WQ0038087_More Information Received_20201118

Initial Review
INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Date Paper Copy 11/18/2020
Received:*
Project Number* WQ0038087
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * David C. Coyle
Email Address*
[e-mail]
Project Information
.........................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0038087
Applicant\Permittee * Terra Renewal Services, Inc
Facility Name * Terra Renewal Services RLAP
Phone Number*
479-747-8192
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
This is the response to the Additional Information Request letter, dated 10/22/20 from Ranveer Katyal, regarding the
review of the application for Renewal & Major Modification of Permit # WQ0038087. One electronic (PDF) copy is
being supplied. Paper copies are NOT being supplied but can be upon request. Ranveer Katyal has left the DEQ
with instructions received to send all additional submittals and correspondence regarding this permit application to
Nathaniel Thornburg. If there are any questions or complications, I can be reached at 479-747-8192 or
[e-mail].
David Coyle
11 /18/20
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
NC_WQ0038087_2020 Ren & Mod_Response to
38.67MB
AIR Letter-1 1-18-20.pdf
upload only 1 RJF docurrent. Miltiple docurrents must be corrbined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 11/18/2020

TERRA
renewal
November 18, 2020
Nathaniel Thornburg; Branch Chief
Non -Discharge Branch
Division of Water Resources
North Carolina Department of Environmental Quality
512 N. Salisbury Street
1617 Mail Service Center
Raleigh, NC 27699-1617
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
RE: Response to Additional Information Request for Renewal & Modification of
Permit # WQ0038087
(A.I.R letter dated October 22, 2020)
Dear Mr. Thornburg,
In response to the request for additional information, dated October 22, 2020 and produced by
Ranveer Katyal, related to the application for renewal and modification of Permit # WQ0038087,
Terra Renewal is providing the following response with corresponding attachments (in order
addressed in A.I.R. letter):
A. Application:
Quantitative Justification: A newly revised Quantitative Justification for Residuals
Production Rate (QJRPR) is provided that includes an estimated volume of residuals to
be land applied from each facility. These volumes and dry tons were calculated using
average values from previous year's records. A calculation is provided on this sheet
showing the weighted average PAN calculation for all residuals sources. First (1") year
through fifth (5t") year mineralized PAN calculations for surface and incorporated
application is also provided for each individual residuals source.
A revised Residuals Source Facility Summary (aka Attachment -A) is provided that
includes the "Maximum Dry Tons per Year" based on the modified volumes obtained in
the QJRPR. All values from the QJRPR were used to recalculate the numbers in sections
111.4.a & 111.4.c of form RLAP 06-16. The revised copy of this form is provided with an
updated signature / date.
Sampling Results: The most current analysis on record is provided and these data were
used to revise the QJRPR and forms RSC 06-16 for each residuals source. Currently,
Tyson - Wilkesboro, River Valley Ingredients — Harmony, and AdvancePierre Foods —
Claremont, are the only sources being land applied under this permit; therefore, these
sources have current analyses, as late as September 2020 for Nutrients & Metals. The
latest TCLP analyses are provided for these three facilities, which were performed in
Page 1 of 3
11 /18/2020 — WQ0038087 — 2020 Permit Modification — Response to Add Info Request

October 2019. New samples are currently being collected for these facilities in Q4 of
2020 for TCLP analysis but results are not yet available. Fecal Coliform analyses are also
provided from September 2020 for these sources to demonstrate pathogen reduction.
Hunter Dairy — High Point is currently sending its residuals to a composter. Terra
Renewal has not land applied any loads from this facility since this began in January of
2020; therefore, the most recent analyses available are from October 2019 (N&M, TCLP)
and December 2019 (Fecal Coliform). Brakebush Brothers — Mocksville is the same
facility as House of Raeford — Mocksville as previously listed in the permit. This facility
was shut down for several years due to fire. It was purchased by Brakebush Brothers
and restarted in 2019. The residuals from this facility are currently sent to a digester.
Terra Renewal has not land applied any loads from this facility since 2017; therefore, the
most recent analyses available are from April 2017 (N&M, TCLP) and December 2016
(Fecal Coliform).
The dates on which the samples were collected for each report provided in this
application are listed below:
Date Sample Collected
Source
N&M
TCLP
Pathogen
Tyson -Wilkesboro
9/8/2020
10/16/2019
9/8/2020
RVI-Harmony
9/8/2020
10/16/2019
9/8/2020
AdvancePierre-Claremont
9/17/2020
10/14/2019
9/17/2020
Hunter Dairy -High Point
10/14/2019
10/14/2019
12/19/2019
Brakebush Brothers-Mocksville
5/4/2017
5/4/2017
11/30/2016
Mathis 1-Storage
5/23/2019
5/23/2019
4/22/2019
Hunter Dairy and Brakebush Brothers have requested that their sources stay "active" on
this permit as a contingency plan in case their primary methods for residuals
management become unviable. Terra Renewal wishes to accommodate their request at
this time. Terra Renewal will collect and process new samples for all parameters
required in the permit prior to land applying any loads from these facilities should
activity resume. The figures demonstrated in the QJRPR represent the maximum
anticipated volumes to be land applied if residuals generated from all facilities were
directed to land application under this permit.
3. Tyson — AdvancePierre Foods: This item is no longer valid since all of the RSC 06-16
forms and five-year PAN calculations were revised with updated analytical data.
B. Setback Waivers:
Fully executed and recorded setback waiver forms are provided for sites which require a
modification due to elimination of setbacks from internal property boundaries. The
setback waiver forms do not include reduced setbacks for residences or places of
assembly, as none were requested as part of this modification.
See above. Net acreages shall remain the same as submitted on form LASC 06-16 in the
permit application.
Page 2 of 3
11/18/2020 — WQ0038087 — 2020 Permit Modification — Response to Add Info Request

C. Compliance Boundaries:
There is no rationale for requested relocation of compliance boundaries, and these were
not included in the maps because there was no such request or changes made. The only
changes made to the land application sites was elimination of internal property buffers,
which should not affect the compliance boundary on these sites. This was addressed in
an email with Ranveer Katyal on October 23, 2020. A copy of that email thread is
provided.
D. Engineering Calculations:
1. Based on the opinion of the Engineer of Record for the storage facility project (Arete
Engineers — Blowing Rock, NC), buoyancy calculations are not applicable for these
structures. A letter is provided explaining their rationale.
2. A document is provided with specifications describing materials to be used, methods of
construction, and means for ensuring quality and integrity of the finished product. The
Engineer of Record will be involved in oversight of construction and inspection. An
Engineering Certification will be submitted to the NC DEQ DWR upon completion. A
sample copy of the certification form is provided. A leakage detection system will be
installed on each tank. A diagram showing the configuration of the system is provided.
The attachments are provided in the same order as submitted in the original permit application
with cover pages corresponding to each section in which they belong. The PDF document is
bookmarked for easier navigation. Attached items are listed below:
• Email from Ranveer Katyal regarding Item-C in A.I.R. Letter.
• Section 2: ND RLAP Form 06-16 (revised)
• Section 3: Form RSC 06-16 (revised)
• Attachment C: Quantitative Justification for Residuals Production Rate (revised)
• Attachment D: Analytical Data for Residuals (updated)
• Attachment H: Landowner Agreement & Setback Waiver Forms (waiver forms provided
with proof of recording at Register of Deeds)
• Attachment M: Storage Facility Design Documents
— Letter from NC PE addressing Buoyancy Calculations
— Materials & Methods, QAQC, Leakage Testing
If you have any questions regarding this response or require additional information, please
contact me at [e-mail] or 479-747-8192. Thank you very much for your
cooperation and assistance.
Sincerely,
David C. Coyle
Environmental Manager
Page 3 of 3
11/18/2020 — WQ0038087 — 2020 Permit Modification — Response to Add Info Request

David Coyle
From: Katyal, Ranveer <[e-mail]>
Sent: Friday, October 23, 2020 4:00 PM
To: David Coyle
Subject: RE: [External] RE: [EXT]WQ0038087 - Terra Renewal Services RLAP - additional
information letter
David,
This was from my review, however on re -reviewing the application I did not see the need for this anymore.
I believe, in the Land Owner Agreement Form Condition III, if you have checked the box for re -defined compliance
boundary then the Item C needs to be addressed. If that box has not been checked for any of the LOA forms, you can
ignore the item C.
I apologize for the confusion.
Ranveer
From: David Coyle [mailto:[e-mail]]
Sent: Friday, October 23, 2020 2:05 PM
To: Katyal, Ranveer <[e-mail]>
Subject: [External] RE: [EXT]WQ0038087 - Terra Renewal Services RLAP - additional information letter
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
Ranveer,
I'm afraid I'm going to need someone to explain exactly what's required to address "Item C" in this letter. I figured that
probably came from Patrick's review but apparently he's out of town until next Thursday. Could you shed some light on
this for me or do I need to wait for Patrick to get back in the office?
David Coyle
Environmental Manager
P.O. Box 1746, Watkinsville, GA 30677
Cell 479-747-8192
david.covlePdenaliwater.com
Denali
WATER SOLUTIONS
IMPORTANT NOTICE: This e-mail message is intended to be received only by persons entitled to receive the confidential information it may contain.
E-mail messages to clients of Denali Water Solutions or any of its affiliates may contain information that is confidential and legally privileged. Please
do not read, copy, forward, or store this message unless you are an intended recipient of it. If you have received this message in error, please
forward it to the sender and delete it completely from your computer system.

From: Katyal, Ranveer <[e-mail]>
Sent: Thursday, October 22, 2020 4:47 PM
To: David Coyle <[e-mail]>
Cc: Thornburg, Nathaniel<[e-mail]>; Mitchell, Patrick <[e-mail]>
Subject: [EXT]WQ0038087 - Terra Renewal Services RLAP - additional information letter
Good afternoon,
This email is with respect to your permit modification application for WQ0038087. Additional information is required to
modify the permit, please submit the required information by close of business November 23, 2020.
Sincerely,
Ranveer Katyal
Environmental Engineer
Non -Discharge Branch
Department of Environmental Quality
919 707 3661 office
[e-mail]
512 N. Salisbury St.
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties
[EXTERNAL EMAIL] This email is not from a Denali Water employee using an @denaliwater.com email address. DO NOT
CLICK links or open attachments unless you recognize the sender and email address and know the content is safe.
IMPORTANT NOTICE: This e-mail message is intended to be received only by persons entitled to receive the confidential information
it may contain. E-mail messages to clients of Denali Water Solutions or any of its affiliates may contain information that is
confidential and legally privileged. Please do not read, copy, forward, or store this message unless you are an intended recipient of
it. If you have received this message in error, please forward it to the sender and delete it completely from your computer system.
This email has been scanned for viruses and malware, and may have been automatically archived.
[EXTERNAL EMAIL] This email is not from a Denali Water employee using an @denaliwater.com email address. DO NOT
CLICK links or open attachments unless you recognize the sender and email address and know the content is safe.

SECTION 2:
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM
Form: RLAP 06-16

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Terra Renewal Services, Inc
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal [!I State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: David C. Cow Title: Environmental Manaaer
Applicant's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: [phone] Email Address: david.co lekterrarenewal.com
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address: _
City: State:
Telephone number: () -
3. Agronomist's name:
Affiliation: ❑ N/A ❑ On Staff
Zip:-�
Email Address:
License Number: —0
❑I Retained (Firm: )
Agronomist's mailing address:
City: ' State: Zip: 41-m—
Telephone number: (_) = Email Address:
4. Soil Scientist's name: David C. CoyleLicense Number: 1315
Affiliation: ❑ N/A ® On Staff ❑ Retained (Firm: )
Soil Scientist's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: [phone] Email Address: david.co lekterrarenewal.com
5. Fee submitted: $395.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0038087
Date of most -recently issued permit: February 12, 2016
Date of most -recently certified Attachment A (if different than the permit): March 16, 2020
Date of most -recently certified Attachment B (if different than the permit): March 16, 2020
FORM: RLAP 06-16 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 615 Mathis Farm Rd (Location of Office of LJC Environmental, LLC)
City: Roaring River State: NC Zip: 25669
Coordinates: Latitude: 36' 08' 51" Longitude: 80' 59' 09"
Datum: NAD 83
Method of measurement: MAP
Level of accuracy: Nearest Second
2. County where residuals land application program is headquartered: Wilkes
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Luke Mathis
LJC Environmental, LLC
1003524
Back -Up ORC
David Coyle
Terra Renewal Services, Inc
995723
Additional Back -Up
Will Hodges
Denali Water Solutions
997282
ORCs
John Pipkin
Denali Water Solutions
990262
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test: P"
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 6,700 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
15.7
20.7
105,190
138,690
Five -Year Maximum Adjusted
22.1
27.1
148,070
181,570
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
1,549.0
Hay
Pasture
Total:
1,549.0
Methods
Surface
6-
Incorporation or Injection
1,549.0
Total:
1,549.0
FORM: RLAP 06-16 Page 2 of 5

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
2,104
2,774
2,961
3,631
100
1,052
1,387
1,481
1,816
150
701
925
987
1,210
200
526
693
740
908
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.):
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
R
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
IF
Land Application Siite
Certification.doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only.
VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM
1. The irrigation system is: ❑ Spray ❑ Drip
2. Disposal system is: k] existing ❑ proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet
below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified: En
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
Fields within Soil Area
Recommended
Loading Rate
in/hr
Recommended
Loading Rate
in/ r
1
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
L Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met:
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field /Zone
Design Area
(ft)
Number of
Nozzles
Maximum Application
Rate allons/hr
Design Annual Loading
Rate allons/ r
■
Total
AM
M
Spray Irrigation Design Element
Plan Sheet
Number
Specification
Pa a Number
Wetted diameter of nozzles
ft
Wetted area of nozzles
ft2
Nozzle capacity
gpm
Nozzle manufacturer / model
/
Elevation of highest nozzle
ft
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, David C. Coyle Environmental Manager
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Terra Renewal Services, Inc
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
Date: 11/13/2020
FORM: RLAP 06-16 Page 5 of 5

SECTION 3:
RESIDUALS SOURCE CERTIFICATION
Form: RCS 06-16

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Terra Renewal Services, Inc
Status a
Code
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Tyson Foods, Inc.
Tyson — Wilkesboro, NC
Wilkes
N/A
5,400
3,800
R
Tyson Foods, Inc.
Rivery Valley Ingredients -
Harmony, NC
Iredell
NC0005126
1,400
1,700
M
Hunter Farms, LLC
Hunter FarmsNC High Point,
Guilford
N/A
450
690
R
Brakebush Brothers, Inc.
Brakebush Brothers —
Mocksville, NC
Davie
N/A
240
480
R
Tyson Foods, Inc.
AdvancePierre Foods —
Claremont, NC
Catawba
N/A
25
30
N
Terra Renewal Services, Inc
Mathis-1 Storage Facility
Wilkes
WQ0038087
0
N/A
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

RSC 06-16
ADVANCE PIERRE FOODS - CLAREMONT, NC

Lilh7l;3
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: MancePierre Food4
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, 0 Div. of Environmental Health,
or ® Other (explain: Facility discharges to local POTW. Residuals consist of DAF
skimmings from pretreatment).
3. Facility contact person and title: Anth 1 o; Environmental Manaeer
Complete mailing address: 1437 E. Maim
City: arem State: &J6 Zip: 286 --
Telephone number: [phone] E-mail address:
4. Facility physical address: 343
City: Llarcmont State: NC Zip:
Coordinates: Latitude: L° 42' 43" Longitude: it- 08' 16"
Datum: JUP 83 Level of accuracy: Nearest Second
Method of measurement: -
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: _ MGD and facility average daily flow: _ MGD
8. Average amount of residuals being generated at this facility 0 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: TM7-_9enerate rom so i s remove rom D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units):
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulatcd undcr 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page] ofi 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Shealy Environmental Servic and Date of analysis: 10/14/2019
Passed corrosivity test: ® yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Eno. HCN: M mg/kg (<250) & 112S: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg/7)
Result
(mg/7)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.25
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.25
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.25
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.25
Methyl Ethyl Ketone
200.0
< 0.50
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
0.089
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
0.089
Selenium
1.0
< 0.20
Cresol
200.0
0.089
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.25
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.25
Trichloroethylene
0.5
< 0.25
1,1-Dichloroethylene
0.7
< 0.25
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.050
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/17/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 11
Cadmium
85
39
< 3.5
Copper
4,300
1,500
1,200
Lead
840
300
< 7.0
Mercury
57
17
< 3.3
Molybdenum
75
n/a
< 28
Nickel
420
420
41
Selenium
100
100
< 14
Zinc
7,500
2,800
190
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(7119/k9)
Ej > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
77 > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.30 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/17/2020
Parameter
Result
(mg1kg)
Aluminum
17,000
Ammonia -Nitrogen
460
Calcium
< 3,500
Magnesium
< 3,500
Nitrate -Nitrite Nitrogen
58
pH (Standard Unit)
4.4
Phosphorus
860
Potassium
4,600
Sodium
14,000
Total Kjeldahl Nitrogen
16,000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 6_0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
6,505
9,850
Injection/Incorporation
6,735
10,080
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
BRAKEBUSH BROTHERS - MOCKSVILLE, NC

Lilh7l;3
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Brakebush Brothers (formerly House of Raeford)
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, 0 Div. of Environmental Health,
or ® Other (explain: Facility discharges to local POTW. Residuals consist of DAF
skimmings from pretreatment).
3. Facility contact person and title: Steve Mixon; Wastewater Manacer
Complete mailing address: 251 Eaton Rd
City: oc svi e State: �JW Zip: _--
Telephone number: [phone] E-mail address:
4. Facility physical address: 251 Eaton Rd
City: E4ocksville State: E Zip: _-V_
Coordinates: Latitude: L° 52' 49" Longitude: F° 33' 12"
Datum: JUP 83 Level of accuracy: Nearest Second
Method of measurement: =
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0.24 MGD and facility average daily flow: 0.08 MGD
8. Average amount of residuals being generated at this facility 480 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: TM7-_9enerate rom so i s remove rom D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): one 12,000 gallon holding tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulatcd undcr 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page] of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Walytical Environmental Services and Date of analysis: -
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Eno. HCN:"mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg/7)
Result
(mg/7)
Arsenic
5.0
< 0.250
Hexachlorobenzene
0.13
< 0.10
Barium
100.0
< 0.500
Hexachloro-1,3-Butadiene
0.5
< 0.10
Benzene
0.5
< 0.10
Hexachloroethane
3.0
< 0.10
Cadmium
1.0
< 0.0250
Lead
5.0
< 0.0500
Carbon Tetrachloride
0.5
< 0.10
Lindane
0.4
< 0.00050
Chlordane
0.03
< 0.0050
Mercury
0.2
< 0.0040
Chlorobenzene
100.0
< 0.10
Methoxychlor
10.0
< 0.0050
Chloroform
6.0
< 0.10
Methyl Ethyl Ketone
200.0
< 0.20
Chromium
5.0
< 0.0500
Nitrobenzene
2.0
< 0.10
m-Cresol
200.0
< 0.10
Pentachlorophenol
100.0
< 0.10
o-Cresol
200.0
< 0.10
Pyridine
5.0
< 0.10
p-Cresol
200.0
< 0.10
Selenium
1.0
< 0.10
Cresol
200.0
< 0.10
Silver
5.0
< 0.0250
2,4-D
10.0
< 0.20
Tetrachloroethylene
0.7
< 0.10
1,4-Dichlorobenzene
7.5
< 0.10
Toxaphene
0.5
< 0.050
1,2-Dichloroethane
0.5
< 0.10
Trichloroethylene
0.5
< 0.10
1,1-Dichloroethylene
0.7
< 0.10
2,4,5-Trichlorophenol
400.0
< 0.10
2,4-Dinitrotoluene
0.13
< 0.10
2,4,6-Trichlorophenol
2.0
< 0.10
Endrin
0.02
< 0.0010
2,4,5-TP (Silvex)
1.0
< 0.20
Heptachlor and its Hydroxide
0.008
< 0.00050
Vinyl Chloride
0.2
< 0.040
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Analytical Environmental Services, Inc. and Date of analysis: 5/4/2017
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 44.4
Cadmium
85
39
< 22.2
Copper
4,300
1,500
< 22.2
Lead
840
300
< 44.4
Mercury
57
17
< 1.98
Molybdenum
75
n/a
< 44.4
Nickel
420
420
< 44.4
Selenium
100
100
< 44.4
Zinc
7,500
2,800
48.2
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(7119/k9)
Ej > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
77 > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: `%.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Analytical Environmental Services, Inc. and Date of analysis: -
Parameter
Result
(mg1kg)
Aluminum
17,300
Ammonia -Nitrogen
3,770
Calcium
1,180
Magnesium
500
Nitrate -Nitrite Nitrogen
< 108
pH (Standard Unit)
3.78
Phosphorus
11,300
Potassium
1,680
Sodium
6,600
Total Kjeldahl Nitrogen
69,200
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): L
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
28,165
42,250
Injection/Incorporation
30,050
44,135
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
HUNTER FARMS - HIGH POINT, NC

Lilh7l;3
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, 0 Div. of Environmental Health,
or ® Other (explain: Facility discharges to local POTW.
skimmings from pretreatment).
3. Facility contact person and title: Gene Dumas; Wastewa er anacer
Complete mailing address: 1900 N. Main St
City: tli Ihomt State: Jii Zip: 27262
Telephone number: [phone] E-mail address: gdumaskharristeeter.com
4. Facility physical address: 1900 N. Main St
City: - State: NC Zip: _-IL_
Coordinates: Latitude: L° 58' 48" Longitude: F° 01' 14"
Datum: ffND 83 Level of accuracy: Nearest Second
Method of measurement: -
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: E MGD and facility average daily flow: MMGD
8. Average amount of residuals being generated at this facility M dry tons per year.
FORM: RSC 06-16
Residuals consist of DAF
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: TM7-_9enerate rom so i s removed trom D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): Lwo 4,000 ,gallon holding tanks
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulatcd undcr 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page] ofi 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Shealy Environmental Servic and Date of analysis: 10/14/2019
Passed corrosivity test: ® yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Eno. HCN: M mg/kg (<250) & 112S: M mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg/7)
Result
(mg/7)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
0.11
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
< 0.040
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.040
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1,1-Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Shealy Environmental Services and Date of analysis: 10/14/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 1.9
Cadmium
85
39
< 0.65
Copper
4,300
1,500
< 1.3
Lead
840
300
< 1.3
Mercury
57
17
< 0.60
Molybdenum
75
n/a
< 5.2
Nickel
420
420
< 5.2
Selenium
100
100
< 2.6
Zinc
7,500
2,800
7.7
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(7119/k9)
Ej > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
77 > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 12.8 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Jhealy Environmental Services, Inc and Date of analysis: 10/14/2019
Parameter
Result
(mg1kg)
Aluminum
3,100
Ammonia -Nitrogen
< 78
Calcium
1,100
Magnesium
< 650
Nitrate -Nitrite Nitrogen
10
pH (Standard Unit)
3.6
Phosphorus
2,500
Potassium
< 650
Sodium
< 650
Total Kjeldahl Nitrogen
12,000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1_4
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
8,020
12,300
Injection/Incorporation
8,080
12,360
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
MATHIS-1 STORAGE FACILITY - RONDA, NC

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Flathis-1 Storage
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: =).
3. Facility contact person and title: David C. Coyle; Environmental Manager — Terra Renewal Services, Inc.
Complete mailing address: P.O. Box 1746
City: W atklnsyille State: Zip: 30677-
Telephone number: (� 9) 747-8192 E-mail address: david.co lekterrarenewal.com
4. Facility physical address: Mathis Mill Rd (dead end of Dr Beale Farm Rd)
City: � State: It Zip: 28669-
Coordinates: Latitude: 36' 12' 35" Longitude: V0° 58' 09"
Datum: — Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and % domestic)
other (explain: Residuals storage in support of land application permit W00038087).
6. Does the facility have an approved pretreatment program: [ij Yes ® No
7. Facility permitted/design flow: M MGD and facility average daily flow: NA MGD
8. Average amount of residuals being generated at this facility M dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment:
Type and volume of residuals storage (i.e., outside of residuals treatment units): k.I MG of passive storage for residuals to
be land applied under permit WQ0038081
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulatcd undcr 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page] of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Walytical Environmental Services and Date of analysis: 5/24/19 (date received
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Eno. HCN:"mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg/7)
Result
(mg/7)
Arsenic
5.0
< 0.250
Hexachlorobenzene
0.13
< 0.10
Barium
100.0
< 0.500
Hexachloro-1,3-Butadiene
0.5
< 0.10
Benzene
0.5
< 0.10
Hexachloroethane
3.0
< 0.10
Cadmium
1.0
< 0.0250
Lead
5.0
< 0.050
Carbon Tetrachloride
0.5
< 0.10
Lindane
0.4
< 0.000050
Chlordane
0.03
< 0.00050
Mercury
0.2
< 0.0040
Chlorobenzene
100.0
< 0.10
Methoxychlor
10.0
< 0.00050
Chloroform
6.0
< 0.10
Methyl Ethyl Ketone
200.0
< 0.20
Chromium
5.0
< 0.050
Nitrobenzene
2.0
< 0.10
m-Cresol
200.0
< 0.10
Pentachlorophenol
100.0
0.50
o-Cresol
200.0
< 0.10
Pyridine
5.0
< 0.10
p-Cresol
200.0
< 0.10
Selenium
1.0
< 0.10
Cresol
200.0
< 0.10
Silver
5.0
< 0.0250
2,4-D
10.0
< 0.20
Tetrachloroethylene
0.7
< 0.10
1,4-Dichlorobenzene
7.5
< 0.10
Toxaphene
0.5
< 0.0050
1,2-Dichloroethane
0.5
< 0.10
Trichloroethylene
0.5
< 0.10
1,1-Dichloroethylene
0.7
< 0.10
2,4,5-Trichlorophenol
400.0
< 0.10
2,4-Dinitrotoluene
0.13
< 0.10
2,4,6-Trichlorophenol
2.0
< 0.10
Endrin
0.02
< 0.00010
2,4,5-TP (Silvex)
1.0
< 0.20
Heptachlor and its Hydroxide
0.008
< 0.000050
Vinyl Chloride
0.2
< 0.040
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 13.6
Cadmium
85
39
< 13.6
Copper
4,300
1,500
16.0
Lead
840
300
< 27.2
Mercury
57
17
< 2.93
Molybdenum
75
n/a
< 27.2
Nickel
420
420
< 27.2
Selenium
100
100
< 19.0
Zinc
7,500
2,800
35.1
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(7119/k9)
Ej > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
77 > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: IL %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Analytical Environmental Services, Inc. and Date of analysis: 5/24/19 (date received)
Parameter
Result
(mg1kg)
Aluminum
< 272
Ammonia -Nitrogen
3,990
Calcium
671
Magnesium
< 272
Nitrate -Nitrite Nitrogen
< 145
pH (Standard Unit)
4.4
Phosphorus
3,890
Potassium
1,110
Sodium
1900
Total Kjeldahl Nitrogen
100,000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
40,545
61,215
Injection/Incorporation
42,540
63,120
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
RIVER VALLEY INGREDIENTS (TYSON) - HARMONY, NC

Lilh7l;3
Division of Water Resources
I.
II.
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: River Valley Ingredients (Tyson Foods, Inc)
2. Facility permit holder is: ❑ Federal, [] State, D Local Government, or Q Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain:).
3. Facility contact person and title: Kevin Ha
'xJVastewater Manager
Complete mailing address: 501 Sheffield Rd
City: harmony State: NC Zip: 28634-
Telephone number: (E) 546-2988 E-mail address: kevin.ha esklyson.com
4. Facility physical address: 501 Sheffield Rd
City: - State: NC
Coordinates: Latitude: 35' 57' 15"
Datum: -
Method of measurement: MAP
5. Purpose of the facility:
Zip: 8634-.
Longitude: V0° 43' 17"
Level of accuracy: Nearest Second
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: E MGD and facility average daily flow: MMGD
8. Average amount of residuals being generated at this facility _ dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 100% generated from solids removed from D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): one 5,000 gallon holding tank
RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes N no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Shealy Environmental Services, Inc. and Date of analysis: 10/18/2019
Passed corrosivity test: yes 19 no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes ❑ no. Flashpoint: > 140 OF (> 140°F)
Passed reactivity test: Z yes Ono. HCN: < 50 mg/kg (<250) & H2S: mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(mg/l)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
3.3
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
3.3
Selenium
1.0
< 0.20
Cresol
200.0
3.3
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/08/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 5.5
Cadmium
85
39
< 1.8
Copper
4,300
1,500
10
Lead
840
300
5.9
Mercury
57
17
< 1.7
Molybdenum
75
n/a
< 15
Nickel
420
420
< 15
Selenium
100
100
< 7.4
Zinc
7,500
2,800
57
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
71 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.48 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/08/2020
Parameter
Result
(mg1kg)
Aluminum
15,000
Ammonia -Nitrogen
21,000
Calcium
19,000
Magnesium
< 1,800
Nitrate -Nitrite Nitrogen
90
pH (Standard Unit)
5.9
Phosphorus
4,700
Potassium
2,200
Sodium
2,600
Total Kjeldahl Nitrogen
32,000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1_0
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
14,990
17,360
Injection/Incorporation
25,490
27,860
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
TYSON - WILKESBORO, NC

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: JR Federal, 0 State, 0 Local Government, or a Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ® Other (explain: Facility discharges to local POTW; Residuals consist of DAF
ikimmin sg from pretreatment).
3. Facility contact person and title: Jim Brown; Wastewater Manaeer
Complete mailing address: 704 Factory Street
City: ilke State: �ii Zip: 28697-
Telephone number: [phone] E-mail address: james.s.brownglyson.com
4. Facility physical address: 704 Factory Street
City: kilkcsb State: NC Zip: _-IL_
Coordinates: Latitude: L° 08' j" Longitude: it- 09' 43"
Datum: ffND 83 Level of accuracy: Nearest Second
Method of measurement: =
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: I MGD and facility average daily flow: N MGD
8. Average amount of residuals being generated at this facility 5,400 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: TM7-_9enerate rom so i s removed trom D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): Lwo 24,000 ,gallon holdingtanks
anks
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulatcd undcr 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
FORM: RSC 06-16 Page] of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Shealy Environmental Servic and Date of analysis: 10/16/2019
Passed corrosivity test: ® yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: 0 yes Eno. HCN: M mg/kg (<250) & 112S: M mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mg/7)
Result
(mg/7)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.25
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.25
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.25
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.25
Methyl Ethyl Ketone
200.0
< 0.50
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
< 0.040
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.040
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.25
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.25
Trichloroethylene
0.5
< 0.25
1,1-Dichloroethylene
0.7
< 0.25
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.050
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/08/2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(Class A Only)
(mglkg)
Result
(mglkg)
Arsenic
75
41
< 2.8
Cadmium
85
39
< 0.94
Copper
4,300
1,500
8.2
Lead
840
300
< 1.9
Mercury
57
17
< 0.89
Molybdenum
75
n/a
< 7.5
Nickel
420
420
< 7.5
Selenium
100
100
< 3.8
Zinc
7,500
2,800
15
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(7119/k9)
Ej > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
> 75 but < 100
46
300
320
77 > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 8.42 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 09/08/2020
Parameter
Result
(mg1kg)
Aluminum
220
Ammonia -Nitrogen
1,400
Calcium
< 940
Magnesium
< 940
Nitrate -Nitrite Nitrogen
33
pH (Standard Unit)
4.8
Phosphorus
450
Potassium
< 940
Sodium
< 940
Total Kjeldahl Nitrogen
6,200
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1_5
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 4 %. This
rate is a (check one): default value, or [I actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111 Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg1kg)
Surface
2,655
3,685
Injection/Incorporation
3,355
4,385
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
es: the results of the latest analys
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
El Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
El Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [� composting, 4 heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class B:
E Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, ii anaerobic digestion,
composting, i I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T. 1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

ATTACHMENT - C:
QUANTITATIVE JUSTIFICATION for RESIDUALS PRODUCTION RATE

Quantitive Justification for Residuals Production Rate
NC DEQ RLAP Permit # WQ0038087
Permittee: Terra Renewal Services
Amount of Dry Tons to be Certified based on Historical Data
Avg. Solids 1
(%)
Loads 1
Est. Volume Z
(Gal/Yr)
Est. Volume z
(Dry Tons/Yr)
Amount to
be Certified
(Dry Tons/Yr)
Residuals Source
Tyson -Wilkesboro
9.5
30/wk
9,360,000
3,708
3,800
RVI (Tyson) -Harmony
5.4
24/wk
7,488,000
1,686
1,700
Hunter Farms -High Point
8.8
6/wk
1,872,000
687
690
Brakebush Bros-Mocksville
6.1
6/wk
1,872,000
476
480
AdvancePierre-Claremont
4.2
2/mo
144,000
25
30
Mathis-1
N/A*
N/A*
N/A*
N/A*
N/A*
Total: 6,700
1) Based on average total solids for samples collected in 2019
2) Based on average residuals generated per facility for years 2016 - 2019
Weighted Average for PAN Calculations
2020 Renewal & Storage Facility Modification
*Revised: Nov 2020
Actual PAN Concentration
Proportion Adjusted PAN Concentration
Year 1
Year 5
Year 1
Year 5
Residuals Source
Est. Volume
(Dry Tons/Yr)
Percent
(%)
Surface PAN
(lbs/DT)
Inject PAN
(Ibs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(Ibs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(lbs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(Ibs/DT)
Tyson -Wilkesboro
3,800
57%
5.31
7.37
6.71
8.77
3.0
4.2
3.8
5.0
RVI (Tyson) -Harmony
1,700
25%
29.98
34.72
50.98
55.72
7.6
8.8
12.9
14.1
Hunter Farms -High Point
690
10%
9.64
14.77
9.71
14.85
1.0
1.5
1.0
1.5
Brakebush Bros-Mocksville
480
7%
56.33
84.5
60.1
88.27
4.0
6.1
4.3
6.3
AdvancePierre-Claremont
30
0%
13.01
19.7
13.47
20.16
0.1
0.1
0.1
0.1
Mathis 1-Storage
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
Total: 6,700 100%
Weighted Average: 15.7 20.7 22.1 27.1
* N/A due to pass through of storage. Residuals are comingled and not generated. Volume of residuals stored will vary from year to year. Mathis-1 is to be certified and sampled as
separate source due to change in characteristics after comingling; however, this should not change the quantity of Dry Tons generated by each facility.

Surface Application PAN
AdvancePierre Foods -Claremont
TKN=
16000
mg/kg
NH3=
460
mg/kg
NO3-NO2-N=
58
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 15,540 230 58.00
PAN= 13.01 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 15,540 6,216
PAN= 3.73 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 9,324 1,865
PAN= 1.59 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 7,459 796
PAN= 0.89 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 6,664 444
PAN= 0.48 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 6.69 Lbs/Pan/DT
Total five-year max. adjusted PAN = 19.70 Lbs/Pan/DT

Injection Application PAN
AdvancePierre Foods -Claremont
TKN=
16000
mg/kg
NH3=
460
mg/kg
NO3-NO2-N=
58
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 15,540 460 58.00
PAN= 13.47 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 15,540 6,216
PAN= 3.73 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 9,324 1,865
PAN= 1.59 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 7,459 796
PAN= 0.89 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 6,664 444
PAN= 0.48 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 6.69 Lbs/Pan/DT
Total five-year max. adjusted PAN = 20.16 Lbs/Pan/DT

Surface Application PAN
Brakebush Brothers - Mocksville
TKN=
69200
mg/kg
NH3=
3770
mg/kg
NO3-NO2-N=
108
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 65,430 1,885 108.00
PAN= 56.33 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 65,430 26,172
PAN= 15.70 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 39,258 7,852
PAN= 6.70 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 31,406 3,350
PAN= 3.74 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 28,056 1,870
PAN= 2.03 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 28.17 Lbs/Pan/DT
Total five-year max. adjusted PAN = 84.50 Lbs/Pan/DT

Injection Application PAN
Brakebush Brothers - Mocksville
TKN=
69200
mg/kg
NH3=
3770
mg/kg
NO3-NO2-N=
108
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 65,430 3,770 108.00
PAN= 60.10 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 65,430 26,172
PAN= 15.70 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 39,258 7,852
PAN= 6.70 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 31,406 3,350
PAN= 3.74 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 28,056 1,870
PAN= 2.03 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 28.17 Lbs/Pan/DT
Total five-year max. adjusted PAN = 88.27 Lbs/Pan/DT

Surface Application PAN
Hunter Farms -High Point
TKN= 12000 mg/kg
NH3= 78 mg/kg
NO3-NO2-N= 10 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 11,922 39 10.00
PAN= 9.64 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 11,922 4,769
PAN= 2.86 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 7,153 1,431
PAN= 1.22 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,723 610
PAN= 0.68 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 5,112 341
PAN= 0.37 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.13 Lbs/Pan/DT
Total five-year max. adjusted PAN = 14.77 Lbs/Pan/DT

Injection Application PAN
Hunter Farms -High Point
TKN= 12000 mg/kg
NH3= 78 mg/kg
NO3-NO2-N= 10 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 11,922 78 10.00
PAN= 9.71 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N1 * 0.002
0.20 11,922 4,769
PAN= 2.86 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N1 * 0.002
0.11 7,153 1,431
PAN= 1.22 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N1 * 0.002
0.07 5,723 610
PAN= 0.68 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N1 * 0.002
0.04 5,112 341
PAN= 0.37 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.13 Lbs/Pan/DT
Total five-year max. adjusted PAN = 14.85 Lbs/Pan/DT

Surface Application PAN
Mathis-1 Storage (Preliminary Composite)
TKN=
100000
mg/kg
NH3=
3990
mg/kg
NO3-NO2-N=
145
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 96,010 1,995 145.00
PAN= 81.09 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 96,010 38,404
PAN= 23.04 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 57,606 11,521
PAN= 9.83 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 46,085 4,916
PAN= 5.49 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 41,169 2,745
PAN= 2.98 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 41.34 Lbs/Pan/DT
Total five-year max. adjusted PAN = 122.43 Lbs/Pan/DT

Injection Application PAN
Mathis-1 Storage (Preliminary Composite)
TKN=
100000
mg/kg
NH3=
3990
mg/kg
NO3-NO2-N=
145
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 96,010 3,990 145.00
PAN= 85.08 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 96,010 38,404
PAN= 23.04 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 57,606 11,521
PAN= 9.83 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 46,085 4,916
PAN= 5.49 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 41,169 2,745
PAN= 2.98 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 41.34 Lbs/Pan/DT
Total five-year max. adjusted PAN = 126.42 Lbs/Pan/DT

Surface Application PAN
River Valley Ingredients (Tyson) -Harmony
TKN=
32000
mg/kg
NH3=
21000
mg/kg
NO3-NO2-N=
90
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 11,000 10,500 90.00
PAN= 29.98 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 11,000 4,400
PAN= 2.64 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 6,600 1,320
PAN= 1.13 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,280 563
PAN= 0.63 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N Sth year min. - N] * 0.002
0.04 4,717 314
PAN= 0.34 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 4.74 Lbs/Pan/DT
Total five-year max. adjusted PAN = 34.72 Lbs/Pan/DT

Injection Application PAN
River Valley Ingredients (Tyson) -Harmony
TKN=
32000
mg/kg
NH3=
21000
mg/kg
NO3-NO2-N=
90
mg/kg
Min Rate=
0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 11,000 21,000 90.00
PAN= 50.98 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 11,000 4,400
PAN= 2.64 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 6,600 1,320
PAN= 1.13 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,280 563
PAN= 0.63 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N Sth year min. - N] * 0.002
0.04 4,717 314
PAN= 0.34 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 4.74 Lbs/Pan/DT
Total five-year max. adjusted PAN = 55.72 Lbs/Pan/DT

Surface Application PAN
Tyson -Wilkesboro
TKN= 6200 mg/kg
NH3= 1400 mg/kg
NO3-NO2-N= 33 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 4,800 700 33.00
PAN= 5.31 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 4,800 1,920
PAN= 1.15 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 2,880 576
PAN= 0.49 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 2,304 246
PAN= 0.27 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 2,058 137
PAN= 0.15 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 2.07 Lbs/Pan/DT
Total five-year max. adjusted PAN = 7.37 Lbs/Pan/DT

Injection Application PAN
Tyson -Wilkesboro
TKN= 6200 mg/kg
NH3= 1400 mg/kg
NO3-NO2-N= 33 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO21 * 0.002
0.40 4,800 1,400 33.00
PAN= 6.71 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N1 * 0.002
0.20 4,800 1,920
PAN= 1.15 LBS/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N1 * 0.002
0.11 2,880 576
PAN= 0.49 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N1 * 0.002
0.07 2,304 246
PAN= 0.27 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N1 * 0.002
0.04 2,058 137
PAN= 0.15 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 2.07 Lbs/Pan/DT
Total five-year max. adjusted PAN = 8.77 Lbs/Pan/DT

ATTACHMENT - D:
ANALYTICAL DATA for RESIDUALS

ADVANCE PIERRE FOODS - CLAREMONT, NC

0
aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:V118101
Date Completed:10/02/2020
10/05/2020 4:00 PM
Approved and released by:
Project Manager II: Lucas Odom
pCC/►F�
24r�14A
"
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: V118101
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: V118101
Sample Number Sample ID Matrix Date Sampled Date Received
001 Perdue/Concord Solid 09/17/20201430 09/18/2020
002 Advanced Foods/Claromont Solid 09/17/2020 1530 09/18/2020
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: V118101
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Perdue/Concord
Solid
% Volatile Solids
SM 2540G-
87 B
%
5
001
Perdue/Concord
Solid
Ammonia - N (gas
350.1
6700
mg/kg
5
001
Perdue/Concord
Solid
Nitrate -Nitrite - N (soluble)
353.2
23
mg/kg
5
001
Perdue/Concord
Solid
Phosphorus
365.1
1200
mg/kg
5
001
Perdue/Concord
Solid
TKN
351.2
22000
mg/kg
5
001
Perdue/Concord
Solid
Aluminum
6010D
17000
mg/kg
5
001
Perdue/Concord
Solid
Copper
6010D
21
mg/kg
5
001
Perdue/Concord
Solid
Potassium
6010D
4000
mg/kg
5
001
Perdue/Concord
Solid
Sodium
6010D
6600
mg/kg
5
001
Perdue/Concord
Solid
Zinc
6010D
51
mg/kg
5
002
Advanced Foods/Claremont
Solid
% Volatile Solids
SM 2540G-
87 B
%
6
002
Advanced Foods/Claremont
Solid
Ammonia - N (gas
350.1
460
mg/kg
6
002
Advanced Foods/Claremont
Solid
Nitrate -Nitrite - N (soluble)
353.2
58
mg/kg
6
002
Advanced Foods/Claromont
Solid
Phosphorus
365.1
860
mg/kg
6
002
Advanced Foods/Claromont
Solid
TKN
351.2
16000
mg/kg
6
002
Advanced Foods/Claromont
Solid
Aluminum
6010D
17000
mg/kg
6
002
Advanced Foods/Claromont
Solid
Copper
6010D
1200
mg/kg
6
002
Advanced Foods/Claromont
Solid
Nickel
6010D
41
mg/kg
6
002
Advanced Foods/Claromont
Solid
Potassium
6010D
4600
mg/kg
6
002
Advanced Foods/Claromont
Solid
Sodium
6010D
14000
mg/kg
6
002
Advanced Foods/Claromont
Solid
Zinc
6010D
190
mg/kg
6
(21 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client:Terra Renewal Services, Inc. Laboratory ID:VI18101-001
Description: Perdue/Concord Matrix: Solid
Date Sampled:09/17/2020 1430 % Solids: 5.66 09/18/2020 2321
Date Received:09/18/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile
S) SM 2540G-1997
1 09/22/2020 0012 MOM
67398
1 350.1
(Ammonia - N ) 350.1
10 09/24/2020 1047 DMA
67705
1
(Nitrate-Nitr) 353.2
1 09/25/2020 0921 AMR
67984
1
(Phosphorus) 365.1
2 10/02/2020 1638 DMA
10/01/2020 1025 67605
1
(Soil pH meas) 9045D
1 09/21/2020 1617 AAB
67392
1 351.4
(TKN) 351.2
1 09/30/2020 1506 DMA
09/26/2020 0850 67906
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
87 B
%
1
Ammonia - N (gas diffusion)
350.1
6700
1800
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
23
3.5
mg/kg
1
Phosphorus
7723-14-0 365.1
1200
180
mg/kg
1
Soil pH measured in water @ 19.7 ° C
9045D
5.0
su
1
TKN
351.2
22000
440
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 09/21 /2020 1437 JAB2
09/21 /2020 1204 67290
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
1.4
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 09/24/2020 2306 KSH2
09/24/2020 0853 67507
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
17000
110
mg/kg
1
Arsenic
7440-38-2 6010D
ND
4.3
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.4
mg/kg
1
Calcium
7440-70-2 6010D
ND
1400
mg/kg
1
Copper
7440-50-8 6010D
21
2.9
mg/kg
1
Lead
7439-92-1 6010D
ND
2.9
mg/kg
1
Magnesium
7439-95-4 6010D
ND
1400
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
11
mg/kg
1
Nickel
7440-02-0 6010D
ND
11
mg/kg
1
Potassium
7440-09-7 6010D
4000
1400
mg/kg
1
Selenium
7782-49-2 6010D
ND
5.7
mg/kg
1
Sodium
7440-23-5 6010D
6600
1400
mg/kg
1
Zinc
7440-66-6 6010D
51
14
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client:Terra Renewal Services, Inc. Laboratory ID:VI18101-002
Description: Advanced Foods/Claromont Matrix: Solid
Date Sampled:09/17/2020 1530 % Solids: 2.30 09/18/2020 2321
Date Received:09/18/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile
S) SM 2540G-1997
1 09/22/2020 0012 MOM
67398
1 350.1
(Ammonia - N ) 350.1
1 09/24/2020 1055 DMA
67705
1
(Nitrate-Nitr) 353.2
1 09/25/2020 0922 AMR
67984
1
(Phosphorus) 365.1
1 10/02/2020 1633 DMA
10/01/2020 1025 67605
1
(Soil pH meas) 9045D
1 09/21/2020 1622 AAB
67392
1 351.4
(TKN) 351.2
1 09/30/2020 1506 DMA
09/26/2020 0850 67906
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
87 B
%
1
Ammonia - N (gas diffusion)
350.1
460
440
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
58
8.7
mg/kg
1
Phosphorus
7723-14-0 365.1
860
220
mg/kg
1
Soil pH measured in water @ 19.5 ° C
9045D
4.4
su
1
TKN
351.2
16000
1100
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 09/21 /2020 1439 JAB2
09/21 /2020 1204 67290
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
3.3
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 09/24/2020 2312 KSH2
09/24/2020 0853 67507
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
17000
280
mg/kg
1
Arsenic
7440-38-2 6010D
ND
11
mg/kg
1
Cadmium
7440-43-9 6010D
ND
3.5
mg/kg
1
Calcium
7440-70-2 6010D
ND
3500
mg/kg
1
Copper
7440-50-8 6010D
1200
7.0
mg/kg
1
Lead
7439-92-1 6010D
ND
7.0
mg/kg
1
Magnesium
7439-95-4 6010D
ND
3500
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
28
mg/kg
1
Nickel
7440-02-0 6010D
41
28
mg/kg
1
Potassium
7440-09-7 6010D
4600
3500
mg/kg
1
Selenium
7782-49-2 6010D
ND
14
mg/kg
1
Sodium
7440-23-5 6010D
14000
3500
mg/kg
1
Zinc
7440-66-6 6010D
190
35
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia,
SC 29172
[phone]
Fax [phone]
www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
SSeoly Bh++irommcnol Scrvirq, Mr. Pbpc t di
LWu" vurnEcr, Mbfili I X-1 S L•'"I li 4 O'd&- %nrMI &
Sample Receipt her fist (SRC}
Climt,. TF.EIR,L RENEWAL Cooler hispccrcd byidate; JIM 19i: 8;20 T"'LA: V118101
❑ SESI ❑Client 0 UPS❑ Fcd�c U Ulizr;
El '{es
No
1- %V Ve emstody seals presant on the cooler?Y
2- Ifu 2Lnl GH!uv,'c=r�-present, were they intactand unbroken?H
es
Iprigj
No
N
SiTip 1D: NA Cldgrble �Sfrrp T17; NA Tosted by:NA
-A tcnrpemlur,.! upun rt=ipl } Derived (Corrected) temperature upon Mtipt MSOlid Snap -Cup iD; �0-1435
-fs e-SA iC NA eNA DC NA INA T7 NA INA PC
Vclhtul; ❑TomperatumJ3lankOAZainst aatt;es JR Grua 'D: IR0Llr Con-cetion factor: oC
Method or coolant; m Vet 10c 11 Ice :'aolcs ❑ Dr-- fee ❑ None
❑ Yee El NO
Ifictnperature of any ',Dlc—exceeded f.{}'� , wN TSrcjr f lVtanagar C�Jodf"ed'%
❑NA:i'
i PM was � Oohed by.,+ phone f email , face to. Face (circle one).
❑NA'•4. Ist1;c comtne~c-al;cau-ier's pLLl:ing blip totluch-�;cl to lhisRn rt? - --
'5. Were pmper cti kdy praacxluras (mlinquishedfreceived) fcllowod:
21 Y51
❑ No
ye.14
❑ No
6� Ya4U
ND
-
G- Were srunple JDs listod on tho COC?
Wcir sampla IDs listed ❑ri Al s:jmpla carltaincre -
1S.
Ycs
E] No
17.
JZ1 Yas
CI No
Was eollceliutt &6: & tinic iistcd on the [.M] .'
6� -ye&j
9- Vas collecting d & time listed on all sample containers?
El NO
❑ Yea
❑ NO
10, Did all cautaincr label informarino (ID, char., fimo) agroa with the COC?
® Ye,;
I❑ No
I i . Were lam; is to bu perfarmcd I fisted inn the ('QC?
[2- I]id-alt samples arrive in the propor containeis Pir er,ul, it-,-;[ andeor in good coMilm
21 Yes
El No
(unbrulc[i, Jids Un, ate,}'2 _--
[ayes
❑ No
13- Wag s3dc;:uAto sample voJulne available?
Yes
❑ No
114.
Were all within %s the heldbi lime ur ,0E hours. whichever comets timO
ye$
121 No
115.
Worc t,ny same lrs oantainers m issi n laxcess (elm[c ogle) sans Rk6q Nnt lixied nn COC?
El Yes
❑ No
N,
14, For VOA and RSK-17-i r r�n�p1;, vrisrr. bubbles presentap-s:tC°' it diameter)
In ally of QIe VOA vials?
f 1 Yes
Lj No
®h1A
IT Were all DMmotalsv uxiienr sannph2c: rereivM at a pH a F < r
i X- Were all ayanide samples received a a 1FH > 12 and suOide sari las receivod at a pH > 9?
19. WeTo all (< .fmg,1I,) samples frea.DfrestdUal �
Q Ycs
[fin
® NA
❑ Yos
❑ No
® 1+A
el:lr�rin�?
❑ YCis ❑ No ® NA 2.0. %Ve--e client reinurks'rUyLLrsts(i.e. requeMd dIIUTOr_9, L'IS/MSD dasignuioris,trtc...)
1,;unvvLIy
lydmcribed frnm sic COC into the cornraert see -ion in r.IMS? '
Yes No I. Was Ole tio4a nuinber Ilstedon floc r;uUlaincr Ape'.? If yes, Quote Ir HA
Sample Prey-erution (Mist be cornplete'd for'any sample(s) inearrectly prescrvcd or with Iiea(EIaru:n-}
52mplu(s) NA %yere, received inOorrverly prate:-v tl and wr:ru adjLWEd acoordilgly
in rani lv rtmivhr g with NA rrl, rttcirele one; F2SO4, HNO�, HC1, NaOH using SR A NA
-
ime of pruerWat urr NA If lnrnme than one prrscr vati-je s needed. pluse none in the aruninertts below,
Sanlpla(s) MA were rw'aiveh with bubbles `6 Irm in diamicta'.
Sample.;(s) NA _ wee FMGNQcl with TRC � 0.5 :rtp/r. (If kl9 is lie) and were
1usted armrdingly in sample rmeivhtg. *wit:s mjirirtl thivskilfafc (Na2S;L}_) with Shealy ID: NA
SR baroadc labols applied by: E7 B Dtlte; 9r 11G20
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Advanced Foods Claromont
Lot Number:UJ15003
Date Completed:11/05/2019
11 /05/2019 4:46 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
pCCRF�4
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 11

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: UJ15003
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
II[a]INLyNZer,
Due to insufficient sample received, the initial sample amount used for the following sample deviated from
the standard procedure:UJ15003-001. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 11

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terra Renewal Services, Inc.
Lot Number: UJ15003
Sample Number Sample ID Matrix Date Sampled Date Received
001 Advanced Foods Claromont Solid 10/14/2019 1530 10/15/2019
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 11

SHEALY
ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terra
Renewal Services, Inc.
Lot Number: UJ15003
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
Advanced Foods Claromont
Solid
% Volatile Solids SM 2540G-
86
%
5
001
Advanced Foods Claromont
Solid
Ignitability (Pensky-Martens 1010A
>140
° F
5
001
Advanced Foods Claromont
Solid
Nitrate -Nitrite - N (soluble) 353.2
170
mg/kg
5
001
Advanced Foods Claromont
Solid
Phosphorus 365.1
4200
mg/kg
5
001
Advanced Foods Claromont
Solid
TKN 351.2
17000
mg/kg
5
001
Advanced Foods Claromont
Solid
3+4-Methylphenol 8270D
0.089
mg/L
6
001
Advanced Foods Claromont
Solid
Aluminum 6010D
3200
mg/kg
8
001
Advanced Foods Claromont
Solid
Copper 6010D
1500
mg/kg
8
001
Advanced Foods Claromont
Solid
Sodium 6010D
26000
mg/kg
8
001
Advanced Foods Claromont
Solid
Zinc 6010D
270
mg/kg
8
(10 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 11

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15003-001
Description: Advanced Foods Claromont Matrix: Solid
Date Sampled:10/14/2019 1530 % Solids: 1.02 10/16/2019 0040
Date Received:10/15/2019
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile S) SM 2540G-1997
1 10/20/2019 2138 MOM
32627
1 350.1
(Ammonia - N ) 350.1
5 10/18/2019 1621 DMA
32376
1
(Ignitability) 1010A
1 10/24/2019 1458 SLC
33236
1
(Nitrate-Nitr) 353.2
1 10/18/2019 2208 AMR
32544
1
(Phosphorus) 365.1
1 10/24/2019 1010 DMA
10/23/2019 1429
32936
1
(Reactive Cya) 7.3.3
1 10/22/2019 2122 KFE
10/16/2019 1034
1
(Reactive Sul) 7.3.4
1 10/21/2019 1622 HET
10/16/2019 1034
1
(Soil pH meas) 9045D
1 10/21/2019 2119 HET
32774
2 351.4
(TKN) 351.2
1 10/22/2019 1442 HKL
10/18/2019 1654
32537
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-
86
%
1
Ammonia - N (gas diffusion)
350.1
ND
4900
mg/kg
1
Ignitability (Pensky-Martens Closed -Cup)
1010A
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
170
20
mg/kg
1
Phosphorus
7723-14-0 365.1
4200
490
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20 ° C
9045D
5.1
su
1
TKN
351.2
17000
2500
mg/kg
2
TCLP Volatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B
8260B
50 10/26/2019 0331 STM
33432 10/23/2019 2034
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260B
ND
0.25
mg/L
1
2-Butanone (MEK)
78-93-3 8260B
ND
0.50
mg/L
1
Carbon tetrachloride
56-23-5 8260B
ND
0.25
mg/L
1
Chlorobenzene
108-90-7 8260B
ND
0.25
mg/L
1
Chloroform
67-66-3 8260B
ND
0.25
mg/L
1
1,2-Dichloroethane
107-06-2 8260B
ND
0.25
mg/L
1
1,1-Dichloroethene
75-35-4 8260B
ND
0.25
mg/L
1
Tetrachloroethene
127-18-4 8260B
ND
0.25
mg/L
1
Trichloroethene
79-01-6 8260B
ND
0.25
mg/L
1
Vinyl chloride
75-01-4 8260B
ND
0.050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
93 70-130
Bromofluorobenzene
93 70-130
Toluene-d8
97 70-130
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 11

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15003-001
Description: Advanced Foods Claromont Matrix: Solid
Date Sampled:10/14/2019 1530 % Solids: 1.02 10/16/2019 0040
Date Received:10/15/2019
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270D 1 10/28/2019 1932 JCG
10/26/2019 2059 33458 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270D
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270D
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270D
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270D
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270D
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270D
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270D
0.089
0.040
mg/L
1
Nitrobenzene
98-95-3 8270D
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270D
ND
0.20
mg/L
1
Pyridine
110-86-1 8270D
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270D
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270D
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
72 37-129
2-Fluorophenol
53 24-127
Nitrobenzene-d5
57 38-127
Phenol-d5
80 28-128
Terphenyl-d14
96 10-148
2,4,6-Tribromophenol
77 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 10/31 /2019 2005 DAL1
10/30/2019 2135 34009 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
69 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A 1 10/21/2019 1732 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
1700
ug/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above
the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 11

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15003-001
Description: Advanced Foods Claromont Matrix: Solid
Date Sampled:10/14/2019 1530 % Solids: 1.02 10/16/2019 0040
Date Received:10/15/2019
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 3660B/3665A 8082A 1 10/21/2019 1732 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1221
11104-28-2 8082A
ND
1700
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
1700
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
1700
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
1700
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
1700
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
1700
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
101 41-132
Tetrachloro-m-xylene
88 35-106
TCLP Pesticides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /3520C
8081 B 1 10/31 /2019 1933 DAL1
10/28/2019 0015 33512 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5 8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B 1 10/19/2019 0759 KSH2
10/18/2019 1422 32494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
7.6
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 11

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15003-001
Description: Advanced Foods Claromont Matrix: Solid
Date Sampled:10/14/2019 1530 % Solids: 1.02 10/16/2019 0040
Date Received:10/15/2019
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 10/28/2019 0551 LLL
10/27/2019 1845 33481 10/23/2019 0103
1 1311/7470A
7470A
1 10/29/2019 0904 JMH
10/28/2019 1406 33559 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/22/2019 1335 LLL
10/18/2019 1115 32478
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
3200
1900
mg/kg
1
Arsenic
7440-38-2 6010D
ND
70
mg/kg
1
Cadmium
7440-43-9 6010D
ND
23
mg/kg
1
Calcium
7440-70-2 6010D
ND
23000
mg/kg
1
Copper
7440-50-8 6010D
1500
47
mg/kg
1
Lead
7439-92-1 6010D
ND
47
mg/kg
1
Magnesium
7439-95-4 6010D
ND
23000
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
190
mg/kg
1
Nickel
7440-02-0 6010D
ND
190
mg/kg
1
Potassium
7440-09-7 6010D
ND
23000
mg/kg
1
Selenium
7782-49-2 6010D
ND
93
mg/kg
1
Sodium
7440-23-5 6010D
26000
23000
mg/kg
1
Zinc
7440-66-6 6010D
270
230
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 11

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 11

SHEALY ENVIRONMENTAL SERVICES, INC.
Chwh7 of CJrs9oaiv Rev Ord
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 11

SHEALY ENVIRONMENTAL SERVICES, INC.
Shiny Erwinimnanlal :{al\IUS, Inc. Pa l of I
Doeumart Humber: blPM-t SC-14 hf eliw Ik51a. R '201 R
Sample Receipt Checkfist (SRQ
Client, TERRA RENEWAL Crxrler Impeczed byJdate; 1-KIJ f 4 AS-2019 LrA-Y- UJ15003
kleatis ofreceipt ❑ SES1 ❑ Client ❑ 4vJ'S ® FedEx Othm -
❑ Ycs
0 NV I
11_ %1l custody seals present; on the cooler'?
Yes
Na 1 0 NA
2- if custody sods were Z2etE, wee thCw i )ri 4 and unbrokcn?
pli Strip ID: NA Chlorine Strip 1D. NA Tc" 1}Jv: KA
iginal temperahlre upon rvcziFlt I�r1�cr vtd (Come=, d) tcm�plurt upon rG"cipt °4SolidSnsp-Cup li_t-
. 19
5.6 j5.6 :; NA 1,NA oC. N.A .INA ll NA 1 ryA 4C.
[Ne3ltad ❑Temperatut� 131ank �A 9inSt aottles IR Gun [D, 5 I Gun CortGCSioa Factor:
Method of coolant: ® Wet ice ❑ lee Faaks ❑ Lhy Ice ❑ Nona
Ilti I
.0
❑ Yes
Ll No
V.�i
1. If tcmperaturr of any cooker exceeded 6.U11C, xas Project h1anaSer Notified?
PM was Netitied by: phorta ? emaiI1 face-to-face (Circle one).
Yee
❑ No
❑-14 A
d. 1s the ceromtxLxi31 courier's packing slip attached to this farin7
VC.-S
❑ 7Kn
15_ Wert prn[ier cilst,�rly prrimrir,rm (reliin[luishedlreceived) followed"
gJ Yl
NLt
6. WeLe mmple ]1DIs listed Orr Elie CDC?
Yesi
No
7_ were sample IN listed on all sarloplc aantaiuc,s7
Yes
❑ No
$_ Was collecfi[tt] daxtc & film liblw Lan IhoCOC?
® Yee
❑ Mi
9_ Was collection date & tulle Ikted on all srrrltpie ounlaincm?
0 Y'cs
❑ N,�
10. Did all container label information (JD, data, lime) at� llvith Iha COC?
(Z Yes
No
1 ] , Wit re Lests to be perform d listed on the UOC7
ICI
El {1
12, Did all samples arrive in the proper containers for cash test and+or i11 good conditi
{unbroken, ]ids a1L etc.)?
>i
®''&;
No
IJ.Was adequatesamplevcplumeavcAi hle^
® Yk
❑ Now
] 4- Were all samples rcudvcd within K the holding time or 4.3 hn11rp, whichever coal
first?
Yes
No
15_ Were au), samples conilaiver's rfussi. tglexucis (cir-lu orw) sal les Not listed on C QC?
❑ 'l
❑ No
❑TEA
16, Ir+r VOA and RSK-175 samples, were bubbles par-ceut `pea -site" (W'ur 6mm in
Iu auy of the VOA vials?
diameter)
[] Y�
7C No
66 KA
1 7_ Weil all DRp. uu-,1Wsr[:utrie[Lt samples moceived at a pl4 txf <: 2?
❑ Y
No
ONA
l S. 5b`l all c anide ll receive l aft a pH > 12 and sulfide sale les neEeiVed st a }
H �- 9?
El Yes
❑ Na
®lvh
l _ Were a[] applieah4e l'[i< N-1a,�T�4Iu}�{�nidu phKmo4'62S (< 0.SrrrgJL) samples t afro
chlorine°
idual
Ye-
❑ No
®NA
20. Were l lent remark -.II Ljts%(i.a. nxtuotcd dilutions, lirlSrhiSD designations, rn
correctly transcribed from the C{:ii'. infra u1be commcra BOCtion in UMS?
,)
❑ ` is
Ate
21. ► a' '.he (I uotc I-unibcr Ilatcd or. the cowziirrer I'll ? if yz5, mote # NA
E.-AmplePrimervation lMust be completed for any sMlnplc(�,) irrcarrret ly preserv&d or with hcadspaoe. )
5zmple(s) NA _ were received incon=dy presmcd and were adjuswd
;I sal.nplc receiving with NA m1-rat circle ore, F125G-7, HNO3, HC'J, NaOl I usutg SF, q NA ._ .
iltno of presexvation NA Ifwnre tlLpn orw pn:.scrvative is nee d plea_ge note in the corrunerrts below.
ar lirtgly
Sample(&) NA were reel with bubbles >6 m m in d i
meter_
alnples(s) NA were received with TRC ,- 0_5 uiF L (if H 19 is Itrr) tot
ae'usl&J ice(nAingl[y in samplc receiving with radium fhiosul*atc wiEli S}re4y iD. NIA
were
SR barcode labels applied by; LKJI Tla1e: 10-15-2019
Cotnmerts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 11

Analytical Results �,* STATESVILLE
ANALYTICAL
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 09/17/2020
Reported: 09/18/2020
For: Claremont Advance
Comments: GM <452 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200917-16-01
Fecal Coliforms
1
<361
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-01
Percent Solids
1
5.54
%
SM2540B-2011
09/17/2020
WC
200917-16-02
Fecal Coliforms
2
<428
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-02
Percent Solids
2
4.67
%
SM2540B-2011
09/17/2020
WC
200917-16-03
Fecal Coliforms
3
<394
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-03
Percent Solids
3
5.07
%
SM2540B-2011
09/17/2020
WC
200917-16-04
Fecal Coliforms
4
<515
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-04
Percent Solids
4
3.88
%
SM2540B-2011
09/17/2020
WC
200917-16-05
Fecal Coliforms
5
<372
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-05
Percent Solids
5
5.37
%
SM2540B-2011
09/17/2020
WC
200917-16-06
Fecal Coliforms
6
<581
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-06
Percent Solids
6
3.44
%
SM2540B-2011
09/17/2020
WC
200917-16-07
Fecal Coliforms
7
<571
MPN/g
SM92210E-2006
09/17/2020
WC
200917-16-07
Percent Solids
7
3.50
%
SM254OB-2011
09/17/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 200917-16-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200917-16-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200917-16-03
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200917-16-04
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200917-16-05
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200917-16-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200917-16-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

BRAKEBUSH BROTHERS - MOCKSVILLE, NC

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
May 16, 2017
David Covle
Terra Renewal Services
P.O. Box 399
Dardanelle AR 72834
TEL: [phone]
FAX:
RE: House of Raeford - Mocksville
Dear David Coyle: Order No: 1705529
Analytical Environmental Services, Inc. received 1 samples on 5/5/2017 10:25:00 AM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative. AES' certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/16-06/30/17.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent,
effective until 12/31/16.
-South Carolina Environmental Laboratory Certification number 98016003 effective until
6/30/17.
These results relate only to the items tested. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Chris Pafford
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: 770.457_S188 • Toll F.,e:800.972.4889
www.aesatlanta.com
Page 1 of 38

ANALYTICAL ENVIRONMENTAL SERVICES, INC
3080 Presidential Drive Atlanta GA 30340- 3906
TEL.: [phone] / TOLL -FREE [phone] / FAX [phone]
CHAIN OF CUSTODY
Work Order. OnWa I
Date: 5/4/17 Page or 2
'DNII'ANY;
ADDRESS:
ANALYSIS REQUESTED
Terra Renewal Services
P.O. Box 399
Malt e
Dardanelle, AR 72834
atl ntaxwebsi
tiv�v�v.aesttlagta,coen to
E
check ou the status of
y our results, place bottle
Orders, etc,
v
PHONE: [phone]
Fix;
SA?,IPLPD BY:
SIO
Todd Hayden
�C
a)
SAMPLED
z
(See Seocodes)
t!
SAMPLER)
r o
REMARKS
DATE
TNIE
i
J
House of Raeford - Dobson
5/4/17
3:30 PM
f
Sludge
v(
2
2
3
,/
S
z
R
9
Jrt
JJ
11
13
Jr
RELINQUISHHDBY DATE/TIME
RECEIVEDBY DATF/TIME
PI203ECTINFORMATION
RECEIPT
1:
1 /f/y/f7
PROJFCT NAME:
House of Raeford -Dobson
TutalkofContainets
2
�01) laAy� �I S y /� 5, 7n�ti
/0; 25
2:
2- LI
PROJECT i :
Turnaround Time Request
M Standard S Business Days
2 Business Dap Rush
SITE ADDRESS:
Dobson, NC
3:
3:.
® Next Business Day Rush
❑ Same Day Rush (atrtlr req.)
SEND REPORT TO: david,[e-mail]
SPECIAL INS'IRUCTIONSICOtti1I4tEN'IS:
SHIPMENT MFTBOD
INVOICE TO:
OUT VIA:
(IF DIFFERENT FROM ABOVE)
Other
STATE PROGRAMti
Cif any):
IN i ( VIA:
Contact Vanya Colburn for PO
rjCLIENT edEx ❑UPSa4AH_[]COURlER
E-mail7 Y/ N: Fax": Y I N
GREYf OUND Q)THER_
QUO'FE#:•_—` PO/J:
DATAPACKAOR I[]II QIQIV
SAMPLES RECEIVED AT1'Cft 3PNI OR ON SATURDAY ARE CONSIDERED RECEIVED TIIE NEXT BUSINESS DAY, IF NO TAT IS AIARKF1) ON COC AES WILL PROCEED NVITII STANDARD'I'AT,
SAMPLES ARE DISPOSED OF 30 DAYS AFTER CONIPLETION OF REPORT UNLL;SS OTHER ARRANGEN11sNTS ARE MADE,
MATRI\CODES: A=Air GIN =Groundwater SE Sedimeat SO=Soil SW=Surface Water W = Water(Blanks) WR'=\Vastewatar DW=DrinkinhWater O= ther(specify)
PRFSERVATIVECODES: H+1=I-Ndrochloricacid +ice I=Ice only N=Nitrioncid S+1=Sulfuric acid+ice St41+I=Sodium BisulfateAtethanol+ice O=Othcr(specifv) NA=None
Page 2 of 38

1 �V5 5Z1
North Carolina Permit Parameters
2_ Residuals shall be analyzed to demonstrate the are aaaens-� source Conservation
and Recovery Act (RCRA). The anal es ycorrosivity, i:gnitability, reactivii and toxicity
characteristic leaching procedure TCLP shalt" 6 zfiarmcd-' equency specified in
Attachment A, and the Permittee shall maintai these results for a minimum of five years. Any
exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per lister
is in parentheses):
Arsenic (5.0)
1,4 Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2 Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexaehlorobenzene (0.13)
Tetrachloroethylene (03)
Chlorobenzene (100A)
Heptachlor (and its hydroxide)
(0.008)
Toxa (0.5)
henep ( )
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2A6 Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2 4-D (IO.0)
4yj ethyt ketone. 200.0
X5t1
3. An .analysis shall be conducted on residuals from each source generating facility at the frequency
specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall .include the following parameters:
ti
4
C
W
W
ly
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium.
Cadmium
Nitrate=Nitrite Nitrogen
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Volatile Solids
Magnesium
PC$'s
TERRA RENEWAL SERVICES
479-747-8192
WQ0036936 Version 1.0 Shell Version 140210 Page 8 of 12
Page 3 of 38

Analytical Environmental Services, Inc
Date: 16-May-17
Client: Terra Renewal Services
Project: House of Raeford - Mocksville Case Narrative
Lab ID: 1705529
Sample Receiving Nonconformance:
Sample ID listed on the Chain of Custody was "House of Raeford -Dobson" however the bottle label listed the sample ID as
"House of Raeford Mocksville". No collection date or time was listed on the bottle label to confirm the sample identity. Per
David Coyle via phone 05-05-17@12.10 the samples are the correct ones and should be reported according to the sample
labels.
pH Analysis by Method 9045D:
Samples for pH analysis by Method SW9045D were received and analyzed outside holding time requirement of "immediate or
15 minutes."
Semi -Volatile Organics Analysis by Method 8270D/1311:
LCS-242443 recovery for o-Cresol, m,p-Cresol, Cresols, Total was outside control limits biased high. Target analyte was not
detected in the analytical samples and data is reportable with high bias.
Page 4 of 38

Analytical Environmental Services, Inc
Date: 16-May-17
Client:
Terra Renewal Services
Client Sample ID:
House of Raeford - Mocksville
Project Name:
House of Raeford - Mocksville
Collection Date:
5/4/2017 3:30:00 PM
Lab ID:
1705529-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatchID
Dilution
Factor
Date Analyzed Analyst
VOLATILES, TCLP SW1311/8260B
(SW5030B)
1, 1 -Dichloroethene
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
1,2-Dichloroethane
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
2-Butanone
BRL
0.20
mg/L 242362
20
05/11/2017 15:55
LJ
Benzene
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Carbon tetrachloride
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Chlorobenzene
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Chloroform
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Tetrachloroethene
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Trichloroethene
BRL
0.10
mg/L 242362
20
05/11/2017 15:55
LJ
Vinyl chloride
BRL
0.040
mg/L 242362
20
05/11/2017 15:55
LJ
Surr:4-Bromofluorobenzene
85.9
68.3-122
%REC 242362
20
05/11/2017 15:55
LJ
Surr: Dibromofluoromethane
107
70.1-125
%REC 242362
20
05/11/2017 15:55
LJ
Surr: Toluene-d8
90.7
81.4-120
%REC 242362
20
05/11/2017 15:55
LJ
Total Phosphorus, soils E365.1
(E365.1)
Phosphorus, Total (As P)
11300
226
mg/Kg-dry 242258
1
05/09/2017 15:39
FS
TOTAL MERCURY SW7471B
(SW7471B)
Mercury
BRL
1.98
mg/Kg-dry 242284
1
05/10/201711:40
AS
Sulfide, Reactive SW846-7.3
(SW7.3.4.2)
Sulfide, Reactive
BRL
100
mg/Kg 242455
1
05/09/2017 10:15
BD
SEMIVOLATILES ORGANICS, TCLP SW1311/8270D
(SW3510C)
1,4-Dichlorobenzene
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
2,4,5-Trichlorophenol
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
2,4,6-Trichlorophenol
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
2,4-Dinitrotoluene
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Hexachlorobenzene
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Hexachlorobutadiene
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Hexachloroethane
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
m,p-Cresol
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Nitrobenzene
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
o-Cresol
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Pentachlorophenol
BRL
0.50
mg/L 242443
1
05/12/201716:21
YH
Pyridine
BRL
0.10
mg/L 242443
1
05/12/201716:21
YH
Cresols, Total
BRL
0.10
mg/L 242443
1
05/12/2017 16:21
YH
Surr:2,4,6-Tribromophenol
109
52.1-146
%REC 242443
1
05/12/201716:21
YH
Surr:2-Fluorobiphenyl
93
50.7-134
%REC 242443
1
05/12/201716:21
YH
Surr:2-Fluorophenol
73
47-122
%REC 242443
1
05/12/201716:21
YH
Surr:4-Terphenyl-dl4
107
54.4-139
%REC 242443
1
05/12/201716:21
YH
Qualifiers: • Value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not confirmed
B Analyte detected in the associated method blank
<
Less than Result value
> Greater than Result value
J
Estimated value detected below
Reporting Limit
Page 5 of 38

Analytical Environmental Services, Inc
Date: 16-May-17
Client:
Terra Renewal Services
Client Sample ID:
House of Raeford - Mocksville
Project Name:
House of Raeford - Mocksville
Collection Date:
5/4/2017 3:30:00 PM
Lab ID:
1705529-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
SEMIVOLATILES ORGANICS, TCLP
SW1311/8270D
Surr: Nitrobenzene-d5
74.4
46.4-135
Surr: Phenol-d5
72.5
48.2-122
Residue, Volatile (SM2540G)
Residue, Volatile
90.0
0.00100
POLYCHLORINATED BIPHENYLS
SW8082A
Aroclor 1016
BRL
780
Aroclor 1221
BRL
780
Aroclor 1232
BRL
780
Aroclor 1242
BRL
780
Aroclor 1248
BRL
780
Aroclor 1254
BRL
780
Aroclor 1260
BRL
780
Surr: Decachlorobiphenyl
80.8
43.2-138
Surr: Tetrachloro-m-xylene
87.1
46-128
PESTICIDES, TCLP SW1311/8081B
Chlordane
BRL
0.0050
Endrin
BRL
0.0010
gamma-BHC
BRL
0.00050
Heptachlor
BRL
0.00050
Heptachlor epoxide
BRL
0.00050
Methoxychlor
BRL
0.0050
Toxaphene
BRL
0.050
Surr: Decachlorobiphenyl
58.5
35.2-135
Surr: Tetrachloro-m-xylene
69.1
47-133
Nitrogen, total Kjeldahl (TKN) Extractable
E351.2M
Nitrogen, total Kjeldahl(TKN)Extractable
69200
5770
Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
Nitrogen, Nitrate-Nitrite(as N)Extractable
BRL
108
Nitrogen, Ammonia (as N) Extractable
E350.1 MOD
Nitrogen, Ammonia (As N) Extractable
3770
233
MERCURY, TCLP SW1311/7470A
Mercury
BRL
0.00400
Laboratory Hydrogen Ion (pH) SW9045D
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW3510C)
%REC 242443
%REC 242443
(E160.4)
wt% 242480
(SW3550C)
ug/xg-drY 242248
ug/xg-drY 242248
ug/xg-drY 242248
ug/xg-drY 242248
ug/xg-drY 242248
ug/xg-drY 242248
ug/xg-drY 242248
%REC 242248
%REC 242248
(SW3510C)
mg/L 242436
mg/L 242436
mg/L 242436
mg/L 242436
mg/L 242436
mg/L 242436
mg/L 242436
%REC 242436
%REC 242436
(E351.2 MOD)
mg/Kg-dry 242204
(E353.2 MOD)
mg/Kg-dry 242539
(E350.1)
mg/xg-dry 242257
(SW7470A)
mg/L 242419
(SW9045D)
1 05/12/201716:21 YH
1 05/12/201716:21 YH
1 05/10/201713:00 JC
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/09/2017 20:38
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
1 05/12/2017 13:41
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
SH
5 05/08/201714:29 TL
1 05/12/201711:55 AM
1 05/09/201710:42 FS
1 05/14/201717:43 AS
E
Estimated (value above quantiitatiion range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not continued
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 6 of 38

Analytical Environmental Services, Inc
Date: 16-May-17
Client:
Terra Renewal Services
Client Sample ID:
House of Raeford - Mocksville
Project Name:
House of Raeford - Mocksville
Collection Date:
5/4/2017 3:30:00 PM
Lab ID:
1705529-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Laboratory Hydrogen Ion (pH) SW9045D
(SW9045D)
pH
3.78
0.01
H pH Units 242503
1
05/11/2017 14:00
BD
Ignitability SW1010A
Ignitability
180
0
> °F R342794
1
05/10/201716:05
JC
ICP METALS, TCLP SW1311/6010C
(SW3010A)
Arsenic
BRL
0.250
mg/L 242466
1
05/12/201714:05
IO
Barium
BRL
0.500
mg/L 242466
1
05/12/201714:05
IO
Cadmium
BRL
0.0250
mg/L 242466
1
05/12/201714:05
IO
Chromium
BRL
0.0500
mg/L 242466
1
05/12/201714:05
IO
Lead
BRL
0.0500
mg/L 242466
1
05/12/201714:05
IO
Selenium
BRL
0.100
mg/L 242466
1
05/12/201714:05
IO
Silver
BRL
0.0250
mg/L 242466
1
05/12/201714:05
IO
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.20
mg/L 242439
1
05/12/2017 16:26
AW
2,4-D
BRL
0.20
mg/L 242439
1
05/12/2017 16:26
AW
Surr: DCAA
86.3
50.1-132
%REC 242439
1
05/12/2017 16:26
AW
Fixed Residues (SM2540G)
% Total Solids
4.30
0.00100
wt% R342849
1
05/10/2017 13:00
JC
Cyanide, Reactive SW846-7.3
(SW7.3.3.2)
Cyanide, Reactive
BRL
1.00
mgxg 242554
1
05/12/2017 10:00
BD
METALS, TOTAL SW6010D
(SW3050B)
Aluminum
17300
444
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Arsenic
BRL
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Cadmium
BRL
22.2
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Calcium
1180
444
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Copper
BRL
22.2
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Lead
BRL
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Magnesium
500
444
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Molybdenum
BRL
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Nickel
BRL
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Potassium
1680
888
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Selenium
BRL
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Sodium
6600
888
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
Zinc
48.2
44.4
mg/Kg-dry 242449
1
05/11/2017 20:00
IO
PERCENT MOISTURE D2216
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not continued
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 7 of 38

Analytical Environmental Services, Inc
Date: 16-May-17
Client:
Terra Renewal Services
Client Sample ID:
House of Raeford - Mocksville
Project Name:
House of Raeford - Mocksville
Collection Date:
5/4/2017 3:30:00 PM
Lab ID:
1705529-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
PERCENT MOISTURE D2216
Percent Moisture 95.7 0 wt% R342849 1 05/10/2017 13:00 JC
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not continued
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 8 of 38

ANALyncAL
JENmommENTAL
"S SERVICES, INC.
1. Client Name: TERRA RENEWAL
2. Carrier: FeclEx ❑• ups ❑ uSPS ❑ Client ❑ Courier[-] Othei
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
Clear
SAMPLE/COOLER RECEIPT CHECKLIST
AES Work Order Number: 1705529
Yes No N/A Details Comments
Save as
Shipping container/cooler received in good condition?
U
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
•
Temperature blanks present?
0•
Cooler temperature(s) within limits of 04C? [See item 13 and 14 for
temperature recordings.]
O
O
O
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (CDC) present?
•
Chain of Custody signed, dated, and timed when relinquished and received?
Sampler name and/or signature on COC?Were
all samples received within holding time?
IF�
TAT marked on the COC?
If no TAT indicated, proceeded with standard TAT per Terms & Conditions. ❑
13. Cooler 1 Temperature 5.4 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27. Comments:
28.
29.
30.
°C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials). AJ 5/4/17
Yes No N/A Details Comments
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
0•
Custody seals intact on sample containers?
0•
Do sample container labels match the COC?
O
O
O
incomplete info ❑ illegible ❑
no label ❑ other 0
See Narrative
Are analyses requested indicated on the COC?
-
Were all of the samples listed on the CDC received?
O
O
O
samples received but not listed on COC ❑
samples listed on COC not received ❑
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•
Were samples received in appropriate containers?
•
O
Were VOA samples received without headspace (< 1/4" bubble)?
•
Were trip blanks submitted?
0O
•
listed on COC ❑ not listed on COC ❑
I certify that I have completed sections 16-27 (dated initials). AJ 5/4/17
Yes No N/A Details Comments
Have containers needing chemical preservation been checked? •
Containers meet preservation guidelines? •
Was pH adjusted? •
I certify that I have completed sections 28-30 (dated initials). AJ 5/4/17
Checklist 1/19/17 Rev 0.
Locked
Page 9 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services
Project Name: House of Raeford - Mocksville Dates Report
Lab Order: 1705529
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name
TCLP Date
Prep Date
Analysis Date
1705529-001A
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
VOLATILES, TCLP Leached
05/10/2017
5/10/2017 10:01:00 AM
05/11/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
IGNITABILITY
05/10/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
TCLP SEMIVOLATILES ORGANICS
05/10/2017
5/12/2017 9:00:00 AM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
HERBICIDES, TCLP Leached
05/10/2017
5/11/2017 4:30:00 PM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
MERCURY, TCLP Leached
05/10/2017
5/12/2017 1:40:00 PM
05/14/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
ICP METALS, TCLP Leached
05/10/2017
5/11/2017 1:24:00 PM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
PESTICIDES, TCLP Leached
05/10/2017
5/11/2017 4:30:00 PM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Residue, Volatile by 160.4/SM2540G
5/10/2017 2:00:00 PM
05/10/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Nitrogen, Ammonia (as N) Extractable
5/8/2017 4:00:00 PM
05/09/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Nitrogen, total Kjeldahl (TKN) Extractable
5/8/2017 9:30:00 AM
05/08/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Nitrogen, Nitrate -Nitrite (as N) Extractable
5/11/2017 4:00:00 PM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Total Phosphorus, soils
5/9/2017 8:35:00 AM
05/09/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
TOTAL METALS BY ICP
5/11/2017 11:41:00 AM
05/11/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Cyanide, Reactive
5/12/2017 10:00:00 AM
05/12/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Sulfide, Reactive
5/9/2017 10:15:00 AM
05/09/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
MERCURY
5/9/2017 1:18:00 PM
05/10/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
POLYCHLORINATED BIPHENYLS
5/8/2017 4:00:00 PM
05/09/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Laboratory Hydrogen Ion (pH)
5/11/2017 2:00:00 PM
05/11/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
PERCENT MOISTURE
05/10/2017
1705529-001 B
House of Raeford - Mocksville
5/4/2017
3:30:OOPM
Sludge
Fixed Residues (SM2540G)
05/10/2017
Page 10 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242204
Sample ID: MB-242204
Client ID:
Units: mg/Kg
Prep Date: 05/08/2017
Run No: 342462
SampleType: MBLK
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 242204
Analysis Date: 05/08/2017
Seq No: 7503707
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta BRL 50.0
Sample ID: LCS-242204
Client ID:
Units: mg/Kg
Prep Date: 05/08/2017
Run No: 342462
SampleType: LCS
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 242204
Analysis Date: 05/08/2017
Seq No: 7503708
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 1020 50.0 1000 26.40 99.4 90 110
Sample ID: 1705610-001BMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/08/2017
Run No: 342462
SampleType: MS
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchlD: 242204 Analysis Date: 05/08/2017
Seq No: 7503729
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 141000 8440 33780 106400 103 90 110
Sample ID: 1705610-001BMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/08/2017
Run No: 342462
SampleType: MSD
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 242204 Analysis Date: 05/08/2017
Seq No: 7503732
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 135400
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
8620 34460 106400 84.3 90 110 141000 4.03 30 S
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 11 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242248
Sample ID: MB-242248
Client ID:
Units: ug/Kg
Prep Date: 05/08/2017
Run No: 342741
SampleType: MBLK
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 242248
Analysis Date: 05/09/2017
Seq No: 7511125
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
BRL
33
Aroclor 1221
BRL
33
Aroclor 1232
BRL
33
Aroclor 1242
BRL
33
Aroclor 1248
BRL
33
Aroclor 1254
BRL
33
Aroclor 1260
BRL
33
Sum Decachlorobiphenyl
14.95
0 16.67 89.7 43.2 138
Surr: Tetrachloro-m-xylene
17.76
0 16.67 107 46 128
Sample ID: LCS-242248
Client ID:
Units: ug/Kg
Prep Date: 05/08/2017
Run No: 342741
SampleType: LCS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchlD: 242248
Analysis Date: 05/09/2017
Seq No: 7511126
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
146.8
33
166.7
88.0
63.7
117
Aroclor 1260
151.4
33
166.7
90.9
70.8
124
Surr: Decachlorobiphenyl
14.39
0
16.67
86.3
43.2
138
Surr: Tetrachloro-m-xylene
15.80
0
16.67
94.8
46
128
Sample ID: 1705624-004BMS
Client ID:
Units: ug/Kg-dry Prep Date: 05/08/2017
Run No: 342741
SampleType: MS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 242248 Analysis Date: 05/09/2017
Seq No: 7511131
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
204.3
46
230.6
88.6
52.8
125
Aroclor 1260
215.3
46
230.6
93.4
56.4
129
Surr: Decachlorobiphenyl
20.67
0
23.06
89.6
43.2
138
Sum Tetrachloro-m-xylene
21.80
0
23.06
94.5
46
128
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 12 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242248
Sample ID: 1705624-004BMSD
Client ID:
Units: ug/Kg-dry Prep Date: 05/08/2017
Run No: 342741
SampleType: MSD
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 242248 Analysis Date: 05/09/2017
Seq No: 7511132
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
191.1
46
230.6
82.9
52.8
125
204.3
6.68
23.8
Aroclor 1260
202.2
46
230.6
87.7
56.4
129
215.3
6.25
19.2
Surr: Decachlorobiphenyl
19.65
0
23.06
85.2
43.2
138
20.67
0
0
Sum Tetrachloro-m-xylene
20.25
0
23.06
87.8
46
128
21.80
0
0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 13 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242257
Sample ID: MB-242257
Client ID:
Units: mg/Kg
Prep Date: 05/08/2017
Run No: 342602
SampleType: MBLK
TestCode: Nitrogen, Ammonia (as N) Extractable E350.1 MOD
BatchID: 242257
Analysis Date: 05/09/2017
Seq No: 7507043
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable BRL 10.0
Sample ID: LCS-242257
Client ID:
Units: mg/Kg
Prep Date: 05/08/2017
Run No: 342602
SampleType: LCS
TestCode: Nitrogen, Ammonia (as N) Extractable E350A MOD
BatchID: 242257
Analysis Date: 05/09/2017
Seq No: 7507044
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable 105.0 10.0 100.0 105 90 110
Sample ID: 1705640-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/08/2017
Run No: 342602
SampleType: MS
TestCode: Nitrogen, Ammonia (as N) Extractable E350.1 MOD
BatchID: 242257 Analysis Date: 05/09/2017
Seq No: 7507076
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable 8686 2630 526.4 7870 155 90 110 S
Sample ID: 1705705-001BMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/08/2017
Run No: 342602
SampleType: MS
TestCode: Nitrogen, Ammonia (as N) Extractable E350A MOD
BatchlD: 242257 Analysis Date: 05/09/2017
Seq No: 7507087
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractablt 55630 17400 3477 50470 148 90 110 S
Sample ID: 1705640-001AMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/08/2017
Run No: 342602
SampleType: MSD
TestCode: Nitrogen, Ammonia (as N) Extractable E350.1 MOD
BatchID: 242257 Analysis Date: 05/09/2017
Seq No: 7507077
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractablt 8469
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
2610 521.2 7870 115 90 110 8686 2.52 30 S
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 14 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242258
Sample ID: MB-242258
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342606
SampleType: MBLK
TestCode: Total Phosphorus, soils E365.1
BatchID: 242258
Analysis Date: 05/09/2017
Seq No: 7507423
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) BRL 10.0
Sample ID: LCS-242258
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342606
SampleType: LCS
TestCode: Total Phosphorus, soils E365.1
BatchID: 242258
Analysis Date: 05/09/2017
Seq No: 7507424
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 400.0 10.0 400.0 100 90 110
Sample ID: 1705640-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/09/2017
Run No: 342606
SampleType: MS
TestCode: Total Phosphorus, soils E365.1
BatchID: 242258 Analysis Date: 05/09/2017
Seq No: 7507470
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 9904 511 2044 8001 93.1 90 110
Sample ID: 1705640-001AMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/09/2017
Run No: 342606
SampleType: MSD
TestCode: Total Phosphorus, soils E365.1
BatchlD: 242258 Analysis Date: 05/09/2017
Seq No: 7507471
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 9984
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
515 2059 8001 96.3 90 110 9904 0.805 30
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 15 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242284
Sample ID: MB-242284
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342694
SampleType: MBLK
TestCode: TOTAL MERCURY Sw7471B
BatchID: 242284
Analysis Date: 05/09/2017
Seq No: 7510302
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury BRL 0.100
Sample ID: LCS-242284
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342694
SampleType: LCS
TestCode: TOTAL MERCURY sw7471B
BatchID: 242284
Analysis Date: 05/09/2017
Seq No: 7510303
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.4433 0.100 0.4000 ill 80 120
Sample ID: 1705455-007CMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/09/2017
Run No: 342694
SampleType: MS
TestCode: TOTAL MERCURY Sw7471B
BatchID: 242284 Analysis Date: 05/09/2017
Seq No: 7510305
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.5238 0.114 0.4569 0.05108 103 70 130
Sample ID: 1705455-007CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/09/2017
Run No: 342694
SampleType: MSD
TestCode: TOTAL MERCURY Sw7471B
BatchlD: 242284 Analysis Date: 05/09/2017
Seq No: 7510306
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.5290
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
0.114 0.4578 0.05108 104 70
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
130 0.5238 1.00 30
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 16 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242362
Sample ID: MB-242362
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: MBLK
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7510185
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene
BRL
0.10
1,2-Dichloroethane
BRL
0.10
2-Butanone
BRL
0.20
Benzene
BRL
0.10
Carbon tetrachloride
BRL
0.10
Chlorobenzene
BRL
0.10
Chloroform
BRL
0.10
Tetrachloroethene
BRL
0.10
Trichloroethene
BRL
0.10
Vinyl chloride
BRL
0.040
Surr:4-Bromofluorobenzene
0.7942
0 1.000 79.4 68.3 122
Sum Dibromofluoromethane
1.140
0 1.000 114 70.1 125
Surr:Toluene-d8
0.9468
0 1.000 94.7 81.4 120
Sample ID: LCS-242362
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: LCS
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7510184
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene
0.9926
0.10
1.000
99.3
58.8
139
1,2-Dichloroethane
1.075
0.10
1.000
107
64.8
134
2-Butanone
2.682
0.20
2.000
134
57.3
143
Benzene
1.125
0.10
1.000
112
75.4
127
Carbon tetrachloride
1.043
0.10
1.000
104
58.5
144
Chlorobenzene
1.093
0.10
1.000
109
77.9
122
Chloroform
0.9652
0.10
1.000
96.5
66.5
130
Tetrachloroethene
1.071
0.10
1.000
107
73
133
Trichloroethene
1.093
0.10
1.000
109
72.1
132
Vinyl chloride
0.9288
0.040
1.000
92.9
56.1
139
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due
to matrix
Page 17 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242362
Sample ID: LCS-242362
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: LCS
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7510184
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Surr:4-Bromofluorobenzene
1.076
0
1.000
108
68.3
122
Surf: Dibromofluoromethane
1.004
0
1.000
100
70.1
125
Surr:Toluene-d8
1.012
0
1.000
101
81.4
120
Sample ID: 1705221-001AMS
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: MS
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7511387
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1, 1 -Dichloroethene
1.203
0.10
1.000
120
61.9
137
1,2-Dichloroethane
1.198
0.10
1.000
120
60.3
134
2-Butanone
2.219
0.20
2.000
ill
51.8
143
Benzene
1.336
0.10
1.000
134
71.8
130 S
Carbon tetrachloride
1.374
0.10
1.000
137
65.8
133 S
Chlorobenzene
1.242
0.10
1.000
124
72
125
Chloroform
1.115
0.10
1.000 0.01880
110
63.6
130
Tetrachloroethene
1.226
0.10
1.000
123
70.8
135
Trichloroethene
1.307
0.10
1.000
131
70.3
133
Vinyl chloride
1.118
0.040
1.000
112
56.4
139
Sum 4-Bromofluorobenzene
1.032
0
1.000
103
68.3
122
Surr: Dibromofluoromethane
1.053
0
1.000
105
70.1
125
Surr:Toluene-d8
1.079
0
1.000
108
81.4
120
Sample ID: 1705221-001ADUP
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: DUP
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7511388
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene BRL 0.10 0 0 30
1,2-Dichloroethane BRL 0.10 0 0 30
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 18 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242362
Sample ID: 1705221-001ADUP
Client ID:
Units: mg/L
Prep Date: 05/10/2017
Run No: 342680
SampleType: DUP
TestCode: voLAT1LES, TCLP SW1311/8260B
BatchID: 242362
Analysis Date: 05/10/2017
Seq No: 7511388
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2-Butanone
BRL
0.20
0
0 30
Benzene
BRL
0.10
0
0 30
Carbon tetrachloride
BRL
0.10
0
0 30
Chlorobenzene
BRL
0.10
0
0 30
Chloroform
BRL
0.10
0.01880
0 30
Tetrachloroethene
BRL
0.10
0
0 30
Trichloroethene
BRL
0.10
0
0 30
Vinyl chloride
BRL
0.040
0
0 30
Surr:4-Bromofluorobenzene
0.8586
0 1.000
85.9 68.3 122 0.8914
0 0
Surf: Dibromofluoromethane
1.099
0 1.000
110 70.1 125 1.081
0 0
Surr:Toluene-d8
0.9006
0 1.000
90.1 81.4 120 0.9104
0 0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 19 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242419
Sample ID: MB-242419
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342992
SampleType: MBLK
TestCode: MERCURY TCLP SW1311/7470A
BatchID: 242419
Analysis Date: 05/12/2017
Seq No: 7517918
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury BRL 0.00400
Sample ID: LCS-242419
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342992
SampleType: LCS
TestCode: MERCURY TCLP SW1311/7470A
BatchID: 242419
Analysis Date: 05/12/2017
Seq No: 7517919
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.03977 0.00400 0.0400 99.4 80 120
Sample ID: 1705516-001AMS
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342992
SampleType: MS
TestCode: MERCURY, TCLP SW1311/7470A
BatchID: 242419
Analysis Date: 05/12/2017
Seq No: 7517921
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.04041 0.00400 0.0400 101 80 120
Sample ID: 1705516-001AMSD
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342992
SampleType: MSD
TestCode: MERCURY TCLP SW1311/7470A
BatchlD: 242419
Analysis Date: 05/12/2017
Seq No: 7517922
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury
0.04081 0.00400 0.0400
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
102 80
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
120 0.04041 0.973 20
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 20 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242436
Sample ID: MB-242436
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: MBLK
TestCode: PESTICIDES, TCLP SW1311/8081B
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517162
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane
BRL
0.0050
Endrin
BRL
0.0010
gamma-BHC
BRL
0.00050
Heptachlor
BRL
0.00050
Heptachlor epoxide
BRL
0.00050
Methoxychlor
BRL
0.0050
Toxaphene
BRL
0.050
Sum Decachlorobiphenyl
0.004249
0 0.0050 85.0 35.2 135
Surr: Tetrachloro-m-xylene
0.003911
0 0.0050 78.2 47 133
Sample ID: LCS-242436-1
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: LCS
TestCode: PESTICIDES, TCLP SW1311i8081B
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517163
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Endrin
0.008930
0.0010
0.0080
112
67.5
148
gamma-BHC
0.008684
0.00050
0.0080
109
67
141
Heptachlor
0.008185
0.00050
0.0080
102
65.3
138
Heptachlor epoxide
0.009494
0.00050
0.0080
119
73.4
142
Methoxychlor
0.02754
0.0050
0.0300
91.8
57.9
128
Surr: Decachlorobiphenyl
0.004398
0
0.0050
88.0
35.2
135
Surr: Tetrachloro-m-xylene
0.004264
0
0.0050
85.3
47
133
Sample ID: LCS-242436-2
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: LCS
TestCode: PESTICIDES, TCLP SW1311/8081B
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517164
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane 0.04198 0.0050 0.0400 105 74.7 130
Toxaphene 0.07510 0.050 0.0800 93.9 70.2 119
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 21 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242436
Sample ID: LCS-242436-2
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: LCS
TestCode: PESTICIDES, TCLP SWI311/808IB
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517164
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Surr: Decachlorobiphenyl 0.004139 0 0.0050 82.8 35.2 135
Surf: Tetrachloro-m-xylene 0.003720 0 0.0050 74.4 47 133
Sample ID: 1705529-OO1BMS-1
Client ID:
House of Raeford - Mocksville
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: MS
TestCode:
PESTICIDES, TCLP SW1311/8081B
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517169
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Endrin
0.007938
0.0010
0.0080
99.2
59.8
150
gamma-BHC
0.008317
0.00050
0.0080
104
63.8
143
Heptachlor
0.007246
0.00050
0.0080
90.6
55
144
Heptachlor epoxide
0.008540
0.00050
0.0080
107
62.8
146
Methoxychlor
0.02460
0.0050
0.0300
82.0
45.5
133
Surr: Decachlorobiphenyl
0.003323
0
0.0050
66.5
35.2
135
Surr: Tetrachloro-m-xylene
0.003903
0
0.0050
78.1
47
133
Sample ID: 1705529-OO1BMS-2
Client ID:
House of Raeford - Mocksville
Units: mg/L
Prep Date: 05/11/2017
Run No: 342966
SampleType: MS
TestCode:
PESTICIDES, TCLP SWI311/808IB
BatchlD: 242436
Analysis Date: 05/12/2017
Seq No: 7517170
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane
0.04166
0.0050
0.0400
104
63.7
139
Toxaphene
0.07468
0.050
0.0800
93.4
48.8
134
Surr: Decachlorobiphenyl
0.003293
0
0.0050
65.9
35.2
135
Sum Tetrachloro-m-xylene
0.004050
0
0.0050
81.0
47
133
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 22 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242439
Sample ID: MB-242439
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342970
SampleType: MBLK
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchlD: 242439
Analysis Date: 05/12/2017
Seq No: 7517228
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 0.3964 0 0.5000 79.3 50.1 132
Sample ID: LCS-242439
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342970
SampleType: LCS
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 242439
Analysis Date: 05/12/2017
Seq No: 7517229
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4535
0.20
0.5000
90.7
50.7
117
2,4-D
0.5114
0.20
0.5000
102
50.1
119
Surr: DCAA
0.4490
0
0.5000
89.8
50.1
132
Sample ID: 1705529-001BMS
Client ID:
House of Raeford - Mocksville
Units: mg/L
Prep Date: 05/11/2017
Run No: 342970
SampleType: MS
TestCode:
HERBICIDES, TCLP SW1311/8151A
BatchID: 242439
Analysis Date: 05/12/2017
Seq No: 7518762
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4942
0.20
0.5000
98.8
46.3
126
2,4-D
0.4862
0.20
0.5000
97.2
43.3
132
Sum DCAA
0.4525
0
0.5000
90.5
50.1
132
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 23 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242443
Sample ID: MB-242443
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342944
SampleType: MBLK
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270D
BatchlD: 242443
Analysis Date: 05/12/2017
Seq No: 7517114
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
BRL
0.10
2,4,5-Trichlorophenol
BRL
0.10
2,4,6-Trichlorophenol
BRL
0.10
2,4-Dinitrotoluene
BRL
0.10
Cresols, Total
BRL
0.10
Hexachlorobenzene
BRL
0.10
Hexachlorobutadiene
BRL
0.10
Hexachloroethane
BRL
0.10
m,p-Cresol
BRL
0.10
Nitrobenzene
BRL
0.10
o-Cresol
BRL
0.10
Pentachlorophenol
BRL
0.50
Pyridine
BRL
0.10
Suff:2,4,6-Tribromophenol
0.9640
0
1.000
96.4
52.1
146
Surr:2-Fluorobiphenyl
0.4725
0
0.5000
94.5
50.7
134
Sum 2-Fluorophenol
0.9122
0
1.000
91.2
47
122
Surr:4-Terphenyl-dl4
0.5245
0
0.5000
105
54.4
139
Surf: Nitrobenzene-d5
0.4536
0
0.5000
90.7
46.4
135
Surr: Phenol-d5
0.9612
0
1.000
96.1
48.2
122
Sample ID: LCS-242443
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 343052
SampleType: LCS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270D
BatchlD: 242443
Analysis Date: 05/15/2017
Seq No: 7519356
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
0.9300
0.10
1.000 93.0
64.7
120
2,4,5-Trichlorophenol
1.021
0.10
1.000 102
67.9
128
2,4,6-Trichlorophenol
1.218
0.10
1.000 122
74.9
133
2,4-Dinitrotoluene
1.206
0.10
1.000 121
68.6
133
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 24 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242443
Sample ID: LCS-242443
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 343052
SampleType: LCS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270D
BatchlD: 242443
Analysis Date: 05/15/2017
Seq No: 7519356
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cresols, Total
2.897
0.10
3.000
96.6
72.1
123
Hexachlorobenzene
1.135
0.10
1.000
113
77.9
137
Hexachlorobutadiene
0.9882
0.10
1.000
98.8
62.3
128
Hexachloroethane
0.9413
0.10
1.000
94.1
53.8
124
m,p-Cresol
1.860
0.10
2.000
93.0
71.5
123
Nitrobenzene
0.9405
0.10
1.000
94.0
72.8
128
o-Cresol
1.036
0.10
1.000
104
71
123
Pentachlorophenol
0.6505
0.50
1.000
65.0
50.2
125
Pyridine
0.4790
0.10
1.000
47.9
10
120
Suff:2,4,6-Tribromophenol
1.203
0
1.000
120
52.1
146
Surr:2-Fluorobiphenyl
0.4954
0
0.5000
99.1
50.7
134
Sum 2-Fluorophenol
0.7940
0
1.000
79.4
47
122
Surr:4-Terphenyl-dl4
0.5621
0
0.5000
112
54.4
139
Surf: Nitrobenzene-d5
0.4005
0
0.5000
80.1
46.4
135
Surr: Phenol-d5
0.7988
0
1.000
79.9
48.2
122
Sample ID: 1705531-001BMS
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342973
SampleType: MS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270D
BatchlD: 242443
Analysis Date: 05/12/2017
Seq No: 7518694
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
0.9185
0.10
1.000 91.8
52
120
2,4,5-Trichlorophenol
1.185
0.10
1.000 118
53.7
133
2,4,6-Trichlorophenol
1.272
0.10
1.000 127
61
132
2,4-Dinitrotoluene
1.224
0.10
1.000 122
49.6
136
Cresols, Total
3.808
0.10
3.000 0.9284 96.0
57.8
122
Hexachlorobenzene
1.132
0.10
1.000 113
61.5
136
Hexachlorobutadiene
1.004
0.10
1.000 100
48.7
125
Hexachloroethane
0.9530
0.10
1.000 95.3
50
120
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 25 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242443
Sample ID: 1705531-001BMS
Client ID:
Units: mg/L
Prep Date: 05/12/2017
Run No: 342973
SampleType: MS
TestCode: SEMIvoLATILES ORGANICS, TCLP SWI311/8270D
BatchID: 242443
Analysis Date: 05/12/2017
Seq No: 7518694
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
m,p-Cresol
2.742
0.10
2.000 0.9284
90.7
58.8
122
Nitrobenzene
0.9392
0.10
1.000
93.9
49.8
130
o-Cresol
1.066
0.10
1.000
107
51.2
126
Pentachlorophenol
1.007
0.50
1.000
101
41
134
Pyridine
BRL
0.10
1.000
0
10
120
Surf:2,4,6-Tribromophenol
1.319
0
1.000
132
52.1
146
Surr:2-Fluorobiphenyl
0.4692
0
0.5000
93.8
50.7
134
Sum 2-Fluorophenol
0.7666
0
1.000
76.7
47
122
Surr:4-Terphenyl-dl4
0.5520
0
0.5000
110
54.4
139
Surf: Nitrobenzene-d5
0.3808
0
0.5000
76.2
46.4
135
Surr: Phenol-d5
0.7383
0
1.000
73.8
48.2
122
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
S
Page 26 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242449
Sample ID: MB-242449
Client ID:
Units: mg/Kg
Prep Date: 05/11/2017
Run No: 342882
SampleType: MBLK
TestCode: METALS, TOTAL SW6010D
BatchID: 242449
Analysis Date: 05/11/2017
Seq No: 7515214
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
BRL
50.0
Arsenic
BRL
5.00
Cadmium
BRL
2.50
Calcium
BRL
50.0
Copper
BRL
2.50
Lead
BRL
5.00
Magnesium
BRL
50.0
Molybdenum
BRL
5.00
Nickel
BRL
5.00
Potassium
BRL
100
Selenium
BRL
5.00
Sodium
BRL
100
Zinc
BRL
5.00
Sample ID: LCS-242449
Client ID:
Units: mg/Kg
Prep Date: 05/11/2017
Run No: 342882
SampleType: LCS
TestCode: METALS, TOTAL SW6010D
BatchID: 242449
Analysis Date: 05/11/2017
Seq No: 7515215
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
457.8
50.0
500.0 0.4512 91.5
80
120
Arsenic
46.04
5.00
50.00 92.1
80
120
Cadmium
46.36
2.50
50.00 92.7
80
120
Calcium
483.9
50.0
500.0 1.300 96.5
80
120
Copper
47.14
2.50
50.00 94.3
80
120
Lead
47.23
5.00
50.00 94.5
80
120
Magnesium
454.5
50.0
500.0 90.9
80
120
Molybdenum
48.42
5.00
50.00 96.8
80
120
Nickel
46.98
5.00
50.00 94.0
80
120
Potassium
452.2
100
500.0 90.4
80
120
Qualifiers: >
Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL
Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J
Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 27 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242449
Sample ID: LCS-242449
Client ID:
Units: mg/Kg
Prep Date: 05/11/2017
Run No: 342882
SampleType: LCS
TestCode: METALS, TOTAL SW6010D
BatchID: 242449
Analysis Date: 05/11/2017
Seq No: 7515215
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Selenium
45.79
5.00
50.00
91.6
80
120
Sodium
441.1
100
500.0 1.034
88.0
80
120
Zinc
46.48
5.00
50.00
93.0
80
120
Sample ID: 1705546-001CMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342882
SampleType: MS
TestCode: METALS, TOTAL SW6010D
BatchID: 242449 Analysis Date: 05/11/2017
Seq No: 7515219
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
17110
52.3
523.0
13660
658
75
125 S
Arsenic
43.88
5.23
52.30
83.9
75
125
Cadmium
46.87
2.61
52.30
89.6
75
125
Calcium
2490
52.3
523.0
1919
109
75
125
Copper
63.79
2.61
52.30
15.12
93.1
75
125
Lead
45.44
5.23
52.30
1.432
84.2
75
125
Magnesium
3529
52.3
523.0
2825
134
75
125 S
Molybdenum
45.63
5.23
52.30
0.4290
86.4
75
125
Nickel
50.79
5.23
52.30
5.002
87.6
75
125
Potassium
3735
105
523.0
2649
208
75
125 S
Selenium
44.17
5.23
52.30
84.5
75
125
Sodium
776.9
105
523.0
161.2
118
75
125
Zinc
98.30
5.23
52.30
47.10
97.9
75
125
Sample ID: 1705546-001CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342882
SampleType: MSD
TestCode: METALS, TOTAL SW6010D
BatchlD: 242449 Analysis Date: 05/11/2017
Seq No: 7515220
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum 17170 52.3 523.0 13660 670 75 125 17110 0.376 20 S
Arsenic 43.18 5.23 52.30 82.6 75 125 43.88 1.60 20
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 28 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242449
Sample ID: 1705546-001CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342882
SampleType: MSD
TestCode: METALS, TOTAL SW6010D
BatchID: 242449 Analysis Date: 05/11/2017
Seq No: 7515220
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Cadmium
46.55
2.61
52.30
89.0
75
125
46.87
0.695
20
Calcium
2533
52.3
523.0
1919
117
75
125
2490
1.72
20
Copper
61.58
2.61
52.30
15.12
88.8
75
125
63.79
3.53
20
Lead
44.70
5.23
52.30
1.432
82.7
75
125
45.44
1.64
20
Magnesium
3391
52.3
523.0
2825
108
75
125
3529
3.98
20
Molybdenum
44.88
5.23
52.30
0.4290
85.0
75
125
45.63
1.66
20
Nickel
50.62
5.23
52.30
5.002
87.2
75
125
50.79
0.339
20
Potassium
3380
105
523.0
2649
140
75
125
3735
9.98
20
Selenium
44.11
5.23
52.30
84.3
75
125
44.17
0.126
20
Sodium
772.9
105
523.0
161.2
117
75
125
776.9
0.515
20
Zinc
96.07
5.23
52.30
47.10
93.6
75
125
98.30
2.30
20
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
S
Page 29 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242455
Sample ID: MB-242455
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342802
SampleType: MBLK
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 242455
Analysis Date: 05/09/2017
Seq No: 7512938
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive BRL 100
Sample ID: LCS-242455
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342802
SampleType: LCS
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 242455
Analysis Date: 05/09/2017
Seq No: 7512939
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 616.0 100 616.0 100 65.5 125
Sample ID: 1705401-001BMS
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342802
SampleType: MS
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 242455
Analysis Date: 05/09/2017
Seq No: 7512950
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 784.0 100 616.0 244.0 87.7 35.6 143
Sample ID: 1705401-001BMSD
Client ID:
Units: mg/Kg
Prep Date: 05/09/2017
Run No: 342802
SampleType: MSD
TestCode: Sulfide, Reactive SW846-7.3
BatchlD: 242455
Analysis Date: 05/09/2017
Seq No: 7512951
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 840.0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
100 616.0 244.0 96.8 35.6 143 784.0 6.90 20
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 30 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242466
Sample ID: MB-242466
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342859
SampleType: MBLK
TestCode: ICP METALS, TCLP SW1311/6010C
BatchID: 242466
Analysis Date: 05/11/2017
Seq No: 7514630
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
BRL
0.250
Barium
BRL
0.500
Cadmium
BRL
0.0250
Chromium
BRL
0.0500
Lead
BRL
0.0500
Selenium
BRL
0.100
Silver
BRL
0.0250
Sample ID: LCS-242466
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342859
SampleType: LCS
TestCode: ICP METALS, TCLP SW1311/6010C
BatchID: 242466
Analysis Date: 05/11/2017
Seq No: 7514633
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.940
0.250
5.000
98.8
80
120
Barium
4.683
0.500
5.000
93.7
80
120
Cadmium
4.831
0.0250
5.000
96.6
80
120
Chromium
4.628
0.0500
5.000
92.6
80
120
Lead
4.576
0.0500
5.000
91.5
80
120
Selenium
4.949
0.100
5.000
99.0
80
120
Silver
0.4886
0.0250
0.5000
97.7
80
120
Sample ID: 1705700-001BMS
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342859
SampleType: MS
TestCode: ICP METALS, TCLP SW1311/6010C
BatchID: 242466
Analysis Date: 05/12/2017
Seq No: 7516903
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.789
0.250
5.000 0.3920 87.9
50
150
Barium
4.237
0.500
5.000 84.7
50
150
Cadmium
4.608
0.0250
5.000 0.04455 91.3
50
150
Chromium
5.972
0.0500
5.000 1.808 83.3
50
150
Qualifiers:
> Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 31 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242466
Sample ID: 1705700-001BMS
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342859
SampleType: MS
TestCode: ICP METALS, TCLP SWI311/6010C
BatchID: 242466
Analysis Date: 05/12/2017
Seq No: 7516903
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Lead
4.756
0.0500
5.000 0.5309
84.5
50
150
Selenium
3.929
0.100
5.000
78.6
50
150
Silver
0.4490
0.0250
0.5000 0.01060
87.7
50
150
Sample ID: 1705700-001BMSD
Client ID:
Units: mg/L
Prep Date: 05/11/2017
Run No: 342859
SampleType: MSD
TestCode: ICP METALS, TCLP SW1311/6010C
BatchID: 242466
Analysis Date: 05/12/2017
Seq No: 7516904
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.802
0.250
5.000
0.3920
88.2
50
150
4.789
0.276 30
Barium
4.215
0.500
5.000
84.3
50
150
4.237
0.515 30
Cadmium
4.594
0.0250
5.000
0.04455
91.0
50
150
4.608
0.304 30
Chromium
5.969
0.0500
5.000
1.808
83.2
50
150
5.972
0.053 30
Lead
4.711
0.0500
5.000
0.5309
83.6
50
150
4.756
0.962 30
Selenium
3.931
0.100
5.000
78.6
50
150
3.929
0.055 30
Silver
0.4492
0.0250
0.5000
0.01060
87.7
50
150
0.4490
0.056 30
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 32 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242480
Sample ID: MB-242480
Client ID:
Units: wt%
Prep Date: 05/10/2017
Run No: 342845
SampleType: MBLK
TestCode: Residue, Volatile (SM2540G)
BatchID: 242480
Analysis Date: 05/10/2017
Seq No: 7513991
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Residue, Volatile BRL 0.00100
Sample ID: 1705531-001BDUP
Client ID:
Units: wt%
Prep Date: 05/10/2017
Run No: 342845
SampleType: DUP
TestCode: Residue, volatile (SM2540G)
BatchID: 242480
Analysis Date: 05/10/2017
Seq No: 7513990
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Residue, Volatile 86.33 0.00100 86.20 0.151 30
Sample ID: 1705904-001BDUP
Client ID:
Units: wt%
Prep Date: 05/10/2017
Run No: 342845
SampleType: DUP
TestCode: Residue, Volatile (SM2540G)
BatchID: 242480
Analysis Date: 05/10/2017
Seq No: 7513989
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Residue, Volatile
66.53 0.00100
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
66.78 0.375 30
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 33 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242503
Sample ID: LCS-242503
Client ID:
Units: pH Units Prep Date: 05/11/2017
Run No: 342892
SampleType: LCS
TestCode: Laboratory Hydrogen Ion (pH) Sw9045D
BatchID: 242503 Analysis Date: 05/11/2017
Seq No: 7515571
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.050 0.01 7.000 101 90 110
Sample ID: 1705466-001BDUP
Client ID:
Units: pH Units Prep Date: 05/11/2017
Run No: 342892
SampleType: DUP
TestCode: Laboratory Hydrogen Ion (pH) SW9045D
BatchID: 242503 Analysis Date: 05/11/2017
Seq No: 7515579
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.190 0.01 7.190 0 10 H
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 34 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242539
Sample ID: MB-242539
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342959
SampleType: MBLK
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 242539
Analysis Date: 05/12/2017
Seq No: 7518001
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta BRL 5.00
Sample ID: LCS-242539
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342959
SampleType: LCS
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 242539
Analysis Date: 05/12/2017
Seq No: 7518002
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 48.20 5.00 50.00 96.4 90 110
Sample ID: 1705401-001BMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342959
SampleType: MS
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 242539 Analysis Date: 05/12/2017
Seq No: 7518004
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 700.4 69.3 693.5 101 90 110
Sample ID: 1705447-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342959
SampleType: MS
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchlD: 242539 Analysis Date: 05/12/2017
Seq No: 7518020
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 1235 59.4 59.39 715.0 876 90 110 S
Sample ID: 1705401-001BMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/11/2017
Run No: 342959
SampleType: MSD
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 242539 Analysis Date: 05/12/2017
Seq No: 7518005
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 698.9
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
70.0 700.3
99.8 90 110
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
700.4 0.220 30
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 35 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• 242554
Sample ID: MB-242554
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342955
SampleType: MBLK
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 242554
Analysis Date: 05/12/2017
Seq No: 7516702
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive BRL 1.00
Sample ID: LCS-242554
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342955
SampleType: LCS
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 242554
Analysis Date: 05/12/2017
Seq No: 7516703
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 8.700 1.00 12.50 69.6 68.5 130
Sample ID: 1705932-001BMS
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342955
SampleType: MS
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 242554
Analysis Date: 05/12/2017
Seq No: 7516717
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 7.150 1.00 12.50 57.2 25.7 130
Sample ID: 1705932-001BMSD
Client ID:
Units: mg/Kg
Prep Date: 05/12/2017
Run No: 342955
SampleType: MSD
TestCode: Cyanide, Reactive SW846-7.3
BatchlD: 242554
Analysis Date: 05/12/2017
Seq No: 7516718
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 6.950 1.00 12.50
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
55.6 25.7 130 7.150 2.84 24.6
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 36 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• R342794
Sample ID: LCS-R342794
Client ID:
Units: OF
Prep Date:
Run No: 342794
SampleType: LCS
TestCode: ignitability SWI010A
BatchID: R342794
Analysis Date: 05/10/2017
Seq No: 7512733
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Ignitability 82.00 0 81.00 101 93.8 106.2
Sample ID: 1705531-001BDUP
Client ID:
Units: OF
Prep Date:
Run No: 342794
SampleType: DUP
TestCode: Ignitability SWI010A
BatchID: R342794
Analysis Date: 05/10/2017
Seq No: 7512738
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Ignitability 180.0 0 180.0 0 20 >
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 37 of 38

Analytical Environmental Services, Inc Date: 16-May-17
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: House of Raeford - Mocksville
Workorder: 1705529 BatchID• R342849
Sample ID: M13-11342849
Client ID:
Units: wt%
Prep Date:
Run No: 342849
SampleType: MBLK
TestCode: Fixed Residues (SM2540G)
BatchlD: R342849
Analysis Date: 05/10/2017
Seq No: 7514265
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
% Total Solids BRL 0.00100
Sample ID: 1705531-001BDUP
Client ID:
Units: wt%
Prep Date:
Run No: 342849
SampleType: DUP
TestCode: Fixed Residues (SM2540G)
BatchID: R342849
Analysis Date: 05/10/2017
Seq No: 7514273
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
% Total Solids
7.840
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
0.00100 6.410
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
7.910 0.889 20
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 38 of 38

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
December 07, 2016
David Covle
Terra Renewal Services
P.O. Box 399
Dardanelle AR 72834
TEL: [phone]
FAX:
RE: House of Raeford - Molksville
Dear David Coyle: Order No: 1612017
Analytical Environmental Services, Inc. received 7 samples on 12/1/2016 10:20:00 AM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative. AES' certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/16-06/30/17.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent,
effective until 12/31/16.
-South Carolina Environmental Laboratory Certification number 98016003 effective until
6/30/17.
These results relate only to the items tested. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Chris Pafford
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: 770.457-S188 • Toll F.,e:800.972.4889
www.aesatlanta.com
Page 1 of 13

ANALYTICAL ENVIRONMENTAL SERVICES, INC
3080 Presidential Drive Atlanta GA 30340- 3906
TEL.: [phone] / TOLL -FREE [phone] / FAX: [phone]
CHAIN OF CUSTODY
Work Order: V
4 ate: Page a of L_ie.
COMPANY:
Terra Renewal Services
ADDRESS:
P.O. Box 399
Dardanelle, AR 72834
ANALYSIS REQUESTED
Visit our website
www.aesatlanta.com to
cheek on the status of
your results, place bottle
orders, etc.
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AMPLES ARE DISPOSED OF 30 DAYS AFTER COMPLETION OF REPORT UNLESS OTHER ARRANGEMENTS ARE MADE.
MATRIX CODES: A = Air GW = Groundwater SE = Sediment SO = Soil SW = Surface Water W = Water (Blanks) W W=Wastewater DW=Drinking Water 0 = Other (specify)
PRESERVATIVE CODES: H+I = Hydrochloric acid + ice I = Ice only N = Nitric acid S+I = Sulfuric acid + ice S/M+I = Sodium Bisulfate/Methanol + ice O = Other (specify) NA = None
Page 2 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client: Terra Renewal Services
Project: House of Raeford - Molksville Case Narrative
Lab ID: 1612017
Sample Receiving Nonconformance:
WO 1612017 was received outside EPA/Method specified holding time of 24 hours for method Fecal Coliform in Sludge.
WO 1612017 as received did not meet method specified preservation requirements as samples were received in unpreserved
plastic containers. Samples were transferred into sterile containers by the lab.
Sample information on the Chain of Custody did not match that on the sample bottle labels for WO 1612017. The sample
containers only had "House of Raeford" present, not 71-FT"
The laboratory proceeded with analysis per David Coyle via phone 12-1-16 and logged in samples F1 through F7 arbitrarily as
requested.
Page 3 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F 1
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 9:50:00 AM
Lab ID:
1612017-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
209000 20900 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
Y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitatiion range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 4 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F2
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 9:55:00 AM
Lab ID:
1612017-002
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
149000 21300 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 5 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F3
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 9:59:00 AM
Lab ID:
1612017-003
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
124000 20700 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 6 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F4
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 10:03:00 AM
Lab ID:
1612017-004
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
214000 22500 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 7 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F5
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 10:08:00 AM
Lab ID:
1612017-005
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
352000 20700 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 8 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F6
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 10:11:00 AM
Lab ID:
1612017-006
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
276000 21300 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 9 of 13

Analytical Environmental Services, Inc
Date: 8-Dec-16
Client:
Terra Renewal Services
Client Sample ID:
HOR F7
Project Name:
House of Raeford - Molksville
Collection Date:
11/30/2016 10:15:00 AM
Lab ID:
1612017-007
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
Fecal Coliform-Soil/Sludge
Fecal Coliform, (MF)
SM9222D-1997
111000 20200 H Colonies/gr-dr R331485 10000 12/01/201616:45 MU
y
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 10 of 13

Analytical Environmental Services, Inc,
Sample/Cooler Receipt Checklist
Client
Checklist completed byL 4-"(A
Signature
Carrier name: FedEx UPS ✓ Courier Client US Mail Other
Shipping container/cooler in good condition? Yes
Custody seals intact on shipping container/cooler? Yes _
Custody seals intact on sample bottles? Yes _
Container/Temp Blank temperature in compliance? (0°56°C)* Yes t/
Cooler #1 — 'n Cooler #2 Cooler #3
Cooler #4
Chain of custody present?
Yes
Chain of custody signed when relinquished and received?
Yes
Chain of custody agrees with sample labels?
Yes
Samples in proper containerlbottle?
Yes
Sample containers intact?
Yes
Sufficient sample volume for indicated test?
Yes
All samples received within holding time?
Yes _
Was TAT marked on the COC?
Yes f
Proceed with Standard TAT as per project history?
Yes _
Water - VOA vials have zero headspace? No VOA vials submitted ✓
Work Order Number �U) 01 1
No _ Not Present _
No Not Present
No _ Not Present
No _
Cooler#5 Cooler #6
No
No ✓�
No
No
No _
No _
No ✓
No
No
Yes
Water - pH acceptable upon receipt? Yes _ No _
Adjusted? Checked by
Sample Condition: Good —*" Other(Explain)
(For diffusive samples or ARIA lead) Is a known blank included? Yes _
See Case Narrative for resolution of the Non -Conformance.
Not Applicable✓
No
Not Applicable
1Im
* Samples do not have to comply with the given range for certain parameters.
\1Aes_server%Sample ReceiptlMy DocumentslCOCs and pH Adjustrnent SheetlSample Cooler Recipi Checklist Revl.rtf
Page 11 of 13

Analytical Environmental Services, Inc Date: 8-Dec-16
Client: Terra Renewal Services
Project Name: House of Raeford - Molksville Dates Report
Lab Order: 1612017
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name TCLP Date Prep Date
Analysis Date
1612017-001A
HOR F1
11/30/2016 9:50:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-002A
HOR F2
11/30/2016 9:55:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-003A
HOR F3
11/30/2016 9:59:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-004A
HOR F4
11/30/2016 10:03:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-005A
HOR F5
11/30/2016 10:08:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-006A
HOR F6
11/30/2016 10:11:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
1612017-007A
HOR F7
11/30/2016 10:15:OOAM
Sludge
Fecal Coliform-Soil/Sludge
12/01/2016
Page 12 of 13

Analytical Environmental Services, Inc
Client: Terra Renewal Services
Project Name: House of Raeford - Molksville
Workorder: 1612017
Date: 7-Dec-16
ANALYTICAL QC SUMMARY REPORT
BatchID: R331485
Sample ID: MB-R331485
Client ID:
Units: Colonies/gr-dry Prep Date:
Run No: 331485
SampleType: MBLK
TestCode: Fecal Coliform-Soil/Sludge SM9222D-1997
BatchID: R331485 Analysis Date: 12/01/2016
Seq No: 7214926
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Fecal Coliform, (MF) BRL 0.200
Sample ID: MB-R331485-2
Client ID:
Units: Colonies/gr-dry Prep Date:
Run No: 331485
SampleType: MBLK
TestCode: Fecal Coliform-Soil/Sludge SM9222D-1997
BatchID: R331485 Analysis Date: 12/O1/2016
Seq No: 7214949
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Fecal Coliform, (MF)
BRL 0.200
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 13 of 13

HUNTER FARMS - HIGH POINT, NC

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Hunter Print High Point
Lot Number:UJ15004
Date Completed:11/05/2019
11 /05/2019 4:48 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
pCCRF�4
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: UJ15004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ15004-001. Due to low % solids, the initial amount of these samples were 3 times the
standard procedure amount. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terra Renewal Services, Inc.
Lot Number: UJ15004
Sample Number Sample ID Matrix Date Sampled Date Received
001 Hunter Print High Point Solid 10/14/2019 1430 10/15/2019
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terra Renewal Services, Inc.
Lot Number: UJ15004
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Hunter Print High Point
Solid
% Volatile Solids SM
2540G-
96
%
5
001
Hunter Print High Point
Solid
Ignitability (Pensky-Martens
1010A
>140
° F
5
001
Hunter Print High Point
Solid
Nitrate -Nitrite - N (soluble)
353.2
10
mg/kg
5
001
Hunter Print High Point
Solid
Phosphorus
365.1
2500
mg/kg
5
001
Hunter Print High Point
Solid
TKN
351.2
12000
mg/kg
5
001
Hunter Print High Point
Solid
2-Butanone (MEK)
8260B
0.11
mg/L
5
001
Hunter Print High Point
Solid
Aluminum
6010D
3100
mg/kg
8
001
Hunter Print High Point
Solid
Calcium
6010D
1100
mg/kg
8
001
Hunter Print High Point
Solid
Zinc
6010D
7.7
mg/kg
8
(9 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15004-001
Description: Hunter Print High Point Matrix: Solid
Date Sampled:10/14/2019 1430 % Solids: 12.8 10/16/2019 0040
Date Received:10/15/2019
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile S) SM 2540G-1997
1 10/20/2019 2138 MOM
32627
1 350.1
(Ammonia - N ) 350.1
1 10/18/2019 1623 DMA
32376
1
(Ignitability) 1010A
1 10/24/2019 1538 SLC
33236
1
(Nitrate-Nitr) 353.2
1 10/18/2019 2209 AMR
32544
1
(Phosphorus) 365.1
10 10/24/2019 1205 DMA
10/23/2019 1429
32936
1
(Reactive Cya) 7.3.3
1 10/22/2019 2123 KFE
10/16/2019 1034
1
(Reactive Sul) 7.3.4
1 10/21/2019 1622 HET
10/16/2019 1034
1
(Soil pH meas) 9045D
1 10/21/2019 2122 HET
32774
2 351.4
(TKN) 351.2
1 10/22/2019 1442 HKL
10/18/2019 1654
32537
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-
96
%
1
Ammonia - N (gas diffusion)
350.1
ND
78
mg/kg
1
Ignitability (Pensky-Martens Closed -Cup)
1010A
>140
140
- F
1
Nitrate -Nitrite - N (soluble)
353.2
10
1.6
mg/kg
1
Phosphorus
7723-14-0 365.1
2500
390
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 20.1 ° C
9045D
3.8
su
1
TKN
351.2
12000
200
mg/kg
2
TCLP Volatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B
8260B
10 10/26/2019 0156 STM
33432 10/23/2019 2034
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260B
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260B
0.11
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260B
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260B
ND
0.050
mg/L
1
Chloroform
67-66-3 8260B
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260B
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260B
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260B
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260B
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260B
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
92 70-130
Bromofluorobenzene
92 70-130
Toluene-d8
96 70-130
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15004-001
Description: Hunter Print High Point Matrix: Solid
Date Sampled:10/14/2019 1430 % Solids: 12.8 10/16/2019 0040
Date Received:10/15/2019
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270D 1 10/28/2019 1955 JCG
10/26/2019 2059 33458 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270D
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270D
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270D
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270D
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270D
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270D
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270D
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270D
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270D
ND
0.20
mg/L
1
Pyridine
110-86-1 8270D
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270D
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270D
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
72 37-129
2-Fluorophenol
41 24-127
Nitrobenzene-d5
56 38-127
Phenol-d5
84 28-128
Terphenyl-d14
86 10-148
2,4,6-Tribromophenol
91 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 10/31 /2019 2028 DAL1
10/30/2019 2135 34009 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
70 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A 1 10/21/2019 1745 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
130
ug/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above
the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15004-001
Description: Hunter Print High Point Matrix: Solid
Date Sampled:10/14/2019 1430 % Solids: 12.8 10/16/2019 0040
Date Received:10/15/2019
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 3660B/3665A 8082A 1 10/21/2019 1745 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1221
11104-28-2 8082A
ND
130
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
130
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
130
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
130
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
130
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
130
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
99 41-132
Tetrachloro-m-xylene
86 35-106
TCLP Pesticides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /3520C
8081 B 1 10/31 /2019 1948 DAL1
10/28/2019 0015 33512 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5 8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
38 20-131
Tetrachloro-m-xylene
77 26-132
CVAA
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B 1 10/19/2019 0806 KSH2
10/18/2019 1422 32494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
0.60
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ15004-001
Description: Hunter Print High Point Matrix: Solid
Date Sampled:10/14/2019 1430 % Solids: 12.8 10/16/2019 0040
Date Received:10/15/2019
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 10/28/2019 0556 LLL
10/27/2019 1845 33481 10/23/2019 0103
1 1311/7470A
7470A
1 10/29/2019 0907 JMH
10/28/2019 1406 33559 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/22/2019 1340 LLL
10/18/2019 1115 32478
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
3100
52
mg/kg
1
Arsenic
7440-38-2 6010D
ND
1.9
mg/kg
1
Cadmium
7440-43-9 6010D
ND
0.65
mg/kg
1
Calcium
7440-70-2 6010D
1100
650
mg/kg
1
Copper
7440-50-8 6010D
ND
1.3
mg/kg
1
Lead
7439-92-1 6010D
ND
1.3
mg/kg
1
Magnesium
7439-95-4 6010D
ND
650
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
5.2
mg/kg
1
Nickel
7440-02-0 6010D
ND
5.2
mg/kg
1
Potassium
7440-09-7 6010D
ND
650
mg/kg
1
Selenium
7782-49-2 6010D
ND
2.6
mg/kg
1
Sodium
7440-23-5 6010D
ND
650
mg/kg
1
Zinc
7440-66-6 6010D
7.7
6.5
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
ShOaly Errwronrnenjal �iEYyi;N, Inc,
105'JanEaga F60 r5 in
ChaollotCu8f4afyReCOM Vw:st-nWmlUk&m%GCe6Wa20172
Yele�7rcr.• u�, {�p4� 391-47C4 Fax nkl. f803; 791-6711
fl. rr irm rx. a.y.
ra.aakc:rytyx Th.N.-rva -0�i�
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441
R USE BALY
qa—'
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Sheri I Fnvivg m wql $Grvige�, L-1C.
Umument Njmbcr J012W1a0-14
1 01'
Sample Reevipt CbeeUist ( R
Client: Lf3dR 1i RENEWAL Cooler Insp'eowii byfdate; t.F.ta i 10-15-2019 Let f: UJ150P4
Mean s of receipt: SrS1 ❑ Cljiml ❑ UPS [] FcdEx Lkthen
❑ Yes ❑ No 1 11- Vk+orc ctk410d ' scstls csfitrt Oil the o00leP
El Vcs El N,, 1 21 NA12- IF oos[. kL seals nj•scniw wcrc they intact and unbroken?
rt... �Irip 113; NA Chlorine Strip ID: NA Tested by, NA
03'i�i:tal teroperalum upon rcrviptl Durivcd (Corrcctod) temperature up,ut rbCeipt 'Asolid $uaprCUp1D, 1 1616
5.6 15.6 �C NA ?NA -C NA -NA 'C NA INA f C
hiathZ❑Temperature Slant- OAgainst 134 ttics IR Gun ID- S IRGun Conv,:-ion Factor; 5C
mkt l god of cwulant, ® wet lce ❑ lee Pads 0-Drybe ❑ None -
❑ Yes ❑ No ® NA'' If =vp-%;ra1urc of any cooler exceeded 6.0"C, was Ptco mt Manager N(Afied?
1 M was. Nolitied by, phone i email I faca-to-face Itcirle onel-
I Yes ❑ No ❑ Nei 4. Ts the cvtmnsrria[ MUlder's paeking slip aWlocd to this form" �
® Yes ❑ No 5. Were m r eu�" rrooedures (relinquishedlr ei,,r;l) followod?
® Yes ❑ N(y 6- Wctm sample JDIs listed an the C C?
® Vcs ❑ No 7. Wcro sample 1Ds listed on all samp[c canm[ne,tc? -
W3 Yes No 8- Wag collection date & time listed Lire lhcCCC?
® Yrrs ❑ Ra 9. was collection date & time fisted an all sample conwiners7
J 'Yes ❑ N01 10, Did W1 eut Wner label information (ID, date, t[tnc) apace with the COC'
0 Ycs ❑ h1a 1 1. Were testlt 13n he llerlComtcd listed aft die HOC? I
rknr.
❑ ve5 ❑ NQ i 2, Did all samples give in the proper comuineN for each tcst andlor in gaud candil imi
(unbroken_ lids nn,
Yrs ❑ No .3. was adequate samplc vv[unie available?
Ym ❑ No i't, Pere all samples reeeNed -within V, the holding titres or 48 [fouls_-Kl1iQbevtr coat first?
Yr-s ® No"' 15. Weep any Samples caitCciltt~es iriissir +crcess(circle one) samples Not listed nn C ?
I ❑ Yes [I NO O NA . Fi. FOr VOA and RSK-175 samples, were bubbles pr,-Ju'nt>"paa size" ('/Par 6rnm in tIflnict,
in any of the VOA v[alsf''
❑ Yos No 0 ETA 17- Were all at a pi I of-f- 7?
LI YL-.,;l Q No NA 19- Were all cy-al.-tidr samples received at a pH > 12 and sulfide samPlca received at a
❑ Yes ❑ Y0 O NA
I"- 1e1ea31 applicable NH;JTF:NAr yaniddphenol,625 (<O,Smgt ft (Ir'7
(L) same f r ideal
vas Q No 0 TEA 20. Were Mien# maiarks inquests (i,c. rcyucsted dilutions, MS,'MSD desigrrptions. etc -) —
❑ �correotly tralnwribW from the C OC: into tht aamatent sectian in LIMB?
© yesl V Nol 121, Was the quate number Iistad Ore the cantairrar label? If 'es, Quotc # NA
Sarmpie >Pmervation (Must be compkted For any sampk(g) imvnwdy prewrvM or w[th headspaL:e-)
mpie(g) NAWCavncrcivcdinmrnxtly'preserved and wcroa.I juslad ordiroly;
in sample rcoeiving with Nib inL of elide unti: H2S[34, I1NM, , HCI, Na H using SR 4. 'S-A
Time of prtsel'vation NA If mere thort Une p1�Servatii� rlccdcd, please note irr the aammerttt heliow_
mple(s) NA _ were tec-rived vlith hulybim. '-6 ruin in di 0 MtCL
mples(s) N, wcre received with T'R.C'..` 0 tp 'i, {[C#19 is nrr) and were
iuslcd Accordingly in sample receivirLg with sodium thiagulfato (NatS,O.) with Shealy III: NA
baromklabcJsappliedby. LK19 Daw 10-15-2019
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
North Carolina Pc-rmit Parameters
2. Residual@ *ball be, analyzad W dzm[m.3Lrals thcy arc .; - ^��. a. ,ara OLl= tong time
and Recovery Act (RCRA). T an orr *os1-vity, i�itability, rear'' and cUy
ch$r nuateriWc leaFthi.ug prow ry sha sped W in
Attachment A, and t11e Peradir.ee sha11 maintain Ihesc rrsUltz for a n riniaum of five years. Any
exceptilms from rk r qu b ments in this. uffiditica shalt be specified in Attackment A.
The TCLP analysis shall in olucL the aiollov>Ming paratx1etels (tlxe regulatory level in mitligrums �ex liner
iS l�Y �541'�f'Itl}e8$6�;
Arsenic (5.0)
Barium (100,1))
Benz= (0.5)
Cadmium (1-0)
Carbon 1.eLrachllaridc (0.5)
j
chlordane (6.03)
ChlorUbcfmnnc (100.0)
qL
Chloroform (6-0)
hromium (5.0)
o-Cresol (200b)
lr-Cresol (200,0)
Crasol (200.0)
1,4-01ic:hlurubcnaene {7,5)
1,2-Dichloyoubane (0-5)
1,1-Diehl oraethylene (0:7)
2.4-Dinitrntrluene (f)-X 3}
lEndrin (0,02)
He chlorobarkuue (0-13)
eptachlor (=d its'hydroxid
11exachloro-1,3-bu1a,di=n (0-5)
HexaPhlomethime )
read (S-oy
Lmdane (OA)
A+Mermwy (0.2)
metiox hlor (10.0)
Nftrol}eI3 eve
Pentarlfloropll!efv�i (1
pyridine (5,0)
�rsleni>.un {1.0�
silver {.4)
Tc1rauhIorocEliy1cn.e
ToXapl p (4,5)
Tri dhrvet1tyleuo (C
2.4,5-Trirhlrmrrhe_no1 (
,,4,5-'YP (Silvex) (1
Vinyl chloride (0,:
,b)
7)
1))
3. An analysis shall b: conducttd m residoaIs from ewh source genuaating facility at the ry
specified in AttacbxnmA A, and the Permki ee Shall maintain the resultsfor a minimumof fs-
The amlysis shall in -elude the frrlluwiug par4mcLcrs:
+r
AlimfnU1n - —
Mercury
1hrMolybd=>,uu
PntassiuTn
Seleziva>x
SrAiurn
ArniTlonlb-Nitrogcn
Mickel
Nitrate Nitrnt)C Nitrogam
Cadmium
Calcium
Percent Total Solids
TN
Capper
pH
Zinc
Lead
phosphorus
Vold Ie solos
agMSium
P PS
TERRA RENEWAL SERVICES
479-747-8192
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

Analytical Results �,* STATESVILLE
ANALYTICAL
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date:
12/19/2019
Reported:
12/20/2019
For:
HUNTER HIGH
Comments:
GM <271 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
191219-12-01
Fecal Coliforms
H1
<224
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-01
Percent Solids
1-11
8.2
%
SM2540B-2011
12/19/2019
WC
191219-12-02
Fecal Coliforms
H2
<261
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-02
Percent Solids
H2
7.65
%
SM2540B-2011
12/19/2019
WC
191219-12-03
Fecal Coliforms
H3
<222
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-03
Percent Solids
H3
9
%
SM2540B-2011
12/19/2019
WC
191219-12-04
Fecal Coliforms
H4
<260
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-04
Percent Solids
H4
7.7
%
SM2540B-2011
12/19/2019
WC
191219-12-05
Fecal Coliforms
H5
<234
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-05
Percent Solids
H5
8.53
%
SM2540B-2011
12/19/2019
WC
191219-12-06
Fecal Coliforms
H6
<294
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-06
Percent Solids
H6
6.8
%
SM2540B-2011
12/19/2019
WC
191219-12-07
Fecal Coliforms
H7
<428
MPN/g
SM92210E-2006
12/19/2019
WC
191219-12-07
Percent Solids
H7
4.67
%
SM254OB-2011
12/19/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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Page 2 of 2

MATHIS-1 STORAGE FACILITY - RONDA, NC

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
May 31, 2019
David Coyle
Terra Renewal Services
P.O. Box 399
Dardanelle AR 72834
RE: WQ0038087 - Storage Comp
Dear David Coyle: Order No: 1905068
Analytical Environmental Services, Inc. received 1 samples on 5/24/2019 9:31:00 AM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the
analyses contained herein will be noted and submitted in the form of a project Case Narrative. AES'
certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/18-06/30/19.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/19.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/19.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Chris Pafford
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: 770.457,8177 • Fax: 770.457-S188 • Toll F.,e:800.972.4889
www.aesatlanta.com
Page 1 of 38

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
3080 Presidential Drive Atlanta, GA 30340-3704
AES Phone: [phone] / TolI-Free: [phone] / Fax: [phone]
CHAIN OF CUSTODY
Work Order: lqjpi�©b g
Date: s�Z 1l/9 Page 1 of 1
COMPANY:
Terra Renewal
ADDRESS:
P.O. Box 399
Dardanelle, AR 72834
ANALYSIS REQUESTED
Visit our website
www.aesatianta.com for
downloadable COCs and to
log in to your AESAccess
account.:
a
E
z
m
Q
N
PHONE: [phone]
EMAIL: [e-mail]
SAMPLED BY:
SIGNATURE
#
SAMPLE ID
SA
ii
0
°
—
x vcc
v_TT
—
DATE
TIME
PRESERVATION (see codes)
REMARKS
I
1
MAt}i1S- (
S 2i !'l
2
✓
Sludge
✓
Z
2
✓
Sludge
be
3
✓
Sludge
✓
4
✓
Sludge
✓
5
✓
Sludge
✓
6
✓
Sludge
✓
7
✓
Sludge
✓
8
✓
Sludge
✓
9
✓
Sludge
✓
10
✓
Sludge
✓
11
12
13
14
RELINQUISHED BY: DATE/TIME:
RECEIVED BY: DATE/TIME:
PROJECT INFORMATION
RECEIPT
1
VAv�1i �o`/�.E. S L3 1i � `l f�A
1
1' \-.J r _7
PROJECT NAME:
n
v✓C�oo;ko87 - SToiC�vE loM1P•
Total # of Containers
2-
2.
2.
PROJECT #:
Turnaround Time (TAT) Request
SITE ADDRESS:
Vfi�u�S Co./+atY� NG
Standard
❑ 2 Business Day Rush
❑Next Business Day Rush
❑ e Day Rush (auth req.)
OLher'r*Kib C• Q11fio��
3.
3.
SEND REPORT TO: }
[e-mail]
SPECIAL INSTRUCTIONS/COMMENTS:
SHIPMENT METHOD
OUT: / / VIA:
IN: ' ' VIA:
UPS US mail courier
client CED
other:
INVOICE TO (IF DIFFERENT FROM ABOVE):
Contact Vanya Colburn for PO
STATE PROGRAM (if any):
E-mail? ❑ Fax? ❑
DATA PACKAGE: I Oil O III ON O
QUOTE #: PO#:
Submission of samples to the laboratory constitutes acceptance of AES's Terms & Conditions. Client assumes sole responsibility for damage or loss of samples before we accept them. Samples received after 3PM or on Saturday are considered as received the following
business day. If no TAT is marked on COC, AES will proceed with standard TAT. Samples are disposed of 30 days after completion of report unless other arrangements are made.
Matrix Codes: A = Air GW = Groundwater SE = Sediment SO = Soil SW = Surface Water ST=Stormwater W W = Waste Water W = Water (Blanks) DW = Drinking Water (Blanks) 0 = Other (specify) 7.11.18_CO
Preservative Codes: H+I = Hydrochloric acid + ice I = Ice only N = Nitric acid S+1 = Sulfuric acid + ice S/M+I = Sodium Bisulfate/Methanol + ice 0 = Other (specify) NA = None White Copy - Original; Yellow Copy - Client
Page 2 of 38

)Q,&S06g
North Carolina Permit Parameters
2. Residuals shall be analyzed to demonstrate they are - 144e ource Conservation
and Recovery Act (RCRA). The ana es corrosivity, ignitability, reactivit and toxicity
characteristic leaching procedure TCLP sha equency specified in
Attachment A, and the Permittce shall maintain these results for a minimum of five years. Any
exceptions from the requirements in this. condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
CO
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
W
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Uj
'�
I
CL
Chlordane (0.03)
Chlorobenzene 100.0
( )
Chloroform (6.0)
Hexachlorobenzene (0.13)
Heptachlor (and its hydroxide)
0.008)
Hexachloro-1,3-butadiene (0.5)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
VChromium
(5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D 00.0) _
Methyl ethyl ketone 200. )
_.
3. An analysis shall be conducted on residuals from each source generating facility at the frequency
specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
W
O
y
LU
Z
W
2
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Volatile Solids
Magnesium
PCB's
TERRA RENEWAL SERVICES
479-747-8192
ATTAC44ME+`►i T- Coc Fet% I'AAZ'KIs_i 5-1 4/tom{
WQ0036936 Version 1.0
Shell Version 140210
Page 8 of 12
Page 3 of 38

Analytical Environmental Services, Inc
Date: 31-May-19
Client: Terra Renewal Services
Project: WQ0038087 - Storage Comp Case Narrative
Lab ID: 1905068
pH Analysis by Method SW9045D:
Samples for pH analysis by Method SW9045D were received and analyzed outside holding time requirement of "immediate or
15 minutes".
Semi Volatile Organic Analysis by Method 8270E/1311:
Percent recovery for the surrogate spiking compound 2,4,6-Tribromophenol & 2-Fluorobiphenyl on the LCS samples for Batch
279677 was outside control limits biased high. All target analytes, other LCS surrogate recoveries and 2,4,6-Tribromophenol &
2-Fluorobiphenyl recoveries in associated samples were within control limits and data was not affected.
Page 4 of 38

Analytical Environmental Services, Inc
Date: 31-May-19
Client:
Terra Renewal Services
Client Sample ID:
Mathis-1
Project Name:
WQ0038087 - Storage Comp
Collection Date:
5/23/2019 2:00:00 PM
Lab ID:
1905068-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatchID
Dilution
Factor
Date Analyzed Analyst
VOLATILES, TCLP SW1311/8260D
(SW5030B)
1, 1 -Dichloroethene
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
1,2-Dichloroethane
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
2-Butanone
BRL
0.20
mg/L 279732
20
05/29/2019 13:42
BK
Benzene
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Carbon tetrachloride
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Chlorobenzene
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Chloroform
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Tetrachloroethene
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Trichloroethene
BRL
0.10
mg/L 279732
20
05/29/2019 13:42
BK
Vinyl chloride
BRL
0.040
mg/L 279732
20
05/29/2019 13:42
BK
Surr:4-Bromofluorobenzene
82.9
63.1-120
%REC 279732
20
05/29/2019 13:42
BK
Surr: Dibromofluoromethane
105
76.1-126
%REC 279732
20
05/29/2019 13:42
BK
Surr: Toluene-d8
95.7
75.3-119
%REC 279732
20
05/29/2019 13:42
BK
Total Phosphorus, soils E365.1
(E365.1)
Phosphorus, Total (As P)
3890
2850
mg/Kg-dry 279666
10
05/28/2019 13:14
MP
TOTAL MERCURY SW7471B
(SW7471B)
Mercury
BRL
2.93
mg/Kg-dry 279613
1
05/24/201914:07
EH
Sulfide, Reactive SW846-7.3
(SW7.3.4.2)
Sulfide, Reactive
BRL
100
mg/Kg 279655
1
05/24/2019 16:05
AT
SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
(SW3510C)
1,4-Dichlorobenzene
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
2,4,5-Trichlorophenol
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
2,4,6-Trichlorophenol
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
2,4-Dinitrotoluene
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Hexachlorobenzene
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Hexachlorobutadiene
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Hexachloroethane
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
m,p-Cresol
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Nitrobenzene
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
o-Cresol
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Pentachlorophenol
BRL
0.50
mg/L 279677
1
05/29/201914:35
YH
Pyridine
BRL
0.10
mg/L 279677
1
05/29/201914:35
YH
Cresols, Total
BRL
0.10
mg/L 279677
1
05/29/2019 14:35
YH
Surr:2,4,6-Tribromophenol
77.2
49.6-128
%REC 279677
1
05/29/201914:35
YH
Surr:2-Fluorobiphenyl
76.5
52.2-124
%REC 279677
1
05/29/201914:35
YH
Surr:2-Fluorophenol
70.5
44-129
%REC 279677
1
05/29/201914:35
YH
Surr:4-Terphenyl-dl4
69.6
63.2-145
%REC 279677
1
05/29/201914:35
YH
Qualifiers: • Value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not confirmed
B Analyte detected in the associated method blank
<
Less than Result value
> Greater than Result value
J
Estimated value detected below
Reporting Limit
Page 5 of 38

Analytical Environmental Services, Inc
Date: 31-May-19
Client:
Terra Renewal Services
Client Sample ID:
Mathis-1
Project Name:
WQ0038087 - Storage Comp
Collection Date:
5/23/2019 2:00:00 PM
Lab ID:
1905068-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatcbID
Dilution
Factor
Date Analyzed Analyst
SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
(SW3510C)
Surr: Nitrobenzene-d5
84
53.6-124
%REC 279677
1
05/29/2019 14:35
YH
Surr: Phenol-d5
73.4
50.6-125
%REC 279677
1
05/29/2019 14:35
YH
Residue, Volatile (SM2540G)
(E160.4)
Residue, Volatile
97.5
0.00100
wt% 279720
1
05/28/2019 11:30
AT
POLYCHLORINATED BIPHENYLS SW8082A
(SW3550C)
Aroclor 1016
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1221
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1232
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1242
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1248
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1254
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Aroclor 1260
BRL
1000
ug/Kg-dry 279625
1
05/24/2019 14:20
UH
Surr: Decachlorobiphenyl
106
45.7-140
%REC 279625
1
05/24/2019 14:20
UH
Surr: Tetrachloro-m-xylene
87.6
45.3-126
%REC 279625
1
05/24/2019 14:20
UH
PESTICIDES, TCLP SW1311/8081B
(SW3510C)
Chlordane
BRL
0.00050
mg/L 279750
1
05/29/2019 13:16
UH
Endrin
BRL
0.00010
mg/L 279750
1
05/29/2019 13:16
UH
gamma-BHC
BRL
0.000050
mg/L 279750
1
05/29/2019 13:16
UH
Heptachlor
BRL
0.000050
mg/L 279750
1
05/29/2019 13:16
UH
Heptachlor epoxide
BRL
0.000050
mg/L 279750
1
05/29/2019 13:16
UH
Methoxychlor
BRL
0.00050
mg/L 279750
1
05/29/2019 13:16
UH
Toxaphene
BRL
0.0050
mg/L 279750
1
05/29/2019 13:16
UH
Surr: Decachlorobiphenyl
73.9
47.7-136
%REC 279750
1
05/29/2019 13:16
UH
Surr: Tetrachloro-m-xylene
55.2
44.7-126
%REC 279750
1
05/29/2019 13:16
UH
Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
(E351.2 MOD)
Nitrogen, total Kjeldahl(TKN)Extractable
100000
14600
mg/Kg-dry 279664
10
05/28/2019 17:58
TL
Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
(E353.2 MOD)
Nitrogen, Nitrate-Nitrite(as N)Extractable
BRL
145
mg/Kg-dry 279632
1
05/24/2019 14:39
AA
Nitrogen, Ammonia (as N) Extractable E350.1 MOD
(E350.1)
Nitrogen, Ammonia (As N) Extractable
3990
299
mg/Kg-dry 279628
1
05/24/2019 13:22
TL
MERCURY, TCLP SW1311/7470A
(SW7470A)
Mercury
BRL
0.00400
mg/L 279760
1
05/29/201915:39
EH
Laboratory Hydrogen Ion (pH) SW9045D
(SW9045D)
Qualifiers: • Value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not confirmed
B Analyte detected in the associated method blank
<
Less than Result value
> Greater than Result value
J
Estimated value detected below Reporting Limit
Page 6 of 38

Analytical Environmental Services, Inc
Date: 31-May-19
Client:
Terra Renewal Services
Client Sample ID:
Mathis-1
Project Name:
WQ0038087 - Storage Comp
Collection Date:
5/23/2019 2:00:00 PM
Lab ID:
1905068-001
Matrix:
Sludge
Analyses
Result
Reporting
Limit
Qual
Units BatcbID
Dilution
Factor
Date Analyzed Analyst
Laboratory Hydrogen Ion (pH) SW9045D
(SW9045D)
pH
4.38
0.01
H
pH Units 279619
1
05/24/2019 14:00
BK
Ignitability SW1010A
Ignitability
180
0
>
°F R398954
1
05/24/2019 00:00
SK
ICP METALS, TCLP SW1311/6010D
(SW3010A)
Arsenic
BRL
0.250
mg/L 279758
1
05/29/201915:19
DG
Barium
BRL
0.500
mg/L 279758
1
05/29/201915:19
DG
Cadmium
BRL
0.0250
mg/L 279758
1
05/29/201915:19
DG
Chromium
BRL
0.0500
mg/L 279758
1
05/29/201915:19
DG
Lead
BRL
0.0500
mg/L 279758
1
05/29/201915:19
DG
Selenium
BRL
0.100
mg/L 279758
1
05/29/201915:19
DG
Silver
BRL
0.0250
mg/L 279758
1
05/29/201915:19
DG
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.20
mg/L 279756
1
05/29/2019 15:53
HB
2,4-D
BRL
0.20
mg/L 279756
1
05/29/2019 15:53
HB
Surr: DCAA
74.1
49.4-120
%REC 279756
1
05/29/2019 15:53
HB
Fixed Residues (SM2540G)
% Total Solids
3.31
0.00100
wt% R398989
1
05/24/2019 13:00
AT
Cyanide, Reactive SW846-7.3
(SW7.3.3.2)
Cyanide, Reactive
BRL
1.00
mg/Kg 279662
1
05/24/2019 16:35
AT
METALS, TOTAL SW6010D
(SW3050B)
Aluminum
BRL
272
mg/Kg-dry 279582
1
05/24/201914:33
DG
Arsenic
BRL
13.6
mg/Kg-dry 279582
1
05/24/201914:33
DG
Cadmium
BRL
13.6
mg/Kg-dry 279582
1
05/24/201914:33
DG
Calcium
671
272
mg/Kg-dry 279582
1
05/24/201914:33
DG
Copper
16.0
13.6
mg/Kg-dry 279582
1
05/24/201914:33
DG
Lead
BRL
27.2
mg/Kg-dry 279582
1
05/24/201914:33
DG
Magnesium
BRL
272
mg/Kg-dry 279582
1
05/24/201914:33
DG
Molybdenum
BRL
27.2
mg/Kg-dry 279582
1
05/24/201914:33
DG
Nickel
BRL
27.2
mg/Kg-dry 279582
1
05/24/201914:33
DG
Potassium
1110
543
mg/Kg-dry 279582
1
05/24/201914:33
DG
Selenium
BRL
19.0
mg/Kg-dry 279582
1
05/24/201914:33
DG
Sodium
1900
543
mg/Kg-dry 279582
1
05/24/201914:33
DG
Zinc
35.1
27.2
mg/Kg-dry 279582
1
05/24/201914:33
DG
PERCENT MOISTURE D2216
Qualifiers: • value exceeds maximum contaminant level
E
Estimated (value above quantitation range)
BRL Below reporting limit
S
Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded
Nan
See case narrative
N Analyte not NELAC certified
NC
Not continued
B Analyte detected in the associated method blank
<
Less than Result value
> Greater than Result value
J
Estimated value detected below Reporting Limit
Page 7 of 38

Analytical Environmental Services, Inc
Date: 31-May-19
Client:
Terra Renewal Services
Client Sample ID:
Mathis-1
Project Name:
WQ0038087 - Storage Comp
Collection Date:
5/23/2019 2:00:00 PM
Lab ID:
1905068-001
Matrix:
Sludge
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
PERCENT MOISTURE D2216
Percent Moisture 96.7 0 wt% R398989 1 05/24/2019 13:00 AT
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E
Estimated (value above quantiitation range)
S
Spike Recovery outside limits due to matrix
Nan'
See case narrative
NC
Not continued
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 8 of 38

A3+fALyncAL Clear Save as
JENmommENTAL
A19S SERVICES, INC. SAMPLE/COOLER RECEIPT CHECKLIST
1. client Name: Terra Renewal Services, Inc. AES Work Order Number: 1905068
2. Carrier: FeclEx ❑• UPS ❑ USPS ❑ Client F Courier[-] Othei
Yes No N/A Details Comments
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
Shipping container/cooler received in good condition?
U
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
•
Temperature blanks present?
0•
Cooler temperature(s) within limits of 040 [See item 13 and 14 for
temperature recordings.]
O
O
O
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (CDC) present?
•
Chain of Custody signed, dated, and timed when relinquished and received?
•
Sampler name and/or signature on COC?
•
Were all samples received within holding time?
•
TAT marked on the COC?
•
If no TAT indicated, proceeded with standard TAT per Terms & Conditions. ❑
13. Cooler 1 Temperature 3.3
14. Cooler 5 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
°C Cooler 2 Temperature °C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 6 Temperature °C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials). MH 5/24/19
Yes No N/A Details Comments
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
0•
Custody seals intact on sample containers?
o•
Do sample container labels match the COC?
O
O
O
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
•
Were all of the samples listed on the CDC received?
O
O
O
samples received but not listed on COC ❑
samples listed on COC not received ❑
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•
Were samples received in appropriate containers?
•
O
Were VOA samples received without headspace (< 1/4" bubble)?
•
Were trip blanks submitted?
O
•
listed on CDC ❑ not listed on COC ❑
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). MH 5/24/19
checked at Sample Receipt. Yes No N/A Details Comments
28. Have containers needing chemical preservation been checked? * •
29. Containers meet preservation guidelines? •
30. Was pH adjusted at Sample Receipt? •
* Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH. MH 5/24/19
I certify that I have completed sections 28-30 (dated initials).
Checklist 6.9.17 Rev 2 Locked
Page 9 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services
Project Name: WO0038087 - Storage Comp Dates Report
Lab Order: 1905068
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name
TCLP Date
Prep Date
Analysis Date
1905068-001A
Mathis-1
5/23/2019
2:00:OOPM
Sludge
VOLATILES, TCLP Leached
05/28/2019
5/28/2019 2:57:OOPM
05/29/2019
1905068-001B
Mathis-1
5/23/2019
2:00:OOPM
Sludge
TCLP SEMIVOLATILES ORGANICS
05/28/2019
5/29/2019 10:15:OOAM
05/29/2019
1905068-001B
Mathis-1
5/23/2019
2:00:OOPM
Sludge
HERBICIDES, TCLP Leached
05/28/2019
5/29/2019 10:30:OOAM
05/29/2019
1905068-001B
Mathis-1
5/23/2019
2:00:OOPM
Sludge
MERCURY, TCLP Leached
05/28/2019
5/29/2019 12:24:OOPM
05/29/2019
1905068-001B
Mathis-1
5/23/2019
2:00:OOPM
Sludge
ICP METALS, TCLP Leached
05/28/2019
5/29/2019 11:59:OOAM
05/29/2019
1905068-001B
Mathis-1
5/23/2019
2:00:OOPM
Sludge
PESTICIDES, TCLP Leached
05/28/2019
5/29/2019 10:30:OOAM
05/29/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
IGNITABILITY
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Residue, Volatile by 160.4/SM2540G
5/24/2019 1:00:OOPM
05/28/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Nitrogen, Ammonia (as N) Extractable
5/24/2019 11:45:OOAM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Nitrogen, total Kjeldahl (TKN) Extractable
5/28/2019 10:40:OOAM
05/28/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Nitrogen, Nitrate -Nitrite (as N) Extractable
5/24/2019 11:43:09AM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Total Phosphorus, soils
5/28/2019 9:00:OOAM
05/28/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
TOTAL METALS BY ICP
5/24/2019 11:15:OOAM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Cyanide, Reactive
5/24/2019 5:32:30PM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Sulfide, Reactive
5/24/2019 4:30:58PM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
MERCURY
5/24/2019 11:59:OOAM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
POLYCHLORINATED BIPHENYLS
5/24/2019 11:00:OOAM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Laboratory Hydrogen Ion (pH)
5/24/2019 1:45:03PM
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
PERCENT MOISTURE
05/24/2019
1905068-001C
Mathis-1
5/23/2019
2:00:OOPM
Sludge
Fixed Residues (SM2540G)
05/24/2019
Page 10 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279582
Sample ID: MB-279582
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398966
SampleType: MBLK
TestCode: METALS, TOTAL SW6010D
BatchID: 279582
Analysis Date: 05/24/2019
Seq No: 8943164
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
BRL
50.0
Arsenic
BRL
2.50
Cadmium
BRL
2.50
Calcium
BRL
50.0
Copper
BRL
2.50
Lead
BRL
5.00
Magnesium
BRL
50.0
Molybdenum
BRL
5.00
Nickel
BRL
5.00
Potassium
BRL
100
Selenium
BRL
3.50
Sodium
BRL
100
Zinc
BRL
5.00
Sample ID: LCS-279582
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398966
SampleType: LCS
TestCode: METALS, TOTAL SW6010D
BatchID: 279582
Analysis Date: 05/24/2019
Seq No: 8943166
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
457.5
50.0
500.0
91.5
80
120
Arsenic
46.97
2.50
50.00
93.9
80
120
Cadmium
43.87
2.50
50.00
87.7
80
120
Calcium
483.8
50.0
500.0
96.8
80
120
Copper
46.35
2.50
50.00
92.7
80
120
Lead
48.36
5.00
50.00
96.7
80
120
Magnesium
454.4
50.0
500.0
90.9
80
120
Molybdenum
48.19
5.00
50.00
96.4
80
120
Nickel
46.90
5.00
50.00
93.8
80
120
Qualifiers: > Greater than Result value < Less than Result value
BRL Below reporting limit E Estimated (value above quantitation range)
J Estimated value detected below Reporting Limit N Analyte not NELAC certified
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 11 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279582
Sample ID: LCS-279582
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398966
SampleType: LCS
TestCode: METALS, TOTAL SW6010D
BatchID: 279582
Analysis Date: 05/24/2019
Seq No: 8943166
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Potassium
457.0
100
500.0
91.4
80
120
Selenium
40.42
3.50
50.00
80.8
80
120
Sodium
508.7
100
500.0
102
80
120
Zinc
44.50
5.00
50.00
89.0
80
120
Sample ID: 1905L23-001CMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398966
SampleType: MS
TestCode: METALS, TOTAL Sw6010D
BatchID: 279582 Analysis Date: 05/24/2019
Seq No: 8943171
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
35.28
2.14
42.88
0.9406
80.1
75
125
Cadmium
35.34
2.14
42.88
0.07126
82.3
75
125
Calcium
2707
42.9
428.8
2401
71.4
75
125 S
Copper
50.47
2.14
42.88
16.42
79.4
75
125
Lead
49.58
4.29
42.88
14.93
80.8
75
125
Molybdenum
33.51
4.29
42.88
0.8814
76.1
75
125
Nickel
38.07
4.29
42.88
4.916
77.3
75
125
Selenium
27.30
3.00
42.88
63.7
75
125 S
Sodium
801.8
85.8
428.8
333.9
109
75
125
Zinc
73.16
4.29
42.88
42.51
71.5
75
125 S
Sample ID: 1905L23-001CMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398966
SampleType: MS
TestCode: METALS, TOTAL sw6010D
BatchID: 279582 Analysis Date: 05/24/2019
Seq No: 8943183
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
25690
4290
428.8
23550
500
75
125 S
Magnesium
7256
4290
428.8
5986
296
75
125 S
Potassium
7112
2140
428.9
5583
357
75
125 S
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 12 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279582
Sample ID: 1905L23-001CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398966
SampleType: MSD
TestCode: METALS, TOTAL SW6010D
BatchID: 279582 Analysis Date: 05/24/2019
Seq No: 8943172
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
36.42
2.14
42.75
0.9406
83.0
75
125
35.28
3.18
20
Cadmium
35.46
2.14
42.75
0.07126
82.8
75
125
35.34
0.349
20
Calcium
2973
42.7
427.5
2401
134
75
125
2707
9.37
20
S
Copper
52.04
2.14
42.75
16.42
83.3
75
125
50.47
3.06
20
Lead
48.03
4.27
42.75
14.93
77.4
75
125
49.58
3.18
20
Molybdenum
32.79
4.27
42.75
0.8814
74.7
75
125
33.51
2.15
20
S
Nickel
39.21
4.27
42.75
4.916
80.2
75
125
38.07
2.95
20
Selenium
27.58
2.99
42.75
64.5
75
125
27.30
1.02
20
S
Sodium
748.5
85.5
427.5
333.9
97.0
75
125
801.8
6.88
20
Zinc
65.78
4.27
42.75
42.51
54.4
75
125
73.16
10.6
20
S
Sample ID: 1905L23-001CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398966
SampleType: MSD
TestCode: METALS, TOTAL SW6010D
BatchID: 279582 Analysis Date: 05/24/2019
Seq No: 8943185
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aluminum
27180
4270
427.5
23550
850
75
125
25690
5.64
20
S
Magnesium
5689
4270
427.5
5986
-69.5
75
125
7256
24.2
20
SR
Potassium
5241
2140
427.5
5583
-80.1
75
125
7112
30.3
20
SR
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 13 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279613
Sample ID: MB-279613
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398967
SampleType: MBLK
TestCode: TOTAL MERCURY SW7471B
BatchID: 279613
Analysis Date: 05/24/2019
Seq No: 8943138
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury BRL 0.100
Sample ID: LCS-279613
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398967
SampleType: LCS
TestCode: TOTAL MERCURY sw7471B
BatchID: 279613
Analysis Date: 05/24/2019
Seq No: 8943139
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.3725 0.100 0.4000 93.1 80 120
Sample ID: 1905J92-003CMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398967
SampleType: MS
TestCode: TOTAL MERCURY Sw7471B
BatchID: 279613 Analysis Date: 05/24/2019
Seq No: 8943142
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.4051 0.112 0.4480 90.4 80 120
Sample ID: 1905J92-003CMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398967
SampleType: MSD
TestCode: TOTAL MERCURY sw7471B
BatchID: 279613 Analysis Date: 05/24/2019
Seq No: 8943143
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.4159 0.113 0.4508
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
92.3 80
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
120 0.4051 2.64 20
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 14 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279619
Sample ID: LCS-279619
Client ID:
Units: pH Units Prep Date: 05/24/2019
Run No: 398912
SampleType: LCS
TestCode: Laboratory Hydrogen Ion (pH) sw9045D
BatchlD: 279619 Analysis Date: 05/24/2019
Seq No: 8941793
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 6.960 0.01 7.000 99.4 90 110 H
Sample ID: 1905N79-003ADUP
Client ID:
Units: pH Units Prep Date: 05/24/2019
Run No: 398912
SampleType: DUP
TestCode: Laboratory Hydrogen Ion (pH) sw9045D
BatchID: 279619 Analysis Date: 05/24/2019
Seq No: 8941797
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
pH 7.290 0.01 7.280 0.137 10 H
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 15 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279625
Sample ID: MB-279525
Client ID:
Units: ug/Kg
Prep Date: 05/24/2019
Run No: 398959
SampleType: MBLK
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 279625
Analysis Date: 05/24/2019
Seq No: 8942997
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
BRL
33
Aroclor 1221
BRL
33
Aroclor 1232
BRL
33
Aroclor 1242
BRL
33
Aroclor 1248
BRL
33
Aroclor 1254
BRL
33
Aroclor 1260
BRL
33
Sum Decachlorobiphenyl
16.89
0 16.67 101 45.7 140
Surr: Tetrachloro-m-xylene
13.41
0 16.67 80.4 45.3 126
Sample ID: LCS-279525
Client ID:
Units: ug/Kg
Prep Date: 05/24/2019
Run No: 398959
SampleType: LCS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchlD: 279625
Analysis Date: 05/24/2019
Seq No: 8942998
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
155.3
33
166.7
93.2
67
128
Aroclor 1260
156.3
33
166.7
93.8
66.5
126
Surr: Decachlorobiphenyl
18.04
0
16.67
108
45.7
140
Surr: Tetrachloro-m-xylene
14.11
0
16.67
84.6
45.3
126
Sample ID: 1905M38-001AMS
Client ID:
Units: ug/Kg-dry Prep Date: 05/24/2019
Run No: 398959
SampleType: MS
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 279625 Analysis Date: 05/24/2019
Seq No: 8943000
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
473.2
97
486.5
97.2
50.7
129
Aroclor 1260
418.3
97
486.5
86.0
52.2
129
Surr: Decachlorobiphenyl
47.66
0
48.66
97.9
45.7
140
Sum Tetrachloro-m-xylene
40.02
0
48.66
82.2
45.3
126
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 16 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279625
Sample ID: 1905M38-OOIAMSD
Client ID:
Units: ug/Kg-dry Prep Date: 05/24/2019
Run No: 398959
SampleType: MSD
TestCode: POLYCHLORINATED BIPHENYLS SW8082A
BatchID: 279625 Analysis Date: 05/24/2019
Seq No: 8943001
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Aroclor 1016
413.4
97
486.5
85.0
50.7
129
473.2
13.5
17
Aroclor 1260
368.7
97
486.5
75.8
52.2
129
418.3
12.6
18.7
Surr: Decachlorobiphenyl
43.40
0
48.66
89.2
45.7
140
47.66
0
0
Sum Tetrachloro-m-xylene
37.35
0
48.66
76.8
45.3
126
40.02
0
0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 17 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279628
Sample ID: MB-279628
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398952
SampleType: MBLK
TestCode: Nitrogen, Ammonia (as N) Extractable E350.1 MOD
BatchID: 279628
Analysis Date: 05/24/2019
Seq No: 8943023
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable BRL 10.0
Sample ID: LCS-279628
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398952
SampleType: LCS
TestCode: Nitrogen, Ammonia (as N) Extractable E350A MOD
BatchID: 279628
Analysis Date: 05/24/2019
Seq No: 8943025
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable 103.8 10.0 100.0 104 90 110
Sample ID: 1905M38-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398952
SampleType: MS
TestCode: Nitrogen, Ammonia (as N) Extractable E350.1 MOD
BatchID: 279628 Analysis Date: 05/24/2019
Seq No: 8943046
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractable 3280 289 289.0 3058 77.0 90 110 S
Sample ID: 1905M38-OOI AMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398952
SampleType: MSD
TestCode: Nitrogen, Ammonia (as N) Extractable E350A MOD
BatchID: 279628 Analysis Date: 05/24/2019
Seq No: 8943049
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Ammonia (As N) Extractablt 3427
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
286 286.2 3058 129 90 110 3280 4.37 30 S
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 18 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279632
Sample ID: MB-279632
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398925
SampleType: MBLK
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 279632
Analysis Date: 05/24/2019
Seq No: 8943059
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta BRL 5.00
Sample ID: LCS-279632
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398925
SampleType: LCS
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 279632
Analysis Date: 05/24/2019
Seq No: 8943060
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 49.50 5.00 50.00 99.0 90 110
Sample ID: 1905M38-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398925
SampleType: MS
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 279632 Analysis Date: 05/24/2019
Seq No: 8943065
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 294.8 14.6 291.9 101 90 110
Sample ID: 1905M38-OOI AMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/24/2019
Run No: 398925
SampleType: MSD
TestCode: Nitrogen, Nitrate -Nitrite (as N) Ext. E353.2
BatchID: 279632 Analysis Date: 05/24/2019
Seq No: 8943066
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, Nitrate-Nitrite(as N)Extracta 289.1
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
14.3 286.2
101 90 110
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
294.8 1.98 30
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 19 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279655
Sample ID: MB-279655
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398976
SampleType: MBLK
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 279655
Analysis Date: 05/24/2019
Seq No: 8943581
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive BRL 100
Sample ID: LCS-279655
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398976
SampleType: LCS
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 279655
Analysis Date: 05/24/2019
Seq No: 8943587
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 272.0 100 272.0 100 65.5 125
Sample ID: 1905J68-001BMS
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398976
SampleType: MS
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 279655
Analysis Date: 05/24/2019
Seq No: 8943591
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 280.0 100 272.0 103 28.7 139
Sample ID: 1905J68-001BMSD
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398976
SampleType: MSD
TestCode: Sulfide, Reactive SW846-7.3
BatchID: 279655
Analysis Date: 05/24/2019
Seq No: 8943592
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Sulfide, Reactive 240.0 100 272.0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
88.2 28.7 139 280.0 15.4 26.9
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 20 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279662
Sample ID: MB-279662
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398983
SampleType: MBLK
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 279662
Analysis Date: 05/24/2019
Seq No: 8943812
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive BRL 1.00
Sample ID: LCS-279662
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398983
SampleType: LCS
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 279662
Analysis Date: 05/24/2019
Seq No: 8943841
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 9.700 1.00 12.50 77.6 63 121
Sample ID: 1905J68-001BMS
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398983
SampleType: MS
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 279662
Analysis Date: 05/24/2019
Seq No: 8943887
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 7.700 1.00 12.50 61.6 28.5 122
Sample ID: 1905J68-001BMSD
Client ID:
Units: mg/Kg
Prep Date: 05/24/2019
Run No: 398983
SampleType: MSD
TestCode: Cyanide, Reactive SW846-7.3
BatchID: 279662
Analysis Date: 05/24/2019
Seq No: 8943888
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cyanide, Reactive 7.450 1.00 12.50
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
59.6 28.5 122 7.700 3.30 25.1
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 21 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279664
Sample ID: MB-279664
Client ID:
Units: mg/Kg
Prep Date: 05/28/2019
Run No: 399096
SampleType: MBLK
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 279664
Analysis Date: 05/28/2019
Seq No: 8946736
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta BRL 50.0
Sample ID: LCS-279664
Client ID:
Units: mg/Kg
Prep Date: 05/28/2019
Run No: 399096
SampleType: LCS
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 279664
Analysis Date: 05/28/2019
Seq No: 8946864
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 1030 50.0 1000 103 90 110
Sample ID: 1905M06-001AMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/28/2019
Run No: 399096
SampleType: MS
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 279664 Analysis Date: 05/28/2019
Seq No: 8946865
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 69000 3510 3510 61390 217 90 110 S
Sample ID: 1905M06-001 AMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/28/2019
Run No: 399096
SampleType: MSD
TestCode: Nitrogen, total Kjeldahl (TKN) Extractable E351.2M
BatchID: 279664 Analysis Date: 05/28/2019
Seq No: 8946741
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Nitrogen, total Kjeldahl(TKN)Extracta 66810
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
3480 3479 61390 156 90 110 69000 3.23 30 S
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 22 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279666
Sample ID: MB-279666
Client ID:
Units: mg/Kg
Prep Date: 05/28/2019
Run No: 399048
SampleType: MBLK
TestCode: Total Phosphorus, soils E365.1
BatchID: 279666
Analysis Date: 05/28/2019
Seq No: 8945540
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) BRL 10.0
Sample ID: LCS-279666
Client ID:
Units: mg/Kg
Prep Date: 05/28/2019
Run No: 399048
SampleType: LCS
TestCode: Total Phosphorus, soils E365.1
BatchID: 279666
Analysis Date: 05/28/2019
Seq No: 8945541
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 382.8 20.0 400.0 95.7 90 110
Sample ID: 1905M05-00I1IMS
Client ID:
Units: mg/Kg-dry Prep Date: 05/28/2019
Run No: 399048
SampleType: MS
TestCode: Total Phosphorus, soils E365.1
BatchID: 279666 Analysis Date: 05/28/2019
Seq No: 8945544
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 28960 2190 1753 25780 182 90 110 S
Sample ID: 1905M05-001BMSD
Client ID:
Units: mg/Kg-dry Prep Date: 05/28/2019
Run No: 399048
SampleType: MSD
TestCode: Total Phosphorus, soils E365.1
BatchID: 279666 Analysis Date: 05/28/2019
Seq No: 8945545
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit High Limit RPD Ref Val %RPD
RPD Limit Qual
Phosphorus, Total (As P) 27990
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
2200 1757 25780 126 90
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
110 28960 3.43 30 S
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 23 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279677
Sample ID: MB-279677
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399021
SampleType: MBLK
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
BatchID: 279677
Analysis Date: 05/28/2019
Seq No: 8946140
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
BRL
0.10
2,4,5-Trichlorophenol
BRL
0.10
2,4,6-Trichlorophenol
BRL
0.10
2,4-Dinitrotoluene
BRL
0.10
Cresols, Total
BRL
0.10
Hexachlorobenzene
BRL
0.10
Hexachlorobutadiene
BRL
0.10
Hexachloroethane
BRL
0.10
m,p-Cresol
BRL
0.10
Nitrobenzene
BRL
0.10
o-Cresol
BRL
0.10
Pentachlorophenol
BRL
0.50
Pyridine
BRL
0.10
Surf:2,4,6-Tribromophenol
1.146
0
1.000
115
49.6
128
Surr:2-Fluorobiphenyl
0.5713
0
0.5000
114
52.2
124
Sum 2-Fluorophenol
0.8372
0
1.000
83.7
44
129
Surr:4-Terphenyl-dl4
0.5837
0
0.5000
117
63.2
145
Surf: Nitrobenzene-d5
0.4846
0
0.5000
96.9
53.6
124
Surr: Phenol-d5
0.7666
0
1.000
76.7
50.6
125
Sample ID: LCS-279677
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399021
SampleType: LCS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
BatchID: 279677
Analysis Date: 05/28/2019
Seq No: 8946142
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
0.9429
0.10
1.000 94.3
61.9
129
2,4,5-Trichlorophenol
1.213
0.10
1.000 121
66.5
129
2,4,6-Trichlorophenol
1.236
0.10
1.000 124
72.6
134
2,4-Dinitrotoluene
1.157
0.10
1.000 116
69
124
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 24 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279677
Sample ID: LCS-279677
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399021
SampleType: LCS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
BatchID: 279677
Analysis Date: 05/28/2019
Seq No: 8946142
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Cresols, Total
3.221
0.10
3.000
107
74.5
134
Hexachlorobenzene
1.236
0.10
1.000
124
70.6
129
Hexachlorobutadiene
1.065
0.10
1.000
107
59.2
124
Hexachloroethane
0.9239
0.10
1.000
92.4
57.8
131
m,p-Cresol
2.119
0.10
2.000
106
72.3
130
Nitrobenzene
1.109
0.10
1.000
ill
72.6
125
o-Cresol
1.102
0.10
1.000
110
75.7
140
Pentachlorophenol
0.9004
0.50
1.000
90.0
50.1
122
Pyridine
0.1254
0.10
1.000
12.5
12.5
120
Surf:2,4,6-Tribromophenol
1.351
0
1.000
135
49.6
128 S
Surr:2-Fluorobiphenyl
0.6463
0
0.5000
129
52.2
124 S
Sum 2-Fluorophenol
0.9882
0
1.000
98.8
44
129
Surr:4-Terphenyl-dl4
0.6518
0
0.5000
130
63.2
145
Surf: Nitrobenzene-d5
0.5416
0
0.5000
108
53.6
124
Surr:Phenol-d5
0.9394
0
1.000
93.9
50.6
125
Sample ID: 1905J92-001BMS
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399021
SampleType: MS
TestCode: SEMIVOLATILES ORGANICS, TCLP SW1311/8270E
BatchID: 279677
Analysis Date: 05/28/2019
Seq No: 8946521
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,4-Dichlorobenzene
0.8918
0.10
1.000 89.2
48.5
131
2,4,5-Trichlorophenol
1.109
0.10
1.000 ill
52.2
129
2,4,6-Trichlorophenol
1.124
0.10
1.000 112
54.3
132
2,4-Dinitrotoluene
1.014
0.10
1.000 101
56.3
120
Cresols, Total
2.942
0.10
3.000 98.0
61.4
136
Hexachlorobenzene
1.130
0.10
1.000 113
58.1
128
Hexachlorobutadiene
0.9771
0.10
1.000 97.7
46.3
123
Hexachloroethane
0.8587
0.10
1.000 85.9
49
129
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix
Page 25 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279677
Sample ID: 1905J92-001BMS
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399021
SampleType: MS
TestCode: SEMIVOLATILES ORGANICS, TCLP SWI311/8270E
BatchID: 279677
Analysis Date: 05/28/2019
Seq No: 8946521
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
m,p-Cresol
1.932
0.10
2.000
96.6
65.2
129
Nitrobenzene
1.022
0.10
1.000
102
61.8
124
o-Cresol
1.009
0.10
1.000
101
65
140
Pentachlorophenol
0.8225
0.50
1.000
82.2
42.3
121
Pyridine
0.1908
0.10
1.000
19.1
10
120
Surf:2,4,6-Tribromophenol
1.174
0
1.000
117
49.6
128
Surr:2-Fluorobiphenyl
0.5670
0
0.5000
113
52.2
124
Sum 2-Fluorophenol
0.8740
0
1.000
87.4
44
129
Surr:4-Terphenyl-dl4
0.5931
0
0.5000
119
63.2
145
Surf: Nitrobenzene-d5
0.4934
0
0.5000
98.7
53.6
124
Surr:Phenol-d5
0.8334
0
1.000
83.3
50.6
125
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 26 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279720
Sample ID: MB-279720
Client ID:
Units: wt%
Prep Date: 05/24/2019
Run No: 399073
SampleType: MBLK
TestCode: Residue, volatile (SM2540G)
BatchID: 279720
Analysis Date: 05/28/2019
Seq No: 8946169
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Residue, Volatile BRL 0.00100
Sample ID: 1905068-001CDUP
Client ID:
Mathis-1
Units: wt%
Prep Date: 05/24/2019
Run No: 399073
SampleType: DUP
TestCode:
Residue, volatile (sM2540G)
BatchlD: 279720
Analysis Date: 05/28/2019
Seq No: 8946171
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Residue, Volatile
96.76 0.00100
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
97.47 0.731 30
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 27 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279732
Sample ID: MB-279732
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: MBLK
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946485
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene
BRL
0.10
1,2-Dichloroethane
BRL
0.10
2-Butanone
BRL
0.20
Benzene
BRL
0.10
Carbon tetrachloride
BRL
0.10
Chlorobenzene
BRL
0.10
Chloroform
BRL
0.10
Tetrachloroethene
BRL
0.10
Trichloroethene
BRL
0.10
Vinyl chloride
BRL
0.040
Surr:4-Bromofluorobenzene
0.8298
0 1.000 83.0 63.1 120
Sum Dibromofluoromethane
1.066
0 1.000 107 76.1 126
Surr:Toluene-d8
0.9564
0 1.000 95.6 75.3 119
Sample ID: LCS-279732
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: LCS
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946524
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene
0.4592
0.10
0.4000
115
57.3
140
1,2-Dichloroethane
0.4304
0.10
0.4000
108
66
134
2-Butanone
0.9128
0.20
0.8000
114
60.5
138
Benzene
0.4102
0.10
0.4000
103
72.4
129
Carbon tetrachloride
0.4806
0.10
0.4000
120
67.9
140
Chlorobenzene
0.4152
0.10
0.4000
104
76
131
Chloroform
0.4578
0.10
0.4000
114
63.7
132
Tetrachloroethene
0.4410
0.10
0.4000
110
73.7
139
Trichloroethene
0.4354
0.10
0.4000
109
72.2
136
Vinyl chloride
0.4860
0.040
0.4000
122
55.8
136
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank
BRL Below reporting limit
E Estimated (value above quantitation
range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
S Spike Recovery outside limits due
to matrix
Page 28 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279732
Sample ID: LCS-279732
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: LCS
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946524
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Surr:4-Bromofluorobenzene
0.9452
0
1.000
94.5
63.1
120
Surf: Dibromofluoromethane
1.077
0
1.000
108
76.1
126
Surr:Toluene-d8
1.046
0
1.000
105
75.3
119
Sample ID: 1905J92-001AMS
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: MS
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946681
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1, 1 -Dichloroethene
0.5506
0.10
0.4000
138
62.3
137 S
1,2-Dichloroethane
0.5150
0.10
0.4000
129
65.8
133
2-Butanone
0.9594
0.20
0.8000
120
57.2
140
Benzene
0.4674
0.10
0.4000
117
72.2
134
Carbon tetrachloride
0.5598
0.10
0.4000
140
69.3
140
Chlorobenzene
0.4886
0.10
0.4000
122
73.8
136
Chloroform
0.5242
0.10
0.4000
131
61.4
136
Tetrachloroethene
0.5136
0.10
0.4000
128
73.1
138
Trichloroethene
0.4854
0.10
0.4000
121
72.5
138
Vinyl chloride
0.4704
0.040
0.4000
118
60.8
135
Sum 4-Bromofluorobenzene
0.9820
0
1.000
98.2
63.1
120
Surr: Dibromofluoromethane
1.084
0
1.000
108
76.1
126
Surr:Toluene-d8
1.050
0
1.000
105
75.3
119
Sample ID: 1905J92-001ADUP
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: DUP
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946680
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
1,1-Dichloroethene BRL 0.10 0 0 30
1,2-Dichloroethane BRL 0.10 0 0 30
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 29 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279732
Sample ID: 1905J92-001ADUP
Client ID:
Units: mg/L
Prep Date: 05/28/2019
Run No: 399055
SampleType: DUP
TestCode: voLAT1LES, TCLP SW1311/8260D
BatchID: 279732
Analysis Date: 05/28/2019
Seq No: 8946680
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2-Butanone
BRL
0.20
0
0 30
Benzene
BRL
0.10
0
0 30
Carbon tetrachloride
BRL
0.10
0
0 30
Chlorobenzene
BRL
0.10
0
0 30
Chloroform
BRL
0.10
0
0 30
Tetrachloroethene
BRL
0.10
0
0 30
Trichloroethene
BRL
0.10
0
0 30
Vinyl chloride
BRL
0.040
0
0 30
Surr:4-Bromofluorobenzene
0.8644
0 1.000
86.4 64.3 123 0.8230
0 0
Surf: Dibromofluoromethane
1.092
0 1.000
109 71.7 127 1.087
0 0
Surr:Toluene-d8
0.9706
0 1.000
97.1 75.1 118 0.9522
0 0
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 30 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279750
Sample ID: MB-279750
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: MBLK
TestCode: PESTICIDES, TCLP SW1311/8081B
BatchID: 279750
Analysis Date: 05/29/2019
Seq No: 8949334
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane
BRL
0.00050
Endrin
BRL
0.00010
gamma-BHC
BRL
0.000050
Heptachlor
BRL
0.000050
Heptachlor epoxide
BRL
0.000050
Methoxychlor
BRL
0.00050
Toxaphene
BRL
0.0050
Sum Decachlorobiphenyl
0.000455
0 0.0005 91.1 47.7 136
Surr: Tetrachloro-m-xylene
0.000379
0 0.0005 75.7 44.7 126
Sample ID: LCS-279750-1
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: LCS
TestCode: PESTICIDES, TCLP SW1311/8081B
BatchID: 279750
Analysis Date: 05/29/2019
Seq No: 8949336
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Endrin
0.000780
0.00010
0.0008
97.5
75
141
gamma-BHC
0.000767
0.000050
0.0008
95.8
78.5
131
Heptachlor
0.000723
0.000050
0.0008
90.4
70.5
129
Heptachlor epoxide
0.000791
0.000050
0.0008
98.9
82.8
133
Methoxychlor
0.002470
0.00050
0.0030
82.3
61.6
132
Surr: Decachlorobiphenyl
0.000476
0
0.0005
95.1
47.7
136
Surr: Tetrachloro-m-xylene
0.000388
0
0.0005
77.6
44.7
126
Sample ID: LCS-279750-2
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: LCS
TestCode: PESTICIDES, TCLP SW1311/8081B
BatchlD: 279750
Analysis Date: 05/29/2019
Seq No: 8949337
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane 0.004344 0.00050 0.0040 109 75.6 130
Toxaphene 0.007709 0.0050 0.0080 96.4 80.4 129
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 31 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279750
Sample ID: LCS-279750-2
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: LCS
TestCode: PESTICIDES, TCLP SWI311/808IB
BatchID: 279750
Analysis Date: 05/29/2019
Seq No: 8949337
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Surr: Decachlorobiphenyl 0.000486 0 0.0005 97.3 47.7 136
Surf: Tetrachloro-m-xylene 0.000411 0 0.0005 82.3 44.7 126
Sample ID: 1905K43-001BMSI
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: MS
TestCode: PESTICIDES, TCLP SWI311/8081B
BatchID: 279750
Analysis Date: 05/29/2019
Seq No: 8949339
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Endrin
0.000811
0.00010
0.0008
101
62.9
144
gamma-BHC
0.000785
0.000050
0.0008
98.1
66
132
Heptachlor
0.000744
0.000050
0.0008
93.1
66.2
130
Heptachlor epoxide
0.000815
0.000050
0.0008
102
65
130
Methoxychlor
0.002542
0.00050
0.0030
84.7
56.4
134
Surr: Decachlorobiphenyl
0.000403
0
0.0005
80.5
47.7
136
Surr: Tetrachloro-m-xylene
0.000381
0
0.0005
76.1
44.7
126
Sample ID: 1905K43-001BMS2
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399196
SampleType: MS
TestCode: PESTICIDES, TCLP SWI311/808IB
BatchID: 279750
Analysis Date: 05/29/2019
Seq No: 8949340
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Chlordane
0.004436
0.00050
0.0040
ill
71
134
Toxaphene
0.007206
0.0050
0.0080
90.1
67.3
130
Surr: Decachlorobiphenyl
0.000398
0
0.0005
79.6
47.7
136
Sum Tetrachloro-m-xylene
0.000394
0
0.0005
78.7
44.7
126
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 32 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279756
Sample ID: MB-279756
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399233
SampleType: MBLK
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 279756
Analysis Date: 05/29/2019
Seq No: 8950108
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 0.4268 0 0.5000 85.4 49.4 120
Sample ID: LCS-279756
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399233
SampleType: LCS
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 279756
Analysis Date: 05/29/2019
Seq No: 8950109
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4148
0.20
0.5000
83.0
49
120
2,4-D
0.4230
0.20
0.5000
84.6
50.9
120
Surr: DCAA
0.4424
0
0.5000
88.5
49.4
120
Sample ID: 1905K43-001BMS
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399233
SampleType: MS
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 279756
Analysis Date: 05/29/2019
Seq No: 8950116
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4445
0.20
0.5000
88.9
48.2
120
2,4-D
0.4420
0.20
0.5000
88.4
45
130
Sum DCAA
0.4251
0
0.5000
85.0
49.4
120
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 33 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279758
Sample ID: MB-279758
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399208
SampleType: MBLK
TestCode: ICP METALS, TCLP SW1311/6010D
BatchID: 279758
Analysis Date: 05/29/2019
Seq No: 8949219
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
BRL
0.250
Barium
BRL
0.500
Cadmium
BRL
0.0250
Chromium
BRL
0.0500
Lead
BRL
0.0500
Selenium
BRL
0.100
Silver
BRL
0.0250
Sample ID: LCS-279758
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399208
SampleType: LCS
TestCode: ICP METALS, TCLP SW1311/6010D
BatchID: 279758
Analysis Date: 05/29/2019
Seq No: 8949222
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.756
0.250
5.000
95.1
80
120
Barium
4.614
0.500
5.000 0.04895
91.3
80
120
Cadmium
4.494
0.0250
5.000
89.9
80
120
Chromium
4.550
0.0500
5.000
91.0
80
120
Lead
4.438
0.0500
5.000
88.8
80
120
Selenium
4.591
0.100
5.000
91.8
80
120
Silver
0.4523
0.0250
0.5000
90.5
80
120
Sample ID: 1905051-007AMS
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399208
SampleType: MS
TestCode: ICP METALS, TCLP SW1311/6010D
BatchID: 279758
Analysis Date: 05/29/2019
Seq No: 8949225
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.730
0.250
5.000
94.6
50
150
Barium
4.746
0.500
5.000 0.2042
90.8
50
150
Cadmium
4.486
0.0250
5.000
89.7
50
150
Chromium
4.575
0.0500
5.000
91.5
50
150
Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank
BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit N Analyte not NELAC certified R RPD outside limits due to matrix
Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix
Page 34 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279758
Sample ID: 1905051-007AMS
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399208
SampleType: MS
TestCode: 1CP METALS, TCLP SW1311/6010D
BatchID: 279758
Analysis Date: 05/29/2019
Seq No: 8949225
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Lead
7.635
0.0500
5.000 3.704
78.6
50
150
Selenium
4.563
0.100
5.000
91.3
50
150
Silver
0.4601
0.0250
0.5000
92.0
50
150
Sample ID: 1905051-007AMSD
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399208
SampleType: MSD
TestCode: 1CP METALS, TCLP SW1311/6010D
BatchID: 279758
Analysis Date: 05/29/2019
Seq No: 8949226
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Arsenic
4.836
0.250
5.000
96.7
50
150
4.730
2.21 30
Barium
4.766
0.500
5.000 0.2042
91.2
50
150
4.746
0.426 30
Cadmium
4.507
0.0250
5.000
90.1
50
150
4.486
0.466 30
Chromium
4.589
0.0500
5.000
91.8
50
150
4.575
0.307 30
Lead
7.839
0.0500
5.000 3.704
82.7
50
150
7.635
2.63 30
Selenium
4.641
0.100
5.000
92.8
50
150
4.563
1.68 30
Silver
0.4632
0.0250
0.5000
92.6
50
150
0.4601
0.682 30
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 35 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• 279760
Sample ID: MB-279760
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399213
SampleType: MBLK
TestCode: MERCURY TCLP SW1311/7470A
BatchID: 279760
Analysis Date: 05/29/2019
Seq No: 8949577
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury BRL 0.00400
Sample ID: LCS-279760
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399213
SampleType: LCS
TestCode: MERCURY TCLP SW1311/7470A
BatchID: 279760
Analysis Date: 05/29/2019
Seq No: 8949578
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.03980 0.00400 0.0400 99.5 80 120
Sample ID: 1905L31-010BMS
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399213
SampleType: MS
TestCode: MERCURY, TCLP SW1311/7470A
BatchID: 279760
Analysis Date: 05/29/2019
Seq No: 8949580
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury 0.03902 0.00400 0.0400 97.6 80 120
Sample ID: 1905L31-010BMSD
Client ID:
Units: mg/L
Prep Date: 05/29/2019
Run No: 399213
SampleType: MSD
TestCode: MERCURY TCLP SW1311/7470A
BatchID: 279760
Analysis Date: 05/29/2019
Seq No: 8949581
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Mercury
0.04011 0.00400 0.0400
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
100 80
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
120 0.03902 2.75 20
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 36 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• R398954
Sample ID: LCS-R398954
Client ID:
Units: OF
Prep Date:
Run No: 398954
SampleType: LCS
TestCode: ignitability SWI010A
BatchID: R398954
Analysis Date: 05/24/2019
Seq No: 8942843
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Ignitability 81.00 0 81.00 100 93.8 106.2
Sample ID: 1905068-001CDUP
Client ID:
Mathis-1
Units: OF
Prep Date:
Run No: 398954
SampleType: DUP
TestCode:
Ignitability SWI010A
BatchID: R398954
Analysis Date: 05/24/2019
Seq No: 8942845
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Ignitability 180.0 0 180.0 0 20 >
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 37 of 38

Analytical Environmental Services, Inc Date: 31-May-19
Client: Terra Renewal Services ANALYTICAL QC SUMMARY REPORT
Project Name: WQ0038087 - Storage Comp
Workorder: 1905068 BatchID• R398989
Sample ID: MB-R398989
Client ID:
Units: wt%
Prep Date:
Run No: 398989
SampleType: MBLK
TestCode: Fixed Residues (SM2540G)
BatchID: R398989
Analysis Date: 05/24/2019
Seq No: 8944000
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
% Total Solids BRL 0.00100
Sample ID: 1905068-001CDUP
Client ID:
Mathis-1
Units: wt%
Prep Date:
Run No: 398989
SampleType: DUP
TestCode:
Fixed Residues (SM2540G)
BatchID: R398989
Analysis Date: 05/24/2019
Seq No: 8944002
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
% Total Solids
3.470 0.00100
Qualifiers: > Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
< Less than Result value
E Estimated (value above quantitation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
3.310 4.72 20
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 38 of 38

AMERICAN
INTERPLEX
CORPORATION
LABORATORIES
Terra Renewal, LLC.
ATTN: Mr. David Coyle
15797 East State HWY 155
Dardanelle, AR 72834
April 25, 2019
Control No. 233767
Page 1 of 5
This report contains the analytical results and supporting information for samples received on April 23, 2019. Attached
please find a copy of the Chain of Custody and/or other documents received. Note that any remaining sample will be
discarded two weeks from the original report date unless other arrangements are made.
This report is intended for the sole use of the client listed above. Assessment of the data requires access to the entire
document.
This report has been reviewed by the Chief Operating Officer or a qualified designee.
1+. &"��
Steve Brad ord
Deputy Laboratory Director
This document has been distributed to the following:
PDF cc: Terra Renewal, LLC.
ATTN: Mr. John Pipkin
[e-mail]
Terra Renewal, LLC.
ATTN: Ms. Vanya Colburn
[e-mail]
Terra Renewal, LLC.
ATTN: Mr. David Coyle
[e-mail]
Denali Water Solutions
ATTN: Mr. Billy Staton
[e-mail]
8600 Kanis Road • Little Rock, AR 72204 www.Americanlnterplex.com Phone [phone] • FAX [phone]

AMERICAN
INTERPLEX
CORPORATION
LABORATORIES
Terra Renewal, LLC.
15797 East State HWY 155
Dardanelle, AR 72834
SAMPLE INFORMATION
Project Description:
Seven (7) sludge sample(s) received on April 23, 2019
Mathis Storage Lagoon
P.O. No. IR44674
Receipt Details:
A Chain of Custody was provided. The samples were delivered in one (1) ice chest.
Ice chest #1 was delivered with shipping documentation.
April 25, 2019
Control No. 233767
Page 2 of 5
Each sample container was checked for proper labeling, including date and time sampled. Sample containers were
reviewed for proper type, adequate volume, integrity, temperature, preservation, and holding times. Any exceptions are
noted below:
Sample Identification:
Laboratory ID
Client Sample ID
Sampled Date/Time
233767-1
Mathis -1 F1
22-Apr-2019 1430
233767-2
Mathis -1 F2
22-Apr-2019 1430
233767-3
Mathis -1 F3
22-Apr-2019 1430
233767-4
Mathis -1 F4
22-Apr-2019 1430
233767-5
Mathis -1 F5
22-Apr-2019 1430
233767-6
Mathis -1 F6
22-Apr-2019 1430
233767-7
Mathis -1 F7
22-Apr-2019 1430
Case Narrative:
The Geometric Mean for the seven (7) samples is <2000 MPN/g dry weight.
Analysis of soils/sludges are reported on a dry -weight basis unless specified.
Notes
References:
"Methods for Chemical Analysis of Water and Wastes", EPA/600/4-79-020 (Mar 1983) with updates and
EPA/600/5-91-010 (Jun 1991), EPA/600/R-92-129 (Aug 1992) and EPA/600/R-93-100 (Aug 1993).
"Test Methods for Evaluating Solid Waste Physical/Chemical Methods (SW846)", Third Edition.
"Standard Methods for the Examination of Water and Wastewaters", (SM).
"American Society for Testing and Materials" (ASTM).
"Association of Analytical Chemists" (AOAC).
supplements
8600 Kanis Road • Little Rock, AR 72204 www.Americanlnterplex.com Phone [phone] • FAX [phone]

AMERICAN
INTERPLEX
CORPORATION
LABORATORIES
Terra Renewal, LLC.
15797 East State HWY 155
Dardanelle, AR 72834
ANALYTICAL RESULTS
April 25, 2019
Control No. 233767
Page 3 of 5
AIC No. 233767-1
Sample Identification: Mathis -1 F1 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330 Batch: W67905
Fecal Coliform < 2000 2000 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
AIC No. 233767-2
Sample Identification: Mathis -1 F2 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330 Batch: W67905
Fecal Coliform < 2000 2000 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
AIC No. 233767-3
Sample Identification: Mathis -1 F3 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330 Batch: W67905
Fecal Coliform 1400 1400 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
AIC No. 233767-4
Sample Identification: Mathis -1 F4 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330 Batch: W67905
Fecal Coliform < 2000 2000 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
AIC No. 233767-5
Sample Identification: Mathis -1 F5 22-Apr-2019 1430
Total Solids
SM 2540 G 2011
Result RL
15 0.01
Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330
Fecal Coliform < 2000 2000
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339
Units Qualifier
wt %
Batch: W67905
MPN/g
Batch: M7692
8600 Kanis Road • Little Rock, AR 72204 www.Americanlnterplex.com Phone [phone] • FAX [phone]

AMERICAN
INTERPLEX
CORPORATION
LABORATORIES
Terra Renewal, LLC.
15797 East State HWY 155
Dardanelle, AR 72834
ANALYTICAL RESULTS
April 25, 2019
Control No. 233767
Page 4 of 5
AIC No. 233767-6
Sample Identification: Mathis -1 F6 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1556 by 330 Analyzed: 25-Apr-2019 1254 by 330 Batch: W67905
Fecal Coliform < 2000 2000 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
AIC No. 233767-7
Sample Identification: Mathis -1 F7 22-Apr-2019 1430
Analyte Result RL Units Qualifier
Total Solids 15 0.01 wt %
SM 2540 G 2011 Prep: 24-Apr-2019 1618 by 330 Analyzed: 25-Apr-2019 1258 by 330 Batch: W67909
Fecal Coliform < 2000 2000 MPN/g
SM 9221 C, E 2006 Prep: 23-Apr-2019 0826 by 339 Analyzed: 23-Apr-2019 1629 by 339 Batch: M7692
8600 Kanis Road • Little Rock, AR 72204 www.Americanlnterplex.com Phone [phone] • FAX [phone]

AMERICAN
INTERPLEX
CORPORATION
LABORATORIES
Terra Renewal, LLC.
15797 East State HWY 155
Dardanelle, AR 72834
DUPLICATE RESULTS
Analyte AIC No. Result
Total Solids 233725-1 99 wt %
Batch: W67905 Duplicate 99 wt %
Total Solids 233777-2 37 wt %
Batch: W67909 Duplicate 37 wt %
April 25, 2019
Control No. 233767
Page 5 of 5
RPD
RPD Limit Preparation Date Analysis Date Dil Qual
24Apr19 1556 by 330
25Apr19 1254 by 330
0.0871 10.0 24Apr19 1556 by 330
25Apr19 1254 by 330
24Apr19 1618 by 330
25Apr19 1258 by 330
1.15 10.0 24Apr19 1618 by 330
25Apr19 1258 by 330
LABORATORY BLANK RESULTS
QC
Analyte
Result
RL
LOQ
Sample
Preparation Date
Analysis Date Qual
Total Solids
< 0.01 wt %
0.01
0.01
W67905-1
24Apr19 1556 by 330
25Apr19 1254 by 330
Total Solids
< 0.01 wt %
0.01
0.01
W67909-1
24Apr19 1618 by 330
25Apr19 1258 by 330
Fecal Coliform
< 200 MPN/g
200
200
M7692-1
23Apr19 0826 by 339
23Apr19 1629 by 339
8600 Kanis Road • Little Rock, AR 72204 www.Americanlnterplex.com Phone [phone] • FAX [phone]

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RIVER VALLEY INGREDIENTS (TYSON) - HARMONY, NC

0
aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:V109002
Date Completed:09/17/2020
N
N
NO � � J
09/21/2020 2:28 PM
Approved and released by:
Project Manager II: Lucas Odom
pCC/►F�
24r�14A
"
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: V109002
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample -001 was weighed out at 3 times the normal amount. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: V109002
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/ Hammond Solid 09/08/2020 1430 09/09/2020
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: V109002
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/ Hammond
Solid
% Volatile Solids
SM 2540G-
91
%
5
001
Tyson/ Hammond
Solid
Ammonia - N (gas
350.1
21000
mg/kg
5
001
Tyson/ Hammond
Solid
Nitrate -Nitrite - N (soluble)
353.2
90
mg/kg
5
001
Tyson/ Hammond
Solid
Phosphorus
365.1
4700
mg/kg
5
001
Tyson/ Hammond
Solid
TKN
351.2
32000
mg/kg
5
001
Tyson/ Hammond
Solid
Aluminum
6010D
15000
mg/kg
6
001
Tyson/ Hammond
Solid
Calcium
6010D
19000
mg/kg
6
001
Tyson/ Hammond
Solid
Copper
6010D
10
mg/kg
6
001
Tyson/ Hammond
Solid
Lead
6010D
5.9
mg/kg
6
001
Tyson/ Hammond
Solid
Potassium
6010D
2200
mg/kg
6
001
Tyson/ Hammond
Solid
Sodium
6010D
2600
mg/kg
6
001
Tyson/ Hammond
Solid
Zinc
6010D
57
mg/kg
6
(12 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client:Terra Renewal Services, Inc. Laboratory ID:VI09002-001
Description: Tyson/ Hammond Matrix: Solid
Date Sampled:09/08/2020 1430 % Solids: 4.48 09/10/2020 0214
Date Received:09/09/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Volatile S) SM 2540G-1997
1 09/13/2020 2016 MOM
66521
1 350.1
(Ammonia - N ) 350.1
25 09/15/2020 1534 KMC
66593
1
(Nitrate-Nitr) 353.2
1 09/10/2020 1457 AMR
66347
1
(Phosphorus) 365.1
5 09/10/2020 1555 DMA
09/10/2020 1043 66200
1
(Soil pH meas) 9045D
1 09/14/2020 1240 AAB
66608
1 351.4
(TKN) 351.2
1 09/10/2020 1820 DMA
09/10/2020 1126 66184
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
91
%
1
Ammonia - N (gas diffusion)
350.1
21000
5600
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
90
4.5
mg/kg
1
Phosphorus
7723-14-0 365.1
4700
560
mg/kg
1
Soil pH measured in
water @ 20.6 ° C
9045D
5.9
su
1
TKN
351.2
32000
560
mg/kg
1
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
36606/3665A 8082A
1 09/10/2020 1756 NCM
09/09/2020 1604 66092
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
370
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
370
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
370
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
370
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
370
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
370
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
370
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
76 41-132
Tetrachloro-m-xylene
80 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 09/11/20201617 JAB2 09/11/20201052 66330
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.7 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client:Terra Renewal Services, Inc. Laboratory ID:VI09002-001
Description: Tyson/ Hammond Matrix: Solid
Date Sampled:09/08/2020 1430 % Solids: 4.48 09/10/2020 0214
Date Received:09/09/2020
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/10/2020 2203 KSH2 09/09/2020 1520 66081
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
15000
150
mg/kg
1
Arsenic
7440-38-2
6010D
ND
5.5
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.8
mg/kg
1
Calcium
7440-70-2
6010D
19000
1800
mg/kg
1
Copper
7440-50-8
6010D
10
3.7
mg/kg
1
Lead
7439-92-1
6010D
5.9
3.7
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1800
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
15
mg/kg
1
Nickel
7440-02-0
6010D
ND
15
mg/kg
1
Potassium
7440-09-7
6010D
2200
1800
mg/kg
1
Selenium
7782-49-2
6010D
ND
7.4
mg/kg
1
Sodium
7440-23-5
6010D
2600
1800
mg/kg
1
Zinc
7440-66-6
6010D
57
18
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9
F
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PACE ANALYTICAL SERVICES, LLC
Shmlyawir qr"=p kNicec, lint. f7rye : 6 L
DULL Lnl Nvmter: }:IMMC-t4 l:tlk lk'a dak: Rl ,'�t�J�
Sample Receipt te-ekli## (SRC)
Client, '[ EKKA _ Cooiar Inspected byldete: J � 09109V2030
T rz ms of rea-ei t: ❑ SAS [ ❑ CTieu' m J PF i Q Fedi;x Other
❑ Yos I 21ED] 11. Were cuswdy sN als preseu4 rill ilw Uaolel'?
Ye%l F1 Nol LA NA I ?- Ifcu3tod sn-Wls wero uresent, wcre ihey irtactmd unbroken,?
PH Strip ID: NA _ Chlorine Strip If)� NA _ Tenor �l bv, Tr A
O-Willai temr(zaturc up -on J�'ceipt I Derived (COmL, l) icrrperature upon rcroipt SnaCr-0jp ID; 20-i438
3,? f $.7 aC NA JNA or. NA f NA ':C NA 11NA °C -
h'itOW; ❑'Temperature Blank 2]Against Bottics I Gun TD: 5 11t0un Colreclirm Factau- 0 °C
h'lpthod aPcoo'.art- ❑ Wor Ice ❑ lc�, Pa :ks [] Dry itxa ❑ forte
© Yes ❑ 10 ONA 3. [fte�nperature of any ux�l�rexceede[kb,Ofii, was Prajat:Malsae r leliradF
1'M wuH Notified by, phone r email i tao�tc-face (circle vne)-
® yrs ❑ No QMA 4- Tstllc cDmmereial Courricr'spackinusl'p amobed to Eu form? -
V, Yrs ❑ No 5, wrro prore,'7imic iy pmc7u.c5 [rdl_�itluiahrd�lpCpiY�d}fa[ipvf�d?
J Yes Nrr f4. V,r:!re sample. IDS listed oil the COC1.1
® Yes ❑ NO 7, ',"Jcrc sample IDS iisterd tul A 61mmple-unnmineXs?
Yes No R- Was 001-leetipu doL, & time listed On die COC?
❑ Yes ® No 9. Wis collection date & tirl,c listed on--][ saTlll)lc CQJ1lai11cr'I?
0 Ves ❑too 10. Vid all cnnixinor label i,tra,_ri n (ID, date, Lima) agree with the CC)C?
❑ Y ffN-7 ] _ . W-e tests to be performed l isted On the COC? .
Did all samples arrive in the proper Gamtalnets for rsich rrsr irl>dAT in goad condition
m Ye: ❑ Jo 1(lunti-oken, ]ids on, cta)7
® '�"ens [� No 13. ;h'as adeq u.ttr camp le vol u rr, � avxilabl-?
671 Yes ❑ No i 1;'erc rlI RrunplasrecciV0dWithul'l, the holding -or49 hours, whu.hever cons ea first'}
Ye9 Ma I S, '`Yens au � sat:tplcs cnntainer� missin e�icess (cis�cle one sorrlples �101 listed orl CQC7
❑ Y{�s ❑ ll o ®NA 16- For -VOA and RSK-175 sRmples, ivviv bubbles prcEent �"pe'.i i4 " ('/."ar 6mnt itt nliaruuinr}-
iu sAny Dfthe VC)A vials?
[l Yes No NA 17- Weroall DR01mclel&Jnurrient %anjpjgs AoCeived ail N pH of<2?
�] ye-4 ❑ No ®l~ A 18. cro a:i anise Senn lea rdCGiv�xJ at a I� � 12 ;8n;i .3u]f L- %mpJw received at a p1A ., 9?
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] 9. Wzrb a, I Rpplicabhe N H- 1'KNV cyrani dalphei1& ' Z (< ,SmW7,) smrp ; tm;; of residival
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El YES CI o ®1�iA '20, Wtjecliarttm Tmrks!requests (ix, n�tested dilution« MS4d8l) desi-gnations, etc:.,,)
cemretlY transeribtd f. om the COC iuta the ConlnlCrl IccLic,n in L]MS?
' ]MO 21, Was the qudcnumber Iis'+d-on the ccm#ainer [ahei? lfyes, QwjC! 0 NA
'ample Pr96serrnNon (] iE4' be-cornpietitd far ally nurnpfc(s) incorrectly pruservi�'i OFwim 1"tvdspme.)
ample(s) N _ }vmrccGived inrion-ectly E3;1.��.Tved anal w6ra adjustarlArwardi�gly
i €ample rel iving with NA FL of c frelo om; ]-125C14, 141NO3, HCI, NaOR using SR't NA
'iNM of preeerusatian NA If morn thou c=te PM4orwat-w is neadcd, pleaw cute in The eotnmstr�t helow.
arlp]L(sj NA _Wore tweiytcd with bubbl �-6 rrm in di�merer-
atnple;5(s) NA � _ v; cro mcei zd with'Fac > 0.5 JngnL (If 41.9 is Ito) and were
TkAl Rd accorxli rigly in m mple receiving %v M Rrdium rt itmulfatc ('*1n whit Sh ea l;• iIJ: NA
Nrev do labels applied by, BMG
Comt±le S.'
Dale.: 091KI 02G
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson/Harmony
Lot Number:UJ17022
Date Completed:11/04/2019
11 /05/2019 4:53 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
pCCRF�4
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: UJ17022
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ17022-001. Due to low % solids the initial amount of these samples were 3 times the
standard procedure amount per PM's request. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terra Renewal Services, Inc.
Lot Number: UJ17022
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/Harmony Solid 10/16/20191430 10/17/2019
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terra
Renewal Services, Inc.
Lot Number: UJ17022
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
Tyson/Harmony
Solid
% Volatile Solids SM 2540G-
86
%
5
001
Tyson/Harmony
Solid
Ammonia - N (gas 350.1
19000
mg/kg
5
001
Tyson/Harmony
Solid
Ignitability (Pensky-Martens 1010A
>140
° F
5
001
Tyson/Harmony
Solid
Nitrate -Nitrite - N (soluble) 353.2
32
mg/kg
5
001
Tyson/Harmony
Solid
Phosphorus 365.1
7600
mg/kg
5
001
Tyson/Harmony
Solid
TKN 351.2
55000
mg/kg
5
001
Tyson/Harmony
Solid
3+4-Methylphenol 8270D
3.3
mg/L
6
001
Tyson/Harmony
Solid
Aluminum 6010D
10000
mg/kg
8
001
Tyson/Harmony
Solid
Calcium 6010D
24000
mg/kg
8
001
Tyson/Harmony
Solid
Copper 6010D
12
mg/kg
8
001
Tyson/Harmony
Solid
Potassium 6010D
3700
mg/kg
8
001
Tyson/Harmony
Solid
Sodium 6010D
4800
mg/kg
8
001
Tyson/Harmony
Solid
Zinc 6010D
51
mg/kg
8
(13 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17022-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:10/16/2019 1430 % Solids: 4.97 10/18/2019 0021
Date Received:10/17/2019
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile
S) SM 2540G-1997
1 10/20/2019 2138 MOM
32627
1 350.1
(Ammonia - N ) 350.1
25 10/24/2019 1700 DFR
32938
1
(Ignitability) 1010A
1 10/25/2019 1147 SLC
33401
1
(Nitrate-Nitr) 353.2
1 10/24/2019 2336 AMR
33258
1
(Phosphorus) 365.1
10 10/24/2019 1157 DMA
10/23/2019 1429
32936
1
(Reactive Cya) 7.3.3
1 10/30/2019 2135 KFE
10/29/2019 1211
1
(Reactive Sul) 7.3.4
1 10/30/2019 2126 HET
10/29/2019 1211
1
(Soil pH meas) 9045D
1 10/27/2019 1658 HET
33493
2 351.4
(TKN) 351.2
2 10/28/2019 1836 DMA
10/23/2019 2113
33077
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-
86
%
1
Ammonia - N (gas diffusion)
350.1
19000
5000
mg/kg
1
Ignitability (Pensky-Martens
Closed -Cup)
1010A
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
32
4.0
mg/kg
1
Phosphorus
7723-14-0 365.1
7600
1000
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 19.7 ° C
9045D
6.0
su
1
TKN
351.2
55000
1000
mg/kg
2
TCLP Volatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B
8260B
10 10/26/2019 0308 STM
33432 10/23/2019 2034
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260B
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260B
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260B
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260B
ND
0.050
mg/L
1
Chloroform
67-66-3 8260B
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260B
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260B
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260B
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260B
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260B
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
94 70-130
Bromofluorobenzene
93 70-130
Toluene-d8
99 70-130
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17022-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:10/16/2019 1430 % Solids: 4.97 10/18/2019 0021
Date Received:10/17/2019
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270D 1 10/28/2019 2105 JCG
10/26/2019 2059
33458 10/23/2019 0103
2 1311/3520C
8270D 10 10/29/2019 1446 SCD
10/26/2019 2059
33458 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270D
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270D
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270D
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270D
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270D
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270D
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270D
3.3
0.40
mg/L
2
Nitrobenzene
98-95-3 8270D
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270D
ND
0.20
mg/L
1
Pyridine
110-86-1 8270D
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270D
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270D
ND
0.040
mg/L
1
Run 1 Acceptance Run
2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery
Limits
2-Fluorobiphenyl
66 37-129 58
37-129
2-Fluorophenol
48 24-127 43
24-127
Nitrobenzene-d5
50 38-127 44
38-127
Phenol-d5
58 28-128 50
28-128
Terphenyl-d14
94 10-148 73
10-148
2,4,6-Tribromophenol
94 41-144 57
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 10/31 /2019 2201 DAL1
10/30/2019 2135
34009 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Surrogate
Run 1 Acceptance
Q % Recovery Limits
DCAA
69 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A 1 10/21/2019 1905 CHG
10/20/2019 2315
32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above
the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17022-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:10/16/2019 1430 % Solids: 4.97 10/18/2019 0021
Date Received:10/17/2019
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 3660B/3665A 8082A 1 10/21/2019 1905 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
340
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
340
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
340
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
340
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
340
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
340
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
340
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
85 41-132
Tetrachloro-m-xylene
79 35-106
TCLP Pesticides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /3520C
8081 B 1 10/31 /2019 2033 DAL1
10/28/2019 0015 33512 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5 8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
70 20-131
Tetrachloro-m-xylene
66 26-132
CVAA
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B 1 10/29/2019 1545 KSH2
10/29/2019 1316 33157
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
1.5
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17022-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:10/16/2019 1430 % Solids: 4.97 10/18/2019 0021
Date Received:10/17/2019
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 10/28/2019 0613 LLL
10/27/2019 1845 33481 10/23/2019 0103
1 1311/7470A
7470A
1 10/29/2019 0914 JMH
10/28/2019 1406 33559 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/26/2019 1543 KSH2
10/24/2019 1314 33115
2 3050B
601 OD
1 10/27/2019 0301 LLL
10/24/2019 1314 33115
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
10000
130
mg/kg
1
Arsenic
7440-38-2 6010D
ND
4.8
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.6
mg/kg
1
Calcium
7440-70-2 6010D
24000
1600
mg/kg
1
Copper
7440-50-8 6010D
12
3.2
mg/kg
1
Lead
7439-92-1 6010D
ND
3.2
mg/kg
1
Magnesium
7439-95-4 6010D
ND
1600
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
13
mg/kg
1
Nickel
7440-02-0 6010D
ND
13
mg/kg
1
Potassium
7440-09-7 6010D
3700
1600
mg/kg
2
Selenium
7782-49-2 6010D
ND
6.5
mg/kg
1
Sodium
7440-23-5 6010D
4800
1600
mg/kg
1
Zinc
7440-66-6 6010D
51
16
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
ShNIJ Enwj")e,k48eF%j . rm
19 CM& ofcasmaryFZGCawd
10rLva mflpMiLDrh+
4%8LC4mllk ,&tM CaWN M72
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Lad—..0 Ir.rb2r.JJEAUe j
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
North Caro in2 P-Brrrijt Parameters
2. Residuals sW be aualyzud to dcliKma#rate that' ere �%Ij'11118
wd R-wowey Act (RCPA)- The Ana cx►rt'osivii idwaeterlltk I�ehi procedure T�bitiy, re$lad toxicit yAttg'AraA,and the 1�cr Aj1tee shall wiatain these results fj- a minimum spars. ed iu
eXq�tion5l�pm [be re of five years. Any
gnir'emertts in thi � cvndifinn� smell be spxx:iineed im Attwlun,t;nt A..
paro al"Qlyais shall i=lude the followiag parameters (the regulak" level b3 mi]ligf-arns por litay
is iji
Arsenic (5.0)
l A-Dich1wubanz= (7.5)
Barium (1 ,0)
1 2-Dicaioraeliie (0 5)
Bye 0.
(
2,]-Dr`,chloroEtliyie:ne(O.i)
to
Cadmir(1.0)
2,I?initrobolueno(4.x)
captcrlcrride (0-5]
pn (0.02)
WMilordaae
{0.0)
l xxcblara+ben a (0,11)
IIL
l er=Rv (100.0)
I taii�lor (and its •tLydr xi{le)
Z
''moro (6,0)
�0.�a�—
Hexachloro-1,3butadl ne (4.5)
hromilxrn (5.0
B xacwo a-}raire(3_Q)
ham—
t c l (200.0)
Lead (5.4)
rasol (200,0)
Liudane (0.4)
.Crfsol (200,0)
M&'Lg4ry (0.2)
2nsol (2ao o)
Nfcthoxyalrlar (10,0) 1
IQCOLPg� (2,0)
Penitachiorcpkenol (100.0)
Pyridine (5,0)
Silver (5-0)
Tetru0W0r0cthy1e (0, 7)
Toxt (0.5)
Tril;hl0rl�ylene {0.5}
2,45-Tkichiaropheuol (4{10.0)
2,4.6mTricjaropbcn0l (2.0) -
2,4,5-TP (Sdvea) (1.o)
Vinyl eblcride (0.2)
�I.
I. Are zlis soli he oozjucWd on resijuals f�nm moh &Dune gaming frlcility at the &equt y
sge�i#Tn AttaA=cnt rmd th,a permiam sbalt ]raRjR 8iir the results fast a m ff mum of f
•he vrshall include- the following pal rpive yearsrs
Alumim=
�`
711T10D� I�'I,t3g4
try
Ataemc
�'a[lmiun�
w
-
Capper
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mm ry Potmsiarn
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Nidbi
lditrata-Niirite Nitre gen
Nfct t ToW Salida • '�
PH
sp>~rnrt�s Volt e, Solids
PCB's
i
TERRA RENEWALSERVICES
479-747-8192
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Q&N F.nvironPYk.hW '3c:r�un , lnc, ] ?i w I
1740n1ueriLNWnaSf: MF}t'+'A DC-14
Sample Receipt Checklist ( R
Client, TERRA RENEWAL C roler Inspected byldaLe: LKH 1 10-17-2019 Lot g= U117022
Figi
f rticcipv ` ESI C1 ietlt UPS ❑ IrOEX Lj Otte c
were custndy seats present on the cooler? Wo NA 2- If Gusto seals)v= present, were fbev intact and unbraieew
1D; NA Chloride Strip I1D; NA Tested hy: NA
=11eratur�e R10a roceipt+ Deriv4d (Corrected)'temperati upon rcaripr " Solid Snap -Cup III, 19-Ifi16
DC N li�A oC NA / NA "C NA rNA 7C
1;etllud;CTemperaoKllreB"ankoAgninstBattles JR.QunlD: 5 IRGun Cotrcotion);ac:vr. 0 C
�geth{xl c,rcc,4lant:
_
21 WCt loC Q lt:p Pacl4s ❑ Ifcc ❑ None
❑ Yea
Q No
V1 NA
'_ lr(terupe:aturc of any odolcr exxCef fed 6,0'C:, was PPojoct lrlanager Tln1 iFicci7
PM v m Nrsti#iod by: phone f email l face-to-face (circle 4:nc)-
❑ Yes
0 No
O NA
4. Iw ;lIc ootnrnemial courier`s Pa-Lkirgsl ip attached 10 this forme?
0 Yes
❑ Nv
5. Wcre properctrstody pruoecluras (relinquiti,c'Vreceived) FollowcV
Ycril
El NO
16. Ware swilpla IUs listed on the COC?
® Yal, I
f D No
7. Werc sa Inp] e I Inc 1 irbcd on R11 Sample aontaijterx?
® Yes
❑ Nu
B. Was collecquu date & time listed on lbe COC7
Yes
❑hro
9. Was collection date & time listed on all sample containers?
It'sEEP
Nrr
10, Did aJI Container laical information. (ID, date, time) 3igrm with 11w COC:
O YesFlo
_
i I- Wcrc tests to be pLTfanned IDAed an the COC?
91 Yes
❑ No
12- Did all samples arrive in the prr.,pcT conrain= for caclo krs1 andfor ill gaud conditicm
(unbroJ.eii_ lids can. ctc,)7
® Yes
No
13. Was adeyuale sample %vlumc available"
Yes
❑ )
14- WeTe all sa,npir.,,; rccrived widiiu K the holding time a. 4S hours, whichewtr csnme5 �u t7
Yej
O No
15- Wue au spruplcs conminers trussin 'exca2 (circle ter,) sam le:- Not listed 4n COC?
❑ Yes
❑No
21 NA
16. For VOA and RS1C-175 samples, water bubbles prrseot >"pea -Size'° (W*ar 6mm in diameter)
Irl a* of the VOA vialsr?
❑ Yes
7INO
NA
17. WeTa all DROhrietakiiiirrri:.nt satiypics rcceiued at s Hof<2?
❑ Yes
❑ Na
®IdA
J 8. Were all 0 anidv sarnlAcs rcLdiretf at FL pH r 12 tvtl sulfide samples receivtd at a piI 9?
❑ Yes ❑ No DNA 14- ea al] uppllcabie NH317 KN(CyHuidc.�phen0l r625 { 0-5mgfL) samples frc:. ❑ r%j
chlorine?
❑ yes 0 No 0 VA 20. Worecliettl xmarksr'regtK�st (i-e. rNuLsied dihiTion5, M&N 3Ddcsiglt2tions, etc---�
cod'r tly transcribed from the COC intrrthe commentseotitan in LIM.S?
❑ Yes N+} _ 2J - %Vas the guate iiurnber listed on the conWricr label'! If' = Quote f NA
temple Prescrration (Mtlat be compIrled far any sautiple(s) irrwrractly preserved or with heads p")
mphe(s) 14A
n mrtplc mxeMng witJ1 NA
'im a of pmsenrjafon NA
_ ware reuLlvcd incorrutly preserved and were ad.lusted
mL Dfcircle one= H2 U4* hTN03, HCI. NaUH Laing iC NA
If more Ihan one rXestrvative k nC.cded, plmsc now in the comtnetrl ; below.
Accordingly
nple(s) NA
- were reaetvett with I:xtb6lcs %6 Torn in diameter,
nples{s} t1li wwc received with TRC = 0.5 mWL (lf ttl9 iq nrr) and w=
Jz;tcd aoc0Nin213� in,'AM lc mceiv[ng-%ith sodium thiogulfRte {N2520)}with 5h.-aly ID— NA
barvA labels applied b)- LKI l
Corntr,ortts:
Hate 10.17-2019
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

Analytical Results �,* STATESVILLE
ANALYTICAL
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 09/08/2020
Reported: 09/10/2020
For: Tyson Harmony
Comments: GM 127584 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200908-34-01
Fecal Coliforms
H1
226131
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-01
Percent Solids
1-11
3.98
%
SM2540B-2011
09/09/2020
WC
200908-34-02
Fecal Coliforms
H2
133333
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-02
Percent Solids
H2
3.75
%
SM2540B-2011
09/09/2020
WC
200908-34-03
Fecal Coliforms
H3
256410
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-03
Percent Solids
H3
3.51
%
SM2540B-2011
09/09/2020
WC
200908-34-04
Fecal Coliforms
H4
122850
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-04
Percent Solids
H4
4.07
%
SM2540B-2011
09/09/2020
WC
200908-34-05
Fecal Coliforms
H5
86806
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-05
Percent Solids
H5
5.76
%
SM2540B-2011
09/09/2020
WC
200908-34-06
Fecal Coliforms
H6
243243
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-06
Percent Solids
H6
3.70
%
SM2540B-2011
09/09/2020
WC
200908-34-07
Fecal Coliforms
H7
274390
MPN/g
SM92210E-2006
09/09/2020
WC
200908-34-07
Percent Solids
H7
3.28
%
SM254OB-2011
09/09/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 200908-34-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200908-34-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-34-03
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-34-04
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-34-05
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-34-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200908-34-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

TYSON - WILKESBORO, NC

0
aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:V109001
Date Completed:09/17/2020
09/21/2020 2:22 PM
Approved and released by:
Project Manager II: Lucas Odom
pCC/►F�
24r�14A
"
ANSI National Accreditation Board
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: V109001
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample -001 was weighed out at 3 times the normal amount. The LOQ has
been elevated to reflect the dilution.
PCBs by GC
The following sample was diluted due to the nature of the sample matrix: V109001-001. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: V109001
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/ Wilkesboro Solid 09/08/2020 1530 09/09/2020
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: V109001
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/ Wilkesboro
Solid
% Volatile Solids SM
2540G-
97
%
5
001
Tyson/ Wilkesboro
Solid
Ammonia - N (gas
350.1
1400
mg/kg
5
001
Tyson/ Wilkesboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
33
mg/kg
5
001
Tyson/ Wilkesboro
Solid
Phosphorus
365.1
450
mg/kg
5
001
Tyson/ Wilkesboro
Solid
TKN
351.2
6200
mg/kg
5
001
Tyson/ Wilkesboro
Solid
Aluminum
6010D
220
mg/kg
6
001
Tyson/ Wilkesboro
Solid
Copper
6010D
8.2
mg/kg
6
001
Tyson/ Wilkesboro
Solid
Zinc
6010D
15
mg/kg
6
(8 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:V109001-001
Description: Tyson/ Wilkesboro Matrix: Solid
Date Sampled:09/08/2020 1530 % Solids: 8.42 09/10/2020 0214
Date Received:09/09/2020
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Volatile S) SM 2540G-1997
1 09/13/2020 2016 MOM
66521
1 350.1
(Ammonia - N ) 350.1
5 09/15/2020 1532 KMC
66593
1
(Nitrate-Nitr) 353.2
1 09/10/2020 1455 AMR
66347
1
(Phosphorus) 365.1
1 09/10/2020 1550 DMA
09/10/2020 1043 66200
1
(Soil pH meas) 9045D
1 09/14/2020 1236 AAB
66608
1 351.4
(TKN) 351.2
1 09/10/2020 1820 DMA
09/10/2020 1126 66184
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
97
%
1
Ammonia - N (gas diffusion)
350.1
1400
590
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
33
2.4
mg/kg
1
Phosphorus
7723-14-0 365.1
450
59
mg/kg
1
Soil pH measured in
water @ 20.5 ° C
9045D
4.8
su
1
TKN
351.2
6200
300
mg/kg
1
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
5 09/11/2020 1036 NCM
09/09/2020 1604 66092
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
1000
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
1000
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
1000
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
1000
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
1000
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
1000
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
1000
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
58 41-132
Tetrachloro-m-xylene
63 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 09/11/20201615 JAB2 09/11/20201052 66330
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 0.89 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:V109001-001
Description: Tyson/ Wilkesboro Matrix: Solid
Date Sampled:09/08/2020 1530 % Solids: 8.42 09/10/2020 0214
Date Received:09/09/2020
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/10/2020 2157 KSH2 09/09/2020 1520 66081
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
220
75
mg/kg
1
Arsenic
7440-38-2
6010D
ND
2.8
mg/kg
1
Cadmium
7440-43-9
6010D
ND
0.94
mg/kg
1
Calcium
7440-70-2
6010D
ND
940
mg/kg
1
Copper
7440-50-8
6010D
8.2
1.9
mg/kg
1
Lead
7439-92-1
6010D
ND
1.9
mg/kg
1
Magnesium
7439-95-4
6010D
ND
940
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
7.5
mg/kg
1
Nickel
7440-02-0
6010D
ND
7.5
mg/kg
1
Potassium
7440-09-7
6010D
ND
940
mg/kg
1
Selenium
7782-49-2
6010D
ND
3.8
mg/kg
1
Sodium
7440-23-5
6010D
ND
940
mg/kg
1
Zinc
7440-66-6
6010D
15
9.4
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10
T

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
:. Residuals sbaM be analvzod to donrdasttate they are UTM C nnaery tirxn
and Rccavcry Ark (1�C;i�A). '1 an3 es
sha rotYYrca-al. Rxj,_-rmGy xpwi$td in
Attacluafatl A, HiA dw Formif oo shall maintain these results for a minimum Qf five years. Any
cuxgtiom fr4.qu thu i uimmunts w dhis condition atoll lie specified m A'_-�t:l mmz A,
ThOGjMpMa1*E shall inolUdc #1C following pal -amain (di : regu atuay lam= in millignm:m per firer
is in p=thewsy.
I An atrtalyds shall be oanduct-2d on rt;.kduals from each sources gewzating £acUy at tote ltr uen;,,y
specified iu AtWchmmt A, and tho PormiucE 4�all maintain the temits fo,• a minimum 4f $ve yCarr.il,
The ami5%iis shO iaclude the folkwing parameter;
rw
Aluminum
1><ercury
t-otassixipa
Ammon, E-Nitrogcw
Molybdenum
Sci�iiun
ZBBL G
&R]
Soli-XM
+1
-
A1U3A
l�iti'�t4f��liiZtlC=rZO�TCt7
LU
�yy
Root Total Scuds
TT N ...
{ lcsult�
Pit
Zinu
Lead
Phosphonis
volatila SO N$
P B's
TERRA RENEWAL EVE S
479-747-819
Attach Brent to CDC ion. --.Sources. r€+ - ke,
Dat$: -
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
st�'.y E.,ri'Q1:r11e1H8l Sr,le:s. Ise.
_7oeurnenm Nwmicr. MUJtrl KC--14
C[ieJlt: TFRP-A
Sample Receipt Checklist {SRC)
Cooler IFI.41UiAL-d lljdatc: hr'- I OWM2020 Lot if= V109001
'nkp I di
ErfccG4cM?U; R?ZVI&
Mmtru of receipt_ © SESI C]icnl. 0 UPS t=cdFx pater.
- -
[1 Yes
! a
I - Wen: cu5iv�y ;'4al3 prc;Amt on 1C CO-Gk_7
. lfcustadyfoals were presenr, we--e thffy in?wr.wadi tmbrokeni
Yes
7tio
NA
PT [ Ship I D= NA Ch4wine Strip Ji7; NA _ TmWd t�v: NA
04bial tsmpecature apou receipt IDerived(C.rmrctecl) ternperaLura'Jpon receipt %Sa[ad Snap-Ottp ]D. 2G-1d38
5.7 ,?5.7 DC NA /NA QC NA )ONA µC NA ;NA °C
Meth&d,. ❑Temperature Blank 2]AgainStBottles IR Cim ID: 5 IR Durk Cprrmlioa Fodor. 0 IC
ethodofroulmil: ® Wcl'ee ❑ lc llmr•ks 11__QryJco ❑ None
❑ Yes
No
®1 A
3- Tf i mmPerature of any coo=er exceeded 6,0°G, was Projoct Manager Na:ifled?
?N1 was Notified tky; pJione I email I too-to-["c (oircJc anc)-
® yw
❑ -Ko
❑ KA
4. 1 Jta wmmcrciul oawier's packin_&Lip auachcd te, tlli� form?
1, Were. proper cy du u:&10 r?ceras(,eN3gvishmlr'rcL=ivs�-d)folJovti+cd?
(3, Wom 3umpla IDs listed an ite C0
7. Were gamplC IDS listed on zill sample arrituinvr:^
IS. Wat tullt,cOun da[c & Hine ]ismd cm the COC? - —
1'p,3
❑lea
W5
No
® YMI
0 No
I Yrw;
Yes
❑ Nu
ONO
9, Was Collection data 4iilme lisped odi idl somple coma-rc`Js'l
10. Did all c,mtainar labo- kifonnatiou (ID, cl;U, lime) agree with the c(x;'}
1 l , Were tc_5 t t' be pt;rformed listed on the COC? -
YJ Ye"
❑ I es
❑ NIr
❑ , to-
Yn
❑rho
I(anbrokcn,
=2. Did a3 samples arrive in the proper cotnlairers forcwJi test aiwkor i,J ¢❑(,d uicnditis;n
lidsrn. roc,;?
13. Was a*L1aU-iwJlrrly wohime im- Jlable7
14- Were all SaMl"-.1cWvcd within ',4 the holding timr, oT 4S himus, WllrA MC L'0Mt3H First?
15, VkWcm any mriipIl�s "ntsivars ]rissilte excess {ti-rtlk� rna) samples Mn lised Ott COC)
16. For VOA and MK-175 �t J,lcs, wore bubbles present "pc size" (V4"or 61mn in dilrnocr)
1
In any of tJte FICA vials?
® Ycs
0 No
Yes
❑ No
FQ `yus
tdo
❑ Ycs
❑ Na
®NA
❑
No
0 KAI
17. W-Qrc ail DX(-VFn57aisl0utrient :Mfplcs rcoci Wed 2l a p[T Of -� 2?
I C Were all c aiiirlc I;rnlrl i received at a pJ4 > 12 ind zilMde at a pl I ? 4°
l -urc a' applimble hiIl� {l:hilcyanidelp ua G25 ( 0-jru l ) samples tree nF resi ua
rdilorine?
❑ Vas
❑ No
® NA
❑ Y-
❑ No
21 NA
Li Yes
❑ Nr`
® NA
2..0. Were client remark-s-'rcg=5tsti,c. requested di[utionz, ]4 &MSDdt!%ignati{rns, etc...)
Morrectly transcribed from lho COC into the comment scctior, in LINTS?
21. Was tJte quote niAmbcr lisl'e,�l a_] the con intr label`? if Q-rote 4 NA
n Yes
Na
sample Preservation (.Must be completed Cor ary� aarlpla(s) inearrectly preserved or wads lwxd.j,ace.)
Sawplc(s) NA war~ rece:vcd InuolTc ly rr �erVarl and were adlr steel ;wcc}rciingly
In m-n-j1e rccciving wljr LNA ntL of eircic one: 112.M43 HNCXI, Kt:.1, Naoll llSJJSig 51t 1r NA
,mc of prescrwation NA 1: �uarc tlt�n o�r� pierJGnr,tivt; i ,taeded, please n0tc in the comment blow.
vmm received wiph brtbt&r. %6 ITi rr, i i i ctiamr«leT,
antple3(s) NA _ _ were -e�eitred witftTRC>00 5 Tn?A,(If919 is uo) and were
djusted arcgrding[y is mmp]a giving with Janhiuni flus4'Nte (NLl S,03) wrih SheFdy ID; NA
SR barcode lahek applied V, BNIC pate; (IRM1200
C.ar,tmentc�
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson/Wilksoboro
Lot Number:UJ17021
Date Completed:11/04/2019
11 /05/2019 4:50 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
pCCRF� 4
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: UJ17021
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ17021-001. Due to low % solids the initial amount of these samples were 3 times the
standard procedure. The LOQ has been adjusted accordingly.
TCLP VOCs
Due to insufficient sample received, the initial sample amount used for the following sample deviated from
the standard procedure: UJ17021-001. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terra Renewal Services, Inc.
Lot Number: UJ17021
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/ Wilkosboro Solid 10/16/2019 1500 10/17/2019
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terra Renewal Services, Inc.
Lot Number: UJ17021
Sample Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
Tyson/ Wilkosboro
Solid % Volatile Solids SM 2540G-
98
%
5
001
Tyson/ Wilkosboro
Solid Ammonia - N (gas 350.1
1500
mg/kg
5
001
Tyson/ Wilkosboro
Solid Ignitability (Pensky-Martens 1010A
>140
° F
5
001
Tyson/ Wilkosboro
Solid Nitrate -Nitrite - N (soluble) 353.2
29
mg/kg
5
001
Tyson/ Wilkosboro
Solid Phosphorus 365.1
3300
mg/kg
5
001
Tyson/ Wilkosboro
Solid TKN 351.2
66000
mg/kg
5
001
Tyson/ Wilkosboro
Solid Aluminum 6010D
180
mg/kg
8
001
Tyson/ Wilkosboro
Solid Copper 6010D
21
mg/kg
8
001
Tyson/ Wilkosboro
Solid Zinc 6010D
43
mg/kg
8
(9 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17021-001
Description: Tyson/ Wilkosboro Matrix: Solid
Date Sampled:10/16/2019 1500 % Solids: 6.27 10/18/2019 0021
Date Received:10/17/2019
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile
S) SM 2540G-1997
1 10/20/2019 2138 MOM
32627
1 350.1
(Ammonia - N ) 350.1
2 10/24/2019 1658 DFR
32938
1
(Ignitability) 1010A
1 10/25/2019 1109 SLC
33401
1
(Nitrate-Nitr) 353.2
1 10/24/2019 2335 AMR
33258
1
(Phosphorus) 365.1
5 10/24/2019 1157 DMA
10/23/2019 1429
32936
1
(Reactive Cya) 7.3.3
1 10/30/2019 2134 KFE
10/29/2019 1211
1
(Reactive Sul) 7.3.4
1 10/30/2019 2126 HET
10/29/2019 1211
1
(Soil pH meas) 9045D
1 10/27/2019 1657 HET
33493
2 351.4
(TKN) 351.2
2 10/28/2019 1836 DMA
10/23/2019 2113
33077
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-
98
%
1
Ammonia - N (gas diffusion)
350.1
1500
320
mg/kg
1
Ignitability (Pensky-Martens
Closed -Cup)
1010A
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
29
3.2
mg/kg
1
Phosphorus
7723-14-0 365.1
3300
400
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 19.8 ° C
9045D
4.7
su
1
TKN
351.2
66000
800
mg/kg
2
TCLP Volatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B
8260B
50 10/26/2019 0355 STM
33432 10/23/2019 2034
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260B
ND
0.25
mg/L
1
2-Butanone (MEK)
78-93-3 8260B
ND
0.50
mg/L
1
Carbon tetrachloride
56-23-5 8260B
ND
0.25
mg/L
1
Chlorobenzene
108-90-7 8260B
ND
0.25
mg/L
1
Chloroform
67-66-3 8260B
ND
0.25
mg/L
1
1,2-Dichloroethane
107-06-2 8260B
ND
0.25
mg/L
1
1,1-Dichloroethene
75-35-4 8260B
ND
0.25
mg/L
1
Tetrachloroethene
127-18-4 8260B
ND
0.25
mg/L
1
Trichloroethene
79-01-6 8260B
ND
0.25
mg/L
1
Vinyl chloride
75-01-4 8260B
ND
0.050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery
Limits
1,2-Dichloroethane-d4
94 70-130
Bromofluorobenzene
94 70-130
Toluene-d8
98 70-130
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17021-001
Description: Tyson/ Wilkosboro Matrix: Solid
Date Sampled:10/16/2019 1500 % Solids: 6.27 10/18/2019 0021
Date Received:10/17/2019
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270D 1 10/28/2019 2041 JCG
10/26/2019 2059 33458 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270D
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270D
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270D
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270D
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270D
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270D
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270D
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270D
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270D
ND
0.20
mg/L
1
Pyridine
110-86-1 8270D
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270D
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270D
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
62 37-129
2-Fluorophenol
38 24-127
Nitrobenzene-d5
48 38-127
Phenol-d5
67 28-128
Terphenyl-d14
92 10-148
2,4,6-Tribromophenol
86 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /8151 A
8151A 1 10/31 /2019 2138 DAL1
10/30/2019 2135 34009 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
74 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A 1 10/21/2019 1852 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
270
ug/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above
the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17021-001
Description: Tyson/ Wilkosboro Matrix: Solid
Date Sampled:10/16/2019 1500 % Solids: 6.27 10/18/2019 0021
Date Received:10/17/2019
PCBs by GC
Run Prep Method
Cleanup Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 3660B/3665A 8082A 1 10/21/2019 1852 CHG
10/20/2019 2315 32608
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1221
11104-28-2 8082A
ND
270
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
270
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
270
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
270
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
270
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
270
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 41-132
Tetrachloro-m-xylene
76 35-106
TCLP Pesticides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311 /3520C
8081 B 1 10/31 /2019 2018 DAL1
10/28/2019 0015 33512 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5 8081B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
36 20-131
Tetrachloro-m-xylene
70 26-132
CVAA
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B 1 10/29/2019 1542 KSH2
10/29/2019 1316 33157
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
1.2
mg/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:UJ17021-001
Description: Tyson/ Wilkosboro Matrix: Solid
Date Sampled:10/16/2019 1500 % Solids: 6.27 10/18/2019 0021
Date Received:10/17/2019
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
601OD
1 10/28/2019 0607 LLL
10/27/2019 1845 33481 10/23/2019 0103
1 1311/7470A
7470A
1 10/29/2019 0912 JMH
10/28/2019 1406 33559 10/23/2019 0103
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 10/26/2019 1538 KSH2
10/24/2019 1314 33115
2 3050B
601 OD
1 10/27/2019 0256 LLL
10/24/2019 1314 33115
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
180
100
mg/kg
1
Arsenic
7440-38-2 6010D
ND
3.9
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.3
mg/kg
1
Calcium
7440-70-2 6010D
ND
1300
mg/kg
1
Copper
7440-50-8 6010D
21
2.6
mg/kg
1
Lead
7439-92-1 6010D
ND
2.6
mg/kg
1
Magnesium
7439-95-4 6010D
ND
1300
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
10
mg/kg
1
Nickel
7440-02-0 6010D
ND
10
mg/kg
1
Potassium
7440-09-7 6010D
ND
1300
mg/kg
2
Selenium
7782-49-2 6010D
ND
5.2
mg/kg
1
Sodium
7440-23-5 6010D
ND
1300
mg/kg
1
Zinc
7440-66-6 6010D
43
13
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
SheiAly EnvlrOnmfnti3I Salvl499, Inc..
Cf rein & C" 101 LAWNULL Paint Ulhn
ram! Rrsord VWL1zl C)AjgYika &XM CWMk a 49,%z Ntimber
Trleftona My M-WW Far 40. n3j?Vj-gj11
EL— T*­p!..'mj *xr5Np7 L com '
T+h to
E"CDy16 :Llw.e Na r wrrblQfth M.
r•yrFda414b, �pK &§4 �+�hra .rr• 417, -Ml lduid.i��L�
O.IWYItl as 73t 4 x
�� "� IIC 7ompa� MSC .'rn n iyyllex
I r nor ` 143Lfr-wowrs Fm
"51 Nr"n1lix• o n hdn Llu r ''el^'° gyy I n3ahqt !I
Urps W F4J Fa,o 741 #a U 1 021
�9 w,. o.
'rF� '17
W.'a Q 7C 7 A.
._�F9'11rno
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RYWntb q4p.=tr 4+d h—.— -W—ph IPn4-W IMf -OM Lk-- I
* 1. i
n.tr "rr RrwadG I Rsh . yy
Hu6aAllsa IpBEr-nvSi'rlBJioriollr'r�MWslrPmrfgPt LA Lbmg0LV ry
f
dSCrl7!$rlperrlF"�k Y19 rn�dC. Potre.w,d x. be iCr F Y +1 Ih.'nIP�1`op •Gt .
coe^R� M�DW PI
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Forth Carolina Permit parameters
2, Re-qiduaLs shall be M;OyZed to dokrten8tr4e thty are
Act or3rce Conservation
and Rocov'ry (R Aj- The Ana rrnsivit}', l njia i 3', rc and taxidty
charsctt t'illle leaLiva}etlu s clue„may aPcci#fuxl in
ALl 1 t1 A, =d Ibc l it#eo sbali maiutuin these resnits far a M u mntn of five -ycar8 Any
exoePd=9fsom the leguinU01I its ill thineonditinia 3h4 be apacificd inAaacTLmtw x
Tile TCLI anal,,ysia shall include the following parameters (the regulatory leval in miiiigr M liner
is in parao=W):
Cr
�u
CL
Ananic (5.0)
$arum (100,G)
�vr2une {U.5) .
Cadmiurn (1,0)
CaPu td ohioike (0,5)
fkkwdaua (0,03)
cc rMbm m-m o cio,o)
11.0mf n (6,0)
�12romsam (5,0)
t-Cresol (200,0)
�C;r 1(200,D)
ynacl (200,0)
1,4-Dichl b ute (7.5
1, Dichlorool
I,l D?idUmlbtlyylene (0.7)
2,4-Dinitrowlueao'(0.13)
-- Emmn (0.02)
is =wh1orobeFAM= (0,13)
i ep hlor (and itis - ydroxi&)
l-icxachioro-1,3-butadicnc (0,5)
HexachiQt�p� (�.�)
_ Lem (5-0).
JL.indana (D.�.�
lwie�t"y (a,2)
I�ethoxyclllnr { 10.0)
N trobegtiaene (2.0).
Pt�tachlomplkeuol {10�.0}
Ieniqm 6 A)
Silver (5.,D)
Te loructhyleae (0.7)
Toxvhene (Q,5)
Tdchloroethylaw (0.5)
2,4-,5-Tric1Aoropheuop (q ,{
2,4, Trichlruvp nol
2,4,5-TP (suyex) (l .0)
Vinyl ddoridc (0.2)
3. An aLais AA1 be conducted oti r0siduals f Dr. eaoh aotuoe e t the 1itgl ramy
sVecif& ttachrmat A, and the Permittegea xting facility
e shall maintain the re�J#s for a mirxiitf iye
The atsis ! ball include the following Parameters
A)!41II1tnA[tl
mlmonia-Mitrom
Arsenic
Cadmium
calcirim
C; r
Lead
PBainm
�r'ry
ybdenuut.
Seleniwix
Nickel
y Sodix�►
jNitrzft-N1UUo-,Nitmgemn
t Total Solids
TKN
pn
>}h°a orue
V6atile Solids i
Inc g's
TERRA RENEWAL ERVI E
47G-747-8 ; 92
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 12

SHEALY ENVIRONMENTAL SERVICES, INC.
Rhs_1r F.nvgr4unrwn1nl Scn+icw. Jnc. 'a 1 nF I
LMchnl[aLNumt+cr:;dE061&['-j¢ I'17•�i�.}:Imr;. ;L'bj19
Sample Receipt Checklist (S
Client: TERRA RFNTWAL CooJerinmciedIwIdate_LxH i 10A7-2019 i.n1 1JIM 21
J coins of rr+coip#:0
SESJ ❑ Client 0 UPS ❑ redr-N L1 Othtr, -
❑ Yes
IlLI .Nv
I . Were eLntody seals preseril on &c ooalcir?
'{ram[]No
n?
pJJ Strip ID, NA
ChU-ine Strili ID; NA TOsresd by. NA
Oriuiinal tcrnperature upon receipt IUtdved (Corrected)tempiunA.uro upon receipt °Solid Snap�cup ID: 19�161b
1.5 13.5 oC
NA fNA QC. NA ,'NA QC NA fNA oC I
Method- ElTamperatu a Blank ®Against bottles FR Qun ID: 5 IR Cut Coriceti-on Factor. 0 ;°C
MetlIPLA ufCOQIkrnt; 0 Wet toe ❑ I=Pmks ❑ Dry ice ❑ No -Lie
0Ym
El No
V1N;A
3_ If temperature of ally' corolw exct%v&-3 6.0'U, was Prgj ect 1t lamtger Not! fled? �
PM was Notified by_ phanc i =mjI / face-to-fw8 (oircic one).
❑ Y0l
❑ No
®hilt
'I. Is the carrime Cial 0ourier's packitg nlip attached to this fi)rrn?
Yes
❑ No
5. V4`M proper ctlstodv prooWwm (mli uished,'rectilvcd) followeV
® Yos
INTO
t}_ Were sumplc 10s Jiscad on the COC?
Ye5l
❑ No
7. Were sum plc Ms I [md on a1J sim ple containers"
Yes
❑ No
89 Wws col.1cetion date {& time: listed au die CDC?
❑ Yes
W1 NO
9_ Was eollm ion date & tim listed on all sample containers?
1Z Yes
E] No
10. Did a]I coutainwr label infarmalloo (ID, date, lino) a� G with t COCOUV :
® yos
❑ No
1 I, WI:rc trots to be perforined listed on the COO
IZI Yei Cl No
IZ_ Dtd ai] samples arrive in the proper containers i* cazll test al4'Or in good condition
(unlb-uken, lids on, etc_)?
Yes ❑ No
M Was adequate saTnpJc volnuie avai6L1e?
Yes E] No
M Were rrll samples received wJthin °�'- the hnldidg truer OF 48 hourz', whichever combs first?
El Yes 0 No,
15. Wurc any sae leg Dams [ners missitlglexcrss (circle one) samples Nat listerl on COC7
❑ Yes L].No
O'IA 16. For VIVA and RS -175 samples, were bubbles present?"pea-sine" (IN"or bmm jn>;dianwetu)
in nny of the VOA wills?
❑ Yes NO
NA 17. Wem all DR pane Ms/nutrienc salmplLn rcce ived at a pH of = 2?
❑ Yes ITNO
21 NA I B. Wem all c aniac sampJ cs r ecelvM at a pH > 12 and sulfide sum les ri ived at a ' Fi ., 4 '�
❑ Yff ❑ No
0 NA t 9. Were all applicable N �.1TKN;eyanida�hetlroL'fi25 (< mm L) samplrZ5 free oL residual
chlorbir"?
I
+
El`❑c
NA
24_ Were client remarks.'Mquests (Le. mqutNi ud diluMtions, SIM D designations, etc.._ k
1 AJ
I
t*rrectly transcribed fro m the COC into the oomment section in i,IMS7
❑ Ycs 6d No
21. Was the uo+r, number liskd on the oontainer label? if yes. Quoit Y NA
Ski rople Pre"r-nation
(MuSL by aomplamd for any samples) inwrrcctly preserved or wiili he spaco,)
Sa.riple() ]Ur1
W$rt racuived irlc4arrectly pmervw and wBre Adj1ivt�j accordJngly
it) s-mple, rwvivirtg with NA iuL of circle 01w; H2S(]L4, 1 tNCl;, HCl,1`1a0H using SR # NA _
lore of preservation NA . If more than one pseservali ve is ncoded, pleasc note in the urrnmows below. '
Sarnple(s) NA
were received with btlbb.les>6mm in di jiiW-1cr,
Sarnplts(s) i A
wcre received with TXC = 0.5 mg'L. (If 919 is no) and wrrr�c
adjusted �iccordingly' insamt+9e receiving u.iQl �+xlium thinst,lfate(Na�FO;}4irh Shealy Ili: 1�A
SR bar,code labels applied fry' M i 17atc; A-17-2019
I
Comments-
I
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 12

Analytical Results �,* STATESVILLE
ANALYTICAL
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 09/08/2020
Reported: 09/10/2020
For: TYSON WILKESBORO
Comments: GM 125033 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200908-35-01
Fecal Coliforms
W1
95420
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-01
Percent Solids
W1
5.24
%
SM2540B-2011
09/09/2020
WC
200908-35-02
Fecal Coliforms
W2
228426
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-02
Percent Solids
W2
3.94
%
SM2540B-2011
09/09/2020
WC
200908-35-03
Fecal Coliforms
W3
129870
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-03
Percent Solids
W3
3.85
%
SM2540B-2011
09/09/2020
WC
200908-35-04
Fecal Coliforms
W4
129534
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-04
Percent Solids
W4
3.86
%
SM2540B-2011
09/09/2020
WC
200908-35-05
Fecal Coliforms
W5
116009
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-05
Percent Solids
W5
4.31
%
SM2540B-2011
09/09/2020
WC
200908-35-06
Fecal Coliforms
W6
100402
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-06
Percent Solids
W6
4.98
%
SM2540B-2011
09/09/2020
WC
200908-35-07
Fecal Coliforms
W7
111857
MPN/g
SM92210E-2006
09/09/2020
WC
200908-35-07
Percent Solids
W7
4.47
%
SM254OB-2011
09/09/2020
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 200908-35-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200908-35-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-35-03
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-35-04
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-35-05
Temp on Arrival: 3.0
Parameter Schedule:
Percent Solids
Received on Ice
Parameter Schedule:
Fecal Coliforms
Sodium Thiosulfate
Received on Ice
Sample Number 200908-35-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200908-35-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

ATTACHMENT - H:
LANDOWNER AGREEMENT & SETBACK WAIVER FORMS

Prepared By: Terra Renewal Services
Parcel Number: 0605291
Parcel Owner: Barker, Kim Thorpe
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED Nov 06, 2020
AT 12:20:29 pm
BOOK 01317
PAGE 0060
INSTRUMENT # 08004
EXCISE TAX (None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I,_ Kim Tharpe Barker , certify that I am a deeded owner of the property located at:
Address: 250 Brandon Rd Parcel No.: 0605291
City: Ronda State: NC Zip Code: 28670 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my propertyline.
For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature: 'a-u / Date: �/241%
FORM: NDRMPW-LAS 11-18
Pagel of 2

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Russellville State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, i COUNTY
a Not ub 'c for County, North Carolina,
�r.
do hereby certify that personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the day of
SE ���f111111lI11/f��i
Y�-
�F -
�� NQi,3ry Ptj C -'S Signature of Notary islc
'Alilkeq
MCam ��m !y My commission expires ,\ jbj
s. 2 7 7 r, Kp. _
4 p. r
y,CA R
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18 Page 2 of 2

Prepared By: Terra Renewal Services
Parcel Number: 0601666
Parcel Owner: Johnson, S L ETAL
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED
Nov 06, 2020
AT
12:20:28 pm
BOOK
01317
PAGE
0059
INSTRUMENT
# 08003
EXCISE TAX (None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
ALA..) •5-6u4s isa..j
certify that I represent Johnson, SL ETAL ,
which is the deeded owner of the property located at: Address: Elkin Hwy 268
City: Ronda State: NC Zip Code: 28670
County: Wilkes
Parcel No.: 0601666
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
❑ For the parcel identified above, I consent to a reduced setback from, _ feet to _ feet, thereby
allowing the application of Class B residuals as near as _ feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature: P I A'ri
FORM: NDRMPW-LAS 11-18
a5ad
Page 1 of 2
NN`GG�
o�,o

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Dardanelle State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, \,j j' b `LZ-.a COUNTY
I` ( a Nntayfr�oCounty, North Carolina,
do hereby certify that fir- personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the-/` day of J %x -y -2b l a,
\���t��
SEAL \\\\������9 D Y R
Nct
W,�ke Obl;c Signature of Notary Public
M CO�nt s
2 y C°mr 1 y My commission expires
O 1 1'30 Ek,D,
iiCA R O-�����``��
Once notarized, thisi /F0V' 'shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18
Page 2 of 2

Prepared By: Terra Renewal Services
Parcel Number: 0100606
Parcel Owner: Mathis John Myrth & Lisa S
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED Nov 06, 2020
AT 12:20:24 pm
BOOK 01317
PAGE 0055
INSTRUMENT # 07999
EXCISE TAX (None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, John M. Mathis certify that I am a deeded owner of the property located at:
Address: 619 Mathis Farm Rd Parcel No.: 0100606
City: Roaring River State: NC Zip Code: 28669 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature:
6 /z-1/ tg
FORM: NDRMPW-LAS 11-18 Page 1 of

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Russellville State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA i
4g2& COUNTY
Ia Not arx P is fy County North Carolina
do hereby certify hat L:V.—.XVV'lA� Y personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the-) day of
���etttii►rrrrri�y�
SE E D Y
ttiNko ���� Signature of Not y Public
t 7^3xp My commission expires J t
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18 Page 2 of
x0e,.s
O koo

Prepared By: Terra Renewal Services
Parcel Number: 0100821
Parcel Owner: Anderson, Charles D & Nina J
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED Nov 06, 2020
AT 12:20:26 pm
BOOK 01317
PAGE 0057
INSTRUMENT # 08001
EXCISE TAX (None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
Nina J or Charles 0 Anderson , certify that I am a deeded owner of the property located at:
Address: 860 Mathis Farm Rd Parcel No.: 0100821
City: Roaring River State: NC Zip Code: 28669 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
0 For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature:
FORM: NDRMPW-LAS 11-18
Page 1 of 2
F^ N 0 E ~Job v�
D to
�

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: W00038087
City: Russellville State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, �3,`G�Q S COUNTY
I, , a Notary Public for \ County, North Carolina,
do hereby certify that mpg KK j. c personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the3A- day of �.ci. -2 � 1
SEAL ' !Votary Publ CEO
Wilkes
County
My Comm. Ex —
Z p 1
/ 0 1-3p-2021
CAR
Signature of tary P blie
My commission expires
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18
Page 2 of 2

Prepared By: Terra Renewal Services
Parcel Number: 0100131
Parcel Owner: Anderson, Nina Jarvis
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED
AT
BOOK
PAGE
Nov 06, 2020
12:20:27 pm
01317
INSTRUMENT #
EXCISE TAX
State of North Carolina
Department of Environmental Quality
Division of Water Resources
0058
08002
(None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS 13 RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, Nina J Anderson , certify that I am a deeded owner of the property located at:
Address: Mathis Farm Rd Parcel No.: 0100131
City: Roaring River State: NC Zip Code: 28669 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature:
FORM: NDRMPW-LAS 11-18
�
k\rj06~{9
Page 1 of 2

Permittee: Terra Renewal
Address: 3308 Bernice Ave PermitNo.: W00038087
City: Russellville State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, V Q. COUNTY
a Nota Public for County, North Carolina,
do hereby certify that personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the21day of
SEALO'D y It �uR��,///
Notary Public
W ikes —_
County _
MY Cornrn, Exp —
'Z 11-,0-2021
.�
CA B
Signature of Nota y Public
My commission expires
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18
Page 2 of 2
boa
P"°
o`
0ho

Prepared By: Terra Renewal Services
Parcel Number: 0100990
Parcel Owner: Mathis, Jeffrey B & Daylee E
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
FILED
WILKES COUNTY
MIS S
REGTER OF DEEDS
FILED Nov 06, 2020
AT 12:20:25 pm
01317
BOOK 0056
PAGE p8000
INSTRUMENT #
EXCISE TAX (None)
State of North Carolina
Department of Environmental Quality
Division of Water Resources
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, Jeffrey B. Mathis , certify that I am a deeded owner of the property located at:
Address: Mathis Farm Rd Parcel No.: 0100990
City: Roaring River State: NC
Zip Code: 28669 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature:
FORM: NDRMPW-LAS 11-18
)ate:
Page l of 2
�EFF
Q `oQ�go

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Russellville State: AR Zip Code: 72802 County: N/A
t
NORTH CAROLINA, COUNTY
I, �a NootBaublic for S County, North Carolina,
do hereby cert fy tha _personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the day of Jk -s-Jl
4.
SE��4
N`o.tar, ti c
—
�;, Signature of Nota Public
MY Corn. Exp, _—
�G 7 7-30-2027
My commission expires
CIA B O;
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18 Page 2 of
�EFF - a `o

Prepared By: Terra Renewal Services
Parcel Number: 1700289
Parcel Owner: Ireland Joel L & Ireland Samuel G
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
WILKES COUNTY
MISTY M. SMITHEY
REGISTER OF DEEDS
FILED Nov 06, 2020
AT 12:20:23 pm
BOOK 01317
PAGE 0054
INSTRUMENT # 07998
EXCISE TAX (None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, Joel L. or Samuel G. or Elon M. Ireland, certify that I am a deeded owner of the property located at:
Address:_ 1556 Mahaffey Rd Parcel No.: 1700289
City: Union Grove State: NC Zip Code: 28689 County: Wilkes
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my propertyline.
For the parcel identified above, I consent to a reduced setback from feet to feet,
thereby allowing the application of Class B residuals as near as feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
Signature:
FORM: NDRMPW-LAS 11-18
C> 6 — 2 1 - Zc7 ('i
Page I of 2

Permittee: Terra Renewal Services Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Dardanelle State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, It ItW, COUNTY
County, North Carolina,
appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the_!I_day of : N a_ l�
,SAL
Notary Public
Wilkes r Signature ofAta'ryublic
County
My Comm. Exp,
y 11-30-2021 My commission expires
°��i, H/CAEO
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18
Page 2 of 2
�2e�"'4
�r7"" Z$q

Prepared By: Terra Renewal Services
Parcel Number: 112742 - PIN: 484400359744
Parcel Owner: Ireland George F Trust &
Ireland Elon M Revocable Trust
Please return to:
Terra Renewal Services
P.O. Box 1746
Watkinsville, GA 30677
State of North Carolina
Department of Environmental Quality
Division of Water Resources
FILED
YADKIN COUNTY NC
ARIC WILHELM
REGISTER OF DEEDS
FILED
Nov 09, 2020
AT
10:55:46 am
BOOK
01304
START PAGE
0034
END PAGE
0035
INSTRUMENT # 04474
EXCISE TAX
(None)
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, Elon M. Ireland (Trustee) , certify that I represent Ireland George F Trust
which is the deeded owner of the property located at: Address: Old Ben Bow Rd
City: Union Grove State: NC Zip Code: 28689 County: `/A b K IN
Parcel No.: 484400359744
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my propertyline.
❑ For the parcel identified above, I consent to a reduced setback from, _ feet to _ feet, thereby
allowing the application of Class B residuals as near as _ feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
FORM: NDRMPW-LAS 11-18
,DC- 2( - Zo (,i
Pagel of 2
,- ,9 Hgoo�SS-rMy

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: WQ0038087
City: Dardanelle State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA. 1 COUNTY
a-Notary Puhl for County, North Carolina,
do hereby certi y that ,�� personally appeared before me this day
and acknowledged the due execution of the foregoing instrument.
Witness my hand and official seal, this the_2lLday of -A-CAL.-, ? n
.° �WA L�o
Notary Public
Wilkes - Signature of lary ublic
M
County =
My Comm, Exp, Il
20 t t-30-202 t �:` My commission expires
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18 Page 2 of
saw 4 '1

FILED
YADKIN COUNTY NC
Prepared By: Terra Renewal Services
ARIL WILHELM
Parcel Number: 112745 - PIN: 484400562719
REGISTER OF DEEDS
Parcel Owner: Ireland Joel L ETAL CoTrustees of
George F Ireland TRS
FILED Nov 09, 2020
AT 10:55:57 am
Please return to:
BOOK 01304
Terra Renewal Services
START PAGE 0036
P.O. Box 1746
END PAGE 0037
Watkinsville, GA 30677
INSTRUMENT # 04475
EXCISE TAX (None)
State of North Carolina
Department of Environmental Quality
Division of Water Resources
NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER
FOR THE APPLICATION OF CLASS B RESIDUALS
AGREEMENT TO WAIVE SETBACKS PURSUANT TO
15A NCAC 02T .1108(c)
I, Elon M. Ireland (Trustee) , certify that I represent Ireland George F Trust ,
which is the deeded owner of the property located at: Address: Old Ben Bow Rd
City: Union Grove State: NC Zip Code: 28689 County:
Parcel No.: 484400562719
Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby
agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following
page.
X For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby
allowing the application of Class B residuals as near as 0 feet from my property line.
❑ For the parcel identified above, I consent to a reduced setback from, _ feet to _ feet, thereby
allowing the application of Class B residuals as near as _ feet from my residence.
"THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED"
FORM: NDRMPW-LAS 11-18
OG _ 21- 2ot i'
Page 1 of 2
U1 W4

Permittee: Terra Renewal Services, Inc.
Address: 3308 Bernice Ave Permit No.: W00038087
City: Dardanelle State: AR Zip Code: 72802 County: N/A
NORTH CAROLINA, V COUNTY
1.
bloc for County, North Carolina,
r
and acknowledged the due execution of the foregoing instrument.
a�
Witness my hand and official seal, this the -)A day of
I1R11
SEAL,z--
Notary Public
VVilkes
County
MY Comm, Exp.
11-30-2021 =T
'12 tl CA,?,(,
appeared before me this day
Signature o Notar Public
My commission expires t t D
Once notarized, this form shall be recorded at the Register of Deeds in the county or
counties in which the described properties are located. A copy of the recorded waiver
shall be sent to the following address:
Division of Water Resources
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
FORM: NDRMPW-LAS 11-18
Page 2 of 2

ATTACHMENT - M:
STORAGE FACILITY DESIGN DOCUMENTS
- Site Plan
- Secondary Containment Specifications
- Geo-Tech Report
- Engineer Report

Arete Engineers, PLLC
Firm License No. P-1357
7668 Valley Blvd.
P.O. Box 745
Blowing Rock, NC 28605
Project #2654
Client:
Denali Water Solutions
Attn: David Coyle
P.O. Box 1746
Watkinsville, GA 30677
[phone]
[e-mail]
Project Location:
360 12' 35" N
800 58' 09" W
Wilkes County, NC
Arete"
1111111111110� E N G I IN E E k 5
November 16, 2020
RE. Limited Structural Assessment of Proposed Residuals Storage Tank Buoyancy
Dear Mr. Coyle,
At your request, we produced a limited structural assessment report and foundation
design for the proposed the Residuals Storage Tank Facility to be located at the above
location. The report and foundation design were dated July 29, 2020.
On October 22, 2020, it was requested by the NCDEQ in a letter (Item D.1, Engineering
Calculations) that we provide all necessary buoyancy calculations pertaining to the sludge
storage tanks, pursuant to 15A NCAC 02T .1104(a)(2).
It is our opinion that buoyancy calculations are not applicable for this storage structure
due to the above -ground design. Buoyancy is typically only a concern for below ground
pools and storage facilities. Per the nature of this design, the above grade tank walls will
be anchored to a concrete footing, which should negate all buoyancy concerns.
Sincerely,
CO"",,,
Q' 10f SS1�j'-
,1
Brian P. Mullin PE
'
Brian Digitally signed by Brian P_
Mullin
, t.
a � ' SL f ',
Structural Engineer
DN:OU="Structural
Engineering ", 0="Arete
_ '
x SEAL i
Arete Engineers, PLLC
Engineers, PLLC", CN=Brian
P P_Mullin,
i9� `
i
E=[e-mail]
Reason: I am the author of this
�.�"
Mullin document
i6:23:
t,-
�/qAf
2C
Date: 2020I11-16
�f

TABLE OF CONTENTS
SECTION 1.01 INTRODUCTION
1)
ABOUT
2)
BACKGROUND
3)
SOP PURPOSE
4)
EH&S PROGRAMS
5)
SUMMARY
SECTION 1.02 AST PLANNING AND PREPARATIONS
1) PLANNING
2) REQUIRED AST ORDER INFORMATION
3) SITE MEETING OR SCHEDULING CALL
4) SITE SOIL PREPARATION
5) PRE -MOBILIZATION ON -SITE MEETING
6) CALL BEFORE YOU DIG "811"
7) AST MATERIAL DELIVERIES
SECTION 1.03 WWS AST PRE RIG UP REQUIREMENTS
1) LOADING REQUIREMENTS
2) JOB SAFETY ANALYSIS (JSA)
3) CHECK SOIL CONDITIONS
4) PROPER TANK POSITIONING
5) EQUIPMENT (WWS PROVIDED)
6) HAND TOOLS RECOMMENDED
SECTION 1.04 WWS AST RIG UP PROCEDURE
1) TANK LAYOUT
2) INITIAL TANK ERECTION PROCESS
3) SECONDARY CONTAINMENT LINERS AND INSTALLATION
4) TANK WALL ERECTION
5) PROPER LINER PLACEMENT AND CLAMPING
6) INSTALLING TANK ACCESSORIES
7) AST COMPLETION STEPS
SECTION 1.05 AST IN USE OPERATIONS
1) INSPECTIONS AND MONITORING
2) INITIAL LEAK DETECTION AND LINER REPAIR
SECTION 1.06 WWS AST RIG DOWN PROCEDURE
SECTION 1.07 WWS AST ENGINEERING STAMPS
SECTION 1.08 WWS AST ENGINEERING SPECS
SECTION 1.09 PROPER AST SETBACK AND LOCATION SAMPLE
SECTION 1.10 JLG APPROVED TELEHANDLER ATTACHMENT AND LOAD CHART
SECTION 1.11 WWS MAN BASKET UPDATED ENGINEERING DRAWINGS
SECTION 1.12 WWS MAN BASKET STAMP AND SOP
SECTION 1.13 GEOMAMBRANE FABRICATION MANUAL AND TESTING CHART
SECTION 1.14 GEOMEMBRANE INSALLATION
SECTION 1.15 WWS PREFERRED LINER SPEC OR COMPARABLE SUBSTITUTE
SECTION 1.16 GEO GRID MESH SPEC
SECTION 1.17 PATENTS AND PATENT PROTECTIONS

Section 1.01 Introduction
1) About
Well Water Solutions and Rentals Inc. aka (WWS), is the original pioneer of the portable Above
GroundStorage Tank industry. The above ground storage tanks or AST's have become an
integral part in saving cost in the oil and gas and industrial industries. WWS has been supplying
and servicing these portable tanks for longer than any other company in the USA. We have
focused our time and experience on providing the best tank products at the highest safety
standards. We continue to learn and adapt every -day in our industry to make sure our
employees are safe and our customers are happy.
Standard Operating Procedures or (SOPS) are a staple for safety and quality here at WWS. Our
SOP for our above ground storage tank (AST) systems including planning, rig up, operations, and
rig down. This SOP will discuss steps to be taken to promote the safest process, as well as list
the potential hazards that should be identified and reviewed during our JSA prior to beginning
the work process.
2) Background
WWS has over 170 AST's that are used for a variety of oil field and industrial applications within
the fluid management operations. AST's can be used in place of traditional 500 BBL trailer tank
farms and in -ground water impoundments, and are suitable for fresh water as well as production
water. WWS tanks have standard sizes, ranging from 6,000 barrel (bbl) capacity to 60,000 bbl
capacities. Through intensive design criteria WWS secured a patented design on the strongest
possible design for as AST tank. We analyzed many methods to secure the panels together and
all other methods failed our criteria. We have also set a standard in the industry for safe
movement of the panels with our patented adaptor plate for a quick attach telehandler. We
were able to successful submit engineering documentation to the Oshkosh Corporation, which
owns JLG and they have stamped and approved our adaptor plate.
3) SOP Purpose
WWS will extensively review this SOP with all new hire employees to assure proper
understanding of all procedures. This SOP will also be reviewed with an employee if his/her
responsibilities change under the plan. An electronic copy of this plan will be available at all
WWS regional offices.
Training our employees to follow our SOP is the first step to a safe and successful work
environment. We also need all our employees to treat everyone with respect and follow the
lead of their supervisor to make sure every day is safe.
STOP WORK authority and who has the power to use it is another tool we use to help
everyone stay involved in the safety process. We highly encourage all employees to feel
comfortable in rising awareness of any unsafe situation happening or providing suggestions to
help make any task safer as well. This helps everyone grow to be a stronger team.
This SOP may also be used to inform customers about WWS's typical equipment and
procedures for setting up an AST system. This SOP will be reviewed and revised on an ongoing
basis to keep pace with best oilfield and industrial practices and applicable OSHA regulations.

4) EH&S Programs
This SOP recognizes that oil and gas operating companies have developed their own health,
safety, and environmental (HSE) programs that contractors who work at customer's sites like
WWS, must comply with. In addition to this SOP, WWS personnel will strictly observe the policies
and procedures of each operating company they are to do work with.
5) Summary
This SOP recognizes that oil and gas operating companies have developed their own health,
safety, and environmental (HSE) programs that contractors who work at customer's sites like
WWS, must comply with. In addition to this SOP, WWS personnel will strictly observe the policies
and procedures of each operating company they are to do work with
Section 1.02 AST Planning and Preparations
1) Planning
Proper planning and documentation will help assure a successful AST rig up and rig down. The
following steps can be utilized to fully, safely, and accurately perform the tank rig up or rig down:
➢ AST Order Information
➢ Customer Meeting
➢ Soil Conditions and Pad Preparation (Completed by Customer)
➢ Pre -Mobilization and On -site Meeting
➢ Notifications
➢ Job Safety Analysis (JSA)
➢ AST material requirements for delivery
2) Required AST Order Information
WWS Manager or Field Supervisor will record general AST order information including the
following:
➢ Site location directions and coordinates
➢ Customer Contact Name, Phone, and Email
➢ Emergency Medical Contacts
➢ Special Safety Requirements
➢ Tank Utilization Dates
➢ Tank size and Accessories
➢ Special piping requests
3) Site Meeting or Scheduling Call
Prior to finalizing the delivery schedule, a meeting or conference call is held with WWS
and our customers required personnel to make sure all parties are coordinating well and
have the same and accurate information.
This meeting is best done in person, but must at least be covered in a phone call, followed up by a brief
email confirming the AST order details, delivery schedule, and noting special conditions, safety
requirements, verification of pad preparation, etc.

KEY MEETING TOPICS:
➢ Introduce all WWS key personnel to our customer's key personnel
➢ Review what tanks are needed and what use they will be needing them for
➢ Review AST scope of work, what is normally included, what is not
➢ Confirm AST size(s) to be used
➢ Assure a 20' working space around each tank for safe working area
➢ Permitting for AST (as needed)
➢ Current site conditions and soil preparation requirements
➢ Site access and truck route requirements, and any weather -related issues that could affect them
➢ Time line for rig up and rig down of the AST
➢ Detailed drawings of the location layout for tank and piping placement
➢ Details on "Fresh Water" source to fill the tank on the day of the set up
➢ Assure a minimum of 24" of water the day of the setup to quickly and safely complete the job
➢ Identify what other charges could be incurred by the customer and result in standby time or
additional charges
➢ Confirm customer is responsible for the used liner, residual
solids left in the tank, removal of all radioactive NORM
materials, and site reclamation
➢ Review any and all additional safety requirements the customer may have
➢ WWS to follow up with an email to review all changes made
4) Site Soil Preparation
Preparation of the soils on site is required to form a dependable base for the AST.
Preparation of the tank pad is solely the responsibility of the customer/operating company.
WWS Soil Requirements are:
➢ Minimum soil compaction of 95%compaction
➢ Soil testing results shall be shared with WWS if requested
➢ Site must be cleared and free of debris such as sticks, sharp rocks, and trash etc.
➢ WWS recommends soil compaction testing to be conducted via Standard Proctor Test
(American Society for Testing and Materials {ASTM) Standard D698) or Modified
Proctor Test (ASTM Standard D1557)
➢ Compaction test results must be provided to WWS prior to the commencement of
AST construction upon request
➢ Proof roll testing maybe be used if there is doubt of site compaction standards
➢ Grade of the inner AST area to be a maximum of .25% or 3" drop per 100' towards sump
location
➢ Site shall be graveled and rolled prior to tank installation, utilizing gravel size 2B or
smaller. (3/4" road grade preferred, or coarse sand with minimum thickness of 4
inches)
➢ *Do Not Use* crushed rock as sharp edges could puncture the tank liner
Completions of all these steps will assure a smooth, safe, and seamless tank set up.
5) Pre -Mobilization Onsite Meeting
WWS's AST team will conduct a pre -mobilization onsite meeting with the customer that
documents the customer requirements for the specific pad location and AST system.

6) CALL BEFORE YOU DIG "811"
Even though the customer or their subcontractor may have already called for utility locates for
the sump hole, the WWS field supervisor should call the local or state underground utility location
service again at least 3 days in advance before construction/digging begins. The ticket or
reference number provided by the one -call service will then be documented.
The following web site has contacts for all the states and provinces.
http://www.ca1181I.com/state-specific.aspx.
Call 811 in United States
7) AST Material Deliveries
Once the delivery route and schedule are established and the pre -project onsite inspection is
completed, the AST materials can be delivered. Updates and notifications will be made as agreed
to during the customer meeting. WWS delivery personnel will use a spotter for the equipment
driver and should unload all materials safely taking extra care to avoid damage to liners, plates,
and all other AST components. Should any problem arise during the scope of operations the
WWS field supervisor will notify to correct customer contact to remedy the issue.
Section 1.03 WWS AST Pre Rig Up Requirements
1) Loading Requirements
WWS will have the field supervisor complete a "Dispatch Load In Load Out Sheet" before and after the
set-up and rig down of the AST system. This sheet will identify all the needed parts and accessories to
complete the AST Rig Up. During Rig Down the "Dispatch load in load out sheet" is also filled out to
ensure all parts and accessories are accounted for and in good working condition. In the event parts or
accessories are missing and/or damaged the customer will assume full responsibility and be billed back for
the parts and accessories.
2) Job Safety Analysis (JSA)
A job safety analysis (JSA) must be completed on -site prior to the beginning of any work. The JSA
will be completed according to WWS protocol and safety programs. Customer's safety
requirements will also be communicated during the JSA. All personnel, third party contractors,
and customer representatives are expected to participate and sign the JSA when the JSA is
completed.
3) Check Soil Conditions
Preparation of the tank pad is solely the responsibility of the customer.
However, bad weather such as wind, rain, and snow events can change the soil conditions
quickly. If soil conditions change the WWS field supervisor will notify the proper customer
contact.
4) Proper Tank Positioning
➢ Check proposed AST site to confirm that a 20' clear work area around the perimeter of
the tank is possible to provide access for equipment and laydown area for AST
materials and erection equipment

➢ Check that the minimum setback distances to existing wells, power lines, etc. are met
➢ Mark out the tank location using WWS marking equipment
➢ Establish and mark out final location for the fill and suction tube(s) and stairs
5) Equipment (WWS provided)
All equipment is subject to daily inspection. (Check condition, rigging, oil, water, fuel and
cleanliness.) Here is a list of the recommended equipment needed to set a tank. Actual
equipment used will vary among region and specific projects.
➢ One 40' and/or 60'extending straight or z boom man -lift
➢ 10,000 lb. or greater capacity, rough terrain forklift (JGL 10-43A is preferred telehandler)
➢ Backhoe or small excavator with bucket
➢ Skid steer
6) Hand Tools Recommended
All hand tools are subject to daily inspection.
➢ Two 16' ladders
➢ Four 4 lb. sledgehammers
➢ 100' or 200' tape measure
➢ 1 case of marking paint — minimum
➢ Set of wrenches %" — 1 %"
➢ Set of sockets %" —1 %2"
➢ One small pry bar
➢ 8' rock bar (digging bar)
➢ Five safety harnesses with retractable tethers
➢ Five retractable lanyards
➢ Duct tape
➢ Covered hook bladed knife
➢ Three 40' lifting straps (minimum of 5,000 lb capacity)
➢ Three 20' 3/8" chains (must have visible certification tags)
➢ Two rolling head pry bars
➢ Two %2" impact guns
➢ Two sets of rigging chains
➢ Patch tape
➢ Rubbing alcohol
➢ Patch roller
➢ Leather gloves
➢ Wire brush or wheel with 4" angle grinder
➢ Generator
➢ Steel toed rubber boots
➢ All personnel must have Fire retardant clothing (FRs) Safety Hard Hats, Safety Glasses, crush
resistant gloves and any safety requirements from customer
Section 1.04 AST Tank Rig Up Procedure

WWS Field Supervisor will double check all paper work and location prior to setup to assure everything is
correct and ready to set the AST.
1) Tank Layout
➢ Determine center of tank and mark with paint. Place a non-abrasive item on the
center point; preferably a sandbag. This will be used to find the center of tank
after liners have been placed
➢ Measure and double check minimum distance from tank center to existing wells or other set
backs
➢ Measure and paint a line to mark the circumference of tank for panel placement using WWS
special design marking tool
➢ Also mark 15' outside the tank circumference as this will show where the liner should reach once
fully stretched flat. This will assure enough liner is present to go over tank walls once placed
2) Initial Tank Erection Process
➢ Determine where suction pipe is to be located in the tank
➢ Dig at least 4' wide x 6' long x 16" deep sump hole for over the wall suction pipe to set
into and taper the edges so there are no sharp corners of the excavation. Or dig 3'
wide x 12' long x 10" deep sump hole for undermount suction pipe
➢ Remove any sharp stones and debris for the digging process
➢ If multiple suction manifolds are required, the sumps should have a minimum of 15' of
separation
Attention:
Barricade any sump pit with appropriate cones, tape, equipment, and/or have a hole watch if left open.
➢ All tank set-ups will utilize a standard 10oz geotextile that will be laid on the grounds
surface to act as a padded protector for the liner
➢ A Standard LLDPE 30 mil or 40 mil liner will then be used as the primary containment,
but may also be used as a secondary containment within the tank upon request.
➢ Check customer specifications and regulatory permitting to assure proper liner and
containment requirements are meet for ASTs
➢ Organized crew inspection walks for the entire tank base area will be performed to
pick up any sharp stones or other sharp debris that could damage the liner
➢ The geotextile pad can now be deployed out fully at this point. It should reach beyond the tank
circumference paint lines by 1'-4'
➢ Once geotextile is completed the liner can be fully deployed. Crews will double check that the
liner will reach to the 15' marks beyond the tank circumference
➢ Crews will then perform a visual inspection of the liner and repair any defects as necessary
➢ Fold the liner towards the middle of the tank until tank circumference paint line is fully
exposed
3) Secondary Containment Liners and Installation
➢ If tank system requires a secondary liner and leak detection system this will be installed on top of the
first liner
➢ WWS Field Supervisor will direct the installation of the various parts and layers of the secondary
containment system

➢ For example, a 220-mil geo grid mesh (Reference Section 1.16 for Spec) or other suitable approved
spacer material can be installed between the top and bottom liner layers to provide a separation for
to water flow. Installation of inspection pipes into to the designed low points of the tank will later be
used for leak inspections
➢ Install any other customer required components for the leak inspections if needed
➢ Unroll top liner over geo grid to completed the secondary containment system
➢ Follow the same setup guidelines for a one liner system for the two -liner system, and make sure to
complete the components installation fully once the first liner is clamped.
4) Tank Wall Erection
➢ Field Supervisor will complete a visual inspection of each panel as it is prepared to be placed
➢ The first tank panel will be placed and secured using the backhoe bucket
➢ once backhoe fully secures the panel the telehandler can then get the next
panel. Crews will continuously provide operators with spotters during all
operations
➢ If higher winds exist crews are cautioned to pay special close attention to all operations
➢ Crews will repeat the panel placement process until entire tank is erected
➢ Personnel secured on man lift or using a ladder (depending on customer policies) then
secure the panels in place with 14 retainer pins per panel.
ATTENTION:
Proper hand and foot placement is crucial when connecting AST panels. Keep hands and feet a
safe distance from pinch points. Discuss where these pinch points are located when reviewing the
JSA. Keep the joints in mid -range; i.e. palms are located between waist and shoulders. Create an
awareness that never goes away and designate one individual to enforce the awareness when
setting panels.
➢ Roll up excess geo pad into minimum 6" diameter cylinders around the inside of the
tank ring to help support the liner at the base of the tank wall as the tank is being
filled.
➢ Prior to lifting liner into place against inside panel, add geo strips over all panel
connections points and use spray glue to secure in place
➢ Prior to covering sump with the geo pad or liner, confirm sump excavation has smooth
sides and corners, and that no sharp stones are present.
5) Proper Liner Placement and Clamping
➢ After 3 or more panels are set, and all liner protections are complete, crews inside
the tank can begin to hand liner up to crews outside the tank that are in the manlift
➢ Crew of 2 inside the tank wall unfolds and pulls the liner toward each panel (final
connection of last panel will not be made until all liner to that point is pulled and secured
to avoid confined space, all personnel must be out of tank before walls are closed)
➢ The inside crew of 2 works with the manlift crew of 2 located outside to pull the liner up
and over the top of each panel. The man lift crew lifts the liner using ropes/straps gently
lowered and attached (by the inside crew). The man lift crew lifts a small liner section to

the top of the panel and folds it over the top of the panel, being sure there is enough
slack in the liner inside the panel wall
➢ Proper slack or excess liner on the vertical wall can be tested by the inside crew. The
crew will pin the liner to the bottom of the wall with their boot and pull liner at chest
level outwards away from the wall. There should be about 3' from wall to liner when
being pulled. This is the appropriate amount of slack. If crew ever has doubt that the
liner slack may not be enough WWS's experience has proven more slack the better, so
just give it a little more slack if needed
NOTE: The crew must allow sufficient slack in the liner at the wall to allow for liner movement
during filling and draining.
ATTENTION: Never place hands on the railing of the man basket that faces the AST panel. Proper hand
placement would be the side or back rail.
➢ Once a section of liner is positioned properly (with liner slack inside the tank) and over
the top of each panel wall, the man lift crew secures the top of the liner with clamps.
(Tools in basket secured with tool lanyards) NOTE: Each clamp is notched where D-rings
on the top of each panel are located. This notch acts as an added safety retainer once
clamps are fully tightened. Each panel will receive 2 liner clamps
➢ Crews will continue to clamp until they have reached the final panel. Crews will leave this
small area of liner down until all internal piping is completed
6) Installing Tank Accessories
➢ Install safety stair system, fill piping, and suction piping. Ensure that stair system and
piping are appropriately secured to the tank walls with ratchet straps of chains
➢ Assemble all interior piping and assure any connections or sharp points are fully wrapped
in geo material for protection
7) AST Completion Steps
➢ Close final panel and secure with pins
➢ Lift liner and secure at the closure point to finish clamping process
➢ Trim liner and allow approximately 2' of liner to hang over edge of tank.
➢ Begin to fill the tank with water and monitor filling process
➢ Inspect all connections and equipment, confirming at least 2 liner clamps are in place
on top of each panel
➢ Have a minimum of 24 inches of water put in the tank to hold liner in place
➢ Fill tank and monitor
➢ Perform periodic inspections of the tank to ensure everything is in proper working order
➢ Every time a tank is fully emptied and refilled, an inspection must be performed
➢ Water should NEVER go below 12 inches at the LOWEST level in the tank. (Mark liner as a
caution).
NOTE: Filling process may begin as early as % of the tank wall panels are set. Only fresh water can be used if
filling while personnel is in the tank. Reasons for early filling is to assist with windy days as the water weight
help to hold liner in place. It is recommended no personnel be in the take with more than 6" of water.

Section 1.05 AST In Use Operations
1) Inspections and Monitoring
AST Operation Phase includes periodic AST monitoring, leak detection, and identifying potential
hazards that may have developed, change on -site conditions or tank use. If the tank is drained, it
should be secured from wind impacts and the liner inspected and re -positioned (to provide
sufficient slack during filling) prior to refilling. Specifically, it may be necessary to rearrange the
liner folds at the walls prior to refilling if the wind has shifted the liner folds when the tank was
empty.
If changes are noted, they should be communicated to the WWS Manager/Field Supervisor.
CAUTION — If conditions are observed that could indicate an imminent tank failure, clear the
area immediately. Advise others in the vicinity to do so also and contact the
customer to drain the tank.
2) Initial Leak Detection and Liner Repair
In the event of a leak in the tank due to a hole in the liner, the following steps should be followed.
➢ If there is a question that it is in fact a leak from the AST, a dye test or a pH balance
test may need to be performed on both the water in the tank and on the ground using
approved dye or a properly calibrated pH meter. Third party test results are
recommended.
➢ If the leak is found to be coming from the tank, narrow down from which panel the leak is
originating.
➢ Use a strap or rope to mark the point where the water is coming out of the tank.
➢ Determine if the water is coming out high or low on the tank.
➢ Locate the puncture or hole in the liner.
➢ Empty the tank to the point of damage in liner if necessary.
➢ Clean area of liner that needs to be repaired.
➢ Cut out piece of material (patch or tape) to overlay liner.
➢ Either weld the patch to the injured area in the liner or stick the tape (2 types — dry or
underwater) over the leak.
➢ Make sure puncture is completely covered.
➢ Monitor as needed.
Section 1.06 WWS AST Rig Down Procedure
The AST breakdown follows the reverse order of the setup steps presented in the AST Rig Up
Procedure above. The sump will be filled in with the same material taken out during excavation.
The customer is responsible for draining and disposing of all liquids and residual solids that have
accumulated in the tank. Additionally, the customer is responsible for proper off -site management
or recycling of the liner and geo pad materials, and final grading and/or reclamation of AST site.
Customer is responsible for any removal of radioactive NORM materials before WWS crews can
rig down any tank.

Permit No. WQ00#####
PERMITTEE
FACILITY
ENGINEERING CERTIFICATION
❑ Partial ❑ Final
Wastewater Irrigation System
DATE OF PF.R MIA
COUNTY County
I, , as a duly licensed North Carolina Professional
Engineer, having ❑ periodically / ❑ fully observed the construction of the permitted facilities, do hereby
state to the best of my abilities that the facility was constructed in compliance with G.S. 143-215.1,
Administrative Code Title 15A Subchapter 02T, this permit, and the Division -approved plans and
specifications.
Documentation of any variation to this permit, and the Division -approved plans and specifications, is in the
attached as -built drawings.
Description of variations:
Professional Engineer's Name
Firm Name
Firm No.
Address
City
State
Zip Code
Telephone
Email
Seal, Signature, and Date
THE COMPLETED ENGINEERING CERTIFICATION, INCLUDING ALL SUPPORTING
DOCUMENTATION, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
NON -DISCHARGE BRANCH
By U.S. Postal Service By Courier/Special Delivery
1617 MAIL SERVICE CENTER 512 N. SALISBURY ST.
RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604
WQ00##### Version #.# Shell Version 200201 Page 23 of #