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HomeMy WebLinkAboutWI0400035_Monitoring (Report)_20050419`v a � rn rn cnc Quarterly HRC Monitoring Report Fairchild Industrial Products Company Winston-Salem, North Carolina Trigon Project No. 015-04-014 ENGINEERING CONSULTANTS, INC. 2 St 119P-201 Anniversary www.trigoneng.com P.O. Box 18846 • Zip 27419-8846 • 313 Gallimore Dairy Road • Greensboro, NC 27409 • p 336.668.0093 • f 336.668.3868 April 14, 2005 Mr. J. Michael Ranck UIC Program Aquifer Protection Section Aquifer CD North Carolina DENR - DWQ s" ro 1636 Mail Service Center Raleigh, North Carolina 27699-1636 Reference: Quarterly HRC Monitoring Report 3 Fairchild Industrial Products Company tv ; Winston-Salem, North Carolina tv " Trigon Project No. 015-04-014 Dear Mr. Ranck: Trigon Engineering Consultants, Inc. (Trigon) is pleased to provide this quarterly monitoring report for the Underground Injection Control (UIC) Permit for treatment of groundwater with Hydrogen Release Compound (HRC) at the referenced site. Enclosed is a copy of the report for your review. Should you have any questions regarding this information, please do not hesitate to contact our office. Very truly yours, TRIGON ENGINEERING CONSULTANTS, INC. Christop er W. Ha I. Engineering Manager CWH/CDN:mes Attachments s:1015 01 projects 1200410141 r504014c. d oc Craig D. Registere T&AYUU Au. UUE bums:(_ . Mr. John Sealey, Fairchild Industrial Products Company April 14, 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-014 TABLE OF CONTENTS 1.0 SITE BACKGROUND..........................................................................................................................1 2.0 RECEPTOR SURVEY...........................................................................................................................2 3.0 HRC INJECTION..................................................................................................................................2 4.0 HRC MONITORING ACTIVITIES......................................................................................................3 5.0 GROUNDWATER ANALYTICAL RESULTS....................................................................................4 6.0 CONCLUSIONS AND RECOMMENDATIONS.................................................................................6 TAl1 LES 1 Monitoring Well Construction Details 2 Historical Groundwater Table Nevations 3 Field Analysis Summary 4 Groundwater Analytical Summary (Inorganics) 5 Groundwater Analytical Summary (Volatile Organic Acids) 6 Historical Groundwater Analytical Summary (VOCs) FIGURES 1 Site Location Map 2 HRC Injection Locations 3 Groundwater Potentiometric Map — March 22, 2005 4 Tetrachloroethene Isoconcentration Map — March 22, 2005 APPENDIX Laboratory Report and Chain -of -Custody Document TRIGON ENGINEERING CONSULTANTS, INC. Page i Mr. John Sealey, Fairchild Industrial Products Company April 14. 2005 Fairchild Industrial Products Company, Winston-Salem, ,North Carolina Trigon Project No. 015-04-0I4 1.0 SITE BACKGROUND The street address of the site is 3920 Westpoint Boulevard in the Westpoint Business Park, Winston- Salem, Forsyth County, North Carolina. The site is located on the south side of Westpoint Boulevard and east of Viceroy Drive (Figure 1). Fairchild Industrial Products Company, who leases the property from Highwoods/Forsyth Partnership Limited, currently occupies the building. Trigon Engineering Consultants, Inc. (Trigon) conducted a Comprehensive Site Assessment (CSA), dated December 11, 1998, concluding that the volatile organic compounds (VOCs) tetrachloroethene or perchloroethene (PCE), trichloroethene (TCE), cis-1,2-dichloroethene (cis-1,2-DCE), and toluene were detected in soils near the source area. VOCs were detected above North Carolina Title 15A NCAC 2L groundwater standards (NCGWS) in monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-b. A Corrective Action Plan (CAP) proposing the application of Hydrogen Release Compound (HRC) was prepared to address these constituents. No free product was encountered at the site during the CSA. Both Forsyth County Tax Maps and the 1950 USGS Winston-Salem West Quadrangle indicate a tributary of Salem Creek formerly crossed the western and southern portions of the site flowing to the southeast. No surface water is currently located within 500 feet of the source area. Buried water, power, and natural gas lines are located along the eastern side of Viceroy Drive running north to south. However, none of these utilities are suspected conduits of contaminant migration or vapor accumulation. The North Carolina Department of Environment and Natural Resources (NCDENR) Groundwater Section approved the CAP in May 2001. The goal of the CAP was to provide details for the remediation of PCE by assuring that known and foreseeable pathways are monitored while natural degradation occurs. The preferred remedial alt.-mative to address soil contamination in the source area was soil vapor extraction (SVE). A SVE system was installed and operated at the site from July 2000 through June 2001. The preferred remedial alternative to address groundwater contamination was the application of HRC. TRIGON ENGINEERING CONSULTAArT$, INC. Page I Mr. John Sealey, Fairchild Industrial Products Company April 14, 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-01 a 2.0 RECEPTOR SURVEY On September 29, 1998, Trigon completed a limited well survey at the site. The limited well survey reconnaissance consisted of viewing the properties within 1,500 feet of the subject site and talking to available property owners. Water meters were identified at properties having public water service. Two water supply wells were identified within 1,500 feet of the source area. One of the water supply wells is actively used. The other water supply well is not actively used since the home was connected to municipal water. The approximate well locations are indicated on Figure 1. Land use in Westpoint Business Park is primarily commercial and industrial. The majority of the properties in the business park are zoned GI. Zone GI is defined as general industrial. The site is bound to the north by Westpoint Boulevard, to the east by Annapolis Drive, to the south by Sides Mobile Home Court, and to the west by Viceroy Drive. Land use surrounding the business park is primarily residential. 3.0 HRC INJECTION Trigon requested a permit from the Underground Injection Control (UIC) Program of the Division of Water Quality to inject HRC for remediation of groundwater contamination identified during the CSA. The original UIC Program permit expired September 30, 2003. The HRC application plan included taking groundwater samples prior to application of HRC to provide baseline contaminant levels, drilling injection wells, injecting seven to eleven pounds of HRC per vertical foot in each well, and conducting remedial monitoring. In August 2001, Trigon initialized the first round of HRC injection. HRC injection locations included twenty-nine injection points (IP-I through IP-29) and six injection wells (IW-1 through IW-6) shown on Figure 2. Four injection points (IP-1 through IP-4) and six injection wells (IW-1 through IW-6) were drilled inside the facility to depths ranging between 24.5 and 35 feet below the ground surface. Seven pounds of HRC per vertical foot were placed in each borehole and injection well inside the facility. Ten injection points (IP-5 through IP-14) were drilled in the parking area downgradient of MW-6 and upgradient of MW-7 to depths of approximately 30 feet below the ground surface. Seven pounds of HRC per vertical foot was placed in each borehole. Fifteen injection points (IP-15 through IP-29) were TRIGON ENGINEERING CONSULTANTS, INC. Page 2 Mr. John Sealey, Fairchild Industrial Products Company April 14, 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-014 drilled upgradient of the source area to depths ranging between 23 and 35 feet below the ground surface. Eleven pounds of HRC per vertical foot were placed in injection points IP-15 through IP-29. Five quarters of groundwater sampling and corrective action monitoring were completed following the injection of HRC into groundwater at the site. Following the November 2002 sampling event, Trigon recommended additional HRC application in the vicinity of MW-9, MW-10, MW-13, and MW-7. Trigon requested a second permit from the Underground Injection Control (UIC) Program of the Division of Water Quality to inject additional HRC. The new UIC Program permit remains effective through November 30, 2006. The HRC application plan included converting monitoring wells MW-6, MW-14, and MW-15 into injection wells, drilling additional injection wells, injecting seven pounds of HRC per vertical foot in each well, and conducting remedial monitoring. On March 11, 2004, Trigon mobilized to the site to begin the installation of injection wells and points. HRC injection locations included twenty-one injection points (IP-30 through IP-50), three new injection wells (IW-7, IW-8, and IW-9), and the conversion of existing monitoring wells (MW-6, MW-14, and MW-15) to injection wells (IW-10, IW-11, IW-12). The locations are shown on Figure 2. Fifteen injection points (IP-30 through IP-44) and six injection wells (IW-7 through IW-12) were drilled inside the facility to depths ranging between 25 and 35 feet below the ground surface. Seven pounds of HRC per vertical foot was placed in each borehole with the exception of IW-10 and IWA I in which four pounds of HRC per vertical foot were placed. Six injection points (IP-45 through IP-50) were drilled in the parking area downgradient of MW-6 and upgradient of MW-7 to depths of 40.0 feet below the ground surface. Seven pounds of HRC per vertical foot were placed in each borehole. HRC injection was completed in March of 2004. Four quarters of groundwater sampling and corrective action monitoring have been completed following the second HRC injection event. 4.0 H RC MONITORING ACTIVITIES On March 22, 2005, static water levels were recorded in each of the monitoring wells on -site. Monitoring well MW-6, which had been dry since August of 2002, has been replaced with MW-6R. Groundwater samples were collected from ten monitoring wells (MW-1, MW-2, MW-5, MW-6R, MW-7, MW-8, MW-9, MW-10, MW-11, and MW-13) and analyzed for VOCs, volatile organic acids, and TRIGON ENGINEERING CONSULTANTS, INC. Page 3 Mr. John Sealey, Fairchild Industrial Products Company April 14, 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-014 inorganic compounds. Field parameters including dissolved oxygen, oxidation-reduction potential (ORP), pH, conductivity, and temperature of representative groundwater samples were also recorded from each monitoring well sampled. Groundwater elevations in the existing monitoring wells were used to determine the groundwater flow direction, average hydraulic gradient, vertical hydraulic gradient, and plume orientation. Table I provides a summary of monitoring well construction details and groundwater elevations measured on March 22, 2005. Historical groundwater table elevation measurements are summarized in Table 2. The static water levels measured on March 22, 2005 between monitoring wells MW-1 and MW-7 indicate a horizontal groundwater flow gradient of 0.03 foot per foot to the south- southeast. Static water levels measured in monitoring wells MW-1 and MW-2 indicate a vertical groundwater gradient of 0.01 foot per foot downward. A potentiometric surface map based on the March 22, 2005 groundwater elevations is shown on Figure 3. In -situ aquifer tests performed on shallow monitoring wells at the site during the CSA indicated that the surficial aquifer has an average hydraulic conductivity of 1.2 feet per day. The average groundwater velocity is estimated to be 0.12 feet per day (44 feet per year), based on the average groundwater gradient from the March 22, 2005 water level measurements and an estimated effective porosity of thirty percent. Groundwater samples were collected on March 22, 2005. The wells were first purged of three well volumes of water, or until dry, with a disposable polyethylene bailer. After allowing the wells to recharge, groundwater samples were collected and placed in laboratory prepared containers. The groundwater samples were maintained on ice until delivery to Pace Analytical in Huntersville, North Carolina. 5.0 GROUNDWATER ANALYTICAL RESULTS In order to assess the condition of the aquifer for degradation of contaminants found at the site, groundwater samples were collected for field analysis of temperature, pH, conductivity, dissolved oxygen, and oxidation-reduction potential. In addition, groundwater samples were collected for laboratory analysis of VOCs to monitor contaminant levels at the site, volatile organic acids to indicate the presence and metabolism of HRC, and inorganic compounds to monitor levels of the primary electron acceptors. TRIGON ENGINEERING CONSULTANTS, INC. Page 4 Mr. John Sealey, Fairchild Industrial Products Company April 14, 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-014 Measurements were collected from groundwater samples for temperature, pH, conductivity, dissolved oxygen, and oxidation-reduction potential using field instrumentation. Results of the groundwater measurements indicate that the subsurface environment is suitable for natural attenuation at the site. The groundwater field analysis generally indicates that the subsurface environment is within acceptable limits for biodegradation to occur. Conductivity is recorded for quality control and sampling consistency. The field measurements recorded on March 22, 2005 are summarized in Table 3, which includes the preferred conditions for natural biodegradation of chlorinated compounds within the groundwater plume. Groundwater samples from monitoring wells MW-1, MW-2, MW-5, MW-6R, MW-7, MW-8, MW-9, MW-10, MW-lll, and MW-13 were analyzed for inorganic compounds including nitrite, total phosphorous, sulfide, dissolved manganese, nitrate, sulfate, dissolved iron, and chloride. Generally, in a pristine aquifer, dissolved oxygen is used as the primary electron acceptor. After the dissolved oxygen is consumed, anaerobic microorganisms typically use additional electron acceptors in the following order of preference: nitrate, iron, sulfate, and carbon dioxide. Concentrations of inorganics indicate that a reductive pathway is possible for dechlorination of chlorinated hydrocarbons. Nitrate, iron, and sulfate do not appear to be competing as electron acceptors. Groundwater analytical results for inorganics are summarized in Table 4. Groundwater sample analytical results indicate that volatile organic acids were detected in three of the ten monitoring wells sampled on March 22, 2005. Volatile organic acids or metabolic acids, other than lactic acid, indicate the presence and metabolism of HRC. Analytical results for volatile organic acids are summarized in Table 5. Groundwater sample analytical results indicate that several VOCs were detected in the monitoring wells sampled. PCE was detected at levels exceeding the state groundwater standard in monitoring wells MW- 1, MW-6R, MW-7, MW-8, MW-9, NRV-10, and MW-11. PCE concentrations in monitoring wells MW- 1, MW-7, MW-8, MW-9, and MW-10 increased slightly since the previous sampling event. A PCE isoconcentration map is shown on Figure 4. TCE was detected at levels exceeding the state groundwater standard in monitoring wells MW-1, MW-6R, MW7, MW-9, MW-10, and MW-11. Cis-1,2-DCE was detected at a level exceeding the state groundwater standard in monitoring well MW-9 and MW-13. Vinyl Chloride was detected at a level exceeding the state groundwater standard in monitoring well MW- TRlGON ENGINEERING CONSUL TANTS, INC. Page 5 Mr. John Sealey, Fairchild Industrial Products Company April 14. 2005 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 015-04-014 1. A summary of historical VOC analytical results is provided in Table 6. A copy of the analytical results including the chain -of -custody form is included in Appendix A. 6.0 CONCLUSIONS AND RECOMMENDATIONS In general, the most definitive evidence of biodegradation of contaminants in groundwater is the reduction in contaminant concentrations and the presence of the constituents into which the contaminants degrade. PCE concentrations in monitoring wells MW-2, MW-5, MW-6R, MW-10, MWA 1, and MW- 13 have either decreased or have not changed significantly since the previous monitoring event. PCE concentrations in monitoring wells MWA, MW-7, MW-8, and MW-9 increased since the previous monitoring period. The presence of daughter products of dechlorination of PCE in monitoring wells MW-1, MW-2, MW-6R, MW-7, MW-9, MW-10, MW-11, and MW-13 also indicates degradation is occurring. Metabolic acid concentrations in monitoring wells MW-2 and MW-13 indicate that HRC is influencing the subsurface environment in the vicinity of those wells. Total VOC concentrations have reduced in monitoring wells MW-2, MW-6R, and MW-13. The total VOC concentration has remained similar to historical levels within monitoring wells MW-1, MW-5, MW-10, and MW-11. The total VOC concentrations in monitoring wells MW-7, MW-8, and MW-9 have increased slightly since the previous sampling event. Based on the results of the monitoring event, we recommend the continuation of corrective action monitoring on a quarterly schedule. The next monitoring event should be scheduled for mid -June 2005. It is our opinion that analysis of inorganics in each well will not be necessary to evaluate the effects of the corrective action in the upcoming monitoring events. Copies of this report have been mailed to the Aquifer Protection in the NCDENR Winston-Salem Regional Office and the UIC Progran-: in Raleigh, North Carolina. TRIGON ENGINEERING CONSULTANTS, INC. Page 6 TABLES Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina April 14, 2005 Trigon Project No. 015-04-014 TABLE 1: MONITORING WELL CONSTRUCTION DETAILS Monitoring Well Date Constructed Total Depth feet b s Screened Interval feet b s) Depth to Groundwater (feet TOC Top of Casing Elevation 100' Datum) Groundwater Elevation 100' Datum MW-1 Se tember-98 27.37 12.37 - 27.37 17.35 94.42 77.07 MW-2 October-98 43.34 38.34 - 43.34 17.30 94.09 76.79 MW-3 Se tember-98 22.32 12.32 - 22.32 15.61 98.17 82.56 MW-4 Se tember-98 18.65 8.65 - 18.65 17.71 91.38 73.67 MW-5 Se tember-98 25.11 15.11 - 25.11 17.92 87.07 69.15 MW-6R March-04 34.40 14.40 - 34.40 22.30 91.55 69.25 MW-7 November-98 26.56 11.56 - 26.56 22.29 86.81 64.52 MW-8 November-98 26.70 16.70 - 26.70 21.70 89.25 67.55 MW-9 March-99 24.41 9.41 - 24.41 17.86 94.24 76.38 MW-10 March-99 29.52 14.52 - 29.52 19.71 94.09 74.38 MW-11 May-99 24.12 9.12 - 24.12 18.30 94.31 76.01 MW-12 Ma -99 25.70 5.70 - 25.70 17.95 94.28 76.33 MW-13 June-99 33.46 1 8.46 - 33.46 20.81 94.22 73.41 feet bgs = Feet below ground surface feet TOC = Feet below top of well casing 100' Datum = Well casings were surveyed to an arbitrary 100 foot Datum. The benchmark is the center of the manhole cover at the south end of Viceroy Street. Note: Static Water Levels were measured March 22, 2005. MW-6, MW-14, and MW-15 were converted to injection wells IW-12, IW-10, and IW-11, respectively. TRIGON ENGINEERING CONSULTANTS, INC. Air. John Sealey, Fairchild industrial Products Company Fairchild Industrial Products Company. Winston-Salem North Carolina April 14. 2005 Trigon Projecl No. 015-04-01 ! TABLE 2: HISTORICAL GROUNDWATER TABLE ELEVATIONS Monitoring Well 06/18/99 08/24/00 11/16/01 02/26/02 05/01/02 08/13/02 11/20/02 06/09/04 09/09/04 12/09/04 03/22/05 MW-1 77.24 75.84 73.92 73.32 73.13 72.68 72.87 77.62 77.21 76.87 77.07 MW-2 77.09 75.77 73.75 73.15 72.93 72.23 72.61 77.47 76.90 76.60 76.79 MW-3 83.23 81.57 79.34 78.89 78.74 77.97 78.26 83.36 82.31 81.95 82.56 MW-4 73.10 DRY DRY DRY DRY DRY 72.77 DRY 73.83 73.49 73.67 MW-5 67.87 67.30 65.05 65.08 65.08 64.58 65.56 69.27 68.35 72.88 69.15 MW-6R --- --- --- --- --- --- --- 69.76 69.59 69.27 69.25 MW-7 64.36 63.35 61.90 61.56 61.36 60.93 61.82 64.90 64.71 64.49 64.52 MW-8 67.53 66.54 64.99 64.42 64.29 64.87 64.28 68.19 67.94 67.58 67.55 MW-9 76.78 75.64 73.26 72.60 72.40 71.84 72.24 77.07 76.63 76.26 76.38 MW-10 74.58 73.29 71.46 70.87 70.61 69.99 70.40 74.81 74.69 74.25 74.38 MW-11 76.00 74.82 72.90 72.28 72.09 71.60 71.91 76.71 76.28 75.97 76.01 MW-12 76.57 74.46 73.28 72.73 72.54 71.92 72.25 77.02 76.44 76.09 76.33 MW-13 72.84 71.57 69.71 69.16 68.91 68.37 68.77 73.50 73.41 73.27 73.41 Elevations are relative to an established benchmark on -site with an assumed elevation of 100.00 feet. Note: MW-6R was installed in March of 2004 to replace MW-6. TRIGON ENGINEERING CONSULTANTS, INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina TABLE 3: FIELD ANALYSIS SUMMARY April 14, 2005 Trigon Project No. 015-04-014 Monitoring Sample Date Temp °C pH Conductivity S/m Dissolved Oxygen m Redox (mV) Pref rll Conditions > 200C 5<pH<9 --- <0.5 mg/L <50 mV MW-1 03/22/05 18 6.0 64 0.3 -11 MW-2 03/22/05 18 6.1 0.3 0.0 -62 MW-3 03/22/05 17 5.8 54 1.5 141 MW-5 03/22/05 13 6.0 38 0.2 -41 MW-6R 03/22/05 18 5.9 39 1.5 164 MW-7 03/22/05 18 6.0 89 0.0 17 MW-8 03/22/05 19 5.7 42 0.0 193 MW-9 03/22/05 20 5.8 79 0.9 25 MW-10 03/22/05 20 5.7 31 2.3 162 MW-11 03/22/05 19 5.7 25 0.0 159 MW-13 03/22/05 20 6.2 0.2 1.1 -69 Redox = oxidation-reduction potential °C = degrees Celsius S/m = siemens per meter mg/1= milligrams per liter, analogous to parts per million mV = millivolts Note: Conductivity is measured for consistency in groundwater sample collection. TRIGON ENGINEERING CONSULTANTS, INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina TABLE 4: GROUNDWATER ANALYTICAL SUMMARY (INORGANICS) April 14. 2005 Trigon Project No. 015-04-014 Monitoring Well Analytical Results m /1 Sampling Date Nitrite Total Phosphorous Sulfide Dissolved Manganese Nitrate Sulfate Dissolved Iron Chloride Preferable Conditions > Background < I mg/l > 1 mg/1 > 1 mg/l < 1 mg/l < 20 mg/1 >1 me > 2x Background M W-1 11/27/01 BDL 1.10 BDL 2 BDL BDL BDL 7.9 02/26/02 0.31 1.50 BDL 26 BDL BDL 13 8.5 05/01/02 0.49 0.52 BDL 28 0.13 BDL 8.4 2.1 08/13/02 BDL 0.69 BDL 42 BDL BDL 3.4 11 11/21/02 0.42 4.80 0.069 54 BDL BDL 58 BDL 06/09/04 BDL 0.157 BDL 7.6 BDL BDL 12 27 09/09/04 BDL 0.350 BDL 8.5 BDL BDL 14 13 1Z109I04 BDL 0.184 13flL 7.7 BDL BDL 13 14 03/22/05 BDL 0.23 6DL 6 BDL BDL 7.8 15 MW-2 11/27/01 BDL 0.34 BDL 0.006 1 2.6 BDL 4.3 02/26/02 BDL 0.83 BDL 0.074 0.95 2.8 4.6 4.1 06/09/04 BDL 1.14 BDL 38 BDL BDL 32 24 09/09/04 BDL 0.953 BDL 73 BDL BDL 86 15 12/09/04 BDL 0.741 BDL 52 BDL BDL 92 20 03/22/051 BDL 1 0.673 BDL 1 64 1 BDL BDL 120 18 MW-3 11/28/01 BDL 0.99 BDL 0.071 0.59 7.6 BDL 18 09/09/041 BDL 0.118 BDL 0.30 0.73 7.6 1.7 22 12/09/041 BDL BDL BDL 3.4 0.60 57 4.5 23 MW-5 09/09/041 BDL BDL BDL 1 2.2 1 BDL BDL 10 29 12/09/041 BDL I BDL I BDL 1 0.26 1 0.43 1 BDL 0.78 1 BDL 03/22/051 BDL I BDL BDL 1 1.3 BDL BDL 1.6 6.6 MW-6R 06/09/04 BDL 0.414 BDL 2.3 BDL BDL 5.2 25 09/09/04 BDL 0.155 BDL 2.4 BDL BDL 5.1 13 12/09/04 BDL 0.609 BDL 1.6 BDL BDL 0.70 12 03/22/05 BDL 0.573 BDL 2.3 BDL BDL 0.42 14 MW-7 11/27/01 BDL 0.53 BDL 0.42 0.21 2A BDL 7.9 06/09/04 BDL 0.200 BDL 1.1 BDL BDL 1.0 21 09/09/04 BDL BDL BDL 2.0 BDL BDL 3.3 11 12/09/04 BDL 0.280 BDL 0.61 BDL BDL 0.64 7.5 03/22/05 BDL 0.756 BDL 1.9 BDL BDL 0.91 10 mg/l = milligrams per liter, analogous to parts per million BDL = Below Laboratory Detection Limits Note: MW-3 is upgradient of the source area and represents background levels at the site. TRIGON ENGINEERING CONSUL"IANTS, INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina TABLE 4: GROUNDWATER ANALYTICAL SUMMARY (INORGANICS) (CONTINUED) April 14, 2005 Trigon Project No. 015-04-014 Monitoring Well Anal ical Results m Sampling Date Nitrite Total Phosphorous Sulfide Dissolved Manganese Nitrate Sulfate Dissolved Iron Chloride Preferable Conditions > Background < 1 mg/l > 1 mg/l > I mg/l < i mg/l < 20 mg/l >1 mg/I > 2x Background MW-8 03/22/051 BDL 1 0.373 BDL 0.061 2.8 40 1.5 19 MW-9 11/27/01 BDI, 0.18 BDL 1 BDL 3.8 BDL 27 11/21/02 BDL 0.19 BDL 1.4 BDL 2.7 0.23 24 06/09/04 BDL 0.110 BDI, 5.9 BDL BDL 6.2 61 09/09/04 BDL BDL BDL 31 BDL BDL 5.8 34 12/09/04 BDL BDL BDL 1.7 BDL BDL 4.6 34 03/22105 BDI, 0.162 BDL 1.5 BDL BDI, 2.4 33 M W-10 _ 11/27/01 BDL 0.26 BDL 0.16 0.17 2.4 BDL 9.4 02/26/02 0.21 0.21 BDL 0.92 BDL BDL 26 9.4 05/01/02 BDL 0.31 BDL 0.41 0.28 1.3 BDL 8 08/13/02 BDI, 0.12 BDL 0.2 BDL 2.1 BDL 8.2 11/21/02 BDL BDL BDL 0.16 0.47 2.4 0.23 7.6 06/09/04 BDL BDL BDL 0.078 0.53 BDL 1.4 21 09/09/04 BDL 0.110 BDL 0.085 0.50 BDL 0.77 11 12/09/04 BDL 0.174 BDL 0.078 0.50 BDL 2.0 11 03/22/05 BDI, BDL BDI, 0.067 0.36 BDL 0.075 10 MW-I1 11/27/01 BDL 0.17 BDL 2 ND 4.7 BDI, 8.9 06/09/04 BDL 0.224 BDL 0.67 1.4 8.0 2.2 25 09/09/04 BDL BDL 13DL 0.59 1.2 BDL 1.6 14 12/09/04 BDL 0.121 BDL 0.042 1.3 BDL 0.24 13 03/22/05 BDI, BDI. BDI. 0.080 1.3 BDL 0.62 13 MW-13 11/27/01 BDL 0,49 BDL 0.59 0.44 3.2 0.07 9.5 11/21/02 BDL 0.75 0.053 0.21 0.39 2.4 0.4 9.9 06/09/04 BDL 0.110 BDL 3.4 BDL BDL 9.6 32 09/09/04 BDL 0.108 BDL 15 BDL BDL 10 19 12/09/04 BDL BDL BDL 20 BDL BDL 27 20 03/22/05 BDL BDL BDL 28 BDL BDL 30 19 mg/l = milligrams per liter, analogous to parts per million BDL = Below Laboratory Detection Limits Note: MW-3 is upgradient of the source area and represents background levels at the site. TRIGON ENGINIiERING CONSULTANTS; INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company Winston-Salem, North Carolina TABLE 5: GROUNDWATER ANALYTICAL SUMMARY (VOLATILE ORGANIC ACIDS) April 14, 2005 Trigon Project No. 015-04-014 Monitoring Well I Analytical Results (mg/1) Sampling Datel P ruvic Acid Lactic Acid Acetic Acid Pro ionic Acid Butyric Acid MW-1 11/27/01 <0.1 <1.0 5.3 17.9 <1.0 02/26/02 <0.1 <0.1 141 207 51 05/01/02 1.8 <1.0 296 482 113 08/12/02 <0.1 <1.0 241 578 18.6 11/20/02 0.7 7.7 680 1,430 141 06/09/04 <0.1 <0.1 <0.1 <0.1 <0.1 09/09/04 <0.1 1.1 <1.0 <1.0 <1.0 12/09/04 1.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <0.1 <0.1 <0.1 <O.1 MW-2 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 <0.1 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 12.7 7 31.8 11/20/02 <0.1 <0.1 41.3 24.8 4.3 06/09/04 0.2 147 511 1,040 607 09/09/04 3.3 153 791 1,670 2,300 12/09/04 1.9 200 1,130 3,770 7,390 03/22/05 7.3 467 1,570 5,030 8,820 MW-3 11/28/01 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 1.8 4.7 9.9 10.4 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 MW-5 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 1.5 <1.0 <1.0 <1.0 <1.0 08/13/02 0.7 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 5.8 1.5 <1.0 <1.0 I <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 03/22/05 <0.1 6.1 <0.1 6.6 -1.0 <0.1 MW-6R 06/09/04 <0.1 <0.1 <0.1 <0.1 <0.1 09/09/04 <0.1 3.9 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <0.1 <0.1 <0.1 <0.1 MW-7 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.3 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.2 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <0.1 <0.1 <0.1 <0.1 09/09/04 <0.1 <1.0 1.8 2.7 <1.0 12/09/04 <0.1 7.4 <1.0 <1.0 <1.0 03/22/05 <0.1 <0.1 I <0.1 I <0.1 I <0.1 mg/l = milligrams per liter, analogous to parts per million Note: Concentrations in bold type exceed detection limits. TRIGON ENGINEERING CONSULTANTS, INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company Winston-Salem, .North Carolina April 14, 1005 Trigon Project No. 015-04-014 TABLE 5: GROUNDWATER ANALYTICAL SUMMARY (VOLATILE ORGANIC ACIDS) (CONTINUED) Monitoring Well I Analytical Results (mg/1) Sampling Datel P ruvic Acid I Lactic Acid I Acetic Acid I Pro ionic Acid I Bu ric Acid MW-8 3/22/05 <0.1 I <0.1 I <0.1 I <0.1 I <0.1 MW-9 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.8 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.2 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 1.6 3.2 <1.0 09/09/04 2.0 3.9 11.3 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 2.0 1.3 03/22/05 <0.1 <0.1 <0.1 <0.1 <0.1 MW-10 11/27/01 <0.1 <1.0 <1.0 9.5 <1.0 02/26/02 <0.1 <1.0 59.1 118 <1.0 05/01/02 1.4 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 1.1 <1.0 <1.0 <1.0 09/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <0.1 <0.1 <0.1 <0.1 MW-11 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.2 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <0.1 <0.1 <0.1 <O.1 MW-13 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 <0.1 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 2.6 15.8 20.4 8.7 09/09/04 0.9 15.7 96.1 103 35.1 12/09/04 <0.1 <1.0 129 122 35.1 03/22/05 <0.1 <0.1 93.7 85.1 30.6 mg/l = milligrams per liter, analogous to parts per million Note: Concentrations in bold type exceed detection limits. TRIGON ENGINEERING CONSULTANTS, INC. Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina April 14, 2005 Trigon Project No. 015-04-014 TABLE 6: HISTORICAL GROUNDWATER ANALYTICAL SUMMARY (VOCs) Sampling Location EPA Method 6230D Analytical Results u ) Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE 1,1-DCE Chloroform Bromochloro- methane Acetone Vinyl Chloride Toluene MTBE Bromomethane Ethylbenzene 1,3,5- Trimethylbenzene Xylenes NCGWS 0.7 2.8 70 70 7 0.00019 0.6 700 0.015 1,000 200 NE 29 350 530 MW-1 10/07/98 15.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 1.5 BDL BDL BDL BDL BDL 4.5 BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 23 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 9.9 BDL BDL BDL BDL 5.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 0.52 BDL BDL BDL BDL BDL 26 BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 0.63 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL 9.6 BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 4.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 2.6 BDL BDL BDL BDL BDL BDL BDL BDL 0.62 BDL BDL BDL BDL BDL 06/09/04 1.7 2.5 BDL 16 BDL BDL BDL NA 1.5 BDL BDL BDL BDL BDL BDL 09/09/041 BDL 1 1.4 1 0.67 14 1 BDL I BDL I BDL I NA 1 1.1 BDL I BDL I BDL BDL BDL BDL 12/09/041 BDL 1 1.2 1 BDL 17 BDL BDL BDL NA 0.67 BDL BDL BDL BDL BDL BDL 03/22/051 1.2 1 6.5 0.55 37 BDL BDL BDL BDL 1.6 BDL BDL BDL BDL BDL BDL MW-2 10/16/98 2.4 BDL BDL BDL BDL 12.9 BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 5.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/01/00 2.5 BDL BDL BDL BDL NA NA NA NA NA BDL BDL BDL BDL BDL 12/01/00 4.8 BDL BDL BDL BDL NA NA NA NA NA BDL BDL BDL BDL BDL 01/03/01 BDL BDL BDL BDL BDL NA NA NA NA NA BDL BDL BDL BDL BDL 06/14/01 BDL BDL BDL BDL BDL 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 0.92 BDL BDL BDL BDL BDL 0.59 BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 0.50 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 2.60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 2.2 BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/04 17 7.2 BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/041 1.2 1 1.4 BDL BDL BDL BDL BDL NA BDL BDL BDL BDL 2.2 BDL BDL 03/22/051 BDL 1 1.2 1 BDL 1.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL 8.1 0.8 MW-3 10/07/98 BDL BDL BDL BDL BDL 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 8DL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/28/01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/041 BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/041 BDL BDL BDL BDL BDL BDL I BDL NA BDL BDL BDL BDL BDL BDL BE NCGWS = North Carolina Groundwater Standards ug/l = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1, 1 -Dichloroethene TRIGON ENGINEERING CONSULTANTS, INC. Page 1 of 4 Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina April 14, 2005 Trigon Project No. 01 5-04-014 TABLE 6: HISTORICAL GROUNDWATER ANALYTICAL SUMMARY (VOCs) Sampling Location EPA Method 6230D Analytical Results u Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE 1,1-DCE Chloroform Bromochloro- methane Acetone Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,3,5 Trimethylbenzene Xylenes NCGWS 0.7 2.8 70 70 7 0.00019 0.6 700 0.015 1,000 200 NE 29 350 530 MW-4 10/07/98 3 3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 2.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 Well was dry on the sampling date 06/14/01 Well was dry on the sampling date 02/26/02 Well was dry on the sampling date 05/01 /02 Well was dry on the sampling date 08/13/02IWellwasdryonthesam lin date MW-5 10/07/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 5.0 4.6 BDL 1.1 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/051 BDL I BDL I BDL I BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-6 10/07/98 10.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 1.3 BDL BDL BDL BDL BDL BDL 130 BDL BDL BDL BDL BDL BDL BDL 06/14/01 Well was dry on the sampling date 11/27/01 Well was dry on the sampling date 02/26/02 Well was dry on the sampling date 05/01/02 Well was dry on the sampling date 08/13/02 Well was dry on the sampling date 11/21/02 Well was dry on the sampling date MW-6R 06/09/04 55 8.2 BDL 22 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/04 58 10 BDL 12 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/04 94 8.1 BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/05 80 9 BDL 1.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NCGWS = North Carolina Groundwater Standards ugA = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1, 1 -Dichloroethene TRIGON ENGINEERING CONSULTANT S, INC. Page 2 oj4 Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina April 14, 2005 Trigon Project No. 015-04-014 TARI.F 6! MSTORICAI, GR0l NDWATF.R ANAI,VTTCAI, STJMMARV (VL7Ccl Sampling Location EPA Method 6230D Analytical Results u ) Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE ],I-DCE Chloroform Bromochloro- methane Acetone Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,3,5- Trimethylbenzene Xylenes NCGWS 0.7 2.8 70 70 7 0.00019 0.6 700 0.015 1,000 200 NE 29 350 530 NM-7 11/16/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 1.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 7.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 3.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 2.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 Well was dry on the sampling date 11/21/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 15 2.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 19 6.9 BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/04 15 5.5 BDL 0.76 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/05 4.3 8.6 BDL 1.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-8 11/16/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-9 04/12/99 144 159 2.4 49 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 177 187 BDL 60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 1,300 920 15 140 3.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 10/31/00 1,700 710 13 190 3.5 NA NA NA NA NA NA NA BDL BDL BDL 12/01/00 1,000 570 8.7 170 2.9 NA NA NA NA NA NA NA BDL BDL BDL O1/03/01 1,100 770 11 330 5 NA NA NA NA NA NA NA BDL BDL BDL 06/14/01 420 220 24 510 6.8 11 BDL BDL 2 BDL BDL BDL BDL BDL BDL 11/27/01 2,800 1,600 BDL 710 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 5,000 1,800 BDL 1,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 5,000 1,900 25 1,200 6.2 BDL 34 BDL 1.5 0.92 2.7 BDL BDL BDL BDL 08/13/02 3,600 1,200 31 1,200 5.4 BDL BDL BDL 2.5 BDL BDL BDL BDL BDL BDL 11/21/02 4,000 1,500 BDL 2,200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 1,400 730 70 2,300 7.5 BDL BDL NA 35 BDL BDL BDL BDL BDL BDL 09/09/04 820 590 60 2,300 BDL BDL BDL NA 15 BDL BDL BDL BDL BDL BDL 12/09/04 540 800 BDL 1,200 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/O5 900 1 1,100 BDL 990 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NCGWS = North Carolina Groundwater Standards ug/1= micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1, 1 -Dichloroethene TRIGON ENGINEERING CONSULTANTS, INC. Page 3 of4 Mr. John Sealey, Fairchild Industrial Products Company Fairchild Industrial Products Company, Winston-Salem, North Carolina April 14, 2005 Trigon Project No. 015-04-01 a TABLE 6: HISTORICAL GROUNDWATER ANALYTICAL SUMMARY (VOCs) Sampling Location EPA Method 6230D Aual tical Results (. Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE ],I-DCE Chloroform Bromochloro- methane Acetone Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,3,5 Trimethylbenzene Xylenes NCGWS 0.7 2.8 70 70 7 0.00019 0.6 700 0.015 1,000 200 NE 29 350 530 MW-10 04/12/99 7.5 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 106 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 240 68 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 440 21 BDL 5.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 270 60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 31 BDL BDL 440 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 65 9.1 0.97 190 BDL BDL 8.1 BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 150 15 BDL 90 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 170 35 BDL 39 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 150 63 BDL 46 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/041 150 1 57 1 BDL 1 48 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/041 150 1 40 BDL 20 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/051 160 28 BDL 18 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-11 06/04/99 415 23 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 200 34 BDL 4.9 BDL BDL BDL 76 BDL BDL BDL BDL BDL BDL BDL 06/14/01 200 74 BDL 21 BDL BDL 34 BDL BDL 0.85 BDL BDL BDL BDL BDL 11/28/01 210 23 BDL 19 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 600 46 BDL 80 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 370 1 30 0.62 31 BDL 1.2 0.96 BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 Well was dry on the sampling date 11/21/02 Insufficient water to sample 06/09/04 380 52 BDL 35 BDL 1.1 BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/04 360 45 BDL 30 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/041 480 59 BDL 43 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/05 430 54 BDL 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NM-12 06/04/991 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-13 06/04/99 112 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 190 2.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 260 6 BDL 1.2 BDL BDL BDL BDL BDL 0.6 BDL BDL BDL BDL BDL 11/27/01 170 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 390 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 270 11 BDL 2.2 BDL 0.59 7.7 BDL BDL BDL BDL 1.2 BDL BDL BDL 08/13/02 320 16 BDL 5.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 210 11 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 270 34 0.56 35 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 37 24 2.9 220 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 09/09/04 BDL BDL BDL 210 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL 250 BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL 03/22/05 BDL BDL BDL 130 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NCGWS = North Carolina Groundwater Standards ug/1= micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1, 1 -Dichloroethene TRIGON ENGINEERING CONSULTANTS, INC. Page 4 of a FIGURES ice% '�•' �:! y � l� ; � � �f\ f �; '�:�; . ��J ���/ � �� �� � .\\ 1\I - i I-. �- • � ` ` „ � � '• �; i 1�" "`.'� .r--'.^' )' ..-.• ,+. i h �. '-� moo^ ! -� :. `(�,\11 ' •j ijI '�''3. J_�-\ o • �' J :�' "�) � �'•`�'i 77 .,_1 /-� � «.�. _ _ -- � •_�� "� � _tom -� —� ��' �-��il�: _ .- . � -� — '� . . •1 ,\ � � �•+b i ( • I '`�, \ ."... : h�''/ �-�.' � �— lil � _•.. ti� � lam• ., rl)%, .�;:: �� � r.� .\• �.✓l •• ��„(i��f(/Q,'� • •\ � �, �J ��- O\ \ 1� , � � , �'� III u �v `\ ,' •- 1, Eki_ it ; j I I 10 � ' Imo' ;a � ' � �� . •� (( I� ' :'/ l„-� ; ` I - �`��'� ./i � ���\� �1/ �� \�� \`��" n •p -.I l,• _ le t,120 �• ��- / �\ - j" '�,.'',,`��^j'-5.-.. ��~' ��� �� 5:3j ` �' � •+ � .. `may `��' � _ I y • � ; �� - VgTOZ- r� �:�'����y77`�t"''/-. ` ���`�� �� • .e'er _'� u�� �` q� � \fin .._ �1� �^^ " I 'mil il(. ra 1 � •'^ ,'�, - Tt`, fj" �� i 'ya �' - ;�-.� ,r��. �v '.�'i�. �. l_• _ _._�- i; ' asp SCALE: DATE: APPROVED BY: SOURCE: 1950 (PHOTOREVISED 1971) 1" = 2000, 04/14/05 USGS MAP, WMSTON-SALEM WEST QUADRANGLE FAIRCHILD INDUSTRIAL PRODUCTS COMPANY 3920 WESTPOINT BOULEVARD TRIGr]N WINSTON SALEM, NORTH CAROLINA Trigon Engineering Consultants, Inc. TRIGON PROJECT NO.015-04-014 313 Gallimore Dairy Road FIGURE Greensboro, North Carolina 27409 SITE LOCATION MAP 1 1 1 �MW-4 Not Sample VICEROY DRIVE \ TYPE III W-3 \ \ MW-2 BDL BDL MW-1 \ 1.2 W-11 430 MW-9 900 1 500 1 16010 1 MW-12 1 Not Sampled 1 BD EXISTING i13 BUILDING MW-5 BDL, I I / 1 " 80� 1 � M 3 7 Z13 . ANNAPOLIS DRIVE MIMPP- WAS LEGEND e MW-1 MONITORING WELL LOCATION 1,000 TETRACHLOROETHENE CONCENTRATION (micrograms per liter) BDL BELOW DETECTION LIMITS TETRACHLOROETHENE ISOCONCENTRATION MAP MARCH 22, 2005 FAIRCHILD INDUSTRIAL. PRODUCTS COMPANY 3920 WESTPOINT BOULEVARD WINSTON-SALEM, NORTH CAROLINA Date 4111/05 Scale 1" = 60' ENGINEERING CONSULTANTS,INC• Drawn by DRK Figure 4 APPENDIX aceAnalytical www.pacelabs.com April 07. 2005 Mr. Chris Hay Trigon Engineering Consultants 313 Gallimore Dairy Rd Greensboro, NC 27409 RE: Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Dear Mr. Hay: Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Enclosed are the analytical results for sample(s) received by the laboratory on March 23, 2005. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. If you have any questions concerning this report please feel free to contact me. Sincerely, Bonnie McKee Bonnie.McKee@pacelabs.com Project Manager Enclosures Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI NIA AP FA79AR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. A«o. p'C s Charlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E 7627 Pace Analytical Services, Inc. ,Analytical ® 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423626 Project Sample Number: 9290570-001 Date Collected: 03/22/05 11:30 Client Sample ID: MW-1 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 15. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887.00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.230 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14.0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 108.86-1 Bromochloromethane ND me/l 0.00050 1.0 03/26/05 21:53 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-27-4 Bromoform ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-25-2 Bromomethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 74-83.9 n-Butylbenzene ND mg/l 0.0010 1.0 03/26/05 21:53 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 108-90-7 Chloroethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-00.3 Chloroform ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 67-66-3 Chloromethane ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 106-43-4 1.2-Dibromo-3-chloropropane ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 106-93-4 Dibromomethane ND mg/1 0.00050 1.0 03/26/05 21:53 PPM 74.95-3 Date: 04/07/05 Page: 1 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , NC Drinking Water 37706 SC Environmental 99030 41 .`� - `f Sc 99006 FI NFI AP FRMAR �'n Ct FI NFI AP F87627 ace Analytical www. pacelahs. cam Lab Sample No: 925423626 Client Sample ID: MW-1 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 9290570 Fax: 704.875.9091 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-001 Date Collected: 03/22/05 11:30 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt 1,2-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 21:53 PPM 95-50.1 1,3-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 21:53 PPM 541-73.1 1,4-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 21:53 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 107-06-2 1.1-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75.35-4 cis-1.2-Dichloroethene 0.037 mg/l 0.00050 1.0 03/26/05 21:53 PPM 156-59-2 trans-1,2-Dichloroethene 0.00055 mg/l 0.00050 1.0 03/26/05 21:53 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 78-87-5 1.3-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 100-41-4 Hexachloro-1.3-butadiene ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 87.68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 1.0 03/26/05 21:53 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 103-65-1 Styrene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 630-20.6 1,1,2.2-Tetrachloroethane ND mg/l 0,00050 -1.0 03/26/05 21:53 PPM 79-34-5 Tetrachloroethene 0.0012 mg/l 0.00050 1.0 03/26/05 21:53 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 108-88-3 Total Trihalomethanes (Galt.) ND mg/1 0.00050 1.0 03/26/05 21:53 PPM 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 87.61-6 1,2.4-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 21:53 PPM 120-82-1 1.1,1-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 71-55-6 1.1.2-Trichloroethane ND mg/1 0.00050 1.0 03/26/05 21:53 PPM 79-00-5 Trichloroethene 0.0065 mg/1 0.00050 1.0 03/26/05 21:53 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 75.69-4 1,2,3-Trichloropropane ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 96-18-4 1,2,4-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 95-63-6 1,3.5-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 108-67-8 Date: 04/07/05 Page: 2 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 r ACCO,b NC Drinking Water 37706 SC Environmental 99030 4tp °R Sc 99006 CI AICI AD C07CAO � ncnrt CI AIM AD C07R97 Pace Analytical Services, Inc. ,Analytical ® 9800 Kincey Avenue, Suite 100 Huntersvilie, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423626 Project Sample Number: 9290570-001 Date Collected: 03/22/05 11:30 Client Sample ID: MW-1 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Vinyl chloride 0.0016 mg/l 0.00050 1.0 03/26/05 21:53 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM o-Xylene ND mg/l 0.00050 1.0 03/26/05 21:53 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 103 x 1.0 03/26/05 21:53 PPM 625-98-9 Date: 04/07/05 Ashevill Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD C07RAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 40 `� ACC0,,0, 1 c Page: 3 of 56 arl NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP FR7697 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423634 Project Sample Number: 9290570-002 Date Collected: 03/22/05 11:51 Client Sample ID: MW-2 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit Cif Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 18. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.673 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide. Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 74-97.5 Bromodichloromethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-27-4 Bromoform ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-25-2 Bromomethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 1.0 03/26/05 22:35 PPM 104-51.8 sec-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 135-98.8 tert-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 56-23.5 Chlorobenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 108-90-7 Chloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-00-3 Chloroform ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 67-66-3 Chloromethane ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 95-49.8 4-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 106-43.4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 96-12.8 Dibromochloromethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 106-93.4 Dibromomethane ND mg/l 0.00053 1.0 03/26/05 22:35 PPM 74-95.3 Date: 04/07/05 Page: 4 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 A«a,?. NC Drinking Water 37706 SC Environmental 99030 Sc 99006 ci Kici ep ca7aea Y=;:;_=': I l�fd((;; FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423634 Client Sample ID: MW-2 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Project Sample Number: 9290570-002 Date Collected: 03/22/05 11:51 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt 1,2-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 22:35 PPM 95.50-1 1,3-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 22:35 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 22:35 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-71-8 1 1,1-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75.35-4 cis-1,2-Dichloroethene 0.0015 mg/l 0.00050 1.0 03/26/05 22:35 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 78.87-5 1,3-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 142-28-9 2.2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 563-58-6 cis-1.3-Dichloropropene ND mg/l 0,00050 1.0 03/26/05 22:35 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 10061-02-6 Diisopropyl ether ND mg/l 0�00050 1.0 03/26/05 22:35 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 100-41-4 Hexachloro-1,3-butadiene ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 1.0 03/26/05 22:35 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 103-65-1 Styrene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 100-42-5 1,1.1,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 79-34-5 Tetrachloroethene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 22:35 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 79.00-5 Trichloroethene 0.0012 mg/l 0.00050 1.0 03/26/05 22:35 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 96.18-4 1,2,4-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 95.63-6 1,3.5-Trimethylbenzene 0.0081 mg/l 0.00050 1.0 03/26/05 22:35 PPM 108-67.8 Date: 04/07/05 Page: 5 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , ,� .«,,, NC Drinking Water 37706 SC Environmental 99030 Sc 99006 CI MCI AD C07CAO y:`__=`�� P_fil� FI NFI AP E87627 Pace Analytical Services, Inc. ,Analytical ® 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 www.pacelabs.com Phone: 704.875.9092 Fax. 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Lab Sample No: 925423634 Project Sample Number: 9290570-002 Date Collected: 03/22/05 11:51 Client Sample ID: MW-2 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Vinyl chloride ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 75-01-4 mbp-Xylene 0.00080 mg/l 0.00050 1.0 03/26/05 22:35 PPM o-Xylene ND mg/l 0.00050 1.0 03/26/05 22:35 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 83 % 1.0 03/26/05 22:35 PPM 625-98-9 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD C97RAA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. �Cpp Rl^C� Y • •� A Page: 6 of 56 harlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. Analytical ® 9800 Kincey Avenue, Suite 100 Hunfersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423642 Project Sample Number: 9290570-003 Date Collected: 03/22/05 12:23 Client Sample ID: MW-5 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 6.6 mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus ND mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 108-86.1 Bromochloromethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75-27-4 Bromoform ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75-25-2 Bromomethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 1.0 03/26/05 23:16 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 108-90-7 Chloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75.00-3 Chloroform ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 67.66-3 Chloromethane ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 74-95-3 Date: 04/07/05 Page: 7 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ^°ce,, NC Drinking Water 37706 Environmental 99030 f• 0 06 ri ICI GI AD CR7�AA n' FL NELAP E8Sc 7627 aceAnalytical www.pacelabs.com Lab Sample No: 925423642 Client Sample ID: MW-5 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax., 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Project Sample Number: 9290570-003 Date Collected: 03/22/05 12:23 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt 1.2-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:16 PPM 95-50-1 1.3-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:16 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:16 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75-71-8 1.1-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75.35-4 cis-1,2-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 563-58-6 cis-1.3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00(150 1.0 03/26/05 23:16 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 100-41-4 Hexachloro-1,3-butadiene ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 98.82.8 p-Isopropyltoluene ND mg/l 0.0010 1.0 03/26/05 23:16 PPM 99.87-6 Methylene chloride ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 103-65-1 Styrene ND mg/l 0.00D50 1.0 03/26/05 23:16 PPM 100-42-5 1.1,1,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 630-20-6 1.1.2.2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 79-34-5 Tetrachloroethene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 1.2,3-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 87.61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 23:16 PPM 120-82.1 1.1,1-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 71-55.6 1.1,2-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 79-00-5 Trichloroethene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0005) 1.0 03/26/05 23:16 PPM 75-69.4 1,2.3-Trichloropropane ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 96-18-4 1,2.4-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 95-63.6 1,3,5-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 108-67-8 Date: 04/07/05 Page: & of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , ,* A«o., NC Drinking Water 37706 SC Environmental 99030 n_:`•t Sc 99006 r' "r' An C°'C"° FL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical ® Huntersville, NC 28078 Phone. 704.875.9092 www.pacelabs.com FAX 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423642 Project Sample Number: 9290570-003 Date Collected: 03/22/05 12:23 Client Sample ID: MW-5 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Vinyl chloride ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM o-Xylene ND mg/l 0.00050 1.0 03/26/05 23:16 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 100 % 1.0 03/26/05 23:16 PPM 625-98-9 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 .- An REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ° Uy npjnr. a Page: 9 of 56 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 ' Analytical ® Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423659 Project Sample Number: 9290570-004 Date Collected: 03/22/05 12:37 Client Sample ID: 6-R Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 14. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.573 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75-27-4 Bromoform ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75-25.2 Bromomethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 74-83.9 n-Butylbenzene ND mg/l 0.0010 1.0 03/26/05 23:58 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 56-23-5 Chlorobenzene ND mg/1 0.00050 1.0 03/26/05 23:58 PPM 108-90-7 Chloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75-00-3 Chloroform ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 67-66-3 Chloromethane ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 106-43-4 1.2-Dibromo-3-chloropropane ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 106-93-4 Dibromomethane ND mg/1 0.00050 1.0 03/26/05 23:58 PPM 74-95-3 Date: 04/07/05 Page: 10 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 % %, AC Co NC Drinking Water 37706 SC Environmental 99030^ Sc 99006 `en [--mbi� ' 1:1 KIrl AD CA7997 nalytical® aceA www.pacelabs.com Lab Sample No: 925423659 Client Sample ID: 6-R Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Phone: 704.875.9092 Fax., 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-004 Date Collected: 03/22/05 12:37 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt 1,2-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:58 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:58 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 1.0 03/26/05 23:58 PPM 106.46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75.35-4 cis-1,2-Dichloroethene 0.0015 mg/l 0.00050 1.0 03/26/05 23:58 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 156.60-5 1.2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 10061-02.6 Diisopropyl ether ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 100-41-4 Hexachloro-1,3-butadiene ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 1.0 03/26/05 23:58 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 103-65-1 Styrene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 79.34-5 Tetrachloroethene 0.080 mg/l 0.0025 5.0 03/26/05 23:58 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 1.0 03/26/05 23:58 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 71-55-6 1.1.2-Trichloroethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 79-00-5 Trichloroethene 0.0090 mg/l 0.00050 1.0 03/26/05 23:58 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75.69-4 1,2,3-Trichloropropane ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 96-18-4 1,2,4-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 95-63-6 1.3,5-Trimethylbenzene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 108-67.8 Date: 04/07/05 Page: 11 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ACC,* NC Drinking Water 37706 SC Environmental 99030 .`% � Sc 99006 " ""'AD cA'r^A n&& FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423659 Client Sample ID: 6-R Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax- 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-004 Date Collected: 03/22/05 12:37 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Vinyl chloride ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 75.01-4 m&p-Xylene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM o-Xylene ND mg/l 0.00050 1.0 03/26/05 23:58 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 100 % 1.0 03/26/05 23:58 PPM 625-98-9 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri ur, An r WM A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. AC pO, .4, n'IP C` Page: 12 of.56 harlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical" Huntersviile, NC 28078 Phone: 704.875.9092 www.pacelabs.com fax. 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423717 Project Sample Number: 9290570.005 Date Collected: 03/22/05 13:21 Client Sample ID: MW-7 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit OF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 10. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00.6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N NO mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N NO mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.756 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate NO mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Sulfide GC Volatiles GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1.2-Dibromo-3-chloropropane Dibromochloromethane 1.2-Dibromoethane (EDB) Dibromomethane Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl Aim An r07CAo Method: EPA 376.2 NO mg/l 0.050 1.0 03/28/05 18:00 JDA1 Method: SM 6230D NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 71-43-2 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 108-86-1 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 74-97-5 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 75-27-4 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 75-25-2 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 74-83-9 NO mg/l 0.0010 1.0 03/27/05 00:39 PPM 104-51-8 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 135-98-8 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 98-06-6 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 56-23-5 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 108-90-7 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 75.00-3 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 67.66-3 NO mg/l 0.0020 1.0 03/27/05 00:39 PPM 74.87-3 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 95-49-8 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 106-43-4 NO mg/l 0.0020 1.0 03/27/05 00:39 PPM 96-12-8 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 124-48-1 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 106.93-4 NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 74-95-3 Page: 13 of 56 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Charlotte Certification IN without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 o A«o,,, NC Drinking Water 37706 Sc 99006 I�1C = FI NFI AP E87627 aceAnalytical® www.pacelabs.com Lab Sample No: 925423717 Client Sample ID: MW-7 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax., 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570.005 Date Collected: 03/22/05 13:21 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt 1,2-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 00:39 PPM 95-50-1 1.3-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 00:39 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 00:39 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 75-71-8 1.1-Dichloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 75.34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 107-06.2 1,1-Dichloroethene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 75-35.4 cis-1,2-Dichloroethene 0.0012 mg/l 0.00050 1.0 03/27/05 00:39 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 156-60.5 1,2-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 10061-02.6 Diisopropyl ether ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 100-41.4 Hexachloro-1,3-butadiene ND mg/l 0.0020 1.0 03/27/05 00:39 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0005C 1.0 03/27/05 00:39 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 1.0 03/27/05 00:39 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 03/27/05 00:39 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/27/05 00:39 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 103-65.1 Styrene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 100-42.5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 79-34-5 Tetrachloroethene 0.0043 mg/l 0.00050 1.0 03/27/05 00:39 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.0 03/27/05 00:39 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 1.0 03/27/05 00:39 PPM 120.82-1 1,1,1-Trichloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 79-00-5 Trichloroethene 0.0086 mg/l 0.00050 1.0 03/27/05 00:39 PPM 79-01.6 Trichlorofluoromethane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 96-18.4 1,2,4-Trimethylbenzene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 1.0 03/27/05 00:39 PPM 108-67.8 Date: 04/07/05 Page: 14 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 % A«o,, NC Drinking Water 37706 SC Environmental 99030 _1t Sc 99006 ci KIM AD MReR `�nr� "'�d(; FL NP AP E87627 Pace Analytical Services, Inc. ,Analytical ® 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 www pacelabs. com Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Lab Sample No: 925423717 Project Sample Number: 9290570-005 Date Collected: 03/22/05 13:21 Client Sample ID: MW-7 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Vinyl chloride NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 75.01-4 m&p-Xylene NO mg/l 0.00050 1.0 03/27/05 00:39 PPM o-Xylene NO mg/l 0.00050 1.0 03/27/05 00:39 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 98 X 1.0 03/27/05 00:39 PPM 625-98-9 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 r, un An rG 70AC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,`� 11 CCCOAO+` C 'runlet Page: 15 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Lab Sample No: 925423725 Project Sample Number: 9290570-006 Date Collected: 03/22/05 13:27 Client Sample ID: MW-8 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 19. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N 2.8 mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.373 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate 40. mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-27-4 Bromoform ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-25-2 Bromomethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 1.0 03/27/05 01:21 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 108-90-7 Chloroethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-00.3 Chloroform ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 67.66-3 Chloromethane ND mg/l 0.0020 1.0 03/27/05 01:21 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 1.0 03/27/05 01:21 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 74-95-3 Date: 04/07/05 Pape: 16 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , %, AC�,,o NC Drinking Water 37706 Environmental 99030 e, 4#1 %SC Sc 99006 C1 K11:1 AD C47CA0 I n:_ FI NFI AP F87677 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax., 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423725 Project Sample Number: 9290570-006 Date Collected: 03/22/05 13:27 Client Sample ID: MW-8 Matrix: water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt 1,2-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 01:21 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 01:21 PPM 541-73.1 1.4-Dichlorobenzene ND mg/l 0.0010 1.0 03/27/05 01:21 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-71-8 1.1-Dichloroethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 107-06-2 1,1-Dichloroethene ND mg/1 0,00050 1.0 03/27/05 01:21 PPM 75.35-4 cis-1,2-Dichloroethene ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 156-60-5 1.2-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 78.87-5 1.3-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 142-28-9 2.2-Dichloropropane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 563-58-6 cis-1.3-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 10061-01.5 trans-1,3-Dichloropropene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 100-41-4 Hexachloro-1.3-butadiene ND mg/l 0.0020 1.0 03/27/05 01:21 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 98-82-8 p-Isopropyltoluene ND mg/1 0.0010 1.0 03/27/05 01:21 PPM 99-87-6 Methylene chloride ND mg/1 0.0020 1.0 03/27/05 01:21 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.0 03/27/05 01:21 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 103-65-1 Styrene ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 100-42-5 1,1.1,2-Tetrachloroethane ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 630-20-6 1.1.2.2-Tetrachloroethane ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 79-34-5 Tetrachloroethene 0.0013 mg/l 0.00050 1.0 03/27/05 01:21 PPM 127-18-4 Toluene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 1.2,3-Trichlorobenzene ND mg/1 0.0020 1.0 03/27/05 01:21 PPM 87-61-6 1,2.4-Trichlorobenzene ND mg/l 0.0020 1.0 03/27/05 01:21 PPM 120.82-1 1.1.1-Trichloroethane ND mg/1 0.00050 1.0 03/27/05 01:21 PPM 71-55-6 1.1.2-Trichloroethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 79-00-5 Trichloroethene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-69-4 1.2.3-Trichloropropane ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 96-18-4 1.2.4-Trimethylbenzene ND mg/l 0,00050 1.0 03/27/05 01:21 PPM 95-63-6 1.3,5-Trimethylbenzene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 108-67-8 Date: 04/07/05 Page: 17 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IDS NC Wastewater 40 without tho written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , �.«�,,, NC Drinking Water 37706 SC Environmental 99030 Sc SC 99006 M hiGl no FA7aAA Ede FL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 ' Analytical ® Huntersville, IVC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423725 Project Sample Number: 9290570-006 Date Collected: 03/22/05 13:27 Client Sample ID: MW-8 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Vinyl chloride ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 75-01.4 mbp-Xylene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM o-Xylene ND mg/l 0.00050 1.0 03/27/05 01:21 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 99 X 1.0 03/27/05 01:21 PPM 625-98-9 Date: 04/07/05 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37712 A«a,, SC Environmental 99030 rR,rl en C07CA0 ,�, nm.C' Page: 18 of 56 rlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 9900 A NFI AP FR7697 aceAnalytical www.pacoiahs.com Lab Sample No: 925423741 Client Sample ID: MW-9 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Project Sample Number: 9290570-007 Date Collected: 03/22/05 14:20 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 33. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00.6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus 0.162 mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate.Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 71-43-2 Bromobenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 108-86-1 Bromochloromethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 74-97-5 Bromodichloromethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-27-4 Bromoform ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75.25-2 Bromomethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 74-83-9 n-Butylbenzene ND mg/l 0.050 50.0 03/27/05 02:02 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.025 50.0 03/27/05 02:02 PPM 56-23-5 Chlorobenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 108-90-7 Chloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-00-3 Chloroform ND mg/l 0.025 50.0 03/27/05 02:02 PPM 67-66-3 Chloromethane ND mg/l 0.10 50.0 03/27/05 02:02 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 106-43-4 1.2-Dibromo-3-chloropropane ND mg/l 0.10 50.0 03/27/05 02:02 PPM 96-12-8 Dibromochloromethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 124-48-1 1.2-Dibromoethane (EDB) ND mg/l 0.025 50.0 03/27/05 02:02 PPM 106-93-4 Dibromomethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 74-95-3 Date: 04/07/05 Page: 19 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IDS NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , " A���,, NC Drinking Water 37706 SC Environmental 99030 4% Sc 99006 C! S FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423741 Client Sample ID: MW-9 Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-007 Date Collected: 03/22/05 14:20 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt 1,2-Dichlorobenzene ND mg/l 0.050 50.0 03/27/05 02:02 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.050 50.0 03/27/05 02:02 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.050 50.0 03/27/05 02:02 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.025 50,0 03/27/05 02:02 PPM 75-35-4 cis-1,2-Dichloroethene 0.99 mg/l 0.025 50.0 03/27/05 02:02 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 156-60.5 1,2-Dichloropropane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 142-28.9 2,2-Dichloropropane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 10061.01-5 trans-1.3-Dichloropropene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 10061.02-6 Diisopropyl ether ND mg/l 0.025 50.0 03/27/05 02:02 PPM 108-20-3 Ethylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 100-41-4 Hexachloro-1.3-butadiene ND mg/l 0.10 50.0 03/27/05 02:02 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.025 50.0 03/27/05 02:02 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.050 50.0 03/27/05 02:02 PPM 99-87.6 Methylene chloride ND mg/l 0.10 50.0 03/27/05 02:02 PPM 75-09.2 Methyl-tert-butyl ether ND mg/l 0.025 50.0 03/27/05 02:02 PPM 1634-04-4 Naphthalene ND mg/l 0.10 50.0 03/27/05 02:02 PPM 91-20-3 n-Propylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 103-65-1 Styrene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 630-20-6 1.1,2.2-Tetrachloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 79-34.5 Tetrachloroethene 0.90 mg/l 0.025 50.0 03/27/05 02:02 PPM 127-18-4 Toluene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 02:02 PPM 1,2,3-Trichlorobenzene ND mg/l 0.10 50.0 03/27/05 02:02 PPM 87-61.6 1,2,4-Trichlorobenzene ND mg/l 0.10 50.0 03/27/05 02:02 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 79-00-5 Trichloroethene 1.1 mg/l 0.025 50.0 03/27/05 02:02 PPM 79-01.6 Trichlorofluoromethane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.025 50.0 03/27/05 02:02 PPM 96-18-4 1,2,4-Trimethylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 108-67-8 1 Date: 04/07/05 Page: 20 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 0 ACC NC Drinking Water 37706 SC Environmental 99030 _°•� u n Sc 99006 C1 RICI eo CQ7RA4 ebc FL NELAP E97627 aceAnalytical www.paceiabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423741 Project Sample Number: 9290570-007 Date Collected: 03/22/05 14:20 Client Sample ID: MW-9 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Vinyl chloride ND mg/l 0.025 50.0 03/27/05 02:02 PPM 75-01-4 mbp-Xylene ND mg/l 0.025 50.0 03/27/05 02:02 PPM o-Xylene ND mg/l 0.025 50.0 03/27/05 02:02 PPM 95.47-6 1-Chloro-3-fluorobenzene (S) 100 % 1.0 03/27/05 02:02 PPM 625-98-9 Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 [I RICI AD rQ7RAQ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page: 21 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 .:?Analytical® Huntersville, NC 28078 www.pacelabs.com Phone. 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423758 Project Sample Number: 9290570.008 Date Collected: 03/22/05 14:47 Client Sample ID: MW-10 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 10. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N 0.36 mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus ND mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate.Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 71-43-2 Bromobenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 108-86-1 Bromochloromethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 74-97-5 Bromodichloromethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-27-4 Bromoform ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-25.2 Bromomethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0050 5.0 03/27/05 02:44 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 56-23.5 Chlorobenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 108-90.7 Chloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-00-3 Chloroform ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 67-66-3 Chloromethane ND mg/l 0.010 5.0 03/27/05 02:44 PPM 74-87.3 2-Chlorotoluene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0)(1 5.0 03/27/05 02:44 PPM 96-12-8 Dibromochloromethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 106-93-4 Dibromomethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 74.95-3 Date: 04/07/05 Page: 22 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 %%_ACC% NC Drinking Water 37706 SC Environmental 99030 , u•'n_:°�� Sc 99006 rt %irl An C070AC �'�, FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423758 Client Sample ID: MW-10 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Project Sample Number: 9290570-008 Date Collected: 03/22/05 14:47 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual ReaLmt 1.2-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 02:44 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 02:44 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 02:44 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-71-8 1.1-Dichloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-35-4 cis-1.2-Dichloroethene 0.018 mg/l 0.0025 5.0 03/27/05 02:44 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 156-60-5 1.2-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 142-28-9 2.2-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 563-58.6 cis-1,3-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 10061-01.5 trans-1,3-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 10061.02.6 Diisopropyl ether ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 108-20-3 Ethylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 100-41-4 Hexachloro-1.3-butadiene ND mg/l 0.010 5.0 03/27/05 02:44 PPM 87.68-3 Isopropylbenzene (Cumene) ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0050 5.0 03/27/05 02:44 PPM 99-87-6 Methylene chloride ND mg/l 0.010 5.0 03/27/05 02:44 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 1634-04-4 Naphthalene ND mg/l 0.010 5.0 03/27/05 02:44 PPM 91-20-3 n-Propylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 103-65.1 Styrene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 630.20-6 1,1,2.2-Tetrachloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 79-34-5 Tetrachloroethene 0.16 mg/l 0.0025 5.0 03/27/05 02:44 PPM 127.18-4 Toluene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 108.88.3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 02:44 PPM 1.2,3-Trichlorobenzene ND mg/l 0.010 5.0 03/27/05 02:44 PPM 87-61-6 1,2.4-Trichlorobenzene ND mg/l 0.010 5.0 03/27/05 02:44 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 71-55-6 1.1,2-Trichloroethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 79.00-5 Trichloroethene 0.028 mg/l 0.0025 5.0 03/27/05 02:44 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 96-18-4 1.2.4-Trimethylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 108-67-8 Date: 04/07/05 Page: 23 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 .��o�, NC Drinking Water 37706 SC Environmental 99030 W'� '- Sc 99006 r' "r' "" CO7411g �. FL NELAP E87627 Pace Analytical Services, Inc. ,Analytical ® 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 www. pacelabs. com Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423758 Project Sample Number: 9290570-008 Date Collected: 03/22/05 14:47 Client Sample ID: MW-10 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Vinyl chloride ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 75-01-4 mbp-Xylene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM o-Xylene ND mg/l 0.0025 5.0 03/27/05 02:44 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 100 % 1.0 03/27/05 02:44 PPM 625-98-9 Date- 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 [i ain An C07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 140t� • Page: 24 of 56 lotte Certification ID NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FL NELAP E87627 Pace Analytical Services, Inc. ,Analytical ® 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423766 Project Sample Number: 9290570-009 Date Collected: 03/22/05 14:25 Client Sample ID: NW-11 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 13. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00.6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N 1.3 mg/l 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus ND mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate.Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 71-43-2 Bromobenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 108-86-1 Bromochloromethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 74-97-5 Bromodichloromethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-27-4 Bromoform ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-25-2 Bromomethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 74-83-9 n-Butylbenzene ND mg/l 0.010 10.0 03/27/05 03:25 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 56.23-5 Chlorobenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 108-90.7 Chloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-00-3 Chloroform ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 67.66-3 Chloromethane ND mg/l 0.020 10.0 03/27/05 03:25 PPM 74.87-3 2-Chlorotoluene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 95.49-8 4-Chlorotoluene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 106-43.4 1.2-Dibromo-3-chloropropane ND mg/l 0.020 10.0 03/27/05 03:25 PPM 96-12-8 Dibromochloromethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 124-48-1 1.2-Dibromoethane (EDB) ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 106-93-4 Dibromomethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 74-95-3 Date: 04/07/05 Page: 25 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IDS NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 "•°�� NC Drinking Water 37706 SC Environmental 99030 n. s° SC 99006 '"'"'" yF'-AC t f1 FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423766 Client Sample ID: NW-11 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax. 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Project Sample Number: 9290570.009 Date Collected: 03/22/05 14:25 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt 1.2-Dichlorobenzene ND mg/l 0.010 10.0 03/27/05 03:25 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.010 10.0 03/27/05 03:25 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.010 10.0 03/27/05 03:25 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-34.3 1,2-Dichloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75.35-4 cis-1.2-Dichloroethene 0.045 mg/l 0.0050 10.0 03/27/05 03:25 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 156-60.5 1,2-Dichloropropane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 108-20-3 Ethylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 100-41-4 Hexachloro-1,3-butadiene ND mg/l 0.020 10.0 03/27/05 03:25 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.010 10.0 03/27/05 03:25 PPM 99-87-6 Methylene chloride ND mg/l 0.020 10.0 03/27/05 03:25 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 1634-04-4 Naphthalene ND mg/l 0.020 10.0 03/27/05 03:25 PPM 91-20-3 n-Propylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 103-65-1 Styrene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 630-20.6 1,1,2.2-Tetrachloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 79-34-5 Tetrachloroethene 0.43 mg/l 0.0050 10.0 03/27/05 03:25 PPM 127-18-4 Toluene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 03:25 PPM 1,2,3-Trichlorobenzene ND mg/l 0.020 10.0 03/27/05 03:25 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.020 10.0 03/27/05 03:25 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 71-55.6 1,1,2-Trichloroethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 79.00-5 Trichloroethene 0.054 mg/l 0.0050 10.0 03/27/05 03:25 PPM 79.01-6 Trichlorofluoromethane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 96-18-4 1,2.4-Trimethylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 108-67-8 Date: 04/07/05 Page: 26 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 a ,• A«o,, NC Drinking Water 37706 SC Environmental 99030 `� , '`°• Sc 99006 rl •Iri An rn7Bln U np1hr-t. FLNFLAP F87627 Analytical www.paceiabs.com Lab Sample No: 925423766 Client Sample ID: NW-11 Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone., 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Project Sample Number: 9290570-009 Date Collected: 03/22/05 14:25 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Vinyl chloride ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 75-01-4 mbp-Xylene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM o-Xylene ND mg/l 0.0050 10.0 03/27/05 03:25 PPM 95.47-6 1-Chloro-3-fluorobenzene (S) 108 % 1.0 03/27/05 03:25 PPM 625-98-9 Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl A/rl An [o7cAe REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. AFFOR Off. o l Oi Page: 27 of 56 harlott NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Serv/ces, Inc. 9800 KinceyAvenue, Suite 100 Analytical ® Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704. 875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423774 Project Sample Number: 9290570-010 Date Collected: 03/22/05 15:00 Client Sample ID: MW-13 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Wet Chemistry Chloride (Mercuric Nitrate) Method: EPA 325.2 Chloride 19. mg/l 5.0 1.0 03/28/05 23:30 BMF 16887-00-6 48 Hour NO3 / NO2 / NOX Method: EPA 353.2 Nitrate as N ND mg/1 0.10 1.0 03/23/05 22:35 JDA1 Nitrite as N ND mg/l 0.10 1.0 03/23/05 22:35 JDA1 Phosphorus, Total Method: EPA 365.2 Phosphorus ND mg/l 0.100 1.0 03/24/05 08:00 TMR 7723-14-0 Sulfate,Turbidimetric Method: EPA 375.4 Sulfate ND mg/l 5.0 1.0 03/28/05 23:30 BMF Sulfide, Total Method: EPA 376.2 Sulfide ND mg/l 0.050 1.0 03/28/05 18:00 JDA1 GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 71-43-2 Bromobenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 108-86-1 Bromochloromethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 74-97-5 Bromodichloromethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-27-4 Bromoform ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-25-2 Bromomethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0050 5.0 03/27/05 04:07 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 56-23-5 Chlorobenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 108-90-7 Chloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-00-3 Chloroform ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 67-66-3 Chloromethane ND mg/l 0.010 5.0 03/27/05 04:07 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 106-43-4 1.2-Dibromo-3-chloropropane ND mg/l 0.010 5.0 03/27/05 04:07 PPM 96-12.8 Dibromochloromethane ND mg/1 0.0025 5.0 03/27/05 04:07 PPM 124-48.1 1,2-Dibromoethane (EDB) ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 106-93-4 Dibromomethane ND mg/1 0.0025 5.0 03/27/05 04:07 PPM 74-95-3 Date: 04/07/05 Page: 28 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 , ,� �«�,, NC Drinking Water 37706 SC Environmental 99030 Sc 99006 n Rip AD GUana n� FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423774 Client Sample ID: MW-13 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04.014 Project Sample Number: 9290570-010 Date Collected: 03/22/05 15:00 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No, Qual RegLmt 1,2-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 04:07 PPM 95.50-1 1,3-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 04:07 PPM 541.73-1 1,4-Dichlorobenzene ND mg/l 0.0050 5.0 03/27/05 04:07 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-71-8 1.1-Dichloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-35-4 cis-1,2-Dichloroethene 0.13 mg/l 0.0025 5.0 03/27/05 04:07 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 156-60.5 1,2-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 142-28-9 2.2-Dichloropropane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 108-20-3 Ethylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 100-41-4 Hexachloro-1,3-butadiene ND mg/l 0.010 5.0 03/27/05 04:07 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0050 5.0 03/27/05 04:07 PPM 99-87-6 Methylene chloride ND mg/l 0.010 5.0 03/27/05 04:07 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 1634-04-4 Naphthalene ND mg/l 0.010 5.0 03/27/05 04:07 PPM 91-20-3 n-Propylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 103-65.1 Styrene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 630.20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 79-34-5 Tetrachloroethene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 127-18-4 Toluene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 108-88-3 Total Trihalomethanes (Calc.) ND mg/l 0.00050 1.0 03/27/05 04:07 PPM 1,2,3-Trichlorobenzene ND mg/l 0.010 5.0 03/27/05 04:07 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.010 5.0 03/27/05 04:07 PPM 120-82.1 1,1,1-Trichloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 79-00-5 Trichloroethene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-69-4 1.2,3-Trichloropropane ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 96-18-4 1,2,4-Trimethylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 95.63-6 1.3,5-Trimethylbenzene ND mg/l 0.0025 5.0 03/27/05 04:07 PPM 108-67-8 Date: 04/07/05 Page: 29 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 .«,,, NC Drinking Water 37706 SC Environmental 99030:_•� Sc 99006 " RIM AD C479A4 1 j FL NELAP E87627 aceAnalytical www.pacelabs.com Lab Sample No: 925423774 Client Sample ID: MW-13 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-010 Date Collected: 03/22/05 15:00 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit OF Analyzed By CAS No. Qual Re9Lmt Vinyl chloride NO mg/l 0.0025 5.0 03/27/05 04:07 PPM 75-01-4 m&p-Xylene NO mg/l 0.0025 5.0 03/27/05 04:07 PPM o-Xylene NO mg/l 0.0025 5.0 03/27/05 04:07 PPM 95-47.6 1-Chloro-3-fluorobenzene (S) 100 X 1.0 03/27/05 04:07 PPM 625-98-9 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI NICI AD C079AA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. n� Page: 30 of 56 harlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace*alytical www.paceiabs.com Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423782 Project Sample Number: 9290570.011 Date Collected: 03/22/05 11:30 Client Sample ID: MW-1/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 7.8 mg/l 0.050 1.0 03/31/05 19:50 ALV 7439-89-6 Manganese, Dissolved 6.0 mg/l 0.0050 1.0 03/31/05 19:50 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI KIP AP GA7AAA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. . Aecn, 40: % `/��00 ■ ■�/e c + Page: 31 of 56 harlotte Certificati NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FL NELAP E87627 ;aneAnalyticalo www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax. 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Lab Sample No: 925423790 Project Sample Number: 9290570-012 Date Collected: 03/22/05 11:51 Client Sample ID: MW-2/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 130 mg/l 0.050 1.0 03/31/05 19:55 ALV 7439.89.6 Manganese, Dissolved 64. mg/l 0.0050 1.0 03/31/05 19:55 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 r, ..r- An rn-rr_ An REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. A000,o I'1�C Page: 32 of 56 harlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax.704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423808 Project Sample Number: 9290570.013 Date Collected: 03/22/05 12:23 Client Sample ID: MW-5/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Metals Dissolved Metals, ICP; Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 1.6 mg/l 0.050 1.0 03/31/05 19:59 ALV 7439-89-6 Manganese, Dissolved 1.3 mg/l 0.0050 1.0 03/31/05 19:59 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI AICI AD C07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ACCCA h`O 041 U J Page: 33 of 56 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FL NELAP E87627 aceAnalytical® www.pacelabs.com Lab Sample No: 925423816 Client Sample ID: 6-R/DISSOLVED Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax. • 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-014 Date Collected: 03/22/05 12:37 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 0.42 mg/l 0.050 1.0 03/31/05 20:03 ALV 7439-89-6 Manganese, Dissolved 2.3 mg/l 0.0050 1.0 03/31/05 20:03 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification I NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD CQ79AQ REPORT OF LABORATORY ANALYSIS This report shall not. be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. . Ace". --next, Page: 34 of 56 Charlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical www.paceiabs.com Lab Sample No: 925423832 Client Sample ID: NW-7/DISSOLVED Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Project Sample Number: 9290570-015 Date Collected: 03/22/05 13:21 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Metals Dissolved Metals, ICP. Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron. Dissolved 0.91 mg/l 0.050 1.0 03/31/05 20:07 ALV 7439-89-6 Manganese. Dissolved 1.9 mg/l 0.0050 1.0 03/31/05 20:07 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 re alrl •n r070A0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,♦BOG . ..40,�1 Page: 35 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical ® Huntersville, NC 28078 Phone: 704.875.9092 www.pacalabs.com Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 Lab Sample No: 925423840 Project Sample Number: 9290570-016 Date Collected: 03/22/05 13:27 Client Sample ID: MW-8/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By GAS No. Qual Re9Lmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron. Dissolved 1.5 mg/l 0.050 1.0 03/31/05 20:21 ALV 7439-89-6 Manganese, Dissolved 0.061 mg/l 0.0050 1.0 03/31/05 20:21 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 r uri An C07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. C ,� ACCp�o O Page: 36 of 56 harlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ;aneAnalyticale www.pacelabs.com Lab Sample No: 925423857 Client Sample ID: MW-9/DISSOLVED Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 9290570 Fax 704.875.9091 Client Project ID: Fairchild 015-04-014 Project Sample Number: 9290570-017 Date Collected: 03/22/05 14:20 Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual Re9Lmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 2.4 mg/l 0.050 1.0 03/31/05 20:25 ALV 7439-89-6 Manganese, Dissolved 1.5 mg/l 0.0050 1.0 03/31/05 20:25 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Data: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI MCI AD C917RAQ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Mekt - Page: 37 of 56 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 Sc 99006 A NFLAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical ® Huntersville, NC 28078 Phone. 704.875.9092 www.pacelabs.com Fax.704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Lab Sample No: 925423865 Project Sample Number: 9290570-018 Date'Collected: 03/22/05 14:47 Client Sample ID: MW-10/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters` Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 0.075 mg/l 0.050 1.0 03/31/05 20:29 ALV 7439-89-6 Manganese, Dissolved 0.067 mg/l 0.0050 1.0 03/31/05 20:29 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Asheville Certification ID NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 O hM An C07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ACC07 Page: 38 of 56 harlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. Analytical ® 9800 KHunterswTleeNC 128078 www. pace/abs. com Phone: 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Lab Sample No: 925423873 Project Sample Number: 9290570-019 Date Collected: 03/22/05 14:25 Client Sample ID: MW-11/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed BY CAS No. Qual ReaLmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron, Dissolved 0.62 mg/l 0.050 1.0 03/31/05 20:33 ALV 7439-89-6 Manganese, Dissolved 0.080 mg/l 0.0050 1.0 03/31/05 20:33 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 Page: 39 of 56 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ,� .��o., NC Drinking Water 37706 SC Environmental 99030 .'�` ''°f Sc 99006 " "'C' AD CQ7rAQ FL NELAP E87627 ;acieAnalyfical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, N«; 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Lab Sample No: 925423881 Project Sample Number: 9290570-020 Date Collected: 03/22/05 15:00 Client Sample ID: MW-13/DISSOLVED Matrix: Water Date Received: 03/23/05 09:30 Parameters Results Units Report Limit DF Analyzed By CAS No. Qual RegLmt Metals Dissolved Metals, ICP, Trace Prep/Method: EPA 200.7 / EPA 200.7 Iron. Dissolved 30. mg/l 0.050 1.0 03/31/05 20:37 ALV 7439-89-6 Manganese, Dissolved 28. mg/l 0.0050 1.0 03/31/05 20:37 ALV 7439-96-5 Date Digested 03/28/05 01:30 03/28/05 01:30 Date: 04/07/05 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37712 SC Environmental 99030 Page: 40 of 56 Mi irlotte Certification JDa NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FL NFI AP F87627 [I RICI AD COWA0 Pace Analytical Services, Inc. ,Analytical ® 9800 Kincey Avenue, Suite 78 0 00 Huntersville, NC 28078 www. pacelabs. com Phone: 704.875.9092 Fax 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 PARAMETER FOOTNOTES Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes in sample preparation, dilution of the extract, or moisture content Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Charlotte laboratory unless otherwise footnoted. Method 9071E modified to use ASE. All pH. Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate hold time. ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit (S) Surrogate Ill Sample preservation does not meet EPA recommendations for analyte. Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. . Al 0 Page: 41 of 56 harlotte Certifi NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FI NFI AP F97677 Analytical® www.pacelahs.com QUALITY CONTROL DATA QC Batch: 124312 QC Batch Method: SM 6230D Associated Lab Samples: METHOD BLANK: 925434862 Associated Lab Samples: Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 Analysis Method: SM 6230D Analysis Description: GC VOCs in Water 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 Blank Reporting Parameter Units Result Limit Footnotes Benzene mg/l NO 0.0005 Bromobenzene mg/l NO 0.0005 Bromochloromethane mg/l NO 0.0005 Bromodichloromethane mg/l NO 0.0005 Bromoform mg/l NO 0.0005 Bromomethane mg/l NO 0.0005 n-Butylbenzene mg/l NO 0.0010 sec-Butylbenzene mg/l NO 0.0005 tert-Butylbenzene mg/l NO 0.0005 Carbon tetrachloride mg/l NO 0.0005 Chlorobenzene mg/l NO 0.0005 Chloroethane mg/l NO 0.0005 Chloroform mg/l NO 0.0005 Chloromethane mg/l NO 0.0020 2-Chlorotoluene mg/l NO 0.0005 4-Chlorotoluene mg/l NO 0.0005 1,2-Dibromo-3-chloropropane mg/l NO 0.0020 Dibromochloromethane mg/l ND 0.0005 1,2-Dibromoethane (EDB) mg/l NO 0.0005 Dibromomethane mg/l NO 0.0005 1,2-Dichlorobenzene mg/l NO 0.0010 1,3-Dichlorobenzene mg/l ND 0.0010 1.4-Dichlorobenzene mg/l NO 0.0010 Dichlorodifluoromethane mg/l NO 0.0005 1,1-Dichloroethane mg/l NO 0.0005 1,2-Dichloroethane mg/l NO 0.00fi 1,1-Dichloroethene mg/l NO 0.0005 cis-1,2-Dichloroethene mg/l NO 0.0005 trans-1,2-Dichloroethene mg/l NO 0.0005 Date: 04/07/05 Certificate NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. u 1 R7Al Page: 42 of 56 rlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FI NFI AP E87627 Analytical www.paceiahs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax. • 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 METHOD BLANK: 925434862 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 Blank Reporting Parameter Units Result Limit Footnotes 1.2-Dichloropropene mg/l NO 0.0005 1,3-Dichloropropane mg/l NO 0.0005 2.2-Dichloropropene mg/l NO 0.0005 1,1-Dichloropropene mg/l NO 0.0005 cis-1,3-Dichloropropene mg/l NO 0.0005 trans-1.3-Dichloropropene mg/l NO 0.0005 Diisopropyl ether mg/l NO 0.0005 Ethylbenzene mg/l NO 0.0005 Hexachloro•1.3•butadiene mg/l NO 0.0020 Isopropylbenzene (Cunene) mg/l NO 0.0005 p-Isopropyltoluene mg/l NO 0.0010 Methylene chloride mg/l NO 0.0020 Methyl-tert-butyl ether mg/l NO 0.0005 Naphthalene mg/l NO 0.0020 n-Propylbenzene mg/l NO 0,0005 Styrene mg/l NO 0.0005 1,1,1,2-Tetrachloroethane mg/l NO 0.0005 1,1.2.2-Tetrachloroethane mg/l NO 0.0005 Tetrachloroethene mg/l NO 0.0005 Toluene mg/l NO 0.0005 Total Trihalomethanes (Calc.) mg/l NO 0.0005 1.2,3-Trichlorobenzene mg/l NO 0.0020 1,2,4-Trichlorobenzene mg/l NO 0.0020 1.1,1-Trichloroethane mg/l NO 0.0005 1.1,2-Trichloroethane mg/l NO 0.0005 Trichloroethene mg/l NO 0.0005 Trichlorofluoromethane mg/l NO 0.0005 1.2,3-Trichloropropane mg/l NO 0.0005 1.2.4-Trimethylbenzene mg/l NO 0.0005 1.3.5-Trimethylbenzene mg/l NO 0.0005 Vinyl chloride mg/l NO 0.0005 map-Xylene mg/l NO 0.0005 o-Xylene mg/l NO 0.0005 1-Chloro-3-fluorobenzene (S) % 101 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl me- An rn9eAe REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc. o`er n.• Page: 43 of 56 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NELAP E87627 Analytical www.pacelabs.com QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: 925434870 Spike LCS LCS Parameter Units Conc. Result X Rec Benzene mg/l 0.0200 0.0196 98 Bromobenzene mg/l 0.0200 0.0195 97 Bromochloromethane mg/l 0.0200 0.0204 102 Bromodichloromethane mg/l 0.0200 0.0216 108 Bromoform mg/l 0.0200 0.0210 105 Bromomethane mg/l 0.0200 0.0224 112 n-Butylbenzene mg/l 0.0200 0.0191 96 sec-Butylbenzene mg/l 0.0200 0.0198 99 tert-Butylbenzene mg/l 0.0200 0.0201 100 Carbon tetrachloride mg/l 0.0200 0.0188 94 Chlorobenzene mg/l 0.0200 0.0212 106 Chloroethane mg/l 0.0200 0.0211 106 Chloroform mg/l 0.0200 0.0209 104 Chloromethane mg/l 0.0200 0.0185 92 2-Chlorotoluene mg/l 0.0200 0.0201 100 4-Chlorotoluene mg/l 0.0200 0.0195 97 1.2-Dibromo-3-chloropropane mg/l 0.0200 0.0215 108 Dibromochloromethane mg/l 0.0200 0.0208 104 1,2-Dibromoethane (EDB) mg/l 0.0200 0.0209 105 Dibromomethane mg/l 0.0200 0.0198 99 1.2-Dichlorobenzene mg/l 0.0200 0.0202 101 1.3-Dichlorobenzene mg/l 0.0200 0.0179 90 1,4-Dichlorobenzene mg/l 0.0200 0.0198 99 Dichlorodifluoromethane mg/l 0.0200 0.0220 110 1.1-Dichloroethane mg/l 0.0200 0.0178 89 1.2-Dichloroethane mg/l 0.0200 0.0199 99 1.1-Dichloroethene mg/l 0.0200 0.0247 123 cis-1.2-Dichloroethene mg/l 0.0200 0.0202 101 trans-1.2-Dichloroethene mg/l 0.0200 0.0195 97 1.2-Dichloropropane mg/l 0.0200 0.0225 113 1.3-Dichloropropane mg/l 0.0200 0.0215 108 2.2-Dichloropropane mg/l 0.0200 0.0155 78 1.1-Dichloropropene mg/l 0.0200 0.0223 111 cis-1.3-Dichloropropene mg/l 0.0200 0.0208 104 trans-1,3-Dichloropropene mg/l 0.0200 0.0207 104 Diisopropyl ether mg/l 0.0200 0.0191 95 Ethylbenzene mg/l 0.0200 0.0209 105 Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI KIM AD CR79ZAQ Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Footnotes REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 'ne cf- Page: 44 of 56 harlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Analytical www.pacelabs.com QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: 925434870 Spike LCS LCS Parameter Units Conc. Result X Rec Hexachloro-1.3-butadiene mg/l 0.0200 0.0179 89 Isopropylbenzene (Cunene) mg/l 0.0200 0.0194 97 p-Isopropyltoluene mg/l 0.0200 0.0197 98 Methylene chloride mg/l 0.0200 0.0165 82 Methyl-tert-butyl ether mg/l 0.0200 0.0158 79 Naphthalene mg/l 0.0200 0.0198 99 n-Propylbenzene mg/l 0.0200 0.0196 98 Styrene mg/1- 0.0200 0.0204 102 1.1,1.2-Tetrachloroethane mg/l 0.0200 0.0216 108 1.1.2.2-Tetrachloroethane mg/l 0.0200 0.0204 102 Tetrachloroethene mg/l 0.0200 0.0216 108 Toluene mg/l 0.0200 0.0206 103 1.2,3-Trichlorobenzene mg/l 0.0200 0.0222 111 1,2,4-Trichlorobenzene mg/l 0.0200 0.0215 107 1,1,1-Trichloroethane mg/l 0.0200 0.0207 104 1,1,2-Trichloroethane mg/l 0.0200 0.0211 106 Trichloroethene mg/l 0.0200 0.0244 122 Trichlorofluoromethane mg/l 0.0200 0.0205 103 1.2,3-Trichloropropane mg/l 0.0200 0.0192 96 1,2,4-Trimethylbenzene mg/l 0.0200 0.0199 100 1,3,5-Trimethylbenzene mg/l 0.0200 0.0202 101 Vinyl chloride mg/l 0.0200 0.0194 97 m&p-Xylene mg/l 0.0400 0.0415 104 o-Xylene mg/l 0.0200 0.0200 100 1-Chloro-3-fluorobenzene (S) 102 SAMPLE DUPLICATE: 925434896 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax.• 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Footnotes 925411688 DUP Parameter Units Result Result RPD Benzene mg/l ND ND NC Bromobenzene mg/l ND ND NC Bromochloromethane mg/l NO NO NC Bromodichloromethane mg/l NO NO NC Bromoform mg/l ND NO NC Bromomethane mg/l NO ND NC Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD C07RAR Footnotes REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. `w •Lp p�O new Page: 45 of 56 C NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 aceAnalytical www.pacelabs.com SAMPLE DUPLICATE: 925434896 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 925411688 DUP Parameter Units Result Result RPD Footnotes n-Butylbenzene mg/l ND ND NC sec-Butylbenzene mg/l ND ND NC tert-Butylbenzene mg/l ND ND NC Carbon tetrachloride mg/l ND ND NC Chlorobenzene mg/l ND ND NC Chloroethane mg/l ND ND NC Chloroform mg/l ND ND NC Chloromethane mg/l ND ND NC 2-Chlorotoluene mg/l ND ND NC 4-Chlorotoluene mg/l ND ND NC 1,2-Dibromo-3-chloropropane mg/l ND ND NC Dibromochloromethane mg/l ND ND NC 1,2-Dibromoethane (EDB) mg/l ND ND NC Dibromomethane mg/l ND ND NC 1,2-Dichlorobenzene mg/l ND ND NC 1,3-Dichlorobenzene mg/l ND ND NC 1,4-Dichlorobenzene mg/l ND ND NC Dichlorodifluoromethane mg/l ND ND NC 1,1-Dichloroethane mg/l ND ND NC 1,2-Dichloroethane mg/l ND ND NC 1,1-Dichloroethene mg/l ND ND NC cis-1,2-Dichloroethene mg/l ND ND NC trans-1.2-Dichloroethene mg/l ND ND NC 1,2-Dichloropropane mg/l ND ND NC 1,3-Dichloropropane mg/l ND ND NC 2,2-Dichloropropane mg/l ND ND NC 1,1-Dichloropropene mg/l ND ND NC cis-1.3-Dichloropropene mg/l ND ND NC trans-1.3-Dichloropropene mg/l ND ND NC Diisopropyl ether mg/l ND ND NC Ethylbenzene mg/l ND ND NC Hexachloro-1,3-butadiene mg/l ND ND NC Isopropylbenzene (Cumene) mg/l ND ND NC p-Isopropyltoluene mg/l ND ND NC Methylene chloride mg/l ND ND NC Methyl-tert-butyl ether mg/l ND ND NC Naphthalene mg/1 ND ND NC Date: 04/07/05 sheville Certification ID NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 n KICi Arn CQUA4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. n� a Page: 46 of 56 harlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 aceAnalytical® www.pacoiahs.com SAMPLE DUPLICATE: 925434896 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 925411688 DUP Parameter Units Result Result RPD Footnotes n-Propylbenzene mg/l ND ND NC Styrene mg/l ND ND NC 1.1.1,2-Tetrachloroethane mg/l ND ND NC 1.1.2.2-Tetrachloroethane mg/l ND ND NC Tetrachloroethene mg/l ND ND NC Toluene mg/l ND ND NC Total Trihalomethanes (Calc.) mg/l ND ND NC 1.2.3-Trichlorobenzene mg/l ND ND NC 1,2,4-Trichlorobenzene mg/l ND ND NC 1,1,1-Trichloroethane mg/l ND ND NC 1,1.2-Trichloroethane mg/l ND ND NC Trichloroethene mg/l ND ND NC Trichlorofluoromethane mg/l ND ND NC 1.2,3-Trichloropropane mg/l ND ND NC 1,2,4-Trimethylbenzene mg/l ND ND NC 1,3.5-Trimethylbenzene mg/l ND ND NC Vinyl chloride mg/l ND ND NC m&p-Xylene mg/l ND ND NC o-Xylene mg/l ND ND NC 1-Chloro-3-fluorobenzene (S) % 110 100 Date: 04/07/05 Ashevill Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RIM AD 1:07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. �� ACC0�0 ��0 '• f WO / f u TIMC1% Page: 47 of 56 rlotte Certifi NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Analytical www.paceiabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 QC Batch: 124414 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: Dissolved Metals, ICP, Trace Associated Lab Samples: 925423782 925423790 925423808 925423816 925423832 925423840 925423857 925423865 925423873 925423881 METHOD BLANK: 925440208 Associated Lab Samples: 925423782 925423790 925423808 925423816 925423832 925423840 925423857 925423865 925423873 925423881 Blank Reporting Parameter Units Result Limit Footnotes Iron, Dissolved mg/l NO 0.050 Manganese, Dissolved mg/l 0.016 0.0050 LABORATORY CONTROL SAMPLE: 925440216 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Iron, Dissolved mg/l 20.00 19.70 98 Manganese, Dissolved mg/l 0.5000 0.5050 101 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 925440224 925440232 925436859 Spike Is MSD MS MSD Parameter Units Result Conc. Result Result X Rec X Rec RPD Footnotes Iron, Dissolved mg/l 14.60 20.00 27.70 29.60 66 75 7 1 Manganese. Dissolved mg/l 0.2670 0.5000 0.6460 0.6750 76 82 4 SAMPLE DUPLICATE: 925440240 Parameter Units Iron, Dissolved mg/l Manganese, Dissolved mg/l Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI 611:I AID GRMAR 925436867 DUP Result Result RPD Footnotes 11.00 12.00 3 0.09500 0.09700 3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pact; Analytical Services, Inc. tO `N ACCO,OI 4 new. - Page: 48 of 56 Charlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ?Analytical® www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax. 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 QC Batch: 124478 Analysis Method: EPA 376.2 QC Batch Method: EPA 376.2 Analysis Description: Sulfide, Total Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 METHOD BLANK: 925442717 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 Blank Reporting Parameter Units Result Limit Footnotes Sulfide mg/l NO 0.050 LABORATORY CONTROL SAMPLE: 925442725 Spike LCS LCS Parameter Units Conc. Result % Rec Footnotes Sulfide mg/l 0.5000 0.5360 107 MATRIX SPIKE: 925442733 925423626 Spike MS MS Parameter Units Result Conc. Result % Rec Footnotes Sulfide mg/l 0 0.5000 0.3310 66 1 SAMPLE DUPLICATE: 925442741 Parameter Units Sulfide mg/l Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri \fin An C07CAO 925423634 DUP Result Result RPD Footnotes NO NO NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ACC°+ Ito c l�: Page: 49 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 'Analytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04.014 QC Batch: 124180 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 48 Hour NO3 / NO2 / NOX Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 METHOD BLANK: 925426595 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 Blank Reporting Parameter Units Result Limit Footnotes Nitrate as N mg/l ND 0.10 Nitrite as N mg/l ND 0.10 LABORATORY CONTROL SAMPLE: 925426603 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Nitrate as N mg/l 5.000 4.920 98 MATRIX SPIKE: 925426611 925419871 Spike MS MS Parameter Units Result Conc. Result X Rec Footnotes Nitrate as N mg/l 0 5.000 5.400 108 SAMPLE DUPLICATE: 925426629 Parameter Units Nitrate as N mg/l Nitrite as N mg/l Date: 04/07/05 925419970 DUP Result Result RPD Footnotes ND ND NC ND ND NC REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37712 •AC SC Environmental 99030 ....... Page: 50 of 56 Chirlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 Sc 9900i rl NFI AP rR7f97 Analytical www.pacelabs.com QUALITY CONTROL DATA QC Batch: 124181 QC Batch Method: EPA 353.2 Associated Lab Samples: 925423774 METHOD BLANK: 925426637 Associated Lab Samples: 925423774 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Phone: 704.875.9092 Fax.- 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Analysis Method: EPA 353.2 Analysis Description: 48 Hour NO3 / NO2 / NOX Blank Reporting Parameter Units Result Limit Footnotes Nitrate as N mg/l ND 0.10 Nitrite as N mg/l ND 0.10 LABORATORY CONTROL SAMPLE: 925426645 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Nitrate as N mg/l 5.000 5.000 100 MATRIX SPIKE: 925426652 925423774 Spike MS MS Parameter Units Result Conc. Result X Rec Footnotes Nitrate as N mg/l 0 5.000 3.400 68 1 SAMPLE DUPLICATE: 925426660 Parameter Units Nitrate as N mg/l Nitrite as N mg/l Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030^ 925426538 DUP Result Result RPD 0.3200 0.3100 3 ND ND NC Footnotes REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. P Page: 51 of 56 r NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FI AIGI AP FR7997 Analytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax.704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 QC Batch: 124199 Analysis Method: EPA 365.2 QC Batch Method: EPA 365.2 Analysis Description: Phosphorus, Total Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 METHOD BLANK: 925427361 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 Blank Reporting Parameter Units Result Limit Footnotes Phosphorus mg/l NO 0.100 LABORATORY CONTROL SAMPLE: 925427379 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Phosphorus mg/l 1.000 1.139 114 MATRIX SPIKE: 925427387 925426090 Spike MS MS Parameter Units Result Conc. Result % Rec Footnotes Phosphorus mg/l 8.948 1.000 9.935 99 SAMPLE DUPLICATE: 925427395 Parameter Units Phosphorus mg/l Date: 04/07/05 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl girl An rn70AO 925411688 DUP Result Result RPD Footnotes NO NO NC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 4"I �1 or Page: 52 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP FR7R)7 :?Analytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 10D Nuntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015.04-014 QC Batch: 124491 Analysis Method: EPA 325.2 QC Batch Method: EPA 325.2 Analysis Description: Chloride (Mercuric Nitrate) Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 METHOD BLANK: 925443087 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 925423774 Blank Reporting Parameter Units Result Limit Footnotes Chloride mg/l ND 5.0 LABORATORY CONTROL SAMPLE: 925443095 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Chloride mg/l 20.00 20.53 103 MATRIX SPIKE: 925443525 925420499 Spike MS MS Parameter Units Result Conc. Result % Rec Footnotes Chloride mg/l 38.91 20.00 52.34 67 2 SAMPLE DUPLICATE: 925443533 Parameter Units Chloride mg/l Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl \Irl An ro7CAo 925423626 DUP Result Result RPD Footnotes 15.00 15.00 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page: 53 of 56 harlotte Certifi NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 Analytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 QC Batch: 124493 Analysis Method: EPA 375.4 QC Batch Method: EPA 375.4 Analysis Description: Sulfate.Turbidimetric Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 METHOD BLANK: 925443160 Associated Lab Samples: 925423626 925423634 925423642 925423659 925423717 925423725 925423741 925423758 925423766 Blank Reporting Parameter Units Result Limit Footnotes Sulfate mg/l ND 5.0 LABORATORY CONTROL SAMPLE: 925443178 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Sulfate mg/l 20.00 20.34 102 MATRIX SPIKE: 925443186 925422511 Spike MS MS Parameter Units Result Conc. Result % Rec Footnotes Sulfate mg/l 281.6 20.00 305.3 118 SAMPLE DUPLICATE: 925443194 Parameter Units Sulfate mg/l Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI MCI AD CR7RAG 925422529 DUP Result Result RPD Footnotes 250.0 250.0 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. C �`rie�at Page: 54 of 56 harlotte Certification ID NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax.704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 QC Batch: 124494 Analysis Method: EPA 375.4 QC Batch Method: EPA 375.4 Analysis Description: Sulfate,Turbidimetric Associated Lab Samples: 925423774 METHOD BLANK: 925443202 Associated Lab Samples: 925423774 Blank Reporting Parameter Units Result Limit Footnotes Sulfate mg/l ND 5.0 LABORATORY CONTROL SAMPLE: 925443210 Spike LCS LCS Parameter Units Conc. Result X Rec Footnotes Sulfate mg/l 20.00 20.15 101 MATRIX SPIKE: 925443228 925423774 Spike MS MS Parameter Units Result Conc. Result % Rec Footnotes Sulfate mg/l 0 20.00 20.65 103 SAMPLE DUPLICATE: 925443236 Parameter Units Sulfate mg/l Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIFI AP 1:R7AAA 925426579 DUP Result Result RPD Footnotes 2800 2900 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Page: 55 of 56 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA PARAMETER FOOTNOTES Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone., 704.875.9092 Fax.' 704.875.9091 Lab Project Number: 9290570 Client Project ID: Fairchild 015-04-014 Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values. LCS(D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) DUP Sample Duplicate ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit RPD Relative Percent Difference (S) Surrogate Ill The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is acceptable. [21 The spike recovery was outside acceptance limits for the MS and/or MSD due to an analyte concentration in the sample at four times greater than the spike concentration. The QC batch was accepted based upon LCS and/or LCSD recoveries within acceptance limits. Date: 04/07/05 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI NFI AP FR7RAR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ..«o, e ■ ■VRAC Page: 56 of 56 harlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Subcontracted Results Pace Project # J,O� B q a9o57o This report includes page Ito I �5A .. O �N ACCpRO LfeystoneelME M 'B ifsINC. eg _ LABORATORIES, Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received 925423626/MW-1 15C1147-01 Water 03/22/0511:30 03/24/0511:00 925423634/MW-2 15C1147-02 Water 03/22/0511:51 03/24/0511:00 925423642/MW-5 15C1147-03 Water 03/22/0512:23 03/24/0511:00 925423659/6-R 15C1147-04 Water 03/22/0512:37 03/24/0511:00 925423717/MW-7 15C1147-05 Water 03/22/0513:21 03/24/0511:00 925423725/MW-8 15C1147-06 Water 03/22/0513:27 03/24/0511:00 925423741/MW-9 15C1147-07 Water 03/22/0514:20 03/24/0511:00 925423758/MW-10 15C1147-08 Water 03/22/0514:47 03/24/0511:00 925423766/MW-11 15C1147-09 Water 03/22/0514:25 03/24/0511:00 925423774/MW-13 15CII47-10 Water 03/22/0515:00 03/24/0511:00 Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jenny King, Ph.D., Laboratory Director Page I of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 ACCOgpq 'y MEMBER �feystone-mail LABORATORIES, INC. a Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423626/MW-1 15CII47-01(Water) Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.1 mg/l 1 1D50518 04/04/05 04/04/05 HPLC/UV Lactic Acid (0) ND 1.0 to to to to toto Acetic Acid (C2) ND 1.0 to to to to toto Propionic Acid (0) ND 1.0 of to to to toto Butyric Acid (C4) ND 1.0 to Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 2 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 ACCOgo stone 42c� MEMBER Lfey LABORATORIES, INC. Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423634[NM-2 15C1147-02 (Water) Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Note! Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) 7.3 1.0 mg/1 10 1D50735 04/07/05 04/07/05 HPLC/UV Lactic Acid (C3) 467 10.0 ti " " " " Acetic Acid (C2) 1570 10.0 " Propionic Acid (C3) 5030 10.0 " Butyric Acid (C4) 8820 10.0 " Keystone Laboratories, Inc. - Newton Jim Eggers For Jeffrey King, Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 3 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 `��n �N ACCpRO�y �feystone MEMBER a LABORfi TORIES, INC. nela Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423642/MW-5 15C1147-03 (Water) Rqmft Analyte Result Limit Units Nation Batch Prepared Analyzed Method Notts Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.5 mg/I 5 1D50735 04/07/05 04/07/05 HPLC/UV R-01 Lactic Acid (U) 6.1 5.0 R-01 Acetic Acid (C2) ND 5.0 R-01 Propionic Acid (C3) 6.6 5.0 R-01 Butyric Acid (C4) ND 5.0 R-01 Keystone Laboratories, Inc. - Newton The results m this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. sly Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 4 of is Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Lfeystone LABORATORIES, INC. MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423659/6-R 15C1147-04 (Water) Reporting Anal to Result Limit Units Dilution Batch Prepared Analyzed Method Note Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) Keystone Laboratories, Inc. - Newton ND 0.5 mg/l 5 ID50735 04/07/05 04/07/05 HPLC/UV R-01 ND 5.0 R-01 ND 5.0 R-01 ND 5.0 R-01 ND 5.0 R-01 Jim Eggers For Jeffrey King, Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Paee 5 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 1 Lfevstone MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 I5:33 925423717/MW-7 15C1147-05 (Water) Reporting Analytr Resuit Limit Units Dilution Batch Prepared Analyzed Method Not Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) ND 0.1 mg/1 1 1D50518 04/04/05 04/04/05 HPLC/UV ND 1.0 " ND 1.0 " ND 1.0 ^ " ND 1.0 ^ ^ Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 6 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 ��\��o �N �CCp9o�y�F Lfeystone MEMBER LABORATORIES, INC. a Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423725/MW-8 15C1147-06 (Water) Reporting ArWyte Result Limit Units Dilution Batch Prqared Analyzed Method Now Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.1 mg/1 1 1 D50518 04/04/05 04/04/05 HPLC/UV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 7 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 stone LABORATORIES, INC. apt ACcog0 q MEMBER nelalU Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423741/MW-9 15CII47-07 (Water) Reporting Analyte Result Limit units Dilution Batch Prepared Analyzed Method Notej Keystone Laboratories, Inc. -Newton Determination of Metabolic Acids Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) ND 0.1 mg/1 1 1D50518 04/04/05 04/04/05 HPLC/UV ND 1.0 ^ ND 1.0 ^ " ND 1.0 ^ ^ ND 1.0 ^ " Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 8 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Lfey \��O � N A C C p A�q2 stone Qp R �� MEMBER LABORATORIES, INC. _ Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423758/MW-10 15CII47-08 (Water) Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Note Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.1 mg/1 l 1D50518 04/04/05 04/04/05 HPLC/UV Lactic Acid (0) ND 1.0 " Acetic Acid (CZ) ND 1.0 " Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 9 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 ��\��O �N ACCpR�9yc� stone MEMBER LABORATORIES, INC. a-4 Inano-1-4 Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423766/MW-11 15CII47-09 (Water) Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Note Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.1 mg/1 1 1D50518 04/04/05 04/04/05 HPLC/UV Lactic Acid (0) ND 1.0 Acetic Acid (C2) ND 1.0 " Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 10 of 15 ��\��O N A C C p H�41P eystone MEMBER LABORATORIES, INC. Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 925423774/MW-13 15C1147-10 (Water) Reporting Anal a Result Limit Units Dilution Batch Prepared Analyzed Method Note Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) ND 0.1 mg/1 1 1D50518 04/04/05 04/04/05 HPLC/UV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) 93.7 1.0 " Propionic Acid (C3) 85.1 1.0 " Butyric Acid (C4) 30.6 1.0 " Keystone Laboratories, Inc. - Newton Jim Eggers For Jeffrev King_ Ph.D__ Laboratory Directnr The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 � \N ACCpq� stone �YMEMBER LABORATORIES, INC. Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 15D0509-1D50518 Calibration Check (15D0509-CCVI) Prepared & Analyzed: 04/04/05 Pyruvic Acid (0) 17.78 mg/l 15.00 119 80-120 Lactic Acid (0) 101.9 94.70 108 80-120 Acetic Acid (0) 113.7 103.0 110 80-120 Propionic Acid (0) 111.5 100.0 112 80-120 Butyric Acid (C4) 117.8 110.0 107 80-120 Calibration Check (15D0509-CCV2) Prepared: O4/04/05 Analyzed: 04/05/05 Pyruvic Acid (0) 16.97 mg/l 15.00 113 80-120 Lactic Acid (0) 104.4 94.70 110 80-120 Acetic Acid (0) 112.1 103.0 109 80-120 Propionic Acid (0) 99.67 100.0 99.7 80-120 Butyric Acid (C4) 112.8 110.0 103 80-120 Batch 15D0711 - 1D50735 Calibration Check (15D0711-CCVI) Prepared & Analyzed: 04/07/05 Pyruvic Acid (0) 15.54 mg/l 15.00 104 80-120 Lactic Acid (0) 95.38 94.70 101 80-120 Acetic Acid (C2) 109.8 103.0 107 80-120 Propionic Acid (0) 108.3 100.0 108 80-120 Butyric Acid (C4) 117.0 110.0 106 80-120 Calibration Check (15D0711-CCV2) Prepared & Analyzed: 04/07/05 Pyruvic Acid (0) 15.99 mg/l 15.00 107 80-120 Lactic Acid (0) 97.62 94.70 103 80-120 Acetic Acid (C2) 104.3 103.0 101 80-120 Propionic Acid (0) 108.7 100.0 109 80-120 Butyric Acid (C4) 114.7 110.0 104 80-120 Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 12 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 \ N A C C p Ro�2 Qa o MEMBER Lfeystone LABORATORIES, INC, a Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 1D50518 - General Prep HPLC/IC Blank (1D50518-BLKI Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) ND 0.1 mg/I ND 1.0 " ND 1.0 " ND 1.0 " ND 1.0 " & Analyzed: 04/04/05 LCS (ID50518-BSI) Prepared & Analyzed: 04/04/05 Pyruvic Acid (0) 24.98 0.1 mg/l 22.00 114 72-137 Lactic Acid (0) 114.5 1.0 112.2 102 72-122 Acetic Acid (C2) 106.7 1.0 102.0 105 88-126 Propionic Acid (0) 107.9 1.0 102.0 106 90-117 Butyric Acid (C4) 125.6 1.0 105.8 119 86-120 Matrix Spike (1D50518-MS1) _ Source:_ 15D0035-09 Prepared & Analyzed: 04/04/05 Pyruvic Acid (0) 21.96 0.1 mg/I 22.00 ND 99.8 67-140 Lactic Acid (0) 107.1 1.0 112.2 0.9 94.7 64-144 Acetic Acid (C2) 137.4 1.0 102.0 29.7 106 79-140 Propionic Acid (0) 139.5 1.0 102.0 24.1 113 75-139 Butyric Acid (C4) 114.6 1.0 105.8 10.0 98.9 79-128 Matrix Spike Dup (1D50518-MSD1) Source: 15D0035-09 Prepared & Analyzed: 04/04/05 Pyruvic Acid (0) 22.95 0.1 mg/I 22.00 ND 104 67-140 4.41 12 Lactic Acid (0) 102.7 1.0 112.2 0.9 90.7 64-144 4.19 19 Acetic Acid (C2) 135.8 1.0 102.0 29.7 104 79-140 1.17 19 Propionic Acid (0) 128.9 1.0 102.0 24.1 103 75-139 7.90 15 Butyric Acid (C4) 119.7 1.0 105.8 10.0 104 79-128 4.35 22 Keystone Laboratories, Inc. - Newton Jim Eggers For Jeffrey King, Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 13 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 �o`��Q \N ACCp�D�ycE Lfey stone MEMBER LABORATORIES, INC. Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD Analyte Result Limit Units Levd Result °/6REC Limits RPD Limit Notes Batch lD50735 - General Prep HPLOIC Blank (1D50735-BLKI) Prepared & Analyzed: 04/07/05 Pyruvic Acid (0) ND 0.1 mgA Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 " Propionic Acid (C3) ND 1.0 " Butyric Acid (C4) ND 1.0 " LCS (1D50735-BSI) Prepared & Analyzed: 04/07/05 Pyruvic Acid (0) 25.39 0.1 mg/1 22.00 115 72-137 Lactic Acid (0) 103.7 1.0 112.2 92.4 72-122 Acetic Acid (C2) 105.2 1.0 102.0 iO3 88-126 Propionic Acid (M) 105.6 1.0 " 102.0 104 90-117 Butyric Acid (C4) 109.7 1.0 105.8 104 86-120 Matrix Spike (1D50735-MS1) Source: ISC1247-01 Prepared & Analyzed: 04/07/05 _ Pyruvic Acid (0) 25.24 0.1 mg/1 22.00 ND 115 67-140 Lactic Acid (0) 101.2 1.0 112.2 ND 90.2 64-144 Acetic Acid (0) 103.3 1.0 102.0 ND 101 79-140 Propionic Acid (M) 109.6 1.0 102.0 ND 107 75-139 Butyric Acid (C4) 106.7 1.0 105.8 ND 101 79-128 Matrix Spike Dup (1D50735-MSDI) Source: 15C1247-01 Prepared & Analyzed: 04/07/05 Pyruvic Acid (0) 25.96 0.1 mg/1 22.00 ND 118 67-140 2.81 12 Lactic Acid (0) 104.5 1.0 112.2 ND 93.1 64-144 3.21 19 Acetic Acid (C2) 102.1 1.0 102.0 ND 100 79-140 1.17 19 Propionic Acid (0) 102.2 1.0 102.0 ND 100 75-139 6.99 15 Butyric Acid (C4) 107.2 1.0 105.8 ND 101 79-128 0.468 22 Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Jim Eggers For Jeffrey King, Ph.D., Laboratory Director Page 14 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Lfeystone �o\��N A C C pR�g2�F MEMBER Q � . U LABORATORIES, INC. Q _ Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 9290570 Reported: Huntersville NC, 28078 Project Manager: Bonnie Kamla 04/07/05 15:33 Notes and Definitions R-01 The Reporting Limit for this analyte has been raised to account for matrix interference. DET Analyte DETECTED ND Aalyte NOT DETECTED at or above the reporting limit NR Not Reported dry Sample results reported on a dry weight basis RPD Relative Percent Difference Keystone Laboratories, Inc. - Newton Jim Eggers For Jeffrey King, Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety. Page 15 of 15 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 .;r v-� �� v �,�yl utlowu ��q■■, aceAnalytical ® The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields-musttbee completed accurately. -Al 883666 www.pacelabs.com Required Client Information: Section B Page: Of / Report To: n r Required Client Information: Section A To Be Completed by Pace Analytical and Client Section C Company L I AA Copy To: } `tif Glent Information (Check Quote Reference: U v 7 quotalcontract): Address J r Invoice To• Requested Due Dale: •TAT: Project Manager. P.O. *Turn around time lass than 14 days subject to Project #: laboratory and contractual obligations and may result in a N Project Name, A t C� Rush Turnaround Surcharge. Turn Around Time (TAT) in calendar days. Profile P. j 7 — c ta• P one n — F r` t l Project N r: / t L Requested Anetyale: . Section D R uired Client Information: eQ valid codes MATRIX � SSE a Preservatives DRINKING WATER DW - GROUNDWATER GW SURFACE WATER SW w o wM a.o �:1 o_ Z w20 F '+ I SAMPLE I D WASTE WATER WW V wU f. U w t One character per box. PRODUCT IL SL OIL OL . ¢ < a. a Q COLLECTED a O V Z a) m co O START END W _ (A-Z, O-9l . Sample IDS; MUST BE UNIQUE p WIPE WP AIR AR OTHER OT i cl)0 U_ in ~ f< c � O _= — = O Z N Z L i m O y L Remarks I Lab ID DATE TIME DATE nME — 2 o f I C3C� 3- j f 3�G k X X y x Z t I X G3 32) 32 - ? 13� > 13� 1K Y x x k •r y ? - G - 1420 36 1` 9Q H K K `� 4 Z �1 y- 3 �4 : 14+� u_ YJ y Y k x71 X ,r i G ��a/, . I V�� : >'�� �:.- f ,—�c� (� y x r� k x r y ,� x 1 4� Other — SAMPLE Temp in °C i Received on Ic Y/N Sealed Cooler Y/' Samples Intact f WN Additional Comments: 4 .■h r I?AU I v to A WO r SIGNAT E ofSAMPLmh DATE Signed: (MM / DID / YY) 0 SEE RE RSE SIDE FOR STRUCTIONS Form C0001 Rev. 0304 1 Trigon Services • Geotechnical Engineering • Construction Materials Engineering/Testing • Roof Engineering/Inspection • Forensic Engineering • Environmental Audits/Site Assessments • Environmental Drilling • Groundwater Studies/Remediation • Stormwater Permitting • Wastewater Engineering • Water Treatment Design • Health & Safety Consulting • Regulatory Compliance Engineering • Waste Minimization Studies • Air Quality Consulting • Atmospheric Computer Dispersion Modeling • Stack Testing and Continuous Emissions Monitoring • Indoor Air Monitoring • Asbestos and Lead -based Paint Inspections • Pollution Prevention Plans OFFICE LOCATIONS Greensboro Raleigh Charlotte North Carolina North Carolina North Carolina 336-668-0093 919-755-5011 704-598-1049 Greenville South Carolina 864-297-3557