.
2"1S Riverside Drive
1,5heville, NC 28804
None: 828.254.7176
Fax 828:252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Analysis Method: EPA 6010
Analysis Description: Trace ICP Metals, TCLP LE!ach.
Blank
Reporting
Result
Limit Footnotes
ND
0.025
ND
0.025
ND
0.0050
NO
0.025
NO
0.025
NO
0.050
NO
0.025
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Arsenic
mg/l
2.500
2.485
99
Barium
mg/l
2.500
2.015
81
Cadmium
mg/l
2.500
2.280
91
Chromium
mg/l
2.500
2.305
92
Lead
mg/1
2.500
2.150
86
Selenium
mg/1
2.500
2.565
103
Silver
mg/1
1.250
1.165
93
MATRIX SPIKE: 927472324
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Date: 10/09/06
927445486
Spike
MS
MS
Units
Result
Conc.
Result
% Rec Footnotes_
mg/l
0
2.500
2.510
100
mg/l
0.1280
2.500
2.150
81
mg/l
0.00063
2.500
2.285
91
mg/1
0.00117
2.500
2.310
92
mg/l
0.08450
2.500
2.265
87
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
Sc 99030
FL NELAP E87648 Wc:F
Page: 14 of 29
Charlotte i;(;rtification IDs
NC Wasteul;iter 12
NC Drinkir ;I Water 37706
Sc 99006
FL NELAP E87627

ace Analytical
www.pacelahs.com
I
MATRIX SPIKE: 927472324
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Pace Anal;yll;al Services, Inc.
'' "'S Riverside Drive
l sheville, NC 28804
Pt orie: 828.254.7176
Fax.- 828.252.4618
Lab Project Number: 92/28129
Client Project ID: QUARTERLY SLUDGE
927445486
Spike
MS
MS
Parameter Units
Result
Conc.
Result
% Rec Footnotes.
Selenium mg/l
0.01295
2.500
2.600
104
Silver mg/l
0.00015
1.250
1.170
94
SAMPLE DUPLICATE: 927472332
927458786
DUP
Parameter
Units
Result
Result
RPD Footnotes
Arsenic
mg/l
ND
ND
NC
Barium
mg/l
2.000
1.800
9
Cadmium
mg/l
0.01000
0.00900
11
Chromium
mg/l
ND
ND
NC
Lead
mg/l
0.1400
0.1300
9
Selenium
mg/l
ND
ND
NC
Silver
mg/l
ND
ND
NC
Date: 10/09/06
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\tO` N . ACCpgo' n
1e1ac.,
Page: 15 of 29
Charlotte l;r.rtification IDs
NC Wastanccter 12
NC Drinkir;c; Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc. Pace Anallil'icat Services, Inc.
9800 Kincey Avenue, Suite 100 "''''S Riverside Drive
Huntersville, NC 28078 /,sheville, NC 28804
�Analv�ieal o Phone: [phone],me: 828.254.7176
Fax: [phone] ax: 828.252.4618
www.pacelahs.com QUALITY CONTROL DATA
Lab Project Number: 9,1128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168585 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: Metals, Trace ICP
Associated Lab Samples: 927460360
METHOD BLANK: 927476143
Associated Lab Samples: 927460360
Parameter
Units
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE: 927476150
Parameter
Units
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 10/09/06
Blank
Reporting
Result
Limit Footnotes
ND
0.10
ND
10.
ND
0.50
ND
0.50
ND
0.50
ND
10.
ND
0.50
ND
100
ND
100
ND
1.0
Spike
Conc.
LCS
Result
50.00
50.60
500.00
488.1
50.00
50.30
50.00
48.50
50.00
50.50
500.00
495.7
50.00
49.30
500.00
470.3
500.00
494.6
50.00
49.60
LCS
% Rec Footnotes
101
98
101
97
101
99
99
94
99
99
Page: 16 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Gi: rtification IDs
rd..Inlast2water
^r
SC
9903G
ifvithoui Gte w ider. co -Ant ui rr,.,v Aualyii,,,' _ '✓w , ;:, .
SC 99006
FL NELAP
E87648
"
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analf,VJcal Services, Inc.
9800 Kincey Avenue, Suite 100 :_'-125 Riverside Drive
Huntersville, NC 28078 iisheville, NC 28804
Analytical o Phone: [phone] Mime: 828.254.7176
Fax: [phone] i ax. 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 9,1128129
Client Project ID: QUARTERLY SLUDGE
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 927476168 927476176
927448498
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
Rec: %
Rec
RPD Footnotes
Cadmium
mg/kg
0.9682
56.40
56.73
52.63
99
97
8
Calcium
mg/kg
564.00
704.3
658.0
7
Chromium
mg/kg
14.77
56.40
71.28
67.79
100
99
5
Copper
mg/kg
56.40
67.56
62.56
8
Lead
mg/kg
8.568
56.40
62.26
58.29
9'li
93
7
Magnesium
mg/kg
564.00
838.7
787.5
6
Nickel
mg/kg
56.40
55.49
51.35
8
Potassium
mg/kg
564.00
993.9
920.3
8 1
Sodium
mg/kg
564.00
701.8
648.0
8
Zinc
mg/kg
56.40
66.21
61.81
7
SAMPLE DUPLICATE: 927476184
Parameter
Units
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 10/09/06
927448506 DUP
Result Result RPD Footnotes
0.6400 0.8100 23 2
270.0 0
13.00 14.00 7
6.700 0
8.200 8.300 1
280.0 0
1.300 0
310.0 0
ND NC
4.400 0
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NO Way}iw^.f.,Aer r`
�iJ:L?rIllklhf.VVat:-.nf,
SC 99030 vvithoui u,e wride Ariaiyiical 6ervices, :r,r::.
�N ACf.Oo
FL NELAP E87648
, enc.,
Page: 17 of 29
Charlotte CE:rtification IN
12
3770fr
SC y9006
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704, 875.9091
QUALITY CONTROL DATA
Pace Ana)Dilical Services, Inc.
:1225 Riverside Drive
4f,heville, NC 28804
P rc ne: 828.254.7176
lax: 828.252.4618
Lab Project Number: 9�128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168307 Analysis Method: Y Moisture
QC Batch Method: Analysis Description: Percent Moisture
Associated Lab Samples: 927460360
SAMPLE DUPLICATE: 927462069
927457895 DUP
Parameter Units Result Result RPD Footnotes
Percent Moisture % 17.30 16.10 7
Date: 10/09/06
Asheville Certification IDs REPORT .OF LABORATORY ANALYSIS
NC Waste%vatcl' 40
1iy.l� :+r /1
SC . J(;n,i I,W r y9U3U Writ: uut ohs ,�_i�r; cu; nL ut z„„ ,ralyticui +, es, ;
FL NELAP E87648
�rac.=
Page: 18 of 29
Charlotte Certification IDs
!2
OU C1t31JUb
FL NELAP E87627

Pace Analytical Services, Inc. Pace Anagl ifJcal Services, Inc.
9800 Kincey Avenue, Suite 100 ?:1,?5 Riverside Drive
Huntersville, NC 28078 /I;;hevi11e, NC 28804
Analytical o Phone: [phone] F11 icne: 828.254.7176
Fax: [phone] -ax: 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168459 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: pH
Associated Lab Samples: 927460360
SAMPLE DUPLICATE: 927470641
927438697 DUP
Parameter Units Result Result RPD Footnotes
pH units 6.300 6.300 0
Date: 10/09/06
Asheville Certification IDs
SC y9030
FL NELAP E87648
Page: 19 of 29
REPORT OF LARI)RAMRX ANIN SIS chari(otte'(I,E1rtification IN
'Patc, .:711"0'
nti;ou� the v;rr<<en Gu:i.,L. L of mace ivi'll ticai :,;,eo, SC 99006
A
FL NELAF' E87627
rc,,h ela ``=

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
: Analytical'5 Phone: 704.875.909
s Fax [phone]
www.pacelabs.com QUALITY CONTROL DATA
Pace Analprl',ical Services, Inc,
,,",1 ?5 Riverside Drive
,iI.;heville, NC28804
H,cne: 828.254.7176
fax: [phone]
Lab Project Number: 9,1128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168555 Analysis Method: EPA 160.3
QC Batch Method: EPA 160.3 Analysis Description: Total Percent Solids
Associated Lab Samples: 927460360
Date: 10/09/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
N'^ Wastr"vz t e' 40
SL 95030 l.t1IWA lfi$ 1V(;"ai, COW'. a'1 . J,":,,
FL NELAP E87648 "`:`
F
�;elc-r
Page: 20 of 29
Charlotte C,;rtification
IDs
12
SG
9yU1U
FL NELAP
E87627

Pace Analytical Services, Inc. Pace AnaJD i'Jcal Services, Inc.
9800 Kincey Avenue, Suite 100 ??5 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
l0 Phone: [phone] F'Jic: ne: 828.254.7176
ace Aral �`ieaFax: 704.875.9091 1 ax. 828.252.4618
www.pacelabs.cnm QUALITY CONTROL DATA
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168748 Analysis Method: EPA 160.4
QC Batch Method: EPA 160.4 Analysis Description: Total Volatile Solids
Associated Lab Samples: 927460360
SAMPLE DUPLICATE: 927486597
927460360 DUP
Parameter Units Result Result RPD Footnotes
Total Volatile Solids mg/kg 13800 13500 2
Date: 10/09/06
Asheville Certification IDs REPORT OF LABORAT9RY ARA � . IS
AC Oilrkoig 4aiiw- 37ri2
SC 99030 wi.riou� Me ,,;JVwn consent ur Pace ; .;,aiytical Ser,:ces, Inc.
FL NELAP E87648
ac_
Page: 21 of 29
Charlotte Grrtification IDs
2
99006
FL NELAP' E87627

Pace Analytical Services, Inc. Pace Analy!il:al Services, Inc.
9800 Kincey Avenue, Suite 100 2,:;:'S Riverside Drive
Huntersville, NC 28078 Aeville, NC 28804
Analvh'cal Phone: [phone] Pl;uge: 828.254.7176
Fax: [phone] Fax [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 169341 Analysis Method Standard Methods
QC Batch Method: Standard Methods Analysis Description-:—S.O.U.R.
Associated Lab Samples: 927460360_---
Date: 10/09/06
Asheville Certification IDs REPORT OF, LABORATORY ANALYSIS
NC WaW'w;'+ 40
SC iu v.,r1ttc-nx6n t
FL NELAP E87648
o
Page: 22 of 29
Charlotte l;trtification IDs
.. I
C. 99U, 6
FL NELAP' E87627

Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
op Ana l v&ica l 0 Fax: [phone] Phone: 704.875.909
J
www.pacelabs-com QUALITY CONTROL DATA
Pace Analy!ii:al Services, Inc.
Riverside Drive
s Jeville, NC 28804
Pl, c qe: 828.254.7176
f: ax: 828.252.4618
Lab Project Number: 92/28129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168299 Analysis Method: EPA 353.2 Modified
QC Batch Method: EPA 353.2 Modified Analysis Description: Nitrogen, Nitrate plus Nitrite
Associated Lab Samples: 927460360
METHOD BLANK: 927461533
Associated Lab Samples: 927460360
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrate as N mg/kg ND 10.
Nitrate -Nitrite (as N) mg/kg NO 10.
LABORATORY CONTROL SAMPLE: 927461541
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrate -Nitrite (as N) mg/kg 500.00 461.0 92
MATRIX SPIKE: 927461558
927407981 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes„
Nitrate -Nitrite (as N) mg/kg 0 1354.00 1354 100
SAMPLE DUPLICATE: 927461566
Parameter Units
Nitrate as N mg/kg
Nitrate�Nitrite (as N) mg/kg
Date: 10/09/06
Asheville Certification IN
�',".'1ntP"vatr:- 40
SC 99030
FL NELAP E87648
927408013
DUP
Result
Result RPD Footnotes
ND
ND NC
NO
ND NC
REPORT OF LABORATORY ANIAL,YS1S
�� nccnR
Page: 23 of 29
Charlotte Certification IDs
99006
FL NELA&' E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
:Mnalvtical ® Phone: [phone]
Fax: 704.875.909
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 168473
QC Batch Method: EPA 350.1 Modified
Associated Lab Samples: 927460360
METHOD BLANK: 927471540
Associated Lab Samples: 927460360
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 927471557
Pace Analy!!? ,al Services, Inc.
Riverside Drive
� b tieville, NC 28804
PI; a r7e: 828.254.7176
Fax: [phone]
Lab Project Number: 92/28129
Client Project ID: QUARTERLY SLUDGE
Analysis Method: EPA 350.1 Modified
Analysis Description: Nitrogen, Ammonia
Blank Reporting
Result Limit Footnotes
NO 10.
Spike LCS LCS
Parameter Units Conc. Result Rec Footnotes
Nitrogen, Ammonia mg/kg 100.00 108.4 108
MATRIX SPIKE: 927471565
927463869 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Nitrogen, Ammonia mg/kg 9.362 53.19 85.90 162 1
SAMPLE DUPLICATE: 927471573
Parameter Units
Nitrogen. Ammonia mg/kg
Date: 10/09/06
927463877 DUP
Result Result RPD Footnotes
7.400 7.300 0
Page: 24 of 29
Asheville Certification IDs
REPORT OF LABORATORY ANAMSIS
Charlotte Certification IDs
.
l r[-jt " srE, i II
SC
99030
':�-itho;d the
SC
99006
FL NELAP
E87648
;�°N �cf�?°q�
FL NELAF'
E87627

aceAna/ytical °
www.pacelahs.com
QC Batch: 168738
QC Batch Method: EPA 351.2
Associated Lab Samples: 927460360
METHOD BLANK: 927485862
Associated Lab Samples: 927460360
Pace Analytical Services, Inc.
Pace Analy, fiwl Services, Inc.
9800 Kincey Avenue, Suite 100
2'l,:5 Riverside Drive
Huntersville, NC 28078
,�::,ieville, NC 28804
Phone: [phone]
R, o 7e: 828.254.7176
Fax [phone]
':w- 828.252.4618
QUALITY CONTROL DATA
Lab Project Number: 92:1.28129
Client Project ID: QUARTERLY SLUDGE
Analysis Method: EPA 351.2
Analysis Description: Total Kjeldahl Nitrogen, ::foil
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrogen, Kjeldahl, Total mg/kg NO 10.
LABORATORY CONTROL SAMPLE: 927485870
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Nitrogen, Kjeldahl. Total
mg/kg
200.00
184.5
92
MATRIX SPIKE: 927485896
927460360
Spike
MS MS
Parameter
Units
Result
Conc.
Result % Rec Footnotes
Nitrogen, Kjeldahl, Total
mg/kg
16320
3082.00
16350 1 3
SAMPLE DUPLICATE: 927485888
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Date: 10/09/06
Asheville Certification IDs
1C 1J`Jaste.r, pier 40
SC 99030
FL NELAP E87648
927460360 DUP
Result Result RPD Footnotes
16000 14000 16
REPORT OF LAIR nPATORYNALYSIS
ov.,hou 'file f !! t8n co,.8on' 6t i"uw;\; . Vi. .:; :it• Ir•
�N nr•r,�go
% Pvi n
Page: 25 of 29
Charlotte l.,ertification IN
;11r !^Iasluduote ' 2
6c 99DC;
FL NELAP E87627

Pace Analytical Services, Inc. Pace Analy'''foal Services, Inc.
9800 Kincey Avenue, Suite 100 2; ,:15 Riverside Drive
Huntersville, NC 28078 ; I s,ieville, NC 28804
�Anal,�tieal ® Phone: [phone] Pho7e.� 828.254.7176
Fax: [phone] , qx: 828.252.4618
www.pace►abs.com QUALITY CONTROL DATA
Lab Project Number: 9,:128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168955
QC Batch Method: EPA 375.4 Modified
Associated Lab Samples: 927460360
METHOD BLANK: 927495549
Associated Lab Samples: 927460360
Parameter Units
Sulfate mg/kg
LABORATORY CONTROL SAMPLE: 927495556
Analysis Method: EPA 375.4 Modified
Analysis Description: Sulfate, Total, Soil
Blank Reporting
Result Limit Footnotes
NO 500
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Sulfate mg/kg 2000.00 1962 98
MATRIX SPIKE: 927495572
927460360 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes_.
Sulfate mg/kg 6737 32050 36970 94
SAMPLE DUPLICATE: 927495564
Parameter Units
Sulfate mg/kg
Date: 10/09/06
927460360 DUP
Result Result RPD Footnotes
NO NO NC
Asheville Certification IDs REPORT OF kABORATORY ANALYSIS
NC Wastewater 40 :pis ;a •; ,t ( � ;:
n ` . ! i
�u'ul n;,.,nl V4'-1..{,s i!12
SC 99030 ^;itf Dui life tt �t ei ... iC.
FL NELAP E87648
_"ilen r
Page: 26 of 29
Charlotte :,,irtification IN
S�� UUUU6
FL NELAF E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Analytical o Phone: 704.875.909
� Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Pace Analylfi al Services, Inc.
2:?;:15 Riverside Drive
As,ieville, NC 28804
Pt o 7e: 828.254.7176
FRx: 828.252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
QC Batch: 168956 Analysis Method: EPA 325.2 Modified
QC Batch Method: EPA 325.2 Modified Analysis Description: Chloride(Mercuric Nitrate-;)
Associated Lab Samples: 927460360
METHOD BLANK: 927495580
Associated Lab Samples: 927460360
Blank Reporting
Parameter Units Result Limit Footnotes
Chloride mg/kg 55. 50.
LABORATORY CONTROL SAMPLE: 927495598
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Chloride mg/kg 2000.00 2194 110
MATRIX SPIKE: 927495606
Parameter
Chloride
Date: 10/09/06
Asheville Certification IDs
NG W,),elevro:lter 40
sC 9903D
FL NELAP E87648
927460360 Spike MS MS
Units Result Conc. Result % Rec Footnotes-
mg/kg 4569 32050 65610 190
REPORT AF LABORATORY ANALYSIS
di!lfli:Jt Jl' U'vi":i=:ft lL,, t aGeian -.;.
�ti ncco,
Page: 27 of 29
Charlotte i;_(:rtification IDs
`:NG l(Va.rte"t12
se 99006
FL NELAF' E87627

aceAnalytical °
www.pacelahs.com
QC Batch: 169067
QC Batch Method: EPA 365.2
Associated Lab Samples: 927460360
METHOD BLANK: 927500330
Associated Lab Samples: 927460360
Pace Analytical Services, Inc.
Pace Analy 1ral Services, Inc.
9800 Kincey Avenue, Suite 100
Riverside Drive
Huntersville, NC 28078
k0eville, NC 28804
Phone: [phone]
Ph n, 7e: 828.254.7176
Fax: [phone]
,` 3x: 828.252.4618
QUALITY CONTROL DATA
Lab Project Number: 92:1128129
Client Project ID: QUARTERLY SLUDGE
Analysis Method: EPA 365.2 .
Analysis Description: Phosphorus, Total, Soil
Blank Reporting
Parameter Units Result Limit Footnotes
Phosphorus mg/kg NO 10.0
LABORATORY CONTROL SAMPLE: 927500348
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Phosphorus mg/kg 20.00 19.42 97
MATRIX SPIKE: 927500363
927460360 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes_
Phosphorus mg/kg 5931 271.60 5273 0 1
SAMPLE DUPLICATE: 927500355
Parameter Units
Phosphorus mg/kg
Date: 10/09/06
Asheville Certification IDs
NC'Aa';; ',8.t {' 10
IVr Ilr{Giti G 1 72'.!r.. : ,7
SC 99030
FL NELAP E87648
927460360 DUP
Result Result RPD Footnotes
NO ND NC
REPORT OF LABORATORY ANALYSIS
uwi�,sout•the �°�;;i��i conse��. of «:., ,'.r,z.,,. �:..::rvfce�, i��c.
"�H ACCpRO ..
ne
o '
Page: 28 of 29
Charlotte Certification IN
Si; Syi�o
FL NELAP E87627

aceAnalytical °
www.pacelabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analy,' val Services, Inc.
2 ,:'S Riverside Drive
'e;
Asoeville, NC 28804
PJh o,7e: 828.254.7176
ix: 828.252.4618
Lab Project Number: 92128129
Client Project ID: QUARTERLY SLUDGE
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Reci:nd RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S),--> Surrogate
]� The spike recovery was outside acceptance limits for the MS and /or MSD due to rnatrix interfere -ice. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the daisi is
acceptable.
C[2]) The calculated RPD was outside QC acceptance limits.
�[3.1 The spike recovery was outside acceptance limits for the MS and/or MSD due to an analyte concentration in the
sample at four times greater than the spike concentration. The QC batch was accepted based upo,i LCS and/or
LCSD recoveries within acceptance limits.
Date: 10/09/06 Page: 29 of 29
Asheville Certification IDs REPORT OF LA90RATORY ANALY, S ISCharlotte_ ortification IDs
Nf Wastevvater 4.�I
;jrls 6f0ilC d.+a:'. 3".r' i .( 1�. I�f'•'iti,l '�, til�$'L'9.i/r'Ur,
SC 9903U vvIiii0L :itb u`s 1ten .:onsent c . ac,c ,�Sol riL.�, .. d ct';' (... JC 99006
FL NELAP E87648 FL NELAP E87627
O F

Subcontracted Re(L ult,,..)
2g � 2g
"
EMS I C to 6
R
This report includes
-A
page Ito I -A _.

Analytical Environmental Services, Inc.
Date: 28-Stp-06
CLIENT:
Pace Analytical Services, Inc.
Client Sample ID: 92745036 /�=fSLUD-IGE
Lab Order:
06091370
Tag Number:
Project:
92128129
Collection Date: 9/21/ !006 2:10:00 PM
LabID:
06091370-001A
Matrix: SURFACE WATER
Analyses
Result
Limit Qual Units
BatchID DF
Date Analyi:i;d
CHLORINATED HERBICIDES
SW8151A
(SW3510B)
Analysl; El
2,4,5-T
BRL
2.0
pg/L
75572 1
9/26/2006 12 39:00 At
2,4,5-TP (Silvex)
BRL
2.0
pg/L
75572 1
9/26/2006 12:-19:00 At
2,4-D
BRL
2.0
pg/L
75572 1
9/26/2006 12 ::19:00 At
2,4-DB
BRL
10
pg/L
75572 1
9/26/2006 12.39:00 At
Dalapon
BRL
10
pg/L
75572 1
9/26/2006 12:39:00 At
Dicamba
BRL
2.0
pg/L
75572 1
9/26/2006 12:39:00 At
Dichlorprop
BRL
2.0
pg/L
75572 1
9/26/2006 12:39:00 At
Dinoseb
BRL
5.0
pg/L
75572 1
9/26/2006 1::29:00 At
MCPA
BRL
500
pg/L
75572 1
9/26/2006 121:; !9:00 At
MCPP
BRL
500
pg/L
75572 1
9/26/2006 T'2:29:00 At I
Surr: DCAA
99.2 39.3-151
%REC
75572 1
9/26/2006 12:::9:00 At
Qualifiers: * —Value exceeds Maximum Contaminant Level B Analyte detected in the associated Method Blank
BRL Below Reporting Limit E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analytc detected below quantitation limi s
N Analyte not NELAC certified P NELAC analyte rcrtification pending ..
Rpt Limit Reporting Limit S Spike Recovery outside accepted rccovoi;i gitl of 1

4 w aceAnalytical
f Secbi3yn A
Requiro:c Client Information:
Compa y
Address
Section B
Required Project Information
Report To:
Copy To:
Email To: Purchase Order No.:
Phone Fax Project Name:
Reque:sF-; Due Date/TAT: Project Number:
: „a: Valid Matrix Codes.
..;.-salon ❑ Required Client Information MATRIX CODE
@ /� �p
DRINKING WATER DW
SAMPLE I D WASTE WATER WW
PRODUCT P
SOIL/SOLID SL
One Character per box. OIL OL
W (A-Z, 0-9 / :) AIR E WP
AR
f Samples IDs MUST BE UNIQUE OTHER OT
TISSUE TS
i
AddiU--,s�- Comments:
SEE RE% MDE FOR INSTRUCTIONS
vHwiiv-Dr--%-Ua 1,001T I Anaiyti.cai Request u®cument
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information:
Attention:
Company Name:
Address:
Pace Quote Reference:
Pace Project Manager:
Pace Profile #:
of
8- NPDES ❑ GROUNDWATER ❑ DRINKING WATER
❑ UST ❑ RCRA .. ❑ Other
❑GA OIL IN El MI ❑MN ❑NC
DOH ❑SC ❑WI ❑OTHER
rL
Preservatives
LUM
EL Z
o
a0
O
ULU
U
x
m
COLLECTED
�
O
2<
(L
z>
�
—
COMPOSITE START
COMPOSITE END/GRAB
�4
¢ F
H
r<U
O
d
O°
O
N
L L
DATE
TIME
DATE
TIME
j
=
_
=
z
z
a C
PRINT Name of SAMPLER:
SIGNATURE of SAMPLER:
®�mmmmmri
TIME ACCEPTED BY / AFFILIA
Filtered (YIN)
Requested
Analysis-
c"
o`
e'a Pace Project Number
Lab LD
SAMPLE. CONDITION
z z z
z z z
z z z
U
o KEm
DATE Signed (MM / DD I YY) F z `o . 0 mCo

aceAnalytical'
i
October 10, 2006
Mr. Stephen Gouge
Baxter Healthcare Corporation
PO Box 1390
Hwy 221N Pitts Station Road
Marion, NC 28752
RE: Lab Project Number: 92128129
Client Project ID: Quarterly Sludge
Dear Mr. Gouge,
I am writing in regard to TCLP Leachate analysis by EPA 8260.
Pace, Analytical Semji,es, Inc.
9800 Kincey Avenue, :';mite 100
Huntersville, INIC 28078
Phone: 704 , E3'75.9092
Fax: 704. f3'75.9091
The sample results were reported from an analytical run outside of the recommended holding r:i me
for the analysis. The sample was unable to be run with in holding time due to an extended pmvor
outage at the laboratory. The results were reported with a qualification statement.
If you have any further questions or need additional information, please contact Annette & ott or
myself at 704-875-9092.
Sincerely,
d
Cheryl Johns
Quality Manager

12/11/ labb 1LI: 5'1 bib lbbbb1b
ace Analytical"'
raw.paoel��s.cam
December 05 2006
Mr. Stephen aduge
Baxter Heal?;Iicare Corporotion
P.O. Box-li'10
HWY 221N, P`tt$ Station toad
P19ribn, NC 28752
b: I bUE (;UWE
Pace Analytlra) Servites, W.
-WV A7nl:A�y Avenue, Build W
HU17tgr$v1N9, NC 28078
Phono: 7rW.875.9N2
Fax.' 704.875.9091
HALL U:3
Pace Aaelftdcal 8ervlcaa, Inc.
J!,!5 RlvaraJdrr Oliva
/i"l1evl/18, NC 28804
F111-mn, RPR P. 4 717R
,Jirx 829.252.4618
RE: Lab Project; Number: 92132110
Client: Project ID: WASTHWATER 11,•14
Dear Mr, Gauge:
Enclosed are the analytical results for $amp1Cs) re4elved by the laboratory on NovpmbAr 14, 2W. Rswul•'fi
reported herein conforn to the most current NEW standards, where applicable, unless otherwise narrato:f 'in the
body of the report.
Inarganie Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic tasting
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If You have any gLastions concerning this report please feel free to contact ma.
Sincerely,
p
Anmtte Scott
annette.scott9pacelabe,con
[phone] ext. 233
Project Manager
Entlosures
Ash�dl!e �' rtifi .ailu!i I!)s
NC Wastewater 40
NC prinking UVgter 37712
So 99050
FL NFLAP E87648
REPORT OF UBORATORY ANALYSIS
This report shall not be reproduced, exr,,ep1 In full,
without the Inrriffen constnt of Pace Analytical Saimees, inr„
is �ernaa
: tfiCdQn1U
NC Wastrri mir 12
NC Drinklnf Plater 37706
6C 99006
ell- NELAP E87627

12/11/2006 10:51 8287566618 STEVE GOUGE PAGE 04
PM.Wlnr, Pimp ArAid:p-H 1AJRJ-u1rrx, ?or
9800 ICIncey Avenue, Suite 100 ; !T;?a R1ve►side Orhm
laarntereVtllo, NC JD79 I , hatr/1/e, AIC 29804
5a'cie j{ n , Jytical" Phone: 704.875,60091 1 h :-ax 828,25�i.i 1 i 8
J"11 f yyFax: 70�.8%,5091 I�ex.• 82$.252,46i8
IXi�W.I1'1rGCI3{µvb'UTAA ,
Lab Pro,iect Number: 9a7W110
Client Pro3ect 10: WASTEWATER 11-14
Lab Sample No, 7687624 Project Sample Number: 92132110-003 Date Collect.o!:: 11/14106 14:10
Client Sample 1e: GW SLUDGE Matrix: Water Date Receive::: 11/14/06 17:00
PICagIters Results Wts Report Limit Analxaed By CAS No, ��;,•,. Realmt
Wot Charmctrj .
Flash Point, Closed. -Cup Method: EPA 1010
Flash Paint ;-200F 11/28/06 16:00 ,]MW
PH method: EPA 150.1
PH 5.05 Lrits 1.1/16108 21:20 N1W
N West cart l�at 40 REPORT of LABORATORY ANALYSIS
NO �fastewatsr 40
NO Drink►ng avatar 37712 This raport ahell not be reproduced, exuept In full,
so. 99030 withoi t the written consent of Pace AnalytVA Services, Inc.
R NELAP l;87548
mama: 3 of 11
0At•lotV,!, 1'>CN.[natla.4JJRA
NC Was14TI.ter
1:
NC Drinblill; Water
3770B
SC
00D06
FL NELAP
E87627

10: 51
8287566618
C ,!" naa lytica "
www.gaeela&.0i"
STEVE GOUGE
Pats Ana4weel Swint, lite.
9900 Ifrncey Avenue, Suite 100
Hanteflie, NIG 28078
Phone: [phone]
rim., 1704ZIU091
PAGE 05
Paee Ania-I it8eal St+ralces, Ine.
;'u6 Riverside Drive
I.09ville, iuL' ZW4
i h7ner 828.854.7176
FdA. 8498,252,419'18
Lab Project Nueber: i)2132110
Client Project ID: WAST'MTER ll•14
PARAMETER EOOTNOT f
m-chod yuws xwi-riea to use ASr.
All pN, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted oat€ide or EPA recornirnded immediate
hold tim.
Dcpbndina on the moisture cortent the PRLS can be elevated for all soil aamplcpa reported on a iiry weight basis,
2-Chloroethyl vinyl ether has bean shown to degrade in the presence of acid.
W Not detected at or above adjusted reporting limit
NC Not Calculable
J F&HMAtPd rnncentration above the adjuctod method detection lialt and below LJII:!. ad,iaai:ed repor':InQ limit
MDL Adjusted Method Detection fJmit
on-01 1.9/e6i06
Nam 4 or ii
MCWast Ce iFi�ratin� I REPORT' OF LABORATORY ANALysis
NC Wastewater 4b �h�rl9tts.,(;c�I�fFiGAtiA.p�
NC Drinking Water 37712 This report shall not be reproduced, except in full, NO Westenaaw 12
5C g1,11130 withal thi Wrlttan consent of Paos Anaytloal ,uervleas, Inr;. NIC DrinR;i,ill Water 3770fi
FL NIEI.AP IEF7648 ,� 8C ggpp�
qA, FL NELAr
E87627

12/11/2006 10:51
8287566518 5TEVE GOUGE
Palm .drl wy(fetl rgffT6-.PT' lite
Analytical`
www.Pavelabs.Dom
QC Satch 17321E
DD 6aLuh HaUjud IPA 116.1.
A990d ated Lab !;aeples:. 927687624
a" Kinsey Avenue. Sur7e 100
Nuntersville, NO 28478
Phone. [phone]
Fax [phone]
WALITY CONTROL DATA
HA4at ab
Pecos Arw�410l Rarl4m foe
25 Riverside. drive
-I!.:hevllle, AC 28804
F v one; 628,254,7176
I nh PrnJPrF Nranhwr! U137110
Client Project ID: WASTEWATER 11.14
Analysis Nethod, EPA 150.1
Analyala Daaurlptluri: pH
SAMPLE DUPLICATE: '927693531 ~
927685834 DUP
ParRWAP• Units aocult-Rocult "D Robtnoteo
pH units 5.800 5.800 0
onto: 12io5106
I
Alley11 Lmat1was
NC Waa!towater 40
NC DrinIdng Water 31712
SC 9f1030
FL NELAP E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be roprodUmd, except in full,
without the written consent of pace Analytical Servioes, Inc.
Arr,
rt��E
POga: 6 OF 11
rx' hRCIO#EL!d I;t;i#•1c��t1..IDr
NO Waslowater 12
NC DrION'i Water $7706
5C 99006
FL NlELAi, C07027

qC Batch: 173969 AnalySla MRZDOp: h?A iuiu
QC Batch Method: EPA 1010 Analysis Docoription: FlaEh Point, Closed Cap
Associated Lab Samples: 927687624
Pate: 12fooloe
I'M 7 of t7
NO Wastewaterste Ashsvr .tu)caribn il�
Wastewater qcI
REPORT OF LABORATORY ANALYSIS
��ss A"llir�utim a
NC Drinking I loror
3171$
Thi¢ report oholl not he rapoQuurd, umepr, In fun,
RIC motastnlar
42
5C
V.,D30
without th9 wrrlttan consent of Parx AnaMlml Services, Inc,
NO Drinkl,i>> Water
37706
FL ELAP
EF7C+46
�n ��cn
g�^�,„••-"°;.:"°,m�
FL NFLAIF
E827

1'1/11/lbwb 1N:bl U�-'Jlbbbblb 4Muukmt mo``ub contractsRelult,,-;,-,!1l)
�j
Pace'Project #
g2132�IC
QCE A C.TIV 1Ty
This report includes
page Ito 2A _0

1 71' 1 1 .'?AAA 1 h m1 A?A'PmIAA 11 A
g FFEwfo AN 11W rritir 1 rV
� ZAna►yrIcal-
Mr. AnrAW S0011
Reap Almiytiosd 6erviom, Inc
CheriWe Laboratory
0800 IGn=y Avenue, Suite 100
WI immo ULm. Nr! 7Rn7R
Client Me: Chance L.abaratory .
CieM SO- 92132110/sext"
Ganaiml Chemilalry
Pin A III W&frr �lcrra Inc
M Td..yp1. I .r.
&part PA 1502
+i enej 7d4.7-2A118f
run. rwfwar.rrou
Lab Pro)"t to:
00.7273
Lab S m,pl.ID,
0911.2966
Cilent Sampla 1b,
027687824/Grob ek.fid ge
Sample Matrix:
did
Date Sampled:
1111412008
Date Reaelved:
11/1412006
Test Method Raadt Reporting Unft Anahrne '���� Nothotl la1 slnk lt LUnik DaA ewnR1V rlrau
Q�nide (Reactluoj 7.3.32=140) -0.0 i 1.01 mgAtg DAM 11/20/20 M COWM9.1 rb 4
16:. mgAtg DAM 11=1201Y 0055070.1 .10 �IRW iRYet.�lvm) gp3pt )
(t) US. fiMrDrfntmtdi Protacticn Aea+tay, ION. Test Meutods for Evatuating Soli! Waste, SW.84E. 3rd ed., bfte of S504 WaW m a nd
Fnlongoncy Raspa�, WenhingMn, t)C.
t+`�reuhll■ [`-�rrwr►ehtoe �iv+,u11■ reported on �r1 ae rooaivad isgai�.
REPOW OF UMRATORY ANALYSIS
Thir mw shall not b¢ mmduemd, mapt in full,
Wfl110ut the Wrfttpn Mmv nt ei Pace Malylknl aal.tu m, Inc.

12111/2006 10: 51 8287566618 b I LVL Cauulzli rmkzlt UJ
Analytical
ww.pacub"'C"
November 2?, 2006
Ms. Annette Scott
lsaaa maly caal sorvicaes, Inc
Charlotte. Laboratory
9900 Kincey Avenue, Suite 100
Huntersville, NC 28078
Dear A1.9. 9md-
Pace Ana' I; 41cal Sa mkos, W.
B203 r/laVe Lane
EXPnrr, N TDO:fL
J' ba7Re; 7R4.7M.1161
Fax [phone]
Enclosed WO anaelyUed results for samples submitted to Pace Analytical by Pace Ana4lica l! Servers, III III, The
661 uplub wdi a avwhmd an November 14, "U. I he resuft reported in this project most the requireme"io as
s Wfkid in GhAlttpr A 4 the NELAC 9tand2rda. Any doWatisms ar a lismpar4j b3 frsii 1 tl sn NELAC standards
are dowmented in the case narradve(s) Af jhif rgpM paraarrAfArA pdnfW In itediC9 ropmaint bbn-Mle`tj.I:
accredited parameters. News re%ronce Paw project number 06.7273 when lnquiAriti about this rep(wi..
Citant ,Situ: Charlotte Laboratory
Gliertt I7asf.. 921321101Baxter
once Sample CWrdSTrnpla
1�4n�on Irdaralrlpgen '
0011- '.�oa 927ra a
Generrl Commants: C ;oiar temperMuro 4 ° G upon receipt, lCe was present.
Please call me if you have any.quertionas regarding the lnfarma kn contained within ttils report.
Sincerely,
tiachel b. ChNstnar
Project Mamger
RDC: JId -
Enclosures
Page 1 of r�
i
REPORT OF LABORATORY ANALYSIS
7tYC rnnnrt than n..l f.. "WM". 4' .—VIA Fit Iwn.
Whhnirtlhv wra4i.n +r.n�rnti =I Ruy: sarrriynnal WWWOUM Ift,
ram' AgC� I IJ,tZ

NoAna"cal
11Uction
A
-pl"Mutrafulnumm -.
CHAIN -OF -CUSTODY I Anaiyticd Request Docume.,rAl
The Maiwaf-Axly is alLEGAL DOCUMENTAll refoyanifelt simust he completed Atc-Cmufty-
. �11
Section B: Seeffon C Page
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-DATE a*,] ¢.,w

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INC.
r237 • [phone]
al-labs-eastern.com
REPORT OF ANALYSIS
copy: ZACH KEY
DATE SAMPLED: 3/8/2006 1530
DATE RECEIVED: 3/10/2006 1045
DATE REPORTED: 3/16/2006 PAGE
Soi s, Total (As is)
2.04
20400
0.01
RD
03/10/06
16:00
SM 254OG
ivit: oo en, Total Kjerdahi
11.03
110300
0.01
JCM
03/13/06
16:00
EPA 351.3
Phi;� horus
2.13
21300
0.01
JM
03/13/06
16:00
SW 846-601OB
PQt -o4�. ium
0.54
5400
0.01
DH
03/13/06
16:00
SW 846-601 OB -
Slti .,,
1.51
15100
0.01
JM
03/13/06
16:00
SW 846-601OB
1.92
19200
0.01
JM
03/13/06
16:00
SW 846-601OB
Mz:
0.42
4200
0.01
JM
03/13/06
16:00
SW 846-601OB
So%.; urn
1.09
10900
0.01
JM
03/13/06
16:00
SW 846-601OB
Iro,-:
14900
1
DH
03/13/06
16:00
SW 846-601OB
Ali;{ '!inum
2770
10
JM
03/13/06
16:00
SW 846-6010B
Mano.Gnese
237
1
JM
03/13/06
16:00
SW 846-601OB
Co,.�per
259
1
DH
03/13/06
15:00
SW 846-601 OB
Zing;
290
1
JM
03/13/06
16:00
SW846-601OB
Ammonia (as N)
0.78
7800
0.01
JM
03/13/06
14:00
EPA 350.2
Nit rwn, NO3+NO2
BDL*
1
KS
03/13/06
15:00
SM 4500-NO3F
3
1
DH
03/13/06
16:00
SW 846-601OB
Chi, s-Eium
110
5
DH
03/13/06
16:00
SW 846-6010B
Nic .:.;
39
5
JM
03/13/06
16:00
SW 846-601 OB
values are on a dry weight basis except as noted.
Our: `. ` and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made
to the ` the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
q� et
AUL C. H. CHU

Le-3d \ /
Me-r Ary
SE?eelli:am
Nitrogen, Organic
Molvibdenum
10.25
REPORT OF ANALYSIS
27
1.0
1.4
0.6
102500
10
5
0.2
0.2
0.1
0.01
5
JM
KM
KM
KM
DCH
JM
)1
copy: ZACH KEY
DATE SAMPLED: 3/8/2006 1530
DATE RECEIVED: 3/10/2006 1045
DATE REPORTED: 3/16/2006 PAGE: 2
03/13/06
16:00
03/15/06
15:00
03/15/06
15:00
03/15/06
15:00
03/16/06
16:00
03/13/06
16:00
,values are on a dry weight basis except as noted.
Our r ; and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made
to thf:. the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
SW 846-6010B
SW 846-7061 A
SW 846-7471A
SW 846-7741A
EPA-350.2/351.3 (Calc.)
SW 846-6010B
q-,
A� C�UL C. H. CHU

BIOSOLIDS SAMPLE TRANSMITTAL FORM/CHAIN OF CUSTODY
A&L Eastern Agricultural Laboratories, Inc.
7621 Whitepine Road Richmond VA 23237 Tel: [phone] Fax: [phone] Email: office a al-labs-eastem.com
Customer Information
Submitted By Charge To Copy Tc
c n 1 ` 5 �R
513ik,",, 5�;1 IJY Ic�trs iv+r, u tr„
Lab Number Colection Information
Sarr T.ID (Lab Use
Only) Type Data Tine
Grab
composite
_Grab
Composite
_ Grab
— Composite
Grab
— Composite
Date Time
i�:31f�
Sample Information
Container Information
Number
Type
Vdlume
SLf
of Bottles
oz
_ Glass
pint
Plastic
qt
Glass
— oz
pint
— Plastic
t
Glass
— oz
—
pint
— Plastic
t
Glass
oz
—pint
Plastic
_,
Test Package Details —
SL1? Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: >"<.sic Test SL1 plus Sulfur, Calcium, Magnesium,Sodium, iron, Aluminum, Manganese, Copper And Zinc
503 Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc Included In SL2)
Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
CC& . ;'aicium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
I :;Ac7co�unt #
I
Special Instructions or Remarks

aceAnalyficai
www.pacoiah.,;.com
September 06, 2006
Mr. Stephen Gouge
Baxter Healthcare Corporation
P.O. Box 1390
Hwy 221N, Pitts Station Road
Marion, NC 28752
RE: Lab Project Number
Client Project ID:
Dear Mr. Gouge:
92125972-----------',
ASTEWATER /
Pace Analyiicai Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace AnvirVcal Services, Inc.
25 Riverside Drive
,' ';heville, NC 28804
f ' one: 828.254.7176
=ax: 828.252.4618
Enclosed are the analytical results for samples) received by the laboratory on August: 23, 2006. Resi.II:s
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrai::d in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organ•:: testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Annette Scott
[e-mail]
[phone] ext. 233
Project Manager
Enclosures
Asheville_Ceiilificaflon 10s
NC Wasfew*er 40
REPORT OF LABORATORY ANALYSIS
This r,' , ,..:I;all excr . in ft!l!
r
Charlol::;:.i:ertification_IDs
NC W�,!J[:Avale r 12
4% Dii bli:_ 1;L'a'Ce
w
FL NEI.. P L-6/621
FL NELAP E87648

.. � i .. ..

aceAnaVical°
www.pacelahs.com
Lab Sample No: 927342493
Client Sample ID: GRAB FR. SLUDGE
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax. [phone]
Pace Anal p ti cal Services, Inc.
19,?5 Riverside Drive
,+Isheville, NC 28804
P.i it: ne: 828.254.7176
! -ax 828.252.4618
Lab Project Number: 92125972
Client Project ID: WASTEWATER
Project Sample Number: 92125972-002 Date Collect,:,:l: 08/23/06 10:43
Matrix: Water Date Receiv 1: 08/23/06 13:03
Parameters Results Units Report Limit Analyzed By ..,CAS No. ual RegLmt
Wet Chemistry
Total Volatile Solids Method: EPA 160.4
Total Volatile Solids 6900 mg/1 5.00 08/29/06 19:50 SAJ
Date: 09/06/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC V-.!: stewafer 4Q
SC 9907 0
FL NELAP E87648
n
"nel c-_
Page: 2 of 7
Charlotte certification IN
NC UVasl :water 12
FL NELA:1 E87627

r•
;acieAna1ytjca1R
www.pacelabs.com
Lab Sample No: 927342501
Client Sample ID: GRAB #1 DIGESTER
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analy, Fi;al Services, Inc.
Riverside Drive
it s,ieville, NC 28804
PI: n ne: 828.254.7176
Fax [phone]
Lab Project Number: 92125972
Client Project ID: WA..`:>TEWATER
Project Sample Number: 92125972-003 Date Collecte:l' 08/23/06 10:50
Matrix: Water Date Receive:) 08/23/06 13:03
Parameters Results Units Report Limit Analyzed By _ - ,CAS No. Qua'!,._ RegLmt
Wet Chemistry
Total Volatile Solids Method: EPA 160.4
Total Volatile Solids 22400 mg/l 5.00 08/29/06 19:50 SAJ
Date: 09/06/06
Asheville certification IDs REPORT OF LABORATORY ANALYSIS
r'.:s
i•,:r� �'C�1�`ii?C .`., _.. ���',_ ; L. � S(iuii !;Sii``. :(i `F'C'F" ;}� ;I�I,
se us0 without the written cons;;,rk of Pace Aiin:y iCdi iiCivlces, Illc.
FL NELAP E87648
" ac
Page: 3 of 7
Charloll:..Certification IDs
ill':' i1113'f5V'ic1iF.?C
SC 99006
FL NEUF E87627

. NCDA&CS Agronomic Division . Phone: (91:9)733-2655 , Web"S- www.ncagr com/agroriomi/
Report No
06496
Grower:
Southern Soil Builders, Inc.
Copies To:
�-
958 Hoots Rd
Roaring River, NC 28669
oil Test Report
..., '
Farm:
10/3/2006 SERVING N.C. RESIDENTS FOR OVER 60 YEARS
Catawba County
Agronomist Comments
C
= 2,
Field Information
Applied Lime
. Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year Lime
P205 K2
Mg S
Cu
Zn B
Mn
See Nc <e
Tl
1st Crop: Fes/OG/Tim,M 1T
120-200 I10-130 30-50
0 0
0
0 .0
0
12
lid Crop:
0
Test Results
Soil Class HM% W/V
CEC BS% Ac pH P-I K-I Ca% Mg%
Mn-I Mn-AI(1)Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-I
SS -I
NO3-N N-.' ..l'
Na
MIN 0.81 1.03
7.3 73.0. 2.0 5.4 9 50 50.0 19.0
55 50 60
60
31
44
0.1
Field, Information
AppliedLame
Recotiunendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year Lime
P205 K2
Mg S
Cu
Zn- B
Mn
See No. R
T2
1st Crop: Fes/OG/rim,M LIT
120-200 60-80 20-40
0 0
0
0 .0
0
12
2nd Crop:
0
Test Results
J
v
Soil Class IIM% W/V
CEC BS% -Ac pH P-I K-I Ca% Mg%
Mn-I Mn-AI(1)Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-I
SS -I
NO3-N [Nip'.-'"
Na
MIN 0.56 1.07
6.3 65.0 2.2 5.4 29 60 43.0 17.0
383 247 62
62
88
57
0.1
Field- Information
"Applied Lime -,-Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year Lime
P205 K2
Mg S
Cu
Zn B
Mn
See Ncs �~
Si
1st Crop: Fes/OG/Tim,M 0
120-200 0-20 0-20
0 0
0
0 .0
pH$
12
2nd Crop:
0
Test Results
Soil Class HM% W/V
CEC BS% Ac pH P-I K-I Ca% Mg%
Mn-I Mn-AI(1)Mn-AI(2) Zn-1
Zn-AI
Cu-I
S-I
SS -I
NO3-N Na <
Na
MIN 0.46 1.04
10.2 92.0 0.8 6.6 61 72 56.0 32.0
167 108 91
91
130
63
0.1
Field Information_
Applied Lime
`" Recommineiidations:
_
Sample No. Last Crop
Mo Yr T/A
Crop or Year Lime
iv P205 K2
Mg S
Cu
Zn B
Mn
See Noa',_
S2
1st Crop: Fes/OG/Pim,M 1.2T
120-200 100-120 50-70
0 0
0
0 .0
0
12
2nd Crop:
0
Test Results
-
Soil Class HM% W/V
CEC BS% Ac pH P-I KI Ca% Mg%
Mn-I Mn-AI(1)Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-I
SS -I
NO3-N NII1-!7
Na
MIN 0.46 1.13
4.5 49.0 2.3 5.3 13 41 31.0 12.0
80 65 34
34
27
57
0.1