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HomeMy WebLinkAboutWI0400035_Monitoring (Report)_20060220Quarterly HRC Monitoring Report Fairchild Industrial Products Company Winston-Salem, North Carolina Trigon Project No. 042-05-154 ENGINEEKINQ CONSULTANTS, INC. Since 1983 www.bigfone,ag'.com P.O. Box 18846 - Zip 27419-8846 • 313 Gallimore Dairy Road • Greensboro, NG 27409 ■ p 336.568.0093 - f 336 568.3868 February 20, 2006 Mr. J. Michael Ranck UIC Program Aquifer Protection Section North Carolina DENR - DWQ 1636 Mail Service Center Raleigh, North Carolina 27699-1636 Reference: Quarterly HRC Monitoring Report Fairchild Industrial Products Company Winston-Salem, North Carolina Trigon Project No. 042-05-154 Dear Mr. Ranck: Trigon Engineering Consultants, Inc. (Trigon) is pleased to provide this quarterly monitoring report for the Underground Injection Control (UIC) Permit for treatment of groundwater with Hydrogen Release Compound (HRC) at the referenced site. Enclosed is a copy of the report for your review. Should you have any questions regarding this information, please do not hesitate to contact our office. Very truly yours, TRIGON ENGINEERING CONSULTANTS, INC. 00oaeeeeee�e�o��e Lo CA '9d. E �• Christopher W. y, E.I. ewa , Engineering Manageregi erecgiAkogiste o m CWH/JMS:mes ✓ ;c��� ®p® OLdd Attachments B pe eaAf SA��Qies� h:104201projects120051154 W205154.doc TAank you for our success. Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 042-05-154 TABLE OF CONTENTS 1.0 SITE BACKGROUND..........................................................................................................................1 2.0 RECEPTOR SURVEY...........................................................................................................................2 3.0 HRC INJECTION..................................................................................................................................2 4.0 HRC MONITORING ACTIVITIES......................................................................................................4 5.0 GROUNDWATER ANALYTICAL RESULTS....................................................................................5 6.0 CONCLUSIONS AND RECOMMENDATIONS.................................................................................6 TABLES 1 Monitoring Well Construction Details 2 Historical Groundwater Table Elevations 3 Field Analysis Summary 4 Groundwater Analytical Summary (Volatile Organic Acids) 5 Historical Groundwater Analytical Summary (VOCs) FIGURES 1 Site Location Map 2 Surrounding Property Owners Map 3 HRC Injection Locations 4 Shallow Groundwater Map — January 5, 2006 5 Tetrachloroethene Isoconcentration Map — January 5, 2006 APPENDIX A Well Construction Forms B Laboratory Report and Chain -of -Custody Document TRIGON ENGINEERING CONSULTANTS, INC. Page i Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 042-05-154 1.0 SITE BACKGROUND The street address of the site is 3920 Westpoint Boulevard in the Westpoint Business Park, Winston- Salem, Forsyth County, North Carolina. The site is located on the south side of Westpoint Boulevard and east of Viceroy Drive (Figure 1). Fairchild Industrial Products Company, who leases the property from Highwoods/Forsyth Partnership Limited, currently occupies the building. Trigon Engineering Consultants, Inc. (Trigon) conducted a Comprehensive Site Assessment (CSA), dated December 11, 1998, which concluded that the volatile organic compounds (VOCs) tetrachloroethene or perchloroethene (PCE), trichloroethene (TCE), cis-1,2-dichloroethene (cis-1,2- DCE), and toluene were detected in soils near the source area. VOCs were detected above North Carolina Title 15A NCAC 2L groundwater standards (NCGWS) in monitoring wells MW-1, MW-2, MW-3, MW-4, and MW-6. A Corrective Action Plan (CAP) proposing the application of Hydrogen Release Compound (HRC) was prepared to address these constituents. No free product was encountered at the site during the CSA. Both Forsyth County Tax Maps and the 1950 USGS Winston-Salem West Quadrangle indicate a tributary of Salem Creek formerly crossed the western and southern portions of the site flowing to the southeast. No surface water is currently located within 500 feet of the source area. Buried water, power, and natural gas lines are located along the eastern side of Viceroy Drive running north to south. However, none of these utilities are suspected conduits of contaminant migration or vapor accumulation. The North Carolina Department of Environment and Natural Resources (NCDENR) Groundwater Section approved the CAP in May 2001. The goal of the CAP was to provide details for the remediation of PCE by assuring that known and foreseeable pathways are monitored while natural degradation occurs. The preferred remedial alternative to address soil contamination in the source area was soil vapor extraction (SVE). A SVE system was installed and operated at the site from July 2000 through June 2001. The preferred remedial alternative to address groundwater contamination was the application of HRC. ejTRIGON ENGINEERING CONSULTANTS, INC. Page I Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 042-05-154 2.0 RECEPTOR SURVEY On September 29, 1998, Trigon completed a limited well survey of the site area. The limited well survey reconnaissance consisted of viewing the properties within 1,500 feet of the subject site and talking to available property owners. Water meters were identified at properties having public water service. Two water supply wells were identified within 1,500 feet of the source area. One of the water supply wells is actively used. The other water supply well is not actively used since the home was connected to municipal water. In November 2005, Trigon updated the well survey by conducting a field reconnaissance of properties and mailing letters to the property owners within 500 feet downgradient of the site. Letters were sent to five property owners by registered mail. No water supply wells were identified within 1,500 feet downgradient of the site. The locations of the water supply wells identified are shown on Figure 1. Based on the locations of the wells identified, they are not anticipated to be impacted by contaminants at the site. Figures 1 and 2 include copies of the USGS Winston-Salem West Quadrangle and a Forsyth County Tax Map, respectively. Both figures indicate that a drainage feature previously crossed the site. The drainage feature is not presently visible at the site or immediately south of the site. Land use in Westpoint Business Park is primarily commercial and industrial. The majority of the properties in the business park are zoned GI. Zone GI is defined as general industrial. The site is bound to the north by Westpoint Boulevard, to the east by Annapolis Drive, to the south by Sides Mobile Home Court, and to the west by Viceroy Drive. Land use surrounding the business park is primarily residential. 3.0 HRC INJECTION Trigon requested a permit from the Underground Injection Control (UIC) Program of the Division of Water Quality to inject HRC for remediation of groundwater contamination identified during the CSA. The original UIC Program permit expired September 30, 2003. The HRC application plan included taking groundwater samples prior to application of HRC to provide baseline contaminant levels, drilling TRIGON ENGINEERING CONSULTANTS, INC. Page 2 Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 042-05-154 injection wells, injecting seven to eleven pounds of HRC per vertical foot in each well, and conducting remedial monitoring. In August 2001, Trigon initialized the first round of HRC injection. HRC injection locations included twenty-nine injection points (IP-1 through IP-29) and six injection wells (IW-1 through IW-6) shown on Figure 3. Four injection points (IP-1 through IP-4) and six injection wells (IW-1 through IW-6) were drilled inside the facility to depths ranging between 24.5 and 35.0 feet below the ground surface. Seven pounds of HRC per vertical foot were placed in each borehole and injection well inside the facility. Ten injection points (IP-5 through IP-14) were drilled in the parking area downgradient of MW-6 and upgradient of MW-7 to depths of approximately 30 feet below the ground surface. Seven pounds of HRC per vertical foot was placed in each borehole. Fifteen injection points (IP-15 through IP-29) were drilled upgradient of the source area to depths ranging between 23 and 35 feet below the ground surface. Eleven pounds of HRC per vertical foot were placed in injection points IP-15 through IP-29. Five quarters of groundwater sampling and corrective action monitoring were completed following the injection of HRC into groundwater at the site. Following the November 2002 sampling event, Trigon recommended additional HRC application in the vicinity of MW-9, MW-10, MW-13, and MW-7. Trigon requested a second permit from the Underground Injection Control (UIC) Program of the Division of Water Quality to inject additional HRC. The new UIC Program permit remains effective through November 30, 2006. The HRC application plan included converting monitoring wells MW-6, MW-14, and MW-15 into injection wells, drilling additional injection wells, injecting seven pounds of HRC per vertical foot in each well, and conducting remedial monitoring. On March 11, 2004, Trigon mobilized to the site to begin the installation of the additional injection wells and points. HRC injection locations included twenty-one injection points (IP-30 through IP-50), three new injection wells (IW-7, IW-8, and IW-9), and the conversion of existing monitoring wells (MW-6, MW-14, and MW-15) to injection wells (IW-10, IW-11, IW-12). The locations are shown on Figure 3. Fifteen injection points (IP-30 through IP-44) and six injection wells (IW-7 through IW-12) were drilled inside the facility to depths ranging between 25 and 35 feet below the ground surface. Seven pounds of HRC per vertical foot was placed in each borehole with the exception of IW-10 and IW-11 in which four pounds of HRC per vertical foot were placed. Six injection points (IP-45 through IP-50) were drilled in the parking area downgradient of MW-6 and upgradient of MW-7 to depths of 40.0 feet below the TRIGON ENGINEERING CONSULTANTS, INC. Page 3 Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston -Sakes, North Carolina Trigon Project No. 042-05-154 ground surface. Seven pounds of HRC per vertical foot were placed in each borehole. HRC injection was completed in March of 2004. Six quarters of groundwater sampling and corrective action monitoring have been completed following the second HRC injection event. 4.0 HRC MONITORING ACTIVITIES Two new deep groundwater monitoring wells (DW-18 and DW-19) were installed in December 2005, to further delineate the vertical extent of the contaminant plume (Figure 3). Well construction forms for DW-18 and DW-19 are included in Appendix A. Static water levels were recorded in all of the monitoring wells on -site between January 5 and 6, 2006. Groundwater samples were collected from fourteen monitoring wells (MW-1, DW-2, MW-5, MW-6R, MW-7, MW-8, MW-9, MW-10, MW-11, MW-13, DW-16, DW-17, DW-18, and DW-19) and analyzed for VOCs. Additionally, monitoring wells MW-6R, MW-7, MW-9, MW-10, MW-11, MW-13, DW-17, and DW-18 were analyzed for metabolic acids. Field parameters including dissolved oxygen, oxidation- reduction potential (ORP), pH, conductivity, and temperature of representative groundwater samples were also recorded from each monitoring well sampled. Groundwater elevations in the existing monitoring wells were used to determine the groundwater flow direction, average hydraulic gradient, vertical hydraulic gradient, and plume orientation. Table 1 provides a summary of monitoring well construction details and groundwater elevations measured on January 5 and 6, 2006. Historical groundwater table elevation measurements are summarized in Table 2. The static water levels measured on January 5 and 6, 2006 between monitoring wells MW-1 and MW-7 indicate a horizontal groundwater flow gradient of 0.03 foot per foot to the southeast. Static water levels measured in monitoring wells MW-1 and DW-2 indicate a vertical groundwater gradient of 0.008 foot per foot downward. Static water levels measured in monitoring wells MW-10 and DW-16 indicate a vertical groundwater gradient of 0.004 foot per foot upnward. Static water levels measured in monitoring wells MW-6R and DW-19 indicate a vertical groundwater gradient of 0.05 foot per foot downward. A groundwater flow map of the shallow aquifer based on the January 5 and 6, 2005 groundwater elevations is shown on Figure 4. In -situ aquifer tests performed on shallow monitoring wells at the site during the CSA indicated that the surficial aquifer has an average hydraulic conductivity of 1.2 feet per day. The average groundwater TRIGONENGINEERING CONSUL7AN7S, INC. Page 4 Mr. Louis Schaab, Allied Capital Corporation February 20, 2006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 042-05-154 velocity is estimated to be 0.12 feet per day (44 feet per year), based on the average groundwater gradient from the January 5 and 6, 2005 water level measurements and an estimated effective porosity of thirty percent. Groundwater samples were collected from the monitoring wells on January 5 and 6, 2005. The wells were first purged of one to two well volumes of water, or until dry, at a low flow rate with a peristaltic pump. After allowing the wells to recharge, groundwater samples were collected and placed in laboratory prepared containers. The groundwater samples were maintained on ice until delivered to Pace Analytical in Huntersville, North Carolina. The samples were analyzed for VOCs by Method 8260 and metabolic acids to monitor contaminant levels at the site and metabolism of HRC. 5.0 GROUNDWATER ANALYTICAL RESULTS The groundwater field analysis generally indicates that the subsurface environment is within acceptable limits for biodegradation to occur. Conductivity is recorded for quality control and sampling consistency. The field measurements recorded on January 5 and 6, 2006 are summarized in Table 3, which includes the preferred conditions for natural biodegradation of chlorinated compounds within the groundwater plume. Groundwater sample analytical results indicate that volatile organic acids were detected in seven of the eight water samples collected on January 5, 2006. Volatile organic acids or metabolic acids indicate the presence and metabolism of HRC. Analytical results for volatile organic acids are summarized in Table 4. Groundwater sample analytical results indicate that several VOCs were detected in the monitoring wells sampled. PCE was detected at levels exceeding the state groundwater standard in monitoring wells DW- 2, MW-6R, MW-7, MW-8, MW-9, MW-10, MW-11, DW-16, DW-17, DW-18, and DW-19. PCE concentrations in monitoring wells in DW-2, MW-8, MW-9, MW-10 and MW-11 increased since the previous sampling event. PCE concentrations in monitoring wells MW-6R, MW-7, DW-16, and DW-17 decreased since the previous sampling event. A PCE isoconcentration map is shown on Figure 5. TCE was detected at levels exceeding the state groundwater standard in monitoring wells MW-6R, MW7, TRIGONENGINEER/NGCONSULTANTS, INC. Page 5 Mr. Louis Schaab, Allied Capital Corporation February 10, 1006 Fairchild Industrial Products Company, Winston-Salem, North Carolina Trigon Project No. 041-05-154 MW-9, MW-10, MW-11, DW-16, DW-17, DW-18, and DW-19. Cis-1,2-DCE was detected at levels exceeding the state groundwater standard in monitoring wells in MW-9, MW-13, DW-16, and DW-17. Vinyl Chloride was detected at a level exceeding the state groundwater standard in monitoring well MW- 9 and DW-16. A summary of historical VOC analytical results is provided in Table 5. A copy of the analytical results including the chain -of -custody form is included in Appendix B. 6.0 CONCLUSIONS AND RECOMMENDATIONS In general, the most definitive evidence of biodegradation of contaminants in groundwater is the reduction in contaminant concentrations and the presence of the constituents into which the contaminants degrade. PCE concentrations in monitoring wells DW-18 and DW-19 are within the same order of magnitude as the other wells at the site. The presence of daughter products of dechlorination of PCE in monitoring wells MW-6R, MW-7, MW-9, MW-10, MW-11, DW-16, DW-17, DW-18, and DW-19 also indicates degradation is occurring. Metabolic acid concentrations in monitoring wells MW-6R, MW-7, MW-9, MW-10, MW-11, MW-13, DW-16, and DW-18 indicate that HRC is influencing the subsurface environment in the vicinity of each of the monitoring wells with elevated contaminant levels. Based on the results of the monitoring event, we recommend the continuation of corrective action monitoring on a quarterly schedule. The next monitoring event should be scheduled for mid -March 2006. In addition, we recommend that additional extended life HRC be purchased for injection in the existing injection wells in the vicinity of MW-6R, MW-9, MW-10, and MW-11. This will accelerate the degradation of contaminants in the center of the contaminant plume. Copies of this report have been mailed to the Aquifer Protection in the NCDENR Winston-Salem Regional Office and the UIC Program in Raleigh, North Carolina. TRIGON ENGINEERING CONSULTANTS, INC. Page 6 TABLES Mr. Louis Schaab, Allied Capital Corporation Fairchild Industrial Products Company, Winston-Salem, North Carolina February 20, 2006 Trigon Project No. 042-05-I54 TABLE 1: MONITORING WELL CONSTRUCTION DETAILS Monitoring Well Date Constructed Total Depth feet b s Screened Interval feet b s Depth to Groundwater feet TOC Top of Casing Elevation 100' Datum Groundwater Elevation 100' Datum MW-1 Se tember-98 27.37 12.37 - 27.37 18.47 94.42 75.95 DW-2 October-98 43.34 38.34 - 43.34 18.30 94.09 75.79 MW-3 Se tember-98 22.32 12.32 - 22.32 17.15 98.17 81.02 MW-4 Se tember-98 18.65 8.65 - 18.65 18.68 91.38 72.70 MW-5 Se tember-98 25.11 15.11 - 25.11 17.27 87.07 69.80 MW-6R March-04 34.40 14.40 - 34.40 22.55 91.55 69.00 MW-7 November-98 26.56 11.56 - 26.56 22.46 86.81 64.35 MW-8 November-98 26.70 16.70 - 26.70 22.16 89.25 67.09 MW-9 March-99 24.41 9.41 - 24.41 18.54 94.24 75.70 MW-10 March-99 29.52 14.52 - 29.52 20.31 94.09 73.78 MW-11 Ma -99 24.12 9.12 - 24.12 19.10 94.31 75.21 MW-12 Ma -99 25.70 5.70 - 25.70 18.84 94.28 75.44 MW-13 June-99 33.46 8.46 - 33.46 21.49 94.22 72.73 DW-16 October-05 35.00 29.50 - 35.00 20.07 93.89 73.82 DW-17 October-05 26.50 21.50 - 26.50 20.03 93.82 73.79 DW-18 December-05 32.50 27.50 - 32.50 19.76 87.5 67.74 DW-19 December-05 54.80 49.80 - 54.80 19.74 87.46 67.72 feet bgs = Feet below ground surface feet TOC = Feet below top of well casing 100' Datum = Well casings were surveyed to an arbitrary 100 foot Datum. The benchmark is the center of the manhole cover at the south end of Viceroy Street. Note: Static Water Levels were measured January 5 and 6, 2006. MW-6, MW-14, and MW-15 were converted to injection wells IW-12, IW-10, and IW-11, respectively. TRIGON ENGINEERING CONSULTANTS, INC. Mr. Louis Schaab, Allied Capital Corporation Fairchild Industrial Products Company, Winston-Salem, North Carolina TABLE 2: HISTORICAL GROUNDWATER TABLE ELEVATIONS February 20. 2006 Trigon Project No. 042-05-154 Monitoring Well 06/18/99 08/24/00 11/16/01 02/26/02 05/01/02 08/13/02 11/20/02 06/09/04 09/09/04 12/09/04 03/22/05 06/09/05 09/28/05 10/24/05 01/05/06 MW-1 77.24 75.84 73.92 73.32 73.13 72.68 72.87 77.62 77.21 76.87 77.07 77.40 76.19 --- 75.95 DW-2 77.09 75.77 73.75 73.15 72.93 72.23 72.61 77.47 76.90 76.60 76.79 76.98 76.08 --- 75.79 MW-3 83.23 81.57 79.34 78.89 78.74 77.97 78.26 83.36 82.31 81.95 82.56 82.64 81.32 81.02 MW-4 73.10 DRY DRY DRY DRY DRY 72.77 DRY 73.83 73.49 73.67 73.92 73.24 72.70 MW-5 67.87 67.30 65.05 65.08 65.08 64.58 65.56 69.27 68.35 72.88 69.15 69.08 68.45 --- 69.80 MW-6R --- --- --- --- --- --- --- 69.76 69.59 1 69.27 69.25 69.46 68.94 --- 69.00 MW-7 64.36 63.35 61.90 61.56 61.36 60.93 61.82 64.90 64.71 64.49 64.52 64.59 64.18 --- 64.35 MW-8 67.53 66.54 64.99 64.42 64.29 64.87 64.28 68.19 67.94 67.58 67.55 67.76 67.33 --- 67.09 MW-9 76.78 75.64 73.26 72.60 72.40 71.84 72.24 77.07 76.63 76.26 76.38 76.74 74.08 --- 75.70 MW-10 74.58 73,29 71.46 70.87 70.61 69.99 70.40 74.81 74.69 74.25 74.38 74.70 76.20 --- 73.78 MW-11 76.00 74.92 72.90 72.28 72.09 1 71.60 71.91 76.71 76.29 75.97 76.01 75.22 75.73 --- 75.21 MW-12 76.57 74.46 73.28 72.73 72.54 71.92 72.25 77.02 76.44 1 76.09 76.33 76.34 73.06 --- 75.44 MW-13 72.84 71.57 69.71 69.16 68.91 68.37 68.77 73.50 73.41 73.27 73.41 73.64 73.04 --- 72.73 DW-16 --- --- --- --- --- --- --- --- --- --- --- --- --- 73.91 73.82 DW-17 --- --- --- --- --- --- --- --- --- --- --- --- 73.94 73.79 D W-18 --- --- --- --- --- --- --- --- --- - --- --- 67.74 DW-19 -- --- --- --- --- --- --- --- --- --- --- --- --- 67.72 Elevations are relative to an established benchmark on -site with an assumed elevation of 100.00 feet. Note: MW-6R was installed in March of 2004 to replace MW-6. TIUGON ENGINEERING CONSUL 7AN7S, INC. Mr. Louis Schaab, Allied Capital Corporation Fairchild Industrial Products Company, Winston-Salem, North Carolina TABLE 3: FIELD ANALYSIS SUMMARY February 10, 1006 Trigon Project No. 041-05-154 Monitoring Well Sample Date (°C) Temp PH Conductivity S/m (mV) Redox Preferred Conditions > 200C 5<pH<9 -- <50 mV MW-1 01/06/06 15.70 6.8 953 -56.7 DW-2 01/06/06 16.23 6.5 479 -9.2 MW-5 01/05/06 14.15 6.6 128 208 MW-6R O1/05/06 17.21 6.4 363 85 MW-7 01/05/06 17.11 6.4 268 165 MW-8 01/05/06 19.16 6.4 337 226 MW-9 01/05/06 20.08 6.2 540 63.8 MW-10 01/05/06 20.58 6.8 238 122 MW-11 01/05/06 19.62 6.7 179 180.4 MW-13 01/05/06 20.32 6.5 1,047 -57.4 MW-16 01/05/06 20.39 6.4 643 -29.8 MW-17 01/05/06 20.50 6.4 703 -32.2 MW-18 01/05/06 19.41 7.1 554 192 MW-19 01/05/06 18.29 6.2 272 246.5 Redox = oxidation-reduction potential °C = degrees Celsius S/m = siemens per meter mg/l = milligrams per liter, analogous to parts per million mV = millivolts Note: Conductivity is measured for consistency in groundwater sample collection. Dissolved oxygen readings were not recorded due to equipment failure. TRIGON ENGINEERING CONSULTANTS, INC. Mr. Louis Schaab, Allied Capital Corporation Fairchild bulustrial Products Company, Winston-Salem, North Carolina February 20, 2006 Trigon Project No. 042-05-154 TABLE 4: GROUNDWATER ANALYTICAL SUMMARY (VOLATILE ORGANIC ACIDS) Monitoring Well Analytical Results m Sampling Date Pyruvic Acid Lactic Acid Acetic Acid Pro ionic Acid Bu ric Acid MW-1 11/27/01 <0.1 <1.0 5.3 17.9 <1.0 02/26/02 <0.1 <1.0 141 207 51 05/01/02 1.8 <1.0 296 482 113 08/12/02 <0.1 <1.0 241 578 18.6 11/20/02 0.7 7.7 680 1,430 141 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 1 1.1 1 <1.0 I <1.0 I <1.0 12/09/04 1.1 1 <1.0 I <1.0 I <1.0 I <LO 03/22/05 <0.1 I <1.0 I <1.0 I <1.0 I <1.0 DW-2 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 <0.1 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 12.7 7 31.8 11/20/02 <0.1 <1.0 41.3 24.8 4.3 06/09/04 0.2 147 511 1,040 607 09/09/04 3.3 153 791 1 1,670 2,300 12/09/041 1.9 1 200 1,130 1 3,770 7,390 03/22/051 7.3 1 467 1„570 5,030 8,820 MW-3 11/28/01 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 1.8 4.7 9.9 10.4 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 MW-5 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 1.5 <1.0 <1.0 <1.0 <1.0 08/13/02 0.7 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 5.8 1.5 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 1 6.1 1 <1.0 1 6.6 <1.0 MW-6R 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 3.9 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/05 0.6 <1.0 <1.0 <1.0 <1.0 09/28/05 2.7 2.3 <1.0 <1.0 <1.0 01/05/06 0.8 1 <1.0 I <LO I <1.0 I <1.0 MW-7 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.3 <1,0 <1.0 <1.0 <1.0 11/20/02 <0.2 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 <1.0 1.8 2.7 <1.0 12/09/04 <0.1 7.4 <1.0 <1.0 <1.0 03/22/05 <0.1 I <1.0 I <1.0 I <1.0 I <1.0 09/28/05 2.6 1 <1.0 I <1.0 I <1.0 <1.0 01/05/06 1.0 <1.0 <I.0 <1.0 <1.0 MW-8 03/22/05 <0.1 I <1.0 I <1.0 I <1.0 I <1.0 mg/1= milligrams per liter, analogous to parts per million Note: Concentrations in bold type exceed detection limits. TRIGON ENGINEERING CONSULTANTS, INC. Mr. Louis Schaab, Allied Capital Corporation Fairchild Industrial Products Con parry, Winston-Salem North Caroluta February 20, 2006 Trigon Project No. 042-05-I54 TABLE 4: GROUNDWATER ANALYTICAL SUMMARY (VOLATILE ORGANIC ACIDS) (CONTINUED) Monitoring Well Analytical Results (m ) Sampling Date I Pyruvic Acid Lactic Acid Acetic Acid Pro ionic Acid Butyric Acid MW-9 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.8 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.2 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 1.6 3.2 <1.0 09/09/04 2.0 3.9 11.3 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 2.0 1.3 03/22/05 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/05 <0.1 <1.0 <1.0 <1.0 <1.0 09/28/05 3.0 <1.0 1.0 <1.0 <1.0 01/05/06 0.8 <1.0 <1.0 <1.0 <1.0 MW-10 11/27/01 <0.1 <1.0 <1.0 9.5 <1.0 02/26/02 <0.1 <1.0 59.1 118 <1.0 05/01/02 1.4 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 1.1 <1.0 <1.0 <1.0 09/09/04 <0.1 <L0 <1.0 <1.0 <1.0 12/09/04 <0.I <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/05 <0.1 <1.0 <1.0 <1.0 <1.0 09/28/05 3.0 <1.0 <1.0 <1.0 <1.0 01/05/06 1.0 <1.0 <1.0 <1.0 <1.0 MW-11 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 0.2 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 09/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 12/09/04 <0.1 <1.0 <1.0 <1.0 <1.0 03/22/05 <0.1 <I.0 <1.0 <1.0 <1.0 06/09/05 <0.1 <I.0 <1.0 <1.0 <1.0 09/28/05 3.1 <1.0 <1.0 <1.0 <1.0 01/05/06 1.4 <1.0 <1.0 <1.0 <1.0 MW-13 11/27/01 <0.1 <1.0 <1.0 <1.0 <1.0 02/26/02 <0.1 <1.0 <1.0 <1.0 <1.0 05/03/02 <0.1 <1.0 <1.0 <1.0 <1.0 08/13/02 <0.1 <1.0 <1.0 <1.0 <1.0 11/20/02 <0.1 <1.0 <1.0 <1.0 <1.0 06/09/04 <0.1 2.6 15.8 20.4 8.7 09/09/04 0.9 15.7 96.1 103 35.1 12/09/04 <0.1 <1.0 129 122 35.1 03/22/05 <0.1 <1.0 93.7 85.1 30.6 06/09/05 0,7 <1.0 123 82.6 9.5 09/28/05 2.3 <1.0 91.3 87.8 7.2 01/05/06 DA <1.0 66.3 59.1 2.7 DW-16 10/24/05 1.8 1 <1.0 112 24.2 22.2 DW-17 10/24/05 <0.1 1 <1.0 15.4 11.0 <1.0 01/05/061 <0I I <0.1 I <0.1 I <0.1 I <0.I DW-18 01/05/06 0.8 1 <0.1 <0.1 <0.1 <0.1 mg/I = milligrams per liter, analogous to parts per million Note: Concentrations in bold type exceed detection limits. TRIGON ENGINEERING CONSULTAN7S. INC. Mr. Lands Schaah, Allied Capital Corporation Fairchild Industrial Products Company, Winston-Salem, North Carolina Febmary 20, 2006 Trigon Project No. 042-05-154 TABLE 5: HISTORICAL GROUNDWATER ANALYTICAL SUMMARY (VOCs) Sampling Location EPA Method 6230D Analytical Results a Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE 1,1-DCE Chloroform Chloromelhane methane Bromochloro- Acetone Vinyl Chloride Toluene MTBE Bromomethane Ethylbenzene 1,2,4- Trimethylbenzene Xylenes Benzene NCGWS 0.7 2.8 70 70 7 0.00019 2.6 0.6 700 0.015 1,000 200 NE 29 350 530 1 MW-1 10/07/98 15.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 1.5 BDL BDL BDL BDL BDL BDL 4.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 23 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 9.9 BDL BDL BDL BDL 5.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 0.52 BDL BDL BDL BDL BDL BDL 26 BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 0.63 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL BDL 9.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 4.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 2.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.62 BDL BDL BDL BDL BDL BDL 06/09/04 1.7 2.5 BDL 16 BDL BDL BDL BDL NA 1.5 BDL BDL BDL BDL BDL BDL BDL 09/09/04 BDL 1.4 0.67 14 BDL BDL BDL BDL NA 1.1 BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL 1.2 BDL 17 BDL BDL BDL BDL NA 0.67 BDL BDL BDL BDL BDL BDL BDL 03/22/05 1.2 6.5 0.55 37 BDL BDL BDL BDL BDL 1.6 BDL BDL BDL BDL BDL BDL BDL 09/28/05 BDL BDL 1.3 60 BDL BDL BDL BDL BDL 4.2 0.51 BDL BDL BDL BDL BDL BDL 01/06/06 0.63 BDL BDL 2.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DW-2 10/16/98 2.4 BDL BDL BDL BDL 12.9 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0625/99 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 53 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/01/00 2.5 BDL BDL BDL BDL NA BDL NA NA NA NA BDL BDL BDL BDL BDL BDL 12/01/00 4.8 BDL BDL BDL BDL NA BDL NA NA NA NA BDL BDL BDL BDL BDL BDL 01/03/01 BDL BDL BDL BDL BDL NA BDL NA NA NA NA BDL BDL BDL BDL BDL BDL 06/14/01 BDL BDL BDL BDL BDL 13 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 0.92 BDL BDL BDL BDL BDL BDL 0.59 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0226/02 0.50 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1121/02 2.60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 2.2 BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 17 7.2 BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 1.2 1.4 BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL 2.2 BDL BDL BDL 03/22/05 BDL 1.2 BDL 1.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 8.1 0.8 BDL 09/28/05 BDL BDL BDL 3.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/06/06 11 0.61 BDL 3.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-3 10/07/98 BDL BDL BDL BDL BDL 13 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/28/01 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 BDL BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 BDL BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/041 BDL BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL NCGWS = North Carolina Groundwater Standards ug/l = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Tichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE= 1,l-Dichloroethene TRIGONFNGINEFRING CONSULTANTS, INC. Mr. I ouis Schaab, Allied Capital Corporation Fairchild Industrial Pradncts Company, Winston-Salem, North Carolina February 20, 2006 Trigon Project No. 042-03-154 TABLE 5: HISTORICAL GROUNDWATER ANALYTICAL SUMMARY fVOCsI Sampling Location I EPA Method 6230D Analytical Results u Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE l,l-DCE Chloroform Chloromethane Bromochloro- methane Acetone Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,2,4 Trimethylbenzene Xylenes Benzene NCGWS 0.7 2.8 70 70 7 0.00019 2.6 0.6 700 0.015 1,000 200 NE 29 350 530 1 MW-4 10/07/98 3.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 2.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 Well was dry on the sampling date 06/14/01 Well was dry on the sampling date 02/26/02 Well was dry on the sampling date 05/01/02 Well was on the sam I� date 08/13/02 Well was d on the sam lin date MW-5 10/07/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL I BDL BDL BDL BDL BDL 08/22/03 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 5.0 4.6 BDL 1.1 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 0.66 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/29/05 0.78 0.53 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/06 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-6 10/07/98 10.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL I BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 1.3 1 BDL BDL BDL BDL BDL BDL BDL 130 BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 Well was dry on the sampling date 11/27/01 Well was dry on the sampling date 02/26/02 Well was dry on the sampling date 05/01/02 Well was dry on the sampling date 08/13/02 Well was dry on the sampling date 11/21/02 Well was dry on the sampling date MW-6R 06/09/04 55 8.2 BDL 22 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 58 10 BDL 12 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 94 8.1 BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 80 9 BDL 1.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 100 9.5 BDL 2.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/05 100 5.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/061 65 6.1 1 BDL I BDL I BDL I BDL BDL I BDL I BDL BDL BDL BDL BDL I BDL I BDL I BDL I BDL NCGWS = North Carolina Groundwater Standards ug/l = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1, 1 -Dichloroethene TRIGON BNGINF.FJMNG CONSULTANTS, INC. Mr. Laois Schaab, Allied Capital Corporative+ Fairchild Indastrial Products Company, Winston-Salem, North Carolina Febraary 20. 2006 7rigon Project No. O42-05-154 TART.V 9- MQTnUWAT. (_R/1TTNDWATFR ANAI.VTTr AT. STTMMARV 1Vn al Sampling Location EPA Method 6230D Anal -cal Results u Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE 1,1-DCE Chloroform Chloromethane Bromochloro- methane Acetone 1 Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,2,4- Trim ethylbenzene Xylenes Benzene NCGWS 0.7 2.8 70 70 7 0.00019 2.6 0.6 700 0.015 1,000 200 NE 29 350 530 1 MW-7 11/16/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 1.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/O1 7.5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 5 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 3.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/O1/02 2.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL O8/13/02 Well was dry on the sampling date 11/21/02 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 15 2.4 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 19 6.9 BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 15 5.5 BDL 0.76 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL BDL BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 4.3 8.6 BDL 1.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL O6/09/05 2.1 9.1 BDL 1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/O5 1.4 8.7 BDL 1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/061 0.98 1 15 1 BDL 2.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.64 BDL BDL MW-8 Y 11/16/98 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 0.67 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/05 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL O1/05/06 1.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.64 BDL BDL MRr-9 04/12/99 144 159 2.4 49 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 177 187 BDL 60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL O8/24/00 1,300 920 15 140 3.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 10/31/00 1,700 710 13 190 3.5 NA BDL NA NA NA NA NA NA BDL BDL BDL BDL 12/01/00 1,000 570 8.7 170 2.9 NA BDL NA NA NA NA NA NA BDL BDL BDL BDL O1/03/01 1,100 770 11 330 5 NA BDL NA NA NA NA NA NA BDL BDL BDL BDL 06/14/01 420 220 24 510 6.8 11 BDL BDL BDL 2 BDL BDL BDL BDL BDL BDL BDL 11/27/01 2,800 1,600 BDL 710 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 5,000 1,800 BDL 1,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 5,000 1,900 25 1,200 6.2 BDL BDL 34 BDL 1.5 0.92 2.7 BDL BDL BDL BDL BDL 08/13/02 3,600 1,200 31 1,200 5.4 BDL BDL BDL BDL 2.5 BDL BDL BDL BDL BDL BDL BDL 11/21/02 4,000 1,500 BDL 2,200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 1,400 730 70 2,300 7.5 BDL BDL BDL NA 35 BDL BDL BDL BDL BDL BDL BDL 09/09/04 820 590 60 2,300 BDL BDL BDL BDL NA 15 BDL BDL BDL BDL BDL BDL BDL 12/09/04 540 800 BDL 1,200 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 900 1100 BDL 990 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 250 830 48 850 3.2 BDL BDL BDL BDL 23 BDL BDL BDL BDL BDL BDL 0.58 09/28/05 80 520 47 960 BDL BDL BDL BDL BDL 34 BDL BDL BDL BDL BDL BDL BDL O1105/06 200 760 54 1 740 BDL BDL BDL BDL BDL 49 BDL BDL BDL BDL BDL BDL BDL NCGWS = North Carolina Groundwater Standards ug/l = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-DicWoroethene 1,1-DCE = 1,1-Dichloroethene 7RIGON ENGINEERING CONSULTANTS, INC. Mr. Loris Schaab, Allied Capital Corporation Fairchild Indusrrial Products Company, Winston-Salem, North Carolina Febntary10, 1006 Trigon Project No. 042-05-134 TART,E 5_ HISTORICAL GROUNDWATER ANALYTICAL SITMMARY tVOCsI Sampling Location EPA Method 6230D nalytical Results u fl Sampling Date PCE TCE Trans-1,2-DCE cis-1,2-DCE I,I-DCE Chloroform Chloromethane Bromoehloro- than mee peel.. L Vinyl Chloride Toluene MTBE Bromo-methane Ethylbenzene 1,2,4 Trimethylbenzene Xylenes Benzene NCGWS 0.7 2.8 70 70 7 0.00019 2.6 0.6 - 700 0.015 1,000 200 NE 29 350 530 I NM-10 04/12/99 7.5 1.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/25/99 106 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 240 68 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 440 21 BDL 5.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/27/01 270 60 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 31 BDL BDL 440 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 65 9.1 0.97 190 BDL BDL BDL 8.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 150 15 BDL 90 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 170 35 BDL 39 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 150 63 BDL 46 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 150 57 BDL 48 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 150 40 BDL 20 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 160 28 BDL 18 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 140 27 BDL 16 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/05 150 12 BDL 13 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/06 180 15 BDL 29 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-11 06/04/99 415 23 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 200 34 BDL 4.9 BDL BDL BDL BDL 76 BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 200 74 BDL 21 BDL BDL BDL 34 BDL BDL 0.95 BDL BDL BDL BDL BDL BDL 11/28/01 210 23 BDL 19 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 600 46 BDL 80 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 370 30 0.62 31 BDL 1.2 BDL 0.96 BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/13/02 Well was dry on the sampling date BDL 11/21/02 Insufficient water to sample BDL 06/09/04 380 52 BDL 35 BDL 1.1 BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 360 45 BDL 30 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 480 59 BDL 43 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 430 54 BDL 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 290 39 BDL 43 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/05 320 36 BDL 33 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/06 360 63 BDL 63 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL PAW-12 06/04/991 BDL I BDL I BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/001 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL MW-13 06/04/99 112 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/24/00 190 2.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/14/01 260 6 BDL 1.2 BDL BDL BDL BDL BDL BDL 0.6 BDL BDL BDL BDL BDL BDL 11/27/01 170 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 02/26/02 390 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 05/01/02 270 11 BDL 2.2 BDL 0.59 BDL 7.7 BDL BDL BDL BDL 1.2 BDL BDL BDL BDL 08/13/02 320 16 BDL 5.3 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11/21/02 210 11 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 08/22/03 270 34 0.56 35 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/04 37 24 2.9 220 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 09/09/04 BDL BDL BDL 210 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 12/09/04 BDL BDL BDL 250 BDL BDL BDL BDL NA BDL BDL BDL BDL BDL BDL BDL BDL 03/22/05 BDL BDL BDL 130 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 06/09/05 BDL BDL BDL 270 BDL BDL BDL, BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 09/28/05 BDL BDL BDL 270 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/061 BDL BDL BDL 220 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DW-16 10/24/OS 490 34 BDL 29 BDL BDL 3.1 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 01/05/061 3.5 1 4.7 1 1.4 470 BDL BDL BDL BDL BDL 1.8 BDL BDL BDL BDL BDL BDL BDL DW-17 10/24/051 18 1 17 25 750 0.83 0.65 BDL BDL BDL 6.3 BDL BDL BDL BDL BDL BDL BDL 01/05/061 5.7 1 43 1 14 400 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL DW-18 01/05/061 110 1 16 1 BDL 2.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.59 BDL BDL DW-19 01/05/061 100 1 3.1 BDL 1.2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.65 BDL BDL NCGWS = North Carolina Groundwater Standards ug/l = micrograms per liter, analogous to parts per billion BDL = Below Laboratory Detection Limits NA = Not Analyzed NE = Not Established Note: Concentrations in bold type exceed NCGWS. PCE = Tetrachloroethene TCE = Trichloroethene Trans-1,2-DCE = trans-1,2-Dichloroethene cis-1,2-DCE = cis-1,2-Dichloroethene 1,1-DCE = 1,1-Dichloroethene nUGON ENGINEERING CONSULTANTS, INC. FIGURES ' ,_�� - ..�. ? x• tiw,.,,� �f� � �... -, (-• U ; : �� • ��r.'s;� •^.` Li lii �f',t/f 7 ,' � , .mot' •ice• '1 J'i �1•. ��=' �... ,.••,�•� .Lf •87.��-. • 8'�°'_-. '` ;%i �i �� _�';%i -ter '�'�J'��., '�•• �,_,•11 '"�; ': .,f �, is • r!" y • •' �� •� f �'�iv 1 ' � � f�'p i1.� J '•ram" .\ �/• :��_� , � �-. ��`.1\� � 1. :n r, It .,�• -tea.•, t�ti1.'- � �r+� � /v�� �. -/,,: j - ���'��. all _ .:%^ r-., -�� � � -tip. �\..�—` f�' � �r - �>� �_ ;1:• 6�•-, �!, )fit =.H, - �' y•r I _ .. "�.v = :-, - -� _ .,�\� • r it - _ • � �.�` Ham- "! r ;- �1 �•� � � _,;���;� _-__-� -.-� _ '-:. �;f_. �_ _V+ '� ' +•'�„` � .1.- ...till` j 43 . ��. ` _ � . `� .`•f--+'.. .1.��� t+ .� -� t.- I' J, - �•;� / --' !'�r �-�:- -'rim \! -� `� as � a : ®f aa- - • • • ' '` i _.�� _ - ass � ^ \' � C If 120 Ir ay i .•� � ✓_ � - _�V . y • • -, ` � \` � �.;�; `j , - -•l �39 2 � of �i".-J' '�'`� / Ter J ;; != �� _ i� �l 1•:;•i. * $ievq' F tey^ •* •" �� '', ._ ITT nn F yN'--_, _•�.-..' r� __--__ �\ ..� 001�-ter "- _�-���: ��, ',; SCALE: DATE: APPROVED BY: SOURCE: 1950 (PHOTOREVISED 1971) 1" = 2000' 1/25/06 USGS MAP, WINSTON—SALEM WEST QUADRANGLE FAIRCHILD INDUSTRIAL PRODUCTS COMPANY 3920 WESTPOINT BOULEVARD TRIGON11 WINSTON SALEM, NORTH CAROLINA Trigon Engineering Consultants, Inc. TRIGON PROJECT NO.042-05-154 313 Gallimore Dairy Road FIGURE Greensboro, North Carolina 27409 SITE LOCATION MAP 1 3 w 9AC ws 124ZS rPolNT eu 2551 ry — 2550 4 1.24AilC 3j Trigon Engineering Consultants, Inc. 313 Gallimore Dairy Road Greensboro, North Carolina 27409 6 1.00AC 5 1,oSAC ail, —F - 7 Ar o.97AC 8 0 �I II II I , ' NORTH I , 11I 1; 05.0 5.00AC � 5.83AC rq 3 ril ►--.I R K 4C r I � I N I I I I 1Pi9 I I T 8' u7a.o I 14.2 II 11, 2 3 9 m II � 3930A SCALE: DATE: I APPROVI�p BY: SOURCE: FORSYTH COUNTY TAX MAP V = 200' 1/27/06 FAIRCHILD INDUSTRIAL PRODUCTS COMPANY 3920 WESTPOINT BOULEVARD WINSTON SALEM, NORTH CAROLINA TRIGON PROJECT NO.042-05-154 FIGURE SURROUNDING PROPERTY OWNERS MAP 2 APPENDIX A NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT -GROUNDWATER SECTION P O. BOX 27687 - RALEIGH, N.C. 27611-7687, PHONE (919) 733-3221 WELL CONSTRUCTION RECORD FOR OFFICE USE ONLY Quad. No. Serial No. Lat. Long. Pc Minor Basin Basin Code Header Ent. GW-1 Ent. DRILLING CONTRACTOR Venable Brothers STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER 3278 (Jamie waters) PERMIT NUMBER: NA 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: Winston-Salem, North Carolina County: Forsyth 3920 Westpoint Boulevard (Road, Community, or Subdivision and Lot No.) DW-18 2. OWNER Fairchild Industrial Products ADDRESS 3920 Westpoint Boulevard (Street or Route No.) Winston-Salem, North Carolina 27103 City or Town State Zip Code 3. DATE DRILLED 12/27/05 USE OF WELL Monitoring 4. TOTAL DEPTH 32.5 CUTTINGS COLLECTED® Yes ❑ No 5, DOES WELL REPLACE EXISTING WELL? ❑ Yes ® No 6. STATIC WATER LEVEL: 19.76 FT. ❑ above TOP OF CASING, ® below TOP OF CASING IS 0 FT. ABOVE LAND SURFACE 7. YIELD (gpm): N/A METHOD OF TEST N/A 8. WATER ZONES (depth): N/A Depth DRILLING LOG From To Formation Description 0.0-8.0 Loose Brown -Orange Slightly Silty Coarse to Fine Sand -fill (moist. non -cohesive) 8.0-32.5 Medium Dense Brown Slightly Silty Medium to Fine Sand -Residual (moist, cohesive). 9. CHLORINATION: Type N/A Amount N/A If additional space is needed, use back of form 10. CASING: Wall Thickness Material LOCATION SKETCH Depth Diameter or Weight/Ft. (Show direction and distance from at least two State Roads, or other map reference points) From 0 To 27.5 Ft. 2" Schedule 40 PVC From To Ft. See Drawing No. 1 From To Ft. 11. GROUT: Depth Material Method From 0 To 24.5 Ft. Portland Tremmie From To Ft. 12. SCREEN: Depth Diameter Slot Size Material From 27.5 To 32.5 Ft. 2" in. 0.010" in. PVC From To Ft. in. in. From To Ft. in. in. 13. GRAVEL PACK: Depth Size Material From 26.5 To 32.5 Ft. filter fine Sand From To Ft. 14. REMARKS: Bentonite at 24.5 to 26.5 feet below ground surface I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACPORDANCE WITH 15 NCAC 2C, WELL CONSTRUCTION SANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED.TO THE VVELL OWNER. zl ( � 14 DATE SIGNATURE OF CONTRACTOR OR AGENT original to Division of Environmental Management and copy to well owner. h:\0420\projects\2005\154 fairchild deep well installation\september monitoring\wcr form dw-18.doc FOR OFFICE USE ONLY NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT - GROUNDWATER SECTION P.O. BOX 27687 - RALEIGH, N.C. 27611-7687, PHONE (919) 733-3221 WELL CONSTRUCTION RECORD Quad. No. Serial No. Lat. Long. Pc Minor Basin Basin Code Header Ent. GW-1 Ent. DRILLING CONTRACTOR Venable Brothers STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER 3278 (Jamie Waters) PERMIT NUMBER: NA 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: Winston-Salem, North Carolina County: Forsyth 3920 Westpoint Boulevard (Road, Community, or Subdivision and Lot No.) DW-19 2. OWNER Fairchild Industrial Products ADDRESS 3920 Westpoint Boulevard (Street or Route No.) _Winston-Salem, North Carolina 27103 City or Town State Zip Code 3. DATE DRILLED 12/28/05 USE OF WELL Monitoring 4. TOTAL DEPTH 54.8 CUTTINGS COLLECTED ® Yes ❑ No 5. DOES WELL REPLACE EXISTING WELL? ❑ Yes ® No 6. STATIC WATER LEVEL: 19.74 FT. ❑ above TOP OF CASING, ® below TOP OF CASING IS 0 FT. ABOVE LAND SURFACE 7. YIELD (gpm): N/A METHOD OF TEST N/A 8. WATER ZONES (depth): N/A 9. CHLORINATION: Type N/A Amount N/A 10. CASING: Wall Thickness Material Depth Diameter or Weight/Ft. From 0 To 49.8 Ft. 2" Schedule 40 PVC From 0 To 42.0 Ft. 6" Schedule 40 PVC From To Ft. 11. GROUT: Depth Material Method From 0 To 46.0 Ft. Portland Tremmie From To Ft. 12. SCREEN: Depth Diameter Slot Size Material From 49.8 To 54.8 Ft. 2" in. 0.010" in. PVC From To Ft. in. in. From To Ft. in. in. 13. GRAVEL PACK: Depth Size Material From 48.0 To 54.8 Ft. filter fine Sand From To Ft. 14. REMARKS: Bentonite at 46.0 to 48.0 feet below ground surface Depth DRILLING LOG From To Formation Description 0.0-8.0 Loose Brown -Orange Slightly Silty Coarse to Fine Sand -fill (moist, non -cohesive) 8.0-54.8 Medium Dense Brown Slightly Silty Medium to Fine Sand -Residual (moist, cohesive). If additional space is needed, use back of forth. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) See Drawing No. 1 I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15 NCAC 2C, WELLCONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE ALL OWNER. Z14 SIGNATURE OF CONTRACTOR OR AGENT original to Division of Environmental Management and copy to well owner. h:\0420\projects\2005\154 fairchild deep well installation\septemhcr monitoring\wcr form dw-19.doc Ol w w Die, ace Analytical www.pacelabs.com January 23, 2006 Mr. Chris Hay Trigon Engineering Consultants 313 Gallimore Dairy Rd Greensboro, NC 27409 RE: Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Dear Mr. Hay: Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone. 704.875.9092 Fax: 704.875.9091 Enclosed are the analytical results for sample(s) received by the laboratory on January 6, 2006. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Charlotte laboratory unless otherwise footnoted. If you have any questions concerning this report please feel free to contact me. Sincerely. &r", 0 C/�d Bonnie McKee Bonnie.McKee@pacelabs.com Project Manager Enclosures Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIFI AP F87R48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,N ACCOg c nelac 4 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical ® Huntersville, NC 28078 www.pacelahs.com SAMPLE SUMMARY Phone:704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Sample Sample Number Number Client Sample ID Matrix Date Collected Date Received 92110924-001 926519000 MW-1 Water 01/06/06 10:30 01/06/06 16:40 92110924-002 926519018 DW-2 Water 01/06/06 11:00 01/06/06 16:40 92110924-003 926519026 MW-5 Water 01/05/06 13:40 01/06/06 16:40 92110924.004 926519034 MW-8 Water 01/05/06 13:10 01/06/06 16:40 92110924-005 926519042 DW-16 Water 01/05/06 15:21 01/06/06 16:40 92110924-006 926519059 MW-6R Water 01/05/06 14:05 01/06/06 16:40 92110924-007 926519067 MW-7 Water 01/05/06 13:23 01/06/06 16:40 92110924-008 926519075 MW-9 Water 01/05/06 14:41 01/06/06 16:40 92110924-009 926519083 MW-10 Water 01/05/06 15:45 01/06/06 16:40 92110924.010 926519091 MW-11 Water 01/05/06 14:17 01/06/06 16:40 92110924-011 926519109 MW-13 Water 01/05/06 16:03 01/06/06 16:40 92110924-012 926519117 DW-17 Water 01/05/06 15:09 01/06/06 16:40 92110924-013 926519125 DW-18 Water 01/05/06 11:17 01/06/06 16:40 92110924-014 926519133 DW-19 Water 01/05/06 12:45 01/06/06 16:40 _Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI NFI AP F87648 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,% PLCOA lt0 09 C °nelac Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 SAMPLE ANALYTE COUNT Phone:704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Analysis Analytes Sample Number Sample No Client Sample ID Code Analysis Description Reported 92110924-001 926519000 MW-1 6230 WL92 GC VOCs in Water 62 92110924.002 926519018 DW-2 6230 WL92 GC VOCs in Water 62 92110924-003 926519026 14W-5 6230 WL92 GC VOCs in Water 62 92110924-004 926519034 14W-8 6230 WL92 GC VOCs in Water 62 92110924-005 926519042 DW-16 6230 WL92 GC VOCs in Water 62 92110924-006 926519059 MW-6R 6230 WL92 GC VOCs in Water 62 92110924-007 926519067 MW-7 6230 WL92 GC VOCs in Water 62 92110924-008 926519075 MW-9 6230 WL92 GC VOCs in Water 62 92110924-009 926519083 MW-10 6230 WL92 GC VOCs in Water 62 92110924-010 926519091 MW-11 6230 WL92 GC VOCs in Water 62 92110924-011 926519109 MW-13 6230 WL92 GC VOCs in Water 62 92110924.012 926519117 DW-17 6230 WL92 GC VOCs in Water 62 92110924-013 926519125 DW-18 6230 WL92 GC VOCs in Water 62 92110924.014 926519133 DW-19 6230 WL92 GC VOCs in Water 62 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI NIFI AP F97MA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N ACC, `t0 5 C nelac Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelahs.com Lab Sample No: 926519000 Client Sample ID: MW-1 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875, 9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924.001 Date Collected: 01/06/06 10:30 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 0.13 1.0 01/13/06 07:08 PPM 71.43-2 Bromobenzene ND mg/l 0.00050 0.34 1.0 01/13/06 07:08 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 0.41 1.0 01/13/06 07:08 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 0.33 1.0 01/13/06 07:08 PPM 75-27-4 Bromoform ND mg/l 0.00050 0.50 1.0 01/13/06 07:08 PPM 75-25-2 Bromomethane ND mg/l 0.00050 0.36 1.0 01/13/06 07:08 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 0.28 1.0 01/13/06 07:08 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 0.45 1.0 01/13/06 07:08 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 0.41 1.0 01/13/06 07:08 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 0.33 1.0 01/13/06 07:08 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 0.24 1.0 01/13/06 07:08 PPM 108-90-7 Chloroethane ND mg/l 0.00050 0.42 1.0 01/13/06 07:08 PPM 75.00.3 Chloroform ND mg/l 0.00050 0.31 1.0 01/13/06 07:08 PPM 67-66.3 Chloromethane ND mg/l 0.0020 0.30 1.0 01/13/06 07:08 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 0.34 1.0 01/13/06 07:08 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 0.32 1.0 01/13/06 07:08 PPM 106-43.4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 0.95 1.0 01/13/06 07:08 PPM 96-12.8 Dibromochloromethane ND mg/l 0.00050 0.29 1.0 01/13/06 07:08 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 0.50 1.0 01/13/06 07:08 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 0.29 1.0 01/13/06 07:08 PPM 74-95.3 1,2-Dichlorobenzene ND mg/l 0.0010 0.23 1.0 01/13/06 07:08 PPM 95-50-1 1.3-Dichlorobenzene ND mg/l 0.0010 0.46 1.0 01/13/06 07:08 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 0.43 1.0 01/13/06 07:08 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 0.18 1.0 01/13/06 07:08 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 0.48 1.0 01/13/06 07:08 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 0.25 1.0 01/13/06 07:08 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 0.47 1.0 01/13/06 07:08 PPM 75-35-4 cis-1,2-Dichloroethene 0.0024 mg/l 0.00050 0.34 1.0 01/13/06 07:08 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 0.18 1.0 01/13/06 07:08 PPM 156-60-5 1.2-Dichloropropane ND mg/l 0.00050 0.43 1.0 01/13/06 07:08 PPM 78-87-5 1.3-Dichloropropane ND mg/l 0.00050 0.28 1.0 01/13/06 07:08 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 0.46 1.0 01/13/06 07:08 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 0.35 1.0 01/13/06 07:08 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 0.29 1.0 01/13/06 07:08 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 0.30 1.0 01/13/06 07:08 PPM 10061.02-6 Diisopropyl ether ND mg/l 0.00050 0.25 1.0 01/13/06 07:08 PPM 108-20.3 Ethylbenzene ND mg/l 0.00050 0.13 1.0 01/13/06 07:08 PPM 100-41.4 Date: 01/23/06 Page: 1 of 36 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 t • Arco" NC Drinking Water 37706 SC Environmental 99030 -11 Sc 99006 Gi NIC] no PIUAAR p nelac FI NFI AP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519000 Project Sample Number: 92110924-001 Date Collected: 01/06/06 10:30 Client Sample ID: MW-1 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual Re9Lmt Hexachloro-1,3-butadiene ND mg/l 0.0020 0.82 1.0 01/13/06 07:08 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/13/06 07:08 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/13/06 07:08 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/13/06 07:08 PPM 75-09.2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/13/06 07:08 PPM 1634-04.4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/13/06 07:08 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 0.18 1.0 01/13/06 07:08 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/13/06 07:08 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/13/06 07:08 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 07:08 PPM 79.34-5 Tetrachloroethene 0.00063 mg/l 0.00050 0.38 1.0 01/13/06 07:08 PPM 127-18-4 Toluene ND mg/l 0.00050 0.18 1.0 01/13/06 07:08 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 07:08 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/13/06 07:08 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 07:08 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 07:08 PPM 79-00-5 Trichloroethene ND mg/l 0.00050 0.12 1.0 01/13/06 07:08 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/13/06 07:08 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/13/06 07:08 PPM 96-18-4 1,2,4-Trimethylbenzene ND mg/l 0.00050 0.28 1.0 01/13/06 07:08 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/13/06 07:08 PPM 108-67-8 Vinyl chloride ND mg/l 0.00050 0.22 1.0 01/13/06 07:08 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/13/06 07:08 PPM o-Xylene ND mg/l 0.00050 1.0 01/13/06 07:08 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 102 % 1.0 01/13/06 07:08 PPM 625-98-9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI hirl AD PR7949 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N ACooq nelac£ Page: 2 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 ;aneAnalyficala www.pacelabs.com Lab Sample No: 926519018 Client Sample ID: DW-2 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704, 875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924-002 Date Collected: 01/06/06 11:00 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 0.13 1.0 01/17/06 15:07 PPM 71-43.2 Bromobenzene ND mg/l 0.00050 0.34 1.0 01/17/06 15:07 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 0.41 1.0 01/17/06 15:07 PPM 74-97.5 Bromodichloromethane ND mg/l 0.00050 0.33 1.0 01/17/06 15:07 PPM 75-27.4 Bromoform ND mg/l 0.00050 0.50 1.0 01/17/06 15:07 PPM 75-25-2 Bromomethane ND mg/l 0.00050 0.36 1.0 01/17/06 15:07 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 0.28 1.0 01/17/06 15:07 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 0.45 1.0 01/17/06 15:07 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 0.41 1.0 01/17/06 15:07 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 0.33 1.0 01/17/06 15:07 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 0.24 1.0 01/17/06 15:07 PPM 108-90-7 Chloroethane ND mg/l 0.00050 0.42 1.0 01/17/06 15:07 PPM 75-00-3 Chloroform ND mg/l 0.00050 0.31 1.0 01/17/06 15:07 PPM 67-66-3 Chloromethane ND mg/l 0.0020 0.30 1.0 01/17/06 15:07 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 0.34 1.0 01/17/06 15:07 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 0.32 1.0 01/17/06 15:07 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 0.95 1.0 01/17/06 15:07 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 0.29 1.0 01/17/06 15:07 PPM 124-48.1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 0.50 1.0 01/17/06 15:07 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 0.29 1.0 01/17/06 15:07 PPM 74-95-3 1,2-Dichlorobenzene ND mg/l 0.0010 0.23 1.0 01/17/06 15:07 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0010 0.46 1.0 01/17/06 15:07 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 0.43 1.0 01/17/06 15:07 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 0.18 1.0 01/17/06 15:07 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 0.48 1.0 01/17/06 15:07 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 0.25 1.0 01/17/06 15:07 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 0.47 1.0 01/17/06 15:07 PPM 75-35-4 cis-1,2-Dichloroethene 0.0033 mg/l 0.00050 0.34 1.0 01/17/06 15:07 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.00050 0.18 1.0 01/17/06 15:07 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 0.43 1.0 01/17/06 15:07 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 0.28 1.0 01/17/06 15:07 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 0.46 1.0 01/17/06 15:07 PPM 594-20-7 1.1-Dichloropropene ND mg/l 0.00050 0.35 1.0 01/17/06 15:07 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 0.29 1.0 01/17/06 15:07 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 0.30 1.0 01/17/06 15:07 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 0.25 1.0 01/17/06 15:07 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 0.13 1.0 01/17/06 15:07 PPM 100-41-4 Date: 01/23/06 Page: 3 of 36 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ,N ACC," NC Drinking Water 37706 SC Environmental Pi NFI AP 99030 Eo "f nelac£ Sc 99006 FR7RdR FI NFI AP F87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 3.Analytical Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519018 Project Sample Number: 92110924-002 Date Collected: 01/06/06 11:00 Client Sample ID: DW-2 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.0020 0.82 1.0 01/17/06 15:07 PPM 87-68.3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/17/06 15:07 PPM 98-82.8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/17/06 15:07 PPM 99-87.6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/17/06 15:07 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/17/06 15:07 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/17/06 15:07 PPM 91-20.3 n-Propylbenzene ND mg/l 0.00050 0.18 1.0 01/17/06 15:07 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/17/06 15:07 PPM 100-42-5 1,1,1.2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/17/06 15:07 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/17/06 15:07 PPM 79-34-5 Tetrachloroethene 0.011 mg/l 0.00050 0.38 1.0 01/17/06 15:07 PPM 127-18-4 Toluene ND mg/l 0.00050 0.18 1.0 01/17/06 15:07 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/17/06 15:07 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/17/06 15:07 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/17/06 15:07 PPM 71-55-6 1.1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/17/06 15:07 PPM 79-00-5 Trichloroethene 0.00061 mg/l 0.00050 0.12 1.0 01/17/06 15:07 PPM 79.01-6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/17/06 15:07 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/17/06 15:07 PPM 96-18.4 1,2,4-Trimethylbenzene ND mg/l 0.00050 0.28 1.0 01/17/06 15:07 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/17/06 15:07 PPM 108-67-8 Vinyl chloride ND mg/l 0.00050 0.22 1.0 01/17/06 15:07 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/17/06 15:07 PPM o-Xylene ND mg/l 0.00050 1.0 01/17/06 15:07 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 113 % 1.0 01/17/06 15:07 PPM 625-98-9 Date: 01/23/06 Page: 4 of 36 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIFI AP F AAR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N AC Cpgp' °nelac Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ;aneAnalyfical@ www.pacelabs.com Lab Sample No: 926519026 Client Sample ID: MW-5 Pace Analytical Services, Inc. 9800 Kincey A venue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 Project Sample Number: 92110924-003 Date Collected: 01/05/06 13:40 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 0.13 1.0 01/13/06 01:34 PPM 71-43.2 Bromobenzene ND mg/l 0.00050 0.34 1.0 01/13/06 01:34 PPM 108.86.1 Bromochloromethane ND mg/l 0.00050 0.41 1.0 01/13/06 01:34 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 0.33 1.0 01/13/06 01:34 PPM 75-27.4 Bromoform ND mg/l 0.00050 0.50 1.0 01/13/06 01:34 PPM 75-25-2 Bromomethane ND mg/l 0.00050 0.36 1.0 01/13/06 01:34 PPM 74-83.9 n-Butylbenzene ND mg/l 0.0010 0.28 1.0 01/13/06 01:34 PPM 104.51.8 sec-Butylbenzene ND mg/l 0.00050 0.45 1.0 01/13/06 01:34 PPM 135.98.8 tert-Butylbenzene ND mg/l 0.00050 0.41 1.0 01/13/06 01:34 PPM 98.06.6 Carbon tetrachloride ND mg/l 0.00050 0.33 1.0 01/13/06 01:34 PPM 56.23-5 Chlorobenzene ND mg/l 0.00050 0.24 1.0 01/13/06 01:34 PPM 108.90.7 Chloroethane ND mg/l 0.00050 0.42 1.0 01/13/06 01:34 PPM 75-00.3 Chloroform ND mg/l 0.00050 0.31 1.0 01/13/06 01:34 PPM 67-66-3 Chloromethane ND mg/l 0.0020 0.30 1.0 01/13/06 01:34 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 0.34 1.0 01/13/06 01:34 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 0.32 1.0 01/13/06 01:34 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 0.95 1.0 01/13/06 01:34 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 0.29 1.0 01/13/06 01:34 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 0.50 1.0 01/13/06 01:34 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 0.29 1.0 01/13/06 01:34 PPM 74-95-3 1,2-Dichlorobenzene ND mg/l 0.0010 0.23 1.0 01/13/06 01:34 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0010 0.46 1.0 01/13/06 01:34 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 0.43 1.0 01/13/06 01:34 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 0.18 1.0 01/13/06 01:34 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 0.48 1.0 01/13/06 01:34 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 0.25 1.0 01/13/06 01:34 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 0.47 1.0 01/13/06 01:34 PPM 75-35-4 cis-1,2-Dichloroethene ND mg/l 0.00050 0.34 1.0 01/13/06 01:34 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 0.18 1.0 01/13/06 01:34 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 0.43 1.0 01/13/06 01:34 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 0.28 1.0 01/13/06 01:34 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 0.46 1.0 01/13/06 01:34 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 0.35 1.0 01/13/06 01:34 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 0.29 1.0 01/13/06 01:34 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 0.30 1.0 01/13/06 01:34 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 0.25 1.0 01/13/06 01:34 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 0.13 1.0 01/13/06 01:34 PPM 100-41-4 Date: 01/23/06 Page: 5 of 36 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 >Ccoga NC Drinking Water 37706 SC Environmental 99030 Sc 99006 Fi AIFI DP FR7RAA -onelac£ A NFI AP F87627 Pace Anaiyticai Services, inc. 9800 Kincey Avenue, Suite 100 Analytical Huntersville, NC 28078 Phone: 704.875.9092 www.paceiabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042.05-154 Lab Sample No: 926519026 Project Sample Number: 92110924-003 Date Collected: 01/05/06 13:40 Client Sample ID: MW-5 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmL Hexachloro-1,3-butadiene ND mg/l 0.0020 0.82 1.0 01/13/06 01:34 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/13/06 01:34 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/13/06 01:34 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/13/06 01:34 PPM 75.09-2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/13/06 01:34 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/13/06 01:34 PPM 91-20-3 n-Propylbenzene ND mg/l 0,00050 0.18 1.0 01/13/06 01:34 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/13/06 01:34 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/13/06 01:34 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 01:34 PPM 79-34-5 Tetrachloroethene ND mg/l 0.00050 0.38 1.0 01/13/06 01:34 PPM 127-18-4 Toluene ND mg/l 0.00050 0.18 1.0 01/13/06 01:34 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 01:34 PPM 87.61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/13/06 01:34 PPM 120.82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 01:34 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 01:34 PPM 79-00.5 Trichloroethene ND mg/l 0.00050 0.12 1.0 01/13/06 01:34 PPM 79.01.6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/13/06 01:34 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/13/06 01:34 PPM 96-18-4 1.2,4-Trimethylbenzene ND mg/l 0.00050 0.28 1.0 01/13/06 01:34 PPM 95.63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/13/06 01:34 PPM 108-67.8 Vinyl chloride ND mg/l 0.00050 0.22 1.0 01/13/06 01:34 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/13/06 01:34 PPM o-Xylene ND mg/l 0.00050 1.0 01/13/06 01:34 PPM 95.47-6 1-Chloro-3-fluorobenzene (S) 116 % 1.0 01/13/06 01:34 PPM 625-98-9 Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI AIFI GP FR7fidR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ALCoq °nelac 4 Page: 6 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical o Huntersville, NC 28078 www.pacelabs.com Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 Lab Sample No: 926519034 Project Sample Number: 92110924-004 Date Collected: 01/05/06 13:10 Client Sample ID: MW-8 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 0.13 1.0 01/13/06 02:15 PPM 71-43-2 Bromobenzene ND mg/l 0.00050 0.34 1.0 01/13/06 02:15 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 0.41 1.0 01/13/06 02:15 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 0.33 1.0 01/13/06 02:15 PPM 75-27-4 Bromoform ND mg/l 0.00050 0.50 1.0 01/13/06 02:15 PPM 75-25-2 Bromomethane ND mg/l 0.00050 0.36 1.0 01/13/06 02:15 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0010 0.28 1.0 01/13/06 02:15 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 0.45 1.0 01/13/06 02:15 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.00050 0.41 1.0 01/13/06 02:15 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.00050 0.33 1.0 01/13/06 02:15 PPM 56-23-5 Chlorobenzene ND mg/l 0.00050 0.24 1.0 01/13/06 02:15 PPM 108-90-7 Chloroethane ND mg/l 0.00050 0.42 1.0 01/13/06 02:15 PPM 75.00-3 Chloroform ND mg/l 0.00050 0.31 1.0 01/13/06 02:15 PPM 67.66-3 Chloromethane ND mg/l 0.0020 0.30 1.0 01/13/06 02:15 PPM 74.87-3 2-Chlorotoluene ND mg/l 0.00050 0.34 1.0 01/13/06 02:15 PPM 95.49-8 4-Chlorotoluene ND mg/l 0.00050 0.32 1.0 01/13/06 02:15 PPM 106.43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 0.95 1.0 01/13/06 02:15 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 0.29 1.0 01/13/06 02:15 PPM 124.48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 0.50 1.0 01/13/06 02:15 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 0.29 1.0 01/13/06 02:15 PPM 74-95-3 1,2-Dichlorobenzene ND mg/l 0.0010 0.23 1.0 01/13/06 02:15 PPM 95.50-1 1,3-Dichlorobenzene ND mg/l 0.0010 0.46 1.0 01/13/06 02:15 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 0.43 1.0 01/13/06 02:15 PPM 106.46-7 Dichlorodifluoromethane ND mg/l 0.00050 0.18 1.0 01/13/06 02:15 PPM 75.71-8 1,1-Dichloroethane ND mg/l 0.00050 0.48 1.0 01/13/06 02:15 PPM 75.34.3 1,2-Dichloroethane ND mg/l 0.00050 0.25 1.0 01/13/06 02:15 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 0.47 1.0 01/13/06 02:15 PPM 75-35.4 cis-1,2-Dichloroethene ND mg/l 0.00050 0.34 1.0 01/13/06 02:15 PPM 156-59.2 trans-1,2-Dichloroethene ND mg/l 0.00050 0.18 1.0 01/13/06 02:15 PPM 156-60.5 1,2-Dichloropropane ND mg/l 0.00050 0.43 1.0 01/13/06 02:15 PPM 78-87-5 1.3-Dichloropropane ND mg/l 0.00050 0.28 1.0 01/13/06 02:15 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 0.46 1.0 01/13/06 02:15 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 0.35 1.0 01/13/06 02:15 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 0.29 1.0 01/13/06 02:15 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 0.30 1.0 01/13/06 02:15 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 0.25 1.0 01/13/06 02:15 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 0.13 1.0 01/13/06 02:15 PPM 100.41-4 Date: 01/23/06 Page: 7 of 36 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI AIFI Ap FR7AAR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, . without the written consent of Pace Analytical Services, Inc. N Acc, Oq � nelac £ Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519034 Project Saalple Number: 92110924-004 Date Collected: 01/05/06 13:10 Client Sample ID: MW-8 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL OF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene NO mg/l 0.0020 0.82 1.0 01/13/06 02:15 PPM 87.68-3 Isopropylbenzene (Cumene) NO mg/l 0,09050 0.15 1.0 01/13/06 02:15 PPM 98-82-8 p-Isopropyltoluene NO mg/l 0.0010 0.25 1.0 01/13/06 02:15 PPM 99.87-6 Methylene chloride NO mg/l 0,0020 1.0 1.0 01/13/06 02:15 PPM 75.09-2 Methyl-tert-butyl ether NO mg/l 0.00050 0.20 1.0 01/13/06 02:15 PPM 1634-04.4 Naphthalene NO mg/l 0.0020 1.7 1.0 01/13/06 02:15 PPM 91-20.3 n-Propylbenzene NO mg/l 0.00050 0.18 1.0 01/13/06 02:15 PPM 103.65-1 Styrene NO mg/l 0.00050 0.12 1.0 01/13/06 02:15 PPM 100-42-5 1,1,1,2-Tetrachloroethane NO mg/l 0.00050 0.38 1.0 01/13/06 02:15 PPM 630-20.6 1,1,2,2-Tetrachloroethane NO mg/l 0.00050 0.30 1.0 01/13/06 02:15 PPM 79-34-5 Tetrachloroethene 0.0012 mg/l 0.0005o 0.38 1.0 01/13/06 02:15 PPM 127-18-4 Toluene NO mg/l 0.00050 0.18 1.0 01/13/06 02:15 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 02:15 PPM 87-61-6 1,2,4-Trichlorobenzene NO mg/l 0.0020 0.87 1.0 01/13/06 02:15 PPM 120.82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 02:15 PPM 71-55-6 1,1,2-Trichloroethane NO mg/l 0.00050 0.30 1.0 01/13/06 02:15 PPM 79-00-5 Trichloroethene NO mg/l 0.00050 0.12 1.0 01/13/06 02:15 PPM 79-01-6 Trichlorofluoromethane NO mg/l 0.00050 0.10 1.0 01/13/06 02:15 PPM 75-69-4 1.2,3-Trichloropropane NO mg/l 0.00050 0.38 1.0 01/13/06 02:15 PPM 96-18.4 1,2,4-Trimethylbenzene 0.00064 mg/l 0.00050 0.28 1.0 01/13/06 02:15 PPM 95-63-6 1,3,5-Trimethylbenzene NO mg/l 0.00050 0.44 1.0 01/13/06 02:15 PPM 108-67-8 Vinyl chloride NO mg/l 0.00050 0.22 1.0 01/13/06 02:15 PPM 75-01-4 m&p-Xylene NO mg/l 0.00050 0.22 1.0 01/13/06 02:15 PPM o-Xylene NO mg/l 0.UU050 1.0 01/13/06 02:15 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 118 % 1.0 01/13/06 02:15 PPM 625-98.9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 GI KIFI AD PURAR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N RCCOFO t <` °nelac Page: 8 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 ace Analytical ° www.pacelabs.com Lab Sample No: 926519042 Client Sample ID: DW-16 Parameters GC Volatiles GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1.2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1.3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rn hirl An 1:07CAO Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax., 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924-005 Date Collected: 01/05/06 15:21 Matrix: Water Date Received: 01/06/06 16:40 Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Method: SM 6230D ND mg/l 0.00050 0.13 1.0 01/13/06 08:31 PPM 71-43-2 ND mg/l 0.00050 0.34 1.0 01/13/06 08:31 PPM 108.86-1 ND mg/l 0.00050 0.41 1.0 01/13/06 08:31 PPM 74-97-5 ND mg/l 0.00050 0.33 1.0 01/13/06 08:31 PPM 75-27-4 ND mg/l 0.00050 0.50 1.0 01/13/06 08:31 PPM 75-25-2 ND mg/l 0.00050 0.36 1.0 01/13/06 08:31 PPM 74-83-9 ND mg/l 0.0010 0.28 1.0 01/13/06 08:31 PPM 104-51-8 ND mg/l 0.00050 0.45 1.0 01/13/06 08:31 PPM 135-98.8 ND mg/l 0.00050 0.41 1.0 01/13/06 08:31 PPM 98-06-6 ND mg/l 0.00050 0.33 1.0 01/13/06 08:31 PPM 56-23-5 ND mg/l 0.00050 0.24 1.0 01/13/06 08:31 PPM 108-90-7 ND mg/l 0.00050 0.42 1.0 01/13/06 08:31 PPM 75-00-3 ND mg/l 0.00050 0.31 1.0 01/13/06 08:31 PPM 67-66-3 ND mg/l 0.0020 0.30 1.0 01/13/06 08:31 PPM 74-87-3 ND mg/l 0.00050 0.34 1.0 01/13/06 08:31 PPM 95-49-8 ND mg/l 0.00050 0.32 1.0 01/13/06 08:31 PPM 106-43-4 ND mg/l 0.0020 0.95 1.0 01/13/06 08:31 PPM 96-12-8 ND mg/l 0.00050 0.29 1.0 01/13/06 08:31 PPM 124-48-1 ND mg/l 0.00050 0.50 1.0 01/13/06 08:31 PPM 106-93.4 ND mg/l 0.00050 0.29 1.0 01/13/06 08:31 PPM 74-95-3 ND mg/l 0.0010 0.23 1.0 01/13/06 08:31 PPM 95-50-1 ND mg/l 0.0010 0.46 1.0 01/13/06 08:31 PPM 541.73-1 ND mg/l 0.0010 0.43 1.0 01/13/06 08:31 PPM 106.46-7 ND mg/l 0.00050 0.18 1.0 01/13/06 08:31 PPM 75-71-8 ND mg/l 0.00050 0.48 1.0 01/13/06 08:31 PPM 75.34-3 ND mg/l 0.00050 0.25 1.0 01/13/06 08:31 PPM 107.06.2 ND mg/l 0.00050 0.47 1.0 01/13/06 08:31 PPM 75-35-4 0.47 mg/l 0.012 8.5 25.0 01/13/06 08:31 PPM 156-59-2 0.0014 mg/l 0.00050 0.18 1.0 01/13/06 08:31 PPM 156-60-5 ND mg/l 0.00050 0.43 1.0 01/13/06 08:31 PPM 78-87-5 ND mg/l 0.00050 0.28 1.0 01/13/06 08:31 PPM 142-28-9 ND mg/l 0.00050 0.46 1.0 01/13/06 08:31 PPM 594-20-7 ND mg/l 0.00050 0.35 1.0 01/13/06 08:31 PPM 563.58-6 ND mg/l 0.00050 0.29 1.0 01/13/06 08:31 PPM 10061-01-5 ND mg/l 0.00050 0.30 1.0 01/13/06 08:31 PPM 10061-02-6 ND mg/l 0.00050 0.25 1.0 01/13/06 08:31 PPM 108-20-3 ND mg/l 0.00050 0.13 1.0 01/13/06 08:31 PPM 100-41-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N ACC, �C °nelac£ Page: 9 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical0 Nuntersville, NC 28078 Phone: 704.875.9092 www.pacelahs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519042 Project Sample Number: 92110924-005 Date Collected: 01/05/06 15:21 Client Sample ID: DW-16 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual ReqAt Hexachloro-1,3-butadiene ND mg/l 0.0020 0.82 1.0 01/13/06 08:31 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/13/06 08:31 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/13/06 08:31 PPM 99-87-6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/13/06 08:31 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/13/06 08:31 PPM 1634-04.4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/13/06 08:31 PPM 91.20-3 n-Propylbenzene ND mg/l 0.00050 0.18 1.0 01/13/06 08:31 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/13/06 08:31 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/13/06 08:31 PPM 630-20.6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 08:31 PPM 79.34-5 Tetrachloroethene 0.0035 mg/l 0.00050 0.38 1.0 01/13/06 08:31 PPM 127-18.4 Toluene ND mg/l 0.00050 0.18 1.0 01/13/06 08:31 PPM 108-88.3 1,2.3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 08:31 PPM 87.61.6 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/13/06 08:31 PPM 120-82.1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 08:31 PPM 71.55-6 1,1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 08:31 PPM 79-00-5 Trichloroethene 0.0047 mg/l 0.00050 0.12 1.0 01/13/06 08:31 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/13/06 08:31 PPM 75-69.4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/13/06 08:31 PPM 96-18.4 1,2,4-Trimethylbenzene ND mg/l 0.00050 0.28 1.0 01/13/06 08:31 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/13/06 08:31 PPM 108-67-8 Vinyl chloride 0.0018 mg/l 0.00050 0.22 1.0 01/13/06 08:31 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/13/06 08:31 PPM o-Xylene ND mg/l 0.00050 1.0 01/13/06 08:31 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 101 % 1.0 01/13/06 08:31 PPM 625-98-9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 n nirt nn ro792no REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M RCCO, v`nPlar Page: 10 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 ;acmnalyfical ° www.pacelabs.com Lab Sample No: 926519059 Client Sample ID: MW-6R Parameters GC Volatiles GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1.2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1.2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1.3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI NCI AD CQ7CZAP Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042.05-154 Project Sample Number: 92110924-006 Date Collected: 01/05/06 14:05 Matrix: Water Date Received: 01/06/06 16:40 Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Method: SM 6230D ND mg/l 0.0025 0.65 5.0 01/13/06 02:57 PPM 71-43-2 ND mg/l 0.0025 1.7 5.0 01/13/06 02:57 PPM 108-86-1 ND mg/l 0.0025 2.0 5.0 01/13/06 02:57 PPM 74-97-5 ND mg/l 0.0025 1.6 5.0 01/13/06 02:57 PPM 75-27-4 ND mg/l 0.0025 2.5 5.0 01/13/06 02:57 PPM 75-25-2 ND mg/l 0.0025 1.8 5.0 01/13/06 02:57 PPM 74-83-9 ND mg/l 0.0050 1.4 5.0 01/13/06 02:57 PPM 104-51-8 ND mg/1 0.0025 2.2 5.0 01/13/06 02:57 PPM 135.98.8 ND mg/l 0.0025 2.0 5.0 01/13/06 02:57 PPM 98.06-6 ND mg/l 0.0025 1.6 5.0 01/13/06 02:57 PPM 56.23-5 ND mg/l 0.0025 1.2 5.0 01/13/06 02:57 PPM 108-90-7 ND mg/l 0.0025 2.1 5.0 01/13/06 02:57 PPM 75-00-3 ND mg/l 0.0025 1.6 5.0 01/13/06 02:57 PPM 67-66-3 ND mg/l 0.010 1.5 5.0 01/13/06 02:57 PPM 74.87-3 ND mg/l 0.0025 1.7 5.0 01/13/06 02:57 PPM 95-49.8 ND mg/l 0.0025 1.6 5.0 01/13/06 02:57 PPM 106-43-4 ND mg/l 0.010 4.8 5.0 01/13/06 02:57 PPM 96-12-8 ND mg/l 0.0025 1.4 5.0 01/13/06 02:57 PPM 124-48-1 ND mg/l 0.0025 2.5 5.0 01/13/06 02:57 PPM 106-93-4 ND mg/l 0.0025 1.4 5.0 01/13/06 02:57 PPM 74-95-3 ND mg/l 0.0050 1.2 5.0 01/13/06 02:57 PPM 95-50-1 ND mg/l 0.0050 2.3 5.0 01/13/06 02:57 PPM 541-73-1 ND mg/l 0.0050 2.2 5.0 01/13/06 02:57 PPM 106-46-7 ND mg/l 0.0025 0.90 5.0 01/13/06 02:57 PPM 75-71-8 ND mg/l 0.0025 2.4 5.0 01/13/06 02:57 PPM 75-34-3 ND mg/l 0.0025 1.2 5.0 01/13/06 02:57 PPM 107.06-2 ND mg/l 0.0025 2.4 5.0 01/13/06 02:57 PPM 75-35-4 ND mg/l 0.0025 1.7 5.0 01/13/06 02:57 PPM 156-59-2 ND mg/l 0.0025 0.90 5.0 01/13/06 02:57 PPM 156-60-5 ND mg/l 0.0025 2.2 5.0 01/13/06 02:57 PPM 78-87-5 ND mg/l 0.0025 1.4 5.0 01/13/06 02:57 PPM 142-28-9 ND mg/l 0.0025 2.3 5.0 01/13/06 02:57 PPM 594.20-7 ND mg/1 0.0025 1.8 5.0 01/13/06 02:57 PPM 563.58-6 ND mg/l 0.0025 1.4 5.0 01/13/06 02:57 PPM 10061-01-5 ND mg/1 0.0025 1.5 5.0 01/13/06 02:57 PPM 10061-02-6 ND mg/1 0.0025 1.2 5.0 01/13/06 02:57 PPM 108.20-3 ND mg/l 0.0025 0.65 5.0 01/13/06 02:57 PPM 100-41.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N RC�ago tt0 9C nelac 4 Page: 11 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NIFI AP FA7R?7 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 .Analytical o Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519059 Project Sample Number: 92110924-006 Date Collected: 01/05/06 14:05 Client Sample ID: MW-6R Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL OF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.010 4.1 5.0 01/13/06 02:57 PPM 87-68-3 Isopropylbenzene (Cumene) NO mg/l 0.0025 0.75 5.0 01/13/06 02:57 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0050 1.2 5.0 01/13/06 02:57 PPM 99-87-6 Methylene chloride NO mg/l 0.010 5.2 5.0 01/13/06 02:57 PPM 75-09-2 Methyl-tert-butyl ether NO mg/l 0,0025 1.0 5.0 01/13/06 02:57 PPM 1634-04.4 Naphthalene ND mg/l 0.010 8.4 5.0 01/13/06 02:57 PPM 91-20-3 n-Propylbenzene NO mg/l 0.0025 0.90 5.0 01/13/06 02:57 PPM 103-65-1 Styrene NO mg/l 0.0025 0.60 5.0 01/13/06 02:57 PPM 100-42.5 1,1.1,2-Tetrachloroethane ND mg/l 0.0025 1.9 5.0 01/13/06 02:57 PPM 630-20.6 1,1,2,2-Tetrachloroethane NO mg/l 0.0025 1.5 5.0 01/13/06 02:57 PPM 79-34-5 Tetrachloroethene 0.065 mg/l 0.0025 1.9 5.0 01/13/06 02:57 PPM 127-18-4 Toluene ND mg/l 0.0025 0.90 5.0 01/13/06 02:57 PPM 108-88.3 1,2.3-Trichlorobenzene NO mg/l 0.010 5.3 5.0 01/13/06 02:57 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.010 4.4 5.0 01/13/06 02:57 PPM 120-82-1 1,1.1-Trichloroethane NO mg/l 0.0025 2.2 5.0 01/13/06 02:57 PPM 71-55-6 1,1.2-Trichloroethane NO mg/l 0.0025 1.5 5.0 01/13/06 02:57 PPM 79-00.5 Trichloroethene 0.0061 mg/l 0.0025 0.60 5.0 01/13/06 02:57 PPM 79.01.6 Trichlorofluoromethane ND mg/l 0.0025 0.50 5.0 01/13/06 02:57 PPM 75.69.4 1.2.3-Trichloropropane ND mg/l 0.0025 1.9 5.0 01/13/06 02:57 PPM 96-18.4 1,2.4-Trimethylbenzene NO mg/l 0.0025 1.4 5.0 01/13/06 02:57 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.0025 2.2 5.0 01/13/06 02:57 PPM 108.67.8 Vinyl chloride NO mg/l 0.0025 1.1 5.0 01/13/06 02:57 PPM 75-01.4 m&p-Xylene ND mg/l 0.0025 1.1 5.0 01/13/06 02:57 PPM o-Xylene ND mg/l 0.0025 5.0 01/13/06 02:57 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 124 % 1.0 01/13/06 02:57 PPM 625-98-9 Date: 01/23/06 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37712 0 ,� SC Environmental 99030 CI hICI AD CQ7CAR s ne lace Page: 12 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL N LAP F87627 ace Analytical www. pacelabs. cam Lab Sample No: 926519067 Client Sample ID: MW-7 Parameters GC Volatiles GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl KIM An C07r-A4 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 fax: 704.875.9091 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924.007 Date Collected: 01/05/06 13:23 Matrix: Water Date Received: 01/06/06 16:40 Results Units Report Limit MDL OF Analyzed By CAS No. Qual RegLmt Method: SM 6230D NO mg/l 0.00050 0.13 1.0 01/13/06 03:39 PPM 71-43-2 NO mg/l 0.00050 0.34 1.0 01/13/06 03:39 PPM 108.86-1 NO mg/l 0.00050 0.41 1.0 01/13/06 03:39 PPM 74-97-5 NO mg/l 0.00050 0.33 1.0 01/13/06 03:39 PPM 75-27-4 NO mg/l 0.00050 0.50 1.0 01/13/06 03:39 PPM 75-25-2 ND mg/l 0.00050 0.36 1.0 01/13/06 03:39 PPM 74-83-9 NO mg/l 0.0010 0.28 1.0 01/13/06 03:39 PPM 104-51-8 NO mg/l 0.00050 0.45 1.0 01/13/06 03:39 PPM 135-98-8 NO mg/l 0.00050 0.41 1.0 01/13/06 03:39 PPM 98-06-6 NO mg/l 0.00050 0.33 1.0 01/13/06 03:39 PPM 56-23-5 NO mg/l 0.00050 0.24 1.0 01/13/06 03:39 PPM 108-90-7 NO mg/l 0.00050 0.42 1.0 01/13/06 03:39 PPM 75-00-3 NO mg/l 0.00050 0.31 1.0 01/13/06 03:39 PPM 67-66-3 NO mg/l 0.0020 0.30 1.0 01/13/06 03:39 PPM 74-87-3 NO mg/l 0.00050 0.34 1.0 01/13/06 03:39 PPM 95-49-8 ND mg/l 0.00050 0.32 1.0 01/13/06 03:39 PPM 106.43-4 ND mg/l 0.0020 0.95 1.0 01/13/06 03:39 PPM 96-12-8 NO mg/l 0.00050 0.29 1.0 01/13/06 03:39 PPM 124.48-1 NO mg/l 0.00050 0.50 1.0 01/13/06 03:39 PPM 106.93-4 NO mg/l 0.00050 0.29 1.0 01/13/06 03:39 PPM 74.95-3 NO mg/l 0.0010 0.23 1.0 01/13/06 03:39 PPM 95-50-1 NO mg/l 0.0010 0.46 1.0 01/13/06 03:39 PPM 541.73-1 NO mg/l 0.0010 0.43 1.0 01/13/06 03:39 PPM 106.46-7 NO mg/l 0.00050 0.18 1.0 01/13/06 03:39 PPM 75-71-8 NO mg/l 0.00050 0.48 1.0 01/13/06 03:39 PPM 75-34-3 NO mg/l 0.00050 0.25 1.0 01/13/06 03:39 PPM 107.06-2 NO mg/l 0.00050 0.47 1.0 01/13/06 03:39 PPM 75-35-4 0.0027 mg/l 0.00050 0.34 1.0 01/13/06 03:39 PPM 156-59-2 NO mg/l 0.00050 0.18 1.0 01/13/06 03:39 PPM 156-60-5 NO mg/l 0.00050 0.43 1.0 01/13/06 03:39 PPM 78-87-5 ND mg/l 0.00050 0.28 1.0 01/13/06 03:39 PPM 142-28-9 NO mg/l 0.00050 0.46 1.0 01/13/06 03:39 PPM 594-20-7 NO mg/l 0.00050 0.35 1.0 01/13/06 03:39 PPM 563-58-6 ND mg/l 0.00050 0.29 1.0 01/13/06 03:39 PPM 10061-01-5 NO mg/l 0.00050 0.30 1.0 01/13/06 03:39 PPM 10061-02-6 NO mg/l 0.00050 0.25 1.0 01/13/06 03:39 PPM 108-20-3 NO mg/l 0.00050 0.13 1.0 01/13/06 03:39 PPM 100.41-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,M AC Cp `t0 qp 9C ��°nelac Page: 13 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI_ NFLAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical ® Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519067 Project Sample Number: 92110924-007 Date Collected: 01/05/06 13:23 Client Sample ID: MW-7 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.0020 0.82 1.0 01/13/06 03:39 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/13/06 03:39 PPM 98.82-8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/13/06 03:39 PPM 99.87-6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/13/06 03:39 PPM 75.09.2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/13/06 03:39 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/13/06 03:39 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 0.18 1.0 01/13/06 03:39 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/13/06 03:39 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/13/06 03:39 PPM 630-20.6 1.1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 03:39 PPM 79-34-5 Tetrachloroethene 0.00098 mg/l 0.00050 0.38 1.0 01/13/06 03:39 PPM 127-18-4 Toluene ND mg/l 0.00050 0.18 1.0 01/13/06 03:39 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 03:39 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/13/06 03:39 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 03:39 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 03:39 PPM 79-00-5 Trichloroethene 0.015 mg/l 0.00050 0.12 1.0 01/13/06 03:39 PPM 79.01-6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/13/06 03:39 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/13/06 03:39 PPM 96-18-4 1,2,4-Trimethylbenzene 0.00064 mg/l 0.00050 0.28 1.0 01/13/06 03:39 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/13/06 03:39 PPM 108-67-8 Vinyl chloride ND mg/l 0.00050 0.22 1.0 01/13/06 03:39 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/13/06 03:39 PPM o-Xylene ND mg/l 0.00050 1.0 01/13/06 03:39 PPM 95.47-6 1-Chloro-3-fluorobenzene (S) 120 % 1.0 01/13/06 03:39 PPM 625-98.9 Date: 01/23/06 Page: 14 of 36 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ,CCogo. NC Drinking Water 37706 SC Environmental 99030 Ea Sc 99006 n nin AD PURAR `�nelac£ EL NELAP E87627 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical o Huntersville, NC 28078 Phone. 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519075 Project Sample Number: 92110924-008 Date Collected: 01/05/06 14:41 Client Sample ID: MW-9 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL OF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene NO mg/l 0.012 3.2 25.0 01/13/06 04:20 PPM 71-43-2 Bromobenzene NO mg/l 0.012 8.5 25.0 01/13/06 04:20 PPM 108-86-1 Bromochloromethane NO mg/l 0.012 10. 25.0 01/13/06 04:20 PPM 74.97-5 Bromodichloromethane NO mg/l 0.012 8.2 25.0 01/13/06 04:20 PPM 75-27-4 Bromoform NO mg/l 0.012 12. 25.0 01/13/06 04:20 PPM 75-25-2 Bromomethane NO mg/l 0.012 9.0 25.0 01/13/06 04:20 PPM 74-83-9 n-Butylbenzene NO mg/l 0.025 7.0 25.0 01/13/06 04:20 PPM 104-51-8 sec-Butylbenzene NO mg/l 0.012 11. 25.0 01/13/06 04:20 PPM 135.98-8 tert-Butylbenzene NO mg/l 0,012 10, 25.0 01/13/06 04:20 PPM 98-06-6 Carbon tetrachloride NO mg/l 0.012 8.2 25.0 01/13/06 04:20 PPM 56-23-5 Chlorobenzene NO mg/l 0.012 6.0 25.0 01/13/06 04:20 PPM 108.90-7 Chloroethane NO mg/l 0.012 10. 25.0 01/13/06 04:20 PPM 75-00-3 Chloroform NO mg/l 0.012 7.8 25.0 01/13/06 04:20 PPM 67-66-3 Chloromethane NO mg/l 0.050 7.5 25.0 01/13/06 04:20 PPM 74-87-3 2-Chlorotoluene NO mg/l 0.012 8.5 25.0 01/13/06 04:20 PPM 95-49-8 4-Chlorotoluene NO mg/l 0.012 8.0 25.0 01/13/06 04:20 PPM 106-43-4 1,2-Dibromo-3-chloropropane NO mg/l 0,050 24. 25.0 01/13/06 04:20 PPM 96-12-8 Dibromochloromethane NO mg/l 0.012 7.2 25.0 01/13/06 04:20 PPM 124-48-1 1,2-Dibromoethane (EDB) NO mg/l 0.012 12. 25.0 01/13/06 04:20 PPM 106-93-4 Dibromomethane NO mg/l 0.012 7.2 25.0 01/13/06 04:20 PPM 74-95-3 1,2-Dichlorobenzene NO mg/l 0.025 5.8 25.0 01/13/06 04:20 PPM 95-50-1 1,3-Dichlorobenzene NO mg/l 0.025 12. 25.0 01/13/06 04:20 PPM 541-73-1 1,4-Dichlorobenzene NO mg/l 0.025 11. 25.0 01/13/06 04:20 PPM 106-46-7 Dichlorodifluoromethane NO mg/l 0.012 4.5 25.0 01/13/06 04:20 PPM 75.71-8 1,1-Dichloroethane NO mg/l 0.012 12. 25.0 01/13/06 04:20 PPM 75-34-3 1,2-Dichloroethane NO mg/l 0.012 6.2 25.0 01/13/06 04:20 PPM 107.06.2 1,1-Dichloroethene NO mg/l 0.012 12. 25.0 01/13/06 04:20 PPM 75-35-4 cis-1,2-Dichloroethene 0.74 mg/l 0,012 8.5 25.0 01/13/06 04:20 PPM 156-59-2 trans-1,2-Dichloroethene 0.054 mg/l 0.012 4.5 25.0 01/13/06 04:20 PPM 156-60-5 1,2-Dichloropropane NO mg/l 0.012 11. 25.0 01/13/06 04:20 PPM 78-87-5 1,3-Dichloropropane NO mg/l 0.012 7.0 25.0 01/13/06 04:20 PPM 142-28-9 2,2-Dichloropropane NO mg/l 0.012 12. 25.0 01/13/06 04:20 PPM 594-20-7 1,1-Dichloropropene NO mg/l 0.012 8.8 25.0 01/13/06 04:20 PPM 563-58-6 cis-1,3-Dichloropropene NO mg/l 0.012 7.2 25.0 01/13/06 04:20 PPM 10061-01.5 trans-1,3-Dichloropropene NO mg/l 0.012 7.5 25.0 01/13/06 04:20 PPM 10061-02-6 Diisopropyl ether NO mg/l 0.012 6.2 25.0 01/13/06 04:20 PPM 108-20-3 Ethylbenzene NO mg/l 0.012 3.2 25.0 01/13/06 04:20 PPM 100-41-4 Date: 01/23/06 Page: 15 of 36 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI hirl AD FA7VA.Q REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,M ACCON c f nelac Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ;aneAnalyficalo www.pacelabs.com Lab Sample No: 926519075 Client Sample ID: MW-9 Parameters Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2.3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene 1-Chloro-3-fluorobenzene (S) Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl IUrl An ro7940 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 Project Sample Number: 92110924-008 Date Collected: 01/05/06 14:41 Matrix: Water Date Received: 01/06/06 16:40 Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt ND mg/l 0.050 20. 25.0 01/13/06 04:20 PPM 87-68-3 ND mg/l 0.012 3.8 25.0 01/13/06 04:20 PPM 98-82-8 ND mg/l 0.025 6.2 25.0 01/13/06 04:20 PPM 99-87-6 ND mg/l 0.050 26. 25.0 01/13/06 04:20 PPM 75-09.2 ND mg/l 0.012 5.0 25.0 01/13/06 04:20 PPM 1634-04-4 ND mg/l 0.050 42. 25.0 01/13/06 04:20 PPM 91-20-3 ND mg/l 0.012 4.5 25.0 01/13/06 04:20 PPM 103.65-1 ND mg/l 0.012 3.0 25.0 01/13/06 04:20 PPM 100-42-5 ND mg/l 0.012 9.5 25.0 01/13/06 04:20 PPM 630-20-6 ND mg/l 0.012 7.5 25.0 01/13/06 04:20 PPM 79.34-5 0.20 mg/l 0.012 9.5 25.0 01/13/06 04:20 PPM 127.18-4 ND mg/l 0,012 4.5 25.0 01/13/06 04:20 PPM 108-88-3 ND mg/l 0.050 26. 25.0 01/13/06 04:20 PPM 87-61-6 ND mg/l 0.050 22. 25.0 01/13/06 04:20 PPM 120.82-1 ND mg/l 0.012 11. 25.0 01/13/06 04:20 PPM 71.55-6 ND mg/l 0.012 7.5 25.0 01/13/06 04:20 PPM 79.00.5 0.76 mg/l 0.012 3.0 25.0 01/13/06 04:20 PPM 79-01-6 ND mg/l 0.012 2.5 25.0 01/13/06 04:20 PPM 75-69-4 ND mg/l 0.012 9.5 25.0 01/13/06 04:20 PPM 96-18-4 ND mg/l 0.012 7.0 25.0 01/13/06 04:20 PPM 95-63-6 ND mg/l 0.012 11. 25.0 01/13/06 04:20 PPM 108-67-8 0.049 mg/l 0.012 5.5 25.0 01/13/06 04:20 PPM 75.01-4 ND mg/l 0.012 5.5 25.0 01/13/06 04:20 PPM ND mg/l 0.012 25.0 01/13/06 04:20 PPM 95-47-6 102 % 1.0 01/13/06 04:20 PPM 625-98-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ACCORD p nekic£ Page: 16 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelabs.com Lab Sample No: 926519083 Client Sample ID: MW-10 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042-05.154 Project Sample Number: 92110924.009 Date Collected: 01/05/06 15:45 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0025 0.65 5.0 01/13/06 05:02 PPM 71-43-2 Bromobenzene ND mg/l 0.0025 1.7 5.0 01/13/06 05:02 PPM 108-86-1 Bromochloromethane ND mg/l 0.0025 2.0 5.0 01/13/06 05:02 PPM 74-97-5 Bromodichloromethane ND mg/l 0.0025 1.6 5.0 01/13/06 05:02 PPM 75-27-4 Bromoform ND mg/l 0.0025 2.5 5.0 01/13/06 05:02 PPM 75-25-2 Bromomethane ND mg/l 0.0025 1.8 5.0 01/13/06 05:02 PPM 74-83-9 n-Butylbenzene ND mg/l 0.0050 1.4 5.0 01/13/06 05:02 PPM 104-51.8 sec-Butylbenzene ND mg/l 0.0025 2.2 5.0 01/13/06 05:02 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.0025 2.0 5.0 01/13/06 05:02 PPM 98-06.6 Carbon tetrachloride ND mg/l 0.0025 1.6 5.0 01/13/06 05:02 PPM 56-23.5 Chlorobenzene ND mg/l 0.0025 1.2 5.0 01/13/06 05:02 PPM 108-90-7 Chloroethane ND mg/l 0.0025 2.1 5.0 01/13/06 05:02 PPM 75-00.3 Chloroform ND mg/l 0.0025 1.6 5.0 01/13/06 05:02 PPM 67-66.3 Chloromethane ND mg/l 0.010 1.5 5.0 01/13/06 05:02 PPM 74-87.3 2-Chlorotoluene ND mg/l 0.0025 1.7 5.0 01/13/06 05:02 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.0025 1.6 5.0 01/13/06 05:02 PPM 106.43-4 1.2-Dibromo-3-chloropropane ND mg/l 0.010 4.8 5.0 01/13/06 05:02 PPM 96-12.8 Dibromochloromethane ND mg/l 0.0025 1.4 5.0 01/13/06 05:02 PPM 124-48-1 1.2-Dibromoethane (EDB) ND mg/l 0.0025 2.5 5.0 01/13/06 05:02 PPM 106.93-4 Dibromomethane ND mg/l 0.0025 1.4 5.0 01/13/06 05:02 PPM 74-95-3 1.2-Dichlorobenzene ND mg/l 0.0050 1.2 5.0 01/13/06 05:02 PPM 95-50-1 1.3-Dichlorobenzene ND mg/l 0.0050 2.3 5.0 01/13/06 05:02 PPM 541-73-1 1.4-Dichlorobenzene ND mg/l 0.0050 2.2 5.0 01/13/06 05:02 PPM 106-46.7 Dichlorodifluoromethane ND mg/l 0.0025 0.90 5.0 01/13/06 05:02 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.0025 2.4 5.0 01/13/06 05:02 PPM 75-34-3 1.2-Dichloroethane ND mg/l 0.0025 1.2 5.0 01/13/06 05:02 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.0025 2.4 5.0 01/13/06 05:02 PPM 75-35-4 cis-1.2-Dichloroethene 0.029 mg/l 0.0025 1.7 5.0 01/13/06 05:02 PPM 156-59-2 trans-1.2-Dichloroethene ND mg/l 0.0025 0.90 5.0 01/13/06 05:02 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.0025 2.2 5.0 01/13/06 05:02 PPM 78-87.5 1,3-Dichloropropane ND mg/l 0.0025 1.4 5.0 01/13/06 05:02 PPM 142.28-9 2.2-Dichloropropane ND mg/l 0.0025 2.3 5.0 01/13/06 05:02 PPM 594.20-7 1,1-Dichloropropene ND mg/l 0.0025 1.8 5.0 01/13/06 05:02 PPM 563.58-6 cis-1.3-Dichloropropene ND mg/l 0.0025 1.4 5.0 01/13/06 05:02 PPM 10061.01-5 trans-1,3-Dichloropropene ND mg/l 0.0025 1.5 5.0 01/13/06 05:02 PPM 10061.02-6 Diisopropyl ether ND mg/l 0.0025 1.2 5.0 01/13/06 05:02 PPM 108-20-3 Ethylbenzene ND mg/l 0.0025 0.65 5.0 01/13/06 05:02 PPM 100.41-4 Date: 01/23/06 Page: 17 of 36 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri eiri nn r0-7cno REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. % np-hrt Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 aceAnalytical ° www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519083 Project Sample Number: 92110924.009 Date Collected: 01/05/06 15:45 Client Sample ID: MW-10 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.010 4.1 5.0 01/13/06 05:02 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0025 0.75 5.0 01/13/06 05:02 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0050 1.2 5.0 01/13/06 05:02 PPM 99-87-6 Methylene chloride ND mg/l 0.010 5.2 5.0 01/13/06 05:02 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0025 1.0 5.0 01/13/06 05:02 PPM 1634-04-4 Naphthalene ND mg/l 0.010 8.4 5.0 01/13/06 05:02 PPM 91-20-3 n-Propylbenzene ND mg/l 0.0025 0.90 5.0 01/13/06 05:02 PPM 103-65-1 Styrene ND mg/l 0.0025 0.60 5.0 01/13/06 05:02 PPM 100-42-5 1,1,1.2-Tetrachloroethane ND mg/l 0.0025 1.9 5.0 01/13/06 05:02 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.0025 1.5 5.0 01/13/06 05:02 PPM 79-34-5 Tetrachloroethene 0.18 mg/l 0.0025 1.9 5.0 01/13/06 05:02 PPM 127-18-4 Toluene ND mg/l 0.0025 0.90 5.0 01/13/06 05:02 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.010 5.3 5.0 01/13/06 05:02 PPM 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.010 4.4 5.0 01/13/06 05:02 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.0025 2.2 5.0 01/13/06 05:02 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.0025 1.5 5.0 01/13/06 05:02 PPM 79-00-5 Trichloroethene 0.015 mg/l 0.0025 0.60 5.0 01/13/06 05:02 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0025 0.50 5.0 01/13/06 05:02 PPM 75-69.4 1,2.3-Trichloropropane ND mg/l 0.0025 1.9 5.0 01/13/06 05:02 PPM 96.18.4 1,2,4-Trimethylbenzene ND mg/l 0.0025 1.4 5.0 01/13/06 05:02 PPM 95-63.6 1,3,5-Trimethylbenzene ND mg/l 0.0025 2.2 5.0 01/13/06 05:02 PPM 108-67-8 Vinyl chloride ND mg/l 0.0025 1.1 5.0 01/13/06 05:02 PPM 75-01-4 m&p-Xylene ND mg/l 0.0025 1.1 5.0 01/13/06 05:02 PPM o-Xylene ND mg/l 0.0025 5.0 01/13/06 05:02 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 101 X 1.0 01/13/06 05:02 PPM 625-98-9 Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI KICI AD Cp7CAQ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. nelac4 Page: 18 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 ace Analytical ° www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519091 Project Sample Number: 92110924.010 Date Collected: 01/05/06 14:17 Client Sample ID: MW-11 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0050 1.3 10.0 01/13/06 05:44 PPM 71-43-2 Bromobenzene ND mg/l 0.0050 3.4 10.0 01/13/06 05:44 PPM 108-86-1 Bromochloromethane ND mg/l 0.0050 4.1 10.0 01/13/06 05:44 PPM 74.97-5 Bromodichloromethane ND mg/l 0.0050 3.3 10.0 01/13/06 05:44 PPM 75-27-4 Bromoform ND mg/l 0.0050 5.0 10.0 01/13/06 05:44 PPM 75-25-2 Bromomethane ND mg/l 0.0050 3.6 10.0 01/13/06 05:44 PPM 74-83-9 n-Butylbenzene ND mg/l 0.010 2.8 10.0 01/13/06 05:44 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.0050 4.5 10.0 01/13/06 05:44 PPM 135-98-8 tert-Butylbenzene ND mg/l 0.0050 4.1 10.0 01/13/06 05:44 PPM 98-06-6 Carbon tetrachloride ND mg/l 0.0050 3.3 10.0 01/13/06 05:44 PPM 56-23-5 Chlorobenzene ND mg/l 0.0050 2.4 10.0 01/13/06 05:44 PPM 108-90-7 Chloroethane ND mg/l 0.0050 4.2 10.0 01/13/06 05:44 PPM 75-00-3 Chloroform ND mg/l 0.0050 3.1 10.0 01/13/06 05:44 PPM 67-66-3 Chloromethane ND mg/l 0.020 3.0 10.0 01/13/06 05:44 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.0050 3.4 10.0 01/13/06 05:44 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.0050 3.2 10.0 01/13/06 05:44 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.020 9.5 10.0 01/13/06 05:44 PPM 96-12-8 Dibromochloromethane ND mg/l 0.0050 2.9 10.0 01/13/06 05:44 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.0050 5.0 10.0 01/13/06 05:44 PPM 106.93-4 Dibromomethane ND mg/l 0.0050 2.9 10.0 01/13/06 05:44 PPM 74.95-3 1,2-Dichlorobenzene ND mg/l 0.010 2.3 10.0 01/13/06 05:44 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.010 4.6 10.0 01/13/06 05:44 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.010 4.3 10.0 01/13/06 05:44 PPM 106.46-7 Dichlorodifluoromethane ND mg/l 0.0050 1.8 10.0 01/13/06 05:44 PPM 75.71-8 1,1-Dichloroethane ND mg/l 0.0050 4.8 10.0 01/13/06 05:44 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0,0050 2.5 10.0 01/13/06 05:44 PPM 107.06-2 1,1-Dichloroethene ND mg/l 0.0050 4.7 10.0 01/13/06 05:44 PPM 75-35-4 cis-1,2-Dichloroethene 0.063 mg/l 0.0050 3.4 10.0 01/13/06 05:44 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.0050 1.8 10.0 01/13/06 05:44 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.0050 4.3 10.0 01/13/06 05:44 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.0050 2.8 10.0 01/13/06 05:44 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.0050 4.6 10.0 01/13/06 05:44 PPM 594.20-7 1,1-Dichloropropene ND mg/l 0.0050 3.5 10.0 01/13/06 05:44 PPM 563.58-6 cis-1,3-Dichloropropene ND mg/l 0.0050 2.9 10.0 01/13/06 05:44 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.0050 3.0 10.0 01/13/06 05:44 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.0050 2.5 10.0 01/13/06 05:44 PPM 108-20-3 Ethylbenzene ND mg/l 0.0050 1.3 10.0 01/13/06 05:44 PPM 100-41-4 Date: 01/23/06 Page: 19 of 36 REPORT OF LABORATORY ANALYSIS Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 N ACOOgo NC Drinking Water 37706 SC Environmental 99030 911 SC 99006 "" ^^,^ �^ a nPlar f FI NFI AP E87627 ace Analytical ° www.pacelahs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875, 9091 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519091 Project Sample Number: 92110924.010 Date Collected: 01/05/06 14:17 Client Sample ID: MW-11 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL OF Analyzed By CAS No. Qual RegLmt Hexachloro-1.3-butadiene ND mg/l 0.020 8.2 10.0 01/13/06 05:44 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0050 1.5 10.0 01/13/06 05:44 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.010 2.5 10.0 01/13/06 05:44 PPM 99-87-6 Methylene chloride ND mg/l 0.020 10. 10.0 01/13/06 05:44 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0050 2.0 10.0 01/13/06 05:44 PPM 1634-04-4 Naphthalene ND mg/l 0.020 17. 10.0 01/13/06 05:44 PPM 91.20-3 n-Propylbenzene ND mg/l 0.0050 1.8 10.0 01/13/06 05:44 PPM 103.65-1 Styrene ND mg/l 0.0050 1.2 10.0 01/13/06 05:44 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.0050 3.8 10.0 01/13/06 05:44 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 05:44 PPM 79-34-5 Tetrachloroethene 0.36 mg/l 0.000 3.8 10.0 01/13/06 05:44 PPM 127-18-4 Toluene ND mg/l 0.0050 1.8 10.0 01/13/06 05:44 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.020 11. 10.0 01/13/06 05:44 PPM 87.61-6 1,2,4-Trichlorobenzene ND mg/l 0.020 8.7 10.0 01/13/06 05:44 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.0050 4.3 10.0 01/13/06 05:44 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 05:44 PPM 79-00-5 Trichloroethene 0.063 mg/l 0.0050 1.2 10.0 01/13/06 05:44 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0050 1.0 10.0 01/13/06 05:44 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0,0050 3.8 10.0 01/13/06 05:44 PPM 96-18-4 1.2,4-Trimethylbenzene ND mg/l 0.0050 2.8 10.0 01/13/06 05:44 PPM 95-63-6 1.3,5-Trimethylbenzene ND mg/l 0.0050 4.4 10.0 01/13/06 05:44 PPM 108-67-8 Vinyl chloride ND mg/l 0.0050 2.2 10.0 01/13/06 05:44 PPM 75-01-4 m&p-Xylene NO mg/l 0.0050 2.2 10.0 01/13/06 05:44 PPM o-Xylene NO mg/l 0.0050 10.0 01/13/06 05:44 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 102 % 1.0 01/13/06 05:44 PPM 625-98-9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ACC, `EO � C 0 nP ar`£ Page: 20 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 Gi nisi AD PUA97 ace Analytical ° www.pacelabs.com Lab Sample No: 926519109 Client Sample ID: MW-13 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042.05-154 Project Sample Number: 92110924-011 Date Collected: 01/05/06 16:03 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.0050 Bromobenzene ND mg/l 0.0050 Bromochloromethane ND mg/l 0.0050 ' Bromodichloromethane ND mg/l 0.0050 Bromoform ND mg/l 0.0050 Bromomethane ND mg/l 0.0050 n-Butylbenzene ND mg/l 0.010 sec-Butylbenzene ND mg/l 0.0050 tert-Butylbenzene ND mg/l 0.0050 Carbon tetrachloride ND mg/l 0.0050 Chlorobenzene ND mg/l 0.0050 Chloroethane ND mg/l 0.0050 Chloroform ND mg/l 0.0050 Chloromethane ND mg/l 0.020 2-Chlorotoluene ND mg/l 0.0050 4-Chlorotoluene ND mg/l 0.0050 1,2-Dibromo-3-chloropropane ND mg/l 0.020 Dibromochloromethane ND mg/l 0.0050 1,2-Dibromoethane (EDB) ND mg/l 0.0050 Dibromomethane ND mg/l 0.0050 1,2-Dichlorobenzene ND mg/l 0.010 1,3-Dichlorobenzene ND mg/l 0.010 1,4-Dichlorobenzene ND mg/l 0.010 Dichlorodifluoromethane ND mg/l 0.0050 1,1-Dichloroethane ND mg/l 0.0050 1,2-Dichloroethane ND mg/l 0.0050 1.1-Dichloroethene ND mg/l 0.0050 cis-1.2-Dichloroethene 0.22 mg/l 0.0050 trans-1,2-Dichloroethene ND mg/l 0.0050 1,2-Dichloropropane ND mg/l 0.0050 1,3-Dichloropropane ND mg/l 0.0050 2,2-Dichloropropane ND mg/l 0.0050 1,1-Dichloropropene ND mg/l 0.0050 cis-1.3-Dichloropropene ND mg/l 0.0050 trans-1,3-Dichloropropene ND mg/l 0.0050 Diisopropyl ether ND mg/l 0.0050 Ethylbenzene ND mg/l 0.0050 Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD C071ZAP MDL DF Analyzed By CAS No. Qual RegLmt 1.3 10.0 01/13/06 06:26 PPM 71-43-2 3.4 10.0 01/13/06 06:26 PPM 108-86-1 4.1 10.0 01/13/06 06:26 PPM 74-97-5 3.3 10.0 01/13/06 06:26 PPM 75-27-4 5.0 10.0 01/13/06 06:26 PPM 75.25-2 3.6 10.0 01/13/06 06:26 PPM 74-83-9 2.8 10.0 01/13/06 06:26 PPM 104-51-8 4.5 10.0 01/13/06 06:26 PPM 135.98-8 4.1 10.0 01/13/06 06:26 PPM 98-06-6 3.3 10.0 01/13/06 06:26 PPM 56-23-5 2.4 10.0 01/13/06 06:26 PPM 108-90-7 4.2 10.0 01/13/06 06:26 PPM 75-00-3 3.1 10.0 01/13/06 06:26 PPM 67-66-3 3.0 10.0 01/13/06 06:26 PPM 74-87-3 3.4 10.0 01/13/06 06:26 PPM 95-49.8 3.2 10.0 01/13/06 06:26 PPM 106-43-4 9.5 10.0 01/13/06 06:26 PPM 96-12-8 2.9 10.0 01/13/06 06:26 PPM 124-48-1 5.0 10.0 01/13/06 06:26 PPM 106-93-4 2.9 10.0 01/13/06 06:26 PPM 74-95-3 2.3 10.0 01/13/06 06:26 PPM 95.50-1 4.6 10.0 01/13/06 06:26 PPM 541-73-1 4.3 10.0 01/13/06 06:26 PPM 106-46-7 1.8 10.0 01/13/06 06:26 PPM 75-71-8 4.8 10.0 01/13/06 06:26 PPM 75.34-3 2.5 10.0 01/13/06 06:26 PPM 107-06-2 4.7 10.0 01/13/06 06:26 PPM 75-35-4 3.4 10.0 01/13/06 06:26 PPM 156-59-2 1.8 10.0 01/13/06 06:26 PPM 156-60-5 4.3 10.0 01/13/06 06:26 PPM 78-87-5 2.8 10.0 01/13/06 06:26 PPM 142.28-9 4.6 10.0 01/13/06 06:26 PPM 594.20-7 3.5 10.0 01/13/06 06:26 PPM 563.58-6 2.9 10.0 01/13/06 06:26 PPM 10061-01-5 3.0 10.0 01/13/06 06:26 PPM 10061-02-6 2.5 10.0 01/13/06 06:26 PPM 108-20-3 1.3 10.0 01/13/06 06:26 PPM 100-41-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. to \M AccoN01 nphr Page: 21 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 A NFI AP F87627 ace Analytical www.pacelabs.com Pace Analytical Services, Inc. 9800 KinceyAvenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519109 Project Sample Number: 92110924-011 Date Collected: 01/05/06 16:03 Client Sample ID: MW-13 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MOIL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.020 8.2 10.0 01/13/06 06:26 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0050 1.5 10.0 01/13/06 06:26 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.010 2.5 10.0 01/13/06 06:26 PPM 99.87-6 Methylene chloride ND mg/l 0.020 10. 10.0 01/13/06 06:26 PPM 75.09-2 Methyl-tert-butyl ether ND mg/l 0.0050 2.0 10.0 01/13/06 06:26 PPM 1634-04-4 Naphthalene ND mg/l 0.020 17. 10.0 01/13/06 06:26 PPM 91.20-3 n-Propylbenzene ND mg/l 0.0050 1.8 10.0 01/13/06 06:26 PPM 103-65-1 Styrene ND mg/l 0.0050 1.2 10.0 01/13/06 06:26 PPM 100-42-5 1,1,1.2-Tetrachloroethane ND mg/l 0.0050 3.8 10.0 01/13/06 06:26 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 06:26 PPM 79.34-5 Tetrachloroethene ND mg/l 0.0050 3.8 10.0 01/13/06 06:26 PPM 127-18-4 Toluene ND mg/l 0.0050 1.8 10.0 01/13/06 06:26 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.020 11. 10.0 01/13/06 06:26 PPM 87.61-6 1.2,4-Trichlorobenzene ND mg/l 0.020 8.7 10.0 01/13/06 06:26 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.0050 4.3 10.0 01/13/06 06:26 PPM 71-55-6 1.1,2-Trichloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 06:26 PPM 79.00-5 Trichloroethene ND mg/l 0.0050 1.2 10.0 01/13/06 06:26 PPM 79.01-6 Trichlorofluoromethane ND mg/l 0.0050 1.0 10.0 01/13/06 06:26 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.0050 3.8 10.0 01/13/06 06:26 PPM 96-18-4 1.2,4-Trimethylbenzene ND mg/l 0.0050 2.8 10.0 01/13/06 06:26 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.0050 4.4 10.0 01/13/06 06:26 PPM 108-67-8 Vinyl chloride ND mg/l 0.0050 2.2 10.0 01/13/06 06:26 PPM 75.01-4 m&p-Xylene ND mg/l 0.0050 2.2 10.0 01/13/06 06:26 PPM o-Xylene ND mg/l 0.0050 10.0 01/13/06 06:26 PPM 95.47-6 1-Chloro-3-fluorobenzene (S) 116 % 1.0 01/13/06 06:26 PPM 625-98-9 Date: 01/23/06 Page: 22 of 36 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 n RICI AD rQ7rAQ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ACCCR nelac4 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 Sc 99006 FL NELAP E876 7 ace Analytical ° www.pacelabs.com Lab Sample No: 926519117 Client Sample ID: DW-17 Parameters GC Volatiles GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane BrQmoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI AICI AD CA7G:AA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 Project Sample Number: 92110924-012 Date Collected: 01/05/06 15:09 Matrix: Water Date Received: 01/06/06 16:40 Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Method: SM 6230D ND mg/l 0.0050 1.3 10.0 01/13/06 09:13 PPM 71-43-2 ND mg/l 0.0050 3.4 10.0 01/13/06 09:13 PPM 108-86-1 ND mg/l 0.0050 4.1 10.0 01/13/06 09:13 PPM 74-97-5 ND mg/l 0.0050 3.3 10.0 01/13/06 09:13 PPM 75-27.4 ND mg/l 0.0050 5.0 10.0 01/13/06 09:13 PPM 75-25.2 ND mg/l 0.0050 3.6 10.0 01/13/06 09:13 PPM 74-83-9 ND mg/l 0.010 2.8 10.0 01/13/06 09:13 PPM 104-51-8 ND mg/l 0.0050 4.5 10.0 01/13/06 09:13 PPM 135-98-8 ND mg/l 0.0050 4.1 10.0 01/13/06 09:13 PPM 98-06.6 ND mg/l 0.0050 3.3 10.0 01/13/06 09:13 PPM 56-23-5 ND mg/l 0.0050 2.4 10.0 01/13/06 09:13 PPM 108-90.7 ND mg/l 0.0050 4.2 10.0 01/13/06 09:13 PPM 75-00-3 ND mg/l 0.0050 3.1 10.0 01/13/06 09:13 PPM 67.66.3 ND mg/l 0.020 3.0 10.0 01/13/06 09:13 PPM 74-87-3 ND mg/l 0.0050 3.4 10.0 01/13/06 09:13 PPM 95-49-8 ND mg/l 0.0050 3.2 10.0 01/13/06 09:13 PPM 106-43-4 ND mg/l 0.020 9.5 10.0 01/13/06 09:13 PPM 96.12-8 ND mg/l 0.0050 2.9 10.0 01/13/06 09:13 PPM 124.48-1 ND mg/l 0.0050 5.0 10.0 01/13/06 09:13 PPM 106-93.4 ND mg/l 0.0050 2.9 10.0 01/13/06 09:13 PPM 74.95.3 ND mg/l 0.010 2.3 10.0 01/13/06 09:13 PPM 95-50-1 ND mg/l 0.010 4.6 10.0 01/13/06 09:13 PPM 541-73-1 ND mg/l 0.010 4.3 10.0 01/13/06 09:13 PPM 106-46-7 ND mg/l 0.0050 1.8 10.0 01/13/06 09:13 PPM 75-71-8 ND mg/1 0.0050 4.8 10.0 01/13/06 09:13 PPM 75-34-3 ND mg/1 0.0050 2.5 10.0 01/13/06 09:13 PPM 107-06-2 ND mg/l 0.0050 4.7 10.0 01/13/06 09:13 PPM 75-35-4 0.40 mg/1 0.0050 3.4 10.0 01/13/06 09:13 PPM 156.59-2 0.014 mg/1 0.0050 1.8 10.0 01/13/06 09:13 PPM 156.60-5 ND mg/l 0.0050 4.3 10.0 01/13/06 09:13 PPM 78-87-5 ND mg/1 0.0050 2.8 10.0 01/13/06 09:13 PPM 142-28-9 ND mg/1 0.0050 4.6 10.0 01/13/06 09:13 PPM 594.20.7 ND mg/l 0.0050 3.5 10.0 01/13/06 09:13 PPM 563-58.6 ND mg/l 0.0050 2.9 10.0 01/13/06 09:13 PPM 10061-01-5 ND mg/1 0.0050 3.0 10.0 01/13/06 09:13 PPM 10061.02-6 ND mg/l 0.0050 2.5 10.0 01/13/06 09:13 PPM 108-20.3 ND mg/l 0.0050 1.3 10.0 01/13/06 09:13 PPM 100-41.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N •CC°A .'neIac 4 Page: 23 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.909 1 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 Lab Sample No: 926519117 Project Sample Number: 92110924-012 Date Collected: 01/05/06 15:09 Client Sample ID: DW-17 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene ND mg/l 0.020 8.2 10.0 01/13/06 09:13 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.0050 1.5 10.0 01/13/06 09:13 PPM 98.82-8 p-Isopropyltoluene ND mg/l 0.010 2.5 10.0 01/13/06 09:13 PPM 99-87-6 Methylene chloride ND mg/l 0.020 10. 10.0 01/13/06 09:13 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.0050 2.0 10.0 01/13/06 09:13 PPM 1634-04-4 Naphthalene ND mg/l 0.020 17. 10.0 01/13/06 09:13 PPM 91-20-3 n-Propylbenzene ND mg/l 0.0050 1.8 10.0 01/13/06 09:13 PPM 103-65-1 Styrene ND mg/l 0.0050 1.2 10.0 01/13/06 09:13 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.0050 3.8 10.0 01/13/06 09:13 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 09:13 PPM 79-34-5 Tetrachloroethene 0.0057 mg/l 0.0050 3.8 10.0 01/13/06 09:13 PPM 127-18-4 Toluene ND mg/l 0.0050 1.8 10.0 01/13/06 09:13 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.020 11. 10.0 01/13/06 09:13 PPM ' 87-61-6 1,2,4-Trichlorobenzene ND mg/l 0.020 8.7 10.0 01/13/06 09:13 PPM 120-82.1 1,1,1-Trichloroethane ND mg/l 0.0050 4.3 10.0 01/13/06 09:13 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.0050 3.0 10.0 01/13/06 09:13 PPM 79-00-5 Trichloroethene 0.043 mg/l 0.0050 1.2 10.0 01/13/06 09:13 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.0050 1.0 10.0 01/13/06 09:13 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.0050 3.8 10.0 01/13/06 09:13 PPM 96.18-4 1,2,4-Trimethylbenzene ND mg/l 0.0050 2.8 10.0 01/13/06 09:13 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.0050 4.4 10.0 01/13/06 09:13 PPM 108-67-8 Vinyl chloride ND mg/l 0.0050 2.2 10.0 01/13/06 09:13 PPM 75-01-4 m&p-Xylene ND mg/l 0.0050 2.2 10.0 01/13/06 09:13 PPM o-Xylene ND mg/l 0.0050 10.0 01/13/06 09:13 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 121 % 1.0 01/13/06 09:13 PPM 625-98-9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIFI AD FA7RAA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. `40 ,N ACCogo �C neIac£- Page: 24 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 ;aneAnalyficale www.pacelabs.com Lab Sample No: 926519125 Client Sample ID: DW-18 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924-013 Date Collected: 01/05/06 11:17 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL GC Volatiles GC VOCs in Water Method: SM 6230D Benzene NO mg/l 0.00050 0.13 Bromobenzene NO mg/l 0.00050 0.34 Bromochloromethane NO mg/l 0.00050 0.41 Bromodichloromethane NO mg/l 0.00050 0.33 Bromoform NO mg/l 0.00050 0.50 Bromomethane NO mg/l 0.00050 0.36 n-Butylbenzene NO mg/l 0.0010 0.28 sec-Butylbenzene NO mg/l 0.00050 0.45 tert-Butylbenzene NO mg/l 0.00050 0.41 Carbon tetrachloride NO mg/l 0.00050 0.33 Chlorobenzene NO mg/l 0.00050 0.24 Chloroethane ND mg/l 0.00050 0.42 Chloroform ND mg/l 0.00050 0.31 Chloromethane ND mg/l 0.0020 0.30 2-Chlorotoluene ND mg/l 0.00050 0.34 4-Chlorotoluene NO mg/l 0.00050 0.32 1,2-Dibromo-3-chloropropane NO mg/l 0.0020 0.95 Dibromochloromethane NO mg/l 0.00050 0.29 1,2-Dibromoethane (EDB) NO mg/l 0.00050 0.50 Dibromomethane NO mg/l 0.00050 0,29 1,2-Dichlorobenzene NO mg/l 0.0010 0.23 1,3-Dichlorobenzene NO mg/1 0.0010 0.46 1,4-Dichlorobenzene NO mg/l 0.0010 0.43 Dichlorodifluoromethane NO mg/l 0.00050 0.18 1,1-Dichloroethane NO mg/l 0.00050 0.48 1,2-Dichloroethane NO mg/l 0.00050 0.25 1,1-Dichloroethene NO mg/l 0.00050 0.47 cis-1,2-Dichloroethene 0.0027 mg/l 0.00050 0.34 trans-1,2-Dichloroethene NO mg/l 0.00050 0.18 1,2-Dichloropropane NO mg/l 0.00050 0.43 1,3-Dichloropropane NO mg/l 0.00050 0.28 2,2-Dichloropropane NO mg/l 0.00050 0.46 1,1-Dichloropropene NO mg/l 0.00050 0.35 cis-1,3-Dichloropropene NO mg/l 0.00050 0.29 trans-1.3-Dichloropropene NO mg/l 0.00050 0.30 Diisopropyl ether NO mg/l 0.00050 0.25 Ethylbenzene NO mg/l 0.00050 0.13 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIFI AP FA7F;Aq OF Analyzed By CAS No. Qual RegLmt 1.0 01/13/06 09:55 PPM 71-43-2 1.0 01/13/06 09:55 PPM 108-86-1 1.0 01/13/06 09:55 PPM 74-97-5 1.0 01/13/06 09:55 PPM 75-27-4 1.0 01/13/06 09:55 PPM 75-25-2 1.0 01/13/06 09:55 PPM 74-83-9 1.0 01/13/06 09:55 PPM 104-51-8 1.0 01/13/06 09:55 PPM 135-98.8 1.0 01/13/06 09:55 PPM 98-06-6 1.0 01/13/06 09:55 PPM 56-23-5 1.0 01/13/06 09:55 PPM 108-90-7 1.0 01/13/06 09:55 PPM 75-00-3 1.0 01/13/06 09:55 PPM 67-66-3 1.0 01/13/06 09:55 PPM 74-87-3 1.0 01/13/06 09:55 PPM 95-49-8 1.0 01/13/06 09:55 PPM 106-43-4 1.0 01/13/06 09:55 PPM 96-12-8 1.0 01/13/06 09:55 PPM 124.48-1 1.0 01/13/06 09:55 PPM 106-93-4 1.0 01/13/06 09:55 PPM 74-95-3 1.0 01/13/06 09:55 PPM 95-50-1 1.0 01/13/06 09:55 PPM 541.73-1 1.0 01/13/06 09:55 PPM 106-46-7 1.0 01/13/06 09:55 PPM 75.71-8 1.0 01/13/06 09:55 PPM 75-34-3 1.0 01/13/06 09:55 PPM 107-06-2 1.0 01/13/06 09:55 PPM 75-35-4 1.0 01/13/06 09:55 PPM 156-59-2 1.0 01/13/06 09:55 PPM 156-60-5 1.0 01/13/06 09:55 PPM 78-87-5 1.0 01/13/06 09:55 PPM 142-28-9 1.0 01/13/06 09:55 PPM 594-20-7 1.0 01/13/06 09:55 PPM 563-58-6 1.0 01/13/06 09:55 PPM 10061-01-5 1.0 01/13/06 09:55 PPM 10061-02-6 1.0 01/13/06 09:55 PPM 108-20-3 1.0 01/13/06 09:55 PPM 100-41-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. tta ,N Acc", nelac£ Page: 25 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FL NELAP E87627 ace Analytical ° www.pacelabs.com Lab Sample No: 926519125 Client Sample ID: DW-18 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Project Sample Number: 92110924-013 Date Collected: 01/05/06 11:17 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MOIL OF Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene NO mg/l 0.0020 0.82 1.0 01/13/06 09:55 PPM 87-68-3 Isopropylbenzene (Cumene) NO mg/l 0.00050 0.15 1.0 01/13/06 09:55 PPM 98.82-8 p-Isopropyltoluene NO mg/l 0.0010 0.25 1.0 01/13/06 09:55 PPM 99.87-6 Methylene chloride NO mg/l 0.0020 1.0 1.0 01/13/06 09:55 PPM 75.09-2 Methyl-tert-butyl ether NO mg/l 0.00050 0.20 1.0 01/13/06 09:55 PPM 1634-04-4 Naphthalene NO mg/l 0.0020 1.7 1.0 01/13/06 09:55 PPM 91-20-3 n-Propylbenzene NO mg/l O.00050 0.18 1.0 01/13/06 09:55 PPM 103-65-1 Styrene NO mg/l 0.00050 0.12 1.0 01/13/06 09:55 PPM 100-42-5 1,1.1.2-Tetrachloroethane NO mg/l 0.00050 0.38 1.0 01/13/06 09:55 PPM 630-20-6 1,1,2,2-Tetrachloroethane NO mg/l 0.00050 0.30 1.0 01/13/06 09:55 PPM 79-34-5 Tetrachloroethene 0.11 mg/l 0.0025 1.9 5.0 01/13/06 09:55 PPM 127-18-4 Toluene NO mg/l 0.00050 0.18 1.0 01/13/06 09:55 PPM 108-88-3 1,2,3-Trichlorobenzene NO mg/l 0.0020 1.1 1.0 01/13/06 09:55 PPM ' 87-61-6 1,2,4-Trichlorobenzene NO mg/l 0.0020 0.87 1.0 01/13/06 09:55 PPM 120-82-1 1,1,1-Trichloroethane NO mg/l 0.00050 0.43 1.0 01/13/06 09:55 PPM 71-55-6 1,1,2-Trichloroethane NO mg/l 0.00050 0.30 1.0 01/13/06 09:55 PPM 79.00-5 Trichloroethene 0.016 mg/l 0.00050 0.12 1.0 01/13/06 09:55 PPM 79-01-6 Trichlorofluoromethane NO mg/l 0.00050 0.10 1.0 01/13/06 09:55 PPM 75-69-4 1,2,3-Trichloropropane NO mg/l O.00050 0.38 1.0 01/13/06 09:55 PPM 96-18-4 1,2,4-Trimethylbenzene 0.00059 mg/l O.00050 0.28 1.0 01/13/06 09:55 PPM 95-63-6 1,3,5-Trimethylbenzene NO mg/l 0.00050 0.44 1.0 01/13/06 09:55 PPM 108.67-8 Vinyl chloride NO mg/l 0.00050 0.22 1.0 01/13/06 09:55 PPM 75.01-4 m&p-Xylene NO mg/l 0.00050 0.22 1.0 01/13/06 09:55 PPM o-Xylene NO mg/l 0.00050 1.0 01/13/06 09:55 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 125 % 1.0 01/13/06 09:55 PPM 625-98-9 Date: 01/23/06 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Drinking Water 37712 0 ncco,n- "yf SC Environmental 99030 rl nlrl An C07CAO nQlaC Page: 26 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 PI AIFI AP FR707 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical o Huntersville, NC 28078 www.pacelabs.com Phone: 704.875.9092 Lab Project Number: 92110924 Fax: 704.875.9091 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519133 Project Sample Number: 92110924-014 Date Collected: 01/05/06 12:45 Client Sample ID: DW-19 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units _Report Limit MDL DF Analyzed By CAS No. Qual RegLmt GC Volatiles GC VOCs in Water Method: SM 6230D Benzene ND mg/l 0.00050 0.13 1.0 01/13/06 10:37 PPM 71.43.2 Bromobenzene ND mg/l 0.00050 0.34 1.0 01/13/06 10:37 PPM 108-86-1 Bromochloromethane ND mg/l 0.00050 0.41 1.0 01/13/06 10:37 PPM 74-97-5 Bromodichloromethane ND mg/l 0.00050 0.33 1.0 01/13/06 10:37 PPM 75.27.4 Bromoform ND mg/l 0.00050 0.50 1.0 01/13/06 10:37 PPM 75.25.2 Bromomethane ND mg/l 0.00050 0.36 1.0 01/13/06 10:37 PPM 74.83.9 n-Butylbenzene ND mg/l 0.0010 0.28 1.0 01/13/06 10:37 PPM 104-51-8 sec-Butylbenzene ND mg/l 0.00050 0.45 1.0 01/13/06 10:37 PPM 135-98.8 tert-Butylbenzene ND mg/l 0.00050 0.41 1.0 01/13/06 10:37 PPM 98-06.6 Carbon tetrachloride ND mg/l 0.00050 0.33 1.0 01/13/06 10:37 PPM 56-23.5 Chlorobenzene ND mg/l 0.00050 0.24 1.0 01/13/06 10:37 PPM 108-90-7 Chloroethane ND mg/l 0.00050 0.42 1.0 01/13/06 10:37 PPM 75-00-3 Chloroform ND mg/l 0.00050 0.31 1.0 01/13/06 10:37 PPM 67-66-3 Chloromethane ND mg/l 0.0020 0.30 1.0 01/13/06 10:37 PPM 74-87-3 2-Chlorotoluene ND mg/l 0.00050 0.34 1.0 01/13/06 10:37 PPM 95-49-8 4-Chlorotoluene ND mg/l 0.00050 0.32 1.0 01/13/06 10:37 PPM 106-43-4 1,2-Dibromo-3-chloropropane ND mg/l 0.0020 0.95 1.0 01/13/06 10:37 PPM 96-12-8 Dibromochloromethane ND mg/l 0.00050 0.29 1.0 01/13/06 10:37 PPM 124-48-1 1,2-Dibromoethane (EDB) ND mg/l 0.00050 0.50 1.0 01/13/06 10:37 PPM 106-93-4 Dibromomethane ND mg/l 0.00050 0.29 1.0 01/13/06 10:37 PPM 74-95-3 1,2-Dichlorobenzene ND mg/l 0.0010 0.23 1.0 01/13/06 10:37 PPM 95-50-1 1,3-Dichlorobenzene ND mg/l 0.0010 0.46 1.0 01/13/06 10:37 PPM 541-73-1 1,4-Dichlorobenzene ND mg/l 0.0010 0.43 1.0 01/13/06 10:37 PPM 106-46-7 Dichlorodifluoromethane ND mg/l 0.00050 0.18 1.0 01/13/06 10:37 PPM 75-71-8 1,1-Dichloroethane ND mg/l 0.00050 0.48 1.0 01/13/06 10:37 PPM 75-34-3 1,2-Dichloroethane ND mg/l 0.00050 0.25 1.0 01/13/06 10:37 PPM 107-06-2 1,1-Dichloroethene ND mg/l 0.00050 0.47 1.0 01/13/06 10:37 PPM 75-35-4 cis-1,2-Dichloroethene 0.0012 mg/l 0.00050 0.34 1.0 01/13/06 10:37 PPM 156-59-2 trans-1,2-Dichloroethene ND mg/l 0.00050 0.18 1.0 01/13/06 10:37 PPM 156-60-5 1,2-Dichloropropane ND mg/l 0.00050 0.43 1.0 01/13/06 10:37 PPM 78-87-5 1,3-Dichloropropane ND mg/l 0.00050 0.28 1.0 01/13/06 10:37 PPM 142-28-9 2,2-Dichloropropane ND mg/l 0.00050 0.46 1.0 01/13/06 10:37 PPM 594-20-7 1,1-Dichloropropene ND mg/l 0.00050 0.35 1.0 01/13/06 10:37 PPM 563-58-6 cis-1,3-Dichloropropene ND mg/l 0.00050 0.29 1.0 01/13/06 10:37 PPM 10061-01-5 trans-1,3-Dichloropropene ND mg/l 0.00050 0.30 1.0 01/13/06 10:37 PPM 10061-02-6 Diisopropyl ether ND mg/l 0.00050 0.25 1.0 01/13/06 10:37 PPM 108-20-3 Ethylbenzene ND mg/l 0.00050 0.13 1.0 01/13/06 10:37 PPM 100-41-4 Date: 01/23/06 Page: 27 of 36 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI An C07CAO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 4to M.4C�pgo� Nf np.hr Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 rl KIFI AP rUr,97 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical o Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Lab Sample No: 926519133 Project Sample Number: 92110924-014 Date Collected: 01/05/06 12:45 Client Sample ID: DW-19 Matrix: Water Date Received: 01/06/06 16:40 Parameters Results Units Report Limit MDL DF Analyzed By CAS No. Qual RegLmt Hexachloro-1.3-butadiene ND mg/l 0.0020 0.82 1.0 01/13/06 10:37 PPM 87-68-3 Isopropylbenzene (Cumene) ND mg/l 0.00050 0.15 1.0 01/13/06 10:37 PPM 98-82-8 p-Isopropyltoluene ND mg/l 0.0010 0.25 1.0 01/13/06 10:37 PPM 99-87.6 Methylene chloride ND mg/l 0.0020 1.0 1.0 01/13/06 10:37 PPM 75-09-2 Methyl-tert-butyl ether ND mg/l 0.00050 0.20 1.0 01/13/06 10:37 PPM 1634-04-4 Naphthalene ND mg/l 0.0020 1.7 1.0 01/13/06 10:37 PPM 91-20-3 n-Propylbenzene ND mg/l 0.00050 0.18 1.0 01/13/06 10:37 PPM 103-65-1 Styrene ND mg/l 0.00050 0.12 1.0 01/13/06 10:37 PPM 100-42-5 1,1,1,2-Tetrachloroethane ND mg/l 0.00050 0.38 1.0 01/13/06 10:37 PPM 630-20-6 1,1,2,2-Tetrachloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 10:37 PPM 79-34-5 Tetrachloroethene 0.10 mg/l 0.0025 1.9 5.0 01/13/06 10:37 PPM 127-18-4 Toluene ND mg/l 0.00050 0.18 1.0 01/13/06 10:37 PPM 108-88-3 1,2,3-Trichlorobenzene ND mg/l 0.0020 1.1 1.0 01/13/06 10:37 PPM 87-61-6 , 1,2,4-Trichlorobenzene ND mg/l 0.0020 0.87 1.0 01/13/06 10:37 PPM 120-82-1 1,1,1-Trichloroethane ND mg/l 0.00050 0.43 1.0 01/13/06 10:37 PPM 71-55-6 1,1,2-Trichloroethane ND mg/l 0.00050 0.30 1.0 01/13/06 10:37 PPM 79-00.5 Trichloroethene 0.0031 mg/l 0.00050 0.12 1.0 01/13/06 10:37 PPM 79-01-6 Trichlorofluoromethane ND mg/l 0.00050 0.10 1.0 01/13/06 10:37 PPM 75-69-4 1,2,3-Trichloropropane ND mg/l 0.00050 0.38 1.0 01/13/06 10:37 PPM 96-18-4 1.2,4-Trimethylbenzene 0.00065 mg/l 0.00050 0.28 1.0 01/13/06 10:37 PPM 95-63-6 1,3,5-Trimethylbenzene ND mg/l 0.00050 0.44 1.0 01/13/06 10:37 PPM 108.67-8 Vinyl chloride ND mg/l 0.00050 0.22 1.0 01/13/06 10:37 PPM 75-01-4 m&p-Xylene ND mg/l 0.00050 0.22 1.0 01/13/06 10:37 PPM o-Xylene ND mg/l 0.00050 1.0 01/13/06 10:37 PPM 95-47-6 1-Chloro-3-fluorobenzene (S) 111 % 1.0 01/13/06 10:37 PPM 625-98-9 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri RIPI AP PA7AAA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ♦CCOF C �¢ nelac Page: 28 of 36 Charlotte Certification IN NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 ace Analytical ° www.pacelabs.com PARAMETER FOOTNOTES Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes in sample preparation, dilution of the extract, or moisture content Method 9071E modified to use ASE. All pH. Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate hold time. Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis. 2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid. ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit (S) Surrogate Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl 111r1 An r07CA0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N ACCpq •C °nPlac4 Page: 29 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 Analytical ° www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 QC Batch: 146981 Analysis Method: SM 6230D QC Batch Method: SM 6230D Analysis Description: GC VOCs in Water Associated Lab Samples: 926519000 926519018 926519026 926519034 926519042 926519059 926519067 926519075 926519083 926519091 926519109 926519117 926519125 926519133 METHOD BLANK: 926527722 Associated Lab Samples: 926519000 926519018 926519026 926519034 926519042 926519059 926519067 926519075 926519083 926519091 926519109 926519117 926519125 926519133 Blank Parameter Units Result Benzene ug/l NO Bromobenzene ug/l NO Bromochloromethane ug/l NO Bromodichloromethane ug/l NO Bromoform ug/l NO Bromomethane ug/l NO n-Butylbenzene ug/l NO sec-Butylbenzene ug/l NO tert-Butylbenzene ug/l NO Carbon tetrachloride ug/l NO Chlorobenzene ug/l NO Chloroethane ug/l NO Chloroform ug/l NO Chloromethane ug/l NO 2-Chlorotoluene ug/l NO 4-Chlorotoluene ug/l NO 1,2-Dibromo-3-chloropropane ug/l NO Dibromochloromethane ug/l NO 1,2-Dibromoethane (EDB) ug/l NO Dibromomethane ug/l NO 1,2-Dichlorobenzene ug/l NO 1,3-Dichlorobenzene ug/l NO 1,4-Dichlorobenzene ug/l NO Dichlorodifluoromethane ug/l NO 1,1-Dichloroethane ug/l NO 1,2-Dichloroethane ug/l NO 1,1-Dichloroethene ug/l NO cis-1,2-Dichloroethene ug/l NO Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 rl KIM An r07CA0 Reporting Limit Footnotes 0.50 0.50 0.50 0.50 0.50 0.50 1.0 0.50 0.50 0.50 0.50 0.50 0.50 2.0 0.50 0.50 2.0 0.50 0.50 0.50 1.0 1.0 1.0 0.50 0.50 0.50 0.50 0.50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M ACC, `t0 � °nPlalr Page: 30 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NIFI AP FR7ri97 Analytical ° www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 METHOD BLANK: 926527722 Associated Lab Samples: 926519000 926519018 926519026 926519034 926519042 926519059 926519067 926519075 926519083 926519091 926519109 926519117 926519125 926519133 Blank Reporting Parameter Units Result Limit Footnotes trans-1,2-Dichloroethene ug/l NO 0.50 1,2-Dichloropropane ug/l ND 0.50 1,3-Dichloropropane ug/l ND 0.50 2,2-Dichloropropane ug/l NO 0.50 1,1-Dichloropropene ug/l NO 0.50 cis-1.3-Dichloropropene ug/l NO 0.50 trans-1,3-Dichloropropene ug/l ND 0.50 Diisopropyl ether ug/l ND 0.50 Ethylbenzene ug/l NO 0.50 Hexachloro-1,3-butadiene ug/l NO 2.0 Isopropylbenzene (Cumene) ug/l NO 0.50 p-Isopropyltoluene ug/l NO 1.0 Methylene chloride ug/l ND 2.0 Methyl-tert-butyl ether ug/l ND 0.50 Naphthalene ug/l ND 2.0 n-Propylbenzene ug/l NO 0.50 Styrene ug/l NO 0.50 1,1,1,2-Tetrachloroethane ug/l NO 0.50 1,1,2,2-Tetrachloroethane ug/l NO 0.50 Tetrachloroethene ug/l NO 0.50 Toluene ug/l NO 0.50 1,2,3-Trichlorobenzene ug/l NO 2.0 1,2,4-Trichlorobenzene ug/l NO 2.0 1,1,1-Trichloroethane ug/l NO 0.50 1,1,2-Trichloroethane ug/l NO 0.50 Trichloroethene ug/l ND 0.50 Trichlorofluoromethane ug/l ND 0.50 1,2,3-Trichloropropane ug/l NO 0.50 1.2,4-Trimethylbenzene ug/l NO 0.50 1,3,5-Trimethylbenzene ug/l NO 0.50 Vinyl chloride ug/l NO 0.50 m&p-Xylene ug/l ND 0.50 o-Xylene ug/l ND 0.50 1-Chloro-3-fluorobenzene (S) % 122 Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI r,ICI AD 1:R79AR REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. N Acc", `�O � C p nelac4 Page: 31 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP PR7697 ;aneAnalyfical') www.pacelabs.com QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: 926527730 926527748 Parameter Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri niri nn [071240 Spike LCS Units Conc. Result ug/l 20.00 20.88 ug/l 20.00 21.92 ug/l 20.00 23.45 ug/l 20.00 20.01 ug/l 20.00 21.80 ug/l 20.00 21.39 ug/l 20.00 21.52 ug/l 20.00 19.93 ug/l 20.00 19.99 ug/l 20.00 21.76 ug/l 20.00 21.81 ug/l 20.00 22.82 ug/l 20.00 23.62 ug/l 20.00 20.98 ug/l 20.00 22.04 ug/l 20.00 20.27 ug/l 20.00 22.40 ug/l 20.00 20.30 ug/l 20.00 22.38 ug/l 20.00 21.31 ug/l 20.00 21.04 ug/l 20.00 23.05 ug/l 20.00 20.76 ug/l 20.00 19.69 ug/l 20.00 21.88 ug/l 20.00 19.18 ug/l 20.00 21.43 ug/l 20.00 22.93 ug/l 20.00 20.78 ug/l 20.00 18.66 ug/l 20.00 19.45 ug/l 20.00 20.09 ug/l 20.00 19.13 ug/l 20.00 18.63 ug/l 20.00 19.02 ug/l 20.00 19.85 ug/l 20.00 21.57 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 LCSD LCS LCSD % Rec Max Result % Rec % Rec Limits RPD RPD Footnotes 20.63 104 103 60.140 1 30 21.78 110 109 60.140 1 30 23.08 117 115 60-140 2 30 20.30 100 102 60-140 1 30 21.51 109 108 60-140 1 30 20.57 107 103 60.140 4 30 21.23 108 106 60-140 1 30 19.83 100 99 60-140 1 30 19.88 100 99 60-140 1 30 21.66 109 108 60-140 0 30 21.03 109 105 60-140 4 30 21.67 114 108 60-140 5 30 24.23 118 121 60-140 3 30 20.80 105 104 60-140 1 30 21.32 110 107 60-140 3 30 19.61 101 98 60-140 3 30 22.72 112 114 60-140 1 30 20.35 102 102 60.140 0 30 22.42 112 112 60.140 0 30 20.76 107 104 60.140 3 30 20.96 105 105 60.140 0 30 22.36 115 112 60.140 3 30 20.59 104 103 60.140 1 30 19.28 98 96 60-140 2 30 21.27 109 106 60.140 3 30 19.09 96 95 60.140 1 30 19.77 107 99 60.140 8 30 19.20 115 96 60.140 18 30 20.02 104 100 60.140 4 30 19.16 93 96 60.140 3 30 19.09 97 95 60.140 2 30 18.09 100 90 60-140 10 30 18.88 96 94 60.140 1 30 18.45 93 92 60-140 1 30 19.14 95 96 60-140 1 30 19.51 99 98 60-140 2 30 21.47 108 107 60-140 0 30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 40 N RCCOF09 C v°nelacfi Page: 32 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP E87627 Analytical ° www.pacelabs.com QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: 926527730 926527748 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result X Rec % Rec Limits RPD RPD Hexachloro-1,3-butadiene ug/l 20.00 20.35 19.49 102 98 60-140 4 30 Isopropylbenzene (Cumene) ug/l 20.00 20.64 20.47 103 102 60.140 1 30 p-Isopropyltoluene ug/l 20.00 20.35 20.97 102 105 60.140 3 30 Methylene chloride ug/l 20.00 24.59 22.88 123 114 60-140 7 30 Methyl-tert-butyl ether ug/l 20.00 19.55 19.40 98 97 60-140 1 30 Naphthalene ug/l 20.00 20.91 19.55 105 98 60-140 7 30 n-Propylbenzene ug/l 20.00 20.67 20.49 103 102 60-140 1 30 Styrene ug/l 20.00 19.39 19.25 97 96 60.140 1 30 1,1,1,2-Tetrachloroethane ug/l 20.00 20.73 20.04 104 100 60.140 3 30 1,1,2,2-Tetrachloroethane ug/l 20.00 20.15 20.45 101 102 60.140 1 30 Tetrachloroethene ug/l 20.00 22.99 22.56 115 113 60-140 2 30 Toluene ug/l 20.00 21.12 20.88 106 104 60-140 1 30 1.2,3-Trichlorobenzene ug/l 20.00 21.06 20.28 105 101 60-140 4 30 1,2,4-Trichlorobenzene ug/l 20.00 20.68 19.49 103 97 60-140 6 30 1.1,1-Trichloroethane ug/l 20.00 21.07 20.76 105 104 60.140 1 30 1,1,2-Trichloroethane ug/l 20.00 20.02 20.02 100 100 60-140 0 30 Trichloroethene ug/l 20.00 23.22 23.10 116 116 60-140 1 30 Trichlorofluoromethane ug/l 20.00 20.97 19.68 105 98 60-140 6 30 1,2,3-Trichloropropane ug/l 20.00 20.38 19.67 102 98 60-140 4 30 1,2,4-Trimethylbenzene ug/l 20.00 19.90 19.73 100 99 60-140 1 30 1,3.5-Trimethylbenzene ug/l 20.00 19.64 19.52 98 98 60-140 1 30 Vinyl chloride ug/l 20.00 21.79 21.63 109 108 60-140 1 30 m&p-Xylene ug/l 40.00 42.53 42.26 106 106 60-140 1 30 o-Xylene ug/l 20.00 19.63 19.47 98 97 60-140 1 30 1-Chloro-3-fluorobenzene (S) 111 109 67-138 SAMPLE DUPLICATE: 926527755 926524794 Parameter Units Result Benzene mg/l NO Bromobenzene mg/l NO Bromochloromethane mg/l NO Bromodichloromethane mg/l NO Bromoform mg/l NO Bromomethane mg/l NO Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI AICI AD CQ7GAA DUP Max Result RPD RPD Footnotes NO NC 30 NO NC 30 NO NC 30 NO NC 30 NO NC 30 NO NC 30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. .N AccoN .9 c .�nehc f Footnotes Page: 33 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NFI AP F87627 Analytical ° www.pacelabs.com QUALITY CONTROL DATA SAMPLE DUPLICATE: 926527755 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05-154 926524794 DUP Max Parameter Units Result Result RPD RPD n-Butylbenzene mg/l ND ND NC 30 sec-Butylbenzene mg/l ND ND NC 30 tert-Butylbenzene mg/l ND ND NC 30 Carbon tetrachloride mg/l ND ND NC 30 Chlorobenzene mg/l ND ND NC 30 Chloroethane mg/l ND ND NC 30 Chloroform mg/l ND ND NC 30 Chloromethane mg/l ND ND NC 30 2-Chlorotoluene mg/l ND ND NC 30 4-Chlorotoluene mg/l ND ND NC 30 1,2-Dibromo-3-chloropropane mg/l ND ND NC 30 Dibromochloromethane mg/l ND ND NC 30 1,2-Dibromoethane (EDB) mg/l ND ND NC 30 Dibromomethane mg/l ND ND NC 30 1,2-Dichlorobenzene mg/l ND ND NC 30 1,3-Dichlorobenzene mg/l ND ND NC 30 1,4-Dichlorobenzene mg/l ND ND NC 30 Dichlorodifluoromethane mg/l ND ND NC 30 1,1-Dichloroethane mg/l ND ND NC 30 1,2-Dichloroethane mg/l ND ND NC 30 1,1-Dichloroethene mg/l ND ND NC 30 cis-1,2-Dichloroethene mg/l ND ND NC 30 trans-1,2-Dichloroethene mg/l ND ND NC 30 1,2-Dichloropropane mg/l ND ND NC 30 1,3-Dichloropropane mg/l ND ND NC 30 2,2-Dichloropropane mg/l ND ND NC 30 1,1-Dichloropropene mg/l ND ND NC 30 cis-1,3-Dichloropropene mg/l ND ND NC 30 trans-1,3-Dichloropropene mg/l ND ND NC 30 Diisopropyl ether mg/l ND ND NC 30 Ethylbenzene mg/l ND ND NC 30 Hexachloro-1,3-butadiene mg/l ND ND NC 30 Isopropylbenzene (Cumene) mg/l ND ND NC 30 p-Isopropyltoluene mg/l ND ND NC 30 Methylene chloride mg/l ND ND NC 30 Methyl-tert-butyl ether mg/l ND ND NC 30 Naphthalene mg/l ND ND NC 30 Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 FI KIGI AP 1:A7RAA Footnotes REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,M CCOHD4 °nelac 4 Page: 34 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI NIFI AP F87627 ace Analytical ° www.pacelabs.com SAMPLE DUPLICATE: 926527755 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042.05-154 926524794 DUP Max Parameter Units Result Result RPD RPD n-Propylbenzene mg/l NO NO NC 30 Styrene mg/l NO NO NC 30 1,1,1,2-Tetrachloroethane mg/l NO NO NC 30 1,1,2,2-Tetrachloroethane mg/l NO NO NC 30 Tetrachloroethene mg/l NO NO NC 30 Toluene mg/l NO NO NC 30 1,2,3-Trichlorobenzene mg/l NO ND NC 30 1,2,4-Trichlorobenzene mg/l NO NO NC 30 1,1,1-Trichloroethane mg/l NO ND NC 30 1.1,2-Trichloroethane mg/l NO NO NC 30 Trichloroethene mg/l NO NO NC 30 Trichlorofluoromethane mg/l NO NO NC 30 1,2,3-Trichloropropane mg/l NO NO NC 30 1,2,4-Trimethylbenzene mg/l NO ND NC 30 1,3,5-Trimethylbenzene mg/l NO NO NC 30 Vinyl chloride mg/l NO NO NC 30 m&p-Xylene mg/l ND NO NC 30 o-Xylene mg/l ND NO NC 30 1-Chloro-3-fluorobenzene (S) % 109 117 Date: 01/23/06 Asheville Certification IDs NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 CI RICI AD CG7RAC Footnotes REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ,M ACCogo `40 � C °nPhIr Page: 35 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 FI KIP AP FA707 Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Analytical Huntersville, NC 28078 Phone: 704.875.9092 www.pacelabs.com Fax: 704.875.9091 Lab Project Number: 92110924 Client Project ID: Fairchild/042-05.154 QUALITY CONTROL DATA PARAMETER FOOTNOTES Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate % Rec and RPD values. LCS(D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) DUP Sample Duplicate ND Not detected at or above adjusted reporting limit NC Not Calculable J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit MDL Adjusted Method Detection Limit RPD Relative Percent Difference (S) Surrogate Date: 01/23/06 Asheville Certification IN NC Wastewater 40 NC Drinking Water 37712 SC Environmental 99030 ri ■ori nn rn-pAn REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. W �Cc"' EO �C ' nPln Page: 36 of 36 Charlotte Certification IDs NC Wastewater 12 NC Drinking Water 37706 SC 99006 GI RIM AD PVA97 fR Pac,paIyticl A Section A ' Required Client Information: Section B Required Project Information CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Page: of" 00 Company _ T�: L_ �,�q�iJ/� � -- Report T r' 1.r:5 Ciu Attention: ❑ NPDES GROUNDWATER ❑DRINKING WATEF Address V Copy To: Company Name_ ❑ UST ❑ RCRA F] Other Address: ❑GA ❑IL ❑IN El MI ❑MN kNC Email To: Purchase Order No.: Pace Quote Reference: ❑OH ❑SC ❑ WI ❑OTHER Phnina (�P Project Name: Fps, ;CI 11 0,( Pace Project Manager: Filtered (YIN) Requested Due Date/TA Project Number: . ` 1 -�' Pace Profile #: `[ 1 lu 5 Requested GCC pr�� fti=rtr.!ircciClleni Inftjimation Valid Matrix Codes MATRI_Y, CODE 0 Preservatives Analysis: = DRINKING WATER WATER DW w w p WF a0 a. z 22 ` �i e� 5 A M r��_',� �. E ID WASTE WATER OL/DUCT WW P v '_� w COLLECTED w U J J LL Z o oC ' One i.halartP.l per box. A SOISOLID OIL SL OL m �4 OJ Z > rn — ;� / �`� z t'r (A /-' a 9 / '� HIRE AR in 11 COMPOSITE START COMPOSITE ENDIGRAB y F ¢ o O� _ y� Pace Project Numt Samples Ills fAUS'i [3E UIVIQLIC OTHER TISSUE OT TS O DATE TIME DATE TIME c N Z U m w D 2 2 S z z 2 t 0 Q° Lab W 1441 1+ � x x � x x f3 w 1 • a • .ACCEPTED BY/ AFFILIAI • • SAMPLE CONDITION Additional Comments: n 21> > i z z z j- } j- z Z z } i i z i z } z } U o 1 o ° PPRINTNameFafSAPPLERI= htI _J. a /..J fJ. �. 1 �i/l/ �P 6�1 M P-I ?I MCI • Requited ulium Section B CHAIN -OF -CUSTODY / Analytical Request ®®current The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C ';, 4 '�: rnation: Page: •2 of el 8.0FU Now'", ".REGULATORY AGrENGY Address .. • I-Oc tiow- JAg • •r�- i •. • . r—` R;q—�.sted Due Date/TAT: ...� Sectionr .. VVT �WE A D :STWATE- WATER Ww -SOIL/SOLIDCT . One Ch-iar.lqi per box, OIL OL AIR AR Pace Project Numl TISSUE TS®�® Lab ■ ■■■■■■■■ �[�11 _ "�1111=©■■■■ 1111 111111111. i# ■■■■■■ ■■mmmm■ 111111111111111111111 0 ■■ ■■■■■■■■■ ■■����■ ■■■■■■■■■ ■■■■■■■■■:■ DATE TIME , ACCEPTED BY / AFFILIATIONS DATE TIIVI�SAMPLECONDITION • RELINQUISHED `BY / AFFILIATION 5AMPLER,JdQME:AND SIGNATURE •� I i) 7. �` MEMBER Lfeystone LABORATORIES INC. a ne hc 19 January 2006 Bonnie McKee Pace Analytical -NC 9800 Kincey Ave. Ste. 100 Huntersville, NC 28078 RE: HRC Monitoring 92110924 Enclosed are the results of analyses for samples received by the laboratory on 01/10/06 10:30. If you have any questions concerning this report, please feel free to contact me at 1-800-858-5227. Sincerely, Kat y Van Zee For Jeffrey King, Ph D. Laboratory Director Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 stone ey I a�,., o� t MEMBE Q -- -- LABORATORIES, INC, a ne Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received 92619059/mw-6r 16AO340-01 Water 01/05/0614:05 01/10/0610:30 92619067/mw-7 16AO340-02 Water 01/05/0613:23 01/10/0610:30 92619075/mw-9 16AO340-03 Water 01/05/0614:41 01/10/0610:30 92619083/mw-10 16AO340-04 Water 01/05/0615:45 01/10/0610:30 92619091/mw-11 16AO340-05 Water 01/05/0614:17 01/10/0610:30 92619109/mw-13 16AO340-06 Water 01/05/0616:03 01/10/0610:30 92619117/dw-17 16AO340-07 Water 01/05/0615:09 01/10/0610:30 92619125/dw-18 16A0340-08 Water 01/05/0611:17 01/10/0610:30 Keystone Laboratories, Inc. - Newton �✓CLiv�► t V �.J Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 1 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 A C C p9D4y Lfeystone p� MEMBER LABORATORIES, INC. Q Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619059/mw-6r 16AO340-01 (Water) Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) 0.8 0.1 mg/1 1 1A61823 01/17/06 01/17/06 HPLC/UV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 " Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analysed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director Page 2 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Lfeystone LABORATORIES, INC. MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619067/mw-7 16AO340-02 (Water) Reporting [Anal Result Limit Units Dilution Batch Prepared Analyzed Method Not Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) 1.0 0.1 mg/l 1 1A61823 01/17/06 01/17/06 HPLGUV ND 1.0 " ND 1.0 " ND 1.0 " ND 1.0 " Keystone Laboratories, Inc. - Newton Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Paae 3 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 4p\� � .yc� MEMBER Lfeystone LABORATORIES, INC. a n ei Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619075/mw-9 16AO340-03 (Water) Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) 0.8 0.1 mg/1 1 1A61823 01/17/06 01/17/06 RPLCIUV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 " Propionic Acid (0) ND 1.0 Butyric Acid (C4) ND 1.0 " Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Kathy Van Zee For Jeffrey Kind, Ph.D., Laboratory Director Pace 4 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feystone LABORATORIES, INC. nelac MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619083/mw-10 16A0340-04 (Water) Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method No Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) 1.0 0.1 mg/l 1 1A61823 01/17/06 01/17/06 HPLC/UV ND 1.0 11 11 11 11 11 11 ND 1.0 X X X X X X ND 1.0 11 X X X X X ND 1.0 ItX X X X .. Keystone Laboratories, Inc. - Newton The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. yop�h cam, 0 Q 1 1 U t Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director Page 5 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 I Lfevstone MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619091/mw-11 16AO340-05 (Water) Reporting Anat Result Limit Units Dilution Batch Prepared Analyzed Method No Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) 1.4 0.1 mg/l I IA61823 01/17/06 01/17/06 HPLGIJV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 " " " ropionic Acid (C3) ND 1.0 " Butyric Acid (C4) ND 1.0 H " 1. " Keystone Laboratories, Inc. - Newton Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Paee 6 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 ��`��� �N ACCOc� 'ycF Lfeystone M E M B E R M 11 LABORATORIES, INC. a �� Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619109/mw-13 16AO340-06 (Water) Reporting Anatyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) 0.8 0.1 mg/l 1 1A61823 01/17/06 01/17/06 HPLGUV Lactic Acid (0) ND 1.0 " Acetic Acid (C2) 66.3 1.0 " Propionic Acid (C3) 59.1 1.0 " Butyric Acid (C4) 2.7 1.0 " Keystone Laboratories, Inc. - Newton `�o�-h� maw^• Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analysed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 7 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 �feystone LABORATORIES, INC. J:t ACC0q)4 nelat MEMBER Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619117/dw-17 16AO340-07 (Water) Reporting Anal to Result Limit Units Dilution Batch Prepared Analyzed Method No Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (0) Lactic Acid (0) Acetic Acid (C2) Propionic Acid (0) Butyric Acid (C4) ND 0.1 mg/I 1 1A61823 01/17/06 01/17/06 HPLGUV ND 1.0 it" ND 1.0 " ND 1.0 " ND 1.0 " Keystone Laboratories, Inc. - Newton Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 8 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 /jA feystone ACCC MEMBER VA LABORATORIES, INC. elac Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 92619125/dw-18 16AO340-08 (Water) Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids Pyruvic Acid (C3) 0.8 0.1 mg/1 1 1A61823 01/17/06 01/17/06 HPLC/UV Lactic Acid (0) ND 1.0 " " Acetic Acid (C2) ND 1.0 is" Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " Keystone Laboratories, Inc. - Newton -Tst hkn Oot Kathy Van Zee For Jeffrey King Ph.D., Laboraloiy Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 9 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 MEMBER Lfeystone LABORATORIES, INC. < nelac t. Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result °/.REC Limits RPD Limit Notes Batch 16A1808 - 1A61823 Calibration Check(16A1808-CCV1) Prepared & Analyzed: 01/17/06 Pyruvic Acid (0) 14.07 mg/1 13.00 108 80-120 Lactic Acid (0) 105.8 97.20 109 80-120 Acetic Acid (C2) 115.1 106.0 109 80-120 Propionic Acid (0) 110.3 105.0 105 80-120 Butyric Acid (C4) 117.0 106.0 110 80-120 Calibration Check(16A1808-CCV2) Prepared & Analyzed: O1/17/06 Pyruvic Acid (0) 13.16 mg/I 13.00 101 80-120 Lactic Acid (0) 109.1 97.20 112 80-120 Acetic Acid (C2) 112.5 106.0 106 80-120 Propionic Acid (0) 109.6 105.0 104 80-120 Butyric Acid (C4) 112.9 106.0 107 80-120 Batch 1A61823 - General Prey BPLC/IC Blank (1A61823-BLKI) Prepared & Analyzed: O1/17/06 Pyruvic Acid (0) ND 0.1 mg/1 Lactic Acid (0) ND 1.0 " Acetic Acid (C2) ND 1.0 " Propionic Acid (0) ND 1.0 " Butyric Acid (C4) ND 1.0 " LCS (1A61823-BSI) Prepared & Analyzed: 01/17/06 Pyruvic Acid (0) 20.27 0.1 mg/1 19.00 107 90-127 Lactic Acid (0) 108.1 1.0 111.8 96.7 70-115 Acetic Acid (C2) 117.1 1.0 107.6 109 90-125 Propionic Acid (0) 107.3 1.0 102.2 105 90-119 Butyric Acid (C4) 111.0 1.0 104.7 106 90-123 Keystone Laboratories, Inc. - Newton -1�hcam, OQ11 Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 10 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 feystone MEMBER LABORATORIES INC. < nelact= Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: �Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 Determination of Metabolic Acids - Quality Control Keystone Laboratories, Inc. - Newton Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 1A61823 - General PreD HPLOIC Matrix Spike (1A61823-MS1) Source: 16A0063-01 Prepared & Analyzed: 01/17/06 Pyruvic Acid (0) 19.54 0.1 mg/I 19.00 ND 103 81-129 Lactic Acid (0) 115.6 1.0 111.8 ND 103 70-116 Acetic Acid (C2) 110.2 1.0 107.6 ND 102 85-125 Propionic Acid (0) 117.9 1.0 102.2 ND 115 88-119 Butyric Acid (C4) 113.9 1.0 104.7 ND 109 85-123 Matrix Spike Dup (1A61823-MSDI) Source: 16A0063-01 Prepared & Analyzed: 01/17/06 Pyruvic Acid (0) 19.32 0.1 mg/I 19.00 ND 102 81-129 1.13 11 Lactic Acid (0) 117.0 1.0 111.8 ND 105 70-116 1.20 17 Acetic Acid (0) 107.8 1.0 107.6 ND 100 85-125 2.20 15 Propionic Acid (0) 120.7 1.0 102.2 ND 118 88-119 2.35 14 Butyric Acid (C4) 122.0 1.0 104.7 ND 117 85-123 6.87 12 Keystone Laboratories, Inc. - Newton Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Page 11 of 12 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 �N ACCOp ���� MEMBER Lfeystone InLABORATORIES, INC. elac Pace Analytical -NC Project: HRC Monitoring 9800 Kincey Ave. Ste. 100 Project Number: 92110924 Reported: Huntersville NC, 28078 Project Manager: Bonnie McKee 01/19/06 15:53 Notes and Definitions DET Analyte DETECTED ND Analyte NOT DETECTED at or above the reporting limit NR Not Reported dry Sample results reported on a dry weight basis RPD Relative Percent Difference Keystone Laboratories, Inc. - Newton �c�-h � l� C;tN► . The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Kathy Van Zee For Jeffrey King Ph.D., Laboratory Director Phone 641-792-8451 600 East 17th Street South Newton, IA 50208 Fax 641-792-7989 Page 12 of 12 Trigon Services • Geotechnical Engineering • Construction Materials Engineering/Testing • Roof Engineering/Inspection • Forensic Engineering • Environmental Audits/Site Assessments • Environmental Drilling • Groundwater Studies/Remediation • Stormwater Permitting • Wastewater Engineering • Water Treatment Design • Health & Safety Consulting • Regulatory Compliance Engineering • Waste Minimization Studies • Air Quality Consulting • Atmospheric Computer Dispersion Modeling • Stack Testing and Continuous Emissions Monitoring • Indoor Air Monitoring • Asbestos and Lead -based Paint Inspections • Pollution Prevention Plans OFFICE LOCATIONS Greensboro Raleigh Charlotte North Carolina North Carolina North Carolina 336-668-0093 9197555011 704-598-1049 Greenville South Carolina 864-2973557