WQ0006242_Additional Information Received_20200925

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 140 River Road
City: Sparta State: NC Zip: 28675..
Coordinates: Latitude: 36' 29' 52" Longitude: 8IQ 06' 15"
Datum: NAD83 Level of accuracy: second
Method of measurement: MAP
2. County where residuals land application program is headquartered: Alleghany
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Michael Wayne Boone
Synagro
987521
Back -Up ORC
Robert Roth
Synagro
1001672
Additional Back -Up
ORCs
(if applicable)
If an ORC and at least one Back -Up ORC are not emrently designated for this residuals land application program, provide
the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training
school and certification test: Alex Fox to take next LA class soon as it becomes avaible.
4. Complete the following tables regarding management of the residuals land application program:
a. P/ar:f Available Nifroeen Set»tntarV: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source-genom ing facilities as currently certified and proposed for certification with this application and list the results in
the following table:
Maximum amount of residuals to be certified: 100 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
Ole Injection
Surface
Incorporation
or Injection
First -Year
20.11
20.26
23011
21026
Five -Year Maximum Adjusted
25,64
25.79
2,564
2,579
b. Land Application Site Use Suttpnnrv: Summarize information regarding the land application sites as currently certified
and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
0.0
Hay
71.5
Pasture
11.8
Total:
83.2
Methods
Surface
83.2
Incorporation or Injection
0
Total:
83.2
FORM: RLAP 06-16 Page 2 of 5

LAND APPLICATION SITE CERTIFICATION
Applicant's name: Town of Sparta
Land application sites currently certified: 74 net acres and Total to be certified: 83.2 net acres.
L LAND APPLICATION SITE INFORMATION (See Instruction B):
Predominant Soil
Mapping Unit
Status
Site/Field ID
Landowner(s)
Lessee(s) or Operator(s)
Net Acres
County
Crop(s)
Code'
Series Name b
or Rep. Slope'
R
NC-AG-05-01
Greg Wagoner
29.6
Alleghany
Fescue Hay
Chester
CeC
R
NC-AG-05-02
Greg Wagoner
3.4
Alleghany
Fescue Hay
Chester
CeC
R
NC-AG-05-03
Greg Wagoner
3.4
Alleghany
Fescue Hay
Chester
CeC
D
NC-AG-06-03
Steve L. Roten
8.3
Alleghany
D
NC-AG-06-04
Steve L. Roten
7.3
Alleghany
D
NC-AG-06-05
Steve L. Roten
233
Alleghany
D
NC-AG-07-01
David Gambill
9.9
Alleghany
D
NC-AG-07-02
David Gambill
10.0
Alleghany
I 'All
D
]Y`-AG 0? 4
David Gambill
1411
Alleghany
R
NC-AG-08-01
Dalton Farms LLC
25.7
Alleghany
Hay
Hayesville
Hayesville
R
NC-AG-08-02
Dalton Farms LLC
93
Alleghany
Hay
ye9�3e
Hayesville
N
NC-AG-09-01
Dustin Sheets
4.9
Alleghany
pasture
Tate
Tate
N
NC-AG-09-02
Dustin Sheets
6.9
Alleghany
pasture
Chandler
Chandler
a Status Code for land application sites are: ♦ N (New)
♦ R (Renewed) ♦ M (Modified)
♦ T (Transferred)
♦ D (Deleted)
n Soil Series Name (i.e. Appling, Cecil, etc.)
`Mapping Unit must be consistent with those used in the
County Soil Survey (i.e. for a 2-8%
slope Cecil in Anson
County the mapping unit is CeB2)
II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C):
Site/Field ID
Latitude
Longitude
Location
Datum
Location Method Code
Location Accuracy
Waterbody Subbasin and
Stream Index No.
Current and Pro osed
p
Class
AG-09-1
3.6=%".!° 47' 64"
-81011' 04"
NAD 83
ADD
Nearest Second
10-9-(1)
C
C
AG-09-2
W 47' 89"
-810 11' 20"
NAD 83
ADD
Nearest Second
10-9-(1)
C
C
FORM: LASC 06-16 Page 1

LEGEND
APPLICATION AREA
PRIVATE ROAD O
STREAM
— DRAIN .
�E x * FENCE ❑
PROPERTY LINE 0
UNSUITABLE AREA
WATER
ONSITE HOUSE
OFFSITE HOUSE
OUTBUILDING
WELL
The compliance boundary is established either 250 ft from the residuals application area or 50 feet within
in the property boundary, whichever is closest to the application area. The review boundary is,established
midway between the compliance boundary and the perimeter of the residuals application area. All
locations are approximate.
GRAPHIC SCALE
sso s sso'
e1mmlm
NC-AG-08
Fields 1-2

M R,
fe
Divislon of Water Resources
State of North Carolina
Department of Environment and Natural Resources
Division of Water Resources
LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are so an ed. Adherence to these
instructions and checking the provided boxes will help producea quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more irrfarmatiox, visit the Wader Quali/y Permitting Section"s Non -Discharge Permitting Unit
General —This document is an agreement between the Applicant and land owners) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100, Do not
submit this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
Ue*`Submit the completed and appropriately executed Residuals Source Certification (FORM: LASC 06-16) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
a plication may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
A" plirant.
lJ' A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or hisrepresentative hereby permits:
Applicant's name: 0,W... at .i� r�
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Site/Field ID
Lease
(yes/no)
Land Use or
Cropping Patterns
Intended Use of Crops
Residuals Source
(optional)
Special note
(no-till/over-seed/
pasture)
Al
P44
i Ars
The landowner or his representative receives, in consideration,. full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Pagel of 3

I. STIPULATIONS:
1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the sites) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application sites) to a third pasty, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met.
4. Notification of cancellation of [his Agreement shall be immediately forwarded [o NCDENR-DWR, Non -Discharge Permitting. Unit, 1636
Mail Service Center, Raleigh, NC 27699-1636.
5. The Pcrmittee must request and obtain a permit modification from the Division prior to a transfer of the Land application sites) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the
land application sim(s).
6. The Pcrmittee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of
the equipment used by the Pcrmittee.
7. The Permittce will provide the landowner or his representative with a copy of [he residuals permit prior to commencement of any residuals
land application event and a copy of the. results of each sail analysis.
8. If the soil pH of [he land application sites) is not maintained at 6.0 or greater, sufficient amounts of lime sha1L be applied to achieve a fmal
soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixmre is suitable for
the specified crop.
9. The landowner or his representative and the Pcrmittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Pcrmittee with information regarding [he amount and analysis of other sources of
nutrients (e:g., fertilizer, unregulated animal waste, etc.) thafhave been applied to the land application site(s).
I1. The landowner or his representative will inforn the Pcrmittee of any revisions or modifications to the intended use and cropping patterns for
the land application sites) prior to each planting season to enable the Pcrmittee to amend this Agreement and schedule residuals land
application events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on [he land application si[e(s) by [he Pcrmittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes [he Pcrmittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, or place on or related to the land application sites) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application sites) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit; takenecessary leachate, surface water, groundwater, or soil samples during the
tern of, and 12 months after termination of, this Agreement.
II. RESTRICTIONS:
1. Appropriate measures must be taken by the Permittce and/or the landowner or his representative to control public access to the land
application sites) during active use and for the 12-month period following a residuals land application event. Such controls may include the
posting of signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application sites) fora 30-day period following a residuals land application event. Land application
sites Drat aze to be used for grazing shall have fencing that will be used [o prevent access during these periods after such residuals land
application events.
3. Food crops, feed crops, and fiber crops shall not be harvested fora 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residualslsoil mixmre and are totally above the land surface shall not be harvested fora 14-
monthperiod following a residuals land application event.
5. Food crops with harvested parts below the surface of the land shall not be harvested fora 20-month period following. a residuals land
application event when the residuals. remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested fora 38-month period Following a residuals land
application event when the residuals. remain on the land surface for less than four months prim' to incorporation into the soil.
7. Turf grown on land where residuals aze applied shall not be harvested fora 12-month period following a residuals land application event.
IILALTERNATIVES FOR WATER SUPPLY WELLS INSH)E THE COMPLIANCE BOUNDARY; (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the. compliance boundary. However, ISA NCAC 02T .0105(h) allows the
compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance
boundary provided the groundwater standards can be met at the newly -established compliance bouhdary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for Feld(s) ID:
(Please include the rationale for the requested re -location of the compliance
�mpliance boundary to the application package)
A re -defined compliance boundary is not needed for this site.
IV.ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
boundary and attach a map showing the newly proposed
❑ The land application fields) ID: is curently permitted under another
residuals land application program; Permit Number WQ: .The land owner hereby acknowledge that by signing this.
agreement, he/she is requesting that the fields) be removed from the previously permitted residuals land application program and transferred
into the new program;
(Name of the new program)
FORM: LOA 06-16 Page 2 of 3

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name: U v 5 f�j ��! e e f i
Address: h • o,
City: �/� a State: zip: o
Phone: _ 3 � 7' 0 a 7 L E-mail address: 6/v J �- ^ e e �s n�% s (� /,'^ , o y
Signature: , 2 Date:Oc
NORTH CAROLINA, v r COUNTY( o I
I, the undersigned Notary Public do hereby certify that use, SIICKc
personally appeared before me this day and acknowledged the due execution of the forgoing instrument. ``,X
WITNESS my hand and official seal this the 2 F� N%v; W a �65,
day of 20 2 J
Signature and seal: (A/
My commission expires: V Z20g4
Lessee's/Operator's Certificatton:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee/operator name
Address:
City:
Phone:
Signature:
Permittee's Certification:
State:
E-mail
Date:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing
Signatur
FORM: LOA 06-16 Page 3 of 3

SUMMIT
ENVIRONMENTAL IECHN❑LOCIZS.INC.
ArlalyNal iab6ralarla2;
September 24, 2020
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Sparta WWTP -REVISED
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com
Order No.: 20010820
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/15/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
le,..
ior
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 30

mm' Summit Environmental Technologies, Inc. Case Narrative
su3310 Win St.
ENVIRONMENTAL I ECHNOLgG1ES, INC. Cuyahoga Falls, Ohio 44223 wo#: 20010820
ArralyVnal Labormldrla; TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com Date: 9/24/2020
CLIENT: Synagro
Project: Sparta WWTP -REVISED
WorkOrder Narrative:
20010820: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20010820-OOIA TCLP-SVOC-CPEST(8081B): Bracketing CCVs were out of range for some analytes.
All samples within the sequence are non -detect for all analytes.
20010820-001A TCLP-SVOC-CPEST(8081B): Surrogate outside recovery limits. Minimum method
criterion of one surrogate within established recovery limits was met.
20010820-OOIA TCLP-SVOC_8270E: Possible low bias for 1,4-Dichlorobenzene and
Hexachloroethane due to low recovery in LCS-41607.
20010820-OOIA TCLP-SVOC_8270E: Sample exhibits high recoveries for all surrogates. Possibly
doubled spiked by extractions analyst.
20010820-OOIA Sulfide,Reactive_NPW(9034): The sample was analyzed outside of hold time.
20010820-001A pH NPW(4500-H+B) 22nd Ed.: pH is an EPA field recommended parameter. Per 40
Revision v1
Page 2 of 30

MM' Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL I ECHNOLgG1ES, INC. Cuyahoga Falls, Ohio 44223 WO#: 20010820
ArralyVcal Labormldrla; TEL: [phone] FAX.- [phone]
Website: http:llwww.settek.com Date: 9/24/2020
CLIENT: Synagro
Project: Sparta WWTP -REVISED
CFR 136.3, hold time is 15 minutes from collection.
Analytical Sequence QC Notes:
LCS-41611 TCLP-SVOC-CPEST_TCLP(8081): LCS-41611 demonstrated high recovery for analyze
Endrin, suggesting a potential high bias for recovery of this analyte. All samples in this batch are non -
detect for Endrin.
LCS TCLP-SVOC-Herb_TCLP(8151): LCS exhibited high recovery, associated samples are ND for all
analytes of interest.
20010820-OOIAMS Sulfide,Reactive_NPW(9034): The sample was analyzed outside of hold time.
20010820-OOIAMSD Sulfide,Reactive_NPW(9034): The sample was analyzed outside of hold time.
20010820-00 1 ADUP pH_NPW(4500-H+B) 22nd Ed.: pH is an EPA field recommended parameter. Per
40 CFR 136.3, hold time is 15 minutes from collection.
REVISED REPORt 9/23/20 Corrected Reporting Limits
Revision v1
Page 3 of 30

��' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win E `�
ENVIRONMEWAL TECHNOLOGIES, INN Cuyahoga Falls, Ohio 442, Wo#: 20010820
ArWyacal Laboralonag TEL: [phone] FAX.- (330) 253-44E
Website: httv:11Www.settek.co Date: 9/24/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
NIB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision vl
Page 4 of 30

MM1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIR619MEWAL rECHHQL4G+1�3, INC Cuyahoga Falls, Ohio 44223
Arrzrlyf�cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
CLIENT: Synagro
Project: Sparta WWTP -REVISED
Lab SampleID Client Sample ID
20010820-001 Sparta WWTP
Tag No Date Collected
1/14/2020 11:30:00 AM
Workorder
Sample Summary
WO#: 20010820
Date Received
1/15/2020 10:20:00 AM
24-Sep-20
Matrix
Sludge
Page 5 of 30

m'
sum
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMEWAL 1rEC„NOLW4ES, INC
Cuyahoga Falls, Ohio 44223
WO#: 20010820
ArralyVcal Laboratorlas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Sep-20
Client:
Synagro
Project:
Sparta WWTP -REVISED
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
20010820-OOIA Sparta WWTP 1/14/2020 11:30:00 AM Sludge Flashpoint 200°F (EPA 1010)
1/16/2020 4:00:00 PM
pH (SM4500-H+ B)
1/29/2020 12:15:53 PM
Reactive Cyanide (9014/7.3.3.2)-Liqui
1/27/2020 1:47:00 PM
Reactive Sulfide (EPA 9034)
1/27/2020 1:47:00 PM
TCLP Herbicides by EPA 8321B
1/19/2020 3:00:00 PM 1/24/2020 1:34:00 AM
TCLP Mercury Analysis (SW1311/7471/19/2020 3:00:00 PM
1/21/2020 5:20:00 PM 1/24/2020 1:32:00 PM
TCLP Metals Analysis (SW1311/6010'1/19/2020 3:00:00 PM
1/21/2020 12:55:00 PM 1/22/2020 11:16:10 PM
TCLP Pesticides Analysis (SW1311/8(1/19/2020 3:00:00 PM
1/20/2020 3:30:00 PM 1/24/2020 12:50:00 AM
TCLP Semi-Volatiles Analysis 1/19/2020 3:00:00 PM
1/21/2020 3:30:00 PM 1/24/2020 8:56:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/19/2020 3:00:00 PM 1/23/2020 5:06:00 PM
Revision vl
Page 6 of 30

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, IMC Cuyahoga Falls, Ohio 44223 (base report)
Arrafytacal La66Yaldrla2; TEL: [phone] FAX: [phone] WO#: 20010820
Website: http://www.settek.com Date Reported: 9/24/2020
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
20010820-001A
Project:
Sparta WWTP -REVISED
Client Sample ID Sparta WWTP
Analyses
Tag Number:
Collection Date: 1/14/2020 11:30:00 AM
Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
RC I
FLASHPOINT 200°F (EPA 1010)
Flashpoint (200°F) >140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
208
Surr: Phenol-d6
224
Surr: Nitrobenzene-d5
240
SW7470A SW7470A Analyst: MJM
0.00200 mg/L 1 1/24/2020 1:32:00 PM
SW6010D SW3010A Analyst: EAM
1.25
mg/L
1
1/22/2020 11:16:10 PM
12.5
mg/L
1
1/22/2020 11:16:10 PM
0.250
mg/L
1
1/22/2020 11:16:10 PM
0.500
mg/L
1
1/22/2020 11:16:10 PM
1.25
mg/L
1
1/22/2020 11:16:10 PM
0.125
mg/L
1
1/22/2020 11:16:10 PM
1.25
mg/L
1
1/22/2020 11:16:10 PM
SW1010 Analyst: TAH
-F 1 1/16/20204:00:00 PM
SW8270 SW3510C Analyst: SFG
0.100
QL-
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
25.0
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
0.100
QL-
mg/L
5
1/24/2020 8:56:00 PM
0.100
mg/L
5
1/24/2020 8:56:00 PM
1.25
mg/L
5
1/24/2020 8:56:00 PM
1.25
mg/L
5
1/24/2020 8:56:00 PM
10 - 109
S
%Rec
5
1/24/2020 8:56:00 PM
10 - 109
S
%Rec
5
1/24/2020 8:56:00 PM
19 - 120
S
%Rec
5
1/24/2020 8:56:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision v1
U Samples with CalcVal < MDL
Page 7 of 30

MMIT Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, IMC Cuyahoga Falls, Ohio 44223
Arrafytacal La66Ya11Jrla2; TEL: [phone] FAX: [phone]
Website: http://www.settek.com
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
20010820-001A
Project:
Sparta WWTP -REVISED
Client Sample ID Sparta WWTP
Analytical Report
(base report)
WO#: 20010820
Date Reported: 9/24/2020
Tag Number:
Collection Date: 1/14/2020 11:30:00 AM
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
SW8270 SW3510C Analyst: SFG
Surr: 2,4,6-Tribromophenol
271
10 - 120
S
%Rec
5
1/24/2020 8:56:00 PM
Surr: 2-Fluorobiphenyl
226
22 - 117
S
%Rec
5
1/24/2020 8:56:00 PM
Surr: p-Terphenyl-d14
262
34 - 116
S
%Rec
5
1/24/2020 8:56:00 PM
NOTES:
Possible low bias for 1,4-Dichlorobenzene and Hexachloroethane due to low recovery in LCS-41607.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
Analyst: SEK
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0200
mg/L
5
1/24/2020 12:50:00 AM
Toxaphene
ND
0.250
mg/L
5
1/24/2020 12:50:00 AM
Endrin
ND
0.00500iQC+QDmg/L
5
1/24/2020 12:50:00 AM
gamma-BHC
ND
0.00500
dQC+
mg/L
5
1/24/2020 12:50:00 AM
Heptachlor
ND
0.00500
dQC+
mg/L
5
1/24/2020 12:50:00 AM
Heptachlor epoxide
ND
0.00500
dQC+
mg/L
5
1/24/2020 12:50:00 AM
Methoxychlor
ND
0.00500
dQC+
mg/L
5
1/24/2020 12:50:00 AM
Surr: TCMX
102
10 - 119
%Rec
5
1/24/2020 12:50:00 AM
Surr: DCB
142
10 - 119
S
%Rec
5
1/24/2020 12:50:00 AM
TCLP HERBICIDES BY EPA 8321B
SW8321A
SW1311M Analyst: BJH
2,4-D
ND
0.500
mg/L
50
1/24/2020 1:34:00 AM
2,4,5-TP
ND
0.500
mg/L
50
1/24/2020 1:34:00 AM
Surr: 2,4-Dichlorophenylacetic aci
79.4
70 - 130
%Rec
50
1/24/2020 1:34:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: RMT
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
MEK
ND
5.00
mg/L
50
1/23/2020 5:06:00 PM
Benzene
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
Chlorobenzene
ND
2.50
mg/L
50
1/23/2020 5:06:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Revision v1
RL
Reporting Detection Limit
U
Samples with CalcVal < MDL
Page 8 of 30

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, IMC Cuyahoga Falls, Ohio 44223 (base report)
Arrafytacal La66Yaldrla2; TEL: [phone] FAX: [phone] WO#: 20010820
Website: http://www.settek.com Date Reported: 9/24/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/14/2020 11:30:00 AM
Lab ID: 20010820-001A
Project: Sparta WWTP -REVISED
Client Sample ID Sparta WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: RMT
TCLP VOLATILES ANALYSIS
Chloroform
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
Tetrachloroethene
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
Trichloroethene
ND
0.250
mg/L
50
1/23/2020 5:06:00 PM
Vinyl chloride
ND
0.100
mg/L
50
1/23/2020 5:06:00 PM
Sum 4-Bromofluorobenzene
101
70 - 130
%Rec
50
1/23/2020 5:06:00 PM
Sum Dibromofluoromethane
97.2
70 - 130
%Rec
50
1/23/2020 5:06:00 PM
Surr: Toluene-d8
93.5
70 - 130
%Rec
50
1/23/2020 5:06:00 PM
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-LIQUID
Cyanide, Reactive
ND
0.485
mg/L
1
1/27/2020 1:47:00 PM
PH (SM4500-H+ B)
A4500-H+B
Analyst: VVK
pH 6.8 H s.u.@20.3C 1 1/29/2020 12:15:53 PM
NOTES:
pH is an EPA field recommended parameter. Per 40 CFR 136.3, hold time is 15 minutes from collection.
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (EPA 9034)
Sulfide, Reactive ND 25.0 H mg/L 1 1/27/2020 1:47:00 PM
NOTES:
The sample was analyzed outside of hold time.
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Revision v1
U Samples with CalcVal < MDL
Page 9 of 30

Summit Environmental Technologies, Inc.
Accreditation
Program
SU3310 Win St.
MM111
Anal te5 Report
Y p
ENVIRONWE TALTE(CWUGWGieS,INC
Cuyahoga Falls, Ohio44223
AnalyOca) Laboratodlaff
TEL: [phone] FAX.- [phone]
WO#:
20010820
Website: hgp:llwww.settek.com
24-Sep-20
Client: Synagro
State: NW
Project: Sparta WWTP -REVISED
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
20010820-OOIA Sludge
Flashpoint 200°F (EPA 1010)
Flashpoint (200°F)
A
Sludge
pH (SM4500-H+ B)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Liquid
Cyanide, Reactive
N
Sludge
Reactive Sulfide (EPA 9034)
Sulfide, Reactive
N
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
NC WW SCM A Accredited
Version #3
Page 10 of 30

Summit Environmental Technologies, Inc.
Accreditation
Program
MM' T
ffISU3310 Win St.
Anal te5 Report
Y p
EHYIRO]q M EuTAL I EC"no LDG1Es, IFIC, Cuyahoga Falls, Ohio 44223
ArralyOal Lab6ralonim TEL: [phone] FAX.- [phone]
WO#:
20010820
Website: hgp:llwww.settek.com
24-Sep-20
Client: Synagro
State: NW
Project: Sparta WWTP -REVISED
Program Name: NC WW SCM
Sample ID Matrix Test Name
Analyte
Status
20010820-OOIA Sludge TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge TCLP Volatiles Analysis
2-Butanone
A
Sludge TCLP Volatiles Analysis
Benzene
A
Sludge TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge TCLP Volatiles Analysis
Chlorobenzene
A
Sludge TCLP Volatiles Analysis
Chloroform
A
Sludge TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge TCLP Volatiles Analysis
Trichloroethene
A
Sludge TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited
Version #3
Page 11 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralor/as TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: 41570B
Sample ID: MB-41570
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: PBS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581728
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
dQC+
gamma-BHC
ND
0.000500
dQC+
Heptachlor
ND
0.000500
dQC+
Heptachlor epoxide
ND
0.000500
dQC+
Methoxychlor
ND
0.000500
dQC+
Sum TCMX
601
1000 60.1 10 119
Sum DCB
1030
1000 103 10 119
Sample ID: LCS-41570
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 108443
Client ID: LCSS
Batch ID: 41570B
TestNo: SW8081
Analysis Date: 1/23/2020
SegNo: 2581729
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.790
0.000500
0.500
0
158
10
130
SmQC-
gamma-BHC
0.482
0.000500
0.500
0
96.5
10
130
QC+
Heptachlor
0.516
0.000500
0.500
0
103
10
130
mQC+
Heptachlor epoxide
0.576
0.000500
0.500
0
115
10
130
QC+
Methoxychlor
0.789
0.000500
0.500
0
158
10
178
mQC+
Sum TCMX
793
1000
79.3
10
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal`
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Revision vl
Page 12 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL IECHNOLOGIES,INC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorfor TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
Client: Synagro
Project: Sparta WWTP -REVISED BatchID: 41572
TCLP Mercury ND 0.00200
TCLP Mercury 0.00402 0.00200 0.00400 0 101 80 120
TCLP Mercury ND 0.00200
Sample ID: TCLP BLANK 1-20-2
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/21/2020
RunNo: 108442
Client ID: PBS
Batch ID: 41572
TestNo: SW7470A SW7470A
Analysis Date: 1/24/2020
SegNo: 2581507
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,INC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: 41572
Sample ID: TCLP BLANK 1-20-2
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/21/2020
RunNo: 108442
Client ID: PBS
Batch ID: 41572
TestNo: SW7470A SW7470A
Analysis Date: 1/24/2020
SegNo: 2581507
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20011053-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/21/2020
RunNo: 108442
Client ID: BatchQC
Batch ID: 41572
TestNo: SW7470A SW7470A
Analysis Date: 1/24/2020
SegNo: 2581515
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00466 0.00200 0.00400 0 116 75 125
Sample ID: 20011053-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/21/2020
RunNo: 108442
Client ID: BatchQC
Batch ID: 41572
TestNo: SW7470A SW7470A
Analysis Date: 1/24/2020
SegNo: 2581516
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00455 0.00200 0.00400 0 114 75 125 0.00466 2.39 20
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal`
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralor/as TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: 41581
Sample ID: 20011053-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/21/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41581
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575555
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.19
0.500
2.000
0
109
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.2056
92.4
70
130
TCLP Cadmium(Cd)
2.14
0.100
2.000
0.001431
107
70
130
TCLP Chromium(Cr)
1.87
0.200
2.000
0.002186
93.3
70
130
TCLP Lead(Pb)
1.75
0.500
2.000
0
87.5
70
130
TCLP Selenium(Se)
2.43
0.0500
2.000
0.02499
120
70
130
TCLP Silver(Ag)
2.31
0.500
2.000
0
116
70
130
Sample ID: 20011053-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/21/2020
RunNo: 108350
Client ID: Batch=
Batch ID: 41581
TestNo: SW6010D SW3010A
Analysis Date: 1/22/2020
SegNo: 2575556
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.27
0.500
2.000
0
114
70
130
2.188
3.77
20
TCLP Barium(Ba)
ND
5.00
2.000
0.2056
93.7
70
130
0
0
20
TCLP Cadmium(Cd)
2.19
0.100
2.000
0.001431
110
70
130
2.140
2.36
20
TCLP Chromium(Cr)
1.89
0.200
2.000
0.002186
94.6
70
130
1.869
1.32
20
TCLP Lead(Pb)
1.79
0.500
2.000
0
89.3
70
130
1.750
2.09
20
TCLP Selenium(Se)
2.62
0.0500
2.000
0.02499
130
70
130
2.430
7.36
20
TCLP Silver(Ag)
2.38
0.500
2.000
0
119
70
130
2.314
2.64
20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision Vl
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralor/as TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: 41581
Sample ID: MB-41581
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/21/2020
RunNo: 108247
Client ID: PBS
Batch ID: 41581
TestNo: SW6010D SW3010A
Analysis Date: 1/21/2020
SegNo: 2575079
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-41581
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/21/2020
RunNo: 108247
Client ID: LCSS
Batch ID: 41581
TestNo: SW6010D SW3010A
Analysis Date: 1/21/2020
SegNo: 2575080
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.82
0.500
2.000
0
91.2
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
92.4
80
120
TCLP Cadmium(Cd)
1.80
0.100
2.000
0
90.2
80
120
TCLP Chromium(Cr)
1.85
0.200
2.000
0
92.7
80
120
TCLP Lead(Pb)
1.88
0.500
2.000
0
94.1
80
120
TCLP Selenium(Se)
1.92
0.0500
2.000
0
96.1
80
120
TCLP Silver(Ag)
2.00
0.500
2.000
0
100
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision Vl
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
BatchID: 41607
WO#: 20010820
24 Sep-20
Sample ID: 20010822-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
3lient ID: Batch=
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586256
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.259
0.200
0.8000
0
32.4
15.2
124
QMR
2,4,5-Trichlorophenol
0.681
0.500
0.8000
0
85.2
30.6
152
2,4,6-Trichlorophenol
0.662
0.500
0.8000
0
82.7
27.6
150
2,4-Dinitrotoluene
0.893
0.100
0.8000
0
112
58
141
o-Cresol
ND
0.500
0.8000
0
61.6
26.9
132
Cresols, Total
ND
10.0
1.600
0
62.4
27.6
132
Hexachloro-1,3-butadiene
0.278
0.0400
0.8000
0
34.7
-5.3
156
QMR
Hexachlorobenzene
0.657
0.100
0.8000
0
82.1
54.3
142
Hexachloroethane
0.227
0.200
0.8000
0
28.4
1.92
131
QMR
Nitrobenzene
0.483
0.200
0.8000
0
60.4
21
135
Pentachlorophenol
0.899
0.500
0.8000
0
112
47.4
134
Pyridine
ND
0.500
0.8000
0
41.8
-10.3
64.2
m
Surr:2-Fluorophenol
0.489
1.000
48.9
9.77
146
Surr: Phenol-d6
0.525
1.000
52.5
20.7
130
Surr: Nitrobenzene-d5
0.581
1.000
58.1
13.9
156
Surr:2,4,6-Tribromophenol
0.942
1.000
94.2
27.3
183
Surr:2-Fluorobiphenyl
0.622
1.000
62.2
21.4
153
Surr: p-Terphenyl-d14
1.02
1.000
102
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
BatchID: 41607
WO#: 20010820
24 Sep-20
Sample ID: 20010822-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
3lient ID: Batch=
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2586257
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.397
0.200
0.8000
0
49.6
15.2
124
0.2588
42.2
30 R
2,4,5-Trichlorophenol
0.741
0.500
0.8000
0
92.6
30.6
152
0.6812
8.38
30
2,4,6-Trichlorophenol
0.793
0.500
0.8000
0
99.2
27.6
150
0.6616
18.1
30
2,4-Dinitrotoluene
0.944
0.100
0.8000
0
118
58
141
0.8932
5.57
30
o-Cresol
0.613
0.500
0.8000
0
76.7
26.9
132
0.4924
21.9
30
Cresols, Total
ND
10.0
1.600
0
76.6
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.470
0.0400
0.8000
0
58.7
-5.3
156
0.2776
51.4
30 R
Hexachlorobenzene
0.728
0.100
0.8000
0
91.0
54.3
142
0.6568
10.3
30
Hexachloroethane
0.378
0.200
0.8000
0
47.2
1.92
131
0.2272
49.7
30 R
Nitrobenzene
0.584
0.200
0.8000
0
73.0
21
135
0.4832
18.8
30
Pentachlorophenol
0.984
0.500
0.8000
0
123
47.4
134
0.8992
9.01
30
Pyridine
ND
0.500
0.8000
0
44.7
-10.3
64.2
0
0
30 m
Surr: 2-Fluorophenol
0.581
1.000
58.1
9.77
146
0
Surr: Phenol-d6
0.650
1.000
65.0
20.7
130
0
Surr: Nitrobenzene-d5
0.682
1.000
68.2
13.9
156
0
Surr:2,4,6-Tribromophenol
1.02
1.000
102
27.3
183
0
Surr:2-Fluorobiphenyl
0.755
1.000
75.5
21.4
153
0
Surr: p-Terphenyl-d14
1.07
1.000
107
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 18 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
BatchID: 41607
WO#: 20010820
24 Sep-20
Sample ID: MB-41607
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
3lient ID: PBS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581886
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.383
Surr: Phenol-d6
0.386
Surr: Nitrobenzene-d5
0.373
Surr: 2,4,6-Tribromophenol
0.640
Surr: 2-Fluorobiphenyl
0.375
Surr: p-Terphenyl-d14
0.859
1.000
38.3
10
109
1.000
38.6
10
109
1.000
37.3
19
120
1.000
64.0
10
120
1.000
37.5
22
117
1.000
85.9
34
116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 19 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
BatchID: 41607
WO#: 20010820
24 Sep-20
Sample ID: LCS-41607
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/21/2020
RunNo: 108448
3lient ID: LCSS
Batch ID: 41607
TestNo: SW8270 SW3510C
Analysis Date: 1/24/2020
SegNo: 2581887
analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.213
0.100
0.8000
0
26.7
36.4
130 S
2,4,5-Trichlorophenol
0.610
0.250
0.8000
0
76.3
31.7
132
2,4,6-Trichlorophenol
0.642
0.250
0.8000
0
80.2
31.1
133
2,4-Dinitrotoluene
0.822
0.0500
0.8000
0
103
43.3
130
o-Cresol
0.448
0.250
0.8000
0
56.0
32.9
130
Cresols, Total
ND
5.00
1.600
0
58.1
31.7
130
Hexachloro-1,3-butadiene
0.263
0.0200
0.8000
0
32.9
31.4
130
Hexachlorobenzene
0.597
0.0500
0.8000
0
74.7
43.1
130
Hexachloroethane
0.188
0.100
0.8000
0
23.5
36.5
130 S
Nitrobenzene
0.438
0.100
0.8000
0
54.7
39.5
130
Pentachlorophenol
0.705
0.250
0.8000
0
88.1
34
130
Pyridine
0.255
0.250
0.8000
0
31.9
10
130
Surr: 2-Fluorophenol
0.434
1.000
43.4
17.1
130
Surr: Phenol-d6
0.482
1.000
48.2
10
130
Surr: Nitrobenzene-d5
0.506
1.000
50.6
32.6
130
Surr: 2,4,6-Tribromophenol
0.831
1.000
83.1
4.43
130
Surr: 2-Fluorobiphenyl
0.521
1.000
52.1
41.8
130
Surr: p-Terphenyl-d14
0.834
1.000
83.4
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,IMC Cuyahoga Falls, Ohio44223
ArWy0c21 Laboralorlas TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: R108275
Sample ID: LCS-R108275
SampType: LCS
TestCode: FlashPt_Oil(1 Units: T
Prep Date:
RunNo: 108275
Client ID: LCSW
Batch ID: R108275
TestNo: SW1010
Analysis Date: 1/16/2020
SegNo: 2570505
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (200T) 137 135.4 0 101 98 102
Sample ID: LCSD-R108275
SampType: LCSD
TestCode: FlashPt_Oil(1 Units: T
Prep Date:
RunNo: 108275
Client ID: LCSS02
Batch ID: R108275
TestNo: SW1010
Analysis Date: 1/16/2020
SegNo: 2570506
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (200T) 137 135.4
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0 101 98 102 137.0 0 20
E Value above quantitation range H Holding times for preparation or anal`
M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision vl
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 30

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVRON MENTAL IECHNOLOG4ES.INC. Cuyahoga Falls, Ohio 44223
Arlalyt�cal iaboratarlas TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
Wo#: 20010820
24-Sep-20
BatchID: R108275
Sample ID: 20010790-007ADUP
SampType: DUP
TestCode: FlashPt_NP Units: °F
Prep Date:
RunNo: 108275
,lient ID: Batch=
Batch ID: R108275
TestNo: SW1010
Analysis Date: 1/16/2020
SegNo: 2570557
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (200T)
188
186.0 1.07 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
R0V1Slori vl
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 30

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL IEcH"aLOG4ES.iP:C
Cuyahoga Falls, Ohio44223
WO#: 20010820
Ar}�t�ca1 iaboralar�as
ia1
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
24 Sep-20
Client:
Synagro
Project:
Sparta WWTP -REVISED
BatchlD: R108542
Cyanide, Reactive ND 0.485
Cyanide, Reactive 9.68 0.490 10.00 0 96.8 85 115
Cyanide, Reactive ND 0.490 0.5000 0 78.9 50 150
Sample ID: 20010820-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 108542
Client ID: Sparta WWTP
Batch ID: R108542
TestNo: SW9014
Analysis Date: 1/27/2020
SegNo: 2587805
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.28 0.490
10.00 0 92.8 81.3
118
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal`
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Revision VI
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 23 of 30

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL IEcH"aLOG4ES.iP:C
Cuyahoga Falls, Ohio44223
WO#: 20010820
Ar}�t�ca1 iaboralar�as
ia1
TEL: [phone] FAX: [phone]
Website: http://www.settek.com
24 Sep-20
Client:
Synagro
Project:
Sparta WWTP -REVISED
BatchlD: R108542
Sample ID: 20010820-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 108542
Client ID: Sparta WWTP
Batch ID: R108542
TestNo: SW9014
Analysis Date: 1/27/2020
SegNo: 2587805
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20010820-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 108542
Client ID: Sparta WWTP
Batch ID: R108542
TestNo: SW9014
Analysis Date: 1/27/2020
SegNo: 2587806
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.37 0.485 10.00 0 93.7 81.3 118 9.285 0.905 5
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 30

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHNOLOGIES,INC Cuyahoga Falls, Ohio44223
Arles/y0c21 Laboralorfor TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
Client: Synagro
Project: Sparta WWTP -REVISED BatchID: R108543
Sulfide, Reactive ND 25.0
Sulfide, Reactive 4510 25.0 4800 0 94.0 85 115
Sulfide, Reactive 4580 25.0 4800 0 95.4 75 125 H
NOTES:
The sample was analyzed outside of hold time.
Sample ID: 20010820-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 108543
Client ID: Sparta WWTP
Batch ID: R108543
TestNo: SW9034
Analysis Date: 1/27/2020
SegNo: 2587818
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 25 of 30

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVRON MENTAL IECHNOLOG4ES.INC. Cuyahoga Falls, Ohio 44223
Arlalyt�cal iaboratarlas TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24-Sep-20
BatchlD: R108543
Sample ID: 20010820-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 108543
Client ID: Sparta WWTP
Batch ID: R108543
TestNo: SW9034
Analysis Date: 1/27/2020
SegNo: 2587818
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4640
NOTES:
The sample was analyzed outside of hold time.
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
25.0 4800 0 96.7 75 125 4580 1.30
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
30 H
Revision vl
Page 26 of 30

Summit Environmental Technologies, Inc
SUMMIT 3310 Win St
ENVIRONMENTAL TECHNOLOGIES,INC Cuyahoga Falls, Ohio44223
ArIa1} t�ca1 Laboralar�as TEL: [phone] FAX: [phone]
Website: http://www.settek.coni
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24 Sep-20
BatchID: R108624
Sample ID: LCS-R108624
SampType: LCS
TestCode: pH_011(9045D Units: s.u.@20.9C
Prep Date:
RunNo: 108624
Client ID: LCSW
Batch ID: R108624
TestNo: A4500-H+B
Analysis Date: 1/29/2020
SegNo: 2592160
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.9 90 110
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_011(9045D Units: s.u.@21.1C
Prep Date:
RunNo: 108624
Client ID: LCSW
Batch ID: R108624
TestNo: A4500-H+B
Analysis Date: 1/29/2020
SegNo: 2592362
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.9 90 110
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_Oil(9045D Units: s.u.@21.3C
Prep Date:
RunNo: 108624
Client ID: LCSW
Batch ID: R108624
TestNo: A4500-H+B
Analysis Date: 1/29/2020
SegNo: 2594509
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal`
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
Revision VI
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 27 of 30

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVRON MENTAL IECHNOLOG4ES.INC. Cuyahoga Falls, Ohio 44223
Arlalyt�cal iaboratarlas TEL: [phone] FAX.- [phone]
Website: hgp:llwww.settek.com
Client: Synagro
Project: Sparta WWTP -REVISED
QC SUMMARY REPORT
WO#: 20010820
24-Sep-20
BatchID: R108624
Sample ID: 20010820-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@20.2C
Prep Date:
RunNo: 108624
,lient ID: Sparta WWTP
Batch ID: R108624
TestNo: A4500-H+B
Analysis Date: 1/29/2020
SegNo: 2592172
analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.8
NOTES:
pH is an EPA field recommended parameter. Per 40 CFR 136.3, hold time is 15 minutes from collection.
6.8 0.3 5 H
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
R0V1Slori vl
ND Not Detected P Second column confirmation exceeds PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 30

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Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTALTECHNOLQCIE$,INC Cuyahoga Falls, Ohio44223 Sample Log -in Check List
Arrzr/yt�caf Laboralorfas TEL: [phone] FAX [phone]
Website: http://www.settek.coni
Client Name: SYN-NC-27028
Logged by: Jesseca E. Westfall
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Loa In
3, Coolers are present?
Work Order Number: 20010820
1/15/2020 10:20:00 AM
1/19/2020 1:09:09 PM
1/28/2020 10:31:28 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
g. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
RcptNo: 1
��., rrr.•r�-�
Yes
❑
No
F
Not Present ❑
UPS
Yes
C
No
❑
NA F
Yes
d❑
No
Yes
❑
No
❑
Not Present
Signed By:
Yes
❑
No
F—
NA
Yes
❑
No
❑
NA
Yes
J❑
No
❑
Yes
d❑
No
❑
Yes
J❑
No
❑
Yes
❑
No
d❑
NA ❑
Yes
❑
No
❑
No VOA Vials ❑�
Yes
❑
No
d❑
Yes
J❑
No
❑
Yes
d❑
No
❑
Yes
d❑
No
❑
Yes
J❑
No
❑
Yes ❑ No ❑ NA ❑d
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed
1 1.2 Good Not Present
Page 30 of 30