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HomeMy WebLinkAboutWI0400023_Post-Injection_20001212ff Corporation ofNorth Carolina, Inc. A bfemher of The IT Croup POST -INJECTION MONITORING REPORT VOLUME II — APPENDIX A W. P. Ballard Property 2701 Branchwood Drive Greensboro, Guilford County, North Carolina NCDENR Groundwater Incident # 6953 IT Corporation of North Carolina Project # 107535 December 12, 2000 Prepared by. IT Corporation of North Carolina, Inc. 2200 Gateway Center Drive, Suite 205 Morrisville, North Carolina 27560 (919) 467-2227 Release / Site Information: IT Corporation ofNorth Carolina, Inc. A Member of The IT Croup APPENDIX A LABORATORY ANALYTICAL REPORTS 'haiu of'Custody Record 1EMAIREHICA INC. Pnfre ' of L-3 Asheville, NC (A) ❑ Bartlett, IL (C) ❑ Cedar Falls, IA (E)❑ Charlotte, NC (G) ❑ Dayton, OH (1) ❑ Lumberton, NC (K) C)-Nashville, TN (M) ❑ Pontiac, N11 (0) ❑ Rockford. II (Q) (828)254-5169 (6-30)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 t-I Ad uta. GA (13) ❑ Brighton, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. IA (J) ❑ Indianapolis, IN (L) ❑ Macon, GA (N) ❑ Orlando, FL (P) ❑ Watertown. WI (R) (7AI),368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Clicut: - - Cc).\ Project No.: I0 535- REQUESTED PARAMETERS Report Address:'': r,U( _ r 3,R 1 ' �': Invoice Address: \C Is this work being conducted for regulatory - - -• —� compliance monitoring? Yes— No — - Alin: __ I Attn: Is this work being conducted for regulatory enforcement action'? Phone No.: �� , /�) ')L Sampled Bye ( Yes No � \ � — — Fax No.: 1!j !'(n" � ,".�(; _ P.O. No: 1303�7 Which regulations apply: RCRA_ NPDESWastewater_ Quote No. ' TURNAROUNDTIME �� (`� UST Drinking Water_ Suite Samples Collected V•Standard Other— None_ Needed: ei ❑ Rush (surcharges may apply) Date �,J # and tvpe of containers Satle II) nt 1 Dale Time COmp (C) Grab (G) Matrix . Lab Use v o M z ��„ r 0 REMARKS o l ( 171,11 I I'� 1, u� IV y f 7 V il. (� r; O r( 1 QC.Deliverahles; ❑ None O Leve12 BatcttQC s f f ❑ Level 3 ❑ Leve1..4 O Other Init Lob Tem L p :"' Ree Lab Teutp c'cm1MENTS: Relinyui,hed By i' ". ,y / ! Date , ' Time Received By: �1 • % �. t [' t e LAB USE ONLY::. ; Reliuyuished By: Date Time Received By: - Dale Time . Custody Seal: Dyes QNo CIN/A Relinquished By: Date I Time Received By: Date Time Relinqui,hed By: Date l Time Received By: Date I Time Bottles Supplied by TA: OYes ON. - in Crrstody Record rE4WIN(';Jta 2 C / o% Page- o ❑ Asheville, NC (A) ❑ Bartlett, IL (C) ❑ Cedar Faills'gl*, )❑ dlLarlotte, I C (Q)) ❑ Dayton, OH (I) ❑ Lumberton, NC (K) 9 Nashville, TN (M) ❑ Pontiac, Ml (0) ❑ Rockford. 11 (Q) (828)254-5169 (630)289-3100 (319)27-7-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 ❑ Atlanta, GA (B) ❑ Brighlon, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. IA (J) ❑ Indianapolis, IN (L) ❑ Macon, GA (N) ❑ Orlando, FL (P) ❑ Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Client: 1-I (' �) ' C Project No.: j 0%53 - REQUESTED PARAMETERS Report Address: Itrvoice Address: - Is this work being conducted for regulatory compliance monitoring? Yes_ No- Is this work being conducted for regulatory enforcement action? Yes_ No Attn: �' r s Attn: - Phone No.: ;;1�1 ^ rJ� Sampled Byre Fax No.: P.O. No:n� \ v Which regulations apply: 1 RCRA NPDESWastewater_ (/�• �� UST Drinking Water_ 'V Other_ None_ '1'UItNAIiOUND Tll\•11s J' Snmdard Quote No. State Samples Collected Rush (surcharges may apply) Date Needed: N and type of containers Sample ID Date Time Grab Con (Gj Matrix Lab Use �o m z z x x r o o z REMARKS I( I r << r �c 2 gjGQ - NOTI -(Z'9 r, VJ QC Deliverables:.:' ❑ None ❑ I,e4l,2 J3atch;QC ❑ Level 3 ❑ Leveh,4 • " ©Othei COMMENTS Relinquished By ,. Received B y:, t'I)�te _: ) ,�( Vme x LAB USE ONLY 71 Custody Seal Yes 1No _ �N/A Relinquished By: Date I Time Received By: _. Date Time Rclinyuishcd By: Date I Time Received By: Date Time - — Relinyuished By: Date I Time I Received By: Date I Time Bottles Supplied by TA::.Oyes 1766 'haul of Custody Record rffNME it iNC■ (�5 (:-) Q [ J Z Page '-3 o(--./I— ❑ Asheville, NC (A) 17 Barden, IL (C) L7 Cedar Falls, IA (E)❑ Char46tter NPTG) /Dayy p OH (I)" }� Lumberton, NC (K) R Nashville, TN (M) Q Pontiac, MI (0) L'7 Rockford. 11(Q) (828) 254-5169 (630) 289-3100 (319) 277-2401 (704)'392'I I64'� `�937)�94-6�56)1910) 738-6190 (6l5) 726-0177 (248) 332-1940 (815) 874-2171 L7 Atlanta, GA (13) Brighton, CO (D)CI Charleston, SC (F)17 Columbia, SC (H) Davenport. IA (J) 17 Indianapolis, IN (L) O Macon, GA (N) ❑ Orlando, FL (P) 171 Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Client: ; I CuKE`' :.� JVC •r", Project No.: /07 REQUESTED PARAMETERS Is this work being conducted for Report Address: CJ Invoice Address: '� AG/f I'C .Lj ., . r �� 7u regulatory compliance monitoring? Yes_ No_ nun: �' •, ICE. �, (xol Attn: ' y �)r)c Is this work being conducted for Phone No.: c w1 ���� fir' Sampled By: }� „t 1h �, r t' regulatory enforcement action? Yes_ No_ lax No.: �li� t�(,) ;j;Z �� P.O. No: Which regulations apply: No. c9" TURNAROUND TIMEQuote RCRA NPDESN'Vasiewater — UST Drinking Water_ State Samples Collected 7 Standard Other_ None — `1 0 Rush (surcharges may apply) Date Needed: - - C) g N and type of contCrnC)ainers Sample 1D Date Time Goa (G) Matrix Lab Use U o z O6 r c REMARKS ;tj-)ll[J( ] �I-%•GU 1,1S-to l�- A 0 r - (.j - Of' n /qU6 ✓ J -c:�- �I�OP� 153(P � ✓ 1 QC Deliverables: Q None_ ❑ Level;2 Batch QC F � � Level 3 f� Level` InitLa ec Lab Tem pO n. COMMENTS: Reliogoished By: :� h r.�r,� „c., ce"L-- Ne. j 1 jt ime Received By: / ; i me LAB USE ON LY Custody SeaYes l:. IJh�No �N/A Relinquished By: Date Time Received Bye Date Time Iteliuquished By: Date Time Received By: Date Time — — Relinquished 13y: Date 1 Time Received By: Date I Time Bottles Supplied by TA: 0Yes ON. 'hair of Custody Record fEVAmEWCA INS; ■ nc,—vn 3 Page of �--, ❑ Asheville, NC (A) ❑ Bartlett, 1L (C) Q Cedar Falls, IA (E)Q Charlotte, NG-1G) `Q Da to "OH (1)� 1 Q� umberton, NC (K) Nashville, TN (M) Q Pontiac, MI (0) Q Rockford. 11(Q) (828) 254-5169 (630) 289-3100 (319) 277-2401 (704) 392-Iy6�. (937) �99-6856/ i (>310) 738-6190 (615) 726-0177 (248) 332-1910 (815) 874-2171 L) Atlanta, GA (13) Q Brighton, CO (D)Q Charleston, SC (F) Q Columbia, SC (H) Q Davenport. IA (J) Q Indianapolis, IN (L) Q Macon, GA (N) Q Orlando, FL (P) Q Watertown, WI (R) , (770) 368-0636 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7944 (317) 842-4261 (912) 757-0811 (407) 851-2560 (920) 261-1660 ('lient:_I-� (�►j ���/� Project No.:—W-t% REQUESTED PARAMETERS Report Address: Invoice Address: Is this work being conducted for regulatory compliance monitoring? Yes_ No— Is this work being conducted for regulatory enforcement action? Yes No — — Which regulations apply: RCRA NPDESWastewater_ UST_ Drinking Water �� Other_ None_ >E and type of containers - �( - Atut: C Attn: jc��rlc PhoneNo.:111t1 `�7 ���� Sampled By: kB �tPS - Fax No.: �I�% c(G7 a9`� 1 P.O. No:� ?j(� J%7 TURNAROUND TIME t,,St:tndard 7 Rush (surcharges may apply) Date Quote No. State Samples Collected /,,(k' Needcd: ID Date Time ConSample Grab (G) Matrix Lab Use O ram„ s c REMARKS CS C7 W - 611►w J 0 ✓ ✓ 5 tz QC Deliverables: Q None ❑ Leve12 Batch:QC Q Level3 'ClLeveT4 L7fGther 1 Iu�tiab'I>emp . RecLabTemp COMMENTS: Relin wished B . 9 y: / L. i t ' LtJ l Ut �� e�, Dai Time Received ( % ,� / ate '� •- CTlme .LAB USE ONLY: . Custody Seal: Oyes ON, ON/A Bottles Supplied by TA: OYes ON. Relinquished By: Date 'time Received y: Date Time Relinquished By: Date I Time Received By: Date Time Relinquished By: Date I Timc Received By: Date I Time 'hair of Custody Record rhTA%EtuCA iN1;. M--�-oa6 y Paee-L- of Q A,hevillc, NC (A) Q Bartlett, IL (C) Q Cedar Falls, IA (E)Q Charlotte, NC (G) ❑ Dayton, OH (1) Q Lumberton, NC (K) Nashville, TN (M) Cl Pontiac, M1 (0) ❑ Rockford. 11 (Q) (828)254-5169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 C7 Atlanta, GA (B) Q Brighton, CO (D)❑ Charleston, SC (F) Q Columbia, SC (H) Q Davenport. IA (J) Q Indianapolis, IN (L) Q Macon, GA (N) ❑ Orlando, FL (11) ❑ Watertown, WI (R) (770)368-0636 (303)659-0497 (843)949-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Client: -1- `(lf;,i? Project No.: �l`1��)�'If REQUESTED PARAMETERS Repot I Addres: Invoice Address: Is this work being conducted for regulatory compliance monitoring? Yes_ No - Attn: !. 'i'. Attn: Is this work being conducted for \ / regulatory enforcement action'? Phone No.: ;l 1 �- `, Sampled By` t �r L �� ��n (k�/l. �-�V Yes_ No \i Fax No.:1.(.�rl' P.O. No: 7Uj �`( - `� Which regulations apply: RCRA_ NPDESWastewater_ n� Water_ TURNA ROUNDITIN-IE Quote No. State Samples Collected J r UST_ Drinking J Standard w\ JJ Other_ None_ 0 Rush (Surcharges may apply) Date Needed: # and t e of containers ID Date Time ComS:uuple Graff (Gj matrix Lab Use /' o ��„ s REMARKS D.d .- i,I'l (-Dud (7 VUL n IM QC Deliverables: ❑ None ❑ Level2 Batch.QC s -41 ❑ Level 3 ❑ Leve14 . ❑Other Imt Lab Temp:; Rec Lab Temp r ('uNIMENTS: Relinquished B ! /'�7�!��Time f. 1 •' !1 Received By Date` ' % +_Time LAB USE ONLY: Custody Seal: CIYe, ONO ON/A Relinquished By: I !; t ! Date' /r� t" .:,-.,Time Received By: Date Time Rclinyuishcd By: Date Time Received By: Date Time Relinquished Ily: D:uc I Time Received 13y: Date I Time Bottles Supplied by TA: Mes ON. 'hair of Custody Record rui wdniCA ING ■ Pajzel� of 17 Asheville, NC (A) 0 Bartlett, IL (C) Q Cedar Falls, IA (E)❑ Charlotte, NC (G) Q Dayton, OH (I) Q Lumberton, NC (K) Nashville, TN (M) Q Pontiac, nil (0) ❑ Rockford. 11 (Q) (828) 254-5169 (630) 289-3100 . (319) 277-2401 (704) 392-1164 (937) 294-6856 t (910) 738-6190 (615) 726-0177 (248) 332-1940 (815) 874=2171 .Q L I Atlanta, GA (B) Q Brighton, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. IA (J) Indianapolis, IN (L) ❑ Macon, GA (N) ❑ Orlando, FL (P) 0 Watertown, WI (R) 070) 369-0636 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7944. (317) 842-4261 (912) 757-0811 (407) 851-2560 (920) 261-1660 Client: T Cu Project No.: 1.�� a] ro REQUESTED PARAMETERS Report Addre<s: Invoice Address: Is this work being conducted for regulatory compliance monitoring? Yes_ No_ inn. Attn: --� —(h,D Is this work being conducted for regulatory enforcement action? Yes_ No_ \ Phone No.:(I I- i; ( _ %7 �- _ Sampled Byit . Ur3E 1 ll C-JCl�1 Pax No.: g II' - (G) _ 2)�� P.O. No: I 7` ` l ` Which regulations apply: Quote No. TURNAROUND TIME RCRA NPDESWastewater_ — State Samples Collected —/ Ii Suutd:ud /`:� :, UST_ Drinking Water_ Other_ None- 7 Rush (surcharges may apply) Date Needed: N and tVpe of contaiComners Sample ID Date Time Crab (G) Matrix Lab Use U O q. r c REMARKS x t S-C A - LI 1 12,11 ), 17 `? QC Deliverables: None , � Lev02 Batch,QC y;. xs , ¢; Lave) 3 O I evel 4 I� Other `": ` ' .., . t, . < .. Intt Lab Temp ' Ree Lab Ten> p CONINIENTS: Relinquished B ; " "% /: / D tP�dre Received By: r Date )/ ( I ' "Tim, LAB -USE ONLY: .' %yr� , Custody, Seal' Oyes ON, ON/A Relinquished By: t, t lJ i? Date ..Time Received By: Date I Time Relinquished By: Date I Time Received By: Date Time Relinquished By: Date I Time Received By: Date I Time Bottles Supplied by TA: Yes [IN. :'/rain o •Custod Record ruirAMEHICA INU. M `} i t-ti `J y PaQe of —4 Q :Asheville, NC (A) 17 Bartlett, IL (C) Q Cedar Falls, IA (E)Q Charlotte, NC (G) Q Dayton, OH (1) Q Lumberton, NC (K) `V Nashville, TN (M) Q Pontiac, NII (0) Q Rockford. II (Q) (828)254-5169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 Q Atlanta. GA (B) Q Brighton, CO (D)Q Charleston, SC (F) Q Columbia, SC (H) Q Davenport. IA (J) Q Indianapolis, IN (L) Q Macon, GA (N) Q Orlando, FL (P) Q Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Clicnt: („ ; Project No.:07(135�REQUESTED PARAMETERS Repurt Address: Invoice Address: Is this work being conducted for regulatory r compliance monitoring? Yes_ No- Attn: M Attn: Is this work being conducted for Phone No.: Sampled By. Q -IU regulatory enforcement action? Yes_ No — Fax No.: P.O: No: Which regulations apply: NPDESWastewater_ UST_ Drinking Water_ 'TURNAROUND TIMERCRA Quote No. State Samples Collected (Standard Other_ None_ Q Rush (surcharges may apply) Date Needed: # and tvpe of containers Sample ID Dale Time Goias (G) Matrix Lab Use o i b o REMARKS tAAy (ti�}tplrJ bdgte�r,t�C r< be 3 ,t 11 I `•rr j- - t i ('AlI 1 12 ✓ 2 ', "A VJ I I I OKI✓ ' - 31Aj- NAP 4 / Z � .i"- t r IBC 77 QC Deliverables: Q None ,.Q LeVel`.2 Batch QC Q Level 3 Q [ eve14 O' Other Intt Lnb TrmP iRec Lab Tem COMMF"N'I :S: Relinquished ByIIithe Received By: ��1,� (<'r Dat��l `, `Time LAB USE ONLY — / • % Custody Seal: Yes ON, �N/A Relinquished By: at D�� ' r dime Received By: Date Time Relinyuished By: Date Time Received By: Date Time — — Relinquished By: Date I Time Received By: Date I Time Bottles Supplied by TA: Yes ONo 'hairs ufEsiAMEHICA INC. f' Crrstudy Record ' Pa et o L7 Asheville, NC(A) ❑ Bartlett, IL (C) ❑ Cedar Falls, IA (E)❑ Charlotte, NC (G) ❑ Dayton, OH (1) ❑ Lumberton, NC (K) ;)"Nashville, TN (M) ❑ Pontiac, MI (0) ❑ Rockford. 11 (Q) (828)254-5169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 1-1 Atlanta, GA (13) ❑ Brighton, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. IA (J) ❑ Indianapolis, IN (L) ❑ Macon, GA (N) ❑ Orlando, FL (P) ❑ Watertown, Wl (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407) 85 1-2560 (920)261-1660 Chem: �� � ProjectNo.: REQUESTED PARAMETERS Report Address: Invoice Address: Is this work being conducted for - regulatory compliance monitoring? Yes_ No t _ _ Ann: �L Attn: I 1 Is this work being conducted for Phone No.: Sampled By:--D. `-U(3EJ-I— r" regulatory enforcement action? Yes_ No_ Which regulations apply: RCRA— NPDESWastewater_ ) UST_ Drinking Water— Fax No.: P.O. No: ' '3 3-1 TURNAROUNDTiME Quote No. State Samples Collected (� Standard 1(/ Other_ None_ L.) Rush (surcharges may apply) Date Needed: N and type of containers Sample ID Dale Time CGra oil (G) matrix Lab Use v o z s o REMARKS m x I. C.�rho-b.r7 t'- `' I I C, Z 1 ( (1 !A N b Z I? QC peliverables:. ❑None . ❑ Level Batch QC ❑ Level 3 ❑ Leve14 ❑ Other <`°, Intt Lab Trmp.' Ric Lab Temp C'ONIMENTS: Relinquished B /; / %; �p ry J ��T' a Received By: �;',�.;f (r i -{ l / `j�� ' r Date{ ,' jl ':"Time LAB USE ONLY: ..,.. '. , .) (- ) •' �: �� CustoYc dy Seal: . �s 0No CIN/A Relinquished By: i' , j- l , `. c: l� �. ilk Date �/; .Time Received By: ` Date Time Relinquished By: Date I Time Received By: Date Time — Relinquished By: Date I Time Received By: Date I Time Bottlei Supplied by TA: Mes [IN. 7uun of y Custod Record -_r u i E H I CA .l N ■ � ) ? C- � C�' Page o ,7—• _ Asheville, NC (A) ❑ Bartlett, IL (C) Cedar Falls, IA (E)❑ ChaSlotte, NC (G) ❑ Dayton, OH (I) Q Lumberton, NC (K) Nashville, TN (M) Q Pontiac, MI (0) O Rockford. II (Q) (828) 254-5 169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874-2171 A lama, GA (13) Cl Brighton, CO (D)Q Charleston, SC (F) ❑ Columbia, SC (H) 0 Davenport. IA (J) ❑ Indianapolis, IN (L) ❑ Macon, GA (N) Q Orlando, FL (P) Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7944 (317)842-4261 (912)757-0811 (407)851-2560 (920)261-1660 Cheat: �- .) .) Project No.: REQUESTED PARAMETERS Report Address: Invoice Address: -- "I'llwork being conducted for regulatory compliance monitoring? Yes— No Attn: �•� 1 �� Attn: Is this work being conducted for regulatory enforcement action? Yes— No — - Phone No.: Sampled 13y71) _ Fax No.: P.O. No: 3 17 Which regulations apply: \RCRA NPDESWastewater — �j , UST Drinking Water- V Other None — TURNAROUND TIDIE 7 Standard Quote No. Suite Samples Collected 171 Rush (surcharges may apply) Date Needed: # and tvpe of containers Sample ID Date Time Com Grab (G) Matrix Lab Use z s o REMARKS -C.-IV, i kA ;1-W)- ' L-, i i l 1) .(ZC Deliverables: Q None 0 Level 3 COMMENTS Relinquished Bt t / ! a t %4i/ l'� e Received By: ' • p ),f� �,� t f' Date %% ! �':Time LAB USE dNLY Relinquished By: J�'FI (.(r I, „r F' 4i Date f 1`'g'ime Received By: + Date / Time f r�7 r-7 Relinquished By: _ _ Date Time Received By: Date Time Custody SealXesNo L.:..rN/A Re inquishcd By: Date I Time Received By: Date I Time Bottles Supplied by TA Mes ON. TestAmerica (��; ' fv � � � �' , R-' 017 4 40. 2960 Foster Creighton Drive •Nashville, TN 37204J�� �- 18001 765-0980 • [6151 726-0177 • Fax [6151 726-3404 Company r ��� Client Number 7�, ❑ 7 ❑ Address ❑ ❑ Co ❑ m 0 ❑ ❑ ❑ City St Zip Sampler Sign/Print °O ❑ N N o Co ❑ LL o❑ Project Name /Prof. # o 0 0 0L ❑ r W w o ❑ aLL Facility Location ( It ,SY L =° L �t N t ❑ H CD j ❑ OI ° L Project Managef � ❑❑ ° � o ` 0 ° � 0 o 'D o ❑ o a) L � ❑❑ ❑ o , PO Number I- /Fac./Site I.D. a W °° ❑� �, °° N ❑ o m Q ° o y LCI °O a ° Phone Number Fax Number E v a °O a> °U) Q W `�� og o x ,- Mr, �° ❑ o o o rn `-' o E N ° � � ° C, °C N ❑ CO o Lf)° m 'n ❑ L o m t 0 m N 0 N �O y ° � 0 .9 rn B.C. # Matrix Method Sampling �, Crin Preserved �, W 0 r M a IL a° 0 Ca 6 J❑ ❑ T _ r F— (Lab Use Only) Z ('f O_ ❑ ❑ ° °° b0 ` r= y al `° U J ,� o d 0 N N N C �n �... Field Sample P SAI Lab#LU c¢ p= pop w w w a w d x �-' O2 oI4iI v ° m LO m rn 0 of v D (Lab Use On y v¢ x 3 O U) Q —i¢ m IL r 0 U 2 z v? 2: ca Z_ V �w o� o F a t- F m a I- z F- a t- O o>> W d a4) a. -i Q Q n n (D O M> x Cm) W a dl a y a m x V F- m ¢ U. p l s-�w-gad 2 TUD St.w-k1UDP22 c v V. �ILS Gaf' I{V ZI 2 140K V11 51s cyt„J �1v�P2 2V, 1331 �S�U�-1.IV0�11 2 11� `�S-curt NVU�' Ig 1 I J � ��s��v� EIVv� ►7 � � U3� v SPECIAL DETECTION LIMITS REMARKS"' TAT / Standard L'f 3-Day ❑ 2-Day ❑ SPECIAL REPORTING REQUIREMENTS SAI PROJECT or QUOTE NUMBER Next Day ❑ (to- insure correct Analysis and Billing) Temperature Received Other: ; Airbill Number et) R evd by:Date Tirpe M ''�'V Ml�) c:l�((•� r � [.�l: ? , j jC_) CUSTODY Rel __quish�d by: f D to Ti Received by: [ Date Time RECORD Relinquished by: Date Time Received by: Laboratory Date Time TestAmerica 8B-054409 2960 Foster Creighton Drive Nashville, TN 37204 [8001765-0980 • [6151 726-0177 • Fax [615] 726-3404 Company M CmClient Number ° ❑ Address co ❑ ❑ . City St Zip Sampler Sign/Print _�f�EL d ❑❑ ° N N ° CO,Zr ° LL ❑❑ Project Name `1 �- /Prof. # 00 ❑ mt ❑ m ❑ ❑ a= Facility Location ( Ity, St) c r =o r °° ° ° ° ° ❑ < � H ° o Project Manager r%F--- F1 � ❑o 0 ` 0 ° � 'D o N ° ° o a ❑❑ o — PO Number /Fac./Site I.D. C. c CL oN oco °❑ _ ❑ ❑a ❑ wo °° o M W ° o o o Ir ° N ° = m N p a c Lq -v oo » .� ❑ ❑ Phone Number Fax Number E ° ° o❑ aa. U) a w as °� O r m C i4 I'. ca N f ° in m t❑ CO t N M� Co m C N c U) °❑ .y i; � ° o (Op B.C. # Matrix Method Sampling �, ¢ w Preserved M m ° H ❑ o w = ° ❑ a a O_ ° H o` WO m o` �,� ca J T _ _ ` (Lab Use Only) Z F-• w 2a ❑° ❑ ❑ 0_D ` r d O d C3 V J d! d m N N y ❑ C 111 Field SAI z ¢ w ¢ w w c7 ° o cc� °_ ¢a v v m m CO cv"7 = a `cc ° o 0 ° 3 a v Sample Lab# ° w a o ¢ ? o °¢ w z x ° w H 0. °a �z a =° o w d ; x x a > H m �, LU �, a a t ; o . ID (Lab Use Only) xc rn Q cn d 0 2 2 2 Z_ o_ F. to I— E t- O W d d J a a a d IL _ ~ ¢ U. f- J1 U 5B-G M 1AVOPI Z �''�li� I5� G YM S GN!-1 3v 10 1W Vv 120�i V ��S- G •NVPP � l l30 TAT SPECIAL DETECTION LIMITS REMARKS K Standard 3-Day ❑ SPECIAL REPORTING REQUIREMENTS 2-Day ❑ Next Da ❑ y SAI PROJECT or QUOTE NUMBER (to insure correct Analysis and Billing) Temperature Received Other: / Airbill Number I elinquishgd. _ p j! i//patQ� ( T� Rec@i�d, f r'i % , p to Time CUSTODY Y t.N6.Ili RECORD Reli qui ed 15y: Date Time Received by: fnafe Time Relinquished by: ate Time Received by: Laboratory . , Date Time TestAmerica N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte ------------------------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . _ Result Units Lab Number: 00-A127681 Sample ID: SLS-GW-MW1 Sample Type: Water Site ID: Date Collected: 9/ 6/00 Time Collected: 15:52 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Limit Analysis Analysis Limit Factor Date Time Analyst Method Batch ND: ug/1 1.0 1.0 1 ND, ug/l 1.0 1.0 9/10/00 ND ug/l 1 1.0 9/10/0 ND ug/1 1.0 1 1.0 9/10/0 ND ug/1 1.0 1 1 0 9/10/00 ND ug/1 1.0 1 1.0 9/10/00 ND ug/1 1.0 1 1.0 9/10/00 ND ug/1 1.0 1 1.0 9/10/00 ND ug/1 1 0 1 1.0 9/10/00 ND ug/1 1 1.0 9/10/00 ND ug/1 1.0 1 1 0 9/10/00 ND ug/l 1 0 1 1.0 9/10/00 ND ug/l 1 1.0 9/10/00 ND ug/1 1.0 1 1.0 9/10/00 ND ug/l 1.0 1 1.0 9/10/00 ND ug/1 1.0 1 1 0 9/10/00 ND ug/l 1.0 1 1.0 9/10/00 ND ug/l 1.0 1 1'0 9/10/00 ND ug/l 1.0 1 1.0 9/10/00 ND ug/1 1 1.0 9/10/00 ND ug/1 1.0 1 0 i 9/10/00 ND ug/1 1.0 1.0 9/10/00 ND ug/1 1.0 1 1.0 9/10/00 1 9/10/00 3:46 M.Himelick 602/601 0 3:46 M.Himelick 602/601 0 3:46 M.Himelick 602/601 3:46 M.Himelick 602/601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3:46 M.Himelick 601 3756 3756 3756. 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 3756 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-09 4 i unn 7a- Test = merica I N C O R P O R A T E D i ANALYTICAL REPORT Analyse ------------------------ Result Units trans-1,3-Dichloropropene ----------- ND _ Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ug/1 Tetrachloroethene ND ug/1 -_ 1,1,1-Trichloroethane 2240 ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethee ND ug/1 Trichlorofluoromethane 3.1 ug/1 ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127681 Sample ID: SLS-GW-MW1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method -------- Batch 1.0 5.0 1.0 1 9/10/00 ----- 3:46 ---------- M.Himelick 601. ___ 3756 1.0 5,0 1 9/10/00 3:46 M.Himelick 601 3756 50.0 1.0 1,0 1 9/10/00 3:46 M.Himelick 601 3756 1.0 1,0 50 9/14/00 9:42 M.Himelick 601 3756 1.0 1.0 1 9/10/00 3:46 M.Himelick 601 3756 1.0 1,0 1 9/10/00 3:46 M.Himelick 601 3756 1.0 1.0 1 9/10/00 3:46 M.Himelick 601 3756 1 9/10/00 3:46 M.Himelick 601 3756 Recovery Target Range ------------------ PID Surr., a,a,a-trifluorotoluene Hall Surr., 2-chloropropane 105 84 Hall Surr., chloroprene Hall Surr., 78 1-chloro-3-fluorobenzene # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F:1.C: 615-726-0954 / g00-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127681 Sample ID: SLS-GW-MW1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: U.,, A !� vy6A,-Ahl- Report Date: 9/19/00 i Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127690 Sample ID: SLS-GW-MW2 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 16:05 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND: ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 602/601 3756 . Bromodichloromethane ND _ ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756. Bromoform ND ug/1 10.0 2.0 10 9/14/00 19:32 M.Himelick 601 3756 . Bromomethane ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Carbon tetrachloride ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Chloroethane ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/l. 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Chloroform ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Chloromethane ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Dibromochloromethane ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Ethylene Dibromide ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Vinyl chloride ND ug/l 10.0 1.0, 10 9/14/00 19:32 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 1,1-Dichloroethene ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 1,2-Dichloropropane ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 -- Sample report continued . . . i 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-72'6=01'77-/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I NCORPO RATED ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 72.0 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND. ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127690 Sample ID: SLS-GW-MW2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 10.0 ------- 1.0 ------ 10 -------- 9/14/00 ----- 19:32 ---------- M.Himelick --------- 601 ----- 3756 50.0 5.0 10 9/14/00 19:32 M.Himelick 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick. 601 3756 10.0 1.0 10 9/14/00 19:32 M.Himelick 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 106. Hall Surr., 2-chloropropane 97. Hall Surr., chloroprene 90. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. F Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127690 Sample ID: SLS-GW-MW2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Q,, W -4- K-kLuV Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical. Serv. Johnny A. Mitchell,.Dir. Technical Serv., Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director - Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. i j 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-72'6-01'77'/ FAX: 615-726-0954 / 800-765-0980 Test _ merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Lab Number: 00-A127713 Sample ID: SLS-GW-— MW3 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Project: 107535 Time Collected: 11:10 Project Name: Date Received: 9/ 9/00 Sampler: D.LUBELL/K.SUMNER Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result -- —------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* - Benzene ND. ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602 3759 Chlorobenzene ND-' ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602/601 3759 1,2-Dichlorobenzene ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602/601 3759 1,4-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 19:51 M.Himelick 602/601 3759: Ethylbenzene ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602 3759 Toluene ND ug/1 5000 1.0 5000 9/15/00 19:51 M.Himelick 602 3759 m,p-Xylenes ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602 3759 o-Xylene ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 602 3759 Bromodichloromethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Bromoform ND ug/l 5000 2.0 5000 9/15/00 19:51 M.Himelick 601 3759 Bromomethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Carbon tetrachloride ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Chloroethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 2-Chloroethylvinylether ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Chloroform ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick _601 3759 Chloromethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Dibromochloromethane ND ug/1 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Vinyl chloride ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 1,1-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 1,2-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 19:51 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca ANALYTICAL REPORT Laboratory Number: 00-A127713 Sample ID: SLS-GW-MW6 MIJ-3 Page 2 Report Quan Dil Analyte ------------------------- Result Units Limit Limit Factor 1,1-Dichloroethene ---=------- ND ------ ug/1 ------ 5000 ------- 1.0 ------ 5000 cis-1,2-Dichloroethene ND ug/l 5000 1.0 5000 trans-1,2-Dichloroethene ND ug/l 5000 1.0 5000 1,2-Dichloropropane ND ug/l 5000 1.0 5000 cis-1,3-Dichloropropene ND ug/l 5000 1..0 5000 trans-1,3-Dichloropropene ND ug/l 5000 1.0 5000 Methylene chloride ND ug/1 25000 5.0 5000 1,1,2,2-Tetrachloroethane ND ug/1 5000 1.0 5000 Tetrachloroethene 154000 ug/l 5000 1.0 5000 1,1,1-Trichloroethane ND ug/1 5000 1.0 5000 1,1,2-Trichloroethane ND ug/1 5000 1.0 5000 Trichloroethene ND ug/l 5000 1.0 5000 Trichlorofluoromethane ND": ug/1 5000 1.0 5000 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 98. Hall Surr., 2-chloropropane 67. Hall Surr., chloroprene 93. Hall Surr., 1-chloro-3-fluorobenzene 85. # - Recovery outside Laboratory historical limits. Sample report continued . . . Analysis Analysis Date Time Analyst Method Batch -------- 9/15/00 ----- 19:51 ---------- M.Himelick --------- 601 ----- 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 9/15/00 19:51 M.Himelick 601 3759 Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127713 Sample ID: SLS-GW-MW6 Mw-3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: -:Vm-�Lk� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 - End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica 1 N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromome thane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Sample report continued . . . Lab Number: 00-A131753 Sample ID: SLS-GW-MW3 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 10:00 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602 9808 ND" ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602/601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602/601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602/601 9808 Na: ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602/601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 602 9808 ND ug/1 10000 1.0 10000 9/21/00 14:30 M.Himelick 602 9808 ND ug/1 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/1 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/1 10000 1.0 10000 9/21/00 14:30 M.Himelick 601, 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/1 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 ND ug/l 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ cis-1,3-Dichloropropene ----------- ND ------- ug/1 trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 130000 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131753 Sample ID: SLS-GW-MW3 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10000 ------ 1.0 ------ 10000 -------- 9/21/00 ------ 14:30 ----------- M.Himelick --------- 601 ----- 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 50000 5.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 10000 1.0 10000 9/21/00 14:30 M.Himelick 601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 80. Hall Surr., chloroprene 91. Hall Surr., 1-chloro-3-fluorobenzene 108. # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F.Ax: 615-726-0954 / 800-765-0980 Testlmerica ANALYTICAL REPORT Laboratory Number: 00-A131753 Sample ID: SLS-GW-MW3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report. Approved By: C gaziAlyi w Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Test merica I N C O R P O RAT E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 �KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Lab Number: 00-A127702 Sample ID: SLS-GW-MW4 Sample Type: Water Site ID: -' Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Date Time Date Time Collected: Collected: Received: Received: 9/ 7/00 17:30 9/ 9/00 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 602 3758 Chlorobenzene I ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 1000 1.0 1000 ,9/15/00 2:49 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 602/601 3758 . 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 602/601 3758. Ethylbenzene ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 602 3738 . Toluene ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 602 3758 m,p-Xylenes ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 602 3758 o-Xylene ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 602 3758 Bromodichloromethane ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Bromoform ND ug/1 1000 2.0 1000 9/15/00 2:49 M.Himelick 601 3758 Bromomethane ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Chloroethane ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Chloroform ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Chloromethane ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Dibromochloromethane ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Vinyl chloride ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / F:ax: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units 1,1-Dichloroethene ND ug/1 cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene ND ug/l 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 41200 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127702 Sample ID: SLS-GW-MW4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 9/15/00 ----- 2:49 ---------- M.Himelick --------- 601 ----- 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 5000 5.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 1000 1.0 1000 9/15/00 2:49 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 106. Hall Surr., 2-chloropropane 66. Hall Surr., chloroprene 63. Hall Surr., 1-chloro-3-fluorobenzene 111. # - Recovery outside Laboratory historical limits. - Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testlimerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127702 Sample ID: SLS-GW-MW4 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (gAejA/ 7;- Jt -. Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S.., Technical Director Glenn L. Norton,,Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 - End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testlimerica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler:.D.LUBELL/K.SUMNER I N C O R P O R A T E D Lab Number: 00-A127692 Sample ID: SLS-GW-MW5 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 11:44 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- ------ -------- ------------------------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ugA 100. 1.0 100 9/14/00 18:48 M.Himelick 602/601 3758 . Bromodichloromethane ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758: Bromoform ND ug/1 100. 2.0 100 9/14/00 18:48 M.Himelick 601 3758 . Bromomethane ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Carbon tetrachloride ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Chloroethane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Chloroform ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Chloromethane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Dibromochloromethane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Vinyl chloride ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 1,2-Dichloroethane ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 cis-1,2-Dichloroethene ND ug/1 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 1,2-Dichloropropane ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 -- Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 6, TestL-�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 5880 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND.- Not detected at the report limit. Laboratory Number: 00-A127692 Sample ID: SLS-GW-MWS Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 100. ------- 1.0 ------ 100 -------- 9/14/00 ----- 18:48 ---------- M.Himelick --------- 601 ----- 3758 500. 5.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 100. 1.0 100 9/14/00 18:48 M.Himelick 601 3758 Surrogate ------------- % Recovery ---------- PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 65. Hall Surr., chloroprene 65. " Hall Surr., 1-chloro-3-fluorobenzene 110. # — Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127692 Sample ID: SLS-GW-MW5 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: -'g Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/19/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestL�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER I N C O R P O R A T E D Lab Number: 00-A127691 Sample ID: SLS-GW-MW6 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 10:56 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND. ug/l 50.0 1.0 50, 9/14/00 20:14 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND' ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 602/601 3756 Bromodichloromethane ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756: Bromoform ND ug/1 50.0 2.0 50 9/14/00 20:14 M.Himelick 601 3756 Bromomethane ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Chloroethane ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Chloroform ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Chloromethane ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Dibromochloromethane ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Vinyl chloride ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 1,1-Dichloroethane ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 1,1-Dichloroethene 445. ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/14/00 20.14 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 1,2-Dichloropropane ND ug/1 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 125. ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127691 Sample ID: SLS-GW-MW6 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time ------ Analyst Method Batch ------ 50.0 ------- 1.0 ------ 50 -------- 9/14/00 20:14 ---------- M.Himelick --------- 601 ----- 3756 250. 5.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 50 9/14/00 20:14 M.Himelick 601 3756 50.0 1.0 . 50 9/14/00 20:14 M.Himelick' 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 106. Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 88. Hall Surr., 1-chloro-3-fluorobenzene 107. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 i Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127691 Sample ID: SLS-GW-MW6 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. a Report Approved By: t,:v�nA,� hl,ut�t, Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A.,,Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F.Ax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane i 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127704 Sample ID: SLS-GW-MW7 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 8:30 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ ------- -------------- ------------------------ ----- ND: ug/l 5.0 1.0 5 9/15/00 4:17 M.Hidelick 602/601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 602/601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 602/601 3758 ND ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 602/601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758_ ND ug/1 5.0 2.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 166. ug/1 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick_ 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 ND ug/l 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 17.5 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND. ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127704 Sample ID: SLS-GW-MW7 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 5.0 ------- 1.0 ------ 5 -------- 9/15/00 ----- 4:17 ---------- M.Himelick --------- 601 ----- 3758 25.0 5.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 5.0 1.0 5 9/15/00 4:17 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 104. Hall Surr., 2-chloropropane 53. Hall Surr., chloroprene 64. Hall Surr., 1-chloro-3-fluorobenzene 72. # - Recovery outside Laboratory historical limits. Sample report continued . . . i Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�meri I ca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127704 Sample ID: SLS-GW-MW7 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: sQ-`.yl I-LA)L/ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica ! I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127683 Sample ID: SLS-GW-MW8 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 10:05 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- ND:. ug/1 1.0 1.0 1 9/15/00 12i48 M.Himelick 602/601 3756 ND'. ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 602/601 3756 ND ug/1 1.0 1.0 1 9/15/.00 12:48 M;Himelick 602/601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 602/601 3756 " ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756. ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3736 . ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 . 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND tig/l 1.0 1.0 1 9/15/00 12:48 M.Himelick 601' 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 ND, ug/1 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene ND ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND. ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127683 Sample ID: SLS-GW-MW8 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1.0 ------- 1.0 ------ 1 -------- 9/15/00 ----- 12:48 ---------- M.Himelick --------- 601 ----- 3756 5.0 5.0 1 9/15/00 12:48 M.Himelick 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick. 601 3756 1.0 1.0 1 9/15/00 12:48 M.Himelick 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 106. Hall Surr., 2-chloropropane 103. Hall Surr., chloroprene 100. Hall Surr., 1-chloro-3-fluorobenzene 122. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726'-0177 / FAX: 615-726-0954 / 800-765-0980 Testl_ merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127683 Sample ID: SLS-GW-MW8 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: 64,4 ►mot 13- tylReport Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131771 KIM TITMUS Sample ID: SLS-GW-MW9 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/12/00 Project: 107535 Time Collected: 17:03 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:0.0 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- - --------'---- ------ -------------- ----------------- --------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 602/601 9809 Bromodichloromethane ND- ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Bromoform ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Bromomethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Chloroethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Chloroform ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Chloromethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/23/00' 23:57 M.Himelick 601 9809 Vinyl chloride ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Methylene chloride ND ug/1 5.0 5.0 1 9/23/00 23:57 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Tetrachloroethene ND ug/l 1.0 1.0 1 9/23/00 23.57 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131771 Sample ID: SLS-GW-MW9 Page 2 Report Quan Dil Analysis Analysis Analyte, Result ------------------------ Units Limit Limit Factor Date Time Analyst Method Batch ----------- 1,1,1-Trichloroethane ND ------- ug/1 ------- 1.0 ------ 1.0 ------ 1 -------- 9/23/00 ------ 23:57 ----------- M.Himelick --------- 601 ----- 9809 1,1,2-Trichloroethane ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Trichloroethene ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 Trichlorofluoromethane ND ug/1 1.0 1.0 1 9/23/00 23:57 M.Himelick 601 9809 ND - Not detected at the report limit. Surrogate ------------- % ---------- Recovery Target ------------ Range 1 PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 77. 49. - 125. Hall Surr., chloroprene 74. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 91. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. I Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177-/ FAx: 615-726-0954 / 800-765-0980 Testmerieca I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131751 ICIM TITMUS Sample ID: SLS-GW-MW10 2200 GATEWAY CTR.'BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/14/00 Project: 107535 Time Collected: 8:15 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ ------------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND. ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Bromoform ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Bromomethane ND ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Chloroethane ND ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Chloroform ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Chloromethane ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Dibromochloromethane ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Vinyl chloride ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/21/00 13.08 M.Himelick 601 9808 1,2-Dichloroethane ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 1,1-Dichloroethene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/1 500.' 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Methylene chloride ND ug/1 2500 5.0 500 9/21/00 13:08 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Tetrachloroethene 6900 ug/l 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726'-0177 / FAX: 615-726-0954 / 800-765-0980 Analyte ------------------------ 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane a' Testl-�merica I NCO RPORATED ANALYTICAL REPORT Result Units ND ug/l ND ug/1 ND ug/1 ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131751 Sample ID: SLS-GW-MW10 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 500. ------ 1.0 ------ 500 -------- 9/21/00 ------ 13:08 ----------- M.Himelick --------- 601 ----- 9808 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 500. 1.0 500 9/21/00 13:08- M.Himelick 601 9808 500. 1.0 500 9/21/00 13:08 M.Himelick 601 9808 Recovery PID Surr., a,a,a-trifluorotoluene 108. Hall Surr., 2-chloropropane 86. Hall Surr.;'chloroprene 89. Hall Surr.,'l-chloro-3-fluorobenzene 104. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: arl QReport Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director .,Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177 / F:Ax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131758 KIM TITMUS Sample ID: SLS-GW-MW11 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/14/00 Project: 107535 Time Collected: 10:05 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Bromoform ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Bromomethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Chloroethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Chloroform ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Chloromethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Dibromochloromethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Vinyl chloride ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Methylene chloride ND ug/l 5.0 5.0 1 9/21/00 15:52 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Tetrachloroethene ND ug/1 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726' 0177 "/ FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131758 Sample ID: SLS-GW-MW11 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit Factor Date Time Analyst Method Batch 1.0 ------ 1.0 ------ 1 -------- 9/21/00 ------ 15:52 ----------- M.Himelick --------- 601 ----- 9808 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 1.0 1.0 1 9/21/00 15:52 M.Himelick 601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 85. Hall Surr., chloroprene 100. Hall Surr., 1-chloro-3-fluorobenzene 87. # — Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This 'report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177-/ Fax: 615-726-0954 / 800-765-0980 Testl�merica. I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131739 Sample ID: SLS-GW-MW12 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 15:45 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- ------ -------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 602/601 9805 Bromodichloromethane ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Bromoform ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Bromomethane ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Chloroethane ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Chloroform ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Chloromethane ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Dibromochloromethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Vinyl chloride ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 1,2-Dichloropropane 277. ug/l 10.0 .1.0 10 9/21/00 11:17 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Methylene chloride ND ug/1 50.0 5.0 10 9/21/00 11:17 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Tetrachloroethene ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131739 Sample ID: SLS-GW-MW12 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1,1-Trichloroethane ----------- ND ------- ug/1 ------- 10.0 ------ 1.0 ------ 10 -------- 9/21/00 ------ 11:17 ----------- M.Himelick --------- 601 ----- 9805 1,1,2-Trichloroethane ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Trichloroethene ND ug/l 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 Trichlorofluoromethane ND ug/1 10.0 1.0 10 9/21/00 11:17 M.Himelick 601 9805 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 109. Hall Surr., chloroprene 97. Hall Surr., 1-chloro-3-fluorobenzene 98. A - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved., By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177"/ FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131768 KIM TITMUS Sample ID: SLS-GW-MW13 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 10:00 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- --- -- -------------- ------ -------------------- ----- *VOLATILE ORGANICS by GC* - Chlorobenzene ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Bromoform ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Bromomethane ND ug/1 1.0 1•.0 1 9/22/00 6:13 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Chloroethane ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808' 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Chloroform ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Chloromethane ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Dibromochloromethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Vinyl chloride ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Methylene chloride ND ug/1 5.0 5.0 1 9/22/00 6:13 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Tetrachloroethene 35.8 ug/l 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177" / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 6.2 ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Laboratory Number: 00-A131768 Sample ID: SLS-GW-MW13 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/22/00 ------ 6:13 ----------- M.Himelick --------- 601 ----- 9808 1.0 1.0 1 9/22/00 6:13 M.Himelick' 601 9808 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 1.0 1.0 1 9/22/00 6:13 M.Himelick 601 9808 Surrogate % Recovery ------------- ---------- PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 80. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 112. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 ICIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131767 Sample ID: SLS-GW-MW14 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 11:05 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 602/601 9808 Bromodichloromethane ND' ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Bromoform ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Bromomethane ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Chloroethane ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Chloroform ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Chloromethane ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Dibromochloromethane ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Vinyl chloride ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1,1-Dichloroethane ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 5.31 M.Himelick 601 9808 Methylene chloride ND ug/l 5.0 5.0 1 9/22/00 5:31 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1,0 1 9/22/00 5:31 M.Himelick 601 9808 Tetrachloroethene 1.8 ug/l 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177 / FAX: 615-726-0954 / 800-765-0980 i Test merica I N C O R P O R A T E D I ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane NDug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131767 Sample ID: SLS-GW-MW14 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit Factor Date Time Analyst Method Batch 1.0 ------ 1.0 ------ 1 -------- 9/22/00 ------ 5:31 ----------- M.Himelick --------- 601 ----- 9808 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 1.0 1.0 1 9/22/00 5:31 M.Himelick 601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. 50. - 150. Hall Surr., 2-chloropropane 89. 49. - 125. Hall Surr., chloroprene 82. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 96. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: C �C�A 2Dz2 G Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Test�merica I N C O R P O R A T E D ANALYTICAL REPORT. IT CORP-SEARS 2338 Lab Number: 00-A131749 KIM TITMUS Sample ID: SLS-GW-MW15 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 17:20 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND, ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND. ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 602/601 9805 Bromodichloromethane ND' ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Bromoform ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Bromomethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 10.0 1.0 10 9/21/00 19:03 'M.Himelick 601 9805 Chloroethane ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Chloroform 22.0 ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Chloromethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Dibromochloromethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Vinyl chloride ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 cis-1,2-Dichloroethene 19.0 ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Methylene chloride ND ug/l 50.0 5.0 10 9/21/00 19:03 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Tetrachloroethene 40.0 ug/1 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726'-0177'/ FAX: 615-726-0954 / 800-765-0980 Testj�merica I NCO RPO,RATED ANALYTICAL REPORT Laboratory Number: 00-A131749 Sample ID: SLS-GW-MW15 Page 2 Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 538. ug/l Trichlorofluoromethane ND ug/1 ND -• Not detected at the report limit. Report' Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10.0 ------ 1.0 ------ 10 -------- 9/21/00 ------ 19:03 ----------- M.Himelick --------- 601 ----- 9805 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 10.0 1.0 10 9/21/00 19:03 M.Himelick 601 9805 Surrogate % Recovery Target Range I _ PID Surr., a,a,a-trifluorotoluene 103. 50. - 150. Hall Surr., 2-chloropropane 94. 49. - 125. Hall Surr., chloroprene 89. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 96. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131770 KIM TITMUS Sample ID: SLS-GW-MW17 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 8:12 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte --------------- ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 602/601 9808 Bromodichloromethane ND. ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Bromoform ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Bromomethane ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Chloroethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Chloroform ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Chloromethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Dibromochlo=omethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Vinyl chloride ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 1,1-Dichloroethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 I 1,2-Dichloropropane ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Methylene chloride ND ug/1 500. 5.0 100 9/22/00 9:01 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/1 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Tetrachloroethene 4090 ug/l 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 1150 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A131770 Sample ID: SLS-GW-MW17 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 100. ------ 1.0 ------ 100 -------- 9/22/00 ------ 9:01 ----------- M.Himelick --------- 601 ----- 9808 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 100. 1.0 100 9/22/00 9:01 M.Himelick 601 9808 100. 1.0 100 9/22/00 9:01 M.Himelick 601 '9808 Surrogate ------------- % Recovery ---------- Target ------------ Range PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 83. 49. - 125. Hall Surr., chloroprene 81. 49. -'142. Hall Surr., 1-chloro-3-fluorobenzene 115. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: C CIAO pal Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director IGail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L.' Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVH.LE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131766 Sample ID: SLS-GW-MW18 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 11:45 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 100. 1.0 100 9/22/00 4:49 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 100. 1.0 100 9/22/00 4:49 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Bromoform ND ug/1 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Bromomethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Chloroethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Chloroform ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Chloromethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Dibromochloromethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Vinyl chloride ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 --- Methylene chloride ND ug/l 500. 5.0 100 9/22/00 4:49 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Tetrachloroethene 1940 ug/1 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane - ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 830. ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A131766 Sample ID: SLS-GW-MW18 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit ------ Factor Date Time Analyst Method Batch 100. 1.0 ------ 100 -------- 9/22/00 ------ 4:49 ----------- M.Himelick --------- 601 ----- 9808 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 100. 1.0 100 9/22/00 4:49 M.Himelick 601 9808 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 83. Hall Surr., chloroprene 86. Hall Surr., 1-chloro-3-fluorobenzene 105. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except'in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly-S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131764 Sample ID: SLS-GW-MW20 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 14:40 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ------------------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Bromoform ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Bromomethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Chloroethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Chloroform ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Chloromethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Dibromochloromethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Vinyl chloride ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1,2-Dichloroethane ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Methylene chloride ND ug/l 5.0 5.0 1 9/22/00 3:26 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Tetrachloroethene 9.0 ug/l 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testlimerica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichlorroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A131764 Sample ID: SLS-GW-MW20 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/22/00 ------ 3:26 ----------- M.Himelick --------- 601 ----- 9808 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 1.0 1.0 1 9/22/00 3:26 M.Himelick 601 9808 Surrogate % Recovery ------------- ---------- PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 83. Hall Surr., 1-chloro-3-fluorobenzene 106. # - Recovery outside Laboratory historical limits. Target Range------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: PL;A (A (A C4 Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131765 Sample ID: SLS-GW-MW21 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 12:45 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- -------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 10.0 1,2-Dichlorobenzene ND' ug/l 10.0 1,3-Dichlorobenzene ND. ug/l 10.0 1,4-Dichlorobenzene ND: ug/l 10.0 Bromodichloromethane ND, ug/1 10.0 Bromoform ND ug/1 10.0 Bromomethane ND ug/l 10.0 Carbon tetrachloride ND ug/1 10.0 Chloroethane ND ug/1 10.0 2-Chloroethylvinylether ND ug/1 10.0 Chloroform ND ug/l 10.0 Chloromethane ND ug/l 10.0 Dibromochloromethane ND ug/l 10.0 Ethylene Dibromide ND ug/l 10.0 Vinyl chloride ND ug/l 10.0 Dichlorodifluoromethane ND ug/l 10.0 1,1-Dichloroethane ND ug/l 10.0 1,2-Dichloroethane ND ug/1 10.0 1,1-Dichloroethene ND ug/1 10.0 cis-1,2-Dichloroethene ND ug/l 10.0 trans-1,2-Dichloroethene ND ug/1 10.0 1,2-Dichloropropane ND ug/1 10.0 cis-1,3-Dichloropropene ND ug/l 10.0 trans-1,3-Dichloropropene ND ug/l 10.0 - Methylene chloride ND ug/1 50.0 1,1,2,2-Tetrachloroethane ND ug/1 10.0 Tetrachloroethene 289. ug/l 10.0 Sample report continued 1.0 10 9/22/00 4:08 M.Himelick 602/601 9808 1.0 10 9/22/00 4:08 M.Himelick 602/601 9808 1.0 10 9/22/00 4:08 M.Himelick 602/601 9808 1.0 10 9/22/00 4:08 M.Himelick 602/601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 .10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 5.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 1.0 10 9/22/00 4:08 M.Himelick 601 9808 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I NCO RPORATED ANALYTICAL REPORT Analyte Result . Units 1,1,1-Trichloroethane ND ug/1 1;1,2-Trichlor6ethane ND ug/l Trichloroethene 46.0 ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131765 Sample ID: SLS-GW-MW21 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit: Factor Date Time Analyst Method Batch 10.0 ------ 1.0 ------ 10 -------- 9/22/00 ------ 4:08 ----------- M.Himelick --------- 601 ----- 9808 10.0 1.0 10 9/22/00 4':'08 M.Himelick 601 9808 10.0 1.0 10 9/22/00 4:08 M.Himelick 601 9808 10.0 1.0 10 9/22/00 4:08 M.Himelick 601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 92. 49. - 125. Hall Surr., chloroprene 85. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 108. 25. - 1.57. # — Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (M A Q (-,tbiynCal Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 % FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131742 ICIM TITMUS Sample ID: SLS-GW-MW22 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 9:40 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/21/00 13:23 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 602/601 9805 Bromodichloromethane ND. ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Bromoform ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick. 601 9805 Bromomethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Chloroethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Chloroform ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Chloromethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Dibromochloromethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Vinyl chloride ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Methylene chloride ND ug/l 250. 5.0 50 9/21/00 13:23 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Tetrachloroethene 1720 ug/l 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 195. ug/l Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131742 Sample.ID: SLS-GW-MW22 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit Factor Date Time Analyst Method Batch 50.0' ------ 1.0 ------ 50 -------- 9/21/00 ------ 13:23 ----------- M.Himelick --------- 601 ----- 9805 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 50.0 1.0 50 9/21/00 13:23 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 93. Hall Surr., chloroprene 96. Hall Surr., 1-chloro-3-fluorobenzene 120. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177 / F.ax: 615-726-0954 / 800-765-0980 Testlimerica I N C 0 R P 0 R A T E 0 ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . . . Lab Number: 00-A131746 Sample ID: SLS-GW-MW23 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 14:45 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 602/601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 602/601 9805 ND. ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 602/601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 602/601 9805 ND ug/l 1:0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/1 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 5.0 5.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 ND ug/l 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merioca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131746 Sample ID: SLS-GW-MW23 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time ------ Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 '11:12 ----------- M.Himelick --------- 601 ----- 9805 1.0 1.0 1 -9/24/00 '11:12 M.Himelick 601 9805 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 1.0 1.0 1 9/24/00 11:12 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 102 Hall Surr., 2-chloropropane 77. Hall Surr., chloroprene 72. Hall Surr., 1-chloro-3-fluorobenzene 79. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: claa CAReport Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M:S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL STE205 Lab Number: 00-A131757 Sample ID: SLS-GW-MW27 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 12:01 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 602/601 .9808 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Bromoform ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Bromomethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick- 601 9808 Carbon tetrachloride ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Chloroethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 2-Chloroethylvinylether-: ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Chloroform ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Chloromethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Dibromochloromethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Vinyl chloride ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 cis-1,2-Dichloroethene 2300 ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 1,2-Dichloropropane ND ug/1 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Methylene chloride ND ug/1 250. 5.0 50 9/22/00 11:07 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Tetrachloroethene 85.0 ug/l 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • Testi-imerica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ �, 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene , 4680 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A131757 Sample ID: SLS-GW-MW27 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 11:07 ----------- M.Himelick --------- 601 ----- 9808 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 50.0 1.0 50 9/22/00 11:07 M.Himelick 601 9808 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 105. Hall Surr., 2-chloropropane 90. Hall Surr., chloroprene 82. Hall Surr., 1-chloro-3-fluorobenzene 102'. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142, 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: kL,-j a-gc(VA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. it 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131756 Sample ID: SLS-GW-MW28 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 12:15 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- --------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1,2-Dichlorobenzene ND ug/l 10.0 _ 1,3-Dichlorobenzene ND ug/l 10.0 1,4-Dichlorobenzene ND ug/l 10.0 Bromodichloromethane ND ug/l 10.0 Bromoform ND ug/1 10.0 Bromomethane ND ug/l 10.0 Carbon tetrachloride ND ug/l 10.0 Chloroethane ND ug/l 10.0 2-Chloroethylvinylether ND ug/l 10.0 Chloroform 10.0 ug/l 10.0 Chloromethane ND ug/1 10.0 Dibromochloromethane ND ug/1 10.0 Ethylene Dibromide ND ug/1 10.0 Vinyl chloride ND ug/1 10.0 Dichlorodifluoromethane ND ug/l 10.0 1,1-Dichloroethane ND ug/1 10.0 1,2-Dichloroethane I ND ug/1 10.0 1,1-Dichloroethene ND ug/1 10.0 cis-1,2-Dichloroethene 385. ug/1 10.0 trans-1,2-Dichloroethene ND ug/1 10.0 1,2-Dichloropropane ND ug/1 10.0 cis-1,3-Dichloropropene ND ug/1 10.0 trans-1,3-Dichloropropene ND ug/1 10.0 Methylene chloride ND ug/l 50.0 1,1,2,2-Tetrachloroethane ND ug/l 10.0 Tetrachloroethene ND ug/l 10.0 Sample report continued . . . 1.0 10 9/21/00 15:11 M.Himelick 602/601 9808 1.0 10 9/21/00 15:11 M.Himelick 602/601 9808 1.0 10 9/21/00 15:11 M.Himelick 602/601 9808 1.0 10 9/21/00 15:11 M.Himelick 602/601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 5.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 1.0 10 9/21/00 15:11 M.Himelick 601 9808 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene '178. ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131756 Sample ID: SLS-GW-MW28 Page 2 Report Quan Dil Analysis Analysis Limit ------- Limit ------ Factor Date Time Analyst Method Batch 10.0 1.0 ------ 10 -------- 9/21/00 ------ 15:11 ----------- M.Himelick --------- 601 ----- 9808 10.0 1.0 10 9/21/00 15:11 M.Himelick 601 9808 10.0 1.0 10 9/21/00 15:11 M.Himelick 601 9808 10.0 1.0 10 9/21/00 15:11 M.Himelick 601 9808 Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 86. - Hall Surr., chloroprene 83. Hall Surr., 1-chloro-3-fluorobenzene 94. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ( Qto' - (KAI C, Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv: Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 'I Project Name: Sampler: D. LUBELL Lab Number: 00-A131759 Sample ID: SLS-GW-LMP1 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 9:30 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Bromoform ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Bromomethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Chloroethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Chloroform ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Chloromethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Dibromochloromethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808. Vinyl chloride ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 1,1-Dichloroethane ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 1,2-Dichloropropane 1370 ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Methylene chloride ND ug/l 100. 5.0 20 9/21/00 16:33 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Tetrachloroethene 586. ug/1 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F.ax: 615-726-0954 / 800-765-0980 T.estl�merica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 120. ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131759 Sample ID: SLS-GW-LMP1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 20.0 ------ 1.0 ------ 20 -------- 9/21/00 ------ 16:33 ----------- M.Himelick --------- 601 ----- 9808 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 20.0 1.0 20 9/21/00 16:33 M.Himelick 601 9808 20.0 1.0 20 9/21/00 16:33 M.Himelick .601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-6hloropropane 85. Hall Surr., chloroprene 85. ,Hall Surr., 1-chloro-3-fluorobenzene 87. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage; Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica [NCO RPO RATED ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131760 ICIM TITMUS Sample ID: SLS-GW-LMP2 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/14/00 Project: 107535 Time Collected: 8:20 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Bromoform ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Bromomethane ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Chloroethane ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Chloroform ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Chloromethane ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Dibromochloromethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Ethylene Dibromide ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Vinyl chloride ND ug/1 5.0 1.0 5 9/21/00. 17:14 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 1,1-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 1,2-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 1,1-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 cis-1,2-Dichloroethene 7.0 ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 5.0 1.0 5 9/21/00 17:14. M.Himelick 601 9808 1,2-Dichloropropane 292. ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Methylene chloride ND ug/l 25.0 5.0 5 9/21/00 17:14 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Tetrachloroethene 65.5 ug/1 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 26.5 ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131760 Sample ID: SLS-GW-LMP2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 5.0 ------ 1.0 ------ 5 -------- 9/21/00 ------ 17:14 ----------- M.Himelick ---------" 601 ----- 9808 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 5.0 1.0 5 9/21/00 17:14 - M.Himelick 601 9808 5.0 1.0 5 9/21/00 17:14 M.Himelick 601 9808 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 84. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 109. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 Ft A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane I Sample report continued . . . Lab Number: 00-A131733 Sample ID: SLS-GW-PT1S Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 9:35 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602/601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 602/601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 602/601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602/601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602. 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 602 9805' ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1" 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/l 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 ND ug/1 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test).�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 2770 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131733 Sample ID: SLS-GW-PT1S Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 100. ------ 1.0 ------ 100 -------- 9/21/00 ------ 6:22 ----------- M.Himelick --------- 601 ----- 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 500. 5.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 100. 1.0 100 9/21/00 6:22 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 102 Hall Surr., 2-chloropropane 92. Hall Surr., chloroprene 85. Hall Surr., 1-chloro-3-fluorobenzene 116 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ Fa: 615-726-0954 / 800-765-0980 Test merica I N C O RPO RATED ANALYTICAL REPORT Laboratory Number-: 00-A131733 Sample ID: SLS-GW-PT1S Page 3 These results.relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: v n ig(Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131734 KIM TITMUS Sample ID: SLS-GW-PT3S 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/12/00 Project: 107535 Time Collected: 10:35 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 200.. 1.0 200 9/21/00 7:05 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 602/601 9805 Bromodichloromethane ND. ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Bromoform ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Bromomethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Chloroethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Chloroform ND ug/1 200. 1.0 , 200 9/21/00 7:05 M.Himelick 601 9805 Chloromethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Dibromochloromethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Vinyl chloride ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 1,1-Dichloroethene ND ug/1 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/1 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/1 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Methylene chloride ND ug/l 1000 5.0 200 9/21/00 7:05 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Tetrachloroethene 2520 ug/1 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerieca I N C 0 R P 0 R A T E 0 ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene 1140 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131734 Sample ID: SLS-GW-PT3S Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 200. ------ 1.0 ------ 200 -------- 9/21/00 ------ 7:05 ----------- M.Himelick --------- 601 ----- 9805 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 200. 1.0 200 9/21/00 7:05 M.Himelick 601 9805 200. 1.0 200 9/21/00 7:05 M.Himelick 601• 9805 Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 96. Hall Surr., chloroprene 98. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- Lab Number: 00-A131736 Sample ID: SLS-GW-PT4S Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 11:00 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date _ Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 602/601 9805 Bromodichloromethane ND. ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Bromoform ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Bromomethane ND ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Chloroethane ND ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Chloroform ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Chloromethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Dibromochloromethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Vinyl chloride ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 cis-1,2-Dichloroethene 1700 ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/1 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Methylene chloride ND ug/l 500. 5.0 100 9/21/00 7:47 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Tetrachloroethene ND ug/l 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Sample report continued 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fix:, 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 890. ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131736 Sample ID: SLS-GW-PT4S Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 100. ------ 1.0 ------' 100 -------- 9/21/00 ------ 7:47 ----------- M.Himelick --------- 601 ----- 9805 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 100. 1.0 100 9/21/00 7:47 M.Himelick 601 9805 Recovery Target Range ------------ PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 95. 49. - 125. Hall Surr., chloroprene 90. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 90. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date:_ 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131732 Sample ID: SLS-GW-PT5,5S Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 8:55 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602 9805 Chlorobenzene ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 602/601 9805 I 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 602/601 9805 Ethylbenzene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602 9805 Toluene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602 9805 m,p-Xylenes ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602 9805 o-Xylene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 602 9805' _ Bromodichloromethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Bromoform ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Bromomethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Chloroethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 - 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Chloroform ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 - Chloromethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Dibromochloromethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Vinyl chloride ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131732 Sample ID: SLS-GW-PT555 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch. ------------------------ cis-1,3-Dichloropropene ----------- ND ------- ug/1 ------- 1000 ------ 1.0 ------ 1000 -------- 9/21/00 ------ 5:41 ----------- M.Himelick --------- 601 ----- 9805 trans-1,3-Dichloropropene ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Methylene chloride ND ug/l 5000 5.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND . ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Tetrachloroethene 10600 ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,1,1-Trichloroethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 1,1,2-Trichloroethane ND ug/l .1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Trichloroethene ND ug/1 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 Trichlorofluoromethane ND ug/l 1000 1.0 1000 9/21/00 5:41 M.Himelick 601 9805 ND - Not detected at the report limit. Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 92. Hall Surr., chloroprene 87. Hall Surr., 1-chloro-3-fluorobenzene 114. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te-)Stj-�merica [NCO RPO RATED ANALYTICAL REPORT Laboratory Number: 00-A131732 Sample ID: SLS-GW-PT55 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report. Approved By: c amo rA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica [NCO RPO RATED ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromi'de Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127688 Sample ID: SLS-GW-HVDP1 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 13:35 Date Received: 9/ 9/00 Time Received: 9:00 Report . Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ----- ---------- --------- ND, ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 602/601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 602/601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 602/601 . 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 602/601 3756 - ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 2.0 20 9/14/00 16:01 M.Himelick 601 3736 . ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l. 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127688 Sample ID: SLS-GW-HVDP1 Page 2 Report Quan Dil Analysis Analysis . Analyte Result ------------------------ Units Limit Limit Factor Date Time Analyst Method Batch •----------- trans-1,3-Dichloropropene ND ------ ug/l ------ 20.0 ------- 1.0 ------ 20 -------- 9/14/00 ----- 16:01 ---------- M.Himelick --------- 601 ----- 3756 Methylene chloride ND ug/l 100. 5.0 20 9/14/00 16:01 M.Himelick 601 3756 1,1,2,2-Tetrachloroethane ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 Tetrachloroethene 922. ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 1,1,1-Trichloroethane ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 1,1,2-Trichloroethane ND ug/l 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 Trichloroethane ND ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 Trichlorofluoromethane ND. ug/1 20.0 1.0 20 9/14/00 16:01 M.Himelick 601 3756 ND - Not detected at the report limit. Surrogate % Recovery Target Range PID Surr., a,a,a-trifluorotoluene 105. 50. - 150. Hall Surr., 2-chloropropane 89. 49. - 125. Hall Surr., chloroprene 91. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 102. 25. - 157. • # - Recovery outside Laboratory historical limits. I Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testlimerica I N C 0 R P 0 R A T E 0 ANALYTICAL REPORT Laboratory Number: 00-A127688 Sample ID: SLS-GW-HVDP1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ` bgjA,✓ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127684 Sample ID: SLS-GW-HVDP2 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 10:50 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------ ------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND' ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 602/601 3756 Bromodichloromethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756: Bromoform ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3736 Bromomethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Chloroethane ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/l. 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Chloroform ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Chloromethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Dibromochloromethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Ethylene'Dibromide ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Vinyl chloride ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 30.3 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethane ND ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Laboratory Number: 00-A127684 Sample ID: SLS-GW-HVDP2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1.0 ------- 1.0 ------ 1 -------- 9/10/00 ----- 5:52 ---------- M.Himelick --------- 601 ----- 3756 5.0 5.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 1.0 1.0 1 9/10/00 5:52 M.Himelick 601 3756 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 89. Hall Surr., chloroprene 80. Hall Surr., 1-chloro-3-fluorobenzene 102. Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127684 Sample ID: SLS-GW-HVDP2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/19/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200.GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- Lab Number: 00-A131755 Sample ID: SLS-GW-HVDP3 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 11:05 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ ------ -------- ----------------- ------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/24/00 12:36- M.Himelick 602/601 9808 _ 1,3-Dichlorobenzene ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 602/601 9808 Bromodichloromethane ND' ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Bromoform ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick" 601 9808 Bromomethane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Chloroethane ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Chloroform ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Chloromethane ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Dibromochloromethane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Vinyl chloride ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Methylene chloride Y ND u /1 g 50.0 5.0 10 /24/ 9 00 12 .36 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Tetrachloroethene 169. ug/l 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 6.15-726-0954 / 800-765-0980 Testl�merica I NCO RFORATED ANALYTICAL REPORT Analyte Result Units ------------------------- 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131755 Sample ID: SLS-GW-HVDP3 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10.0 ------ 1.0 ------ 10 -------- 9/24/00 ------ 12:36 ----------- M:Himelick --------- 601 ----- 9808 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 10.0 1.0 10 9/24/00 12:36 M.Himelick 601 9808 Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 73. Hall Surr., chloroprene 75. Hall Surr., 1-chloro-3-fluorobenzene 97. # — Recovery outside Laboratory historical limits. Target Range ------------ 5Q. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ftw-u " IReport Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te)stl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127705 Sample ID: SLS-GW-HVDP4 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 9:25 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/13/00 20:41 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/13/00 20:41 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 602/601 3758 - Bromodichloromethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758: Bromoform ND ug/l 50.0 2.0 50 9/13/00 20:41 M.Himelick 601 3758 Bromomethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Chloroethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Chloroform ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Chloromethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Dibromochloromethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Vinyl chloride ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 cis-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Sample report continued 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • T_est merl ca I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 2480 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Laboratory Number: 00-A127705 Sample ID: SLS-GW-HVDP4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 50.0 ------- 1.0 ------ 50 -------- 9/13/00 ----- 20:41 ---------- M.Himelick --------- 601 ----- 3758 250. 5.0 50 9/13/00 20:41 M.Himelick 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick. 601 3758 50.0 1.0 50 9/13/00 20:41 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 57. Hall Surr., chloroprene 64. Hall Surr., 1-chloro-3-fluorobenzene 111. # — Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127705 Sample ID: SLS-GW-HVDP4 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (R,,N� a VU-1A4 Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVTLLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica 2 1 N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127715 Sample ID: SLS-GW-HVDP5 Sample Type: Water Site ID: Date Collected: 9/.8/00 Time Collected: 11:43 Date Received: 9/ 9/00 Time Received: 9:00. Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- -------------- '--------------- - ------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 602/601 3759 - 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 602/601 3759 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/15/00 21:13 M.Himelick 602/601 3759 Bromodichloromethane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759: Bromoform ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Bromomethane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 ,- Carbon tetrachloride ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Chloroethane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 - 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/15/00 .21:13 M.Himelick 601 3759 Chloroform ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 j Chloromethane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Dibromochloromethane ND ug/1 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 - Vinyl chloride ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/15/.00 21:13 M.Himelick 601 3759 1,1-Dichloroethane ND ug/1 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1,1-Dichloroethene 1.1 ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 cis-1,2-Dichloroethene 28.5 ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 ! 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E O i ANALYTICAL REPORT Laboratory Number: 00-A127715 Sample ID: SLS-GW-HVDP5 Page 2 Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 21.2 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 46.3 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1.0 ------- 1.0 ------ 1 -------- 9/15/00 ----- 21:13 ---------- M.Himelick --------- 601 ----- 3759 5.0 5.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 1.0 1.0 1 9/15/00 21:13 M.Himelick 601 3759 Surrogate ------------- % Recovery ---------- Target ------------ Range PID Surr., a,a,a-trifluorotoluene 101. 50. - 150. Hall Surr., 2-chloropropane 57. 49. - 125. j Hall Surr., chloroprene 85. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 115. 25. - 157. # - Recovery outside Laboratory historical limits. --� Sample report continued . I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�mepqq I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127715 Sample ID: SLS-GW-HVDP5 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: UfA-4j )g- Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. ICelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 ICIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Result Units ----------- ------ Lab Number: 00-A127701 Sample ID: SLS-GW-HVDP6 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 16:45 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- ND ug/l 5000 1.0 5000 9/13/00 15:19 M.Himelick 602/601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 602/601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 602/601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 602/601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758: ND ug/l 5000 2.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000. 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 96500 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127701 Sample ID: SLS-GW-HVDP6 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 5000 ------- 1.0 ------ 5000 -------- 9/13/00 ----- 15:19 ---------- M.Himelick --------- 601 ----- 3758 25000 5.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 5000 1.0 5000 9/13/00 15:19 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chlorop=opane 63. Hall Surr., chloroprene 70. Hall Surr., 1-chloro-3-fluorobenzene 100. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127701 Sample ID: SLS-GW-HVDP6 Page 3 These results relate only to the items tested. This report shall not be reproduced except'in full and'with permission of the laboratory. Report Approved By: 04ZV J9,-.rLAAA-./ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith,'Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 -i End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHvu,cE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127695 Sample ID: SLS-GW-HVDP7 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 15:36 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------ ------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 602/601 3758 - Bromodichloromethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758. Bromoform ND ug/l 1000 2.0 1000 9/14/00 20:59 M.Himelick 601 3738 Bromomethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Chloroethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Chloroform ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Chloromethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Dibromochloromethane ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Ethylene Dibromide ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Vinyl chloride ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1,1-Dichloroethene ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 cis-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1,2-Dichloropropane ND ug/l 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/1 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl:�merica I NCORPO RATED ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 41800 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethee ND ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Laboratory Number: 00-A127695 Sample ID: SLS-GW-HVDP7 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 9/14/00 ----- 20:59 ---------- M.Himelick --------- 601 ----- 3758 5000 5.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:59 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 69. Hall Surr., chloroprene 67. Hall Surr., 1-chloro-3-fluorobenzene 100. # — Recovery outside Laboratory historical limits. - Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127695 Sample ID: SLS-GW-HVDP7 Page 3 These results relate only to the items tested. ' This report shall not be reproduced except in full and with. permission of the laboratory. Report Approved By: &4AM A-,. j11, Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S.,- Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testj--�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127694 Sample ID: SLS-GW-HVDP8 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 14:06 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND- ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 602/601 3758 - Bromodichloromethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758: Bromoform ND ug/1 1000 2.0 1000 9/14/00 20:16 M.Himelick 601 3758 'Bromomethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Carbon tetrachloride ND ug/1 1000 1.0 1000 M4/00 20:16 M.Himelick 601 3758 Chloroethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 661 3758 2-Chloroethylvinylether ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Chloroform ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Chloromethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Dibromochloromethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Ethylene Dibromide ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Vinyl chloride ND ug/l 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1,2-Dichloroethane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1,1-Dichloroethene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 cis-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1,2-Dichloropropane ND ug/1 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/l 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testi�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 38400 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127694 Sample ID: SLS-GW-HVDP8 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 9/14/00 ----- 20:16 ---------- M.Himelick --------- 601 ----- 3758 5000 5.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick 601 3758 1000 1.0 1000 9/14/00 20:16 M.Himelick" 601 3758 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 71. Hall Surr., chloroprene 66. Hall Surr., 1-chloro-3-fluorobenzene 110. # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127694 Sample ID: SLS-GW-HVDP8 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: a4�- fa 4"A)L- Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director. Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127693 Sample ID: SLS-GW-HVDP9 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 13:04 Date Received: 9/ 9/00 .Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- --------------- --------- ----- ND, ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 602/601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 602/601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 602/601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 602/601 3758 - ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758: ND ug/l 200. 2.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/1 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/1 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/1 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/1 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 ND ug/l 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 11600 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A127693 Sample ID: SLS-GW-HVDP9 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 200. ------- 1.0 ------ 200 -------- 9/14/00 ----- 19:32 ---------- M.Himelick --------- 601 ----- 3758 1000 5.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0 200 9/14/00 19:32 M.Himelick 601 3758 200. 1.0. 200 - 9/14/00 19:32 M.Himelick 601. 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 104. Hall Surr., 2-chloropropane 60. Hall Surr., chloroprene 63. Hall Surr., 1-chloro-3-fluorobenzene 107. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 % FAX: 615-726-0954 / 800-765-0980 11 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127693 Sample ID: SLS-GW-HVDP9 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (�,a �Q-_,�,t� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene i 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane - 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . I Lab Number: 00-A127706 Sample ID: SLS-GW-HVDP10 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 13:05 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 602/601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 602/601 3758 ND ug/l 10.0 1.0 10 9/13/06 21:25 M.Himelick 602/601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 602/601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758: ND ug/l 10.0 2.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 43.0 ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/1 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 ND ug/l 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 31.0 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 474. ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A127706 Sample ID: SLS-GW-HVDP10 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 10.0 ------- 1.0 ------ 10 -------- 9/13/00 ----- 21:25 ---------- M.Himelick --------- 601 ----- 3758 50.0 5.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 10.0 1.0 10 9/13/00 21:25 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 65. Hall Surr., chloroprene 64. Hall Surr., 1-chloro-3-fluorobenzene 76. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . i i _ 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127706 Sample ID: SLS-GW-HVDP10 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (4dzL&/. A} A" rA-/ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. __ 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT 'i IT CORP-SEARS 2338 Lab Number: 00-A131796 KIM TITMUS Sample ID: SLS-GW-HVDP11 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Project: 107535 Project Name: Sampler: D. LUBELL Date Time Date Time Collected: Collected: Received: Received: 9/ 9/00 11:30 9/16/00 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date ------ -- Time ------ Analyst --------------------- Method Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 602/601 9810 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 602/601 9810 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 602/601 9810 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 602/601 9810 Bromodichloromethane ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Bromoform ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Bromomethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Carbon tetrachloride ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810- Chloroethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 2-Chloroethylvinylether 260. ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Chloroform ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Chloromethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Dibromochloromethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Vinyl chloride ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 -- 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 cis-1,2-Dichloroethene 140. ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 1,2-Dichloropropane ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Methylene chloride ND ug/1 250. 5.0 50 9/22/00 21:13 M.Himelick 601 9810 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Tetrachloroethene 430. ug/l 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 • Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 5600 ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Laboratory Number: 00-A131796 Sample ID: SLS-GW-HVDP11 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 21:13 ----------- M.Himelick --------- 601 ----- 9810 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 500. 1.0 500 9/23/00 23:15 M.Himelick 601 9810 50.0 1.0 50 9/22/00 21:13 M.Himelick 601 9810 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 107. Hall,Surr., 2-chloropropane 89. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 102. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. -, 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director ' Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE2O5 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte ------------------------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127716 Sample ID: SLS-GW-HVDP12 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 13:13 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch ----------- ------ ------------- -------------- ------------------------ ----- ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 602/601 3759 ND ug/1 200. 1.0 200 9/13/00 21.:59 M.Himelick 602/601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick' 602/601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 602/601 3759 .ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759: ND ug/l 200. 2.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/l 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 300. ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 ND ug/1 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL Y ICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 7640 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND. ug/l ND - Not detected at the report limit. Laboratory Number: 00-A127716 Sample ID: SLS-GW-HVDP12 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 200. ------- 1.0 ------ 200 -------- 9/13/00 ----- 21:59 ---------- M.Himelick --------- 601 ----- 3759 1000 5.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 200. 1.0 200 9/13/00 21:59 M.Himelick 601 3759 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 70. Hall Surr., chloroprene 82. Hall Surr., 1-chloro-3-fluorobenzene 86. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127716 Sample ID: SLS-GW-HVDP12 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: k '" �9- nAAA - Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv., Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127718 Sample ID: SLS-GW-HVDP13 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 14:48 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- ------ -------- ----- ------------------- ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602 3759 Chlorobenzene ND" ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602/601 3759 1,2-Dichlorobenzene ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602/601 3759 1,4-Dichlorobenzene ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602/601 3759 Ethylbenzene ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602 3759 Toluene ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 602 3759 m,p-Xylenes ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 602 3759 o-Xylene ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 602 3759 Bromodichloromethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Bromoform ND ug/1 500. 2.0 500 9/14/00 16:27 M.Himelick 601 3759 Bromomethane ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Carbon tetrachloride ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Chloroethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 2-Chloroethylvinylether ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Chloroform ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Chloromethane ND ug/1 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Dibromochloromethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Vinyl chloride ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 1,2-Dichloroethane ND ug/l 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 cis-1,2-Dichloroethene ND ug/1 trans-1,2-Dichloroethene ND ug/l 1,2-Dichloropropane ND ug/1 cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 16700 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127718 Sample ID: SLS-GW-HVDP13 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 500. ------- 1.0 ------ 500 -------- 9/14/00 ----- 16:27 ---------- M.Himelick --------- 601 ----- 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 2500 5.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 500. 1.0 500 9/14/00 16:27 M.Himelick 601 3759 Recovery PID Surr., a,a,a-trifluorotoluene 99. Hall Surr.,, 2-chloropropane 69. Hall Surr., chloroprene 93. Hall Surr., 1-chloro-3-fluorobenzene 88. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127718 Sample ID: SLS-GW-HVDP13 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. t-- Report Approved By: 19--VLa.tA,,L� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A.'Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv'. Laboratory Certification Number: 387 End of Sample Report. _ 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl_ merica j I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131794 Sample ID: SLS-GW-HVDP14 Sample Type: Ground water Site ID: Date Collected: 9/ 9/00 Time Collected: 12:33 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------ .------------ ----------- -------------- ------ -------------- ------ -------------------- ----- *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Sample -report continued . . . ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 602/601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602/601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602/601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602/601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602 9810. ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 602 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810. ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick '601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/1 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 . ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 ND ug/l 5.0 1.0 5 9/23/00 22:33 M.Himelick 601 9810 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131794 Sample ID: SLS-GW-HVDP14 Page 2 Report Quan Dil Analyte Result Units Limit Limit Factor ------------------------ cis-1,3-Dichloropropene ----------- ND ------- ug/l ------- 5.0 ------ 1.0 ------ 5 trans-1,3-Dichloropropene ND ug/l 5.0 1.0 5 Methylene chloride ND ug/l 25.0 5.0 5 1,1,2,2-Tetrachloroethane ND ug/l 5.0 1.0 5 Tetrachloroethene 180. ug/1 5.0 1.0 5 1,1,1-Trichloroethane ND ug/l 5.0 1.0 5 1,1,2-Trichloroethane ND ug/l 5.0 1.0 5 Trichloroethene 150. ug/l 5.0 1.0 5 Trichlorofluoromethane ND ug/1 5.0 1.0 5 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 73. Hall Surr., chloroprene 77. Hall Surr., 1-chloro-3-fluorobenzene 105. # - Recovery outside Laboratory historical limits. Sample report continued . . . Analysis Analysis Date Time Analyst Method Batch -------- 9/23/00 ------ 22:33 ----------- M.Himelick --------- 601 ----- 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 9/23/00 22:33 M.Himelick 601 9810 Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I NCO RPORATED ANALYTICAL REPORT Laboratory Number: 00-A131794 Sample ID: SLS-GW-HVDP14 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report. Approved By: (Ago G Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director `" Gail A'. Lage, Technical Serv. Michael H. Dunn, M.S.,'Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131790 KIM TITMUS Sample ID: SLS-GW-HVDP15 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/ 9/00 Project: 107535 Time Collected: 15:36 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1000 1.0 1000 9/23/00 14:48 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND. ug/l 1000 1.0 1000 9/23/00 14:48 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 9/23/00 14:48 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Bromoform ND ug/l 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Bromomethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Chloroethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Chloroform ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Chloromethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Dibromochloromethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Vinyl chloride ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1,2-Dichloroethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 cis-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Methylene chloride ND ug/1 5000 5.0 1000 9/23/00 14:48 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Tetrachloroethene 1000 ug/1 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Samplereportcontinued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 42600 ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A131790 Sample ID: SLS-GW-HVDP15 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor ' Date Time Analyst Method Batch ------- 1000 ------ 1.0 ------ 1000 -------- 9/23/00 ------ 14:48 ----------- M.Himelick --------- 601 ----- 9809 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 1000 1.0 1000 9/23/00 14:48 M.Himelick 601 9809 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 103 Hall Surr., 2-chloropropane 74. Hall Surr., chloroprene 79. Hall Surr., 1-chloro-3-fluorobenzene 90. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. . Report Approved By: �-�Q rL'-O" / Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131789 Sample ID: SLS-GW-HVDP16 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 9:33 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- -------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 1000 1.0 1000 9/24/00 10:30 M.Himelick 601 9809 Bromoform ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Bromomethan6 ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Chloroethane ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Chloroform ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Chloromethane ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Dibromochloromethane ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Vinyl chloride ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 cis-1,2-Dichloroethene 2280 ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 1000 1.0 1000 9/24/00 10:30 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Methylene chloride ND ug/1 250. 5.0 50 9/23/00 12:41 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Tetrachloroethene ND ug/1 1000 1.0 1000 9/24/00 10:30 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 78100 ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131789 Sample ID: SLS-GW-HVDP16 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 12:41 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 1000 1.0 1000 9/24/00 10:30 M.Himelick 601 9809 50.0 1.0 50 9/23/00 12:41 M.Himelick 601 9809 Recovery PID Surr., a,a,a-trifluorotoluene 105. Hall Surr., 2-chloropropane 75. Hall Surr., chloroprene 74. Hall Surr., 1-chloro-3-fluorobenzene -84. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASIIVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte ------------------------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride i Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . Lab Number: 00-A131788 Sample ID: SLS-GW-HVDP17 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 10:37 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch ----------- ------- ------- ------ -------------- -------------------------- ----- ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 602/601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 602/601 9809 NO ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 602/601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 602/601 9809 ND ug/l 1.0 IA 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 5.0 5.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 34.4 ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 - 9809 2960 FOSTER CRE►GHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Analyte ------------------------ 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Tes t = merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131788 Sample ID: SLS-GW-HVDP17 Page 2 Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch ----------- ND ------- ug/l ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 ------ 8:23 ----------- M.Himelick --------- 601 ----- 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 68.5 ug/l 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND ug/1 1.0 1.0 1 9/24/00 8:23 M.Himelick 601 9809 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 105. Hall Surr., 2-chloropropane 82. Hall Surr., chloroprene 87. Hall Surr., 1-chloro-3-fluorobenzene 103. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: AL -Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 I, End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131787 Sample ID: SLS-GW-HVDP18 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 11:14 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------------------------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 27Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 602/601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 602/601 9809 ND. ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 602/601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 602/601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 95.0 ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/1 250. 5.0 50 9/23/00 11:13 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 2870 ug/l 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 2640 ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A131787 Sample ID: SLS-GW-HVDP18 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 11:13 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 50.0 1.0 50 9/23/00 11:13 M.Himelick 601 9809 Surrogate =------------ % Recovery ---------- PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 78. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 109. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (ques-i q&CA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131786 KIM TITMUS Sample ID: SLS-GW-HVDP19 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water. MORRISVILLE, NC 27560 Site ID: Date Collected: 9/11/00 ,- Project: 107535 Time Collected: 11:50 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* - Chlorobenzene ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 602/601 9809 - 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Bromoform ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Bromomethane ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 P Chloroethane ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Chloroform ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Chloromethane ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Dibromochloromethane ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 j Vinyl chloride ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 i Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 1,2-Dichloroethane ND ug/1 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 cis-1,2-Dichloroethene 475. ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Methylene chloride ND ug/l 250. 5.0 50 9/23/00 10:29 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 - Tetrachloroethene 540. ug/l 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene 325. ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131786 Sample ID: SLS-GW-HVDP19 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 10:29 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 50.0 1.0 50 9/23/00 10:29 M.Himelick 601 9809 Recovery PID Surr., a,a,a-trifluorotoluene 101 Hall Surr., 2-chloropropane 84. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 96. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131785 KIM TITMUS Sample ID: SLS-GW-HVDP20 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/11/00 Project: 107535 Time Collected: 13:31 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Bromoform ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick- 601 9809 Bromomethane ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 . Chloroethane ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Chloroform ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Chloromethane ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Dibromochloromethane ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Vinyl chloride ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 cis-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 1,2-bichloropropane ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Methylene chloride ND ug/1 250. 5.0 50 9/23/00 9:08 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Tetrachloroethene 1860 ug/1 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 Sample report continued . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Analyte 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131785 Sample ID: SLS-GW-HVDP20 Page 2 Report Quan Dil. Analysis Analysis Result ----------- Units Limit Limit Factor Date Time I Analyst Method Batch ND ------- ug/1 ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 9:08 ----------- M.Himelick --------- 601 ----- 9809 ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 9:08 M.Himelick 601 9809 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 100. 50. - 150. Hall Surr., 2-chloropropane 93. 49. - 125. Hall Surr., chloroprene - 97. 49. - 142. Hall Surr.., 1-chloro-3-fluorobenzene 112. 25. - 157. # — Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By:( a Q �,/.. Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical.,Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. J 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test_ merica I N C O R P O R A.T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131784 Sample ID: SLS-GW-HVDP21 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 14:08 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Bromoform ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Bromomethane ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Carbon tetrachloride ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Chloroethane ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Chloroform ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Chloromethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Dibromochloromethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Vinyl chloride ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 cis-1,2-Dichloroethene 1090 ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Methylene chloride ND ug/l 250. 5.0 50 9/23/00 6:56 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Tetrachloroethene 605. ug/l 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 - 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F.ax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Laboratory Number: 00-A131784 Sample ID: SLS-GW-HVDP21 ME Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 6:56 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 50.0 1.0 50 9/23/00 6:56 M.Himelick 601 9809 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 76. Hall Surr., 1-chloro-3-fluorobenzene 99. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director - Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT.CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . . . Lab Number: 00-A131783 Sample ID: SLS-GW-HVDP22 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 15:00 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 602/601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 602/601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 602/601 9809 ND. ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 602/601 9809 ND. ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M:Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 225. ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/1 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 250. 5.0 50 9/23/00 6:12 M.Himelick 601 9809 ND ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 2880 ug/l 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 1120 ug/1 Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131783 Sample ID: SLS-GW-HVDP22 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 6:12 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 50.0 1.0 50 9/23/00 6:12 M.Himelick 601 9809 50.0 1.0,, 50 9/23/00 6:12 M.Himelick 601 9809 Recovery Target Range --- PID Surr., a,a,a-trifluorotoluene 100. 50. - 150. Hall Surr., 2-chloropropane 80. 49. - 125. Hall Surr., chloroprene 75. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 104. 25. - 157. # — Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: l �� �Q 9��f Qa Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical:Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 i, End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Lab Number: 00-A131782 Sample ID: SLS-GW-HVDP23 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Project: 107535 Time Collected: 15:46 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- ------ -------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND. ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 602/601 9809 Bromodichloromethane NO ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Bromoform ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Bromomethane ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 . Carbon tetrachloride ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Chloroethane ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 ` 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Chloroform ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Chloromethane ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 I_ Dibromochloromethane ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Vinyl chloride ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 1,2-Dichloroethane ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 cis-1,2-Dichloroethene 50.0 ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 SO 9/23/00 5:28 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 50.0 1..0 50 9/23/00 5:28 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Methylene chloride ND ug/l 250. 5.0 50 9/23/00 5:28 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Tetrachloroethene 1140 ug/1 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica INC ORPO RATED ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 3500 ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A131782 Sample ID: SLS-GW-HVDP23 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 5:28 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 50.0 1.0 50 9/23/00 5:28 M.Himelick 601 9809 Surrogate ------------- % Recovery ---------- Target ------------ Range PID Surr., a,a,a-trifluorotoluene 101. 50. - 150. Hall Surr., 2-chloropropane 79. 49. - 125. Hall Surr., chloroprene 75. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 91. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. - Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I NCO R P O RAT E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- Lab Number: 00-A131781 Sample ID: SLS-GW-HVDP24 Sample Type: Ground water Site ID: Date Collected: 9/11/00 Time Collected: 16:15 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- ----------------- ------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 10.0 1.0 10 9/24/00 7:41 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 10.0 1.0, 10 9/24/00 7:41 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Bromoform ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Bromomethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Chloroethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Chloroform ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Chloromethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Dibromochloromethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Vinyl chloride ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 1,2-Dichloroethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 cis-1,2-Dichloroethene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Methylene chloride ND ug/1 50.0 5.0 10 9/24/00 7:41 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Tetrachloroethene 266. ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te-Sti-imerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131781 Sample ID: SLS-GW-HVDP24 -' Page 2 Analyse ------------------------ i 1,1,1-Trichloroethane — 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch ----------- ND ------- ug/l ------- 10.0 ------ 1.0 ------ 10 -------- 9/24/00 ------ . 7:41 ----------- M.Himelick --------- 601 ----- 9809 ND ug/l 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 146. ug/l 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 ND ug/1 10.0 1.0 10 9/24/00 7:41 M.Himelick 601 9809 ND — Not detected at the report limit. Surrogate ------------- % Recovery ---------- PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 78. Hall Surr., chloroprene 78. Hall Surr., 1-chloro-3-fluorobenzene 109. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O RAT E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131780 KIM TITMUS Sample ID: SLS-GW-HVDP25 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Project: 107535 is Project Name: Sampler: D. LUBELL Date Time Date Time Collected: Collected: Received: Received: 16:48 9/16/00 9:00 9/11/00 _ Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Bromoform ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Bromomethane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 . Carbon tetrachloride 7.5 ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Chloroethane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 . 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Chloroform 3.2 ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Chloromethane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Dibromochloromethane ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Vinyl chloride ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 -- 1,2-Dichloroethane 5.1 ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 1,1-Dichloroethene 1.2 ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 - cis-1,2-Dichloroethene 14.5 ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Methylene chloride ND ug/1 5.0 5.0 1 9/24/00 6:59 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Tetrachloroethene 3.6 ug/l 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 42.9 ug/1 Trichlorofluoromethane ND ug/1 - ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131780 Sample ID: SLS-GW-HVDP25 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 ------ 6:59 ----------- M.Himelick --------- 601 ----- 9809 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 1.0 1.0 1 9/24/00 6:59 M.Himelick 601 9809 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 70. 49. - 125. Hall Surr., chloroprene 76. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 95. 25. - 157. - Recovery outside Laboratory historical limits. These results relate only.to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: t y-Q1k9 a OCLCA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director IGail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVII,LE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 - KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131779 Sample ID: SLS-GW-HVDP26 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 8:55 Date'Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst --------------------- Method Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Bromoform ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick- 601 9809 Bromomethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 . Carbon tetrachloride ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 • Chloroethane ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Chloroform ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Chloromethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Vinylchloride ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 -- 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 cis-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Methylene chloride ND ug/l 5.0 5.0 1 9/24/00 18:56 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Tetrachloroethene ND ug/l 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131779 Sample ID: SLS-GW-HVDP26 Page 2 ' Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- 1,1,1-Trichloroethane ND ------- ug/l ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 ------ 18:56 ----------- M.Himelick --------- 601 ----- 9809 1,1,2-Trichloroethane ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Trichloroethene ND t ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 Trichlorofluoromethane, ND ug/1 1.0 1.0 1 9/24/00 18:56 M.Himelick 601 9809 ND — Not detected at the report limit. Surrogate % Recovery Target Range - PID Surr., a,a,a-trifluorotoluene 103. 50. - 150. Hall Surr., 2-chloropropane 79. 49. - 125. Hall Surr., chloroprene 74. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 91. 25. - 157. # — Recovery outsideLaboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/o0 Paul E. Lane, Jr., Lab Director Gail A. Lage-, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. __ 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica [NCO RF0 RATED ANALYTICAL REPORT IT-CORP-SEARS 2338 -. KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131778 Sample ID: SLS-GW-HVDP27 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 9:22 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Bromoform ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Bromomethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 . Carbon tetrachloride ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Chloroethane ND ug/l 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 . 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Chloroform ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Chloromethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Dibromochloromethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Vinyl chloride ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 1,2-Dichloroethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 cis-1,2-Dichloroethene 1200 ug/l 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Methylene chloride ND ug/1 250. 5.0 50 9/23/00 2:33 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Tetrachloroethene 2520 ug/1 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Sample report continued . . . I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte. Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 1660 ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131778 Sample ID: SLS-GW-HVDP27 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/23/00 ------ 2:33 ----------- M.Himelick --------- 601 ----- 9809 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 50.0 1.0 50 9/23/00 2:33 M.Himelick 601 9809 Recovery PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 86. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 114 Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: L,Q �,���Q� Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 _. KIM TITMUS 2200 GATEWAY CTR. BLVD. MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL STE205 Lab Number: 00-A131777 Sample ID: SLS-GW-HVDP28 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 9:50 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte j------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- I *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 602/601 9809 Bromodichloromethane � I ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Bromoform ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Bromomethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Chloroethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 1.0 1.0 .1 9/24/00 5:34 M.Himelick 601 9809 Chloroform ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Chloromethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 " Vinyl chloride ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Dichlorodifluoromethane i ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 - 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 cis-1,2-Dichloroethene 22.2 ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Methylene chloride ND ug/l 5.0 5.0 1 9/24/00 5:34 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Tetrachloroethene 55.2 ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerioca I N C 0 R P 0 R A T r: D ANALYTICAL REPORT Laboratory Number: 00-A131777 Sample ID: SLS-GW-HVDP28 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1,1-Trichloroethane ----------- ND ------- ug/l ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 ------ 5:34 ----------- M.Himelick --------- 601 ----- 9809 1,1,2-Trichloroethane ND ug/1 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Trichloroethene 41.2 ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 Trichlorofluoromethane ND ug/l 1.0 1.0 1 9/24/00 5:34 M.Himelick 601 9809 ND — Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 78. Hall Surr., chloroprene 82. Hall Surr., 1-chloro-3-fluorobenzene 120. # — Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: l �� C,tY�� 04 Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131776 Sample ID: SLS-GW-HVDP29 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 10:16 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC*_ Chlorobenzene ND ug/1 1.0 1.0 1 9/24/00 4:52 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/24/00 4:52 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Bromoform ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick. 601 9809 Bromomethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Chloroethane ND ug/1 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Chloroform ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Chloromethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Vinyl chloride ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1,2-Dichloroethane 4.8 ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 - cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 - Methylene chloride ND ug/l 5.0 5.0 1 9/24/00 4:52 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Tetrachloroethene 2.5 ugll 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestL�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131776 Sample ID: SLS-GW-HVDP29 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/24/00 ------ 4:52 ----------- M.Himelick --------- 601 ----- 9809 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1.0 1.0 1 9/24/00 4:52 M.Himelick 601 9809 1.0 1.0 1 9/24/00 4:52 '. M.Himelick 601 9809 Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 80. Hall Surr., chloroprene 77. Hall Surr., 1-chloro-3-fluorobenzene 91. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (��(� �?,� Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director ' Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director .Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. IZelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI. 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 I; Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER I Lab Number: 00-A127689 Sample ID: SLS-GW-DW1 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 15:22 Date Received: 9/ 9/00 Time Received: 9:00 Report - Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/1 20.0 1.0, 20 9/14/00 16:43 M.Himelick 602/601 3756 - Bromodichloromethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756. Bromoform ND ug/1- 20.0 2.0 20 9/14/00 16:43 M.Himelick 601 3756 Bromomethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Carbon tetrachloride ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Chloroethane ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 . Chloroform ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Chloromethane ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Dibromochloromethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Ethylene Dibromide ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Vinyl chloride ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 1,1-Dichloroethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 1,1-Dichloroethene 26.0 ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 1,2-Dichloropropane ND ug/l 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/1 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT Analyte. Result Units trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 464. ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127689 Sample ID: SLS-GW-DWI Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 20.0 ------- 1.0 ------ 20 -------- 9/14/00 ----- 16:43 ---------- M.Himelick --------- 601 ----- 3756 100. 5.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 20.0 1.0 20 9/14/00 16:43 M.Himelick 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 105. Hall Surr., 2-chloropropane 85. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 112. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�meriqca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127689 Sample ID: SLS-GW-DW1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (p„4A4 4 _.Vl 4-4,v✓ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / .800-765-0980 Testl�meriqca I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene r Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropee Sample report continued I I Lab Number: 00-A127682 Sample Ib: SLS-GW-DW2 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 9:18 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ----------------L------- ----- ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 602/601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 602/601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 602/601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 602/601 3756 - ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756; ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 'ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 5.2 ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 . ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/1 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 ND ug/l 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 43.8 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- I N C O R P O R A T E D Laboratory Number: 00-A127682 Sample ID: SLS-GW-DW2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1.0 ------- 1.0 ------ 1 -------- 9/14/00 ----- 12:31 ---------- M.Himelick --------- 601 ----- 3756 5.0 5.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 1.0 1.0 1 9/14/00 12:31 M.Himelick 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 104 Hall Surr., 2-chloropropane 79. Hall Surr., chloroprene 86. Hall Surr., 1-chloro-3-fluorobenzene 115 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testj�merica ANALYTICAL REPORT Laboratory Number: 00-A127682 Sample ID: SLS-GW-DW2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (I.Z;44 A_1'it4-ti Report Date: '9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical.Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127699 Sample ID: SLS-GW-DW3 Sample Type: Water. Site ID: Date Collected: 9/ 7/00 Time Collected: 18:49 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 602 3758 Chlorobenzene ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 602/601 3758 - 1,4-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 602/601 3758: Ethylbenzene ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 602 3758 Toluene ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 602 3758 m,p-Xylenes ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 602 3758 o-Xylene ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 602 3758 Bromodichloromethane ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Bromoform ND ug/l 500. 2.0 500 9/15/00 1:22 M.Himelick 601 3758 Bromomethane ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Chloroethane ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l .500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Chloroform ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Chloromethane ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Dibromochloromethane ND ug/l .500. 1.0 500 9/15/00 1:22 M.Himelick 601 37.58 Ethylene Dibromide ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Vinyl chloride ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 1,2-Dichloroethane ND ug/1 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 T Test merica I N C O R P O RAT E D ANALYTICAL REPORT Laboratory Number: 00-A127699 Sample ID: SLS-GW-DW3 Page 2 Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 cis-1,2-Dichloroethene_ ND ug/1 - trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 27600 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane i ND ug/l ND - Not detected at the report limit. Surrogate ------------- Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 500. ------- 1.0 ------ 500 -------- 9/15/00 ----- 1:22 ---------- M.Himelick --------- 601 ----- 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 2500 5.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500- 9/15/00 1:22 M.Himelick 601 3758 500. 1.0 500 9/15/00 1:22 M.Himelick 601 3758 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 104. Hall Surr., 2-chloropropane 60. Hall Surr., chloroprene 67. Hall Surr., 1-chloro-3-fluorobenzene 111. # - Recovery outside Laboratory historical limits. -i Sample report continued . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAY: 615-726-0954 / 800-765-0980 TeNtAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127699 Sample ID: SLS-GW-DW3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: &,(AAA �(}_ j'�.,�,� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CRE(GHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica �J I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . . . Lab Number: 00-A131752 Sample ID: SLS-GW-DW4 Sample Type: Ground water Site ID: Date Collected: 9/14/00 Time Collected: 8:45 Date Received: 9/16/00 Time Received: 9:00 Report Quan• Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 602/601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 602/601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 602/601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 602/601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/1 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 5000 5.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 ND ug/l 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Analyte 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Testlimerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Result Units ND ug/l ND ug/l ND ug/l ND ug/l ND'— Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131752 Sample ID: SLS-GW-DW4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 1000 1.0 1000 9/21/00 13:49 M.Himelick 601 9808 Recovery PID Surr., a,a,a-trifluorotoluene 104 Hall Surr., 2-chloropropane 84. Hall Surr., chloroprene 54. Hall Surr., 1-chloro-3-fluorobenzene 80. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: A, I OA2 Report Dater 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131762 KIM TITMUS Sample ID: SLS-GW-DW5 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 17:15 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 - Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Bromoform ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Bromomethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Carbon tetrachloride 63.0 ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Chloroethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Chloroform 23.0 ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Chloromethane ND ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Dibromochloromethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Vinyl chloride ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 cis-1,2-Dichloroethene 20.0 ug/l 10.0 1.0 10 9/22/00 2:02. M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Methylene chloride ND ug/l 50.0 5.0 10 9/22/00 2:02 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Tetrachloroethene 70.0 ug/l 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica [NCO RPO RATED ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 449. ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131762 Sample ID: SLS-GW-DW5 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10.0 ------ 1.0 ------ 10 -------- 9/22/00 ------ 2:02 ----------- M.Himelick --------- 601 ----- 9808 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 10.0 1.0 10 9/22/00 2:02 M.Himelick 601 9808 Recovery PID Surr.; a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 93. Hall Surr., chloroprene 91. Hall Surr.,'l-chloro-3-fluorobenzene 97. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: A Q ago 0A Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director - Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 (j End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Test merica ' I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200'GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Lab Number: 00-A131738 Sample ID: SLS-GW-DW7 Sample Type: Ground water Site ID: _ Project: 107535 Project Name: '_- Sampler: D. LUBELL Date Time Date Time Collected: Collected: Received: Received: 9/12/00 15:05 9/16/00 9:00 Report Quan Dil Analysis Analysis Analyte ------------ .------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- i I , *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 602/601 9805 Bromodichloromethane ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Bromoform ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick- 601 9805 Bromomethane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Chloroethane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Chloroform ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Chloromethane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Dibromochloromethane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Vinyl chloride ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805, 1,1-Dichloroethene ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 !, 1,2-Dichloropropane ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Methylene chloride ND ug/l 50.0 5.0 10 9/21/00 9:11 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Tetrachloroethene 295. ug/l 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Sample report continued . . . 1 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica [NCO RPO RATED ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131738 Sample ID: SLS-GW-DW7 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10.0 ------ 1.0 ------ 10 -------- 9/21/00 ------ 9:11 ----------- M.Himelick --------- 601 ----- 9805 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 10.0 1.0 10 9/21/00 9:11 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 105. Hall Surr., chloroprene 91. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: AP Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director . Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 i End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131769 Sample ID: SLS-GW-DW8 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 8:55 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ ------ -------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 200. 1.0 200 9/22/00 8:19 'M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Bromoform ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Bromomethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Chloroethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Chloroform ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Chloromethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Dibromochloromethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Vinyl chloride ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 1,2-Dichloroethane ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 cis-1,2-Dichloroethene 420. ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Methylene chloride ND ug/l 1000 5.0 200 9/22/00 8:19 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/1 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Tetrachloroethene 4020 ug/l 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Sample report continued . . . I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 { Test merica I N C O R P O RAT E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 1380 ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131769 Sample ID: SLS-GW-DW8 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 200. ------ 1.0 ------ 200 -------- 9/22/00 ------ 8:19 ----------- M.Himelick --------- 601 ----- 9808 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 200. 1.0 200 9/22/00 8:19 M.Himelick 601 9808 Recovery PID Surr., a,a,a-trifluorotoluene 102 Hall Surr., 2-chloropropane 85. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 109 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. It Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • Test rl e m ca I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 f KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131763 Sample ID: SLS-GW-DW12 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 16:30 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------ .------------ ------------------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/22/00 2:44 M.Himelick 602/601 9808 Bromodichloromethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Bromoform ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Bromomethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Carbon .tetrachloride ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Chloroethane ND ug/1 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Chloroform ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Chloromethane ND ug/l 1.0 .1.0 1 9/22/00 2:44 M.Himelick 601 9808 Dibromochloromethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Vinyl chloride ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Methylene chloride ND ug/l 5.0 5.0 1 9/22/00 2:44 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Tetrachloroethene ND ug/l 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 it Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Laboratory Number: 00-A131763 Sample ID: SLS-GW-DW12 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/22/00 ------ 2:44 ----------- M.Himelick --------- 601 ----- 9808 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 1.0 1.0 1 9/22/00 2:44 M.Himelick 601 9808 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 91. Hall Surr., chloroprene 91. Hall Surr., 1-chloro-3-fluorobenzene 97. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ( k-t A p (j-&0((kCA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131743 KIM TITMUS Sample ID: SLS-GW-DW13 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 11:05 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ .------------ Result ------------ Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND u /l g 20.0 1. 0 20 9/21/00 14:05 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 602/601 9805 Bromodichloromethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Bromoform ND ug/1 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Bromomethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Chloroethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Chloroform ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Chloromethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Dibromochloromethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Vinyl chloride ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 j Dichlorodifluoromethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 - cis-1,2-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 - 1,2-Dichloropropane ND ug/1 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Methylene chloride ND ug/1 100. 5.0 20 9/21/00 14:05 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Tetrachloroethene 680. ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl-�merica IN CORPO RATED ANALYTICAL REPORT Laboratory Number: 00-A131743 Sample ID: SLS-GW-DW13 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ 1,1,1-Trichloroethane ----- - ----- ND ------- ug/l ------- 20.0 ------ 1.0 ------ 20 -------- 9/21/00 ------ 14:05 ----------- M.Himelick --------- 601 ----- 9805 1,1,2-Trichloroethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 Trichloroethene 44.0 ug/l 20.0 1.0 20 9/21%00 14:05 M.Himelick 601 9805 Trichlorofluoromethane ND ug/l 20.0 1.0 20 9/21/00 14:05 M.Himelick 601 9805 ND - Not detected at the report limit. Surrogate ------------- % Recovery ---------- Target ------------ Range PID Surr., a,a,a-trifluorotoluene 100. 50. - 150. Hall Surr., 2-chloropropane 88. 49. - 125. Hall Surr., chloroprene 83. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 116. 25. - 157. # - Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.. Report Approved By: l k,J CA P&A _ , Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 i End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131744 KIM TITMUS Sample ID: SLS-GW-DW14 2200 GATEWAY CTR. BLVD. 8TE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Project: 107535 Project Name: Sampler: D. LUBELL Date Time Date Time Collected: Collected: Received: Received: 9/13/00 12:35 9/16/00 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 5.0 1.0 5 9/21/00 14:47 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 5.0 1.0 5 9/21/00 14:47 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 602/601 9805 Bromodichloromethan e ND u g 1 / 5.0 1.0 5 9/21/00 14:47 M.Himelick 60 1 9805 I Bromoform ND ug/l 5.0 1.0 5 9/21/00 14:47 M.Himelick, 601 9805 Bromomethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Chloroethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/1 5.0 1.0 5 W21/00 14:47 M.Himelick 601 9805 Chloroform ND ug/l 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Chloromethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Dibromochloromethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Ethylene Dibromide ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Vinyl chloride ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 .9805 1,2-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 1,1-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Methylene chloride ND ug/1 25.0 5.0 5 9/21/00 14:47 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Tetrachloroethene 252. ug/1 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte . Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 93.0 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A131744 Sample ID: SLS-GW-DW14 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor ' Date Time Analyst Method Batch ------- 5.0 ------ 1.0 ------ 5 -------- 9/21/00 ------ 14:47 ----------- M.Himelick --------- 601 ----- 9805 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 5.0 1.0 5 9/21/00 14:47 M.Himelick 601 9805 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 101 Hall Surr., 2-chloropropane 105 Hall Surr., chloroprene 88. Hall Surr., 1-chloro-3-fluorobenzene 120 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: CPau cka (LA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 - MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131747 Sample ID: SLS-GW-DW15 Sample Type:.Ground water Site ID: Date Collected: 9/13/00 Time Collected: 15:35 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 602/601 9805' 1,3-Dichlorobenzene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 20.0 1.0 .20 9/21/00 16:11 M.Himelick 602/601 9805 Bromodichloromethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Bromoform ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Bromomethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Chloroethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Chloroform ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Chloromethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Dibromochloromethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Vinyl chloride ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/1 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Methylene chloride ND ug/l 100. 5.0 20 9/21/00 16:11 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Tetrachloroethee 688. ug/1 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestL�merica ANALYTICAL REPORT Laboratory Number: 00-A131747 Sample ID: SLS-GW-DW15 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units Limit Limit Factor Date Time Analyst Method Batch 1,1,1-Trichloroethane ND ------- ug/1 ------- 20.0 ------ 1.0 ------ 20 -------- 9/21/00 ------ 16:11 ----------- M.Himelick --------- 601 ----- 9805 1,1,2-Trichloroethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Trichloroethene 164. ug/1 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 Trichlorofluoromethane ND ug/l 20.0 1.0 20 9/21/00 16:11 M.Himelick 601 9805 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 90. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 116. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: C ku., C &", Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 �IEnd of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131761 Sample ID: SLS-GW-DMP1 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 17:55 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------------------------------- ------ -------------- ----------------- --------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/22/00 1:21 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50, 9/22/00 1:21 M.Himelick 602/601 9808 Bromodichloromethane ND ug/1 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Bromoform ND ug/l. 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Bromomethane NO ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Chloroethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Chloroform ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Chloromethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Dibromochloromethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Vinyl chloride ND ug/1 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 cis-1,2-Dichloroethene 2200 ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Methylene chloride ND ug/l 250. 5.0 5,0 9/22/00 1:21 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Tetrachloroethee 270. ug/1 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Sample report continued . . . I 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fu: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 300. ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Laboratory Number: 00-A131761 Sample ID: SLS-GW-DMP1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 1:21 ----------- M.Himelick --------- 601 ----- 9808 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 50.0 1.0 50 9/22/00 1:21 M.Himelick 601 9808 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 101 Hall Surr., 2-chloropropane 84. Hall Surr., chloroprene 81. Hall Surr., 1-chloro-3-fluorobenzene 98. # — Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: �a i Q ( Law, Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL STE205 Lab Number: 00-A131750 Sample ID: SLS-GW-DMP2 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 18:05 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis _Analysis Analyte ------------ --------- --- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 602/601 9805 Bromodichloromethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Bromoform ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Bromomethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Chloroethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Chloroform ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Chloromethane ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Dibromochloromethane ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Vinyl chloride ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 { 1,1-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 10.0 1.0 10 9/21/00, 19:46 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Methylene chloride ND ug/l 50.0 5.0 10 9/21/00 19:46 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Tetrachloroethene 421. ug/l 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 865. ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131750 Sample ID: SLS-GW-DMP2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 10.0 ------ 1.0 ------ 10 -------- 9/21/00 ------ 19:46 ----------- M.Himelick --------- 601 ----- 9805 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 10.0 1.0 10 9/21/00 19:46 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 104 Hall Surr., 2-chloropropane 92. Hall Surr., chloroprene 85. Hall Surr., 1-chloro-3-fluorobenzene 117 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: - Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. „! Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131740 Sample ID: SLS-GW-DMP3 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 17:00 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------ - ----------- ----------- -------------- ------ ------ -------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene j Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . . . ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 602/601 9805 ND ug/1 20.0 1.0.. 20 9/21/00 11:59 M.Himelick 602/601 .9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 602/601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 602/601 9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND. ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 .20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ' ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/l 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/l 100. 5.0 20 9/21/00 11:59 M.Himelick 601 9805 ND ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 474. ug/1 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 1 2960 FOSTER CREIGHTON DRIVE / NASHVN,LE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 68.0 ug/l Trichlorofluoromethane ND ug/1 ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131740 Sample ID: SLS-GW-DMP3 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 20.0 ------ 1.0 ------ 20 -------- 9/21/00 ------ 11:59 ----------- M.Himelick --------- 601 ----- 9805 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 20.0 1.0 20 9/21/00 11:59 M.Himelick 601 9805 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. 50. - 150. Hall Surr., 2-chloropropane 93. 49. - 125. Hall Surr., chloroprene 89. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 116. 25. - 157. # — Recovery outside Laboratory historical limits. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ( Qn A I (An CA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director I Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica' I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131741 KIM TITMUS Sample ID: SLS-GW-DMP4 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/13/00 Project: 107535 Time Collected: 9:00 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit Limit ------ Factor ------ Date Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 602/601 9805 j 1,2-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 602/601 9805 _ 1,3-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 602/601 9805 Bromodichloromethane i ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Bromoform ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Bromomethane ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Chloroethane ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Chloroform ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Chloromethane ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Dibromochloromethane ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Vinyl chloride ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805. 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 _. cis-1,2-Dichloroethene 460. ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Methylene chloride ND ug/1 500. 5.0 100 9/21/00 12:41 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Tetrachloroethene 4090 ug/1 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 1340 ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131741 Sample ID: SLS-GW-DMP4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 100. ------ 1.0 ------ 100 -------- 9/21/00 ------ 12:41 ----------- M.Himelick --------- 601 ----- 9805 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 100. 1.0 100 9/21/00 12:41 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 102. Hall Surr., chloroprene 93. Hall Surr., 1-chloro-3-fluorobenzene 115. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: JR.1- 1 (ggaVj Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 Lab Number: 00-A127711 KIM TITMUS Sample ID: SLS-GW-BMW1 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/ 8/00 Project: 107535 Time Collected: 9:05 Project Name: Date Received: 9/ 9/00 Sampler: D.LUBELL/K.SUMNER Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602 3758 Chlorobenzene ND ug/1 20.0 1.0 20 9/15/00 6:28 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602/601 3758 Ethylbenzene ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602 3758 Toluene ND ug/1 20.0 1.0 20 9/15/00 6:28 M.Himelick 602 3758 m,p-Xylenes ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 602 3758 o-Xylene ND ug/1 20.0 1.0 20 9/15/00 6:28 M.Himelick 602 3758 Bromodichloromethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Bromoform ND ug/l 20.0 2.0 20 9/15/00 6:28 M.Himelick 601 3758 Bromomethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Chloroethane ND ug/1 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 2-Chloroethylvinylether ND_ ug/1 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Chloroform ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Chloromethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Dibromochloromethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Vinyl chloride ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHViLLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 cis-1,2-Dichloroethene ND ug/l . trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/1 cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 802. ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 52.0 ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127711 Sample ID: SLS-GW-BMW1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 20.0 ------- 1.0 ------ 20 -------- 9/15/00 ----- 6:28 ---------- M.Himelick --------- 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 100. 5.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 20.0 1.0 20 9/15/00 6:28 M.Himelick 601 3758 % Recovery Target Range PID Surr., a,a,a-trifluorotoluene 106. 50..- 150. Hall Surr., 2-chloropropane 66. 49. - 125. Hall Surr., chloroprene 67. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 112. 25. - 157. # - Recovery outside Laboratory historical limits. Sample report continued JII 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127711 Sample ID: SLS-GW-BMW1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (rvt�/ 19-�.� Report Date: 9/19/00 I' _) Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. i—, l_! 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127698 Sample ID: SLS-GW-BMW2 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 17:58 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602 3758 Chlorobenzene ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602/601 3758 Ethylbenzene ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602 3758 Toluene ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602 3758 m,p-Xylenes ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602 3758 o-Xylene ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 602 3758 Bromodichloromethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Bromoform ND ug/l 1000 2.0 1000 9/14/00 22:27 M.Himelick 601 3758 Bromomethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Chloroethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Chloroform ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Chloromethane ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Dibromochloromethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Vinyl chloride ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1,2-Dichloroethane ND ug/1 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 I Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/l cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/1 cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 45700 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127698 Sample ID: SLS-GW-BMW2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 9/14/00 ----- 22:27 ---------- M.Himelick --------- 601 ----- 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 5000 5.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000• 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 1000 1.0 1000 9/14/00 22:27 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 75. Hall Surr., chloroprene 78. Hall Surr., 1-chloro-3-fluorobenzene 114. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. i 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127698 Sample ID: SLS-GW-BMW2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131737 KIM TITMUS Sample ID: SLS-GW-BMW3 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/12/00 Project: 107535 Time Collected: 13:45 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 602/601 9805 _ 1,3-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 602/601 9805 Bromodichloromethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Bromoform ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick. 601 9805 Bromomethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Chloroethane NO ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Chloroform ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Chloromethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Dibromochloromethane ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Vinyl chloride ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 1,1-Dichloroethene I� ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Methylene chloride ND ug/l 50.0 5.0 10 9/21/00 8:28 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Tetrachloroethene 278. ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131737 Sample ID: SLS-GW-BMW3 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/l ------- 10.0 ------ 1.0 ------ 10 -------- 9/21/00 ------ 8:28 ----------- M.Himelick --------- 601 ----- 9805 1,1,2-Trichloroethane ND ug/1 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Trichloroethene ND ug/l. 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 Trichlorofluoromethane ND ug/l 10.0 1.0 10 9/21/00 8:28 M.Himelick 601 9805 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 99. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: � W Q ( U CA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131745 Sample ID: SLS-GW-BMW4 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 13:15 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- -------------- ------ -------------- ------ -------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 602/601 9805 - 1,3-Dichlorobenzene, ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 602/601 9805 Bromodichloromethane ND ug/1 5.0 1.0 5 V21/00 15:29 M.Himelick 601 9805 Bromoform ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Bromomethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805. Chloroethane ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Chloroform ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Chloromethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Dibromochloromethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Vinyl chloride ND ug/l 5.0 1.0 5. 9/21/00 15:29 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 ` 1,1-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 1,1-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 :- cis-1,2-Dichloroethene ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 1,2-Dichloropropane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 j cis-1,3-Dichloropropene ND ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Methylene chloride ND ug/1 25.0 5.0 5 9/21/00 15:29 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Tetrachloroethene 244. ug/l 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Sample.report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 84.0 ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A131745 Sample ID: SLS-GW-BMW4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 5.0 ------ 1.0 ------ 5 -------- 9/21/00 ------ 15:29 ----------- M.Himelick --------- 601 ----- 9805 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 5.0 1.0 5 9/21/00 15:29 M.Himelick 601 9805 Surrogate % Recovery ------------- ---------- PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 91. Hall Surr., chloroprene 87. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: � 9ja�- 646LCa Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. I2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-01.77 / FAX: 615-726-0954 / 800-765-0980 J Testl_ merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 Lab Number: 00-A127719 KIM TITMUS Sample ID: SLS-GW-PT1D 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 Site ID: Date Collected:' 9/ 8/00 Project: 107535 Time Collected: 15:22 Project Name: Date Received: 9/ 9/00 Sampler: D.LUBELL/K.SUMNER Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ----------------- Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time -----. Analyst --- ,------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 602/601 3759 j 1,2-Dichlorobenzene ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 602/601 3759 1,4-Dichlorobenzene ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 602/601 3759 I Bromodichloromethane ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Bromoform ND ug/l 100. 2.0 100 9/14/00 17:09 M.Himelick 601 3759 Bromomethane ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Carbon tetrachloride ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Chloroethane ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 2-Chloroethylvinylether ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Chloroform ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Chloromethane ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Dibromochloromethane ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Vinyl chloride ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 1,2-Dichloroethane ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 1,1-Dichloroethene ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 . cis-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 trans-1,2-Dichloroethene ND ug/1 100. 1.0 100 9/14/00. 17:09 M.Himelick 601 3759 1,2-Dichloropropane ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 cis-1,3-Dichloropropene ND ug/1 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fxx: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 3510 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 210. ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A127719 Sample ID: SLS-GW-PT1D Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 100. ------- 1.0 ------ 100 -------- 9/14/00 ----- 17:09 ---------- M.Himelick --------- 601 ----- 3759 500. 5.0 100 9/14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/-14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 100. 1.0 100 9/14/00 17:09 M.Himelick 601 3759 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 72. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 88. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127719 Sample ID: SLS-GW-PT1D Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (u��,/ �ytt.a.�.� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell,.Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 - End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0'177 / FAX: 615-726-0954 / 800-765-0980 Test merica __- I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127707 Sample ID: SLS-GW-PT2D Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 13:50 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602 3758 Chlorobenzene ND ug/l 100. 1.0 100 9/15/00 5:00 M-.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 100. 1.0 100 9/15/00 5:00 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602/601 3758 Ethylbenzene ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602 3758 Toluene ND ug/1 100. 1.0 100 9/15/00 5:00 M.Himelick 602 3758 m,p-Xylenes ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602 3758 o-Xylene ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 602 3758 Bromodichloromethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Bromoform ND ug/l 100. 2.0 100 9/15/00 5:00 M.Himelick 601 3758 Bromomethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Carbon tetrachloride ND ug/1 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Chloroethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/15/00 5,:00 M.Himelick 601 3758 Chloroform ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Chloromethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Dibromochloromethane ND ug/1 100. 1.6 100 9/15/00 5:00 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Vinyl chloride ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Sample report continued . . . i 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E 0 ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/l cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene ND ug/l 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/l 1,1,2,27Tetrachloroethane ND ug/1 Tetrachloroethene 2440 ug/l 1,1,1-Trichloroethane ND. ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127707 Sample ID: SLS-GW-PT2D Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 100. ------- 1.0 ------ t00 -------- 9/15/00 ----- 5:00 ---------- M.Himelick --------- 601 ----- 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 500. 5.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 100. 1.0 100 9/15/00 5:00 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 68. Hall Surr., chloroprene 66. Hall Surr., 1-chloro-3-fluorobenzene 96. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D � I ANALYTICAL REPORT Laboratory Number: 00-A127707 Sample ID: SLS-GW-PT2D Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: )9- -VLj-i✓ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 i Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- Lab Number: 00-A131792 Sample ID: SLS-GW-PT3D Sample Type: Ground water Site ID: Date Collected: 9/ 9/00 Time Collected: 14:28 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 602/601 9810 1,2-Dichlorobenzene ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 602/601 9810 1,3-Dichlorobenzene ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 602/601 9810 1,4-Dichlorobenzene ND. ug/l 100. 1.0 100 9/22/00 18:24: M.Himelick 602/601 9810 Bromodichloromethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Bromoform ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick. 601 9810 Bromomethane ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Carbon tetrachloride ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Chloroethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 2-Chloroethylvinylether ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Chloroform ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Chloromethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Dibromochloromethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Ethylene Dibromide ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Vinyl chloride ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Dichlorodifluoromethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 1,1-Dichloroethane ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 604 9810 1,2-Dichloroethane ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 1,1-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 cis-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 1,2-Dichloropropane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 cis-1,3-Dichloropropene ND ug/1 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 trans-1,3-Dichloropropene ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Methylene chloride ND ug/1 500. 5.0 100 9/22/00 18:24 M.Himelick 601 9810 1,1,2,2-Tetrachloroethane ND ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Tetrachloroethene 140. ug/l 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHvu.►.EJN 37204 / 615-726-01'77 / FAX: 615-726-0954 / 800-765-0980 Analyte 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Test merica I N C O R P O R A T E D ANALYTICAL REPORT Result Units ----------- ND ------- ug/l ND ug/l 6390 ug/1 ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131792 Sample ID: SLS-GW-PT3D Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 100. ------ 1.0 ------ 100 -------- 9/22/00 ------ 18:24 ----------- M.Himelick --------- 601 ----- 9810 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 100. 1.0 100 9/22/00 18:24 M.Himelick 601 9810 Recovery PID Surr., a,a,a-trifluorotoluene 104 Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 104 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: _ Report Date: 9/26/00 - Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project:.107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131791 Sample ID: SLS-GW-PT4D Sample Type: Ground water Site ID: Date Collected: 9/ 9/00 Time Collected: 15:04 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ------------------------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND' ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 602/601 9810 1,2-Dichlorobenzene ND" ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 602/601 9810 1,3-Dichlorobenzene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 602/601 9810 1,4-Dichlorobenzene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 602/601 9810 Bromodichloromethane ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Bromoform ND ug/1 500. 1:0 500 9/22/00 14:38 M.Himelick 601 9810 Bromomethane ND ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Carbon tetrachloride ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Chloroethane ND ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 2-Chloroethylvinylether ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Chloroform Nb ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 ,9810 Chloromethane i ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Dibromochloromethane ND ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Ethylene Dibromide ND ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Vinyl chloride ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 1,1-Dichloroethane ND ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 60-1 9810 1,2-Dichloroethane ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 1,1-Dichloroethene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 cis-1,2-Dichloroethene 1150 ug/1 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 trans-1,2-Dichloroethene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 1,2-Dichloropropane ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 cis-1,3-Dichloropropene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 trans-1,3-Dichloropropene ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Methylene chloride ND ug/1 2500 5.0 500 9/22/00 14:38 M.Himelick 601 9810 1,1,2,2-Tetrachloroethane ND ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Tetrachloroethene 1350 ug/l 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Sample report continued 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726--0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R F 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/1 Trichloroethene 15400 ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Laboratory Number: 00-A131791 Sample ID: SLS-GW-PT4D Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 500. ------ 1.0 ------ 500 -------- 9/22/00 ------ 14:38 ----------- M.Himelick --------- 601 ----- 9810 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 500. 1.0 500 9/22/00 14:38 M.Himelick 601 9810 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 90. Hall Surr., chloroprene 94. Hall Surr., 1-chloro-3-fluorobenzene 101. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: C �n D Ct a C' Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-01'77 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT IT CORPORATION/GTI 2309 i KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name:. Sampler: D.LUBELL/K.SUMNER Analyte ------------------------ *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane Lab Number: 00-A127717 Sample ID: SLS-GW-PT5D Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 13:58 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch 800. ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602/601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602/601 . 3759 ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 602/601 3759 ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 602/601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602 3759 600. ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 602 3759 ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/1 500. 2.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759' ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl-�merica ANALYTICAL REPORT Laboratory Number: 00-A127717 Sample ID: SLS-GW-PT5D Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1-Dichloroethene ----------- ND ------ ug/l ------- 500. ------- 1.0 ------ 500 -------- 9/14/00 ----- 11:30 ---------- M.Himelick --------- 601 ----- 3759 cis-1,2-Dichloroethene ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 trans-1,2-Dichloroethene ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 1,2-Dichloropropane ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 cis-1,3-Dichloropropene ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 trans-1,3-Dichloropropene ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 Methylene chloride ND ug/1 2500 5.0 500 9/14/00 11:30 M.Himelick 601 3759 1,1,2,2-Tetrachloroethane ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 Tetrachloroethene 18300 ug/1 1000 1.0 1000 9/19/00 0:57 M.Himelick 601 3759 1,1,1-Trichloroethane ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 1,1,2-Trichloroethane ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 Trichloroethene ND ug/1 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 Trichlorofluoromethane ND ug/l 500. 1.0 500 9/14/00 11:30 M.Himelick 601 3759 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 71. Hall Surr., chloroprene 86. Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. Sample report continued . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�me'rica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler:.D.LUBELL/K.SUMNER Lab Number: 00-A127685 Sample ID: SLS-GW-SVE1 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 11:50 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND" ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 602/601 3756 - Bromodichloromethane ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756. Bromoform ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Bromomethane - - ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Carbon tetrachloride ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Chloroethane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Chloroform ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Chloromethane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Dibromochloromethane ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Vinyl chloride ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 1,2-Dichloroethane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 cis-1,2-Dichloroethene 7.5 ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177"/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127685 Sample ID: SLS-GW-SVE1 Page 2 Report Quan Dil Analysis Analysis Analyte Result ------------------------ Units Limit Limit Factor Date Time Analyst Method Batch ----------- trans-1,3-Dichloropropene ND ------ ug/l ------ 1.0 ------- 1.0 ------ 1 -------- 9/10/00 ----- 6:34 ---------- M.Himelick --------- 601 ----- 3756 Methylene chloride ND ug/l 5.0 5.0 1 9/10/00 6:34 M.Himelick 601 3756 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Tetrachloroethene 2760 ug/l .50.0 1.0 50 9/14/00 13:55 M.Himelick 601 3756 1,1,1-Trichloroethane ND ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 1,1,2-Trichloroethane ND ug/1 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Trichloroethene 17.4 ug/l 1.0 1.0 1 9/10/00 6:34 M.Himelick 601 3756 Trichlorofluoromethane ND ug/l 1.0 1.0. 1 9/10/00 6:34 M.Himelick 601 3756 ND - Not detected at the report limit. Surrogate % Recovery Target Range PID Surr., a,a,a-trifluorotoluene 105. 50. - 150. Hall Surr., 2-chloropropane 81. 49. - 125. Hall Surr., chloroprene 87. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 109. 25. - 157. # - Recovery outside Laboratory historical limits. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177-/ FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127685 Sample ID: SLS-GW-SVE1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. tl- Report Approved By: LUAU l � �jv�. Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical. Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 T,e,stj�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte ------------------------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A127703 Sample ID: SLS-GW-SVE2 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 18:50 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Result Units Limit Limit Factor Date Time Analyst Method Batch ----------- ------ ------------- -------------- ------------------------ ----- ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 602/601 3758 ND' ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 602/601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 602/601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 602/601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758: ND ug/l 500. 2.0 500 9/15/00 3:33 M.Himelick 601 3738 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00, 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 1850 ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/1 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 ND ug/l 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 3700 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/L Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A127703 Sample ID: SLS-GW-SVE2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 500. =------ 1.0 ------ 500 -------- 9/15/00 ----- 3:33 ---------- M.Himelick --------- 601 ----- 3758 2500 5.0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1..0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1'.0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 500. 1.0 500 9/15/00 3:33 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 75. Hall Surr., chloroprene 73. Hall Surr., 1-chloro-3-fluorobenzene 95. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • Test merica 1 N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127703 Sample ID: SLS-GW-SVE2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full' and with permission of the laboratory. Report Approved By: (,��;/.� Report Date: 9/19/00 Pau1.E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv., Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical. Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 ;I End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-01"77 % FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte ------------------------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl.chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Result Units ----------- ------ Lab Number: 00-A127697 Sample ID: SLS-GW-SVE3 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 17:08 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- --------------- --------- ----- ND. ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 602/601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 602/601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 602/601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 602/601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758: NO ug/1 5000 2.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/1 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 ND ug/l 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177"/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloroprop6ne ----------- ND ------ ug/l Methylene chloride ND ug/l 111,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 65000 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report -limit. Laboratory Number: 00-A127697 Sample ID: SLS-GW-SVE3 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 5000 ------- 1.0 ------ 5000 -------- 9/13/00 ----- 12:23 ---------- M.Himelick --------- 601 ----- 3758 25000 5.0 5000 9/13/00 12:23 M.Himelick 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick- 601 3758 5000 1.0 5000 9/13/00 12:23 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 63. Hall Surr., chloroprene 65. Hall Surr., 1-chloro-3-fluorobenzene 93. # - Recovery outside Laboratory historical limits. Sample report continued . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 -/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127697 Sample ID: SLS-GW-SVE3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: UZAAJ 4 - rLkA AA/ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S:., Technical Director Glenn L. Norton, Technical. Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0"177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 - Lab Number: 00-A127687 Sample ID: SLS-GW-SVE4 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Project: 107535 Time Collected: 13:00 Project Name: Date Received: 9/ 9/00 Sampler: D.LUBELL/K.SUMNER Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units ------------------------ ----------- ------ Limit Limit Factor ------------- ------ Date Time -------- ----- Analyst Method Batch ------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 602/601 3756 1,3-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 602/601 3756.. Bromodichloromethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756; Bromoform ND ug/l 5000 2.0 5000 9/15/00 14:12 M.Himelick 601 3756 . Bromomethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Carbon tetrachloride ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Chloroethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Chloroform NO ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Chloromethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Dibromochloromethane ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Ethylene Dibromide ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Vinyl chloride ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 1,1-Dichloroethane ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 1,1-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 1,2-Dichloropropane ND ug/1 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 cis-1,3-Dichloropropene ND ug/l 50b0 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 126000 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l ND - Not detected at the report.limit. Surrogate ------------- Laboratory Number: 00-A127687 Sample ID: SLS-GW-SVE4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 5000 ------- 1.0 ------ 5000 -------- 9/15/00 ----- 14:12 ---------- M.Himelick --------- 601 ----- 3756 25000 5.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 5000 1.0 5000 9/15/00 14:12 M.Himelick 601 3756 Recovery PID Surr., a,a,a-trifluorotoluene 107. Hall Surr., 2-chloropropane - 97. Hall Surr., chloroprene 92. Hall Surr., 1-chloro-3-fluorobenzene 120. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127687 Sample ID: SLS-GW-SVE4 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical S.erv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv: Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0477 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127686 Sample ID: SLS-GW-SVE5 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 12:20 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ --- ------ ------ ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 602/601 3756 1,2-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 602/601 3756 a 1,3-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 602/601 3756 1,4-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick .602/601 3756 Bromodichloromethane ND. ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756: Bromoform ND ug/1 5000 2.0 5000 9/15/00 13:30 M.Himelick 601 3756 Bromomethane ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Carbon tetrachloride ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Chloroethane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 2-Chloroethylvinylether ND ug/1. 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Chloroform ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Chloromethane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Dibromochloromethane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Ethylene Dibromide ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Vinyl chloride ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Dichlorodifluoromethane ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 1,1-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 1,2-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 1,1-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 cis-1,2-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 trans-1,2-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756- 1,2-Dichloropropane ND ug/l 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 j cis-1,3-Dichloropropene ND ug/1 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 TuAnstl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 130000 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethane ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A127686 Sample ID: SLS-GW-SVE5 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst ---------- Method Batch ------ 5000 ------- 1.0 ------ 5000 -------- 9/15/00 ----- 13:30 M.Himelick --------- 601 ----- 3756 25000 5.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 5000 1.0 5000 9/15/00 13:30 M.Himelick 601 3756 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 105. Hall Surr., 2-chloropropane 100. Hall Surr., chloroprene 100. Hall Surr., 1-chloro-3-fluorobenzene 113. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. ,- Sample report continued . . . I ' 1 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A127686 Sample ID: SLS-GW-SVE5 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: _"-A 9 KA-4-W Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S.., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford,.Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127712 Sample ID: SLS-GW-SVE6 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 10:10 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis... Analyte ------------------------ Result ----------- Units ------ Limit ----=- Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND` ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 602/601 3759 1,2-Dichlorobenzene ' ND: ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 602/601 3759 1,4-Dichlorobenzene ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 602/601 3759 Bromodichloromethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759. Bromoform ND ug/l 500. 2.0 500 9/13/00 19:15 M.Himelick 601 3759 Bromomethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Carbon tetrachloride ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Chloroethane ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 2-Chloroethylvinylether ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Chloroform ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Chloromethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Dibromochloromethane ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 500. 1:0 500 9/13/00 19:15 M.Himelick 601 3759 Vinyl chloride ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 1,2-Dichloroethane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 1,1-Dichloroethene ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 cis-1,2-Dichloroethene ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 trans-1,2-Dichloroethene ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 1,2-Dichloropropane ND ug/l 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 cis-1,3-Dichloropropene ND ug/1 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 I Sample report continued . . . i 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 7 FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 20600 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Laboratory Number: 00-A127712 Sample ID: SLS-GW-SVE6 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 500. ------- 1.0 ------ 500 -------- 9/13/00 ----- 19:15 ---------- M.Himelick --------- 601 ----- 3759 2500 5.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 500. 1.0 500 9/13/00 19:15 M.Himelick 601 3759 Surrogate % Recovery ----------------------- PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 72. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 91. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca IN CORPO RATED ANALYTICAL REPORT Laboratory Number: 00-A127712 Sample ID: SLS-GW-SVE6 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. <' Report Approved By: UAAJ '4 ,,/L4AA,,Al Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S:., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assis.tant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177T/ FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 Lab Number: 00-A127696 KIM TITMUS Sample ID: SLS-GW-SVE7 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/ 7/00 Project: 107535 Time Collected: 16:20 Project Name: Date Received: 9/ 9/00 Sampler: D.LUBELL/K.SUMNER Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units ----------------------------------- ------ Limit Limit Factor ------------- ------ Date Time -------- ----- Analyst Method Batch ------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 602/601 3758 1,3-Dichlorobenzene NO ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 602/601 3758 Bromodichloromethane ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758: Bromoform ND ug/1 100. 2.0 100 9/14/00 21:43 M.Himelick 601 3758 Bromomethane ND ug/l 100. 1.0 100 9/14/00 21.43 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Chloroethane ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Chloroform ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Chloromethane ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Dibromochloromethane ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Vinyl chloride ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 1,1-Dichloroethane ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 1,1-Dichloroethene ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 cis-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 1,2-Dichloropropane ND ug/l 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/1 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Testl�merisca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 5310 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report -limit. Laboratory Number: 00-A127696 Sample ID: SLS-GW-SVE7 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 100. ------- 1.0 ------ 100 -------- 9/14/00 ----- 21:43 ---------- M.Himelick --------- 601 ----- 3758 500. 5.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 100. 1.0 100 9/14/00 21:43 M.Himelick 601 3758 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 103. Hall Surr., 2-chloropropane 67. Hall Surr., chloroprene 64. Hall Surr., 1-chloro-3-fluorobenzene 113. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT Laboratory Number: 00-A127696 Sample ID: SLS-GW-SVE7 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (ta 1A,(_ '., n-LLkA/ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E 0 ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE20.5 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127708 Sample ID: SLS-GW-SVE8 Sample Type: Water Site ID: Date Collected: 9/.8/00 Time Collected: 14:40 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602 3758 Chlorobenzene ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602/601 3758: Ethylbenzene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602 3758 Toluene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602 3758 m,p-Xylenes ND ug/l 500. 1.0. 500 9/15/00 5:44 M.Himelick 602 3758 o-Xylene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 602 3758 Bromodichloromethane ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Bromoform ND ug/l 500. 2.0 500 9/15/00 5:44 M.Himelick 601 3758 Bromomethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Chloroethane ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Chloroform ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Chloromethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Dibromochloromethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 . Vinyl chloride ND ug/l 500. 1.0 500 9/15/00. 5:44 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Sample report continued . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testllmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127708 Sample ID: SLS-GW-SVE8 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1-Dichloroethene ----------- ND ------ ug/1 ------ 500. ------- 1.0 ------ 500 -------- 9/15/00 ----- ,5:44 ---------- M.Himelick --------- 601 ----- 3758 cis-1,2-Dichloroethene ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 1,2-Dichloropropane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 trans-1,3-Dichloropropene ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Methylene chloride ND ug/1 2500 5.0 500 9/15/00 5:44 M.Himelick 601 3758 1,1,2,2-Tetrachloroethane ND. ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Tetrachloroethene 13200 ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 1,1,1-Trichloroethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 1,1,2-Trichloroethane ND ug/l 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Trichloroethene ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 Trichlorofluoromethane ND ug/1 500. 1.0 500 9/15/00 5:44 M.Himelick 601 3758 ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 77. Hall Surr., chloroprene 65. Hall Surr., 1-chloro-3-fluorobenzene 108. # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT, Laboratory Number: 00-A127708 Sample ID: SLS-GW-SVE8 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: W-�AA '-- VL-1j/j Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S'_ Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Txestllmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------------------ ----------- ------- *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Sample report continued . . . Lab Number: 00-A131795 Sample ID: SLS-GW-SVE9 Sample Type: Ground water Site ID: Date Collected: 9/ 9/00 Time Collected: 12:04 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ ------ -------- -------------------------- ----- ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 602 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 602/601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 602/601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 602/601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 602/601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 602 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 602 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 602 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 602 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick- 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/l 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 ND ug/1 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ cis-1,3-Dichloropropene ----------- ND ------- ug/1 trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 1090 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND. ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate' ------------- Laboratory Number: 00-A131795 Sample ID: SLS-GW-SVE9 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 20:30 ----------- M.Himelick --------- 601 ----- 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 250. 5.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0 50 9/22/00 20:30 M.Himelick 601 9810 50.0 1.0. 50 9/22/00 20:30 M.Himelick 601 9810 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 81. Hall Surr., chloroprene 85. Hall Surr., 1-chloro-3-fluorobenzene 105. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726=0177' / FAX: 615-726-0954 / 800-765-0980 Te merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131795 Sample ID: SLS-GW-SVE9 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: arT f f Paul-E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly.S. Comstock, Technical Serv.. Pamela A. Langford, Technical Serv. Laboratory Certification Number:,387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131775 KIM TITMUS Sample ID: SLS-GW-SVE10 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/12/00 Project: Time Collected: 13:02 Project Nammee:: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 602/601 .9809 1,3-Dichlorobenzene ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND. ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 602/601 9809 Bromodichloromethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Bromoform ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick. 601 9809 Bromomethane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Carbon tetrachloride ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Chloroethane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Chloroform ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Chloromethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Vinyl chloride ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 cis-1,2-Dichloroethene 4600 ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Methylene chloride ND ug/l 5000 5.0 1000 9/24/00 4:10 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Tetrachloroethene ND ug/l 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Sample,report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 7 FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T S D ANALYTICAL REPORT Laboratory Number: 00-A131775 Sample ID: SLS-GW-SVE10 Page 2 Report Quan Di1 Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1,1-Trichloroethane ----------- ND ------- ug/l ------- 1000 ------ 1.0 ------ 1000 -------- 9/24/00 ------ 4:10 ----------- M.Himelick --------- 601 ----- 9809 1,1,2-Trichloroethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Trichloroethene 60600 ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 Trichlorofluoromethane ND ug/1 1000 1.0 1000 9/24/00 4:10 M.Himelick 601 9809 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 105 Hall Surr., 2-chloropropane 76. Hall Surr., chloroprene 80. Hall Surr., 1-chloro-3-fluorobenzene 92. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Qaa (Tact(, Report Date: 9/26/00 Paul E. Lane, Jr.,, Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 _ KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131774 Sample ID: SLS-GW-SVE11 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 13:38 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Sample report continued . . . ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 602/601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 602/601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 602/601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 602/601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 _ 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 13200 ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 5000 5.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/l 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 ND ug/1 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND — Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131774 Sample ID: SLS-GW-SVE11 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1000 ------ 1.0 ------ 1000 -------- 9/24/00 ------ 3:28 ----------- M.Himelick --------- 601 ----- 9809 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 1000 1.0 1000 9/24/00 3:28 M.Himelick 601 9809 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 79. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 79. # — Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 ICIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131773 Sample ID: SLS-GW-SVE12 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 15:22 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------ - ----------- Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 1000 1.0 lobo 9/24/00 1:22 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 1000 1.0 1000 9/24/00 1 M M.Himelick 601 9809 Bromoform ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick. 601 9809 Bromomethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Carbon tetrachloride ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809. Chloroethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Chloroform ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Chloromethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Dibromochloromethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Vinyl chloride ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1,1-Dichloroethane ND ug/1 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1,1-Dichloroethene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 cis-1,2-Dichloroethene 12200 ug/1 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Methylene chloride ND ug/l 5000 5.0 1000 9/24/00 1:22 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Tetrachloroethene ND ug/1 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene 12800 ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131773 Sample ID: SLS-GW-SVE12 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1000 ------ 1.0 ------ 1000 -------- 9/24/00 ------ 1:22 ----------- M.Himelick --------- 601 ----- 9809 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 1000 1.0 1000 9/24/00 1:22 M.Himelick 601 9809 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 76. Hall Surr., chloroprene 82. Hall Surr., 1-chloro-3-fluorobenzene 81. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By:C , A w o o a Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131772 Sample ID: SLS-GW-SVE13. Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 16:03 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------ - ----------- ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 602/601 9809 1,2-Dichlorobenzene ND ug/l 5.0 1.0' 5 9/24/00 0:39 M.Himelick 602/601 9809 1,3-Dichlorobenzene ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 602/601 9809 1,4-Dichlorobenzene ND ug/1 5.0 1.0 5 9/24/00 0:39 M.Himelick 602/601 9809 Bromodichloromethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Bromoform ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Bromomethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Carbon tetrachloride ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Chloroethane ND ug/1 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 2-Chloroethylvinylether ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Chloroform ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Chloromethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Dibromochloromethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Ethylene Dibromide ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Vinyl chloride ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Dichlorodifluoromethane ND ug/1 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 1,1-Dichloroethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 1,2-Dichloroethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 1,1-Dichloroethene ND ug/1 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 cis-1,2-Dichloroethene 140. ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 trans-1,2-Dichloroethene ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 1,2-Dichloropropane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 cis-1,3-Dichloropropene ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 trans-1,3-Dichloropropene ND ug/1 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Methylene chloride ND ug/l 25.0 5.0 5 9/24/00 0:39 M.Himelick 601 9809 1,1,2,2-Tetrachloroethane ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Tetrachloroethene ND ug/l 5.0 1.0 5 9/24/00 0:39 M.Himelick 601 9809 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177' / FAX: 615-726-0954 / 800-765-0980 Analyte 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Result Units ND ug/l ND ug/l ND ug/l ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131772 Sample ID: SLS-GW-SVE13 Page 2 Report Quan Dil Limit Limit Factor ------- ------ ------ 5.0 1.0 5 5.0 1.0 5 5.0 1.0 5 5.0 1.0 5 Analysis Analysis Date Time Analyst Method Batch -------- 9/24/00 ------ 0:39 ----------- M.Himelick --------- 601 ----- 9809 9/24/00 0:39 M.Himelick 601 9809 9/24/00 0:39 M.Himelick 601 9809 9/24/00 0:39 M.Himelick 601 9809 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 76. Hall Surr., chloroprene 80. Hall Surr., 1-chloro-3-fluorobenzene 81. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Lab Number: 00-A127700 Sample ID: SLS-GW-DUP01 Sample Type: Water Site ID: Date Collected: 9/ 7/00 Time Collected: 18:49 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602 3758 Chlorobenzene ND'- ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/1 500. 1.0 500 9/15/00 2:06 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602/601 3758 - 1,4-Dichlorobenzene ND ug/1 500. 1.0 500 9/15/00 2:06 M.Himelick 602/601 3758: Ethylbenzene ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602 3758 Toluene ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602 3758 m,p-Xylenes ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602 3758 o-Xylene ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 602 3758 Bromodichloromethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Bromoform ND ug/l 500. 2.0 500 9/15/00 2:06 M.Himelick 601 3758 Bromomethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Chloroethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Chloroform ND ug/1 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Chloromethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Dibromochloromethane ND ug/1 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Vinyl chloride ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ Fat: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/l cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 26200 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A127700 Sample ID: SLS-GW-DUP01 Page 2 Report Quan Dil Analysis, Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 500. ------- 1.0 ------ 500 -------- 9/15/00 ----- 2:06 ---------- M.Himelick --------- 601 ----- 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 2500 5.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0, 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3`758 500. 1.0 500 9/15/00 2:06 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 105 Hall Surr., 2-chloropropane 63. Hall Surr., chloroprene 65. Hall Surr., 1-chloro-3-fluorobenzene 107 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177"/ FAx: 615-726-0954 / 800-765-0980 Testl= merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127700 Sample ID: SLS-GW-DUP01 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: r„�,,,/ mk,'-C� Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S.., Technical Director Glenn L. Norton, Technical.Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL STE205 Lab Number: 00-A131748 Sample ID: SLS-GW-DUP04 Sample Type: Ground water Site ID: Date Collected: 9/13/00 Time Collected: 15:35 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------- Limit ------- Limit ------ Factor ------ Date -------- Time ------ Analyst ----------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/21/00. 21:51 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 602/601 9805 Bromodichloromethane i, ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Bromoform ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Bromomethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Chloroethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Chloroform ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Chloromethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Dibromochloromethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Vinyl chloride ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 cis-1,2-Dichloroethene ND . ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 ,9805 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Methylene chloride ND ug/l 250. 5.0 50 9/21/00 21:51 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Tetrachloroethene 650. ug/l 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 100. ug/l Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131748 Sample ID: SLS-GW-DUP04 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/21/00 ------ 21:51 ----------- M.Himelick --------- 601 ----- 9805 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 50.0 1.0 50 9/21/00 21:51 M.Himelick 601 9805 Recovery PID Surr., a,a,a-trifluorotoluene 102 Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 109 # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By:( kA - �-164(t(j Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0477 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Lab Number: 00-A127714 Sample ID: SLS-GW-DUP02 Sample Type: Water Site ID: Date Collected: 9/ 8/00 Time Collected: 11:10 Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- Benzene ND: ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 602 3759 Chlorobenzene ND. ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602%601 3759 1,2-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602/601 3759 1,3-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602/601 3759 . 1,4-Dichlorobenzene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602/601 3759 Ethylbenzene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602 3759 . Toluene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602 3759 m,p-Xylenes ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602 3759 o-Xylene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 602 3759 Bromodichloromethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Bromoform ND ug/1 5000 2.0 5000 9/15/00 20:32 M.Himelick 601 3759 Bromomethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Carbon tetrachloride ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Chloroethane ND. ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 2-Chloroethylvinylether ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Chloroform ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Chloromethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Dibromochloromethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Ethylene Dibromide ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Vinyl chloride ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Dichlorodifluoromethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 1,1-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 1,2-Dichloroethane ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0'177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127714 Sample ID: SLS-GW-DUP02 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 ------ 5000 ------- 1.0 ------ 5000 -------- 9/15/00 ----- 20:32 ---------- M.Himelick --------- 601 ----- 3759 cis-1,2-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 trans-1,2-Dichloroethene ND ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 1,2-Dichloropropane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 cis-1,3-Dichloropropene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 trans-1,3-Dichloropropene ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Methylene chloride ND ug/1 25000 5.0 5000 9/15/00 20:32 M.Himelick 601 3759 1,1,2,2-Tetrachloroethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Tetrachloroethene 154000 ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 37.59 1,1,1-Trichloroethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 1,1,2-Trichloroethane ND ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Trichloroethene ND' ug/l 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 Trichlorofluoromethane ND" ug/1 5000 1.0 5000 9/15/00 20:32 M.Himelick 601 3759 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 100 Hall Surr., 2-chloropropane 63. Hall Surr., chloroprene 86. Hall Surr., 1-chloro-3-fluorobenzene 89. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177' / FAX: 615-726-0954 / 800-765-0980 Test merica II N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127714 Sample ID: SLS-GW-DUP02 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (44 AAJ n {r'U-&A-)'/ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131793 Sample ID: SLS-GW-DUP03 Sample Type: Ground water Site ID: Date Collected: 9/ 9/00 Time Collected: 14:28 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ -------------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 602/601 9810 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 602/601 9810 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 602/601 9810 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 602/601 9810 Bromodichloromethane ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Bromoform ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Bromomethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Chloroethane ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/22%00 19:06 M.Himelick 601 9810 Chloroform ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Chloromethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Dibromochloromethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Vinyl chloride ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Dichlorodifluoromethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 1,1-Dichloroethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 1,2-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 1,1-Dichloroethene ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 cis-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 cis-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Methylene chloride ND ug/l 250. 5.0 50 9/22/00 19:06 M.Himelick 601 9810 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Tetrachloroethene 145. ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�mericNCO RPO a ANALYTICAL REPORT Laboratory Number: 00-A131793 Sample ID: SLS-GW-DUP03 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch 1,1,1-Trichloroethane ----------- ND ------- ug/1 -----'-- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 19:06 ----------- M.Himelick --------- 601 ----- 9810 1,1,2-Trichloroethane ND ug/l 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 Trichloroethene 4900 ug/l 500. 1.0 500 9/23/00 21:51 M.Himelick 601 9810 Trichlorofluoromethane ND ug/1 50.0 1.0 50 9/22/00 19:06 M.Himelick 601 9810 ND — Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 107. Hall Surr., 2-chloropropane 95. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 106. # — Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Paul E. Lane, Jr., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Serv. Eric S. Smith, Assistant Technical Director End of Sample Report. Report Date: 9/26/00 Gail A. Lage, Technical Serv. Glenn L. Norton, Technical Serv. Kelly S. Comstock, Technical Serv. Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D. LUBELL Lab Number: 00-A131735 Sample ID: SLS-GW-DUP03 Sample Type: Ground water Site ID: Date Collected: 9/12/00 Time Collected: 10:35 Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ ------ -------- -------------------------- ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 602/601 9805 Bromodichloromethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Bromoform ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Bromomethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Carbon tetrachloride ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Chloroethane ND ug/1 - 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Chloroform ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Chloromethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Dibromochloromethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Ethylene Dibromide ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Vinyl chloride ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 1,2-Dichloroethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 trans=1,2-Dichloroethene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 cis-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 trans-1,3-Dichloropropene ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Methylene chloride ND ug/l 250. 5.0 50 9/21/00 20:28 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Tetrachloroethene 2280 ug/1 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1,1-Trichloroethane ----------- ND ------- ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 1230 ug/1 Trichlorofluoromethane ND ug/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A131735 Sample ID: SLS-GW-DUP03 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 50.0 ------ 1.0 ------ 50 -------- 9/21/00 ------ 20:28 ----------- M.Himelick --------- 601 ----- 9805 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 50.0 1.0 50 9/21/00 20:28 M.Himelick 601 9805 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 96. Hall Surr., chloroprene 104. Hall Surr., 1-chloro-3-fluorobenzene 119. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: 0 ku-s (ugho Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director G1enn.L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131754 KIM TITMUS Sample ID: SLS-GW-DUP05 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Date Collected: 9/14/00 Project: 107535 Time Collected: 10:00 Project Name: Date Received: 9/16/00 Sampler: D. LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------- ------- ------ ------ -------- -------------------------- ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 602 9808 Chlorobenzene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 602/601 9808 1,2-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 602/601 9808 1,3-Dichlorobenzene ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 602/601 9808 1,4-Dichlorobenzene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 602/601 9808 Ethylbenzene ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 602 9808 Toluene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 602 9808 m,p-Xylenes ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 602 9808 o-Xylene ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 602 9808 Bromodichloromethane ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Bromoform ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Bromomethane ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Carbon tetrachloride ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Chloroethane ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 2-Chloroethylvinylether ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Chloroform ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Chloromethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Dibromochloromethane 50.0 ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Ethylene Dibromide ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 _ Vinyl chloride ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Dichlorodifluoromethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 1,1-Dichloroethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 1,2-Dichloroethane ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 1,1-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 cis-1,2-Dichloroethene 175. ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 trans-1,2-Dichloroethene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 1,2-Dichloropropane ND ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177'/ FAX: 615-726-0954 / 800-765-0980 Testj�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131754 Sample ID: SLS-GW-DUP05 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units Limit Limit Factor Date Time Analyst Method Batch cis-1,3-Dichloropropene ND ------- ug/1 ------- 50.0 ------ 1.0 ------ 50 -------- 9/22/00 ------ 9:43 ----------- M.Himelick --------- 601 ----- 9808 trans-1,3-Dichloropropene ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Methylene chloride ND ug/l 250. 5.0 50 9/22/00 9:43 M.Himelick 601 9808 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Tetrachloroethene 90500 ug/l 5000 1.0 5000 9/25/00 12:32 M.Himelick 601 9808 1,1,1-Trichloroethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 1,1,2-Trichloroethane ND . ug/1 50.0 1.0 50 9/22/00 9:43 M.Himelick_ 601 9808 Trichloroethene 75.0 ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 Trichlorofluoromethane ND ug/l 50.0 1.0 50 9/22/00 9:43 M.Himelick 601 9808 ND — Not detected at the report limit. Surrogate % Recovery ------------- PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 78. Hall Surr., chloroprene 77. Hall Surr., 1-chloro-3-fluorobenzene 96. # — Recovery outside Laboratory historical limits. I Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177"/ FAX: 615-726-0954 / 800-765-0980 Testlimerieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT i Laboratory Number: 00-A131754 Sample ID: SLS-GW-DUP05 Page 3 These results.relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (I�G,1- -, CIA (I OA Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.. Eric S. Smith, :Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testj�merica ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Lab Number: 00-A127709 Sample ID: SLS-GW-TB01 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- Benzene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602 3758 Chlorobenzene ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602/601 3758 Ethylbenzene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602 3758 Toluene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602 3758 m,p-Xylenes ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 602 3758 o-Xylene ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 602 3758 Bromodichloromethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Bromoform ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Bromomethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Chloroethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Chloroform ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Chloromethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Dibromochloromethane ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Ethylene Dibromide ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Vinyl chloride ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te-,Stj�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127709 Sample ID: SLS-GW-TB01 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/l ------ 1.0 ------- 1.0 ------ 1 -------- 9/13/00 ----- 5:05 ---------- M.Himelick --------- 601 ----- 3758 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 trans-1,2-Dichloroethene ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 1,2-Dichloropropane ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 trans-1,3-Dichloropropene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Methylene chloride ND ug/l 5.0 5.0 1 9/13/00 5:05 M.Himelick 601 3758 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Tetrachloroethene ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 1,1,1-Trichloroethane ND. ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 1,1,2-Trichloroethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Trichloroethene ND ug/1 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 Trichlorofluoromethane ND ug/l 1.0 1.0 1 9/13/00 5:05 M.Himelick 601 3758 ND - Not detected at the report limit. Surrogate ------------- Recovery PID Surr., a,a,a-trifluorotoluene 98. Hall Surr., 2-chloropropane 68. Hall Surr., chloroprene 77. Hall Surr., 1-chloro-3-fluorobenzene 72. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127709 Sample ID: SLS-GW-TB01 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: ChAq 4 ,✓ Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT IT CORPORATION/GTI 2309 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL/K.SUMNER Analyte Result Units ------------------------ ----------- ------ Lab Number: 00-A127710 Sample ID: SLS-GW-TB02 Sample Type: Water Site ID: Date Collected: Time Collected: Date Received: 9/ 9/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ ------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Benzene ND. ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 602 3758 Chlorobenzene ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602/601 3758 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 602/601 3758 1,3-Dichlorobenzene ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602/601 3758 1,4-Dichlorobenzene ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602/601 3758 Ethylbenzene ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602 3758 Toluene ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602 3758 m,p-Xylenes ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 602 3758 o-Xylene ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 602 3758 Bromodichloromethane ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Bromoform ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Bromomethane ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Carbon tetrachloride ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Chloroethane ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Chloroform ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Chloromethane ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Dibromochloromethane ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Vinyl chloride ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Dichlorodifluoromethane ND ug/1 1.0 1.0 1 9/13/00 5:48 M.Himelick. 601 3758 1,1-Dichloroethane ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A127710 Sample ID: SLS-GW-TB02 Page 2 Analyte Result Units 1,1-Dichloroethene ND ug/1 cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene ND ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l ND - Not detected at the report limit. Surrogate ------------- Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1.0 ------- 1.0 ------ 1 -------- 9/13/00 ----- 5:48 ---------- M.Himelick --------- 601 ----- 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 5.0 5.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 1.0 1.0 1 9/13/00 5:48 M.Himelick 601 3758 Recovery PID Surr., a,a,a-trifluorotoluene 98. Hall Surr., 2-chloropropane 68. Hall Surr., chloroprene 67. Hall Surr., 1-chloro-3-fluorobenzene 73. Recovery outside Laboratory historical limits. Sample report continued . . . Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testllmerica ANALYTICAL REPORT I N C O R P O R A T E D Laboratory Number: 00-A127710 Sample ID: SLS-GW-TB02 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: b.,,�A *--r AA^J Report Date: 9/19/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical. Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A131731 KIM TITMUS Sample ID: SLS-GW-TB04 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water MORRISVILLE, NC 27560 Site ID: Project: 107535 Project Name: Sampler: D. LUBELL Date Time Date Time Collected: Collected: Received: Received: 9/16/00 9:00 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *VOLATILE ORGANICS by GC* Benzene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602 9805 Chlorobenzene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602/601 9805 1,2-Dichlorobenzene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602/601 9805 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602/601 9805 1,4-Dichlorobenzene ND. ug/l 1.0 1.0. 1 9/21/00 4:59 M.Himelick 602/601 9805 Ethylbenzene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick. 602 9805 Toluene 3.8 ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602 9805 m,p-Xylenes ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602 9805 o-Xylene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 602 9805 Bromodichloromethane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Bromoform ND ug/l .1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Bromomethane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Carbon tetrachloride ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Chloroethane ND ug/1' 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 2-Chloroethylvinylether ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Chloroform ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Chloromethane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Dibromochloromethane ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Ethylene Dibromide ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Vinyl chloride ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Dichlorodifluoromethane ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,1-Dichloroethane ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,2-Dichloroethane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,1-Dichloroethene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 cis-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,2-Dichloropropane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 61.5-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D - ANALYTICAL REPORT Laboratory Number: 00-A131731 Sample ID: SLS-GW-TB04 Page 2 Report Quan Dil Analysis Analysis Analyte ------------------------ Result Units Limit Limit Factor Date Time Analyst Method Batch cis-1,3-Dichloropropene ----------- ND ------- ug/l ------- 1.0 ------ 1.0 ------ 1 -------- 9/21/00 ------ 4:59 ----------- M.Himelick --------- 601 ----- 9805 trans-1,3-Dichloropropene ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Methylene chloride ND ug/1 5.0 5.0 1 9/21/00 4:59 M.Himelick 601 9805 1,1,2,2-Tetrachloroethane ND ug/l 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 Tetrachloroethene ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,1,1-Trichloroethane ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 1,1,2-Trichloroethane ND . ug/1 1.0 1.0 1 9/21/00 '4:59 M.Himelick 601 9805 Trichloroethene ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick. 601 9805 Trichlorofluoromethane ND ug/1 1.0 1.0 1 9/21/00 4:59 M.Himelick 601 9805 ND - Not detected at the report.limit. Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 103. Hall Surr., chloroprene 95. Hall Surr., 1-chloro-3-fluorobenzene 94. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131731 Sample ID: SLS-GW-TB04 Page 3 These results.relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.- Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 KIM TITMUS 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 - Project: 107535 Project Name: Sampler: D. LUBELL Analyte Result Units ------------ ------------ ----------- ------- *VOLATILE ORGANICS by GC* Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Toluene m,p-Xylenes o-Xylene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane _2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane Sample report continued . . . Lab Number: 00-A131797 Sample ID: SLS-GW-TB03 Sample Type: Ground water Site ID: Date Collected: Time Collected: Date Received: 9/16/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- ------ -------------- -------------------------- ----- ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602/601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602/601 9810 ND. ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602/601 9810 ND: ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602/601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602 9810 3.6 ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602 _ 9810 ND" ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 602 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/l 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 . ND ug/l 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/l 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/1 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 ND ug/l 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ cis-1,3-Dichloropropene ----------- ND ------- ug/1 trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene ND ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND" ug/1 ND - Not detected at the report.limit. Surrogate ------------- Laboratory Number: 00-A131797 Sample ID: SLS-GW-TB03 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------- 1.0 ------ 1.0 ------ 1 -------- 9/22/00 ------ 21:55 ----------- M.Himelick --------- 601 ----- 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 5.0 5.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 1.0 1.0 1 9/22/00 21:55 M.Himelick 601 9810 Recovery Target Range PID Surr., a,a,a-trifluorotoluene 102. Hall Surr., 2-chloropropane 87. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 86. # - Recovery outside Laboratory,historical limits. I Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 = Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: 00-A131797 Sample ID: SLS-GW-TB03 Page 3 These results relate only to the items tested. This report shall -not be reproduced except in full and with permission of the laboratory. Report. Approved By: Report Date: 9/26/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S..Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica PROJECT QUALITY CONTROL DATA Matrix Spike Recovery Analyte units Orig. Val. MS Val Spike Conc Recovery Target Range Q.C. Batch Spike Sample --------------- Benzene ------- mg/l ---------- < 0.0010 --------- 0.0219 ---------- 0.0200 --------- 110 ------------ 39. - 150. ---------- 9805 ------------ blank Benzene mg/1 < 0.0010 0.0256 0.0200 128 39. - 150. 9810 00-A132483 Benzene mg/1 < 0.0010 0.0239 0.0200 120 39. - 150. 9810 00-A132487 Chlorobenzene mg/1 < 0.0010 0.0215 0.0200 108 55. - 135. 9805 blank Chlorobenzene mg/1 < 0.0010 0.0216 0.0200 108 55. - 135. 9805 00-A131746 Chlorobenzene mg/1 < 0.0010 0.0231 0.0200 116 55. - 135. 9808 00-A131758 Chlorobenzene mg/1 < 0.0010 0.0207 0.0200 104 55. - 135. 9808 00-A131763 Chlorobenzene mg/1 < 1.000 0.0172 0.0200 86 55. - 135. 9809 00-A131771 Chlorobenzene mg/1 < 1.000 0.0206 0.0200 103 55. - 135. 9809 00-A131776 Chlorobenzene mg/1 < 0.0010 0.0201 0.0200 100 55. - 135. 9810 00-A132483 Chlorobenzene mg/l < 0.0010 0.0247 0.0200 124 55. - 135. 9810 00-A132487 1,2-Dichlorobenzene mg/1 < 0.0010 0.0182 0.0200 91 37. - 154. 9805 blank 1,2-Dichlorobenzene mg/1. < 0.0010 0.0217 0.0200 108 37. - 154. 9805 00-A131746 1,2-Dichlorobenzene mg/1 < 0.0010 0.0216 0.0200 108 37. - 154. 9808 00-A131758 1,2-Dichlorobenzene mg/l < 0.0010 0.0197 0.0200 98 37. - 154. 9808 00-A131763 1,2-Dichlorobenzene mg/l < 1.000 0.0211 0.0200 106 37. - 154. 9809 00-A131771 1,2-Dichlorobenzene mg/l < 1.000 0.0230 0.0200 115 37. - 154. 9809 00-A131776 1,2-Dichlorobenzene mg/l < 0.0010 0.0205 0.0200 102 37. - 154. 9810 00-A132483 1,2-Dichlorobenzene mg/1 < 0.0010 0.0189 0.0200 94 37. - 154. 9810 00-A132487 1,3-Dichlorobenzene mg/1 < 0.0010 0.0221 0.0200 110 50. - 141. 9805 blank 1,3-Dichlorobenzene mg/1 < 0.0010 0.0229 0.0200 114 50. - 141. 9805 00-A131746 1,3-Dichlorobenzene mg/1 < 0.0010 0.0209 0.0200 104 50. - 141. 9808 00-A131758 1,3-Dichlorobenzene mg/1 < 0.0010 0.0221 0.0200 110 50. - 141. 9808 00-A131763 1,3-Dichlorobenzene mg/1 < 1.000 0.0286 0.0200 143# 50. - 141. 9809 00-A131771 1,3-Dichlorobenzene mg/1 < 1.000 0.0253 0.0200 126 50. - 141. 9809 00-A131776 - 1,3-Dichlorobenzene mg/l < 0.0010 0.0221 0.0200 110 50. - 141. 9810 00-A132483 1,3-Dichlorobenzene mg/l < 0.0010 0.0179 0.0200 90 50. - 141. 9810 00-A132487 1,4-Dichlorobenzene mg/l < 0.0010 0.0226 0.0200 113 42. - 143. 9805 blank _ 1,4-Dichlorobenzene mg/l < 0.0010 0.0152 0.0200 76 42. - 143. 9805 00-A131746 1,4-Dichlorobenzene mg/l < 0.0010 0.0166 0.0200 83 42. - 143. 9808 00-A131758 1,4-Dichlorobenzene mg/1 < 0.0010 0.0164 0.0200 82 42. - 143. 9808 00-A131763 1,4-Dichlorobenzene mg/l < 1.000 0.0157 0.0200 78 42. - 143. 9809 00-A131771 1,4-Dichlorobenzene mg/l < 1.000 0.0165 0.0200 82 42. - 143. 9809 00-A131776 1,4-Dichlorobenzene mg/1 < 0.0010 0.0175 0.0200 88 42. - 143. 9810 00-A132483 1,4-Dichlorobenzene mg/1 < 0.0010 0.0160 0.0200 80 42. - 143. 9810 00-A132487 Ethylbenzene mg/1 < 0.0010 0.0199 0.0200 100 32. - 160. 9805 blank Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 � I Test merica I N C O R P O R A T E D PROJECT -QUALITY CONTROL DATA Ethylbenzene mg/1 < 0.0010 0.0224 0.0200 112 32. - 160. 9810 00-A132483 Ethylbenzene mg/1 < 0.0010 0.0218 0.0200 109 32. - 160. 9810 00-A132487 Toluene mg/1 < 0.0010 0.0213 0.0200 106 46. - 148. 9805 blank Toluene mg/1 < 0.0010 0.0239 0.0200 120 46. - 148. 9810 00-A132483 Toluene mg/1 < 0.0010 0.0233 0.0200 116 46. - 148. 9810 00-A132487 6-Xylene mg/1 < 0.0010 0.0215 0.0200 108 74. - 126. 9805 blank _ o-Xylene mg/1 < 0.0010 0.0243 0.0200 122 74. - 126. 9810 00-A132483 o-Xylene mg/1 < 0.0010 0.0240 0.0200 120 74. - 126. 9810 00-A132487 Bromodichloromethane mg/1 < 0.0010 0.0245 0.0200 122 42. - 172. 9805 blank Bromodichloromethane mg/1 < 0.0010 0.0216 0.0200 108 42. - 172. 9805 00-A131746 Bromodichloromethane mg/1 < 0.0010 0.'0195 0.0200 98 42. - 172. 9808 00-A131758 -- Bromodichloromethane mg/1 < 0.0010 0.0208 0.0200 104 42. - 172. 9808 00-A131763 Bromodichloromethane mg/l < 1.000 0.0244 0.0200 122 42. - 172. 9809 00-A131771 Bromodichloromethane mg/l: < 1.000 0.0218 0.0200 109 42. - 172. 9809 00-A131776 Bromodichloromethane mg/1 < 0.0010 0.0198 0.0200 99 42. - 172. 9810 00-A132483 Bromodichloromethane i mg/1 < 0.0010 0.0194 0.0200 97 42. - 172. 9810 00-A132487 Bromoform mg/l < 0.0010 0.0229 0.0200 114 13. - 159. 9805 blank Bromoform mg/1- < 0.0010 0.0177 0.0200 88 13. - 159. 9805 00-A131746 Bromoform mg/1 < 0.0010 0.0177 0.0200 88 13. - 159. 9808 00-A131758 Bromoform mg/1 < 0.0010 0.0189 0.0200 94 13. - 159. 9808 00-A131763 Bromoform mg/1 < 1.000 0.0227 0.0200 114 13. - 159. 9809 00-A131771 _ Bromoform mg/1 < 1.000 0.0209 0.0200 104 13. - 159. 9809 00-A131776 Bromoform mg/1 < 0.0010 0.0169 0.0200 84 13. - 159. 9810 00-A132483 Bromoform mg/1 < 0.0010 0.0203 0.0200 102 13. - 159. 9810 00-A132487 Bromomethane mg/1 < 0.0010 0.0210 0.0200 105 10. - 144. 9805 blank Bromomethane mg/1 < 0.0010 0.0223 0.0200 112 10. - 144. 9805 00-A131746 Bromomethane mg/1 < 0.0010 0.0210 0.0200 105 10. - 144. 9808 00-A131758 Bromomethane mg/1 < 0.0010 0.0212 0.0200 106 10. - 144. 9808 00-A131763 Bromomethane mg/l < 1.000 0.0210 0.0200 105 10. - 144. 9809 00-A131771 Bromomethane mg/1 < 1.000 0.0237 0.0200 118 10. - 144. 9809 00-A131776 Bromomethane mg/1 < 0.0010 0.0205 0.0200 102 10. - 144. 9810 00-A132483 Bromomethane mg/1 < 0.0010 0.0212 0.0200 106 10. - 144. 9810 00-A132487 Carbon tetrachloride i mg/1 < 0.0010 0.0220 0.0200 110 43. - 143. 9805 blank _ Carbon tetrachloride mg/1 < 0.0010 0.0229 0.0200 114 43. - 143. 9805 00-A131746 Carbon tetrachloride mg/1 < 0.0010 0.0211 0.0200 106 43. - 143. 9808 00-A131758 Carbon tetrachloride mg/1 < 0.0010 0.0212 0.0200 106 43. - 143. 9808 00-A131763 Carbon tetrachloride mg/l < 1.000 0.0216 0.0200 108 43. - 143. 9809 00-A131771 Carbon tetrachloride mg/1 < 1.000 0.0213 0.0200 106 43. - 143. 9809 00-A131776 - _ Carbon tetrachloride mg/1 < 0.0010 0.0218 0.0200 109 43. - 143. 9810 00-A132483 Carbon tetrachloride mg/l < 0.0010 0.0198 0.0200 99 43. - 143. 9810 00-A132487 Chloroethane mg/1 < 0.0010 0.0221 0.0200 110 46. - 137. 9805 blank Project QC continued . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Chloroethane mg/l < 0.0010 0.0212 0.0200 106 46. - 137. 9805 00-A131746 Chloroethane mg/l < 0.0010 0.0188 0.0200 94 46. - 137. 9808 00-A131758 Chloroethane mg/l < 0.0010 0.0177 0.0200 88 46. - 137. 9808 00-A131763 Chloroethane mg/1 1.000 0.0209 0.0200 104 46. - 137. 9809 00-A131771 Chloroethane mg/l < 1.000 0.0216 0.0200 108 46. - 137. 9809 00-A131776 Chloroethane mg/1 < 0.0010 0.0200 0.0200 100 46. - 137. 9810 00-A132483 Chloroethane mg/l < 0.0010 0.0191 0.0200 96 46. - 137. 9810 00-A132487 2-Chloroethylvinylether mg/l < 0.0010 0.0193 0.0200 96 14. - 186. 9805 blank 2-Chloroethylvinylether mg/1 < 0.0010 < 0.0010 0.0200 N/A 14. - 186. 9805 00-A131746 2-Chloroethylvinylether mg/l < 0.0010 < 0.0010 0.0200 N/A 14. - 186. 9808 00-A131758 2-Chloroethylvinylether mg/1 < 0.0010 < 0.0010 0.0200 N/A 14. - 186. 9808 00-A131763 2-Chloroethylvinylether mg/l < 1.000 < 0.0010 0.0200 N/A 14. - 186. 9809 00-A131771 2-Chloroethylvinylether mg/l < 1.000 < 0.0010 0.0200 N/A 14. - 186. 9809 00-A131776 2-Chloroethylvinylether mg/1 < 0.0010 0.0058 0.0200 29 14. - 186. 9810 00-A132483 2-Chloroethylvinylether mg/1 < 0.0010 0.0048 0.0200 24 14. - 186. 9810 00-A132487 Chloroform mg/l < 0.0010 0.0211 0.0200 106 49. - 133. 9805 blank Chloroform mg/1 < 0.0010 0.0202 0.0200 101 49. - 133. 9805 00-A131746 Chloroform mg/l < 0.0010 0.0176 0.0200 88 49. - 133. 9808 00-A131758 Chloroform mg/l < 0.0010 0.0214 0.0200 107 49. - 133. 9808 00-A131763 Chloroform mg/l < 1.000 0.0208 0.0200 104 49. - 133. 9809 00-A131771 Chloroform mg/l < 1.000 0.0210 0.0200 105 49. - 133. 9809 00-A131776 Chloroform mg/l < 0.0010 0.0215 0.0200 108 49. - 133. 9810 00-A132483 Chloroform mg/l < 0.0010 0.0190 0.0200 95 49. - 133. 9810 00-A132487 Chloromethane mg/l < 0.0010 0.0208 0.0200 104 10. - 193. 9805 blank Chloromethane mg/l < 0.0010 0.0188 0.0200 94 10. - 193. 9805 00-A131746 Chloromethane mg/l < 0.0010 0.0186 0.0200 93 10. - 193. 9808 00-A131758 Chloromethane mg/1 < 0.0010 0.0176 0.0200 88 10. - 193. 9808 00-A131763 Chloromethane mg/1 < 1.000 0.0193 0.0200 96 10. - 193. 9809 00-A131771 Chloromethane mg/l < 1.000 0.0176 0.0200 88 10. - 193. 9809 00-A131776 Chloromethane mg/1 < 0.0010 0.0158 0.0200 79 10. - 193. 9810 00-A132483 Chloromethane mg/1 < 0.0010 0.0190 0.0200 95 10. - 193. 9810 00-A132487 Dibromochloromethane mg/l < 0.0010 0.0226 0.0200 113 24. - 191. 9805 blank Dibromochloromethane mg/l < 0.0010 0.0211 0.0200 106 24. - 191. 9805 00-A131746 Dibromochloromethane mg/l < 0.0010 0.0187 0.0200 94 24. - 191. 9808 00-A131758 Dibromochloromethane mg/l < 0.0010 0.0209 0.0200 104 24. - 191. 9808 00-A131763 Dibromochloromethane mg/l < 1.000 0.0192 0.0200 96 24. - 191. 9809 00-A131771 Dibromochloromethane mg/1 < 1.000 0.0232 0.0200 116 24. - 191. 9809 00-A131776 Dibromochloromethane mg/l < 0.0010 0.0191 0.0200 96 24. - 191. 9810 00-A132483 Dibromochloromethane mg/l < 0.0010 0.0225 0.0200 112 24. - 191. 9810 00-A132487 Ethylene Dibromide mg/l < 0.0010 0.0218 0.0200 109 70. - 130. 9805 blank Ethylene Dibromide mg/l < 0.0010 0.0215 0.0200 108 70. - 130. 9805 00-A131746 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Ethylene Dibromide mg/1 < 0.0010 0.0198 0.0200 99 70. - 130. 9808 00-A131758 Ethylene Dibromide mg/l < 0.0010 0.0184 0.0200 92 70. - 130. 9808 00-A131763 Ethylene Dibromide mg/l < 1.000 0.0198 0.0200 99 70. - 130. 9809 00-A131771 Ethylene Dibromide mg/1 < 1.000 0.0208 0.0200 104 70. - 130. 9809 00-A131776 Ethylene Dibromide mg/l < 0.0010 0.0179 0.0200 90 70. - 130. 9810 00-A132483 Ethylene Dibromide mg/1 < 0.0010 0.0208 0.0200 104 70. - 130. 9810 00-A132487 Vinyl chloride mg/1 < 0.0010 0.0227 0.0200 114 28. - 163. 9805 blank Vinyl chloride mg/l < 0.0010 0.0216 0.0200 108 28. - 163. 9805 00-A131746 Vinyl chloride mg/l < 0.0010 0.0233 0.0200 116 28. - 163. 9808 00-A131758 Vinyl 'chloride mg/l < 0.0010 0.0241 0.0200 120 28. - 163. 9808 00-A131763 Vinyl chloride mg/1 < 1.000 0.0214 0.0200 107 28. - 163. 9809 00-A131771 Vinyl chloride mg/1 < 1.000 0.0219 0.0200 110 28. - 163. 9809 00-A131776 Vinyl chloride mg/1 < 0.0010 0.0220 0.0200 110 28. - 163. 9810 00-A132483 Vinyl chloride mg/l. < 0.0010 0.0205 0.0200 102 28. - 163. 9810 00-A132487 1,1-Dichloroethane mg/1 < 0.0010 0.0233 0.0200 116 47. - 132. 9805 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0242 0.0200 121 47. - 132. 9805 00-A131746 1,1-Dichloroethane mg/1 < 0.0010 0.0208 0.0200 104 47. - 132. 9808 00-A131758 1,1-Dichloroethane mg/1 < 0.0010 0.0202 0.0200 101 47. - 132. 9808 00-A131763 1,1-Dichloroethane mg/1 < 1.000 0.0215 0.0200 108 47. - 132. 9809 00-A131771 1,1-Dichloroethane mg/1 < 1.000 0.0226 0.0200 113 47. - 132. 9809 00-A131776 1,1-Dichloroethane mg/l < 0.0010 0.0219 0.0200 110 47. - 132. 9810 00-A132483 _ 1,1-Dichloroethane mg/1 < 0.0010 0.0187 0.0200 94 47. - 132. 9810 '00-A132487 1,2=Dichloroethane mg/1 < 0.0010 0.0197 0.0200 98 51. - 147. 9805 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0184 0.0200 92 51. - 147. 9805 00-A131746 1,2-Dichloroethane mg/l < 0.0010 0.0178 0.0200 89 51. - 147. 9808 00-A131758 1,2-Dichloroethane mg/l < 0.0010 0.0184 0.0200 92 51. - 147. 9808 00-A131763 1,2-Dichloroethane mg/l < 1.000 0.0196 0.0200 98 51. - 147. 9809 00-A131771 1,2-Dichloroethane mg/1 0.0048 0.0247 0.0200 100 51. - 147. 9809 00-A131776 1,2-Dichloroethane mg/1 < 0.0010 0.0166 0.0200 83 51. - 147. 9810 00-A132483 1,2-Dichloroethane mg/l < 0.0010 0.0186 0.0200 93 51. - 147. 9810 00-A132487 1,1-Dichloroethene mg/l < 0.0010 0.0233 0.0200 116 28. - 167. 9805 blank 1,1-Dichloroethene mg/1 < 0.0010 0.0209 0.0200 104 28. - 167. 9805 00-A131746 1,1-Dichloroethene mg/1 < 0.0010 0.0213 0.0200 106 28. - 167. 9808 00-A131758 1,1-Dichloroethene mg/1 < 0.0010 0.0221 0.0200 110 28. - 167. 9808 00-A131763 1,1-Dichloroethene mg/l < 1.000 0.0222 0.0200 111 28. - 167. 9809 00-A131771 1,1-Dichloroethene mg/1 < 1.000 0.0207 0.0200 104 28. - 167. 9809 00=A131776 1,1-Dichloroethene mg/1 < 0.0010 0.0237 0.0200 118 28. - 167. 9810 00-A132483 1,1-Dichloroethene mg/1 < 0.0010 0.0207 0.0200 104 28. - 167. 9810 00-A132487 cis-1,2-Dichloroethene mg/1 < 0.0010 0.0217 0.0200 108 76. - 123. 9805 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0226 0.0200 113 76. - 123. 9805 00-A131746 cis-1,2-Dichloroethene mg/1 < 0.0010 0.0198 0.0200 99 76. - 123. 9808 00-A131758 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA cis-1,2-Dichloroethene mg/l < 0.0010 0.0205 0.0200 102 76. - 123. 9808 00-A131763 cis-1,2-Dichloroethene mg/l < 1.000 0.0219 0.0200 110 76. - 123. 9809 00-A131771 cis-1,2-Dichloroethene mg/1 < 0.0010 0.0218 0.0200 109 76. - 123. 9809 00-A131776 cis-1,2-Dichloroethene mg/l < 0.0010 0.0218 0.0200 109 76. - 123. 9810 00-A132483 cis-1,2-Dichloroethene mg/l < 0.0010 0.0196 0.0200 98 76. - 123. 9810 00-A132487 trans-1,2-Dichloroethene mg/l < 0.0010 0.0206 0.0200 103 38. - 155. 9805 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0215 0.0200 108 38. - 155. 9805 00-A131746 trans-1,2-Dichloroethene mg/l < 0.0010 0.0207 0.0200 104 38. - 155. 9808 00-A131758 trans-1,2-Dichloroethene mg/l < 0.0010 0.0205 0.0200 102 38. - 155. 9808 00-A131763 trans-1,2-Dichloroethene mg/l < 1.000 0.0218 0.0200 109 38. - 155. 9809 00-A131771 trans-1,2-Dichloroethene mg/l < 1.000 0.0225 0.0200 112 38. - 155. 9809 00-A131776 trans-1,2-Dichloroethene mg/l < 0.0010 0.0215 0.0200 108 38. - 155. 9810 00-A132483 trans-1,2-Dichloroethene mg/l < 0.0010 0.0220 0.0200 110 38. - 155. 9810 00-A132487 1,2-Dichloropropane mg/l < 0.0010 0.0245 0.0200 122 44. - 156. 9805 blank' 1,2-Dichloropropane mg/l < 0.0010 0.0220 0.0200 110 44. - 156. 9805 00-A131746 1,2-Dichloropropane mg/l < 0.0010 0.0198 0.0200 99 44. - 156. 9808 00-A131758 1,2-Dichloropropane mg/l < 0.0010 0.0246 0.0200 123 44. - 156. 9808 00-A131763 1,2-Dichloropropane mg/1 < 1.000 0.0223 0.0200 112 44. - 156. 9809 00-A131771 1,2-Dichloropropane mg/l < 1.000 0.0192 0.0200 96 44. - 156. 9809 00-A131776 1,2-Dichloropropane mg/1 < 0.0010 0.0184 0.0200 92 44. - 156. 9810 00-A132483 1,2-Dichloropropane mg/l < 0.0010 0.0231 0.0200 116 44. _ 156. 9810 00-A132487 cis-1,3-Dichloropropene mg/l < 0.0010 0.0193 0.0200 96 22. - 178. 9805 blank cis-1,3-Dichloropropene mg/1 < 0:0010 0.0201 0.0260 100 22. - 178. 9805 00-A131746 cis-1,3-Dichloropropene mg/l < 0.0010 0.0178 0.0200 89 22. - 178. 9808 00-A131758 cis-1,3-Dichloropropene mg/l < 0.0010 0.0170 0.0200 85 22. - 178. 9808 00-A131763 cis-1,3-Dichloropropene mg/l < 1.000 0.0198 0.0200 99 22. - 178. 9809 00-A131771 cis-1,3-Dichloropropene mg/l < 1.000 0.0184 0.0200 92 22. - 178. 9809 00-A131776 cis-1,3-Dichloropropene mg/1 < 0.0010 0.0179 0.0200 90 22. - 178. 9810 00-A132483 cis-1,3-Dichloropropene mg/l < 0.0010 0.0203 0.0200 102 22. - 178. 9810 00-A132487 trans-1,3-Dichloropropene mg/1 < 0.0010 0.0259 0.0200 130 22. - 178. 9805 blank . trans-1,3-Dichloropropene mg/1 < 0.0010 0.0195 0.0200 98 22. - 178. 9805 00-A131746 trans-1,3-Dichloropropene mg/l < 0.0010 0.0220 0.0200 110 22. - 178. 9808 00-A131758 trans-1,3-Dichloropropene mg/1 < 0.0010 0.0220 0.0200 110 22. - 178. 9808 00-A131763 trans-1,3-Dichloropropene mg/1 < 1.000 0.0237 0.0200 118 22. - 178. 9809 00-A131771 trans-1,3-Dichloropropene mg/1 < 1.000 0.0199 0.0200 100 22. - 178. 9809 00-A131776 trans-1,3-Dichloropropene mg/1 < 0.0010 0.0214 0.0200 107 22. - 178.. 9810 00-A132483 trans-1,3-Dichloropropene mg/l < 0.0010 0.0235 0.0200 118 22. - 178. 9810 00-A132487 Methylene chloride mg/1 < 0.0050 0.0205 0.0200 102 25. - 162. 9805 blank Methylene chloride mg/1 < 0.0050 0.0269 0.0200 134 25. - 162. 9805 00-A131746 Methylene chloride mg/1 < 0.0050 0.0176 0.0200 88 25. - 162. 9808 00-A131758 Methylene chloride mg/1 < 0.0050 0.0165 0.0200 82 25. - 162. 9808 00-A131763 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Methylene chloride mg/1 < 5.000 0.0242 0.0200 121 25. - 162. 9809 00-A131771 Methylene chloride mg/1 < 5.000 0.0204 0.0200 102 25. - 162. 9809 00-A131776 Methylene chloride mg/1 < 0.0050 0.0172 0.0200 86 25. - 162. 9810 00-A132483 Methylene chloride mg/1 < 0.0050 0.0229 0.0200 114 25. - 162. 9810 00-A132487 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0238 0.0200 119 8. - 184. 9805 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0172 0.0200 86 8. - 184. 9805 00-A131746 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0188 0.0200 94 8. - 184. 9808 00-A131758 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0200 0.0200 100 8. - 184. 9808 00-A131763 1,1,2,2-Tetrachloroethane mg/1 < 1.000 0.0197 0.0200 98 8. - 184. 9809 00-A131771 1,1,2,2-Tetrachloroethane mg/1 < 1.000 0.0202 0.0200 101 8. - 184. 9809 00-A131776 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0174 0.0200 87 8. - 184. 9810 00-A132483 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0186 0.0200 93 8. - 184. 9810 00-A132487 Tetrachloroethene mg/1 < 0.0010 0.0194 0.0200 97 26. - 162. 9805 blank Tetrachloroethene mg/1 < 0.0010 0.0198 0.0200 99 26. - 162. 9805 00-A131746 Tetrachloroethene mg/1 < 0.0010 0.0187 0.0200 94 26. - 162. 9808 00-A131758 Tetrachloroethene mg/1 < 0.0010 0.0204 0.0200 102 26. - 162. 9808 00-A131763 Tetrachloroethene mg/1 0.0010 0.0222 0.0200 111 .26. - 162. 9809 00-A131771 Tetrachloroethene mg/1 < 1.000 0.0216 0.0200 108 26. - 162. 9809 00-A131776 Tetrachloroethene mg/1 < 0.0010 0.0184 0.0200 92 26. - 162. 9810 00-A132483 Tetrachloroethene mg/1 < 0.0010 0.0224 0.0200 112 26. - 162. 9810 00-A132487 1,1,1-Trichloroethane mg/1 < 0.0010 0.0208 0.0200 104 41. - 138. 9805 blank 1,1,1-Trichloroethane mg/1 < 0.0010 0.0206 0.0200 103 41. - 138. 9805 00-A131746 1,1,1-Trichloroethane mg/1 < 0.0010 0.0222 0.0200 111 41. - 138. 9808 00-A131758 1,1,1-Trichloroethane mg/1 < 0.0010 0.0208 0.0200 104 41. - 138. 9808 00-A131763 1,1,1-Trichloroethane mg/1 < 1.000 0.0218 0.0200 109 41. - 138. 9809 00-A131771 1,1,1-Trichloroethane mg/l < 1.000 0.0215 0.0200 108 41. - 138. 9809 00-A131776 1,1,1-Trichloroethane mg/1 < 0.0010 0.0202 0.0200 101 41. - 138. 9810 00-A132483 1,1,1-Trichloroethane mg/l < 0.0010 0.0205 0.0200 102 41. - 138. 9810 00-A132487 1,1,2-Trichloroethane mg/1 < 0.0010 0.0231 0.0200 116 39. - 136. 9805 blank 1,1,2-Trichloroethane mg/1 < 0.0010 0.0199 0.0200 100 39. - 136. 9805 00-A131746 1,1,2-Trichloroethane mg/1 < 0.0010 0.0203 0.0200 102 39. - 136. 9808 00-A131758 1,1,2-Trichloroethane mg/l < 0.0010 0.0193 0.0200 96 39. - 136. 9808 00-A131763 1,1,2-Trichloroethane mg/1 < 1.000 0.0215 0.0200 108 39. - 136. 9809 00-A131771 1,1,2-Trichloroethane mg/1 < 1.000 0.0215 0.0200 108 39. - 136. 9809 00-A131776 1,1,2-Trichloroethane mg/1 < 0.0010 0.0193 0.0200 96 39. - 136. 9810 00-A132483 1,1,2-Trichloroethane mg/1 < 0.0010 0.0192 0.0200 96 39. - 136. 9810 00-A132487 Trichloroethene mg/1 < 0.0010 0.0216 0.0200 108 35. - 146. 9805 blank Trichloroethene mg/1 < 0.0010 0.0230 0.0200 115 35. - 146. 9805 00-A131746 Trichloroethene mg/1 < 0.0010 0.0185 0.0200 92 35. - 146. 9808 00-A131758 Trichloroethene mg/1 < 0.0010 0.0208 0.0200 104 35. - 146. 9808 00-A131763 Trichloroethene mg/1 < 0.0010 0.0230 0.0200 115 35. - 146. 9809 00-A131771 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Trichloroethene mg/1 0.0025 0.0211 0.0200 93 35. - 146. 9809 00-A131776 Trichloroethene mg/l < 0.0010 0.0179 0.0200 90 35. - 146. 9810 00-A132483 Trichloroethene mg/l < 0.0010 0.0204 0.0200 102 35. - 146. 9810 00-A132487 Trichlorofluoromethane mg/l < 0.0010 0.0217 0.0200 108 21. - 156. 9805 blank Trichlorofluoromethane mg/l < 0.0010 0.0222 0.0200 111 21. - 156. 9805 00-A131746 Trichlorofluoromethane mg/l < 0.0010 0.0215 0.0200 108 21. - 156. 9808 00-A131758 Trichlorofluoromethane mg/l < 0.0010 0.0232 0.0200 116 21. - 156. 9808 00-A131763 Trichlorofluoromethane mg/l < 1.000 0.0225 0.0200 112 21. - 156.. 9809 00-A131771 Trichlorofluoromethane mg/l < 1.000 0.0215 0.0200 108 21. - 156. 9809 00-A131776 Trichlorofluoromethane mg/l < 0.0010 0.0246 0.0200 123 21. - 156. 9810 00-A132483 Trichlorofluoromethane mg/1 < 0.0010 0.0232 0.0200 116 21. - 156. 9810 00-A132487 Laboratory Control Data Analyte units Rnown Val. Analyzed Val % Recovery Target Range Q.C. Batch --------------- Benzene ------- mg/1 ---------- 0.0200 ------------ 0.0218 ---------- 109 ------------ 77 - 123 --------- 9805 Benzene mg/l 0.0200 0.0221 110 77 - 123 9808 Benzene mg/l 0.0200 0.0226 113 77 - 123 9810 Chlorobenzene mg/l 0.0200 0.0176 88 81 - 120 9805 Chlorobenzene mg/l 0.0200 0.0202 101 81 - 120 9808 Chlorobenzene mg/l 0.0200 0.0242 121 # 81 - 120 9809 Chlorobenzene mg/l 0.0200 0.0218 109 81 - 120 9810 1,2-Dichlorobenzene mg/l 0.0200 0.0172 86 68 - 132 9805 1,2-Dichlorobenzene mg/1 0.0200 0.0206 103 68 - 132 9808 1,2-Dichlorobenzene mg/l 0.0200 0.0222 111 68 - 132 9809 1,2-Dichlorobenzene mg/l 0.0200 0.0197 98 68 - 132 9810 1,3-Dichlorobenzene mg/l 0.0200 0.0235 118 73 - 128 9805 1,3-Dichlorobenzene mg/l 0.0200 0.0166 83 73 - 128 9808 1,3-Dichlorobenzene mg/l 0.0200 0.0192 96 73 - 128 9809 1,3-Dichlorobenzene mg/l 0.0200 0.0218 109 73 - 128 9810 1,4-Dichlorobenzene mg/l 0.0200 0.0172 86 70 - 131 9805 1,4-Dichlorobenzene mg/l 0.0200 0.0214 107 70 - 131 9808 1,4-Dichlorobenzene mg/l 0.0200 0.0188 94 70 - 131 9809 1,4-Dichlorobenzene mg/l 0.0200 0.0200 100 70 - 131 9810 Ethylbenzene mg/l 0.0200 0.0199 100 63 - 137 9805 Ethylbenzene mg/l 0.0200 0.0196 98 63 - 137 9808 Ethylbenzene mg/l 0.0200 0.0207 104 63 - 137 9810 Toluene mg/1 0.0200 0.0212 106 78 - 123 9805 Toluene mg/l 0.0200 0.0213 106 78 - 123 9808 Toluene mg/l 0.0200 0.0221 110 78 - 123 9810 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / Rm 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch m,p-Xylenes ------- mg/l ---------- 0.0400 ------------ 0.0421 ---------- 105 ------------ 70 - 130 --------- 9805 m,p-Xylenes mg/l 0.0400 0.0417 104 70 - 130 9808 m,p-Xylenes mg/l 0.0400 0.0437 109 70 - 130 9810 o-Xylene mg/1 0.0200 0.0221 110 70 - 130 9805 o-Xylene mg/1 0.0200 0.0216 108 70 - 130 9808 o-Xylene mg/l 0.0200 0.0227 114 70 - 130 9810 Bromodichloromethane mg/l 0.0200 0.0206 103 76 - 124 9805 Bromodichloromethane mg/l 0.0200 0.0200 100 76 - 124 9808 Bromodichloromethane mg/l. 0.0200 0.0197 98 76 - 124 9809 Bromodichloromethane mg/L 0.0200 0.0212 106 76 - 124 9810 Bromoform mg/l 0.0200 0.0194 97 74 - 127 9805 Bromoform mg/l 0.0200 0.0219 110 74 - 127 9808 Bromoform mg/l 0.0200 0.0230 115 74 - 127 9809 Bromoform mg/1 0.0200 0.0193 96 74 - 127 9810 Bromomethane mg/l 0.0200 0.0193 96 59 - 142 9805 Bromomethane mg/1 0.0200 0.0170 85 59 - 142 9808 Bromomethane mg/l 0.0200 0.0191 96 59 - 142 9809 Bromomethane mg/l 0.0200 0.0193 96 59 - 142 9810 Carbon tetrachloride mg/l 0.0200 0.0185 92 69 - 132 9805 Carbon tetrachloride mg/l 0.0200 0.0207 104 69 - 132 9808 Carbon tetrachloride mg/l 0.0200 0.0246 123 69 - 132 9809 Carbon tetrachloride mg/l 0.0200 0.0207 104 69 - 132 9810 Chloroethane mg/1 0.0200 0.0176 88 77 - 123 9805 Chloroethane mg/l 0.0200 0.0192 96 77 - 123 9808 Chloroethane mg/1 0.0200 0.0224 112 77 - 123 9809 Chloroethane mg/1 0.0200 0.0198 99 77 - 123 9810 2-Chloroethylvinylether mg/l 0.0200 0.0156 78 60 - 140 9805 2-Chloroethylvinylether mg/1 0.0200 0.0181 90 60 - 140 9808 - 2-Chloroethylvinylether mg/l 0.0200 0.0221 110 60 - 140 9809 2-Chloroethylvinylether mg/1 0.0200 0.0175 88 60 - 140 9810 Chloroform mg/l 0.0200 0.0234 117 75 - 125 9805 Chloroform mg/l 0.0200 0.0222 111 75 - 125 9808 Chloroform mg/1 0.0200 0.0246 123 75 - 125 9809 - Chloroform mg/1 0.0200 0.0228 114 75 - 125 9810 Chloromethane mg/l 0.0200 0.0183 92 60 - 141 9805 - Chloromethane mg/l 0.0200 0.0155 78 60 - 141 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch Chloromethane ------- mg/1 ---------- 0.0200 ------------ 0.0208 ---------- 104 ------------ 60 - 141 --------- 9809 Chloromethane mg/1 0.0200 0.0164 82 60 - 141 9810 Dibromochloromethane mg/1 0.0200 0.0197 98 66 - 135 9805 Dibromochloromethane mg/1 0.0200 0.0245 122 66 - 135 9808 Dibromochloromethane mg/1 0.0200 0.0226 113 66 - 135 9809 Dibromochloromethane mg/1 0.0200 0.0213 106 66 - 135 9810 Ethylene Dibromide mg/1 0.0200 0.0189 94 70 - 130 9805 Ethylene Dibromide mg/1 0.0200 0.0224 112 70 - 130 9808 Ethylene Dibromide mg/L 0.0200 0.0223 112 70 - 130 9809 Ethylene Dibromide mg/1. 0.0200 0.0191 96 70 - 130 9810 Vinyl chloride mg/1 0.0200 0.0187 94 70 - 130 9805 Vinyl chloride mg/1 0.0200 0.0200 100 70 - 130 9808 Vinyl chloride mg/1• 0.0200 0.0232 116 70 - 130 9809 Vinyl chloride mg/1 0.0200 0.0202 101 70 - 130 9810 Dichlorodifluoromethane mg/1 0.0200 0.0157 78 70 - 130 9805 Dichlorodifluoromethane mg/1 0.0200 0.0187 94 70 - 130 9808 Dichlorodifluoromethane mg/1 0.0200 0.0176 88 70 - 130 9809 Dichlorodifluoromethane mg/1 0.0200 0.0169 84 70 _ 130 9810 1,1-Dichloroethane mg/1 0.0200 0.0202 101 84 - 116 9805 1,1-Dichloroethane mg/1 0.0200 0.0211 106 84 - 116 9808 1,1-Dichloroethane mg/1 0.0200 0.0244 122 # 84 - 116 9809 1,1-Dichloroethane mg/1 0.0200 0.0207 104 84 - 116 9810 1,2-Dichloroethane mg/1 0.0200 0.0191 96 72 - 129 9805 1,2-Dichloroethane mg/1 0.0200 0.0193 96 72 - 129 9808 1,2-Dichloroethane mg/1 0.0200 0.0227 114 72 - 129 9809 - 1,2-Dichloroethane mg/1 0.0200 0.0200 100 72 - 129 9810 1,1-Dichloroethene mg/1 0.0200 0.0312 156 # 63 - 137 9805 1,1-Dichloroethene mg/1 0.0200 0.0231 116 63 - 137 9808 1,1-Dichloroethene mg/1 0.0200 0.0223 112 63 - 137 9809 1,1-Dichloroethene mg/1 0.0200 0.0213 106 63,- 137 9810 cis-1,2-Dichloroethene mg/1 0.0200 0.0216 108 70 - 130 9805 cis-1,2-Dichloroethene mg/1 0.0200 0.0219 110 70 - 130 9808 cis-1,2-Dichloroethene mg/1 0.0200 0.0220 110 70 - 130 9809 cis-1,2-Dichloroethene mg/1 0.0200 0.0227 114 70 - 130 9810 trans-1,2-Dichloroethene mg/1 0.0200 0.0191 96 64 - 136 9805 - trans-1,2-Dichloroethene mg/1 0.0200 0.0191 96 64 - 136 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAY: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch trans-1,2-Dichloroethene ------- mg/1 ---------- 0.0200 ------------ 0.0218 ---------- 109 ------------ 64 - 136 --------- 9809 trans-1,2-Dichloroethene mg/1 0.0200 0.0206 103 64 - 136 9810 1,2-Dichloropropane mg/1 0.0200 0.0188 94 74 - 126 9805 1,2-Dichloropropane mg/1 0.0200 0.0213 106 74 - 126 9808 1,2-Dichloropropane mg/1 0.0200 0.0210 105 74 - 126 9809 1,2-Dichloropropane mg/1 0.0200 0.0210 105 74 - 126 9810 cis-1,3-Dichloropropene mg/1 0.0200 0.0191 96 63 - 136 9805 cis-1,3-Dichloropropene mg/1 0.0200 0.0171 86 63 - 136 9808 cis-1,3-Dichloropropene mg/1 0.0200 0.0226 113 63 - 136 9809 cis-1,3-Dichloropropene mg/1 0.0200 0.0176 88 63 - 136 9810 trans-1,3-Dichloropropene mg/1 0.0200 0.0191 96 70 - 130 9805 trans-1,3-Dichloropropene mg/1 0.0200 0.0215 108 70 - 130 9808 trans-1,3-Dichloropropene mg/1 0.0200 0.0216 108 70 - 130 9809 trans-1,3-Dichloropropene mg/1 0.0200 0.0201 100 70 - 130 9810 Methylene chloride mg/1 0.0200 0.0245 122 78 - 123 9805 Methylene chloride mg/1 0.0200 0.0160 80 78 - 123 9808 Methylene chloride mg/1 0.0200 0.0214 107 78 - 123 9809 Methylene chloride mg/1 0.0200 0.0188 94 78 - 123 9810 ._ 1,1,2,2-Tetrachloroethane mg/1 0.0200 0.0179 90 49 - 151 9805 1,1,2,2-Tetrachloroethane mg/1 0.0200 0.0210 105 49 - 151 9808 j 1,1,2,2-Tetrachloroethane mg/1 0.0200 0.0249 124 49 - 151 9809 1,1,2,2-Tetrachloroethane mg/1 0.0200 0.0207 104 49 - 151 9810 Tetrachloroethene mg/1 0.0200 0.0160 80 70 - 130 9805 Tetrachloroethene mg/1 0.0200 0.0200 100 70 - 130 9808 Tetrachloroethene mg/1 0.0200 0.0228 114 70 - 130 9809 Tetrachloroethene mg/1 0.0200 0.0190 95 70 - 130 9810 1,1,1-Trichloroethane mg/1 0.0200 0.0207 104 71 - 129 9805 1,1,1-Trichloroethane mg/1 0.0200 0.0221 110 71 - 129 9808 1,1,1-Trichloroethane mg/1 0.0200 0.0237 118 71 - 129 9809 1,1,1-Trichloroethane mg/1 0.0200 0.0214 107 71 - 129 9810 1,1,2-Trichloroethane mg/1 0.0200 0.0203 102 79 - 122 9805 1,1,2-Trichloroethane mg/1 0.0200 0.0233 116 79 - 122 9808 1,1,2-Trichloroethane mg/1 0.0200 0.0250 125 # 79 - 122 9809 1,1,2-Trichloroethane mg/1 0.0200 0.0201 100 79 - 122 9810 Trichloroethene mg/1 0.0200 0.0197 98 77 - 123 9805 - Trichloroethene mg/1 0.0200 0.0191 96 77 - 123 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 % FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data - Analyte units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch --------------- Trichloroethene ------- mg/1 ---------- ------------ 0.0200 0.0233 ------------------------------- 116 77 - 123 9809 Trichloroethene mg/1 0.0200 0.0217 108 77 - 123 9810 Trichlorofluoromethane mg/1 0.0200 0.0205 102 67 - 134 9805 Trichlorofluoromethane i mg/1 0.0200 0.0234 117 67 - 134 9808 Trichlorofluoromethane mg/1 0.0200 0.0199 100 67 - 134 9809 Trichlorofluoromethane mg/1 0.0200 0.0211 106 67 - 134 9810 Blank Data Analyte Blank Value Units Q.C. Batch --------------- Benzene ------------ < 0.0010 --------- mg/1 ---------- 9805 Benzene < 0.0010 mg/1 9805 - Benzene < 0.0010 mg/1 9808 Benzene < 0.0010 mg/1 9808 - Benzene < 0.0010 mg/1 9810 Benzene < 0.0010 mg/1 9810 Chlorobenzene < 0.0010 mg/1 9805 Chlorobenzene < 0.0010 mg/1 9805 Chlorobenzene < 0.0010 mg/1 9808 Chlorobenzene < 0.0010 mg/1 9808 Chlorobenzene < 0.0010 mg/1 9809 Chlorobenzene < 0.0010 mg/1 9810 Chlorobenzene < 0.0010 mg/1 9810 Chlorobenzene < 0.0010 mg/1 9809 1,2-Dichlorobenzene < 0.0010 mg/1 9805 1,2-Dichlorobenzene < 0.0010 mg/1 9805 1,2-Dichlorobenzene < 0.0010 mg/1 9808 1,2-Dichlorobenzene < 0.0010 mg/1 9808 1,2-Dichlorobenzene < 0.0010 mg/1 9809 1,2-Dichlorobenzene < 0.0010 mg/1 9810 1,2-Dichlorobenzene < 0.0010 mg/1 9810 1,2-Dichlorobenzene < 0.0010 mg/1 9809 1,3-Dichlorobenzene < 0.0010 mg/l 9805 1,3-Dichlorobenzene < 0.0010 mg/1 9805 1,3-Dichlorobenzene < 0.0010 mg/1 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TuAnstl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch --------------- 1,3-Dichlorobenzene ------------ < 0.0010 --------- mg/l ---------- 9808 1,3-Dichlorobenzene < 0.0010 mg/1 9809 1,3-Dichlorobenzene < 0.0010 mg/l 9810 1,3-Dichlorobenzene < 0.0010 mg/1 9810 1,3-Dichlorobenzene < 0.0010 mg/l 9809 1,4-Dichlorobenzene < 0.0010 mg/1 9805 1,4-Dichlorobenzene < 0.0010 mg/l 9805 1,4-Dichlorobenzene < 0.0010 mg/1 9808 1,4-Dichlorobenzene < 0.0010 mg/1 9808 1,4-Dichlorobenzene < 0.0010 mg/1 9809 1,4-Dichlorobenzene < 0.0010 mg/l 9810 1,4-Dichlorobenzene < 0.0010 mg/l 9810 1,4-Dichlorobenzene < 0.0010 mg/1 9809 Ethylbenzene < 0.0010 mg/l 9805 Ethylbenzene < 0.0010 mg/1 9805 Ethylbenzene < 0.0010 mg/1 9808 Ethylbenzene < 0.0010 mg/l 9808 Ethylbenzene < 0.0010 mg/1 9810 Ethylbenzene < 0.0010 mg/l 9810 Toluene < 0.0010 mg/1 9805 Toluene < 0.0010 mg/l 9805 Toluene < 0.0010 mg/l 9808 Toluene < 0.0010 mg/1 9808 Toluene < 0.0010 mg/l 9810 Toluene < 0.0010 mg/1 9810 m,p-Xylenes < 0.0010 mg/l 9805 m,p-Xylenes < 0.0010 mg/1 9805 m,p-Xylenes < 0.0010 mg/1 9808 m,p-Xylenes < 0.0010 mg/l 9808 m,p-Xylenes < 0.0010 mg/l 9810 m,p-Xylenes < 0.0010 mg/1 9810 o-Xylene < 0.0010 mg/l 9805 o-Xylene < 0.0010 mg/l 9805 o-Xylene < 0.0010 mg/l 9808 o-Xylene < 0.0010 mg/l 9808 o-Xylene < 0.0010 mg/l 9810 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte --------------- Blank Value Units Q.C. Batch o-Xylene ------------ < 0.0010 --------- mg/1 ---------- 9810 Bromodichloromethane < 0.0010 mg/l 9805 Bromodichloromethane < 0.0010 mg/1 9805 Bromodichloromethane < 0.0010 mg/1 9808 Bromodichloromethane < 0.0010 mg/l 9808 Bromodichloromethane < 0.0010 mg/1 9809 Bromodichloromethane < 0.0010 mg/l 9810 Bromodichloromethane < 0.0010 mg/l 9810 Bromodichloromethane < 0.0010 mg/l 9809 Bromoform < 0.0010 mg/l 9805 Bromoform < 0.0010 mg/l 9805 Bromoform < 0.0010 mg/l 9808 Bromoform < 0.0010 mg/1 9808 Bromoform < 0.0010 mg/l 9809 Bromoform < 0.0010 mg/1 9810 Bromoform < 0.0010 mg/l 9810 Bromoform < 0.0010 mg/l 9809 Bromomethane < 0.0010 mg/l 9805 Bromomethane < 0.0010 mg/l 9805 Bromomethane < 0.0010 mg/l 9808 Bromomethane < 0.0010 mg/1 9808 Bromomethane < 0.0010 mg/l 9809 Bromomethane < 0.0010 mg/l 9810 Bromomethane < 0.0010 mg/l 9810 Bromomethane < 0.0010 mg/1 9809 Carbon tetrachloride < 0.0010 mg/l 9805 Carbon tetrachloride < 0.0010 mg/l 9805 Carbon tetrachloride < 0.0010 mg/1 9808 Carbon tetrachloride < 0.0010 mg/1 9808 Carbon tetrachloride < 0.0010 mg/l 9809 Carbon tetrachloride < 0.0010 mg/1 9810 Carbon tetrachloride < 0.0010 mg/1 9810 Carbon tetrachloride < 0.0010 mg/1 9809 Chloroethane < 0.0010 mg/1 9805 Chloroethane < 0.0010 mg/1 9805 Chloroethane < 0.0010 mg/l 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NAsHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Tent merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch Chloroethane < 0.0010 mg/1 9808 Chloroethane < 0.0010 mg/l 9809 Chloroethane < 0.0010 mg/1 9810 Chloroethane < 0.0010 mg/1 9810 Chloroethane < 0.0010 mg/1 9809 2-Chloroethylvinylether < 0.0010 mg/1 9805 2-Chloroethylvinylether < 0.0010 mg/1 9805 2-Chloroethylvinylether < 0.001b mg/1 9808 2-Chloroethylvinylether < 0.0010 mg/1 9808 2-Chloroethylvinylether < 0.0010 mg/1 9809 2-Chloroethylvinylether < 0.0010 mg/1 9810 2-Chloroethylvinylether < 0.0010 mg/1 9810 2-Chloroethylvinylether < 0.0010 mg/1 9809 Chloroform < 0.0010 mg/l 9805 Chloroform < 0.0010 mg/l 9805 Chloroform < 0.0010 mg/l 9808 Chloroform < 0.0010 mg/1 9808 Chloroform < 0.0010 mg/1 9809 Chloroform < 0.0010 mg/1 9810 Chloroform < 0.0010 mg/1 9810 Chloroform < 0.0010 mg/1 9809 Chloromethane < 0.0010 mg/1 9805 Chloromethane < 0.0010 mg/l 9805 Chloromethane < 0.0010 mg/l 9808 Chloromethane < 0.0010 mg/l 9808 Chloromethane < 0.0010 mg/l 9809 Chloromethane < 0.0010 mg/l 9810 Chloromethane < 0.0010 mg/1 9810 Chloromethane < 0.0010 mg/1 9809 Dibromochloromethane < 0.0010 mg/1 9805 Dibromochloromethane < 0.0010 mg/1 9805 Dibromochloromethane < 0.0010 mg/1 9808 Dibromochloromethane < 0.0010 mg/1 9808 Dibromochloromethane < 0.0010 mg/1 9809 Dibromochloromethane < 0.0010 mg/1 9810 Dibromochloromethane < 0.0010 mg/l 9810 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch --------------------------- Dibromochloromethane < 0.0010 --------- mg/l ---------- 9809 Ethylene Dibromide < 0.0010 mg/l 9805 Ethylene Dibromide < 0.0010 mg/l 9805 Ethylene Dibromide < 0.0010 mg/l 9808 Ethylene Dibromide < 0.0010 mg/l 9808 Ethylene Dibromide < 0.0010 mg/l 9809 Ethylene Dibromide < 0.0010 mg/l 9810 Ethylene Dibromide < 0.0010 mg/l 9810 Ethylene Dibromide < 0.0010 mg/l 9809 Vinyl chloride < 0.0010 mg/l 9805 Vinyl chloride < 0.0010 mg/l 9805 Vinyl chloride < 0.0010 mg/l 9808 Vinyl chloride < 0.0010 mg/l 9808 Vinyl chloride < 0.0010 mg/l 9809 Vinyl chloride < 0.0010 mg/l 9810 Vinyl chloride < 0.0010 mg/1 9810 Vinyl chloride < 0.0010 mg/1 9809 Dichlorodifluoromethane < 0.0010 mg/1 9805 Dichlorodifluoromethane < 0.0010 mg/l 9805 Dichlorodifluoromethane < 0.0010 mg/l 9808 Dichlorodifluoromethane < 0.0010 mg/1 9808 Dichlorodifluoromethane < 0.0010 mg/l 9809 Dichlorodifluoromethane < 0.0010 mg/l 9810 Dichlorodifluoromethane < 0.0010 mg/l 9810 Dichlorodifluoromethane < 0.0010 mg/l 9809 1,1-Dichloroethane < 0.0010 mg/1 9805 1,1-Dichloroethane < 0.0010 mg/1 9805 1,1-Dichloroethane < 0.0010 mg/1 9808 1,1-Dichloroethane < 0.0010 mg/1 9808 1,1-Dichloroethane < 0.0010 mg/1 9809 1,1-Dichloroethane < 0.0010 mg/1 9810 1,1-Dichloroethane < 0.0010 mg/l 9810 1,1-Dichloroethane < 0.0010 mg/1 9809 1,2-Dichloroethane < 0.0010 mg/l 9805 1,2-Dichloroethane < 0.0010 mg/l 9805 1,2-Dichloroethane < 0.0010 mg/l 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch --------------- ------------ 1,2-Dichloroethane < 0.0010 --------- mg/l ---------- 9808 1,2-Dichloroethane < 0.0010 mg/l 9809 1,2-Dichloroethane < 0.0010 mg/l 9810 1,2-Dichloroethane < 0.0010 mg/l 9810 1,2-Dichloroethane < 0.0010 mg/l 9809 1,1-Dichloroethene < 0.0010 mg/l 9805 1,1-Dichloroethene < 0.0010 mg/1 9805 1,1-Dichloroethene < 0.'0010 mg/l 9808 1,1-Dichloroethene < 0.0010 mg/l 9808 1,1-Dichloroethene < 0.0010 mg/l 9809 1,1-Dichloroethene < 0.0010 mg/l 9810 1,1-Dichloroethene < 0.0010 mg/l 9810 1,1-Dichloroethene < 0.0010 mg/l 9809 cis-1,2-Dichloroethene < 0.0010 mg/l 9805 cis-1,2-Dichloroethene < 0.0010 mg/l 9805 cis-1,2-Dichloroethene < 0.0010 mg/1 9808 cis-1,2-Dichloroethene < 0.0010 mg/l 9808 cis-1,2-Dichloroethene < 0.0010 mg/1 9809 cis-1,2-Dichloroethene < 0.0010 mg/l 9810 cis-1,2-Dichloroethene < 0.0010 mg/l 9810 cis-1,2-Dichloroethene < 0.0010 mg/l 9809 trans-1,2-Dichloroethene < 0.0010 mg/l 9805 trans-1,2-Dichloroethene < 0.0010 mg/l 9805 trans-1,2-Dichloroethene < 0.0010 mg/l 9808 trans-1,2-Dichloroethene i. < 0.0010 mg/l 9808 trans-1,2-Dichloroethene < 0.0010 mg/l 9809 trans-1,2-Dichloroethene < 0.0010 mg/l 9810 trans-1,2-Dichloroethene < 0.0010 mg/l 9810 trans-1,2-Dichloroethene < 0.0010 mg/l 9809 1,2-Dichloropropane < 0.0010 mg/1 9805 1,2-Dichloropropane < 0.0010 mg/1 9805 1,2-Dichloropropane < 0.0010 mg/l 9808 1,2-Dichloropropane < 0.0010 mg/l 9808 1,2-Dichloropropane < 0.0010 mg/l 9809 1,2-Dichloropropane < 0.0010 mg/l 9810 1,2-Dichloropropane < 0.0010 mg/1 9810 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testj�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch --------------------------- 1,2-Dichloropropane < 0.0010 --------- mg/l ---------- 9809 cis-1,3-Dichloropropene < 0.0010 mg/1 9805 cis-1,3-Dichloropropene < 0.0010 mg/l 9805 cis-1,3-Dichloropropene < 0.0010 mg/1 9808 cis-1,3-Dichloropropene < 0.0010 mg/l 9808 cis-1,3-Dichloropropene < 0.0010 mg/1 9809 cis-1,3-Dichloropropene < 0.0010 mg/l 9810 cis-1,3-Dichloropropene < 0.0010 mg/1 9810 cis-1,3-Dichloropropene < 0.0010 mg/l 9809 trans-1,3-Dichloropropene < 0.0010 mg/1 9805 trans-1,3-Dichloropropene < 0.0010 mg/l 9805 trans-1,3-Dichloropropene < 0.0010 mg/l 9808 trans-1,3-Dichloropropene < 0.0010 mg/l 9808 trans-1,3-Dichloropropene < 0.0010 mg/l 9809 trans-1,3-Dichloropropene < 0.0010 mg/l 9810 trans-1,3-Dichloropropene < 0.0010 mg/l 9810 trans-1,3-Dichloropropene < 0.0010 mg/1 9809 Methylene chloride < 0.0050 mg/l 9805 Methylene chloride < 0.0050 mg/1 9805 Methylene chloride < 0.0050 mg/l 9808 Methylene chloride < 0.0050 mg/l 9808 Methylene chloride < 0.0050 mg/l 9809 Methylene chloride < 0.0050 mg/l 9810 Methylene chloride < 0.0050 mg/l 9810 Methylene chloride < 0.0050 mg/l 9809 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9805 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9805 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9808 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9808 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9809 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9810 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 9810 1,1,2,2-Tetrachloroethane < 0.0010 mg/1 9809 Tetrachloroethene < 0.0010 mg/l 9805 Tetrachloroethene < 0.0010 mg/l 9805 Tetrachloroethene < 0.0010 mg/l 9808 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte --------------- Blank Value Units Q.C. Batch Tetrachloroethene ------------ < 0.0010 --------- mg/l ------_--- 9808 -' Tetrachloroethene < 0.0010 mg/l 9809 Tetrachloroethene 0.0010 mg/l 9810 Tetrachloroethene < 0.0010 mg/l 9810 Tetrachloroethene < 0.0010 mg/l 9809 1,1,1-Trichloroethane < 0.0010 mg/l 9805 1,1,1-Trichloroethane < 0.0010 mg/l 9805 1,1,1-Trichloroethane < 0.0010 mg/l 9808 1,1,1-Trichloroethane < 0.0010 mg/l 9808 1,1,1-Trichloroethane < 0.0010 mg/l 9809 1,1,1-Trichloroethane < 0.0010 mg/1 9810 - 1,1,1-Trichloroethane < 0.0010 mg/l 9810 1,1,1-Trichloroethane < 0.0010 mg/1 9809 1,1,2-Trichloroethane < 0.0010 mg/l 9805 1,1,2-Trichloroethane < 0.0010 mg%l 9805 1,1,2-Trichloroethane < 0-0010 mg/l 9808 1,1,2-Trichloroethane < 0.0010 mg/1 9808 1,1,2-Trichloroethane < 0.0010 mg/l 9809 1,1,2-Trichloroethane < 0.0010 mg/l 9810 1,1,2-Trichloroethane < 0.0010 mg/l 9810 1,1,2-Trichloroethane < 0.0010 mg/l 9809 Trichloroethene < 0.0010 mg/1 9805 Trichloroethene <.0.0010 mg/l 9805 Trichloroethene < 0.0010 mg/1 9808 Trichloroethene < 0.0010 mg/1 9808 Trichloroethene < 0.0010 mg/1 9809 Trichloroethene < 0.0010 mg/l 9810 Trichloroethene I ' < 0.0010 mg/1 9810 Trichloroethene < 0.0010 mg/1 9809 Trichlorofluoromethane < 0.0010 mg/1 9805 Trichlorofluoromethane < 0.0010 mg/1 9805 Trichlorofluoromethane < 0.0010 mg/1 9808 Trichlorofluoromethane < 0.0010 mg/l 9808 Trichlorofluoromethane < 0.0010 mg/l 9809 Trichlorofluoromethane < 0.0010 mg/l 9810 Trichlorofluoromethane < 0.0010 mg/l 9810 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�meric'a I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch ---------------------------------------------- Trichlorofluoromethane < 0.00.10 mg/1 9809 # - Value outside Laboratory historical QC limits. End of Report for Project 208014 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAY: 615-726-0954 / 800-765-0980 Testl�merica -- I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Matrix Spike Recovery Analyte --------------- units Orig. Val. MS Val Spike Conc Recovery Target Range Q.C. Batch Spike Sample i Benzene ------- mg/1 ---------- < 0.0010 --------- 0.0187 ---------- 0.0200 --------- 94 ------------ 39. - 150. ---------- 3758 ------------ blank Benzene mg/1 < 0.0010 0.0191 0.0200 96 39. - 150. 3759 blank Benzene mg/1 0.0010 0.0249 .0.0200 124 39. - 150. 3758 blank Benzene mg/1 < 0.0010 0.0201 0.0200 100 39. - 150. 3759 blank Chlorobenzene mg/1 < 0.0010 0.0230 0.0200 115 55. - 135. 3756 blank Chlorobenzene mg/1 0.0010 0.0153 0.0200 76 55. - 135. 3758 blank - Chlorobenzene mg/1 < 0.0010 0.0209 0.0200 104 55. - 135. 3759 blank Chlorobenzene mg/1 < 0.0010 0.0143 0.0200 72 55. - 135. 3756 blank Chlorobenzene mg/1 < 0.0010 0.0158 0.0200 79 55. - 135. 3758 blank Chlorobenzene mg/1 < 0.0010 0.0245 0.0200 122 55. - 135. 3759 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0219 0.0200 110 37. - 154. 3756 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0183 0.0200 92 37. - 154. 3758 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0204 0.0200 102 37. - 154. 3759 blank • 1,2-Dichlorobenzene mg/1 < 0.0010 0.0248 0.0200 124 37. - 154. 3756 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0162 0.0200 81 37. - 154. 3758 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0241 0.0200 120 37. - 154. 3759 blank 1,3-Dichlorobenzene mg/1 < 0.0010 0.0164 0.0200 82 50. - 141. 3756 blank 1,3-Dichlorobenzene mg/l < 0.0010 0.0168 0.0200 84 50. - 141. 3758 blank 1,3-Dichlorobenzene mg/1 < 0.0010 0.0194 0.0200 97 50. - 141. 3759 blank 1,3-Dichlorobenzene mg/l < 0.0010 0.0222 0.0200 111 50. - 141. 3756 blank 1,3-Dichlorobenzene mg/1 < 0.0010 0.0190 0.0200 95 50. - 141. 3758 blank 1,3-Dichlorobenzene mg/l < 0.0010 0.0232 0.0200 116 50. - 141. 3759 blank 1,4-Dichlorobenzene mg/1 < 0.0010 0.0200 0.0200 100 42. - 143. 3756 blank -- 1,4-Dichlorobenzene mg/1 < 0.0010 0.0181 0.0200 90 42. - 143. 3758 blank 1,4-Dichlorobenzene mg/1 < 0.0010 0.0201 0.0200 100 42. - 143. 3759 blank 1,4-Dichlorobenzene mg/1 < 0.0010 0.0240 0.0200 120 42. - 143. 3756 blank 1,4-Dichlorobenzene mg/1 0.0010 0.0158 0.0200 79 42. - 143. 3758 blank 1,4-Dichlorobenzene mg/1 < 0.0010 0.0238 0.0200 119 42. - 143. 3759 blank Ethylbenzene mg/1 < 0.0010 0.0186 0.0200 93 32. - 160. 3758 blank Ethylbenzene mg/1 < 0.0010 0.0186 0.0200 93 32. - 160. 3759 blank • Ethylbenzene mg/1 < 0.0010 0.0251 0.0200 126 32. - 160. 3758 blank Ethylbenzene mg/1 < 0.0010 0.0199 0.0200 100 32. - 160. 3759 blank _ Toluene mg/l < 0.0010 0.0185 0.0200 92 46. - 148. 3758 blank Toluene mg/l < 0.0010 0.0191 0.0200 96 46. - 148. 3759 blank Toluene mg/1 < 0.0010 0.0249 0.0200 124 46. - 148. 3758 blank - Toluene mg/1 < 0.0010 0.0201 0.0200 100 46. - 148. 3759 blank Project QC continued . . . -- 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA o-Xylene mg/l 0.0010 0.0195 0.0200 98 74. - 126. 3758 blank o-Xylene mg/l < 0.0010 0.0186 0.0200 93 74. - 126. 3759 blank o-Xylene mg/1 < 0.0010 0.0250 0.0200 125 74. - 126. 3758 blank o-Xylene mg/l < 0.0010 0.0199 0.0200 100 74. - 126. 3759 blank Bromodichloromethane mg/l < 0.0010 0.0214 0.0200 107 42. - 172. 3756 blank Bromodichloromethane mg/l < 0.0010 0.0184 0.0200 92 42. - 172. 3758 blank Bromodichloromethane mg/1 < 0.0010 0.0220 0.0200 110 42. - 172. 3759 blank Bromodichloromethane mg/l < 0.0010 0.0221 0.0200 110 42. - 172. 3756 blank Bromodichloromethane mg/l < 0.0010 0.0178 0.0200 89 42. - 172. 3758 blank Bromodichloromethane mg/l < 0.0010 0.0248 0.0200 124 42. - 172. 3759 blank Bromoform mg/l < 0.0010 0.0196 0.0200 98 13. - 159. 3756 blank Bromoform mg/l < 0.0010 0.0172 0.0200 86 13. - 159. 3758 blank Bromoform mg/l < 0.0010 0.0199 0.0200 100 13. - 159. 3759 blank Bromoform mg/l 0.0010 0.0223 0.0200 112 13. - 159. 3756 blank Bromoform mg/l < 0.0010 0.0164 0.0200 82 13. - 159. 3758 blank Bromoform mg/1 < 0.0010 0.0235 0.0200 118 13. - 159. 3759 blank Bromomethane mg/l < 0.0010 0.0191 0.0200 96 10. - 144. 3756 blank Bromomethane mg/l < 0.0010 0.0176. 0.0200 88 10. - 144. 3758 blank Bromomethane mg/l < 0.0010 0.0179 0.0200 90 10. - 144. 3759 blank Bromomethane mg/l < 0.0010 0.0236 0.0200 118 10. - 144. 3756 blank Bromomethane mg/l < 0.0010 0.0175 0.0200 88 10. - 144. 3758 blank Bromomethane mg/l < 0.0010 0.0196 0.0200 98 10. - 144. 3759 blank Carbon tetrachloride mg/l < 0.0010 0.0190 0.0200 95 43. - 143. 3756 blank Carbon tetrachloride mg/l < 0.0010 0.0190 0.0200 95 43. - 143. 3758 blank Carbon tetrachloride mg/l < 0.0010 0.0212 0'.0200 106 43. - 143. 3759 blank Carbon tetrachloride mg/l < 0.0010 0.0243 0.0200 122 43. - 143. 3756 blank Carbon tetrachloride mg/1 < 0.0010 0.0160 0.0200 80 43. - 143. 3758 blank Carbon tetrachloride mg/l < 0.0010 0.0238 0.0200 119 43. - 143. 3759 blank Chloroethane mg/1 < 0.0010 0.0193 0.0200 96 46. - 137. 3756 blank I Chloroethane mg/l < 0.0010 0.0191 0.0200 96 46. - 137. 3758 blank Chloroethane mg/l < 0.0010 0.0148 0.0200 74 46. - 137. 3759 blank Chloroethane mg/l < 0.0010 0.0240 0.0200 120 46. - 137. 3756 blank Chloroethane mg/l < 0.0010 0.0168 0.0200 84 46. - 137. 3758 blank Chloroethane mg/l 0.0010 0.0159 0.0200 80 46. - 137. 3759 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0171 0.0200 86 14. - 186. 3756 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0152 0.0200 76 14. - 186. 3758 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0181 0.0200 90 14. - 186. 3759 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0195 0.0200 98 14. - 186. 3756 blank 2-Chloroethylvinylether mg/1 < 0.0010 0.0135 0.0200 68 14. - 186. 3758 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0214 0.0200 107 14. - 186. 3759 blank Chloroform mg/1 < 0.0010 0.0202 0.0200 101 49. - 133. 3756 blank Project QC continued . . . -- 2960 FOSTER CREICHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica PROJECT QUALITY CONTROL DATA Chloroform mg/1 0.0010 0.0194 0.0200 97 49. - 133. 3758 blank Chloroform mg/1 0.0010 0.0204 0.0200 102 49. - 133. 3759 blank Chloroform mg/1 < 0.0010 0.0253 0.0200 126 49. - 133. 3756 blank Chloroform mg/1 < 0.0010 0.0177 0.0200 88 49. - 133. 3758 blank Chloroform mg/1 < 0.0010 0.0259 0.0200 130 49. - 133. 3759 blank Chloromethane mg/l < 0.0010 0.0156 0.0200 78 10. - 193. 3756 blank Chloromethane mg/1 < 0.0010 0.0172 0.0200 86 10. - 193. 3758 blank Chloromethane mg/1 < 0.0010 0.0175 0.0200 88 10. - 193. 3759 blank Chloromethane mg/1 < 0.0010 0.0175 0.0200 88 10. - 193. 3756 blank Chloromethane mg/1 < 0.0010 0.0166 0.0200 83 10. - 193. 3758 blank Chloromethane mg/1 < 0.0010 0.0172 0.0200 86 10. - 193. 3759 blank Dibromochloromethane mg/1 < 0.0010 0.0225 0.0200 112 24. - 191. 3756 blank Dibromochloromethane mg/1 < 0.0010 0.0181 0.0200 90 24. - 191. 3758 blank Dibromochloromethane mg/1 < 0.0010 0.0205 0.0200 102 24. - 191. 3759 blank Dibromochloromethane mg/l < 0.0010 0.0242 0.0200 121 24. - 191. 3756 blank Dibromochloromethane mg/l < 0.0010 0.0165 0.0200 82 24. - 191. 3758 blank Dibromochloromethane mg/l < 0.0010 0.0242 0.0200 121 24. - 191. 3759 blank Ethylene Dibromide mg/l < 0.0010 0.0239 0.0200 120 70. - 130. 3756 blank Ethylene Dibromide mg/l < 0.0010 0.0176 0.0200 88 70. - 130. 3758 blank Ethylene Dibromide mg/l < 0.0010 0.0201 0.0200 100 70. - 130. 3759 blank Ethylene Dibromide mg/1 < 0.0010 0.0241 0.0200 120 70. - 130. 3756 blank Ethylene Dibromide mg/1 < 0.0010 0.0165 0.0200 82 70. - 130. 3758 blank Ethylene Dibromide mg/1 < 0.0010 0.0236 0.0200 118 70. - 130. 3759 blank Vinyl chloride mg/1 < 0.0010 0.0210 0.0200 105 28. - 163. 3756 blank Vinyl chloride mg/1 < 0.0010 0.0173 0.0200 86 28. - 163. 3758 blank Vinyl chloride mg/1 < 0.0010 0.0187 0.0200 94 28. - 163. 3759 blank Vinyl chloride mg/1 < 0.0010 0.0244 0.0200 122 28. - 163. 3756 blank Vinyl chloride mg/1 < 0.0010 0.0159 0.0200 80 28. - 163. 3758 blank Vinyl chloride mg/1 < 0.0010 0.0208 0.0200 104 28. - 163. 3759 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0227 0.0200 114 47. - 132. 3756 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0173 0.0200 86 47. - 132. 3758 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0208 0.0200 104 47. - 132. 3759 blank 1,1-Dichloroethane mg/l < 0.0010 0.0247 0.0200 124 47. - 132. 3756 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0160 0.0200 80 47. - 132. 3758 blank 1,1-Dichloroethane mg/l 0.0010 0.0241 0.0200 120 47. - 132. 3759 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0218 0.0200 109 51. - 147. 3756 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0188 0.0200 _94 51. - 147. 3758 blank 1,2-Dichloroethane mg/l < 0.0010 0.0198 0.0200 99 51. - 147. 3759 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0210 0.0200 105 51. - 147. 3756 blank 1,2-Dichloroethane mg/l < 0.0010 0.0160 0.0200 80 51. - 147. 3758 blank 1,2-Dichloroethane mg/l < 0.0010 0.0234 0.0200 117 51. - 147. 3759 blank Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAR: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA 1,1-Dichloroethene mg/l < 0.0010 0.0199 0.0200 100 28. - 167. 3756 blank 1,1-Dichloroethene mg/l < 0.0010 0.0182 0.0200 91 28. - 167. 3758 blank 1,1-Dichloroethene mg/l 0.0010 0.0173 0.0200 86 28. - 167. 3759 blank 1,1-Dichloroethene mg/l < 0.0010 0.0232 0.0200 116 28. - 167. 3756 blank 1,1-Dichloroethene mg/l < 0.0010 0.0163 0.0200 82 28. - 167. 3758 blank 1,1-Dichloroethene mg/l < 0.0010 0.0188 0.0200 94 28. - 167. 3759 blank cis-1,2-Dichloroethene mg/l < 0.0010 0.0196 0.0200 98 76. - 123. 3756 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0181 0.0200 90 76. - 123. 3758 blank cis-1,2-Dichloroethene mg/l < 0.0010 0.0194 0.0200 97 76. - 123. 3759 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0268 0.0200 134# 76. - 123. 3756 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0169 0.0200 84 76. - 123. 3758 blank cis-1,2-Dichloroethene mg/l < 0.0010 0.0242 0.0200 121 76. - 123. 3759 blank trans-1,2-Dichloroethene mg/1 < 0.0010 0.0202 0.0200 101 38. - 155. 3756 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0175 0.0200 88 38. - 155. 3758 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0198 0.0200 99 38. - 155. 3759 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0236 0.0200 118 38. - 155. 3756 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0165 0.0200 82 38. - 155. 3758 blank trans-1,2-Dichloroethene mg/1 < 0.0010 0.0232 0.0200 116 38. - 155. 3759 blank 1,2-Dichloropropane mg/1 < 0.0010 0.0193 0.0200 96 44. - 156. 3756 blank 1,2-Dichloropropane mg/l < 0.0010 0.0179 0.0200 90 44. - 156. 3758 blank 1,2-Dichloropropane mg/1 < 0.0010 0.0211 0.0200 106 44. - 156. 3759 blank 1,2-Dichloropropane mg/1 < 0.0010 0.0252 0.0200 126 44. - 156. 3756 blank 1,2-Dichloropropane mg/l < 0.0010 0.0162 0.0200 81 44. - 156. 3758 blank 1,2-Dichloropropane mg/1 < 0.0010 0.0241 0.0200 120 44. - 156. 3759 blank cis-1,3-Dichloropropene mg/l < 0.0010 0.0224 0.0200 112 22. - 178. 3756 blank cis-1,3-Dichloropropene mg/1 < 0.0010 0.0158 0.0200 79 22. - 178. 3758 blank cis-1,3-Dichloropropene mg/1 < 0.0010 0.0197 0.0200 98 22. - 178. 3759 blank cis-1,3-Dichloropropene mg/l < 0.0010 0.0243 0.0200 122 22. - 178. 3756 blank cis-1,3-Dichloropropene mg/l < 0.0010 0.0155 0.0200 78 22. - 178. 3758 blank cis-1,3-Dichloropropene mg/l < 0.0010 0.0230 0.0200 115 22. - 178. 3759 blank trans-1,3-Dichloropropene mg/l < 0.0010 0.0207 0.0200 104 22. - 178. 3756 blank trans-1,3-Dichloropropene mg/l < 0.0010 0.0152 0.0200 76 22. - 178. 3758 blank trans-1,3-Dichloropropene mg/l < 0.0010 0.0183 0.0200 92 22. - 178. 3759 blank trans-1,3-Dichloropropene mg/1 < 0.0010 0.0221 0.0200 110 22. - 178. 3756 blank trans-1,3-Dichloropropene mg/l < 0.0010 0.0155 0.0200 78 22. - 178. 3758 blank trans-1,3-Dichloropropene mg/l < 0.0010 0.0218 0.0200 109 22. - 178. 3759 blank Methylene chloride mg/l < 0.0050 0.0177 0.0200 88 25. - 162. 3756 blank Methylene chloride mg/1 < 0.0050 0.0181 0.0200 90 25. - 162. 3758 blank Methylene chloride mg/l < 0.0050 0.0162 0.0200 81 25. - 162. 3759 blank Methylene chloride mg/l < 0.0050 0.0240 0.0200 120 25. - 162. 3756 blank Methylene chloride mg/l < 0.0050 0.0163 0.0200 82 25. - 162. 3758 blank Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 /.800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Methylene chloride mg/1 0.0050 0.0179 0.0200 90 25. - 162. 3759 blank 1,1,2,2-Tetrachloroethane mg/l 0.0010 0.0211 0.0200 106 8. - 184. 3756 blank 1,1,2,2-Tetrachloroethane mg/l 0.0010 0.0195 0.0200 98 8. - 184. 3758 blank 1,1,2,2-Tetrachloroethane mg/l < 0.0010 0.0196 0.0200 98 8. - 184. 3759 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0227 0.0200 114 8. - 184. 3756 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0158 0.0200 79 8. - 184. 3758 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0225 0.0200 112 8. - 184. 3759 blank Tetrachloroethene mg/l < 0.0010 0.0198 0.0200 99 26. - 162. 3756 blank Tetrachloroethene mg/l < 0.0010 0.0184 0.0200 92 26. - 162. 3758 blank Tetrachloroethene mg/l < 0.0010 0.0194 0.0200 97 26. - 162. 3759 blank Tetrachloroethene mg/1 0.0010 0.0237 0.0200 118 26. - 162. 3756 blank Tetrachloroethene mg/l < 0.0010 0.0158 0.0200 79 26. - 162. 3758 blank Tetrachloroethene mg/l < 0.001.0 0.0225 0.0200 112 26. - 162. 3759 blank 1,1,1-Trichloroethane mg/l < 0.0010 0.0209 0.0200 104 41. - 138. 3756 blank 1,1,1-Trichloroethane mg/l < 0.0010 0.0193 0.0200 96 41. - 138. 3758 blank 1,1,1-Trichloroethane mg/l < 0.0010 0.0213 0.0200 106 41. - 138. 3759 blank 1,1,1-Trichloroethane mg/1 < 0.0010 0.0233 0.0200 116 41. - 138. 3756 blank 1,1,1-Trichloroethane mg/l < 0.0010 0.0165 0.0200 82 41. - 138. 3758 blank 1,1,1-Trichloroethane mg/l 0.0010 0.0242 0.0200 121 41. - 138. 3759 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0216 0.0200 108 39. - 136. 3756 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0183 0.0200 92 39. - 136. 3758 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0206 0.0200 103 39. - 136. 3759 blank 1,1,2-Trichloroethane mg/1 < 0.0010 0.0250 0.0200 125 39. - 136. 3756 blank 1,1,2-Trichloroethane mg/1 < 0.0010 0.0165 0.0200 82 39. - 136. 3758 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0240 0.0200 120 39. - 136. 3759 blank Trichloroethene mg/1 < 0.0010 0.0198 0.0200 99 35. - 146. 3756 blank Trichloroethene mg/1 < 0.0010 0.0177 0.0200 88 35. - 146. 3758 blank Trichloroethene mg/1 < 0.0010 0.0208 0.0200 104 35.. - 146. 3759 blank Trichloroethene mg/l < 0.0010 0.0237 0.0200 118 35. - 146. 3756 blank Trichloroethene mg/l < 0.0010 0.0177 0.0200 88 35. - 146. 3758 blank Trichloroethene mg/l < 0.0010 0.0234 0.0200 117 35. - 146. 3759 blank Trichlorofluoromethane mg/1 < 0.0010 0.0192 0.0200 96 21. - 156. 3756 blank Trichlorofluoromethane mg/l < 0.0010 0.0169 0.0200 84 21. - 156. 3758 blank Trichlorofluoromethane mg/l < 0.0010 0.0187 0.0200 94 21. - 156. 3759 blank Trichlorofluoromethane mg/1 < 0.0010 0.0231 0.0200 116 21. - 156. 3756 blank Trichlorofluoromethane mg/1 < 0.0010 0.0145 0.0200 72 21. - 156. 3758 blank Trichlorofluoromethane mg/1 0.0010 0.0202 0.0200 101 21. - 156. 3759 blank Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch Benzene ------- mg/1 ---------- 0.0500 ------------ 0.0494 ---------- 99 ------------ 77 - 123 --------- 3759 Benzene mg/l 0.0500 0.0537 107 77 - 123 3758 Chlorobenzene mg/1 0.0200 0.0236 118 81 - 120 3756 Chlorobenzene mg/l 0.0500 0.0536 107 81 - 120 3759 Chlorobenzene mg/1 0.0500 0.0493 99 81 - 120 3758 1,2-Dichlorobenzene mg/1 0.0200 0.0227 114 68 - 132 3756 1,2-Dichlorobenzene mg/l 0.0500 0.0529 106 68 - 132 3759 1,2-Dichlorobenzene mg/l 0.0500 0.0438 88 68 - 132 3758 1,3-Dichlorobenzene mg/1 0.0200 0.0232 116 73 - 128 3756 1,3-Dichlorobenzene mg/l 0.0500 0.0595 119 73 - 128 3759 1,3-Dichlorobenzene mg/l 0.0500 0.0419 84 73.- 128 3758 1,4-Dichlorobenzene mg/1 0.0200 0.0195 98 70 - 131 3756 1,4-Dichlorobenzene mg/1 0.0500 0.0520 104 70 - 131 3759 1,4-Dichlorobenzene mg/l 0.0500 0.0482 96 70 - 131 3758 Ethylbenzene mg/1 0.0500 0.0501 100 63 - 137 3759 Ethylbenzene mg/1 0.0500 0.0534 107 63 - 137 3758 Toluene mg/l 0.0500 0.0496 99 78 - 123 3759 Toluene mg/1 0.0500 0.0525 105 78 - 123 3758 m,p-Xylenes mg/1 0.1000 0.1046 105 70 - 130 3759 m,p-Xylenes mg/1 0.1000 0.0986 99 70 - 130 3758 o-Xylene mg/1 0.0500 0.0506 101 70 - 130 3759 o-Xylene mg/l 0.0500 0.0445 89 70 - 130 3758 Bromodichloromethane mg/1 0.0200 0.0190 95 76 - 124 3756 Bromodichloromethane mg/1 0.0500 0.0604 121 76 - 124 3759 Bromodichloromethane mg/1 0.0500 0.0437 87 76 - 124 3758 Bromoform mg/1 0.0200 0.0217 108 74 - 127 3756 Bromoform mg/1 0.0500 0.0578 116 74 - 127 3759 Bromoform mg/l 0.0500 0.0421 84 74 - 127 3758 Bromomethane mg/1 0.0200 0.0181 90 59 - 142 3756 Bromomethane mg/1 0.0500 0.0487 97 59 - 142 3759 Bromomethane mg/1 0.0500 0.0435 87 59 - 142 3758 Carbon tetrachloride mg/l 0.0200 0.0211 106 69 - 132 3756 - Carbon tetrachloride mg/l 0.0500 0.0538 108 69 - 132 3759 Carbon tetrachloride mg/l 0.0500 0.0448 90 69 - 132 3758 Chloroethane mg/1 0.0200 0.0214 107 77 - 123 3756 Chloroethane mg/1 0.0500 0.0374 75 # 77 - 123 3759 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch Chloroethane mg/1 0.0500 0.0444 89 77 - 123 3758 2-Chloroethylvinylether mg/l 0.0200 0.0147 74 60 - 140 3756 2-Chloroethylvinylether mg/1 0.0500 0.0562 112 60 - 140 3759 2-Chloroethylvinylether mg/l 0.0500 0.0396 79 60 - 140 3758 Chloroform mg/l 0.0200 0.0219 110 75 - 125 3756 Chloroform mg/l 0.0500 0.0581 116 75 - 125 3759 Chloroform mg/l 0.0500 0.0472 94 75 - 125 3758 Chloromethane mg/1 0.0200 0.0144 72 60 - 141 3756 Chloromethane mg/l 0.0500 0.0414 83 60 - 141 3759 Chloromethane mg/1 0.0500 0.0414 83 60 - 141 3758 Dibromochloromethane mg/l 0.0200 0.0200 100 66 - 135 3756 Dibromochloromethane mg/l 0.0500 0.0584 117 66 - 135 3759 Dibromochloromethane mg/1 0.0500 0.0430 86 66 - 135 3758 Ethylene Dibromide mg/l 0.0200 0.0245 122 70 - 130 3756 Ethylene Dibromide mg/1 0.0500 0.0570 114 70 - 130 3759 Ethylene Dibromide mg/l 0.0500 0.0433 87 70 - 130 3758 Vinyl chloride mg/l 0.0200 0.0223 112 70 - 130 3756 Vinyl chloride mg/l 0.0500 0.0508 102 70 - 130 3759 Vinyl chloride mg/l 0.0500 0.0431 86 70 - 130 3758 Dichlorodifluoromethane mg/1 0.0200 0.0170 85 70 - 130 3756 Dichlorodifluoromethane mg/l 0.0500 0.0488 98 70 - 130 3759 Dichlorodifluoromethane mg/1 0.0500 0.0363 73 70 - 130 3758 1,1-Dichloroethane mg/1 0.0200 0.0209 104 84 - 116 3756 1,1-Dichloroethane mg/1 0.0500 0.0566 113 84 - 116 3759 1,1-Dichloroethane mg/l 0.0500 0.0436 87 84 - 116 3758 1,2-Dichloroethane mg/l 0.0200 0.0209 104 72 - 129 3756 1,2-Dichloroethane mg/l 0.0500 0.0561 112 72 - 129 3759 1,2-Dichloroethane mg/l 0.0500 0.0459 92 72 - 129 3758 1,1-Dichloroethene mg/1 0.0200 0.0197 98 63 - 137 3756 1,1-Dichloroethene mg/l 0.0500 0.0473 95 63 - 137 3759 1,1-Dichloroethene mg/l 0.0500 0.0460 92 63 - 137 3758 cis-1,2-Dichloroethene mg/l 0.0200 0.0207 104 70 - 130 3756 " cis-1,2-Dichloroethene mg/l 0.0500 0.0571 114 70 - 130 3759 cis-1,2-Dichloroethene mg/l 0.0500 0.0444 89 70 - 130 3758 trans-1,2-Dichloroethene mg/l 0.0200 0.0199 100 64 - 136 3756 trans-1,2-Dichloroethene mg/1 0.0500 0.0570 114 64 - 136 3759 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 i f Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units Known Val. Analyzed Val. % Recovery Target Range Q.C. Batch trans-1,2-Dichloroethene ------- mg/l ---------- 0.0500 ------------ 0.0443 ---------- 89 ------------ 64 - 136 --------- 3758 1,2-Dichloropropane mg/l 0.0200 0.0183 92 74 - 126 3756 1,2-Dichloropropane mg/1 0.0500 0.0597 119 74 - 126 3759 1,2-Dichloropropane mg/l 0.0500 0.0440 88 74 - 126 3758 cis-1,3-Dichloropropene mg/l 0.0200 0.0199 100 63 - 136 3756 cis-1,3-Dichloropropene mg/l 0.0500 0.0523 105 63 - 136 3759 cis-1,3-Dichloropropene mg/l 0.0500 0.0436 87 63 - 136 3758 trans-1,3-Dichloropropene mg/l 0.0200 0.0196 98 70 - 130 3756 trans-1,3-Dichloropropene mg/1. 0.0500 0.0522 104 70 - 130 3759 trans-1,3-Dichloropropene mg/1 0.0500 0.0436 87 70 - 130 3758 Methylene chloride mg/l 0.0200 0.0198 99 78 - 123 3756 Methylene chloride mg/1. 0.0500 0.0431 86 78 - 123 3759 Methylene chloride mg/1 0.0500 0.0439 88 78 - 123 3758 1,1,2,2-Tetrachloroethane mg/l 0.0200 0.0183 92 49 - 151 3756 1,1,2,2-Tetrachloroethane mg/1 0.0500 0.0530 106 49 - 151 3759 1,1,2,2-Tetrachloroethane mg/l 0.0500 0.0479 96 49 - 151 3758 Tetrachloroethene mg/l 0.0200 0.0221 110 70 - 130 3756 Tetrachloroethene mg/l 0.0500 0.0403 81 70 - 130 3759 Tetrachloroethene mg/1 0.0500 0.0428 86 70 - 130 3758 1,1,1-Trichloroethane mg/l 0.0200 0.0234 117 71 - 129 3756 1,1,1-Trichloroethane mg/l 0.0500 0.0585 117 71 - 129 3759 1,1,1-Trichloroethane mg/1 0.0500 0.0456 91 71 - 129 3758 1,1,2-Trichloroethane mg/l 0.0200 0.0214 107 79 - 122 3756 1,1,2-Trichloroethane mg/l 0.0500 0.0527 105 79 - 122 3759 1,1,2-Trichloroethane mg/l 0.0500 0.0414 83 79 - 122 3758 Trichloroethene mg/1 0.0200 0.0202 101 77 - 123 3756 Trichloroethene mg/1 0.0500 0.0502 100 77 - 123 3759 Trichloroethene mg/l 0.0500 0.0467 93 77 - 123 3758 Trichlorofluoromethane mg/l 0.0200 0.0189 94 67 - 134 3756 Trichlorofluoromethane mg/l 0.0500 0.0505 101 67 - 134 3759 Trichlorofluoromethane mg/1 0.0500 0.0452 90 67 - 134 3758 Project QC continued . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica �- I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Blank Data - Analyte --------------- Blank Value Units Q.C. Batch Benzene ------------ < 0.0010 --------- mg/1 ---------- 3758 Benzene < 0.0010 mg/1 3758 Benzene < 0-.0010 mg/1 3759 Benzene < 0.0010 mg/l 3759 Chlorobenzene < 0.0010 mg/1 3756 Chlorobenzene < 0.0010 mg/l 3756 Chlorobenzene < 0.0010 mg/l 3758 Chlorobenzene < 0.0010 mg/l 3758 Chlorobenzene < 0.0010 mg/1 3759 Chlorobenzene < 0.0010 mg/1 3759 1,2-Dichlorobenzene < 0.0010 mg/1 3756 1,2-Dichlorobenzene < 0.0010 mg/1 3756 1,2-Dichlorobenzene < 0.0010 mg/1 3758 1,2-Dichlorobenzene < 0.0010 mg/l 3758 1,2-Dichlorobenzene < 0.0010 mg/l 3759 1,2-Dichlorobenzene < 0.0010 mg/l 3759 1,3-Dichlorobenzene < 0.0010 mg/l 3756 1,3-Dichlorobenzene <.0.0010 mg/1 3756 1,3-Dichlorobenzene < 0.0010 mg/1 3758 1,3-Dichlorobenzene < 0.0010 mg/1 3758 1,3-Dichlorobenzene < 0.0010 mg/1 3759 1,3-Dichlorobenzene < 0.0010 mg/1 3759 1,4-Dichlorobenzene < 0.0010 mg/1 3756 1,4-Dichlorobenzene < 0.0010 mg/l 3756 1,4-Dichlorobenzene < 0.0010 mg/l 3758 1,4-Dichlorobenzene < 0.0010 mg/1 3758 1,4-Dichlorobenzene < 0.0010 mg/l 3759 1,4-Dichlorobenzene < 0.0010 mg/l 3759 Ethylbenzene < 0.0010 mg/l 3758 Ethylbenzene < 0.0010 mg/1 3758 Ethylbenzene < 0.0010 mg/1 3759 " Ethylbenzene < 0.0010 mg/1 3759 Toluene < 0.0010 mg1l 3758 Toluene < 0.0010 ing/l 3758 Toluene < 0.0010 mg/1 3759 Toluene < 0.0010 mg/1 3759 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch m,p-Xylenes < 0.0010 mg/l 3758 m,p-Xylenes < 0.0010 mg/l 3758 m,p-Xylenes < 0.0010 mg/l 3759 m,p-Xylenes < 0.0010 mg/l 3759 o-Xylene < 0.0010 mg/l 3758 o-Xylene < 0.0010 mg/1 3758 o-Xylene < 0.0010 mg/1 3759 o-Xylene < 0.0010 mg/l 3759 Bromodichloromethane < 0.0010 mg/1 3756 Bromodichloromethane < 0.0010 mg/l 3756 Bromodichloromethane < 0.0010 mg/l 3758 Bromodichloromethane < 0.0010 mg/l 3758 Bromodichloromethane < 0.0010 mg/l 3759 Bromodichloromethane < 0.0010 mg/l 3759 Bromoform < 0.0010 mg/l 3756 Bromoform < 0.0010 mg/l 3756 Bromoform < 0.0010 mg/l 3758 Bromoform < 0.0010 mg/1 3758 Bromoform < 0.0010 mg/1 3759 Bromoform < 0.0010 mg/l 3759 Bromomethane < 0.0010 mg/1 3756 Bromomethane < 0.0010 mg/1 3756 Bromomethane < 0.0010 ing/l 3758 Bromomethane < 0.0010 mg/l 3758 Bromomethane < 0.0010 mg/l 3759 Bromomethane < 0.0010 mg/1 3759 Carbon tetrachloride < 0.0010 mg/l 3756 Carbon tetrachloride < 0.0010 mg/l 3756 Carbon tetrachloride < 0.0010 mg/l 3758 Carbon tetrachloride < 0.0010 mg/l 3758 Carbon tetrachloride < 0.0010 mg/l 3759 Carbon tetrachloride < 0.0010 mg/l 3759 Chloroethane < 0.0010 mg/l 3756 Chloroethane < 0.0010 mg/l 3756 Chloroethane < 0.0010 mg/l 3758 Chloroethane < 0.0010 mg/l 3758 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 • Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value --------------- Units Q.C. Batch ------------ Chloroethane 0.0010 --------- mg/l ---------- 3759 Chloroethane < 0.0010 mg/l 3759 2-Chloroethylvinylether < 0.0010 mg/l 3756 2-Chloroethylvinylether < 0.0010 mg/l 3756 2-Chloroethylvinylether < 0.0010 mg/l 3758 2-Chloroethylvinylether < 0.0010 mg/l 3758 2-Chloroethylvinylether < 0.0010 mg/l 3759 2-Chloroethylvinylether < 0.0010 mg/l 3759 Chloroform 0.0010 mg/l 3756 Chloroform < 0.0010 mg/l 3756 Chloroform < 0.0010 mg/l 3758 Chloroform < 0.0010 mg/l 3758 Chloroform < 0.0010 mg/1 3759 Chloroform < 0.0010 mg/l 3759 Chloromethane < 0.0010 mg/l 3756 Chloromethane < 0.0010 mg/l 3756 Chloromethane < 0.0010 mg/l 3758 Chloromethane < 0-0010 mg/l 3758 Chloromethane < 0.0010 mg/1 3759 Chloromethane < 0.0010 mg/1 3759 Dibromochloromethane < 0.0010 mg/l 3756 Dibromochloromethane < 0.0010 mg/1 3756 Dibromochloromethane < 0.0010 mg/l 3758 Dibromochloromethane < 0.0010 mg/l 3758 Dibromochloromethane < 0.0010 mg/l 3759 Dibromochloromethane < 0.0010 mg/l 3759 Ethylene Dibromide < 0.0010 mg/l 3756 Ethylene Dibromide < 0.0010 mg/1 3756 Ethylene Dibromide < 0.0010 mg/l 3758 Ethylene Dibromide < 0.0010 mg/1 3758 Ethylene Dibromide < 0.0010 mg/1 3759 Ethylene Dibromide < 0.0010 mg/1 3759 Vinyl chloride < 0.0010 mg/l 3756 Vinyl chloride < 0.0010 Png/l 3756 Vinyl chloride < 0.0010 mg/l 3758 Vinyl chloride < 0.0010 mg/l 3758 Project QC continued . . . Ii 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te)stl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value --------------- Units Q.C. Batch _------------ Vinyl chloride < 0.0010 --------- mg/1 ---------- 3759 Vinyl chloride < 0.0010 mg/l 3759 Dichlorodifluoromethane < 0.0010 mg/l 3756 Dichlorodifluoromethane < 0.0010 mg/l 3756 Dichlorodifluoromethane < 0.0010 mg/l 3758 Dichlorodifluoromethane < 0.0010 mg/l 3758 Dichlorodifluoromethane < 0.0010 mg/l 3759 Dichlorodifluoromethane < 0.0010 mg/l 3759 1,1-Dichloroethane < 0.0010 mg/l 3756 1,1-Dichloroethane < 0.0010 mg/l 3756 1,1-Dichloroethane < 0.0010 mg/l 3758 1,1-Dichloroethane < 0.0010 mg/l 3758 1,1-Dichloroethane < 0.0010 mg/l 3759 - 1,1-Dichloroethane < 0.0010 mg/l 3759 1,2-Dichloroethane < 0.0010 mg/l 3756 1,2-Dichloroethane < 0.0010 mg/l 3756 1,2-Dichloroethane < 0.0010 mg/1 3758 1,2-Dichloroethane < 0.0010 mg/l 3758 1,2-Dichloroethane < 0.0010 mg/1 3759 1,2-Dichloroethane < 0.0010 mg/1 3759 1,1-Dichloroethene < 0.0010 mg/l 3756 i 1,1-Dichloroethene < 0.0010 mg/l 3756 1,1-Dichloroethene < 0.0010 mg/l 3758 1,1-Dichloroethene < 0.0010 mg/1 ,3758 1,1-Dichloroethene < 0.0010 mg/1 3759 1,1-Dichloroethene < 0.0010 mg/l 3759 cis-1,2-Dichloroethene < 0.0010 mg/l 3756 cis-1,2-Dichloroethene < 0.0010 mg/l 3756 cis-1,2-Dichloroethene < 0.0010 mg/1 3758 cis-1,2-Dichloroethene < 0.0010 mg/l 3758 cis-1,2-Dichloroethene < 0.0010 mg/l 3759 cis-1,2-Dichloroethene < 0.0010 mg/1 3759 trans-1,2-Dichloroethene < 0.0010 mg/1 3756 trans-1,2-Dichloroethene < 0.0010 mg/l 3756 trans-1,2-Dichloroethene < 0.0010 mg/1 3758 trans-1,2-Dichloroethene < 0.0010 mg/1 3758 I r Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value Units Q.C. Batch trans-1,2-Dichloroethene < 0.0010 mg/l 3759 trans-1,2-Dichloroethene < 0.0010 mg/l 3759 1,2-Dichloropropane < 0.0010 mg/l 3756 1,2-Dichloropropane < 0.0010 mg/l 3756 1,2-Dichloropropane < 0.0010 mg/l 3758 1,2-Dichloropropane < 0.0010 mg/1 3758 1,2-Dichloropropane < 0.0010 mg/l 3759 1,2-Dichloropropane < 0.0010 mg/1 3759 ,- cis-1,3-Dichloropropene < 0.0010 mg/l 3756 cis-1,3-Dichloropropene < 0.0010 mg/1 3756 cis-1,3-Dichloropropene < 0.0010 mg/1 3758 cis-1,3-Dichloropropene < 0.0010 mg/l 3758 cis-1,3-Dichloropropene < 0.0010 mg/1 3759 cis-1,3-Dichloropropene < 0.0010 mg/1 3759 trans-1,3-Dichloropropene < 0.0010 mg/l 3756 trans-1,3-Dichloropropene < 0.0010 mg/l 3756 trans-1,3-Dichloropropene < 0.0010 mg/l 3758 trans-1,3-Dichloropropene < 0.0010 mg/l 3758 trans-1,3-Dichloropropene < 0.0010 mg/l 3759 trans-1,3-Dichloropropene < 0.0010 mg/l 3759 Methylene chloride 1 < 0.0050 mg/1 3756 Methylene chloride < 0.0050 mg/l 3756 Methylene chloride < 0.0050 mg/l 3758 Methylene chloride < 0.0050 mg/l 3758 Methylene chloride < 0.0050 mg/l 3759 Methylene chloride < 0.0050 mg/l 3759 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 3756 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 3756 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 3758 1,1,2,2-Tetrachloroethane < 0.0010 mg/1 3758 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 3759 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 3759 Tetrachloroethene < 0.0010 mg/l 3756 Tetrachloroethene < 0.0010 *mg/l 3756 Tetrachloroethene < 0.0010 mg/1 3758 Tetrachloroethene < 0.0010 mg/l 3758 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica -J I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value --------------- Units Q.C. Batch ------------ Tetrachloroethene < 0.0010 --------- mg/l ---------- 3759 Tetrachloroethene < 0.0010 mg/1 3759 1,1,1-Trichloroethane < 0.0010 mg/1 3756 1,1,1-Trichloroethane < 0.0010 mg/1 3756 1,1,1-Trichloroethane < 0.0010 mg/1 3758 1,1,1-Trichloroethane < 0.0010 mg/1 3758 1,1,1-Trichloroethane < 0.0010 mg/1 3759 1,1,1-Trichloroethane < 0.0010 mg/1 3759 1,1,2-Trichloroethane < 0.0010 mg/1 3756 1,1,2-Trichloroethane < 0.0010 mg/1 3756 1,1,2-Trichloroethane < 0.0010 mg/1 3758 1,1,2-Trichloroethane < 0.0010 mg/1 3758 1,1,2-Trichloroethane < 0.0010 mg/1 3759 1,1,2-Trichloroethane < 0.0010 mg/1 3759 Trichloroethene < 0.0010 mg/1 3756 Trichloroethene < 0.0010 mg/1 3756 Trichloroethene < 0.0010 mg/1 3758 Trichloroethene < 0.0010 mg/1 3758 Trichloroethene < 0.0010 mg/1 3759 Trichloroethene < 0.0010 mg/l 3759 Trichlorofluoromethane < 0.0010 mg/1 3756 Trichlorofluoromethane < 0.0010 mg/1 3756 Trichlorofluoromethane < 0.0010 mg/l 3758 Trichlorofluoromethane < 0.0010 mg/l 3758 Trichlorofluoromethane < 0.0010 mg/1 3759 Trichlorofluoromethane < 0.0010 mg/1 3759 # - Value outside Laboratory historical QC limits. End of Report for Project 206985 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica Incorporated PURCHASE ORDER FOR INTERLAB ANALYSIS Purchase Order # d© —0 in �, Account # a. ,-� Q Sending Division M 041k c C E Receiving Division S' _ Initiated By Accepted By Client Project # (s) :M f O7s 3 5 Sending Date Report Due Date 6y Holding Time See COC QC Deliverables See COC . Certifications Required Special Reporting Limit(s) i Additional Comments and Specific Requests (Example: Analytes, Client Specific QC) Attach copy or original TestAmerica Incorporated COC(s). Use shaded lab use areas to designate lab being sent to and total number of containers sent Ensure that methods aredesignated. Reference PO# of this form on original COC(s). Sign enclosed COC to relinquish and receive samples. Return original signature copy with final report If samples are logged in at `original lab" prior to subbing, a copy of login summary may be attached. Price per Sample Based on: Price Charged to Client List Price Method Matrix # of Samples Price per Sample Inter -Lab Discount Inter -Lab Revenue O ( w 3? ) O l� 2'. 2 Inter -Lab Revenue Rush Charge % QC Charge % TOTAL INTER -LAB REVENUE SO - ■ - - 1,-)Gq 0) 4, Page t' of Q NC (K) 0-1qashville, TN (M) 0 Pontiac, MI (0) 0 Rockford. 11 (Q) 0 Asheville, NC (A) 0 Bartlett, IL (C) 0 Ceda 0 0 0 7 3 2 242-- 1190 (615)726-0177 (248)332-1940 (815)874-2171 (828)254-5169 (630)289-3100 (319: O Atlanta, GA (B) 0 Brighton, CO (D)0 Chan. MORRISVILLE NC s, IN (L) 0 Macon, GA (N) 0 Orlando, FL (P) 0 Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 g (319)3LJ-/944 t.)L1)o4z-4261 (912)757-0811 (407)851-2560 (920)261-1660 Client: 11., Project No.: IO 1535 REQUESTED PARAMETERS Report Address:22 Invoice Address: Is this work being conducted for regulatory compliance monitoring? Yes_ No- Is this work being conducted for regulatory enforcement action? Yes_ No_ O Which regulations apply: RCRA_ NPDESWastewater_ //,, 1 •VILL Z,7 V Attn: Attn: � Phone No.: _ 2 z Sampled By. L� Fax No.: q P.O. No: 13037r Quote No. TURNAROUND TIA1F. UST_ Drinking Water_ Other_ None_ State Sample; Collected O'Standard 0 Rush (surcharges mDate may apply) Needed: a and tVDe of containers Sample 1D Date Time Grati (Gj Matrix Lab Use u o ��„ r,,°. o REMARKS q-a,00 15�2 htk . 01 s 2CC 1335 &' F S[v�Sr G w i� 3 ' y'. VV�� Deliverables: I. None 0 Leve12 Hatch K.0., —PC r R3 x�- x E' aRec TeiOsiiz 66 `' 'A "--.-F:. 0 Level 3 O Ue A l Other,.. r -x �� ,s9 RA,. f. .•� .,.s:. ,. YR -'x .?��'.i 3..,g3 �° i'�,i' F _. v°3 m:°�. >;` v..,; ,-Y' t0 COMMENTS: MOI.1-ISVilIe Office FAX# (919) 3 17 - By: v �e LABUS>� UriLY Relinquished By6 Date •�, Time Received . Relinquished By: y(S a Received B Date Time r� Relinquished By: Date Time Received By: Date Time Custody Seal ( Yes ON �N/A n (� O g,..:......:..... u... Il•i r t Time• Rrr ived Rv I 1.� YN� �:i�Cg O l Og�Time Bottles Supplied by TA: OYes L1No - W"mAke Ali- .haiu of Custody Record v ❑ Asheville, NC (A) ❑ Bartlett, IL (C) ❑ Cedar Falls, IA (E)(-7 Chark n� O� (828)254-5169 (630)289-3100 (319)277-2401 (7(4I v J �/ ❑ Atlanta, GA (B) ❑ Brighton, CO (D)❑ Charleston, SC (F) ❑ Culut (770)368-0636 (303)659-0497 (843)849-6550 (803)7yu-o—, noo� ni c, TN (M) ❑ Pontiac, MI (0) ❑ Rockford. Il (Q) 6-0177 (248)332-1940 (815)874-2171 GA (N) ❑ Orlando, FL (P) ❑ Watertown, WI (R) i7-0811 (407)851-2560 (920)261-1660 Client: -F " Project No.: —Yt� /0.n'. 3-�' REQUESTED PARAME I r AS Report Address: 2)w Invoice Address: Is this work being conducted for regulatory compliance monitoring? Yes_ No- Is this work being conducted for regulatory enforcement action? Yes_ No_ Which regulations apply: RCRA_ NPDESWastewater_ p� S f �^�S I%C✓ .. �. j NL Attn: � Attn: 5qj" Phone No.:�(d I� 2�j -/I Sampled By: k e Sli"r)e` r(�', r r� �l q Fax No.: �� -I `fG 7 �l o` / P.O. No: I BUJ i 30 3%7 Quote No. TURNAROUND TIME UST_ Drinking Water_ State Samples Collected #( Standard Q Other_ None_ ❑ Rush (surcharges may apply) Date Needed: — Cho �J y and type of containers ID Date Time COMSample Grab (Gj Matrix Lab Use o .$ o REMARKS 6ML) I M05 G! Iq Q ✓ ✓ 3 �S Gw-SUS loin ✓ 2 StS• &W Do 02- If I � ✓ ,/ 3 i1LA ✓ 2 Qs—Gtj— WOO /313 c' ✓ 2 as - c-w - PrSd TSB : ! >' '� ✓ 3 SCS �-u- 11��P 13 ►y�� . ✓ ✓ 3 Sc s_Gw Pr 1 d77 i sad �q ✓ QC Deliverables ': O 1Vane . ❑ Leve12 BaCch QC A � (7 Level 3 O Leve14 L"1 Qther,.i<. I!ttit Lab Rec Lab Temp e. .: Z . U COMMENTS: Morrisville office FAXI! (919) 380-9717 -Y • w / 7 3 Time Received a�e9 �e i.A#'USE ONLY Relinquished By Da t Relinquished By: .� Z t%Q) Received y: Date Time Custody Sea]: ::. OYes ONO ON/A Relinquished B Date Time Received By: Date Time f Received By: (, . W"Time pQTime Bottles Supplied by TA: OYes ONO •Relinnu; ;,, d Rv Date I — CO_ OIRECEIPT F� Client: Z'C 0 o And Opened On: q. oD By: Chris Wilmoth Cooler Received On: (Signature) Temperature of Cooler when opened 50 De tees elsius 1. Tem P ........YES NO Were custody seals on outside of cooler? ............................................... 2. — a. If yes, how many, what kind and where: ............YES b, Were the seals intact, signed, and dated correctly? •••'••'•""' .....NO YES custody seals on containers and intact? ............. 3, Were•••• .... S O papers inside coo ............... 4• Were custody p cooler? NO Were custody papers properly filled out (inksigned,etc) .................... 5. lace? ............................. 6. Did you sign the custody Paper s in the appropriate p 7• What kind of packing material used? ubble p Peanuts Vermiculite Other None ..................... 8• Was sufficient ice used (if appropriate)?—*--.... yq NO unbroken)? ............................ 9• Did all bottles arrive in good condition( .. NO edpres,etc)? ............... 10. Were all bottle labels complete #,date,sign• """" ......... �$ NO 11. Did all bottle labels and tags agree with custody papers?..............NO 12. Were correct bottles used for the analysis req vials received?............ 13. a. Were VOAYES observable head space present in any VOA vial?•............ b• Was there any 5.YE NO NO 14. Was sufficient amount of sample sent in each bottle? ................... .::::::.::....•• 15. Were correct preservatives use ................. ..........................NO YES 16. Was residual chlorine present? ................. 17. Corrective action taken, if necessary: See attached for resolution 8/15100 LF-1 Cooler Receipt Form 1 '6 Tk ('habi of Custody Record '-,`j -) UO-0764 7 r\,hey ille, NC (A) ❑ Bartlett, IL (C) 17 Cedar Palls, IA (E)❑ Charlotte, I Y (M) ❑ Pontiac, MI (0) ❑j Rocl ford (Q)1, :Il (828) 254-5109 (630) 289-3100 (319) 277-2401 (704) 392-1 MORRISVILLE, NC 77 (248)332.1940 (8:15) 874 2t71 7 1-1 Atlanta. G;1(Il ) ❑ Brighuat, CO (D)❑ Ch:uicston, SC (P) ❑ Columbia, SC (I i) ❑ Davenport. IA (J) ❑Indianapolis, IN (L) O Macon, GA (N) ❑Orlando, FL (P) 'j❑ iWateaown;Wl;:(It (7701 368-0636 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7944 (317) 842-4261 (912) 757-0911 (407) 851-2560 (920)261-1660 project No.: M535 REQUESTED PARAMETERS Invoice Address: 111•:-, _._ Is this work being conducted for regulatoryr r 'z compliance monitoring ►.yesN Is this work being conducted for \ O'V YeulatoNoenforcet(+e acho�� arti n 1 N kt i ----- Rhone No.: (�'�" ��"l .. 2z2� 1 Sampled Bye L��� Fax No.: C P.o. No. — Which regulations appl440. RCRA" NPDk:SWastete UST ; 1 nn 1, 1. gI Wattr r Cl)�tNAROUtiU'1lNih: Quote No. Suac Samples Collected rol/ t Scuulard/ Other fx t ityNone*- • - — Needed: 1 Rush (surcharges may apply) Date and t of of containers . r . • . r n t +- , >JEe: Sample 1D Date Timc Comp (C) Crab ((;) rvlatrix l.ab use � O a .O C °�' 9 '; e 0 +� 1�3� Ri;MARKS •r S^ i r— Akr drt UJ - 5S �S l 3 IN ;4L,� 4 t y . r.:.-{ #b .'y/':d.M 4'•�l'1} l 1 ` ! , ` , 't�(� I1 0q0 QC Dellverahles: ❑ None r7l Levu 2 - Batch QCy.- i n Level 0 Level -..❑ Other ,/ p ('(t11\II:N1;S: s`'t Morro i SV��r f�1c FAX# (010) / ff Date t �ime Lr� ffS)~yS' K lin ui,hed l3 i )ate Inne Received By: - - i:.•lul, uish.d By: Date ime Received By: Date Time l Gnyui>h d Li). Date 1---- Time Received By: Date I Time v zz $ A' Utumamoo Y Im+c Received By: � l •'7) ODTimelpttleBSINe�'!' i"• y A LA iw+r r ^r M Am AN I 1 t n ZJ J Z5 I tai' MiCii1 A 1HUM �- � V f � � jb I�;� o 'ruin of Cnstod y Record 1; Pa e' 1-3 Cedar Falls, IA (E)Q Charlotte, NC (G) [I Dayton, OH (I) Q Lumberton, NC (K) Nashville, TN (NT) ❑!'Pontiac, MI (0) l Q Rockford II (Q)F. r +I (248)332-1940 '�815)874 2171. (8_'S)_)54 5169 (630)289-3100 (319)277-3401 (704) 3921164 (937)294-6856 -1 CO (D)❑ Charleston, SC (F) Q Columbia, SC (11) ❑ Davenport. IA (J) (910)738-6190 (615)726.0177 Q Indianapolis, IN (L) Q Macon, GA (N) ❑ :Orlando; FL (P) ❑ °Watertown` Wl- R� 26W660 :\danta. GA (13) L7 fitirhion, 070) 30S-0036 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7944 (317) 842-4261 (912) 757-0811 I(407) 851-2560 (920) REQUESTED PARAMETERSProjectNo.: 35 11:at i Address: �{1►+� � ri ' I s+ I'; pol l ,\Jdre,,: Invoice Is this work,lietng conducted for+`e�:? ---'---- J` regulatory,i'bauaw,.;? -'- Attn: cb compitance monitoring?Yes ,44- `a a i for utrl ,( - o Is this work tieing condtcted regulatory enforcement action? : (I'^ 1'la)nNu.: Sampled By. Yes_ No`tl� ll�i' Fax No.: IC- 1 (' t O. No: —1 Which regulahons`apply I Quote No. RC]Z ,NPDESWastewater� UST ` r r Dnnktng Water ru1zNARounD rinlr, J State Samples Collected I '`J �., i Other y„ rat : " J�Ione m vi standard 'V I nth, yy, 7 Rush (surcharges may apply) Date Needed: # and type of containers Croup (C) Matrix Lai) Use Date rime •; p o�, �- a nyt�'�) REMARKS V e : € ,r l )�A -.,. ) Sample ID Grab (G) .: 40 0 7 7 1 SNO ;eAw 4A,'xJt k I t . 5 s �1- 53SV// �. -law 15 20 UL - y QC Deliverables: Q None Q Level 2 - Batch QC ON i r Q Level 3 Q Level ❑ Other (t)NIlvlliNl'S: Mornsvill r AX# (9119)f380,97-(1?' �. J Received B Dales Relinquished Time, I—]uaµu,he.I By: Dat�/!rl Z. �imc Received By: Date $ lw ui.h� I l3 i Y_ — - Date Time Received By: -- ----- 1 — t):,, • r I'ilne Received C3V: �1 i� U� Date Time CttSMdy Sb81 € '- CS c= a.: tLk lOZi S �., �t I�i / I lime 11Ott(CSSupp)iEd I',' ..,. �,.-I1,-,i it, 7rcrirr (i% Custody Recurcf JJ f Lb rhiviEHICA Mi. Ou-b t G, I J ref 71 Asheville, NC (A) ❑ Bartlett, IL (C) ❑ Cedar Falls, lA (G)❑ Charlotte, NC (G) ❑ Dayton, Oil (1) ❑ Lumberton, NC (K) Nashville, TN (M) ❑ Pontiac, MI (0) ' ❑Rockford II (Q), t828)254-5109 (030)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 (615)726-0177 (248)332-1940 (815)874 2171 71 .\Manta. GA (13) ❑ 13ri hton, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. IA (J) ❑ Indianapolis, IN (L) ❑ Macon, GA (N) ❑ Orlando,FL (P) • : ❑ Waiertown WI ;(R} 77u) 368 U636 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7944 (317) 842-4261 (912) 757-0811 (407) 851-2560 (920) 261-1660 ( hciu O Project No.: Invoice Address: REQUESTED PARAMETERS Re,oliAddies,: Is this work being conducted for 3 s. IX regulatory,:, s�_Nb compliance monitoring Y 4010 Cks Is this work being conducted;for; Attn: Phone N,,.: Sampled B''(� jj� ����•-- P Y '/' nU regulatory enforcement action? Yes s — Fax No.. P.O. No: -[ Which regulations apply I'4 %RCRA' NPDF.SWas4water6 Quote No. i7N \ROUND TIAIP: UST Drinking Water State Samples Collected �f'/ Swndard Other None Needed: 11 Rw h (surcharges may apply) Date a # and type of containers Sample 11) Date 1'imc Gralip (G) Matrix Lab Use iJ o '0 1 ;i" RI'sMARKS a Ti= MR (0L(r) A►1GA►�n'cKbt 11 1' �`LS nt\f; 3 I` i` tt It l ✓ i„ )UPUS �t S-T') —M I2-01 ✓ 2 ? '�'7w ., s.'r .t.. �1U , �.L ' nc•i vel:c Dell None ❑Level 2 - }3atch QC s , , 3 x� s � ^S � � v� I?�(�4•�, tt��r�t �)�,IF )���t )� �i �I!'tliui. �� f C1 Level 3 CI Level 4 ❑Other -- aX r), l ()11,\11:N'I S: y 0, , IVl0r6Ile o f� FAX# 1( Im,!uishcd It ;r�s I-Aw Received B -— Date 03 ime I eliioluished By: 'Y/ Did"X,,24,:��4inic Received By: Date Time Ischu,,uish� 1 Bs: Date Time Received By: Da a Timet` -- --- Ctts�i►d'SCal es o �Ax �� t ?urirt a/•Cuslurl)' Record 2338 h MlEkiGh ift I�1 Banleu, IL (C) ❑ Crdar I :Ills, IA (li)L-3 Charlotte, NC (G) ❑Dayton, OI I (I) Cl Lumberton, NC (K) 1828)254-5169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-6856 (910)738-6190 71 Athnta. GA (11) 11 Brionon, CO (D)i7 Charleston, SC (F) L-1 Columbia, SC (II) ❑ Davenport. IA (1) ❑ Indianapolis, IN (L) .,,,, I. Qnz, '7oi_Qos10 (I101 "3Tt_7944 (317) 942-4261 rp(Nasliville,TN(M) ❑(: Pontiac, MI (0) D Rockford:.11(Q) (615) 726-0177 (248) 332-1940 (815) 874 2t71 ;� O Macon, GA (N) Of Orlando, FL(P) Q Wa(t rtown WT; (R) (912) 757.0811 f (407) 851-2560 . ';' jr, (920) 261-1660 •;..`ti Project No.: ' REQUESTED PARAMETERS E rya , , ,via t licnt: C�7P I:r „Irt ldlhess: I Invoice Address: � f ti 4F Is this work being conducted for regulatory '„q,pn pt >: — �\ complianceiinomtonng?Yes Is this work 6eing•conductedfor +h till KCi7�' An"• I,Ijti11LNo.:Sampled By: �[C3 • eu— n� \' �/ Q regulatory enforcement action?,;, c Yes_ No_t�, -- Fax No.: Which regulattoris apply 13U 3�14, P.O. No RCR-A NPDESWastewater7 !v ' ^` UST Drinking Water S 1'UIL\:> ROIiNU'1'IMI? quote No. �Standa,lt State Samples Collected V Other None '�7 7 hush (surchal�cs may apply) Date Needed: # and type of containers Sample ID Date 'Time Comp (C) Grab (G) matrix Lab Use v O C g ,RENfARKS, tt ty� 77,�t!„ BLS -G W-U'W 31 t2. f °lx� ,- ILIA D i {12 U y{ ;•`� 1, t Y_.7N',tyyt /� QC Deliverables: ❑None ICI I..eve1 3 - Batch QC 0 L..evel 3 O Leve14 n Other _ <s 011i- ttb"a _ - (, m,nn:N'rs: Morrisville 'office -, FAX# (919 �t/'FitS1e Received By {�✓ Datt 1fk, ?.??"),rime LAD USE ONLSC kt �� A,� Date Z me Received By: Date Time Y.ri - Time Received By: Date > Time p'' I kx o CusMd "Sea Iiuyui hrJ Lay: Date ! — RcceivedBy: D toJae 21Vch-e Bottles .Snpptied byTA: r,,t, I Ii,uc K. 2338 i� zi ihvifkWA W16. ��~ v �' '..Page o 'Costae! Record luijr (•I y NC ❑ Bartlett, IL (C) ❑ Cedar Palls, IA (F)CICharlotte, NC (G) ❑ Dayton, 01( (I) ClLumberton, NC (K) . Nashville, TN (M) ❑Pontiac, MI (0) ❑Rockford. Il (Q) ti (815)874 2171 11 Asheville, (,�) (8_8) _54-5109 � 89_;100 (319)277-2401 (7U4)392-1164 (937)294-6856 (910)738-6190 (630) _ ❑ Davenport. IA (1) ❑ Indianapolis, IN (L) (615)726-0177 Macon, GA (N) (248)332-1940 ❑ :Orlando, FL (P) ❑ ; WateRown WI (R) � -1 \tlani;, GA ((;) ❑ Brighton, CO (D)❑ Charleston, SC (P) ❑ Columbia, SC (H) c c c 319 323-7944 (317)842-4261 849-6550 (803)7)6-8)8) ( )- (912)757-0811 (407)851-2560 (920)261-1660 (770)308-0030 (303)659-0497 (843 REQUESTED PARAMETERS f lip ut. t� l r„n Project No.: I<. i `'t+l1el,,l' JlK Invoice Address: Is this work being conducted for Inli — — regulatory;`%,f 4' .` compliance monitoring? YesNo Attn: Is this work lieing conducted for,�i' inn: �1 Sampled [3yD. Lu ie. D Cb ^/ �!D oV regulatory enforcement action? r Yes. No_ — Phone No.: Fix No.: P.O. No: Which regulations apply: Quote No. �1 lv RCRA ,NPDESWastewater UST_ '• Drinking Water ' I'UItN:UtOU\p'r111F. State Samples Collected Other 1 Rush (surcharges may apply) Date Needed: -- 1/ and t e of containers r Time Comp (C) Matrix Lab Use ; m O O Col. d d o : REMARKS Sample ID Date Grab (G) ,LS- .13 912 152 ✓ ;Z� � ; r -t �1 t�il�I — Sv�O �3UZ ��<� �a►�� IVY io�h ✓ tYy�::t st.:. Z r ( J4.7 V VV l \ 2 I b t q.'+ i)C Deliverables: ❑ None ❑ Level Batch QC Level 3 (-1 Level4 ❑ Other to a� ao 1i l'O11I\ Morris 1:NTS: office X FAX# 919 - f/�/� -- - USE » Date LAD S 0 ie Received By: Reltuyulshed 13 Dale 10krinic Received By Date Time p_.•ica" k<4R if �' 1�'tllli�llf �t led );}'. �'•{V -_ __ � .—.__ ._ {� ,• Date Time . ; < Yes k %A 1. iu1.,ul.h .1 li Date -- _ -rime Received By: - -- -- Q`p5fodp e8 , Daa• I '1 imc Receive) B 1 ale I �� Time 1lgtUes Supplttid byaxA.. ' �' f:, oxr�: Testmerca Ai �"����' 8B 054.408 f j 2960 Poster Creighton Drive •Nashville, TN 37204 M 18001 765-0980 • 16151 726-0177 • Fax 16151 72' -- --A Company 11�� CI 2338 ANALYSIS ❑ REQUEST °.� �..}¢ Address ----- - ° ° ° N o F ! o �� o 0D ° ,�� 's{gyp❑ ,j;;-; o❑ � , Y. a _ ;' 1" 3, 1 �t' _ City — - St Zip I. F�� — dT �' Sampler Sign/Printer o ❑❑ a) N o 0 o a ,� �.a V Project Name — /Proj. # o o ❑ m mL 2 ❑ a O° ° O ❑ ° ❑ Q E n LL rn ❑ .� Facility Location ( ity, St) EtT (0�$ r N ❑ ° o m av Project Mana er ° _o N io rN QoQo "❑{ ' ❑0- i PO Number Q37 /Fac./Site I.D. a (D ❑x LO ❑❑ ❑ o10 X ° � °cli o °O op Phone Number Fax Number E °' m t C\j O° °Cf)-1 Q U ° aw N N O O N c o 0 4 y Method r B.C. # Matrix Sampling o d y❑ o oPreserved mO�w I�. (Lab u,aOnly) z 020 c aiJ ° a1y*� w SAI w w 0 0'13CL 7 x o H uField u Q Lij = ab# O oO W 7= w z o o N . J oSample s� Cr o z (Lab Use Only) I D o w a a w > w a a sU) x CC LLf -+ ;� }y t31-5� 3 2 !x, NO i 1331 , f L S V��rJ-ZD— �= , .1 c � , f_ SG ry �� i�Di'I t 1 IVV I /(�Q 1- sit V 033 _ 1 {` TAT SPECIAL DETECTION LIMITS REMARKS 5 , � t ., Ot' � p ; r Slarlllard 17 3-Day 2-Day U SPECIAL REPORTING REQUIREMENTS SAI PROJECT or QUOTE NUMBER Temperature Received ! Nuxt Day ij (to insure correct Analysis and Billing) Alrblll Number fir' OUlur. in %ish r t e RWciedby: DateZ�?a CUSTODY RECORD /� R! nquisl d by: at Tirne c�� Received by: Date Time P , I of.;l4r 1 l Rulinquished by: Date Time Rec L ora Dat I T1melr' i TestAmerica dV0 8B-0�5 4 4 0 9 ; le 2960 Foster Creighton Drive • Nashville, T . 3 J 8 Tor 18001 765-0980 • [6151 726-0177 • Fax [6151 7 ANALYSIS REQUES' Company A Client Number ❑ Address CQ City St Zip ❑ ❑ CO ❑ Sampler Sinn/Print 1 r. �1� DC1-L— 00 ❑ o o Project Name ('IA /Prof. # o o ❑ mL =o ❑ t ° °° °° ° ❑ a Facility Location ( ity, St) o Q r t ° ❑ ❑ o L ❑ N ❑ Project Manager E►TN XEN� o o° �o o O,�-. �o o O O 10 o ❑~ M ❑ N PO Number _ /Fac./Site I.D. a (00 oo OT- OO 00 0 o o � ❑ o c Phone Number `� �—. Fax Number ra oN o .0 ❑ a 0 o ❑ Q N ❑ 00 11 ❑❑ a 2 NU) oa X ~ ❑ 'T o al o N ❑ m o B.C. # �`� Matrix Method Sampling ���v �;' w Preserved M w no oo co y m ❑ - „ w ❑ o o J a a O H m a m (Lab use Only) z f- U ° �a 03 OS v 0 v v a N m Field SAI o wiz o x O o Q a w a w a w 0 o W �� C7= �a ow = m �' m Com rn „ El 0 x y H Sample Lab# r- a _' o o ? z rn @ wa Q t= ,, a z o t- - i7 o w 0 0 J 0 n o > W O D (Lab Use Only) u rn Q rn 'L 0 2 2 2 Z_ of F- m SS 1 AD q3 2g i W~NVPP jai `�`� V3 TAT SPECIAL DETECTION LIMITS REMARKS Standard 3-Day Ll 2-Day ,i SPECIAL REPORTING REQUIREMENTS SAI PROJECT or QUOTE NUMBER Next Day U (to insure correct Analysis and Billing) Other. � — ) Ve quish d .y.Sa , a� l Re CUSTODY G Date Ti e Received by: RECORD Rel qu's e y: �Q�� A, n �4� I Relinquished by: [� ate C/ Time Receive La L 1brtvy 0 0D J ❑ O G *.• ❑ ao � A= ❑ � d u- .0 ❑ '�i ;. 0. OO c a ~ ¢a ❑ O O to O a C m m 0 C v v f) U a a I Ln .� . 2 ❑ �, yy :t �. Cq d ❑Q L In 4 - N m LL .f ar Z. 'd to iO ILL O ' Ix jam, +>,��v . `.,. • {� 1 �`'� i :•f t o vq� tG y 4 y� 4t rlr 1' rQ'F ' J -fy 1 ,*{! t •.Ms 1. L f�.H R, Temperature Received AlrbIII Number 'D to Tkne 1 �Zl. Date Time . 3 Date : Time S�p,r i Teserca Incorporated PURCHASE ORDER FOR INTERLAB ANALYSIS Purchase Order # (�C� ` �� `� Account # 3 Sending Division r 5 U L t Receiving Division S Initiated By Accepted By Client Project # (s) T /0.) S3s Sending Date Report Due Date _� . 5-- c)Holding Time See COC . QC Deliverables See COC . Certifications Required Special Reporting Limits) Additional Comments and Specific Requests (Example: Analytes, Client Specific QC) Attach copy or original TestAmerica Incorporated COC(s). Use shaded lab use areas to designate lab being sent to and total number of containers sent Ensure that methods are designated. Reference PO# of this form on original COC(s). Sign enclosed COC to relinquish and receive samples. Return original signature copy with final report If samples are logged in at "original lab" prior to subbing, a copy of log -in suminary may be attached. Price per Sample Based on: Price Charged to Client List Price Method Matrix. # of Samples Price per Sample Inter -Lab Discount Inter -Lab Revenue o f UJ & Ao a a 12.,5 d -T.�..r -.--_:­�..,_. I____ --r.-, - r_s--�'- .-1.1 --_--,..--_ -- T _ Inter -Lab Revenue e_. - Rush Char %� CC Charge �.._�rTOTAL INTER -LAB REVENUE TESTAMERICA INC.-NASHVILLE Clien COOLER RECEIPT FORM -ZT BC# a duo ly Cooler Received On: R 1 ao And Opened On: `' ►4 By: Paul Buckingham (Signature) 1. Temperature of Cooler when opened '3•D Degrees Celsius 2. Were custody seals on outside of cooler?.......................................................YES a. If yes, how many, what kind and where:y` — b. Were the seals intact, signed, and dated correctly?.............................YES 'O 3. Were custody seals on containers and intact?...........................................400 YES 4. Were custody papers inside cooler?.............................................................0 NO 5. Were custody papers properly filled out (ink,signed,etc)?...............................� nTO T 6. Did you sign the custody papers in the appropriate place? ............................. . ]\O 7. What kind of packing material used? ubblewrap Peanuts Vermiculite Other None 8. Was sufficient ice used (if appropriate)?....................................................� NO 9. Did all bottles arrive in good condition( unbroken)? .................................... C� NO 10. Were all bottle labels complete (#,date,signed,pres,etc)? ............................... YES NO 11. Did all bottle labels and tags agree with custody papers? ..............................(�) NO 12. Were correct bottles used for the analysis requested? ................................. 4iS NO 13. a. Were VOA vials received?...............................................................YES NO b _Was there any observable head space p11 resent in any VOA vials ....:.......� YES 14.. Was sufficient amount of sample sent in each bottle? ................................ (v NO 15 YE NO Were correct preservatives used? .. r s=� 16 Was residual chlorine present' v s s r :� ti fi•1 + 7 .rrr C. it a tvQ +a -_..4 s "iH- ._> SY �. � a-.. ¢ ;"` -. T' b k.7" -� -•�- ���__ tncar.�i�'� _;-rr _-5:.,= '�eof it--s�.'rs`�i^,��Y'�-�e` � its-z-, r3�"-�"L�' -Fr ri -._ ,. ---`' _ .: "r`-'.-_ y`�-'+.+. +�--a.� �i:�T'r. _ , .-- _r�'• ,et atcacnea for re5utuuvu r - a, s ;MICROSEEPS.:::::: •••••••••••••••••••••••••••••••••••••••••• • University of Pittsburgh Applied Research Center 220 William Pitt Way, Pittsburgh, PA 15238 (412) 826-5245 FAX (412) 826-3433 October 2, 2000 Keith Ogden IT Corporation 2200 Gateway Centre Boulevard Suite 205 Morrisville, NC 27560 Dear Keith: Attached is the final data listing for the sample(s) we received on September 13, 2000, your project #107535-30202000. Please give me a call if you have questions or I can be of further assistance. Thank you for using Microseeps. I Sincerely, Linda S. Tibensky LST/lsp Attachment: IT202-203 614 L ` Geochemical and Environmental Surveying for Government and Industry MICROSEEPS IT202-203614 ----- IT CORPORATION ---- ----- PROJECT LOC: SLS GREENSBORO, NC ----- AM 4.02 ----- PROJECT NUM: 107535-30202000 ----- ----- 601/602 SCAN ----- ----- CONCENTRATIONS IN ug/L (mg/m3) ----- ---------------------------------------------------------------------------------------------------------------- SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID COMPOUND NAME ---------------------------------------------------------------------------------------------------------------- SMVP12 SVMP11 SVMP10 SVMP9 SVMP8 LDLs CHLOROMETHANE < 2 < 2 < 2 < 2 < 2 2 VINYL CHLORIDE 18 < 6 < 6 < 6 < 6 6 BROMOMETHANE/CHLOROETHANE* < 3 < 3 < 3 < 3 < 3 3 FLUOROTRICHLOROMETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 1,1 DICHLOROETHYLENE 0.44 4.25 6.91 2.15 0.87 0.04 METHYLENE CHLORIDE < 6 7 647 97 31 6 TRANS-1,2 DICHLOROETHYLENE 2.8 5.6 11.9 < 0.4 < 0.4 0.4 1,1 DICHLOROETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CIS-1,2 DICHLOROETHYLENE 85.7 254.1 671.4 263.6 13.3 0.4 CHLOROFORM 0.32 0.56 0.53 0.78 0.95 0.02 1,1,1 TRICHLOROETHANE 0.07 2.07 < 0.03 < 0.03 0.06 0.03 CARBON TETRACHLORIDE 0.08 0.90 0.03 < 0.03 0.26 0.03 1,2 DICHLOROETHANE < 0.04 < 0.04 < 0.04 0.37 < 0.04 0.04 TRICHLOROETHYLENE 111.42 84.92 168.55 49.21 7.12 0.03 1,2 DICHLOROPROPANE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 BROMODICHLOROMETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 CIS-1,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 TRANS-1,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 1,1,2 TRICHLOROETHANE < 0.03 0.10 0.03 0.04 0.07 0.03 TETRACHLOROETHYLENE 8326 15020 . 6291 4327 13247 0.03 CHLORODIBROMOMETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CHLOROSENZENE < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 0.3 BROMOFORM < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 1,1,2,2 TETRACHLOROETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 1,3 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,4 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,2 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 BENZENE < 0.3 4.6 90.1 102.1 < 0.3 0.3 TOLUENE 0.4 4.2 285.2 98.7 6.5 0.3 ETHYLBENZENE < 0.3 1.0 52.3 18.1 5.5 0.3 ---------------------------------------------------------------------------------------------------------------- FILE NAME W99 396 W99 397 W99 398/443 W99 399/442 W99 411 DATE SAMPLED 09/09/00 09/09/00 09/09/00 09/09/00 09/09/00 DATE RECEIVED 09/13/00 09/13/00 09/13/00 09/13/00 09/13/00 DATE ANALYZED 09/21/00 09/21/00 09/21/00 09/21/00 09/25/00 ANALYST ---------------------------------------------------------------------------------------------------------------- NAM MAM MAM MAM MAM * COMPOUNDS ELUTE TOGETHER ON ECD: VALUES REPRESENT EITHER OR A COMBINATION OF BOTH. 10-Oct-2000 ANALYST INITIALLS� REVIEW MICROSEEPS IT202-203614 ----- IT CORPORATION ---- ----- PROJECT LOC: SLS GREENSBORO, NC ----- AM 4.02 ----- PROJECT NUM: 107535-30202000 ----- ----- 601/602 SCAN ----- ----- CONCENTRATIONS IN ug/L (mg/m3) ----- SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID ----------------------------------------------------------------------------------=----------------------------- COMPOUND NAME SVMP7 SVMP6 SVMP5 SVMP4 SVMP3 LDLs ---------------------------------------------------------------------------------------------------------------- CHLOROMETHANE < 2 < 2 < 2 < 2 < 2 2 VINYL CHLORIDE < 6 < 6 < 6 < 6 < 6 6 BROMOMETHANE/CHLOROETHANE* < 3 < 3 < 3 < 3 < 3 3 FLUOROTRICHLOROMETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 1,1 DICHLOROETHYLENE 0.79 0.64 0.60 0.08 0.36 0.04 METHYLENE CHLORIDE < 6 < 6 < 6 < 6 < 6 6 TRANS-1,2 DICHLOROETHYLENE 0.8 1.2 < 0.4 < 0.4 < 0.4 0.4, 1,1 DICHLOROETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CIS-1,2 DICHLOROETHYLENE 20.7 < 0.4 < 0.4 < 0.4 < 0.4 0.4 CHLOROFORM 1.95 1.97 2.18 0.51 1.16 0.02 1,1,1 TRICHLOROETHANE 0.19 0.05 0.05 < 0.03 0.03 0.03 CARBON TETRACHLORIDE 0.61 0.47 0.23 0.04 0.13 0.03 1,2 DICHLOROETHANE < 0.04 < 0.04 < 0.04 0.28 < 0.04 0.04 TRICHLOROETHYLENE 24.40 10.82 9.31 6.13 4.71 0.03 1,2 DICHLOROPROPANE < 0.05. < 0.05 < 0.05 < 0.05 < 0.05 0.05 BROMODICHLOROMETHANE < 0.03 < 0.03 0.03 < 6.03 < 0.03 0.03 CIS-1,3 DICHLOROPROPYLENE < 0.05 0.05 < 0.05 < 0.05 < 0.05 0.05 . TRANS-1,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 1,1,2 TRICHLOROETHANE 0.31 0.06 : 0.69 0.04 0.26 0.03 TETRACHLOROETHYLENE 21390 14080 12915 2815 3168 0.03 CHLORODIBROMOMETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CHLOROBENZENE < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 0.3 BROMOFORM < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 1,1,2,2 TETRACHLOROETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 1,3 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,4 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1.2 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 BENZENE 0.6 0.8 2.5 3.0 8.4 0.3 TOLUENE 1.9 1.1 1.7 2.3 0.4 0.3 ETHYLBENZENE 1.0 0.3 2.0 0.6 0.4 0.3 ---------------------------------------------------------------------------------------------------------------- FILE NAME W99 401 W99 402 W99 403 W99 4047 W99 412 DATE SAMPLED 09/09/00 09/09/00 09/09/00 09/09/00 09/09/00 DATE RECEIVED 09/13/00 09/13/00 09113/00_ 09/13/00 09/13/00 DATE ANALYZED 09/21/00 09/21/00 09/21/00 09/21/00 09/25/00 ANALYST MAM MAM MAM MAM MAM * COMPOUNDS ELUTE TOGETHER ON ECD: VALUES REPRESENT EITHER OR A COMBINATION OF BOTH. 10-Oct-2000 ANALYST INITIAL$' REVIEW MICROSEEPS IT202-203614 ----- IT CORPORATION ---- ----- PROJECT LOC: SLS GREENSBORO, NC ----- AM 4.02 --=-- PROJECT NUM: 107535-30202000 ----- ----- 601/602 SCAN ----- ----- CONCENTRATIONS IN ug/I (mg/m3) ----- ---------------------------------------------------------------------------------------------------------------- SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID COMPOUND NAME ---------------------------------------------------------------------------------------------------------------- SVMP2 SVMP1 PT5S SVE8 PT1S LDLs CHLOROMETHANE < 2 < 2 < 2 < 2 < 2 2 VINYL CHLORIDE < 6 < 6 < 6 < 6 < 6 6 - BROMOMETHANE/CHLOROETHANE* < 3 < 3 < 3 < 3 < 3 3 FLUOROTRICHLOROMETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 -- 1,1 DICHLOROETHYLENE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 METHYLENE CHLORIDE < 6 < 6 < 6 < 6 < 6 6 ,- TRANS-1,2 DICHLOROETHYLENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,1 DICHLOROETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CIS-1,2 DICHLOROETHYLENE 3.1 4.1 < 0.4 1.0 <•O.4 0.4 CHLOROFORM 0.49 0.61 < 0.02 0.12 < 0.02 0.02 1,1,1 TRICHLOROETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 CARBON TETRACHLORIDE 0.08 0.13 < 0.03 < 0.03 < 0.03 0.03 1,2 DICHLOROETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 TRICHLOROETHYLENE 1.51 2.28 < 0.03' 1.44 < 0.03 0.03 1,2 DICHLOROPROPANE i < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 BROMODICHLOROMETHANE < 0.03 < 0.03 < 0.03 < 0.03. < 0.03 0.03 CIS-1,3 DICHLOROPROPYLENE < 0.05 2 0.05 < 0.05 < 0.05 < 0.05 0.05 TRANS-1,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 . 1,1,2 TRICHLOROETHANE < 0.03 < 0.03 < 0.03 0.03 < 0.03 0.03 TETRACHLOROETHYLENE 3876 5707 11.26 375.14 3.03 0.03 CHLORODIBROMOMETHANE < 0.04 < 0.04 < 0.04 < 0.04 < 0.04 0.04 CHLOROBENZENE < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 0.3 BROMOFORM < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.05 - 1,1,2,2 TETRACHLOROETHANE < 0.03 < 0.03 < 0.03 < 0.03 < 0.03 0.03 1,3 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,4 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 1,2 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.4 BENZENE 0.3 0.5 < 0.3 < 0.3 < 0.3 0.3 -, TOLUENE 0.3 0.5 0.4 < 0.3 < 0.3 0.3 ETHYLBENZENE ---------------------------------------------------------------------------------------------------------------- < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 0.3 FILE NAME W99 413 W99 414 W99 415 W99 416 W99 417 DATE SAMPLED 09/09/00 09/09/00 09/11/00 09/11/00 09/11/00 ' DATE RECEIVED 09/13/00 09/13/00 09/13/00 09/13/00 09/13/00 DATE ANALYZED 09/25/00 09/25/00. 09/25/00 09/25/00 09/25/00 ANALYST ---------------------------------------------------------------------------------------------------------------- MAM MAM MAM MAM MAM * COMPOUNDS ELUTE TOGETHER ON ECD: VALUES REPRESENT EITHER OR A COMBINATION OF BOTH. 10-Oct-2000 ANALYST INITIAL5g::�W-_ REVIEW MICROSEEPS IT202-203614 ----- IT CORPORATION ---- ----- PROJECT LOC: SLS GREENSBORO, NC ----- AM 4.02 ----- PROJECT NUM: 107535-30202000 ----- ----- 601/602 SCAN ----- CONCENTRATIONS IN.ug/L (mg/m3) ----- SAMPLE ID SAMPLE ID SAMPLE ID -------------------------------------------------------------------------------------- COMPOUND NAME -------------------------------------------------------------------------------------- SVE9 PT3S PT4S LDLs CHLOROMETHANE < 2 < 2 < 2 2 VINYL CHLORIDE < 6 < 6 < 6 6 BROMOMETHANE/CHLOROETHANE* < 3 < 3 < 3 3 FLUOROTRICHLOROMETHANE < 0.03 < 0.03 < 0.03 0.03 1,1 DICHLOROETHYLENE < 0.04 < 0.04 < 0.04 0.04 METHYLENE CHLORIDE < 6 < 6 < 6 6 TRANS-1,2 DICHLOROETHYLENE < 0.4 < 0.4 < 0.4 0.4 1,1 DICHLOROETHANE <'0.04 < 0.04 < 0.04 0.04. CIS-1,2 DICHLOROETHYLENE < 0.4 < 0.4 < 0.4 0.4 CHLOROFORM < 0.02 0.11 < 0.02 0.02 1,1,1 TRICHLOROETHANE < 0.03 < 0.03 < 0.03 0.03 CARBON TETRACHLORIDE < 0.03 < 0.03 < 0.03 0.03 1,2 DICHLOROETHANE < 0.04 < 0.04 < 0.04 0.04 TRICHLOROETHYLENE 0.32 3.46 0.23 0.03 1,2 DICHLOROPROPANE < 0.05 < 0.05 < 0.05 0.05 BROMODICHLOROMETHANE < 0.03 < 0.03 < 0.03 0.03 CIS-1,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 0.05 TRANS4,3 DICHLOROPROPYLENE < 0.05 < 0.05 < 0.05 0.05 1,1,2.TRICHLOROETHANE < 0.03 < 0.03 < 0.03 0.03 TETRACHLOROETHYLENE 8.52 9.38 4.58 .0.03 CHLORODIBROMOMETHANE < 0.04 < 0.04 < 0.04 0.04 CHLOROBENZENE < 0.3 < 0.3 < 0.3 0.3 BROMOFORM' < 0.05 < 0.05 < 0.05 0.05 1,1,2,2 TETRACHLOROETHANE < 0.03 < 0.03 < 0.03 0.03 1,3 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 0.4 1,4 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 ' 0.4 1,2 DICHLOROBENZENE < 0.4 < 0.4 < 0.4 0.4 BENZENE < 0.3 < 0.3 < 0.3 0.3 TOLUENE < 0.3 < 0.3 0.5 0.3 ETHYLBENZENE < 0.3 < 0.3 < 0.3 0.3 . -------------------------------------------------------------------------------------- FILE NAME. W99 418 W99 419 W99 420 DATE SAMPLED 09/11/00 09/11/00 09/11/00 DATE RECEIVED 09/13/00 09/13/00 09/13/00 DATE ANALYZED 09/25/00 09/25/00 09/25/00 ANALYST NAM MAN! MAM * COMPOUNDS ELUTE TOGETHER ON ECD: VALUES REPRESENT EITHER OR A COMBINATION OF BOTH. I 10-Oct-2000 ANALYST INITIA:S!�� REVIEW Microseeps IT202-203614 -- IT Corporation -- Project: 107535-30202000 --- Location: SLS-Greensboro, NC --- - Concentrations in PPMV --- -- 601/602 Analysis --- Sample ID Compound Name SVMP6 SVMP5 SVMP4 SVMP3 SVMP2 SVMP1 e[ec[[on Chloromethane < 1 < 1 < 1 < 1 < 1 < 1 1 Vinyl Chloride < 3 < 3 < 3 < 3 < 3 < 3 3 Bromomethane/ Chloroethane" . < 1 < I < 1 < 1 < 1 < I 1 Fluorotrichloromethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1 Dichloroethylene 0.16 0.15 0.02 0.09 < 0.01 < 0.01 0.01 Methylene Chloride < 2 < 2 < 2 < 2 < 2 < 2 2 trans-1,2 Dichloroethylene 0.3 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 0.1 1,1 Dichloroethane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Chloroform 0.402 0.445 0.105 0.237 0.101 0.125 0.005 1,1,1 Trichloroethane 0.009 0.009 <0.005 0.005 <0.005 <0.005 0.005 Carbon Tetrachloride 0.075 0.036 0.007 0.021 0.012 0.020 0.005 Benzene 0.26 0.79 0.94 2.62 0.10 0.17 0.07 1,2Dichloroethane <0.01 <0.01 0.07 <0.01 <0.01 <0.01 0.01 Trichloroethylene 2.009 1.728 1.138 0.874 0.280 0.424 0.005 1,2 Dichloropropane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Bromodichloromethane . < 0.005 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 cis-1,3 Dichloropropylene 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Toluene 0.30 0.45 0.62 0.10 0.09 0.13 0.07 trans-1,3 Dichloropropylene < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 1,1,2 Trichloroethane 0.011 0.126 0.007 / 0.048 < 0.005 < 0.005 0.005 Tetrachloroethylene 2080 1908 415.9 468.0 572.6 843.1 0.005 Chlorodibromomethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Chlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 Ethyl Benzene 0.07 0.46 0.13 0.09 < 0.07 < 0.07 0.07 Bromoform < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1,2,2 Tetrachloroethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,3 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,4 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,2 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 File ID W99 402 W99 403 W99 404 W99 412 W99 413 W99 414 Date Sampled 9/9/00 9/9/00 9/9/00 9/9/00 9/9/00 9/9/00 Date Received 9/13/00 9113/00 9/13/00 9/13/00 9/13/00 9/13/00 Date Analyzed 9/21/00 9/21/00 9/21/00 9/25/00 9/25/00 9/25/00 Analyst MAM MAM MAM MAM MAM MAM Compounds elute together on ECD: values represent either or 9/28/00 Analys�� Reviewed Microseeps I7202-203614 ----- IT Corporation --- --- Project: 107535-30202000 --- ---- Location: SLS-Greensboro, NC ----- Concentrations in PPMV ---- --- 601/602 Analysis ---- Sample ID Compound Name SVMP12 SVMP11 SVMPIO SVMP9 SVMP8 SVMP7 T:-:,Detection Chloromethane < 1 < 1 < 1 < 1 < I < I I Vinyl Chloride 7 < 3< 3 < 3 < 3 < 3 3 Bromomethane/ Chloroethane* < 1 < 1 < 1 < 1 < 1 < 1 I Fluorotrichloromethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1 Dichloroethylene 0.11 1.07 1.74 0.54 0.22 0.20 0.01 Methylene Chloride < 2 2 186 28 9 < 2 2 trans-1,2 Dichloroethylene 0.7 1.4 3.0 < 0.1 < 0.1 0.2 0.1 1,1 Dichloroethane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Chloroform 0.066 0.115 0.108 0.160 0.194 0.398 0.005 1,1,1 Trichloroethane 0.012 0.379 <0.005 <0.005 0.011 0.034 0.005 Carbon Tetrachloride. 0.013 0.143 0.005 < 0.005 0.042 0.697 0.005 Benzene < 0.07 1.43 28.13 31.89 < 0.07 0.19 0.07 1,2 Dichloroethane < 0.01 < 0.01 < 0.01 0.09 < 0.01 < 0.01 0.01 Trichloroethylene 20.69 15.77 31.30 9.139 1.322 4.531 0.005 1,2 Dichloropropane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Bromodichloromethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 cis-1,3 Dichloropropylene <.0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Toluene 0.11 1.12 75.52 26.15 1.72 0.49 0.07 trans-1,3 Dichloropropylene < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 1,1,2 Trichloroethane < 0.005 0.019 0.005 0.008 0.013 0.056 0.005 Tetrachloroethylene 1230 2219 929.4 639.3 1957 3160 0.005 Chlorodibromomethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Chlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 Ethyl Benzene < 0.07 0.24 12.03 4.17 1.26 0.23 0.07 Bromoform < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1,2,2 Tetrachloroethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,3 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,4 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,2 Dichlorobenzene < 0.07 1 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 File M W99 396 W99 397 W99 399/443 W99 399/442 W99 411 W99 401 Date Sampled 9/9/00 9/9/00 9/9/00 9/9/00 9/9/00 9/9/00 Date Received 9/13/00 9/13/00 9/13/00 9/13/00 9/13/00 9/13/00 _ Date Analyzed 9/21/00 9/21/00 9/21100 9/21/00 9/25/00 9/21/00 Analyst MAM MAM MAM MAM MAM MAM * Compounds elute together on ECD: values represent either or Al 9/28/00 Analyst Reviewed % L Microseeps M02-203614 --- IT Corporation - - Project: 107535-30202000 --- - Location: SLS-Greensboro, NC - --- Concentrations in PPMV -- --- 601/602 Analysis -- Sample ID Compound Name PT5S SVE8 PTIS SVE9 PT3S PT4S etecton Chloromethane < 1 < I < I < 1 < 1 < 1 1 Vinyl Chloride < 3 < 3 < 3 < 3 < 3 < 3 3 Bromomethane/ Chloroethane* < I < I < I < 1 < 1 < 1 I Fluorotrichloromethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1 Dichloroethylene <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.01 Methylene Chloride < 2 < 2 < 2 < 2 < 2 < 2 2 trans-1,2 Dichloroethylene < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 0.1 1,1 Dichloroethane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Chloroform < 0.005 0.024 < 0.005 < 0.005 0.023 < 0.005 0.005 1,1,1 Trichloroethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Carbon Tetrachloride < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Benzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,2 Dichloroethane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Trichloroethylene < 0.005 0.267 < 0.005 0.060 0.643 0.043 0.005 1,2 Dichloropropane < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Bromodichloromethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 cis-1,3 Dichloropropylene -0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 Toluene 0.11 < 0.07 < 0.07 < 0.07 < 0.07 0.13 0.07 trans-1,3 Dichloropropylene < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 0.01 1,1,2 Trichloroethane <.0.005 0.006 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Tetrachloroethylene 1.664 55.42 0.448 1.259 1.386 0.676 0.005 Chlorodibromomethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 Chlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 Ethyl Benzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 Bromoform < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,1,2,2 Tetrachloroethane < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 < 0.005 0.005 1,3 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,4 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 1,2 Dichlorobenzene < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 < 0.07 0.07 File ID - W99 415 W99 416 W99 417 W99 418 W99 419 W99 420 Date Sampled 9/11/00 9/11/00 9/11/00 9/11/00 9/11/00 9/11/00 Date Received 9/13/00 9/13/00 9/13/00 9/13/00 9/13/00 9/13/00 Date Analyzed 9/25/00 9/25/00 925/00 9/25/00 9/25/00 9/25/00 Analyst MAM MAM MAM MAM MAM MAM * Compounds elute together on ECD: values represent either or 9/28/00 Analys Reviewed 1� 1 Microseeps M02-203614 ***** Quality Control ***** -- IT Corporation ----- Project: 107535-30202000 -- --- Location: SLS-Greensboro, NC - --- Concentrations in PPMV - Continuing Calibration Standards 09/21/00 . IN2 in vial 09/21/00 Comnound Lab ID True Conc. Measured 51. Diff. Lab ID Report. Limit Measured Chloromethane W99 393 2.08 2.10 0.82 W99 395 1 ND Vinyl Chloride W99 385 1000 1000 0.00 W99 395 3 ND Bromomethanel Chloroethane* W99 393 2.74 2.67 2.48 W99 395 1 ND Fluorotrichloromethane W99 393 0.765 0.758 0.92 W99 395 0.005 ND 1,1 Dichloroethylene W99 393 1.09 1.07 1.38 W99 395 0.01 ND Methylene Chloride W99 393 1.24 1.06 14.38 W99 395 2 ND trans-1,2 Dichloroethylene W99 393 1.09 ( 1.06 2.30 W99 395 0.1 ND 1,1 Dichloroethane W99 393 1.06 1.05 1.13 W99 395 0.01 ND Chloroform W99 393 0.881 0.874 0.79 W99 395 0.005 ND 1,1,1 Trichloroethane W99 393 0.788 0.813 3.17 W99 395 0.005 ND Carbon Tetrachloride W99 393 0.684 0.695 1.61 W99 395 0.005 ND Benzene W99 394 1.25 1.24 0.80 W99 395 0.07 ND 1,2 Dichloroethane W99 393 1.06 1.00 5.84 W99 395 0.01 ND Trichloroethylene W99 393 0.800 0.775 3.13 W99 395 0.005 ND 1,2 Dichloropropane W99 393 0.93 0.92 0.97 W99 395 0.01 ND Bromodichloromethane W99 393 0.642 0.645 0.47 W99 395 0.005 ND cis-1,3 Dichloropropylene W99 393 0.95 0.99 4.54 W99 395 0.01 ND Toluene W99 393 1.14 1.14 0.00 W99 395 0.07 ND trans-1,3 Dichloropropylene W99 393 0.95 0.99 4.54 W99 395 0.01 ND 1,1,2 Trichloroethane W99 393 0.788 0.777 1.40 W99 395 0.005 ND Tetrachloroethylene W99 393 0.634 0.621 2.05 W99 395 0.005 ND Chlorodibromomethane W99 393 0.505 0.513 1.58 W99 395 0.005 ND Chlorobenzene W99 393 0.93 0.92 1.08 W99 395 0.07 ND Ethyl Benzene W99 393 0.99 0.98 1.01 W99 395 0.07 ND Bromoform W99 393 0.416 0.424 1.92 W99 395 0.005 ND 1,1,2,2 Tetrachloroethane W99 393 0.626 0.634 1.28 W99 395 0.005 ND 1,3 Dichlorobenzene W99 393 0.72 0.68 4.90 W99 395 0.07 ND 1A Dichlorobenzene W99 393 0.72 0.68 4.90 W99 395 0.07 ND 1,2 Dichlorobenzene W99 393 0.72 0.72 0.70 W99 395 0.07 ND Analyst Reviewed //*- Microseeps M02-203614 ***** Quality Control ***** --- IT Corporation -- Project: 107535-30202000 -- -- Location: SLS-Greensboro, NC -- ----- Concentrations in PPMV -- Continuing Calibration Standards 09/25/00 IN2 in via109/25/00 Cmm�nnnd Lab ID True Conc. Measured % Diff iah II) Rennrt_ Limit Meac-M Chloromethane W99 409 2.08 2.45 17.62 W99 410 1 ND Vinyl Chloride W99 406 1000 1055 5.50 W99 410 3 ND Bromomethane/ Chloroethane* W99 409 2.74 2.81 2.63 W99 410 1 ND Fluorotrichloromethane W99 409 0.765 0.786 2.75 W99 410 0.005 ND 1,1 Dichloroethylene W99 409 1.09 1.08 0.46 W99 410 0.01 ND Methylene Chloride W99 409 1.24 1.10 11.15 W99 410 2 ND trans-1,2 Dichloroethylene W99 409 1.09 1.05 3.23 W99 410 0.1 ND 1,1 Dichloroethane W99 409 1.06 1.05 1.13 W99 410 0.01 ND Chloroform W99 409 0.881 0.875 0.68 W99 410 0.005 ND 1,1,1 Trichloroethane W99 409 0.788 0.690 12.44 W99 410 0.005 ND Carbon Tetrachloride W99 409 0.684 0.681 0.44 W99 410 0.005 ND Benzene W99 408 1.25 1.29 3.20 W99 410 0.07 ND 1,2 Dichloroethane W99 409 1.06 1.08 1.69 W99 410 0.01 ND Trichloroethylene W99 409 0.800 0.772 3.50 W99 410 0.005 ND 1,2 Dichloropropane W99 409 0.93 0.87 6.55 W99 410 0.01 ND Bromodichloromethane W99 409 0.642 0.633 1.40 W99 410 0.005 ND cis-1,3 Dichloropropylene W99 409 0.95 0.79 16.58 W99 410 0.01 ND Toluene W99 409 1.14 1.18 3.51 W99 410 0.07 ND trans-1,3 Dichloropropylene W99 409 0.95 0.77 18.69 W99 410 0.01 ND 1,1,2 Trichloroethane W99 409 0.788 0.766 2.79 W99 410 0.005 ND Tetrachloroethylene W99 409 0.634 0.636 0.32 W99 410 0.005 ND Chlorodibromomethane W99 409 0.505 0.494 2.18 W99 410 0.005 ND Chlorobenzene W99 409 0.93 0.94 1.08 W99 410 0.07 ND Ethyl Benzene W99 409 0.99 0.98 1.01 W99 410 0.07 ND Bromoform W99 409 0.416 0.397 4.57 W99 410 0.005 ND 1,1,2,2 Tetrachloroethane W99 409 0.626 0.624 0.32 W99 410 0.005 ND 1,3 Dichlorobenzene W99 409 0.72 0.70 2.10 W99 410 0.07 ND 1A Dichlorobenzene W99 409 0.72 0.66 7.69 W99 410 0.07 ND 1,2 Dichlorobenzene W99 409 0.72 0.69 3.50 W99 410 0.07 ND Analy"t ltd__ Reviewed IA -Ow- MICROSEEPS, inc, 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 Company Name: Address: Proj. Manager: &r'ft?' 6i0cA/ Proj. Location: S] S - U'Lusan 0 Proj. Number: % —,qCEnZ-(M- Phone # : 7 Sampler's, signature: _ Results to CHAIN -OF -CUSTODY RECORD Note: Enter proper letters in Requested Analyses columns below. Analysis Options Note: If analysis D,E,or K is selected, scratch (option) NOT wanted. CI -C4 Chlorinated HC Hydrogen & Helium .............. X: i­' BTEX X.. Perman ent Gases (CH4, CO, CO2, N2, 02 BTEX & C5 - C10 Mere (Soil) or (Air Me ...... jK: TPH (C5 - CIO) or (C4 -C12 TO -14 by GC/MS (Ambient) or( Source—) <':> z' C11 - C18 2 Compounds 601 & 60 Specify below. • An additional 22 nil vial of sample is required when requested in combination with another analysis. Available upon request. Invoice to : Rel'. ui by -t Company. D te Time - Received: Company 5 Date Time RAInjuished ry Y---' Company Date Time Received by Company Date Time: Relinquished by : Company Date Time: Received by Company Date Time : WHITE COPY : Laboratory to return. YELLOW COPY: Laboratory PINK COPY : Submitter Company Address: Proj. Mang Proj. Location: Sj Proj. Number: Phone # : Sampler's signature MICROSEEPS, Inc. 220 William Pitt Way, Pittsburgh, PA 15238 Phone: (412) 826-5245 Fax: (412) 826-3433 WAVIAIV�a��� 14 ---T7-2 C�- CHMN-OF-CUSTODY RECORD Note: Enter proper letters in Requested Analyses columns below. knalysi.s Options Note: If analysis D,E,or K is selected, scratch (option) NOT wanted. C1 -C4 Chlorinated HC Hydrogen & Helium BTEX Permanent Gases (cm, co, CO2, N2, BTEX & C5. CIO nn o2 Mercury X (Soil) or (Air TPH (C5 - CIO) or (C4 -C12 T 0 -14 by GC/MS (Ambient) or (-Source C11 - C18 601 & 602 Compounds Specify below. • An additional 22 ml vial of sample is required when requested in combination with another analysis. Available upon request. Number of 1 "Summa" I I Sjunple Containers if Can. used Identcation MORE �A. , 01190 Results to : r67n 7 -COK-P Invoice to q shed ll�110!1 11=� Company Date - Time 7�-IC` Received Jy: Company: Date: Time: -,�Zju /zOn Re inqutehed by Company : Date Time: Received by Company Date Time: Relinquished by Company: Date: Time : iReceived by Company Date Time: WHITE COPY : Laboratory to return. YELLOW COPY: Laboratory PINK COPY : Submitter Chain of Custody Record 2338 TESTAMEr Me% Pave---L of -- - L7 Asheville, NC (A) ❑ Bartlen, 1L (C) ❑ Cedar Falls, IA MO Charlotte, NC (G) 0 Dayton, OR 00-0961 i u R«:ktoi. fl (Q)Q)(828) 254-5169 (630) 289-3100 (319) 277-2401 (704) 392.-1164 (937) 294-68 (815) 874-2171 O Atlanta. GA (B) 0 Brighton, CO (DO Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. L MOMSVILLS NC � ❑ Watertown, (R) (770) 368-0636 (303) 659-0497 (843) 849-6550 (803) 796-8989 (319) 323-7! __. (920) 261-166 0 Client I'i'CKAY Project No.: 0 53S / Z REQUESTED PARAMETERS ort Addt,�'+C+ress:12W tWR � Invoice Address: � 1s this work bring conducted for compliance rronituring? Yes_ No- �—Vt y Attn: Attn: �' \(� `�-+ is this work bring conducted for regulatory en(orcetnenl action? Phwx No.: Sampled By: -D- n , ��` �' V � Yes_ No_ Which la ionsapply: a RCRA_ NpD6SWstewater_ Fax No.: j P.O. No: TURNAROUND TtMF Quote No.p� of [ 4 Standard SW&Ssrnp1mcollected [t�TB n� l`t (� C(/ IIST_ Drinking WaIIx_ Other_ None_ ❑ Rush (surcharges may apply) Date Needed. Band MW oWWt*rA Sample 1D e (G) Matra Lab Use �$ d °� REMARKS I v�l uw3 jDja j1W-eGr�ali G A� ✓ ✓ l Cs ✓ ✓ ✓ 3 i &S-GW-eNl ov PQ✓ .3: 1 � -GW "l"W 2 bigfin 1349 ,/ 3 l D 153a Ala t5-GW— VW Jq G- AdQ'I =—Q-m �. COMMENTS: � �7 Received By: Dat me Ralinquish+xlBy r Relinquished By: DO 2A I f t Time Received By: DateI Tina Relinquished By: Date I rum Received By: Date I Time K + a' = T z '•l, '` Received By:JA�174't/"� r t7 C u .OHO Date I Ye/7 Y1 selr .. 'runt . RrlirtquishedBy: Data 1 7lme _ C9 Q 0- • Test rl e m ca I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A151602 j KIM PRZYBYL Sample ID: SLS-GW-MW2 2200IGATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 _ Site ID: _ Date Collected: 10/19/00 Project: 107535 Time Collected: 10:45 Project Name: Date Received: 10/21/00 y Sampler: D.LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ I ' Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Chlorobenzene ND. ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 602/601 2666 1,2-Dichlorobenzene ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 602/601 2666 1,4-Dichlorobenzene ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 602/601 2666 Bromodichloromethane ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666. Bromoform ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 . Bromomethane ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Carbon tetrachloride ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 jChloroethane ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Chloroform ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Chloromethane ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 -- Dibromochloromethane ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Ethylene Dibromide ND ug/1 1.0 1.0 .1 10/27/00 12:15 M.Himelick 601 2666 Vinyl chloride ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1,1-Dichloroethane ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 L_ 1,2-Dichloroethane ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1,1-Dichloroethene l ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 cis-1,2-Dichloroethene ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 trans-1,2-Dichloroethene ND ug/l 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1,2-Dichloropropane ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 cis-1,3-Dichloropropene ND ug/1 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 Sample report continued . . . r� S 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 46.2 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 2.0 ug/1 Trichlorofluoromethane ND ug/l *MISCELLANEOUS CHEMISTRY* Chloride ND mg/l ND - Not detected at the report limit. I N C O R P O R A T E D Laboratory Number: 00-A151602 Sample ID: SLS-GW-MW2 Page 2 Report Quan Dil Analysis Analysis Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 5.0 5.0 1. 10/27/00 12:15 M.Himelick- 601 2666 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1.0 1.0 . 1 10/27/00 12:15 M.Himelick 601 2666 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1.0 1.0 1 10/27/00 12:15 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 76. Hall Surr., chloroprene 84. Hall Surr., 1-chloro-3-fluorobenzene 104. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P' 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151602 Sample ID: SLS-GW-MW2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. IZelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv: Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 i Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Lab Number: 00-A151594 Sample ID: SLS-GW-MW3 Sample Type: Water Site ID: Date Collected: 10/18/00 Time Collected: 11:35 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 602 2666 Chlorobenzene ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 602/601 2666 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/1 1000, 1.0 1000 10/27/00 5:57 M.Himelick 602/601 2666 - 1,4-Dichlorobenzene ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 602/601 2666 Ethylbenzene ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 602 2666 Toluene ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 602 2666 m,p-Xylenes ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 602 2666 o-Xylene ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 602 2666 Bromodichloromethane ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Bromoform ND ug/l 1000 2.0 1000 10/27/00 5:57 M.Himelick 601 2666 Bromomethane ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Carbon tetrachloride ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Chloroethane ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Chloroform ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Chloromethane ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Dibromochloromethane ND ` ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Ethylene Dibromide ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Vinyl chloride ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1,1-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1,2-Dichloroethane ND ug/1 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 Sample report continued . . . j 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 cis-1,2-Dichloroethene ND ug/1 trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/1 cis-1,3-Dichloropropene ND ug/1 trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 148000 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND. ug/1 *MISCELLANEOUS CHEMISTRY* Chloride 5.30 mg/1 ND - Not detected at the report limit. Laboratory Number: 00-A151594 Sample ID: SLS-GW-MW3 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch- ------ 1000 ------- 1.0 ------ 1000 -------- 10/27/00 ----- 5:57 ---------- M.Himelick --------- 601 ----- 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 5000 5.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick -601 2666 5000 1.0 5000 10/30/00 12:23 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00- 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1000 1.0 1000 10/27/00 5:57 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 - Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 81. Hall Surr., chloroprene 86. Hall Surr., 1-chloro-3-fluorobenzene 123. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. -- Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAY: 615-726-0954 / 800-765-0980 TestAmerieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151594 Sample ID: SLS-GW-MW3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S.., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A151600-- KIM PRZYBYL Sample ID: SLS-GW-MW4 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 Site ID: Date Collected: 10/19/00 Project: 107535 Time Collected: 12:30 Project Name: Date Received: 10/21/00 Sampler: D.LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor. ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* -- Benzene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602 2666 Chlorobenzene ND ug/1 1000 1.0 1000 10/27/00 10:50 M.Himelick 602/601 2666 '_. 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602/601 2666 - 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602/601 2666. Ethylbenzene ND ug/1 1000 1.0 1000 10/27/00 10:50 M.Himelick 602 2666 Toluene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602 2666 m,p-Xylenes ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602 2666 o-Xylene ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 602 2666 Bromodichloromethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Bromoform ND ug/l 1000 2.0 1000 10/27/00 10:50 M.Himelick 601 2666 Bromomethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Carbon tetrachloride ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Chloroethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Chloroform ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Chloromethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Dibromochloromethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Ethylene Dibromide ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Vinyl chloride ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick -601 2666 1,1-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1,2-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 Sample report continued 1 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / Fm 615-726-0954 / 800-765-0980 Test = merica I N C O R P O R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ----- ug /l cis-1,2-Dichloroethene ND ug/1 trans-1,2-Dichloroethene ND ug/1 1,2-Dichloropropane ND ug/1 ' cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND` ug/1 Tetrachloroethene 54800 ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethee ND ug/1 Trichlorofluoromethane ND ug/l *MISCELLANEOUS CHEMISTRY* Chloride 1.60 mg/1 ND - Not detected at the report limit. Laboratory Number: 00-A151600 Sample ID: SLS-GW-MW4 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 5000 5.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1000 1.0 1000 10/27/00 10:50 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 - Surrogate % Recovery Target Range r ----------------------- ------------ PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 84. Hall Surr., chloroprene 87. j Hall Surr., 1-chloro-3-fluorobenzene 117. # - Recovery outside Laboratory historical limits. '.- Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHvtLLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151600 Sample ID: SLS-GW-MW4 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / F.Ax: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: .Sampler: D.LUBELL Lab Number: 00-A151598 Sample ID: SLS-GW-MW5 Sample Type: Water Site ID: Date Collected: 10/19/00 Time Collected: 14:10 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis - Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ ----------- ------ ------------- ------ -------- --------------- - ------ ----- *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane. Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 602/601 2666 ND' ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 602/601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 602/601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 602/601 2666 - ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666. ND ug/l 100. 2.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/1 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/1 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666_ ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/1 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 ND ug/l 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 P, A T E D ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/l Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethene 5060 ug/1 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/l Trichlorofluoromethane ND ug/l *MISCELLANEOUS CHEMISTRY* Chloride 1.40 mg/1 ND - Not detected at the report limit. Laboratory Number: 00-A151598 Sample ID: SLS-GW-MW5 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 100. ------- 1.0 ------ 100 -------- 10/27/00 ----- 10:08 ---------- M.Himelick --------- 601 ----- 2666 500. 5.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 100. 1.0 100 10/27/00 10:08 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 Surrogate % Recovery PID Surr., a,a,a-trifluorotoluene 99. Hall Surr., 2-chloropropane 81. Hall Surr., chloroprene 78. Hall Surr., 1-chloro-3-fluorobenzene 109. # - Recovery outside Laboratory historical limits. Sample report continued . . . Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151598 Sample ID: SLS-GW-MW5 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT _ IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1�,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A151599 Sample ID: SLS-GW-MW6 Sample Type: Water Site ID: Date Collected: 10/19/00 Time Collected: 13:30 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 602/601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 602/601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 602/601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 602/601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 2.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 470. ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Analyte Result Units trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 255. ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/l *MISCELLANEOUS CHEMISTRY* Chloride 1.60 mg/l ND - Not detected at the report limit. Laboratory Number: 00-A151599 Sample ID: SLS-GW-MW6 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch - ------ 50.0 ------- 1.0 ------ 50 -------- 10/25/00 --:-- . 9.25 ---------- M.Himelick --------- 601 ----- 2666 250. 5.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 50.0 1.0 50 10/25/00 9:25 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 Surrogate ------------- % Recovery ---------- Target ------------ Range PID Surr., a,a,a-trifluorotoluene 100. 50. - 150. Hall Surr., 2-chloropropane 85. 49. - 125. Hall Surr., chloroprene 93. 49. - 142. Hall Surr., 1-chloro-3-fluorobenzene 107. 25. - 157. # - Recovery outside Laboratory historical limits. r Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica ANALYTICAL REPORT Laboratory Number: 00-A151599 Sample ID: SLS-GW-MW6 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. IZelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 i End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Test merica I N C O R P O R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Lab Number: 00-A151601 Sample ID: SLS-GW-DW1 Sample Type: Water Site ID: Date Collected: 10/19/00 Time Collected: 11:35 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor ------------- ------ Date Time -------- ----- Analyst Method Batch ------------------- ----- Chlorobenzene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick, 602/601 2666 1,2-Dichlorobenzene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 602/601 2666 1,4-Dichlorobenzene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 602/601 2666 Bromodichloromethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Bromoform ND ug/1 10.0 2.0 10 10/27/00 11:33 M.Himelick 601 2666 Bromomethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Carbon tetrachloride ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Chloroethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Chloroform ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Chloromethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Dibromochloromethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Ethylene Dibromide ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Vinyl chloride ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 1,1-Dichloroethane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 1,2-Dichloroethane ND ug/l 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 1,1-Dichloroethene ND ug/l 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 cis-1,2-Dichloroethene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 trans-1,2-Dichloroethene ND ug/1 10.0. 1.0 10 10/27/00 11:33 M.Himelick 601 2666 1,2-Dichloropropane ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 cis-1,3-Dichloropropene ND ug/1 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestLmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ trans-1,3-Dichloropropene ----------- ND ------ ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 298. ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/l Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 *MISCELLANEOUS CHEMISTRY* Chloride ND mg/1 ND - Not detected at the report limit. Laboratory Number: 00-A151601 Sample ID: SLS-GW-DW1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 10.0 ------- 1.0 ------ 10 -------- 10/27/00 ----- 11:33 ---------- M.Himelick --------- 601 ----- 2666 50.0 5.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 10.0 1.0 10 10/27/00 11:33 M.Himelick 601 2666 r - 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 Surrogate % Recovery ------------- ---------- PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 89. Hall Surr., chloroprene 81. Hall Surr., 1-chloro-3-fluorobenzene 108. # - Recovery outside Laboratory historical limits. Target Range 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica ANALYTICAL REPORT Laboratory Number: 00-A151601 Sample ID: SLS-GW-DW1 Page 3 These results relate only to the items tested. This report shall not -be reproduced except in full and with permission of the laboratory. Report Approved B r rr y Report Date: 10i31i00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testlimerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Lab Number: 00-A151595 Sample ID: SLS-GW-DW3 Sample Type: Water Site ID: Date Collected: 10/18/00 Time Collected: 12:15 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit ------- Factor ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602 2666 Chlorobenzene ND ug/1 1000 1.0 1000 10/27/00 6:39 M.Himelick 602/601 2666 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602/601 2666 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602/601 2666 Ethylbenzene ND ug/l 1000 1.0 1000 10/27/00 _ 6:39 M.Himelick 602 2666 Toluene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602 2666 m,p-Xylenes ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602 2666 o-Xylene ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 602 2666 Bromodichloromethane ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Bromoform ND ug/l 1000 2.0 1000 10/27/00 6:39 M.Himelick 601 2666 Bromomethane ND ug/1 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Carbon tetrachloride ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Chloroethane ND ug/1 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Chloroform ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Chloromethane ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Dibromochloromethane ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Ethylene Dibromide ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Vinyl chloride ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1,1-Dichloroethane ND ug/1 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1,2-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 i, - Testl�merica I N C O R P O R A T E D ANALYTICAL REPORT _ Analyte Result Units ------------------------ 1,1-Dichloroethene ----------- ND ------ ug/1 cis-1,2-Dichloroethene ND ug/l trans-1,2-Dichloroethene NO ug/1 1,2-Dichloropropane NO ug/1 cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 48800 ug/l 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene ND ug/1 Trichlorofluoromethane ND ug/1 *MISCELLANEOUS CHEMISTRY* Chloride 37.0 mg/1 NO - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A151595 Sample ID: SLS-GW-DW3 Page 2 Report Quan Dil I Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 10/27/00 ----- 6:39 ---------- M.Himelick --------- 601 ----- 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 . 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 5000 5.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 1000 1.0 1000 10/27/00 6:39 M.Himelick 601 2666 5.00 1.00 5 10/25/00 21:54 A Hardison 300 1534 - Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 79. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 107. # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151595 Sample ID: SLS-GW-DW3 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report APProved By Report Date: 10/31/00 - Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv., Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerieca I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Analyte Result Units ------------------------ ----------- ------ *VOLATILE ORGANICS by GC* Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chloroethane 2-Chloroethylvinylether Chloroform Chloromethane Dibromochloromethane Ethylene Dibromide Vinyl chloride Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene Sample report continued . . . Lab Number: 00-A151603 Sample ID: SLS-GW-DW4 Sample Type: Water Site ID: Date Collected: 10/19/00 Time Collected: 14:55 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 602/601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 602/601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 602/601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 602/601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666: ND ug/l 50.0 2.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 r 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I NCORPO RATED ANALYTICAL REPORT Laboratory Number: 00-A151603 Sample ID: SLS-GW-DW4 Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch ------------------------ trans-1,3-Dichloropropene ----------- .ND ------ ug/1 ------ 50.0 ------- 1.0 ------ 50 -------- 10/27/00 ----- 13:15 ---------- M.Himelick --------- 601 ----- 2666 Methylene chloride ND ug/1 250. 5.0 50 10/27/00 13:15 M.Himelick 601 2666 1,1,2,2-Tetrachloroethane ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 Tetrachloroethene ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 1,1,1-Trichloroethane ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 1,1,2-Trichloroethane ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 Trichloroethene ND ug/l 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 Trichlorofluoromethane ND ug/1 50.0 1.0 50 10/27/00 13:15 M.Himelick 601 2666 *MISCELLANEOUS CHEMISTRY* Chloride ND mg/1 50.0 1.00 50 10/25/00 21:54 A Hardison 300 1534 Volatile sample was diluted and the surrogate is outside QC limits due to sample matirx. ND - Not detected at the report limit. Surrogate ------------- Recovery Target Range PID Surr., a,a,a-trifluorotoluene 101. Hall Surr., 2-chloropropane 93. Hall Surr., chloroprene 38. # Hall Surr., 1-chloro-3-fluorobenzene 82. # - Recovery outside Laboratory historical limits. 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Te-,Stj�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151603 Sample ID: SLS-GW-DW4 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 L Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 Lab Number: 00-A151596 �r KIM PRZYBYL Sample ID: SLS-GW-BMW1 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water MORRISVILLE, NC 27560 Site ID: Date Collected: 10/18/00 - Project: 107535 Time Collected: 13:00 Project Name: Date Received: 10/21/00 Sampler: D.LUBELL Time Received: 9:00 Report Quan Dil Analysis Analysis Analyte ------------------------ Result ----------- Units ------ Limit ------ Limit Factor ------- ------ Date -------- Time ----- Analyst ---------- Method --------- Batch ----- *VOLATILE ORGANICS by GC* Benzene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602 2666 Chlorobenzene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602/601 2666 1,2-Dichlorobenzene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick: 602/601 2666 1,3-Dichlorobenzene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602/601 2666 1,4-Dichlorobenzene i ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602/601 2666 Ethylbenzene ND ug/l 20.0 1.0 20 10/27/00 7:21 M.Himelick 602 2666 Toluene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602 2666 m,p-Xylenes ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602 2666 o-Xylene ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 602 2666 Bromodichloromethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Bromoform Nb ug/1 20.0 2.0 20 10/27/00 7:21 M.Himelick 601 2666 Bromomethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Carbon tetrachloride ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Chloroethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Chloroform ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Chloromethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Dibromochloromethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Ethylene Dibromide ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Vinyl chloride ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/1 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 1,1-Dichloroethane ND ug/l 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 1,2-Dichloroethane ND ug/l 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Analyte Result Units ------------------------ 1,1-Dichloroethene • ----------- ND ------ ug/1 cis-1,2-Dichloroethene ND ug/1 trans-1,2-Dichloroethene ND ug/l 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/1 trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/1 1,1,2,2-Tetrachloroethane ND ug/l Tetrachloroethee 380. ug/1 1,1,1-Trichloroethane ND ug/1 1,1,2-Trichloroethane ND ug/1 Trichloroethene 28.0 ug/1 Trichlorofluoromethane ND ug/1 *MISCELLANEOUS CHEMISTRY* Chloride 2.80 mg/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A151596 Sample ID: SLS-GW-BMW1 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 20.0 ------- 1.0 ------ 20 -------- 10/27/00 ----- 7:21 ---------- M.Himelick --------- 601 ----- 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 100. 5.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick -601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 20.0 1.0 20 10/27/00 7:21 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 - Recovery Target Range PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 71. Hall Surr., chloroprene 89. Hall Surr., 1-chloro-3-fluorobenzene 112. # - Recovery outside Laboratory historical limits. Sample report continued . . . 50. - 150. 49. - 125. 49. - 142. 25. - 157. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT Laboratory Number: 00-A151596 Sample ID: SLS-GW-BMW1 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica I N C 0 R P 0 R A T E D ANALYTICAL REPORT IT CORP-SEARS 2338 KIM PRZYBYL 2200 GATEWAY CTR. BLVD. STE205 MORRISVILLE, NC 27560 Project: 107535 Project Name: Sampler: D.LUBELL Analyte Result Units Lab Number: 00-A151597 Sample ID: SLS-GW-BMW2 Sample Type: Water Site ID: Date Collected: 10/18/00 Time Collected: 13:45 Date Received: 10/21/00 Time Received: 9:00 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------------- -------------- ------------------------ ----- *VOLATILE ORGANICS by GC* Benzene - ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick. 602 2666 Chlorobenzene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602/601 2666 1,2-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602/601 2666 1,3-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602/601 2666 1,4-Dichlorobenzene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602/601 2666. Ethylbenzene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602 2666 Toluene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602 2666 m,p-Xylenes ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602 2666 o-Xylene ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 602 2666 Bromodichloromethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Bromoform ND ug/l 1000 2.0 11000 10/27/00 8:02 M.Himelick 601 2666 Bromomethane ND ug/1 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Carbon tetrachloride ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Chloroethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 2-Chloroethylvinylether ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Chloroform ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Chloromethane ND ug/1 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Dibromochloromethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Ethylene Dibromide ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 - Vinyl chloride ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Dichlorodifluoromethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1,1-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 -- 1,2-Dichloroethane ND ug/l 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLEJN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 Testl�merica I N C 0 R F 0 R A T E D ANALYTICAL REPORT Analyte Result Units 1,1-Dichloroethene ND ug/l cis-1,2-Dichloroethene ND ug/1 trans-1,2-Dichloroethene ND ug/l j 1,2-Dichloropropane ND ug/l cis-1,3-Dichloropropene ND ug/l trans-1,3-Dichloropropene ND ug/1 Methylene chloride ND ug/l 1,1,2,2-Tetrachloroethane ND ug/1 Tetrachloroethene 53500 ug/l 1,1,1-Trichloroethane ND ug/l 1,1,2-Trichloroethane ND ug/l Trichloroethee ND ug/1 Trichlorofluoromethane ND ug/l *MISCELLANEOUS CHEMISTRY* Chloride 2.70 mg/1 ND - Not detected at the report limit. Surrogate ------------- Laboratory Number: 00-A151597 Sample ID: SLS-GW-BMW2 Page 2 Report Quan Dil Analysis Analysis Limit Limit Factor Date Time Analyst Method Batch ------ 1000 ------- 1.0 ------ 1000 -------- 10/27/00 ----- 8:02 ---------- M.Himelick --------- 601 ----- 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 .8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 5000 5.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1000 1.0 1000 10/27/00 8:02 M.Himelick 601 2666 1.00 1.00 1 10/25/00 21:54 A Hardison 300 1534 - Recovery PID Surr., a,a,a-trifluorotoluene 100. Hall Surr., 2-chloropropane 82. Hall Surr., chloroprene 88. Hall Surr., 1-chloro-3-fluorobenzene 112. # - Recovery outside Laboratory historical limits. Target Range ------------ 50. - 150. 49. - 125. 49. - 142. 25. - 157. Sample report continued . . . 2960 FosTse CREIGHTON Dews / NAsNvis[ s,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl merica j - I NCO R P O RAT E D ANALYTICAL REPORT Laboratory Number: 00-A151597 Sample ID: SLS-GW-BMW2 Page 3 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 10/31/00 Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. r� 2960 FOSTER CREIGHTON DRIVE / NASHviLLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 __ . Test merica I N C O R P O R A T E D PROJECT QUALITY CONTROL DATA Matrix Spike Recovery Analyte --------------- units ------- Orig. Val. MS Val Spike Conc Recovery Target Range Q.C. Batch Spike Sample Chloride mg/1 ---------- 5.30 --------- 7.60 ---------- 3.00 --------- 77# ------------ 80. - 120. ---------- 1534 ------------ 00-A151594 Benzene mg/l < 0.0010 0.0217 0.0200 108 39. - 150. 2666 blank Benzene mg/l < 0.0010 0.0213 0.0200 106 39. - 150. 2666 blank Chlorobenzene mg/l < 0.0010 0.0204 0.0200 102 55. - 135. 2666 blank Chlorobenzene mg/l < 0.0010 0.0199 0.0200 100 55. - 135. 2666 blank 1,2-Dichlorobenzene mg/1 < 0.0010 0.0224 0.0200 112 37. - 154. 2666 blank 1,2-Dichlorobenzene mg/l < 0.0010 0.0212 0.0200 106 37. - 154. 2666 blank 1,3-Dichlorobenzene mg/1 < 0.0010 0.0168 0.0200 84 50. - 141. 2666 blank. 1,3-Dichlorobenzene mg/l < 0.0010 0.0176 0.0200 88 50. - 141. 2666 blank 1,4-Dichlorobenzene mg/1 < 0.0010 0.0182 0.0200 91 42. - 143. 2666 blank 1,4-Dichlorobenzene mg/l < 0.0010 0.0196 0.0200 98 42. - 143. 2666 blank Ethylbenzene mg/l < 0.0010 0.0234 0.0200 117 32. - 160. 2666 blank Ethylbenzene mg/1 < 0.0010 0.0227 0.0200 114 32. - 160. 2666 blank Toluene mg/1 < 0.0010 0.0218 0.0200 109 46. - 148. 2666 blank Toluene mg/l < 0.0010 0.0212 0.0200 106 46. - 148. 2666' blank o-Xylene mg/1 < 0.0010 0.0215 0.0200 108 74. - 126. 2666 blank o-Xylene mg/1 < 0.0010 0.0210 0.0200 105 74. - 126. 2666 blank Bromodichloromethane mg/1 < 0.0010 0.0196 0.0200 98 42. - 172. 2666 blank Bromodichloromethane mg/l, < 0.0010 0.0228 0.0200 114 42. - 172. 2666 blank Bromoform mg/1 < 0.0010 0.0211 0.0200 106 13. - 159. 2666 blank Bromoform mg/1 < 0.0010 0.0201 0.0200 100 13. - 159. _ 2666 blank Bromomethane mg/1 < 0.0010 0.0159 0.0200 80 10. - 144. 2666 blank Bromomethane mg/l < 0.0010 0.0180 0.0200 90 10. - 144. 2666 blank Carbon tetrachloride mg/l < 0.0010 0.0196 0.0200 98 43. - 143. 2666 blank Carbon tetrachloride mg/l < 0.0010 0.0225 0.0200 112 43. - 143. 2666 blank Chloroethane mg/l < 0.0010 0.0173 0.0200 86 46. - 137. 2666 blank Chloroethane mg/1 < 0.0010 0.0202 0.0200 101 46. - 137. 2666 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0168 0.0200 84 14. - 186. 2666 blank 2-Chloroethylvinylether mg/l < 0.0010 0.0196 0.0200 98 14. - 186. 2666 blank Chloroform mg/l < 0.0010 0.0174 0.0200 87 49. - 133. 2666 blank Chloroform mg/1 < 0.0010 0.0212 0.0200 106 49. - 133. 2666 blank Chloromethane mg/l < 0.0010 0.0162 0.0200 81 10.. - 193. 2666 blank Chloromethane mg/l < 0.0010 0.0189 0.0200 94 10. - 193. 2666 blank Dibromochloromethane mg/l < 0.0010 0.0191 0:0200 96 24. - 191. 2666 blank Dibromochloromethane mg/l < 0.0010 0.0216 0.0200 108 24. - 191. 2666 blank I` Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerioca I N C 0 R P 0 R A T E D - PROJECT QUALITY CONTROL DATA Ethylene Dibromide mg/l < 0.0010 0.0235 0.0200 118 -70. - 130. 2666 blank Ethylene Dibromide mg/l < 0.0010 0.0239 0.0200 120 70. - 130. 2666 blank Vinyl chloride mg/l < 0.0010 0.0181 0.0200 90 28. - 163. 2666 blank Vinyl chloride mg/l < 0.0010 0.0200 0.0200 100 28. - 163. 2666 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0208 0.0200 104 47. - 132. 2666 blank 1,1-Dichloroethane mg/1 < 0.0010 0.0222 0.0200 111 47. - 132. 2666 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0210 0.0200 105 51. - 147. 2666 blank 1,2-Dichloroethane mg/1 < 0.0010 0.0201 0.0200 100 51. - 147: 2666 blank 1,1-Dichloroethene mg/1 < 0.0010 0.0203 0.0200 102 28. - 167. 2666 blank 1,1-Dichloroethene mg/1 < 0.0010 0.0212 0.0200 106 28. - 167. 2666 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0217 0.0200 108 76. - 123. 2666 blank cis-1,2-Dichloroethene mg/1 < 0.0010 0.0201 0.0200 100 76. - 123. 2666 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0238 0.0200 119 38. - 155. 2666 blank trans-1,2-Dichloroethene mg/l < 0.0010 0.0168 0.0200 84 38. - 155. 2666 blank 1,2-Dichloropropane mg/l < 0.0010 0.0173 0.0200 86 44. - 156. 2666 blank 1,2-Dichloropropane mg/1 < 0.0010 0.0203 0.0200 102 44. - 156. 2666 blank cis-1,3-Dichloropropene mg/1 < 0.0010 0.0219 0.0200 110 22. - 178. 2666 blank cis-1,3-Dichloropropene mg/1 < 0.0010 0.0234 0.0200 117 22. - 178. 2666 blank trans-1,3-Dichloropropene mg/1 < 0.0010 0.0183 0.0200 92 22. -.178. 2666 blank trans-1,3-Dichloropropene mg/1 < 0.0010 0.0237 0.0200 118 22. - 178. 2666 blank Methylene chloride mg/1 < 0.0050 0.0175 0.0200 88 25. - 162. 2666 blank Methylene chloride mg/1 < 0.0050 0.0190 0.0200 95 25. - 162. 2666 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0195 0.0200 98 8. - 184. 2666 blank 1,1,2,2-Tetrachloroethane mg/1 < 0.0010 0.0253 0.0200 126 8. - 184. 2666 blank Tetrachloroethene mg/1 < 0.0010 0.0219 0.0200 110 26. - 162. 2666 blank Tetrachloroethene mg/1 < 0.0010 0.0235 0.0200 118 26. - 162. 2666 blank 1,1,1-Trichloroethane mg/1 < 0.0010 0.0178 0.0200 89 41. - 138. 2666 blank 1,1,1-Trichloroethane mg/l < 0.0010 0.0226 0.0200 113 41. - 138. 2666 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0208 0.0200 104 39. - 136. 2666 blank 1,1,2-Trichloroethane mg/l < 0.0010 0.0212 0.0200 106 39. - 136. 2666 blank Trichloroethene mg/1 < 0.0010 0.0192 0.0200 96 35. - 146. 2666 blank Trichloroethene mg/l < 0.0010 0.0253 0.0200 126 35. - 146. 2666 blank Trichlorofluoromethane mg/l < 0.0010 0.0186 0.0200 93 21. - 156. 2666 blank Trichlorofluoromethane mg/1 < 0.0010 0.0213 0.0200 106 21. - 156. 2666 blank Matrix Spike Duplicate Analyte units Orig. Val. Duplicate RPD Limit Q.C. Batch -------------------------------- -------------------- ----- ---------- Chloride mg/1 7.60 7.60 0.00 20. 1534 Project QC continued . . . r 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestL-�merica I N C 0 R P 0 R A T E D ,PROJECT QUALITY CONTROL DATA Laboratory Control Data Analyte --------------- units ------- Known Val. Analyzed Val % Recovery Target Range Q.C..Batch Benzene mg/l ---------- 0.0200 ------------ 0.0213 ---------- 106 ------------ 77 - 123 --------- 2666 Chlorobenzene mg/l 0.0500 0.0608 122 # 81 - 120 2666 - 1,2-Dichlorobenzene mg/l 0.0500 0.0571 114 68 - 132 2666 1,3-Dichlorobenzene mg/l 0.0500 0.0455 91 73 - 128 2666 1,4-Dichlorobenzene . mg/l 0.0500 0.0483 97 70 - 131 2666 Ethylbenzene mg/l 0.0500 0.0523 105 63 - 137 2666 Toluene mg/l 0.0500 0.0455 91 78 - 123 2666 m,p-Xylenes mg/l 0.1000 0.0965 96 84 - 115 2666 o-Xylene mg/1 0.0500 0.0470 94 83 - 124 2666 Bromodichloromethane mg/1 0.0500 0.0485 97 76 - 124 2666 Bromoform mg/1 0.0500 0.0468 94 74 - 127 2666 Bromomethane mg/l 0.0500 0.0473 95 59 - 142 2666 Carbon tetrachloride mg/l 0.0500 0.0560 112 69 - 132 2666 Chloroethane mg/l 0.0500 0.0557 111 77 - 123 2666 2-Chloroethylvinylether mg/1 0.0500 0.0479 96 60 - 140 2666 Chloroform mg/l 0.0500 0.0462 92 75 - 125 2666 Chloromethane mg/1 0.0500 0.0662 132 60 - 141 2666 Dibromochloromethane mg/l 0.0500 0.0538 108 66 - 135 2666 Ethylene Dibromide mg/1 0.0500 0.0588 118 82 - 119 2666 Vinyl chloride mg/1 0.0500 0.0503 101 69 - 132 2666 Dichlorodifluoromethane mg/l 0.0500 0.0587 117 75 - 124 2666 1,1-Dichloroethane mg/l 0.0500 0.0506 101 84 - 116 2666 1,2-Dichloroethane mg/1 0.0500 0.0489 98 72 - 129 2666 1,1-Dichloroethene mg/1 0.0500 0.0572 114 63 - 137 2666 cis-1,2-Dichloroethene mg/l 0.0500 0.0594 119 76 - 124 2666 trans-1,2-Dichloroethene mg/l 0.0500 0.0638 128 64 - 136 2666 1,2-Dichloropropane mg/1 0.0500 0.0483 97 74 - 126 2666 cis-1,3-Dichloropropene mg/l 0.0500 0.0491 98 63 - 136 2666 trans-1,3-Dichloropropene mg/l 0.0500 0.0562 112 63 - 136 2666 Methylene chloride mg/l 0.0500 0.0496 99 78 - 123 2666 1,1,2,2-Tetrachloroethane mg/l 0.0500 0.0559 112 49 - 151 2666 Tetrachloroethene mg/1 0.0500 0.0479 96 70 - 130 2666 1,1,1-Trichloroethane mg/l 0.0500 0.0502 100 71 - 129 2666 1,1,2-Trichloroethane mg/l 0.0500 0.0505 101 79 - 122 2666 Trichloroethene mg/l 0.0500 0.0529 106 77 - 123 2666 Project QC continued . . . l r 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 � r1 Test me ca I N C O R P O R A T E D ---PROJECT QUALITY CONTROL DATA r Laboratory Control Data Analyte units Known Val. Analyzed Val % Recovery Target Range Q.C. Batch --------------------------------------------------------------------------- Trichlorofluoromethane mg/1 0.0500 0.0532 106 67 - 134 2666 Chloride mg/1 30.0 27.3 91 90 - 110 1534 Analyte Chloride Benzene Benzene Chlorobenzene Chlorobenzene 1,2-Dichlorobenzene i 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene Ethylbenzene Toluene Toluene m,p-Xylenes m,p-Xylenes o-Xylene o-Xylene Bromodichloromethane Bromodichloromethane Bromoform Bromoform Bromomethane Bromomethane Carbon tetrachloride Carbon tetrachloride Chloroethane Project QC continued Blank Data Blank Value Units Q.C. Batch < 1.00 mg/l 1534 * 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/l 2666 < 0.0010 mg/l 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0:0010 mg/1 2666 < 0.0010 mg/l 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/l 2666 < 0.0010 mg/l 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/l 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 '< 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/l 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 < 0.0010 mg/1 2666 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Testl�merica I N C O R P O R A T E D i n PROJECT QUALITY CONTROL DATA Blank Data Analyte Blank Value --------------- Units Q.C. Batch ------------ Chloroethane < 0.0010 --------- mg/l ---------- 2666 2-Chloroethylvinylether < 0.0010 mg/l 2666 2-Chloroethylvinylether < 0.0010 mg/1 2666 j Chloroform < 0.0010 mg/1 2666 Chloroform < 0.0010 mg/1 2666 Chloromethane < 0.0010 mg/l 2666 f Chloromethane < 0.0010 mg/l 2666 Dibromochloromethane < 0.0010 mg/l 2666 Dibromochloromethane < 0.0010 mg/1 2666 Ethylene Dibromide < 0.0010 mg/l 2666 Ethylene Dibromide < 0.0010 mg/l 2666 Vinyl chloride < 0.0010 mg/1 2666 -, Vinyl chloride < 0.0010 mg/1 2666 Dichlorodifluoromethane < 0.0010 mg/1 2666 Dichlorodifluoromethane < 0.0010 mg/1 2666 1,1-Dichloroethane < 0.0010 mg/1 2666 1,1-Dichloroethane <- 0.0010 mg/l 2666 1,2-Dichloroethane < 0.0010 mg/l 2666 1,2-Dichloroethane < 0.0010 mg/l 2666 1,1-Dichloroethene < 0.0010 mg/l 2666 1,1-Dichloroethene < 0.0010 mg/l 2666 cis-1,2-Dichloroethene < 0.0010 mg/1 2666 cis-1,2-Dichloroethene < 0.0010 mg/1 2666 trans-1,2-Dichloroethene < 0.0010 mg/1 2666 trans-1,2-Dichloroethene < 0.0010 mg/1 2666 1,2-Dichloropropane < 0.0010 mg/l 2666 1,2-Dichloropropane < 0.0010 mg/l 2666 cis-1,3-Dichloropropene < 0.0010 mg/l 2666 cis-1,3-Dichloropropene < 0.0010 mg/l 2666 --1 trans-1,3-Dichloropropene < 0.0010 mg/l 2666 trans-1,3-Dichloropropene < 0.0010 mg/l 2666 Methylene chloride < 0.0050 mg/1 2666 Methylene chloride < 0.0050 mg/l 2666 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 2666 1,1,2,2-Tetrachloroethane < 0.0010 mg/l 2666 Project QC continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TelstAmerica I N C O R P O R A T E D -,PROJECT QUALITY CONTROL DATA I Blank Data Analyte Blank Value --------------- Units Q.C. Batch ------------ Tetrachloroethene < 0.0010 --------- mg/l ---------- 2666 Tetrachloroethene < 0.0010 mg/l 2666 1,1,1-Trichloroethane < 0.0010 mg/l 2666 1,1,1-Trichloroethane < 0.0010 mg/1 2666 1,1,2-Trichloroethane < 0.0010 mg/l 2666 1,1,2-Trichloroethane < 0.0010 mg/1 2666 Trichloroethene < 0.0010 mg/l 2666 Trichloroethene < 0.0010 mg/l 2666 Trichlorofluoromethane < 0.0010 mg/l 2666 Trichlorofluoromethane < 0.0010 mg/l 2666 # — Value outside Laboratory historical QC limits. End of Report for Project 212822 i 2960 FOSTER CREIGHTON DRIVE / NASHVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 S TAMERICA.YNC.-1 \t1 SHVIL1rJE • ti rl '1 .r - COOLER RECEIPT FOMM Client: I3C4 Cooler Received On: in.zt-can Aud Opened Ou:(o-z1-ck-o. By: Michael McBride %-A (Signature) ' • i. Temperature of Cooler )tihen opened 3 Degrees elsius •• -. ....................:..................................YES i10 Were custody seals on outside of cooler? ' a. If yes, hose many, what kind and where: _ 3. Were custody seals on containers and intact? ........................... :................ CO 'YES 4. Were the seals intact., signed, and dated correctly? ..................................... ' 5. Were custody papers inside cooler?........................................................... \'O 6. Were custody papers properly filled out ink siaued etc ? �M No 7. Did you sign the custody papers in the appropriate place?...............................4iTJ NO s. What kind of packing material used? u blesvrap Peanuts Vermiculite Other None 9. Was sufficient ice used (if appropriate)?.......................................................ZS NO 10. Did all bottles arrive in good condition unbroken 11. Were all bottle Iabels complete (#,date,signed,pres,etc)?............................... O.D NO 12. Did all bottle labels and tags agree pith custody papers?........... � 13. Were correct bottles used for the analysis requested? .................. ................. 14. a. Were VOA vials received? ..................... ......................... I ............... 1!0 NO - b. Was there any observable head space present in aayYOA Sial?...........:::. 'O YES • •• •-- - •- • 15.- Was sufficient amount of sample sent in each bottle .................................••••- 16. Were correct preservatives used? ............................. ................................... ®h0 17. Was residual chlorine present?........................................................... 0 YES 17. r.a Corrective action talon, if necessary: See attached for resolution _ . '"' "'" Chain of Custody Record 2338 TESTAMEr Page--1— or —1- ❑ Asheville, NC (A) ❑ Bartlett, IL (C) ❑ Cedar Falls, IA (E)❑ Charlotte, NC (G) ❑ Dayton, OH 00-0961 Li Rockford II (Q) (828)254-5169 (630)289-3100 (319)277-2401 (704)392-1164 (937)294-68 (815)874-2171 ❑ Atlanta, GA (B) ❑ Brighton, CO (D)❑ Charleston, SC (F) ❑ Columbia, SC (H) ❑ Davenport. 1, MORRISVILLE, NC 1 ❑ Watertown, WI (R) (770)368-0636 (303)659-0497 (843)849-6550 (803)796-8989 (319)323-7t Client: `j CC) 0 Project No.: 0753!� REQUESTED PARAMETERS Report Address:2X0 w(wiltv Invoice Address: y 'l Is this work being conducted for �UT�f1 SVl Z7� U Q� regulatory compliance monitoring? Yes_ No — Phone �� Ann: — Phone No.: 1 1— Sampled By: 'D. Is this work being conducted for 1LURELL regulatory enforcement action? Fax No.: q1q— el— � P.O. No: �* (v Yes_ No — TURNAROUND k Which regulations apply: Quote No. gnu RCRA_ NPDESWastewater_ TURNAROUND TIME �� "'�[3�0 �/ State Samples Collected 43?g Q' UST_ Drinking Water_ L►7 Standard g Other_ None_ ❑ Rush (surcharges may apply) Date Needed: V # and type of containers _ LOmp Sample ID Date Time (C) Matrix Grab (G)cj OM c REMARKS Lab Use nn G ME; ore ME Ism M"WOMMMMM FAMMMMMMMMMMANNEEN�■■ ���©�1MMMMMMMMM■■■■■n ►. Nor, t d = COMMENTS Relinquished By �t�w Datf6 zA 1 Date Date I �/ 1,1Time Time Time Received Received By: Received By: ReceiV—l11 1 A�•/ 1 Dat ?Astim. LA$ USE,QNLY = :: Date Time Date Time Seal C�N/A ustody Yes 0No fe.� pp P'Ctt� T Ar,Y' hullo _ (� Relinquished By: Relinquished By: Relinquished Bv: --