NC0005177_Regional Office Historical File Pre 2018 (5)

.3 S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 C n� PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R C l.a F RIE D COUNTY:Gaston RECEIVEDMCDENR/DWR
OWNER NAME:Fmc Lithium USA Corporation ORC:RodneyStoughWilli 2 019 ORC CERT NUMBER:28624 OCT2 r 19
�° ACT 01 - 7 �����
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION: 1.0 CE N i'WL FILES STATUS:Processed.. WOROS
DWR SECTION IOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
• 50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3a
41
A ) I •
a ;
® A Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
-°. 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a 6$ a
CS u F OA FLOW pH HOD-Caw T88-Cone DO TOTAL N- TOTAL P-Can CHLORIDE CRR7DCHV
2400 clack He. 2400 deck Hn VBIN mgd su mg/I mg/1 mg/I mg/I mg/I mg/I percent
I 0730 9.5 Y 0.389
2 0730 9.5 Y 0.389
3 0.389
4 0.387
5 0730 9.5 Y 0.387
6 0730 9 Y 0.386
7 0730 8.5 Y 0.386 8 <2 <2.5 8.6
a 0730 9.5 Y 0.386
9 0600 10 B 0.384
IO 0.383
II 0.382
12 0730 8.5 Y 0.38
13 0730 9.0 Y 0.379
14 0730 8.5 Y 0.377 8 8.2
15 0730 9 Y 0.374
16 0600 10 B 0.37
17 0.369
18 0.367
19 0730 9 Y 0.364
20 0730 9.5 Y 0.364
21 0730 9.5 Y 0.364 7.8 2.7 7.4
22 0730 9.5 Y 0.364
23 0730 9.5 Y 0.364
24 0.366
23 0.366
26 0730 9.5 Y 0.366
27 0730 9.5 Y 0.366
20 0730 10 Y 0.366 7.8 7
29 0730 5 Y 0.366
30 0645 7.5 Y 0.366
31 0.366
Monthly Average Limit 0.615 30 30
Headily Average: 0.374581 0 1.35 7.8
Dolly Maim: 0.389 8 0 2.7 8.6
Daily Omimom: 0.364 7.8 0 0 7
6965 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094
A I j A :
8
I
< Fi 18I Grab
1 O CENUCTYY
2400 dads Hn 2400 dock Hn Y/11/91 umhos/Cm
I 0730 9.5 Y
2 0730 9.5 Y
3
4
5 0730 9.5 Y
6 0730 9 Y
7 0730 8.5 Y 1022
8 0730 9.5 Y
9 0600 10 B
10
II
12 0730 8.5 Y
13 0730 9.0 Y
14 0730 8.5 Y
15 0730 9 Y
16 0600 10 B
17
IS
19 0730 9 Y
28 0730 9.5 Y
21 0730 9.5 Y
22 r 0730 9.5 Y
23 0730 9.5 Y
24
25
26 0730 9.5 Y
27 0730 9.5 Y
28 0730 10 Y
29 0730 5 Y
30 0645 7.5 Y
31
Ma.Mb Avenge Limit
Maet 17 Aveeage: 1022
Daily Masim®. 1022
Da""": 1022
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
• 50050 00400 C0310 C05J0 00300 C0600 CO665 N040 NM
II,� i 1 Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u 8 d k Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
1. 1 S U 1 1- Ze FLOW PH BOD-Cs.e TES-Cow DO TOTAL N- TOTAL P-Caw CHLORIDE CNDUCIYY
2400 deck Hn 2400 dock Hn Y/B/N mgd su mg/I mg/I mg/I mg/1 mg/1 mg/1 umhos/cm
I 0730 9.5 Y
2 0730 9.5 Y
3
4
5 0730 9.5 Y
4 0730 9 Y
7 0730 8.5 Y
a 0730 9.5 Y
9 0600 10 B
I.
it -
12 0730 8.5 Y
13 0730 9 Y
14 0730 8.5 Y
15 0730 9 Y
14 0600 10 B
17
10
I, 0730 9 Y
20 0730 9.5 Y
21 0730 9.5 Y
22 0730 9.5 Y
23 0730 9.5 V
24
25
24 0730 9.5 Y
27 0730 9.5 Y
20 0730 10 Y .
20 0730 5 Y
30 0645 7.5 Y
31
k
Monthly Average L1mit:
Money Average:
Day MAXIMUM:
Daa3 M4I
sees No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
.8 I A
L
3 u d o&
u $ o z
2400 dock Hn 2400 code Hn Yl11/N
1 0730 9.5 Y
2 0730 9.5 Y
3
4
5 0730 9.5 Y
6 0730 9 Y
7 0730 8.5 Y
s 0730 9.5 Y
9 0600 10 B
10
u
13 0730 8.5 Y
13 0730 9 Y
14 0730 8.5 Y
15 0730 9 Y
16 0600 10 B
17
I0
19 0730 9 Y
20 0730 9.5 Y
21 0730 9.5 Y
22 0730 9.5 Y
23 0730 9.5 Y
24
25
26 0730 9.5 Y
27 0730 9.5 Y
20 0730 10 Y
29 0730 5 Y
30 0645 7.5 Y
31
Moodily Avenge L1.611:
Moodily Avenge:
D. M..mum:
Daily Minimum:
9"e No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50050 81400 C0530 0009/ 40556
i
I IId •
g ,� i I Monthly Monthly Monthly Monthly Quarterly
e
u i t
s 8 Instantaneous Grab Grab Grab Grab
eI Cu
$ d $ 5 p A FLOW pH 788-Cow CNDUCTVY OIL-GRSE
2400 dock Hn 2400 dock Hn Y/a/N mgd su mg/I umhos/cm mg/I
I 0730 9.5 Y
2 0730 9.5 Y
3
4
5 0730 9.5 Y
6 0730 9 Y
7 0730 8.5 Y 0.079 7.7 <2.7 852
8 0730 9.5 Y
9 0600 10 B
11
II
12 0730 8.5 V
13 0730 9 V
14 0730 8.5 Y
Is 0730 9 Y
16 0600 10 B
17
18
19 0730 9 Y
20 0730 9.5 Y
21 0730 9.5 Y
22 0730 9.5 V
23 0730 9.5 V
24
25
26 0730 9.5 V
27 0730 9.5 Y
28 0730 10 Y
29 0730 5 V
30 0645 7.5 Y
31
?deathly Average LINN:
Monthly Average: 0.079 0 852
Daly Ma'`®' 0.079 7.7 0 852
Daly MMI ar' 0.079 7.7 0 852
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:09/23/2019
V l3tl.t ja.1
09/23/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
C09/23/2019
Permittee/SubmitteerSignture:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lithium,PAce Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2019(August 2019) VERSION:1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Aug.Week#1,Weekly sampling of DO and pH were completed on July 31,2019

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R r C FRIED COUNTY:Gaston RECEIVEDMCDENRIDWR
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis 0 C 0 1 2019 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No 1 i
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 l ti 1�r�L FILES STATUS:Processed WORDS
DWR SECTION MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
50050 004N C0310 C0530 00300 C0600 C0665 00940 40094
p 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
! S 8Recorder Grab Grab Grab Grab Grab Grab Grab Grab
U
1 at I PLOW PH HOD-Case TSS-Caw DO TOTAL N. TOTAL P-Case CHLORIDE CNDUCIVY
2400 dock He. 2400 dunk Hee Y/B/N mgd su mg/1 mg/I mg/I mg/I mg/I mg/I umhos/cm
I 0730 9.5 Y NOFLOW
2 0730 9.5 Y NOFLOW
3 0730 9 Y NOFLOW
4 N HOLIDAY
5 0600 10 B NOFLOW
4 N NOFLOW
7 N NOFLOW
8 0730 11.5 Y 0.159 8.1 6.3
0 0730 10.5 Y 0.409
IS 0730 9.5 Y 0.407 7.94 <2 <2.5 7.2 <0.52 <0.05 15.8 1019
II 0730 10 Y 0.407
12 0600 10 B 0.409
13 N 0.41
14 N 0.412
IS 0540 II B 0.415
16 0745 4 Y 0.416
17 0545 10 B 0.407 8 8.2
I0 0545 10 B 0.403
19 0545 10 B 0.402
20 0.402
21 0.402
22 0540 II B 0.399
23 1000 7 Y 0.397
24 0730 10 Y 0.397 7.9 <2.5 7.6
25 0730 9.5 Y 0.397
26 0730 8.5 Y 0.397
27 0.396
20 0.395
29 0730 10 Y 0.392
30 0730 9.5 Y 0.389
31 0730 9.5 Y 0.389 8.1 6.5
Moldy Avenge Unit a61s 30 30
Heathy Averse: 0.392 0 0 7.16 0 0 15.8 1019
Daly Madman:
0.416 8.1 0 0 8.2 0 0 15.8 1019
Dilly assee 0.159 7.9 0 0 6.3 0 0 15.8 1019
eaee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
TGP3B THP3B
I.
'� j ?! Quarterly
e t-
4 1 8 a 5 z��
L Grab Calculated
1 8 a S Ij CERI7DPF CLR7DCHV
2400 dock Hee 2400 deck Hn Y/9:N pass/fail percent
1 0730 9.5 Y NOFLOW
2 0730 9.5 Y NOFLOW
3 0730 9 Y NOFLOW
4 N HOLIDAY
5 0600 10 B NOFLOW
6 N NOFLOW
7 N NOFLOW
0 0730 11.5 Y •
9 0730 10.5 Y
le 0730 9.5 Y
II 0730 10 Y >100
12 0600 10 B
13 N
14 N
15 0540 11 B
16 0745 4 Y
17 0545 10 B
IS 0545 10 B
If 0545 10 B
2e
21
22 0540 II B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27
20
2 0730 10 Y
3e 0730 9.5 Y
31 0730 9.5 Y
Me.Mly Avenge L1•11:
Meanly Avenge:
100
Daily%Wm= 100
Deny Minimum 100
44 4e No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
50009 Moss C031s C0530 11306 COMM C0665 as340 61134
A l a
I I 7 d
€ Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u 3` = d Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
a I it 1 ' 000ZZ�
S Ua F O Z FLOW pH DOD-Come Tas-One DO TOTAL N. TOTAL P-Caae CHLORIDE CNDUCTVY
2400 dock Hn 2400 dad. Hn YBrN 8Pd su mg/I mg/I mg/I mg/1 my/I mg/I umhos/cm
I 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y 4320 7.1 <2 10.4 7.4 <0.52 <0.05 32.9 693
4 HOLIDAY
5 0600 10 B
4 N
7 N
a 0730 11.5 Y
3 0730 10.5 Y
as 0730 9.5 Y
11 0730 10 Y
12 0600 10 B
13 N
14 N
15 0540 II B
16 0745 4 Y
17 0545 10 B
18 0545 10 B
13 0545 10 B
20 N
21 N
22 0540 11 B
23 1000 7 Y .
24 0730 10 Y
25 0730 9.5 Y
24 0730 8.5 Y
27 N
28 N
29 0730 10 Y
3s 0730 9.5 Y
31 0730 9.5 Y
Meatrlp Average Limit
Mea161y Average: 4320 0 10.4 7.4 0 0 32.9 693
Daly Mau . 4320 7.1 0 10.4 7.4 0 0 32.9 693
DAV Mi"I""' 4320 7.1 0 10.4 7.4 0 0 32.9 693
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
a
A 1 A
as 1 € A i €
u° E 8
S CI o z
2400 cock Hn 2400 dock Hn WHIN
1 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y
4 HOLIDAY
5 0600 10 B
4 N
7 N
8 0730 11.5 Y
9 0730 10.5 Y
10 0730 9.5 Y
11 0730 10 Y
12 0600 10 B
13 N
14 N
15 0540 11 B
16 0745 4 Y
17 0545 10 B
18 0545 10 B
19 0545 10 B
20 N
21 N
22 0540 II B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27 N
20 N
29 0730 10 Y
38 0730 9.5 Y
31 0730 9.5 Y
Monthly Avenge Limit:
Monthly Avenge:
Dolly Mulmnm:
Doily Ml annnm:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
5M30 101N C0530 OWN as556
I i 7 a
Monthly Monthly Monthly Monthly Quarterly
u 8` I8 I. Instantaneous Grab Grab Grab Grab
8 Fi1 1
z now pH rss-Caw cNDUCIYY off case
2400 dock Hn 2400 dock Hn 'MAN mgd su mg/1 umhos/cm mg/I
I 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y 0.135 7.2 <2.6 814 <4.8
4 N HOLIDAY
5 0600 10 B
6 N
7 N
8 0730 11.5 Y
9 0730 10.5 Y
I0 0730 9.5 Y
II 0730 10 Y
12 0600 10 B
13 N
14 N
15 0540 11 B
16 0745 4 Y
17 0545 10 B
IS 0545 10 B
I0 0545 10 B
20 N
21 N
22 0540 lI B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27 N
—
28 N
20 0730 10 Y
30 0730 9.5 Y
31 0730 9.5 Y
M..uy Avenge L It:
Monthly Average: 0.135 0 814 0
Daly M.a . 0.135 7.2 0 814 0
Dray Mehra. 0.135 7.2 0 814 0
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:09/23/2019
wskt09/09/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
L09/23/2019
Permittee/Submitter {gna ure:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Charllot,Pace Asheville
CERTIFIED LAB#:5023,12,40
PERSON(s)COLLECTING SAMPLES:Lance Crayton,Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION:2.0 STATUS:Processed
Outfit!!001-Effluent Comments:
Revised 1st thru 7th as"No Flow"under column,No reporting reason. Originally had flow as 0

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 �1 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 ' \ E'\!/ OUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis REC �AUG 2 3 2019 FILES ORC CERT NUMBER:28624 RECEIVEDRVCDENR/DW
GRADE:PC-2 ORC HAS CHANGED:No
- CENT STATUS:Processed )EP . of
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 DWR SECTION ,,
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARG1VILLE REGIONAL OF
• 50050 00400 C0310 C0530 00300 C0600 C0665 00940 00094
Q li I
.5 F 6 • z
E` s
A 8 C € y Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
E
u' !2 C 6 g Recorder Grab Grab Grab Grab Grab Grab Grab Grab
n e` 3 z z
o V .2. a- g O 2 FLOW pH BOD-Cone TES-Cone DO TOTALN- TOTALP-Cone CHLORIDE CNDUCFVY
2400 clock tin 2400 clock Hn Y/B/N mgd su mg/1 mg/I mg/I mg/I mg/I mg/I umhos/cm
I 0730 9.5 Y 0
2 0730 9.5 Y 0
3 0730 9 Y 0
4 N HOLIDAY
5 0600 10 B 0
6 N 0
7 N 0
0 0730 11.5 Y 0.159 8,1 6.3
9 0730 10.5 Y 0.409
t6 0730 9.5 Y 0.407 7.94 <2 <2.5 7.2 <0.52 <0.05 15.8 1019
II 0730 10 Y 0.407
12 0600 10 B 0.409
13 N 0.41
14 N 0.412
15 0540 II B 0.415
16 0745 4 Y 0.416
17 0545 10 B 0.407 8 8.2
IS 0545 10 B 0.403
19 0545 10 B 0.402
20 0.402
21 0.402
22 0540 II B 0.399
23 1000 7 Y 0.397
24 0730 I O Y 0.397 7.9 <2.5 7.6
25 0730 9.5 Y 0.397
26 0730 8.5 Y 0.397
27 0.396
28 0.395
29 0730 10 Y 0.392
30 0730 9.5 Y 0.389
31 0730 9.5 Y 0 389 8.1 6.5
Monthly Average Limit: 0.615 30 30
Mnnthly Average: 0.3136 0 0 7.16 0 0 15.8 1019
DnIiy Maximum: 0.416 8.1 0 0 8.2 0 0 15.8 1019
Dilly Minimum: 0 7.9 0 0 6.3 0 0 15.8 1019
'99•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
TGP3B THP3B
A ii 8t
A ; Quarterly
I u i dct Grab Calculated
n a8r
a U F O A CERI7DPF CER7DCHY
2400 deck Hes 2400 deck Him Y/BIN pass/fail percent
I 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y
4 N HOLIDAY
5 0600 10 B
4 N
7 N
8 0730 11.5 Y
f 0730 10.5 Y
IS 0730 9.5 Y
II 0730 10 Y >100
12 0600 10 B
13 N
14 N
15 0540 II B
Ia 0745 4 Y
17 0545 10 B ,
10 0545 10 B
N 0545 10 B
20
21
22 0540 II B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
24 0730 8.5 Y
27
20
25 0730 10 Y
30 0730 9.5 Y
31 0730 9.5 Y
Meatky Average Lilt:
Moatky Average:
100
Daily Meimu®: 100
Daily MrW: 100
88 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
5050 00100 C0310 C0530 00360 CONS C0665 55940 00194
i� a ;
gI < 1Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
J 8.2 = a k Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
ia U Ze FLOW pH BOD-Can T5B-Ceaa DO TOTAL N- TOTAL P-Cow CHLORIDE CNDUCTVY
2400 doh Nn 2400 deck Hn Y/B/N 8Pd su mg/I mg/I mg/I mg/I mg/1 mg/I umhos/cm
I 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y 4320 7.1 <2 10.4 7.4 <0.52 <0.05 32.9 693
4 HOLIDAY
5 0600 10 B
6 N
7 N
0 0730 11.5 Y
9 0730 10.5 Y
II 0730 9.5 Y
II 0730 10 Y
12 0600 10 B
13 N
14 N
15 0540 I I B
16 0745 4 Y
17 0545 10 B
I0 0545 10 B
15 0545 10 B
20 N
21 N
22 0540 II B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27 N
20 N
29 0730 10 Y
30 0730 9.5 Y
31 0730 9.5 Y
Mesa ly Avenge Link:
Maelhly A
v
er"'
4320 0 10.4 7.4 0 0 32.9 693
Daily Ma'm°" 4320 7.1 0 10.4 7.4 0 0 32.9 693
DaOY hatln` 4320 7.1 0 10.4 7.4 0 0 32.9 693
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
A B 8 €
I. € l
a 8
a H
A ;1i 1 I o z
2400 clock fin 2400 clock Nth Y/B/N
1 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y
4 HOLIDAY
5 0600 10 B
6 N
7 N
e 0730 11.5 Y
9 0730 10.5 Y
10 0730 9.5 Y
II 0730 10 Y
12 0600 10 B
13 N
14 N
13 0540 II B
16 0745 4 Y
17 0545 10 B
Is 0545 10 B
19 0545 10 B
20 N
21 N
22 0540 II B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27 N
2s N
29 0730 10 Y
30 0730 9.5 Y
31 0730 9.5 Y
Monthly Average Limit:
Monthly Average:
Daily Methane:
Dolly Minimum:
aaa"No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
59050 00400 C0530 00904 00534
Jr
a
F
,ii y� I Monthly Monthly Monthly Monthly Quarterly
Y
Si
{af' u� t a 8 Instantaneous Grab Grab Grab Grab
d u
] f 1 o A FLOW pH 73a-Cam crmucrvY 01LCR8e
2400 deck He. 2400 deck Hn Y/B/N mgd su mg/1 umhos/cm mgil
I 0730 9.5 Y
2 0730 9.5 Y
3 0730 9 Y 0.135 7.2 <2.6 814 <4.8
4 N HOLIDAY
5 0600 10 B
4 N
7 N
a 0730 11.5 Y
a 0730 10.5 Y
10 0730 9.5 Y
11 0730 10 Y
12 0600 10 B
13 N
14 N
15 0540 11 B
14 0745 4 Y
17 0545 10 B
IS 0545 10 B
If 0545 10 B
2e N
21 N
22 0540 11 B
23 1000 7 Y
24 0730 10 Y
25 0730 9.5 Y
26 0730 8.5 Y
27 N
2s N
25 0730 10 Y
3a 0730 9.5 Y
31 0730 9.5 Y
Monthly Average Limit:
Moety Avenge 0.135 0 814 0
Daly Masewto: 0.135 7.2 0 814 0
Dal'Illiehavn' 0.135 7.2 0 814 0
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2019(July 2019) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:08/14/2019
num,. 08/14/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
Z0, . 08/14/2019
Permittee/Submitter ignature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Charllot,Pace Asheville
CERTIFIED LAB#:5023,12,40
PERSON(s)COLLECTING SAMPLES:Lance Crayton,Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

'PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 REC F V O EruNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis , " 4 RC CERT NUMBER:JUL 1 7 2019 2862LCEIVED/NCDE NR/DWR
GRADE:PC-2 ORC HAS CHANGED:No eDMR PERIOD:06-2019(June 2019) VERSION:1.0 CEN'iFu .FILESSTATUS:Processed Jill_ 2 2 2019
DWR SECTION
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DisabiatetatackEcioNAL OFFICE
• 50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
A I A •
•
3 A 1y 8y
c ,g g Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
9 ` p a p
t3 a 8` 8 C$ Recorder Grab Grab Grab Grab Grab Grab Grab Composite
I $$ a m
V F t5 O L FLOW pH BOD-Gm T88-Cam DO TOTAL N- TOTAL P-Cone CHLORIDE CER7DCHV
2400 dock Hn 2400 dock Hn Y/B/N mgd su mg/I mg/ mg/I mg/I mg/I mg/I percent
1 0.412
2 0.413
3 0730 9.5 Y 0.413
4 0730 8 Y 0.412
5 0730 10 Y 0.412 7.8 2.8 <2.5 6.8
6 0730 9.5 Y 0.412
7 0730 9 Y 0.412
8 0600 10 B 0.41
9 0.41
10 0730 9.5 Y 0.41
II 0730 9.5 Y 0.409
12 0730 10 Y 0.407 7.8 7.8
13 0730 9.5 Y 0.407
14 0730 2.5 Y 0.407
IS 0.407
16 0.405
17 0730 9.5 Y 0.405
18 0730 9.5 Y 0.405
19 0730 9.5 Y 0.405 7.9 <2.5 7.2
20 0730 8.5 Y 0.403
21 0730 9 Y 0.403
22 0.403
23 0.402
24 0730 9.5 Y 0.402
25 0730 9.5 Y 0.4
26 0730 9.5 Y 0.4 8 6.9
27 0730 8.5 Y 0.405
28 0600 7 Y 0.172
29 0
3e 0
6.
Monthly Avenge Limit: 0.615 30 30
Monthly Average: 0.3721 2.8 0 7.175
Dolly Moaboum: 0.413 8 2.8 0 7.8
Daily Minimum: 0 7.8 2.8 0 6.8
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2019(June 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094
Y 8
I6 ig Monthly
u 8`C 8 d Grab
a I $ Y u
4 u F O 6 O Ze CNDUCIVY
2400 dock Hn 2400 dock Hn YIWN umhos/cm
2
3 0730 9.5 Y
4 0730 8 Y
5 0730 10 Y 1019
6 0730 9.5 Y
7 0730 9 Y
8 0600 10 B
9
10 0730 9.5 Y
11 0730 9.5 Y
12 0730 10 Y
13 0730 9.5 Y
14 0730 2.5 Y
15
16
I7 0730 9.5 Y
IN 0730 9.5 Y
19 0730 9.5 Y
20 0730 8.5 Y
21 0730 9 Y
22
23
24 0730 9.5 Y
25 0730 9.5 Y
26 0730 9.5 Y
27 0730 8.5 Y
28 0600 7 Y
29
30
MeeMly Avenge Lima:
M*elhly Avenge: 1019
Daily Meohkmm: 1019
Deily Mioheem: 1019
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2019(June 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
50050 00400 C0310 C0530 00300 C0600 C0665 02940 00094
1
< A y ; Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u° a a k Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
3
I F � 1 O 1t FLOW pH 60D•Can TOa-Can DO TOTAL N- TOTAL P-Cane CHLORIDE CNDUCIYY
2400 dock xn 2400 dock xn v/e/N mgd su mg/I mg/I mg/I mg/I mgd mg/I umhos/cm
2
3 0730 9.5 Y
4 0730 8 Y
5 0730 10 Y
6 0730 9.5 Y
7 0730 9 Y
a 0600 10 B
f
1I 0730 9.5 Y
II 0730 9.5 Y
12 0730 10 Y
13 0730 9.5 Y
14 0730 2.5 Y
15
16
17 0730 9.5 Y
IS 0730 9.5 Y
If 0730 9.5 Y
21 0730 8.5 Y
21 0730 9 Y
22
23
24 0730 9.5 Y
25 0730 9.5 Y
26 0730 9.5 Y
—
27 0730 8.5 Y
2* 0600 7 Y
2*
30
Mwd.y Avenge Limit:
Marbly Avenge:
Dolly Macro a=
Dolly Mbdmam:
*a**No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2019(June 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
I : C
Y g � 8y .
.9e 6$ i 9 8
I.
m
b a 3 cgg c Li
6 I
c u' r~ 6 6' o z
2400 clock Mrs 2400 clock Ms WB'N
1
2
3 0730 9.5 Y
4 0730 8 Y
5 0730 10 Y
6 0730 9.5 Y
7 0730 9 Y
s 0600 10 B
9
10 0730 9.5 Y
II 0730 9.5 Y
12 0730 10 Y
13 0730 9.5 Y
14 0730 2.5 Y
15
16
17 0730 9.5 Y
10 0730 9.5 Y
19 0730 9.5 Y
20 0730 8.5 Y
21 0730 9 Y
22
23
24 0730 9.5 Y
73 0730 9.5 Y
26 0730 9.5 Y
27 0730 8.5 Y
28 0600 7 Y
29
30
Monthly Avenge Lhmih
Monthly Avenge:
Dolly Maximum:
Dolly Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2019(June 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50050 00400 C0530 NO94 N556
1 t 1 a ;
Monthly Monthly Monthly Monthly Quarterly
ue a Instantaneous Grab Grab Grab Grab
6
!j
U F I. O 14 FLOW pH 73a-Ce.c CNDUC7W OI4GROE
2400 dock Hr. 2400 dock Hr. Y/a/N mgd su mg/1 umhos/em mg/1
1
2
3 0730 9.5 Y
4 0730 8 Y
3 0730 10 Y 0.135 7.8 <2.6 919
6 0730 9.5 Y
7 0730 9 Y
s 0600 10 B
9
10 0730 9.5 Y
II 0730 9.5 Y
12 0730 10 Y
13 0730 9.5 Y
14 0730 2.5 Y
Is
16
17 0730 9.5 Y
Ia 0730 9.5 Y
19 0730 9.5 Y
2• 0730 8.5 Y
21 0730 9 Y
22
23
24 0730 9.5 Y
23 0730 9.5 Y
26 0730 9.5 Y
27 0730 8.5 Y
2a 0600 7 Y
29
30
M.elky Aver.ae Limit:
M..MIy Average' 0.135 0 919
Dolly M.slmam: 0.135 7.8 0 919
Dollyhm' 0.135 7.8 0 919
aa'a No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2019(June 2019) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:07/08/2019
t07/03/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
e
07/08/2019
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lithium,PAce Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 ��jj PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R P'^•F I VE D COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis JUL 01 2019 ORC CERT NUMBER:2 'gCEIVEDMCDENRIDWR
GRADE:PC-2 ORC HAS CHANGED:No eDMR PERIOD:05-2019(May 2019) VERSION: 1.0 C'EN rci�L FILES STATUS:Processed All. - g 19
DWR SECTION
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCIu-1EGIONAL OFFICE
• 500e 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
I. € r" a •
7 a
6 1 , 1 I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u 8 k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a pub
S u t5gg O Z FLOW PH DOD-Cone TES-Cone DO TOTALN- TOTAL P-Can CHLORIDE CER7DCHV
2400 deck Hn 2400 dad. Hn WI/N mgd su mg/I mgii mg/1 mg/I mg/I mg/1 percent
1 0730 11.5 Y 0.448 7.8 <2 <2.5 8
2 0730 9 Y 0.443
3 0800 8 Y 0.441
4 0.438
5 0.435
6 0730 8.5 Y 0.432
7 0730 8 Y 0.429
8 0730 9 Y 0.419 7.9 7.7
9 0630 11.5 Y 0.423
10 0730 8.5 Y 0.426
11 0.429
12 0.429
13 0730 8.5 Y 0.429
14 0730 9 Y 0.429
15 0700 9 Y 0.429 7.8 9.6 7.8
16 0730 9 Y 0.429
17 0600 10 B 0.429
18 0.429
19 0.428
20 0730 9.5 Y 0.428
21 0730 10 Y 0.428
22 0730 12.5 Y 0.428 7.9 7.6
23 0600 10 B 0.428
24 0730 9.5 Y 0.428
i5 0.428
26 0.429
27 HOLIDAY
28 0730 8 Y 0.431
29 0730 11.5 Y 0.432 7.9 7.1
3e 0700 9 Y 0.432
31 0730 2 Y 0.432 _
?deathly Average Lida 0.61s 30 30
?fe,ethly AYeraO" 0.4306 0 4.8 7.64
1»1Y Maxhar® 0.448 7.9 0 9.6 8
D. Mithema 0.419 7.8 0 0 7.1
e1ie No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
.0094
1 A A
A a 8
I
I
'iy' i Monthly
8 I Gr.b au I O Z CNDUCIVY —
2400 deli Hn 2400 deck Hn Y/BIN I011lt05/Cn1
1 0730 11.5 Y 936
2 0730 9 Y
3 0800 8 Y
4
5
6 0730 8.5 Y
7 0730 8 Y
$ 0730 9 Y
9 0630 11.5 Y
10 0730 8.5 Y
II
12
13 0730 8.5 Y
14 0730 9 Y
15 0700 9 Y
16 0730 9 Y
17 0600 10 B
18
19
2. 0730 9.5 Y
21 0730 10 Y
22 0730 12.5 Y
23 0600 10 B
34 0730 9.5 Y
25
26
27 HOLIDAY
28 0730 8 Y
29 0730 11.5 Y
30 0700 9 Y
31 0730 2 Y
M.alky Avenge Link:
Monthly Avenge: 936
Deily Maximus' 936
Daily Mini 936
•*te No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
3 1I I M
8
Ii
d 1
4
a i 'a d
8 d 4 e o z
2400 dock Hr. 2400 dock Ms YIBIN
1 0730 11.5 Y
2 0730 9 Y
0800 8 Y
4
,5
6 0730 8.5 Y
7 0730 8 Y
8 0730 9 Y
9 0630 11.5 Y
10 0730 8.5 Y
II
12
13 0730 8.5 Y
14 0730 9 Y
15 0700 9 Y
16 0730 9 Y
17 0600 10 B
18
10
20 0730 9.5 Y
21 0730 10 Y
22 0730 12.5 Y
23 0600 10 B
24 0730 9.5 Y
25
26
27 HOLIDAY
20 0730 8 Y
20 0730 11.5 Y
J0 0700 9 Y
31 0730 2 Y
Monthly Avenge Lea:
Monthly Avenge:
Daly Maximum:
Dray Minimum
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
• 30050 00400 C0310 C0530 00300 C0600 C0665 00840 66694
iti
? d
< , y ; Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u° 8` a 2 Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
22 U 1+
a a b Z FLOW pH BOO-C... TES-Cone DO TOTAL N- TOTAL P-Cone CHLORIDE CNDUCTVY
2400 cloak Hn 2400 clock Hn Y/B/N mgd su mg/I mg/I mg/I mg/I mg/I mgA umhos/cm
I 0730 11.5 Y
2 0730 9 Y
3 0800 8 Y
4
5 .
6 0730 8.5 Y
7 0730 8 Y
6 0730 9 Y
f 0630 11.5 Y
10 0730 8.5 Y
II
12
13 0730 8.5 Y
14 0730 9 Y
15 0700 9 Y
16 0730 9 Y
17 0600 10 B
18
If
26 0730 9.5 Y
21 0730 10 Y
22 0730 12.5 Y
23 0600 10 B
24 0730 9.5 Y
25
26
27 HOLIDAY
29 0730 8 Y
28 0730 11.5 Y
36 0700 9 Y
31 0730 2 Y
Maatky Average LMII:
Monthly Average:
Daily Malheur:
Dag Mariw=
aaaa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
30050 00600 C0530 00094 ee556
i 8
I. A 1 Monthly Monthly Monthly Monthly Quarterly
u° $ 1 d Instantaneous Grab Grab Grab Grab
I F 8. 1 O g FLOW pH TSB-Conn CNDUCIYY OIL-GRSE
2400 dock Hn 2400 dock Hn Y/U/N mgd su mg/I umhos/cm mg/I
I 0730 11.5 Y 0.653 7.68 2.6 881
2 0730 9 Y
3 0800 8 Y
5
6 0730 8.5 Y
7 0730 8 Y
8 0730 9 Y
9 0630 11.5 Y
10 0730 8.5 Y
II
12
13 0730 8.5 Y
14 0730 9 Y
15 0700 9 Y
16 0730 9 Y
17 0600 10 B
10
19
20 0730 9.5 Y
21 0730 10 Y
22 0730 12.5 Y
73 0600 10 B
2I 0730 9.5 Y
25
26
27 HOLIDAY
2s 0730 8 Y
29 0700 11.5 Y
30 0700 9 Y
31 0730 2 Y
Mouthy Avenge Lisa:
Monthly Avenge: 0.653 2.6 881
Daq Ma'das. 0.653 7.68 2.6 881
Daily MYhnus. 0.653 7.68 2.6 881
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION:1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:06/24/2019
t,/iej 06/24/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
e h 06/24/2019
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lithium,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Lance Crayton,Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2019(May 2019) VERSION: 1.0 STATUS:Processed
Report Comments:
Outfall 002,quarterly sampling completed in April

IPr
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 -RECEIVED COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
RECEtVEDM1CpENR/pwR
MAY 31 2019
GRADE:PC-2 ORC HAS CHANGED:N,Q
ENT
RAt eDMR PERIOD:04-2019(April 2019) VERSION: 1.0 p, FILES STATUS:Processed
SECTION JUN 1 0 2019
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHA FF*• NOWQROS
ORESVILLE REGIONAL OFFICE
50058 00400 C0310 COIN 00300 CONO CO665 ONO 0aa04
a
Ay I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u 3 ae$ �di k Recorder Grab Grab Grab Grab Grab Grab Grab Grab
A u $ O O Pc
O A FLOW pH ROD-Caw TES-Cow DO TOTAL N- TOTAL P-Cone CHLORIDE CNDUCTVY
241111 dock Hn 2400 dada Hn WREN mgd so mg/I mg/I mg/I mg/I mg/i mg/I umhos/cm
I 0730 9 Y 0.461
2 0730 9 Y 0.471
3 0730 II Y 0.478 7.92 3 <2.5 10.63 0.6 <0.05 15.6 878
4 0730 8.5 Y 0.461
s 0730 9.5 Y 0.439
a 0.439
7 0.439
I 0730 9 Y 0.439
• 0730 9 Y 0.439
II 0730 9.5 Y 0.439 7.95 8.9
II 0730 4 Y 0.439
12 0730 9 Y 0.446
13 0.446
I4 0.446
IS 0745 9 Y 0.439
16 0730 • 9 Y 0.439
17 0730 9 Y 0.439 7.81 <2.5 7.87
II 0730 9 Y 0.446
I0 N HOLIDAY
20 0.446
21 0.446
22 0700 10 B 0.446
23 0730 8.5 Y 0.446
24 0730 8 Y 0.448 7.83 8.62
23 0730 8 Y 0.448
20 0730 8 Y 0.448
27 0.448
2a 0.448
28 0730 8.5 Y 0.448
30 0730 4.5 Y 0.448
,
Noddy Avenge Unit: /.015 30 30
Manthly Avenge: 0.447069 3 0 9.005 0.6 0 15.6 878
Daily Minimum 0.478 7.95 3 0 10.63 0.6 0 15.6 878
Daly MYYs.: 0.439 7.81 3 0 7.87 0.6 0 15.6 878
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather. NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2019(April 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
• TGP39 THP311
4 8
Quarterly
7x 8k Grab Calculated
4 a F p A CERI7DPF CER7DCHV
2400 clock Hn 2400 dock Hr. YHVH pass/fail percent
I 0730 9 Y
2 0730 9 Y
3 0730 II Y
4 0730 8.5 Y >100
5 0730 9.5 Y
a
7
8 0730 9 Y
9 0730 9 Y
Ia 0730 9.5 Y
II 0730 4 Y
I2 0730 9 Y
13
14
15 0745 9 Y
Ia 0730 9 Y
17 0730 9 Y
IS 0730 9 Y •
III N HOLIDAY
2e
21
22 0700 10 B
23 0730 8.5 Y
24 0730 8 Y
25 0730 8 Y
2c 0730 8 Y
27
211
28 0730 8.5 Y
39 0730 4.5 Y
Monthly Arena.Lkaa:
Monthly Arenas.
100
Dag MuMnn:
100
Dog Ml.laow
100
•*"No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—I loliday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2019(April 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
• 301/34 00499 CO3t. COS.14 NM C0694 COKS 011940 000e4
iQuarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u d Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
8
tE uI u er
pr
O >! FLOW PH ROD-Cow TB8-Cone DO TOTAL N• TOTAL P-Corrc CHLORIDE CNDUCTW
2404 elms Hn IIN clock Hn YIBIN gPd au mg/I mg/I mg/I mg/I mg/ mg/1 umbos/cm
I 0730 9 Y
2 0730 9 Y
3 0730 I I Y 96 7.28 3.4 5.5 11.54 c 0.52 _0.05 41.3 734
4 0730 8.5 Y
3 0730 9.5 Y
6 N
7 N
a 0730 9 Y
se 0730 9 Y
Ia 0730 9.5 Y
II 0730 4 Y
12 0730 9 Y
13 N
14 N
IS 0745 9 Y
II 0730 9 Y
17 0730 9 Y
III 0730 9 Y
II N HOLIDAY
2. Y
21 Y
22 0700 10 B HOLIDAY
23 0730 8.5 Y
24 0730 8 Y
23 0730 8 Y
26 0730 8 Y
27
2.
27 0730 8.5 Y
3. 0730 4.5 Y
Moodily Avenge LWt:
Maadaly Average:
96 3.4 5.5 11.54 0 0.05 41.3 734
Daily Maalndaw: 96 7.28 3.4 5.5 11.54 0 0.05 41.3 734
Daily MYben:
% 7.28 3.4 5.5 11.54 0 0.05 41.3 734
ea.2a No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2019(April 2019) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant {{` CONTACT PHONE#:[phone] SUBMISSION DATE:05/21/2019
t. _Jii .S1..-__. 05/20/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge:
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
' 46---0
05/21/2019
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.l am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,R&A,Pace Asheville,Pace Huntersville
CERTIFIED LAB#:5023,14,40,12
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 ERMIT STATUS:Active 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 REC E I v`,E�OUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis APR 2 3 2019 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No RECEIVED/NCDENR/DWR
- CENTRAL FILES
eDMR PERIOD:03-2019(March 2019) VERSION:2.0 DWR SECTION STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHu��RR�� *• ROS
`�MODR VILL .REGIONAL OFFICE
50050 00600 C0310 C0530 00300 core C0665 00948 THP3B
A !
,if i 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
:Ia
I 8` 1 a Recorder Grab Grab Grab Grab Grab Grab Grab Composite
u
il Ig yT FLOW pH BOD-Cow T88-Cow DO TOTALN- TOTAL P-Caw CHLORIDE CER7DCHV
2000 dads _Has 2600 cloak Has Yn4N mgd su mg/1 mg/I mg/I mg/I mg/I mg/I percent
I 730 10 Y 0.461
2 N 0.458
3 N 0.458
4 730 9 Y 0.458
5 730 10.5 Y 0.454
6 730 9 Y 0.448 7.6 3 <5 10.6
7 730 9 Y 0.454
a 730 9.5 Y 0.454
9 N 0.458
to N 0.458
1t 1100 7 Y 0.465
12 730 10.5 Y 0.465
13 730 10 Y 0.465 7.5 11.7
14 730 9.5 Y 0.468
15 730 9 Y 0.474
16 N 0.474
17 N 0.474
10 1030 7 Y 0.474
19 730 11 Y 0.475
20 730 8 Y 0.475 7.6 <2.6 9.9
21 545 10 B 0.472
23 540 10 B 0.471
23 N 0.471
24 N 0.472
25 730 9.5 Y 0.472
26 745 9.5 Y 0.474
37 745 10 Y 0.474 7.7 10.8
28 730 9.5 Y 0.471
39 730 8.5 Y 0.469
30 N 0.469
31 N 0.469
a
Monthly Average Link: 0.615 30 30
Monthly Average: 0.466258 3 0 10.75
Daa1an 0.475 7.7 3 0 11.7
Daily Im` 0.448 7.5 3 0 9.9
000*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2019(March 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094
' C 'A ye Monthly
I Grab
s u
a u I Cg A CtmUC1vY
2400 dock lin 2400 dock an Y/BIN umhos/cm
I 730 10 Y
2 N
3 N
4 730 9 Y
5 730 10.5 Y
4 730 9 Y 793
7 730 9 Y
8 730 9.5 Y
N
l• N
11 1100 7 Y
12 730 10.5 Y
13 730 10 Y
14 730 9.5 Y
15 730 9 Y
I4 N
17 N
IS 1030 7 Y
If 730 11 Y
20 730 8 Y
21 545 10 B
22 540 10 B
21 N
24 N
23 730 9.5 Y
24 745 9.5 Y
27 745 10 Y
20 730 9.5 Y
25 730 8.5 Y
38 N
31 N
Moab Avec.g.Ll.k:
M.e1kl3 Avenge: 793
D. M"IMn. 793
Dolly Mier...: 793
***No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2019(March 2019) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
500S0 00400 C0314 C053000300 CO4BO C0665 003N OWNO4
I! a
I g Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
1 I a I 8 I
Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
6; `8 FLOW pH BOD-Cone TSS-Cnan DO TOTAL N- TOTAL P-Cove CHLORIDE CNDUCTVY
2400 deck Hn 24110 deck Hn Y/s:N mgd su mg/1 mg/1 mg/I mg/1 mg/1 mg/I umhos/em
I 730 10 Y
2 N
3 N
4 730 9 Y
5 730 10.5 Y
6 730 9 Y
7 730 9 Y
5 730 9.5 Y
f N
it N
I 1100 7 Y
12 730 10.5 Y
13 730 10 Y
14 730 9.5 Y
t5 730 9 Y
16 N
17 N
IS 1030 7 Y
If 730 11 Y
20 730 8 Y
21 545 10 B
22 540 10 B
23 N
24 N
25 730 9.5 Y
24 745 9.5 Y
27 745 10 Y
20 730 9.5 Y
2f 730 8.5 Y
30 N
31 N
Monthly Avenge Link:
.M.n W Average:
Averag
_Daley Madn®s :
Deny MYlnae:
aa'f No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2019(March 2019) VERSION:2.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:04/10/2019
21.1 u AL.. 04/10/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
9
�'�/ 04/10/2019
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lihtuium, Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 R E C F I\ f EMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R Al i q�!qi„+�COUJNTY:Gaston
3
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis MAR !d 20[52C CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No CENTRAL FILES RECEIVED/NC%EN1R/DLVR
eDMR PERIOD:02-2019(February 2019) VERSION: 1.0 DWR SECTICk#ATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO CS
MOCPF vit.LE R G O".1AL OFFICE
• 30050 00400 C0310 C0530 00300 C0600 C0665 00949 THP3B
i A A •
a 14
I. i A : i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
8 8 k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
8 ; i S U f+ O 2 FLOW pH BOD-Cone TSS-Cone DO TOTAL N- TOTAL P P.Cone CHLORIDE CER7DCHY
2400 clock Hr. 2400 dock Hes YnIIN mgd su mg/1 mg/I mg/I mg/I mg/I mg/I percent
1 0700 9 Y 0.461
2 0.461 RECEIVED
3 0.461
4 0730 9 Y 0.461 LIAR 2 7 2019
5 0730 8 Y 0.461
6 0730 9.5 Y 0.461 8.02 3 5.3 11.65 i"LN 1.RAL FILES
7 0715 9.5 Y 0.461 DIAIR SECTION
a 0730 9 Y 0.461
9 0.461
to 0.461
11 0700 8 Y 0.461
12 0730 9 Y 0.461
13 0730 8 Y 0.461 7.82 11.45
14 0730 9.5 Y 0.461
15 0730 9.5 Y 0.461
16 0.461
17 0.461
18 0730 8 Y 0.459
19 0730 9 Y 0.455
20 0730 6.5 Y 0.452 7.76 <2.6 11.42
21 0600 10 B 0.452
22 0600 10 B 0.456
23 0.458
24 0.459
25 0730 10.5 Y 0.461
26 0730 10.5 Y 0.462
27 0730 10.5 Y 0.462 7.51 11.55
20 0745 8.5 Y 0.461
•
Monthly Avenge Limit 0.615 30 30
Monthly Avenge: 0.459786 3 2.65 11.5175
Dolly Maximum 0.462 8.02 3 5.3 11.65
Dolly tHlnimnm. 0.452 7.51 3 0 11.42
"i6 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2019(February 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
40094
j J 1 I —
Monthly
u a` $ a I
u o A CNDUrnY
2400 dock Hn 2400 dock Hn Y/B/N umhos/Cm
I 0700 9 Y
2
3
4 0730 9 Y
s 0730 8 Y
4 0730 9.5 Y 796
7 0715 9.5 Y
6 0730 9 Y
9
U
II 0700 8 Y
12 0730 9 Y
IS 0730 8 Y
14 0730 9.5 Y
Is 0730 9.5 Y
Ig
17
II 0730 8 Y
19 0730 9 Y
29 0730 6.5 Y
21 0600 10 B
22 0600 10 B
23
24
23 0730 10.5 Y
26 0730 10.5 Y
27 0730 10.5 Y
20 0745 8.5 Y
Monaiy Avenge U..k:
Monthly Avenge:
796
Dolly Madams: 796
D.By 1V11414“m: 796
4444 No Repotting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2019(February 2019) VERSION:1.0 STATUS:Processed
•
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
30050 0000 C0310 C0530 40300 C0600 C0665 80940 00004
8 L' 8 :
C .� I Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
< F
u a t a Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
a p�1
d tJ t O A FLOW pH BOD-Coe TES-Coat DO TOTAL N- TOTAL P-Cow CHLORIDE CNDUCIYY
2400 dock Hre 2400 dock Ws Y/B/N mgd su mg/I mg/I mg/1 mg/I mg/I mg/I umhos/cm
I 0700 9 Y
2
3
4 0730 9 Y
5 0730 8 Y
6 0730 9.5 Y
7 0715 9.5 Y
8 0730 9 Y
8
14 .
11 0700 8 Y
12 0730 9 Y
IS 0730 8 Y
14 0730 9.5 Y
Is 0730 9.5 Y
16
17
10 0730 8 Y
I0 0730 9 Y
20 0730 6.5 Y
21 0600 10 B
22 0600 10 B
23
24
25 0730 10.5 Y
26 0730 10.5 Y
27 0730 10.5 Y
21 0745 8.5 Y
Mothl3 Average Lill:
Monthly Average:
D. Maximus:
Dal'MYka:
Mee*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2019(February 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
e .t 11 I
a
d F i e d
3
8 u $ b g
2400 clack Hn 2400 dock Hn YIBIH
I 0700 9 Y
2
3
4 0730 9 Y
5 0730 8 Y
6 0730 9.5 Y
7 0715 9.5 Y
0 0730 9 Y
9
10
11 0700 8 Y
12 0730 9 Y
13 0730 8 Y
14 0730 9.5 Y
IS 0730 9.5 Y
14
17
10 0730 8 Y
10 0730 9 Y
M 0730 6.5 Y
21 0600 10 B
22 0600 10 B
23
24
23 0730 10.5 Y
26 0730 10.5 Y
27 0730 10.5 Y
20 0745 8.5 Y
Monthly Avenge Lima:
Meanly Avenge:
Dray Madmnm:
Daily Minimum:
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2019(February 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 01400 C0530 0005. 00554
< F a3
8
,� jj Monthly Monthly Monthly Monthly Quarterly
3 8 8 d ci Instantaneous Grab Grab Grab Grab
I & i I
a o 1 FLOW pH 788UCr, oB GRBE
2400 del: Hn 2400 dark Hrr Y/env mgd su mg/I umhos/cm mg/I
I 0700 9 Y
2
3
4 0730 9 Y
5 0730 8 Y
0730 9.5 Y 0.754 7.84 <I 945
7 0715 9.5 Y
8 0730 9 Y
f
to
It 0700 8 Y
12 0730 9 Y
13 0730 8 Y
14 0730 9.5 Y
15 0730 9.5 Y
16
17
18 0730 8 Y
If 0730 9 Y
le 0730 6.5 Y
21 0600 10 B
22 0600 10 B
23
24
25 0730 10.5 Y
24 0730 10.5 Y
27 0730 10.5 Y
28 0745 8.5 Y
Mw64 Avenge Liana
Meanly Average: 0.754 0 945
Dail'Mannan' 0.754 7.84 0 945
Dela'Mialar.ar' 0.754 7.84 0 945
aa'a No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2019(February 2019) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:03/14/2019
03/11/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
03/14/2019
Permittee/Submitter Signature:*** Larr A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lithium,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No 74ECEIVEDlNCDENRIDWFB
eDMR PERIOD:01-2019(January 2019) VERSION: 1.0 STATUS:Processed I:I A R 1 0 2 fl 1 q
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCH,�R * N oRos
" ? EOk_I REGIONAL OFFICE
• 50050 00400 C0310 C0530 00300 C0600 C0665 00940 00094
i1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
s` a` 8 ci Recorder Grab Grab Grab Grab Grab Grab Grab Grab
Y >� ez pv�
8 U F O O Z FLOW pH BOD-Ceae TSS-Can DO TOTAL N- TOTAL P-Can CHLORIDE CNDUCTVY
2400 dock Hn 2400 dodo Hn Y/SM mgd su mg/I mg/I mg/I mg/I mg/I mg/I umhos/cm
I 0615 1.5 Y 0.454
2 0730 9 Y 0.454 7.88 <2 <5 11.16 <0.52 <0.05 18.2 713
3 0730 9 Y 0.454
4 0730 9.5 Y 0.454
5 0.454
6 0.454
7 0730 8.5 Y 0.455
0 0715 7 Y 0.455
9 0730 9.5 Y 0.454 8.01 12.48
t0 0730 9.5 Y 0.451
it 0730 9.5 Y 0.451
12 0.451
13 0.451
14 0730 8.5 Y 0.451
15 0730 9.5 Y 0.451
16 0730 9.5 Y 0.451 7.68 <2.6 11.45
17 0730 8 Y 0.449
18 0730 .10 B 0.448R rN_ 1\(F D
19 0.45566
20
0.443 -
MAR 1 4 2C19
21 HOLIDAY
22 0730 9 Y 0.441 _
23 0730 9 V 0.448 7.76 12.32 ti,il'1`t 1
24 0800 4 Y 0.454 ': • ''
25 1100 5 Y 0.454
24 0.454
27 0.452
20 0730 8 Y 0.452
29 0730 II Y 0.446
30 0730 10.5 Y 0.432 7.79 11.64
31 0700 6.5 Y 0.446
Meerhly Avenge Limit: 0.615 30 30
MonWyAvenge: 0.450667 0 0 11.81 0 0 18.2 713
Ddly Madman: 0.456 8.01 0 0 12.48 0 0 18.2 713
Dail'Minkssum 0.432 7.68 0 0 11.16 0 0 18.2 713
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2019(January 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
TGP3B THP3B
A ;7;
I6 < IIi Quarterly
V 3 E 8 $ Grab Calculated
7t u a�
I E t A CERI7DPF CER7DCHY
2400 dock Hn 2400 dock Hn WWI pass/fail percent
1 0615 1.5 Y
2 0730 9 Y
3 0730 9 Y
4 0730 9.5 Y
s
6
7 0730 8.5 Y
a 0715 7 Y
0730 9.5 Y
II 0730 9.5 Y >100
11 0730 9.5 Y
12
I3
14 0730 8.5 Y
15 0730 9.5 Y
16 0730 9.5 Y
17 0730 8 Y
to 0730 10 B
1)
20
21 HOLIDAY
22 0730 9 Y
23 0730 9 Y
24 0800 4 Y
23 1100 5 Y
26
27
20 0730 8 Y
29 0730 11 Y
34 0730 10.5 Y
31 0700 6.5 Y
Monthly Avenge unit:
Monthly Avenge:
100
Daly Maximum:
100
Daly Mom: I®
eee6 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2019(January 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
y YY 50050 00400 C0310 C0530 00300 C0600 C0665 00940 00994
F F
F 4
AQuarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
! a 8 rt Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
Y 1 a
a U F u O a
g FLOW pH BOD-Caw TSB-Cone DO TOTAL N- TOTAL P-Case CHLORIDE CNDUCIYY
2400 dock Hn 2400 dark Hn YIBIN 8Pd as mg/1 mg/I mg/1 mg/I mg/I mg/I umhos/cm
I 0615 1.5 Y
2 0730 9 Y 8640 7.15 <2 6.9 9.4 <0.52 0.063 34.8 626
3 0730 9 Y
4 0730 9.5 Y
5
6
7 0730 8.5 Y
0 0715 7 Y
9 0730 9.5 Y
to 0730 9.5 Y
II 0730 9.5 Y
12
13
14 0730 8.5 Y
15 0730 9.5 Y
16 0730 9.5 Y
17 0730 8 Y
II 0730 10 B
19
20
21 HOLIDAY
22 0730 9 Y
23 0730 9 Y
24 0800 4 Y
25 1100 5 Y
26
27
20 0730 8 Y
2f 0730 11 Y
30 0730 10.5 Y
31 0700 6.5 Y
Monthly Avenge LBW*:
Monthly Avenge: 8640 0 6.9 9.4 0 0.063 34.8 626
Daily Maximom. 8640 7.15 0 6.9 9.4 0 0.063 34.8 626
Daly im= 8640 7.15 0 6.9 9.4 0 0.063 34.8 626
4444 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2019(January 2019) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
I I s<
P. F m
I 0
a7
s.e . I
a a
8 u f 1 $ o x
2400 dock Mrs 2400 dock H. Y!&N
1 0615 1.5 Y
2 0730 9 Y
3 0730 9 Y
4 0730 9.5 Y
s
6
7 0730 8.5 Y
8 0715 7 Y
9 0730 9.5 Y
10 0730 9.5 Y
11 0730 9.5 Y
12
13
14 0730 8.5 Y
15 0730 9.5 Y
16 0730 9.5 Y
17 0730 8 Y
I0 0730 10 B
19
20
21 HOLIDAY
22 0730 9 Y
23 0730 9 Y
24 0800 4 Y
25 1100 5 Y
26
27
20 0730 8 Y
29 0730 11 Y
J0 0730 10.5 Y
31 0700 6.5 Y
Monthly Avenge Limit:
Monthly Avenge:
_Daily Mo:imom:
Daily Minim:
eete No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2019(January 2019) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
•
50050 00400 C0530 00094 00556
••
s 4 8
$ t `I' Monthly Monthly Monthly Monthly Quarterly
B
D p 8 1 Instantaneous Grab Gab Grab Grab
Ca Ua F G O Za FLOW pH 7'8.4-Cone CNDUCTVY OH,-GRSE
2400 dank Hn 2400 dank Hn Y/BIN mgd su mg/1 umhos/cm mg/1
1 0615 1.5 Y
2 0730 9 Y 1.322 7.75 <2.6 719 <4.8
3 0730 9 Y
4 0730 9.5 Y
5
6
7 0730 8.5 Y
0 0715 7 Y
9 0730 9.5 Y
10 0730 9.5 Y
II 0730 9.5 Y
12
13
14 0730 8.5 Y
15 0730 9.5 Y
16 0730 9.5 Y
17 0730 8 Y
18 0730 10 B
19
20
21 HOLIDAY
22 0730 9 Y
23 0730 9 Y
24 0800 4 Y
25 1100 5 Y
26
27
28 0730 8 Y
29 0730 11 Y
30 0730 10.5 Y
31 0700 6.5 Y
Monthly Avenge Limn:
Monthly Avenge: 1.322 0 719 0
u.By Mnsimam. 1.322 7.75 0 719 0
»all1imag' 1.322 7.75 0 719 0
a999 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2019(January 2019) VERSION:1.0 •
STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:02/26/2019
6221 U.;001/4,
02/25/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
G 7 02/26/2019
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville,Pace Charlotte
CERTIFIED LAB#:5023,40,12
PERSON(s)COLLECTING SAMPLES:Rodney WIllis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active 3
ACILITY NAME:Lithium Division Plant CLASS:PC-2 RE C F w NTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis CERT NUMBER:28624
JAN 2 9 2019 RECEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2018(December 2018) VERSION: 1.0 (` ..., 1, )ATUS:Processed FEB 0 4 2 fl 1 y
C'VIR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC �R ��ii'', os
�Of YrF\7ICL G I 0 N A L OFFICE
y 50050 00400 C031e COSH 00300 C0600 C0665 60949 THP38
I 4 Y 7 d .
I I I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
y
1 a` a
u pb�
k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
p
a U O L' FLOW pH ROD-Conn TSS-Cone DO TOTALN- TOTAL P-Cone CHLORIDE CER7DCHV
2400 deck Hn 2400 dock Hn V/BIN mgd su mg/1 mg/I mg/I mg/I mg/I mg/I percent
t N 0.451
2 N 0.451
3 0730 9 Y 0.451
4 0730 9 Y 0.451
5 0730 9 Y 0.451 7.61 <2 <5 8.82
6 0600 10 B 0.451
7 0530 10 B 0.446
5 N 0.451
9 N 0.451
to 0930 7 Y 0.451
11 0730 9.5 Y 0.451
12 0745 11 Y 0.451 7.55 11.4
13 0815 10 Y 0.451
14 0600 10 B 0.451
15 N 0.451
16 N 0.451
17 0730 II Y 0.451
15 0730 6 Y 0.451
19 0730 11.5 Y 0.451 7.68 <2.5 11.45
2e 0730 11.5 Y 0.451
21 1645 0.5 Y 0.451
22 1000 4 Y 0.451
23 N 0.451
24 1030 0.5 Y 0.451
25 N HOLIDAY
26 0700 8.5 Y 0.451 7.71 12.69
27 0730 9.5 Y 0.451
25 0900 10.5 Y 0.451
29 N 0.451
3e N 0.451
31 N HOLIDAY
Monthly Avenge Link: e.615 30 39
Monthly Avenge: 0.450828 0 0 11.09
DailY 1Nn:imnn' 0.451 7.71 0 0 12.69
Doily ims= 0.446 7.55 0 0 8.82
's"No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 12-2018(December 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
8
I
I
I I Monthly
gd Ou Z CNDUCTVY
2608 dodc Hn 2400 dsek Hn Y/B/N umhos/cm
1 N
2 N
3 0730 9 Y
6 0730 9 Y
5 0730 9 Y 695.8
6 0600 10 B
7 0530 10 B
8 N
9 N
10 0930 7 Y
11 0730 9.5 Y
12 0745 11 Y
13 0815 10 Y
14 0600 10 B
15 N
16 N
17 0730 Il Y
18 0730 6 Y
19 0730 11.5 Y
20 0730 11.5 Y
21 1645 0.5 Y
22 1000 4 Y
23 N
2* 1030 0.5 Y
25 N HOLIDAY
26 0700 8.5 Y
27 0730 9.5 Y
28 0900 10.5 Y
29 N
30 N
31 N HOLIDAY
MN61y Avenge Liao:
Mouthy Average: 695.8
Daily Ma*Naa. 695.8
Daily Mi.I.n: 695.8
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2018(December 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
30050 00400 C0310 C0530 00300 C0600 C0665 00940 00094
1 1 8
i < I jj ; Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
ti = ! 8
aZ
Lg Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
Cx u
S I 1 O 2 FLOW pH BOD-Cone TS8-Cow DO TOTALN- Turn P-Cow CHLORIDE CNDOCTVY
2400 dock Hn 2400 dock Hn Y/BIN mgd su mg/ mg/I mg/I mg/I mg/I mg/I umhos/cm
I N
2 N
3 0730 9 Y
4 0730 9 Y
5 0730 9 Y
6 0600 10 B
7 0530 10 B
8 N
9 N
10 0930 7 Y
II 0730 9.5 Y
12 0745 I I Y
13 0815 10 Y
14 0600 10 B
IS N
16 N
17 0730 11 Y
18 0730 6 Y
19 0730 11.5 Y
2• 0730 11.5 Y
21 1645 0.5 Y
22 1000 4 Y
23 N
24 1030 0.5 Y
25 N HOLIDAY
26 0700 8.5 Y
27 0730 9.5 Y
28 0730 10.5 Y
29 N
30 N
31 N HOLIDAY
Monthly Avenge UAW:
Monthly Avenge:
Dilly Madame:
.Day MYm:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2018(December 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
A i A A
1 F 8
x
A e f 4 q I g
8.
oI
a ea1. u
8 u F o z
2400 dodo Hn 2400 dock Hn If/BIN
t N
2 N
3 0730 9 Y
4 0730 9 Y
5 0730 9 Y
6 0600 10 B
7 0530 10 B
0 N
9 N
to 0930 7 Y
II 0730 9.5 Y
12 0745 11 Y
13 0815 10 Y
14 0600 10 B
15 N
16 N
17 0730 11 Y
18 0730 6 Y
19 0730 11.5 Y
20 0730 11.5 Y
21 1645 0.5 Y
22 1000 4 Y
23 N
24 1030 0.5 Y
25 N HOLIDAY
26 0700 8.5 Y
27 0730 9.5 Y
20 0730 10.5 Y
29 N
30 N
31 N HOLIDAY
Monthly Avenge Limit:
Monthly Avenge:
Daily Maximum:
Daily Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2018(December 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00094 00556
A A A •
8y
B ! 9 Monthly Monthly Monthly Monthly Quarterly
.S 1 , .. C
a 8 Instantaneous Grab Grab Grab Grab
E= O O 0
8 i e$ C$ pub
a N A FLOW pH 793-Cam CNDUCTVY OII.CRSC
2400 dodo Hn 2400 dodo Hn Y/B/N mgd su mg/1 umhos/cm mg/1
1 N
2 N
3 0730 9 Y
4 0730 9 Y
5 0730 9 Y 0.686 7.75 <2.6 716.6
6 0600 10 B
7 0530 10 B
a N
N
Ie 0930 7 Y
II 0730 9.5 Y
12 0745 11 Y
13 0815 10 Y
14 0600 10 B
Is N
16 N
17 0730 11 Y
18 0730 6 Y
19 0730 11.5 Y
20 0730 11.5 Y
21 1645 0.5 Y
22 1000 4 Y
23 N
24 1030 0.5 Y
75 N HOLIDAY
26 0700 8.5 Y
27 0730 9.5 Y
20 0900 10.5 Y
20 N
30 N
31 N HOLIDAY
Monthly Avenge Limit:
Monthly Avenge. 0.686 0 716.6
Daily gym. 0.686 7.75 0 716.6
Daily Waleson 0.686 7.75 0 716.6
***'No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2018(December 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:01/15/2019
OL _ \ 01/15/2019
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
01/15/2019
Permittee/Submitt r Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:Lithium,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Lance Crayton,Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 12-2018(December 2018) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Flow for 12/25/18 0.451 MGD
Flow for 12/31/18 0.451 MGD
System would not allow entry of"No Visitation Holiday"and flow to be saved

RMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active 5
ACILITY NAME:Lithium Division Plant CLASS:PC-2 R E(' IN/E D COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis JA N Is 7 2017 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No RECEIVEDINCDENRIDWR
-CENlimieDMR PERIOD:11-2018(November 2018) VERSION:1.0 3 STATUS:Certified i;_ ; .1 4 1!!1`.;
MYR3L:CTIOti
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCU�,A�RR(��,* *a os
1U�pCJRE5Vla. .�M GIONAL OFFICE
50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
6 C
SJ 1 A y i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
i 7
g u° L I. 8 L Recorder Grab Grab Grab Grab Grab Grab Grab Composite
s d a A.
g a a
S aF 6 (8O Z FLOW PH BOD-Cone TSS-Cane DO TOTAL N- TOTAL P-Cone CHLORIDE CER7DCHV
2400 dock H.n 2400 deck Hn WWI mgd su mg/1 mg/I mg/I mg/1 mg/I mg/I percent
1 0730 9 Y 0.459
2 0700 9 B 0.459
3 0.459
4 0.459
5 0730 8.5 Y 0.459
6 0730 9 Y 0.459
7 0730 8 Y 0.459 7.6 <2 <2.5 6.43
a 0730 10.5 Y 0.459
9 0730 9.5 Y 0.459
10 0.458
11 0.458
12 0715 9.5 Y 0.456
13 0730 9.5 Y 0.456
14 0730 9.5 Y 0.456 7.53 6.09
15 0745 10 Y 0.456
16 0600 10 B 0.454
17 0.455
10 0.452
19 0700 9 B 0.448
20 0600 10 B 0.452
21 0600 10 B 0.461 7.61 <2.5 7.26
22 0600 10 B 0.458
23 0600 10 B 0.452
24 0.452
25 0.452
26 0730 9.5 Y 0.454
27 0730 9.5 Y 0.454 7.59 10.4
20 0700 11.5 Y 0.452
29 0700 10 Y 0.452
30 0730 9.5 Y 0.452
Monthly Average Lhaa: 0.615 30 30
Monthly Average: 0.4557 0 0 7.545
Day Masimam: 0.461 7.61 0 0 10.4
Dolly 07e1anm. 0.448 7.53 0 0 6.09
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2018(November 2018) VERSION:1.0 STATUS:Certified
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094
F
a d
i6 i A `1 Monthly
6 1 Grab
a�h P 3
Li U E% O Z CNDUCTVY
2400 dock Hn 2100 deck Hn Y/B/N umhos/cm
I 0730 9 Y
2 0700 9 B
3
1
5 0730 8.5 Y
6 0730 9 Y
7 0730 8 Y 711
8 0730 10.5 Y
9 0730 9.5 Y
t0
11
12 0715 9.5 Y
13 0730 9.5 Y
11 0730 9.5 Y
15 0745 10 Y
16 0600 10 B
17
II
19 0700 9 B
20 0600 10 B
21 0600 10 B
22 0600 10 B
23 0600 10 B
24
25
26 0730 9.5 Y
27 0730 9.5 Y
28 0700 11.5 Y
29 0700 10 Y
30 0730 9.5 Y
Monthly Avenge Limit:
Monthly Avenge: 711
Dully Madman. 711
Daily Minimum: 711
"'•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2018(November 2018) VERSION: 1.0 STATUS:Certified
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
80030 00400 C0310 C0530 00300 C0600 C0665 00940 00094
Iit i
. , 8 i
fi < El 'y ; Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
3 8 g Gr
ab ab Grab Grab Grab Grab Grab Grab Grab
g it of
S G F O FLOW pH DOD-Cone T83-Cone DO TOTAL N- TOTAL P-Cone CHLORIDE CNDUCTVY
2400 deck Hn 2400 deck Hrs WHIN mgd su mg/I mg/1 mg/1 mg/I mg/I mg/I umhos/cm
I 0730 9 Y
2 0700 9 B
3
4
5 0730 8.5 Y
6 0730 9 Y
7 0730 8 Y
8 0730 10.5 Y
9 0730 9.5 Y
10
II
12 0715 9.5 Y
13 0730 9.5 Y
14 0730 9.5 Y
15 0745 10 Y
16 0600 10 B
17
18
19 0700 9 B
20 0600 10 B
21 0600 10 B
22 0600 10 B
23 0600 10 B
24
23
26 0730 9.5 Y
27 0730 9.5 Y
28 0700 11.5 Y
29 0700 10 Y
30 0730 9.5 Y '
Monthly Avenge Lida:
Monthly Avenge:
Dilly Mnimum:
Daily Minimum:
0000 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2018(November 2018) VERSION: 1.0 STATUS:Certified
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
A A y 1
J A E.
s e 3 °p £p c
q U F O O O Z
2400 dock Hr. 2400 clock Hn Y/11/N
I 0730 9 Y
2 0700 9 B
J
4
5 0730 8.5 Y
6 0730 9 Y
7 0730 8 Y
8 0730 10.5 Y
9 0730 9.5 Y
10
It
12 0715 9.5 Y
13 0730 9.5 Y
14 0730 9.5 Y
15 0745 10 Y
16 0600 10 B
17
18
19 0700 9 B
20 0600 10 B
21 0600 10 B
22 0600 10 B
23 0600 10 B
24
25
26 0730 9.5 Y
27 0730 9.5 Y
28 0700 11.5 Y
29 0700 10 Y
30 0730 9.5 Y
Monthly Average Limit:
Monthly Avenge:
Dolly Maximum:
Dolly Minimum:
s•'•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2018(November 2018) VERSION:1.0 STATUS:Certified
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
•
50050 00400 C0530 00094 00556
q it
- 8I
J s L •
8 C A m Monthly Monthly Monthly Monthly Quarterly
I e
u° i 8g Instantaneous Grab Grab Grab Grab
s B g
8 V Ib O FLOW pH sus-Cone CNDUCIVY OR GRSE
2400 dock Hn 2400 dock Hn WW1 mgd su mg/I umhos/om mg/I
1 0730 9 Y
2 0700 9 B
3
4
5 0730 8.5 Y
6 0730 9 Y
7 0730 8 Y 1.122 7.7 <5 715
0 0730 10.5 Y
9 0730 9.5 Y
l0
II
12 0715 9.5 Y
13 0730 9.5 Y
14 0730 9.5 Y
15 0745 10 Y
16 0600 10 B
17
10
19 0700 9 B
20 0600 10 B
21 0600 10 B
22 0600 10 B
23 0600 10 B
24
25
26 0730 9.5 Y
27 0730 9.5 Y
25 0730 11.5 Y
29 0730 10 Y
30 0730 9.5 Y
'
Monthly Avenge Limit
Monthly Average: 1.122 0 715
Doily Ma lmam: 1.122 7.7 0 715
Doily Minimum: 1.122 7.7 0 715
*0*0 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5 0 PERMIT S TA'I I'S:Acme
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis OR('CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2018(November 2018) VERSION:1 0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE N:7048687630 SUBMISSION DATE: 12/22/2018
12/22/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:rodney.willislvfmc.com Phone 4:704-868-7630 Date
By this signature.I certify that this report is accurate and complete to the best of my knowledge.
The pertnittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the pcmiittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the perrtittee becomes aware of the circumstances.
If the facility is noncompliant please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part H.E.6 of
the NPDI:S permit. I_ - ,,�
C. �`�"--`" 12/22/2018
Permittee/Submitter Signature:•'• Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/312023
1 certify,under penalty of lass.that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and esaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of-my knowledge and belief,true,
accurate.and complete I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CE:RTIFIEI)LABORA1 DRIES
I tB N EMI:I MC-thrum.Pace&shevil►e
c I.R7 1 FOI t)1 SR re:5021,40
PERM/NW COLLECTING SAMPLES:lance Cravto,Rodney N itlis
PARAMETER('ODES
Parameter('ode krone may he obtained by calling the NPDI.S Unit(9191 807-63(N)or by visiting htip.,'portal.npdenr.orgweb'w q swlupit npdes forms.
l'OO174O11.S
l se only units of measurement designated in the reporting facility's NPDES permit bor reporting data.
• No Flow'Discharge Flom Site:Check this hos if no discharge occurs and.as a rewh,there are no data to be entered tor all of the parameters on the DMR
I r entire monitoring period.
••t)R('on Site' ORC must visit facility and document visitation of facility as required per I SA NCAC BC.0204.
•••Signature of Perrnince If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 213
(1SO6082$D)

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 C '� PERMIT STATUS:Active 3
NAME:Lithium Division Plant CLASS:PC-2 \C`.f El VEITY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis NOV 1 6 ZQ O C CERT NUMBEIfiE NCDENRIDINR
GRADE:PC-2 ORC HAS CHANGED:No CAN l NOV A 2018
eDMR PERIOD: 10-2018(October 2018) VERSION: 1.0 CENIJLL FI��Pj1►TUS:Processed D
DWR SECTION
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DIS® tt INVIONAL OFFICE
gy
x 50050 00400 C0310 C0530 00300 COMM C0665 00940 00094
g •
A F y
y i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
tli _ d ri Recorder Grab Grab Grab Grab Grab Grab Grab Grab
a o
S U t O z PLOW pH aOD-Cove TSO-Gene DO TOTALN- TOTAL P-Con CHLORIDE CNDUCTVY
2400 dock Hn 2400 clock Hn Y/B/N mgd su mg/I mg/1 mg/I mg/I mg/1 mg/I umhos/cm
1 0730 9 Y 0.461
2 0700 4 Y 0.461
3 0730 10 Y 0.461 7.42 <2 3 6.6 <0.52 <0.05 26.1 740
4 0600 10 B 0.465
5 0600 10 B 0.465
4 0.465
7 0.465
a 0730 9.5 Y 0.465
9 0730 9.5 Y 0.458
to 0730 9.5 Y 0.462 7.3 5.91
II 0545 8 Y 0.462
12 0600 IO B 0.462
13 0.462
14 0.462
15 0730 10.5 Y 0.462
16 0715 12.5 Y 0.461
17 0715 10 Y 0.461 7.7 4.7 7.7
19 0600 10 B 0.461
19 0600 10 B 0.461
20 0.461
21 0.46I
22 0730 8.5 Y 0.456
23 0730 8 Y 0.456
24 0730 8.5 Y 0.456 7.4 7.2
25 0730 9 Y 0.456
26 0700 9 B 0.456
27 0.455
20 0.454
29 0700 9.5 B 0.452
30 0715 9 Y 0.452
31 0730 9 Y 0.452 7.6 8.6
Meath Avenge Llnll: 0.615 30 30
Monthly Avenge: 0.459645 0 3.85 7.202 0 0 26.1 740
Daly `ben®` 0.465 7.7 0 4.7 8.6 0 0 26.1 740
Do* heeme 0.452 7.3 0 3 5.91 0 0 26.1 740
•i4 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2018(October 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
TGP3B THP3B
J I A
I y 7 8
fi I g 1 Quarterly
4 u 2 I. Grab Calculated
2e $ 1 E 8 a
S aF t O Zo CERI7DPF CER7DCHV
2400 dock Hn 2400 dock Hn Y/BIN pass/fail percent
1 0730 9 Y
2 0700 4 Y
3 0730 10 Y
4 0600 10 B >100
5 0600 10 B
6
7
8 0730 9.5 Y
9 0730 9.5 Y
10 0730 9.5 Y
11 0545 8 Y
12 0600 10 B
13
14
15 0730 10.5 Y
16 0715 12.5 Y
17 0715 10 Y
18 0600 10 B
19 0600 10 B
20
21
22 0730 8.5 Y
23 0730 8 Y
24 0730 8.5 Y
25 0730 9 Y
26 0700 9 B
27
28
29 0700 9.5 B
30 0715 9 Y
31 0730 9 Y
Monthly Avenge Link:
Monthly Avenge: 100
Dolly Madmam: 100
Daily Minimum: 100
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2018(October 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
•
50050 00000 C0310 C0530 00300 C0600 C0665 00940 00094
A i
S F I
3 f8
6 C 5 Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u° S 3 8 a Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
E e` 3ec
S u 8 O Z FLOW pH ROD-Cone TS4-Coat DO TOTAL N- TOTAL P-Cone CHLORIDE CNDUCTVY
2400 dock Hn 2400 dock Hn Y/WN gpd su mg/I mg/1 mg/I mg/1 mg/1 mg/1 umhos/cm
I 0730 9 Y
2 0700 4 Y
3 0730 10 Y 3600 6.9 10.1 23.2 7 <0.52 0.1 46.4 856
4 0600 10 B
5 0600 10 B
6
7
8 0730 9.5 Y
9 0730 9.5 Y
10 0730 9.5 Y
II 0545 8 Y
12 0600 10 B
13
14
15 0730 10.5 Y
16 0715 12.5 Y
17 0715 10 Y
18 0600 10 B
19 0600 10 B
20
21
22 0730 8.5 Y
23 0730 8 Y
24 0730 8.5 Y
25 0730 9 Y
26 0700 9 B
27
28
29 0700 9.5 B
70 0715 9 Y
31 0730 9 Y
Monthly Average Link:
Mouthy Avenge: 3600 10.1 23.2 7 0 0.1 46.4 856
Daily Moalmum. 3600 6.9 10.1 23.2 7 0 0.1 46.4 856
Daily Minimum: 3600 6.9 10.1 23.2 7 0 0.1 46.4 856
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2018(October 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
I. l A Y
BA I
s P 3
A :3rr 15 o z
2400 clock Hra 2400 dock H.. Y/ILN
1 0730 9 Y
2 0700 4 Y
3 0730 10 Y
4 0600 10 B
3 0600 10 B
6
7
0 0730 9.5 Y
9 0730 9.5 Y
t9 0730 9.5 Y
II 0545 8 Y
12 0600 10 B
13
14
15 0730 10.5 Y
16 0715 12.5 Y
17 0715 10 Y
1s 0600 10 B
19 0600 10 B
20
21
22 0730 8.5 Y
23 0730 8 Y
24 0730 8.5 Y
25 0730 9 Y
26 0700 9 B
27
28
29 0700 9.5 B
30 0715 9 Y
31 0730 9 Y
Moodily Average Limit:
Monthly Average:
Dilly Midmom:
Dolly Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2018(October 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
30050 00400 C0530 00094 00556
A
s 8
I8
8 E I i Monthly Monthly Monthly Monthly Quarterly
3 6 ? 8 Instantaneous Grab Grab Grab Grab
a z
O G i2 G 8' O Z FLOW pH TOO-Cone CNDUCTVY OIL-CRSE
2400 dock Hn 2400 clock Hn Y/R/N mgd su mgd umhos/cm mg/1
1 0730 9 Y
2 0700 4 Y
3 0730 10 Y
4 0600 10 B
5 0600 10 B
6
7
a 0730 9.5 Y
9 0730 9.5 Y
tO 0730 9.5 Y
II 0545 8 Y
12 0600 10 B
13
14
15 0730 10.5 Y
16 0715 12.5 Y
17 0715 10 Y 0.079 7.4 <2.6 304 <4.8
18 0600 10 B
19 0600 10 B
20
21
22 0730 8.5 Y
23 0730 8 Y
24 0730 8.5 Y
25 0730 9 Y
26 0700 9 B
27
28
29 0700 9.5 B
30 0715 9 Y
31 0730 9 Y
Monthly Avenge Limit:
Monthly
"Vey` 0.079 0 304 0
Dully Maximum
0.079 7.4 0 304 0
Duly Minimum: 0.079 7.4 0 304 0
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2018(October 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 11/08/2018
LCems-' 11/08/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
/ 11/08/2018
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Charlotte,Pace Asheville
CERTIFIED LAB#:5023,12,40
PERSON(s)COLLECTING SAMPLES:Rodney WIllis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PERMIT NO.:NC000S177 PERMIT VERSION:5.0 (�a PERMIT STATUS:Active
\
FACILITY NAME:Lithium Division Plant CLASS:PC-2 1 C C E'VE)�1 :Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis FEBORC CERT NUMBER:28624 RECEIVEp/N�D NR/DWR
D � 02019
GRADE:PC-2 ORC HAS CHANGED:No 2 !fJ,y
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 ',NR' F US:Processed
SECTIO,�+ WORDS
MOOR
ESVILLE REGIONAL
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO OFF
• 50050 00400 C0310 C0530 00300 C0600 C0665 00640 THP3B
I A LA 8 •
C , di Continuous Weekly Monthly 2 X month _ Weekly Quarterly Quarterly Quarterly__ _Monthly _
ct
u I d a Recorder Grab Grab Grab Grab Grab Grab Grab Composite
Y (1
a u F Z FLOW pH DOD-Cow TSB-Cow DO TOTAL N- TOTAL P-C.ae CHLORIDE CLR7DCHV
2400 deck Hn 2400 dock Hn Y/B/N mgd su mg/I mg/I mg/I mg/I mg/1 mg/1 percent
1 N NOFLOW
2 N NOFLOW
3 N HOLIDAY
4 0730 10 Y NOFLOW
5 0730 10 Y NOFLOW
6 0540 10 B NOFLOW
7 0540 10 B NOFLOW
a N NOFLOW
6 N NOFLOW
to 0715 11 Y 0.255 7.33 <2 <2.5 5.73 <0.52 <0.05 23.6
II 0700 11 Y 0.458
12 0700 11 Y 0.458
13 0745 4 Y 0.458
14 0600 2.5 Y 0.458
15 1400 4 Y 0.458
16 0530 5 Y 0.458
17 0730 10 Y 0.459
10 0730 11.5 Y 0.459
16 0730 10 Y 0.468 7.34 6.25
ze 0730 11.5 Y 0.468 >100
21 0600 7.5 Y 0.468
22 N 0.468
23 N 0.468
24 0715 9 Y 0.468
25 0730 9.5 Y 0.468
26 0730 10.5 Y 0.464 7.15 <2.6 6.83
27 0730 3 Y 0.464
2a 0600 10 B 0.464
25 N 0.464
20 N 0.464
Mead y Average Liss: 0.ets 30 30
Maerky Average: 0.45319 0 0 6.27 0 0 23.6 100
Ddy Ma:Imam. 0.468 7.34 0 0 6.83 0 0 23.6 100
Ddl'Rilethewa. 0.255 7.15 0 0 5.73 0 0 23.6 100
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
• 00094
7 ' 8
A L € I Monthly
z
B < F m
$ 8 I Grab
g U
c u F 6' o z cNDUCTVY
2400 dock Hn 2400 dock Hn Y/BIN umhos/cm
1 N NOFLOW
2 N NOFLOW
3 N HOLIDAY
4 0730 10 Y NOFLOW
5 0730 10 Y NOFLOW
6 0540 10 B NOFLOW
7 0540 10 B NOFLOW
8 N NOFLOW
9 N NOFLOW
10 0715 II Y 782
II 0700 11 Y
12 0700 II Y
13 0745 4 Y
14 0600 2.5 Y
15 1400 4 Y
16 0530 5 Y
17 0730 10 Y
10 0730 11.5 Y
19 0730 10 Y 738
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
25 0730 9.5 Y
26 0730 10.5 Y 739
27 0730 3 Y
2e 0600 10 B
29 N
30 N
Monthly Avenge I3mIt
Monthly Avenge: 753
Daily Maximum 782
Dolly Minimum: 738
f eRe No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
30050 00400 C0310 C0530 00300 C0600 C0665 00940 00094
A I� I
d
fiA i Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
I u eI$ u a1 Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
3
aF O O 7Z FLOW pH BOD-Case TSB-Geer DO TOTALN- TOTAL P-Cone CHLORIDE CNDUCIVY
2400 dock Hn 2400 dock Hn Y/B/N 8Pd su mg/I mg/1 mg/1 mg/1 mg/1 mg/I umhos/cm
I N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y 3226 6.71 7.1 17.8 7.59 <0.52 0.074 34.7 750
6 0540 10 B
7 0540 10 B
0 N
9 N
is 0715 11 Y
II 0700 11 Y
12 0700 11 Y
13 0745 4 Y
14 0600 5 Y
15 1400 2.5 Y
16 0530 4 Y
17 0730 10 Y
10 0730 11.5 Y
19 0730 10 Y
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
25 0730 9.5 Y
26 0730 10.5 Y
27 0730 3 Y
20 0600 10 B
29 N
30 N
Monthly Average Limit
Monthly Average: 3226 7.1 17.8 7.59 0 0.074 34.7 750
Dull Ma:imam' 3226 6.71 7.1 17.8 7.59 0 0.074 34.7 750
17a0Yamm' 3226 6.71 7.1 17.8 7.59 0 0.074 34.7 750
aaaa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
e A 8
al ei t
v° 1 I
a a
c •
E.3 IS d' o z
2400 clock Mrs 2400 clock Hn Y/B/N
t N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y
6 0540 10 B
7 0540 10 B
8 N
s N
to 0715 II Y
tt 0700 II Y
12 0700 11 Y
13 0745 4 Y
14 0600 5 Y
15 1400 2.5 Y
16 0530 4 Y
17 0730 10 Y
10 0730 11.5 Y
19 0730 10 Y
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
25 0730 9.5 Y
26 0730 10.5 Y
27 0730 3 Y
28 0600 10 B
29 N
w N
Monthly Avenge Limit:
Monthly Avenge:
Dolly Mailman:
Dolly Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00094 00556
I
1 _ Monthly Monthly Monthly Monthly Quarterly
el$ C$ C$d a 1 Instantaneous Grab Grab Grab Grab
3
I F O O O A FLOW pH US-Con. CNDUCTVY OIL-GRSE
2400 deck Hn 2400 deck Hn YIaIN mgd su mg/I umhos/cm mg/I
I N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y
6 0540 10 B
7 0540 10 B
S N
9 N
10 0715 11 Y
it 0700 II Y
12 0700 11 Y 0.048 6.94 5.7 502
13 0745 4 Y
14 0600 2.5 Y
15 1400 4 Y
ra 0530 5 Y
17 0730 10 Y
IS 0730 11.5 Y
19 0730 10 Y
26 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
25 0730 9.5 Y
26 0730 10.5 Y
.27 0730 3 Y
28 0600 10 B
29 N
30 N
Mea1413 Average Ling:
Manr6ly Average: 0.048 5.7 502
Da117a°® 0.048 6.94 5.7 502
Daily Minimum 0.048 6.94 5.7 502
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:02/12/2019
julL02/06/2019
ORC/Certifier Signature: Rodney Stough Willis [e-mail] fmc.com Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
ZG4-7. 57p 02/12/2019
Permittee/Submitter SSigna ure:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,R&A,Pace,Pace Asheville
CERTIFIED LAB#:5023,14,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

DES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:2.0 STATUS:Processed
Outfall 004-Effluent Comments:
The site received their new NPDES permit during the month of September,last month of the quarter,it was not recognized during the month of September that quarterly oil and
grease analysis had been added to the sampling requirements for outfall 004. Oil and grease was sampled for outfall 004 and analyzed during following month of October.

, .
, .
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active3 1
__
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVED
COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis OCT2 9 2018 ORC CERT NUMBER:28624
l• RI_CEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
—
eDMR PERIOD:09-2018(September 2018) VERSION: 1.0 CEO 'k<LAL FILES DwR N STATUS:Processed
WeRSS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISQI4iJF : 'IONAL OFFICE
• seem N400 C0310 COSM 00300 COON COWS MN TIIPJB
t A 'y Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly< E a 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
3 ey g
A 3 a' AFLOW pH SOD-Cask TSs-Gene DO TOTAL N- TOTAL P-Cwe CHLORIDE CLR7DCHV
2400 deck Hn 2400 deck Her YAWN mgd su mg/1 mg/1 me mg/1 nigh mg/I percent
1 N 0 1
2 N 0
3 N HOLIDAY
4 0730 10 Y 0
5 0730 10 Y 0 ,
O 0540 10 B 0
7 0540 10 B 0
O N 0
f N 0
l0 0715 II Y 0.255 7.33 <2 <2.5 5.73 <0.52 <0.05 23.6
II 0700 II Y 0.458
12 0700 II Y 0.458
13 0745 4 Y 0.458 '
14 0600 2.5 Y 0.458
15 1400 4 Y 0.458 i
IC 0530 5 Y 0.458
17 0730 10 Y 0.459
t0 0730 11.5 Y 0.459 .
If 0730 10 Y 0.468 7.34 6.25
20 0730 11.5 Y 0.468 >100 .
21 0600 7.5 Y 0.468
22 N 0.468
23 N 0.468
24 0715 9 Y 0.468
Lf 0730 9.5 Y 0.468
20 0730 10.5 Y 0.464 7.15 <2.6 6.83
27 0730 3 Y 0.464
2s 0600 10 B 0.464
21 N 0.464
30 N 0.464
MeaMb Avenge I.IeeM: tits 30 30 I
Mouthy Average: 0.328172 .0 0 6.27 0 0 23.6 100
DaVr Maisons:
ua .. 0.468 7.34 0 0 6.83 0 0 23.6 100
Dolly anaw 0 7.15 0 0 5.73 0 0 23.6 100
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

i
i
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION: 1.0 STATUS:Processed
•
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
•
aaos4
8 8
1 A d r Monthly
EGrab
a V t=. p et
A CNDUC VY
2400 dark Iles 2400 dock Hn Y!B/N umhos/cm
1 N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y
6 0540 10 B
•
7 0540 10 B '
a N
0 N
to 0715 II Y 782
11 0700 II Y
12 0700 II V
12 0745 4 Y
1 1
14 0600 2.5 Y I '
IS 1400 4 Y
16 0530 5 V
17 0730 10 V
IS 0730 11.5 Y
If 0730 10 V 738
20 0730 11.5 V
21 0600 7.5 V
22 N
23 N
I
24 0715 9 Y
25 0730 9.5 V
24 0730 10.5 Y 739
27 0730 3 V
Zs 0600 10 B
29 N
30 N
Mw11.1y Avenger Lk.a: '
Muddy Avenge: 753
Dally ns' 782
Daily Makwn: 738
eete No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624 •
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION:1.0 STATUS:Processed
•
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO
• 30050 00400 C0310 C0530 00300 C0600 C0665 00940 00094 •
3t a
2 I
Y
J I. Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly Quarterly
u° 8 1
Instantaneous Grab Grab Grab Grab Grab Grab Grab Grab
u
o u 1OA FLOW pH DOD-Cone Taa-Cane DO TOTALN- TOTALP-Cane CHLORIDE CNDUCTVY
2400 d.ek Hr. 24a11 dank Hn WWI 8Pd su mg/I mg/i mg/I mg/I mg/1 mg/i umbos/cm
1 N
-
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y 3226 6.71 7.1 17.8 7.59 <0.52 0.074 34.7 750
6 0540 10 B
7 0540 10 B
a N
9 N
IS 0715 11 Y
tI 0700 II Y
I2 0700 II Y
13 0745 4 Y
14 0600 5 Y
15 1400 2.5 Y
16 0530 4 Y
17 0730 10 Y
Is 0730 11.5 Y
19 0730 I0 Y
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N i
24 0715 9 Y
25 0730 9.5 Y
26 0730 10.5 Y _
27 0730 3 Y
2a 0600 10 B
29 N
30 N
I Monthly Avenge LBnll:
Man10y Aven8r. 3226 7.1 17.8 7.59 0 0.074 34.7 750
D.IIy Kuhn= 3226 6.71 7.1 17.8 7.59 0 0.074 34.7 750
D.11"1"wn: 3226 6.71 7.1 17.8 7.59 0 0,074 34.7 750
east No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CIIANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 002 NO DISCHARGE*: NO (Continue)
F is F y e
n
e 0S. u 8 t
a 0 3 U
S u 1- 0' i o z
240E cock Hr. 2400 eoek lire V/elN
1 N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y
6 0540 10 B
7 0540 10 B
0 N
9 N
10 0715 II Y
11 0700 I I Y
12 0700 I1 Y
13 0745 4 Y
14 0600 5 Y
10 1400 2.5 Y
16 0530 4 Y
17 0730 10 Y
10 0730 11.5 Y
19 0730 10 Y
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
20 0730 9.5 Y
26 0730 10.5 Y
37 0730 3 Y
28 0600 10 B
29 N
30 N
MeaMy Avenge L4k:
Mmahly Average:
Dilly Muknon:
Daly Mla n an:
•9••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

i
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
YB yy9 30030 00400 C0530 00094 0K54
F i
I S 8ii
Monthly Monthly Monthly Monthly Quarterly
u° s 8 Instantaneous Grab Grab Grab Grab
ce
Uo H o Z FLOW pH T88-Cone CTNDUCTVY OIL-GRSE
2400 deck On 2400 clock Hr. YHYN mgd su mg/1 umhos/cm mg/1
1 N
2 N
3 N HOLIDAY
4 0730 10 Y
5 0730 10 Y
4 0540 10 B
7 0540 10 B
a N .
9 N
1a 0715 II Y
It 0700 II Y
t2 0700 II Y 0.048 6.94 5.7 502
13 0745 4 V
14 0600 2.5 Y
IS 1400 4 V
1s 0530 5 V
17 0730 10 Y
1s 0730 11.5 V
19 0730 10 Y
20 0730 11.5 Y
21 0600 7.5 Y
22 N
23 N
24 0715 9 Y
25 0730 9.5 Y
24 0730 10.5 Y
27 0730 3 V
20 0600 10 B
29 N
30 N
Monthly Avenge Llns:
Monthly Avenge: 0.048 5.7 502
Daily Mulwn: 0.048 6.94 5.7 502
Dray MOhlhenn: 0.048 6.94 5.7 502
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:5.0 PERMIT STATUS:Active
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2018(September 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 10/15/2018
10/09/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] fmc.com Phone 11:704-868-7630 Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit. n
C I��: -4,/
Lq,.♦� 10/15/2018
Permittee/Submiitter ignature:*** Larry A Spickard E-Mail:[e-mail] fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2023
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,R&A,Pace,Pace Asheville
CERTIFIED LAB#:5023,14,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Lance Crayton
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Usc only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there arc no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

3
IT NO.:NC0005177 PERMIT VERSION:4.0 R F C E I\I E E tMIT STATUS:Inactive
TY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis OCT 02 2018 ORC CERT NUMBER: EIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No CENT KAL FILES pp
eDMR PERIOD:08-2018(August 2018) VERSION:2.0 DWR SECTIOTATUS:Processed 1 1 T 8 ?i1.R
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHWW6WILVEgGIONAL OFFICE
50050 00400 C0310 C0530 00300 C0600 C0665 60640 111106
A I-
Y a
II6 t 9 'g' ; Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
gg$ u d I Recorder Grab Grab Grab Grab Grab Grab Grab Composite
8
C C'J F+ g O Zo FLOW pH lOD-Cone TM-Cone DO TOTAL N- TOTAL P-Cone CHLORIDE CP.R7DCHY
2400 dock Hn 2400 clock Hn Y/&N mgd su mg/I mg/1 mg/I mg/I mg/I mg/I percent
I 0730 9.5 Y 0
2 0630 10 Y 0
3 0730 7 Y 0
4 0
5 0
6 0730 9 Y 0
7 0730 8 Y 0
6 0730 9.5 •Y 0
6 0730 9.5 Y 0
t0 0730 9 Y 0
II 0
12 0
13 0745 9.5 Y 0
14 0745 9 Y 0
I5 0715 10.5 Y 0
16 0630 I1 Y 0
17 0715 8.5 Y 0
III 0
0 0
20 0700 10 Y 0
21 0700 11 Y 0
22 0700 10 Y 0
23 0640 10 5 Y 0
24 0645 8 Y 0
25 0
26 0
27 0730 II Y 0
26 0730 10 Y 0
20 0715 II Y 0
36 0730 10 Y 0
31 0730 II Y 0
Monthly Average Limit: 0.615 30 30
Monthly Avenge: 0
Daly Mashsm: 0
Daly MYheem: 0
•et6 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

IT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Inactive
ITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2018(August 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00094
i I 1
iv 7 8 A
8
a £ t 1-1 .1
Monthly
4 u
2. 1 8 Grab
:, g
c u 3 8' 6 o z CNDUGTVY
2400 dodo Hn 2400 dodo Hn Y/B/N umhos/cm
1 0730 9.5 Y
2 0630 10 Y
3 0730 7 Y
4
5
6 0730 9 Y
7 0730 8 Y
8 0730 9.5 Y
9 0730 9.5 Y
10 0730 9 Y
11
12
13 0745 9.5 Y
14 0745 9 Y
15 0715 10.5 Y
16 0630 I1 Y
17 0715 8.5 Y
10
19
28 0700 10 Y
21 0700 11 Y
22 0700 10 Y
23 0640 10.5 Y
24 0645 8 Y
25
26
27 0730 11 Y
20 0730 10 Y
29 0715 11 Y
30 0730 10 Y
J1 0730 II Y
Monthly Avenge Limit:
Monthly Avenge:
Daily Mon mnm:
Daily Minimum:
"9••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

IT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Inactive
ITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2018(August 2018) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00940 00094
o ,� i 1 Monthly Monthly Monthly Quarterly Monthly
8 4
m
u ! ! 8 k Instantaneous Grab Grab Grab Grab
a e a g U
U 8 F° 5 g O Z FLOW pH T5g-Cone CHLORIDE CNDUCPVY
2400 dodo Hn 2400 dodo Hn Y/BIN mgd su mg/1 mg/1 umhos/cm
1 0730 9.5 Y 0.824 7.25 3.7 659
2 0630 10 Y
3 0730 7 Y
5
6 0730 9 Y
7 0730 8 Y
8 0730 9.5 Y
9 0730 9.5 Y
10 0730 9 Y
11
12
13 0745 9.5 Y
14 0745 9 Y
15 0715 10.5 Y
16 0630 11 Y
17 0715 8.5 Y
18
19
20 0700 10 Y
21 0700 11 Y
22 0700 10 Y
23 0640 10.5 Y
24 0645 8 Y
25
26
27 0730 11 Y
28 0730 10 Y
29 0715 II Y
30 0730 10 Y
31 0730 11 Y
Moodily Avenge Limn:
Monthly Avenge: 0.824 3.7 659
Daily Muimam: 0.824 7.25 3.7 659
Daily Minimum: 0.824 7.25 3.7 659
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

IT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Inactive
ITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2018(August 2018) VERSION:2.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:09/27/2018
£ 11, 111/4-115 09/27/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
I
C' �'� '✓S�_ 09/27/2018
Permittee/Submitter Signature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Lithium
CERTIFIED LAB#:5023
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 RECEIVED PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis AUG 2 9 2018 ORC CERT NUMBER:iggEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:NoCENTIv\L FILES
eDMR PERIOD:07-2018(July 2018) VERSION:1.0 OVVR SECTION STATUS:Processed S E P . 4 2018
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCRIABCWILLYUgGioNAL OFFICE
• 50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
A I
I '' Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
ue 3` 8 . Recorder Grab Grab Grab Grab Grab Grab Grab Composite
i 1
T U 1O Z FLOW pH BOD-Coat T88-Cane DO TOTAL N- TOTAL P-Cone CHLORIDE CER7DCHV
2400 deck Hn 2400 dodo Hn Y/B/N mgd su mg/I mg/I mg/I mg/I mg/I mg/I percent
1
2 0600 10 B
3 0700 9.5 Y
4 N HOLIDAY
3 0715 10.5 Y
4 0730 9 Y
7 N
0 N
9 0730 10 Y
t0 1000 10 Y
tl 0730 10 Y
12 0730 10 Y
13 0730 10 Y
14 N
15 N
16 0730 8 Y
17 0700 10 Y
18 0700 10.5 Y
19 0730 11.5 Y
20 0730 9.5 Y
21 N
22 N
23 0730 9.5 Y
24 0730 9.5 Y
25 0745 8 Y
24 0600 10 B
27 0600 10.5 B
20 N
29 N
30 0545 11 B
31 0545 8 B
Monthly Avenge Limit: 0.615 30 30
Meathy Avenge:
Daily Maahaam:
Daily Mioletam:
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2018(July 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00004 TGP3B
Ili
6 j i i Monthly Quarterly
Grab Grab
:O.g' I I i p�O A CNDUCTVY CERI7DPF
2400 dock Hn 2400 clack Hn Y/B/N umhos/cm pass/fail
1
2 0600 10 B
3 0700 9.5 Y
4 N HOLIDAY
5 0715 10.5 Y
4 0730 9 Y
7 N
s N
f 0730 10 Y
to 1000 10 Y
II 0730 10 Y
12 0730 10 Y
13 0730 10 Y
14 N
15 N
16 0730 8 Y
17 0700 10 Y
II 0700 10.5 Y
is 0730 11.5 Y
ri 0730 9.5 Y
21 N
22 N
23 0730 9.5 Y
24 0730 9.5 Y
25 0745 8 Y
24 0600 10 B
27 0600 10.5 B
28 N
25 N
30 0545 11 B
31 0545 8 B
MosIhly Avenge Galt
Monthly Avenge:
Daly Minims:
Daly M elo:
aaae No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2018(July 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00406 COSJO 00940 00094
A qqg 3 A
Y F
21 8
eC . 1 Monthly Monthly Monthly Quarterly Monthly
2 d g Instantaneous Grab Crab Grab Grab
us 1 S U [3+ S a ai
O Z4 FLOW pH IRS-Cove CHLORIDE CNDUCI VY
2400 dock Hn 2400 check Hn Y/a1N mgd su mg/I mg/1 umhos/cm
1
2 0600 10 B
3 0700 9.5 Y
4 N HOLIDAY
5 0715 10.5 Y
6 0730 9 Y
y N
8 N
9 0730 10 Y
10 1000 10 Y
II 0730 10 Y
12 0730 10 Y
13 0730 11 Y
14 N
15 N
16 0730 8 Y
17 0700 10 Y
18 0700 10.5 Y
19 0730 11.5 Y
20 0730 9.5 Y
21 N
22 N
23 0730 9.5 Y
24 0730 9.5 Y
25 0915 0745 9 Y 1.122 7.25 <2.6 24.8 739
26 0600 10 B
27 0600 10.5 B
28 N
29 N
3O 0545 II B
31 0545 8 B
Monthly Avenge Limit:
Monaty Avenge. 1.122 0 24.8 739
Deny Mulaome 1.122 7.25 0 24.8 739
Daily Minimum: 1.122 7.25 0 24.8 739
esse No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2018(July 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:08/21/2018
Rk,Witit
08/21/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
lti 08/21/2018
Permittee/5ubmitter ignature:*** Larry A Spickard E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PERMIT NO.:NC0005I77 PERMIT VERSION:4.0 PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVE EYUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:286
GRADE:PC-2 ORC HAS CHANGED:No J U L 2 4 2018 ECEIVED/NCDENR/DWR
eDMR PERIOD:06-2018(June 2018) VERSION:1.0 CEN I KAL EILEgTATUS:Processed , '} 'i•;
DWR SECTION
QROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARIGFAVINpREGIONAL OFFICE
NON «oa C0310 C0530 tu3COMPa CO CONS 000M THP3B
A 1 aYY
< F I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u 8 E 8 ct Recorder Grab Grab Grab Grab Grab Grab Grab Composite
7g pUG
Oy u F 1 I. 0 L FLOW pH a00-Cow T9a-Coot DO TOTAL N- TOTAL P-Com CHLORIDE CER7DCHV
2400 dock Hn 2400 clock Hn Y1em mgd su mg/I mg/I mg/I mg/I mg/I mg/I percent
I 0730 9 Y 0.422
2 0.422
3 0.422
4 0700 II Y 0.422
5 0700 9 Y 0.422
6 0811 0700 11.5 Y 0.425 8.27 <2 <2.7 7.03
7 0715 4.5 Y 0.4
a 0600 10 B 0.416
9 0.416
10 0.416
11 0730 11.5 Y 0.416
12 0730 10 Y 0.416
13 0904 0730 11 Y 0.409 8.05 6.22
14 0730 11.5 Y 0.409
IS 0730 9.0 Y 0.409
I6 0.409
17 0.409
IS 0730 11.5 Y 0.409
19 0730 9.5 Y 0.409
20 1005 0730 10 Y 0.403 8.17 <2.8 7.47
21 0730 9.5 Y 0.403
22 0730 9 Y 0.403
23 0.403
24 0.403
25 0730 12 Y 0.403
26 0730 II Y 0.403
37 0845 0730 10 Y 0.151 8.12 6.6
20 0730 11.5 Y 0
25 0600 10 B 0
30 0
Monday Average Lilt: 0.615 30 30
Maetkly Average. 0.361667 0 0 6.83
MathesonDolly 0.425 8.27 0 0 7.47
Dolly Mbr= 0 8.05 0 0 6.22
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2018(June 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00494
A t
2� 8
C .1 Monthly
<
g 8 F
a Grab
G U Fo O 1 O Z CNDUCTVY
2400 dock Hn 2400 deli Hn Y/a/N umhos/cm
I 0730 9 Y
2
l
4 0700 11 Y
S 0700 9 Y
6 0811 0700 11.5 Y 826
7 0715 4.5 Y
O 0600 10 B
9
10
11 0730 11.5 Y
12 0730 10 Y
13 0904 0730 Il Y
14 0730 11.5 Y
13 0730 9.0 Y
16
17
18 0730 11.5 Y
19 0730 9.5 Y
20 1005 0730 10 Y
21 0730 9.5 Y
22 0730 9 Y
23
24
2s 0730 12 Y
26 0730 11 Y
27 0845 0730 10 Y
28 0730 11.5 Y
29 0600 10 B
le
Monthly Avenge Limit:
Mouthy Avenge: 826
Daily Mazimam: 826
Daily Minima.: 826
*00*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2018(June 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 30050 00400 C0530 00940 00094
3 F I A
g d
6 A I 1 Monthly Monthly Monthly Quarterly Monthly
Iua Id k Instantaneous Grab Grab Grab Grab
AO x mow OH 72t8-Cone CHLORIDE CNDUCTYY
2400 deck Her 2490 clock Hn YIB/H mgd su mg/I mg/I umhos/cm
1 0730 9 Y
2
3
4 0700 II Y
5 0700 9 Y
6 0824 0700 11.5 Y 0.177 7.58 <2.5 709
7 0715 4.5 Y
8 0600 10 B
9
10
11 0730 11.5 Y
12 0730 10 Y
13 0730 II Y
14 0730 11.5 Y
IS 0730 9 Y
16
17
18 0730 11.5 Y
19 0730 9.5 Y
20 0730 10 Y
21 0730 9.5 Y
22 0730 9 Y
23
24
25 0730 12 Y
26 0730 11 Y
27 0730 10 Y
28 0730 11.5 Y
20 0600 10 B
30
'Monthly Avenge Limit
Monthly Avenge. 0.177 _0 709
Daily Maximum 0.177 7.58 0 709
Dolly Minlemm: 0.177 7.58 0 709
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2018(June 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:07/12/2018
' 1 Ii
07/12/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
1/{(t'LeijR(."-- 1/1"1/4/ 07/12/2018
Permittee/Submitter Signature:*** l Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per I5A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2018(June 2018) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
First week monitoring for pH,and DO,completed on May 30th

ES PERMIT NO.:NC0005I77 PERMIT VERSION:4.0 R r PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 l I VEDCOUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis JUL 0$ z018 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No-CE RECEIVEpMCDENR/DWR
eDMR PERIOD:05-2018(May 2018) VERSION: 1.0N I KNL. FILES STATUS:Processed
DWR SECTION
JUL 9 2018
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARR��iO
MOORESVILLE REGIONAI.OFFICE
• 58058 MIN c0318 Co538 MN CONN COK5 00948 THP3B
A 1 a •
1 I € Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
I ¢ 4 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
u d
u F a$ Ze PLOW pH BOD-Can T99-Can DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DCHV
Mt dock Ms 7.489 slack Hn Y/BIN mgd su mg/I mg/ me mg/I mg/I mg/I percent .
I 0730 IO Y 0.436
2 1000 0730 8.5 Y 0.436 8.15 <2 <5 8.92
3 0700 8.5 Y 0.438
4 0730 8.5 Y 0.438
s 0 N 0.436
a 0 N 0.435
7 0745 7 Y 0.435
e 0730 9 Y 0.435
9 0920 0730 6 Y 0.445 8.24 8.21
II 0730 9 Y 0.443
It 0730 7 Y 0.442
12 0 N 0.438
13 0 N 0.435
14 0730 9 Y 0.431
15 0730 8 Y 0.432
19 0905 0730 Il Y 0.435 8.32 <2.6 8.11
17 0700 9 Y 0.431
18 0600 10 B 0.426
I9 0 N 0.423
2• 0 N 0.423
21 0730 9.5 Y 0.423
22 0730 10 Y 0.425
23 0845 0730 8 Y 0.419 8.11 8.03
24 0700 9.5 Y 0.419
25 0600 10 B 0.419
24 0 N 0.418
27 0 N 0.418
n 0 N HOLIDAY
29 0715 10.5 Y 0.418
38 0915 0730 8 Y 0.415 7.96 7.42
31 0600 10 B 0.416
blesahly Avenge Ian& „is 38 38
fib'Arnow 0.429433 0 0 8.138
Daly Ma`ima 0.445 8.32 0 0 8.92 •
Daly atrv= 0.415 7.96 0 0 7.42
sts«No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2018(May 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
NON
1 •
a
l 4 Monthly
e a GrabI u I 1i ffi A CNDUCTVY
MI deck Hee 24011 deck firs Y/B/N umhos/cm
1 0730 10 Y
2 1000 0730 8.5 Y 832
3 0700 8.5 Y
i 0730 8.5 Y
3 0 N
f 0 N
7 0745 7 Y
a 0730 9 Y
9 0920 0730 6 Y
I. 0730 9 Y
II 0730 7 Y
12 0 N
13 0 N
14 0730 9 Y
13 0730 8 Y
19 0905 0730 11 Y
17 0700 9 Y
1a 0600 10 B
If 0 N
z• 0 N
21 0730 9.5 Y
22 0730 10 Y
23 0845 0730 8 Y
24 0700 9.5 Y
L+ 0600 10 B
0 N
27 0 N
m 0 N HOLIDAY
2f 0715 10.5 Y
39 0915 0730 8 Y
31 0600 10 B
Me.ay Average tilt
McNY1y Average: 832
Daily Mesteaoi 832
wilyMVve= 832
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2018(May 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
.0400 Cow 00940 00e5 t
•
A 1! i
S 3 Monthly Monthly Monthly Quarterly Monthly
d . Instantaneous Grab Grab Grab Grab
I
puG ai
1 C. f p i FLOW pH TSB-Cow CHLORIDE CNDUCTVY
24N clack Hn 2490 cluck Hn Y/B/N mgd su mg/I mg/ umhos/cm
I 0730 10 Y
2 0730 8.5 Y 0.177 6.92 2.7 822
3 0730 8.5 Y
4 0730 8.5 Y
5 N
6 N
7 0745 7 Y
e 0730 9 Y
t 0730 6 Y
R 0730 9 Y
II 0730 7 Y
12 N
13 N
14 0730 9 Y
15 0730 8 Y
16 0730 11 Y
17 0700 9 Y
19 0600 10 B
15 N
20 N
21 0730 9.5 Y
u 0730 10 Y
23 0730 8 Y
24 0700 9.5 Y
25 0600 10 B
20 N
27 N
20 N HOLIDAY
20 0715 10.5 Y
A 0730 8 Y
31 0600 10 B
NUalY4 Average LYN
NoNbly"Vey 0.177 2.7 822
Daly Mulws 0.177 6.92 2.7 822
Daily 1111Noma
0.177 6.92 2.7 822
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:Fmc Lithium USA Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2018(May 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant ' CONTACT PHONE#:[phone] SUBMISSION DATE:06/25/2018
L.).
a.._ 1���✓. 06/22/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit. 4, , ..e.A..........
06/25/2018
Permittee/Submitter Signature:*** ichael aul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
'FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

,TNO.:NC0005
177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ME:LithiumDivisionPlant CLASS:PC-2 RECEIVED COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willi�l f i 2018 ORC CERT NUMBER:re6 NEDMCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No N 0 1 Y pp
eDMR PERIOD:04-2018(April 2018) VERSION: 1.0 CENTRAL FILES STATUS:Processed J l�N L I 201(1
DWR SECTION
WOROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC �L GIONAL OFFICE
• 30054 N400 C0314 C0530 00300 COON C0665 00840 THP3B
3
1; 8 ;
I. < m I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
g4 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
I
i a
S d 1 1 1 O Lo FLOW pH SOD-Cone TM-Can DO TOTAL N- TOTAL P-Cone CHLORIDE CER7DCHV
2400 dodo Hn 2404 dock tin Y/B/N mgd su mg/1 mg/I mg/I mg/I mg/I mg/I percent
1 N NOFLOW
2 0700 12 B NOFLOW
3 0730 9 Y NOFLOW
4 0730 9 Y NOFLOW
5 0730 8.5 Y NOFLOW
6 0645 10 Y NOFLOW
7 N NOFLOW
a N NOFLOW
9 0730 9 Y NOFLOW
re 0730 9 Y 0.39
11 0921 0715 9 Y 0.454 8.05 <2 <5 10.28 <0.52 <0.05 42.9
12 0730 9 Y 0.452
13 0700 9 Y 0.451
14 N 0.449
15 N 0.446
16 0730 8 Y 0.445
17 0730 8.5 Y 0.452
10 0730 8 Y 0.456 8.16 9.34
19 0730 10 Y 0.455 >100
20 0715 9 Y 0.454
21 N 0.449
22 N 0.449
23 0730 9 Y 0.449
24 0715 9.5 Y 0.449
25 0730 12 Y 0.449 8.16 <2.5 8.86
26 0730 10 Y 0.449
27 0600 10 B 0.445
28 N 0.445
29 N 0.445
30 0730 9 Y 0.445
Moodily Avenge Llolt: 0.615 30 30
Mad61y Average: 0.446571 0 0 9.493333 0 0 42.9 100
Dolly Maximo= 0.456 8.16 0 0 _10.28 0 0 42.9 100
D+BYhann' 0.39 8.05 0 0 8.86 0 0 42.9 100
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2018(April 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094 TGP3B
F
t I I Monthly Quarterly
18 Grab Grab
y u
t] u' Ir i d O Zo CNDUCIYY CERI7DPF
2400 dud: Hn 2404 do& Hn Y/B/H unthos/cnt pass/fail
I N NOFLOW
2 0700 12 B NOFLOW
3 0730 9 Y NOFLOW
4 0730 9 Y NOFLOW
5 0730 8.5 Y NOFLOW
6 0645 10 Y NOFLOW
7 N NOFLOW
8 N NOFLOW
9 0730 9 Y NOFLOW
II 0730 9 Y
II 0921 0715 9 Y 842
12 0730 9 Y
13 0700 9 Y
14 N
15 N
16 0730 8 Y
17 0730 8.5 Y
II 0730 8 Y
19 0730 10 Y
28 0715 9 Y
21 N
22 N
23 0730 9 Y
24 0715 9.5 Y
25 0730 12 Y
26 0730 10 Y
27 0600 10 B
28 N
29 N
38 0730 9 Y
Moodily Avenge Limit:
Meathy Average: 842
Rally Maximum: 842
Deny Mio600m: 842
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2018(April 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50039 00400 C0530 00940 - 00094
A A A
a ;
9 '� a 1 Monthly Monthly Monthly Quarterly Monthly
u° `I i 8 Instantaneous Grab Grab Grab Grab
a s a
d Uo Fo 1 O I. FLOW pH 7Ba-Cone CHLORIDE CNDUCIVY
2.409 deck Hn 2400 dodk Hn Y/BIH mgd su mg/I mg/I umhos/cm
I N
2 0700 12 B
3 0730 9 Y
4 0922 0730 9 Y 0.222 6.67 <5.3 31.5 1012
5 0730 8.5 Y
4 0645 10 Y
7
0
9 0730 9 Y
t9 0730 9 Y
11 0715 9 Y
12 0730 9 Y
13 0700 9 Y
14
15
16 0730 8 Y
17 0730 8.5 Y
IS 0730 8.0 Y
19 0730 10.0 Y
20 0715 9 Y
21
22
23 0730 9 Y
24 0715 9.5 Y
25 0730 12 Y
26 0730 10 Y
27 0600 10 B
29
29
30 0730 9 Y
Monthly Avenge Limit:
Monthly Average: 0.222 0 31.5 1012
Daily Minimum 0.222 6.67 0 31.5 1012
Dilly Minimum: 0.222 6.67 0 31.5 1012
eeie No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2018(April 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:05/17/2018
L _j, j_2.._.%
05/15/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
161
dL V 05/17/2018
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis,Thomas Lewis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2018(April 2018) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Began discharge for month on 4/10/18

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 RE
C E i /,�ii IT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 1 � 6 . TY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis MAY 01 2O1SIC CERT NUMBER:280,ECENED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No CEN I hU\L FI l C;;
eDMR PERIOD:03-2018(March 2018) VERSION: 1.0 DWR SECTIC�9ATUS:Processed
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHAVWPYVE§EGIONAL OFFICE
y 5603E 00400 C0310 C0530 00300 C0600 WPM 00 THP3B
9
1� aY :
I < F Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
c$ d k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
i i a
0 U F O Z W pH BOO-Cone T88•Cone DO TOTAL N- TOTAL P-Cow CHLORIDE CER7DCHV
2400 dock Hra 2400 dadr Hn Y/BIN mgd su mg/1 mg/I mg/1 mg/i mg/I mg/ percent
I 0700 9.5 Y
2 0600 10 B
3 0 N
4 0 N
5 0715 9 Y
6 0730 9 Y
7 0715 10.5 Y
0 0730 II Y
9 0645 9 Y
10 0 N
11 0 N
12 0545 14 B
13 0545 13 B
14 0545 12.5 B
15 0545 12 B
16 0545 12 B
17 0 N
18 0 N
19 0730 8.5 Y
20 0745 8.5 Y
21 0730 9 Y
22 0715 9.5 Y
23 0730 9.5 Y
24 0 N
25 0 N
26 0730 9.5 Y
27 0700 8.5 Y
28 0700 9.5 Y
29 0730 9.0 Y
30 0 N HOLIDAY
31 0 N
Moodily Avenge Lie*: 0.615 30 30
Monthly Average:
Daly Madman:
Daly Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2018(March 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00094
I I. I
8 a Monthly
e g
I
u 8 d Grab
s a
C U F% O o L CNDUCTVY
2400 dodo Hn 2400 deck Hn Y/BIN umhos/cm
I 0700 9.5 Y
2 0600 10 B
3 0 N
4 0 N
5 0715 9 Y
6 0730 9 Y
7 0715 10.5 Y
8 0730 11 Y
9 0645 9 Y
18 0 N
II 0 N
12 0545 14 B
13 0545 13 B
14 0545 12.5 B
15 0545 12 B
16 0545 12 B
17 0 N
15 0 N
19 0730 8.5 Y
28 0745 8.5 Y
21 0730 9 Y
22 0715 9.5 Y
23 0730 9.5 Y
24 0 N
25 0 N
26 0730 9.5 Y
27 0700 8.5 Y
28 0700 9.5 Y
29 0730 9.0 Y
30 0 N HOLIDAY
31 0 N
Monthly Avenge Unit:
Monthly Avenge:
Deily Ma:lmum:
Daily Medawar
•"•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2018(March 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50090 00400 C0530 00946 00094
A I I a
6 < m Monthly Monthly Monthly Quarterly Monthly
7u7 2 0 a Instantaneous Grab Grab Grab Grab
a 3
O u F O Z FLOW pH TES-Cone CHLORIDE CNDUCTYY
2400 d..k Hn 2400 dock Hn EDEN mgd su mg/1 mg/1 umhos/cm
1 0700 9.5 Y
2 0600 10 B
3 0 N
4 0 N
5 0715 9 Y
a 0730 9 Y
7 0917 0715 10.5 Y 0.86 6.81 <2.6 1071
a 0730 11 Y
9 0645 9 Y
10 0 N
11 0 N
12 0545 14 B
13 0545 13 B
14 0545 12.5 B
15 0545 12 B
16 0545 12 B
17 0 N
1n 0 N
19 0730 8.5 Y
20 0745 8.5 Y
21 0730 9 Y
22 0715 9.5 Y
23 0730 9.5 Y
24 0 N
25 0 N
24 0730 9.5 Y
27 0700 8.5 Y
28 0700 9.5 Y
29 0730 9 Y
30 0 N HOLIDAY
31 0 N
Monthly Average Limit
Monthly Avenge` 0.86 0 1071
D•ar Mnle•tm. 0.86 6.81 0 1071
Daily Minimum 0.86 6.81 0 1071
*5*0 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2018(March 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:04/23/2018
G,. L1 -.-- 04/23/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
tract 't k 04/23/2018
Permittee/Submitter Signature:*** ichael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

: R/DWR
PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 pp COUNTY:Gaston DECEIVED/N
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis R I\/ RC CERT NUMBER:28624N
GRADE:PC-2 ORC HAS CHANGED:No APR 0 4 2 018R APR 0 9 2 018
eDM PERIOD:02-2018(February 2018) VERSION:1.0 STATUS:Processed
r MOORESVIL WORDS
r '�V :E.,"`7iO.i•.' LE RE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES GIONAL oFFICE
• 58050 00400 C0310 C0530 00300 C0600 C0645 00940 THP3B
At F 8
8I
9 y i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u' Q$8 d . Recorder Grab Grab Grab Grab Grab Grab Grab Composite
pub of
u 12 O O Z FLOW PH BOD-Cow TSS-Case DO TOTAL N- TOTAL P-Cow CHLORIDE CERSDCFIV
24M deck Hn 2400 dock Hre V/BIN mgd su mg/I mg/I mg/I mg/I mg/I mg/I percent
t 0730 9 Y
2 0730 9 Y
3 0 N
4 0 N
5 0730 9 Y
6 0730 9 Y
7 0745 9.5 Y
8 0730 9 Y
9 0715 8 Y
me 0 N
II 0 N
12 0730 6 Y
13 0600 11 B
14 0600 11 B
15 0745 9 Y
16 0715 9 Y
17 N
18 N
19 0730 9 Y
20 0730 9 Y
21 0830 7 Y
22 0700 12 B
23 0730 9.5 Y
24 N
25 N
26 0715 9.5 Y
27 0730 9 Y
20 0700 11.5 Y
M..tky A.M.Link: 0.61s 30 30
Monty Average:
Nay Meet
Daily Minims:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2018(February 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
a
6 ) i 1� Monthly
u = a gk
Crab
a u
d I F o CNDUCIVY
2400 dock Hn 240e dock Hn Y/9/N umhos/cm
I 0730 9 Y
2 0730 9 Y
3 0 N
4 0 N
5 0730 9 Y
4 0730 9 Y
7 0745 9.5 Y
0 0730 9 Y
6 0715 8 Y
I. 0 N
11 0 N
12 0730 6 Y
13 0600 11 B
14 0600 11 B
tS 0745 9 Y
14 0715 9 Y
17 N
IS N
to 0730 9 Y
20 0730 9 Y
21 0830 7 Y
22 0700 12 B
23 0730 9.5 Y
24 N
25 N
24 0715 9.5 Y
27 0730 9 Y
26 0700 11.5 Y
MenHly Avenge L111:
M.IhIy Avenge:
Daily Maximum:
Deny MYimam:
Me"No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2018(February 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00940 00094
Bi 1 A
4 e e I! Monthly Monthly Monthly Quarterly Monthly
r 8 3 Instantaneous Grab Grab Grab Grab
a 3 c$ pub
S G Fe ! O o< £ FLOW pH TES-Cam CHLORIDE CNDUCIVY
2400 deck Hrs 2400 dear it., Y/B/N mgd su mall mg/1 umhos/cm
I 0730 9 Y
2 0730 9 Y
3 N
4 N
5 0730 9 Y
4 0730 9 Y
7 0745 9.5 Y 1.084 6.77 10.8 36.2 819
0 0730 9 Y
9 0715 8 Y
10 N
II N
12 0730 6 Y
13 0600 11 B
14 0600 11 B
15 0745 9 Y
10 0745 9 Y
17 N
10 N
19 0730 9 Y
20 0730 9 Y
21 0830 7 Y
22 0700 12 B
23 0730 9.5 Y
24 N
25 N
20 0715 9.5 Y
27 0730 9 Y
20 0700 11.5 Y
Monthly Avenge Limit:
Monthly Average: 1.084 10.8 36.2 819
Daily Ma han=_1.084 6.77 10.8 36.2 819
Daily M . 1.084 6.77 10.8 36.2 819
"'I'No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2018(February 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:03/22/2018
i - t t ) J -y 03/22/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
4
03/22/2018
1t.'e1Lc_l
Permittee/Submitter Signature: ** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Charlotte,Pace Ashville
CERTIFIED LAB#:5023,12,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per I5A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2018(February 2018) VERSION: 1.0 STATUS:Processed
Outfit!!004-Effluent Comments:
Representative Storm Sampling Event

3
DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 L G PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVED IVED COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis MAR Q a 2018 ORC CERT NUMBER:28 24C EIVEDNCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2018(January 2018) VERSION: 1.0 CENTRAL,FILES STATUS:Processed
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHkSti;LU ONAL OFFICE
50050 00400 C0310 C0430 003110 C0000 C0665 00944 TIIP311
I a •
A S i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
1 eu d d $ Recorder Grab Grab Grab Grab Grab Grab Grab Composite
g u of
aF, g. FLOW pH DOD-Cape T8S•Csae DO TOTAL N- TOTAL P-Ceae CHLORIDE CER7DC7rV
2400edod: He. 2400eleek Hen YHVH mgd su mg/I mg/I mg/I mg/I mg/ mg/I percent
1 N HOLIDAY
2 0845 8 Y
3 0745 9 Y
4 0730 8.5 Y
5 0740 8 Y
4 N
7 N
8 0730 8.5 Y
9 0745 8.5 Y
to 0730 10 Y ,
tl 0730 8.5 Y
12 0730 8.5 Y
13 N
14 N
IS N HOLIDAY
16 1100 5 Y
17 0830 8 Y
10 0800 8.5 Y
19 0800 9 Y
20 N
31 N
22 0745 8.5 Y
23 0730 8.5 Y
34 0745 9 Y
35 0730 8 Y
20 0715 8.5 Y
27 N
is N
29 0700 8.5 Y
30 0700 5 Y
31 0730 7 Y
,
M.th. ly Army Lb*: e.015 30 .10
Mualhly Avenge:
Dully Maximum
Day MYram:
o***No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-lloliday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2018(January 2018) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
A 1 00094 TGP3B
I 14 1
A iL C A Monthly Quarterly
S. u• 8 ! es a Grab Grab
a apur a
a U tg O Z CNDUCTVY CERI7DPF
2400 clock Hn 2400e1aek Hn Y/BIN umhos/cm pass/fail
I N HOLIDAY
2 0845 8 Y
3 0745 9 Y
4 0730 8.5 Y
s 0740 8 Y
6 N
7 N
a 0730 8.5 Y
9 0745 8.5 Y
10 0730 10 Y
II 0730 8.5 Y
12 0730 8.5 Y
13 N
14 N
13 N HOLIDAY
16 1100 5 Y
17 0830 8 Y
Ia 0800 8.5 Y
19 0800 9 Y
20 N
21 N
22 0745 8.5 Y
23 0730 8.5 Y
24 0745 9 Y
23 0730 8 Y
26 0715 8.5 Y
27 N
2a N
29 0700 8.5 Y
30 0700 5 Y
31 0730 7 Y
Monthly Avenge Unlit
Monthly Avenge•.
Daily Maximum:
Daily MMIa.m:
•et•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather. NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2018(January 2018) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
.50050 00400 C0530 00840 RIMA I A
Y I P 3 8
fit j y Monthly Monthly Monthly Quarterly Monthly
a E 3 8 k Instantaneous Grab Grab Grab Grab
0
tS U' Fe $ O i FLOW pH TES-Cone CHLORIDE CNDUCTVY
2400 duck Hr. 2400 deck Hrs Y/BIN mgd su mg/I mg/I umhos/cm
I N HOLIDAY
2 0845 8 Y
3 0745 9 Y 0.135 6.85 <2.7 66.8 1414
4 0730 8.5 V
a 0740 8 V
4 N
7 N
O 0730 8.5 Y
f 0745 8.5 Y
to 0730 10 Y
II 0730 8.5 Y
12 0730 8.5 Y
13 N
14 N
15 HOLIDAY
16 1100 5 Y
17 0830 8 Y
It 0800 8.5 V
If 0800 9 Y
20 N
21 N
22 0745 8.5 Y
23 0730 8.0 Y
24 0745 9 Y
25 0730 8.0 Y
26 0715 8.5 Y
27 N
20 N
28 0700 8.5 Y
30 0700 5 Y
J1 0730 7 Y
M.nmly Avenge Limit
Monthly Avenge: 0.135 0 66.8 1414
Daily Maximum 0.135 6.85 0 66.8 1414
Daily Minimum 0.135 6.85 0 66.8 1414
e tc*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2018(January 2018) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:02/26/2018
LL-4 ; 02/20/20I8
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permitter became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permitter becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 1I.E.6 of
the NPDES permit.
, ./44.)jurttl
02/26/2018
Permittee/Submitter Signature:*** Mic ael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the infonnation submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace
CERTIFIED LAB#:5023,40
I'ERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there arc no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per I5A NCAC 213
.0506(b)(2)(D).

MIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston 3
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
RECEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2017(December 2017) VERSION:1.0 STATUS:Processed !
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGEoR 4LE REGIONAL OFFIC
50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
3 ll A A
3i 1 I. 8
6 AA 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u d 8` 8 . Recorder Grab Grab Grab Grab Grab Grab Grab Composite
8 1 1 1 a
S d F' O Z FLOW PH ROD-Cane Tab-Cone DO TOTAL N- TOTAL P-Cent CHLORIDE CER7DCHV
2400 dock Hrs 2400 data Hn Y/BIN mgd su mg/I mg/I mg/I mg/I mg/ mg/I percent
I 0730 8 Y
2 N
3 N
4 0730 8 Y
5 0730 8 Y
4 0730 8 Y
7 0730 6 Y
a 0730 8 Y
9 N
t0 N
It 0730 11 Y
'
12 0730 10 Y
13 0730 1I Y
14 0745 9 Y
15 0700 12 B
16 N
17 N
IS 0730 9 Y
19 0600 11.5 Y
20 0730 9.5 Y
21 0600 12 B
22 N HOLIDAY
23 N
24 N
25 N HOLIDAY
26 1000 12 B
27 0730 8 Y
26 0745 9 Y
29 0720 8 Y
30 N
31 N
Monthly Average Lima: 0.615 30 30
,MeanlyMeanlyAverage:
Daily Maximum:
-Daily Minimum:
4i*0 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2017(December 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
e0094
1 P I
A 21 8 ;
as 6 e i ? Monthly
u s` 18 8 Grab
a 1 'a cy
S 8 5 b• o z UCIVY
2400 clock Hn 2400 clock Hn Y/B/N umhos/Cm
1 0730 8 Y
2 N
3 N
4 0730 8 Y
3 0730 8 Y
6 0730 8 Y
7 0730 6 Y
8 0730 8 Y
0 N
10 N
11 0730 11 Y
12 0730 10 Y
13 0730 II Y
14 0745 9 Y
13 0700 12 B
16 N
17 N
18 0730 9 Y
19 0600 11.5 Y
20 0730 9.5 Y
21 0600 12 B
22 N HOLIDAY
23 N
24 N
2.a N HOLIDAY
26 1000 12 B
27 0730 8 Y
28 0745 9 Y
29 0720 8 Y
30 N
31 N
Monthly Average Lora:
Monthly Avenge:
Daily Maximum:
Daily M1a`am:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2017(December 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 • 00400 C0530 00940 00094
3 i
I9 11 I 1 Monthly Monthly Monthly Quarterly Monthly
u° 3` B $ Instantaneous Grab Grab Grab Grab
a a € a a m
G u F 5 g O A FLOW pH T30-Cone CHLORIDE CNDUCINY
2400 dock Hn 2400 dock Hn Y/a/N mgd su mg/I mg/I umhos/cm
I 0730 8 Y
2 N
3 N
4 0730 8 Y
5 0730 8 Y
4 0730 8 Y
7 0730 8 Y 0.115 7.07 <2.6 38.4 1128
0 0730 8 Y
9 N
10 N
II 0730 II Y
12 0730 10 Y
13 0730 11 Y
14 0745 9 Y
15 0700 12 B
16 N
17 N
IS 0730 9 Y
19 0600 11.5 Y
20 0730 9.5 Y
21 0600 12 B
22 N HOLIDAY
23 N
24 N
25 N HOLIDAY
26 1000 12 B
27 0730 8 Y
20 0745 9 Y
29 0720 8 Y
30 N
31 N
Monthly Average Limit:
Monthly Mengel 0.115 0 38.4 1128
Daly 04a:lowm: 0.115 7.07 0 38.4 1128
Daily INtnheam: 0.115 7.07 0 38.4 1 128
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2017(December 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:01/24/2018
W� 01/23/2018
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
A4W *)Q"`j
r / 01/24/2018
v
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Chralotte,Pace Ashville
CERTIFIED LAB#:5023,12,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2017(December 2017) VERSION: 1.0 STATUS:Processed
Outfall 004-Effluent Comments:
Sample collected during Representative Storm Event.

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R P7 ,F I\/F C�UNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis JAN 0 9 2018 ORC CERT NUMBER: EIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2017(November 2017) VERSION: 1.0 MVP.SECTION STATUS:Processed �'N t 6 L ii l t,
►M,ORMATION PROCESSING UNIT •
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCF :� TF�GIONAL OFFICE
�
50050 00400 C0310 C0530 00300 C0600 C0665 0000 THPSB
A l a •
:
AA i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
$ 2 2 8 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
1. a
G F O Zo FLOW pH BOD-Can TOS-Cone DO TOTAL N• TOTAL P-Gene CHLORIDE CER7DCHY
2400 clack Hn 2400 dock Hn Y/B/N mgd su mg/1 mg/I mg/1 mg/I mg/I mg/1 percent
1 0600 8 B 0.429
2 0600 8 B 0.432
3 0600 8 B 0.436
4 N 0.432
5 N 0.432
6 0730 8 Y 0.432
7 0730 8 Y 0.432
8 0700 8 Y 0.428 7.42 6.5 <2.7 8.13
9 0730 8 Y 0.432
t6 0700 8 Y 0.425
tt N 0.425
12 N 0.425
13 0730 8 Y 0.42
14 0600 8 B 0.42
IS 0700 8 Y 0.42 7.3 7.98
16 0745 8 Y 0.419
17 0645 8 Y 0.418
to N 0.412
19 N 0.41
20 0630 1 Y 0.403 4.3
21 0545 8 B 0.302
22 0600 8 B 0.302
23 N 0.302
24 N 0.301
25 N 0.301
26 N 0.299
27 0730 8 Y 0.298 7.72 9.87
28 0730 8 Y 0.298
29 0715 8 Y 0.173 7.74 10.07
30 0745 8 Y NOFLOW
Monthly Average Limn: 0.615 30 30
Meutkly Avenge: 0.38131 6.5 2.15 9.0125
Daily Muimom: 0.436 7.74 6.5 4.3 10.07
`
Daly Minimum: 0.173 7.3 6.5 0 7.98
#eat No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2017(November 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00094
A 1.28 .
I u
'€ l i i Monthly
fi < F
1 ii 6k
Grab
U
U F O Z CNDUCIYY
2400 dock Hn 3400 dads Hn YB N umhos/cm
1 0600 8 B
2 0600 8 B
3 0600 8 B
4 N
5 N
6 0730 8 Y
7 0730 8 Y
8 0700 8 Y 907
f 0730 8 Y
to 0700 8 Y
it N
12 N
13 0730 8 Y
14 0600 8 B
15 0700 8 Y
16 0745 8 Y
17 0645 8 Y
10 N
If N
20 0630 1 Y
21 0545 8 B
22 0600 8 B
23 N
24 N
25 N
26 N
27 0730 8 Y
28 0730 8 Y
29 0715 8 Y
>0 0745 8 Y NOFLOW
Monthly Avenge Limit:
Monthly Avenge: 907
Daily Munson: 907
Daily Minlmam. 907
's°°No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=NoVisitation—AdverseWeather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2017(November 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50050 00400 C0530 1111940 00094
A i i
1 I1 sI
$ i '2'• I Monthly Monthly Monthly Quarterly Monthly
5 6 8 Instantaneous Grab Grab Grab Grab
x 3
C U F+ O Z• e FLOW pH T83-Cone CHLORIDE CNDUCTVY
2400 dodo Hn 2400 dock Hn Y/B/N m8d su mg/I mg/I umhos/cm
t 0600 8 B
2 0600 8 B
3 0600 8 B
4 N
5 N
6 0730 8 Y
7 0730 8 Y
O 0700 8 Y
9 0730 8 Y
t0 0700 8 Y
It N
12 N
13 0730 8 Y
14 0600 8 B
15 0700 8 Y 0.115 7.23 <2.6 1045
16 0745 8 Y
t7 0645 8 Y
10 N
19 N
20 0630 1 Y
21 0545 8 B
22 0600 8 B
23 N
24 N
u N
26 N
27 0730 8 Y
28 0730 8 Y
29 0715 8 Y
30 0745 8 Y
Moodily Aver..Limit:
Monthly Avenge: 0.115 0 1045
Dal Minlosuov 0.115 7.23 0 1045
Daily aRnimnm: 0.115 7.23 0 1045
aaaa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2017(November 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Non-Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 12/14/2017
`^�1lMJ 12/13/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES pe
9 44(1
V q4, 12/14/2017
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per ISA NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per ISA NCAC 2B
.0506(b)(2)(D).

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2017(November 2017) VERSION: 1.0 STATUS:Processed
Report Comments:
Non-Compliance Week 3,Outfall 001;During the 3rd week of November(11/19 thru 11/25)the weekly DO and pH was inadvertently missed due to miscommunication between
ORC and Back-up ORC. ORC was on vacation during this period. Upon ORC returning to work on Monday 11/27/17,and realizing the weekly DO and pH had not been
obtained for the prior week a sample was immediately analyzed for pH and DO and communicated to Ori Tuvia of the Mooresville Regional Office.
Week 1,outfall 001;weekly sampling was completed on 10/31/17 for pH and DO,therefore compliant with weekly permit monitoring requirements.

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2017(November 2017) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Week 1 pH and DO completed Tuesday 10/31/17.
During the 3rd week of November(1 l/19 thru 11/25)the weekly DO and pH was inadvertently missed due to miscommunication between ORC and Back-up ORC. ORC was on
vacation during this period. Upon ORC returning to work on Monday 11/27/17,and realizing the weekly DO and pH had not been obtained for the prior week a sample was
immediately analyzed for pH and DO and communicated to Ori Tuvia of the Mooresville Regional Office.

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVE 1yOUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis R•/ORC CERT NUMBilt:/8624
DEC 01 2017
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2017(October 2017) VERSION:1.0 CENTRAL FILES STATUS:Processed
CW'✓ii SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO r''
50050 00409 C0530 09940 00094
I I
I x
i '1 C Monthly Monthly Monthly Quarterly Monthly
F m
1 1
9` 8 8
o7
L Instantaneous Grab Grab Grab Grab
a a
a u 1- o A FLOW pH 3B9-Can CHLORIDE CNoucrvv
2400 deer Hn 2400 clock Hn Y/Ba4 mgd su mg/I mg/1 umhos/cm
1 N
2 0730 8 Y
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
4 0730 8 Y
7 N
8 N
9 0745 8 Y
19 0730 8 Y
11 0700 8 Y
12 0730 8 Y
13 0730 8 Y
14 N
15 N
16 0715 8 Y
17 1300 4 Y
to 0745 8 Y
19 0600 8 B
20 0600 8 B
21 N
22 N
23 0600 8 B
24 0600 a B
25 0730 8 Y 0.494 7.05 3.1 31.3 808
26 0730 8 Y
27 0730 8 Y
2s N
29 N
79 0730 8 Y
J1 0730 8 Y
Meanly Average Limit:
Mearhy Average: 0.494 3.1 31.3 808
Daily Maaheam: 0.494 7.05 3.1 31.3 808
Daily nI . 0.494 7.05 3.1 31.3 808
0000 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2017(October 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 11/10/2017
1 1/09/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
/44 a G j 11/10/2017
Permittee/Submitter Signature:* * Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney S.Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per I5A NCAC 2B
.0506(b)(2)(D).

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2017(October 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
• 50050 00400 C0310 C0530 00300 C0600 C0665 00040 THP3B
l I •
I 8 ;
a7 s
I .1 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
g < E.0 8 8 I Recorder Grab Grab Grab Grab Grab Grab Grab Composite
ti I t% 1 O ex aO '>< FLOW pH DOD-Cane T88-Case DO TOTAL N- TOTAL P-Can CHLORIDE CER7DCHV
2400 deck Hn 24414 dodo Hn YIB1N mgd su mg/I mg/I mg/I mg/I mg/ mg/I percent
1 N 0
2 0730 8 Y 0.272
3 0730 8 Y 0.451
4 0730 8 Y 0.454 7.2 4.2 <2.7 5.94 <0.5 <0.05 74.2 >100
5 0730 8 Y 0.451
6 0600 8 B 0.449
7 N 0.448
8 N 0.448
0 0745 8 Y 0.466
10 0730 8 Y 0.439
11 0700 8 Y 0.429 7.74 6.9
12 0730 8 Y 0.432
13 0730 8 Y 0.432
14 N 0.432
IS N 0.433
16 0715 8 Y 0.436
17 1300 4 Y 0.439
18 0745 8 Y 0.446 7.34 <2.6 7.17
I5 0600 8 B 0.448
20 0600 8 B 0.446
21 N 0.445
22 N 0.439
23 0600 8 B 0.438
24 0600 8 B 0.438
25 0730 8 Y 0.438 7.72 7.2
26 0730 8 Y 0.438
27 0730 8 Y 0.438
28 N 0.438
28 N 0.435
30 0730 8 Y 0.435
31 0730 8 Y 0.432 7.55 7.86
Ma.tky Avenge Ludt: 0.615 30 30
Maetky Average: 0.421452 _4.2 0 7.014 0 0 74.2 100
Daly Maximum: 0.466 7.74 4.2 0 7.86 0 0 74.2 100
Daily Minimum 0 7.2 4.2 0 5.94 0 0 74.2 100
aaaa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2017(October 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
• 80994 TGP3B
y
,� A i Monthly Quarterly
6 I
Fu a` a i Grab Grab
a I a u
.S u [= O ie CNDUCTYY CERI7DPF
2400 dolt Hn 2409 dock Hn V/B/N tunl os/cm pass/fail
1 N
2 0730 8 Y
3 0730 8 Y
4 0730 8 Y 950
5 0730 8 Y
4 0600 8 B
7 N
s N
9 0745 8 Y
10 0730 8 Y
It 0700 8 Y
12 0730 8 Y
13 0730 8 Y
14 N
15 N
14 0715 8 Y
17 1300 4 Y
18 0745 8 Y
19 0600 8 B
20 0600 8 B
21 N
22 N
23 0600 8 B
24 0600 8 B
25 0730 8 Y
24 0730 8 Y
27 0730 8 Y
28 N
29 N
30 0730 8 Y
31 0730 8 Y
MwHy Average Limit
Monthly Avenge: 950
Daly Maahaam: 950
Daily Minimum 950
....No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

3
ES PERMIT NO.:NC0005177 PERMIT VERSION: PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2C IV E D COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney StoughStout_WLN 0U 0 3 2017 ORC CERT NUMBER:28624 NRIDwp
GRADE:PC-2 ORC HAS CHANGED:No '�E CEN~;�.
eDMR PERIOD:09-2017(September 2017) VERSION:1.0 CENTRAL FILES DWR SECTION .�,.STATUS:Processeds''''D';-1/`l1'
I J
0•Bos
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHAG9 *.,,:;X loNNI-oFFicE
Moo
• 50050 00000 C0310 C0530 00300 COW C0665 00940 THP3B
14.
y
lWeeklyMonthlyWeekly Quarterly Quarterly Quarterly Monthly
Continuous 2 X month ed arterl erl
tj S 3 a H 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
u ay
Iu y° FLOW pH eon-Cone T88-Cone DO TOTAL N- TOTAL P-Cone CHLORIDE CeR7DCHY
2400 deck Hn 2400 dock Hn Y/B/N mgd su mg/I mg/I mg/I mg/I mg/I mg/I percent
1 0730 8 Y 0
2 N 0
3 N 0
4 N HOLIDAY
5 0730 8 Y 0
6 0730 8 Y 0
7 0730 8 Y 0
8 0730 8 Y 0
9 N 0
10 N 0
1t 0730 8 Y 0
12 0730 8 Y 0
13 0730 8 Y 0
14 0600 8 B 0
15 0600 8 B 0
16 N 0
17 N 0
18 0730 8 Y 0
19 1000 7 Y 0
20 0700 8 Y 0
21 0600 8 B 0 -
22 0600 8 B 0
23 N 0
24 N 0
25 0730 8 Y 0
26 0730 8 Y 0
27 0715 8 Y 0
2s 0600 8 B 0
29 0600 8 B 0
30 N 0
Monthly Avenge Lira: 0.615 30 30
Monthly Avenge: 0
Dilly Man .: 0
Daly Mtn`.: 0
a•aa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2017(September 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
COM
11
I « p Monthly
E
gg
a S 8 Grab
8 u 0. CNDUCIVY
2400 dock lin 2400 clock thy Y/a/N umhos/cm
1 0730 8 Y
2 N
3 N
4 N HOLIDAY
5 0730 8 Y
6 0730 8 Y
7 0730 8 Y
s 0730 8 Y
t N
10 N
11 0730 a Y
12 0730 8 Y
13 0730 8 Y
14 0600 8 B
15 0600 8 B
16 N
17 N
IS 0730 8 Y
D 1000 7 Y
26 0700 8 Y
21 0600 8 B
22 0600 8 B
23 N
24 N
25 0730 8 Y
26 0730 8 Y
27 0715 8 Y
29 0600 8 B
29 0600 a B
30 N
M..ay Average Lldt:
M.&hy Avenge:
Dilly Madman:
Dolly M eImam:
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2017(September 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00940 00094
11
t 8 ;
II I. <C A i i Monthly Monthly Monthly Qusnerly Monthly
t-
SS P a k Instantaneous Grab Grab Grab Grab
s
I F O Z FLOW pH 7'98-Case CHLORIDE CNDUCTVY
2400 dock Hn 2400dodk Hn WHIN mgd su mg/I mg/I umhos/cm
I 0730 8 Y
2 N
3 N
4 N HOLIDAY
5 0730 8 Y
6 0730 8 Y
7 0730 8 Y
8 0730 8 Y
9 N
1e N
tt 0730 8 Y
Is 0730 8 Y
13 0730 8 Y 0.72 6.74 <2.6 874
14 0600 8 B
Is 0600 8 B
16 N
17 N
II 0730 8 Y
19 1000 7 Y
20 0700 8 Y
21 0600 8 B
22 0600 8 B
7b N
24 N
25 0730 8 Y
26 0730 8 Y
27 0715 8 Y
28 0600 8 B
20 0600 8 B
50 N
M.nlhy Avenge Wit:
Menly Avenge` 0.72 0 874
Dolly Maximum 0.72 6.74 0 874
Dolly Minim.m. 0.72 6.74 0 874
e"6 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2017(September 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 10/26/2017
W49.L 10/25/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
/U"/ _ !� /1/ (A 10/26/2017
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired .3
ACILITY NAME:Lithium Division Plant CLASS:PC-2 RE C E I V E DCOUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis 0 C T 03 2017 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No RECEIVED/NCDENR/DWR
eDMR PERIOD:08-2017(August 2017) VERSION:1.0 CENTRAL FILES STATUS:Processed
DWR SECTION (1! ' 9 2011
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES WOROS
MOORESVILLE REGIONAL OFF
50050 00400 C0310 C0030 00300 C0600 C0665 00940 THP3B
8
9 ,� y i Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u° a a8 g Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a l it ci g S u !- Z FLOW pH ROD-Cone TES•Cone DO TOTAL N• TOTAL P-C.ee CHLORIDE CER7DC11Y
2/00dock Firs 2400 dock Het YIBTt mgd su mg/I mg/I mg/I mg/I mg/I mg/I percent
1 0745 8 Y
2 0745 8 Y
3 0730 8 Y
4 0730 8 Y
s
6
7 0720 8 Y
a 0720 8 Y
f 0730 8 Y
10 0720 8 Y
II 0720 8 Y
12
13
14 0740 8 Y
Is 0730 8 Y
16 0730 8 Y
17 0730 8 Y
II 0730 8 Y
If
20
21 0730 8 Y
i2 0730 8 Y
23 0730 8 Y
24 0730 8 Y
23 0730 8 Y
26
27
}8 0730 8 Y
2f 0730 8 Y
30 0730 8 Y
31 0730 8 Y
Monthly Avenge Lilt: 0.61s 30 30
Monthly Avenge:
Daly Mailman,:
Dolly Minimum:
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
'ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2017(August 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00094
I. i 1 I Monthly
4 E 3 d 8. Grab
u of
d u F o z crDucrvv
2400 deck Hn 2400 dedt Hn Y/BIN umhos/cm
1 0745 8 Y
2 0745 8 Y
3 0730 8 Y
4 0730 8 Y
5
6
7 0720 8 Y
s 0720 8 Y
f 0730 8 Y
is 0720 8 Y
it 0720 8 Y
12
13
14 0740 8 Y
Is 0730 8 Y
16 0730 8 Y
17 0730 8 Y
18 0730 8 Y
If
20
21 0730 8 Y
22 0730 8 Y
23 0730 8 Y
24 0730 8 Y
25 0730 8 Y
26
27
28 0730 8 Y
2! 0730 8 Y
30 •
0730 8 Y
31 0730 8 Y
Monthly Avenge Link:
M.ethly Avenge:
Only Mailers:
Daly Mlainon:
*08*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
'ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2017(August 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50030 0040e C0530 00940 00094
A
I
Ai Monthly Monthly Monthly Quarterly Monthly
u a a s k Instantaneous Grab Grab Grab Grab
g' 1
a u 1-I z' FLOW pH TES-Cone CHLORIDE CNDUCTVY
2400 door Hn 2400 deck xn Y/BM mgd su mg/I mg/I umhos/cm
1 0745 8 Y
2 0745 8 Y
3 0730 8 Y
4 0730 8 Y
5
6
7 0720 8 Y
8 0715 8 Y
O 0730 8 Y 0.048 6.94 <2.5 29.4 813
I0 0720 8 Y
II 0720 8 Y
12
13
14 0740 8 Y
IS 0730 8 Y
16 0730 8 Y
17 0730 8 Y
18 0730 8 Y
I,
20
21 0730 8 Y
23 0730 8 Y
23 0730 8 V
24 0730 8 Y
25 0730 8 Y
26
n
n 0730 8 Y
25 0730 8 Y
38 0730 8 Y
31 0730 8 Y
Mouthy Avenge Liege
Monthy Average: 0.048 0 29.4 813
Daily Ma'hwon 0.048 6.94 0 29.4 813
1>•83Minimum: 0.048 6.94 0 29.4 813
e00*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ERM1T NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2017(August 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:09/19/2017
09/12/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
1 0uci"`� 09/19/2017
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney S Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVE D COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis AU G 2 3 2017 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
RECEIVED/NCDENR/DWR
eDMR PERIOD:07-2017(July 2017) VERSION:1.0 CENTRAL FILES STATUS:Processed
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*a YESIQROS
RESVILLE REGIONAL OFFICE
50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
I
8 , Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
6
u° 3 i 8 k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
aI Fl 5i a
II u f+ O Za FLOW pH HOD-C.... TSa-Can DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DCHV
24N d.dr tin 2400 deck Hn Y/BIN mgd su mg/I mg/1 mg/I mg/1 mg/1 mg/1 percent
I 0
2 0
3 HOLIDAY
4 HOLIDAY
5 0730 8 Y 0
s 0730 8 Y 0
7 0730 8 Y 0
8 0
0 0
10 0730 8 Y 0
It 0730 8 Y 0
12 0730 8 Y 0
13 0715 8 Y 0
14 0730 8 Y 0
15 0
16 0
17 0715 8 Y 0
18 0730 8 Y 0
19 0730 8 Y 0
m 0730 8 Y 0
21 0730 8 Y 0
22 0
23 0
24 0730 8 Y 0
25 0730 8 Y 0
24 0715 8 Y 0
27 0600 8 B 0
m 0600 8 B 0 _
20 0
30 0
31 0600 8 B 0
Moldy Avenge L16621: it,,, 30 30
at.1by Avenge: 0
Day M.st.e.: 0
Wily Mrtw.: 0 —
e*•s No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2017(July 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00006 TGP3B
''� i Monthly Quarterly
4 < F
u E d 8 Grab Grab
I I g 1 O Zo CNDUCIYY CERflDPP
2400 dock Hn 2400 dock Hn Y/B:N umhos/em pass/fail
1
2
3 HOLIDAY
4 HOLIDAY
5 0730 8 Y
6 0730 8 Y
7 0730 8 Y
a
f
IO 0730 8 Y
11 0730 8 Y
12 0730 8 Y
13 0715 8 Y
14 0730 8 Y
15
If
17 0715 8 Y
II 0730 8 Y
If 0730 8 Y
20 0730 8 Y
21 0730 8 Y
22
23
24 0730 8 Y
25 0730 8 Y
26 0715 8 Y
27 0600 8 B
28 0600 8 B
2f
30
31 0600 8 B
Monthly Avenge LW,:
Monthly Avenge:
Day Madman:
Dolly Minimum:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2017(July 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50858 00400 C0530 00940 00094
A A a a
i1 Monthly Monthly Monthly Quarterly Monthly
r! ac 2 aa7
. Instantaneous Grab Grab Grab Grab
x C
2 I 1-� 5 O FLOW pH 7'89-Cone CHLORIDE CNDUCTVY
2400 dodo H. 2400 deck Hn WHIN mgd su mg/I mg/1 umhos/cm
1
3
3 HOLIDAY
4 HOLIDAY
5 0730 Y 8 0.246 7.03 <2.5 28 822
4 0730 Y 8
7 0730 Y 8
e
9
10 0730 Y 8
tt 0730 Y 8
12 0730 Y 8
13 0715 Y 8
14 0730 Y 8
15
If
17 0715 Y 8
18 0730 Y 8
19 0730 Y 8
28 0730 Y 8 _
21 0730 Y 8
22
23
24 0730 Y 8
25 0730 Y 8
24 0715 Y 8
27 0600 Y 8
28 0600 Y 8
29
3s
31 0600 Y 8
Meanly Avenge Limit:
Monthly Average: 0.246 0 28 822
Dolly Maaimuw. 0.246 7.03 _0 28 822
13$MYinese 0.246 7.03 0 28 822
88ee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:07-2017(July 2017) VERSION:1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:08/16/2017
GOL s._J /v 08/10/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
de„..41
08/16/2017
Permittee/Submitter Signatu ‘:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC-Lithium,Pace Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

I ri
I°li'lliF 1 P P-,
PDES PERMIT NO.:NC000S177 PERMIT VERSION:4.0 RECEIVEDRMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 J U L 4 8 2017 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis CENTRAL FILESQRC CERT NUMB DINCDENRIDWR
GRADE:PC-2 ORC HAS CHANGED:No DWR SECTION ._ / ,)i l i 7
eDMR PERIOD:06-2017(June 2017) VERSION: 1.0 STATUS:Processed
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISliefiiiitittitigNAL OFFICE
A i ii
0 50050 400 C0310 C0530 00300 C0600 C0665 009/0 THP38
d :
i1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u I
8I Recorder Grab Gab Grab Grab Grab Grab Grab Composite
27te$ pubB o F O O A FLOW pH BOD-Cone T88-Cone DO TOTALN- TOTAL P-Can CHLORIDE CER7DCHV
2400 deck He. 2409 dodk Hn Y/B/N mgd su mg/I mg/I mg/1 mg/1 mg/I mg/I percent
I 730 8 Y 0
2 730 8 B 0
3 N 0
4 N 0
5 730 8 Y 0
6 730 8 Y 0
7 730 8 Y 0
8 730 8 Y 0
9 700 8 B 0
10 N 0
tI N 0
12 730 8 Y 0
13 730 8 Y 0
10 730 8 Y 0
15 715 8 Y 0
16 705 8 Y 0
17 N 0
18 N 0
19 730 8 Y 0
2a 730 8 Y 0
21 730 8 Y 0
22 700 8 Y 0
23 730 8 Y 0
24 N 0
25 N 0
26 730 8 Y 0
27 735 8 Y 0
28 730 8 Y 0
29 0700 8 Y 0
30 0730 8 Y 0
I
Mont LI Monthly Average n11: 0.615 30 3a -
Monthly Average: 0
Daily Maximum. 0
Daily Mbdmam: 0
***I'No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

rPDES
PERMIT Na:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
•
eDMR PERIOD:06-2017(June 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00094
l
2 d
6 1 A i / Monthly
a u F I I o k Grab
i CNDUCIVY
2400 clock His 2400 deck HIS Y/BIN umhos/cm
I 730 8 Y
2 730 8 B
3 N
4 N
5 730 8 Y
4 730 8 Y
7 730 8 Y
a 730 8 Y
0 700 8 B
to N
tt N
12 730 8 Y
13 730 8 Y
14 730 8 Y
15 715 8 Y
16 705 8 Y
17 N
18 N
19 730 8 Y
20 730 8 Y
21 730 8 Y
22 700 8 Y
23 730 8 Y
24 N
25 N
20 730 8 Y
27 735 8 Y
2a 730 8 Y
29 0700 8 Y
30 0730 8 Y
Monthly Avenge Lima:
Monthly Average:
Dolly Mashnonn
Dolly MMhnnn.:
sees No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PITNO.:NCOOO5I7l PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2017(June 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50054 004E0 C0330 00940 00094
I A A a :
L
'� A I Monthly Monthly Monthly Quarterly Monthly
< F
7 S a A Instantaneous Gab Grab Grab Grab
§ Z p8r
d U [u�+ O AFLOW pH 788-Cwe CHLORIDE CNDUCfVY
2400 deck Hrs 3400 deck Hrs Y/9IN mgd su mg/I mg/I umhos/cm
I 730 8 Y
2 730 8 B
3 N
4 N
5 730 8 Y
6 730 8 Y
7 730 8 Y 0.271 7.05 <2.6 875
a 730 8 Y
3 700 8 B
N N
11 N
12 730 8 Y
13 730 8 Y
14 730 8 Y
15 715 8 Y
16 705 8 Y
17 N
IS N
I9 730 8 Y
30 730 8 Y
21 730 8 Y
22 700 8 Y
33 730 8 Y
24 N
35 N
26 730 8 Y
27 735 8 Y
20 730 8 Y
25 700 8 Y
30 730 8 Y
Monthly Average Limit:
Mouthy Average: 0.271 0 875
Day Ma'le.e: 0.271 7.05 0 875
Daly ua 0.271 7.05 0 875
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

P;ERMITNO.:NC000S 177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:06-2017(June 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:07/14/2017
07/14/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
4.1 07/14/2017
Permittee/Submitter Sign ure:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.:NC0005I77 PERMIT VERSION:4.0 PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 OUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis R E C ic.w I V C CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No JUN 2 1 2017
eDMR PERIOD:05-2017(May 2017) VERSION:1.0 CENTRAL FILESTATUS:Processed
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 5e430 00400 C0330 00940 000+4
A A is
1 i Monthly Monthly Monthly Quarterly Monthly
4 «! I. Instantaneous Grab Grab Grab Grab
d u r 1 1 o $ FLOW H+ rss-c..e CHLORIDE CNDUCTVY
2400 dolt Hn 2400 doh Hn Y/9/N mgd su mg/1 mg/1 umhos/cm
I 730 8 Y
2 730 8 Y
3 1011 730 8 Y 0.222 7.42 <2.6 786
)
+ 730 0 V PEE LIVED/VCDENR/DWR
s 730 8 Y
4 0 N _ .1 2 [
7 0 N
a 730 8 Y WCROS
+ 730 8 Y MOORFSVILLE areloN !OFFICE
to 730 8 Y
II 730 8 Y
12 730 8 Y
13 0 N
14 0 N
15 730 8 Y
1s 730 8 Y
17 730 8 Y
10 730 8 Y
I1 730 8 B
20 0 N
21 0 N
22 730 8 Y
23 730 8 Y
24 730 8 Y
2•S 700 8 B
26 700 8 B
27 0 N
2A 0 N
20 0 N HOLIDAY
30 730 8 Y
31 730 8 Y
Monthly Annie LM.k
Monthly Arenas: 0.222 0 786
Dolly M.ob..ar: 0.222 7.42 0 786
Mk Minimum: 0.222 7.42 0 786
e"e No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2017(May 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES
•
Se/SS euoe C031e code Will CONS COW NMI THP3a
I
3t 1 8
J L 1 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
a i Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a 1S U H O ci FLOW pH DOD-Cow Tab-C.rre DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DCHV
2400 sleek Hn 2400 desk Hn Y/PJN mgd su mg/1 mgA mg/1 mg/I mg/I mgA percent
I 730 8 Y NOFLOW
2 730 8 Y NOFLOW
3 730 8 Y NOFLOW
4 730 8 Y NOFLOW
5 730 8 Y NOFLOW
e 0 N NOFLOW
7 0 N NOFLOW
a 730 8 Y NOFLOW
730 8 Y NOFLOW
le 730 8 Y NOFLOW
II 730 8 Y NOFLOW
12 730 8 Y NOFLOW
13 0 N NOFLOW
14 0 N NOFLOW
IS 730 8 Y NOFLOW
Ia 730 8 Y NOFLOW
17 730 8 Y NOFLOW
In 730 8 Y NOFLOW
If 700 8 B NOFLOW
20 0 N NOFLOW
21 0 N NOFLOW
22 730 Y NOFLOW 8
23 730 8 Y NOFLOW
24 730 8 Y NOFLOW
23 700 8 B NOFLOW
2s 700 8 B NOFLOW
27 0 N NOFLOW
2a 0 N NOFLOW
20 0 N HOLIDAY
30 730 8 Y NOFLOW
31 730 8 Y NOFLOW
MeaI Average Lladl:,e.el3 3e 3s• '
_Mselbly
Daly Meslnaee
Daly Mina=
eeae No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2017(May 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
00004
1 a A A
r A 7 aI
. L 1 I , Monthly
" d d $ Grab
a 1 3 u B
el A o A CNDUC VY
2400 deck Hn 2400 deck Hn Y/BIN umhos/clll
I 730 8 Y NOFLOW
2 730 8 Y NOFLOW
3 730 8 Y NOFLOW
4 730 8 Y NOFLOW
8 730 S Y NOFI.OW
a 0 N NOFLOW
7 0 N NOFLOW
a 730 S Y NOFLOW
f 730 8 Y NOFLOW
to 730 8 Y NOFLOW
II 730 8 Y NOFLOW
12 730 8 Y NOFLOW
13 0 N NOFLOW
14 0 N NOFI.OW
13 730 8 Y NOFLOW
16 730 8 Y NOFLOW
17 730 8 Y NOFLOW
10 730 8 Y NOFLOW
17 700 8 B NOFLOW
20 0 N NOFLOW
21 0 N NOFLOW
22 730 S Y NOFLOW
23 730 8 Y NOFLOW
24 730 8 Y NOFLOW
2s 700 8 B NOFLOW
26 700 8 B NOFLOW
27 0 N NOFLOW
2a 0 N NOFLOW
29 0 N HOLIDAY
30 730 8 V NOFLOW
31 730 8 Y NOFLOW
Measly Avenge LIaM:
M.aMy Avenge:
Dolly Moskwn:
Dolly M4k.an:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather. NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:05-2017(May 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:06/08/2017
06/08/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittce becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of
the NPDES pe
L0.4 06/08/2017
Permittee/Submitter Signa ure:*** Michael Paul McGowan E-Mail:paul.mcgowan«fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney S willis
PARAMETER CODES
Parameter Codc assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdcs/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired 3
FACILITY NAME:Lithium Division Plant CLASS:PC-2 RECEIVED COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
JUN 0 7 2017 REUEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION: 1.0 CENTRAL FILES STATUS:Processed JuN ! 3 ; i r
DWR SECTION
WQROs
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCIDISCU2kROPM4PGIONAL OFFICE
• 58050 00400 C0310 C0530 00300 C0010 C0645 00940 THP3B
A Y I
Y 8
2
< i I Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
a ® aRecorder Grab Grab Grab Grab Grab Grab Grab Composite
pO S u F ub 1 1 A FLOW pH DOD-Cenr Taa-Cent DO TOTAL N. TOTAL P-Cent CHLORIDE CER7DCHV
2400 deck Hn 2400 deck Hn V/879 mgd su mg/1 mg/I mg/I mg/1 mg/I mg/I percent
1 0 N 0.429
2 0 N 0.429
3 0730 8 Y 0.429
4 0730 8 Y 0.429
5 0730 8 Y 0.425 8.3 <2 2.8 8.71 <0.12 <0.05 105
6 0730 8 Y 0.423 >100
7 0730 8 Y 0.423
a 0 N 0.423
9 0 N 0.419
to 0730 8 Y 0.419
II 0730 8 Y 0.419
12 0730 8 Y 0.352 8.1 9.25
13 0730 8 Y 0.311
14 0 N HOLIDAY
15 0 N 0.311
16 0 N 0.311
17 0730 8 Y 0.311
18 0730 8 Y 0.305
19 0730 8 Y 0.297 8.1 <2.6 9.1
20 0730 8 Y 0.302
21 0730 8 Y 0.104
22 0 N NOFLOW
23 0 N NOFLOW
24 0730 8 Y NOFLOW
35 0730 8 Y NOFLOW
26 0730 8 Y NOFLOW -
27 0730 8 V NOFLOW
is 0700 8 B NOFLOW
29 0 N NOFLOW
30 0 N NOFLOW
Meanly Avenge LAM: 0.615 30 30
Ninthly Average: 0.36355 0 1.4 9.02 0 0 105 100
Daily Muluon: 0.429 8.3 0 2.8 9.25 0 0 105 100
Daly Mlelem®: 0.104 8.1 0 0 8.71 0 0 105 100
eeie No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Y • 00094 TGP3B
F
A� gp
6 e m I Monthly Quarterly
I u° $ 1 8 S. Grab Grab
A 1 'a a a
O a 1 1 6• O Zo CNDUCTVY CERI7DPF
2400 cloak Hn 2400 leek Hn Y/B/N umhos/cm pass/fail
1 0 N
2 0 N
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y 1055
6 0730 8 Y
7 0730 8 Y
a 0 N
9 0 N
to 0730 8 Y
II 0730 8 Y
12 0730 8 Y
I3 0730 8 Y
14 0 N HOLIDAY
IS 0 N
16 0 N
17 0730 8 Y
IO 0730 8 Y
19 0730 8 Y
20 0730 8 Y
21 0730 8 Y
22 0 N NOFLOW
23 0 N NOFLOW
24 0730 8 Y NOFLOW
25 0730 8 Y NOFLOW
26 0730 8 Y NOFLOW
27 0730 8 Y NOFLOW
20 0700 8 B NOFLOW
29 0 N NOFLOW
30 0 N NOFLOW
Monthly Avenge Linn:
Monthly Average: 1055
Daily Mashm: 1055
Daily Minimum: 1055
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Week 1 samples collected in March DMR.
Week 5 No flow for Week
Week 6 No flow for Week

PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0530 00946 00094
i
9 8
L
'� IitMonthly Monthly Monthly Quarterly Monthly
I
I 1-.
u 1 8 8 a8 Instantaneous Grab Grab Grab Grab
a 7 3
S V' F 0) Zo FLOW pH TES-Cow CHLORIDE CNDUCTVY
2400 cock Hn 2400 cock Hn YIBIN mgd su mg/I mg/I umhos/cm
1 0 N
2 0 N
3 0730 8 Y
4 0730 8 Y
$ 0730 8 Y 0.588 7.74 <2.5 32.6 955
6 0730 8 Y
7 0730 8 Y
s 0 N
9 0 N
10 0730 8 Y
II 0730 8 Y
12 0730 8 Y
13 0730 8 Y
14 0 N HOLIDAY
15 0 N
16 0 N
17 0730 8 Y
10 0730 8 Y
19 0730 8 Y 0.222 7.79 <2.6 32.6 944
20 0730 8 Y
21 0730 8 Y
22 0 N
23 0 N
Z4 0730 8 Y
25 0730 8 Y
26 0730 8 Y
27 0730 8 Y
20 0700 8 B
29 0 N
30 0 N
Monthly Avenge Limit:
Monthly Avnr.0n 0.405 0 32.6 949.5
Dolly Maximum 0.588 7.79 0 32.6 955
Day Milkmen: 0.222 7.74 0 32.6 944
4"•No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION: 1.0 STATUS:Processed
Outfall 004-Effluent Comments:
Sample Collected on 4/19 was during a represenative storm event.e-DMR does not allow for entry of BOD and TPH. They are reported here,BOD-<2.0,and TPH-<5.0.
Qualitative Monitoring report also completed will it will be included with mailing.

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:04-2017(April 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:05/18/2017
CL __
05/17/2017
k✓v�
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of .
the NPDES pe
ii
/ 05/18/2017
Permittee/Submitter Signatur :*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Corp.,Pace Ashville,R&A Labs
CERTIFIED LAB#:5023,40,14
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

t47711,
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form,please visit: http://portal.ncdenr,org/web/wq/ws/su/npdessw#tab-4
Permit No.: Ng./ / / / / / / / or Certificate of Coverage No.: N/C/G/ / / / / / /
Facility Name: FMC ccessoeil=n00 Uri W.
County: qA4tv►J Phone No.
Inspector: goilv.)E,r.kV,.11
Date of Inspection:
Time of Inspection:
Total Event Precipitation(inches): O AC .__
Was this a"Representative Storm Event"or"Measureable Storm Event"as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event"or"measureable storm event"(requirements vary,depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a"representative storm event"or during a"measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions,if applicable.
A"representative storm event"is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A"measurable storm event"is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period,and the permittee
obtains approval from the local DWQ Regional Office.
By this signature,I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242,Last modified 10/25/2012

1. Outfall Des ription:
Outfall No. Structure(pipe,ditch,etc.) 1 Sf it-c-iA'M
Receiving Stream: 11Z�S C R .EK
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red,brown,blue,etc.) and tint
(light,medium,dark) as descriptors: Ll.E.A -
3. Odor: Describe any distinct odors that the discharge may have(i.e.,smells strongly of oil,
weak chlorine odor,etc.): 1Jot.1E
4. Clarity: Choose the number which best describes the clarity of the discharge,where 1 is
clear and 5 is very cloudy:
2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge,where 1 is no solids and 5 is the surface covered with floating solids:
V 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge,where 1 is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? Yes CI))
8. Is there an oil sheen in the stormwater discharge? Yes all
9. Is there evidence of erosion or deposition at the outfall? Yes o
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Iaor sS \k
Note: Low clarity,high solids,and/or the presence of foam,oil sheen,or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242,Last modified 10/25/2012

_ RECEIVED 3
PPERMITO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 MAY 02 Z017 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis CENTRAL FILES ORC CERT NUMBER:28624
-RECEIVEDJNCDENRIDWR
GRADE:PC-2 ORC HAS CHANGED:No DWR SECTION
eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed WAY Y • 11
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCuA.D�T -�T caRas
`�`ilffe t is REGIONAL OFFICE
•
SOON N400 C0310 C0530 00300 CO6N CONS 000a THP3B
1 1 Continuous Weekly Monthly 2 X month Weekly Quarterly .Quarterly Quarterly Monthly
e
� 8!( 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a O 0 0
S U F' Z' FLOW pH Boo-C.ae Tss-Cone DO TOTAL n- TOTAL P-Cone CHLORIDE CER7DCHV
24N deck Hr. 24N dodo Hn Y/BIN mgd su mg/I mg/I mg/1 mg/I mg/1 mg/1 percent
1 7:30 8 Y 0.451 8.36 <2 <5.9 10.85
2 7:30 8 Y 0.443
3 7:30 8 Y 0.431
4 N 0.431
5 N 0.431
4 7:30 8 Y 0.431
7 7:30 8 Y 0.443
a 7:30 8 Y 0.435 8.2 11.6
4 7:30 8 Y 0.435
10 7:30 8 Y 0.435
11 N 0.435
12 N 0.435
13 7:30 8 Y 0.431
14 7:30 8 Y 0.431
15 7:30 8 Y 0.428 8.28 4.1 10.18
16 7:30 8 Y 0.428
17 7:00 8 B 0.419
IS N 0.419
If N 0.419
2e 7:30 8 Y 0.419
21 7:30 8 Y 0.431
22 7:30 8 Y 0.431 8.22 10.76
23 7:30 8 Y 0.432
24 7:30 8 Y 0.432
25 N 0.432
26 N 0.432
27 7:30 8 Y 0.432
2a 7:30 8 Y 0.431
20 7:30 8 Y 0.431 8.31 9.79
N 7:30 8 Y 0.431
31 7:30 8 Y 0.429
Meetly Avenge LW*: 0.615 so 30
Noddy AY°rye' 0.431419 0 2.05 10.636
Daly Mu`m. 0.451 8.36 0 4.1 11.6
Daily Minimum: 0.419 8.2 0 0 9.79
t 444 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
• 99994 TGP3B
3 A 1 A :
A •
Monthly
I8 a k Grab Composite
Y 1 Qx p8�
8 a 1 O Z CNDUCTVY CERI7DPP
2409 deck Hn 2409 d.d: Hn Y/BIN umhos/cm pass/fail
I 7:30 8 Y 1113
2 7:30 8 Y
3 7:30 8 Y
4 N
3 N
a 7:30 8 Y
7 7:30 8 Y
8 7:30 8 Y
9 7:30 8 Y
to 7:30 8 Y
It N
12 N
13 7:30 8 Y
14 7:30 8 Y
15 7:30 8 Y
16 7:30 8 Y
17 7:00 8 B
la N
19 N
29 7:30 8 Y
21 7:30 8 Y
22 7:30 8 Y
23 7:30 8 Y
24 7:30 8 Y
25 N
36 N
27 7:30 8 Y
2a 7:30 8 Y
29 7:30 8 Y
38 7:30 8 Y
31 7:30 8 Y
M..thly Avenge Limit:
MwWly Avenge: 1113
Day ara'Vaa: 1113
Dolly Minimum 1113
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PNPDESliriV
PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2017(March 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 30050 00400 C0530 00940 00094
8
Ii Monthly Monthly Monthly Quarterly Monthly
a
8 8 k Recorder Grab Grab Grab Grab
pur
d ,3O i4 FLOW pH T88-C. CHLORIDE CNDUCTVY
2400 dark Hn 2400 d.dc Hn YnVN mgd su mg/I mg/I umhos/cm
1 7:30 8 Y 0.097 7.94 <2.5 1069
2 7:30 8 Y
3 7:30 8 Y
4 N
5 N
4 7:30 8 Y
7 7:30 8 Y
e 7:30 8 Y
9 7:30 8 Y
10 7:30 8 Y
II 0 N
12 0 N
13 7:30 8 Y
14 7:30 8 Y
15 7:30 8 Y
16 7:30 8 Y
17 7:00 8 B
18 0 N
19 0 N
2e 7:30 8 Y
21 7:30 8 Y
22 7:30 8 Y
23 7:30 8 Y
24 7:30 8 Y
25 0 N
26 0 N
27 7:30 8 Y
28 7:30 8 Y
29 7:30 8 Y
30 7:30 8 Y
31 7:30 8 Y
M..1ry Avenge LtmR:
?Muddy Avenge: 0.097 0 1069
Dolly Mashnnr: 0.097 7.94 0 1069
Daly Minimum 0.097 7.94 0 1069
00 0 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:03-2017(March 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:04/11/2017
LJ-_ .\ 04/05/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 1I.E.6 of
the NPDES pe
41/(
04/11/2017
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Corp Lithium Division,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

3
ERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 ®Eee.IVE C�UNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis I'[C ORC CERT NUMBER:PROCCIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No APR 0 3 2017
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 CENTRAL FIIESTATus:Processed PR 1 0 2017
DWR SECTION WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC PR W IONAL OFFICE
50 00400 C0310 CMG 00300 C0600 C0605 80940 TIIP3B
F w50
8 :
_ .1 ,� '�y Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
` r
e 8 �. Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a a
S u t= Z° FLOW pH BOD-Cow TSB-Cone DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DC71V
2400 clock Hr. 2400 clack Ha Y//N mgd su mg/I mg/1 mg/1 mg/I mg/1 mg/1 percent
1 0730 8 Y 0.451 8.23 <2 <2.9 12.37
2 0730 8 Y 0.446
3 0730 8 Y 0.441
4 N 0.441 ,
5 N 0.442
a 0730 8 Y 0.443
7 0730 8 V 0.445
8 0730 8 Y 0.446 8.21 13.73
0 0730 8 Y 0.446 ,
10 0730 4 V 0.445
II N 0.445 .
12 N 0.443
13 0730 8 Y 0.442 ,
14 0730 8 Y 0.442
15 0730 8 Y 0.441 8.24 <2.5 14.62
10 0730 8 Y 0.441
17 0730 8 V 0.442
1a N 0.441
10 N 0.442 ,
2a 0730 8 V 0.442
21 0730 8 Y 0,442
22 0630 8 V 0.442 8.24 12.94
23 0630 8 B 0.439
24 0730 8 Y 0.435
25 N 0.436
20 N 0.438
27 0730 8 Y 0.441
20 0730 8 Y 0.442
•
Melly Average Lknk: 0.015 30 30
Movably Avenge 0.442214 0 0 13.415
MIN ism' 0.451 8.24 0 0 14.62 -
Daly MkrMwm: 0.435 8.21 0 0 12.37
aaaa No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
eao,4
'� .5 8
fi t '.y i Monthly
u° i 8 8 Grab
s g g IL u
S u r $ o i CNDUC VY
2400 deck an 2400 cloak Hrs Y/BIN umhos/cm
1 0730 8 Y 1047
2 0730 8 Y
3 0730 8 Y
4 N
5 N
6 0730 8 Y
7 0730 8 Y
a 0730 8 Y
a 0730 8 Y
to 0730 4 Y
II N
12 N
13 0730 8 Y
14 0730 8 Y
IS 0730 8 Y
16 0730 8 Y
17 0730 8 Y
to N
If N
28 0730 8 Y
21 0730 8 Y
22 0630 8 Y
23 0630 a a
24 0730 8 Y
25 N
26 N
27 0730 8 Y
21i 0730 8 Y
Maalhy Average Lhaa:
M.aMy Avenge: 1047
Daily Mailmen: 1047
Dolly Mlaimam: 1047
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PERMIT NO.:NC0005 177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00600 C0530 00940 00091
a a
< � Ai I Monthly Monthly Monthly Quarterly Monthly
g
u 5 2 d g Instantaneous Grab Grab Grab Grab
3 a
8 u h O L= FLOW pH TES-One CHLORIDE CNDUCTVY
2400 deck Hn 2400 gift* Hn Y/BIN mgd su mg/I mg/ umhos/cm
I 0730 8 Y 1.122 7.53 <2.5 1039
2 0730 8 Y
3 0730 8 Y
6 N
5 N
6 0730 8 Y
7 0730 8 Y
a 0730 8 Y
9 0730 8 Y
10 0730 4 Y
tt N
12 N
13 0730 8 Y
14 0730 8 Y
15 0730 8 Y
16 0730 8 Y
17 0730 8 Y
is N
19 N
20 0730 8 Y
21 0730 8 Y
22 0630 8 Y
23 0630 8 e
24 0730 8 Y
25 N
26 N
27 0730 8 Y
2a 0730 8 Y
Monthly Average Lhelr
Monthly Avenge: 1.122 0 1039
Daly Maslmom: 1.122 7.53 0 1039
D.0y Mlnhwm: 1.122 7.53 0 1039
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather. NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC IIAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:03/22/2017
ó'2_I? 03/22/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
ilj1/44tiliP
j 03/22/2017
Permitter/Submitter Signature:*** Michael Paul M Gowan E-Mail:[e-mail] fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdcnr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Usc only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:I'C-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC IIAS CIIANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
Outfit!!001-Effluent Comments:
Weekly Sample for 5th week,pl l and DO was collected March 1st,2017 for that week.

3
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
RECEIVE
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No APR 0 3 2017 t
RECEIVED/NCDENR/DWR
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 CENTRAL FILES STATUS:Processed
DWR SECTION Ai.-,1- !. f? ' )17
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: 11Ros
MOORESVILLE REGIONAL OFFICE
• 50050 00400 C0310 C0530 00304 C0600 C0665 00540 THP3B
I .I A •
I
1 A I :
® '� IContinuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
E` .18 k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
Y p��
d U il O ie FLOW pH BOD-Caw T88-Coat DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DCHV
2400doek Hn 2400 cloak Hn Y/B/N mgd su mg/1 mg/i mg/1 mg/I mg/I mg/1 percent
1 0730 8 Y 0.451 8.23 <2 <2.9 12.37
2 0730 8 Y 0.446
3 0730 8 Y 0.441
4 N 0.441
5 N 0.442
4 0730 8 Y 0.443
7 0730 8 Y 0.445
a 0730 8 Y 0.446 8.21 13.73
5 0730 8 Y 0.446
10 0730 4 Y 0.445
It N 0.445
12 N 0.443
13 0730 8 Y 0.442
14 0730 8 Y 0.442
15 0730 8 Y 0.441 8.24 <2.5 14.62
16 0730 8 Y 0.441
17 0730 8 Y 0.442
18 N 0.441
If N 0.442
20 0730 8 Y 0.442
21 0730 8 Y 0.442
22 0630 8 Y 0.442 8.24 12.94
23 0630 8 B 0.439
24 0730 8 Y 0.435
25 N 0.436
26 N 0.438
27 0730 8 Y 0.441
28 0730 8 Y 0.442
Men0k13 Average LWt: 0.615 30 30
Monthly Average: 0.442214 0 0 13.415
Daily Mnabsana. 0.451 8.24 0 0 14.62
Daily Mktimn®` 0.435 8.21 0 0 12.37
aeea No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

PNPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00034
I I A
I
I
I Monthly
Su o7 Grab
I I i' z CNDUCTVY
2400 deck Hn 2400 deck Hn WHIN umhos/cm
I 0730 8 Y 1047
2 0730 8 Y
3 0730 8 Y
4 N
3 N
6 0730 8 Y
7 0730 8 Y
8 0730 8 Y
f 0730 8 Y
1f 0730 4 Y
II N
12 N
13 0730 8 Y
14 0730 8 Y
II 0730 8 Y
16 0730 8 Y
17 0730 8 Y
19 N
If N
23 0730 8 Y
21 0730 8 Y
22 0630 8 Y
23 0630 8 B
24 0730 8 Y
rs N
26 N
27 0730 8 Y
2n 0730 8 Y
MeaM1y Avenge Limit:
Monthly Average: 1047
Deny Maximum: 1047
Daily MMimm: 1047
4"e No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PNPIPPIrlir-
DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 58050 00400 C0530 00940 00094
j g 1 1
8
i i
pub.
a g
1 Monthly Monthly Monthly Quarterly Monthly
u' d d Instantaneous Grab Grab Grab Grab
A u 4O 2 PLOW pH Tss-One CHLORIDE CNDUCTVY
2400 dude Hn 2409 dock Hn V/BM mgd su mg/I mg/1 umhos/cm
1 0730 8 Y 1.122 7.53 <2.5 1039
2 0730 8 Y
3 0730 8 Y
4 N
5 N
6 0730 8 Y •
7 0730 8 Y
a 0730 8 Y
9 0730 8 Y
le 0730 4 Y
It N
12 N
13 0730 8 Y
14 0730 8 Y
15 0730 8 Y
16 0730 8 Y
17 0730 8 Y
is N
19 N
20 0730 8 Y
21 0730 8 Y
22 0630 8 Y
23 0630 8 B
24 0730 8 Y
25 N
26 N
27 0730 8 Y
20 0730 8 Y
,Marbly Avenge IJdt:Mo
Meathy A.er.gn 1.122 0 1039
Daily Maximum: 1.122 7.53 0 1039
Daily Mtalsm. 1.122 7.53 0 1039
ee'6 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

Prillir
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION:1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:03/22/2017
62'�L.i
lf_ i?i1_1
03/22/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part Il.E.6 of
the NPDES permit.
ilAt"LiPj 03/22/2017
Permittee/Submitter Signature:*** Michael Paul M Gowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Asheville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

IIIIIIIIIPP° r
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:02-2017(February 2017) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Weekly Sample for 5th week,pH and DO was collected March 1st,2017 for that week.

a
S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 RMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 R EC E IVEpUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis MAR 0 6 2017 ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No CENTRAL FILES RECEIVEDINCDENRIDWR
eDMR PERIOD:01-2017(January 2017) VERSION: 1_0 DWR SECTION STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*:,,dos
MOORESVILLE REGIONAL OFFICE
• 50050 00400 C0319 C0330 00300 C0600 C0665 09940 THP3B
A 1 . a •
II Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly .Monthly
3` $t.
8 k Recorder Grab Grab Grab Grab Grab Grab Grab Composite
C$ 8 CU
S O tS O 2 FLOW pH BOD-Cone TES-Cow DO TOTAL N- TOTAL P-Cane CHLORIDE CER7DCHV
2400 dock Hn 2401 dodr }In Y/BIN mgd su mg/1 mg/1 mg/1 mg/I mg/I mg/1 percent
1 0 N 0
2 0 Y HOLIDAY
3 0730 8 Y 0
4 0730 8 Y 0
s 0730 8 Y 0
6 0730 8 Y 0.234 7.8 <2 <12.5 10.76 0.9 <0.05 84.9
7 0 N 0.432
8 0 N 0.432
9 0730 8 Y 0.432
10 0730 8 Y 0.429
it 0730 8 Y 0.439 8 14.2
12 0730 8 Y 0.439
13 0730 8 Y 0.439
14 0 N 0.439
15 0 N 0.439
16 0 N HOLIDAY
17 0730 8 Y 0.443
10 0730 8 Y 0.446 8.1 <2.8 14.2
19 0730 8 Y 0.446 >100
20 0730 8 Y 0.446
21 0 N 0.446
22 0 N 0.446
23 0730 8 Y 0.446
24 0730 8 Y 0.446
23 0730 8 Y 0.461 8.1 11.6
26 0730 8 Y 0.446
—
27 0730 8 Y 0.446
28 0 N 0.446
29 0 N 0.446
30 0730 8 Y 0.446
31 0730 8 Y 0.446
Me lky Average Limit: MI5 30 30
Moodily Avenge: 0.374345 0 0 12.69 0.9 0 84.9 100
Dray Maalem.. 0.461 8.1 0 0 _14.2 0.9 0 84.9 100
Day Miolmamo 0 7.8 0 0 10.76 0.9 0 84.9 100
aaea No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2017(January 2017) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
00054 TGP3B
F
¢ a
u Monthly Quarterly
e t- i
u 8 Ia rt Grab Grab
y Q v
d v F O A CNDUCTVY CERI7DPP
2188 deck W. 2400 dodo tin Y/a/N umhos/cm pass/fail
I 0 N
2 0 Y HOLIDAY
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6 0730 8 Y 1026
7 0 N
8 0 N
e 0730 8 Y
18 0730 8 Y
11 0730 8 Y
12 0730 8 Y
13 0730 8 Y
14 0 N
15 0 N
16 0 N HOLIDAY
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
20 0730 8 Y
21 0 N
22 0 N
23 0730 8 Y
24 0730 8 Y
25 0730 8 Y
26 0730 8 Y
27 0730 8 Y
28 0 N
22 0 N
30 0730 8 Y
31 0730 8 Y
Meathly Average Limit:
MeaIlly Average 1026
Daily Maximum: 1026
Daily Menem: 1026
*0*0 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2017(January 2017) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
50040 00400 C0530 00940 00094
A A A A '
d
i I r Monthly Monthly Monthly Quarterly Monthly
u 8 Instantaneous Grab Grab Grab Grab
a 3 c
S U' F O L FLOW pH IRS-Case CHLORIDE CNDUCfYY
2480 dock Hr. 2408 clock Hn YBIN mgd su mg/I mg/I umhos/cm
1 0 N
2 0 N HOLIDAY
3 0730 8 Y
4 0730 8 Y 0.933 7.5 5.2 32.6 797
5 0730 8 Y
6 0730 8 Y
7 0 N
a 0 N
9 0730 8 Y
to 0730 8 Y
II 0730 8 Y
12 0730 8 Y
13 0730 8 Y
14 0 N
IS 0 N
Iii 0 N HOLIDAY
17 0730 8 Y
is 0730 8 Y
19 0730 8 Y
2a 0730 8 Y
21 0 N
22 0 N
23 0730 8 Y
24 0730 8 Y
25 0730 8 Y
24 0730 8 Y
S7 0730 8 Y
2s 0 N
29 0 N
39 0730 8 Y
31 0730 8 Y
Monthly Average Limit:
Meath Avenge: 0.933 5.2 32.6 797
Dray at.amk.o. 0.933 7.5 5.2 32.6 797
Daily Mlsmnek: 0.933 7.5 5.2 32.6 797
a"a No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2017(January 2017) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:02/27/2017
02/24/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
02/27/2017
Permittee/Submitter Signature:*** ichael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Corporation,Pace Asheville,R&A Lab
CERTIFIED LAB#:5023,40,14
PERSON(s)COLLECTING SAMPLES:Rodney S Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:01-2017(January 2017) VERSION: 1.0 STATUS:Processed
OutftII 001-Effluent Comments:
Due to Lab error for TSS Sample collected on 1/6/16 resulting in a high reportable limt of 12.5,one additional sample was collected and is reported here.Therefore a total of 3
TSS samples were collected and reported for the montH.
Report Correction Needed,CER7DCHV should be Quarterly not Monthly

3
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 RECEIVED PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
FEB 0 2 2017
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER: 30 EIVEDMCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:No CENTRAL FILES
— DWR SECTION ,5 - £i '''J17
eDMR PERIOD:12-2016(December 2016) VERSION: 1.0 STATUS:Processed
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCWQM tEGIONAL OFFICE
• 50050 00400 C0530 00940 11194
1
I a a
'� A i Monthly Monthly Monthly Quarterly Monthly
< 14
a �. Instantaneous Grab Grab Grab Grab
a
C U F a a
O 24 FLOW pH TES-Cone CHLORIDE CNDUCTVY
2400 dock Hn 2400 dock Hn Y/BIN mgd su mg/I mg/I umhos/cm
1 0730 8 Y
2 0730 8 Y
3 N
4 N
5 0730 8 Y
6 0730 8 Y
0900 0730 8 Y 1.122 7.42 <2.5 956
8 0730 8 Y
9 0730 8 Y
10 N
It N
12 0730 8 Y
13 0730 8 Y
14 0730 8 Y
IS 0730 8 Y
16 0700 8 B
17 N
IS 1338 1230 2 Y 0.063 7.91 <2.5 35.8 1054
19 0700 8 B
2g 0730 8 Y
21 0730 8 Y
22 0730 8 Y
23 0700 8 B
24 N
25 N
26 N HOLIDAY
27 0700 8 B
20 0730 8 Y
29 0730 8 Y
30 0700 8 B
31 N
Mosby Average Link:
Monthly AvengCO 0.5925 0 35.8 1005
Daily Ma ® 1.122 7.91 0 35.8 1054
Daily Minnow 0.063 7.42 0 35.8 956
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

VNPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2016(December 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES
gp y y $ • 50080 00400 C0310 C0830 00300 C0600 C0665 00940 THP3B
F q F a
I
¢ 8
® 1 'a 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
u 8` d e Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a a 1
a U F 1 0 29 FLOW pH BOD•Cone TSS-Cone DO TOTAL N.. TOTAL P-Cone CHLORIDE CER7DCHY
2400 dock Hn 2400 dock His Y/WN mgd su mg/I mg/1 mg/I mg/I mg/1 mg/I percent
1 0730 8 Y NOFLOW
2 0730 8 Y NOFLOW
3 N NOFLOW
4 N NOFLOW
5 0730 8 Y NOFLOW
6 0730 8 Y NOFLOW
7 0730 8 Y NOFLOW
8 0730 8 Y NOFLOW
9 0730 8 Y NOFLOW
II N NOFLOW
II N NOFLOW
12 0730 8 Y NOFLOW
13 0730 8 Y NOFLOW
14 0730 8 Y NOFLOW
15 0730 8 Y NOFLOW
16 0700 8 B NOFLOW
17 N NOFLOW
I0 1230 2 Y NOFLOW
19 0700 8 B NOFLOW
m 0730 8 Y NOFLOW
21 0730 8 Y NOFLOW
22 8 B NOFLOW
23 N HOLIDAY
24 N NOFLOW
25 N NOFLOW
26 N HOLIDAY
27 0700 8 B NOFLOW
28 0730 8 Y NOFLOW
29 0730 8 Y NOFLOW
30 0700 8 B NOFLOW
31 N NOFLOW
Monthly Avenge L It: 0.615 39 30
Monty Avenge:
Daily Maximum:
Daily Moowm:
t999 No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PNPDEPVF-
S PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:12-2016(December 2016) VERSION:1.0 STATUS:Processed
•
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
041094
1 7 a
E. 2C i i Monthly
lal 8` 8` 8 d Grab
S I ): ctwucrvY
MOO deck Hn 26911 desk Hn Y/BIN umhos/cm
I 0730 8 Y NOFLOW
2 0730 8 Y NOFLOW
3 N NOFLOW
4 N NOFLOW
5 0730 8 Y NOFLOW
6 0730 8 Y NOFLOW
7 0730 8 Y NOFLOW
8 0730 8 Y NOFLOW
9 0730 8 Y NOFLOW
to N NOFLOW
II N NOFLOW
12 0730 8 Y NOFLOW
13 0730 8 Y NOFLOW
14 0730 8 Y NOFLOW
IS 0730 8 Y NOFLOW
16 0700 8 B NOFLOW
• 17 N NOFLOW
18 1230 2 Y NOFLOW
19 0700 8 B NOFLOW
28 0730 8 Y NOFLOW
21 0730 8 Y NOFLOW
22 8 B NOFLOW
23 N HOLIDAY
24 N NOFLOW
25 N NOFLOW
26 N HOLIDAY
27 0700 8 B NOFLOW
2s 0730 8 Y NOFLOW
29 0730 8 Y NOFLOW
30 0700 8 B NOFLOW
31 N NOFLOW
Monthly Avenge Usk:
Monthly Average:
Dray MuMsm:
Daily hUNInvalon
e•ie No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

ilPry
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 12-2016(December 2016) VERSION: 1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant �� CONTACT PHONE#:[phone] SUBMISSION DATE:01/27/2017
62Z--\4A._)j99.. __ 01/26/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
44/i-r-yet j dc.44_,(
/0/rm./L.,
01/27/2017
Permittee/Submitter Signature:* Mic el Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC
CERTIFIED LAB#:5023
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 12-2016(December 2016) VERSION: 1.0 STATUS:Processed
Report Comments:
Outfall 001 had no discharge for the month.
Outfall 004 Sample collected on 12/18/2017 was during a represenative storm event. Total rainfall was 0.2".

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 12-2016(December 2016) VERSION: 1.0 STATUS:Processed
Outfall 004-Effluent Comments:
Sample collected on 12/18/2017 was during a represenative storm event. Total rainfall was 0.2". e-DMR does not allow for BOD and TPH on form. They are listed here.
Results are BOD<2.0 mg/I, TPH<5.0 mg/I.
A Qualitative Monitoring Report was aslo completed during the storm event of 12/18/16

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2REC COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis LIVED
ORC CERT NUMBER: 624-
GRADE:PC-2 ORC HAS CHANGED:No JAN 04 201/
eDMR PERIOD:11-2016(November 2016) VERSION: 1.0 CENTRAL FILES STATUS:Processed
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
80050 00400 C0310 C0530 00300 C0640 C0665 00840 THP3a
8 ;
i y Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
7uu a ad3 el Recorder Grab Grab Grab Grab Gab Grab Grab Composite
8 aI- 1 I O A FLOW pH DOD-Caw T88-Cow DO TOTAL N- TOTAL P-Caw CHLORIDE CER7DCHV
2400 deck Has 2400 Hoek Has YHVH mgd sit mg/I mg/I mg/I mg/I mg/I mg/I percent
I 0730 8 Y 0.115 2.7
2 0730 8 Y 0.094 7.8 <2.6 6.7
3 0700 8 B NOFLOW
4 0700 8 B NOFLOW
5 N NOFLOW
6 N NOFLOW
7 0700 8 B NOFLOW
8 0700 8 B NOFLOW
8 0700 8 B NOFLOW
II 0700 8 B NOFLOW
II 0700 8 B NOFLOW
12 N NOFLOW
13 N NOFLOW
14 0700 8 B NOFLOW
IS 0700 8 B NOFLOW
16 0700 8 B NOFLOW
17 0700 8 B NOFLOW
Is 1530 I Y NOFLOW
I0 N NOFLOW
2s N NOFLOW
21 0730 8 Y NOFLOW
22 0730 8 Y NOFLOW
23 0700 8 B NOFLOW
24 N HOLIDAY
25 N HOLIDAY
26 N NOFLOW
27 N NOFLOW
28 0730 8 Y NOFLOW
29 0730 8 Y NOFLOW
30 0730 8 Y NOFLOW
i
Monthly Avenge Limit 0.615 30 30
Moatky Average: 0.1045 1.35 6.7
Daly Maximum. 0.115 7.8 2.7 6.7
Daly MYlmum. 0.094 7.8 0 6.7
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2016(November 2016) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
j
a
i I Monthly
u gI
I
a i Grab
a
S z CNDUCTVY
2400 dock Hn 2480 deck Hn YBIN umhos/cm
1 0730 8 Y
2 0730 8 Y 1129
3 0700 8 B NOFLOW
4 0700 8 B NOFLOW
5 N NOFLOW
6 N NOFLOW
7 0700 8 B NOFLOW
0 0700 8 B NOFLOW
8 0700 8 B NOFLOW
10 0700 8 B NOFLOW
11 0700 8 B NOFLOW
12 N NOFLOW
13 N NOFLOW
16 0700 8 B NOFLOW
15 0700 8 B NOFLOW
16 0700 8 B NOFLOW
17 0700 8 B NOFLOW
18 1530 I Y NOFLOW
If N NOFLOW
20 N NOFLOW
21 0730 8 Y NOFLOW
22 0730 8 Y NOFLOW
23 0700 8 B NOFLOW
24 N HOLIDAY
u N HOLIDAY
26 N NOFLOW
27 N NOFLOW
2B 0730 8 Y NOFLOW
29 0730 8 Y NOFLOW
70 0730 8 Y NOFLOW
Moodily Avenge Limb:
Monthly Avenger 1129
Dolly Msahnwn 1129
Daily M61mo . 1129
••6*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2016(November 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: YES
50050 00400 CO530 00940 00094
A
d
! < A L Monthly Monthly Monthly Quarterly Monthly
c.: 2 a Instantaneous Grab Grab Grab Grab
y I 0u�O S u 1 i FLOW OH Tsa-Coto CHLORIDE CNDUCIVY
2400 dock Hn 2400 deck Hn Y/BM mgd su mg/I mg/I umhos/cm
I 0730 8 Y NOFLOW
2 0730 8 Y NOFLOW
3 0700 8 B NOFLOW
4 0700 8 B NOFLOW
S N NOFLOW
6 N NOFLOW
7 0700 8 B NOFLOW
O 0700 8 B NOFLOW
9 0700 8 B NOFLOW
10 0700 8 B NOFLOW
II 0700 8 B NOFLOW
12 N NOFLOW
13 N NOFLOW
14 0700 8 B NOFLOW
15 0700 8 B NOFLOW
16 0700 8 B NOFLOW
17 0700 8 B NOFLOW
10 0730 I Y NOFLOW
19 N NOFLOW
n N NOFLOW
21 0730 8 Y NOFLOW
22 0730 8 Y NOFLOW
23 0700 8 B NOFLOW
24 N HOLIDAY
25 N HOLIDAY
26 N NOFLOW
27 N NOFLOW
29 0700 8 Y NOFLOW
29 0700 8 Y NOFLOW
J0 0700 8 Y NOFLOW
Monthly Avenge Limit:
Monthly Avenge:
Dolly Maximum:
Davy Mehemet:
""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Slough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2016(November 2016) VERSION:1.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:12/21/2016
LJdit,, I2/21/2016
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part 11.E.6 of
the NPDES permit.
1�
12/21/2016
Permittee/Submitter Signature:** Michael Paul McGowan E-Mail:paul.mcgowan(a?fmc.com Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:Pace
•
CERTIFIED LAB#:40
PERSON(s)COLLECTING SAMPLES:Rodney S Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permitter,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(bX2)(D).

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2016(November 2016) VERSION: 1.0 STATUS:Processed
Report Comments:
Dicontinued discharge of 001 on 11/2/16
No discharge occured at outfall 004 for month

rNPDESiiiiiiiiiiir
PERMIT NO.:NC0005177
PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 11-2016(November 2016) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
Flow stopped through outfall 001 11/2/16 at 10:50 am.
Note:Parameter code THP3B should be quaterly by permit. On this form lists as monthly.
Monhtly BOD analysis inadvertently missed.
As a follow up to completing the November 2016 DMR I realized that I had inadvertently missed the monthly BOD sample/analysis and would ask that you take into
consideration the following information. On Monday October 31st due to drought conditions experienced at that time it was decided to discontinue discharging from our
equalization pond,outfall 001. Upon arriving Tuesday November 1st I realized the weekly sampling of pH and DO had not been completed. Therefore the pond discharge was
restarted in order to obtain the weekly samples. Realizing in addition to the weekly analysis I would now need to obtain 2-monthly TSS samples and 1-conductivity. The TSS
samples were collected on 11/1 and 11/2 and the weekly pH and DO and monthly conductivity on 11/2. Upon completing the field analysis and collecting the TSS samples the
discharge was stopped. Unfortunately during this process the BOD was inadvertently missed. I would like to point out that a BOD sample was collected on October 12 with
results of 3.1 mg/land given the retention time of the equalization pond it is reasonable to assume that the BOD concentration would be comparable to that of the October sample.
Historically BOD has never been a problem for this outfall.
As of the date of this letter outfall 001 is still off. Depending on weather conditions and plant production the discharge may be restarted in January.

PNPDESlir
PERMIT NO.:NC0005177
PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:11-2016(November 2016) VERSION: 1.0 STATUS:Processed
Outfall 004-Effluent Comments:
No dischagred occured at 004 for month of November

Re., Skz OC.T. 2OIb
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.ORECEIVED PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis FEB 02 2017 ORC CERT NUMBER:28624 RECEIVED/NCDENR/DWR
GRADE:PC-2 ORC HAS CHANGED:NoCENTRAL FILES =I- H 6 /117
eDMR PERIOD: 10-2016(October 2016) VERSION:2.0 DVVR SECTION STATUS:Processed
WQROS
MOORESVILLE REGIONAL OFFII
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
• 30000 00400 C0310 C0530 00300 C0600 C0665 00940 THP3D
C a 1 Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
e `
4 E d 8 Recorder Grab Grab Grab Grab Grab Grab Grab Composite
a 1 t' 1 g A V Z FLOW pH BOD-Cow TDD-Cow DO TOTALN- TOTALP-Caw CHLORIDE CER7DCHV
2400 dock His 2400 clock Hn WWI mgd su mg/I mg/I mg/1 mg/I mg/1 mg/I percent
t N 0
2 N 0
3 0730 8 Y 0
4 0730 8 Y 0
5 0730 8 Y 0
6 0700 8 B 0
7 0730 8 Y 0
0 N 0
9 N 0
to 0730 8 Y 0
tt 0730 8 Y 0.242
t2 0730 8 Y 0.426 6.9 3.1 <2.7 8 0.48 <0.05 93.4
13 0730 8 Y 0.431
14 0700 8 B 0.431 ,
15 N 0.431
t6 N 0.431
Cr 0730 8 Y 0.43
10 0730 8 Y 0.431 >100
19 0730 8 Y 0.427 7.8 7.4
20 0730 7 Y 0.436
21 0730 8 Y 0.429
22 N 0.429
23 N 0.429
24 0730 8 Y 0.429
25 0730 8 Y 0.435
26 0730 7 Y 0.408 7.6 <4.7 7.3
27 0730 8 Y 0.42
20 0700 8 B 0.42
29 N 0.42
30 N 0.422
31 0730 8 Y 0.422
Meetly Average Link: 0.615 30 30
Monthly Avenue: 0.283194 3.1 0 7.566667 0.48 0 93.4 100
Daily Madera. 0.436 7.8 3.1 0 8 0.48 0 93.4 100
D.13 Milkman: 0 6.9 3.1 0 7.3 0.48 0 93.4 100
0*0*No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2016(October 2016) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
• 00094 TGP3B
gg A A
I 8
a < I
g Monthly Quarterly
I $ 1 ! 8 I Grab Grab
a I CI g u
8 U 1 O 5 o Z' CNDUCTVY cERI7DPF
2400 dock Hn 2400 deck /In Y/BMN umhos/cm pass/fail
1 N
2 N
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6 0700 8 B
7 0730 8 Y
s N
9 N
to 0730 8 Y
1l 0730 8 Y
12 0730 8 Y 1072
13 0730 8 Y
14 0700 8 B
15 N
16 N
17 0730 8 Y
is 0730 8 Y
19 0730 8 Y
20 0730 7 Y
21 0730 8 Y
22 N
23 N
24 0730 8 Y
25 0730 8 Y
26 0730 7 Y
27 0730 8 Y
29 0700 8 B
29 N
30 N
31 0730 8 Y
Monthly Avenge Unit:
Monthly Avenge: 1072
Dnar Masimnm: 1072
Daily Mebane: 1072
****No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2016(October 2016) VERSION:2.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
• 50050 00400 C0534 00940 00094
A
8
a7 ® i ) *I � Monthly Monthly Monthly Quarterly Monthly
u' 1pub a 1 Instantaneous Grab Grab Grab Grab
3
d� Fe I I 1 O £ FLOW pH TSS-Cone CHLORIDE CNDUCTVY
2400 clods Hn 2400 deck Hn Y/&N mgd su mg/I mg/I umhos/cm
1
2
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6 0700 8 B
7 0730 8 Y
a
9
10 0730 8 Y
II 0730 8 Y •
12 0730 8 Y 0.063 7.18 <2.5 29.8 841
13 0730 8 Y
14 0700 8 B
I5
16
17 0730 8 Y
HI 0730 8 Y
19 0730 8 Y
20 0730 8 Y
21 0730 8 Y
22
23
24 0730 8 Y
25 0730 8 Y
26 0730 8 Y
27 0730 8 Y
25 0700 8 B
29
30
31 0730 8 Y
Maelkly Avenge Unit
Monthly Avenge: 0.063 0 29.8 841
Duly Maim. 0.063 7.18 0 29.8 841
Day
Mama: 0.063 7.18 0 29.8 841
eeee No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather, NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2016(October 2016) VERSION:2.0 STATUS:Processed
COMPLIANCE STATUS:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:01/27/2017
01/26/2017
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
,i(AiLitiasz/0
01/27/2017
Permittee/Submitter Signature. ** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Labs Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2016(October 2016) VERSION:2.0 STATUS:Processed
Report Comments:
No discharge occured for outfall 001 until 10/10/16 for month

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2016(October 2016) VERSION:2.0 STATUS:Processed
Outfall 001-Effluent Comments:
REVISION 1/26/17
lnadvertatly recorded CER7DCHV on 10/12/16. Revised sample collection/results date of CER7DCHV to 10/18/16,

3
DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
RECEIVEDiNCDENR/DWR
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No N O V 1 6 c/0 i 6
eDMR PERIOD: 10-2016(October 2016) VERSION: 1.0 STATUS:Processed
V.'
MOORES'll_LE REC'O."•!A!OFFIC
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
a i 1 50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP3B
y P.
a .
ci 6 < rn i E Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
o t `n n
U l! Vi)
Recorder Grab Grab Grab Grab Grab Grab Grab Composite
0 tJ F O 0 0 Z FLOW pH SOD-Cone TSS-Cone DO TOTAL N. TOTAL P- CHLORIDE CER7DCHV
2400 dock firs 2400 deck Hn Y/B/N mgd su mg/1 mg/I mg/1 mg/1 mg/1 mg/1 percent
I N 0
2 N 0
3 0730 8 Y 0
4 0730 8 Y 0
5 0730 8 Y 0
6 0700 8 B 0
7 0730 8 Y 0
8 N 0
9 N 0
10 0730 8 Y 0
11 0730 8 Y 0.242
12 0730 8 Y 0.426 6.9 3.1 <2.7 8 0.48 <0.05 93.4 >100
13 0730 8 Y 0.431
14 0700 8 B 0.431
15 N 0.431
16 N 0.431
17 0730 8 Y 0.43
18 0730 8 Y 0.431
19 0730 8 Y 0.427 7.8 7.4
20 0730 7 Y 0.436
21 0730 8 Y 0.429
22 N 0.429
23 N 0.429
24 0730 8 Y 0.429
25 0730 8 Y 0.435
26 0730 7 Y 0.408 7.6 <4.7 7.3
27 0730 8 Y 0.42
28 0700 8 B 0.42
29 N 0.42
30 N 0.422
31 0730 8 Y 0.422
Monthly Average Limit: 0.615 30 30
Monthly Average: 0.283194 3.1 0 7.566667 0.48 0 93.4 100
Daily Maximum: 0.436 7.8 3.1 0 8 0.48 0 93.4 100
Daily Minimum: 0 6.9 3.1 0 7.3 0.48 0 93.4 100
o•o'No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday
RECEIVED
NOV 092016
CENTRAL FILES
DWR SECTION

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2016(October 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
z 00094 TGP3B
$ s a
6
s e F g i I Monthly Quarterly
a It
c i I Gran Grab
O t I- F° O O O i CNDUCTVY CERI7DPF
2400 dock Hra 2400 clock Urn Y/B/N umhos/cm pass/fail
t N
2 N
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6 0700 8 B
7 0730 8 Y
8 N
9 N
10 0730 8 Y
11 0730 8 Y
12 0730 8 Y 1072
13 0730 8 Y
14 0700 8 B
15 N
16 N
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
20 0730 7 Y
21 0730 8 Y
22 N
23 N
24 0730 8 Y
25 0730 8 Y
26 0730 7 Y
27 0730 8 Y
28 0700 8 B
29 N
30 N
31 0730 8 Y
Monthly Average Limit:
Monthly Average: 1072
Daily Maximum: 1072
Daily Minimum: ton
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

DES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:10-2016(October 2016) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: NO
6 I 50050 00400 C0530 00940 00094
I d
a r
6 (-� m 1 Monthly Monthly Monthly Quarterly Monthly
S e $ e e
g �' C 1 11 Instantaneous Grab Grab Grab Grab
C u F" i2 O S. O Z FLOW pH TSS-Cone CHLORIDE CNDUCTVY
2400 dock firs 2400 dock Hrs Y/B/N mgd su mg/1 mg/I umhos/cm
1
2
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6 0700 8 8
7 0730 8 Y
8
9
10 0730 8 Y
I1 0730 8 Y
12 0730 8 Y 0.063 7.18 <2.5 29.8 841
13 0730 8 Y
14 0700 8 B
l5
16
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
20 0730 8 Y
21 0730 8 Y
22
23
24 0730 8 Y
25 0730 8 Y .
26 0730 8 Y
27 0730 8 Y
28 0700 8 B
29
30
31 0730 8 Y
Monthly Average Limit
Monthly Average: 0.063 0 29.8 841
Daily Maximum: 0.063 7.18 0 29.8 841
Daily Minimum: 0.063 7.18 0 29.8 841
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2016(October 2016) VERSION: 1.0 STATUS:Processed
COMPLIANCE:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 11/01/2016
11/01/2016
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
11/01/2016
Permittee/Submitter Signatu :*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC,Pace Labs Ashville
CERTIFIED LAB#:5023,40
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

PDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD: 10-2016(October 2016) VERSION: 1.0 STATUS:Processed
Report Comments:
No discharge occured for outfall 001 until 10/10/16 for month

3
NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No RECEIVED/NCDENR/DWR
eDMR PERIOD:09-2016(September 2016) VERSION: 1.0 STATUS:Processed
NOV — 7 ,.u16
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*I: i►'iEjS
MOORESVILLE REGIONAL OFFICE
iR 50050 00400 C0310 C0530 00300 C0600 C0665 00940 THP38
1 1 n ,
9 < 1
a - m Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
'a e a 8 a
& G.) C V u Recorder Grab Grab Grab Grab Grab Grab Grab Composite
0 U I: l 0 0 0 Z FLOW pH BOD-Cone TSS-Cone DO TOTAL N- TOTAL P- CHLORIDE CER7DCHV
2400 clock Hra 2400 clock Hrs V/B/N mgd su mg/1 mg/l MA mg/1 mg/I mg/I percent
1 0730 8 Y 0
2 0730 8 Y 0 RECEIVED
3 0 N 0
4 0 ,N 0 NOV 0 2 2016
5 0 N HOLIDAY
6 0730 8 Y 0 CENTRAL FILES
7 0730 8 Y 0 DWR SECTION
8 0700 8 B 0
9 0700 8 B 0
10 0 N 0
11 0 N 0
12 0730 8 Y 0
13 0730 8 Y 0
14 0730 8 Y 0
15 0730 8 Y 0
16 0730 8 Y 0
17 0 N 0
18 0 N 0
19 0700 8 B 0
20 0730 6 Y 0
21 0700 8 B 0
22 0700 8 B 0
23 0700 8 B 0
24 0 N 0
25 0 N 0
26 0730 8 Y 0
27 0730 8 Y 0
28 0730 8 Y 0
29 0700 8 B 0
30 0700 8 B 0
Monthly Average Limit: 0.05 30 30
Monthly Average: 0
Daily Maximum: 0
Daily Minimum: 0
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENV WTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2016(September 2016) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
al 00094
9 < l: 7, i : Monthly
e 1 3 C 8 $ Grab
o c 1: F' 0 0 C Z t" CNDUCrVY
2400 dock Hrs 2400 clock Hrs Y/B/N umhos/cm
1 0730 8 Y
2 0730 8 Y
3 0 N
4 0 N
5 0 N HOLIDAY
6 0730 8 Y
7 0730 8 Y
8 0700 8 B
9 0700 8 B
10 0 N
II 0 N
12 0730 8 Y __- _
13 0730 8 Y
14 0730 8 Y _
15 0730 8 Y
16 0730 8 Y
17 0 N
18 0 N
19 0700 8 B __
20 0730 6 Y
21 0700 8 B
22 0700 8 B
23 0700 8 B
2A 0 N
25 0 N
26 0730 8 Y
27 0730 8 Y
28 0730 8 Y
29 0700 8 B
30 0700 8 B
Monthly Average Limit:
Monthly Average:
---Daily Maximum:
Daily Minimum:
"""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2016(September 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGE*: YES
al 50050 00400 C0530 00940 00094
a f a S
I E 1 a
S e < F: in i ' Monthly Monthly Monthly Quarterly Monthly
I U ° S
r4g Instantaneous Grab Grab Grab Grab
C U l: E O O O Z at FLOW pH TSS-Conc CHLORIDE CNDUCIVY
2400 dock Hra 2400 clock Hrs Y/B/N mgd su mg/1 mg/I umhos/cm
1 0730 8 Y
2 0730 8 Y
3 0 N
4 0 N
5 0 N HOLIDAY
6 0730 8 Y
7 0730 8 Y
8 0700 8 B
9 0700 8 B
10 N
11 N
12 0730 8 Y
13 0730 8 Y
14 0730 8 Y
15 0730 8 Y
16 0730 8 Y
17 N
18 N
19 0700 8 B
20 0730 6 Y
21 0700 8 B
22 0700 8 B
23 0700 8 B
24 N
25 N
26 0730 8 Y
27 0730 8 Y
28 0730 8 Y
29 0700 8 B
30 0700 8 B
Monthly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
'ts"No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

NPDES PERMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
FACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:09-2016(September 2016) VERSION: 1.0 STATUS:Processed
COMPLIANCE:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE: 10/26/2016
611.
/(.. W 1►J��^� 10/25/2016
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
(tojej
10/26/2016
Permittee/Submitter Signat re:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC-Lithium
CERTIFIED LAB#:NC01237
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

IT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
LITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston �2)
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No RECEIVED/NCDENR/DWR
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed 0 C T — 3 2016
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 004 NO DISCHARGrigNel
OORESVILLE REGIONAL OFFICE
Y w
8 i in 50050 00400 C0530 00940 00094
[-
8 7
■ 0 o ea
6 ` F ti Monthly Monthly Monthly Quarterly Monthly
I e •
U w cs g 3 Instantaneous Grab Grab Grab Grab
el
G U' I-. 1-° O O O 'z° d FLOW pH TSS-Cone CHLORIDE CNDUCTVY
2400 clock Hrs 2400 clock Hrs Y/B/N mgd su mg/1 mg/1 umhos/cm
1 0730 8 B
2 0730 8 Y
3 0730 8 Y 1.703 7.01 3.1 26.4 589
4 0730 8 Y RECEIVEC
0730 8 Y RECEIVEC
6
7 SEP 23 2016
$ 0730 8 Y
CEN1 RAL FILES
9 0730 8 Y DWR SECTION'
10 0730 8 Y
11 0730 8 Y
12 0730 8 Y
13
14
15 0730 8 Y
16 0730 8 Y
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
-
20
21
22 0730 8 Y
33 0730 8 Y
24 0730 8 Y .
25 0730 8 Y
26 0730 8 Y
27
28
29 0730 8 Y
30 0730 8 Y
31 0730 8 Y
Monthly Average Limit
Monthly Average: 1703 3.1 26.4 589
Daily Maximum: 1.703 7.01 3.1 26.4 589
Daily Minimum: 1.703 7.01 3.1 26.4 589
* $No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation-Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation-Holiday

MIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES
r
g 9 e 50050 00400 C0310 C0530 ;00300 C0600 C0665 00940 THP3B
u 7 0
6 Iso
E. < •o ' Continuous Weekly Monthly 2 X month Weekly Quarterly Quarterly Quarterly Monthly
e I
e
® U ' g Recorder Grab Grab Grab Grab Grab Grab Grab Composite
C U F. F 0 0O z° H FLOW pH BOD-Cone TSS-Cone DO TOTALN- TOTAL P- CHLORIDE CER7DCHV
2400 clock Hn 2400 dock Hrs Y/B/N mgd su mgA mgA mg/I mg/I mgA mg/I percent
t 0730 8 B
2 0730 8 Y
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6
7
8 0730 8 Y
9 0730 8 Y
10 0730 8 Y
II 0730 8 Y
12 0730 8 Y
13
14
15 0730 8 Y
16 0730 8 Y
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
20
21
22 0730 8 Y
23 0730 8 Y - - - --- _ - -- - _ --- - - - - - . - -
24 0730 8 Y
25 0730 8 Y
26 0730 8 Y
27
•
28
29 0730 8 Y
30 0730 8 Y
31 0730 8 Y
Monthly Average Limit 0.615 30 30
Monthly Average:
Daily Maximum:
Daily Minimum:
••••No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

MIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION:1.0 STATUS:Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: YES (Continue)
Y .Y.
® � e 00094
ft. 0 % o
€ I L I 9 :
gY < F �, • Monthly
3 Y V i ` S i e Grab
O u F I- O O O Z M CNDUCTVY
2400 dock Bra 2400 clock Hrs Y/B/N umhos/cm
1 0730 8 B
2 0730 8 Y
3 0730 8 Y
4 0730 8 Y
5 0730 8 Y
6
7
8 0730 8 Y
9 0730 8 Y
l0 0730 8 Y
11 0730 8 Y
12 0730 8 Y
13
14
15 0730 8 Y
16 0730 8 Y
17 0730 8 Y
18 0730 8 Y
19 0730 8 Y
20
21
22 0730 8 Y
23 0730 8 Y
24 0730 8 Y
25 0730 8 Y
26 0730 8 Y
27
28
29 0730 8 Y
30 0730 8 Y
31 0730 8 Y
Monthly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
•°° No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed
SAMPLING LOCATION: INFLUENT DISCHARGE NO.: 001
. F e
a o
E v C9 .
m 8 e F 'rii
E B 3 o. cee
A U f F O O O z°
2400 clock Hrs 2400 clock Hrs Y/B/N
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Monthly Average Limit:
Monthly Average:
Daily Maximum:
Daily Minimum:
s""No Reporting Reason:ENFRUSE=No Flow-Reuse/Recycle; ENVWTHR=No Visitation—Adverse Weather; NOFLOW=No Flow; HOLIDAY=No Visitation—Holiday

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed
COMPLIANCE:Compliant CONTACT PHONE#:[phone] SUBMISSION DATE:09/16/2016
rCj)—jlJ )LL .J., 09/15/2016
ORC/Certifier Signature: Rodney Stough Willis E-Mail:[e-mail] Phone #:[phone] Date
By this signature,I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances.A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
Aitjj j,i,t9L,
09/16/2016
Permittee/Submitter Signature:*** Michael Paul McGowan E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:NC Hwy 161 Bessemer City NC 28016 Permit Expiration Date:08/31/2015
I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted.Based on my inquiry of the person or persons who managed the
system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME:FMC Corporation Lithium Dvision
CERTIFIED LAB#:5023
PERSON(s)COLLECTING SAMPLES:Rodney Willis
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit(919)807-6300 or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
*No Flow/Discharge From Site:Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
**ORC on Site?:ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee:If signed by other than the permittee,then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
ACILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY':Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed
Outfall 001-Effluent Comments:
No Discharge for outfall 001 for month of August

RMIT NO.:NC0005177 PERMIT VERSION:4.0 PERMIT STATUS:Expired
CILITY NAME:Lithium Division Plant CLASS:PC-2 COUNTY:Gaston
OWNER NAME:FMC Corporation ORC:Rodney Stough Willis ORC CERT NUMBER:28624
GRADE:PC-2 ORC HAS CHANGED:No
eDMR PERIOD:08-2016(August 2016) VERSION: 1.0 STATUS:Processed
Outfall 001-Influent Comments:
This page was created in error. No influent exists in permit

EFFLUENT 3 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH July YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED I I NO FLOW/DISCHARGE FROM SITE* n
a):)....._
'
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER (SIGNATURE OF OPER TOR IN RESPOSIBLE CHARGE)
RALEIGH, NC 27699-1617 BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00300 00094 00530 C0310 C0600 00940 C0665 THP3B TGP3B RE �IAIC
UW i� FLOW Enter Parameter Code U)
a 0 F W Above Name and Units Z C►
a W EFT © Below 9 I- 0 - >. >+ 2 to tt,,
O
a o . a z oo INFO > <n 0 z Z 0 2 m co
o W °W' 0 0 t1 = 0 46 ~ m 3 +
U c��a [� m MOOREoVILLE PROS
a. P o R a ci z GIORIAL OFFICE
0 0
I-
HRS HRS Y/B/N MGD units _ mg/I umho mg/I mg/I mg/I mg/I mg/I ChV% P or F
1 7:30 8.0 Y 0.000
2 --- 0.0 N 0.000 A
3 --- 0.0 N 0.000 +'
4 7:30 8.0 Y 0.000 `""C.`..; .. . .2 L'
5 7:30 8.0 Y 0.000
6 7:30 8.0 Y 0.000 Q�6 p s ?�1B 4�.' , 2. 3 't,i'"
7 7:30 8.0 Y 0.000 !+
8 7:30 8.0 Y 0.000NI -+ •. :'+_. i;..-':
9 --- 0.0 N 0.000 ME" LVVK t.,I ION
10 --- 0.0 N 0.000
11 7:30 8.0 Y 0.000
12 7:30 8.0 Y 0.000
13 7:30 8.0 Y 0.000
14 7:30 8.0 Y 0.000
15 6:30 8.0 B 0.000 No Discharge Occured duringthe month of July
16 --- 0.0 N 0.000
17 --- 0.0 N 0.000
18 7:30 8.0 Y 0.000
19 7:30 8.0 Y 0.000
20 7:30 8.0 Y 0.000 ��
21 7:30 8.0 Y 0.000
22 7:30 8.0 Y 0.000
23 --- 0.0 N 0.000 A U 12 5 D IF
24 --- 0.0 N 0.000
25 7:30 8.0 Y 0.000
26 7:30 7.0 Y 0.000
27 7:30 8.0 Y 0.000
28 6:30 8.0 B 0.000
29 6:30 8.0 B 0.000
30 --- 0.0 N 0.000
31 --- 0.0 N 0.000 _
AVERAGE 0.000
MAXIMUM 0.000
MINIMUM 0.000
Comp.(C)Grab(G) Cont. G G G G G G G G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0 NA _ NA NA 78%
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
I AlUSI Zola
Signature of ermi e*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 PauI.McGowan(cfmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 004 MONTH July YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
CERTIFIED LABORATORIES(1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED I NO FLOW/DISCHARGE FROM SITE* I I
Mail ORIGINAL and ONE COPY to: > A, 0 k
ATTN:CENTRAL FILES (SIGNATURE OF OP ATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
a 50050 00400 00095 100530 00940
> e. FLOW
rzd O W Enter Parameter Code Above
Qy-I `� F EFF Q Name and Units Below J
Q p � Fz INF ❑ O
O G
} w 2
yF O 0 J ~ Q. -0 U
O p 0
0
HRS HRS jY/BfN MGD units umho mg/I mg/I
1 7:30 8.0 Y
2 --- 0.0 N
3 --- 0.0 N
4 7:30 8.0 Y
5 7:30 8.0 Y
6 7:30 8.0 Y 0.199 7.6 810 <2.5 26.8
7 7:30 8.0 Y
8 7:30 8.0 Y
9 --- 0.0 N
10 --- 0.0 N
11 7:30 8.0 Y
12 7:30 8.0 Y
13 7:30 8.0 Y
14 7:30 8.0 Y
15 6:30 8.0 B
16 --- 0.0 N
17 --- 0.0 N
18 7:30 8.0 Y
19 7:30 8.0 Y
20 7:30 8.0 Y
21 7:30 8.0 Y
22 7:30 8.0 Y
23 --- 0.0 N
24 --- 0.0 N
25 7:30 8.0 Y
26 7:30 7.0 Y
27 7:30 8.0 Y
28 6:30 8.0 B
29 6:30 8.0 B
30 --- 0.0 N
31_ --- 0.0 N
AVERAGE 0.199- 810 0.0 26.8
MAXIMUM 0.199 7.6 810 <2.5 26.8
MINIMUM 0.199 7.6 810 <2.5 26.8
Comp.(C)Grab(G) Cont. G G G G
Monthly Limit NA 6.0-9.0 NA NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or, pe)
iajl/ If 0s/.Zol�
Signature of Permit a*** Date
(Required unless su mitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 Pa_ul.McGowan • fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES •
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 3 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH June YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED Q NO FLOW/DISCHARGE FROM SITE* n
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES ,J
a 1,6...L.
DIVISION OF WATER QUALITY 1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR IN RESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617 BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
60060 00400 00300 00094 00530 C0310
Uis FLOW Enter Parameter Code
0 H c' Above Name and Units
EFr' El Below
v
d x F B
I- o ' °�' z INF ❑ U) 0
z
o E.
w ° o0 >- w = O .8 ~ m
w 0-. o --II- ad a
of om 0
WG
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/Ir
1 7:30 8.0 Y 0.395 8.1 7.8 1023 <2.7 <2.0 A�;I� 2J16 REte v
2 7:30 8.0 Y 0.395
3 11:00 5.0 Y 0.395 JUL 't 6 ZVi6
4 --- 0.0 N 0.395
5 --- 0.0 N 0.395 CENTRAL FILLS
DWR SECTION
6 7:30 8.0 Y 0.395
7 7:30 8.0 Y 0.395
8 7:30 8.0 Y 0.406 8.1 7.2
9 7:30 8.0 Y 0.407
10 7:30 8.0 B 0.407
11 --- 0.0 N 0.407
12 --- 0.0 N 0.413 GA
13 7:30 8.0 Y 0.413 _
14 7:30 8.0 Y 0.413 A!1 ; ; ..
15 7:30 8.0 Y 0.173 8.3 7.5 <2.8
16 7:30 8.0 Y 0.000
17 7:30 8.0 Y 0.000
18 --- 0.0 N 0.000
19 --- 0.0 N 0.000
20 7:30 8.0 Y 0.000
21 7:30 8.0 Y 0.000
22 7:30 8.0 Y 0.000 REC7_11''is ' ; %,. , ,i
23 7:30 8.0 Y 0.000
24 7:30 8.0 Y 0.000 .
25 --- 0.0 N 0.000 ,
26 --- 0.0 N 0.000 WQRUS
27 7:30 8.0 Y 0.000 MOOR=SVILLE REGIONAL OFFICE
28 7:30 8.0 Y 0.000
29 7:30 8.0 Y 0.000
30 7:30 8.0 Y 0.000
31 0.000
AVERAGE 0.187- 7.5 1023 0.0 0.0
MAXIMUM 0.413 8.3 7.8 1023 <2.8 <2.0
MINIMUM 0.000 8.1 7.2 1023 <2.7 <2.0
Comp.(C)Grab(G) Cont. G G G G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print o type)
Zz 1u11 Zol (0
Signatur of Permitte ** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 PauI.McGowan@,fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance'may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 004 MONTH June YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
CERTIFIED LABORATORIES(1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED r7 NO FLOW I DISCHARGE FROM SITE*
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00095 00530
FLOW
O r`sj Enter Parameter Code Above
U o EFF Name and Units Below
p z o INF ❑
w � ci >- w 2
F0 o 1 a H
O p E U
HRS HRS Y/B/N MGD units umho mg/I
1 7:30 8.0 Y 0.135 7.9 787 <2.5
2 7:30 8.0 Y
3 11:00 5.0 Y
4 --- 0.0 N
5 --- 0.0 N
6 7:30 8.0 Y
7 7:30 8.0 Y
8 7:30 8.0 Y
9 7:30 8.0 Y
10 7:30 8.0 B
11 --- 0.0 N
12 --- 0.0 N
13 7:30 8.0 Y
14 7:30 8.0 Y
15 7:30 8.0 Y
16 7:30 8.0 Y
17 7:30 8.0 Y
18 --- 0.0 N
19 --- 0.0 N
20 7:30 8.0 Y
21 7:30 8.0 Y
22 7:30 8.0 Y
23 7:30 8.0 Y
24 7:30 8.0 Y
25 --- 0.0 N
26 --- 0.0 N
27 7:30 8.0 Y
28 7:30 8.0 Y
29 7:30 8.0 Y
30 7:30 8.0 Y
31
AVERAGE 0.135rE 787 0.0
MAXIMUM 0.135 7.9 787 <2.5
MINIMUM 0.135 7.9 787 <2.5
Comp.(C)Grab(G) Cont. G G G
Monthly Limit NA 6.0-9.0 NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please prin:or type)
1J
�ZJ)(1 2Dao
Signa re of Pe ttee ** * Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 3 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO 004 MONTH May YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
CERTIFIED LABORATORIES(1) FMC Corp. Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED a NO FLOW/DISCHARGE FROM SITE*
Mail ORIGINAL and ONE COPY to: �/
CENTRAL FILES Q (SIGNATURE/OF OPERA OR INRESPOSIBLE CHA GE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 JUL 1 2 201EkCCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00095 100530 RECEIVED
v + FLOW Enter Parameter Code ,n l G
O Gj Above Name and Units Y v
Below
� xF � EFF �7 JJ� 05tu��
o INF ❑ JJL 11 2016
cn CENTRAL FILES
DWR SECTION
a, F O 0 Jp d F- CL c
0 0
HRS HRS Y/B/N MGD units umho mg/I
1 --- 0.0 N
2 7:30 8.0 Y
3 7:30 8.0 Y
4 7:30 8.0 Y 0.653 7.8 779 <2.5
5 7:30 8.0 Y
6 7:30 8.0 Y
7 --- 0.0 N
8 --- 0.0 N
9 7:30 8.0 Y
10 6:30 8.0 B
11 7:30 8.0 Y
12 7:30 8.0 Y
13 7:30 8.0 Y
14 --- 0.0 N
15 --- 0.0 N
16 7:00 8.0 Y
17 7:00 8.0 Y
18 7:15 8.0 Y
19 7:30 8.0 Y
20 6:30 8.0 B
21 --- 0.0 N
22 --- 0.0 N
23 6:30 8.0 B
24 6:30 8.0 B
25 7:30 4.0 Y
26 6:30 8.0 B
27 6:30 8.0 B
28 --- 0.0 N
29 --- 0.0 N
30 7:30 8.0 Y
31 7:30 8.0 Y
AVERAGE 0.653 -: ;" 779 0.0
MAXIMUM 0.653 7.8 779 <2.5
MINIMUM 0.653 7.8 779 <2.5
Comp.(C)Grab(G) Cont. G G G
Monthly Limit NA 6.0-9.0 NA NA _
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee Please print , type)
Signa e of erm. tee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 Paul.McGowan(@fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH May YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED Q NO FLOW/DISCHARGE FROM SITE* n
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617 BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
60060 00400 00300 100094 00530 C0310
UW FLOW Enter Parameter Code
rgO �`,,j Above Name and Units
d 0 S F En' © Below
a 8 N < z o INF ❑ > u) o
a a0 O J H a. q I- co
O F O O
U
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I
1 --- 0.0 N 0.420
2 7:30 8.0 Y 0.420
3 7:30 8.0 Y 0.425
4 7:30 8.0 Y 0.429 8.3 8.2 1167 4.6 <2.0
5 7:30 8.0 Y 0.406
6 7:30 8.0 Y 0.410
7 --- 0.0 N 0.410
8 --- 0.0 N 0.410
9 7:30 8.0 Y 0.412
10 6:30 8.0 B 0.413
11 7:30 8.0 Y 0.413 8.2 8.8
12 7:30 8.0 Y 0.413
13 7:30 8.0 Y 0.413
14 --- 0.0 N 0.413
15 --- 0.0 N 0.415
16 7:00 8.0 Y 0.416
17 7:00 8.0 Y 0.406
18 7:15 8.0 Y 0.415 8.2 8.9 3.1
19 7:30 8.0 Y 0.413
20 6:30 8.0 B 0.412
21 --- 0.0 N 0.413
22 --- 0.0 N 0.418
23 6:30 8.0 B 0.425
24 6:30 8.0 B 0.428
25 7:30 4.0 Y 0.432 8.1 8.7
26 6:30 8.0 B 0.400
27 6:30 8.0 B 0.399
28 --- 0.0 N 0.403
29 --- 0.0 N 0.403
30 7:30 8.0 Y 0.406
31 7:30 8.0 Y 0.413
AVERAGE 0.414-- 8.6 1167 3.9 0.0
MAXIMUM 0.432 8.3 8.9 1167 4.6 <2.0
MINIMUM 0.399 8.1 8.2 1167 <3.1 <2.0
Comp.(C)Grab(G) Cont. G G G G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or t e)
Zo j v�i_ Zo
Stgna re of Permi1,1/()
* Date
(Required unless sed electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 Paul.MC GowanAfmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 1 of 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH April YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED El ^NO FLOW/DISCHARGE eIIITE• n
Mail ORIGINAL and ONE COPY to: , ifs
ATTN:CENTRAL FILES
1 (..A.....)35%:AS.,
DIVISION OF WATER QUALITY (.71
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617 BY SIGNATURE,1 CERTIFY THA'I"PHIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
a 50050 00400 100300 00094 00530 C0310 C0600 00940 C0665 THP3B TGP3B
C_) W * FLOW Enter Parameter Code ` ;7; C - -
O kj Above Name and Units Z O
z NN' © Below U) o M v 0 N h
Q OFN dz O > 0) 0 ZZ
0 t f_6 CO
dW OW U } IL = v I m T + L d O O
a. 0w 0 I- p - in m
Fo CO ¢
0
Z 0 CAI.: ,
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I mg/I mg/I mg/I ChV% P or F
1 7:30 8.0 Y 0.432 ' �_it. .LI.VED
2 --- 0.0 N 0.432
3 --- 0.0 N 0.435 MAY 2 4 Lib
4 7:30 8.0 Y 0.438
5 7:30 8.0 Y 0.438 f „v." . ,L. ^;i"`
f'r
6 7:30 8.0 Y 0.439 8.1 9.1 1229 <3.8 <2.0 <0.12 121 <0.050
7 7:30 8.0 Y 0.439 ,
8 7:30 8.0 Y 0.433
9 --- 0.0 N 0.432
10 --- 0.0 N 0.432
11 7:30 8.0 Y 0.428
12 7:30 8.0 Y 0.433
13 7:30 8.0 Y 0.429 8.1 9.7
14 7:30 8.0 Y 0.429 >100 " -
15 7:30 8.0 Y 0.426 N.r-' ..-_- • _ (
16 --- 0.0 N 0.425
17 --- 0.0 N 0.420 MA`' 2 b' 2016
18 7:30 8.0 Y 0.420
19 7:30 8.0 Y 0.420 r,r}rRltfc r,
20 7:00 8.0 Y 0.420 8.2 9.8 3.1
21 7:00 8.0 Y 0.420
22 7:00 8.0 Y 0.420
23 --- 0.0 N 0.422
24 --- 0.0 N 0.420
25 7:30 8.0 Y 0.420
26 7:30 8.0 Y 0.423
27 7:30 8.0 Y 0.422 8.2 8.8
28 7:30 8.0 Y 0.418
29 6:30 8.0 B 0.415
30 --- 0.0 N 0.418
31
AVERAGE 0.427 w 9.3 1229 1.6 0.0 0.00 121 0.000 >100
MAXIMUM 0.439 8.2 9.8 1229 3.1 <2.0 <0.12 121 <0.050 >100
MINIMUM 0.415 8.1 8.8 1229 <3.8 <2.0 <0.12 121 <0.050 >100
Comp.(C)Grab(G) Cont. G G G G GGG G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0 NA NA NA 78%
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
Z(4 L, I/ M/3y Zo c C,
Signature of Permittee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 PauI.McGowan0,fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO 004 MONTH April YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp. Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED I=1 NO FLOW/DISCHARGE FROM SITE* n
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT'IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00095 100530 00940
J * FLOW Enter Parameter Code
0 Above Name and Units
E m EFL,' r-i Below N
1- z o o z INF c
Q hry o
o O W = U (n t
O O 0 -Ig Q. ~ V
a
� U
HRS HRS 1Y/B/N MGD units umho mg/I mg/I
1 7:30 8.0 Y
2 --- 0.0 N
3 --- 0.0 N
4 7:30 8.0 Y
5 7:30 8.0 Y
6 7:30 8.0 Y 0.350 8.0 921 <2.5 25.4
7 7:30 8.0 Y
8 7:30 8.0 Y
9 --- 0.0 N
10 --- 0.0 N
11 7:30 8.0 Y
12 7:30 8.0 Y
13 7:30 8.0 Y
14 7:30 8.0 Y
15 7:30 8.0 Y
16 --- 0.0 N
17 --- 0.0 N
18 7:30 8.0 Y
19 7:30 8.0 Y
20 7:00 8.0 Y
21 7:00 8.0 Y
22 7:00 8.0 Y
23 --- 0.0 N
24 --- 0.0 N
25 7:30 8.0 Y
26 7:30 8.0 Y
27 7:30 8.0 Y
28 7:30 8.0 Y
29 6:30 8.0 B
30 --- 0.0 N
31
AVERAGE 0.350 ^` 921 0.0 25.4
MAXIMUM 0.350 8.0 921 <2.5 25.4
MINIMUM 0.350 8.0 921 <2.5 25.4
Comp.(C)Grab(G) Cont. G GGG
Monthly Limit NA 6.o-9.o NA NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
'k'( i l� iW4-y zol�
Signature of Permitt *** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 Pau_(.McGowan [e-mail] 8/31/2015
Pennittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH March YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis,Michael Dehart ORC PHONE [phone]
CHECK BOX IF ORC HAStaNGED Q NO FLOW/DISCHARGE FROM SITE*
Mail ORIGINAL and ONECOPY to ijATTN CENTRALFILES � 212016
DIVISION OF WATER NTilI'PY
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH, NC 27699-1617 BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00300 100094 00530 C0310
UW * FLOW Enter Parameter Code
O a It? EFT © Above Name and Units PECEIV:11:
Below
° z 1.0
I- o INF ❑ ow o o o o 0 CF Jn •¢ V woRFS`/'' c • i O11ICE
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I -- --
1 7:30 8.0 Y 0.445
2 7:30 8.0 Y 0.432 8.2 10.1 1133 3.3 <2.0 n C
3 7:30 7.0 Y 0.425 K
016
4 7:30 8.0 Y 0.428
5 --- 0.0 N 0.429 I, .,•
6 --- 0.0 N 0.432
7 7:30 8.0 Y 0.436
8 7:00 9.0 Y 0.443
9 7:30 8.0 Y 0.451 8.2 10.8
10 7:30 8.0 Y 0.446
11 7:30 8.0 Y 0.439
12 --- 0.0 N 0.439
13 --- 0.0 N 0.441
14 7:30 10.0 Y 0.441
15 7:30 8.0 Y 0.443
16 7:00 8.0 B 0.446 8.1 8.4 2.9
17 7:30 8.0 Y 0.435
18 7:30 8.0 Y 0.433
19 --- 0.0 N 0.432
20 --- 0.0 N 0.431
21 7:30 12.0 Y 0.429
22 7:30 11.0 Y 0.432 OA
23 7:00 10.0 Y 0.436 8.0 9.6
24 7:30 8.0 Y 0.425
25 --- 0.0 H 0.425 a P 1 t. 2 2 11
26 --- 0.0 N 0.425
27 --- 0.0 N 0.426
28 7:30 8.0 Y 0.426
29 7:30 8.0 Y 0.428
30 7:30 8.0 Y 0.435 8.2 9.4
31 7:30 8.0 Y 0.432
AVERAGE 0.434 = 9.7 1133 3.1 0.0
MAXIMUM 0.451 8.2 10.8 1133 3.3 <2.0
MINIMUM 0.425 8.0 8.4 1133 2.9 <2.0
Comp.(C)Grab(G) Cont. G G G G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
.4(Gizol(o
Signature of Permitte ** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO 004 MONTH March YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
CERTIFIED LABORATORIES (1) FMC Corp. Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED Q NO FLOW I DISCHARGE FROM SITE* I I
Mail ORIGINAL and ONE COPY to: f A�
ATTN:CENTRAL FILES (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
50050 00400 00095 100530
> o * FLOW Enter Parameter Code
x 0 -. Uj Above Name and Units
• U a F EFF Below
Qo 7) INF ❑
F 0 O O c I-
O 2 U
HRS HRS IY/B/N MGD units umho mg/I
1 7:30 8.0 Y
2 7:30 8.0 Y 0.720 8.0 801 <2.6
3 7:30 7.0 Y
4 7:30 8.0 Y
5 --- 0.0 N
6 --- 0.0 N
7 7:30 8.0 Y
8 7:00 9.0 Y
9 7:30 8.0 Y
10 7:30 8.0 Y
11 7:30 8.0 Y
12 --- 0.0 N
13 --- 0.0 N
14 7:30 10.0 Y
15 7:30 8.0 Y
16 7:00 8.0 B
17 7:30 8.0 Y
18 7:30 8.0 Y
19 --- 0.0 N
20 --- 0.0 N
21 7:30 12.0 Y
22 7:30 11.0 Y
23 7:00 10.0 Y
24 7:30 8.0 Y
25 --- 0.0 H
26 --- 0.0 N
27 --- 0.0 N
28 7:30 8.0 Y
29 7:30 8.0 Y
30 7:30 8.0 Y
31 7:30 8.0 Y
AVERAGE 0.720 801 0.0
MAXIMUM 0.720 8.0 801 <2.6
MINIMUM 0.720 8.0 801 <2.6
Comp.(C)Grab(G) Cont. G G G
Monthly Limit NA 6.0-9.o NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or pe)
4 )
Signa re of Permitte ** Date 4/6/C,
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 PauI.McGowan(a.fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

/ P 7 f j c F/LF
NCO ' Sift EFFLUENT 2OF2
NPDES PERMIT NO NC 0005177 DISCHARGE NO 004 MONTH February YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED n NO FLOW/DISCHARGE FROM SITE* 1]
Mail ORIGINAL and ONE COPY to: a LA......);32L--1
ATTN:CENTRAL FILES (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT ISEc Er`.' i•.;,-i,-
RALEIGH,NC 27699.1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
.a 60050 00400 00095 100530 C0310 00940 45501
> J al
�. FLOW Enter Parameter Code E 0 RECEIVED/NCD,E. IDWR
5 0 :l �7 Above Name and Units 7 c
x U `' ,z] F' E�,'�,' LZJ Below a) N 0 - :C
xF �' � � MAR142�16
~ 0 , � z 0 INF ❑ 0 O N co
Qo t., `'
0 a � w 2 " m 0_ o
F 0 o D u) v ai ;, Water Quaky
3.0 0 I Permitting Section
HRS HRS V/B/N MGD units umho mg/I mg/I mg/I mg/I
1 7:30 8.0 Y
2 7:30 8.0 Y
3 7:30 8.0 Y 0.525 7.4 870 <2.6 <2.0 22.0 <5.0 Sample collected on 2/3/16 was -
4 7:30 8.0 Y during a Represenative Storm Event. -
5 7:30 8.0 Y Total Rainall 0.30"
7 --- 0.0 N
8 7:30 8.0 Y
9 7:30 8.0 Y
10 7:30 8.0 Y
11 7:30 8.0 Y
12 7:30 8.0 Y
13 --- 0.0 N
14 --- 0.0 N
15 7:30 8.0 Y
16 7:30 8.0 Y
17 7:30 8.0 Y
18 7:30 8.0 Y
19 7:30 8.0 Y
20 --- 0.0 N
21 --- 0.0 N
22 7:00 8.0 B
23 7:00 8.0 B
24 7:15 8.0 B
25 7:30 8.0 Y
26 7:30 8.0 Y
27 --- 0.0 N
28 --- 0.0 N _
29 7:30 8.0 Y
30
31 .
AVERAGE 0.525 M 870 0.0 0.0 22.0 0.0
MAXIMUM 0.525 7.4 870 <2.6 <2.0 22.0 <5.0
MINIMUM 0.525 7.4 870 <2.6 <2.0 22.0 <5.0
Comp.(C)Grab(G) Cont. G GGGGG
Monthly Limit NA 6.0-9.0 NA NA 30.0 NA 15.0
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
44.1i Pe201C.
Signature of ittee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH February YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis,Michael Dehart ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED Q NO FLOW/DISCHARGE FROM SITE* n
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617 BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
60050 00400 00300 100094 00530 C0310 C0600 00940 C0665
U ;,4 .1c FLOW Enter Parameter Code
0 F W F Above Name and Units Z
V ENT © Below N 1- t
w xo O � � (n aL o� U uO.
I-
° N ¢ Z o INF > u) O zZ o 2
° 0 u � w O 5 I- coLo + L a
w ° 0 -II' a 0 o O
P. P. O Q g c � �
0 [L U F-
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I mg/I mg/I mg/I
1 7:30 8.0 Y 0.448
2 7:30 8.0 Y 0.446
3 7:30 8.0 Y 0.446 7.4 11.7 1149 4.0 <2.0 <0.12 107 <0.050
4 7:30 8.0 Y 0.443
5 7:30 8.0 Y 0.443
6 --- 0.0 N 0.439
7 --- 0.0 N 0.439
8 7:30 8.0 Y 0.436
9 7:30 8.0 Y 0.436
10 7:30 8.0 Y 0.446 7.2 11.6
11 7:30 8.0 Y 0.445
12 7:30 8.0 Y 0.443
13 --- 0.0 N 0.442
14 --- 0.0 N 0.439
15 7:30 8.0 Y 0.438
16 7:30 8.0 Y 0.431
17 7:30 8.0 Y 0.436 7.9 12.3 3.2
18 7:30 8.0 Y 0.431
19 7:30 8.0 Y 0.435
20 --- 0.0 N 0.438
21 --- 0.0 N 0.443
22 7:00 8.0 B 0.448
23 7:00 8.0 B 0.445
24 7:15 8.0 B 0.446
25 7:30 8.0 Y 0.446 8.2 11.1
26 7:30 8.0 Y 0.431
27 --- 0.0 N 0.432
28 --- 0.0 N 0.432
29 7:30 8.0 Y 0.442
30
31
AVERAGE 0.440_ 11.7 1149 3.6 0.0 0.00 107 0.000
MAXIMUM 0.448 8.2 12.3 1149 4.0 <2.0 <0.12 107 <0.050
MINIMUM 0.431 7.2 11.1 1149 3.2 <2.0 <0.12 107 <0.050
Comp.(C)Grab(G) Cont. G G G G G G G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0 NA NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
yarlb•-• mitizoi.
Signature of Pei u tee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 PauI.McGowan a fmc.com 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Pace Charlotte Certification No. 12
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

;lJ-//i�- F, I. r S'
fJ C -)O d /4'=i- EFFLUENT
3
20F2
,RMIT NO NC 0005177 DISCHARGE NO 004 MONTH February YEAR 2016
ITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II GASTON
RTIFIED LABORATORIES (1) FMC Corp. Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED O NO FLOW/DISCHARGE FROM SITE*
Mail ORIGINAL and ONE COPY to: aa�Q /
ATTN:CENTRAL FILESEt ��//w ��-'"' i , .. n,Ii?
DIVISION OF WATER QUALITY (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
1617 MAIL SERVICE CENTER mAF . > 20ifT BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
60060 00400 00095 100530 C0310 00940 45501 t' _, i'�i=
> .d al
> CD * FLOW Enter Parameter Code
d F.
r Er r=i 1, 0 Above Nameio and Units 0 O
o R INF ❑ o -0 e RECE VED/NCDEQIDWR
"Ss mac' -eo ° 5 p o m °
a F.� w } u, I 0° °' MAR ] 4 ?flt
o ° J ~ a ' H
° o � U I0 I
Water Ouait,
HRS HRS iY/B/N MGD units umho mg/I mg/I mg/I mg/I Permitting Sec ion
1 7:30 8.0 Y
2 7:30 8.0 Y
3 7:30 8.0 Y 0.525 7.4 870 <2.6 <2.0 22.0 <5.0 Sample collected on 2/3/16 was -
4 7:30 8.0 Y during a Represenative Storm Event. -
5 7:30 8.0 Y Total Rainall 0.30" -
6 --- 0.0 N --- -
7 --- 0.0 N
8 7:30 8.0 Y
9 7:30 8.0 Y R CEIV EID
10 7:30 8.0 Y
11 7:30 8.0 Y MAK I ' .LUII
12 7:30 8.0 Y
13 --- 0.0 N �., N 1 KA r r i LEIS
14 --- 0.0 N �1N!Z Qr 7.T10N
15 7:30 8.0 Y
16 7:30 8.0 Y
17 7:30 8.0 Y
18 7:30 8.0 Y
19 7:30 8.0 Y
20 --- 0.0 N
21 --- 0.0 N
22 7:00 8.0 B
23 7:00 8.0 B
24 7:15 8.0 B ��
25 7:30 8.0 Y
26 7:30 8.0 Y
27 --- 0.0 N 4611; 1 720 ► .
28 --- 0.0 N
29 7:30 8.0 Y
30
31
AVERAGE 0.525- 870 0.0 0.0 22.0 0.0
MAXIMUM 0.525 7.4 870 <2.6 <2.0 22.0 <5.0
MINIMUM 0.525 7.4 870 <2.6 <2.0 22.0 <5.0
Comp.(C)Grab(G) Cont. G G GGGG
Monthly Limit NA 6.0-9.0 NA NA 30.0 NA 15.0
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
441064j16
Signature of Pe nittee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per I5A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 1 OF 2
MIT NO NC 0005177 DISCHARGE NO. 001 MONTH February YEAR 2016
TY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
TIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willie,Michael Dehart ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED n NO FLOW/DISCHARGE FROM SITE* n
Mail ORIGINAL and ONE COPY to:
ATI'N:CENTRAL FILES au
DIVISION OF WATER QUALITY 1
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617 BY SIGNATURE, I CERTIFY THAT PHIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
-- .� 60060 00400 100300 00094 00530 C0310 C0600 00940 C0665
U W * FLOW Enter Parameter Code co
c cGj Above Name and Units Z 8
U a it" cnt EFF ® Below y 1- N t ,6
p8 °m 7 1NF ❑ cn p ° � c u) r �c 7rync
gW o o >, w = 0 'u I- 0 ZZ o CL x / LU�Q
aE. ao o J ~ a p CO To
0 a
To
o Q g o ~ Z o
U
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I mg/I mg/I mg/I
1 7:30 8.0 Y 0.448
2 7:30 8.0 Y 0.446
3 7:30 8.0 Y 0.446 7.4 11.7 1149 4.0 <2.0 <0.12 107 <0.050
4 7:30 8.0 Y 0.443
5 7:30 8.0 Y '. 0.443
6 --- 0.0 N 0.439
7 --- 0.0 N 0.439
8 7:30 8.0 Y 0.436
9 7:30 8.0 Y 0.436
10 7:30 8.0 Y 0.446 7.2 11.6
11 7:30 8.0 Y 0.445
12 7:30 8.0 Y 0.443
13 --- 0.0 N 0.442
14 --- 0.0 N 0.439
15 7:30 8.0 Y 0.438
16 7:30 8.0 Y 0.431
17 7:30 8.0 Y 0.436 7.9 12.3 3.2
18 7:30 8.0 Y 0.431
19 7:30 8.0 Y 0.435
20 --- 0.0 N 0.438
21 --- 0.0 N 0.443
22 7:00 8.0 B 0.448
23 7:00 8.0 B 0.445 _
24 7:15 8.0 B 0.446
25 7:30 8.0 Y 0.446 8.2 11.1
26 7:30 8.0 Y 0.431
27 --- 0.0 N 0.432
28 --- 0.0 N 0.432
29 7:30 8.0 Y 0.442
30
31
AVERAGE 0.440_ 11.7 1149 3.6 0.0 0.00 107 0.000
MAXIMUM 0.448 8.2 12.3 1149 4.0 <2.0 <0.12 107 <0.050
MINIMUM 0.431 7.2 11.1 1149 3.2 <2.0 <0.12 107 <0.050
Comp.(C)Grab(G) Cont. G G G G GGG G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0 NA NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
'fit 7 Mkao zo i
Signature of Pe tee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Pennittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Pace Charlotte Certification No. 12
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wcis and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DM R for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 3 1 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO. 001 MONTH January YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp.Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis,Mike Dehart ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED n NO FLOW/DISCHARGE.FROM SITE'. :c
Mail ORIGINAL and ONE COPY to:
ATTN:CENTRAL FILES A i 14-=x.
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
RALEIGH,NC 27699-1617
FEB p 2016n BY SIGNATURE,I CERTIFY THAN."T1 JS REPORT_ IS -V
ACCURATE AND COMPLETE TO THE BEST OF KNOWLEDGE
a 50050 00400 100300 100094 00530 C0310 C0600 00940 C0665 THP3B TGP3B
C..) * FLOW Enter Parameter Code 7
O - w Above Name and Units Z
v E" w mt EFF © Below at 1- co2 >. >.
LU o: F to + -0 Q CO (6
A o ° N z INF ❑ U) o ° o o to to
z
0 o W w ° 0 >- = 0 .0 ~ m o + .E a o 0
w T. O � H . p - F°- N U m m m
0 F ° Q d U Z 0
O
HRS HRS Y/B/N MGD units mg/I umho mg/I mg/I mg/I mg/I mg/I ChV% P or F
1 --- 0.0 H 0.480
2 --- 0.0 N 0.480 R i.- - IV t: D
3 --- 0.0 N 0.480 V Lo
4 7:30 8.0 Y 0.480 EL I 14 La 16
5 7:30 8.0 Y 0.497 ,
6 7:30 8.0 Y 0.450 7.4 10.4 1143 3.3 <2.0 <0.12 116 <0.050 C EN r k A i F: LES
7 7:30 8.0 Y 0.448 DWR QECT.ON
8 7:30 8.0 Y 0.448
9 --- 0.0 N 0.448
10 --- 0.0 N 0.449
11 7:30 8.0 Y 0.449
12 7:30 8.0 Y 0.449
13 7:30 8.0 Y 0.446 7.6 11.7
14 7:30 8.0 Y 0.461 >100
15 7:30 8.0 Y 0.445
16 --- 0.0 N 0.445
17 --- 0.0 N 0.446
18 --- 0.0 H 0.445
19 7:30 8.0 Y 0.446 lJ A
20 7:00 8.0 B 0.445 7.3 12.7 <2.6 , FEB 2 2 Z 016
21 7:00 8.0 B 0.448
22 7:00 8.0 B 0.445
23 --- 0.0 N 0.446
24 --- 0.0 N 0.448
25 7:30 8.0 Y 0.449
26 7:30 8.0 Y 0.439
27 7:30 8.0 Y 0.442 6.9 12.5
28 7:30 8.0 Y 0.442
29 7:30 8.0 Y 0.442
30 --- 0.0 N 0.442
31 --- 0.0 N 0.442
AVERAGE 0.452 S 11.8 1143 1.7 0.0 0.00 116 0.000 >100
MAXIMUM 0.497 7.6 12.7 1143 3.3 <2.0 <0.12 116 <0.050 >100
MINIMUM 0.439 6.9 10.4 1143 <2.6 <2.0 <0.12 116 <0.050 >100
Comp.(C)Grab(G) Cont. G G G G GGG G G
Monthly Limit 0.615 6-9 >5.0 NA 30.0 30.0 NA NA NA 78%
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
lirvi.A__
/4/ /Sfr'g to(L
Signature of Permit a*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Research and Analytical Certification No. 14
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).

EFFLUENT 2 OF 2
NPDES PERMIT NO NC 0005177 DISCHARGE NO 004 MONTH January YEAR 2016
FACILITY NAME FMC CORPORATION/LITHIUM DIVISION CLASS II COUNTY GASTON
CERTIFIED LABORATORIES (1) FMC Corp. Lithium Div. CERTIFICATION NO. 5023
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPOSIBLE CHARGE (ORC) Rodney S.Willis GRADE II CERTIFICATION NO. PC 28624
PERSON(S) COLLECTING SAMPLES Rodney Willis ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED Q NO FLOW/DISCHARGE FROM SITE* I I
Mail ORIGINAL and ONE COPY to:
ATTN CENTRAL FILES (SIGNATURE OF OPERATOR INRESPOSIBLE CHARGE)
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER BY SIGNATURE,I CERTIFY THAT THIS REPORT IS
RALEIGH,NC 27699-1617 ACCURATE AND COMPLETE'1'O THE BEST OF KNOWLEDGE
50050 00400 00095 100530 00940
> " * FLOW Enter Parameter Code
0 csj Above Name and Units
d F • EFF Below
:17 i =
Q p � � z o INF ❑ �'
0 oga FEB I 9 2010
U
HRS HRS YB/N MGD units umho mg/I mg/I .
•
1 --- 0.0 H
2 --- 0.0 N
3 --- 0.0 N
4 7:30 8.0 Y
5 7:30 8.0 Y
6 7:30 8.0 Y 0.686 7.5 719 3.8 12.5
7 7:30 8.0 Y
8 7:30 8.0 Y
9 --- 0.0 N
10 --- 0.0 N
11 7:30 8.0 Y
12 7:30 8.0 Y
•
13 7:30 8.0 Y
14 7:30 8.0 Y
15 7:30 8.0 Y
16 --- 0.0 N
17 --- 0.0 N
18 --- 0.0 H
19 7:30 8.0 Y
20 7:00 8.0 B
21 7:00 8.0 B
22 7:00 8.0 B
23 --- 0.0 N
24 --- 0.0 N
25 7:30 8.0 Y
26 7:30 8.0 Y
27 7:30 8.0 Y
28 7:30 8.0 Y
29 7:30 8.0 Y
30 --- 0.0 N
31 --- 0.0 N
AVERAGE 0.68611. 719 3.8 12.5
MAXIMUM 0.686 7.5 719 3.8 12.5
MINIMUM 0.686 7.5 719 3.8 12.5
Comp.(C)Grab(G) Cont. G G G G
Monthly Limit NA 6.0-9.o NA NA NA
DEM Form MR-1 (01/00)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages,if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware
If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based
Paul McGowan
Permittee (Please print or type)
' tJ IS-f V)g o
Signature of ermittee*** Date
(Required unless submitted electronically)
Box 795 Bessemer City,NC 28016 704-868-7610 [e-mail] 8/31/2015
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory(2) Pace Ashville Certification No. 40
Certified Laboratory(3) Certification No.
Certified Laboratory(4) Certification No.
Certified Laboratory(5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).