WI0400023_W/ Corrective Action_20011129

U -'�L
ED
IT CORPORATION
A Member of The /T Croup
CORRECTIVE ACTION/MONITORING REPORT
March 2001 Through October 2001
W. P. Ballard Property
2701 Branchwood Drive
Greensboro, Guilford County, North Carolina
NCDENR Groundwater Incident # 6953
IT Corporation of North Carolina Project # 107535
November 29, 2001
Prepared by. -
IT Corporation of North Carolina, Inc.
2200 Gateway Center Drive, Suite 205
Morrisville, North Carolina 27560
[phone]
Volume llofll

IT Corporation of 1Yorih Carolina, Inc.
A Alcrnhcr of The 17' Croup
Appendix A
Laboratory Analytical Data Reports — Groundwater Samples

TestAmerica
I N C O R P O R A T E D
I
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118374
KIM PRZYBYL Sample ID: MW1
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water
MORRISVILLE, NC 27560 Site ID:
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
I .
Date
Time
Date
Time
Collected:
Collected:
Received:
Received:
8/22/01
8:05
8/23/01
9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
F------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Chlorobenzene
ND
ug/l
50.0
1.0
50
8/28/01
8:14
CHollingsw
602/601
73
1,2-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
602/601
7121
1,4-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
0:58
CHollingsw
602/601
7121
'- Bromodichloromethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Bromoform
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Bromomethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7 12 1
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
2-Chloroethylvinylether
{
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Chloroform
1.5
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Chloromethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
60.1
7121
Dibromochloromethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
1,1-Dichloroethene
ND
ug/1
1'.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
cis-1,2-Dichloroethene
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
trans-1,2-Dichloroethene
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
1,2-Dichloropropane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
cis-1,3-Dichloropropene
ND
ug/1
1.0
1.0
1
8/25/01
-0:58
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Methylene chloride
ND
ug/1
5.0
5.0
1
8/25/01
0:58
CHollingsw
601
7121
-' 1,1,2,2-Tetrachloroethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE. / NASNVILLE.TN 37204 / 613-726-0177 / F:kx: 615-726-0954 / 800-765-0980

i
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118374
Sample ID: MW1
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
- Analyte
----------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
--
Tetrachloroethene
2310
ug/1
-------
50.0
------
1.0
------
50
--------
8/28/01
------
8:14
-----------
CHollingsw
---------
601
-----
73
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Trichloroethene
1.2
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
Trichlorofluoromethane
ND
ug/1
1.0
1.0
1
8/25/01
0:58
CHollingsw
601
7121
ND - Not detected at the
report limit.
Surrogate % Recovery Target Range
I-----------------------------------
PID Surr., a, a, a- tri fluoro toluene 95. 50. - 150.
Hall Surr., 2-chloropropane 85. 50. - 128.
Hall Surr., chloroprene 82. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 134. # 49. - 132.
Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. ICelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CRRlcti•ro` DRIVE / NASII n.i.E.TN 37204 / 615-726-0177 / F.xx: 615-726-0954 / 800-765-0980

TABLE 4
Historical Groundwater Analytical Data Summary - Shallow Wells
W. P. Ballard and Downgradient Properties
Greensboro, North Carolina
Sample Location:
MW-26
MW-27
MW-28
Sample Date:
10/7/96 A
I 0/7/96 B
1 8/26/97 B
12/2/98 B
10/27/99 B
3/22/00 B
9/14/00 B
3/8/01 8
8/22/01 B
8/26/97 B
12/2/98 B
10/27/99 B
3/22100 B
9/14/00 B
3/8/01 B
8/22/01 B
Analyte
NCAC 2L
Benzene (ug/L)
1.0
NA
NA
NA
<1.0
<500
NS
NA
NA
NA
NA
<1.0
<10.0
<1.0
NA
NA
NA
Ethylbenzene (ug/L)
29
NA
NA
NA
<1.0
<500
NS
NA
NA
NA
NA
<1.0
<10.0
<1.0
NA
NA
NA
Methylene Chloride (ug/L)
5.0
<2.5
<1.0
<200
<5.0
<2500
NS
<250
<5.0
<5
<200
<5.0
<50.0
<5.0
<50.0
<5.0
<5
Chloroform (ug/L)
0.19
0.97
0.49
<200
<1.0
<500
NS
<50
<1.0
<1
<200
<1.0
<10.0
<1.0
10
<1.0
<1
Chloromethane (ug/L)
none
<0.50
<2.0
<200
<1.0
<500
NS
<50
<1.0
<1
<200
<11.0
<10.0
<1.0
<10.0
<1.0
<t
Carbon Tetrachloride (ug/L)
0.3
<0.50
<0.30
<200
<1.0
<500
NS
<50
<1.0
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
1,1-Dichloroethane (ug/L)
700
<0.50
<1.0
c200
<1.0
< 500
NS
<50
6
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
1,2-Dichloroethane (ug/L)
0.38
<0.50
<1.0
<200
<1.0
<500
NS
<50
3
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
1,1-Dichloroethene (ug/L)
7.0
<0.50
<7.0
<200
<1.0
<500
NS
<50
9
1.7
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
cis-1,2-Dichloroethene (ug/L)
70
NA
NA
12,000
2,300
3,700
NS
2,300
3,270
527
280
1,170
323
413
385
162
583
trans-1,2-Dichlorcethene (ug/L)
70
NA
NA
<200
13
<500
NS
<50
12
<1
<200
3
<10.0
1.2
<10.0
<1.0
<1
1,2-Dichloropropane (ug/L)
0.56
<0.50
<0.20
<200
<1.0
<500
NS
<50
<1.0
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
Methyl tent -butyl ether (MTBE) (ug/1)
200
NA
NA
NA
NA
<500
NS
NA
NA
<1
NA
NA
<10.0
NA
NA
NA
<1
Trichloroethene (ug/L)
2.8
<0.50
<1.0
64,000
8,340
15,900
NS
4,680
6,040
442
180
Boo
192
126
178
69
134
Tetrachloroethene (ug/L)
1
<0.50
<0.70
<200
<1.0
<500
NS
85
23
<1
<200
70
<10.0
20
<10.0
9
<1
1,1,2,2-Tetrachloroethane (ug/L)
none
<0.50
<1.0
<200
<1.0
<500
NS
<50.0
<1.0
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
Toluene (ug/L)
1,000
NA
NA
NA
NA
<500
NS
NA
NA
NA
NA
<1.0
<10.0
<1.0
NA
NA
NA
1,1,1-Trichloroethane (ug/L)
200
<0.50
<1.0
<200
<1.0
<500
NS
<50
<1.0
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
1,1,2-Trichloroethane (ug/L)
none
<0.50
<1.0
<200
<1.0
<500
NS
<50
1
<1
<200
<1.0
<10.0
<1.0
<10.0
<1.0
<1
Xylenes, Total (ug/L)
NA
NA
NA
NA
<1,000
NS
NA
NA
NA
NA
<2.0
<20.0
<2.0
NA
NA
NA
Total VOCs Detected (ug/L)
1
0
76,000
10,653
19,600
0
7,065
9,364
971
460
2,043
515
561
573
240
717
Sample Location:
PT-1S
PT-2S
PT-3S
PT-4S
PT-5S
Sample Date:
8/29/97 B
1 3123/00 B
9/12/00 B
8/29197 B
3/23/00 B
9/12/00 B
8/29/97 B
3/23/00 B
9/12/00 B
8/29/97 B
3/23/00 B
9/12/00 B
8129/97 B
3/23/00 B
1 9111/00 B
Analyte
NCAC 2L
Benzene (ug/L)
1.0
<500
NS
<100
<500
310
NS
<50
<1.0
<200
<5
<1.0
<100
<500
2.2
<1,000
Ethylbenzene (ug/L)
29
<500
NS
<100
<500
5.6
NS
<50
<1.0
<200
<5
<1.0
<100
<500
<1.0
<1,000
Methylene Chloride (ug/L)
5.0
<500
NS
<500
<500
<5.0
NS
<50
<5.0
<1,000
<5
<5.0
<100
<500
<5.0
<1,000
Chloroform (ug/L)
0.19
<500
NS
<100
<500
69.5
NS
<50
20.6
<200
<5
4.3
<100
<500
5.2
<1,000
Chloromethane (ug/L)
none
<1,000
NS
<100
<1,000
<1.0
NS
<100
<1.0
<200
<10
<1.0
<100
<1,000
<1.0
<1,000
Carbon Tetrachloride (ug/L)
0.3
<500
NS
<100
<500
<1.0
NS
<50
<1.0
<200
<5
2.5
<100
<500
<1.0
<1,000
1,1-Dichloroetttane (ug/L)
700
<500
NS
<100
<500
<1.0
NS
<50
<1.0
<200
<5
<1.0
<100
<500
<1.0
<1,000
1,2-Diichloroethane (ug/L)
0.38
<500
NS
<100
<500
72.2
NS
<50
3.6
<200
<5
3.6
<100
<500
<1.0
<1,000
1,1-D'ichlorcethene (ug/L)
7.0
<500
NS
<100
<Spp
<1.0
NS
<50
<1.0
<200
5.4
4.4
<100
<500
<1.0
<1,000
cis-1,2-Dichloroethene (ug/L)
70
<500
NS
<100
<500
8.6
NS
<50
34.3
<200
3,900
5,800
1,700
<500
<500
<1,000
trans-1,2-Dichloroethene (ug/L)
70
<500
NS
<100
<500
<1.0
NS
<50
<1.0
<200
<5
8.5
<100
<500
<1.0
<1,000
1,2-Dichloropropane (ug/L)
0.56
<500
NS
<100
<500
<1.0
NS
<50
<1.0
<200
<5
<1.0
<100
<500
<1.0
<1,000
Methyl tert-butyl ether (MTBE) (ug/1)
200
<500
NS
<100
<500
NS
NS
<50
NS
<200
<5
NS
<100
<500
NS
<1,000
Trichloroethene (ug/L)
2.8
<500
NS
<100
<500
100
NS
1,800
2,650
<200
2,900
2,290
890
<500
39.1
<1,000
Tetrachloroethene (ug/L)
0.7
12,000
NS
2,770
9,800
12,100
NS
2,400
6,400
2,520
120
180
<100
20,000
40,400
10,600
1,1,2,2-Tetrachloroethane (ug/L)
none
<500
NS
<100
<5o0
<1.0
NS
<50
<1.0
<200
<5
<1.0
<100
<500
2.1
<1,000
Toluene (ug/L)
1,000
<500
NS
<100
<500
51
NS
<50
<1.0
<200
<5
<1.0
<100
<500
<1.0
<1,000
1,1,1-Trichlorcethane (ug/L)
200
<500
NS
<100
<500
<1.0
NS
<50
<1.0
<200
<5
<1.0
<100
<500
<1.0
<1,000
1,1,2-Trichloroethane (ug/L)
none
<500
NS
<100
<500
11.5
NS
<50
3.6
<200
<5
<1.0
<100
<500
37.4
<1,000
Xylenes, Total (ug/L)
530
<500
NS
<100
<500
90.6
NS
<50 1
<2.0
<200
<5
<2.0
<100
<500
<2.0
<1,000
Total VOCs Detected (ug/L)
12,000 1
0
2,770 1
9,800
12,819
0
4,200
9,112
2,520
6,925 1
8,293 1
2,590
20,000
40,486 1
10.600
Notes: Compounds detected above the North Carolina 2L Standard are shown in bold.
A - indicates samples collected by Mortensen Engineering, Inc.
B - indicates samples collected by IT Corporation of North Carolina, Inc. (formerly Fluor Daniel GTI, Inc.)
NA denotes compound not analyzed
NS denotes well not sampled
Monitoring wells MW-16, MW-19, MW-24, MW-25 and MW-26 were destroyed during site construction acttiities.
Shallow gw Hist summary.xls Page 6 of 6 Revised 11/18/01

- TestAmerica
iINCO RPO RATED
ANALYTICAL REPORT
it IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118382
Sample ID: MW2
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected: 13:55
Date Received: 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- ------ ------- ------ ------------ -- ------ -------------------- -----
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
i
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
i Carbon tetrachloride
Chloroethane
I
2-Chloroethylvinylether
` Chloroform
Chloromethane
Dibromochloromethane
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
j 1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Sample report continued .
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
602/601
7121
NO
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
602/601
7121
NO
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
NO
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
5.2
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
NO
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
NO
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
5.9
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
88.0
ug/l
20.0
1.0
20
8/28/01
12:44
CHollingsw
601
73
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
NO
ug/1
5.0
5.0
1
8/27/01
19:39
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
2960 FOSTER CREIGHTON DRIVE / N:\SHVII,I.E,TN 37204 / 615-726-0177 / F%x: 615-726-0954 / 800-765-0980

i I
_I rl
TestA•
m
e ca
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118382
Sample ID: MW2
Project: 107535-30205000
Page 2
� i
Report
p
Quan
Dil�
Analysis
Analysis
Analyte
Result
----
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
_
Tetrachloroethene
184.
ug/l
-------
20.0
------
1.0
------
20
--------
8/28/01
------
12:44
-----------
CHollingsw
---------
601
-----
73
_ 1,1,1-Trichloroethane
1.7
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/1
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
Trichloroethene
39.8
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
Trichlorofluoromethane
ND
ug/l
1.0
1.0
1
8/27/01
19:39
CHollingsw
601
7121
ND - Not detected at the
I'
report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 94. 50. - 150.
Hall Surr., 2-chloropropane 84. 50. - 128.
Hall Surr., chloroprene 73. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 109. 49. - 132.
- Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: c,.��R.► Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / N:\slnn.I,E.TN 37204 / 615-726-0177 / Fx.Y: 61.5-726-0954 / 800-765-0980

TestAmerica
INCO RPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
i Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118378
Sample ID: MW3
Sample Type: Water
Site ID.
Date Collected: 8/22/01
Time Collected: 11:05
Date Received: 8/23/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*ORGANIC PARAMETERS*
Benzene
ND
ug/l
1.00
1.00
1
8/26/01
19:28
D.Ramey
602
7282
Toluene
15.5
ug/l
1.00
1.00
1
8/26/01
19:,28
D.Ramey
602
7282
Ethylbenzene
ND
ug/l
1.00
1.00
1
8/26/01
19:28
D.Ramey
602
7282'
Xylenes, total
3.5&
ug/l
1.00
1.00
1
8/26/01
19:28
D.Ramey
602
7282
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Chlorobenzene
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
602/601
73
1,2-Dichlorobenzene
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
602/601
73
1,3-Dichlorobenzene
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
602/601
73
1,4-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/27/01
22:45
CHollingsw
602/601
73
Bromodichloromethane
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
601
73
Bromoform
ND
ug/1
500.
2.0
500
8/27/01
22:45
CHollingsw
601
73
Bromomethane
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Carbon tetrachloride
4.6
ug/1
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Chloroform
43.7
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Chloromethane
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Dibromochloromethane
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
601
73
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1,1-Dichloroethene
2.9
ug/l
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
cis-1,2-Dichloroethene
ND
ug/l
500.
1.0
500
8/27/01
22:45
CHollingsw
601
73
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / NASHVII.I.E.TN 37204 / 615-726-0177 / Fix: 615-726-0951 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Analyte Result Units
trans-1,2-Dichloroethene
2.2
ug/1
1,2-Dichloropropane
ND
ug/1
cis-1,3-Dichloropropene
ND
ug/1
trans-1,3-Dichloropropene
5.0
ug/1
Methylene chloride
ND
ug/l
1,1,2,2-Tetrachloroethane
ND
ug/1
Tetrachloroethene
126000
ug/1
1,1,1-Trichloroethane
3.0
ug/1
1,1,2-Trichloroethane
40.2
ug/1
Trichloroethene
ND
ug/1
Trichlorofluoromethane
NDj
ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118378
Sample ID: MW3
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.0
1.0
------
1
--------
8/25/01
------
3:46
-----------
CHollingsw
---------
601
-----
7121
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
2500
5.0
500
8/27/01
22:45
CHollingsw
601
73
500.
1.0
500
8/27/01
22:45
CHollingsw
601
73
5000
1.0
5000
8/28/01
13:25
CHollingsw
601
91
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
500.
1.0
500
8/27/01
22:45
CHollingsw
601
73
1.0
1.0
1
8/25/01
3:46
CHollingsw
601
7121
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
121.
67.
- 135.
PID Surr., a,a,a-trifluorotoluene
94.
50.
- 150.
Hall Surr., 2-chloropropane
83.
50.
- 128.
Hall Surr., chloroprene
83.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
125.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
' Sample report continued . . .
2960 FOSTER CREIGHTO\ DRivF, / NASHVII,I,E,TN 37204 / 615-726-0177 / F\.x: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Laboratory Number: 01-A118378
Sample ID: MW3
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FIISTER CREIGHTON DRIVE / N;%SHVILI,E.TN 37204 / 615-726-0177 / F": 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E 0
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118379
Sample ID: DUP02
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected:
Date Received: 8/23/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*ORGANIC PARAMETERS*
Benzene
ND
ug/1
1.00
1.00
1
8/26/01
19:58
D.Ramey
602
7282
Toluene
15.4
ug/1
1.00
1.00
1
8/26/01
19:58
D.Ramey
602
7282
Ethylbenzene
ND:-
ug/l
1.00
1.00
1
8/26/01
19:58
D.Ramey
602
7282
%ylenes, total
3.50
ug/l
1.00
1.00
1
8/26/01
19:58
D.Ramey
602
7282
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Chlorobenzene
ND
ug/l
500.
1.0
500
8/27/01
23:26
CHollingsw
602/601
73
1,2-Dichlorobenzene
ND
ug/l
500.
1.0
500
8/27/01
23:26
CHollingsw
602/601
73
1,3-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/27/01
23:26
CHollingsw
602/601
73
1,4-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/27/01
23:26
CHollingsw
602/601
73
Bromodichloromethane
ND
ug/1
500.
1.0
500
8/27/01
23:26
CHollingsw
601
73
Bromoform
ND
ug/i
500.
2.0
500
8/27/01
23:26
CHollingsw
6vi
;3
Bromomethane
ND
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Carbon tetrachloride
5.1
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Chloroform
45.9
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Chloromethane
NO
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Dibromochloromethane
ND
ug/1
500.
1.0
500
8/27/01
23:26
CHollingsw
601
73
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1,1-Dichloroethene
4.2
ug/l
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
cis-1,2-Dichloroethene
ND
ug/l
500.
1.0
500
8/27/01
23:26
CHollingsw
601
73
Sample report continued .
2960 FOSTER CREIGHTO;N DRIVE / NASHVII,I,EJN 37204 / 615-726-0177 / R: x: 615-726-0954 / 800-765-0980

I - .
Test_ m e 1Ca
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte
------------------------
Result
Units
trans-1,2-Dichloroethene
-----------
3.8
-------
ug/l
1,2-Dichloropropane
ND
ug/l
cis-1,3-Dichloropropene
ND
ug/1
i } trans-1,3-Dichloropropene
6.8
ug/1
I 't Methylene chloride
ND
ug/1
1,1,2,2-Tetrachloroethane
ND
ug/1
r Tetrachloroethene
123000
ug/1
1,1,1-Trichloroethane
3.6
ug/1
'- 1,1,2-Trichloroethane
43.0
ug/1
Trichloroethene
ND
ug/1
Trichlorofluoromethane
2.5
ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118379
Sample ID: DUP02
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.0
1.0
------
1
--------
8/25/01
------
4:28
-----------
CHollingsw
---------
601
-----
7121
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1.0
1.0
1
8/25/01
4:28
CHollingsw
.601
7121
2500
5.0
500
8/27/01
23:26
CHollingsw
601
73
500.
1.0
500
8/27/01
23:26
CHollingsw
601
73
5000
1.0
5000
8/28/01
14:08
CHollingsw
601
91
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
500.
1.0
500
8/27/01
23:26
CHollingsw
601
73
1.0
1.0
1
8/25/01
4:28
CHollingsw
601
7121
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
119.
67.
- 135.
PID Surr., a,a,a-trifluorotoluene
94.
50.
- 150.
Hall Surr., 2-chloropropane
87.
50.
- 128.
Hall Surr., chloroprene
82.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
125.
49.
- 132.
# - Recovery outside Laboratory historical or
method prescribed
limits.
? 1 Sample report continued . . .
� I
2960 FOSTER CRFi(;[rr .N DRIVE / N;\sItt ii,i,E.TN 37204 / 615-726-0177 / F%.e: 613-726-0954 / 800-765-0980

•
TestAmerica
I N C O R P O R A T E D
I
ANALYTICAL REPORT
Laboratory Number: 01-A118379
Sample ID: DUP02
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: C44 '4-4 Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical.Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith,,Ass is.tant.Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHT(1N DRNE, / N sH%'ILLE.TN 37204 / 615-726-0177 / F. x: 6.15-726-0954 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number: 01-A119820
KIM PRZYBYL
Sample ID: MW-4
2200 GATEWAY CTR. BLVD. STE205
Sample Type: Water
MORRISVILLE, NC 27560
Site ID:
Date Collected: 8/23/01Time
Project: 107535-30205000
Collected: 10:30
Project Name: SEARS-GREENSBORO
Date Received: 8/25/01
Sampler:.DAVID LUBERO
Time Received: 10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
------
Limit
------
Limit
-------
Factor
------
Date
--------
Time
---=-
Analyst
----------
Method
---------
Batch
-----
*ORGANIC PARAMETERS*
Benzene
2.30
ug/l
1.00
1.00
1
8/28/01
10:26
D.Ramey
602
8829
Toluene
2.40
ug/1
1.00
1.00
1
8/28/01
10:26
D.Ramey
602
8829
Ethylbenzene
1.40
ug/l
1.00
1.00
1
8/28/01
10:26
D.Ramey
602
8829
Xylenes, total
16.4
ug/l
1.0
1.0
1
8/28/01
10:26
D.Ramey
602
8829
j *VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
602/601
9840
1,3-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
60:
9840
{ Bromoform
ND
ug/l
50.0
2.0
50
8/29/01
8:55
CHollingsw
601
9840
Bromomethane
ND
ug/1
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Chloroethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
2-Chloroethylvinylether
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
- Chloroform
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Chloromethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Dibromochloromethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
-_ Ethylene Dibromide
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Vinyl chloride
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
-', Dichlorodifluoromethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
1,1-Dichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
- Sample report continued . . .
2960 FOSTER CREICHrON DRIVE / NASHVII,I,E,TN 37204 / 615-726-0177 / F. x: 615-726-0954 / 800-765-0980

•
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A119820
Sample ID: MW-4
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
Limit
Limit
Factor
Date
Time
Analvst
Method
Batch
1,2-Dichloroethane
ND
------
ug/l
------
50.0
-------
1.0
------
50
--------
8/29/01
-----
8:55
----------
CHollingsw
---------
601
-----
9840
1,1-Dichloroethene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
cis-1,2-Dichloroethene
90.0
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
trans-1,2-'Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
trans-1,3-Dichloropropene
ND
ug/1
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Methylene chloride
ND
ug/l
250.
5.0
50
8/29/01
8:55
CHollingsw
601
9840
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Tetrachloroethene
12800
ug/1
500.
1.0
500
8/29/01
13:43
CHollingsw
601
781
1,1,1-Trichloroethane
ND
ug/l
50.0
1.0
50'
8/29/01
8:55
CHollingsw
601
9840
1,1,2-Trichloroethane
ND'
ug/l
50_0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Trichloroethee
370.
ug/1
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
Trichlorofluoromethane
ND:
ug/1
50.0
1.0
50
8/29/01
8:55
CHollingsw
601
9840
ND - Not detected at the report limit.
Surrogate
-------------
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
95.
67. -
135.
?ID Surr., a,a,a-trifluorotoluene
88.
50.
- 150.
Hall Surr., 2-chloropropane
101.
50.
- 128.
Hall Surr., chloroprene
106.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
105.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / N,\SIICII,LE,TN 37204 / 615-726-0177 / F. x: 615-726-0954 / 800-765-0980

r
TestAmerica
1 I N C O R P O R A T E D.
ANALYTICAL REPORT
Laboratory Number: 01-A119820
Sample ID: MW-4
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: - !' Report Date: 8/29/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHTON DRIVF: / N:%SHVH.LE.TN 37204 / 615-726-0177 / Fk.x: 615-726-0954 / 800-765-0980

i
TestAmerica
�I
I NCO RPORATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number: 01-A118377
KIM PRZYBYL
Sample ID: MW5
2200 GATEWAY CTR. BLVD. STE205
Sample Type: Water
MORRISVILLE, NC 27560
Site ID:
Date Collected:
8/22/01
Project: 107535-30205000
Time Collected:.
10:10
Project Name: SLS-GREENSBORO
Date Received:
8/23/01
Sampler: DAVID
Time Received:
9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
{
Result
Units
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
*ORGANIC PARAMETERS*
Benzene
ND
ug/1
1.00
1.00
1
8/26/01
18:58
D.Ramey
602
7282
Toluene
ND
ug/1
1.00
1.00
1
8/26/01
18:58
D.Ramey
602
7282
Ethylbenzene
ND
ug/1
1.00
1.00
1
8/26/01
18:58
D.Ramey
602
7282
Xylenes, total
ND.
ug/1
1.00
1.00
1
8/26/01
18:58
D.Ramey
602
7282
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7 12 1
Chlorobenzene
ND
ug/1
100.
1.0
100
8/27/01
21:23
CHollingsw
602/601
73
I_ 1,2-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
602/601
7121
1,4-Dichlorobenzene
i
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
602/601
7121
Bromodichloromethane
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Bromoform
ND
ug/1
100.
2.0
100
8/27/01
21:23
CHollingsw
601
73
Bromomethane
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/1
1.0
1.0
1
8/25/01
3:04.
CHollingsw
601
7121
Chloroform
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Chloromethane
ND
ug/1
L.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Dibromochloromethane
1.9
ug/l
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
- 1,1-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1,1-Dichloroethene
34.9
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
cis-1,2-Dichloroethene
3.1
ug/1
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / NASHVII•LE.TN 37204 / 615-726-0177 / F.v.x: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
trans-1,2-Dichloroethene
ND
ug/l
1,2-Dichloropropane
ND
ug/1
cis-1,3-Dichloropropene
ND
ug/l
trans-1,3-Dichloropropene
ND
ug/1
Methylene chloride
9.8
ug/1
1,1,2,2-Tetrachloroethane
ND
ug/1
Tetrachloroethene
7520
ug/1
1,1,1-Trichloroethane
ND
ug/1
1,1,2-Trichloroethane
1.0
ug/1
Trichloroethene
1.4
ug/1 .
Trichlorofluoromethane
ND
ug/l
ND - Not detected at the report.limit.
Surrogate
-------------
Laboratory Number: 01-A118377
Sample ID: MW5
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
1.0
------
1.0
------
1
--------
8/25/01
------
3:04
-----------
CHollingsw
---------
601
-----
7121
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
5.0
5.0
1
8/25/01
3:04
CHollingsw
601
7121
100.
1.0
100
8/27/01
21:23
CHollingsw
601
73
100.
1.0
100
8/27/01
21:23
CHollingsw
601
73
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:04
CHollingsw
601
7121
1.0
1.0
1
8/25/01
3:04,
CHollingsw
601
7121
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
107.
67.
- 135.
PID Surr., a,a,a-trifluorotoluene
89.
50.
- 150.
Hall Surr., 2-chloropropane
90.
50.
- 128.
Hall Surr., chloroprene
94.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
91.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
Sample report continued . . .
2960 FoSTF.R CREICHTON DRIVE; / NASHVILLR,TN 37204 / 615-726-0177 / Fx.e: 615-726-0954 / 800-765-0980

TestAmerica
I NCO RPORATED
ANALYTICAL REPORT
Laboratory Number: 01-A118377
Sample ID: MW5
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: L., JcJ Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical.Serv.
Johnny A. Mitchell, Dir. Technical Serv. ICelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical. Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / N,%siian,LE,TN 37204 / 615-726-0177 / F\.x: 615-726-0954 / 800-765-0980

I
I 1
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118376
KIM PRZYBYL Sample ID: MW6
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water
MORRISVILLE, NC 27560 Site ID:
Date
Collected:
8/22/01Time
Project: 107535-30205000
Collected:
9:30
Project Name: SLS-GREENSBORO
Date
Received:
8/23/01
Sampler: DAVID
Time
Received:
9:00
Report
Qua.
Dil
Analysis
Analysis
Analyte
Result
Units
Limit
Limit
Factor
DateTime
Analyst
Method
Batch
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
i
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Chlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
602/601
7121
1,2-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
602/601
7121
1,4-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
602/601
7121
-- Bromodichloromethane
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Bromoform
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
I ! Bromomethane
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/1
1.0
1.'0 '
1
8/25/01
2:22
CHollingsw
601
7121
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
2-Chloroeth lvin Tether
y y
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Chloroform
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Chloromethane
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Dibromochloromethane
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
j Vinyl chloride
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
_i Dichlorodifluoromethane
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
1,1-Dichloroethane
9.4
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
1,2-Dichloroethane
4.4
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
1,1-Dichloroethene
450.
ug/1
20.0
1.0
20
8/28/01
7:32
CHollingsw
601
73
cis-1,2-Dichloroethene.
6.5
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
trans-1,2-Dichloroethene
3.7
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
1,2-Dichloropropane
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
cis-1,3-Dichloropropene
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/1
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Methylene chloride
ND
ug/1
5.0
5.0
1
8/25/01
2:22
CHollingsw
601
7121
1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / !NASHVII,LEJN 37204 /.615-726-01,77 / F%x: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118376
Sample ID: MW6
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
----------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
Tetrachloroethene
166.
ug/l
-------
20.0
------
1.0
------
20
--------
8/28/01
------
7:32
-----------
CHollingsw
---------
601
-----
73
1,1,1-Trichloroethane
30.3
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
1,1,2-Trichloroethane.
9.0
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
Trichloroethene
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
TrichloroLuoromethane
ND
ug/l
1.0
1.0
1
8/25/01
2:22
CHollingsw
601
7121
ND — Not detected at the
report limit.
Surrogate % Recovery Target Range
I 1
PID Surr., a,a,a-trifluorotoluene 94. 50. - 150.
Hall Surr., 2-chloropropane 77. 50. - 128.
Hall Surr., chloroprene 77. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 106. 49. - 132.
— Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and -with
permission of the laboratory.
Report Approved By: k'-L4 ,,^ Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell., Dir. Technical Serv. ICelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
j End of Sample Report.
1 2960 FOSTER CREIGHTQ;N DRIVE / N,ks[iviu.E.TN 37204 / 615-726-0177 / F%x: 615-726-0954 / 800-765-0980

I
T � es� merica
I N C O R P O R A T E D
t �
r,
ANALYTICAL REPORT
I'
IT CORP-SEARS 2338 Lab Number: 01-A118383
" KIM PRZYBYL Sample ID: MW7
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water
MORRISVILLE, NC 27560 Site ID:
Date Collected: 8/22/01
Project: 107535-30205000 Time Collected: 14:30
Project Name: SLS-GREENSBORO Date Received: 8/23/01
Sampler: DAVID Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
I '------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
` Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Chlorobenzene
ND'
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
602/601
7121
1,2-Dichlorobenzene
ND'
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
602/601
7121
1,4-Dichlorobenzene
ND
ug/l
1..0
1.0
1
8/27/01
20:21
CHollingsw
602/601
7121
Bromodichloromethane
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Bromoform
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Bromomethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Chloroethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
" 2-Chloroethylvinylether
ND
ug/l
1.0
1,.0
1
8/27/01
20:21
CHollingsw
601
7121
Chloroform
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Chloromethane
ND
ug/1
i.v'
1.0
8/27/C1
20:21
C3oiiingsw
601
Dibromochloromethane
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
--' Dichlorodifluoromethane
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
1,1-Dichloroethane
1.2
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
1,1-Dichloroethene
2.0
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
cis-1,2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
trans-1,2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
1,2-Dichloropropane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
- cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
{ Methylene chloride
ND
ug/l
5.0
5.0
1
8/27/01
20:21
CHollingsw
601
7121
I 1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Sample report continued . . .
I
2960 FOSTER CREIGHTON DRIVE / NASIIVII,I,E,TN 37204 / 615-726-0177 / F%.r: 6.15-726-0954 / 800-765-0980

i
•
TestAmerica
INCO R P O RATED
ANALYTICAL REPORT
Laboratory Number: 01-A118383
Sample ID: MW7
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
Tetrachloroethene
25.8
ug/l
-------
1.0
------
1.0
------
1
--------
8/27/01
------
20:21
------------
CHollingsw
---------
601
-----
7121
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Trichloroethene
ND
ug/1
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
Trichlorofluoromethane
ND
ug/l
1.0
1.0
1
8/27/01
20:21
CHollingsw
601
7121
ND — Not detected at the
report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 94. 50. - 150.
Hall Surr., 2-chloropropane 80. 50. - 128.
Hall Surr., chloroprene 81. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 129. 49. - 132.
# — Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This.report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L.-Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREwtrro)l DRIVE / N:1SIfVII,I,E.TN 37204 / 615-726-0177 / Fir: 615-726-0954 / 800-765-0980

TestAmerica
INC O RPORATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
'I 2200-GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118640
Sample ID: MW9
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 18:40
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
_-,------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time-
------
Analyst
-----------
Method
---------
Batch
-----
- *VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
602/601
1249
1,2-Dichlorobenzene
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
602/601
1249
1,3-Dichlorobenzene
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
602/601
1249
1,4-Dichlorobenzene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
602/601
1249
Bromodichloromethane
i
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Bromoform
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Bromomethane
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Carbon tetrachloride
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Chloroethane
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
2-Chloroethylvinylether
NO
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Chloroform
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Chloromethane
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Dibromochloromethane
NO
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Ethylene Dibromide
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Vinyl chloride
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Dichlorodifluoromethane
I
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
1,1-Dichloroethane
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
1,2-Dichloroethane
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
j 1,1-Dichloroethene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
cis-1,2-Dichloroethene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
trans-1,2-Dichloroethene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
1,2-Dichloropropane
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
60.1
1249
cis-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
trans-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
_ Methylene chloride
ND
ug/l
5.00
5.00
1
8/31/01
9:20
CHollingsw
601
1249
1,1,2,2-Tetrachloroethane
ND
ug/1
1.00
1.00
1
8/31/01
9.20
CHollingsw
601
1249
' Tetrachloroethene
ND
ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Sample report continued . . .
2960 Fos,ri•:h Chi•:wirmn Dhni: / N�sm37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118640
Sample ID: MW9
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte Result Units
------------- ----------- -------
Limit
Limit
Factor Date
Time
Analyst
Method
Batch
1,1,1-Trichloroethene ND ug/1
-------
1.00
------
1.00
------
1
--------
8/31/01
------
9:20
-----------
CHollingsw
---------
601
-----
1249
i 1,1,2-Trichloroethane ND ug/l
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Trichloroethene ND ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
Trichlorofluoromethane ND ug/1
1.00
1.00
1
8/31/01
9:20
CHollingsw
601
1249
ND - Not detected at the report limit.
Surrogate % Recovery
------------- ----------
Target
------------
Range
PID Surr., a,a,a-trifluorotoluene
91.
50.
- 150.
Hall Surr., 2-chloropropane
96.
50.
- 128.
Hall Surr., chloroprene
90.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
84.
49.
- 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to
the items tested.
This report shall not be reproduced
except
in full and with
permission of the laboratory.
Report Approved By: Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fns•ri•:h Cki.:wirro% I)ki% / NAS11%11,1.F:,'rN 37204 / 615-726-0177 / F1\: 615-726-0954 / 800-765-0980

TestAmerica
I N C O -R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118375
Sample ID: MW10
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected: 8:55
Date Received: 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
----------------------------------- ------- ------- ------ -------------- ----------------- --------- -----
*ORGANIC PARAMETERS*
Benzene
Toluene
Ethylbenzene
Xylenes, total
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
j Bromodichloromethane
Bromoform
Bromome thane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
Sample report continued
1.70
ug/1
1.00
1.00
1
8/26/01
17:28
D.Ramey
602
7282
ND
ug/l
1.00
1.00
1
8/26/01
17:28
D.Ramey
602
7282
ND
ug/1
1.00
1.00
1
8/26/01
17:28
D.Ramey
602
7282
ND
ug/1
1.00
1.00
1
8/26/01
17:28
D.Ramey
602
7282
ND
ug/1
1.0
1.0
1
8/25/01
1:40
_CHollingsw
601
7121
ND
ug/1
200.
1.0
200
8/27/01
22:04
CHollingsw
602/601
73
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
_8/25/O1
1:40
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/l
200.
2.0
200
8/27/01
22:04
CHollingsw
601
73
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
5.5
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
200.
1.0
200
8/27/01
22:04
CHollingsw
601
73
ND
ug/l
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
8.0
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
11.6
ug/1
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
2960 FOSTER CREI(iHT(IN DRIVE / NASHVILLEJN 37204 / 615-726-0177 / Fps: 61.5-726-0954 / 800-765-0980

Ii-
I � •
T TestAmerica
jI N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
trans-1,2-Dichloroethene
ND
ug/1
1,2-Dichloropropane
ND
ug/1
cis-1,3-Dichloropropene
ND
ug/l
trans-1,3-Dichloropropene
ND
ug/l
Methylene chloride
ND
ug/l
1.1,2,2-Tetrachloroethane
ND
ug/l
Tetrachloroethene
16800
ug/l
1,1,1-Trichloroethane
ND
ug/1
1,1,2-Trichloroethane
24.4
ug/1
Trichloroethene
30.6
ug/1
Trichlorofluoromethane
ND
ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118375
Sample ID: MW10
Project: 107535-30205000
Page 2
0
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.0
1.0
------
1
--------
8/25/01
------
1:40
-----------
CHollingsw
---------
601
-----
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
5.0
5.0
1
8/25/01
1:40
CHollingsw
601
7121
200.
1.0
200
8/27/01
22:04
CHollingsw
601
73
200.
1.0
200
8/27/01
22:04
CHollingsw
601
73
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7121
1.0
1.0
1
8/25/01
1:40
CHollingsw
601
7.121
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
105.
67.
- 135.
PID Surr., a,a,a-trifluorotoluene
89.
50.
- 150.
Hall Surr., 2-chloropropane
91.
50.
- 128.
Hall Surr., chloroprene
90.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
98.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
Sample report continued . . .
2960 Fos-rER CRE6(;HT0\ DRIVE. / N:\siivnJ,E.TN 37204 / 615-726-0177 / F.�.x: 615-726-0954 / 800-765-0980

TestAmeric'a
I N C 0 R P 0 R A T E 0
ANALYTICAL REPORT
Laboratory Number: 01-A118375
Sample ID: MW10
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: IL �.r�tJ`� Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report..
2960 FOSTER CREIGHTON DRIVF7 / NASHVII,LEJN 37204 / 615-726-0177 / F.\.x: 615-726-0954 / 800-765-0980

i
TestAmerica
I N t O R P 0 R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
- MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118633
Sample ID: MW12
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 13:35
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND.
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Bromoform
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Bromomethane
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Chloroethane
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Chloroform
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Chloromethane
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
1.00
1.00
1
9/
1/01
18.17
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw.
601
1248
1,2-Dichloroethane
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
cis-1,2-Dichloroethene
5.20
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248,
trans-1,2-Dichloroethene
ND
ug/l
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
1,2-Dichloropropane
60.0
ug/l
50.0
1.00
50
9/
1/01
7:13
CHollingsw
601
3658
cis-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Methylene chloride
ND
ug/l
5.00
5.00
1
9/.1/01
18:17
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Tetrachloroethene
7.70
ug/1
1.00
1.00
1
9/
1/01
18:17
CHollingsw
601
1248
Sample report continued . . .
2960 Fus•rr:k Chr:icirron Dkn'i-: / NASHNIi,i.H,JN 37204 / 615-726-0177 / Fix: 615-726-0954 / 800-765-0980

TestLmerica
I N C 0 R F 0 R A T E D
ANALYTICAL REPORT
Analyte
Result
Units
------------------------
1,1,1-Trichloroethane
-----------
ND
-------
ug/1
1,1,2-Trichloroethane
ND
ug/l
Trichloroethene
5.20
ug/l
Trichlorofluoromethane
ND
ug/1
-" ND - Not detected at the
report limit.
Surrogate
-------------
Laboratory Number: 01-A118633
Sample ID: MW12
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.00
1.00
------
1
--------
9/ 1/01
------
18:17
-----------
CHollingsw
---------
601
-----
1248
1.00
1.00
1
9/ 1/01
18:17
CHollingsw
601
1248
1.00
1.00
1
9/ 1/01
18:17
CHollingsw
601
1248
1.00
1.00
1
9/ 1/01
18:17
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 87. 50. - 128.
Hall Surr.., chloroprene 86. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 80. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: (,� :-u�� Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
'( Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director. Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
-, End of Sample Report.
I
?96(1 Fos•n-:R CRI-:wn•run Dkm-i•: / N:%smim,i;.TN 37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

•
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
i_7 IT CORP-SEARS 2338
KIM PRZYBYL
- 2200 GATEWAY CTR. BLVD. STE205
_ MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118627
Sample ID: MW13
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 10:25
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
. Analysis
Analysis
- Analyte
_------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
I` *VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
.602/601
1248
1,2-Dichlorobenzene
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
602/601
1248
- 1,4-Dichlorobenzene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
I Bromoform
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Bromomethane
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Chloroethane
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Chloroform
ND
ug/l
-1-.-00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
- Chloromethane
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
- Ethylene Dibromide
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
1.00
1.00
1
9/ 1/01
17.35
CHollingsw
601,
1248
i Dichlorodifluoromethane
ND
ug/1
1.00.
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
- 1,1-Dichloroethene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
_ trans-1,2-Dichloroethene
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
-_ trans-1,3-Dichloropropene
ND
ug/l
-1-:00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Methylene chloride
ND
ug/1
5.00
5.00
1
9/ 1/01
17:35
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Tetrachloroethene
ND
ug/1
1.00
1.00
1
9/ 1/01
17:35
CHollingsw
601
1248
Sample report continued . . .
2960 Fos-n-;R Ch1:IC11'1'0N Dwu / NAS11%11.1.E.TN 37204 / 615-726-0177 / FAX: [phone]

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR
MORRISVILLE, NC
BLVD. STE205
27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118636
Sample ID: MW15
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 15:50
Date Received: 8/22/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ------------------------- ------ -------------- -------------------------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chlorcethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene.
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1.2,2-Tetrachloroethane
Tetrachloroethene
__ Sample report continued . . .
i
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
602/601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
602/601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
602/601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
602/601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
25.0
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
22.0
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/1
50.0
5.00
10
8/31/01
12:04
CHollingsw
601
1249
ND
ug/l
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
11.0
ug/1
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
2960 Fos-n--'k CREIGHTON DRi%E / NAs11%11,1.E.TN 37204 / 615-726-01 77 / F�\: 615-726-0954 / 800-765-0980

f�l
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene 345. ug/l
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118636
Sample ID: MW15
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
10.0
1.00
------
10
--------
8/31/01
------
12:04
-----------
CHollingsw
---------
601
-----
1249
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
10.0
1.00
10
8/31/01
12:04
CHollingsw
601
1249
% Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 94. 50. - 128.
Hall Surr., chloroprene 83. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 94. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in.full and with
permission of the laboratory.
Report Approved By: u �,� —t-4� Report Date: 9/ 4/01
r,
I ,
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
I
2960 Fos-rH:h Chiaciriw\ DRnr: / NAS11%11,1.E,TN 37204 / 615-726-0177 / F\..: 615-726-095.1 / 800-765-0980

TestAmerica
I
i
-' ANALYTICAL REPORT
i
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUB ELL
I N C O R P O R A T E D
Lab Number: 01-A118629
Sample ID: MW17
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01-
Time Collected: 11:20
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
' Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
i
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
602/601
1248
i 1,2-Dichlorobenzene
ND.
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Bromoform
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Bromomethane
ND'
ug/l
50.0
1.00.
50
9/ 1/01
4:25
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Chloroethane 11
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Chloroform
55.0
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
- Chloromethane
ND
ug/1
50.0
1.00
50
9/ 1/01
4.25
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
- Ethylene Dibromide
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
cis-1,2-Dichloroethene
`
165.
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/1
50.0
1.00
50
9/ 1/01
4.25
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
--' trans-1,3-Dichloropropene
ND
ug/1
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Methylene chloride._
ND
ug/l
250.
5.00
50
9/ 1/01
4:25
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Tetrachloroethee
2340
ug/l
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Sample report continued .
I
l
2960 FOSTER CRI-IGIFI.ON
DKnis / NAs11%11,1'1-.JN
37204 / 615-726-0177
/
F\x: 615-726-0954
/ 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyze Result Units
1,1,1-Trichloroethane ND ug/1
1,1,2-Trichloroethane ND ug/1
Trichloroethene 555. ug/l
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118629
Sample ID: MW17
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
50.0
1.00
------
50
--------
9/ 1/01
------
4:25
-----------
CHollingsw
---------
601
-----
1248
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
50.0
1.00
50
9/ 1/01
4:25
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 92. 50. - 128.
Hall Surr., chloroprene 82. 55. - 123:
Hall Surr., 1-chloro-3-fluorobenzene 123. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: "t1_114 :; , mac/ Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fos'n-:h Chr!G!rrun DRii / !NAsutn.!,F:.TN 37204 / 615-726-01 77 / F%-\: 615-726-0954 / 800-765-0980

Test'= merica
I N C O R P O R A T E D
i
�---' ANALYTICAL REPORT
r IT CORP-SEARS 2338
KIM PRZYBYL
-' 2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
�1
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118630
Sample ID: DUP01
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected:
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND.
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND.
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND-
ug/1
50.0
1.00
50
9/ 1/01,
5:07
CHollingsw
602/601
1248
Bromodichloromethane
ND.
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
' Bromoform
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
--' Bromomethane
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
50.0
1.00
50
9/ 1/01
5.07
CHollingsw
601
1248
Chloroethane
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
2-Chlorcethylvinylether
ND
ug/l
50.0
1.00
50
9/ 1/01
5.07
CHollingsw
601
1248
Chloroform
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Chloromethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
- 1,1-Dichloroethene
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
cis-1,2-Dichloroethene
155.
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
--- 1,2-Dichloropropane
ND
ug/1
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
trans-1.3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Methylene chloride
ND
ug/l
250.
5.00
50
9/ 1/01
5:07
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Tetrachloroethene
2480
ug/l
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Sample report continued . . .
1 r 2960 Fus•m.:R Chi.:wirro,, Nivi, / NAS]k 11.1,E,TN ;37204 / 615-726-0177 / FAQ: 615-726-0954 / 800-765-0980

it TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/1
1,1,2-Trichloroethane ND ug/l
Trichloroethene 610. ug/1
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118630
Sample ID: DUP01
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
50.0
------
1.00
------
50
--------
9/ 1/01
------
5:07
-----------
CHollingsw
---------
601
-----
1248
50.0
1.00
50
9/ 1/O1
5:07
CHollingsw
-601
1248
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
50.0
1.00
50
9/ 1/01
5:07
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 89. 50. - 128.
Hall Surr., chloroprene 80. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 125. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: L &L Report Dater 9/ 4/01
I
�. Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
- Laboratory Certification Number: 387
i
End of Sample Report.
2960 Fos-ri•:R CRi-:ic;irron DRIVE / NAstnn,i,t:.TN 37204 i 615-726-01 1 7 / F:%x: 615-726-095 4 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
IT CORP-SEARS 2338
ICIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Lab Number: 01-A118632
Sample ID: MW18
Sample Type: Ground water
Site ID:
Date
Collected:
8/21/01
Project: 107535
Time
Collected:
13:10
Project Name: SLS-GREENSBORO
Date
Received:
8/22/01
Sampler: DAVID LUBELL
Time
Received:
9:00
Report Quan Dil
Analysis Analysis
Analyte Result Units
------------------------ ------------------
Limit Limit Factor
------- ------ ------
Date Time
-------- ------
Analyst Method Batch
----------- --------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Bromoform
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Bromomethane
ND
ug/1
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Chloroethane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Chloroform
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Chloromethane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/1
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
50.0
1.00
50
9/
1/01
6.31
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/1
50.0
1.00
50
9/
1/01
6.31
CHollingsw
601
1248
1.2-Dichloroethane
ND
ug/l
50.0
1.00
50
9/
1/01
6.31
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/1
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Methylene chloride
ND
ug/1
250.
5.00
50
9/
1/01
6:31
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Tetrachloroethene
940.
ug/l
50.0
1.00
50
9/
1/01
6:31
CHollingsw
601
1248
Sample report continued . . .
2960 Fus•n•:R Chra(;wron DRIVE / N:�smII.i.E,TN '37204 / 615-726-0177 / F %\: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene ND ug/1
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118632
Sample ID: MW18
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
50.0
1.00
------
50
--------
9/ 1/01
------
6:31
-----------
CHollingsw
---------
601
-----
1248
50.0
1.00
50
9/ 1/01
6:31
CHollingsw
601
1248
50.0
1.00
50
9/ 1/01
6:31
CHollingsw
601
1248
50.0
1.00
50
9/ 1/01
6:31
CHollingsw
601
1248
% Recovery Target Range
IN
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 88. 50. - 128.
Hall Surr., chloroprene 86. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 105. 49. - 132.
# - Recovery outside Laboratory, historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
! Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fos•rE:c: Cc Eacu'ron DRIVE, / NA811%11,1,E.I'N 37204 / 615-726-0177 / F": 615-726-0951 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
I'- ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118623
KIM PRZYBYL Sample ID: MWIf
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water
MORRISVILLE, NC 27560 Site ID:
Date Collected: 8/20/01
Project: 107535 Time Collected: 18:22
Project Name: SLS-GREENSBORO Date Received: 8/22/01
Sampler: DAVID LUBELL Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Bromoform
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Bromomethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Chloroethane
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Chloroform
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Chloromethane
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/1
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Methylene chloride
ND
ug/l
250.
5.00
50
8/31/01
22:49
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Tetrachloroethene
1790
ug/l
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Sample report.continued . . .
2960 Fos,n.'R (;hh:ICI[TON DRivi•: / -XAS1 1,1,E.TN 37204 / 615-726-0177 / Fx%: 615-726-0954 / 800-765-0980

TestAmeric'a
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene 180. ug/1
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118623
Sample ID: MW� r`i w — z Z
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
50.0
1.00
------
50
--------
8/31/01
------
22:49
-----------
CHollingsw
---------
601
-----
1248
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
50.0
1.00
50
8/31/01
22:49
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 95. 50. - 128.
Hall Surr., chloroprene 83. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 118. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: cci� %1 -,iyt� Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fo s-rl•:h Ckr!(,u-roN Nivi•: / !NAain!m.H:.TN 37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

i rl �
- Testy= me ca
I NCORPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118620
Sample ID: MW23
Sample Type: Ground water
Site ID:
Date Collected: 8/20/01
Time Collected: 16:20
Date Received: 8/22/01
Time Received: 9:00,
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ------------------------- ------ -------------- -------------------------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
j 2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
I! Tetrachloroethene
i Sample report continued .
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
602/601
1248
ND'
ug/1
1.00
1.00
1
9/
1/01
11:24
CHollingsw
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
.1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/1
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/1
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
5.00
5.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
11:24
CHollingsw
601
1248
2960 Fus•rr;k Dwn r: / NASIII ILLE.,rN 37204 / Ei 15-726-0177 / F %\: 615-726-09':34 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene ND ug/1
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118620
Sample ID: MW23
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
- ------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.00
1.00
------
1
--------
9/ 1/01
------
11:24
-----------
CHollingsw
---------
601
-----
1248
1.00
1.00
1
9/ 1/01
11:24
CHollingsw
601•,
1248
1.00
1.00
1
9/ 1/01
11:24
CHollingsw
601
1248
1.00
1.00
1
9/ 1/01
11:24
CHollingsw
601
1248
Recovery Target Range
j PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 88. 50. - 128.
Hall Surr., chloroprene 90. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 83. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
I These results relate only to the items tested.
i-' This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: :,,t,rc.l o - -(-G� Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
+ Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fu,n•:k Chi•:i(m-i-oN llRno-: / N:\aII im,P.JN 37204 / 615-726-0177 / F'%\: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118385
Sample ID: MW27
Sample Type: Water
Site ID:
Date Collected: 8/22/01Time Collected: 15:15
Date Received: 8/23/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
---------------
--Result
------
Units-
------
Limit
-------
Limit
------
Factor
------
Date
--------
-Time-
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Chlorobenzene
ND
ug/1
1.0
1.0
1
8/25/01
10:03
CHollingsw
602/601
7121
1,2-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
602/601
7121
1,4-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
602/601
7121
Bromodichloromethane
ND'
ug/l
10.0
1.0
10
8/28/01
5:26
CHollingsw
601
73
Bromoform
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Bromomethane
ND
ug/l
1.0
1.0
1
8/25/01'
10:03
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Chloroethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Chloroform
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Chloromethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Dibromochloromethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Vinyl chloride
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
1,2-Dichloroethane
III
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
1,1-Dichloroethene
1.7
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
cis-1,2-Dichloroethene
527.
ug/l
10.0
1.0
10
8/28/01
5:26
CHollingsw
601
73
trans-1.2-Dichloroethene
ND
ug/1
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
• 1,2-Dichloropropane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
cis-1,3-Dichloropropene
ND
ug/1
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Methylene chloride
ND
ug/l
5.0
5.0
1
8/25/01
10:03
CHollingsw
601
7121
•_ 1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / NASHVILI.E.TN 37204 / 615-726-0177 / F.x.r: 615-726-095 4 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118385
Sample ID: MW27
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
-----------------------
Result
-----------
Units
-------
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
Tetrachloroethene
ND
ug/1
10.0
------
1.0
------
10
--------
8/28/01
------
5:26
-----------
CHollingsw
--------=
601
-----
73
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/l
.1.0
1.0
1
8/25/01
10:03'
CHollingsw
601
7121
Trichloroethene
442.
ug/1
10.0
1.0
10
8/28/01
5:26
CHollingsw
601
73
Trichlorofluoromethane
ND
ug/1
1.0
1.0
1
8/25/01
10:03
CHollingsw
601
7121
ND - Not detected at the
report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 93. 50. - 150.
Hall Surr., 2-chloropropane- 87. 50. - 128.
Hall Surr., chloro rene
P 76. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 95. 49. - 132.
- Recovery outside Laboratory historical or method prescribed limits.
i
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
j Report Approved By: G�•c., ,� Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
I; End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / NASIIVII,I.E.TN 37204 / 615-726-0177 / Fx.e: 615-726-0954 / 800-765-0980

i I
TestAmerica
I NCO RPORATEO
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118384
Sample ID: MW28
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected: 14:45
Date Received: 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ------------------ ------- ------ -------------- ----------------- --------- -----
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
- Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethend
II 1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Sample report continued . . .
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
602/601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
602/601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
602/601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND'
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
12.5
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
583.
ug/l
10.0
1.0
10
8/28/01
4:44
CHollingsw
601
73
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
5.0
5.0
1
8/25/01
9:21
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
0
i 1 2960 FOSTER CREIGHTON DRIVE / N:\SHVH.LEJN 37204 / 615-726-0177 / Fx,t: 615-726-0954 / 800-765-0980

7 TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118384
Sample ID: MW28
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
Tetrachloroethene
ND
ug/l
-------
10.0
------
1.0
------
10
--------
8/28/01
------
4:44
-----------
CHollingsw
---------
601
-----
73
1,1,1-Trichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
Trichloroethee
134.
ug/l
10.0
1.0
10
8/28/01
4:44
CHollingsw
601
73
Trichlorofluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
9:21
CHollingsw
601
7121
ND — Not detected at the
report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 94. 50. - 150.
Hall Surr., 2-chloropropane 88. 50. - 128.
Hall Surr., chloroprene 74. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 95. 49. - 132.
# — Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
! Report Approved By: Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
1' End of Sample Report.
2960 FoSTF.R CREIGHTON DRIVR / N:ismi1,1.e.TN 37204 / 615-726-0177 / Fk.r: 615-726-0954 / 800-765-0980

Test= merica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number: 01-A118639
ICIM PRZYBYL
Sample ID: LMP1
2200 GATEWAY CTR. BLVD. STE205
Sample Type: Ground water
MORRISVILLE, NC 27560
Site ID:
Date Collected: 8/21/01
Project: 107535
Time Collected: 18:00
-, Project Name: SLS-GREENSBORO
Date Received: 8/22/01
Sampler: DAVID LUBELL
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
602/601
1249
1,2-Dichlorobenzene
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
602/601
1249
1,3-Dichlorobenzene
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
602/601
1249
1,4-Dichlorobenzene
ND
ug/1
10.0
1.00
10
8/31/61
16:57
CHollingsw
602/601
1249
Bromodichloromethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Bromoform
ND
ug/l
10.0
.1.00
10
8/31/01
16:57
CHollingsw,
601
1249
Bromomethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Carbon tetrachloride
ND
ug/l
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Chloroethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
2-Chloroethylvinylether
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Chloroform
11.0
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Chloromethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Dibromochloromethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Ethylene Dibromide
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Vinyl chloride
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Dichlorodifluoromethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
1,1-Dichloroethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
1,2-Dichloroethane
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
1,1-Dichloroethene
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
cis-1,2-Dichloroethene
65.0
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
trans-1,2-Dichloroethene
ND
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
1,2-Dichloropropane
595.
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
cis-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
trans-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Methylene chloride
ND
ug/l
50.0
5.00
10
8/31/01
16:57
CHollingsw
601
1249
1,1,2,2-Tetrachloroethane
ND
ug/l
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Tetrachloroethene
81.0
ug/1
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Sample report continued . . .
2960 Fus'rt-:h Chiacinn% Dhnr / N:\simi.i,F:.TN 37204 / 615-726-0177 / F\.X: 615-726-0954 / 800-765-0980

T •
estt merlca
I N C O R F O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene 67.0 ug/1
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118639
Sample ID: LMP1
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
10.0
1.00
------
10
--------
8/31/01
------
16:57
-----------
CHollingsw
---------
601
1249
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
10.0
1.00
10
8/31/01
16:57
CHollingsw
601
1249
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 98. 50. - 128.
Hall Surr., chloroprene 85. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 105. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: U,«F L Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fos'I'h:R DRiri•: / N\sn%'n.m--..'1'\ 37204 / 615-726-0177 / F�\: (;15-726-0954 / 800-765-09f3O

TestAmerica
ANALYTICAL REPORT
-- IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC '27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118635
Sample ID: LMP2
Sample Type: Ground water
Site ID:
Date Collected: 8/21/0,1
Time Collected: 14:50
Date Received: 8/22/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- ------- ------- ------ --- /---------- ------ -------------------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1.1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Sample report continued . . .
ND
ug/1
1.00
1.00
1
9/
1/01
18:59
CHollingsw.
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw,
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
602/601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/1
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248 -
1.70
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/1
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
13.8
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
250.
ug/l
50.0
1.00
50
9/
1/01
8:36
CHollingsw
601
3658
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
5.00
5.00
1
9/
1/01
18:59
CHollingsw
601
1248
ND
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
51.8
ug/l
1.00
1.00
1
9/
1/01
18:59
CHollingsw
601
1248
21)(30 Fos-ri.:R (:Rr.wirrox Dhnr. / NAs11%11.1,E:.TN 37204 / 615-726-0177 / F\%: 615-726-0954 / 800-765-0980

Testl�merica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/1
Trichloroethene 6.90 ug/l
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118635
Sample ID: LMP2
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.00
1.00
------
1
--------
9/ 1/01
------
18:59
-----------
CHollingsw
---------
601
-----
1248
1.00
1.00
1
9/ 1/01
18:59
CHollingsw
601
1248
1.00
1.00
1
9/ 1/01
18:59
CHollingsw
601
1248
1.00
1.00
1
9/ 1/01
18:59
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 92. 50. - 128.
-- Hall Surr., chloroprene 81. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 86. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: h.�.t/Z�-�.vt�� Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L'. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fos'rr:k DRIVE / N:%sn1u.i.E,TN 37204 / 615-726-0177 / FN\: 61:5-726-0954 / 800-765-0980

i .
1C.1-stAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118380
Sample ID: DW3
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected: 11:45
Date Received: 8/23/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
----=-
Analyst
-----------
Method.
---------
Batch
-----
*ORGANIC PARAMETERS*
Benzene
3.20
ug/1
1.00
1.00
1
8/26/01
20:30
D.Ramey
602
7282
Toluene
11.0
ug/l
1.00
1.00
1
8/26/01
20:30
D.Ramey
602
7282
Ethylbenzene
ND
ug/1
1.00
1.00
1
8/26/01
20:30
D.Ramey
602
7282
Xylenes, total
ND
ug/1
1.00
1.00
1
8/26/01
20:30
D.Ramey
602
7282
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Chlorobenzene
ND
ug/1
500.
1.0
500
8/28/01
0:07
CHollingsw
602/601
73
1,2-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/28/01
0:07
CHollingsw
602/601
73
1,3-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/28/01
0:07
CHollingsw
602/601
73
1,4-Dichlorobenzene
ND
ug/1
500.
1.0
500
8/28/01
0:07
CHollingsw
602/601
73
Bromodichloromethane
ND
ug/l
1.0
1.0
1'
8/25/01
6:34
CHollingsw
601
7121
Bromoform
i+D
ug/1
500.
2.0
500
8/28/01
0:07
CHollingsw
601
73
Bromomethane
ND'
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Chloroethane
ND
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Chloroform
4.5
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Chloromethane
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Dibromochloromethane
ND
ug/l
500.
1.0
5.00
8/28/01
0:07
CHollingsw
601
73
Vinyl chloride
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
1,1-Dichloroethene
1.7
ug/l
1.0
1.0
1
8/25/0C
6:34
CHollingsw
601
7121
cis-1,2-Dichloroethene
6.4
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
�,- Sample report continued . . .
2960 FOSTER CREIGHTO:N DRIVE / NA5HVILLE.TN 37204 / 615-726-0177 / Fm 615-726-0954 / 800-765-0980
-I

r TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118380
Sample ID: DW3
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
trans-1,2-Dichloroethene
ND
ug/1
-------
1.0
------
1.0
------
1
--------
8/25/01
------
6:34
-----------
CHollingsw
---------
601
-----
7121
1,2-Dichloropropane
ND
ug/1
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Methylene chloride
ND
ug/l
2500
5.0
500
8/28/01
0:07
CHollingsw
601
73
1,1,2,2-Tetrachloroethane
ND
ug/1
500.
1.0
500
8/28/01
0:07
CHollingsw
601
73
Tetrachloroethene
62000
ug/l
5000
1.0
5000
8/28/01
14:50
CHollingsw
601
91
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
1,1,2-Trichloroethane
22.3
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Trichloroethene
19.5
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
Trichlorofluoromethane
ND
ug/l
1.0
1.0
1
8/25/01
6:34
CHollingsw
601
7121
ND - Not detected at the
report limit.
Surrogate
-------------
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
132.
67.
- 135.
PID Surr., a, a, a- tri fluoro toluene
95.
50.
- 150.
Hall Surr., 2-chloropropane
85.
50.
- 128.
Hall Surr., chloroprene
84.
55.
- 123.
flail Surr., 1-chloro-3-fluorobenzene
117.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
I
Sample report continued . . .
2960 FOSTF,R CREV;t(TON Dm-F, / N:1sKILLE.TN 37204 / 615-726-0177 / F\.x: 615-726-0954 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
l'
L_
ANALYTICAL REPORT
f
Laboratory Number: 01-A118380
Sample ID: DW3
Project: 107535-30205000
Page 3
-- These results' relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: tr,��L <.�c� Report Date: 8/28/01
Paul E. Lane, Jr.,, Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
J
J
i_
r End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / NASIIVILI.E,TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118372
Sample ID: DW4
Sample Type: Water
Site ID:
Date Collected: 8/22/01
Time Collected: 10:20
Date Received: 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- -------------- ------ ------ -------- ----------------- --------- -----
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Chlorobenzene
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
602/601
7121
1,2-Dichlorobenzene
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
602/601
7121
1,3-Dichlorobenzene
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
602/601
7121
1,4-Dichlorobenzene
ND.
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
602/601
7121
Bromodichloromethane
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Bromoform
ND
ug/1
500.
2.0
500
8/24/01
23:33
CHollingsw
601
7121
Bromomethane
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Carbon tetrachloride
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Chloroethane
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
2-Chloroethylvinylether
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Chloroform .
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Chloromethane
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Dibromochloromethane
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Vinyl chloride
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Dichlorodifluoromethane
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
1,1-Dichloroethane
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
1,2-Dichloroethane
ND
ug/1,
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
1,1-Dichloroethene
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
cis-1,2-Dichloroethene
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
trans-1,2-Dichloroethene
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
1,2-Dichloropropane
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
cis-1,3-Dichloropropene
ND
ug/1
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
trans-1,3-Dichloropropene
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Methylene chloride
ND
ug/l
2500
5.0
500
8/24/01
23:33
CHollingsw
601
7121
1,1,2,2-Tetrachloroethane
ND
ug/l
500.
1.0
500
8/24/01
23:33
CHollingsw
601
7121
Sample report continued
2960 Fos•rER CREI(;H'rON DRIVE / NASIIVILLE,TN 37204 / 615-726-0177 / F:xx: 615-726-095=4 / 800-765-0980

Analyte
------------------------
Tetrachloroethene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
TestAmerica
ANALYTICAL REPORT
Result
Units
-----------
ND
-------
ug/l
ND
ug/l
ND
ug/l
ND
ug/l
ND
ug/1
I N C O R P O R A T E D
Laboratory Number: 01-A118372
Sample ID: DW4
Project: 107535-30205000
Page 2
Report Quan Dil
Limit Limit Factor
------- ------ ------
500. 1.0 500
500. 1.0 500
500. 1.0 500
500. 1.0 500
500. 1.0 500
Volatile 601 report limit elevated due to sample matrix.
ND — Not detected at the report, limit.
Surrogate
-------------
Analysis
Analysis
Date
--------
Time
Analyst
Method
Batch
8/24/01
------
23:33
-----------
CHollingsw
---------
601
-----
7121
8/24/01
23:33
CHollingsw
601
7121
8/24/01
23:33
CHollingsw
601
7121
8/24/01
23:33
CHollingsw
601
7121
8/24/01
23:33
CHollingsw
601
7121
Recovery Target Range
-- PID Surr., a,a,a-trifluorotoluene 93. 50. - 150. l
Hall Surr., 2-chloropropane 92. 50. - 128.
Hall Surr., chloroprene 88. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 82. 49. - 132.
— Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: kt. k
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
Report Date: 8/28/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
ICelly S. Comstock, Technical Serv:
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FII5TER CREW11TON DRIVE / NASIIVILI.E,TN 37204 / 615-726-0177 / Fix: 615-726-0954 / 800-765-0980

TestAmerica
O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118637
Sample ID: DW5
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 16:30
Date Received: 8/22/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- -------------- ------ -------------- ------ -------------------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1 ' 1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
- Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
jDibromochloromethane
-_ Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1.2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
- trans-1,3-Dichloropropene
Methylerie chloride
1,1,2,2-Tetrachloroethane
1
Tetrachloroethene
r- Sample report continued . . .
ND ug/l
50.0
1.00
50
8/30/01
21:26
CHollingsw
602/601
1249
ND ug/l
50.0
1.00
50
8/30/01
21:26
CHollingsw
602/601
1249
ND ug/l
50.0
1.00
50
8/30/01
21:26
CHollingsw
602/601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
602/601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND" ug/l
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26.
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
14D ug/1
250.
5.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
ND ug/1
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
2960 Fos•ri•:k (M-:ir,irroN DRu i.: / N ism n,u.:.TN 37204 / 615-726-0177 / F\\: 615- i 26-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/1
Trichloroethene 655. ug/1
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118637
Sample ID: DW5
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
50.0
------
1.00
------
50
--------
8/30/01
------
21:26
-----------
CHollingsw
---------
601
-----
1249
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
50.0
1.00
50
8/30/01
21:26
CHollingsw
601
1249
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 90. 50. - 150.
Hall Surr., 2-chloropropane 100. 50. - 128.
Hall Surr., chloroprene 85. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 92. 49. - 132.
# - Recovery outside Laboratory, historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: _ rL4,-�l ti � Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
j 2960 Fos•ri,-,R Cn --wi •rm, Dm r: / 1 %sup n,1.E.'rn 37204 / 615-726-0177 / F.\x: 615-726-0954 / 800-765-0980

TestAmerica
t I N C O R P O R A T E D
I
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118634
Sample ID: DW7
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 14:40
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Bromoform
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Bromomethane
ND'
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Chloroethane
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Chloroform
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Chloromethane
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
_. yl chloride
iau
ug/1
-0
i.00
5
c/
2/01
0:35
CHollingsw
61:
1248
Dichlorodifluoromethane
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/1
5.00
1.00
5
9/
2/01
0.35
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Methylene chloride
ND
ug/l
25.0
5.00
5
9/
2/01
0:35
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
Tetrachloroethene
226.
ug/1
5.00
1.00
5
9/
2/01
0:35
CHollingsw
601
1248
- Sample report continued . . .
2960 Fus•n•:h Cni•:ir,irrox Dhn r: / \ �:n1 n.i,r:.TN 37204 / 615-126-0177 / F\\: 6l 5-726-0954 / 800-765-0980

r
I
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1.1,2-Trichloroethane ND ug/l
Trichloroethene ND ug/l
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118634
Sample ID: DW7
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
5.00
------
1.00
------
5
--------
9/ 2/01
------
0:35
-----------
CHollingsw
---------
601
-----
1248
5.00
1.00
5
9/ 2/01
0:35
CHollingsw
601
1248
5.00
1.00
5
9/ 2/01
0:35
CHollingsw
601
1248
5.00
1.00
5
9/ 2/01
0:35
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 102. 50. - 128.
Hall Surr., chloroprene 97. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 131. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: h vj� ate/ Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
_- Laboratory Certification Number: 387
End of Sample Report.
i
2960 Fus,rF:h CREICHTON Niii.: / N:vsm 11,i.F:.'rN 37204 / 615-726-0177 / F.\x: 615-726-0954 / 800-765-0980
i

TestAmerica
INC ORPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118628
KIM PRZYBYL Sample ID: DW8
- 2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water
MORRISVILLE, NC 27560 Site ID:
Date Collected: 8/21/01
Project: 107535 Time Collected: 10:55
Project Name: SLS-GREENSBORO Date Received: 8/22/01
Sampler: DAVID LUBELL _ Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Bromoform
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
- Bromomethane
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Chloroethane
ND
ug/l
50.0
1.00
.50
9/
1/01
3:43
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Chloroform
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Chloromethane
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
50.0
1.00
50
9/
1/01
303
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
50.0
1.00
50
9/
1/01
3.43
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
.1248
1248
trans-1,3-Dichloropropene
ND
ug/l
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Methylene chloride
ND
ug/1
250.
5.00.
50
9/
1/01
3:43
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Tetrachloroethene
1100
ug/1
50.0
1.00
50
9/
1/01
3:43
CHollingsw
601
1248
Sample report continued . . .
2960 Fus•rr,tz I)Rwi•., / NAsInN,i,F,.TN 37204 ; 615-726-0177 / F:\x: 615-726-0954 / 800-765-0980
l

I /
e
Test: m r
Ica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A118628
Sample ID: DW8
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Esalyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
1,1,1-Trichloroethane
ND
ug/1
-------
50.0
------
1.00
------
50
--------
9/ 1/01
------
3:43
-----------
CHollingsw
---------
601
-----
1248
1,1,2-Trichloroethane
ND
ug/1
50.0
1.00
50
9/ 1/01
3:43
CHollingsw
601
1248
Trichloroethene
ND
ug/1
50.0
1.00
50
9/ 1/01
3:43
CHollingsw
601
1248
Trichlorofluoromethane
ND
ug/1
50.0
1.00
50
9/ 1/01
3:43
CHollingsw
601
1248
ND - Not detected at the report limit.
Surrogate % Recovery Target Range
-----------------------------------
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 91. 50. - 128.
Hall Surr., chloroprene 87. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 109. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be --reproduced except in full and with
permission of the laboratory.
Report Approved By: u Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fus•ri;R Dki%i•; / Ms11V11,1,@.TN 37204 / 615-726-0177 / Fax: [phone]

TestAmerica
I N C O R P D R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
ICIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118625
Sample ID: DW13
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 8:30
Date Received: 8/22/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ------------------ ------- ------ -------------- ------ -------------------- -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Bromoform
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Bromomethane
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Chloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Chloroform
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Chloromethane
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
I- 1,1-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248,
trans-1,2-Dichloroethene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
_ 1,2-Dichloropropane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
it cis-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Methylene chloride
ND
ug/1
50.0
5.00
10
9/
1/01
21:05
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Tetrachloroethene
447.
ug/1
10.0
1.00
10
9/
1/01
21:05
CHollingsw
601
1248
Sample report continued . . .
I " 12960. Fus•ri•:h CREIGii ru'N DRi r: / N.\sm n.u-:.TN 37204 / 615-726-017 7 / FAX: [phone]

TestAmerica
ANALYTICAL REPORT
Analyze
Result
Units
------------------------
1.1,1-Trichloroethane
-----------
ND
-------
ug/l
1,1,2-Trichloroethane
ND
ug/l
Trichloroethene
32.0
ug/l
Trichlorofluoromethane
ND
ug/l
ND — Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118625
Sample ID: DW13
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
10.0
------
1.00
------
10
--------
9/ 1/01
------
21:05
-----------
CHollingsw
---------
601
-----
1248
10.0
1.00
10
9/ 1/01
21:05
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
21:05
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
21:05
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 100. 50. - 128.
Hall Surr., chloroprene 88. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 130. 49. - 132.
# — Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: .�,��.i� 1z �,��c/ Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 F( s-m.h CRE]G11TOX DRIVE / NA511CII,1,E,TN 37204 / 615-726-0177 / F%\: 615-726-0954 / 800-765-0980

TestAmerica
� I
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118622
ICIM PRZYBYL Sample ID: DW14
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water
MORRISVILLE, NC 27560 Site ID:
Date
Collected:
8/20/01
Project: 107535
Time
Collected:
17:45
Project Name: SLS-GREENSBORO
Date
Received:
8/22/01
Sampler: DAVID LUBELL
Time
Received:
9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
----- ----
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND,
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Bromoform
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Bromomethane
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Chloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
1M
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Chloroform
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Chloromethane
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
20.23
CHoilingsw
601
1248
1.2-Dichloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Methylene chloride
ND
ug/1
50.0
5.00
10
9/
1/01
20:23
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/1
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Tetrachloroethene
455.
ug/l
10.0
1.00
10
9/
1/01
20:23
CHollingsw
601
1248
Sample report continued . . .
2960 Fus'rrk Uhnr; / \,\sn\n.i.E.TN 37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

Testl�merica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
.&zalyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene 116. ug/l
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118622
Sample ID: DW14
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
10.0
------
1.00
------
10
--------
9/ 1/01
------
20:23
-----------
CHollingsw
---------
601
-----
1248
10.0
1.00
10
9/ 1/01
20:23
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
20:23
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
20:23
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 101. 50. - 128.
Hall Surr., chloroprene 87. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 129. 49. - 132.
# - Recovery outside laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: ,.�,� L,,,�� Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
- End of Sample Report.
2960 Fus•n•;k CREICIITON Dkn:r. / NAs11%11.1.E,'1'N 37204 / 615-726-0177 / F%\: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
ICIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118621
Sample ID: DW15
Sample Type: Groundwater
Site ID:
Date Collected: 8/20/01
Time Collected: 11:05
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
10.0
1.00
10
9/
1/01
19:41
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
602/601
1248
Bromodichloromethane
ND-.
ug/l
10.0'
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Bromoform
ND
ug/1
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Bromomethane
NO
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/1
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Chloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/1
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Chloroform
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Chloromethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
1,1-Dichloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
19:'41
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
1,2-Dichloropropane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/1-
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Methylene chloride
ND
ug/l
50.0
5.00
10
9/
1/01
19:41
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Tetrachloroethene
469.
ug/l
10.0
1.00
10
9/
1/01
19:41
CHollingsw
601
1248
Sample report continued . . _
2960 FuS•H-:k Chi;ir,irrux Dkni•: / NASinu,u:.TN 37204 / 615-726-0177 / F'%\: 615-726-0954 / 800-765-0980

I
TestAmerica
l I N C O R P O R A T E D
ANALYTICAL REPORT
Analvte Result Units
1,1.1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene 92.0 ug/l
Trichiorofluoromethane ND ug/l
ND - Not detected at the report limit.
Laboratory Number: 01-A118621
Sample ID: DW15
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
Factor
Date
Time
Analyst
Method
Batch
10.0
------
1.00
------
10
--------
9/ 1/01
------
19:41
-----------
CHollingsw
---------
601
-----
1248
10.0
1.00
10
9/ 1/01
19:41
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
19:41
CHollingsw
601
1248
10.0
1.00
10
9/ 1/01
19:41
CHollingsw
601
1248
Surrogate % Recovery Target Range
------------- ----------------------
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 102. 50. - 128.
Hall Surr., chloroprene 88. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 132. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: .AA.'J. I Luc/✓ Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail,A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
1
2960 Fos-n.:R Cni:ir,irr, ,% Dkni•: / NASHCILLF:,'rN 37204 / 615-726-0177 / F\x: 615-726-0954 / 800-765-0980

TestAmerica,i
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SEARS-GREENSBORO
Sampler:.DAVID LUBERO
Analyte Result Units
------------------------ ----------- ------
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromome thane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropee
Sample report continued . . .
Lab Number: 01-A119814
Sample ID: DMP-1
Sample Type: Water
Site ID:
Date Collected: 8/23/01
Time Collected: 11:00
Date Received: 8/25/01
Time Received: 10:00
Report Quan Dil Analysis Analysis
Limit Limit Factor Date Time Analyst Method Batch
------ ------- ------ -------- ----- ------------------- -----
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
602/601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
602/601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw,
602/601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
602/601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw.
601
9840
ND
ug/l
500.
2.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500'.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/1
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/1
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/l
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/1
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
ND
ug/1
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
2960 FOSTER CRBI(;HTO:V DRIVE / NASHVII,6E.TN 37204 / 615-726-0177 / F.\x: 615-726-0954 / 800-765-0980

TestAmerica
I NCORPO RATED
ANALYTICAL REPORT
Analyte
Result
Units
------------------------
trans-1,3-Dichloropropene
-----------
ND
------
ug/1
Methylene chloride
ND
ug/1
1,1,2,2-Tetrachloroethane
ND
ug/l
Tetrachloroethene
ND
ug/l
1,1,1-Trichloroethane
ND
ug/1
1,1,2-Trichloroethane
ND
ug/l
Trichloroethene
ND
ug/l
Trichlorofluoromethane
ND
ug/l
VOA PQL's elevated due to sample matrix.
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A119814
Sample ID: DMP-1
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
------
Limit
-------
Factor
Date
Time
Analyst
Method
Batch
500.
1.0
------
500
--------
8/29/01
-----
3:28
----------
CHollingsw
---------
601
-----
9840
2500
5.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
500.
1.0
500
8/29/01
3:28
CHollingsw
601
9840
Recovery Target Range
PID Surr., a.a,a-trifluorotoluene
88.
50.
- 150.
Hall Surr., 2-chloropropane
91.
50.
- 128.
Hall Surr., chloroprene
93.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
89.
49.
- 132.
- Recovery outside Laboratory historical
or method
prescribed limits.
Sample report continued . . .
i
2960 FU5TER CKeu,tiTON DRIVE. / N,�suvii.i.e.TN 37204 / 615-726-0177 / F:xx: 615-726-0954 / 800-765-0980
;I

TestAmerica
ANALYTICAL REPORT
Laboratory Number: 01-A119814
Sample ID: DMP-1
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and.with
permission of the laboratory.
1
Report Approved By: 0, Report Date: 8/29/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FosTER CRF.ICHTO:N DRIVE. / NASHVILLR,TN 37204 / 615-726-0177 / F:%x: 615-726-0954 / 800-765-0980

Tpstl�merica
1 N c O R P O R A T E 0
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A118638
KIM PRZYBYL Sample ID: DMP2
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Ground water
MORRISVILLE, NC 27560 Site ID:
'-
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Date
Time
Date
Time
Collected:
Collected:
Received:
Received:
8/21/01
17:30
8/22/01
9:00
Report
Quan
Dil
Analysis
Analysis
- Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
--------
Date
Time
------
Analyst
-----------
Method
---------
Batch
-----
_ *VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
602/601
1249
j 1,2-Dichlorobenzene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
602/601
1249
1,3-Dichlorobenzene
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
602/601
1249
1,4-Dichlorobenzene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
602/601
1249
Bromodichloromethane
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Bromoform
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Bromomethane
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Carbon tetrachloride
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
j Chloroethane
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
2=Chloroethylvinylether
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Chloroform
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Chloromethane
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
j Dibromochloromethane
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Ethylene Dibromide
ATD
uo/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
_ Vinyl chloride
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Dichlorodifluoromethane
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
-' 1,1-Dichloroethane
ND
ug/l
50.0
1.00
50
8/30/01
22.08
CHollingsw
601
1249
1,2-Dichloroethane
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
- ' 1,1-Dichloroethene
i
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
cis-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
trans-1,2-Dichloroethene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
1,2-Dichloropropane
ND
ug/1
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
cis-1,3-Dichloropropene.
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
- trans-1.3-Dichloropropene
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Methylene chloride
ND
ug/l
250.
5.00
50
8/30/01
22:08
CHollingsw
601
1249
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Tetrachloroethene
150.
ug/l
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Sample report continued . . .
I
2960 Fos'mR N,xsmim.b:jN 37204 / 615-726-0177 / F:\\: 615-726-0951 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/1
1,1,2-Trichloroethane ND ug/l
Trichloroethene 1480 ug/l
Trichlorofluoromethane ND ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118638
Sample ID: DMP2
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
50.0
1.00
------
50
--------
8/30/01
------
22:08
-----------
CHollingsw
---------
601
-----
1249
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
50.0
1.00
50
8/30/01
22:08
CHollingsw
601
1249
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 103. 50. - 128.
Hall Surr.,. chloroprene 87. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 107. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: c:.,Zi- , Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER (:RI•:ICII'1'ON DRi%'r: / N�smIl,I.f,.TN 37204 / G15-726-0177 / Fig: 615-726-0954 / 800-765-0980

Testl�merica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/1
1,1,2-Trichloroethane ND ug/l
Trichloroethene 21.5 ug/l
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118631
Sample ID: DMP3
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
5.00
1.00
------
5
--------
9/ 1/01
------
23:53
-----------
CHollingsw
---------
601
-----
1248
5.00
1.00
5
9/ 1/01
23:53
CHollingsw
601
1248
5.00
1.00
5
9/ 1/01
23:53
CHollingsw
601
1248
5.00
1.00
5
9/ 1/01
-23:53
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 101. 50. - 128.
Hall Surr., chloroprene 88. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 124. 49. - 132.
A - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: ��,-c.t,�CJ Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIG11-1-On DRivF: / NAS11V11,1,E.TN 37204 / 615-726-0177 / FAX: [phone]

•
Te=st m
erlca
I N C O R P O R A T E D
i
-- ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number: 01-A118631
KIM PRZYBYL
Sample ID: DMP3
2200 GATEWAY CTR. BLVD. STE205
Sample Type: Ground water
MORRISVILLE, NC 27560
Site ID:
Date Collected: 8/21/01
Project: 107535
Time Collected: 12:45
Project Name: SLS-GREENSBORO
Date Received: 8/22/01
Sampler: DAVID LUBELL
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by_GC*
Chlorobenzene
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
602/601
1248
Bromodichloromethane
I
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Bromoform
ND'
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Bromomethane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
.601
1248
Carbon tetrachloride
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Chloroethane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Chloroform
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Chloromethane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Dibromochloromethane
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Vinyl chloride
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
-_ 1,1-Dichloroethane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/1
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/1
5.00,
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
trans-1,2-Dichloroethene
NO
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
-- 1,2-Dichloropropane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248_
cis-1,3-Dichloropropene
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Methylene chloride
ND
ug/l
25.0
5.00
5
9/
1/01
23:53
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Tetrachloroethene
144.
ug/l
5.00
1.00
5
9/
1/01
23:53
CHollingsw
601
1248
Sample report continued
2960 F0„•1'1•:k Dmi: / NAsH%'ii, H:,TN 37204 / 6 15-726-0 177 / Fx.x: 615-726-0954 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
I
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number:
01-A118626
KIM PRZYBYL
Sample ID: DMP4
2200 GATEWAY CTR.
BLVD.
STE205
Sample Type:
Ground water
MORRISVILLE, NC 27560
Site
ID:
-
Date
Collected:
8/21/01
Project: 107535
Time
Collected:
9:05
Project Name: SLS-GREENSBORO
Date
Received:
8/22/01
Sampler: DAVID LUBELL
Time
Received:
9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
i
li
-- *VOLATILE ORGANICS by GC*
-
Chlorobenzene
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
602/601
1248
1,3-Dichlorobenzene
ND
ug/1
5000
1.00
5000
9/ 1/O1
23:11
CHollingsw
602/601
1248
1,4-Dichlorobenzene
NO
ug/1
5000
1.00
5000
9/ 1/01.
23:11
CHollingsw
602/601
1248
Bromodichloromethane
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Bromoform
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
.1248
Bromomethane
ND'
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Carbon tetrachloride
NO
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
! Chloroethane
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Chloroform
NO
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Chloromethane
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Dibromochloromethane
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Vinyl chloride
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
i Dichlorodifluoromethane
ND
ug/1
5000
1.00
5000
9/ 1/01
23.11
CHollingsw
601
1248
! 1,1-Dichloroethane
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
1,2-Dichloropropane
NO
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
cis-1,3-Dichloropropene
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
trans-1,3-Dichloropropene
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Methylene chloride
ND
ug/l
25000
5.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
1,1,2,2-Tetrachloroethane
ND
ug/l
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Tetrachloroethene
ND
ug/1
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Sample report continued . . .
2960 Fus•rl•:I: Crl•:uarror\ ORICI': / NASI1%]M.R.TN'' 37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

Testl merica
I N C O R P D R A T E D
ANALYTICAL REPORT
Analyte Result Units
1,1,1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethee ND ug/l
Trichlorofluoromethane ND ug/l
601 dilution due to sample matrix.
ND — Not detected at the report limit
Surrogate
-------------
Laboratory Number: 01-A118626
Sample ID: DMP4
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
-------
5000
------
1.00
------
5000
--------
9/ 1/01
------
23:11
-----------
CHollingsw
---------
601
-----
1248
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
5000
1.00
5000
9/ 1/01
23:11
CHollingsw
601
1248
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 90. 50. - 150.
Hall Surr., 2-chloropropane 100. 50. - 128.
Hall Surr., chloroprene 87. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 81. 49. - 132.
# — Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: 't•,,,, n Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End.of Sample Report.
2960 Fos'rr:R N.\su\n,i,r..TN 37204 / 61.5-726-0177 / F: x: 615-726-0954 / 800-765-0980

i •
TestAmerica
I N C O R P O R A T E 0
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118381
Sample ID: BMW2
Sample Type: Water
Site ID:
Date Collected: 8/22/01-,
Time Collected: 13:20
Date Received: 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ------------------------- ------ ------ -------- -------------------------- -----
*ORGANIC PARAMETERS*
Benzene
Toluene
Ethylbenzene
%ylenes, total
*VOLATILE ORGANICS by GC*
Ethylene Dibromide
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
Sample report continued .
ND,
ug/1
1.00
1.00
1
8/26/01
21:00
D.Ramey -
602
7282
1.90
ug/1
1.00
1.00
1
8/26/01
21:00
D.Ramey
602
7282
ND.
ug/1
1.00
1.00
1
8/26/01
21:00
D.Ramey
602
7282
ND
ug/l
1.00
1.00
1
8/26/01
21:00
D.Ramey
602
7282
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
500.
1.0
500
8/28/01
0:48
CHollingsw
602/601
73
ND
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
602/601
73
ND
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
602/601
73
ND
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
602/601
73
ND
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
,TO
ug/1
500.
2.0
500
8/28/01
0:48
CHollingsw
601
73
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
71_"_
ND
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/l
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
ND
ug/1
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
45.2
ug/1
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
13100
ug/l
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
2960 FOSTER CREIGHTON DRIVE, / N,%sHVH,LE,TN 37204 / 615-726-0177 / Fk.r: 615-726-0954 / 800-765-0980

I TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT ,
Laboratory Number: 01-A118381
Sample ID: BMW2
Project: 107535-30205000
Page 2
Analyte Result Units
trans-1,2-Dichloroethene
ND
ug/l
1,2-Dichloropropane
ND
ug/l
cis-1,3-Dichloropropene
ND
ug/l
trans-1,3-Dichloropropene
ND
ug/l
Methylene chloride
ND
ug/l
1,1,2,2-Tetrachloroethane
ND
ug/l
Tetrachloroethene
r
30400
ug/1
1,1,1-Trichloroethane
ND
ug/l
1,1,2-Trichloroethane
8.9
ug/1
Trichloroethene .
2300
ug/l
Trichlorofluoromethane
ND
ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
----=-
Factor
Date
Time
Analyst
Method
Batch
500.
1.0
------
500
--------
8/28/01
------
0:48
-----------
CHollingsw
---------
601
-----
73
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
5.0
5.0
1
8/25/01
7:16
CHollingsw
601
7121
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
500.
1.0
500
8/28/01
0:48
CHollingsw
601
73
1.0
1.0
1
8/25/01
7:16
CHollingsw
601
7121
Recovery Target Range
BTEX/GRO Surr., a,a,a-TFT
82.
67.
- 135.
PID Surr., a,a,a-triflucrotoluene
89.
50.
- 150.
Hall Surr., 2-chloropropane
58.
50.
- 128.
'Hall Surr., chloroprene
63.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
66.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
Sample report continued .
i
2960 FOSTER CREIGIITON DRIVE / NASIien,LE,TN 37204 / 615-726-0177 / F\x: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
I N C O R P O R A T E D
Laboratory Number: 01-A118381
Sample ID: BMW2
Project: 107535-30205000
Page 3
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
I
End of Sample Report.
2960 FOSTER CREI(;HT(1S DRIVE / NASHFII.I.E.TN 37204 / 615-726-0177 / F.": 615-726-0954 / 800-765-0980

TestAmerica
INCO RPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SEARS-GREENSBORO
Sampler: DAVID LUBERO
Lab Number: 01-A119819
Sample ID: HVDP-10
Sample Type: Water
Site ID:
Date Collected: 8/23/01
Time Collected: 12:15
Date Received: 8/25/01
Time Received: 10:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- ------ ------------- -------------- ------------------------ -----
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Sample report continued . . .
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
602/601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
602/601
9840
ND
ug/1
'50.0
1.0
50
8/29/01
8:14
CHollingsw
602/601
9840
ND'
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
602/601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
2.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
8:14
CHollingsw
601
9840
2960 FOSTER CREIGHTON DRIVE: / N,1SfiVII.LE.TN 37204 / 615-726-0177 / F\..x: 615-726-0954 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A119819
Sample ID: HVDP-10
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
Units
Limit
Limit
Factor
Date
Time
trans-1,3-Dichloropropene
-----------
ND
------
ug/1
------
50.0
-------
1.0
------
50
--------
8/29/01
-----
8:14
Methylene chloride
ND
ug/1
250.
5.0
50
8/29/01
8:14
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.0
50
8/29/01
8:14
Tetrachloroethene
755.
ug/l
50.0
1.0
50
8/29/01
8:14
1,1,1-Trichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
8:14
1,1,2-Trichloroethane
ND
ug/l
50.0 .
1.0
50
8/29/01
8:14
Trichloroethene
1180
ug/1
50.0
1.0
50'
8/29/01
8:14
Trichlorofluoromethane
ND
ug/l
50.0
1.0
50
8/29/01
8:14
ND - Not detected at the report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene
88.
50.
- 150.
Hall Surr., 2-chloropropane
90.
50.
- 128.
Hall Surr., chloroprene
88.
55.
- 123.
Hall Surr., 1-chloro-3-fluorobenzene
90.
49.
- 132.
# - Recovery outside Laboratory historical
or method
prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By:
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
Analyst Method Batch
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FOSTER CREIGIITO:V DRIVE / N:ksIIFILI.E.TN 37204 / 615-726-0177 / Fix: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number: 01-A119818
KIM PRZYBYL
Sample ID,: HVDP-15
2200 GATEWAY CTR. BLVD. STE205
Sample Type: Water
MORRISVILLE, NC 27560
Site ID:
I
Date Collected: 8/23/01
Project: 107535-30205000
Time Collected: 11:55
Project Name: SEARS -GREENSBORO
Date Received: 8/25/01
Sampler: DAVID LUBERO
Time Received: 10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
------
Limit
------
Limit
-------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND.
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
602/601
9840
_ 1,3-Dichlorobenzene
ND'
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Bromoform
ND
ug/l
50.0
2.0
50
8/29/01
7:33
CHollingsw
601
9840
Bromomethane
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
__.Chloroethane
i
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
2-Chloroethylvinylether
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Chloroform
ND
ug/1
50.0
.1.0
50
8/29/01
7:33
CHollingsw
601
9840
Chloromethane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Dibromochloromethane
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Ethylene Dibromide
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Vinyl chloride
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Dichlorodifluoromethane
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
- 1,1-Dichloroethane
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
1,2-Dichloroethane
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
1,1-Dichloroethene
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
cis-1,2-Dichloroethene
2800
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840'
trans-1,2-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/l
50.0
1.0
50
8/29/01
7:33
CHollingsw
601
9840
Sample report continued . . .
2960 FOSTER CREIGHTO.N DRIVE / NASIIVII,I.E.TN 37204 / 615-726-0177 / F\.x: 615-726-0954 / 800-765-0980

Test -America
1 NCO RPORATED
ANALYTICAL REPORT
Laboratory Number: 01-A119818
Sample ID: HVDP-15
Project: 107535-30205000
Page 2
Report
Quan
Di1
Analysis
Analysis
Analyte
------------------------
Result
Units
Limit
Limit
Factor
Date
Time
trans-1,3-Dichloropropene
-----------
ND
------
ug/1
------
50.0
-------
1.0
------
50
--------
8/29/01
-----
7:33
Methylene chloride
ND
ug/1
250.
5.0
50
8/29/01
7:33
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
Tetrachloroethene
1440
ug/l
50.0
1.0
50
8/29/01
7:33
1,1,1-Trichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
1,1,2-Trichloroethane
ND
ug/l
50.0 •
1.0
50
8/29/01
7:33
Trichloroethee
72700
ug/l
1000
1.0
1000
8/29/01
13:02
Trichlorofluoromethane
ND
ug/l
50.0
1.0
50
8/29/01
7:33
ND — Not detected at the report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene
89.
50.
- 150.
Hall Surr., 2-chloropropane
89.
50.
- 128.
Hall Surr., chloroprene
99.
55.
- 123.
Hall Surr., 1-chlora-3-fluorobenzene
100.
49.
- 132.
# — Recovery outside Laboratory historical
or method prescribed
limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: (�
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
Analyst Method Batch
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
781
CHollingsw
601,
9840
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FOSTER CREIGHTON DRIVE, / NASmH.I,E,TN 37204 / 615-726-01 77 / Fxx: 615-726-0951 / 800-765-0980

TestAmerica
I N C O RPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SEARS-GREENSBORO
Sampler: DAVID LUBERO
Analyte
-.
------------------------
*VOLATILE ORGANICS by GC*
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Ethylene Dibromide
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
Sample report continued . . .
Lab Number: 01-A119817
Sample ID: HVDP-22
Sample Type: Water
Site ID:
Date Collected: 8/23/01
Time Collected: 11:40
Date Received: 8/25/01
Time Received: 10:00
Report
Quan
Dil
Analysis
Analysis
Result Units Limit
----------- ------ ------
Limit
-------
Factor
------
Date
--------
Time
-----
Analyst Method Batch
------------------- -----
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
602/601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
602/601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
602/601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
602/601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/1
50.0
2.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6.52
CHollingsw
601
9840
ND
ug/1
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
215.
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
ND
ug/l
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
2960 Fos'rEK CREIGHTON DRIVE / N:\sIIVII,1.6.TN 37204 / 615-726-0177 / F:\.r: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Analyte
Result
Units
------------------------
trans-1,3-Dichloropropene
-----------
ND
------
ug/l
Methylene chloride
ND
ug/l
1,1,2,2-Tetrachloroethane
ND
ug/l
Tetrachloroethene
2150
ug/l
1,1,1-Trichloroethane
ND
ug/l
1,1,2-Trichloroethane
ND
ug/l
Trichloroethene
2030
ug/l
Trichlorofluoromethane
ND
ug/1
ND - Not detected at the report -limit.
Surrogate
-------------
Laboratory Number: 01-A119817
Sample ID: HVDP-22
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
------
Limit
-------
Factor
Date
Time
Analyst
Method
Batch
50.0
1.0
------
50
--------
8/29/01
-----
6:52
----------
CHollingsw
---------
601
-----
9840
250.
5.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
50.0
1.0
50
8/29/01
6:52
CHollingsw
601
9840
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 88. 50. - 150.
Hall Surr., 2-chloropropane 99. 50. - 128.
Hall Surr., chloroprene 91. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 98. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
t Report Approved By: Report Date: 8/29/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / N:\SHVILI,E.TN 37204 / 615-726-0177 / F.\.x: 613-726-0954 / 800-765-0980

Testltlmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A119815
KIM PRZYBYL - Sample ID: HVDP-27
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water
MORRISVILLE, NC 27560 Site ID:
Date
Collected:
8/23/01
Project: 107535-30205000
Time
Collected:
11:15
Project Name: SEARS
-GREENSBORO
Date
Received:
8/25/01
Sampler: DAVID LUBERO,
Time
Received:
10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
- ------------------------
Result
-----------
Units
------
Limit
------
Limit
-------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
602/601
9840
1,3-Dichlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Bromoform
ND
ug/1
50.0
2.0
50
8/29/01
4:08
CHollingsw
601
9840
Bromomethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Chloroethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
-- 2-Chloroethylvinylether
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Chloroform
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Chloromethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Dibromochloromethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Ethylene Dibromide
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Vinyl chloride
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Dichlorodifluoromethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
1,1-Dichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
1,2-Dichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
1,1-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
cis-1,2-Dichloroethene
600.
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
trans- 1, 2-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/1
50.0
1.0
50
8/29/01
4:08
CHollingsw
601
9840
Sample report continued .
I
2960 FOSTER CREIGHTON DRIVE / NASIIVILLF],TN 37204 / 615-726-0177 / F�.t: 615-726-0954 / 800-765-0980

Fin
TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A119815
Sample ID: HVDP-27
Project: 107535-30205000
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
Limit
Limit
Factor
Date
Time
trans-1,3-Dichloropropene
ND
------
ug/l
------
50.0
-------
1.0
------
50
--------
8/29/01
-----
4:08
Methylene chloride
ND
ug/l
250.
5.0
50
8/29/01
4:08
1,1,2,2-Tetrachloroethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
Tetrachloroethene
2930
ug/l
50.0
1.0
50
8/29/01
4:08
1,1,1-Trichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
1,1,2-Trichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
4:08
Trichloroethene
1350
ug/1
50.0
1.0
50
8/29/01
4:08
Trichlorofluoromethane
ND
ug/1
50.0
1.0
50
8/29/01
4:08
ND — Not detected at the report limit.
Surrogate
-------------
Recovery Target Range
PID Surr.,
a,a,a-trifluorotoluene
89.
50.
- 150.
Hall Surr.,
2-chloropropane
72.
50.
- 128.
Hall Surr.,
chloroprene
74.
55.
- 123.
Hall Surr.,
1-chloro-3-fluorobenzene
79.
49.
- 132.
# — Recovery outside Laboratory historical
or method prescribed
limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By:
_ Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
Analyst Method Batch
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
CHollingsw
601
9840
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FOSTER CREICH•rON DRIVE / N,1sHSI1,LE,TN 37204 / 615-726-0177 / Fix: 615-726-0954 % 800-765-0980

TestAmerica
[NCO RPO RATED
ANALYTICAL REPORT
IT CORP-SEARS 2338 Lab Number: 01-A119816
KIM PRZYBYL Sample ID: HVDP-29
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Water
MORRISVILLE, NC 27560 Site ID:
Date
Collected:
8/23/01
Project: 107535-30205000
Time
Collected:
11:30
Project Name: SEARS-GREENSBORO
Date
Received:
8/25/01
Sampler: DAVID LUBERO
Time
Received:
10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
------
Limit
------
Limit
-------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
602/601
9840
1,3-Dichlorobenzene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Bromoform
ND
ug/1
50.0
2.0
50
8/29/01
6:11
CHollingsw
601
9840
Bromomethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Chloroethane
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
2-Chloroethylvinylether
ND
ug/l
50.0
1.0
50
8/29/01
- 6:11
CHollingsw
601
9840
Chloroform
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Chloromethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Dibromochloromethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Ethylene Dibromide
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Vinyl chloride
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Dichlorodifluoromethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
1,1-Dichloroethane
ND
ug/l
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
1.2-Dichloroethane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
1,1-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
cis-1,2-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
trans-1,2-Dichloroethene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/1
50.0
1.0
50
8/29/01
6:11
CHollingsw
601
9840
Sample report continued .
2960 FOSTER CREIGHTON DmF, / Nwivim,EJN 37204 / 615-726-0177 / Fez: 615-726-095.1 / 800-765-0980

.TestAmerica
I N C O R P O R A T E 0
ANALYTICAL REPORT
Laboratory Number: 01-A119816
Sample ID: HVDP-29
Project: 107535-30205000
Page 2
Report
Quan Dil Analysis Analysis
Analyte
------------------------
Result
-----------
Units
------
Limit
Limit Factor Date Time
Analyst
Method
Batch
trans-1,3-Dichloropropene
ND
ug/l
------
50.0
-------
1.0
------ -------- -----
50 8/29/01 6:11
----------
CHollingsw
---------
601
-----
9840
Methylene chloride
ND
ug/1
250.
5.0
50 8/29/01 6:11
CHollingsw
601
9840
1,1,2,2-Tetrachloroethane
ail
ND
ug/l
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
'i Tetrachloroethene
780.
ug/l
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
.1,1,1-Trichloroethane
ND
ug/l
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
1,1,2-Trichloroethane
ND
ug/1
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
Trichloroethene
75.0
ug/l
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
Trichlorofluoromethane
ND
ug/l
50.0
1.0
50 8/29/01 6:11
CHollingsw
601
9840
ND - Not detected at the report.limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 88. 50. - 150.
Hall Surr., 2-chloropropane 97. 50. - 128.
Hall Surr., chloroprene 94. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 101. 49. - 132.
-_ # - Recovery outside Laboratory historical or method prescribed limits.
i -
- These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
� Report Approved By:
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
1
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FOSTER CREIGHTON DRIVF / NAsi1viu.E,TN 37204 / 613-726-0177 / FAX: [phone]

TestAmerica
ANALYTICAL REPORT
IT CORP-SEARS 2338
Lab Number:
01-A118641
KIM PRZYBYL
Sample
ID: TRIP
BLANK-0.1
2200 GATEWAY CTR.
BLVD.
STE205
Sample
Type:
Ground
water
MORRISVILLE, NC 27560
Site
ID:
Date
Collected:
Project: 107535
Time
Collected:
Project Name: SLS-GREENSBORO
Date
Received:
8/22/01
Sampler: DAVID LUBELL
Time
Received:
9:00
I
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
----=------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
--' *VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
602/601
1249
1,2-Dichlorobenzene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
602/601
1249
1,3-Dichlorobenzene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
602/601
1249
1,4-Dichlorobenzene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
602/601
1249
Bromodichloromethane
ND
ug/l
1, 1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
j Bromoform
ND
ug/1 -
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
' - Bromomethane
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Carbon tetrachloride
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Chloroethane
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
2-Chloroethylvinylether
ND
g/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Chloroform
ND
Z/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Chloromethane
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Dibromochloromethane
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Ethylene Dibromide
ND
ug/1
1.00
1.00
1
8/30/01
20.02
CHollingsw
601
1249
Vinyl chloride
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Dichlorodifluoromethane
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
1,1-Dichloroethane
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
1,2-Dichloroethane
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
1,1-Dichloroethene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
cis-1,2-Dichloroethene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
trans-1,2-Dichloroethene
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
- 1,2-Dichloropropane
ND
ug/l
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
cis-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
trans-1,3-Dichloropropene
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Methylene chloride
ND
ug/1
5.00
5.00
1
8/30/01
20:02
CHollingsw
601
1249
1,1,2,2-Tetrachloroethane
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Tetrachloroethene
ND
ug/1
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
Sample report continued . . .
Fus•ri-:k (;Ri.;i(;wroN DRIVE / NAsu1n,1.s.TN 37204 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R F 0 R A T E D
ANALYTICAL REPORT
Analyte Result Units
1.1.1-Trichloroethane ND ug/l
1,1,2-Trichloroethane ND ug/l
Trichloroethene ND ug/1
Trichlorofluoromethane ND ug/1
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A118641
Sample ID: TRIP BLANK-01
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Limit
-------
Limit
------
Factor
Date
Time
Analyst
Method
Batch
1.00
1.00
------
1
--------
8/30/01
------
20:02
-----------
CHollingsw
---------
601
-----
1249
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
1.00
1.00
1
8/30/01
20:02
CHollingsw
601
1249
1.00
1.00
1
8/30/01
20:02
CHollingsw
601 -
1249
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 91. 50. - 150.
Hall Surr., 2-chloropropane 104. 50. - 128.
Hall Surr., chloroprene 89. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 81. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Ck" , Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fo :n:R NiU' / N-AS11%i i.L.TN 37201 / 615-726-0177 / F\\: 615-726-0954 / 800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338'
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Lab Number: 01-A119822
Sample ID: TRIP BLANK
Sample Type: Water
Site ID:
Project: 107535-30205000
Project Name: SEARS -GREENSBORO
Sampler: DAVID LUBERO
Date
Date
Time
Collected:Time Collected:
Received:
Received:
8/25/01
10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
------
Limit
------
Limit Factor
------- ------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
----- t
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
602/601
9840
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Bromoform
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Bromomethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Chloroethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
-- 2-Chloroethylvinylether
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Chloroform
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Chloromethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Dibromochloromethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Vinyl chloride
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
1,1-Dichloroethane
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
1,2-Dichloroethane
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
1,1-Dichloroethene
ND
ug/1
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
cis-1,2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
trans- 1, 2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/28/01
23:22
CHollingsw
601
9840
Sample report continued . . .
2960 FOSTER CREIGHTON DRIVE / N.ASEIVn,t.E,TN 37204 / 615-726-0177 / FAX: [phone]

Analyte
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethee
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethee
Trichlorofluoromethane
TestAmerica
ANALYTICAL REPORT
Laboratory Number: 01-A119822
Sample ID: TRIP BLANK
Project: 107535-30205000
Page 2
Report
Quan
Dil
Result
-----------
Units
Limit
Limit
Factor
ND
------
ug/l
------
1.0
-------
1.0
------
1
6.8
ug/l
5.0
5.0
1
ND
ug/l
1.0
1.0
1
ND
ug/1
1.0
1.0
1
ND
ug/1
1.0
1.0
1
ND
ug/l
1.0
1.0
1
ND
ug/1
1.0
1.0
1
ND
ug/1
1.0
1.0
1
ND - Not detected at the report limit.
Surrogate
-------------
Analysis
Analysis
Date
--------
Time
Analyst
Method
Batch
8/28/01
-----
23:22
----------
CHollingsw
---------
601
-----
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
8/28/01
23:22
CHollingsw
601
9840
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 88. 50. - 150.
Hall Surr., 2-chloropropane 103. 50. - 128.
Hall Surr., chloroprene 108. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 99. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
+ permission of the laboratory.
Report Approved By: �
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
End of Sample Report.
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
2960 FOSTER CREIGHTON DRIVE / NASIIVII,I,E,TN 37204 / 615-726-0177,/ F%x: 615-726-0954 / 800-765-0980

iestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SLS-GREENSBORO
Sampler: DAVID
Lab Number: 01-A118386
Sample ID: TRIP BLANK2
Sample Type: Water
Site ID:
Date Collected:
Time Collected:
Date Received: - 8/23/01
Time Received: 9:00
Report Quan Dil Analysis Analysis
Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch
------------------------ ----------- -------------- ------ ------ -------- -------------------------- -----
*VOLATILE ORGANICS by GC*
� I
Ethylene Dibromide
Chlorobenzene
1.2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Bromodichloromethane
Bromoform
Bromome thane
Carbon tetrachloride
Chloroethane
2-Chloroethylvinylether
Chloroform
Chloromethane
Dibromochloromethane
Vinyl chloride
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethene
1.1-Dichloroethene
cis-1,2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Sample report continued . . .
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.G
1
8/27/01
18:15
CHollingsw
602/601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
602/601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
602/601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
602/601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/l
1.0
1.0
1
8/27/01
18:15
CHollingsw.
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/l
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
-18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/l
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
5.0
5.0
1
8/27/01
18:15
CHollingsw
601
7121
ND ug/1
1.0
1.0
1
8/27/01
18:15
CHollingsw
601
7121
2960 FOSTER CREIGHTON DRIVE / NASHVII,I.E.TN 37204 / 615-726-0177 / F.%.x: 615-726-0954 / 800-765-0980

TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory
Sample
Project:
Page 2
Number: 01-A118386
ID: TRIP BLANK2
107535-30205000
Report
Quan
Dil
Analysis Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date Time
Analyst
Method
Batch
Tetrachloroethene
ND
ug/1
-------
1.0
------
1.0
------
1
-------- ------
8/27/01 18:15
-----------
CHollingsw
---------
601
-----
7121
1,1,1-Trichloroethane
ND.
ug/1
1.0
1.0
1
8/27/01 18:15
CHollingsw
601
7121
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
1
8/27/01 18:15
CHollingsw
601
7121
Trichloroethene
ND
ug/l
1.0
1.0
1
8/27/01 18:15
CHollingsw
601
7121
Trichlorofluoromethane
ND
ug/l
1.0
1.0
1
8/27/01 18:15
CHollingsw
601
7121
ND - Not detected at the
report limit.
Surrogate
-------------
%
----------
Recovery
Target Range
------------
-
PID Surr., a,a,a-trifluorotoluene 94. 50. - 150.
Hall Surr., 2-chloropropane 84. 50. - 128.
Hall Surr., chloroprene 81. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 89. 49. - 132.
- Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: alt'411 Report Date: 8/28/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 Fos•rER CREIGHTON DRIVE / NASHVII.I.E.TN 37204 / 615-726-0177 / F�.C: 615-726-0954 / 800-765-0980

_. 1 e i
r1 TestAm ca
I N C O R P O R A T E D
ANALYTICAL REPORT.
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535-30205000
Project Name: SEARS-GREENSBORO
Sampler: DAVID LUBERO
Lab Number: 01-A119821
Sample ID: FB-02
Sample Type: Water
Site ID:
Date Collected: 8/23/01
Time Collected: 10:45
Date Received: 8/25/01
Time Received: 10:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
------
Limit
-------
Factor
------
Date
--------
Time
-----
Analyst
----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
602/601
9840
1,2-Dichlorobenzene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
602/601
9840
1,3-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/29/01
12:21
CHollingsw
602/601
9840
1,4-Dichlorobenzene
ND
ug/1
1.0
1.0
1
8/29/01
12:21
CHollingsw
602/601
9840
Bromodichloromethane
ND
ug/1
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Bromoform
ND
ug/1
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Bromomethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Carbon tetrachloride
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Chloroethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
2-Chloroethylvinylether
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Chloroform
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Chloromethane
ND
ug/l
-1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Dibromochloromethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Ethylene Dibromide
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Vinyl chloride
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1,1-Dichloroethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1,2-Dichloroethane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1,1-Dichloroethene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
cis-1,2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
trans-1,2-Dichloroethene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1,2-Dichloropropane
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Sample report continued . . .
2960 FOSTER CREIGH'TON DRIVE. / iN,ksm-iI.LE.TN 37204 / 615-726-0177 / R: x: 615-726-0951 / 800-765-0980

Analyte
trans-1,3-Dichloropropene
Methylene chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethee
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Result Units
ND
ug/l
ND
ug/l
ND
ug/l
13.1
ug/l
ND
ug/1 -
ND
ug/1
ND
ug/1
ND
ug/l
ND - Not detected at the report limit.
Surrogate
-------------
Laboratory Number: 01-A119821
Sample ID: FB-02
Project: 107535-30205000
Page 2 .
Report
Quan
Dil
Analysis
Analysis
Limit
------
Limit
Factor
Date
Time
Analyst
Method
Batch
1.0
-------
1.0
------
1
--------
8/29/01
-----
12:21
----------
CHollingsw
---------
601
-----
9840
5.0
5.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
1.0
1.0
1
8/29/01
12:21
CHollingsw
601
9840
Y Recovery Target Range
PID Surr.,
a,a,a-trifluorotoluene
88.
50.
- 150.
Hall Surr.,
2-chloropropane
102.
50.
- 128.
Hall Surr.,
chloroprene
96.
55.
- 123.
Hall Surr.,
1-chloro-3-fluorobenzene
104.
49.
- 132.
# - Recovery outside Laboratory historical
or method prescribed
limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
i
Report Approved By:
Paul E. Lane, Jr., Lab Director
Michael H. Dunn, M.S., Technical Director
�__' Johnny A. Mitchell, Dir. Technical Serv.
Eric S. Smith, Assistant Technical Director
Report Date: 8/29/01
Gail A. Lage, Technical Serv.
Glenn L. Norton, Technical Serv.
Kelly S. Comstock, Technical Serv.
Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
- End of Sample Report.
2960 FoSTBR CREIGHTON DRIVE: / NASIA-11,1.8.TN 37204 / 615-726-0177 / Fk.t: 615-726-0954 / 800-765-0980

1 �
T
est merlca
I N C O R P O R A T E D
I !
l�
ANALYTICAL REPORT
I
IT CORP-SEARS 2338
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project: 107535
Project Name: SLS-GREENSBORO
Sampler: DAVID LUBELL
Lab Number: 01-A118624
Sample ID: FB01
Sample Type: Ground water
Site ID:
Date Collected: 8/21/01
Time Collected: 19:05
Date Received: 8/22/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS by GC*
Chlorobenzene
ND.
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
602/601
1248
1,2-Dichlorobenzene
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
602/601
1248 `
1,3-Dichlorobenzene
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
602/601
1248
1,4-Dichlorobenzene
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
602/601
1248
- Bromodichloromethane
ND.
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Bromoform
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Bromomethane
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Carbon tetrachloride
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Chloroethane
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
2-Chloroethylvinylether
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Chloroform
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Chloromethane
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Dibromochloromethane
I
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Ethylene Dibromide
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
_ Vinyl chloride
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Dichlorodifluoromethane
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
_ 1,1-Dichloroethane
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
1,2-Dichloroethane
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
1,1-Dichloroethene
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
cis-1,2-Dichloroethene
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
trans-1,2-Dichloroethene
ND
ug/l
1.00
1.00
1
9/
1/01
16.53
CHollingsw
601
1248
- 1,2-Dichloropropane
ND
ug/1
1.00
1.00
1
9/
1/01
16.53
CHollingsw
601
1248
j cis-1,3-Dichloropropene
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
- trans-1,3-Dichloropropene
ND
ug/l
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Methylene chloride
ND
ug/l
5.00
5.00
1
9/
1/01
16:53
CHollingsw
601
1248
I 1,1,2,2-Tetrachloroethane
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Tetrachloroethene
ND
ug/1
1.00
1.00
1
9/
1/01
16:53
CHollingsw
601
1248
Sample report continued . . .
21)60 F1) 1.:r Chi;I(;,rr„\ 1)hni•: / N:%sii v ii.i,r,.'I'N 37204 615-726-0177 / F%v 615-726-095 I / 800-765-0980

i
I ,
--J TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 017A118624
Sample ID: FB01
Project: 107535
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
1.1,1-Trichloroethane
ND
ug/l
-------
1.00
------
1.00
------
1
--------
9/ 1/01
------
16:53
-----------
CHollingsw
---------
601
-----
1248
1,1,2-Trichloroethane
ND
ug/1
1.00
1.00
1
9/ 1/01
16:53
CHollingsw
601
1248
Trichloroethene
ND
ug/1
1.00
1.00
1
9/ 1/01
16:53
CHollingsw
601
1248
Trichlorofluoromethane
ID
ug/1
1.00
1.00
1
9/ 1/01
16:53
CHollingsw
601
1248
ND - Not detected at the report limit.
Surrogate
-------------
Recovery Target Range
PID Surr., a,a,a-trifluorotoluene 92. 50. - 150.
Hall Surr., 2-chloropropane 96. 50. - 128.
+ - Hall Surr., chloroprene 91. 55. - 123.
Hall Surr., 1-chloro-3-fluorobenzene 83. 49. - 132.
# - Recovery outside Laboratory historical or method prescribed limits.
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: n,Lt/( n .�,��` Report Date: 9/ 4/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
j End of Sample Report.
i f 2960 Fns•n•:R Nini-: / NASIR11,1,E,TN 37204 / 615-726-0177 / F\%: 615-726-0954 / 800-765-0980

Test mar. ica
Divisiori/Laboratory Name;
IN CO RP O P A T! 0
Client Name- %_� �IDda2(RrWr .01\) Client#:
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Telephone Number: � . 7- � Fax:C`, � • .��?
Sampler Name: (Print Name)
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To assist us In using the proper analytical methods,
is this work being conducted for regulatory purposes?
Compliance Monitoring
Project Name: �L 5 C7/' j;=�lfSCi�S G
Project #:
Site/Location ID: State:
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Client Name 7-rog Client#:
Address:
City/State/Zip Coder
Project Manager:
Telephone Number:
Sampler Name: (Print Name)
Sampler Signature:
'To assist
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is this work, being conducted for regulatory purposes?
Compliance Monitoring
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Project Name:
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Compliance Monitoring
Project Name: , - AE3-

IT Corporation oPNorth Carolinn, Inc.
A Member of The /T Croup
Appendix B
Laboratory Analytical Data Reports - Source Area Soil Samples

T
estAmerlca
I N C O R P O R A T E 0
ANALYTICAL REPORT
-- IT CORP-SUN 2337
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project:
Project Name: SLS GREENSBORO
Sampler: ELIZABETH VAN FLEET
Lab Number: 01-A95099
Sample ID: GP 7-10-01-1
Sample Type: Soil
Site ID:
Date Collected: 7/10/01
Time Collected: 10:45
Date Received: 7/11/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS*
Acetone
ND
mg/kg
3.676
0.0500
50
7/17/01
20:52
J.Gott
8260E
9576
Benzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Bromobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Bromochloromethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Bromoform
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Bromomethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
2-Butanone
ND
mg/kg
3.676
0.0500
50
7/17/01
20:52
J.Gott
8260B
9576
n-Butylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
sec-Butylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
t-Butylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260E
9576
Carbon disulfide
ND
mg/kg
0.1471
0.0020
50 -
7/17/01
20:52
J.Gott
8260B
9576
Carbon tetrachloride
0.4044
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Chlorobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Chloroethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260E
9576
Chloroform
3.382
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Chloromethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
2-Chlorotoluene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
4-Chlorotoluene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.7353
0.0100
50
7/17/01
20:52
J.Gott
8260B
9576
Dibromochloromethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1.2-Dibromoethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
-- Dibromomethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2-Dichlorobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,3-Dichlorobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,4-Dichlorobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Dichlorodifluoromethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Sample report continued . . .
2960 FOsTRR CREIGHTON DRIVE / NASHVII,I,E,TN 37204 / 615-726-0177 / FAX: [phone]

Test America
I N C O R P O R A T E D
' I
ANALYTICAL REPORT
Laboratory Number: 01-A95099
Sample ID: GP 7-10-01-1
Project:
Page 2
Report
Quan
Di1
Analysis
Analysis
Analyte
------------------------
Result
Units
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
1,1-Dichloroethane
-----------
ND
-------
mg/kg
-------
0.1471
------
0.0020
------
50
--------
7/17/01
------
20:52
-----------
J.Gott
---------
8260B
-----
9576
1,2-Dichloroethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,1-Dichloroethene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260E
9576
cis-1,2-Dichloroethene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
trans-1,2-Dichloroethene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2-Dichloropropane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,3-Dichloropropane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
2,2-Dichloropropane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,1-Dichloropropene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
cis-1,3-Dichloropropene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
trans-1,3-Dichloropropene
"ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Ethylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Hexachlorobutadiene
ND
mg/kg
0.1471
0.0020
'50
7/17/01
20:52
J.Gott
8260B
9576
2-Hexanone
ND
mg/kg
0.7353
0.0100
50
7/17/01
20:52
J.Gott
8260B
9576
Isopropylbenzene
ND_
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
4-Isopropyltoluene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
4-Methyl-2-pentanone
ND
mg/kg
0.7353
0.0100
50
7/17/01
20:52
J.Gott
8260B
9576
Methylene chloride
ND
mg/kg
0.3676
0.0050
50
7/17/01
20:52
J.Gott
8260E
9576
Naphthalene
0.4412
mg/kg
0.3676
0.0050
50
7/17/01
20:52
J.Gott
8260B
9576
n-?ropylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
32660B
95%6
Styrene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,1,1,2-Tetrachloroethane
2.515
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,1,2,2-Tetrachloroethane
0.1691
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Tetrachloroethene
2537.
mg/kg
147.1
0.0020
50000
7/18/01
16:47
C. Wani
8260B
2946
Toluene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2,3-Trichlorobenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
32603
9576
1,2,4-Trichlorobenzene
ND
mg/kg
0.1471
0.0020
56
7/17/01
_20:52
J.Gott
8260B
9576
1,1,1-Trichloroethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,1,2-Trichloroethane
0.7794
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Trichloroethene
0.8162
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2,3-Trichloropropane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,2,4-Trimethylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
1,3,5-Trimethylbenzene
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Vinyl chloride
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Xylenes, Total
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Bromodichloromethane
ND
mg/kg
0.1471
0.0020
50
7/17/01
20:52
J.Gott
8260B
9576
Sample report continued
2960 Fus•rER CREIGHroa DRRE / NAS11%'11.1,E,TN 37204 / 615-726-0177 / F:\.\: 615-726-0954 / 800-765-0980
!I

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A95099
Sample ID: GP 7-10-01-1
Project:
Page 3
Report Quan Dil
Analysis
Analysis
Analyte Result Units
------------------------
Limit Limit Factor
Date
Time Analyst Method Batch
----------- -------
Trichlorofluoromethane ND mg/kg
------- ------ ------
0.1471 0.0020 50
--------
7/17/01
------ -------------------- -----
20:52 J.Gott 8260B 9576
*GENERAL CHEMISTRY PARAMETERS*
Dry Weight 68. %
1
7/12/01
8:05 B. Powell CLP 8649
ND - Not detected at the report limit.
-----------------------------------------------------------------------------------------------------------------------------
Sample Extraction Data
Wt/Vol
Parameter Extracted Extract Vol Date Time Analyst Method
---------------- --------- ----------- -------- ----- ---------- ---------
Volatile Organics 8.1 g 5.0 ml 7/10/01 10:45 C.Bates 5035
Surrogate % Recovery
-------------
VOA Surr 1,2-DCA-d4 79.
VOA Surr-Toluene d8 93.
VOA Surr, 4-BFB 81.
_ VOA Surr, DBFM 84.
I
# - Recovery outside Laboratory historical limits.
Target Range
50. - 140.
75. - 141.
69. - 131.
76. - 136.
Results for metals or Organic analyses, if requested, have been corrected for dry weight.
9
Sample report continued . . .
I
2960 Fo1'rER CREIGHTON DRIVE / N:�sum,i,E.TN 37204 / 615-726-0177 /-K: x: 615-726-095 ! / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Laboratory Number: 01-A95099
Sample ID: GP 7-10-01-1
Project:
Page 4
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Q Report Date: 7/18/01
j Paul E. Lane, Jr., Lab.Director Gail A. Lage, Technical Serv.
Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FoSTER CREIGHTON DRIVE: / NASH6H,LE.'rN 37204 / 615-726-0177 / R%x: 615-726-0954 / 800-765-0980

til �
TestAmerica
-- I N C O R P O R A T E D
ANALYTICAL REPORT
-G IT CORP-SUN 2337
KIM PRZYBYL
2200 GATEWAY CTR. BLVD. STE205
MORRISVILLE, NC 27560
Project:
Project Name: SLS GREENSBORO
Sampler: ELIZABETH VAN FLEET
Lab Number: 01-A95100
Sample ID: GP 7-10-01-2
Sample Type: Soil
Site ID:
Date Collected: 7/10/01
Time Collected: 10:30
Date Received: 7/11/01
Time Received: 9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS*
Acetone.
ND
mg/kg
0.0490
0.0368
1
7/18/01
10:07
J.Gott
8260B
9576
Benzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Bromobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Bromochloromethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Bromoform
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
Bromomethane
ND
mg/kg '
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
2-Butanone
ND
mg/kg
0.0490
0.0368
1
7/18/01
10:07
J.Gott
8260B
9576
n-Butylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
sec-Butylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
t-Butylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
826OB
9576
Carbon disulfide
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Carbon tetrachloride
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Chlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Chloroethane
ND
mg/kg
0.0020
0.0015
1
7/18/Ol
10:07
J.Gott
8260E
9576
Chloroform
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Chloromethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
2-Chlorotoluene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
4-Chlorotoluene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0098
0.0074
1
7/18/01
10:07
J.Gott
8260B
9576
Dibromochloromethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,2-Dibromoethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Dibromomethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,2-Dichlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
1,3-Dichlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,4-Dichlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Dichlorodifluoromethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Sample report continued . . .
2960 Fos-rER CREwwro.N Niu / NASIA n.i.E,TN 37204 / 615-726-0177 / Ru: 615-726-0954 /.800-765-0980

TestAmerica
I N C 0 R P 0 R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A95100
Sample ID: GP 7-10-01-2
Project:
Page 2
Report
Quan
Dil
Analysis
Analysis
I Analyte
------------------------
Result
Units
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
-
1,1-Dichloroethane
-----------
ND
-------
mg/kg
-------
0.0020
------
0.0015
------
1
--------
7/18/01
------
10:07
-----------
J.Gott
---------
8260E
-----
9576
1,2-Dichloroethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,1-Dichloroethene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
cis-1,2-Dichloroethene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
trans-1,2-Dichloroethene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,2-Dichloropropane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,3-Dichloropropane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
2,2-Dichloropropane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,1-Dichloropropene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
cis-1,3-Dichloropropene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
trans-1,3-Dichloropropene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Ethylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Hexachlorobutadiene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
2-Hexanone
ND
mg/kg
0.0098
0.0074
1
7/18/01
10:07
J.Gott
8260B
9576
Isopropylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
4-Isopropyltoluene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
4-Methyl-2-pentanone
ND
mg/kg
0.0098
0.0074
1
7/18/01
10:07
J.Gott
8260B
9576
Methylene chloride
ND
mg/kg
0.0049
0.0037
1
7/18/01
10:07
J.Gott
8260B
9576
Naphthalene
ND
mg/kg
0.0049
0.0037
1
7/18/01
10:07
J.Gott
8260B
9576
n-Propylbenzene
ND
mg/kg
0.0020
0.0015
1
•
7/18/01
10:07
J.Gott
8260B
9576
Styrene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
i 1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Tetrachloroethene
0.0028
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Toluene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
82603
9576
I 1,2,3-Trichlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
I 1,2,4-Trichlorobenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,1,1-Trichloroethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,1,2-Trichloroethane
i
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Trichloroethene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
1,2,3-Trichloropropane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
-- 1,2,4-Trimethylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
1,3,5-Trimethylbenzene
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
-- Vinyl chloride
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Xylenes, Total
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260E
9576
Bromodichloromethane
ND
mg/kg
0.0020
0.0015
1
7/18/01
10:07
J.Gott
8260B
9576
Sample report continued . . .
2960 FUSTBR CREwin'ON DRIVE / NAsn%'n,i,F,'PN 37204 / 615-726-0177 / F\.x: 615-726-095.1 / 800-765-0980

LJ T � ri est me ca
�- I N C O R P O R A T E D
Y
I
ANALYTICAL REPORT
Laboratory Number: 01-A95100
Sample ID: GP 7-10-01-2
Project:
Page 3
Report Quan Dil
Analysis
Analysis
Analyte Result Units
------------------------
Limit Limit Factor
Date
Time Analyst Method Batch
----------- -------
Trichlorofluoromethane ND mg/kg
------- ------ ------
0.0020 0.0015 1
--------
7/18/01
----------------- --------- -----
10:07 J.Gott 8260B 9576
*GENERAL CHEMISTRY PARAMETERS*
Dry Weight 75. %
1
7/12/01
8:05 B. Powell CLP 8649
ND - Not detected at the report limit.
-----------------------------------------------------------------------------------
Sample Extraction Data
------------------------------------------
Wt/Vol
Parameter Extracted Extract Vol
---------------- --------- ----------- --------
Date Time
-----
Analyst
----------
Method
---------
Volatile Organics 6.8 g 5.0 ml
7/10/01 10:30
C.Bates
5035
Surrogate
% Recovery
Target
Range
1
- VOA Surr 1,2-DCA-d4
108.
50.
- 140.'
VOA Surr-Toluene d8
i
115.
75.
- 141.
VOA Surr, 4-BFB
101.
69.
- 131.
VOA Surr, DBFM
119.
76.
- 136.
# - Recovery outside Laboratory historical
limits.
Results for metals or Organic analyses, if requested, have been corrected for dry weight.
Sample report continued . . .
2960 Fos,rER CREimrroN DRIVE / NASIIVII.I,E,TN 37204 / 615-726-0177 / K, x: 615-726-0954 / 800-765-0980

TestAmerica
ANALYTICAL REPORT
Laboratory Number: 01-A95100
Sample ID: GP 7-10-01-2
Project:
Page 4
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
Report Approved By: Report Date: 7/18/01
I Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
! Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
i
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
End of Sample Report.
2960 FOSTER CREIGHTON DRIVE / NASFIVII.LE.TN 37204 / 615-726-0177 / F:%x: 615-726-0954 / 800-765-0980

TestAmerlca
-- INCO RPO RATED
ANALYTICAL REPORT
IT CORP-SUN 2337 Lab Number: 01-A95101
KIM PRZYBYL Sample ID: GP 7-10-01-3
2200 GATEWAY CTR. BLVD. STE205 Sample Type: Soil
MORRISVILLE, NC 27560 Site ID:
Date
Collected:
7/10/01
Project:
Time
Collected:
13:45
Project Name: SLS GREENSBORO
Date
Received:
7/11/01
Sampler: ELIZABETH VAN FLEET
Time
Received:
9:00
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
-----------
Units
-------
Limit
-------
Limit
------
Factor
------
Date
--------
Time
------
Analyst
-----------
Method
---------
Batch
-----
*VOLATILE ORGANICS*
Acetone
ND
mg/kg
0.0605
0.0424
1
7/18/01
10:43
J.Gott
8260E
9576
Benzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Bromobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Bromochloromethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Bromoform
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Bromomethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
2-Butanone
ND
mg/kg
0.0605
0.0424
1
7/18/01
10:43
J.Gott
8260B
9576
n-Butylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
sec-Butylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
t-Butylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Carbon disulfide
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Carbon tetrachloride
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Chlorobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
82603
9576
Chloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Chloroform
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Chloromethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
2-Chlorotoluene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
4-Chlorotoluene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0121
0.0085
1
7/18/01
10:43
J.Gott
8260E
9576
Dibromochloromethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2-Dibromoethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Dibromomethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2-Dichlorobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,3-Dichlorobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,4-Dichlorobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Dichlorodifluoromethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Sample report continued . . .
2960 Fos'rER CREi(;wr0N DRIVE / N;\iiIvii,I,N.TN 37204 / 615-726-0177 / K: x: 615-726-0954 / 800-765-0980

r
TestAmerica
I N C O R P O R A T E D
ANALYTICAL REPORT
Laboratory Number: 01-A95101
Sample ID: GP 7-10-01-3
Project:
Page 2
Report
Quan
Dil
Analysis
Analysis
Analyte
------------------------
Result
Units
Limit
Limit
Factor
Date
Time
Analyst
Method
Batch
1,1-Dichloroethane
-----------
ND
-------
mg/kg
-------
0.0024
------
0.0017
------
1
--------
7/18/01
------
10:43
-----------
J.Gott
---------
8260B
-----
9576
1,2-Dichloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,1-Dichloroethene
ND
mg/kg
0.0024
0.0017
1,
7/18/01
10:43
J.Gott
8260B
9576
cis-1,2-Dichloroethene
0.0149
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
trans-1,2-Dichloroethene
ND
mg/kg
0.0024
0.0017
1
7/18/01-
10:43
J.Gott
8260B
9576
1,2-Dichloropropane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,3-Dichloropropane
ND.
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
2,2-Dichloropropane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,1-Dichloropropene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
_ cis-1,3-Dichloropropene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
trans-1,3-Dichloropropene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Ethylbenzene
•ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Hexachlorobutadiene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
2-Hexanone
ND
mg/kg
0.0121
0.0085
1
7/18/01
10:43
J.Gott
8260B
9576
Isopropylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
4-Isopropyltoluene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
-- 4-Methyl-2-pentanone
ND
mg/kg
0.0121
0.0085
1
7/18/01
10:43
J.Gott
8260B
9576
Methylene chloride
ND
mg/kg
0.0061
0.0042
1
7/18/01
10:43
J.Gott
8260B
9576
Naphthalene
ND
mg/kg
0.0061
0.0042
1
7/18/01
10:43
J.Gott
8260E
9576
n-Propylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Styrene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1112-Te i tr achloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Tetrachloroethene
0.0051
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260E
9576
Toluene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2,3-Trichlorobenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
- 1,2,4-Trichlorobenzene
ND
mg/kg
0.0024
0.0017
16
7/18/01
10:43
J.Gott
8260B
9576
1,1,1-Trichloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,1,2-Trichloroethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Trichloroethene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2,3-Trichloropropane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
1,2,4-Trimethylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
II 1,3,5-Trimethylbenzene
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
- Vinyl chloride
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Xylenes, Total
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260B
9576
Bromodichloromethane
ND
mg/kg
0.0024
0.0017
1
7/18/01
10:43
J.Gott
8260E
9576
Sample report continued . . .
2960 Fosn.R CREwirrON DRIVE / NAS1R'11.1,F..TN 37204 / 615-726-0177 / Fix: 615-726-0954 / 800-765-0980

i - TestAmerica
�INCORPO RATE D
ANALYTICAL REPORT
Laboratory Number: 01-A95101
Sample ID: GP 7-10-01-3
Project:
Page 3
Report Quan Di1
Analysis
Analysis
Analyte Result Units
------------------------
Limit Limit Factor
Date
Time Analyst Method Batch
------------------
Trichlorofluoromethane ND mg/kg
------- ------ ------
0.0024 0.0017 1
--------
7/18/01
-------------------------- -----
10:43 J.Gott 8260B 9576
*GENERAL CHEMISTRY PARAMETERS*
Y Dry Weight 70. %
1
7/12/01
8:05 B. Powell CLP 8649
ND - Not detected at -the report limit.
-----------------------------------------------------------------------------------------------------------------------------
Sample Extraction Data
I Wt/Vol
i
Parameter Extracted Extract Vol Date Time Analyst Method
---------------------------------------- ------------------------
Volatile Organics 5.9 g 5.0 ml 7/10/01 13:45 C.Bates 5035
Surrogate % Recovery Target Range
----------- ---------- ------------
VOA Surr 1,2-DCA-d4 113. 50. - 140.
VOA Surr-Toluene d8 114. 75. - 141.
VOA Surr, 4-BFB 100. 69. - 131.
VOA Surr, DBFM 118. 76. - 136.
j- Recovery outside Laboratory historical limits.
Results for metals or Organic analyses, if requested, have been corrected for dry weight.
Sample report continued . . .
2960 FOSTER CRF.IGHTON DRIVE / N!�sHVn.I.E.TN 37204 / 615-726-0177 / F%.r: 615-726-0954 / 800-765-0980

Test[lmerica
ANALYTICAL REPORT
I N C O R P O R A T E D
Laboratory Number: 01-A95101
Sample ID: GP 7-10-01-3
Project:
Page 4
These results relate only to the items tested.
This report shall not be reproduced except in full and with
permission of the laboratory.
- Report Approved By: Report Date: 7/18/01
Paul E. Lane, Jr., Lab Director Gail A. Lage, Technical Serv.
_+ Michael H. Dunn, M.S., Technical Director Glenn L. Norton, Technical Serv.
Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv.
Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv.
Laboratory Certification Number: 387
I
I
End of Sample Report.
2960 FosTER CREWHTON DRIVE / M, sumi.E.TN 37204 / 615-726-0177 / F:kx: 615-726-0954 / 800-765-0980

To assist us In using the proper analytical methods,
Test merlca Divisiori/Laboratory Name: _ is this work being conducted for regulatory purposes?
I N C O A P O X A T E U
Compliance Monitoring
Client Name J-F C n2r7 ()-t:;
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Client#:
Address: 77:t'IA�Ah�
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City/State/Zip Code: VIA OU t ill l L_L_1e
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Project M
Project Manager: N
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Site/Location ID: ( ���/=� �G
State: Mc
Telephone Number: j Cj 1- (D 1 -
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Fax: L�(
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Report To:
Sampler Name: (Print Name)
V
Invoice To:
Sampler Signature:
Quote M PO#:
atrix Preservation & # of Contalner4
Analyze For:
TAT
Standard
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era es
_
_ Rush (surcharges may apply)
°=
3 ?
n
— None
Level 2
;s 9
_
Date Needed:
E
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(Batch QC)
Fax Results: N
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_Level 3
Level
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Other:
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SAMPLE ID
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REMARKS
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Special Inestructlona:
'I-•lo t,l lb ICJ
Date:: Time: Received
Date: Time: Received
Date: Time: Received
Date: (Time:
onMY ed
� 02�1�18'l8

IT CaToradon ofNorih Carolina, Inc.
A Member of The 17' Croup
Appendix C
Laboratory Analytical Data Reports - Soil Vapor Samples

Page 4 of 12
Order #: P0108371
Report Date: 09/10/01
- Client Proj Name: SOS Greensboro
i Client Proj #: 107535
Client Name: IT Corporation Lab Sample #: P0108371-03
Contact: Dave Lubell
i_. Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix Sampled Date/Time Received
SVMP-1 Vapor 23 Aug. 01 13:50 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
1,1,1-Trichloroethane
0.034
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1, 1 -Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
2.7
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
-1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
12-Dichloropropane'
<0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
916101
.Benzene
< 0.10
0.10
PPMV
mm
916101
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
'Carbon Tetrachloride
0.021
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.021
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis-1,2-Dichloroethene
0.020
0.010
PPMV
mm
9/6/01
'cis-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
< 0.10
0.10
PPMV
mm
9/6/01
- Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
280
0.005
PPMV
mm
9/6/01
Toluene
< 0.10
0.10
PPMV
mm
9/6/01
trans-1,2-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
trans-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.051
0.005
PPMV
mm
9/6/01
r--Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
';Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

_ - Order #:
Report Date:
Client Proj Name:
Client Proj #:
Page 3 of 12
P0108371
09/10/01
SOS Greensboro
107535
Client Name: IT Corporation Lab Sample #: P0108371-02
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix Sampled Date/Time Received
SUMP-2 Vapor 23 Aug. 01 13:33 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
1,1,1-Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
<0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1, 1 -Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Benzene
< 0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
Carbon Tetrachloride
< 0.005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.013
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
0 9/6/01
cis-1,2-Dichloroethene
0.031
0.010
PPMV
mm
9/6/01
cis- 1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
< 0.10
0.10
PPMV
mm
9/6101
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
24
0.005
PPMV
mm
9/6/01
Toluene
<0.10
0.10
PPMV
mm
9/6/01
trans- 1,2-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
trans- l,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.029
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gatewav Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix
SUMP-3 Vapor
Order #:
Report Date:
Client Proj Name:
Client Proi #:
Page 2 of 12
P0108371
09/10/01
SOS Greensboro
107535
Lab Sample #: P0108371-01
Sampled Date/Time Received
23 Aug. 01 13:10 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
'1,1,1-Trichloroethane
<0.005
0.005
PPMV
AM4.02 mm
9/6101
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
,1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
916101
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
- ' 1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Benzene
<,0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
Carbon Tetrachloride
< 0.005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.009
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis- 1,2-Dichloroethene
0.018
0.010
PPMV
mm
9/6/01
cis-1,3-Dichloropropene
<0.01C
O.010
PPMV
mm
9/6/01
Ethylbenzene
< 0.10
0.10
PPMV
mm
9/6/01
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
8.4
0.005
PPMV
mm
9/6/01
Toluene
0.12
0.10
PPMV
mm
9/6/01
trans- 1,2-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
trans-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.020
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
I, ,Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Page 7 of 12
Order #:
P0108371
Report Date:
09/10/01
Client Proj Name: .
SOS Greensboro
Client Proj #:
107535
Lab Sample #: P0108371-06
Morrisville, NC 27560
Sample Description
Matrix
Sampled Date/Time
Received
SVMP-4
Vapor
23 Aug. 01 14:48
27 Aug. 01
Analyte(s)
Result
PQL
Units Method #
Analyst Analysis Date
RiskAnally is
Vapor
1,1,1-Trichloroethane
< 0.005
0.005
PPMV AM4.02
mm
9/6/01
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
0.021
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane -
0.056
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
`Benzene
0.38
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
Carbon Tetrachloride
< 0.005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
�Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.030
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis-1,2-Dichloroethene
0.35
0.010
PPMV
mm
9/6/01
cis-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
<0.10
0.10
PPMV
mm
916101
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
25
0.005
PPMV
Ulm
9/6/01
Toluene
0.83
0.10
PPMV
mm
9/6/01
trans- 1,2-Dichloroethene
< 0.010
0.010
PPMV
nun.
9/6/01
;trans-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.17
0.005
PPMV
mm
9/6/01
---Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
(Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Page 6 of 12
Order #: P0108371
Report Date: 09/10/01
' Client Proj Name: SOS Greensboro
Client Proj #: 107535
Client Name: IT Corporation Lab Sample #: P0108371-05
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix Sampled Date/Time Received
SVMP-5 Vapor 23 Aug. 01 14:30 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalxsI
Vapor
1,1,1-Trichloroethane
<0.005
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
<0.005
0.005
PPMV
mm
9/6/01
1,12-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
<0.010
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
- 1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
916101
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
'Benzene
<0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6%O1
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
Carbon Tetrachloride
0.006
0.005
PPMV
mm
9/6/01
_ Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
- Chloroform
0.23
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis- 1,2-Dichloroethene
0.18
0.010
PPMV
mm
9/6/01
cis-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
0.18
0.10
PPMV
mm
9/6/O1
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
800
0.005
PPMV
mm
9/6/01
Toluene
0.31
0.10
PPMV
mm
9/6/01
trans- 1,2-Dichloroethene
0.015
0.010
PPMV
mm
9/6/01
trans- l ,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.46
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
i Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix
SVMP-6 Vapor
Page 5 of 12
Order #:
P0108371
Report Date:
09/10/01
Client Proj Name:
SOS Greensboro
Client Proj #:
107535
Lab Sample #: P0108371-04
Sampled Date/Time Received
23 Aug. 01 14:10 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
.1,1,1-Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
'1,1,2,2-Tetrachloroethane
<0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
<0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
,1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01.
1,4-Dichlorobenzene
< 0.070
0:070
PPMV
mm
9/6/01
Benzene
<0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
!Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
-'Carbon`Tetrachloride
0.006
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
j iChlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.26
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis-1,2-Dichloroethene
1.5
0.010
PPMV
mm
9/6/01
,cis-1,3-Dichloropropene
0.013
0.010
PPMV
mm
9/6/01
Ethylbenzene
0.12
0.10
PPMV
mm
9/6/01
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
710
0.005
PPMV
mm
9/6/01
Toluene
0.20
0.10
PPMV
mm
9/6/01
trans-1,2-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
trans-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.97
0.005
PPMV
mm
916/01
-- Trichlorofluoromethane
< 0.005
0.005
PPMV
mm _
9/6/01
'Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix
SVMP-7 Vapor
Page 10 of 12
1 Order #:
P0108371
Report Date:
09/10/01
Client Proj Name:
SOS Greensboro
Client Proj #:
107535
Lab Sample #: P0108371-09
Sampled Date/Time Received
23 Aug. 01 15:40 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
` RiskAnalysis
Vapor
1,1,1-Trichloroethane
<0.005
0.005
PPMV
AM4.02 mm
9/6/01
- 1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
_- :1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
- ,1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Benzene
< 0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
Carbon Tetrachloride
0.007
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.081
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
!cis-1,2-Dichloroethene
0.058
0.010
PPMV
mm
9/6/01
- cis-1,3-Dichl6ropropene
< 0.010
0.010
PPMV
mm
9/6i01
Ethylbenzene
<0.10
0.10
PPMV
mm
9/6/01
,Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6i01
Tetrachloroethene
1300
0.005
PPMV
mm
9/6/01
Toluene
0.12
0.10
PPMV
mm
9/6/01
trans-1,2-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
trans- 1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.36
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
(Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix
SVMP-8 Vapor
Page 9 of 12
Order #:
P0108371
Report Date:
09/10/01
Client Proj Name:
SOS Greensboro
Client Proj #:
107535
Lab Sample #: P0108371-08
Sampled DateMme Received
23 Aug. 01 15:21 27 Aug. 01
' Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
1, 1, 1 -Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1-Dichloroethane
0.077
0.010
PPMV
mm
9/6/01
'',1,1-Dichloroethene
0.020
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
,1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
rBenzene
< 0.10
0.10
PPMV
mm
9/6/01
- Bromodichloromethane
< 0.005
0..005
PPMV
mm
9/6/01
_ Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9%6/01
Carbon Tetrachloride
0.007
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
'- Chloroform
0.23
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
j ,cis-1,2-Dichloroethene
0.80
0.010
PPMV
mm
9/6/01
cis- 1,3-Dichloropropene
< 0.010
0.010
PPMV
Ulm
9r6 01
Ethylbenzene
<0.10
0.10
PPMV
mm
9/6/01
,Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
.Tetrachloroethene
1100
0.005
PPMV
mm
9/6/01
Toluene
0.96
0:10
PPMV
mm
9/6/01
^,trans-1,2-Dichloroethene
0.034
0.010
PPMV
mm
9/6/01
1 trans- l,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.70
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
I 'Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description
SVM P-9
Matrix
Vapor
Page 8 of 12
Order #:
P0108371
Report Date:
09/10/01
Client Proj Name:
SOS Greensboro
Client Proj #:
107535
Lab Sample #: P0108371-07
Sampled Date/Time Received
23 Aug. 01 15:05 27 Aug. 01
Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
1,1,1-Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1, 1 -Dichloroethane
0.083
0.010
PPMV
mm
9/6/01 -
1,1-Dichloroethene
0.022
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
- 1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/0 i
'Benzene
2.0
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
Bromomethane and Chloroethane
< 1.0
-1.0
PPMV
mm
916101
Carbon Tetrachloride
< 0.005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.008
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis-1,2-Dichloroethene
0.050
0.010
PPMV
mm
9/6/01
cis-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
0.62
0.10
PPMV
mm
9/6/01
Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
Tetrachloroethene
14
0.005
PPMV
mm
9/6/01
Toluene
7.0
0.10
PPMV
mm
9/6/01
trans-1,2-Dichloroethene
0.030
0.010
PPMV
mm
9/6/01
trans- 1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.069
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

Client Name: IT Corporation
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix
SVMP-10 Vapor
Page 11 of 12
Order #: P0108371
Report Date: 09/10/01
Client Proj Name: SOS Greensboro
Client Proj #: 107535
Lab Sample #: P0108371-10
Sampled Date/Time Received
23 Aug. 01 15:58 27 Aug. 01
Analyte(s)
'
Result
PQL
Units
Method # Analyst Analysis Date
I I
RiskAnalysis
Vapor
'1,1,1-Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
'1,1-Dichloroethane
0.074
0.010
PPMV
mm
9/6/01
1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
916101
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
916101
{ ! 1,2-Dichloropropane'
< 0.010
0.010.
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Benzene
< 0.10
0.10
PPMV
mm
9/6/01
Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
- , Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
;Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
9/6/01
'Carbon Tetrachloride
< 0:005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
iChlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
'Chloroform
< 0.005
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis- 1,2-Dichloroethene
4.1
0.010
PPMV
mm
9/6/01
cis- 1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
1.2
0.10
PPMV
mm
9/6/01
'Methylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
.Tetrachloroethene
20
0.005
PPMV
mm
9/6/01
Toluene
2.3
0.10
PPMV
mm
9/6/01
trans- 1,2-Dichloroethene
0.041
0.010
PPMV
mm
9/6/01
trans- 1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
0.84
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
',Vinyl Chloride
< 3.0
3.0
PPMV
mm
9/6/01

i
Page 12 of 12
Order #: P0108371
Report Date: 09/10/01
Client Proj Name: SOS Greensboro
Client Proj #: 107535
Client Name: IT Corporation Lab Sample #: P0108371-11
Contact: Dave Lubell
Address: 2200 Gateway Center Blvd
Suite 205
Morrisville, NC 27560
Sample Description Matrix Sampled Date/Time Received
SVMP-12 Vapor 23 Aug. 01 16:15 27 Aug. 01
' Analyte(s)
Result
PQL
Units
Method # Analyst Analysis Date
RiskAnalysis
Vapor
1,1,1-Trichloroethane
< 0.005
0.005
PPMV
AM4.02 mm
9/6/01
- _ 1,1,2,2-Tetrachloroethane
< 0.005
0.005
PPMV
mm
9/6/01
1,1,2-Trichloroethane
< 0.005
0.005
PPMV
mm
9/6/01
j ;1,1-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
i_J1,1-Dichloroethene
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,2-Dichloroethane
< 0.010
0.010
PPMV
mm
9/6/01
1,2-Dichloropropane'
< 0.010
0.010
PPMV
mm
9/6/01
1,3-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
1,4-Dichlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Benzene
< 0.10
0.10
PPMV
mm
9/6/01
-'Bromodichloromethane
< 0.005
0.005
PPMV
mm
9/6/01
,- ,Bromoform
< 0.005
0.005
PPMV
mm
9/6/01
j !Bromomethane and Chloroethane
< 1.0
1.0
PPMV
mm
916101
Carbon Tetrachloride
< 0.005
0.005
PPMV
mm
9/6/01
Chlorobenzene
< 0.070
0.070
PPMV
mm
9/6/01
Chlorodibromomethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloroform
0.009
0.005
PPMV
mm
9/6/01
Chloromethane
< 1.0
1.0
PPMV
mm
9/6/01
cis-1,2-Dichloroethene
4.6
0.010
PPMV
mm
9/6/01
,! cis-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Ethylbenzene
< 0.10
0.10
PPMV
mm
9/6/01
Nethylene Chloride
< 2.0
2.0
PPMV
mm
9/6/01
7etrachloroethene
440
0.005
PPMV
mm
9/6/01
Toluene
<0.10
0.10
PPMV
mm
9/6/01
Itrans-1,2-Dichloroethene
0.085
0.010
PPMV
mm
9/6/01
(trans-1,3-Dichloropropene
< 0.010
0.010
PPMV
mm
9/6/01
Trichloroethene
3.5
0.005
PPMV
mm
9/6/01
Trichlorofluoromethane
< 0.005
0.005
PPMV
mm
9/6/01
Chloride
< 3.0
3.0
PPMV
mm
9/6/01
JVinyl

ly
CHAIN,- OF - CU§TODY RECORD
P14.60; 01 0204M ' Uqose.*epS,: Inc,W :220:WWWO: Pitt# ... --:.P1ttsburh,P-A15238 FAX N
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Company
Co. Address I E144Y 0 1>,110"_ N-162 AhV?_PL-'1j.1U I P1 -A
Proj. Manager:
Proj. Location: Vrb'I Sal IN"
Proj. Number:
Phone # Fax �J' Ij -
nature
Sampler's signat
Results to
f K10
1\,c
Invoice to
C11-
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Cooler ID',:
,w
s"k. ID:::
.;:'S4qVj0 Descrtpgda
Dolt
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Cont.
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2,
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Relinquished by,..
Company
Date
Time
Received by
Company
Date:
Time
It
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11. 1 4N-4
J'.
) V,
Relinquished by
Company
Date
Time al
c'c,:ivcd by: f
Company
Date
Time:
J.i
Relinquished by
Company
Date
Time
I ect I ived by
Company
Date
Time
WHITE COPY : Accompany Samples YELLOW COPY; Laboratory File PINK COPY: Submilter

IT Corporation ofNorih Carolina, Inc.
A Member of The IT Croup
Appendix D
Field Data Sheets - Phase I Full Scale ISCO Injection

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S(o� ( J _� _ Project Number:
Site Location: r o r:! IT Personnel:
Date: _ Ct Subcontractor: rrC
Injection
Probe Advancement
Injection Interval Field Monitoring Data
Point
3
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
�'
Z (
z7 .
v
8-12
15
o
(Zo
So
^
12 - 14
14-20
(o
I ("lot
25
1a —
20 - 24
30-
24 - 28
35
' o
28 - 32
40
W
b
I CI-s
32 - 36
45
i �i
o
I
3 Z,
3 Z
36 - 40
50
40 - 44
55
44 48
t�P�
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake _ In clio Tool
60 - 64
- Injection Method: Top -Down B o up
Comments:
V\ of.111

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: �v ��� Project Number:
Site Location:IT Personnel: .��..
Date: (y l.ci Subcontractor:
Injection
Probe Advancement
Injection Interval Field Monitoring Data
Point Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initlal
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
S„ 0-4
1 V
5
4-8
10
8- 12
15
_
12 - 14
20
y
-��
5 . a
14-20
25
•
�•U
OtU
20 - 24
30
Q
—
' v
OD
'�
24 - 28
35
(0
28-32
40
�.0
vO-lue
J�
32-36
36 - 40
50
40 - 44
55
44 - 8
00
60
48 - 52
64
52 - 56
Type of Oxidant Injected., Sodium Permanganate Form of Oxidant Liquid
56 - 60
60 - 64
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake _In c n Tool
Injection Method: Top -Down ottom-u
Comments: -
�•%c'. �_,r'�-.S ��Uj� 1��,_�..�_Jl {�� Ic��-,_a� ((�TcC,�V� t �.J'-�--�, -(�..� �-� n-;.n,i`�� � I.. �c�(c.-.�

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: 5eC,, S S�S Project Number:
Site Location: `� S �o�, o, (� IT Personnel: cis
Date: Subcontractor: (
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (R)
Start
Time
Ir�itsial
HHewmeter
Stop
Time
Final
ft�
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
lS3
5
4-8
10-
8-12
15
-
12-14
20
0IOpZ
SS
�S.0
�Op
—
14-20
25
O
Z
�a�c1
��
j�U
—
s
20 - 24
30
p
3
ZS
O D
24 - 28
35
28 - 32
40
1 T19
d
Z
to
ZfU •.
32 - 36
45
3 v
0
36 - 40
50
I �oS�
10 O
(�
toS
40 - 44
55
44 - 48
60
48 - 52
1
64
-52 - 56
X003
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake lnjecO Tool
60 - 64
_
Injection Method: Top -Down Bo om up
Comments:
of, a n- -- �� .: � P �� a �. CO (S3� I,c�i n C" .�e (C� I
(-ro����.
�)e
uSe_�
'Csfi'�
-L.,, fir,f r, e.

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S�
Site Location: —(a cni L NC
Date: o
Project Number:
IT Personnel: C
Subcontractor:
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
m_rInittal L
FloAgrleter�^^
Stop
Time
Fiq IT
r�loaun�tect
Total Gallons
Injected
Injection
Pressure
Back
Pressure
3(0
0-4
p
5
4-8
10
ZvJ
(
S
d
8-12
15
OO
12-14
20
�22i
2 S
1 Z
ZL)
���
9)"-)
14 - 20
25
2
I
I o c,
3
U 0
20-24
30
o3b
3
�y
3(v
>>
too
24-28
35
0��-
28-32
40
up
ylj
O i3
�%�1
3S
(o v
32 - 36
45
CK1,A
36 - 40
50
40 - 44
55
44 - 48
60
Sou
Zio
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
injection Tools: Geoprobe: Injection Tip _ Mill -Slot Intake Inj ction ool
Injection Method: Top -Down B tto -up
60 - 64
Comments:
k, (1
(I
{j . P e,--, -c%X `,,, ��� — ��r 4, ~ti2,
7o'jt.

FORM 2
cPhase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: SPS�� JL,� Project Number:
Site Location:IT Personnel:
Date: Subcontractor:
AL -
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
-F 16r.
Stop
Time
Finial_
Flawniefer
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
ILI
0
M 613,
8-12
15
1 o1
3
b 11 MM
59P
0O
12-14
20
'-,g-
S
G�
—
14-20
25
ow�S
0lcck
C7
,,
� Qp
20 - 24
30
S
0 o
�Q _
t �`
� v 0
24 - 28
35
o Cl
Cto
�0 0
28 - 32
(4
)
--
32 - 36
45
36 - 40
50
40-
7/
�ja
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
_ _
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake Inj ti TO
60 - 64
_
Injection Method: Top -Down t m-up
rnmman►c

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S�t (A' I-S SLR Project Number:
Site Location: r a — N IT Personnel:
Date: p ` Subcontractor:
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
AFdo
Stop
Time
Final
AR+r�
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
8 - 12
15
12 - 14
20
14-20
25
20 - 24
30
24 - 28
35
28 -32'
rh
40
32 - 36
45
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected_: Sodium Permanganate Form of Oxidant Liquid
56 - 60
_
Injection Tools: Geoprobe: Inj ti Ti �l Mill -Slot Intake_
60 - 64
_
lInjection Method: Top -Down Bot om
Comments: A
StIA C N-M4
011 II
1 �I , �t �.nn',�. o �{ P ct t✓(� iVti
Ed
�1i1 (-� A� � •� j
A
F� ti r
u(

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: �Cct(S Project Number:
Site Location: o N C IT Personnel:
Date:—jaz�1p ` Subcontractor:
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
n ti I
r
Stop
Time
Final
El
Total Gallons
Injected
Injection
Pressure
Back
Pressure
`{
0 - 4
5
4-8
10
egO
8-12
15
`
-zoo3j
n
12-14
20
,
O
`
5
L-t
U
14-20
25
0-
r'
a U
0
20 - 24
30
; Z
�
� Z
,it!
7A 13
�S
24 - 28
35
. �0
-SHID
35NO
—
28-32
40
'4`i
32 - 36
45
36 - 40
50
40 - 44
55
44 —W
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake In' coon Too
60 - 64
Injection Method: Top -Down B Cto p
Comments:
1 nn
C/
-5— —I i�>

FORM 2
Phase I:Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S�_� �(� Project Number: I U 7rj72 )
Site Location: = IT Personnel: 1 ) (I go J_
Date: _ �P: �2_! Subcontractor:-( , F () J_rl(t,i r
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
—'-�-
4-8
10
1033
-7 315
-3t57
4 -- C 7
--
8 - 12
ISA
15VI
15
- 2,
73�
IDO
Ly
12 - 14
20
%SU
605
1-5-5-j
w
f 2a
- --
14 - 20
25
ivo
A
20 - 24
30
fAD5-
140
24 - 28
3
U
1?_0 00
�-
28 - 32
40
32 - 36
45
36-4
50
44
55
44 - 48
60
48 - 52
64
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid60
k6052�56
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake Injection Tool
- 64ti
Injection Method: Top- overt k3 p)
Comments:
10 7011,
S t0 --
j�
✓i'
NI} f„
b
F

FORM 2
Phase 1 Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S J �L� Project Number: �y�_7�� �"�Lj� —t)_�
Site Location: IT Personnel:
Date: L 21 'ol Subcontractor: l7l 1�11^�=sIL 5' ,lY
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
_fJpiawz=r
Stop
Time
.�j�inal
416WRi6ter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
4-8
10
1JVqj
(�
--
8 - 12
15
14 - 20
25
�
n
; -
20 - 24
30
24 - 28
35
`_7
g
28 - 32
40
t-
32 - 36
45
36 - 40
0
40 - 44
55
44 - 48
60
48-52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake Injection Tool
60 - 64
1
lInjection
Method: Top -Down ottorn-u
r'
4-120 i'f4�Purf'
e-
5 (G
S Cv
s to
7 �7J
5 /U

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
f
Site Name: Project Number: I v 5X-
Site Location: IT Personnel: i , L U a ^ �
Date: 1 'O Subcontractor:_(,'C�t?�-(?L1(�'
Injection
Probe Advancement
Injection
Interval Field Monitoring
Data 020 ;
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
F,p
QFW Fvf'�
4-8
10
8 - 12
15
12-14
20
Q(
I
14 - 20
25
Oaf
"�
t' 0
20 - 24
30
on-
2E'�
S
24-28
35
60
00
�b0
28 - 32
40
7 !(1
'�
D Z,O
32 - 36
36 - 40
50
40 - 44
^
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Li
56 - 60
Injection Tools: Geoprobe: Injection Tip ill -Slot Intak --Injection Tool
Injection Method: Top -Down Bott m-u
60 - 64
Comments:
Wn N
fty�T

FORM 2
c (Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Seq( JI'S Project Number:
Site Location: r �S r C. IT Personnel:
Date: A 1, , Subcontractor: L
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (k)
Start
Time
Initial
Ffedritteter
Stop
Time
Final
f4L�
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
UJ'Gp
5
4-8
10
o
�j
U
8-12
15
A40
12 -14
20
0t)
4i�L�1V
Z
2')()
14-20
25
Zv
u
20 - 24
30
-- —
�-
24-28
LA kv
oq
�0
v
28 - 32
40
32 - 36
45
36 -AT
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake InjoToo_ I
Injection Method: Top -Down B 9Eo up
56 - 60
60 64
Comments:
r'w-�
�u( ii1 u ��,✓
O
v
t4 At
�.. A- 'o %C (: 7 .1 (t opt. Ji(• rt lc.-. � l�:.f•-/,
r,��t ��., ���-^ T> � GC(f,:� -�-r � r`I(rPr-• I t-(tl �(.l.,IiKfl,�� 1-

^/
FORM 2 '
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name:
Site Location:
Point
Depth I Start Stop Injection Start
Time I Time 04 Time
ProjectNumber:
,/0 Z—
IT Personnel: --'
Sui
|ndla|
Flowmeter
r%-
Oil Back
re Pressure
'
'
Sodium permu &—e—o—probe. Injection Tip �M
|
—— meuio^Tool--
Top -Down It. -un
,Bottom up
Comments:
o��^J

�? ; ; f- s. `� FORM 2 ' G ���a✓
4
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Lp,.�' Project Number:
Site Location: IT Personnel: L G
Date: o?,� p/ Subcontractor:
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
�,^�� E: iQel
0-4
4-8
5
10
i•-
i
/
8 - 12
15
'3
C, OCR
3 S
/own
12 - 14
20
lt�o`.��
S—c J
/c�U
14-20
25
3S
/ /O140
20 - 24
30
�
24 - 28
35
0
28 - 32
40
32 - 36
45
- 40
Q
50
- 44
55
i•
44 - 48
60
02 Q
48 - 52
64
_._-
-_
52 - 56
56 - 60
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
Injection Tools: Ge probe: Injection Tip Mill -Slot Intake Injection Tool
Injection Method: Top -Down Boltom-u
60 - 64
Comments:

f
FORM 2q
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: C ����z—_�. , r;� p Project Number: /0 7
Site Location: IT Personnel: C L a
/ba e: �� _ ' / Subcontractor: PaL o ; C '' `- i o..Q
Injection
-Probe Advancement
Injection
Interval Field Monitoring Data
Point
—15
Depth
Start
Time
Stop
Time
Injectloii
Depth (h)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
,s
5
4-8
10
8 - 12
15
12-14
20
w
D
14 - 20
25
20 - 24
30
Q
24 - 28
35
28 - 32
40
45
L
36 - 40
50
40 - 44
55
44 - 48
60
48-52
64
52 - 56
Type of Oxidant Injected: o ium Ferman anate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake Injection Tool
60 64
Injection M,;fhod: Top -Down Bottom -up
Comments:
70--�Xz- h. C:)
-6o-

�2-�
5*-13) 25)
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: _ -- yr �L� I ) Project Number: I U ? J 35-
Site Lo(ation: IT Personnel: T)- LU (Xl-L
Date: s Subcontractor: (1,FlALoGf
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
(pi 7 0
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
3c'
5
4-8
10
8 - 12
15
1
5<QQ
oil i&
7�
00
12 - 14
20
1ZZD
I
W-'
;D
14 - 20
25
y f U
2fl
Sy
lip
20 - 24
30
%
ll
V
--
24 - 28
35
)
28 - 32
40
32 - 36
45
36 - 40
(
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip ill -Slot i ke Injection Tool
60 - 64
Injection Method: Top -Down Bottom -
Comments:
fA2C)
5 �

2(
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Project Number:
Site Location: IT Personnel:
Date: li ?��� Subcontractor: (�-�I
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
149t
4-8
10
'--
--
--
--
8 - 12
15
/,7
SOW
q
�--
12-14
20
'
)
DO
14 - 20
25
0
_)
JC0-
20 - 24
30
_3
U
--�
24 - 28
35
28 - 32
40
32 - 36
"lj
45
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
56 - 60
Type of Oxidant Injected: Sodium Permanganate _ Forin of Oxidant Liquid-
Injection Tools: Geoprobe: Injection Tip ill -Slot Intake Injection Tool
Injection Method: Top -Down oltom-up
60 - 64
Comments:
3U'
V

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Project Number: (�- 3rj
Site Location: �� IT Personnel: `(], Uf ac L
Date: (o �[�` Subcontractor: _I-(� 61E _c�;�U j(Ulj
Injection
Probe Advancement
Injection Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
- -�
_
8 - 12
15(�
2
12 - 14
20
l
> rU
G'L��SINU
C4,�--
14 - 20
25
20 - 24
30
, i]-
24 - 28
5
28 - 32
40
32 - 36
45
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant
56 - 60
Injection Tools_ Geoprobe: Injection Tip Mill -Slot Inta Injection Tool
Injection Method: Top -Down ottom p
60 - 64
Comments:
P? D

FORM 2
05
Phase I Full Scale Sodium Pertnanganate Injection Monitoring Data Sheet
Site Name: S I,S Project Number: U753-T
Site Location: ��1�� IT Personnel: p Lj lriE�l
Date: ��(o.•�� Subcontractor: I dc— -San%
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
LS�01
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
t'
54-8
8
10
8 - 12
15
423
(
---
12-14
20
4ZQ
14 - 20
25
-
! �'
I QO--
20 - 24
3WSD
It)
24 - 28
28 - 32
40
32-36
�'-g
45
36 - 40
50
40 - 44
55
44 - 48
60
48-52
64
52 - 56
56 - 60
Typo of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
- —----------------------- --
Injection Tools: Geoprobe: Injection Tip till -Slot Intake Injection Tool_
Injection Method. Top -Down Bottom-. p
60 - 64
Comments: �- f MkP�Il►LtEA1t 1PInLVm r�r 7p,.T (V L �Ux �1'l.«I fAl he' A W t2 L ¢9 Akd 4 O,L,1l wd)
tE�aAL lc
Hz
11v`D�CQW
l�n

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Project Number:
Site Location: f rat n1 5 IT Personnel:
Date: �,r.e,2( d / Subcontractor: r-; t O C p
—7r
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
/
5
�^
4-8
10
\
8 - 12
15
12 - 14
20
/ (�
Rfl
14-20
25
20 - 24
0
24 -
28 - 32
t
40
32 - 36
45
36 - 40
50
40 - 44
55
ZZ
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: odium Perman anal of Ox_idgnt-Liquid��
56 - 60
60_64
1
1
_Form
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake ? Injection Too_ I
1 Injection Method: Top -Down <' Bottom -up
Comments:
loi—,/iC NzJ

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: BLS — G p_t�Enis'!�crz o Project Number: I CZ S-3�
Site Location: IT — IT Personnel: L
Date: ('� -2 G -Ld Subcontractor:
Injection
Probe Advancement
Injection Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter.
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
i
i
8-12
15
- —
12-14
20
i
c
14 - 20
25
5
O
20 - 24
3
( `v
24 - 28
28 - 32
5
40
32 - 36
2S
45
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
��
Injection Tools: Geoprobe: Injection Tip (Mil of intake j Injection Tool
Injection Method: Top -Down tom- �'----�
60 - 64
r-,,.,, —.- f �
f-7 vZ
SAP
� j�

e��,4 Vl�'
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: L Project Number:
Site Location: �'i�� ��= �' _ IT Personnel:
Date: r�� �/ Subcontractor: C �"
—T�
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0 4
3
5
4-8
10
8 - 12
15
12 - 14
20
O
00
14 - 20
25
l
/
O
<3
O
S
20 - 24
30
24-28
3
3
28 - 32
40
32 - 36
45
36
t
50
40 - 44
55
44 - 48
60
48-52
64
52 - 56
Type of Oxidant Injected. Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake _ Injection Tool
lInjection Method: Top -Down ('Bottom -up TC' — —
60 - 64 1
1
Comments:
r

FORM 2
i'.
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Project Number:
Site Name: Z-
IT Personnel:
Site Location:� �- � ZS'o , c7
Subcontractor:
n.ea•
7 - L,-- 4 �_,, (
Comments:

i t2-o
\ C. C,
FORM 2 NnA
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S 45 Project Number: • l n-7 c;3L�
Site Location: IT Personnel: 'D- (J,(2f-J
Date: �,.i -�� Subcontractor: C-,F-tJ L)61L - ;Tp-yr_-
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Tlme
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
10
8 - 12
15
all
1 2
-- --
12 - 14
20
-7qo
i w-:z -
5
N
—_
14 - 20
25
162.
35
20 - 24
30
1131
35�
o
—
24 - 28
5
110
Bqt5
1
I 1%p-7115
I
_-
28 - 32
40
1 DO
1
Q
--
4p
32 - 36
36 - 40
45
50
5_
315
)w
(C)o
---
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
I
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant
56 - 60
Injection Tools: Geoprobe: Injection Tip ill -Slot Intake Injection Tool
Injection Method: Top -Down Bottom up
60 - 64
Comments:
w4%fll�=Aff--
f (-2- U
--T-07GC77q\,/

;_� �L tnCk)
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: .S-S Project Number: m753,
Site Location: a=3 IT Personnel: 'D, _
Date: %2,7-Q( Subcontractor: -EfL(sc 'SE1
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
Ibm5
4-8
10
8 - 12
15
12 - 14
20
17
W
_
55
14-20
25
43
S
20 - 24
3
J
npp
17 3
24 - 28
35
28 - 32
40
32 - 36
45
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
1
64
52 - 56
Type of Oxidant Injected. Sodium Permanganate Form of Oxidant
56 - 60
_
Injection Tools: Geoprobe: Injection Tip Injection Tool
60 - 64
Injection Method: Top -Down - Bottom-u
Comments:
F?S� n1Piti�,fl l Gt�Y»r���', riN In
a 2_0
TfzC1,it_P
qz-c>
5�jo

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: >�I2`J Project Number: I b7rj j
Site Location: j If IT Personnel:
Date: & L7`bl Subcontractor: C''%LLC,:gC , — /atU lU�
Injection
Probe Advancement
Injection
Interval Field Monitoring Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
f
0-4
5
4-8
10
8 - 12
15
��
"—
12-14
20
b
S
��{ll
r5�
31
14 - 20
25
970
_31"'
140—
S
20 - 24
30
(p
S
24 - 28
35
��ZZ
fo'(S
S
-�
5
28 - 32
722
IyEd
(015
41�
105'--
5
32 - 36
/,
36 - 40
50
40 - 44
55
44 - 48
60
48 - 52
64
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidant Liquid
56 - 60
Injection Tools: Geoprobe: Injection Tip Mill-Slo Intake Injection Tool
60 - 64
_ _
Injection Method: Top -Down Bottom -up
Comments:
_J

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
SL� Project Number.
Site Name: ,
IT Personnel:
Site Location: �f���
Subcontractor
Date:
Injection Probe Advancement In action interval Field Monitoring Data
Final Total Gallons Injection Back
Point�l Depth Start Stop T
Injection Start Initial top Pressure Pressure •_`� - /_ ______
T Time
Time Depth (it) Time Flowmeter Time Flowmetar Infected \
i
Injecifon Method., .. i*
Comments:
O
/CA-1—
101 a
0
r
�
i
Tool

Site Name: �CpR�
Site Location: �11P IO
Date: ( F6 -D
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Project Number: i o7,i3S
IT Personnel: _D _ A W_�,
Subcontractor: C--� E{-)i nc, i c,
Injection
Probe Advancement
Injection
Interval Field Monitoring
Data
Point
Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowm er
Stop
Time
Final
Flow t
Total Gallons
Injected,
Injection
Pressure
Back
Pressure
0-4
/
5
4-8
10
X
8- 12
15f
1,$(
l
12-14
20
i1
14 - 20
25
20 - 24
30
47—D
1 11
24 - 28
35
1 DILj
28 - 32
40
163
_
32 - 36
45
,
36 - 40
50
40 - 44
p'I
55
44 - 48
60
48 - 52
64
%
52 - 56
Type of Oxidant Injected: Sodium Permanganate Form of Oxidantliquid-,
56 60
—`:l
Injection Tools: I Geoprobe: Injection Tip Mill -Slot Intake Injection Tool
60 - 64
_ _
Injection Method: Top -Down —('Bottom-up
Comments: r p t
D �►� i)i <�� `f�n t � hlQ - <.I�x� ��P_!'t7i�l - (L'�i�h�ol m�� � nyt nl('h 0( _,

�L
FORM 2 -
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: t
Site Locatlon: ��EEra o c--
Oata:
Project Number:
IT Personnel..
Subcontractor.
-
Injection Probe Advancement
in
action inter
Point Depth
Start
Stop
injection Start
Initial
Stop
Time
Time
Depth (ft) Time
Flowmater
Time
0-4
V00
5
4-8
10
15
8 - 12
20
12-14
14 20
25
-
Z-7.30
/ /
20 - 24
30
24-28
35�
04
/
28 - 32
40
0
3
/ a�
32 - 38
45
50
70
36 - 40
55
OG
40 - 44
44 - 48
48 - 52
64
Type of oxidant injected:
odium Permangana
52 - W
56 - 60
!'��
Injection Tools:
Geoprobe:
n CCdon 1
0-_ 84
injection Method:
Top
WE
A

Site Name:
Site Location:
Date:
FORM 2
(f,�7uo�61
Phase l Full Scala 8odlum Petmanganats InJectlon Mon toring Data Sheet
Project Number• t
IT Penwnnel: k
Subcontractor: (, mi (__- S
comments:
[
Vi'a"m
�-2-D

'
FORM 2
Phase I Full Scale Sodium Permanganate Injection
Monitoring Data Sheet
�1
Project Number:
O
Site Name:
L
�
IT Personnel:
Site location;
'
Subcontractor,
Date:
a
In action Interval Field MonitoP;4j
Infection Probe Advancement
Stop
Injection
Start
Stop
initial p
Final
njection
Back
PressureTime
Depth
Start
Depth (ftjTime
4=lowmeter 11me
Flowmeter
ressure
Time
0-4
5
' --
4-8
10
8 - 12
15
12 - 14
20
25
14-20
30
20 - 24
35
24 - 28
40
/off/
8 D O28-32
S
/ 6 D
32 - 36
45
36 - 40
so
�s�=
� �
i cS
�/ i b
�sS
40-44
55
P v
O 9a
44 - 48
60
>C
—
48-52
64
Form of Ozldan IquidD
52 - 56
T of Oxidant In ted:
Sodium Perms
IN Slot Intake
Injection Tod
58 - 60
90
IrVection Tools:
Geopr— Injection Tt
_
80 - 84
Injection Method:
Top -Dawn
BQttom-u
Comments:
�- )
i ;

i
FORM 2
Phase I Full Scalu Sodium Permanganate Injection Monitoring Data Sheet
Site Name. LS Project Number:
81te t_ocatton: � IT Personnel: T) u
Gate: subcontractor ' > > W'
���
ter,.Sri.��►.i..�rriir..rr.�irr.����r�
��r��rrr�r�����rrrr�ri►.�
..
r�
��
`• a/1 M • •/'1 1MAW
/ • Ir. 1 ..•
Comments.
d2o
w
24b
� j�
34s
3bc
y/s

FORM 2
Phase I Full Scale Sodium Permanganate injection Monitoring Data Sheet
Site Name: SEC-
IT Personnel: Project Number: I V 75
LL
Site Locative: 1
I Subcontractor: �" f� FJ( S► _ 5 %� f1 n
Date: l
In ectlon Interval Fief
atop
Injection Probe Advancement
injection
Start
Initial
Point Depth Start Stop
Time Time
Depth (ft)
Time
Flowmeter
T
0-4
5
4-8
10
8-12
12 - 14
15
I r
s
20
25
14-20
20 - 24
30
1 Z1 l
24 - 28
35
28 - 32
40
32 - 36
45
36 - 40
50
I Z `
40 - 44
55
1 1 D
44 - 48
60
0
48-52
52 - 56
T or ox ent
Infected. Sodium Pernu
56 - 60
injection Tools: Geo
60 - 64
In%ection Method: Top
Comments:
ata
otal Gallons injection
'ejected Pressure
i'�
I --
�
...
D
ti�

N
FORM 2 1 "
Phase I Full Seal* SOCHUM P*rmang&n*W NOW" Monitoring Data Shoot
; (�c - I (v 1-1) 3 o r Prolod Number
Site Nwne rl,� __ ---
aim location: ITPersonntf.
w.
Data: 7- 3-
subconb*c
Probe
AdvarwwrA"'A
immf
n
ectlon kv Field Mo i
Data
Iron
Mint D"2th I
Mot
Thus
stop
TUM
Start
Tin"
tnttlal
Flowmew
stop
Tlnw
Mel
FkwmwW
TOW Ga"O"
Ml«
"Oction
Prow"
back
Pre"Uro
0-4
"aD
4-8
10
B-12
15
12-14
20
_31
17'if_i
17?_
U - 20
20-24
25
30
1740
JILL
5
24 - 2b
36
28-32
40
32-36
Cl
I-'
3 go
38-40
40.44
50 q21
5
a4
Of or 14boted,
k Toots:
-*P!W—
So&mn Pomwomia*
/131
4ection TIP
If -
(7
Fbim of OW@nt
MNF Skit ift;
W400W Tod
44-48
4a - 52
56
&D
a4
�=
Afo&3d.,
lw.;�= _.-
- __p@_ ('
-
commeaft:
.1 20.
-4
4
_4

' FORM 2
Site Name:—�-�
Bit* Location:
Date,
Phase t Full Scala Sodlum Permanganate Infection Monitoring Data Sheet
Project Number:
IT Pommel.
{r►jact{on Probe
PointDepth
d
12 -14
14-2025
20 - 24
arc-2g
Advancerrwnt
Start
Time
stop
k*ocdm+
15
30
Start
Timeme
NNI
2'
2
I
tnttial
3
30
lion Interval
Stop
Ti
!7
?$
f(
Flew Mona
Final
Fdowmebsr
423
S
Data
Total Gallons
Mj
3�
2,
3S
injectloa
Pressure
f)(
I
,>
back
Pressure
,. .; .
j.
Aftwo"Goomn
46
50ir
64
is
32-36
38-�
40 - 4'{55
48 - 52
52 - 86
a
/VoclAbn
of o�lxldW t d: Sodium PenrzanAana>e Fnmt o/ Oxidant
Tools: eclion _._ "Sid Intake M Toad
AWW. ' soft u
08 - 80
80 - B4
Comments: _ r
�•l�•j� ,r, r�1�n✓' iS � >>:� �-!Ai;� 1 � r ,i •'1 rah v ��0 ���,n�1 l ( i � ,
, , ! , ; , P
Ii,(:>•
11 jiEc I l ill i
�--15
-v
SS
5 S'
5"S
J

W4� 1
FORM 2 4yv
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: S L S Project Number: / o r-
7� �a —� IT Personnel•
Site Location: 2 --�
r.
Subcontracto
Date:
In action Interval Field Monitorin
Data
Jett on Probe
Advancement
Initial
Stop
Final
Total Gallo
injection
Back
Point Depth
Start
Stop
Injection Start
Depth (tt) Time
Flowmeter
Time
Flowmeter
Injected
Pressure
Pressure \
Time
Time
--
_ 0-4
/
5
c
_--
4-8
10
8 -12
15
,3
12 - 14
20
/n
14 - 20
25
20-24
30
24 - 28
35
28-32
40
45
32-36
50
36-40
o�
40 - 44
55
44 - 48-
48 - 52
84
of Oxidant Infected:
odium Permanganate
Form of oxidant liquid
--
_
Injection Tool
-
Injection Tools:
t;eo
to coon Tip
-Slot lnt3ks�
—
—
60 - 64
/
Injection Method:
Top -Down
Comments:

FORM 2
Phase 1 Full Sceie Sodium PerrttanWmats Injection Monitoring Data S[wW
Site Namr: i ) h 5 Proleat Kuaber: () I Cl 3 5
Sfta Location: r 1 / h -1 �/ rf Parsomoi: T)I I R* I
Dab ;� ? D ( Subaonb*ctar: (= rat �r ► = �l�
r��r�iz�re�
c��■w��rr�rr�r�r�
commenft:
_2

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: ✓
Site Location: �— U
Date:
Project Number: /
IT Personnel: G _
Subcontractor. t�U C vim; �� x�L o�J✓ %o .
Injection Probe Advancement
Point Depth Start Stop
Time Time
0-4
In
Injection start Initial
Depth (R) 71me Flowmeter
5
action tntervat rteto mu,
Stop Final
Time Flowmet
10
15
20
25
P-3
30
35
40
45
50
55
Q
C
T of Oxidant Injects . o�tu Permanganate Form of
Tip
injection Tools: Geoprobe: injection
Injection Method:
Comments:

' FORM 2
Phase I Full Scale Sodium Permanganate injection Monitoring Data Sheet
site Name:
Site t_ocation:'� —
Date: —
Project Number:
IT Personnel: L
Subcontractor:
Injection Probe Advancement
In
action Inter
Point Depth
start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
0-4
5
4-8
8- 12
10
15
12 - 14
20
14-20
25
20 - 24
24 - 28
30
28-32
32 - 36
36 - 40
45
50
44 - 48
48-52
52 - 56
56 - 60
60 - 64
55
60
64
Type of OXidant Infected: um Permanganat
to/ection Tools: Geoprobe: Injection Til
Injection Method: Top -Down
comments:

(1/
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
�� �" Project Number: / O 7 � J .
Site Name:
Site Location: Subcontractor:
�� IT Personnel:
Subcontractor: —
Date:
Injection Probe
Point Depth
0-4
4-8
8 - 12
Advancement
Start
Time
Stop
Tlme
in action Interval Field Monitorin uata
Injection Start Initial Stop Final Total Gallons Injection Back
Depth Time Flowmeter Time Flowmeter Injected Pressure Pressure
5
10
15
20
c
35
40
45
50
55
60
64
T of Oxidant Injected: Penn Form of Oxidant U uld
Injection Tools: Geoprobe: In action Tip t�{ill-S►ot 1 Injection Tod
Injection Method: Top -Down Bottom -up
�J `
12 - 14
14 - 20
20 - 24
24 - 28
28 - 32
- 3
36 - 40
40 - 44
_�
/S-J
44 - 48
48 - 52
52 - 56
58 - 60
60 - 64
comments:
✓�lJ�� � . � � �% ' � �./ Cam" T c i� � o�

� V CORM 2
Phase I Full Scale Sodlum Permanganate injection Monitoring Data Sheet
Site Name: Project Number: /o -,;z
Site Location: `� IT Personnel:
Date: 3 p/ Subcontractor:
Injection Probe Advancement
In
action Interval Field Monitoring
Data
Point Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
/
---
a 8
8 12
12 - 14
14 - 20
10
15C�
20
- /F
25
�0
B
8
20 - 24
24 - 28
30
35
-
28
40
lr fb
45
36 - 40
50
40 - 44
35
44 - 48
60
48 - 52
52 _ 56
56 IL::i�
60
Type of Oxidant Injected: odium Permanganate form of Oxidant L T _
Injectlon Tools: eo Totre: in ction Tip Mill -Slot Intake i [injection Tool
injection Method: Top -Down -13s14�'uD
Comments:

it
FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: �� 2- Project Number.
Site Location: � t � o �� �� __ _� 1T Personnel:
Date: Z ISubcontractor:�f`c c�T, e
LD
injection Probe Advancement
injection Interval Field MonitoringData
Point Depth
start
Time
Stop
Time
injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
4-8
8- 12
10
15
O a
U
12 - 14
20
S
J�O
`�.s—
01
14 - 20
20 - 24
25
30
- O
o
/o�o�
/
cam"?
-?
J S
Oc J
24 - 28
35
S
.36—zo
28-32
OU
32 - 36
45
36 - 40
50
44 - 48
60
48 - 52
64
52 - 56
M_56 - 60
60.64
1 -Ainjection
Ty of Oxidant In acted: Sodium Parma a Form of Oxidant LI uld
Tools: Gao obe: In coon Tip ,= Hii-Slot In Injection Tool
MJectlon Method: Top -Down
Comments: -
r
-------------
r --

FORM 2
Phase I Pull Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: o.� G-� Project Number: /O
Site Location: IT Personnel:
Date:' o/ Subcontractor:6c"aC
Injection Probe Advancement
In Jectton Interval Field Morwi ng Data
Point Depth
Scut
Time
stop
Time
injection
Depth {ft)
Start
Time
initial
Flowmeter
Stop
Time
Finat
Flowmeter
Total Gallons
Injected
Injectlon
Pressure
Back
Pressure
0-4
5
4-8
10
�.
8- 12
15
00
/O
3 C,, 0
3J
b
12 -14
20
14 - 20
25
20 - 24
30
24 - 28
OO
28 - 32
40
32 - 36
45
38 -
40 - 44
a
50
55
44 - 48
60
48 - 52
64
52 - 58
TM of Oxldent injected: odium Permanganate Form of Oxidan 'dam
58 - 60
60 - 64
Non Tools: G robe: InJection Tip i In Injection Tool
inJectbn Method: T Down Bottom-u
Comments:
l�✓Z�cn�'/� �-?C��v��Q� iT� l�it/rf�•Jc�� �5�4�� l�c) /�-t�j:��•
LJA!c�
sP �
L

FORM 2
Phi 1 Full Scats Sodium RanmpWab Injection Monitoring Data Shea
aft Mama: {- i Prolod tlwnb�r:
sue l opitlon: �11'- (�� ff Psnwnnef: )- O'` •, / 1
Dow. 7 n� eulwonbraaEor: /Y,(C
INNER
SIMON
i
iC 'ma��
INN
,
111.011010
gall
_
�NONE
OWENS
Jl
Codua�nls:
w50.

fir' •�� - • .
FORM 2
Phase 1 Full Scale Soc lum Pa mansanaW Injection Monitoring Data Shoot
8Ete Mama: SEPrS
Project Kwnbw. ;
$us Location: - lT Pwsonnel: n,.1 igfDData: I_ - h r _ 8uboorrbraator: r�s(h hc;lc Sk`l�
��
wInrin
y
MIN
ram
,. ...
.
��
Comraminft:
s,2D

(FORM 2
Phase I Full Scab Sodium ParmanW*W Inaction Monitoring Data Shut
sat NwTw: S-- E �. ` i Projed Kmber.
stoe l ocatlon: T/ b IT P«sonnN: !
Dow. /^4 (?I aubo��baaeor: (' s � �f
®e�r�
im oil
'►r�r
�r �
"n�rr�■�n�
��
r���■c�rn�r��s��i�-,ice
SWIM
MINE
NNE
.,
NNEMON_
H,D
C,Of7NO�i1Ib: ��I hl)v ✓�/ �� (7'� '�i�� ���✓ -,0 t 1 -)

� L FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: L. Project Number: /p
Site Location: IT Personnel:
Date: O Subcontractor:
Injection Probe Advancement
In
ection Interval Field Monitor) Data
Point Depth
Start
Stop
Injection
Start
Initial
Stop
Final
Total Gallons
Injection
Back
fro �C�nL\
)_
Time
Time
Depth (tt)
Time
Flowmeter
Time
Flowmeter
Injected
Pressure
Pressure
_ram 0-4
/
5
4-8
10
-
�
8-12
12 - 14
15
20
25
O
_ -
14 20
20 - 24
30
24 - 28
28-32
32 -
t
45
50
36 - 40
0-44
55
44 - 48
60
48 - 52
64
Type of oxidant Injected: Sodium Permanganate 'Form of ox.
52 - 56
56 - 60
! action Too/S.- Ge obe: tlon Tip in -Slot �Intalk'@-Tool
60-64'Injection
Injection Method: Top -Down Bottom -up _
Comments:

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
site Name: Project Number:
IT Personnel: G
Site Location:
Subcontractor: 0!
Date:
Injection Probe Advancement in action Interval Field Monitoring Data
Injection Start Initial Stop Final Total Gallons Injection Back
Point Depth Start Stop 1 �✓� O
D th MI Time Flowmeter Time Flowmeter Injected Pressure Pressure
Time
Time
ep
5a2 0-4
i//J
5
4-8
10
15
8 12
20
/v2�
12 - 14
25
a�
14 - 20
20 - 24
30
24 - 28
35
40•
o1D
28 - 32
45
32 - 36
50 S
36 - 40
40 - 44
55
44 - 48
60
5
64
►
52 - 56
T of Oxidant injected: f6 Pen
5- 60
injection Toots:
60_ 64
Injection Method: Top -Down
Comments:
s.
O .�2-
//.S6
/177�7
Form of
D
U
i
i0
j
—
min -Slot intake / _ Injection Toot

FORM 2Z�
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Project Number: /O
Site Location; Cz =�` ` �' ^' L IT Personnel: e44-6'
Date: O Subcontractor: e6; pI- ¢ 4/G
Injection Probe Advancement
Point Depth start Stop
Time Time
In
ection Interval Field Monito
nq Data
r
(�
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
injected
Injection
Pressure
Back
Pressure
0-4
4-8
8 12
5
L�
10
15
20
-A-�Zgo
-
12 -14
14-20
20 - 24
_
d
- -- -- -
—
24 - 28
3
1
Ji
28 - 32
40
32-3
36-40
45
50
40 - 44
55
44 - 48
48-52
60
52 - 56
Ty a of Pont Injected: Sodium Permanganat Form of Oxidant L1 uld
56 - 80
tnjectlon Toils: Geopro . injection Tip Mill -Slot Intake IndTool
injectlon Method: Top -Down ottom-up _
w
A

F'ORM
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
site Name: Z - L 5 Project Number: � 0
Site Location:
: �' IT Personnel: C� j
'� ��-�, ` \
Date: - subcontractor: lC� e o �'r C'
Injection Probe Advancement
In action interval Field Monitor ng Data
Point Depth
$tart
Time
Stop
Time
Injection
Depth (R)
start
Time
Inttlal
Flowmeter
Stop
Time
final
Flowmetsr
Total Gallons
Injected
Injection
Pressure
Back
Pressure
0-4
5
4-8
90
8-12
12 - U
14 - 20
20 - 24
24 - 28
15
20
25
30
Form of Oxidant Liquid — —
28 - 32
0
32 _
45
38-4
'�
50
0-44
55
44 - 48
60
48 - 52
52 - 56
64
T of Oxidant
Injected:
ennan
Hate
56 - 60
60 - 64
IriJectiorr Tools: _ Injection Tip II -Slot Intake injection Tool
In/ection Method: Top -Down
Comments: /sue l

(FORM 2
Phase 1 Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: L Project Number:
IT Personnel:
Site Location: !�• c
Date: .S~p Subcontractor: �C�� acj iG �ui✓"i'
Injection Probe Advancement
Point Depth start Stop
Time Time
In action Interval Field Monitoring Data
Injection Start Initial Stop Final Total Gallons Injection Back
Depth (ft) Time Flowmeter Time Flowmeter Injected Pressure Pressure
- 0-4
5
4-6
10
8 - 12
15
12 -14
20
14-20
25
20 - 24
30
24 - 28
35
28.32
40
32 - 36
36 - 40
40 - 44
65
150
44 - 48
'
/O
64
5 48 -
_
56 _ 80
Ty of Oxidant in ted luM ParmanganateForm of Oxidant uld
in BGtbn Toots: Tip Mfll-Slot Intake injection Tod
60 - 64
in[=EJ �lectbn Method Top -Down BOt
Comments:
yZ`�j02 p �S .-

FORM 2
Phase I. Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: Project Number:
'- - Site location: IT Personnel•
_'�<-'E-� _�.. ' ..� r� �--e, �fG.
Date' _ .� /, i Subcontractor: �1 e
Injection Probe Advancement
In
action interval Field Monitorin Data
Point Depth
Start
Time
Stop
Time
Injection
Depth (ft)
Start
Time
Initial
Flowmeter
Stop
Time
Final
Flowmeter
Total Gallons
Injected
Injection
Pressure
Back
Pressure
/� c.L14-
5
10
15
20
25
20 - 24
-
24 - 28
28 - 32
35
40
32 - 36
45
36 •
50
/
ro-2C)
55
44 - 48
48 - 52
52 _
60
64
Ty of Oxidant tnJected: i um Parma ter Form of Oxidant Liquid —
56.60
Injection Tools: Geoprobe: Injection Tip Mill -Slot Intake _ ' Injection Tool
60 - 64
lnJection Method: T -Down Bottom -up
Comments:
. ,� �-, ;� �,�� ._i-�=�'� ��� ,�;�n � �-�-�'�/✓y��

FORM 2
Phsse 1 Full Seal* SocHum Pormanganota Injection Monitoring Data Sh"t
and Nwm; S� X1 J Protect Number. ��15
stt. h ocsticn: IT PersonnN:
SubeonVoctor
Comment&:
It
_. _ , _ „—. ..r11 1--

�'nl_�aEli�
FORM --�
Phase I Full Scale 8odlum Pumartsanate Ir► ocdon Monitortng laata Shea
Site Narta: Project Number. / )7 3
not ocaUon: I rr Pommies: fi 111T7
D.W. "
-��� 8ubaorrbao>eor: i �i 01 rf7Ir - Sf?---
�r■��ar���r�r�i
Comments:
L44 Irk') i,t'�l ��f ; �t,; •_�,tl,,., , .1�-11�.�n� ;y�.,�i�U�i ���
tITYI-Acl 1CA s
��I

FORM 2
Phase I Full ftals sodium Permanganate Infection Monttoring Data She*
Sao Nam. Project Kwdw- '7,
ITPersonnol:
Data. Suboont*ctor—
�r�
�� i�r��� err
fj
J M
1,-,:
Comraonft:
01 2-0

L�
FORM
Phase i Full Scale S"um Pennsng&n&W Injection Monitoring Data Shoot
gild Nanw: ..`l r,_(: r,) Proled MumMr. 101 S
She LD"don: �A ) I_rf) IT Pad: T�/�''11(i
oats I - ` , - n 1 suboonb *awr:
.,

FORM 2 CT�
Phase I Full Scale Sodium pmnn&ngan&w injection Monitoring Data Shoot
er-.
sit's Marta:Pm1od ltwnb
IT PenwmW:
She LOG"00,
DmU: 0
IMF
v m
-0
7P)n-nnf,. 4 Tu-i
S-0

Y'� M
FORM 2 �— f
Phase I Full Scale Sockum Parmanyanab Inlaction Monitoring Oats Sheet
sits !fair»: (\ �' S Proj•at Mua►ba: fl r, �C
ilia t.ocatlon: h CAM F' 1 r1 fr PKsonnou L
Dew. I I - n L Suboorraola -
r„� n �; 'i �; nr - r �, n �'r% �'� � la ► i; ' L ��t i, 0 0A1'�,
C)_t__',

FORM 2
Phase 1 Full Scalar Sod}um pomum anab lr4ectlon Monitoring Data Sh**
site Marne: n ti' Project Kmib . (D 1'13�� —
sta Locadon: ( c IT Perso+x ep I 1 ar)e L—
D&W. _ -n ate: GL-0tn(",►r I
.
,
1
oil
MEN
�rMENEW72�
cs�w�r�w
eft:
5-1- rD
TIC)
tio
t-io

FORM z
Phase I fuH Scitle Sodium Permanganate Injection MoultorIN Data Sheet
ij Site Name:
G
Site Location:
Hate:
Project Number: D L��
iT Persorump ,�
•
Em!�r�!!rrr��rr ��i
i,r��

FORM 2
Phase I Full Scale Sodium Pwowngs"te Injection Moaitodng Data Sheet
site Name: > Project wenber. / 6 �� a S-
"�_ IT Perwnnai:
its 4rouil on: � f ' .�
Data:
�.

FORM 2
Phase 1 Full Scale Sodium Permanganate Injection Monitoring Data Sheet
i
Site Name:
Site Location: .=- � ��✓ G
Date: O
Project Number:
IT Personnel:
Subcontractor: � �� i ` �:- << �r e
Injection Probe Advancement
pth Start Stop
Point __�;Tlme Time
In action Interval Field Monitort Data
Injection Start Initial Stop Final Total Gallons Injection Back
Depth (ft) Time Flowmeter Time Flowmeter Injected Pressure Pressure
0-4
5
4-8
10
8 - 12
15
20
25
12 - 14
14 - 20
30
20 - 24
24 - 28
28 - 32
32 - 36
35
40
45
36-40
4
44 -
48-52
/�/
55
60
64
52 - 56
Type of Oxidant Injected: odium Perm_an anal _ Form of Oxidant Liquid
56 - 60
_ Mill -Slot Intake Injecdon Tod
In' ction Toois: Geoprobe: Injection Tip ^_
60 - 64
Infection Method.' Top -Down Bottom up _
Comments:

bRa Nam.:
Scr\p.�--j
sta t.ocatlon: ��. ��
Dow.
FORM 2
Ph#Ao I Full Scala Sodium Patmangan*W InJoction Monitoring Data Shoet
Project xumbw. 1t)7
R Per: T�►� LurL_L
!lubcw*aQw.. C F fy nr> , Sl 1 � /,- - OX"I —
FIR.
SOS
IL
COOUI~tx
3J1

FORM 2
Phase 1 Full Scale Sodium Permanganate Injectlon Monitoring Data Sheet
Site Name; L �� Project Number:
_ IT Personnel: GAG ✓5
Site Location: -� C
Subcontractor: x
zr.s %'
Date:
Injection Interval Field Monitorin Data
Injection Probe
Advanc�mant
initial�311:Gp:Final Total Gallons
InJectlon Back
Point Depth
Start
Stop
Injection g
n1Time Time FlowmeFlowmeter Injected
Pressure Pressure
Time
Depth (ft)
0-4
S
4-8
10
8-12
15
20
25
12 - 14
14 - 20
20 - 24
30
24,28
35
28 - 32
40
32 - 36
/�
45
50
8-4
40 - 44
35
44 - 48
60
48 - 52
of Oxidant !n aoted� um Pertnanga_ Form of Oxtda d--�—�,--
—_-----
Injection Tool
52 _
M
In t/on Toils: Gaoprobe: injection Tip 111 Slot intak
— ---- — —
58 80
Ir>jeatloa Method: Top Down Bottom -up_
60 - 64
comments:

FORM 2
Phase I Full Scale 30dium PWMWWDaW 'nJectlo" Moalloring Data 3hd4A
5tto Name:
ff Pwoonnot; 2� L
She LAI)G&tlw:
�,��;�-...ter �i�
. �.
r�w�r
.- -
J

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Phase I FUH ac*W Sodium Parrmng"s Inledlon MoaltOCIng 04ta Sheet
prolod Nwpber. /�' ---5-
She wArno.. -7,2-75
ff Par"Mot. , -Z-,->
ano Location: ;is �---
Subconkidar.
MOM -
mom
C*Awnents:
)< 114,49

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Project Number. '
Site Name:
IT Personnel:
Site Location:
Subcontractor: ci cOG
Date:
vancement
Point tart Stop
hns T1rne
Injectionj14
injection interval Field Monitorin Data
Injection Start Initial Stop Final Total Gallons Injection Back
pew () TIC Flowmeter Time Flowmeter Injected Pressure Pressure
0
5
10
15
20
14 - 20
25
24-28
30
28
40
45
50
55
F60-64
60
64
T of Oxidant lnject �. Ium Permanganate Fonn of Oxidan!n/ecmn action Tip lu-slot Intake Injection Tool
Method: Top -Down Bottom -up
1Einjection
Comments:
To

FORM 2
Phase I Full Scale Sodium Permanganate Injection Monitoring Data Sheet
Site Name: c Site Location:
Date:
Project Number: %O Y-� IT Personnel: G --
', s,
Subcontractor: CeG zz2_
1
action interval Field Monitodn Data
Injection Probe Advancement
Initial
Stop Final Total Gallons
Injection Back
Point Depth Start Stop
IrtjeWon start
Time Flowmeter
Time Flowmeter In)ected
Pressure Pressure
ttFt) TI►T►s Tlma
DeptfiiDl
0-4
5
4-8
10
8 - 12
15
12 - 14
20
25
30
,
14 - 20
O
L
20 - 24
24-28
35
28 - 32
40
45
32 - 36
38 - 4
50
40 - 44
55
44 - 48
60
48 - 52
84
of Oxidant infected: Sodium Perrnan Hate Form of Oxklant Liquid __-- —_-- _--
52 - 58
Geoprobe• In}ection Tip Mill -Slot Intake , _ Injection Tool
58 - 60
! ectlon Toofs: ----
60 - 64
JaAscfion Method: Top -Down Bottom -up

IT Corporation ofNortb Carolinn, Inc.
A Member of The IT Croup
Appendix E
Field Monitoring Data Sheets - Phase I Full Scale ISCO Injection

FORM 1
L:
Daily Groundwater Monitoring bats Neet
$;., .
Phase I Full Scale In Situ Chemic*'Oxtdation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: 61Y1�9��
Project Number: 107535
IT Personnel: Dz-
Sample
Location
to
Water
(ft)
Remarks
-- --- --
MME
MEM
r 1 -
��yyyy����`•��
'M jwll
�Cssii�
/ ice-[
J �7
r �
✓
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♦
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r / i
raw"
r
�
PAM. mpir,
ml-
���
. -
���a�
L�
• . s.
MAMMA
-00
ice
0-7

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date:--6�0114-
6
Project Number:
IT Personnel:
107535
Sample
Location
Time
Depth
to
Water
(ft)
ield Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(oC)
ORP
(mV)
Color
MW-12
p
o2
8.
L
✓ho i i o %ice).-,
MVV-13
U3.46r
MW-17
MW-18
MW-22
MW-23
LMP-1
LMP-2
DW-5
DW-7
O. D
DW-8
DW-13
DW-14
DW-15
DMP-1
DMP-3
DMP-4
BMW-3
B8�'3
1 O.
/
—
BMW-4
�,1

Md
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: �1
Project Number: 107535
IT Personnel: Ce
Sample
Location
Depth
•
Water
Remarks
'' ` /
Specific
Conductivity
•
•
®1111111111111110
_---�-
�i'ri��,��G�'�
ii�.��
ll���'
•
�1-�-
DATA 115,

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: -0.1
Project Number: 107535
IT Personnel: G14
Sample
Location
Time
Depth
to
Water
ft)
leld Monitoring Parameters '
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(m 1L)
Temp.
(oC)
ORP
(mV)
Color
MW-12
§-: 43
n X 1,q
3- /3
M W-13
1;&45
MW-15
MW-17
MW-18
8
id. 7
.5 D
/ ./a
//��. /
.�
tea, -5
MW-22
MW-23
LMP-1
LMP-2
D -5
D
-1$
-14
DW-15
DMP-1
DMP-3
DMP-4
BMW-3
/D,
2
BMW-4

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: -6Q2i26@4- _ , )
� 7 i ,s
Project Number: 107535
IT Personnel: �4,.� �?� �, �� 0 0
Sample
Location
Time
Depth
to
Water
leld Monitoring Parameters
Remarks
r� �� za A 1: ,•�.'= ( Win"
pH
Specific
Conductivity
(US)
DO
(m IL)
Temp.
(oC
ORP
(mV)
Color_
MW-12
/
MW-13�
MW-15
W-17
MW-18
2/
6,1,4 v'
c� J Tl L
MW-22
'D
tro
/1i�?/
<�n' n ✓J Ir
E v�
G% n . �„ % 24) L
MW-23
LMP-1
LMP-2
DW-5
DW-7
DW-8
DW-13
DW-14
DW-15
DMP-1
DMP-3
DMP-4
BMW-3
BMW-4

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: - SLS Greensboro
Site Location: Greensboro, NC
Date: 6/22/2901 1 . ✓,� - /Y�b-��j1�/ i
Project Number: 107535
IT Personnel:-
Sample
Location
Time
Depth
to
Water
ft)
leld Monitoring Parameters
Remarks
i�i�-�' �' T� -.� • `, - . ;: ' : r 'i
pH
(S.U.)
Speclflc
Conductivity
(us)
DO
(mg/L)
Temp.
(oC)(mV
ORP
Color
MW-12
.3-'
MW-13
-
MW-15
MW-17
08 O
3o
d • b
(, 3
/
MW-1 S
7
4.10
0 S
MW-22
�� ./Jf�-:'�. ,'•.J " - �.' v < <�
LMP-1
LMP-2
DW-5
DW-13
DW-14
DW-15
DMP-1
DMP-3
77, 5"
DMP-4
i3M W-3
�• S "
�. 1-
h �/
t) _ Sri' G�
C7 _ s
/9- o d-
- (3�2-
BMW-4

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: 6/22/2001
Project Number: 107535
IT Personnel: lid
Sample
Location
Time
Depth
to
Water
(ft)
ield Monitoring Parameters
Remarks
t�� 7-, : 2:.cJ , 1 • ; ;;
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
oC)
ORP
(mV)
Color
MW-12
0? .
=;^
O.
c-,),
MW-13
12.45
'
MW-15
MW-17
D'
,5-32
MW-18
/� ; ✓
lc2l./
/
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c3
M W-22
MW-23
LMP-1
LMP-2
OW-5
DW-7
O
—
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a:U
/
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/3_ 20
,orb
�.cf>�
��,
'S�
`.�.i.n
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DW-13
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O
o2
C7- //D
/ X
M P-4
BMW-3
,I O
/
C)•
/
/•
—
0_ o
BMW-4

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase 1 Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date:
Project Number: 107535
IT Personnel:
Sample
Location
Depth
Water
.:
•-
..Remarks
®�Mzw"��
r
"'
I
`"
` '
®�lf�,

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro NC
Date:
Project Number: 107535
IT Personnel:
Sample
Location
Depth
to
Water
Specific
Conductivity
�•
M-Nm

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro
Site Location: Greensboro, NC
Date: srzarP� 6 z6 0/
Project Number:
IT Personnel:
107535
Sample
Locatlpn
Time
Depth
to
Water
(ft)
field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(oC)
ORP
(mv)
Color
MW-12 -
11
h • 2
0 100
Y. 72-
Cui
MW-13 --
2if PM
16.25-
a.
17-5�7
/`f.
lv
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ZZo
d , 62-
0. 08
4.03
.3
7 5-
MW-18 -
Z M
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MW-22
MW-23
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z °� PM
6.10
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0, IqV.
9
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,.,
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2-7-W
s, 3
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i YsZl.ql
S q 3
n.-
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7.
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I

Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro
Greensboro, NC
L7 01
Project Number: / 107535
IT Personnel: NOW
Sample
Location
Time
Depth
to
Water
(flr)/
Monitoring Well
Field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(°C)
ORP
(mV)
Color
MW-12
12 °PM
q 73
%
. 1 1 ))
q.,20
q.. 1
4
��-1 /. )
MW-13 -
us PM
. SS
6, 36
- � (�_
, Z9
17, zq
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r'Zsf M
6,23.
7.Oq
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3
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q,15-
, .33
69. q
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`t. 37
`13
0. 1oZ
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DW-5
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6 �l
0. I q c
q. 0;
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FORM 1
Daily GrOUndwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro Project Number: 107535
Site Location: Greensboro, NC IT Personnel:��(� �� r
Date: G• ZR-O� nNn
Location�•
DepthSample to
,•
.-•
..
u
C
✓ r
..
LI.
•
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•
r'ilt,
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►

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro Project Number:
Site Location: Greensboro, NC IT Personnel:
Date: (0 - AA, D/ Q
107535
NG ��t• L��.t a �ltt
Sample
Depth
to
Remarks
.-
�
�r"�1J
�
i71�L
t
I
� • .

Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro Project Number: 107535
Greensboro, NC IT Personnel: L 71 (li4e 1 Fe E�►�'
1?� n7
Sample
Location
Depth
to
Water
Specific
Conductivity
�•
•••
• .
wo MEN
�r
•
i Iif
• _•
mn
% i1
F-M,"momsi
,• �.
�`�A--�
m_m
____
mm
y'
—9
�
0
� --
MR.N.W.'"r
MIn
Fm
rWWWASAS

FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation .
Site Name: SLS Greensboro Project Number: C),7 5 35 107535
Site Location: Greensboro, NC IT Personnel: t•1 f.' I �_
Date:
Sample
Location
r
J
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
)
pH
Specific
Conductivity.
(US) `
DO v/
(mg/L)
Temp.
(°C)
ORP
(mV)
Color
MW-12
,
/(S.U.))
fJ GJ
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s/lfL
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FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro Project Number: 107535
Site Location: Greensboro, NC IT Personnel:
—
Date: -J.O Fa - p
Sample
Location
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
pH
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(°C)
ORP
(mV)
Color
MW-12
11 65
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G(S.U.)
7.05
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15
MW-13
10:2.
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15.96
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0.65
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MW-17
Q
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MW-18
MW-22
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Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro Project Number: 107535
Greensboro, NC IT Personnel:
7-OK-0 1
Sample
Location
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(°C)
ORP
(mV)
Color
MW-12
1&2
5.Siq
021
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MW-13
0
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1245
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FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
Site Name: SLS Greensboro Project Number: 107535
Site Location: Greensboro, NC IT Personnel:
Date: '7 - D 5 0!
if/.
Sample
Location
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(°C) .
ORP
(mV)
Color
MW-12
/Q : 15
W.
MW-13
�t
i, 7l
. q
MW-15
:3
O.0 r!'
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%
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011
1
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51
r,6
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DW-14
DW-15
DMP-1
: Z
j .Cj(5,
Ligii.5r
�So
Zo•5
DMP-3
/O: Z
.�I&Zd.0�1
2
DMP-4
0:5
.ID
s.6b
.51
15.46
45S,lb
BMW-3
lA
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. %0.9Z .
a: 5L
� 71
5.1
6. 55
, e s
R.
.
Vnw-v

Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro Project Number:
Greensboro, NC IT Personnel:
107535
Sample
Location
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L))(0c)
Temp.
ORP
(mV)
Color
MW-12
:q-3
q.
.D
10-2-10
3.rt /
lot
qfit.
MW-13
r
(e.5(
6•ILIq
D.7�
��F
t
704�
MW-15
01-'6
. 1
SO
a. 031
?.0
1D.&
MW-17
:Cj
1
0. Ito
.qq
MW-18
9.0(5
5.31
�. (
t
L
'
MW-22
I DT
. 1J
0-111
560
MW-23
LMP-1
G,
' 2 /
5.7/
5-q
0. 2.772,.7o
.q310L.1
c4,e,
LMP-2
87141
15,191
G-61
0- IOIe
2-tou
DW-5
17. l 0
5.50
0, [ Z-
.21
Zo.qf.rj
DW-7
Q;
$.ilZ7L
D.
,3
DW-8
O •
Gt
.�
DW-13
!�:
.Z
�i
54
DW-14
DW-15
DMP-1
(s.. Ifo
5.-1t
1)�1, .3
I.yS
6.
D P-3
M
G,
. 'R
DMP-4
_
BMW-3
�:
�.
smvr�,
qtg1
,�U
D. c
PJUPz

Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro Project Number: 107535
Greensboro, NC IT Personnel: $•,}� j/•,� �� (vim
- IS-ef
Sample
Location
Time
Depth
to
Water
(ft)
Monitoring Well
Field Monitoring Parameters
Remarks
pH
(S.U.)
Specific
Conductivity
(US)
DO
(mg/L)
Temp.
(°C)
ORP
(mV)
Color
MW-12
•
• MW-13
+p
L
• MW-15
• MW-17
i
6.36
• MW-18
II
• MW-22
I I
4 MW-23
13S601
6to
• LMP-1
II.qq'7
�. Q
1.Z4
Zo ZZ
• LMP-2
12.00
4�
!Lt
• DW-5
1 :Drj
• DW-7
�j
• DW-8
12, 4-5 6
5.72,cpQ(tn�
• DW-13
ls,-S6
if.
•
• DW-14
17:05
• DW-15
1 2:
Z�• �l
DMP-1
I 1:5
13•17-
TV .
• DMP-3
�Z •2.�
$.Qp'S
• DMP-4
BMW-3
• BMW-4
3:
L
• p�P2 ��:01 �1S•SD (Q,tatr

e,Q)
Site Name:
Site Location:
Date:
FORM 1
Daily Groundwater Monitoring Data Sheet
Phase I Full Scale In Situ Chemical Oxidation
SLS Greensboro Project Number: 107535
Greensboro, NC IT Personnel:
R• 3-Ol
Sample
Location
DepthMonitoring
Water•Conductivity�•
Well
Field Monitoring Parameters
'
•-•
. .
IM.
�.•.'
ram,%ra„..
.i
--
r .
��
�
':
r 0
` ►
i'� �y1Unw,M
yrm,
�ffmffm
- i
cm
_ IMI '
rmvfflmr
M..
MR
�
N
IM,I
Iml
M.,12MUM
..
�LTSIMEM
,1U �<WV
C)Alp,Z
N15
aD.I0Z
I.oc,
0.1 Vt
Z.Ko
11"T1 F'1h
e,�✓
HAIP 1
1;1A
1 U• �10
SS.�°I
Z-b$to
q�1�
•
11.�'�i} 10AAA

IT Corporation of iVorth Carolina, Inc.
A Member of The IT Croup
Appendix F
Field Monitoring Results Graphs - Phase I Full Scale ISCO Injection

MWA 2: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
8.50
8.00
7.50
7.00
6.50
S
Q 6.00
5.50
5.00
4.50
4.00
Oxidation Reduction Potential
600.0
500.0 �t
400.0
E
a
o: 300.0
O
200.0
100.0
0.0
6118101 6125101 7/2/01 7/9/01 7/ 16/01 7123/01 7130101 8/6101 8/13101 8120/01
O.VV
5.00
4.00
J
Q!
E 3.00
O
0 2.00
1.00
0.00 .
6/18/01 6125101 7/2/01 7/9/01 7/16/01 7123101 7/30/01 8/6/01 8/13101 8120101
Specific Conductivity
0.250
0.200
u
c 0.100
a
U
0.050
0.000 ' 1
6/ 18/01 6/25/01 7/2/01 7/9101 7/ 16101 7123101 7/30/01 8/6/01 8113/01 8120/01

MW-13 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
I U.UU
9.00
8.00
7.00
6.00
a 5.00
4.00
3.00
2.00
1.00
0.00
6118/01 6/25101 7/2101 719/01 7/ 16/01 7/23101 7/30/01 8/6101 8/13/01 8120/01
Oxidation Reduction Potential
700.0
600.0
500.0
E
�- 400.0
a
Ir
0 300.0
200.0
100.0
0.0
6118/01 6125/01 712/01 719/01 7/16101 7/23/01 7/30/01 8/6/01 8/13101 8120/01
Dissolved Oxygen
10 00
9.00
8.00
7.00
6.00
o�
E 5.00
0 4.00
3.00
2.00
1.00
0.00
6/18/01 6/25/01 7/2101 7/9/01 7116/01 7/23/01 7/30/01 8/6/01 8/13/01 8/20/0
Specific Conductivity
0.180
0.160
0.140
0.120
0.100
0.080
a
0 0.060
U
0.040
0.020
0.000
6118/01 6/25/01 7/2/01 7/9/01 7/ 16/01 7/23/01 7/30/01 816101 8113/01 8120/01

MW-15: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
7 00
Dissolved Oxygen
6.00
5.00
4.00
2
a
3.00
2.00
1.00
0.00
6/18/01 6/25/01 7/2/01 7/9/01 7/16/01 7/23101 7/30101 8/6/01 8/13/01 8120/01
Oxidation Reduction Potential
600.0
600.0
5 400.0
E
rZ 300.0
O
200.0
100.0
0.0
6/ 18/01 6125/01 712/01 7/9/01 7/ 16101 7/23/01 7130101 8/6/01 8/ 13/01 8/2 0101
7.00
6.00
J 5.00
as
4.00
O
3.00 ---- ---
2.00
1.00
0.00
6118/01 6125101 7/2101 7/9/01 7/16101 7/23/01 7/30/01 8/6/01 8113/01 8120/C
Specific Conductivity
0.090
0.080
0.070
U) 0.060 -
k 0.050
u 0.040
v
c 0.030
0
U
0.020
0.010
0.000
6118/01 6/25101 712/01 7/9/01 7/16/01 7123/01 7/30101 816101 8113101 8/2010

MW-17 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
PH
Dissolved Oxygen
9.00
8.00
7.00
6.00
5.00
a 4.00
3.00
2.00 _
1.00
0.00
6/18101 6/25101 7/2/01 7/9101 7/16/01 7/23/01 7/30/01 8/6/01 8113/01 8/20101
Oxidation Reduction Potential
600.0 -
500.0
400.0
E
IL
w 300.0
O
200.0
100.0
1 - .1
0.0
6118/01 6/25/01 7/2/01 7/9/01 7116101 7/23101 7/30/01 8/6/01 8113/01 8/20/01
O.VV
7.00
6.00
-1 5.00
E 4.00
O
3.00
2.00---
1.00
0.00
6/18/01 6/25/01 7/2/01 7/9/01 7/16/01 7/23/01 7130/01 8/6/01 8/13101 8120101
Specific Conductivity
1.000
0.900 -
0.800
0.700
0.600
.>3 0.500 _
u
� 0.400
O
U 0.300
0.200
0.100
0.000 A
6/18/01 6125101 7/2/01 7/9/01 7/16/01 7123/01 7130/01 816101 8/13/01 8/20/(

A
MW-18: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH Dissolved Oxygen }
8.00
7.00
6.00
5.00
: 4.00
3.00
2.00
1.00
0.00 .
6118/01 6/25101 7/2/01 719/01 7/16101 7123/01 7 /30/01 8l6/01 8/13/01 8/20/0
o.Vu
5.00
1
6118101 625/01 712/01 719101 7116/01 7/23101 7130/01 8/6101 8113101 8/20/01 6118/01 6/25/01 7001 7/9/01 7/16/01 7/23/01 7130/01 816101 8/13/01 8/20A

MW-22 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
Dissolved Oxygen
pH
9
U.VV
8.00
7.00
6.00
5.00
c 4.00
3.00
2.00
1.00
0.00
6118101 6/25101 7/2/01 7/9101 7/16/01 7/23/01 7/30/01 8/6/01 8113/01 8/20/01
Oxidation Reduction Potential
600.0
500.0
j 400.0
E
W 300.0
O
200.0
100.0
0.0
6118101 6125/01 7/2/01 7/9/01 7116/01 7/23/01 7/30/01 816/01 8113/01 8/20/01
.00
8.00
7.00
6.00
J
p1 5.00
E
O 4.00
O
3.00
2.00
1.00
0.00
6/18/01 6/25/01 7/2/01 7/9/01 7/ 16101 7/23/01 7130/01 816101 8/ 13/01 8120/0'
Specific Conductivity
0.140
0.120
to 0.100 -
2' 0.080
0.060
a
c
0
U 0.040
0.020
0.000 .
6118/01 6/25/01 7/2/01 7/9/01 7/16101 7/23/01 7/30/01 8/6/01 8/13/01 8/20/01

MW-23: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH Dissolved Oxygen
9.00
8.00
7.00
6.00
5.00
2
a
4.00
3.00
2.00
1.00
0.00
6/16/01 6125101 712/01 7/9/01 7116/01 7/23/01 7130/01 8/6/01 8113/01 8/20/01
Oxidation Reduction Potential
250.0
200.0 —
150.0
E 100.0
a
0
0 50.0
0.0
-50.0
-100.0
6118101 6125101 7/2/01 719101 7116101 7/23101 7130/01 8/6/01 8/13/01 8/20101
2 50
2.00
1.50
w
E
p 1.00 _
Q
0.50
0.00 .
6/1 B/01 6125101 7/2/01 7/9/01 7/16/01 7/23/01 7/30/01 8/6101 8113/01 8/201
Specific Conductivity
0.900
0.800
0.700
) 0.600
0.500
0.400
,3
c 0.300
U
0.200
0.100
0.000 .
6/18/01 6/25/01 712/01 7/9/01 7/16/01 7/23/01 7/30/01 8/6/01 8/13101 81201.

LMP-1 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
7.00
6.00 — -
5.00
4.00
3.00
2.00
1.00
0.00
6118/01 6125101 7/2/01 7/9/01 7/16101 7123/01 7/30101 816/01 8/13/01 8120101
Oxidation Reduction Potential
500.0
450.0
400.0
350.0
E 300.0
IL
250.0
O
200.0
150.0
100.0
50.0
0.0
6118/01 6125/01 7/2/01 7/9/01 7116/01 7/23/01 7/30101 8/6/01 8113101 8/20/01
9.00
8.00
7.00
6.00
J
CD 5.00
E
O 4.00
3.00
2.00
1.00
0.00 .
6/18/01 6/25/01 7/2101 7/9/01 7/16/01 7/23101 7/30/01 8/6/01 8113101 8/20/0'
0.400 Specific Conductivity
0.350
0.300
W
0.250
0.200
= 0.150
0
U
0.100
0.050
0.000
611 B/01 6125/01 712101 7/9/01 7/16/01 7/23/01 7/30/01 8/6101 8/13/01 812010'

LMP-2 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
W.VU
8.00
7.00
6.00
5.00
2
0 4.00
3.00
2.00
1.00
0.00
6/ 18101 6125/01 7/2/01 719101 7/ 16/01 7/23/01 7/30/01 816/01 8113/01 8/20/01
Oxidation Reduction Potential
600.0
500.0
j 400.0
E
� 300.0
O
200.0
100.0
0.0
6/18101 6/25101 712101 7/9/01 7/16101 7/23/01 7/30101 816/01 8/13101 8/20/01
V.VV
5.00
4.00
J
rn
E 3.00
O
2.00
1.00
0.00
6/18/01 6/25/01 712101 7/9/01 7/16/01 7123/01 7/30/01 8/6/01 8113/01 8/20/:
Specific Conductivity
0.400
0.350
0.300
in
0.250
w 0.200
u
0.150
0
U 0.100
0.050
0.000
6/ 18101 6/25101 712/01 7/9101 7/ 16101 7123/01 7/30/01 8/6/01 8/13101 8/20/.

DW-5 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH Dissolved Oxygen
O.VV
7.00
6.00
5.00
a 4.00
3.00
' 2.00
1.00
0.00
6118/01 6125101 712/01 7/9101 7/ 16/01 7/23101 7/30/01 8/6/01 8113101 8/20/01
Oxidation Reduction Potential
3
E 3
CL
0= 2
O
2
50.0
00.0
50.0
00.0
50.0
00.0
50.0
00.0
50.0
0.0
6118101 6/25101 712/01 7/9/01 7/16/01 7/23/01 7/30/01 816101 8113/01 8120/01
/.VV
6.00
5.00
4.00
E
O 3.00
2.00
1.00 -- - -- -- - --- ---- -- - ----- - - ---
6118/01 6125101 7/2101 719/01 7/ 16101 7123101 7/30/01 6/5!01 6 ! 13!01 8: 201:
Specific Conductivity
0 140
0
0
0
Z
U
V 0
C
U 0
0
0
.120
.100
.080
.060
.040
.020
.000
6/18/01 6/25101 7/2/01 7/9101 7/16101 7/23/01 7/30101 8/6/01 8/13101 8120f

DW-7: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
Dissolved Oxygen
9.00
8.00
7.00
6.00
5.00
4.00
3.00
2.00
1.00
0.00
6/ 18/01 6/25/01 7/2/01 719/01 7116/01 7/23/01 7/30101 8/6/01 8/ 13/01 8/20/01
Oxidation Reduction Potential
600.0
500.0
> 400.0
E
Cr 300.0
O
200.0
100.0
0.0
6118101 625/01 7/2/01 719/01 7/16/01 7123/01 7130101 816/01 8/13/01 8/20101
U.UU
5.00
4.00
J
rn
E 3.00
O
93
2.00
1.00
0.00
6/18/01 6/25101 712/01 7/9/01 7/16/01 7123101 7/30/01 8/6/01 8/ 13/01 8/20/0'.
Specific Conductivity
0.250
0.200
iq
0.150
0
a 0.100 --- — —
c
0
U
0.050
0.000
6118/01 6/25101 712101 719/01 7/16/01 7123101 7130/01 8/6/01 8113/01 8/20/01

DW-8: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
8.00
7.00
6.00
5.00
2
4.00
3.00
2.00
1.00
0.00
6118/01 6/25/01 712/01 7/9101 7/ 16/01 7123/01 7/30/01 8/6/01 8/13101 8/20/01
Oxidation Reduction Potential
900.0
800.0
700.0
E 600.0
a 500.0
a:
p 400.0
300.0
200.0
100.0
0.0
6118101 6125/01 712101 7/9101 7116101 7/23101 7130101 8/6101 8/13/01 8/20101
V.UU
8.00
7.00
6.00
J
`pi 5.00
E
O 4.00
0
3.00
2.00
1.00
0.00 ' 1
6/ 18/01 6125/01 712101 7/9/01 7/ 16/01 7123101 7/30/01 816101 8/13/01 8/20/G
Specific Conductivity
0.096
0.094
0.092
0.090
�+ 0.088
'- 0.086
o O.oe4
c
o 0.082
U -
0.080
0.078 _
0.076 A
6118/01 6/25/01 7/2/01 7/9101 7116/01 7123/01 7/30/01 8l6/01 8/13101 8/20/0-

DW-13: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
PH
9.00
8.00
7.00
6.00
5.00
2
4.00
3.00
2.00
1.00
0.00
6/18101 6/25/01 712/01 7/9101 7/16/01 7/23/01 7130/01 816101 8113/01 8/20/C
Oxidation Reduction Potential
E
a
O
700.0
500.0
500.0
400.0
300.0
200.0
100.0
0.0
Dissolved Oxygen
7.00
6.00
J 5.00
rn
E 4.00
p 3.00
2.00
1.00
0.00
1 6118101 6125/01 7/2/01 7/9101 7/16101 7/23/01 7/30/01 8/6101 8113/01 8/20/C
Specific Conductance
0.140
0.120
n 0.100
3
0.080 ---------
0.060
0
c
j 0.040 -_--
0.020
0.000 .
6/18101 6/25/01 712/01 7/9/01 7116/01 7/23/01 7/30/01 816/01 8113/01 8/20/01 6118/01 6125/01 712/01 7/9101 7/16/01 7/23/01 7130101 8/6101 8/13/01 8/2 0/(

DW-14: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
12.00
10.00
8.00
= 6.00
4.00
2.00
0.00
Dissolved Oxygen
3.50
3.00
2.50
2.00
E
O 1.50
O
1.00
0.50
0.00 1
6/18101 6125/01 712101 7/9/01 7/16101 7/23/01 7/30/01 8/6101 8113/01 8/20101 6/18/01 6/25/01 7/2/01 719/01 7116/01 7/23/01 7130/01 8/6/01 8113/01 8/20/01
Oxidation Reduction Potential
soD.O S ecif C d to
250.0
200.0
E
d 150.0
w
O
100.0
50.0
0.0
0.600
p is on uc nce
0.500
0.400
w 0.300
u
a
p 0.200
U
0.100
0.000
6118101 6125/01 72/01 7/9/01 7116/01 7/23101 7130/01 816/01 8/13101 B20/01 6/18/01 6/25101 712101 7/9/01 7116/01 7/23101 7/30/01 8/6/01 8/13101 8/20/01

i
DW-15: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
10.00
8.00
G 6.00
4.00
2.00
0.00
6/18/01 6125/01 7/2/01 7/9101 7/ 16/01 7/23101 7130/01 8/6/01 8/ 13/01 8/20/01
Oxidation Reduction Potential
JOU.0
300.0
250.0
E 200.0
Er 150.0
O
100.0
50.0
0.0
6118101 625101 7/2101 7/9/01 7116101 7123/01 7/30/01 8/6/01 8/13101 8120101
6.00
5.00
4.00
J
Of
E 3.00
O
0
2.00
1.00
0.00 .
6118/01 6/25101 7/2/01 7/9/01 7/ 16/01 7123/01 7/30/01 8/6/01 8/ 13/01 812 0/01
Specific Conductance
U. IOU
0.140
in 0.120
3
0.100
0.080
0.060
O
U 0.040
0.020 _
0.000 .
6/18101 6125/01 712/01 7/9/01 7116/01 7123101 7/30101 816/01 8113101 8/20/C

DMP-1: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH Dissolved Oxvaen
IL.VV
10.00
8.00
a 6.00
4.00
2.00
0.00
6/18/01 6125/01 712/01 719/01 7/16/01 7123/01 7/30/01
Oxidation Reduction Potential
500.0
450.0
400.0
350.0
> 300.0
E
a 250.0
w 200.0
O
150.0
100.0
50.0
0.0
6118101 6/25/01 7/2/01 7/9101 7/ 16101 7123101 7130/01
.J
t
at
E
O
0
1.80
1.60
1.40
1.20
1.00
--
D.80
0.60
0.40
D.20
D.00
6/ 18/01 6/25/01 7/2101 7/9/01 7/16/01 7123101 7/30101
Specific Conductivity
1.200
1.000
rn
0.800 --- ----
w
0.600
M
c 0.400
0
U
0.200
0.000
6/ 18/01 6/25/01 7/2101 7/9/01 7/16/01 7/23/01 7130101

DMP-2 : Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
7.50
7.00
6.50
6.00 •
2
1
5.50
5.00
4.50
4.00
6/18/01 6125/01 72/01 7/9101 7116101 7123/01 7/30/01
Oxidation Reduction Potential
400.0
350.0
300.0
57
E 250.0
n'
a: 200.0
0
150.0
100.0
50.0
0.0
6118/01 625101 72101 7/9/01 7/ 16/01 7/23/01 7/30/01
Dissolved Oxygen
O.UU
5.00
4.00
J
0)
E 3.00
O
2.00
1.00
0.00
6/18/01 625/01 712/01 7/9/01 7/ 16/01 7/23/01 7130101
Specific Conductivity
0.600
0.500
N
0.400
w 0.300
a
C 0.200
U
0.100 _
0.000
6/18/01 6/25/01 72/01 7/9/01 7/16/01 7/23/01 7/30/01

DMP-3: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH Dissolved Oxygen
10.00
9.00
8.00
2
n
7.00
6.00
5.00
4.00
6118/01 6125101 7/2/01 7/9/01 7116/01 7123/01 7/30/01 8/6101 8/ 13101 8/20/
Oxidation Reduction Potential
VUU.0
500.0
400.0
E
E 300.0 —
71
IL
0:
O
200.0
100.0
0.0
6118101 6/25/01 M01 719/01 7/16101 7123101 7/30101 8/6101 8/13/01 8/20/01
V.VV
9.00
8.00
7.00
-J 6.00
rn
E 5.00
0 4.00
3.00
2.00
1.00
0.00 .
C 6/18/01 6125/01 7/2/01 7/9/01 7/16/01 7/23/01 7130101 816/01 8/13/01 8120/C
Specific Conductance
0.200
0.180
0.160
in 0.140
3
0.120
0.100
0.080
c
0.060
U --
0.040
0.020
0.000
6118/01 6/25/01 7/2/01 7/9/01 7/16/01 7/23/01 7/30/01 816/01 8/13101 8/201 C

DMP-4: Variation of Field Parameters During and After The Phase I Full Scale ISCO Application
pH
8.00
7.50
7.00
6.50
a 6.00
5.50
5.00
4.50
4.00
6118/01 6/25/01 7/2/01 719/01 7/16/01 7/23/01 7130/01 8/6/01 8113/01 8/20101
Oxidation Reduction Potential
I UVV.0
900.0
800.D
700.D
j 600.0
E
`" 500.0
IL
0 400.0
300.0
200.0
100.0
0.0
6/18/01 6125/01 7001 7/9101 7116/01 7/23101 7/30/01 8/6101 8/13/01 8120/01
Dissolved Oxygen
9.00
8.00
7.00
6.00
J iq�
as 5.00
E
O 4.00
0
3.00
2.0D
1.00
0.00 .
6/18101 6/25/01 7/2/01 7/9101 7/16/01 7123/01 7/30101 8/6/01 8/ 13/01 8/20101
Specific Conductance
U.UUV
7.00D
6.00D
Cn
5.000
4.000
3.000
0
U 2.000
1.000
0.000
6118/01 6/25/01 7/2101 7/9/01 7/16/01 7/23/01 7130/01 8/6/01 8/13101 8120101

BMW-3 Field Parameters Variation During the Injection Period
pH Dissolved Oxygen
I.V V
1.40
1.20
1.00
0.80
0.60
0.40
0.20
0.00
s.so
9.60
.
6/18101 6/25101 7/2/01 7/9/01 7/16/01 7123/01 7/30/01
Oxidation Reduction Potential
-400.0
-450.0
-500.0
-550.0
E -600.0
� -650.0
0 -700.0
-750.0
-800.0
-850.0
-900.0
6/18/01 6125101 7/2/01 719/01 7/16/01 7123/01 7/30/01
I.OV
1.60
1.40
1.20
J
1.00
E
O 0.80
0
0.60
0.40 _
0.20
0.00 .
6118/01 6/25/01 7/2/01 7/9/01 7/16/01 7/23/01 7/30/01
Specific Conductivity
0.950
0.900
in
0.850
.�- 0.800
0
c 0.750
0
U
0.700
0.650 .
6118/01 6/25/01 7/2101 7/9101 7116/01 7/23/01 7/30/01

IT Corporation ofNorth Carolina, Inc.
A Alember of The IT Croup
Appendix G
Treatment System - Laboratory Analytical Data Reports

aceAnalytical `M
www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Keith Ogden
Phone: [phone]
Pace Analytical Services, Inc.
9800 Xincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536538 Project Sample Number: 9221720-001 Date Collected: 03/28/01 15:15
Client Sample ID• WSP-1 Matrix: Water Date Received: 03/29/01 16:45
Parameters
Results
Units PRL
Dilution
Analyzed .
Analyst
CAS#
GC Semivolatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
Dichlorodifluoromethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-71-8
Chloromethane
NO
ug/l
50.
25.0
04/04/01
22:38
PPM
74-87-3
Vinyl chloride
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
75-01-4
Bromomethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
74-83-9
Chloroethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-00-3
Trichlorofluoromethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-69-4
1,1-Dichloroethene
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-35-4
Methylene chloride
NO
ug/l
50.
25.0
04/04/01
22:38
PPM
75-0972
trans-1,2-Dichloroethene
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
156-60-5
1,1-Dichloroethane
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
75-34-3
Chloroform
NO
ug/t
25.
25.0
04/04/01
22:38
PPM
67-66-3
1,1,1-Trichloroethane
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
71-55-6
Carbon tetrachloride
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
56-23-5
1,2-Dichloroethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
107-06-2
Trichloroethene
490
ug/l
25.
25.0
04/04/01
22:38
PPM
79-01-6
1,2-Dichloropropane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
78-87-5
Bromodichloromethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-27-4
cis-1,3-Dichlo�opropene
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
10061-01-5
trans-1,3-Dichloropropene
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
10061-02-6
1,1,2-Trichloroethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
79-00-5
Tetrachloroethene
1200
ug/l
25.
25.0
04/04/01
22:38
PPM
127-18-4
Dibromochloromethane
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
124-48-1
Bromoform
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
79-34-5
Methyl-tert-butyl ether
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
1634-04-4
Diisopropyl ether
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
108-20-3
Benzene
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
71-43-2
Date: 04/24/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Ftnote Limit
Page: 1
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical`M
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9221720
Client
Project ID:
SLS-Greensboro/010305/107535
Lab Sample No: 921536538
Project Sample
Number:
9221720-001
Date Collected: 03/28/01 15:15
Client Sample ID• WSP-1
Matrix:
Water
Date Received:
03/29/01 16:45
Parameters
Results
Units
PRL
Dilution Analyzed
Analyst
CAS# Ftnote Limit
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
108-88-3
Toluene
Chlorobenzene
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
108-90-7
Ethylbenzene
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
100-41-4
m&p-Xylene
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
7816-60-0
o-Xylene
ND
Ug/l
25.
25.0
04/04/01
22:38
PPM
95-47-6
1,3-Dichlorobenzene
ND
ug/l
25.
25.0
04/04/01
22:38
PPM
541-73-1
1,4-Dichlorobenzene
ND
Ug/l
25.
25.0
04/04/01
22:38
PPM
106-46-7,
1,2-Dichlorobenzene
NO
ug/l
25.
25.0
04/04/01
22:38
PPM
95-50-1
1-Chloro-3-fluorobenzene (S)
105
%
1.0
04/04/01
22:38
PPM
625-98-9
Date: 04/24/01
Page: 2
Laoratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

1
aceAnalytical "'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 1(,10
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536561 Project Sample Number: 9221720-002 Date Collected: 03/28/01 15:20
Client Sample ID: WSP-2 Matrix: Water Date Received: 03/29/01 16:45
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
GC Semivolatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
Dichlorodifluoromethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-71-8
Chloromethane
NO
ug/l
2.0
1.0
04/03/01
23:33
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-00-3
Trichlorofluoromethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-69-4
1,1-Dichloroethene
NO
ug/t
1.0
1.0
04/03/01
23:33
PPM
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
04/03/01
23:33
PPM
75-09-2
trans-1,2-Dichloroethene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
156-60-5
1,1-Dichloroethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-34-3
Chloroform
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
67-66-3
1,1,1-Trichloroethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
56-23-5
1,2-Dichloroethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
107-06-2
Trichloroethene
26.
ug/l
1.0
1.0
04/03/01
23:33
PPM
79-01-6
1,2-Dichloropropane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
78-87-5
Bromodichloromethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-27-4
cis-1,3-Dichloropropene i
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
10061-01-5
trans-1,3-Dichloropropene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
10061-02-6
1,1,2-Trichloroethane
NO
ug/l
1.0
1.0
04/03/01(
23:33
PPM
79-00-5
Tetrachloroethene
51.
ug/l
1.0
1.0
04/03/01
23:33
PPM'
127-18-4
Dibromochloromethane
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
124-48-1
Bromoform
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
75-25-2
1,1,2,2-Tetrachloroethane
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
79-34-5
Methyl-tert-butyl ether
NO
ug/l
1..0
1.0
04/03/01
23:33
PPM
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
108-20-3
Benzene
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
71-43-2
Toluene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
108-88-3
Chlorobenzene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
7816-60-0
o-Xylene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
95-47-6
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
04/03/01
23:33
PPM
541-73-1
1,4-Dichlorobenzene
NO
ug/l
1.0
1.0
04/03/01
23:33
PPM
106-46-7
Date: 04/24/01 Page: 3
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 1 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aceAnaIXicaIrm
www. pacelabs. cam
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville. NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536561 Project Sample Number: 9221720-002 Date Collected: 03/28/01 15:20
client Sample ID• WSP-2 Matrix: Water Date Received: 03/29/01 16:45
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit _
1,2-Dichlorobenzene ND ug/l 1.0 1.0 04/03/01 23:33 PPM 95-50-1
1-Chloro-3-fluorobenzene (S) 114 % 1.0 04/03/01 23:33 PPM 625-98-9
Date: 04/24/01
Page: 4
Laboratory Certification INREPORT OF LABORATORY ANALYSIS KY Laboratory Certification IDs
NC Wastewater 12 Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
e Analytical'
9800 Kincey rsvillAvenue, Suite too
Huntersvifle. NC 2807878
Phone: [phone]
www.pacelabs.com
Fax:[phone]
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536579 Project Sample Number: 9221720-003 Date Collected: 03/28/01 15:00
Client Sample ID• WSP-3 Matrix: Water Date Received: 03/29/01 16:45
Parameters
Results
Units PRL
Dilution
Analyzed
Analyst
CAS#
GC SemivolatiLes
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
DichlorodifLuoromethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
04/04/01
00:15
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-01-4
Bromomethane
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-69-4
1,1-Dichloroethene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
75-35-4
.Methylene chloride
ND
ug/l
2.0
1.0
04/04/01
00:15
PPM
75-09-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
156-60-5
1,1-Dichloroethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-34-3
Chloroform
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
67-66-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
56-23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
107-06-2
Trichloroethene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
79-01-6
1,2-Dichloropropane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
75-27-4
cis-1,3-Dichloropropene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
10061-02-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
79-00-5
TetrachLoroetherie
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
127-18-4
Dibromochloromethane
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
124-48-1
Bromoform
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM '
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
79-34-5
Methyl-tert-butyl ether
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
108-20-3
Benzene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
71-43-2
Toluene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
108-88-3
Chlorobenzene
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
100-41-4
m&p-Xylene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
7816-60-0
o-Xylene
ND
ug/l
1.0
1.0
04/04/01
00:15
PPM
95-47-6
1,3-Dichlorobenzene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1.0
04/04/01
00:15
PPM
106-46-7
Date: 04/24/01
Laboratory Certification IDS
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Ftnote Limit
Page: 5
Laborator,/Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical "
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax. [phone]
Lab Project Number: 9221720
Client Project ID: 9LS-Greensboro/010305/107535
Lab Sample No: 921536579 Project Sample Number: 9221720-003 Date Collected: 03/28/01 15:00
Client Sample ID: WSP-3 Matrix: Water Date Received: 03/29/01 16:45
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
1,2-Dichlorobenzene ND ug/L 1.0 1.0 04/04/01 00:15 PPM 95-50-1
1-Chloro-3-fLuorobenzene (S) 115 % 1.0 04/04/01 00:15 PPM 625-98-9
Date: 04/24/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical'M
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536587 Project Sample Number: 9221720-004 Date Collected: 03/28/01 14:30
Client Sample ID: WSP-4 Matrix: Water Date Received: 03/29/01 16:45
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Wet Chemistry
Trace ICP Metals
Iron
Lead
Manganese
Date Digested
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
Oil and Grease
Ion Chromatography
Nitrate -Nitrite (as N)
GC/MS Volatiles
Volatile GC/MS by 624
Vinyl chloride
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
Methyl-tert-butyl ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
1,1,1-Trichloroethane
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Date: 04/24/01
Method: EPA
200.7
Prep Method:
EPA 200.7
12.
mg/l
0.050
1.0
04/08/01
16:14
RWF
7439-89-6
0.049 mg/l
0.0050
1.0
04/08/01
16:14
RWF
7439-92-1
0.71 mg/l
0.0050
1.0
04/08/01
16:14
RWF
7439-96-5
04/05/01
Method: EPA
160.2
Prep Method:
EPA 160.2
92.
mg/l
6.7
6.7
04/03/01
CDE
Method: EPA
1664
Prep Method:
EPA 1664
14.
mg/l
5.0
1.0
04/03/01
BYH
Method: EPA
300.0
Prep Method:
EPA 300.0
ND
mg/l
0.30
1.0
03/30/01
YMH
7727-37-9
Method: EPA
624
Prep Method:
EPA 624
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
75-01-4
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
75-35-4
ND
ug/L
5.0
1.0
04/01/01
00:23
JRS
75-09-2
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
156-60-5
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
1634-04-4
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
75-34-3
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
156-59-2
18.
ug/l
5.0
1.0
04/01/01
00:23
JRS
67-66-3
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
71-55-6
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
107-06-2
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
56-23-5
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
71-43-2
Page: 7
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full. VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

w
aceAnalXical `''
www.pacelabs.com
Face Analytical Services, inc.
9800 Kinney Avenue. Suite 100
Hunrerswlle, NC 28078
Phone:
Fax: [phone]
--
Lab Project Number: 9221720
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921536587
Project Sample
Number: 9221720-004
Date Collected:
03/28/01 14:30
. Client Sample ID: WSP-4
Matrix: Water
Date Received: 03/29/01 16:45
Parameters
Results
Units
PRL
Dilution
Analyzed
Analyst
CAS# Ftnote Limit
Trichloroethene
NO
ug/L
5.0
1.0
04/01/01
00:23
JRS
79-01-6
1,2-Dichloropropane
NO
ug/l
5.0
1.0
04/01/01
00:23
JRS
78-87-5
Toluene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
108-88-3
1,1,2-Trichloroethane
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
79-00-5
Tetrachloroethene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
127-18-4
Ethylbenzene
NO
ug/l
5.0
1.0
04/01/01
00:23
JRS
100-41-4
m$p-Xylene
ND
ug/l
10.
1.0
04/01/01
00:23
JRS
7816-60-0
o-Xylene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
95-47-6
Bromoform
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
79-34-5
1,3-Dichlorobenzene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
541-73-1
1,2-Dichlorobenzene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
95-50-1
Dibromofluoromethane (S)
96
%
1.0
04/01/01
00:23
JRS
Toluene-d8 (S)
99
%
1.0
04/01/01
00:23
JRS
2037-26-5
4-Bromofluorobenzene (S)
115
%
1.0
04/01/01
00:23
JRS
460-00-4 1
Naphthalene
NO
ug/l
5.0
1.0
04/01/01
00:23
JRS
91-20-3
1,2-Dibromoethane (EDB)
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
106-93-4
i-
1,3,5-Trimethylbenzene
NO
ug/l
5.0
1.0
04/01/01
00:23
JRS
108-67-8
1,2,4-Trimethylbenzene
ND
ug/l
5.0
1.0
04/01/01
00:23
JRS
95-63-6
Date: 04/24/01
Page: 8
Laboratory certification IDS lDs
REPORT OF LABORATORY ANALYSIS Laboratory Certification
NC Wastewater 12 KY Drinking Water 90090
90
NC Drinking Water 37706 This report shall not be reproduced, except in full. VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

rm
woA lalytical
www.pacelabs.com
r IASI Inc. Charlotte
l ';800 Kincey Ave.
Suite 100
"untersville, NC 28078
Attn: Project Management
Rhone: [phone]
I !
jab Sample No: 921536587
�lient Sample ID: WSP-4
Parameters
i
Wet Chemistry
Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
f
i
I
i
I
I
Date: 04/10/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
I
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phcr e 828?54.7175
Fax: [phone]
Lab Project Number: 9319384
Client Project ID: IT CORP - 9221720
Project Sample Number: 9319384-001 Date Collected: 03/28/01 14:30
Matrix: Water Date Received: 03/29/01 16:45
Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: EPA 351.2 Prep Method: EPA 351.2
0.15 mg/l 0.10 04/10/01 JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

7ceAnalytical
,
r
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Lab Project Number: 1043229
Client Project ID: 9221720 IT
Lab Sample No: 921536595 Project Sample Number: 1043229-003 Date Collected: 03/28/01 17:00
Client Sample ID: ASP-2 #200 Matrix: Air Date Received: 03/29/01 16:45
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Air
GC/MS VOCs, in Air
Method: TO-14 Source
Prep Method:
TO-14 Source
Dichlorodifluoromethane
ND
ppmv
0.13
04/09/01
15:51
RGY
75-71-8
Chloromethane
ND
ppmv
0.13
04/09/01
15:51
RGY
74-87-3
Dichlorotetrafluoroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
76-14-2
Vinyl chloride
ND
ppmv
0.13
04/09/01
15:51
RGY
75-01-4
Bromomethane
ND
ppmv
0.13
04/09/01
15:51
RGY
74-83-9
Chloroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
75-00-3
Trichlorofluoromethane
ND
ppmv
0.13
04/09/01
15:51
RGY
75-69-4
1,1-Dichloroethene
ND
ppmv
0.13
04/09/01
15:51
RGY
75-35-4
1,1,2-Trichlorotrifluoroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
76-13-1
Methylene chloride
ND
ppmv
0.13
04/09/01
15:51
RGY
75-09-2
1,1-6ichloroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
75-34-3
cis-1,2-Dichloroethene
0.39
ppmv,
0.13
04/09/01
15:51
RGY
156-59-2
Chloroform
ND
ppmv
0.13
04/09/01
15:51
RGY
67-66-3
1,1,1-Trichloroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
71-55-6
1,2-Dichloroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
107-06-2
Benzene
ND
ppmv
0.13
04/09/01
15:51
RGY
71-43-2
Carbon tetrachloride
ND
ppmv
0.13
04/09/01
15:51
RGY
56-23-5
1,2-Dichloropropane
ND
ppmv
0.13
04/09/01
15:51
RGY
78-87-5
Trichloroethene
0.33
ppmv
0.13
04/09/01
15:51
RGY
79-01-6
cis-1,3-Dichloropropene
ND
ppmv
0.13
04/09/01
15:51
RGY
10061-01-5
trans-1,3-Dichloropropene
ND
ppmv
0.13
04/09/01
15:51
RGY
10061-02-6
Toluene
ND
ppmv
0.13
04/09/01
15:51
RGY
108-88-3
1,1,2-Trichloroethane
ND
ppmv
0.13
04/09/01
15:51
RGY
79-00-5
1,2-Dibromoethane (EDB)
ND
ppmv
0.13
04/09/01
15:51
RGY
106-93-4
Tetrachloroethene
2.4
ppmv
1.3
04/09/01
15:51
RGY
127-18-4
Chlorobenzene
ND
ppmv
0.13
04/09/01
15:51
RGY
108-90-7
Ethylbenzene
ND
ppmv
0.13
04/09/01
15:51
RGY
100-41-4
Date: 04/11/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

i
aceAnalytical
Lab Sample No: 921536595
Client Sample ID: ASP-2 #200
Parameters
m&p-Xylene
o-Xylene
Styrene
1,1,2,2-Tetrachloroethane
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2,4-Trichlorobenzene
Hexachloro-1,3-butadiene
THC as Gas
4-Methyl-2-pentanone (MIBK)
2-Butanone (MEK)
Lab Sample No: 921536603
Client Sample ID: ASP-3 #174
Parameters
Lab Project Number: 1043229
Client Project ID: 9221720 IT
Project Sample Number: 1043229-003 Date Collected: 03/28/01 17:00
Matrix: Air Date Received: 03/29/01 16:45
Results Units PRL Analyzed Analyst CAS# Ftnote Limit
i
Air
GC/MS VOCs, in Air
Dichlorodifluoromethane
Chloromethane
Dichlorotetrafluoroethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
1,1,2-Trichlorotrifluoroethane
Methylene chloride
1,1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
Date:.04/11/01
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
7.4
ppmv
1.3
ND
ppmv
0.27
ND
ppmv
0.27
04/09/01 15:51 RGY ` 7816-60-0
04/09/01 15:51 RGY 95-47-6
04/09/01 15:51 RGY 100-42-5
04/09/01 15:51 RGY 79-34-5
04/09/01 15:51 RGY 108-67-8
04/09/01 15:51 RGY 95-63-6
04/09/01 15:51 RGY 541-73-1
04/09/01 15:51 RGY 106-46-7
04/09/01 15:51 RGY 95-50-1
04/09/01 15:51 RGY 120-82-1
04/09/01 15:51 RGY 87-68-3
04/09/01 15:51 RGY
04/09/01 15:51 RGY 108-10-1 1
04/09/01 15:51 RGY 78-93-3 1
Project Sample Number: 1043229-002
Matrix: Air
Results Units PRL Analyzed
Method: TO-14 Source
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
ND
ppmv
0.13
Date Collected: 03/28/01 17:30
Date Received: 03/29/01 16:45
Analyst CAS# Ftnote Limit
Prep Method: TO-14 Source
04/06/01 14:24 RGY 75-71-8 2
04/06/01 14:24 RGY 74-87-3
04/06/01 14:24 RGY 76-14-2
04/06/01 14:24 RGY 75-01-4
04/06/01 14:24 RGY 74-83-9
04/06/01 14:24 RGY 75-00-3
04/06/01 14:24 RGY 75-69-4
04/06/01.14:24 RGY 75-35-4
04/06/01 14:24 RGY 76-13-1
04/06/01 14:24 RGY 75-09-2
04/06/01 14:24 RGY 75-34-3
04/06/01 14:24 RGY 156-59-2
04/06/01 14:24 RGY 67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2

2ceAnalytical-
Lab Project Number: 1043229
Client Project ID: 9221720 IT
Lab Sample No: 921536603
Project Sample
Number: 1043229-002
Date Collected: 03/28/01 17:30
Client Sample ID: ASP-3 #174
Matrix: Air
Date Received: 03/29/01 16:45
Parameters
Results
Units
PRL
Analyzed
Analyst CAS# Ftnote Limit
1,1,1-Trichloroethane
ND
ppmv
0.13
04/06/01
14:24
RGY
71-55-6
1,2-Dichloroethane
ND
ppmv
0.13
04/06/01
14:24
RGY
107-06-2
Benzene
ND.
ppmv
0.13
04/06/01
14:24
RGY
71-43-2
Carbon tetrachloride
ND
ppmv
0.13
04/06/01
14:24
RGY
56-23-5
1,2-Dichloropropane
ND
ppmv
0.13
04/06/01
14:24
RGY
78-87-5
Trichloroethene
ND
ppmv
0.13
04/06/01
14:24
RGY
79-01-6
cis-1,3-Dichloropropene
ND
ppmv
0.13
04/06/01
14:24
RGY
10061-01-5
trans-1,3-Dichloropropene
ND
ppmv
0.13
04/06/01
14:24
RGY
10061-02-6
Toluene
ND
ppmv
0.13
04/06/01
14:24
RGY
108-88-3
1,1,2-Trichloroethane
ND
ppmv
0.13
04/06/01
14:24
RGY
79-00-5
1,2-Dibromoethane (EDB)
ND
ppmv
0.13
04/06/01
14:24
RGY
106-93-4
Tetrachloroethene
0.17
ppmv
0.13
04/06/01
14:24
RGY
127-18-4
Chlorobenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
108-90-7
Ethylbenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
100-41-4
m&p-Xylene
ND
ppmv
0.13
04/06/01
14:24
RGY
7816-60-0
o-Xylene
ND
ppmv
0.13
04/06/01
14:24
RGY
95-47-6
Styrene
ND
ppmv
0.13
04/06/01
14:24
RGY
100-42-5
1,1,2,2-Tetrachloroethane
ND
ppmv
0.13
04/06/01
14:24
RGY
79-34-5
1,3,5-Trimethylbenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
108-67-8
1,2,4-Trimethylbenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
95-63-6
1,3-Dichlorobenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
541-73-1
1,4-Dichlorobenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
106-46-7
1,2-Dichlorobenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
95-50-1
1,2,4-Trichlorobenzene
ND
ppmv
0.13
04/06/01
14:24
RGY
120-82-1 3
Hexachloro-1,3-butadiene
ND
ppmv
0.13
04/06/01
14:24
RGY
87-68-3
THC as Gas
ND
ppmv
1.3
04/06/01
14:24
RGY
4-Methyl-2-pentanone (MIBK)
ND
ppmv
0.27
04/06/01
14:24
RGY
108-10-1 4
2-Butanone (MEK)
ND
ppmv
0.27
04/06/01
14:24
RGY
78-93-3 4
Date: 04/11/01 Page: 3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

i - _.-_AI_ _ --JIF _ J5 .-_JY . _ kni icy...."ec St __cu nt
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required Chant Infonnahon: Section A Required Client Information: Section B I Page: f Of To Be Completed by Paco Analytical and Client Section C
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__---- �&.�/_Z
— -- — — I Client Information Check quote/contract):
Jdress rInvoice To, Roque stad Due ale: 'TAT: Project Manager:
r�tJ z L�l -ZW4 y e AL V _b � ,�! o D �>ti% y �i o j c-; %D_
_�_ 2/� / Pp' t/ • Torn around limes less than 14 days subject to Prolecr M.
gel�r,v�Lt.,c x� � _ �7� Awl6it�dsr�All --_ laburalory and contractual obligations and may result in a
Project Name: • Rush Turnaround Surcharge. Profile M:
Turn Around Time (rAT) in calendar days.
'hun - Fa Project Number: Requested Analysts:/ ! T�
Section D Required Client Information: Valid Matrix Codes 4—
MATRIX cone o Preservatives
WATER W T w w U w
S A M P L C I D sou_ sl $ �_ J
OIL OLAlt
One character per box. WIPE wP x O m N 0
c =
A—Z, 0-9 / .- F o a c�' O
W ( ) TISSUE Ts ¢ U c rn, z U m to
t_ Sample IDS MUST BE UNIQUE OTH€n_,_.. -___oi _-_ mm / rld / yy hh: rmn a/p :w D x = = Z z �� 7 Remarks / Lab ID
T-r-
41.
/315
S P a= I<
J S 31 1F r
- _ 50-v---
f —r
lArl 36-I YX- x - - — - -- Sr---
t — - -
S � V D
• 3 � 7 t�' ��v I+73o Is'3���
�I r:r:
Sample Condition Sample Notes Item No. vulshid By I Coi Time Accepted By I Company
Temp in °C:
Received on ICE: — — Y / N �/n —— ��o
Sealed Cooler: Y / N H F
Sal yrles Intact: Y / N
Additional Comments: NAME AND SIGNATURE
PRINT Name of SAMPLER:
SIGNATURE oI SAMPI FR: —
SEE REVERSE SIDE FOR INSTRUCTIONS
OHIG11rinl
DATE Signad:
(MM / DD / YY)
Pace Analytical Services, If
Form COCuI u,.uu

aceAnalyticalTM
www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Charles Bertz
Phone: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921583209
Project Sample
Number:
9222475-001
Date Collected: 04/26/01 10:30
Client Sample ID: WSP-1
Matrix:
Water
Date Received: 04/26/01 15:20
Parameters
Results
Units
PRL
Dilution
Analyzed
Analyst CAS# Ftnote
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method: EPA 601/602
Dichlorodiflupromethane
ND
ug/l
50.
50.0
04/28/01
KST
75-71-8
Chloromethane
ND
ug/l
100
50.0
04/28/01
KST
74-87-3
Vinyl chloride
ND
ug/l
50.
50.0
04/28/01
KST
75-01-4
Bromomethane
ND
ug/l
50.
50.0
04/28/01
KST
74-83-9
Chloroethane
ND
ug/l
50.
50.0
04/28/01
KST
75-00-3
Trichlorofluoromethane
ND
ug/l
50.
50.0
04/28/01
KST
75-69-4
1.1-Dichloroethene
ND -
ug/l
50.
50.0
04/28/01
KST
75-35-4
Methylene chloride
ND
ug/l
100
50.0
04/28/01
KST
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
50.
50.0
04/28/01
KST
156-60-5
1.1-Dichloroethane
ND
ug/l
50.
50.0
04/28/01
KST
75-34-3
Chloroform
ND
ug/l
50.
50.0
04/28/01
KST
67-66-3
1.1.1-Trichloroethane
ND
ug/l
50.
50.0
04/28/01
KST
71-55-6
Carbon tetrachloride
ND
ug/l
50.
50.0
04/28/01
KST
56-23-5
1.2-Dichloroethane
ND
ug/l
50.
50.0
04/28/01
KST
107-06-2
Trichloroethene
ND
ug/l
50.
50.0
04/28/01
KST
79-01-6
1.2-Dichloropropane
ND
ug/l
50.
50.0
04/28/01
KST
78-87-5
Bromodichloromethane
ND
ug/l
50.
50.0
04/28/01
KST
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
50.
50.0
04/28/01
KST
10061-01-5
trans-1.3-Dichloropropene
ND
ug/l
50.
50.0
04/28/01
KST
10061-02-6
1.1.2-Trichloroethane
ND
ug/l
50.
50.0
04/28/01
KST
79-00-5
Tetrachloroethene
1600
ug/l
50.
50.0
04/28/01
KST
127-18-4
Dibromochloromethane
ND
ug/l
50.
50.0
04/28/01
KST
124-48-1
Bromoform
ND
ug/l
50.
50.0
04/28/01
KST
75-25-2
1.1.2.2-Tetrachloroethane
ND
ug/l
50.
50.0
04/28/01
KST
79-34-5
Methyl-tert-butyl ether
ND
ug/1
50.
50.0
04/28/01
KST
1634-04-4
Diisopropyl ether
ND
ug/l
50.
50.0
04/28/01
KST
108-20-3
Benzene
ND
ug/l
50.
50.0
04/28/01
KST
71-43-2
Date: 05/08/01
Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

1
ace Analytical "'
www.pacelabs.com
Lab Sample No: 921583209
Client Sample ID: WSP-1
Parameters
mit
Toluene
Chlorobenzene
Ethylbenzene
m&p-Xylene
o-Xylene
1.3-Dichlorobenzene
1.4-Dichlorobenzene
1,2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
Date: 05/08/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9222475-001 Date Collected: 04/26/01 10:30
Matrix: Water Date Received: 04/26/01 15:20
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
ND
ug/1
50.
50.0
04/28/01
KST
108-88-3
ND
ug/l
50.
50.0
04/28/01
KST
108-90-7
ND
ug/1
50.
50.0
04/28/01
KST
100-41-4
ND
ug/l
50.
50.0
04/28/01
KST
7816-60-0
ND
ug/l
50.
50.0
04/28/01
KST
95-47-6
ND
ug/l
50.
50.0
04/28/01
KST
541-73-1
ND
ug/l
50.
50.0
04/28/01
KST
106-46-7
ND
ug/l
50.
50.0
04/28/01
KST
95-50-1
106
%"
1.0
04/28/01
KST
625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical'"
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Huntersville. NC 28078
Phone. [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
- Lab Sample No: 921583233 Project Sample Number: 9222475-002 Date Collected: 04/26/01 10:25
Client Sample ID: WSP-2 Matrix: Water Date Received: 04/26/01 15:20
imit
Parameters
GC Volatiles
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
04/28/01
04:23
KST
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-01-4
Bromomethane
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
74-83-9
Chlorcethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-69-4
1,1-Dichloroethene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
04/28/01
04:23
KST
75-09-2
trans-1,2-Dichloroethene
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
156-60-5
1.1-Dichloroethane
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
75-34-3
Chloroform
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
67-66-3
1.1.1-Trichloroethane
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
56-23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
107-06-2
Trichloroethene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
79-01-6
1.2-Dichloropropane
ND
ug/l
1.0
1.0
04/128/01
04:23
KST
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
10061-01-5
trans-1,3-Dichloropropene
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
10061-02-6
1.1.2-Trichloroethane
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
79-00-5
Tetrachloroethene
16.
ug/1
1.0
1.0
04/28/01
04:23
KST
127-18-4
Dibromochloromethane
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
124-48-1
Bromoform
ND
ug/1
1.0
1.0
04/28/01
04:23
KST
75-25-2
1.1.2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
79-34-5
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
108-20-3
Benzene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
71-43-2
Toluene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
108-88-3
Chlorobenzene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
7816-60-0
o-Xylene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
95-47-6
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
541-73-1
1,4-Dichlorobenzene
ND
ug/l
1.0
1.0
04/28/01
04:23
KST
106-46-7
Date: 05/08/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page: 3
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical rM
- www.pacelabs.com
Lab Sample No: 921583233
Client Sample ID: WSP-2
Parameters Results
;imit
1.2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
Date: 05/08/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
ND
95
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone.- 704.875.9092
Fax: 704.875,9091
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9222475-002 Date Collected: 04/26/01 10:25
Matrix: Water Date Received: 04/26/01 15:20
Units PRL Dilution Analyzed Analyst CAS# Ftnote
ug/l 1.0 1.0 04/28/01 04:23 KST 95-50-1
% 1.0 04/28/01 04:23 KST 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical "
www.pacelabs.com
I
Pace Analytical Services, Inc.
9300Kince}•Avenue. Suite 100
Huntersville. NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921583241 Project Sample Number: 9222475-003 Date Collected: 04/26/01 10:35
Client Sample ID: WSP-3 Matrix: Water Date Received: 04/26/01 15:20
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
imit
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA
601/602
Prep Method:
EPA
601/602
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
04/28/01
05:09
KST
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
. 75-01-4
Bromomethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
75-69-4
1.1-Dichloroethene
ND
ug/1
1.0
1.0
04/28/01
05:09
KST
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
04/28/01
05:09
KST
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
156-60-5
1.1-Dichloroethane
ND
ug/1
1.0
1.0
04/28/01
05:09
KST
75-34-3
Chloroform
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
67-66-3
1.1,1-Trichloroethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
_ 56-23-5
1.2-Dichloroethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
107-06-2
Trichloroethene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
79-01-6
1.2-Dichloropropane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
10061-01-5
trans-1.3-Dichloropropene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
10061-02-6
1.1.2-Trichloroethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
79-00-5
Tetrachloroethene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
127-18-4
Dibromochloromethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
124-48-1
Bromoform
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
75-25-2
1.1.2.2-Tetrachloroethane
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
79-34-5
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
108-20-3
Benzene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
71-43-2
Toluene
ND
ug/1
1.0
1.0
04/28/01
05:09
KST
108-88-3
Chlorobenzene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
7816-60-0
o-Xylene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
95-47-6
1.3-Dichlorobenzene
ND
ug/l
1.0
1.0
04/28/01
05:09
KST
541-73-1
1,4-Dichlorobenzene
ND
ug/l.
1.0
1.0
04/28/01
05:09
KST
106-46-7
Date: 05/08/01
Page: 5
Laboratory Certification IDs
REPORT OF
LABORATORY
ANALYSIS
Laboratory Certification IDs
NC Wastewater 12
KY Drinking Water 90090
NC Drinking Water 37706
This report shall
not be reproduced,
except in
full,
VA Drinking Water 213
SC 99006
without
the written
consent of Pace Analytical Services,
Inc.
FL NELAP E87627

aceAnalytical'M
www.pacelabs.com
I
Lab Sample No: 921583241
Client Sample ID: WSP-3
Parameters
I _imit
.1.2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
J1
Date: 05/08/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kin^ Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9222475-003 Date Collected: 04/26/01 10:35
Matrix: Water Date Received: 04/26/01 15:20
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
ND ug/l 1.0 1.0 04/28/01 05:09 KST 95-50-1
97 % 1.0 04/28/01 05:09 KST 625-98-9
Page: 6
REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
KY Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

1
aceAnalytical'M
www.pacelabs.com
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921583308 Project Sample Number: 9222475-004 Date Collected: 04/26/01 10:15
Client Sample ID: WSP-4 Matrix: Water Date Received: 04/26/01 15:20
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
_imit
Metals
Trace ICP Metals
Method: EPA
200.7
Prep Method:
EPA
200.7
Iron
1.4
mg/l
0.050
1.0
05/05/01
00:25
RWF
7439-89-6
Lead
0.0077
mg/,1
0.0050
1.0
05/05/01
00:25
RWF
7439-92-1
Manganese
1.2
mg/l
0.0050
1.0
05/05/01
00:25
RWF
7439-96-5
Date Digested
05/03/01
Wet Chemistry
Total Suspended Solids
Method: EPA
160.2
Prep Method:
EPA
160.2
Total Suspended Solids
15.
mg/l
2.0
2.0
05/01/01
CDE
Hexane Extractable Material
Method: EPA
1664
Prep Method:
EPA
1664
Oil and Grease
ND
mg/l
5.0
1.0
04/27/01
BYH
Ion Chromatography
Method: EPA
300.0
Prep Method:
EPA
300.0
Nitrate -Nitrite (as N)
ND
mg/l
0.30
1.0
04/27/01
YMH
7727-37-9
GC/MS Volatiles
Volatile GC/MS by 624
Method: EPA
624
Prep Method:
EPA
624
Vinyl chloride
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
75-01-4
1,1-Dichloroethene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
75-35-4
Methylene chloride
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
156-60-5
Methyl-tert-butyl ether
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
1634-04-4
1.1-Dichloroethane
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
75-34-3
cis-1.2-Dichloroethene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
156-59-2
Chloroform
17.
ug/l
5.0
1.0
05/07/01
19:14
RPJ
67-66-3
1,1.1-Trichloroethane
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
71-55-6
j 1.2-Dichloroethane
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
107-06-2
Carbon tetrachloride
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
56-23-5
-- Benzene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
71-43-2
Trichloroethene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
79-01-6
1.2-Dichloropropane
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
78-87-5
Toluene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
108-88-3
Date: 05/08/01
Page: 7
Laboratory certification lDs
REPORT
OF
LABORATORY ANALYSIS
Laborator�Certification IN
NC Wastewater 12
KY Drinking Water 90090
INC Drinking Water 37706
This report shall
not be reproduced, except
in
full,
VA Drinking Water 213
Sc 99006
without the written
consent of Pace Analytical
yt
Service
s. Inc.
FL NEL 27
AP E876

ace Analytical r
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222475
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921583308 Project Sample Number: 9222475-004 Date Collected: 04/26/01 10:15
Client Sample ID: WSP-4 Matrix: Water Date Received: 04/26/01 15:20
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote
.imi t
1,1.2-Trichloroethane
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
79-00-5
Tetrachloroethene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
127-18-4
Ethylbenzene
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
100-41-4
m&p-Xylene
NO
ug/l
10.
1.0
05/07/01
19:14
RPJ
7816-60-0
--, o-Xylene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
95-47-6
Bromoform
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
75-25-2
-. 1.1.2.2-Tetrachloroethane
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
79-34-5
1.3-Dichlorobenzene
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
541-73-1
1.2-Dichlorobenzene
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
95-50-1
Dibromofluoromethane (S)
104
%
1.0
05/07/01
19:14
RPJ
Toluene-d8 (S)
107
%
1.0
05/07/01
19:14
RPJ
2037-26-5
4-13romofluorobenzene (S)
92
%
1.0
05/07/01
19:14
RPJ
460-00-4
1.2-Dibromoethane
NO
ug/l
5.0
1.0
05/07/01
19:14
RPJ
106-93-4
Naphthalene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
91-20-3
1,3.5-Trimethylbenzene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
108-67-8
1..2.4-Trimethylbenzene
ND
ug/l
5.0
1.0
05/07/01
19:14
RPJ
95-63-6
Date: 05/08/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 8
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i
' I
- ace Analytical m
www.pacelabs.com
OASI Inc. Charlotte
)800 Kincey Ave.
Suite 100
duntersviLLe, NC 28078
Attn: Project Management
,hone: [phone]
ab Sample No: 921583308
;Bent Sample ID: WSP-4
!arameters
4et Chemistry
-Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
I
Date: 05/04/01
Laboratory Certification IDS
NC Wastewater 40
NC Drinking Water 37712
Results
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax:[phone]
Lab Project Number: 9319999
Client Project ID: IT-9222475
Project Sample Number: 9319999-001 Date Collected: 04/26/01 10:15
Matrix: Water Date Received: 04/26/01 15:20
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: EPA 351.2 Prep Method: EPA 351.2
0.16 mg/l 0.10 05/03/01 JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDS
TN Drinking Water 02980
SC Environmental 99030

L
:11.1.7-aceAnalXical
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Lab Project Number: 1044095
Client Project ID: 9222475 IT
Lab Sample No: 921583340 Project Sample Number: 1044095-001
Client Sample ID: ASP-2 #10 Matrix: Air
Parameters Results Units PRL Analyzed
Air
GC/MS VOCs, in Air
Dichlorodiflucromethane
Chloromethane
Dichlorotetrafluoroethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
1,1,2-Trichlorotrifluoroethane
Methylene chloride
1,1-Dichloroethene
cis-1,2-Dichloroethene
Chloroform
1,1,1-Trichloroethane
1,2-Dichloroethane
Benzene
Carbon tetrachloride
1,2-Dichloropropane
Trichloroethene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Toluene
1,1,2-Trichloroethane'
1,2-Dibromoethane (EDB)
Tetrachloroethene
Chlorobenzene
Ethylbenzene
Date: 05/08/01
Date Collected: 04/26/01 11:00
Date Received: 04/26/01 15:20
Analyst CAS# Ftnote Limit
Method: TO-14 Source
Prep
Method:
TO-14 Source
ND
ppmv
0.13
05/04/01
15:03
RGY
75-71-8 1
ND
ppmv
0.13
05/04/01
15:03
RGY
74-87-3
ND
ppmv
0.13
05/04/01
15:03
RGY
76-14-2
ND
ppmv
0.13
05/04/01
15:03
RGY
75-01-4
ND
ppmv
0.13
05/04/01
15:03
RGY
74-83-9
ND
ppmv
0.13
05/04/01
15:03
RGY
75-00-3
ND
ppmv
0.13
05/04/01
15:03
RGY
75-69-4
ND
ppmv
0.13
05/04/01
15:03
RGY
75-35-4
ND
ppmv
0.13
05/04/01
15:03
RGY
76-13-1
ND
ppmv
0.13
05/04/01
15:03
RGY
75-09-2
ND
ppmv
0.13
05/04/01
15:03
RGY
75-34-3
1.2
ppmv
0.13
05/04/01
15:03
RGY
156-59-2
ND
ppmv
0.13
05/04/01
15:03
RGY
67-66-3
ND
ppmv
0.13
05/04/01
15:03
RGY
71-55-6
ND
ppmv
0.13
05/04/01
15:03
RGY
107-06-2
ND
ppmv
0.13
05/04/01
15:03
RGY
71-43-2
ND
ppmv
0.13
05/04/01
15:03
RGY
56-23-5
ND
ppmv
0.13
05/04/01
15:03
RGY
78-87-5
0.68
ppmv
0.13
05/04/01
15:03
RGY
79-01-6
ND
ppmv
0.13
05/04/01
15:03
RGY
10061-01-5
ND
ppmv
0.13
05/04/01
15:03
RGY
10061-02-6
0.20
ppmv
0.13
05/04/01
15:03
RGY
108-88-3
ND
ppmv
0.13
05/04/01
15:03
RGY
79-00-5
ND
ppmv
0.13
05/04/01
15:03
RGY
106-93-4
20.
ppmv
2.7
05/04/01
15:03
RGY
127-18-4
ND
ppmv
0.13
05/04/01
15:03
RGY
108-90-7
ND
ppmv
0.13
05/04/01
15:03
RGY
100-41-4
REPORT OF LABORATORY ANALYSIS
This report shall'not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

(i
ii
aceAnalytical
Lab Sample fic: 92/-583340
Client Sample ID: ASP-2 '10
Parameters
m&p-Xylene
o-Xylene
Styrene
1,1,2,2-Tetrachloroethane
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2,4-Trichlorobenzene
Hexachloro-1,3-butadiene
THC as Gas
Lab Sample No: 921583399
Client Sample ID: ASP-3 #59
s
Parameters
Lab Project Number: 1044095
Client Project ID: 9222475 IT
Project Sample
Number: 1044095-001
Date Collected: 04/26/01 11:00
Matrix: Air
Date Received: 04/26/01 15:20
Results
Units
PRL
Analyzed
Analyst CAS' Ftnote Limit
ND
ppmv
0.13
05/04/01
15:03
RGY
7816-60-0
ND
ppmv
0-3
05/04/01
15:03
RGY
95-47-6
ND
ppmv
0.13
05/04/01
15:03
RGY
100-42-5
ND
ppmv
0.13
05/04/01
15:03
RGY
79-34-5
ND
ppmv
0.13
05/04/01
15:03
RGY
108-67-8 -
ND
ppmv
0.13
05/04/01
15:03
RGY
95-63-6
ND
ppmv
0.13
05/04/01
15:03
RGY
541-73-1
ND
ppmv
0.13
05/04/01
15:03
RGY
106-46-7
ppmv
u._
05/04/6=
15:03
RGY
95-50-1
ND
ppmv
0.13
05/04/01
15:03
RGY
120-82-1
ND
ppmv
0.13
05/04/01
15:03
RGY
87-68-3
26.
ppmv
1.3
05/04/01
15:03
RGY
Project Sample Number: 1044095-002 Date Collected: 04/26/01 11:15
Matrix: Air Date Received: 04/26/01 15:20
Results Units PRL- Analyzed Analyst CAS„ Ftnote Limit
Air
I
GC/MS VOCs, in Air
Method: TO-14
Ambient Air
Dichlorodifluoromethane
0.83
ppbv
0.67
Chloromethane
ND
ppbv
0.64
Dichlorotetrafluoroethane
ND
ppbv
0.76
Vinyl chloride
ND
ppbv
0.67
Sromomethane
i
ND
ppbv
0.67
I Chloroethane
ND
ppbv
0.67
Trichlorofluoromethane
ND
ppbv
0.70
1,1-Dichloroethene
ND
ppbv
0.64
1,1,2-Trichlorotrifluoroethane
ND
ppbv
0.71
Methylene chloride
2.2
ppbv
0.67
1,1-Dichloroethane
ND
ppbv
0.64
cis-1,2-Dichloroethene
ND
ppbv
0.64
Chloroform
ND
ppbv
0.64
1,1,1-Trichloroethane
ND
ppbv
0.58
1,2-Dichloroethane
ND
ppbv
0.54
Date: 05/08/01
Prep Method: TO-14 Ambient Air
05/08/01 01:08 RGY 75-71-8 2
05/08/01 01:08 RGY 74-87-3
05/08/01 01:08 RGY 76-14-2
05/08/01 01:08 RGY 75-01-4
05/08/01 01:08 RGY 74-83-9
05/08/01 01:08 RGY 75-00-3
05/08/01 01:08 RGY 75-69-4
05/08/01 01:08 RGY 75-35-4
05/08/01 01:08 RGY 76-13-1
05/08/01 01:08 RGY 75-09-2
05/08/01 01:08 RGY 75-34-3
05/08/01 01:08 RGY 156-59-2
05/08/01 01:08 RGY 67-66-3
05/08/01 01:08 RGY 71-55-6
05/08/01 01:08 RGY 107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2

i
i I
_J
:..
aceAnalytical
I
Lab Project Number:
1044095
Client Project
ID:
9222475 IT
Lab Sample No: 921583399
Project Sample
Number: 1044095-002
Date Collected: 04/26/01 11:15
Client Sample ID: ASP-3 #59
Matrix: Air
Date Received: 04/26/01 15:20
Parameters
Results
Units
PRL
Analyzed
Analyst CAS;# Ftnote Limit
ppbv
0.58
05/08/01
01:08
RGY
71-43-2
Benzene
ND
Carbon tetrachloride
ND
ppbv
0.56
05/08/01
01:08
RGY
56-23-5
1,2-Dichlorcpropane
ND
ppbv
0.50
05/08/01
01:08
RGY
78-87-5
Trichloroethene
ND
ppbv
0.55
05/08/01
01:08
RGY
79-01-6
cis-1,3-Dichloropropene
ND
ppbv
0.64
05/08/01
01:08
RGY
10061-01-5
trans-1,3-Dichloropropene
ND
ppbv
0.67
05/08/01
01:08
RGY
10061-02-6
Toluene
1.2
ppbv
0.64
05/08/01
01:08
RGY
108-88-3
1,1,2-Trichloroethane
ND
ppbv
0.59
05/08/01
01:08
RGY
_ 79-00-5
1,2-Dibromoethane (EDB)
ND
ppbv
0.58
05/08/01
01:08
RGY
106-93-4
Tetrachloroethene
5.3
ppbv
0.64
05/08/01
01:08
RGY
127-18-4
Chlorobenzene
ND
ppbv
0.56
05/08/01
01:08
RGY
108-90-7
Ethylbenzene
ND
ppbv
0.56
05/08/01
01:08
RGY
100-41-4
m&p-Xylene
ND
ppbv
0.54
05/08/01
01:08
RGY
7816-60-0
o-Xylene
ND
ppbv
0.51
05/08/01
01:08
RGY
95-47-6
Styrene
ND
ppbv
0.54
05/08/01
01:08
RGY
100-42-5
1,1,2,2-Tetrachloroethane
ND
ppbv
0.51
05/08/01
01:08
RGY
79-34-5
1,3,5-Trimethylbenzene
ND
ppbv
0.64
05/08/01
01:08
RGY
108-67-8
1,2,4-Trimethylbenzene
ND
ppbv
0.64
05/08/01
01:08
RGY
95-63-6
1,3-Dichlorobenzene
ND
ppbv
0.40
05/08/01
01:08
RGY
541-73-1
1,4-Dichlorobenzene
ND
ppbv
0.40
05/08/01
01:08
RGY
106-46-7
1,2-Dichlorobenzene
ND
ppbv
0.64
05/08/01
01:08
RGY
95-50-1
1,2,4-Trichlorobenzene
ND
ppbv
0.28
05/08/01
01:08
RGY
120-82-1
Hexachloro-1,3-butadiene
ND
ppbv
0.17
05/08/01
01:08
RGY
87-68-3
THC as Gas
70.
ppbv
27.
05/08/01
01:08
RGY
Date: 05/08/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 3

I c t _-al _IL —I _ _ 1H1_ _ or _ _Jb _ - U ti _ _ ►tt���(;�_ _ cei, stAV
the Right ('lremr....,,; 771E Rig {tl Sohrtiuir'
w The Chain-oi lody Is a LEGAL DOCUMENT. All relevant fields must be completed accura►
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1equired Client Information: Section A
Required Client Information:
Section B
Page: of /
To Be Completed by Pace Analytical
and Client Section C
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Report To: ' aw^ Aj '
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Quote Reference: ---
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'TAT:
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P.O.
�N�h!
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Project Name: %� ,
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Project Number:
--
Requested Analysis: r
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Section D Required Client Information: Valid Matr x C e_ -4 _•
MATRIX CODE
1
W°
w
Preservatives
SAMPLE I D
WATER
son
WT
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mm / dd / yy
hh: in a/p
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Received on ICE: Y /
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Sealed Cooler: Y / la
Samples Intact:) / N
Additional Comments:
SAMPLER NAME ANO
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PRINT Name ul SAMPLER:
SIGNATURE of SAMPLER:
DATE Signet: (MM / DO ! Y'(j
SEE REVERSE SIDE FOR INSTRUCTIONS Pace Analytical Sefvices, Inc. Foun l:0001.XLS 12/99
r tRl(;II,JAI

li
-i
ace Analyticaf"
j www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Keith Ogden
Phone: [phone]
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suile 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610341 Project Sample Number: 9222882-001 Date Collected: 05/11/01 13:00
Client Sample ID: WSP-1 Matrix: Water Date Received: 05/11/01 17:10
Parameters
Results
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote
Limit
I GC Volatiles
- Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep.Method:
EPA 601/602
- Dichlorodifluoromethane
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
75-71-8
Chloromethane
NO
ug/l
100
50.0
05/17/01
23:35
PPM
74-87-3
Vinyl chloride
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
75-01-4
Bromomethane
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
74-83-9
Chloroethane
D N
ug/1
50.
50.0
05/17/01
23:35
PPM
75-00-3
Trichlorofluoromethane
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
75-69-4
1,1-Dichloroethene
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
75-35-4
Methylene chloride
ND
ug/l
100
50.0
05/17/01
23:35
PPM
75-09-2
trans-1,2-Dichloroethene
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
156-60-5
1.1-Dichloroethane
NO
ug/l
50.
50.0
05/17/01
23:35'
PPM
75-34-3
Chloroform
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
67-66-3
1.1,1-Trichloroethane
i
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
71-55-6
Carbon tetrachloride
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
56-23-5
1,2-Dichloroethane
ND
ug/1
50.
50.0
05/17/01
23:35
PPM
107-06-2
Trichloroethene
540
u9 /l
50.
50.0
05/17/01
23:35
PPM
79-01-6
j 1.2-Dichloropropane
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
78-87-5
Bromodichloromethane
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
75-27-4
-, cis-1.3-Dichloropropene
ND
ug/1
50.
50.0
05/17/01
23:35
PPM
10061-01-5
trans-1,3-Dichloropropene
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
10061-02-6
- 1.1,2-Trichloroethane
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
79-00-5
Tetrachloroethene
1300
ug/l
50.
50.0
05/17/01
23:35
PPM
127-18-4
Dibromochloromethane
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
124-48-1
-_ Bromoform
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
75-25-2
1,1.2.2-Tetrachloroethane
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
79-34-5
� Methyl-tert-butyl ether
NO
ug/1
50.
50.0
05/17/01
23:35
PPM
1634-04.4
Diisopropyl ether
NO
ug/l
50.
50.0
05/17/01
23:35
PPM
108.20.3
Benzene
ND
ug/l
50.
50.0
05/17/01
23:35
PPM
71-43.2
Date: 05/24/01
_
Page: 1
- -,aboratory Certification IDs
REPORT
OF
LABORATORY ANALYSIS
Laboratory Certification IDs
NC Wastewater 12
KY Drinking Water
90090
NC Drinking Water 37706
This report shall not be reproduced, except
in full,
VA Drinking Water
213
Sc 99006
without
the written
consent of Pace
Analytical Services, Inc.
FL NELAP
E87627

i
An iM
ace al ical
.1�
www.pacelabs.com
--'
I
Lab Sample No: 921610341
Client Sample ID: WSP-1
Parameters
Toluene
Chlorobenzene
Ethylbenzene
- m&p-Xylene
o-Xylene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
�4
L-.
Date: 05/24/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Results
ND
ND
ND
ND
ND
ND
ND
ND
97
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222882
Client
Project
ID: SLS-Greensboro/010305/107535
Project Sample
Number:
9222882.001
Date Collected: 05/11/01 13:00
Matrix:
Water
Date Received: 05/11/01 17:10
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote Limit
ug/1
50.
50.0
05/17/01
23:35
PPM 108-88.3
ug/l
50.
50.0
05/17/01
23:35
PPM 108-90-7
ug/l
50.
50.0
05/17/01
23:35
PPM 100-41-4
ug/l
50.
50.0
05/17/01
23:35
PPM
ug/l
50.
50.0
05/17/01
23:35
PPM 95-47-6
ug/l
50.
50.0
05/17/01
23:35
PPM 541-73-1
ug/l
50.
50.0
05/17/01
23:35
PPM 106-46-7
ug/l
50.
50.0
05/17/01
23:35
PPM 95-50-1
%
1.0
05/17/01
23:35
PPM 625-98.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 2
Laboratory IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i�
Pace Analytical Services, Inc.
ace A ulXical `
9800 Kincey Avenue. Suile 100
Huntersville. NC 28078
Phone: [phone]
www.pacelabs.com
Fax: [phone]
I
Lab Project Number: 9222882
Client
Project
ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610374
Project Sample
Number:
9222882-002
Date Collected: 05/11/01 13:05
Client Sample ID: WSP-2
Matrix:
Water
Date
Received: 05/11/01 17:10
Parameters
Results
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote Limit
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA
601/602
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
05/18/01
00:18
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75.69-4
1,1-Dichloroethene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
05/18/01
00:18
PPM
75-09-2
trans-1,2-Dichloroethene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
156-60-5
1,1-Dichloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-34-3
Chloroform
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
67-66-3
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
56.23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
107-06.2
Trichloroethene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
79-01-6
1,2-Dichloropropane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
78-87-5
-" Bromodichloromethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
10061-02-6
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
79-00-5
Tetrachloroethene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
127-18-4
Dibromochloromethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
124-48-1
j Bromoform
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
79-34-5
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
1634-04-4
j Diisopropyl ether
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
108-20-3
Benzene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
71-43-2
Toluene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
108-88-3
Chlorobenzene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
o-Xylene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
95-47-6
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
541-73-1
1,4-Dichlorobenzene
ND
ug/l
1.0
1.0
05/18/01
00:18
PPM
106-46-7
Date: 05/24/01
Page: 3
Laboratory Certification IDs Laboratory Certification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
- ' NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

�A'ceAnalyficafm
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone., 704.875.9092
Fax: [phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610374 Project Sample Number: 9222882-002 Date Collected: 05/11/01 13:05
Client Sample ID: WSP-2 Matrix: Water Date Received: 05/11/01 17:10
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
1.2-Dichlorobenzene ND ug/l 1.0 1.0 05/18/01 00:18 PPM 95-50-1
1-Chloro-3-fluorobenzene (S) 95 X 1.0 05/18/01 00:18 PPM 625-98-9
0
Date: 05/24/01
I
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification. IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalyticalTM
www.pacelabs.com
Lab Sample No: 921610382
Client Sample ID: WSP-3
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9222882-003 Date Collected: 05/11/01 13:10
Matrix: Water Date Received: 05/11/01 17:10
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Method: EPA
601/602
Prep Method:
EPA
601/602
Dichlorodifluoromethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-71-8
Chloromethane
NO
ug/l
2.0
1.0
05/18/01
01:01
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-01-4
Bromomethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
74-83.9
r Chloroethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-00-3
Trichlorofluoromethane
i
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-69-4
1.1-Dichloroethene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-35-4
Methylene chloride
NO
ug/l
2.0
1.0
05/18/01
01:01
PPM
75-09-2
trans-1.2-Dichloroethene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
156-60-5
_ 1,1-Dichloroethane
ND
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-34-3
Chloroform
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
67-66-3
1.1.1-Trichloroethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
71-55-6
Carbon tetrachloride
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
56.23-5
1,2-Dichloroethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
107.06-2
Trichloroethene
NO
u9 /l
1.0
1.0
05/18/01
01:01
PPM
79-01-6
1,2-Dichloropropane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
78-87-5
Bromodichloromethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-27-4
cis-1.3-Dichloropropene
ND
ug/l
1.0
1.0
05/18/01
01:01
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
05/18/01
01:01
PPM
10061-02-6
1,1,2-Trichloroethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
79-00-5
Tetrachloroethene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
127-18-4
Dibromochloromethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
124-48-1
Bromoform
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
75-25-2
- 1,1,2,2-Tetrachloroethane
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
79-34-5
Methyl-tert-butyl ether
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
1634-04-4
r Diisopropyl ether
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
108-20-3
Benzene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
71-43-2
Toluene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
108-88-3
Chlorobenzene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
108.90-7
Ethylbenzene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
100-41-4
m&p-Xylene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
o-Xylene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
95-47-6
1.3-Dichlorobenzene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
541.73-1
1,4-Dichlorobenzene
NO
ug/l
1.0
1.0
05/18/01
01:01
PPM
106-46-7
Date: 05/24/01
I,
Page: 5
Laboratory Certification IDs
REPORT
OF
LABORATORY
Laboratory Certification IDs
NC Wastewater 12
ANALYSIS
KY Drinking Water 90090
NC Drinking Water 37706
This report shall not be reproduced,
except
in full,
VA Drinking Water 213
Sc 99006
'I
without
the written
consent of Pace
Analytical Services,
Inc.
FL NELAP E87627

1
Pace Analytical Services, Inc.
a cal TM 9800 Kinsey Avenue, Suite 100
ce Anal
�/t Nunlersville, NC28078
j' Phone: [phone]
www.pacelabs.com Fax:[phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610382 Project Sample Number: 9222882-003 Date Collected: 05/11/01 13:10
Client Sample ID: WSP-3 Matrix: Water Date Received: 05/11/01 17:10
Parameters Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
1.2-Dichlorobenzene ND ug/1 1.0 1.0 05/18/O1 01:01 PPM 95-50-1
1-Chloro-3-fluorobenzene (S) 96 X 1.0 05/18/01 01:01 PPM 625-98-9
Date: 05/24/01 Page: 6
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

Lab Project'Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610390 Project Sample Number: 9222882-004 Date Collected: 05/11/01 13:15
Client Sample ID: WSP-4 Matrix: Water Date Received: 05/11/01 17:10
Parameters Results Units PRL Dilution Analyzed Analyst CASn
Metals
Trace ICP Metals
Iron
Lead
Manganese
Date Digested
Wet Chemistry
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
Oil and Grease
- Ion Chromatography
Nitrate -Nitrite (as N)
GC/MS Volatiles
Volatile GC/MS by 624
Vinyl chloride
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
Methyl-tert-butyl ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
1,1,1-Trichloroethane
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
1,2-Dichloropropane
Toluene
_ Date: 06/12/01
Page: 7
Method: EPA 200.7
44. mg/l 0.050
ND mg/l 0.0050
0.66 mg/l 0.0050
Method: EPA 160.2
180 mg/1 10.
Method: EPA 1664
ND mg/l 5.0
Method: EPA 300.0
ND mg/l 0.30
Prep Method: EPA 200.7
1.0 05/16/01 16:56 RWF 7439-89-6
1.0 05/16/01 16:56 RWF 7439-92-1
1.0 05/16/01 16:56 RWF 7439-96-5
05/16/01
Prep Method: EPA 160.2
10.0 05/15/01 CDE
Prep Method: EPA 1664
1.0 05/15/01 BYH
Prep Method: EPA 300.0
1.0 05/10/01 YMH 7727-37-9
Method: EPA 624
Prep Method:
EPA 624
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-01-4
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
75-35-4
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
75-09-2
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
156-60-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
1634-04-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-34-3
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
156-59-2
19.
ug/l
5.0
1.0
05/17/01
16:56
JRS
67-66-3
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
71-55-6
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
107-06-2
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
56-23-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
71-43-2
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
79-01-6
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
78-87-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
108-88-3

Lab Sample No: 921610390
Client Sample ID: WSP-4
Parameters
1,1,2-Trichloroethane
Tetrachloroethene
Ethylbenzene
m&p-Xylene
o-Xylene
Bromoform
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dibromomethane
Naphthalene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
PARAMETER FOOTNOTES
i } 7
ND Not Detected
NC Not Calculable
PRL Pace Reporting Limit
(S) Surrogate
Date: 06/12/01
-rage: 9
Lab Project Number: 9222882
Client Project ID:�SLS-Greensboro/010305/107535
Project
Sample
Number: 9222882-004
Date
Collected: 05/11/01 13:15
Matrix:
Water
Date
Received: 05/11/01
17:10
Results
Units
PRL
Dilution
Analyzed
Analyst
CAS#
ND
ug/1
5.0
1.0
05/17/01
JRS
79-00-5
16:56
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS,
127-18-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
100-41-4
ND
ug/l
10.
1.0
05/17/01
16:56
JRS
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
95-47-6
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
75-25-2
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
79-34-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
541-73-1
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
95-50-1
104
1.0
05/17/01
16:56
JRS
92
1.0
05/17/01
16:56
JRS
2037-26-5
97
%
1.0
05/17/01
16:56
JRS
460-00-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
106-93-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
91-20-3
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
108-67-8
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
95-63-6

�Pa'ceAnalvticaf"
www.pacelabs.com
Lab Sample No: 921610390
Client Sample ID: WSP-4
Parameters
_ Metals
Trace ICP Metals
Iron
Lead
Manganese
Date Digested
-1
i Wet Chemistry
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
} Oil and Grease
Ion Chromatography
Nitrate -Nitrite (as N)
GC/MS Volatiles
Volatile GC/MS by 624
Vinyl chloride
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
Methyl-tert-butyl ether
1.1-Dichloroethane
cis-1.2-Dichloroethene
Chloroform
1.1.1-Trichloroethane
+ 1.2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
1,2-Dichloropropane
Toluene
Date: 05/24/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville. NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9222882-004 Date Collected: 05/11/01 13:15
Matrix: Water Date Received: 05/11/01 17:10
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Method: EPA 200.7 Prep Method: EPA 200.7
44. mg/l 0.050 1.0 05/16/01 16:56 RWF 7439-89-6
ND mg/l 0.0050 1.0 05/16/01 16:56 RWF 7439.92-1
0.66 mg/l 0.0050 1.0 05/16/01 16:56 RWF 7439-96-5
05/16/01
Method: EPA 160.2 Prep Method: EPA 160.2
180 mg/1 10. 10.0 05/15/01 CDE
Method: EPA 1664 Prep Method: EPA 1664
NO mg/1 5.0 1.0 05/15/01 BYH
Method: EPA 300.0 Prep Method: EPA 300.0
ND mg/l 0.30 1.0 05/10/01 YMH 7727-37-9
Method: EPA 624
Prep Method:
EPA
624
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-01-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-35-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-09-2
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
156-60.5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
1634-04-4
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-34.3
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
156-59.2
19.
ug/l
5.0
1.0
05/17/01
16:56
JRS
67-66-3
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
71-55-6
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
107-06-2
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
56.23-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
71-43-2
ND
ug/1
5.0
1.0
05/17/01
16:56
JRS
79-01-6
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
78-87-5
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
108-88.3
Page: 7
REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
KY Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
qcleAn011yfical" Huntersville, NC28078
Phone. [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9222882
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921610390
Project Sample
Number:
9222882-004
Date Collected:
05/11/01 13:15
Client Sample ID: WSP-4
Matrix: Water
Date
Received: 05/11/01 17:10
Parameters
Results
Units
PRL
Dilution Analyzed
Analyst
CAS# Ftnote Limit
1,1.2-Trichloroethane
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
79-00-5
Tetrachloroethene
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
127-18-4
Ethylbenzene
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
100-41.4
m&p-Xylene
ND
ug/l
10.
1.0
05/17/01
16:56
JRS
o-Xylene
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
95.47-6
'Bromoform
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
75-25-2
1,1.2.2-Tetrachloroethane
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
79.34-5
1.3-Dichlorobenzene
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
541-73-1
1.2-Dichlorobenzene
ND
ug/l
5.0
1.0
05/17/01
16:56
JRS
95-50-1
i, Dibromofluoromethane (S)
104
X
1.0
05/17/01
16:56
JRS
Toluene-d8 (S)
92
X
1.0
05/17/01
16:56
JRS
2037-26-5
4-Bromofluorobenzene (S)
97
X
1.0
05/17/01
16:56
JRS
460-00-4
,I
1
i
I
Date: 05/24/01 Page: 8
VLaboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

,mace Analyticaf"
} www.pacelabs.com
PASI Inc. Charlotte
— 9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
Attn: Project Management
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
fax.• 828.254.4618
Lab Project Number: 9320409
Client Project ID: IT - 9222882
Lab Sample No: 921610390 Project Sample Number: 9320409-001 Date Collected: 05/11/01 13:15
Client Sample ID: WSP-4 Matrix: Water Date Received: 05/11/01 17:10
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
,Wet Chemistry
Total Kjeldahl Nitrogen Method: EPA 351.2 Prep Method: EPA 351.2
Nitrogen, Kjeldahl, Total 5.2 mg/l 0.10 05/22/01 JDA
Date: 05/23/01 Page: 1
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
-i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IN -
TN Drinking Water 02980
SC Environmental 99030

ace Analytical...
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Lab Sample No: 921610416
Client Sample ID: ASP-2 (#104)
Parameters Results
Air
GC/MS VOCs, in Air
Vinyl chloride
Bromomethane
Methylene chloride
cis-1,2-Dichloroethene
Chloroform
Benzene
Carbon tetrachloride
Trichloroethene
Tetrachloroethene
Date: 05/24/01
Lab Project Number: 1044682
Client Project ID: 9222882-IT
Project Sample Number: 1044682-002 Date Collected: 05/11/01 13:15
Matrix: Air Date Received: 05/11/01 17:10
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: TO-14 Source
Prep
Method:
TO-14 Source
ND
ppmv
0.13
05/23/01
08:48
RGY
75-01-4
ND
ppmv
0.13
05/23/01
08:48
RGY
74-83-9
ND
ppmv
0.13
05/23/01
08:48
RGY
75-09-2
1.0
ppmv
0.13
05/23/01
08:48
RGY
156-59-2 1
ND
ppmv
0.13
05/23/01
08:48
RGY
67-66-3
ND
ppmv
0.13
05/23/01
08:48
RGY
71-43-2
ND
ppmv
0.13
05/23/01
08:48
RGY
56-23-5
0.50
ppmv
0.13
05/23/01
08:48
RGY
79-01-6
46.
ppmv
5.4
05/23/01
08:48
RGY
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

aceri, icilyticaf
www.odcalabs.com
�. !A -IF �JS - U1 , . fin"., :icy... ie.-,—_st ct _. nt
The Chain-ut Jody is a LEGAL DOCUMENT. All relevant fields must be completed accurat
Ranuirad Client Inhxmatinrt ; Section B t � i I ` I I t
Report To:
�.• a. [__ .....
lequired Client iuluunatiun:
Section A
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Page.
Of
To Be Completed by
Quote Reference:
Pace Analytical and
Client Section C
,umpany
Copy To:
t r�� r s•' ' '
Client Information Check quote/contract):
Adress
_
! •":•
Invoice To:
Requested Due D e:
'TAT:
Project Manager:
/'
P.O.
• Turn around time less than 14 days subject to
Project tY:
+ .�
1.(�k R:v:G•.i
laboratory and contractual obligations and may result in a
Rush Turnaround Surcharge.
Project Narne: _ „ r
Profile 8:
Turn Around Time (TAT) in
calendar days.
rhona
Fax
Project Number, +
Requested Analysis:
Section D Required Client Information:
Valid Matrix Cudes 4— _-
MATRIX CODE
p
w
o
F
Preservatives
SAMPLE I D
WATER
oar
WT
o�
W
o
W V
o f
W O
P
at
One character per box.
IL
WIPE
AIR
WP
AR
X
Fr
O
U
O
O
ro
H
N
O`
=
O
O
uj
t
f
%/
t1J
(A—Z, 0-9 / .—)
TISSUE
TS
¢
U
r)
z
U
z
/
/
Remarks / Lab ID
Sample IDS MUST BE UNIQUE
oTtiER __-
_o?
2
mm / dd / yy
hh: mm a/p
as
x
x
x
z
i
;
/�
it
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k, l+
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'� `"i ..; -
-
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,
r
' /
�
,
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t r i .
jt
ACCEPTED
BY /AFFILIATION
Additional Comments:
f
7--
Pace Project No.:
SAMPLE
CONDIIION
Temp: __ °C
Received on Ice:,, Y /'N
Sealed Cooler:
YIN 1
Samples Intact: Y / N JAI _ _

i
I
aceAnalytical'M,
www.pacelabs.com
I
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Keith Ogden
Phone: [phone] x224
Lab Sample No: 92164.1726
Client Sample ID: WSP-4
Parameters
Metals
Trace ICP Metals
Iron
Lead
Manganese
Date Digested
Wet Chemistry,
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
Oil and Grease
Ion Chromatography
Nitrate -Nitrite (as N)
GC/MS Volatiles
Volatile GC/MS by 624
Vinyl chloride
1,1-Dichloroethene
Methylene chloride
trans-1.2-Dichloroethene
- Methyl-tert-butyl ether
1.1-Dichloroethane
cis-1,2-Dichloroethene
_ Chloroform
Date: 06/14/01
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax:[phone]
Lab Project Number: 9223345
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223345-001 Date Collected: 05/31/01 11:00
Matrix: Water Date Received: 06/01/01 14:10
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Method: EPA 200.7 Prep Method: EPA 200.7
3.4 mg/l 0.050 1.0 06/05/01 18:47 RWF 7439-89-6
0.017 mg/l 0.0030 1.0 06/05/01 18:47 RWF 7439-92.1
0.38 mg/l 0.0050 1.0 06/05/01 18:47 RWF 7439-96-5
06/05/01
Method: EPA 160.2
20. mg/l
Method: EPA 1664
NO mg/l
Method: EPA 300.0
NO mg/l
Method: EPA 624
NO
ug/l
NO
ug/l
NO
ug/l
NO
ug/l
ND
ug/l
NO
ug/l
NO
ug/l
9.8
ug/l
1.0
5.0
0.30
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5:0
Prep Method: EPA 160.2
1.0 06/08/01 CDE
Prep Method: EPA 1664
1.0 06/05/01 BYH
Prep Method: EPA 300.0
1.0 06/02/01 YMH 7727-37-9
Prep Method: EPA 624
1.0 06/08/01 02:16 RPJ 75-01-4
1.0 06/08/01 02:16 RPJ 75-35-4
1.0 06/08/01 02:16 RPJ 75-09-2
1.0 06/08/01 02:16 RPJ 156-60-5
1.0 06/08/01 02:16 RPJ 1634-04-4
1.0 06/08/01 02:16 RPJ 75-34-3
1.0 06/08/01 02:16 RPJ 156-59-2
1.0 06/08/01 02:16 RPJ 67-66-3
Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

' ace Analytical m
_ www.pacelabs.com
Lab Sample No: 921641726
Client Sample ID: WSP-4
Parameters
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
far.• 704.875.9091
Lab Project Number: 9223345
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223345-001
Matrix: Water
Results Units
1.1.1-Trichloroethane
ND
ug/1
1.2-Dichloroethane
ND
ug/l
Carbon tetrachloride
ND
ug/l
Benzene
ND
ug/l
Trichloroethene
ND
ug/l
1.2-Dichloropropane
ND
ug/l
Toluene
ND
ug/l
1.1.2-Trichloroethane
ND
ug/l
Tetrachloroethene
ND
ug/l
Ethylbenzene
ND
ug/l
m&p-Xylene
ND
ug/l
o-Xylene
ND
ug/l
Bromoform
ND
ug/l
1.1.2.2-Tetrachloroethane
ND
ug/1
1.3-Dichlorobenzene
ND
ug/l
1.2-Dichlorobenzene
ND
ug/l
Dibromofluoromethane (S)
100
X
Toluene-d8 (S)
90
X
4-Bromofluorobenzene (S)
96.
X
Naphthalene
ND
ug/l
1.2-Dibromoethane (EDB)
ND
ug/l
1.3.5-Trimethylbenzene
ND
ug/l
1.2.4-Trimethylbenzene
ND
ug/l
Date: 06/14/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Date Collected: 05/31/01 11:00
Date Received: 06/01/01 14:10
PRL
Dilution Analyzed
Analyst CAS#
5.0
1.0
06/08/01
02:16
RPJ
71-55-6
5.0
1.0
06/08/01
02:16
RPJ
107-06-2
5.0
1.0
06/08/01
02:16
RPJ
56.23-5
5.0
1.0
06/08/01
02:16
RPJ
71-43-2
5.0
1.0
06/08/01
02:16
RPJ
79.01-6
5.0
1.0
06/08/01
02:16
RPJ
78-87-5
5.0
1.0
06/08/01
02:16
RPJ
108-88-3
5.0
1.0
06/08/01
02:16
RPJ
79-00-5
5.0
1.0
06/08/01
02:16
RPJ
127-18-4
5.0
1.0
06/08/01
02:16
RPJ
100-41-4
10.
1.0
06/08/01
02:16
RPJ
5.0
1.0
06/08/01
02:16
RPJ
95-47-6
5.0
1.0
06/08/01
02:16
RPJ
75-25-2
5.0
1.0
06/08/01
02:16
RPJ
79-34-5
5.0
1.0
06/08/01
02:16
RPJ
541-73-1
5.0
1.0
06/08/01
02:16
RPJ
95-50-1
1.0
06/08/01
02:16
RPJ
1.0
06/08/01
02:16
RPJ
2037-26-5
1.0
06/08/01
02:16
RPJ
460-00-4
5.0
1.0
06/08/01
02:16
RPJ
91-20-3
5.0
1.0
06/08/01
02:16
RPJ
106-93-4
5.0
1.0
06/08/01
02:16
RPJ
108-67.8
5.0
1.0
06/08/01
02:16
RPJ
95-63-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Ftnote Limit
Page: 2
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

010
PacetiliaVical
www.pacelabs. coin
Required Client Information: Section A
Comps'y Add es
<'y 10 'At7 er�/0<y_6
t -d /`tG d7
_ %LNG ? • I W )d-eg
Section D Required client Information:
SAMPLE ID
g One character per box.
I-_ Sample
0-9 / .-)
Sample IDs MUST BE UNIQUE
Additional Comments:
-.1A -)t JS D' �n�., tic. Aet. ,.:st _mac
The Chain -or —stody is a LEGAL DOCUMENT. All relevant fields must be completed accuratt,,.
fired Client Information: Section B 5 8.19 7 "'
rt Te/t- (�G, G ��� � Page: Of / To Be G mpleted by Pace Analytical and Client Section C
re:
"/ t/ Client information(Check uote/contract
e To: Requested Due ate: 'TAT: Project t+ nrager. -- - --
(��� f *Turn ar nd If s less than 14 days subject to
laboratory and contractual obligations and may result In a
:t Ume °_ r � y 1 Rush Turnaround Surcharge. Profile M: — d
-1 , A vJ(J� Turn Around Time (TAT) In calendar days.
a Number. -71 � / Requesr•dlAnalysts:
Valid Codes w
MATRIX IX w Preservatives
CODE
WATER WT W W F U ff){
SOIL SL 0 Q V w /� i
OIL OL O F d [Lit
WIPE WP X O O w o 'tf
AIR AR U U 0 = O a . ((�� /
TISSUE TS < U c r H Z V Oro N d �` ~ /
OTHER Or _ mm / dd l -�36 � yy hh: mm a/p ap 7) x x x z z Remarks /Lab IC.
MEN
Project No.: — - —
SAMPLE CONDITION
_—°C Received on Ice: Y, N Sealed Cooler: Y N \ Samples Intact

aceAnalytical'"
www.pacelabs.com
IT Corporation
- 2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Charles Bertz
Phone: [phone] x236
Lab Sample No: 921664074
Client Sample ID: WSP-1
Parameters
GC Volatiles
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax:[phone]
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223723-001 Date Collected: 06/14/01 16:00
Matrix: Water Date Received: 06/15/01 10:00
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Halogen. & Aromatic Vol. Orgs.
Method: EPA
601/602
Prep Method:
EPA 601/602
Dichlorodifluoromethane
ND
ug/1
100
100
06/28/01
KST
75-71-8
Chloromethane
ND
ug/l
200
100
06/28/01
KST
74-87-3
_- Vinyl chloride
ND
ug/1
100
100
06/28/01
KST
75-01-4
Bromomethane
ND
ug/1
100
100
06/28/01
KST
74-83-9
Chloroethane
ND
ug/l
100
100
06/28/01
KST
75-00-3
Trichlorofluoromethane
ND
ug/l
100
100
06/28/01
KST
75-69-4
1.1-Dichloroethene
ND
ug/l
100
100
06/28/01
KST
75-35-4
Methylene chloride
ND
ug/l
200
100
06/28/01
KST
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
100
100
06/28/01
KST
156-60-5
' 1,1-Dichloroethane
ND
ug/l
100
100
06/28/01
KST
75-34-3
Chloroform
ND
ug/l
100
100
06/28/01
KST
67-66-3
1 1.1,1-Trichloroethane
ND
ug/l
100
100
06/28/01
KST
71-55-6
Carbon tetrachloride
ND
ug/l
100
100
06/28/01
KST
56-23-5
1.2-Dichloroethane
ND
ug/l
100
100
06/28/01
KST
107-06-2
Trichloroethene
3300
ug/l
100
100
06/28/01
KST
79-01-6
1,2-Dichloropropane
ND
ug/l
100
100
06/28/01
KST
78-87-5
Bromodichloromethane
ND
ug/l
100
100
06/28/01
KST
75-27-4
cis-1.3-Dichloropropene
ND
ug/l
100
100
06/28/01
KST
10061-01.5
trans-1,3-Dichloropropene
ND
ug/l
100
100
06/28/01
KST
10061-02-6
1,1.2-Trichloroethane
ND
ug/l
100
100
06/28/01
KST
79-00-5
Tetrachloroethene
5000
ug/l
100
100
06/28/01
KST
127-18-4
Dibromochloromethane
ND
ug/1
100
100
06/28/01
KST
124-48-1
Bromoform
ND
ug/1
100
100
06/28/01
KST
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
100
100
06/28/01
KST
79-34-5
- Methyl-tert-butyl ether
ND
ug/l
100
100
06/28/01
KST
1634-04-4
Diisopropyl ether
ND
ug/l
100
100
06/28/01
KST
108-20-3
Benzene
ND
ug/l
100
100
06/28/01
KST
71-43-2
Date: 07/03/01
Page: 1
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Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

i
ace Analytical m
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Lab Sample No: 921664074
Client Sample ID: WSP-1
Parameters
Results
Toluene
ND
Chlorobenzene
ND
Ethylbenzene
ND
m&p-Xylene
ND
o-Xylene
ND
1.3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
1.2-Dichlorobenzene
ND
1-Chloro-3-fluorobenzene (S)
110
Date: 07/03/01
Laboratory Certification IDs
'NC Wastewater 12
-NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]—
Fax: [phone]
Lab Project Number: 9223723
Client
Project ID:
SLS-Greensboro/010305/107535
Project Sample
Number:
9223723.001
Date Collected: 06/14/01 16:00
Matrix:
Water
Date Received: 06/15/01 10:00
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote Limit
ug/l
100
100
06/28/01
KST 108-88-3
ug/l
100
100
06/28/01
KST 108-90-7
ug/l
100
100
06/28/01
KST 100-41-4
ug/l
100
100
06/28/01
KST
ug/l
100
100
06/28/01
KST 95-47.6
ug/l
100
100
06/28/01
KST 541-73-1
ug/l
100
100
06/28/01
KST 106-46-7
ug/l
100
100
06/28/01
KST 95-50.1
X
1.0
06/28/01
KST 625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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ace Analytical r"
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Lab Sample No: 921664082
Client Sample ID: WSP-2
Parameters
GC Volatiles
Halogen. & Aromatic Vol. Orgs
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1.1-Dichloroethene
Methylene chloride
trans-1.2-Dichloroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1.2-Dichloroethane
Trichloroethene
1.2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
trans-1.3-Dichloropropene
1.1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1.1.2,2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
m&p-Xylene
-- o-Xylene
1,3-Dichlorobenzene
1.4-Dichlorobenzene
Date: 07/03/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Far 704.875.9091
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223723-002 Date Collected: 06/14/01 16:00
Matrix: Water Date Received: 06/15/01 10:00
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Method: EPA 601/602
Prep Method:
EPA
601/602
ND
ug/l
1.0
1.0
06/26/01
KST
75-71-8
ND
ug/l
2.0
1.0
06/26/01
KST
74.87-3
ND
ug/l
1.0
1.0
06/26/01
KST
75.01-4
ND
ug/l
1.0
1.0
06/26/01
KST
74-83-9
ND
ug/l
1.0
1.0
06/26/01
KST
75-00-3
ND
ug/1
1.0
1.0
06/26/01
KST
75-69-4
ND
ug/l
1.0
1.0
06/26/01
KST
75-35-4
ND
ug/l
2.0
1.0
06/26/01
KST
75-09-2
ND
ug/l
1.0
1.0
06/26/01
KST
156-60-5
ND
ug/l
1.0
1.0
06/26/01
KST
75.34-3
ND
ug/l
1.0
1.0
06/26/01
KST
67-66-3
ND
ug/1
1.0
1.0
06/26/01
KST
71-55.6
ND
ug/l
1.0
1.0
06/26/01
KST
56-23.5
ND
ug/l
1.0
1.0
06/26/01
KST
107-06-2
22.
ug/l
1.0
1.0
06/26/01
KST
79-01-6
ND
ug/l
1.0
1.0
06/26/01
KST
78-87-5
ND
ug/l
1.0
1.0
06/26/01
KST
75-27-4
ND
ug/l
1.0
1.0
06/26/01
KST
10061-01-5
ND
ug/l
1.0
1.0
06/26/01
KST
10061-02-6
ND
ug/1
1.0
1.0
06/26/01
KST
79-00-5
18.
ug/l
1.0
1.0
06/26/01
KST
127-18-4
ND
ug/l
1.0
1.0
06/26/01
KST
124-48-1
ND
ug/l
1.0
1.0
06/26/01
KST
75.25-2
ND
ug/l
1.0
1.0
06/26/01
KST
79.34-5
ND
ug/l
1.0
1.0
06/26/01
KST
1634-04-4
ND
ug/l
1.0
1.0
06/26/01
KST
108-20-3
ND
ug/l
1.0
1.0
06/26/01
KST
71.43-2
ND
ug/l
1.0
1.0
06/26/01
KST
108-88-3
ND
ug/l
1.0
1.0
06/26/01
KST
108-90-7
ND
ug/l
1.0
1.0
06/26/01
KST
100-41.4
ND
ug/l
1.0
1.0
06/26/01
KST
ND
ug/l
1.0
1.0
06/26/01
KST
95-47-6
ND
ug/l
1.0
1.0
06/26/01
KST
541-73-1
ND
ug/l
1.0
1.0
06/26/01
KST
106-46-7
Page: 3
REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
KY Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey /lvenue, Suite 100
aceAI ln alyfical T A Huntersville, NC 28078
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number:
Client Project ID:
9223723
SLS-Greensboro/010305/107535
Lab Sample No: 921664082
Project Sample
Number: 9223723-002
Date Collected: 06/14/01 16:00
Client Sample ID: WSP-2
Matrix: Water
Date Received: 06/15/01 10:00
Parameters Results
Units
PRL Dilution Analyzed
Analyst CAS# Ftnote Limit
1,2-Dichlorobenzene ND
ug/l
1.0 1.0 06/26/01
KST 95-50-1
1-Chloro-3-fluorobenzene (S) 96
X
1.0 06/26/01
KST 625-98-9
Date: 07/03/01 Page: 4
.aboratory Certification IDS REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
'JC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

ace Analytical "'
www.pacelabs.com
Lab Sample No: 921664090
Client Sample ID: WSP-3
Parameters
GC Volatiles
Pace Analytical Services, Inc.
9800 Kincey A venue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223723.003 Date Collected: 06/14/01 16:00
Matrix: Water Date Received: 06/15/01 10:00
Results Units PRL
Dilution Analyzed Analyst CAS# Ftnote Limit
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
Dichlorodifluoromethane
ND
uo/l
1.0
1.0
06/26/01
KST
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
06/26/01
KST
74.87-3
Vinyl chloride
ND
ug/l
1.0
1.0
06/26/01
KST
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
06/26/01
KST
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
75-00-3
Trichlorofluoromethane
ND
ug/1
1.0
1.0
06/26/01
KST
75-69-4
1,1-Dichloroethene
ND
ug/l
1.0
1.0
06/26/01
KST
75-35.4
Methylene chloride
ND
ug/l
2.0
1.0
06/26/01
KST
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
1.0
1.0
06/26/01
KST
156-60-5
1,1-Dichloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
75-34-3
Chloroform
ND
ug/l
1.0
1.0
06/26/01
KST
67-66-3
1.1.1-Trichloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
06/26/01
KST
56-23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
107-06-2
Trichloroethene
6.0
ug/l
1.0
1.0
06/26/01
KST
79-01-6
1.2-Dichloropropane
ND
ug/1
1.0
1.0
06/26/01
KST
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
06/26/01
KST
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
06/26/01
KST
10061-01-5
trans-1.3-Dichloropropene
ND
ug/1
1.0
1.0
06/26/01
KST
10061 02 6
1,1.2-Trichloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
79-00-5
Tetrachloroethene
5.3
ug/l
1.0
1.0
06/26/01
KST
127-18-4
- Dibromochloromethane
ND.
ug/1
1.0
1.0
06/26/01
KST
124-48-1
Bromoform
ND
ug/l
1.0
1.0
06/26/01
KST
75-25-2
1.1,2.2-Tetrachloroethane
ND
ug/l
1.0
1.0
06/26/01
KST
79-34-5
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
06/26/01 _
KST
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
06/26/01
KST
108-20-3
Benzene
ND
ug/l
1.0
1.0
06/26/01
KST
71.43-2
Toluene
ND
ug/l
1.0
1.0
06/26/01
KST
108-88.3
Chlorobenzene
ND
ug/l
1.0
1.0
06/26/01
KST
108 90 7
Ethylbenzene
ND
ug/l
1.0
1.0
06/26/01
KST
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
06/26/01
KST
o Xylene
ND
ug/l
1.0
1.0
06/26/01
KST
95-47-6
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
06/26/01
KST
541-73-1
-- 1.4-Dichlorobenzene
ND
ug/l
1.0
1.0
06/26/01
KST
106.46-7
Date: 07/03/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 5
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

III r
aceAnalyticalM
www.pacelabs.com
Lab Sample No: 921664090
Client Sample ID: WSP-3
Parameters
1.2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
Date: 07/03/01
'Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
\1
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223723-003 Date Collected: 06/14/01 16:00
Matrix: Water Date Received: 06/15/01 10:00
Results Units PRL Dilution Analyzed Analyst CAS# 'Ftnote Limit
ND ug/l 1.0 1.0 06/26/01 KST 95-50-1
96 X 1.0 06/26/01 KST 625-98-9
REPORT OF LABORATORY ANALYSIS
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aceAnalyicaf7
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i
Lab Sample No: 921664116
Client Sample ID: WSP-4
Parameters
Metals
Trace ICP Metals
Iron
Lead
Manganese
Date Digested
` Wet Chemistry
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
Oil and Grease
Ion Chromatography
Nitrate -Nitrite (as N)
GC/MS Volatiles
Volatile GC/MS by 624
Vinyl chloride
1.1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
Methyl-tert-butyl ether
1.1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
1,.1,1-Trichloroethane
1,2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
1,2-Dichloropropane
Toluene
Date: 07/03/01
Laboratory Certification IDs
1 iNC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: 704, 875.9092
Fax- 704.875.9091
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9223723-004 Date Collected: 06/14/01 16:00
Matrix: Water Date Received: 06/15/01 10:00
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Method: EPA 200.7 Prep Method: EPA 200.7
6.3 mg/l 0.050 1.0 06/21/01 21:57 RWF 7439-89-6
0.067 mg/l 0.0030 1.0 06/21/01 21:57 RWF 7439-92.1
0.18 mg/l 0.0050 1.0 06/21/01 21:57 RWF 7439-96-5
06/18/01
Method: EPA 160.2 Prep Method: EPA 160.2
41. mg/l 2.0 2.0 06/21/01 CDE
Method: EPA 1664 Prep Method: EPA 1664
NO mg/1 5.0 1.0 06/19/01 BYH
Method: EPA 300.0 Prep'Method: EPA 300.0
0.59 mg/l 0.30 1.0 06/18/01 DJR 7727-37-9
Method: EPA 624
Prep Method:
EPA 624
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
75.01-4
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
75-35-4
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
75-09-2
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
156.60-5
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
1634-04-4
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
75-34-3
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
156-59-2
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
67-66-3
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
71-55-6
NO
ug/l
5.0
1.0.
06/21/01
14:13
RPJ
107-06-2
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
56-23-5
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
71-43-2
NO
ug/l
5.0
1.0
06/21/01
14:13
RPJ
79-01.6
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
78.87-5
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 7
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical'N
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9223723
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921664116
Project Sample
Number:
9223723-004
Date Collected: 06/14/01 16:00
Client Sample ID: WSP 4
Matrix:
Water
Date Received: 06/15/01 10:00
- Parameters
Results
Units
PRL
Dilution Analyzed
Analyst CAS# Ftnote Limit
1.1.2-Trichloroethane
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
79-00-5
Tetrachloroethene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
127-18-4
Ethylbenzene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
100-41-4
m&p-Xylene
ND
ug/l
10.
1.0
06/21/01
14:13
RPJ
o-Xylene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
95-47.6
Bromoform
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
75-25-2
1.1.2.2-Tetrachloroethane
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
79-34-5
1.3-Dichlorobenzene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
541-73-1
1.2-Dichlorobenzene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
95-50-1
Dibromofluoromethane (S)
106
X
1.0
06/21/01
14:13
RPJ
Toluene-d8 (S)
99
X
1.0
06/21/01
14:13
RPJ
2037-26-5
4-Bromofluorobenzene (S)
85-
X
1.0
06/21/01
14:13
RPJ
460-00-4 1
' Naphthalene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
91-20-3
1,2-Dibromoethane (EDB)
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
106-93-4
1.3.5-Trimethyl.benzene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
108-67-8
1.2.4-Trimethylbenzene
ND
ug/l
5.0
1.0
06/21/01
14:13
RPJ
95-63-6
Date: 07/03/01 Page: 8
Wboratory certification IDs REPORT OF LABORATORY ANALYSIS Laboratory certification IDS
C Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627
i
_i _

i
ace Analytical "'
www.pacelabs.com
PASI Inc. Charlotte
9800 Kincey Ave.
ite 100
ntersville, NC 28078
tn: Project Management
one: [phone]
Lab Project Number: 9321237
Client Project ID: IT-9223723
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax:[phone]
b Sample No: 921664116 Project Sample Number: 9321237-001 Date Collected: 06/14/01 16:00
ient Sample ID: WSP-4 Matrix: Water Date Received: 06/15/01 10:00
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
t Chemistry
Total Kjeldahl Nitrogen
4itrogen, Kjeldahl. Total
Date: 06/25/01
Laboratory Certification ID
i N1C Wastewater 40
—iVC Drinking Water 37712
Method: EPA 351.2 Prep Method: EPA 351.2
ND mg/l 0.10 06/22/01 FDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

aceAnapical
-- WrM paaelaDS.Com
Pace Analytical Services, Ind.
9800 Kincey Avenue
Suite 100
Huntereville, NC 28078
Attn: Client Service
Phone: [phone]
Lab Sample No: 921664124
Client Sample ID: ASP-2 (#161)
Pace Analytical Services, Inc.
1700 Elm Street Suite 200
MinnwpoliA MN 55414
Phone: 612.607,1700
Fax:[phone]
Lab Project Number: 1045798 F
Client Project ID: 9223723 IT
Project Sample Number: 1045798-001 Date Collected: 06/14/01 16:00
Matrix: Air Date Received: 06/15/01 10:00
Air
GC/MS VOCs, in Air
Prep/Method:
TO-14
Source / TO-14
Source
Vinyl chloride
ND
ppmv
0.15
06/23/01
11:29
MTG
75-01-4
Methylene chloride-
ND
ppmv
0.15
06/23/01
11:29
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppmv
0.15
06/23/01
11:29
MTG
156-59-2
Chloroform
ND
ppmv
0.15
06/23/01
11:29
MTG
67-66-3
Benzene
ND
ppmv
0.15
06/23/01
11:29
MTG
71-43-2, 1
Carbon tetrachloride
ND
ppmv
0.15
06/23/01
11:29
MTG
56-23-5
Trichloroethene•
ND
ppmv
0.15
06/23/01
11:29
MTG
79-01-6
Tetrachloroethene
0.86
ppmv
0.15
06/23/01
11:29
MTG
127-18-4
THC as Gas
2.3
ppmv
1.5
06/23/01
11:29
MTG
Lab Sample No: 921664132
Project Sample
Number: 1045798-002
Date Collected: 06/14/01 16:00
Client Sample ID: ASP-3 (#180)
Parameters
Results
Matrix: Air
Date Received: 06/15/01 10:00
Air
Units
Report Limit
Analyzed
CAS No. Ftnote Rev Limit
GC/MS VOCs, in Air
Prep/Method:
TO-14 Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.14 -
06/23/01
12:24
MTG
75-01-4
Methylene chloride
ND
ppmv
0.14
06/23/01
12:24
MTG
75-09-2
cis-1,2-Dichloroethene
0.37
ppmv
0.14
06/23/01
12:24
MTG
156-59-2
Chloroform
ND
ppmv
0.14
06/23/01
12:24
MTG
67-66-3
Benzene
ND
ppmv
0.14
06/23/01
12:24
MTG
71-43-2 1
Carbon tetrachloride
ND
ppmv
0.14
06/23/01
12:24
MTG
56-23-5
Trichloroethene
0.69
ppmv
0.14
06/23/01
12:24
MTG
79-01-6
Tetrachloroethene
96.
ppmv
14.
06/23/01
12:24
MTG
127-18-4
THC as Gas
38.
ppmv
1.4
06/23/01
12:24
MTG
-Date- 06/25/01
1H ACCC
A41 4�1 4,
iefi,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
0

Pa e Analytical -
www nanalahs i,nm
%,dAijim-JF-%,JS _ _ D% , Am;,,ydc,.• .1eL,Nvst a.F..r,cLsza%o111
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
oe.•�Lvar-iie..,;.,r....,,ar;,..,• qw-finn R
lequired Client Information: Section A
Report To:
UC (] r f0/
Page: of
Client Information Check uote/contract
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Quote Reference:
Section C
;ompany �
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Copy To:
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t Turn ound des less than 14 days subject to
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Project #:
J
Project Name�J�t /r` r�.n
iJ
Profile #:
Turn Around Time (TAT) In calendar days.
'Bone
Fax
Project Number:
Requested Analysis:
r
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Section D Required Client Information:
SAMPLE ID
— —
Valid Matrix •odes
MATRIX CODE
WATER WT
solL sL
OIL OL
1
W
g
o
W
W U
Q�
o
W U
gW
~
c
Preservatives
Z
U
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box.
WIPE WP
U
X
O
U
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U
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H
=O
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u
per
(A-Z, 0-9 /.-)
AIR AR
TlssuE TS
¢
a
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U
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U
m
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m
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Sample
IDS MUST BE UNIQUE
O—TF€lL. -_ T
2
mm / dd / y
hh: mm a/p
ax
D
I
x
x
z
z
Remarks
Lab ID
o
-a
Et
r�
_
3
r
r
0
i .k•
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Y
,.
--
_
`'w'l
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SHIPMENT
METHOD
AIRBILL
NO.
ACCEPTED BY AFFILIATION
Additional Comments:
Pace Project No.:
SAMPLE CONDITION
Temp: °C Received
on Ice: `l /
Sealed Cooler: Y / N
Samples Intact. Yt
pH __

i
;acieAnalyficafm
www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Keith Ogden
Phone: [phone] x224
Lab Project Number: 9224662
Client Project ID: SLS-Greensboro/010305/107535
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax.• 704.875.9091
Lab Sample No: 921723847 Project Sample Number: 9224662-001 Date Collected: 07/19/01 15:30
Client Sample ID: WSP-1 Matrix: Water Date Received: 07/20/01 13:45
Parameters
Results
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Prep/Method
Dichlorodifluoromethane
NO
Chloromethane,
NO
Vinyl chloride
NO
Bromomethane
NO
Chloroethane
NO
Trichlorofluoromethane
NO
1.1-Dichloroethene
1.5
Methylene chloride
NO
trans-1.2-Dichloroethene
3.2
1.1-Dichloroethane
NO
Chloroform
3.3
1.1.1-Trichloroethane
NO
Carbon tetrachloride
7.9
1.2-Dichloroethane
2.2
Trichloroethene
1400
1.2-Dichloropropane
11.
Bromodichloromethane
NO
cis-1,3-Dichloropropene
NO
trans-1.3-Dichloropropene
NO
1.1.2-Trichloroethane
NO
Tetrachloroethene
1200
Dibromochloromethane
NO
Bromoform
NO
1.1.2.2-Tetrachloroethane
NO
Methyl-tert-butyl ether
NO
Diisopropyl ether
NO
Benzene
NO
Toluene
NO
Date- 07/31/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Units
Report Limit Dilution Analyzed
CAS No. Ftnote Reg Limit
EPA 601/602
/ EPA 601/602
ug/l
1.0
1.0
07/26/01
KST
75-71-8
ug/l
2.0
1.0
07/26/01
KST
74-87-3
ug/l
1-0
1.0
07/26/01
KST
75-01-4
ug/l
1.0
1.0
07/26/01
KST
74-83-9
ug/l
1.0
1.0
07/26/01
KST
75-00-3
ug/l
1.0
1.0
07/26/01
KST
75-69-4
ug/l
1.0
1.0
07/26/01
KST
75-35-4
ug/l
2.0
1.0
07/26/01
KST
75-09-2
ua/l
1.0
1.0
07/26/01
KST
156-60-5
ug/l
1.0
1.0
07/26/01
KST
75-34-3
ug/1
1.0
1.0
07/26/01
KST
67-66-3
ug/l
1.0
1.0
07/26/01
KST
71-55-6
ug/l
1.0
1.0
07/26/01
KST
56-23-5
ug/l
1.0
1.0
07/26/01
KST
107-06-2
u9/1
50.
50.0
07/26/01
KST
79-01-6
ug/l
1.0
1.0
07/26/01
KST
78-87-5
ug/l
1.0
1.0
07/26/01
KST
75-27-4
ug/l
1.0
1.0
07/26/01
KST
10061-01-5
ug/1
1.0
1.0
07/26/01
KST
10061-02-6
ug/l
1.0
1.0
07/26/01
KST
79-00-5
ug/l
50.
50.0
07/26/01
KST
127-18-4
ug/l
1.0
1.0
07/26/01
KST
124-48-1
ug/l
1.0
1.0
07/26/01
KST
75-25-2
ug/l
1.0
1.0
07/26/01
KST
79-34-5
ug/1
1.0
1.0
07/26/01
KST
1634-04-4'
ug/l
1.0
1.0
07/26/01
KST
108-20-3
ug/l
1.0
1.0
07/26/01
KST
71-43-2
ug/l
1.0
1.0
07/26/01
KST
108-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ACC09
0�
Page: 1
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

;acieAnalyfical'"
www.pacelabs.com
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
—"
Lab Project Number:
Client Project ID:
9224662
SLS-Greensboro/010305/107535
Lab Sample No: 921723847
Project Sample
Number: 9224662-001
Date Collected: 07/19/01 15:30
Client Sample lD: WSP-1
Matrix: Water
Date Received: 07/20/01 13:45
Parameters
Results
Units
Report Limit
Dilution
Analyzed CAS No. Ftnote Rea Limit
ChloroDenzene
NO
ug/l
1.0
1.0
07/26/01
KST 108-90-7
Ethylbenzene
NO
ug/l
1.0
1.0
07/26/01
KST 100-41-4
i__i m&p-Xylene
NO
ug/l
1.0
1.0
07/26/01
KST
o-Xyiene
NO
ug/l
1.0
1.0
07/26/01
KST 95-47-6
1.3-Dichlorobenzene
NO
ug/1
1.0
1.0
07/26/01
KST 541-73-1
1.4-Dichlorobenzene
NO
ug/l
1.0
1.0
07/26/01
KST 106-46-7
1.2-Dichlorobenzene
NO
ug/l
1.0
1.0
07/26/01
KST 95-50-1
1-Chloro-3-fluorobenzene (S)
102
%
1.0
07/26/01
KST 625-98-9
Date. 07/31/01
1
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 12
NC Drinking Water 37706 This report shall not be reproduced, except in full,
Sc 37706 without the written consent of Pace Analytical Services, Inc.
�C[Q
i L
n Nac
Page: 2
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

I ,
I
i;
ace Analytical o
www.pacelabs.com
Lab Project Number: 9224662
Client Project ID: SLS-Greensboro/010305/107535
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, Z 28078
Phone: [phone]
Fax: [phone]
Lab Sample No: 921723854 Project Sample Number: 9224662-002 Date Collected: 07/19/01 15:45
Client Sample ID: WSP-2 Matrix: Water Date Received: 07/20/01 13:45
Parameters
Results
Units
Report Limit Dilution Analyzed
GC Volatiles
Halogen. 8 Aromatic Vol. Orgs.
Prep/Method:
EPA 601/602
/ EPA 601/602
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
07/26/01 K
Chloromethane
NO
ug/l
2.0
1.0
07/26/01 K',
Vinyl chloride
NO
ug/l
1.0
1.0
07/26/01 K',
Bromomethane
NO
ug/l
1.0
1.0
07/26/01 K
Chloroethane
NO
ug/l
1.0
1.0
07/26/01 r
Trichlorofluoromethane
NO
ug/l
1.0
1.0
07/26/01 K',
1.1-Dichloroethene
NO
ug/l
1.0
1.0
07/26/01 K',
Methylene chloride
ND
ug/l
2.0
1.0
07/26/01 K',
trans-1.2-Dichloroethene
ND
ug/l
1.0
1.0
07/26/01 K:
1.1-Dichloroethane
ND
ug/l
1.0
1.0
07/26/01 K:
Chloroform
ND
ug/1
1.0
1.0
07/26/01 K
1.1.1-Trichloroethane
ND
ug/l
1.0
1.0
07/26/01 K.
Carbon tetrachloride
ND
ug/l
1.0
1.0
07/26/01 K'
1.2-Dichloroethane
ND
ug/l
1.0
1.0
07/26/01 K'
Trichloroethene
ND
ug/l
1.0
1.0
07/26/01 K'
1.2-Dichloropropane
ND
ug/l
1.0
1.0
07/26/01 K
Bromodichloromethane
NO
ug/l
1.0
1.0
07/26/01 K'
cis-1.3-Dichloropropene
ND
ug/l
1.0
1.0
07/26/01 K'
trans-1.3-Dichloropropene
ND
ug/l
1.0
1.0
07/26/01 K'
1.1.2-Trichloroethane
ND
ug/l
1.0
1.0
07/26/01 K'
Tetrachloroethene
NO
ug/l
1.0
1.0
07/26/01 K'
Dibromochloromethane
NO
ug/l
1.0
1.0
07/26/01 K:
Bromoform
NO
ug/l
1.0
1.0
07/26/01 K
1.1,2.2-Tetrachloroethane
NO
ug/l
1.0
1.0
07/26/01 K'
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
07/26/01 K'
Diisopropyl ether
ND
ug/l
1.0
1.0
07/26/01 K'
Benzene
ND
ug/l
1.0
1.0
07/26/01 K!
Toluene
ND
ug/l
1.0
1.0
07/26/01 1:
Chlorobenzene
ND
ug/l
1.0
1.0
07/26/01 r
Ethylbenzene
ND
ug/l
1.0
1.0
07/26/01 K!
m&p-Xylene
ND
ug/l
1.0
1.0
07/26/01 K
o-Xylene
ND
ug/l
1.0
1.0
07/26/01 K'
1.3-Dichlorobenzene
ND
ug/l
1.0
1.0
07/26/01 K
1.4-Dichlorobenzene
NO
ug/l
1.0
1.0
07/26/01 K!
1.2-Dichlorobenzene
NO
ug/l
1.0
1.0
07/26/01 K!
Date: 07/31/01
Laboratory Certification IDs
j NC Wastewater 12
NC Drinking Water 37706
- Sc 99006
I
CAS No. Ftnote Reg Limit
iT 75-71-8
iT 74-87-3
iT 75-01-4
iT 74-83-9
iT 75-00-3
iT 75-69-4
iT 75-35-4
7 75-09-2
iT 156-60-5
7 75-34-3
iT 67-66-3
>T 71-55-6
')T 56-23-5
7 107-06-2
;T 79-91-6
iT 78-87-5
7 75-27-4
7 10061-01-5
7 10061-02-6
;T 79-00-5
iT 127-18-4
;T 124-48-1
;T 75-25-2
;T 79-34-5
;T 1634-04-4
;T 108-20-3
7 71-43-2
;T 108-88-3
7 108-90-7
.T 100-41-4
IT
,T 95-47-6
;T 541-73-1
;T 106-46-7
IT 95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
`to[• 4CCaq�l^
eo �V x
Page: 3
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

I
'i
aceAnalytical"
j www.pacelabs.com
,I
Lab Project Number: 9224662
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No 921723854 Project Sample Number: 9224662-002 Date Collected: 07/19/01 15:45
Client Sample ID: WSP-2 Matrix: Water Date Received: 07/20/01 13:45
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Rea Limit
1-Chloro-3-fluorobenzene (S) 97 % 1.0 07/26/01 KST 625-98-9
Date: 07/31/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
� 4C(Qq
miac
Pao-: 4
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical m
-- www.pacelabs.com
Lab Project Number: 9224662
Client Project ID: SLS-Greensboro/010305/107535
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Lab Sample No: 921723862 Project Sample Number: 9224662-003 Date Collected: 07/19/01 15:40
Client Sample ID: WSP-3 Matrix: Water Date Received: 07/20/01 13:45
Parameters
GC Volatiles
Halogen. 8 Aromatic Vol. Orgs
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
-rich'_ luc,oaethane
1.1-Dichloroethene
Methylene chloride
trans-1.2-Dichloroethene
1.1-Dichloroethane
Chloroform
1.1.1-Trichloroethane
Carbon tetrachloride
1.2-Dichloroethane
Trichloroethene
1.2-Dichloropropane
Bromodichloromethane
cis-1.3-Dichloropropene
trans-1.3-Dichloropropene
1.1.2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1.1.2.2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
m&p-Xylene
o-Xylene
1.3-Dichlorobenzene
1.4-Dichlorobenzene
1.2-Dichlorobenzene
Date: 07/31/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Results
Units
Report Limit Dilution Analyzed
CAS No. Ftnote Rea Limit
Prep/Method:
EPA 601/602
/ EPA 601/602
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
75-71-8
ND
ug/l
2.0
1.0
07/26/01
07:53
KST
74-87-3
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
75-01-4
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
74-83-9
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
75-00-3
NO
1
1.0
07/26/01
07:53
KST
75-69-4
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
75-35-4
ND
ug/l
2.0
1.0
07/26/01
07:53
KST
75-09-2
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
156-60-5
ND
ua/l
1.0
1.0
07/26/01
07:53
KST
75-34-3
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
67-66-3
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
71-55-6
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
56-23-5
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
107-06-2
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
79-01-6
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
78-87-5
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
75-27-4
ND
ug/1
1.0
1.0
07/26/01
07:53
KST
10061-01-5
ND
ug/1
1.0
1.0
07/26/01
07:53
KST
10061-02-6
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
79-00-5
ND
ug/1
1.0
1.0
07/26/01
07:53
KST
127-18-4
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
124-48-1
NO
ug/1
1.0
1.0
07/26/01
07:53
KST
75-25-2
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
79-34-5
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
1634-04-4
NO
ug/l
1.0
1..0
07/26/01
07:53
KST
108-20-3
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
71-43-2
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
108-88-3
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
108-90-7
NO
ug/l
1.0
1.0
07/26/01
07:53
KST
100-41-4
ND
ug/1
1.0
1.0
07/26/01
07:53
KST
ND
ug/1
1.0
1.0
07/26/01
07:53
KST
95-47-6
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
541-73-1
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
106-46-7
ND
ug/l
1.0
1.0
07/26/01
07:53
KST
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 5
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627
A11 CCOM
\C

ace Analytical "
www.pacelabs.com
Lab Project Number: 9224662
Client Project ID: SLS-Greensboro/0j0305/107535
Lab Sample No: 921723862 Project Sample Number: 9224662-003 Date Collected: 07/19/01 15:40
Client Sample ID: WSP-3 Matrix: Water Date Received: 07/20/01 13:45
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
1-Chloro-3-fluorobenzene (S) • 99 % 1.0 07/26/01 07:53 KST 625-98-9
Date: 07/31/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�neh
Page. 6
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i
aceAnalyticalm
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number:
9224662
Client
Project
ID:
SLS-Greensboro/010305/107535
Lab Sample No. 921723870
Project Sample
Number: 9224662-004
Date Collected: 07/19/01 15:50
Client Sample ID: WSP-4
Matrix: ,Dater
Date Received: 07/20/01 13:45
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Limit
Metals
Trace ICP Metals
Prep/Method:
EPA 200.7
/ EPA 200.7
Iron
0.96
mg/l
0.050
1.0
07/26/01
03:26
RWF
7439-89-6
Lead
0.0065
mg/l
0.0030
1.0
07/26/01
03:26
RWF
7439-92-1
Manganese
0.041
mg/l
0.0050
1.0
07/26/01
03:26
RWF
7439-96-5
Date Digested
07/24/01
Wet Chemistry
Total Suspended Solids
Prep/Method:
EPA 160.2
/ EPA 160.2
Total Suspended Solids
16.
mg/l
2.0
1.0
07/26/01
CDE
Hexane Extractable Material
Prep/Method:
EPA 1664 /
EPA 1664
Oil and Grease
NO
mg/l
5.0
1.0
07/24/01
BYH
Ion Chromatography
Prep/Method:
EPA 300.0
/ EPA 300.0
Nitrate -Nitrite (as N)
NO
mg/1
0.30
1.0
07/20/01
CBJ
7727-37-9
GC/MS Volatiles
Volatile GUMS by 624
Prep/Method:
EPA 624 /
EPA 624
Vinyl chloride
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
75-01-4
1.1-Dichloroethene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
75-35-4
Methylene chloride
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
75-09-2
trans-1.2-Dichloroethene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
156-60-5
Methyl-tert-butyl ether
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
1634-04-4
1.1-Dichloroethane
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
75-34-3
cis-1.2-Dichloroethene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
156-59-2
Chloroform
NO
ug/1
5.0
1.0
07/24/01
04:12
RWS
67-66-3
1.1.1-Trichloroethane
ND
ug/1
5.0
1.0
07/24/01
04:12
RWS
71-55-6
1.2-Dichloroethane
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
107-06-2
Carbon tetrachloride
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
56-23-5
Benzene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
71-43-2
Trichloroethene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
79-01-6
1.2-Dichloropropane
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
78-87-5
Toluene
NO
ug/1
5.0
1.0
07/24/01
04:12
RWS
108-88-3
1.1.2-Trichloroethane
NO ti
uo/l
5.0
1.0
07/24/01
04:12
RWS
79-00-5
Date: 07/31/01
Page: 7
Laboratory Certification IDs REPORT OF LABORATORY AIIfALYSIS
NC Wastewater 12
NC Drinking Water 37706 This report shall not be reproduced, except in full,
-- Sc 99006 without the written consent of Pace Analytical Services, Inc.
fmiacs
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

1 �
aceAnalyf icafm
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersvflle, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number:
Client Project ID:
9224662
SLS-Greensboro/010305/107535
Lab Sample No: 921723870
Project Sample
Number: 9224662-004
Date Collected: 07/19/01 15:50
Client Sample ID: WSP-4
Matrix: Water
Date
Received: 07/20/01 13:45
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Limit
Tetrachloroethene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
127-18-4
Ethylbenzene
ND
ug/l
5.0
1.0
07/24/01
04:12
RWS
100-41-4
m8p-Xylene
NO
ug/l
10.
1.0
07/24/01
04:12
RWS
o-Xylene
NO
ug/l
5.0
1.0
07/24M
04:12
RWS
95-47-6
Bromoform
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
75-25-2
1.1.2.2-Tetrachloroethane
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
79-34-5
1.3-Dichlorobenzene
ND
ug/l
5.0
1.0
07/24/01
04:12
RWS
541-73-1
1.2-Dicnlorobenzene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
95-50-1
Dibromofluoromethane (S)
102
%
-
1.0
07/24/01
04:12
RWS
Toluene-d8 (S)
98
1.0
07/24/01
04:12
RWS
2037-26-5
4-Bromofluorobenzene (S)
106
a
1.0
07/24/01
04:12
RWS
460-00-4
1.2-Dibromoethane(EDB)
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
106-93-4
Naphthalene
ND
ug/l
5.0
1.0
07/24/01
04:12
RWS
91-20.3
1.3.5-Trimethylbenzene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
108-67-8
1.2.4-Trimethylbenzene
NO
ug/l
5.0
1.0
07/24/01
04:12
RWS
95-63-6
Date: 07/31/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
to Y �C�pgo
1
� f
f nek 4z
Page: 8
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Anal ical "
j www.pacelabs.com
)ASI Inc. Charlotte
�i800 Kincey Ave.
Suite 100
Huntersville, NC 28078
Attn: Project Management
'hone: [phone]
'.ab Sample No: 921723870
:Bent Sample ID: WSP-4
I
Parameters
Jet Chemistry
Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
Date: 07/31/01
age: 1
Laborat ry Certification IN
NC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number: 9322100
Client Project ID: IT-9224662
Project Sample Number: 9322100-001
Matrix: Water
Results Units Report Limit Analyzed
Prep/Method: EPA 351.2 / EPA 351.2
ND mg/l 0.10 07/31/01
M
Date Collected: 07/19/01 15:50
Date Received: 07/20/01 13:45
CAS No. Ftnote Reg Limit
JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,Y ACCOA
err
4
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

r
Pacetr...ilytical
Required Client Information Section A Required Client Information:
_' IAI-' _7F Aci ' -kec st " cu nt
The Chain-c tody is a LEGAL DOCUMENT. All relevant fields roust be completed accura
31 419
Section B Page: of To Be Completed by Pace Analytical and Client Section C
Company — A --
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Report To: /� �/ _
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Client Information Check quotelrontract : __ _
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Invoice To:
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Turn Around Time (TAT) in calendar days.
Project Name n �f /��,/
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Section D Required Client Information:
q
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f.7ATRIX CODE
1
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Preservatives
m
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SAMPLE I D
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Date Time
Temp in °C:
-
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Additional Comments:
AND
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ORIGINAL
SEE REVERSE SIDE FOR INSTRUC S� ci Pace Analytical Service Ir1 r Form COCO1 02ln

90000?
ceAnalytical '"
i i,;'..: paceiabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Pace Analytical Services, Inc.
1700 Elm Street Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax:[phone]
Lab Project Number: 1047138
Client Project ID: 9224852-IT
Lab Sample No: 921735106
Project Sample
Number: 1047138-002
Date Collected: 07/26/01 13:45
Client Sample ID: ASP-2(#196)
INF
Matrix: Air
Date Received: 07/27/01 00:00
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
(Air
GC/MS VOCs, in Air
Prep/Method:
TO-14 Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.26
08/08/01
10:07
MTG
75-01-4
Methylene chloride
ND
ppmv
0.26
OB/08/01
10:07
MTG
75-09-2 1
cis-1,2-Dichloroethene
ND
ppmv
0.26
08/08/01
10:07
MTG
156-59-2
Chloroform
ND
ppmv
0.26
08/08/01
10:07
MTG
67-66-3
Benzene
ND
ppmv
0.26
08/08/01
10:07
MTG
71-43-2
-- Carbon tetrachloride
ND
ppmv
0.26
08/08/01
10:07
MTG
56-23-5
Trichloroethene
ND
ppmv
0.26
08/08/01
10:07
MTG
79-01-6
Tetrachloroethene
2.2-
ppmv
0.26
08/08/01
10:07
MTG
127-18-4
THC as Gas
ND
ppmv
2.6
08/08/01
10:07
MTG
d
Date: 08/08/01
.. ..,I ACCn,,
a nelac.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

II - -
_ ceAnalXical
+ :; r;:;: pace/abs.cotn
Pace Analytical Services, Inc.
1700 Elm Street Suite 200
Minneapolis, MN55414
Phone.- 612.607.1700
Fax. • 612.607.6444
Lab Project Number: 1047138
Client Project
ID: 9224852-IT
Lab Sample No: 921735114
Project Sample
Number: 1047138j003
Date Collected: 07/26/01 13:47
Client Sample ID: ASP-3(#052)
EFF
Matrix: Air
Date Received: 07/27/01 00:00
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Air
GC/MS VOCs, in Air
Prep/Method:
TO-14 Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.14
08/08/01
09:02
MTG
75-01-4
Methylene chloride
ND
ppmv
0.14
08/08/01
09:02
MTG
75-09-2 1
cis-1,2-Dichloroethene
ND
ppmv
0.14
08/08/01
09:02
MTG
156-59-2
Chloroform
ND
ppmv
0.14
08/08/01
09:02
14TG
67-66-3
Benzene
ND
ppmv
0.14
OB/08/01
09:02
MTG
71-43-2
Carbon tetrachloride
ND
ppmv
0.14
08/08/01
09:02
MTG
56-23-5
Trichloroethene
ND
ppmv
0.14
08/08/01
09:02
MTG
79-01-6
Tetrachloroethene
ND
ppmv
0.14
08/08/01
09:02
MTG
127-18-4
THC as Gas
ND
ppmv
1.4
08/08/01
09:02
MTG
r
Date: 08/08/01
�o -
""'' REPORT OF LABORATORY ANALYSIS
e This report shall not be reproduced, except in full,
dielac. without the written consent of Pace Analytical Services, Inc.
Page: 2

Facet,,alytical'
www.pacelabs.com
; st _,�c it.nt
1'he Chain -of ,tody is a LEGAL DOCUMENT. All relevant fields must be completed accurat, -
Re ulred Client Inlormation: Section B
f; (l -1 A -i
Required Client Information:Rep
Section A
Report To:
% ` - p
/ ��y�X v
Page: of
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Io Be Completed by Pace
Oumte Rererence:----
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Proiite N:
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Turn Around Time (TAT) in calendar days.
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Requested Analysis:
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Section f) Required Client Information:
Vali Matrix Codes 4—___
MATRIX CODE
❑
❑
Preservatives
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SAMPLE
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pH --

i
ace Anal Yticaf"
www.pacelahs.com
I
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Charles Bertz
Phone: [phone] x236
Lab Sample No: 921782439
Client Sample ID: WSP-1
Parameters
GC Volatiles 1
Halogen. & Aromatic Vol. Orgs
Dichlorodifluoromethane
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Trichloroethene
1.2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
trans-1.3-Dichloropropene -
1,1.2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1,1,2.2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Date: 09/17/0l
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225589-001 Date Collected: 08/23/01 16:00
Matrix: Water Date Received: 08/24/01 15:52
Results
Units
Reoort
Limit Dilution Analyzed
CAS No. Ftnote Reg Limit
Prep/Method:
EPA 601/602
/ EPA
601/602
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-71-8
NO
ug/l
100
50.0
08/28/01
04:33
PPM
74-87-3
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-01-4
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
74-83-9
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-00-3
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-69-4
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-35-4
ND
ug/l
100
50.0
08/28/01
04:33
PPM
75-09-2
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
156-60-5
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
75-34-3
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
67-66-3
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
71-55-6
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
56-23-5
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
107-06-2
1100
ug/l
50.
50.0
08/28/01
04:33
PPM
79-01-6
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
78-87-5
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-27-4
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
10061-01-5
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
10061-02-6
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
79-00-5
2600
ug/l
50.
50.0
08/28/01
04:33
PPM
127-18-4
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
124-48-1
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
75-25-2
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
79-34-5
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
1634-04.4
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
108-20-3
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
71-43-2
NO
ug/l
50.
50.0
08/28/01
04:33
PPM
108-88-3
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 12
NC Drinking Water 37706 This report shall not be reproduced, except in full,
Sc 99006 without the written consent of Pace Analytical Services, Inc.
ACCo,
O�
a
Me
Page: 1
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

;acieAnalyticafm
www.pacelabs.com
it
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921782439
Project Sample
Number:
9225589-001
Date Collected: 08/23/01 16:00
Client Sample ID: WSP-1
Matrix:
Water
Date
Received: 08/24/01 15:52
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Reg Limit
Chlorobenzene
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
108-90-7
Ethylbenzene
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
100-41-4
m&p-Xylene
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
o-Xylene
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
95-47-6
1.3-Dichlorobenzene
ND
ug/1
50.
50.0
08/28/01
04:33
PPM
541-73-1
1.4-Dichl'orobenzene
ND
ug/l
50.
50.0
08/28/01
04:33
PPM
106-46.7
1.2-Dichlorobenzene
ND
ug/l
50.
50.0
08/28/61
04:33
PPM
95-50-1
1-Chloro-3-fluorobenzene (S)
100
X
1.0
08/28/01
04:33
PPM
625-98-9
I
i
I ,
Date: 09/17/01 Page: 2
Laboratory Certification IN Laboratory Certification IN
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
full,
This report shall not be reproduced, except in fu,
- NC Drinking Water 37706 VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627
,y �CCOA

i`
;acieAnalyficafA
www.pacelabs.com
_I
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921782447
Project
Sample
Number: 9225589.002
Date Collected: 08/23/01 16:00
Client Sample ID: WSP-2
Matrix: Water
..Date
Received: 08/24/01 15:52
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
GC Volatiles
Halogen. & Aromatic Vol. Orgs.
Prep/Method:
EPA 601/602
/ EPA 601/602'
Dichlorodifluoromethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
08/28/01
05:16
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
74-83-9
Chloroethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-69-4
1,1-Dichloroethene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
08/28/01
05:16
PPM
75-09-2
trans-1.2-Dichloroethene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
156-60-5
1,1-Dichloroethane
ND
ug/1
1.0
1.0
08/28/01
05:16
PPM
75-34-3
Chloroform
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
67-66-3
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
71-55-6
Carbon tetrachloride
ND
ug/1
1.0
1.0
08/28/01
05:16
PPM
56-23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
107-06-2
Trichloroethene
4.0
ug/l
1.0
1.0
OB/28/01
05:16
PPM
79-01-6
1,2-Dichloropropane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
10061-01-5
trans-1.3-Dichloropropene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
10061.02-6
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
79-00-5
Tetrachloroethene
4.9
ug/l
1.0
1.0
08/28/01
05:16
PPM
127-18-4
Dibromochloromethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
124-48-1
Bromoform
ND
ug/1
1.0
1.0
08/28/01
05:16
PPM
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
79-34-5
Methyl-tert-butyl ether
ND
ug/1
1.0
1.0.
08/28/01
65:16
PPM
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
108-20-3
Benzene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
71-43-2
Toluene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
108-88-3
Chlorobenzene
ND
ug/1
1.0
1.0
08/28/01
05:16
PPM
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
100-41-4
m&p-Xylene
ND
ug/1
1.0
1.0
08/28/01
05:16
PPM
o-Xylene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
95-47-6
1,3-Dichlorobenzene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
541-73-1
1.4-Dichlorobenzene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
106-46-7
1,2-Dichlorobenzene
ND
ug/l
1.0
1.0
08/28/01
05:16
PPM
95-50-1
Date: 09/17/01 Page: 3
Laborato Certification IDs Laboratory Certification IDs
ry REPORT OF LABORATORY ANALYSIS �
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627
•CCOgO„
nelac

ace Analytical u
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921782447 Project Sample Number: 9225589-002 Date Collected:. 08/23/01 16:00
Client Sample ID: WSP-2 Matrix: Water Date Received: 08/24/01 15:52
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
1-Chloro-3-fluorobenzene (S) 100 % 1.0 08/28/01 05:16 PPM 625-98-9
Date: 09/17/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,x ACC0909
4
�`nerac:=
Page: 4
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

I
J ;acieAnalyfical"'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921782454
Project Sample
Number: 9225589-003
Date Collected: 08/23/01 16:00
Client Sample ID: WSP-3
Matrix: Water
Date
Received: 08/24/01 15:52
Parameters
Results
Units
Report Limit Dilution Analyzed
CAS No. Ftnote Reg Limit
GC Volatiles
- Halogen. & Aromatic Vol. Orgs.
Prep/Method:
EPA 601/602
/ EPA 601/602
Dichlorodifluoromethane
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
75.71-8
Chloromethane
NO
ug/l
2.0
1.0
08/28/01
05:58
PPM
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
74-83.9
Chloroethane
ND
ug/1
1.0
1.0
08/28/01
05:58
PPM
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-69-4
1.1-Dichloroethene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-35-4
Methylene chloride
NO
ug/l
2.0
1.0
08/28/01
05:58
PPM
75-09.2
i trans-1,2-Dichloroethene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
156.60-5
1.1-Dichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-34-3
Chloroform
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
67-66-3
1.1.1-Trichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
56.23-5
1.2-Dichloroethane
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
107-06-2
Trichloroethene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
79-01-6
1,2-Dichloropropane
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
78-87-5
- Bromodichloromethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
10061-01-5
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
10061-02.6
1,1.2-Trichloroethane
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
79-00-5
Tetrachloroethene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
127-18-4
Dibromochloromethane
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
124-48-1
Bromoform
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
75-25-2
1.1.2,2-Tetrachloroethane '
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
79-34-5
- Methyl-tert-butyl ether
!
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
1634-04.4
i
Diisopropyl ether
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
108-20.3
Benzene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
71-43-2
Toluene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
108-88-3
Chlorobenzene
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
108-90-7
Ethylbenzene
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
100-41-4
m&p-Xylene
ND
ug/l
1.0
1.0
08/28/01
05:58
PPM
o-Xylene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
95-47-6
1,3-Dichlorobenzene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
541-73-1
1,4-Dichlorobenzene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
106-46-7
1.2-Dichlorobenzene
NO
ug/l
1.0
1.0
08/28/01
05:58
PPM
95-50-1
Date: 09/17/01 Page: 5
LaboratoryCertification IDs Laboratory Certification IDs
REPORT OF LABORATORY ANALYSIS y
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627
' ,H •C[ON
1�
°ndac=

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921782454 Project Sample Number: 9225589.003 Date Collected: 08/23/01 16:00
Client Sample. ID: WSP-3 Matrix: Water Date Received: 08/24/01 15:52
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
1-Chloro-3-fluorobenzene (S) 98 % 1.0 08/28/01 05:58 PPM 625.98-9
Date: 09/17/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
ACCaMO'
O�
nelac =
Page: 6
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

1
I__
ace Analytical'm
www.pacelabs.com
Lab Sample No: 921782462
Client Sample ID: WSP-4
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225589-004 Date Collected: 08/23/01 16:00
Matrix: Water Date Received: 08/24/01 15:52
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
Metals
Trace ICP_Metals
Iron
Lead
Manganese
Date Digested
Wet Chemistry
Total Suspended Solids
Total Suspended Solids
Hexane Extractable Material
Oil and Grease
Ion Chromatography
Nitrate -Nitrite (as N)
GUMS Volatiles
Volatile GUMS by 624
Vinyl chloride
1.1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
Methyl-tert'-butyl ether
1,1-Dichloroethane
cis-1,2-Dichloroethene
Chloroform
1,1.1-Trichloroethane
1.2-Dichloroethane
Carbon tetrachloride
Benzene
Trichloroethene
1.2-Dichloropropane
Toluene
1.1.2-Trichloroethane
Date: 09/17/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Prep/Method:
EPA 200.7 / EPA 200.7
4.1
mg/l 0.050
ND
mg/l 0.0030
0.098
mg/1 0.0050
Prep/Method: EPA 160.2 / EPA 160.2
26. mg/l 5.0
Prep/Method: EPA 1664 / EPA 1664
ND mg/l 5.0
Prep/Method: EPA 300.0 / EPA 300.0
NO mg/l 0.30
Prep/Method: EPA 624 / EPA 624
ND
ug/l
5.0
ND
ug/l
5.0
NO
ug/1
5.0
NO
ug/l
5.0
NO
ug/1
5.0
ND
ug/l
5.0
NO
ug/l
5.0
NO
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
NO
ug/1
5.0
NO
ug/l
5.0
NO
ug/l
5.0
NO
ug/l
5.0
NO
ug/l
5.0
1.0 08/31/01 14:55 RWF 7439-89-6
1.0 08/31/01 14:55 RWF 7439-92-1
1.0 08/31/01 14:55 RWF 7439-96-5
08/30/01
5.0 08/29/01 AST
1.0 09/04/01 BYH
1.0 08/24/01, COE 7727-37.9
1.0 08/28/01 10:57 RPJ 75-01-4
1.0 08/28/01 10:57 RPJ 75-35-4
1.0 08/28/01 10:57 RPJ 75-09-2
1.0 08/28/01 10:57 RPJ 156-60-5
1.0 08/28/01 10:57 RPJ 1634-04-4
1.0 08/28/01 10:57 RPJ 75-34-3
1.0 08/28/01 10:57 RPJ 156-59-2
1.0 08/28/01 10:57 RPJ 67-66-3
1.0 08/28/01 10:57 RPJ 71.55-6
1.0 08/28/01 10:57 RPJ 107-06-2
1.0 08/28/01 10:57 RPJ 56.23-5
1.0 08/28/01 10:57 RPJ 71-43-2
1.0 08/28/01 10:57 RPJ 79-01-6
1.0 08/28/01 10:57 RPJ 78-87-5
1.0 08/28/01 10:57 RPJ 108-88-3
1.0 68/28/01 10:57 RPJ 79-00-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\M •CC09
`nela&
r
Page: 7
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical
www.pacelabs.com
Lab Sample No: 921782462
Client Sample ID: WSP-4
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
fax [phone]
Lab Project Number: 9225589
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225589.004 Date Collected: 08/23/01 16:00
Matrix: Water Date Received: 08/24/01 15:52
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Tetrachloroethene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
127-18-4
Ethylbenzene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
100-41-4
m&p-Xylene
ND
ug/l
10.
1.0
08/28/01
10:57
RPJ
o-Xylene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
95-47-6
Bromoform
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
75-25-2
1,1.2.2-Tetrachloroethane
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
79-34-5
1.3-Dichlorobenzene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
541-73-1
1.2-Dichlorobenzene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
95-50-1
Dibromofluoromethane (S)
99
X
1.0
08/28/01
10:57
RPJ
Toluene-d8 (S)
99
X
1.0
08/28/01
10:57
RPJ
2037-26-5
4-Bromofluorobenzene (S)
102
X
1.0
08/2B/01
10:57
RPJ
460-00-4
Naphthalene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
91-20-3
1.2-Dibromoethane (EDB)
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
106-93-4
1,3.5-Trimethylbenzene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
108-67-8
1.2.4-Trimethylbenzene
ND
ug/l
5.0
1.0
08/28/01
10:57
RPJ
95-63-6
Date: 09/17/01
_Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 12 This report shall not be reproduced, except in full,
NC Drinking Water 37706
Sc 99006 without the written consent of Pace Analytical Services, Inc.
,y ACCOA
Mel
Page: 8
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical
www.pacelabs.com
PASI Inc. Charlotte
9800 Kincey Ave.
Suite 100
HuntersviLLe,.NC 28078
Attn: Project Management
Phone: [phone]
.Lab Sample No: 921782462
Client Sample ID: WSP-4
Parameters
Wet Chemistry
Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, TotaL
Date: 09/04/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax., 828.254.4618
Lab Project Number: 9322940
Client Project ID: IT-9225589
Project Sample Number: 9322940-001
Matrix: Water
Results Units Report Limit
Prep/Method: EPA 351.2 / EPA 351.2
Date Collected: 08/23/01 16:00
Date Received: 08/24/01 15:52
Analyzed CAS No. Ftnote Reg Limit
ND mg/1 0.10 08/31/01 JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
M ACcp�
' Page: 1
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

i
i
an
eAnalyicaf"
wrAypace/ebscom
i sty
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100'
Huntersville, NC 28078
Attn. Client Service
Phone: [phone]
Pace Analytical Services, Inc.
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Far 612.607.6444
Lab Project Number: 1048111
Client Project ID: 9225589 IT
Lab Sample No: 921782496 Project Sample Number: 1048111-001 Date Collected: 08/23/01 16:00
Client Sample ID: ASP-1B (#24) Matrix: Air Date Received: 08/24/01 15:52
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Rea Limit
Air
GC/MS VOCs, in Air
Vinyl chloride
Methylene chloride
cis-1,2-Dichloroethene
Chloroform
Benzene
Carbon tetrachloride
Trichloroethene
Tetrachloroethens
THC as Gas
Prep/Method: TO-14 Source
/ TO-14
Source
ND
ppmv
0.14
09/14/01
09:30
MTG
75-01-4 1
ND
ppmv
0.14
09/14/01
09:30
MTG
75-09-2
ND
ppmv
0.14
09/14/01
09:30
MTG
156-59-2
ND
ppmv
0.14
09/14/01
09:30
MTG
67-66-3
ND
ppmv
0.14
09/14/01
09:30
MTG
71-43-2
ND
ppmv
0.14
09/14/01
09:30
MTG
56-23-5
0.63
pp=7
0.14
09/14/01
09:30
MTG
79-01-6
1.1
ppmv
0.14
09/14/01
09:30
MTG
127-18-4
ND
ppmv
1.4
09/14/01
09:30
MTG
Lab Sample No: 921782504
Project Sample Number: 1048111-002
Date Collected: 08/23/01 16:00
Client Sample ID: ASP-2 (#108)
Matrix: Air
Date Received: 08/24/01 15:52
Parameters
Results
Units
Report Limit
Analyzed
CAS No. F note Rea Limit
Air
GC/MS VOCs, in Air
Prep/Method:
TO-14
Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.23
09/13/01
11:56
MTG
75-01-4 1
Methylene chloride
ND
ppmv
0.23
09/13/01
11:56
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
156-59-2
Chloroform
ND
ppmv
0.23
09/13/01
11:56
MTG
67-66-3
Benzene
ND
ppmv
0.23
09/13/01
11:56
MTG
71-43-2
Trichloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
79-01-6 -
Tetrachloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
127-18-4
THC as Gas
ND
ppmv
2.3
09/13/01
11:56
MTG
Date: 09/17/01 Pape: 1
ACCp9CgH� REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

i
- aciaAnalytical m
Wvhv, pacelabs cow
k
Pace Analytical Services, Inc.
1700 Elm Street, Suite 200
Minneapolis, AN 55414
Phone. [phone]
Far 612.607.6444
Lab Project Number: 1048111
Client Project
ID: 9225589 IT
Lab Sample No: 921782512
Project Sample Number: 1048111-003
Date Collected: 08/23/01 16:00
Client Sample ID: ASP-3 (#233)
Matrix: Air
Date Received: 08/24/01 15:52
Parameters
Results
units
Report Limit
Analyzed
CAS No. Ftnote Rea Limit
Air
GUMS VOCs, in Air
Prep/Method: TO-14 source / TO-14 Source
Vinyl chloride
ND
ppmv
0.14
09/13/01 11:26
MTG
75-01-4 1
Methylene chloride
ND
ppmv
0.14
09/13/01 11:26
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppmv
0.14
09/13/01 11:26
MTG
156-59-2
Chloroform
ND
ppmv
0.14
09/13/01 11:26
MTG
67-66-3
Benzene
ND
ppmv
0.14
09/13/01 11:26
MTG
71-43-2
Trichloroethene
ND
ppmv
0.14
09/13/01 11:26
MTG
79-01-6
Tetrachloroethene
ND
pp=7
0.14
09/13/01 11:26
MTG
127-18-4
TBC as Gas
ND
ppmv
1.4
09/13/01 11:26
MTG
Date: 09/17/01
ACCo'90
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

/0
PC, cef,r,�ilytical
www.pacelabs.cunl
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Required Client Information: Section B
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(IU41(.I hl AI Or-r- mf_11rnrlr _P"n r_n • ._. _o r.. —...,

a ceAnalytical"
w:vw.pacerabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Pace Ana/ytIcal Services, Inc.
1700 Elm Street Suite 200
Minneapolis, MN 55414
Phone: [phone]'
Fax., 612.607.6444
Lab Project Number: 1048111
Client Project ID: 9225589 IT
Lab Sample No: 921782496 Project Sample Number: 1048111-001 Date Collected: 08/23/01 16:00
Client Sample ID: ASP-lB (#24) Matrix: Air Date Received: 08/24/01 15:52
Air
GC/MS VOCs, in Air
Prep/Method:
TO-14
Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.14
09/14/01
09:30
MTG
75-01-4 1
Methylene chloride
ND
ppmv
0.14
09/14/01
09:30
MTG
75-09,-2
cis-1,2-Dichloroethene
ND
ppmv
0.14
09/14/01
09:30
MTG
156-59-2
Chloroform
ND
ppmv
0.14
09/14/01
09:30
MTG
67-66-3
Benzene
ND
ppmv
0.14
09/14/01
09:30
MTG
71-43-2
Carbon tetrachloride
ND
ppmv
0.14
09/14/01
09:30
MTG
56-23-5
Trichloroethene
0.63
ppmv
0.14
09/14/01
09:30
MTG
79-01-6
Tetrachloroethene
1.1
ppmv
0.14
09/14/01
09:30
MTG
127-18-4
THC as Gas
ND
ppmv
1.4
09/14/01
09:30
MTG
Lab Sample No: 921782504
Project Sample Number: 1048111-002
Date Collected:
08/23/01 16:00
Client Sample ID: ASP-2 (#108)
Parameters
Results
Matrix: Air
Date Received:
08/24/01 15:52
Air
Units
Report Limit
Analyzed
CAS No. Ftnote
Rea Limit
GC/MS VOCs, in Air
Prep/Method:
TO-14
Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.23
09/13/01
11:56
MTG
75-01-4 1
Methylene chloride
ND
ppmv
0.23
09/13/01
11:56
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
156-59-2
Chloroform
ND
ppmv
0.23
09/13/01
11:56
MTG
67-66-3
Benzene
ND
ppmv
0.23
09/13/01
11:56
MTG
71-43-2
Trichloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
79-01-6
Tetrachloroethene
ND
ppmv
0.23
09/13/01
11:56
MTG
127-18-4
THC as Gas
ND
ppmv
2.3
09/13/01
11:56
MTG
Date. 09/17/01
_
Page: 1
'"-?°�tiv REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

aceAnalytical'
w: nv. pacelabs. corn
Pace Analytical Servlcas, Inc.
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
Fax: [phone]
Lab Project Number:
1048111
Client Project
ID:
9225589 IT
Lab Sample No: 921782512
Project Sample
Number: 1048111-003
Date Collected: 08/23/01 16:00
Client Sample ID: ASP-3 (#233)
Results
Matrix: Air
Date Received: 08/24/01 15:52
Parameters
Air
Units
Report Limit
Analyzed
CAS No. Ftnote RReg Limit
GC/MS VOCs, in Air
Prep/Method:
TO-14 Source / TO-14 Source
Vinyl chloride
ND
ppmv
0.14
09/13/01
11:26
MTG
75-01-4 1
Methylene chloride--
ND
ppmv
0.14
09/13/01
11:26
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppmv
0.14
09/13/01
11:26
MTG
156-59-2
Chloroform
ND
ppmv
0.14
09/13/01
11:26
MTG
67-66-3
Benzene
ND
ppmv
0.14
09/13/01
11:26
MTG
71-43-2
Trichloroethene
ND
ppmv
0.14
09/13/01
11:26
MTG
79-01-6
Tetrachloroethene
ND
ppmv
0.14
09/13/01
11:26
MTG
127-18-4
THC as Gas
ND
ppmv
1.4
09/13/01
11:26
14TG
Date: 09/17/01 ?age: 2
r�0 \N Ac`og0
ti
q
_. ed 6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I

aceAnalyticaf"
www.pacelahs.com
iT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Keith Ogden
Phone: [phone] x224
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax- 704.875.9091
Lab Project Number: 9225907
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921805818 Project Sample Number: 9225907-001 Date Collected: 09/06/01 16:30
client Sample ID: wSP-1 Matrix: water Date Received: 09/07/01 11:10
Parameters
Limit
GC Volatiles
Halogen. & Aromatic vol. Orgs
Dichlorodifluoromethane
Chloromethane
vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Chlorobenzene
Date: 09/24/01
Laboratory Certification IN
, NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Results
units Report
Limit Dilution Analyzed
CAS No. Ftno a Reo
Prep/Method:
EPA 601/602 /
EPA
601/602
.ND
ug/l
50.
50.0
09/13/01
KST
75-71-8
NO
ug/1
100
50.0
09/13/01
KST
74-87-3
NO
ug/1
50.
50.0
09/13/01
KST
75-01-4
NO
ug/1
50.
50.0
09/13/01
KST
74-83-9
NO
ug/1
5o.
50.0
09/13/01
KST
75-00-3
NO
ug/1
so.
50.0
09/13/01
KST
75-69-4
NO
ug/1
so.
50.0
09/13/01
KST
75-35-4
NO
ug/1
100
50.0
09/13/01
KST
75-09-2
NO
ug/1
so.
50.0
09/13/01
KST
156-60-5
NO
ug/1
so.
50.0
09/13/01
KST
75-34-3
NO
ug/1
50.
50.0
09/13/01
KST
67-66-3
NO
ug/1
50.
50.0
09/13/01
KST
71-55-6
-ND
ug/l
50.
50.0
09/13/01
KST
56-23-5
ND
ug/1
50.
50.0
09/13/01
KST
107-06-2
1100
ug/1
50.
50.0
09/13/01
KST
79-01-6
NO
ug/1
50.
50.0
09/13/01
KST
78-87-5
ND
ug/1
50.
50.0
09/13/01
KST
75-27-4
NO
ug/1
50.
50.0
09/13/01
KST
10061-01-5
NO
ug/1
so.
50.0
09/13/01
KST
10061-02-6
NO
ug/1
so.
50.0
09/13/01
KST
79-00-5
6800
ug/1
200
200
09/13/01
KST
127-18-4
NO
ug/1
so.
50.0
09/13/01
KST
124-48-1
NO
ug/1
50.
50.0
09/13/01
KST
75-25-2
NO
ug/l
50.
50.0
09/13/01
KST
79-34-5
NO
ug/l
50.
50.0
09/13/01
KST
1634-04-4
NO
ug/l
50.
50.0
09/13/01
KST
108-20-3
120
ug/l
50.
50.0'
09/13/01
KST
71-43-2
140
ug/l
so.
50.0
09/13/01
KST
108-88-3
NO
ug/1
50.
50.0
09/13/01
KST
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page: 1
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

1
ace Analytical
www.pacelabs.com
I
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number:
9225907
client
Project ID:
SLS-Greensboro/010305/107535
Lab sample No: 921805818
Project sample
Number:
9225907-001
Date collected: 09/06/01 16:30
client sample ID: WSP-1
Matrix:
water
Date Received: 09/07/01 11:10
Parameters
Results
units
Report
Limit Dilu ion Analyzed CAS No. Ftnote Req
Limit
Ethylbenzene
ND
ug/l
50.
50.0
09/13/01
KST 100-41-4
m&p-xylene
54.
ug/l
50.
50.0
09/13/01
KST
o-xylene
ND
ug/l
50.
50.0
09/13/01
KST 95-47-6
1,3-Dichlorobenzene
ND
ug/l
50.
50.0
09/13/01
KST 541-73-1
1,4-Dichlorobenzene
ND
ug/l
so.
50.0
09/13/01
KST 106-46-7
1,2-Dichlorobenzene
ND
ug/l
50.
50.0
09/13/01
KST 95-50-1
1-chloro-3-fluorobenzene (s)
105
%
1.0
09/13/01
KST 625-98-9
I
Date: 09/24/01
N
Page: 2
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS 4aboratdry Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

KcieAnalyticaf'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax:[phone]
Lab Project Number: 9225907
Client Project ID' SLS-Greensboro/010305/107535
Lab Sample No: 921805826 Project Sample Number: 9225907-002 Date collected: 09/06/01 16:30
Client Sample ID: wSP-2 Matrix: water Date Received: 09/07/01 11:10
Parameter$
Limit
GC volatiles
Halo en. & Aromatic vol. Orgs
Dichlorodifluoromethane
Chloromethane
vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
Chloroform
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1,1,2,2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Chlorobenzene
Ethylbenzene
m&p-Xylene
o-Xylene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1-Chloro-3-fluorobenzene (S)
Results Units Report Limit Dilu ion_ Analyzed CAS No. Ftnote Reg_
Prep/Method: EPA 601/602 / EPA 601/602
NO
ug/1
1.0
1.0
NO
ug/1
2.0
1:0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
2.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1.
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
1.4
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/1
1.0
1.0
5.2
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/1
1.0
1.0
NO
ug/l
1.0
1.0
4.7
ug/l
1.0
1.0
1.3
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
NO
ug/l
1.0
1.0
98
%
1.0
Date: 09/24/01 _
j
Laboratory certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 12
NC Drinking Water 37706 This report shall not be reproduced, except in full,
SC 99006, without the written consent of Pace Analytical Services, Inc.
06:46
06:46
06:46
06:46
06:46
06:46
06.46
06:46
06.46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
06:46
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
KST
75-71-8
74-87-3
75-01-4
74-83-9
75-00-3
75-69-4
75-35-4
75-09-2
156-60-5
75-34-3
67-66-3
71-55-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
10061-01-5
10061-02-6
79-00-5
127-18-4
124-48-1
75-25-2
79-34-5
1634-04-4
108-20-3
71-43-2
108-88-3
108-90-7
100-41-4
95-47-6
541-73-1
106-46-7
95-50-1
625-98-9
Page: 3
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical,M
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100,
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 9225907
client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921805834 Project Sample Number: 9225907-003 Date Collected: 09/06/01 16:30
Client Sample ID: wSP-3 Matrix: water Date Received: 09/07/01 11:10
Parameters
_' Limit
GC Volatiles
Halogen. & Aromatic vol. Orgs
Dichlorodifluoromethane
Chloromethane
vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dichloroethane
chloroform
1,1,1-Trichloroethane
carbon tetrachloride
1,2-Dichloroethane -
__ Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethene
Dibromochloromethane
Bromoform
1,1,2 2-Tetrachloroethane
Methyl-tert-butyl ether
Diisopropyl ether
Benzene
Toluene
Chlorobenzene
f Ethylbenzene
m&p-xylene
o-xylene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1-Chloro-3-fluorobenzene (s)
Date: 09/24/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Results
units Report
Limit
Dilution
Analyzed
CAS No. Floora Req
Prep/Method:
EPA 601/602 /
EPA 601/602
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
75-71-8
ND
ug/1
2.0
1.0
09/13/01
07:32
KST
74-87-3
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
75-01-4
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
74-83-9
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
75-00-3
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
75-69-4
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
75-35-4
NO
ug/l
2.0
1.0
09/13/01
07:32
KST
75-09-2
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
156-60-5
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
75-34-3
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
67-66-3
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
71-55-6
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
56-23-5
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
107-06-2
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
79-01-6
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
78-87-5
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
75-27-4
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
10061-01-5
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
10061-02-6
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
79-00-5
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
127-18-4
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
124-48-1
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
75-25-2
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
79-34-5
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
1634-04-4
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
108-20-3
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
71-43-2
ND
ug/1
1.0
1.0
09/13/01
07:32
KST
108-88-3
NO
ug/1
1.0
1.0
09/13/01
07:32
KST
108-90-7
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
100-41-4
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
95-47-6
ND
ug/l
1.0
1.0
09/13/01
07:32
KST
541-73-1
NO
ug/l
1.0
1.0.
09/13/01
07:32
KST
106-46-7
NO
ug/l
1.0
1.0
09/13/01
07:32
KST
95-50-1
109
%
1.0
09/13/01
07:32
KST
625-98-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical T M
www.pacelabs.com
I
Pace Analytical Services, Inc.
00
9800 KHunter vine,cey Suite 78
Huntersville, NC 28078
Phone. [phone]
Fax: [phone]
Lab Project Number: 9225907
Client Project ID: SAS-Greensboro/010305/107535
Lab Sample No: 921805842
Project
Sample Number: 9225907-004
Date Collected: 09/06/01 16:30
Client sample ID: WSP-4
Matrix: water
Date Received: 09/07/01 11.10
Parameters
Results
units
Report Limit
Dilu ion Analyzed
CAS No. F note Recce
Metals
Trace ICP Metals
Prep/Method:
EPA 200.7
/ EPA 200.7
Iron
0.69
mg/l
0.050
1.0
09/11/01
16:28
RWF
7439-89-6
read
0.0035
mg/l
0.0030
1.0
09/11/01
16:28
RWF
7439-92-1
Manganese
0.033
mg/l
0.0050
1.0
09/11/01
16:28
RwF
7439-96-5
Date Digested
09/10/01
wet Chemistry
Total Suspended solids
Prep/Method:
EPA 160.2
/ EPA 160.2
Total Suspended solids
11.
mg/l
5.0
5.0
09/11/01
CDE
Hexane Extractable Material
Prep/Method:
EPA 1664 / EPA 1664
oil and Grease
ND
mg/l
5.0
1.0
09/10/01
BYH
ion Chromatography
Prep/Method:
EPA 300.0
/ EPA 300.0
Nitrate -Nitrite (as N)
0.35
mg/l
0.30
1.0
09/07/01
CDE
7727-37-9
GC/MS Volatiles
volatile GC/MS by 624
Prep/Method:
EPA 624 /
EPA 624
vinyl chloride
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
75-01-4
1,1-Dichloroethene
'_a
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
75-35-4
Methylene chloride
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
75-09-2
trans-1,2-Dichloroethene
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
156-60-5
Methyl-tert-butyl ether
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
1634-04-4
1,1-Dichloroethane
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
75-34-3
cis-1,2-Dichloroethene
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
156-59-2
Chloroform
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
67-66-3
_ 1,1,1-Trichloroethane
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
71-55-6
1,2-Dichloroethane
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
107-06-2
Carbon tetrachloride
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
56-23-5
Benzene
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
71-43-2
z Trichloroethene
ND
ug/1
5.0
1.0
09/19/01
09:43
RPJ
79-01-6
1,2-Dichloropropane
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
78-87-5
-- Toluene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
108-88-3
1,1,2-Trichloroethane
ND
ug/l
5.0
1.0
09/19/01'09:43
RPJ
79-00-5
Tetrachloroethene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
127-18-4
Ethylbenzene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
100-41-4
m&p-xylene
ND
ug/l
10.
1.0
09/19/01
09:43
RPJ
Date: 09/24/01
Page: 5
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

-I
ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225907
Client
Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921805842
Project Sample
Number: 9225907-004
Date Collected: 09/06/01 16:30
Client Sample ID: WSP-4
Matrix: water
Date
Received: 09/07/01 11:10
Parameters
Results
units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reeq
Limit
o-xylene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
95-47-6
Bromoform
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
79-34-5
1,3-Dichlorobenzene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
541-73-1
1,2-Dichlorobenzene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
95-50-1
Dibromofluoromethane (S)
102
%
1.0
09/19/01
09:43
RPJ
Toluene-d8 (S)
4-Bromofluorobenzene (S)
98
98
%
%
1.0
1.0
09/19/01
09/19/01
09:43
09:43
RPJ
RPJ
2037-26-5
460-00-4
1,2-Dibromoethane
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
106-93-4
Naphthalene
1,3,5-Trimethylbenzene
ND
ND
ug/l
ug/l
5.0
5.0
1.0
1.0
09/19/01
09/19/01
09:43
09:43
RPJ
RPJ
91-20-3
108-67-8
1,2,4-Trimethylbenzene
ND
ug/l
5.0
1.0
09/19/01
09:43
RPJ
95-63-6
Date: 09/24/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Page: 6
REPORT W LABORATORY ANALYSIS Laboratory Certification IN
KY Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

f
I
ace Analyticaf"
www.pacelabs.com
s
PASI Inc. Charlotte
9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
Attn: Project Management
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax.' 828.254.4618
Lab Project Number: 9323313
Client Project ID: IT-9225907
°.ab Sample No: 921805842 Project Sample Number: 9323313-001
;Bent Sample ID: WSP-4 Matrix: Water
__Parameters Results Units Report Limit Analyzed
Jet Chemistry
_ Total Kjeldahl Nitrogen Prep/Method: EPA 351.2 / EPA 351.2
Nitrogen, Kjeldaht, Total ND mg/L 0.10 09/18/01
_ Date: 09/19/01
boratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Date Collected: 09/06/01 16:30
Date Received: 09/07/01 11:10
CAS No. Ftnote Reg Limit
JDA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
h`o M •CCOIpI
uoV z
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 9903G

ace Analy�ical lj"
vrvnv. pacelabs coin
Pace Analytical Services, Inc.
9800 Kincey Avenue
Suite 100
Huntersville, NC 28078
Attn: Client Service
Phone: [phone]
Lab Sample No: 921805859
Client Sample ID: ASP-2 (#90)
Pace Analytical Services, Inc.
1700 Elm Street, Suite 200
Minneapolis, MN 55414
Phone: [phone]
fax [phone]
Lab Project Number: 1048773
Client Project ID: 9225907 IT
Project Sample Number: 1048773-001 Date Collected: 09/06/01 16:30
Matrix: Air Date Received: 09/07/01 11:10
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Rea Limit
Air
GC/MS VOCs, in Air
Prep/Method:
TO-14 Ambient
Air /
TO-14 Ambient
Air
Vinyl chloride
ND
ppbv
4.9
09/20/01
13:19
MTG
75-01-4
Methylene chloride
ND
ppbv
4.9
09/20/01
13:19
MTG
75-09-2
cis-1,2-Dichloroethene
93.
ppbv
4.7
09/20/01
13:19
MTG
156-59-2
Chloroform
ND
ppbv
4.7
09/20/01
13:19
MTG
67-66-3
Benzene
80.
ppbv
4.2
09/20/01
13:19
MTG
71-43-2 1
Carbon tetrachloride
ND
ppbv
4.1
09/20/01
13:19
MTG
56-23-5
Trichloroethene
200
ppbv
40.
09/20/01
13:19
MTG
79-01-6
Tetrachloroethene
23000
ppbv
750
09/20/01
13:19
MTG
127-18-4
THC as Gas
3000
ppbv
190
09/20/01
13:19
MTG
Lab Sample No: 921805867
Project
Sample Number: 1048773-002
Date Collected: 09/06/bl 16:30
Client Sample ID: ASP-3 (#294)
Matrix: Air
Date Received: 09/07/01 11:10
Parameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Rea Limit
Air
GC/MS VOCs, in Air
Prep/Method: TO-14 Ambient Air / TO-14
Ambient
Air
Vinyl chloride
ND
ppbv
0.69
09/20/01
14:34
MTG
75-01-4
Methylene chloride
ND
ppbv
0.69
09/20/01
14:34
MTG
75-09-2
cis-1,2-Dichloroethene
ND
ppbv
0.66
09/20/01
14:34
MTG
156-59-2
Chloroform
ND
ppbv
0.66
09/20/01
14:34
MTG
67-66-3
Benzene
7.3
ppbv
0.59
09/20/01
14:34
MTG
71-43-2 1
Carbon tetrachloride
ND
ppbv
0.58
09/20/01
14:34
MTG
56-23-5
Trichloroethene
ND
ppbv
0.57
09/20/01
14:34
MTG
79-01-6
Tetrachloroethene
5.0
ppbv
0.66
09/20/01
14:34
MTG
127-18-4
THC as Gas
160
ppbv
28.
09/20/01
14:34
MTG
Date: 09/21/01 P6Qe: 1
¢o\��o IN A0009� REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.

acerr, talytical "
www.pacelaDs.com
. AA..- ''t _ U; _ _V'. , An , tic... 3e%p.,asi )cI nL
The Chain-(, itody is a LEGAL DOCUMENT. All relevant fields must be completed tccura.
Required Client Information: Section B ,-j /I , J 1
Required Client Information: Section A
Report To:
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Page: 17 of
To Be Completed by Pace Analytical
Ouote Reference:
and
Client
Sectic Il C
Company . r
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Copy To: �
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Client Information Check quote/contract):
Address
Invoice To:
Request Date
'TAT.
Project Manager:
P.O.
* Turn Cround mes; less than 14 days subject to
Project
laboratory and contractual obligations and may result in a
Rush Turnaround Surcharge.
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Project Number. ' r
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Requested
Analysis:
2"
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/
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Section D Required Client Information:
valid Matrix Codes
MATRIX CODE
WATER Wr
0
W
w
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Preservatives
d
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SAMPLE ID
One character per box.
soft sL
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mm / dd / yy
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Additional Comments:
Pace Project No.:
SAMPLE CONDITION
Temp:
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Received on Ice: atN
Sealed Cooler: Y(Cfj,
Samples Intact: N
pH
ORl(;It`jAl CIF-1- nr-trrnnr r+rrnr -- ..T...•.

i
I �
aceAnalyticafm
www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Keith Ogden
Phone: [phone] x224
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225358.001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution_
Analyzed
CAS No. Ftnote Reg Limit
Metals
Metals by Trace ICP
Prep/Method:
EPA 3010 /
EPA 6010
Aluminum
2.2
mg/l
0.10
1.0
08/22/01
17:25
RWF
7429.90.5
Antimony
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-36-0
Arsenic
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-38-2
Barium
0.064
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-39-3
Beryllium
ND
mg/l
0.0010
1.0
08/22/01
17:25
RWF
7440-41-7
Boron
ND
mg/l
0.010
1.0
08/22/01
17:25
RWF
7440.42.8
Cadmium
ND
mg/l
0.0010
1.0
08/22/01
17:25
RWF
7440-43-9
Calcium
6.2
mg/l
0.10
1.0
08/22/01
17:25
RWF
7440-70-2
Chromium
0.0067
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440-47-3
Cobalt
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-48-4
Copper
0.33
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440-50-8
Iron
5.4
mg/l
0.050
1.0
08/22/01
17:25
RWF
7439-89-6
Lead
0.051
mg/l
0.0030
1.0
08/22/01
17:25
RWF
7439-92-1
Magnesium
3.7
mg/l
0.10
1.0
08/22/01
17:25
RWF
7439-95-4
Manganese
0.14
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7439-96-5
Molybdenum
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7439-98-7
Nickel
0.0088
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-02-0
Potassium
ND
mg/l
1.0
1.0
08/22/01
17:25
RWF
7440-09-7
Selenium
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7782-49-2
Silicon
15.
mg/l
0:30
1.0
08/22/01
17:25
RWF
7440-21-3
Silver
ND
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440-22.4
Sodium
3.6
mg/l
1.0
1.0
08/22/01
17:25
RWF
7440-23-5
Strontium
0.078
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-24-6
Thallium
ND
mg/l
0.010
1.0
08/22/01
17:25
RWF
7440.28-0
Tin
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-31-5
Titanium
0.12
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-32-6
Vanadium
0.0094
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-62-2
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i
I I
ace Analytical'
www.pacelabs.com
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received:.08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Zinc
1.4
mg/1
0.010
1.0
08/22/01
17:25
RWF
7440-66-6
Date Digested
08/21/01
Wet Chemistry
Total Dissolved Solids
Prep/Method:
EPA 160.1
/ EPA 160.1
Total Dissolved Solids
56.
mg/l
10.
1.0
08/17/01
COE
Total Suspended Solids
Prep/Method:
EPA 160.2
/ EPA 160.2
Total Suspended Solids
10.
mg/l
1.0
1.0
08/17/01
CDE
Cyanide. Total, Water
Prep/Method:
EPA 335.3
/ EPA 335.3
Cyanide
NO
mg/l
0.0020
1.0
08/24/01
DJR
57-12-5
Ammonia
Prep/Method:
EPA 350.1
/ EPA 350.1
Nitrogen, Ammonia
NO
mg/l
0.10
1.0
08/21/01
DJR
7727-37-9
,GC/MS Semivolatiles
Semivolatile Organics
Prep/Method:
EPA 3510 /
EPA 8270
Acenaphthene
NO
ug/l
10.
1.0
08/20/01
20:23
83-32-9
Acenaphthylene
NO
ug/l
10.
1.0
08/20/01
20:23
208.96.8
Aniline
NO
ug/l
10.
1.0
08/20/01
20:23
62-53.3
Anthracene
NO
ug/l
10.
1.0
08/20/01
20:23
120.12-7
Benzo(a)anthracene
NO
ug/l
10.
1.0
08/20/01
20:23
56-55-3
Benzo(a)pyrene
ND
ug/l
10.
1.0
08/20/01
20:23
50.32-8
Benzo(b)fluoranthene
ND
ug/l
10.
1.0
08/20/01
20:23
205-99-2
Benzo(g,h,i)perylene
ND
ug/l
10.
1.0
08/20/01
20:23
191.24.2
Benzo(k)fluoranthene
ND
ug/l
10.
1.0
08/20/01
20:23
207.08-9
Benzoic acid
ND
ug/l
52.
1.0
08/20/01
20:23
65-85-0
Benzyl alcohol
NO
ug/l
21.
1.0
08/20/01
20:23
100-51-6
4-Bromophenylphenyl ether
NO
ug/l
10.
1.0
08/20/01
20:23
101-55.3
Butylbenzylphthalate
NO
ug/1
10.
1.0
08/20/01
20:23
85-68-7
4-Chloro-3,-methylphenol
NO
ug/l
21.
1.0
08/20/01
20:23
59-50-7
4-Chloroaniline
NO
ug/1
21.
1.0
08/20/01
20:23
106.47-8
bis(2-Chloroethoxy)methane
NO
ug/l
10.
1.0
08/20/01
20:23
111.91-1
bis(2-Chloroethyl) ether
NO
ug/1
10.
1.0
08/20/01
20:23
111-44-4
bis(2-Chloroisopropyl) ether
NO
ug/1
10.
1.0
08/20/01
20:23
39638-32-9
2-Chloronaphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-58-7
Date: 08/27/01
Page: 2
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

ace Analytical r"
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767638 Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
2-Chlorophenol
ND
ug/l
10.
1.0
08/20/01
20:23
95.57-8
4-Chlorophenylphenyl ether
NO
ug/l
10.
1.0
08/20/01
20:23
7005.72-3
Chrysene
NO
ug/l
10.
1.0
08/20/01
20:23
218-01-9
Dibenz(a.h)anthracene
NO
ug/l
10.
1.0
08/20/01
20:23
53-70-3
Dibenzofuran
NO
ug/l
10.
1.0
08/20/01
20:23
132-64-9
1,2-Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
95-50-1
i Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
541-73-1
1.4-Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
106-46-7
3.3'-Dichlorobenzidine
NO
ug/l
21.
1.0
08/20/01
20:23
91.94-1
2,4-Dichlorophenol
NO
ug/l
10.
1.0
08/20/01
20:23
120-83-2
Diethylphthalate
ND
ug/l
10.
1.0
08/20/01
20:23
84-66-2
2.4-Dimethylphenol
NO
ug/l
10.
1.0
08/20/01
20:23
105-67-9
Dimethylphthalate
ND
ug/l
10.
1.0
08/20/01
20:23
131-11-3
Di-n-butylphthalate
ND
ug/l
10.
1.0
08/20/01
20:23
84-74-2
4.6-Dinitro-2-methylphenol
ND
ug/l
52.
1.0
08/20/01
20:23
534-52-1
2.4-Dinitrophenol
NO
ug/l
52.
1.0
08/20/01
20:23
51-28-5
2.4-Dinitrotoluene
NO
ug/l
10.
1.0
08/20/01
20:23
121-14-2
2,6-Dinitrotoluene
NO
ug/l
10.
1.0
08/20/01
20:23
606-20.2
Di-n-octylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
117-84-0
1.2-Diphenylhydrazine
ND
ug/l
21.
1.0
08/20/01
20:23
122-66-7
bis(2-Ethylhexyl)phthalate
63.
ug/l
10.
1.0
08/20/01
20:23
117-81-7
Fluoranthene
NO
ug/l
10.
1.0
08/20/01
20:23
206.44-0
Fluorene
NO
ug/l
10.
1.0
08/20/01
20:23
86-73-7
Hexachloro-1.3-butadiene
NO
ug/l
10.
1.0
08/20/01
20:23
87-68-3
Hexachlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
118-74-1
Hexachlorocyclopentadiene
NO
ug/l
10.
1.0
08/20/01
20:23
77-47-4
Hexachloroethane
ND
ug/l
10.
1.0
08/20/01
20:23
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/l
10.
1.0
08/20/01
20:23
193.39-5
Isophorone
ND
ug/l
10.
1.0
08/20/01
20:23
78-59-1
2-Methylnaphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-57-6
2-Methylphenol (o-Cresol)
ND
ug/1
10.
1.0
08/20/01
20:23
95-48-7
3&4-Methylphenol
NO
ug/l
10.
1.0
08/20/01
20:23
Naphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-20-3
2-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
88-74-4
3-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
99-09-2
4-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
100-01-6
Nitrobenzene
ND
ug/l
10.
1.0
08/20/01
20:23
98.95-3
Date: 08/27/01 Page: 3
Laboratory Certification IDs
i NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i
ace Analytical r'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey A venue, Suite 100
Nuntersville. NC 28078
Phone. [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767638 Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
2-Nitrophenol
ND
4-Nitrophenol
ND
N-Nitrosodimethylamine
ND
N-Nitroso-di-n-propylamine
ND
N-Nitrosodiphenylamine
ND
Pentachlorophenol
ND
Phenanthrene
ND
Phenol
ND
Pyrene
ND
1.2.4-Trichlorobenzene
ND
2,4.5-Trichlorophenol
ND
2.4,6-Trichlorophenol
ND
Nitrobenzene-d5 (S)
54
2-Fluorobiphenyl (S)
51
Terphenyl-d14 (S)
56
Phenol-d6 (S)
19
2-Fluorophenol (S)
31
2.4.6-Tribromophenol (S)
66
Date Extracted
GUMS Vol ati l es
GC/MS VOCs by 8260
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Date- 08/27/01
I Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Units
Report Limit
Dilution
Analyzed
CAS No. Ftnote Reg Limit
ug/l
10.
1.0
08/20/01
20:23
88-75-5
ug/l
52.
1.0
08/20/01
20:23
100-02.7
ug/l
10.
1.0
08/20/01
20:23
62-75.9
ug/l
10.
1.0
08/20/01
20:23
621-64-7
ug/l
10.
1.0
08/20/01
20:23
86-30-6
ug/l
52.
1.0
08/20/01
20:23
87.86-5
ug/1
10.
1.0
08/20/01
20:23
85-01-8
ug/1
10.
1.0
08/20/01
20:23
108-95-2
ug/l
10.
1.0
08/20/01
20:23
129-00-0
ug/1
10.
1.0
08/20/01
20:23
120-82.1
ug/l
52.
1.0
08/20/01
20:23
95-95.4
ug/1
10.
1.0
08/20/01
20:23
88-06-2
%
1.0
08/20/01
20:23
4165-60.0
X
1.0
08/20/01
20:23
321-60.8
%
1.0
08/20/01
20:23
1718-51.0
%
1.0
08/20/O1
20:23
13127.88-3
%
1.0
08/20/01
20:23
367-12-4
X
1.0
08/20/01
20:23
08/17/01
Prep/Method: EPA 8260 / EPA 8260
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
10.
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/l
5.0
ND
ug/1
5.0
ND
ug/l
5.0
ND
ug/l
10.
ND
ug/l
5.0
ND
ug/l
10.
1.0 08/18/01 13:38 YLJ 71-43-2
1.0 08/18/01 13:38 YLJ 108.86-1
1.0 08/18/01 13:38 YLJ 74-97-5
1.0 08/18/01 13:38 YLJ 75-27-4
1.0 08/18/01 13:38 YLJ 75-25-2
1.0 08/18/01 13:38 YLJ 74-83-9
1.0 08/18/01 13:38 YLJ 104-51-8
1.0 08/18/01 13:38 YLJ 135.98-8
1.0 08/18/01 13:38 YLJ 98-06-6
1.0 08/18/01 13:38 YLJ 56-23-5
1.0 08/18/01 13:38 YLJ 108.90-7
1.0 08/18/01 13:38 YLJ 75-00-3
1.0 08/18/01 13:38 YLJ 67-66-3
1.0 08/18/01 13:38 YLJ 74-87-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalyticaf"
www.paceiabs.com
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax. [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No.
2-Chlorotoluene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95.49-8
4-Chlorotoluene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-43-4
1.2-Dibromo-3-chloropropane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
96-12-8
Dibromochloromethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
124-48.1
1,2-Dibromoethane (EDB)
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-93.4
Dibromomethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
74-95.3
1.2-Dichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-50.1
1.3-Dichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
541-73-1
1.4-Dichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-46-7
Dichlorodifluoromethane
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-71.8
1.1-Dichloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-34-3
1.2-Dichloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
107-06-2
1.1-Dichloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-35-4
cis-1,2-Dichloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
156-59-2
trans-1.2-Dichloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
156-60-5
1.2-Dichloropropane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
78-87-5
1.3-Dichloropropane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
142-28-9
2.2-Dichloropropane
ND
ug/l
5.0
1.0
08/18/01
13:3B
YLJ
594-20-7
1.1-Dichloropropene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
563-58-6
Diisopropyl ether
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-20-3
Ethylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
100-41-4
Hexachloro-1.3-butadiene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
87-68-3
Isopropylbenzene (Cumene)
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
98-82-8
p-Isopropyltoluene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
99-87-6
Methylene chloride
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-09-2
Methyl-tert-butyl ether
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
1634.04-4
Naphthalene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
91-20.3
n-Propylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
103.65-1
Styrene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
100-42-5
1,1.1,2-Tetrachloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38'
YLJ
630-20-6
1.1.2".2-Tetrachloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
79-34-5
Tetrachloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
127-18.4
Toluene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-88-3
1.2.3-Trichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
87-61-6
1.2,4-Trichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
120-82-1
1,1.1-Trichloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
71-55-6
1.1.2-Trichloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
79-00-5
Date: 08/27/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Ftnote Reg Limit
Page: 5
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

i
aceAnalyticalTM
www.pacelabs.com
t j
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767638
Project Sample
Number: 9225358-001
Date Collected:- 08/14/01 11:55
1 Client Sample ID: EFFLUENT
Matrix: Water
Date
Received: 08/15/01 18:25
— Parameters
Results
Units
Report Limit
Dilution_
Analyzed
CAS No. Ftnote Reg Limit
Trichloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
79-01-6
'— Trichlorofluoromethane
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-69-4
1.2.3-Trichloropropane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
96-18-4
1.2.4-Trimethylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-63.6
1.3.5-Trimethylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-67-8
Vinyl chloride
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-01-4
m&p-Xylene
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
o-Xylene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-47.6
Toluene-d8 (S)
96
%
1.0
08/18/01
13:38
YLJ
2037-26-5
_ 4-Bromofluorobenzene (S)
105
X
1.0
08/18/01
13:38
YLJ
460-00-4
Dibromofluoromethane (S)
91
%
1.0
08/18/01
13:38
YLJ
1.2-Dichloroethane-d4 (S)
88
%
1.0
08/18/01
13:38
YLJ
17060-07-0
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical TM
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone. [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767646 Project Sample Number: 9225358-002 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT DISSOLVED Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Metals
Dissolved Metals. Trace ICP
Prep/Method:
EPA 3010
/ EPA 6010
Aluminum. Dissolved
2.3
mg/l
0.10
1.0
08/22/01
RWF
7429-90-5
Antimony, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7440-36-0
Arsenic, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7440-38-2
Barium, Dissolved
0.063
mg/l
0.0050
1.0
08/22/01
RWF
7440-39-3
Beryllium, Dissolved
NO
mg/l
0.0010
1.0
08/22/01
RWF
7440-41.7
Boron, Dissolved
NO
mg/l
0.010
1.0
08/22/01
RWF
7440-42-8
Cadmium, Dissolved
NO
mg/l
0.0010
1.0
08/22/01
RWF
7440-43-9
Calcium, Dissolved
6.1
mg/1
0.10
1.0
08/22/01
RWF
7440-70-2
Chromium, Dissolved
0.0070
mg/l
0.0020
1.0
08/22/01
RWF
7440-47-3
Cobalt, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7440-48-4
Copper, Dissolved
0.26
mg/l
0.0020
1.0
08/22/01
RWF
7440-50-8
Iron, Dissolved
5.6
mg/l
0.050
1.0
08/22/01
RWF
7439-89.6
Lead, Dissolved
0.042
mg/l
0.0030
1.0
08/22/01
RWF
7439-92-1
Magnesium, Dissolved
4.0
mg/l
0.10
1.0
08/22/01
RWF
7439-95-4
Manganese, Dissolved
0.14
mg/l
0.0050
1.0
08/22/01
RWF
7439-96-5
Molybdenum, Dissolved
ND
mg/l
0.0050
1.0
08/22/01
RWF
7439-98.7
Nickel, Dissolved
0.0083
mg/l
0.0050
1.0
08/22/01
RWF
7440-02-0
Potassium, Dissolved
1.0
mg/l
1.0
1.0
08/22/01
RWF
7440-09.7
Selenium, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7782.49.2
Silicon, Dissolved
16.
mg/l
0.10
1.0
08/22/01
RWF
7440-21-3
Silver, Dissolved
NO
mg/l
0.0020
1.0
08/22/01
RWF
7440-22-4
Sodium, Dissolved
3.9
mg/l
1.0
1.0
08/22/01
RWF
7440-23-5
Strontium, Dissolved
0.076
mg/l
0.0050
1.0
08/22/01
RWF
7440-24-6
Thallium, Dissolved
NO
mg/l
0.010
1.0
08/22/01
RWF
7440-28-0
Tin, Dissolved
ND
mg/l
0.0050
1.0
08/22/01
RWF
7440-31.5
Titanium, Dissolved
0.14
mg/l
0.0050
1.0
08/22/01
RWF
7440-32-6
Vanadium, Dissolved
0.010
mg/l
0.0050
1.0
08/22/01
RWF
7440.62-2
Zinc, Dissolved
0.91
mg/l
0.010
1.0
08/22/01
RWF
7440-66.6
Date Digested
08/21/01
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 7
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

s�
acekialytical
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Required Client Information: Section A
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pli I

ace Analytical "'
www.pacelabs.com
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Charles Bertz
Phone: [phone] x236
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone:[phone]
Fax.' 704.875.9091
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution_ Analyzed
CAS No. Ftnote Reg Limit
Metals
Metals by Trace ICP
Prep/Method:
EPA 3010 /
EPA 6010
Aluminum
2.2
mg/l
0.10
1.0
08/22/01
17:25
RWF
7429-90-5
Antimony
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-36.0
Arsenic
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-38.2
Barium
0.064
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440.39-3
Beryllium
ND
mg/l
0.0010
1.0
08/22/01
17:25
RWF
7440-41-7
Boron
ND
mg/l
0.010
1.0
08/22/01
17:25
RWF
7440-42.8
Cadmium
ND
mg/l
0.0010
1.0
08/22/01
17:25
RWF
7440-43-9
Calcium
6.2
mg/l
0.10
1.0
08/22/01
17:25
RWF
7440-70.2
Chromium
0.0067
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440-47-3
Cobalt
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-48-4
Copper
0.33
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440-50-8
Iron
5.4
mg/l
0.050
1.0
08/22/01
17:25
RWF
7439-89-6
Lead
0.051
mg/l
0.0030
1.0
08/22/01
17:25
RWF
7439.92-1
Magnesium
3.7
mg/l
0.10
1.0
08/22/01
17:25
RWF
7439-95-4
Manganese
0.14
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7439-96-5
Molybdenum
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7439-98-7
Nickel
0.0088
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440.02-0
Potassium
ND
mg/l
1.0
1.0
08/22/01
17:25
RWF
7440-09-7
Selenium
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7782-49-2
Silicon
15.
mg/l
0.10
1.0
08/22/01
17:25
RWF
7440-21-3
Silver
ND
mg/l
0.0020
1.0
08/22/01
17:25
RWF
7440.22.4
Sodium
3.6
mg/l
1.0
1.0
08/22/01
17:25
RWF
7440-23-5
Strontium
0.078
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-24-6
Thallium
ND
mg/l
o.olb
1.0
08/22/01
17:25
RWF
7440.28.0
Tin
ND
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-31-5
Titanium
0.12
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-32-6
Vanadium
0.0094
mg/l
0.0050
1.0
08/22/01
17:25
RWF
7440-62-2
Date: 08/27/01
Laboratory Certification IDs
! NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical "'
www.pacelabs.com
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225358.001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Zinc
1.4
mg/l
0.010
1.0
08/22/01
17:25
RWF
7440.66.6
Date Digested
08/21/01
Wet Chemistry
Total Dissolved Solids
Prep/Method:
EPA 160.1
/ EPA 160.1
Total Dissolved Solids
56.
mg/l
10.
1.0
08/17/01
CDE
Total Suspended Solids
Prep/Method:
EPA 160.2
/ EPA 160.2
Total Suspended Solids
10.
mg/l
1.0
1.0
08/17/01
CDE
Cyanide, Total, Water
Prep/Method:
EPA 335.3
/ EPA 335.3
Cyanide
NO
mg/l
0.0020
1.0
08/24/01
DJR
57.12-5
Ammonia
Prep/Method:
EPA 350.1
/ EPA 350.1
Nitrogen. Ammonia
ND
mg/l
0.10
1.0
08/21/01
DJR
7727.37-9
GUMS Semivolatiles
Semivolatile Organics
Prep/Method:
EPA 3510 /
EPA 8270
Acenaphthene
NO
ug/l
10.
1.0
08/20/01
20:23
83-32-9
Acenaphthylene
NO
ug/l
10.
1.0
08/20/01
20:23
208.96-8
Aniline J
ND
ug/l
10.
1.0
08/20/01
20:23
62-53-3
Anthracene
ND
ug/l
10.
1.0
08/20/01
20:23
120-12-7
Benzo(a)anthracene
-ND
ug/l
10.
1.0
08/20/01
20:23
56-55-3
Benzo(a)pyrene
ND
ug/l
10.
1.0
08/20/01
20:23
50-32.8
Benzo(b)fluoranthene
NO
ug/l
10.
1.0
08/20/01
20:23
205-99-2
Benzo(g.h.i)perylene
NO
ug/l
10.
1.0
08/20/01
20:23
191-24-2
Benzo(b)fluoranthene
NO
ug/l
10.
1.0
08/20/01
20:23
207-08-9
Benzoic acid
NO
ug/l
52.
1.0
08/20/01
20:23
65-85-0
Benzyl alcohol
NO
ug/l
21.
1.0
08/20/01
20:23
100-51.6
4-Bromophenylphenyl ether
NO
ug/l
10.
1.0
08/20/01
20:23
101-55-3
Butylbenzylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
85-68-7
4-Chloro-3-methylphenol
NO
ug/l
21.
1.0
08/20/01
20:23
59-50-7
4-Chloroaniline
NO
ug/l
21.
1.0
08/20/01
20:23
106-47-8
bis(2-Chloroethoxy)methane
NO
ug/l
10.
1.0
06/20/01
20:23
111-91-1
bis(2-Chloroethyl) ether
NO
ug/l
10.
1.0
08/20/01
20:23
111-44-4
bis(2-Chloroisopropyl) ether
NO
ug/l
10.
1.0
08/20/01
20:23
39638-32-9'
2-Chloronaphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-58-7
Date: 08/27/01
Page: 2
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

eacteAnalyficalr"
I' www.pacolabs.com
Lab Sample No: 921767638
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: i O4. d75.9091
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number:- 9225358-001 Date Collected: 08/14/01 11:55
Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution
Analyzed
CAS No. Ftnote Reg Limit
2-Chlorophenol
NO
ug/l
10.
1.0
08/20/01
20:23
95-57-8
+_ 4-Chlorophenylphenyl ether
NO
ug/l
10.
1.0
08/20/01
20:23
7005-72-3
Chrysene
NO
ug/l
10.
1.0
08/20/01
20:23
218-01-9
Dibenz(a,h)anthracene
ND
ug/l
10.
1.0
08/20/01
20:23
53-70-3
Dibenzofuran
NO
ug/l
10.
1.0
08/20/01
20:23
132-64-9
1.2-Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
95-50-1
,- 1.3-Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
541-73-1
1.4-Dichlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
106-46-7
3.3'-Dichlorobenzidine
NO
ug/l
21.
1.0
08/20/01
20:23
91-94-1
_ 2.4-Dichlorophenol
NO
ug/l
10.
1.0
08/20/01
20:23
120.83-2
Diethylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
84-66-2
2.4-Dimethylphenol
NO
ug/l
10.
1.0
08/20/01
20:23
105-67.9
Dimethylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
131-11-3
Di-n-butylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/l
52.
1.0
08/20/01
20:23
534-52-1
2,4-Dinitrophenol
NO
ug/l
52.
1.0
08/20/01
20:23
51-28-5
2,4-Dinitrotoluene
NO
ug/l
10.
1.0
08/20/01
20:23
121-14-2
2.6-Dinitrotoluene
NO
ug/l
10.
1.0
08/20/01
20:23
606-20-2
Di-n-octylphthalate
NO
ug/l
10.
1.0
08/20/01
20:23
117-84-0
1.2-Diphenylhydrazine
NO
ug/l
21.
1.0
08/20/01
20:23
122.66-7
b:,s(2-Ethylhexyl)phthalate
63.
ug/l
10.
1.0
08/20/01
20:23
117-81-7
Fluoranthene
NO
ug/l
10.
1.0
08/20/01
20:23
206-44-0
Fluorene
NO
ug/l
10.
1.0
08/20/01
20:23
86-73-7
Hexachloro-1,3-butadiene
NO
ug/l
10.
1.0
08/20/01
20:23
87-68-3
Hexachlorobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
118.74-1
Hexachlorocyclopentadiene
ND
ug/l
10.
1.0
08/20/01
20:23
77-47-4
Hexachloroethane
NO
ug/l
10.
1.0
08/20/01
20:23
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug/l
10.
1.0
08/20/01
20:23
193-39-5
Isophorone
NO
ug/l
10.
1.0
08/20/01
20:23
78.59-1
2-Methylnaphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-57-6
2-Methylphenol (o-Cresol)
NO
ug/l
10.
1.0
08/20/01
20:23
95-48-7
3&4-Methylphenol
NO
ug/l
10.
1.0
08/20/01
20:23
Naphthalene
NO
ug/l
10.
1.0
08/20/01
20:23
91-20-3
2-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
88.74-4
3-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
99-09-2
-- 4-Nitroaniline
NO
ug/l
52.
1.0
08/20/01
20:23
100.01-6
Nitrobenzene
NO
ug/l
10.
1.0
08/20/01
20:23
98-95-3
Date: 08/27/01 Page: 3
Laboratory Certification IN REPORT 0� LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, ' VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite f00
Analytical... Nuntersville, NC 28078
Phone.' 704.875.9092
www.pacelabs.com Far: 704.875.9091
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767638 Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution_- Analyzed
CAS No. Ftnote Reg Limit
2-Nitrophenol
ND
ug/l
10.
1.0
08/20/01
20:23
88.75-5
4-Nitrophenol
ND
ug/l
52.
1.0
08/20/01
20:23
100.02.7
N-Nitrosodipethylamine
ND
ug/l
10.
1.0
08/20/01
20:23
62-75-9
N-Nitroso-di-n-proPylamine
ND
ug/l
10.
1.0
08/20/01
20:23
621-64-7
N-Nitrosodiphenylamine
ND
ug/l
10.
1.0
08/20/01
20:23
86-30.6
Pentachlorophenol
ND
ug/l
52.
1.0
08/20/01
20:23
87.86-5
--, Phenanthrene
ND
ug/l
10.
1.0
08/20/01
20:23
85-01-8
Phenol
ND
ug/l
10.
1.0
08/20/01
20:23
108-95-2
- Pyrene
ND
ug/l
10.
1.0
08/20/01
20:23
129.00.0
1,2.4-Trichlorobenzene
ND
ug/l
10.
1.0
08/20/01
20:23
120-82-1
2,4.5-Trichlorophenol
ND
ug/l
52.
1.0
08/20/01
20:23
95-95-4
2.4.6-Trichlorophenol
ND
ug/l
10.
1.0
08/20/01
20:23
88-06-2
Nitrobenzene-d5 (S)
54
Y.
1.0
08/20/01
20:23
4165-60-0
2-Fluorobiphenyl (S)
51
%
1.0
08/20/01
20:23
321.60-8
Terphenyl-d14 (S)
56
%
1.0
08/20/01
20:23
1718-51-0
Phenol-d6 (S)
19
%
1.0
08/20/01
20:23
13127-88-3
2-Fluorophenol (S)
31
%
1.0
08/20/01
20:23
367-12-4
2,4.6-Tribromophenol (S)
66
1.0
08/20/01
20:23
Date Extracted
08/17/01
GUMS Vol ati l es
GC/MS VDCs by 8260
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
71-43-2
Bromobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-86-1
Bromochloromethane
ND
ug/1
5.0
1.0
08/18/01
13:38
YLJ
74.97-5
Bromodichloromethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-27-4
Bromoform
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-25-2
Bromomethane
ND
ug/l
10.
1.0
.08/18/01
13:38
YLJ
74-83-9
n-Butylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
104-51-8
sec-Butylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
135-98-8
tert-Butylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
98-06-6
Carbon tetrachloride
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
56-23-5
- Chlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-90-7
Chloroethane
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-00.3
Chloroform
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
67-66-3
Chloromethane
ND
ug/l
10.
1.0
08/18/01
13:38
YLJ
74-87-3
Date: 08/27/01
Laboratorf Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc ' 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

Pace Analytical Services, Inc.
,,,
� Al l�7 al �%ficaI
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
J'
www.pacelabs.com
Phone. [phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767638 Project Sample Number: 9225358-001 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Rea Limit
2-Chlorotoluene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-49-8
4-Chlorotoluene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
96-12-8
Dibromochloromethane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
124-48-1
1,2-Dibromoethane (EDB)
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-93-4
Dibromomethane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
74-95-3
1.2-Dichlorobenzene
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
95-50-1
1,3-Dichlorobenzene
ND
ug/1
5.0
1.0
08/18/01
13:38
YLJ
541-73-1
1,4-Dichlorobenzene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
106-46-7
Dichlorodifluoromethane
NO
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-71-8
1,1-Dichloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75.34-3
1,2-Dichloroethane
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
107-06-2
1,1-Dichloroethene
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
75-35-4
cis-1.2-Dichloroethene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
156-59-2
trans-1.2-Dichloroethene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
156-60-5
1,2-Dichloropropane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
78-87-5
1,3-Dichloropropane
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
142-28-9
2,2-Dichloropropane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
594-20-7
1.1-Dichloropropene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
563-58-6
Diisopropyl ether
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-20-3
Ethylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
100-41-4
Hexachloro-1.3-butadiene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
87.68-3
Isopropylbenzene (Cumene)
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
98-82-8
p-Isopropyltoluene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
99-87-6
Methylene chloride
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
75-09-2
Methyl-tert-butyl ether
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
1634-04-4
Naphthalene
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
91-20-3
n-Propylbenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
103-65-1
Styrene
NO
ug/1
5.0
1.0
08/18/01
13:38
YLJ
100-42-5
1.1,1,2-Tetrachloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
79-34-5
Tetrachloroethene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
127-18-4
Toluene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
108-88-3
1,2.3-Trichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
87.61.6
1,2.4-Trichlorobenzene
ND
ug/l
5.0
1.0
08/18/01
13:38
YLJ
120-82-1
1,1,1-Trichloroethane
NO
ug/l
5.0
1.0
08/18/01
13:38
YLJ
71-55-6
1,1.2-Trichloroethane
ND
ug/l
5.0
1:0
08/18/01
13:38
YLJ
79-00-5
Date: 08/27/01 Page: 5
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IN
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aceAnalytical'M
www.paceiabs.com
Lab Sample No: 921767638
i� Client Sample ID: EFFLUENT
Parameters
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2.4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Toluene-d8 (S)
4-Bromofluorobenzene (S)
i
Dibromofluoromethane (S)
1,2-Dichloroethane-d4,(S)
Date: 08/27/01
Laboratory Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Results
NO
ND
ND
ND
ND
NO
NO
NO
96
105
91
88
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225358
Client
Project
ID: SLS-Greensboro/010305/107535
Project Sample
Number: 9225358-001
Date Collected: 08/14/01 11:55
Matrix: Water
Date
Received: 08/15/01 18:25
_ Units
Report Limit
Dilution -Analyzed
CAS No. Ftnote Reg Limit
ug/l
5.0
1.0
08/18/01
13:38
YLJ
79-01.6
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-69-4
ug/l
5.0
1.0
08/18/01
13:38
YLJ
96-18-4
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-63-6
ug/l
5.0
1.0-
08/18/01
13:38
YLJ
108.67-8
ug/l
10.
1.0
08/18/01
13:38
YLJ
75-01-4
ug/l
10.
1.0
08/18/01
13:38
YLJ
ug/l
5.0
1.0
08/18/01
13:38
YLJ
95-47.6
%
1.0
08/18/01
13:38
YLJ
2037-26-5
1.0
08/18/01
13:38
YLJ
460-00-4
X
1.0
08/18/01
13:38
YLJ
Y,
1.0
08/18/01
13:38
YLJ
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical "
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 9225358
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921767646 Project Sample Number: 9225358-002 Date Collected: 08/14/01 11:55
Client Sample ID: EFFLUENT DISSOLVED Matrix: Water Date Received: 08/15/01 18:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Metals
Dissolved Metals, Trace ICP
Prep/Method:
EPA 3010 /
EPA 6010
Aluminum, Dissolved
2.3
mg/l
0.10
1.0
08/22/01
RWF
7429-90-5
Antimony, Dissolved
NO
mg/1
0.0050
1.0
08/22/01
RWF
7440-36-0
Arsenic, Dissolved
NO
mg/1
0.0050
1.0
08/22/01
RWF
7440-38-2
Barium. Dissolved
0.063
mg/l
0.0050
1.0
08/22/01
RWF
7440.39.3 .
Beryllium. Dissolved
NO
mg/l
0.0010
1.0
08/22/01
RWF
7440-41-7
Boron, Dissolved
NO
mg/l
0.010
1.0
08/22/01
RWF
7440-42-8
Cadmium. Dissolved
NO
mg/l
0.0010
1.0
08/22/01
RWF
7440-43-9
Calcium, Dissolved
6.1
mg/l
0.10
1.0
08/22/01
RWF
7440-70-2
Chromium. Dissolved
0.0070
mg/l
0.0020
1.0
08/22/01
RWF
7440-47-3
Cobalt, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7440.48-4
Copper. Dissolved
0.26
mg/1
0.0020
1.0
08/22/01
RWF
7440.50-8
Iron. Dissolved
5.6
mg/l
0.050
1.0
08/22/01
RWF
7439-89-6
Lead, Dissolved
0.042
mg/l
0.0030
1.0
08/22/01
RWF
7439-92-1
Magnesium, Dissolved
4.0
mg/l
0.10
1.0
08/22/01
RWF
7439-95-4
Manganese, Dissolved
0.14
mg/l
0.0050
1.0
08/22/01
RWF
7439.96.5
Molybdenum, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7439.98.7
Nickel, Dissolved
0.0083
mg/l
0.0050
1.0
08/22/01
RWF
7440-02-0
Potassium, Dissolved
1.0
mg/l
1.0
1.0
08/22/01
RWF
7440-09-7
Selenium, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7782-49-2
Silicon, Dissolved
16.,
mg/l
0.10
1.0
08/22/01
RWF
7440.21-3
Silver. Dissolved
ND
mg/l
0.0020
1.0
08/22/01
RWF
7440-22-4
Sodium, Dissolved
3.9
mg/l
1.0
1.0
08/22/01
RWF
7440-23-5
Strontium. Dissolved
0.076
mg/1
0.0050
1.0
08/22/01
RWF
7440-24-6
Thallium, Dissolved
NO
mg/1
0.010
1.0
08/22/01
RWF
7440-28-0
Tin, Dissolved
ND
mg/l
0.0050
1.0
08/22/01
RWF
7440.31-5
Titanium. Dissolved
0.14
mg/l
0.0050
1.0
08/22/01
RWF
7440-32-6
Vanadium, Dissolved
0.010
mg/l
0.0050
1.0
08/22/01
RWF
7440-62-2
Zinc, Dissolved
0.91
mg/l
0.010
1.0
08/22/01
RWF
7440-66-6
Date Digested
08/21/01
Date: 08/27/01
Page: 7
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MATRIX CODE W W V
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ace Analytical "'
www.pacelabs.com
1
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville. NC 27560
Attn: Mr. Charles Bertz
Phone: [phone] x236
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax.- 704.875.9091
Lab Project Number: 9225400
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921770178
Project Sample
Number: 9225400-001
Date Collected: 08/17/01 10:30
Client Sample ID: EFFLUENT
Matrix: Water
Date
Received: 08/17/01 13:35
Parameters
Results
Units
Report Limit
Dilution
Analyzed
CAS No. Ftnote Reg Limit
Metals
;- Metals by Trace ICP
Prep/Method:
EPA 3010 /
EPA 6010
Aluminum
2.9
mg/1
0.10
1.0
08/22/01
18:12
RWF
7429-90-5
__? Antimony
ND
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7440-36-0
Arsenic
ND
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7440-38-2
'! Barium
0.087
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7440-39-3
Beryllium
ND
mg/1
0.0010
1.0
08%22/01
18:12
RWF
7440-41-7
Boron
ND
mg/1
0.010
1.0
08/22/01
18:12
RWF
7440-42-8
Cadmium
ND
mg/l
0.0010
1.0
08/22/01
18:12
RWF
7440-43-9
Calcium
6.9
mg/l
0.10
1.0
08/22/01
18:12
RWF
7440.70-2
Chromium
0.0070
mg/l
0.0020
1.0
08/22/01
18:12
RWF
7440-47-3
Cobalt
ND
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7440-48-4
Copper
0.0042
mg/l
0.0020
1.0
08/22/01
18:12
RWF
7440-50-8
Iron
5.4
mg/l
0.050
1.0
08/22/01
18:12
RWF
7439-89.6
Lead
ND
mg/l
0.0030
1.0
08/22/01
18:12
RWF
7439-92-1
Magnesium
4.7
mg/l
0.10
1.0
08/22/01
18:12
RWF
7439-95-4
Manganese
0.11
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7439.96-5
Molybdenum
ND
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7439.98-7
Nickel
0.0057
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7440-02-0
' Potassium
1.6
mg/1
1.0
1.0
08/22/01
18:12
RWF
7440-09-7
-' Selenium
ND
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7782-49-2
Silicon
18.
mg/l
0.10
1.0
08/22/01
18:12
RWF
7440-21-3
Silver
ND
mg/l
0.0020
1.0
08/22/01
18:12
RWF
7440-22-4
Sodium
3.3
mg/l
1.0
1.0
08/22/01
18:12
RWF
7440-23-5
Strontium
0.078
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7440-24-6
Thallium
ND
mg/l
0.010
1.0
08/22/01
18:12
RWF
7440-28-0
Tin
ND
mg/1
0.0050
1.0
08/22/01
18:12
RWF
7440-31-5
Titanium
0.24
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7440-32-6
Vanadium
I i
0.013
mg/l
0.0050
1.0
08/22/01
18:12
RWF
7440-62-2
Date: 08/27/01
;Laboratory Certification IDs
MC Wastewater 12
NC Drinking Water 37706
Sc 99006
i
I '
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalyical
www.pacelabs.com
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921770178 Project Sample Number: 9225400-001 Date Collected: 08/17/01 10:30
Client Sample ID: EFFLUENT Matrix: Water Date Received: 08/17/01 13:35
Parameters
Results
Units
Report Limit
Dilution_ Analyzed
CAS No.
i Zinc
0.030
mg/l
0.010
1.0
08/22/01
18:12
RWF
7440-66.6
Date Digested
08/21/01
Wet Chemistry
Total Dissolved Solids
Prep/Method:
EPA 160.1
/ EPA 160.1
Total Dissolved Solids
44.
mg/l
10.
1.0
08/23/01
YMH
Total Suspended Solids
Prep/Method:
EPA 160.2
/ EPA 160.2
Total Suspended Solids
100
mg/l
4.0
4.0
08/21/01
CDE
Cyanide. Total. Water
Prep/Method:
EPA 335.3
/ EPA 335.3
- Cyanide
ND
mg/l
0.0020
1.0
08/24/01
DJR
57-12-5
Ammonia
Prep/Method:
EPA 350.1
/ EPA 350.1
Nitrogen, Ammonia
NO
mg/l
0.10
1.0
08/21/01
DJR
7727-37-9
GUMS Semivolatiles
Semivolatile Organics
Prep/Method:
EPA 3510 /
EPA 8270
Acenaphthene
ND
ug/l
10.
1.0
08/20/01
12:28
83.32-9
Acenaphthylene
NO
ug/l
10.
1.0
08/20/01
12:28
208-96-8
Aniline
ND
ug/l
10.
1.0
08/20/01
12:28
62-53.3
-' Anthracene
ND
ug/l
10.
1.0
08/20/01
12:28
120-12-7
Benzo(a)anthracene
NO
ug/l
10.
1.0
08/20/01
12:28
56-55-3
Benzo(a)pyrene
ND
ug/l
10.
1.0
08/20/01
12:28
50-32-8
Benzo(b)fluoranthene
NO
ug/l
10.
1.0
08/20/01
12:28
205-99-2
Benzo(g.h.i)perylene
NO
ug/1
10.
1.0
08/20/01
12:28
191-24-2
Benzo(k)fluoranthene
ND
ug/l
10.
1.0
08/20/01
12:28
207-08-9
Benzoic acid
NO
ug/1
50.
1.0
08/20/01
12:28
65-85-0
Benzyl alcohol
ND
ug/1
20.
1.0
08/20/01
12:28
100-51-6
4-13romophenylphenyl ether
NO
ug/l
10.
1.0
08/20/01
12:28
101-55-3
Butylbenzylphthalate
NO
ug/l
10.
1.0
08/20/01
12:28
85-68-7
4-Chloro-3-methylphenol
ND
ug/l
20.
1.0
08/20/01
12:28
59-50-7
4-Chloroaniline
NO
ug/l
20.
1.0
08/20/01
12:28
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/l
10.
1.0
08/20/01
12:28
111-91-1
bis(2--Chloroethyl) ether
NO
ug/l
10.
1.0
08/20/01
12:28
111-44-4
bis(2-Chloroisopropyl) ether
NO
ug/l
10.
1.0
08/20/01
12:28
39638-32-9
2-Chloronaphthalene
ND
ug/l
10.
1.0
08/20/01
12:28
91-58-7
Date: 08/27/01
Ftnote Rea Limit
Page: 2
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
- SC 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

i
ace Analytical v
www.pacelabs.com
Lab Sample No: 921770178
Client Sample ID: EFFLUENT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID: SLS- Greens boro/010305/107535
Project Sample Number: 9225400-001 Date Collected,: 08/17/01 10:30
Matrix: Water Date Received: 08/17/01 13:35
Parameters
Results
Units
2-Chlorophenol
ND
ug/l
4-Chlorophenylphenyl ether
ND
ug/l
Chrysene
ND
ug/l
Dibenz(a.h)-anthracene
ND
ug/l
Dibenzofuran
ND
ug/l
1,2-Dichlorobenzene
ND
ug/1
1.3-Dichlorobenzene
ND
ug/l
1.4-Dichlorobenzene
ND
ug/l
3.3'-Dichlorobenzidine
ND
ug/l
2.4-Dichlorophenol
ND
ug/l
Diethylphthalate
ND
ug/l
2.4-Dimethylphenol
ND
ug/l
Dimethylphthalate
ND
ug/l
Di-n-butylphthalate
ND
ug/l
4,6-Dinitro-2-methylphenol
ND
ug/l
2.4-Dinitrophenol
ND
ug/l
2.4-Dinitrotoluene
ND
ug/1
2.6-Dinitrotoluene
ND
ug/l
Di-n-octylphthalate
ND
ug/l
1,2-Diphenylhydrazine
ND
ug/l
bis(2-Ethylhexyl)phthalate
76.
ug/l
Fluoranthene
ND
ug/l
Fluorene
ND
ug/l
Hexachloro-1,3-butadiene
ND
ug/l
Hexachlorobenzene
ND
ug/l
Hexachlorocyclopentadiene
ND
ug/l
Hexachloroethane
ND
ug/l
Indeno(1.2.3-cd)pyrene
ND
ug/l
Isophorone
ND
ug/l
2-Methylnaphthalene
ND
ug/1
2-Methylphenol (o-Cresol)
ND
ug/l
3&4-Methylphenol
ND
ug/1
Naphthalene
ND
ug/1
2-Nitroaniline
ND
ug/l
3-Nitroaniline
ND
ug/l
4-Nitroaniline
ND
ug/l
Nitrobenzene
ND
ug/l
Date: 08/27/01
Laboratory Certification IDs
INC Wastewater 12
NC Drinking Water 37706
-_,SC 99006
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
10.
1.0
08/20/01
12:28
95.57.8
10.
1.0
08/20/01
12:28
7005-72-3
10.
1.0
08/20/01
12:28
218-01-9
10.
1.0
08/20/01
12:28
53-70-3
10.
1.0
08/20/01
12:28
132-64-9
10.
1.0
08/20/01
12:28
95.50-1
10.
1.0
08/20/01
12:28
541-73-1
10.
1.0
08/20/01
12:28
106-46-7
20.
1.0
08/20/01
12:28
91.94-1
10.
1.0
08/20/01
12:28
120.83-2
10.
1.0
08/20/01
12:28
84-66-2
10.
1.0
08/20/01
12:28
105.67-9
10.
1.0
08/20/01
12:28
131-11-3
10.
1.0
08/20/01
12:28
84-74.2
50.
1.0
08/20/01
12:28
534.52-1
50.
1.0
08/20/01
12:28
51.28-5
10.
1.0
08/20/01
12:28
121-14-2
10.
1.0
08/20/01
12:28
606-20-2
10.
1.0
08/20/01
12:28
117-84-0
20.
1.0
08/20/01
12:28
122-66-7
10.
1.0
08/20/01
12:28
117-81-7
10.
1.0
08/20/01
12:28
206-44-0
10.
1.0
08/20/01
12:28
86-73-7
10.
1.0
08/20/01
12:28
87-68-3
10.
1.0
08/20/01
12:28
118-74-1
10.
1.0
08/20/01
12:28
77-47-4
10.
1.0
08/20/01
12:28
67-72.1
10.
1.0
08/20/01
12:28
193-39-5
10.
1.0
08/20/01
12:28
78.59-1
10.
1.0
08/20/01
12:28
91-57.6
10.
1.0
08/20/01
12:28
95-48-7
10.
1.0
08/20/01
12:28
10.
1.0
08/20/01
12:28
91-20-3
50.
1.0
08/20/01
12:28
88.74-4
50.
1.0
08/20/01
12:28
99-09-2
50.
1.0
08/20/01
12:28
100-01-6
10.
1.0
08/20/01
12:28
98-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page: 3
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical '
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, IJC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921770178
Project
Sample
Number:
9225400-001
Date Collected: 08/17/01 10:30
Client Sample ID: EFFLUENT
Matrix:
Water
Date
Received: 08/17/01 13:35
Parameters
Results
Units
Report Limit Dilution
Analyzed
CAS No. Ftnote Rea Limit
2-Nitrophenol
NO
ug/l
10.
1.0
08/20/01
12:28
88-75-5
4-Nitrophenol
NO
ug/l
50.
1.0
08/20/01
12:28
100-02.7
. N-Nitrosodimethylamine
NO
ug/l
10.
1.0
08/20/01
12:28
62-75.9
N-Nitroso-di-n-propylamine
NO
ug/l
10.
1.0
08/20/01
12:28
621-64-7
_ N-Nitrosodiphenylamine
NO,
ug/l
10.
1.0
08/20/01
12:28
86-30-6
Pentachlorophenol
NO
ug/l
50.
1.0
08/20/01
12:28
87-86-5
Phenanthrene
NO
ug/l
10.
1.0
08/20/01-12:28
85-01-8
Phenol
NO
ug/l
10.
1.0
08/20/01
12:28
108-95-2
Pyrene
NO
ug/l
10.
1.0
08/20/01
12:28
129-00-0
1.2.4-Trichlorobenzene
NO
ug/l
10.
1.0
08/20/01
12:28
120-82.1
2.4,5-Trichlorophenol
NO
ug/l
50.
1.0
08/20/01
12:28
95-95-4
2,4,6-Trichlorophenol
NO
ug/l
10.
1.0
08/20/01
12:28
88.06-2
Nitrobenzene-d5 (S)
60
X
1.0
08/20/01
12:28
4165-60-0
2-Fluorobiphenyl (S)
59
%
1.0
08/20/01
12:28
321-60-8
Terphenyl-d14 (S)
64
X
1.0
08/20/01
12:28
1718-51-0
Phenol-d6 (S)
17
X
1.0
08/20/01
12:28
13127-88.3
2-Fluorophenol (S)
30
Y,
1.0
08/20/01
12:28
367-12-4
2,4.6-Tribromophenol (S)
70
X
1.0
08/20/01
12:28
Date Extracted
08/19/01
I
GUMS Vol ati l es
GC/MS VOCs by 8260
Prep/Method:
EPA 8260 /
EPA 8260
Benzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
71-43-2
! Bromobenzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
108-86-1
Bromochloromethane
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
74-97-5
Bromodichloromethane
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
75.27-4
Bromoform
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
75-25.2
Bromomethane
NO
ug/1
10.
1.0
08/21/01
09:15
RWS
74-83.9
n-Butylbenzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
104-51-8
sec-Butylbenzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
135-98-8
tert-Butylbenzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
98-06-6
Carbon tetrachloride
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
56-23-5
Chlorobenzene
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
108-90-7
Chloroethane
NO
ug/1
10.
1.0
08/21/01
09:15
RWS
75-00.3
Chloroform
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
67-66-3
Chloromethane
NO
ug/1
10.
1.0
08/21/01
09:15
RWS
74-87-3
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 4
Laboratory Certification IN
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

7aceAnalyfical'h'
/ www.pacelabs.com
iI
Lab Sample No: 921770178
Client Sample ID: EFFLUENT
Parameters
2-Chlorotoluene
4-Chlorotoluene
1.2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1.2-Dichloroethane
1.1-Dichloroethene
cis-1,2-Dichloroethene
trans-1.2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1.1.2.2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1.2.4-Trichlorobenzene
1.1,1-Trichloroethane
1.1.2-Trichloroethane
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID:.SLS-Greensboro/010305/107535
Project Sample Number: 9225400-001 Date Collected: 08/17/01 10:30
Matrix: Water Date Received: 08/17/01 13:35
Results
Units
Report Limit
Dilution Analyzed
ND
ug/1
5.0
1.0
08/21/01
09:15
RWS
ND
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
10.
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/l
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
NO
ug/1
5.0
1.0
08/21/01
09:15
RWS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
CAS No. Ftnote Reg Limit
95-49-8
106.43-4
96-12-8
124.48-1
106.93-4
74-95-3
95.50-1
541.73-1
106-46-7
75-71.8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87.6
75-09.2
1634.04-4
91.20-3
103.65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
Page: 5
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID: SLS-Greensboro/010305/107535
Lab Sample No: 921770178
Project Sample
Number: 9225400-001
Date Collected: 08/17/01 10:30
Client Sample ID: EFFLUENT
Matrix: Water
Date
Received:
08/17/01 13:35
Parameters
Results
Units
Report Limit
Dilution
Analyzed
CAS No. Ftnote Reg Limit
Trichloroethene
ND
ug/1
5.0
1.0
08/21/01
09:15
RWS
79-01-6
Trichlorofluoromethane
ND
ug/1
10.
1.0
08/21/01
09:15
RWS
75.69-4
1,2.3-Trichloropropane
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
96-18-4
1.2.4-Trimethylbenzene
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
95-63-6
1,3,5-Trimethylbenzene
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
108-67-8
Vinyl chloride
ND.
ug/l
10.
1.0
08/21/01
09:15
RWS
75-01-4
m&p-Xylene
ND
ug/l
10.
1.0
08/21/01
09:15
RWS
o-Xylene
ND
ug/l
5.0
1.0
08/21/01
09:15
RWS
95-47-6
Toluene-d8 (S)
95
X
1.0
08/21/01
09:15
RWS
2037-26-5
4-13romofluorobenzene (S)
102
%
1.0
08/21/01
09:15
RWS
460-00-4
Dibromofluoromethane (S)
100
%
1.0
08/21/01
09:15
RWS
1.2-Dichloroethane-d4 (S)
97
%
1.0
08/21/01
09:15
RWS
17060-07-0
-I
Date: 08/27/01
I
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 6
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KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

L!
ace Analytical "'
www.pacelabs.com
Lab Sample No: 921770186
Client Sample ID: EFFLUENT DISSOLVED
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 9225400
Client Project ID: SLS-Greensboro/010305/107535
Project Sample Number: 9225400-002 Date Collected: 08/17/01 10:30
Matrix: Water Date Received: 08/17/01 13:35
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
Metals
Dissolved Metals. Trace ICP
Prep/Method:
EPA 3010 /
EPA 6010
Aluminum, Dissolved
5.3
mg/l
0.10
1.0
08/22/01
RWF
7429-90-5
Antimony, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7440-36-0
Arsenic. Dissolved
NO
mg/1
0.0050
1.0
08/22/01
RWF
7440.38-2
Barium. Dissolved
0.14
mg/l
0.0050
1.0
08/22/01
RWF
7440-39-3
Beryllium, Dissolved
NO
mg/1
0.0010
1.0
08/22/01
RWF
7440-41-7
Boron, Dissolved
ND
mg/l
0.010
1.0
08/22/01
RWF
7440-42-8
Cadmium, Dissolved
NO
mg/l
0.0010
1.0
08/22/01
RWF
7440-43-9
Calcium. Dissolved
7.4
mg/l
0.10
1.0
08/22/01
RWF
7440-70-2
Chromium, Dissolved
0.012
mg/l
0.0020
1.0
08/22/01
RWF
7440-47.3
Cobalt, Dissolved
0.0059
mg/l
0.0050
1.0
08/22/01
RWF
7440-48-4
Copper. Dissolved
0.020
mg/1
0.0020
1.0
08/22/01
RWF
7440-50-8
Iron, Dissolved
10.
mg/l
0.050
1.0
08/22/01
RWF
7439-89.6
Lead, Dissolved
NO
mg/l
0.0030
1.0
08/22/01
RWF
7439-92-1
Magnesium, Dissolved
7.0
mg/l
0.10
1.0
08/22/01
RWF
7439-95-4
Manganese. Dissolved
0.22
mg/l
0.0050
1.0
08/22/01
RWF
7439-96-5
Molybdenum, Dissolved
ND
mg/1
0.0050
1.0
08/22/01
RWF
7439-98-7
Nickel. Dissolved
0.010
mg/l
0.0050
1.0
08/22/01
RWF
7440-02-0
Potassium, Dissolved
2.4
mg/l
1.0
1.0
08/22/01
RWF
7440-09-7
Selenium, Dissolved
NO
mg/l
0.0050
1.0
08/22/01
RWF
7782-49-2
Silicon, Dissolved
22.
mg/1
0.10
1.0
08/22/01
RWF
7440-21-3
Silver, Dissolved
ND
mg/l
0.0020
1.0
08/22/01
RWF
7440-22-4
Sodium, Dissolved
4.2
mg/l
1.0
1.0
08/22/01
RWF
7440-23-5
Strontium, Dissolved
0.080
mg/l
0.0050
1.0
08/22/01
RWF
'7440-24-6
Thallium. Dissolved
NO
mg/1
0.010
1.0
08/22/01
RWF
7440-28-0
Tin, Dissolved
NO
mg/1
0.0050
1.0
08/22/01
RWF
7440-31.5
Titanium, Dissolved
0.44
mg/l
0.0050
1.0
08/22/01
RWF
7440.32-6
Vanadium, Dissolved
0.025
mg/l
0.0050
1.0
08/22/01
RWF
7440-62-2
Zinc, Dissolved
0.050
mg/l
0.010
1.0
08/22/01
RWF
7440-66-6
Date Digested
08/21/01
Date: 08/27/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page: 7
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KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

I f—& s&ylav IL/a -. .. ,.1 I Iti�ir...,.lt.e„ ei�'.LA..►+SL . as &t u.As"11L
hwit /I ndly6cal •••� •:hain- custody r� d LEGHr_ r.LICUMci.r. All rereitanr /ielos must be completes accurately.
, n
www.paeelabs.rom Required Client Information: Section B 59420
Report To:
Required Client Into nation: Section A •'.� /t, " Page: / Of To Sr, Completed by Pace Analytical and Client Section C
Companv ) Copy To: Ouoi� Reference:
Client Information Checkquote/contract:
Ad ess J.invoice To; ., n `/' Requested Dun Date: 'TAT: Prof —I Manager:
P.O. Turn around times less Than 14 da s subject to Proj�•t a: r )
laboratory and contractual obligations and may result in a
Project Name: `9 Rush Turnaround Surcharge.
/�' Ar r� / ' �• Turn Around Time (TAT) in calendar days.
Phone Fax Project Number: Requested Analysis: / .
Section 1) Required Client Information: Valid Matrix Codes �— p o Preservatives
MATRIX W W A. U
WATER WT 1 w W V W V
SAMPLE ID ooa IL oL o aw J
WIPE WP U O O (D
One character per box. AIR AR Q 0 O c o x m
W (A-Z, 0-9 /.-) TISSUE TS F a O O N
Sample IDS MUST BE UNIQUE OTHER OT— 2 mm / old / yy hh: mm a/p a Z _ _ = z zRemarks /Lab ID
I L
Additional Cone ents:
act:
' y
rr
oil
�i
A tt
Pace Project No.:
SAMPLE CONDITION
i
Temp: [—°C I Received on Ice: (Y't/ 11! Sealed Cooler. Y /. Samples Intact:
Sr-E REVERSF 'AnE FOR INSTRUCTIONS

ace Analytical m
/ /— www.pacelabs.com
_
PT -_'Inc. Charlotte
�9800 Kincey Ave.
(Suite 100
Huntersville. NC 28078
r�
�I
Attn: Project Management
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9321585
Client Project ID: C. dubia Pass/Fail-IT
Lab Sample No: 93914349 Project Sample Number: 9321585-001 Date Collected: 06/25/01 15:55
.lient Sample ID: IT COMPOSITE EFFLUENT Matrix: Water Date Received: 06/27/01 15:55
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
3ioassay
1C.dubia Pass/Fail Chronic NC Method: EPA 600/4-91/002 Prep Method: EPA 600/4-91/002
C.dubia Pass/Fail Chronic FAIL No units 06/27/01 JGJ
Date: 07/11/01
Laboratory Certification IDs
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NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
ace Analytical 54 Rao/tDrive
Ashevilllele,, N NC 28801
' ace/abs.com Phone:[phone]
www.pacelabs.com Fax, 828.254.4618
I Lab Project Number: 9321585
Client Project ID: C. dubia Pass/Fail-IT
Lab Sample No: 93914356 Project Sample Number: 9321585-002 Date Collected: 06/28/01 15:55
Client Sample ID: 2ND IT COMPOSITE EFFLUENT Matrix: Water Date Received: 06/30/01 15:55
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
(Bioassay
C.dubia Pass/Fail Chronic NC Method: EPA 600/4-91/002 Prep Method: EPA 600/4-91/002
C.dubia Pass/Fail Chronic No units 06/27/01 JGJ
I
Date: 07/11/01
Page: 2
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

Pace Analytical Services, Inc.
54 Ravenscrolt Drive
ace Analytical TM Asheville, NC 28801
Phone: [phone]
www.pacel .bWt Toxicity Report AT-1 Form Chronic Pass/Fail and Acute LC50 Fax; 828.254.4618
Date 7\11\01
Facility: IT NPDES#NC 0086886
of Opecator in R le Charge
Pipe # 001
Comments
County Guilford
I Samples Not Aerated Unless Otherwise Noted
i
Environmental Sciences Branch Chronic Test Results
MAIL ORIGINAL TO: N of t I
r Quality ca,a,� t 9.7
40
1621 Mail Service Center
North Carolina Cenodeahnia Chronic Pass/Fail Reproduction Toxicity
Test
Raleigh, North Carolina 27699-1621
Tabular t
% Reduction
CONTROL ORGANISMS
1
2
3
4
5
6
7
8
9
10
11
12
% Mortality
# Young Produced
27
22
18
25
17
23
16
10
18
18
12
18
Corttrol
Adult Live Dead
L
L
L
L
I L
LJ
L
L
L
L
L
L
0.00
Effluent%
90
Treatment 2
41.70
TREATMENT 2 ORGANISMS
1
2
3
4
5
6
7
8
9
10
11
12
Control CV
26.6
# YoungProduced
6
7
2
7
1
0
0
0
5
0
2
0
^—
woduckV 3rd brood
Adult (L)ive (D)ead
L
L
L
L
D
O
D
L
L
L
D
D
91.7
1 St 1 St 2nd
pH Control 7.6 7.6 7.7 7.8 7.8 8.0
Treatment 7.4 7.6 7.5 7.7 7.6 8.0
S E S E S E
t n t n t n
a d a d a d
r r r
t t t
1 St 1 St 2nd
D.O Control 7.6 7.6 7.9 7.2 8.3 7.5
Treatment
LC50/Acute Toxicity Test
(Mortality expressed as % , combining replicates)
LC50= % Method of Determination
95% Confidence Moving Avg. Probit
off' - % Spearman Other
organism Tested: Cerioda hnia dubia Test Duration (Hours):
2.508
86.6
Avg. Reprod.
Control
18.70
Treatment 2
2.50
PASS FAIL
Check One
6\27\01
Sample 6\25\01 Sample 2
6\28\01
Sampel Type/Duration
Grab Cones.
N
w o
Sample
X
x
a x
2a
in
a
0 d
Sample
X
v
2a
Hardness (mg/I)
40
Spec. Cond. (umhos)
138
94
as
Chlorine (mg/1)
0.04
0.07
Sample temp. at receipt
0.6
2.2
Concentration Note: Please
Complete This
Mortality Section also
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS
NO Wastewater 40
NO Drinking Water 37712 This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
startiend startiend
Control
High
Conc.
P
Laboratory Certification IDs
TN Drinking Water 02980
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PACE ANALYTICAL SERVICES,
- _ AQUATIC v.XICULOGY LABOF " TORY
CHAIN-OF-CUSTOIDY AND FIELD ANti.�YSIS FORM
CLIENT / FACILITY NAME: PURCHASE ORDER #:
�T Gv lief' ,
COUNTY: ,-� f c ��r, s t STATE: JJ�
NPDES PERMIT #: I- K 60I"FAL1- I PIPE #:
54 RAVENSCROFT DRIVE
ASHEVILLE,NC 26801
PHONE: [phone]
FAX: [phone]
INFORMATION ON THIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.TEST REQUIREMENTS (Please check the appropriate lost typo and species required,)
Testfvpe Specles f
Acute, circle Ilia appropriate lost duration: 24 48 96 hours Cedodaphnia dubla (Water flea)
�,Cluonlc, 7-days Philephales prornelas (Fathead inInnow)
Pass / Fail, dilution required: A.
I Daphnia pulex
Full Range Definitive, dllu8on3 required: Cypfinodon Vsfiegsfus (Sheepshead minnow)
Other, specify: Men/da beryNna (Inland siiverslde)
Mysidopsls bahis (Mysld shrimp)
Other, specify:
SAMPLE TYPE
Coniposito san7ple Sample lntormarlon
Start dale: L-3 .�) <-O /
Start tlr,Te: 13SC%
End dale: fUti/o7 G%G2 i
_
End time: ( 3—: G
Samplea per hour: 1-/
C_hllled during colleclion7:
y e e�
If chilled, specify temperature:
'Ll c' c-
Grab sample
Date: NIA Time: jtJ
Sample location: (after chlorination, above outfall, at weir, effluent outfall, eta.)
_Approximate volume collected for testing:
Number of containers filled for testing: l
Total residual chlorine (rng/L): M'A
Temperature at lime of collection °C : y a e
Method of transport to PACE: '41 N
Note: Rinse containers with Ills sample before filling. Pack sample In loose Ice.
_ Samples must he received at PACE at or below 4°C. Sample should Trot be frozen.
REMARKS
SAMPLE CUSTODY
collected by:
r„InT U .
Relinquished by: r'N
0 - -A r ( t
rninI 1 SIGNATURE
DATE AND TIME.
Rellnqulshed to PACE by. -
PAIN T SIn N/11 UDE
DATE AND TIME
FOR OFFICE USE ONLY
PROJECT
ACODE:
SAMPLE
Race/ved by: v
MINT A,S AI DE AlE AND TIME
Recelved at PACE by:
�.�6►�, PS /3
141,971,11
ry71Nr NArU DAT AND TIME
Sample ton►perature u;111
iv get at ACE (' Q:

PACE ANAL't"1ICAL SERVICES,''
AQum FIG i
--- ' -- - - XI6oi:0G r LABUrr •' TOtzY :
CHAIN -OF -CUSTODY AND FIELD ANk;_-- I(SIS FORM
CLIENT / FACILI•IY NAME: PURCHASI: ORDER #:
COUNTY: L--u" I- F C'r R.J STATE: • ;QC _.
NPDES PERMIT #: OUTFALL I PIPE #: C-5>
54 RAVENSCROFT DRIVE
ASHEVtI LE, I`JC 2aWl
PttONE: [phone]
FAX: [phone]
INFORMATION ON TIIIS FORM IS REQUIRED
_ BY STATE AND FEI)ERAI. AGENCIES.
TEST REQUIREMENTS (Please check the appropriate lost type and species required.)
Test fy e Spocles
Acute, circle the appropriate lost duration: 24 46 96 hours Ceriodaphnia dubla (Water Ilea)
Chronlc, 7-days Pln)epha/es promelas (Fathead n)Irtnow)
✓ Pass I Fail, dilution required: Daptinla pulex .
Full Range Definitive, dilutions required: Cyprinodon vadegatus (Sheepshead minnow)
Other, specify: _ Menida beryfflna (Inland silverside)
Mysldopsls bahis (Mysld sh(lmp)
Other, specify:
SAMPLE TYPE �—
Composite sample Sample lnthimation
Start date: G 6'" oq"-() l
End date: C) (: - ;Yy -L1
Start
End llme:Samples
per hour: Lr
Chilled during collection?: yr'C'S
If chilled, specify temperature:
Grab sample
[Date:
Sample location: (after chlorination, above outfall, at welr, effluent outfall• etc.)
FF1-
Approximate volume collected for testing: I .
Number of containers filled for testing: r
Total residual chlorine (ITIWI_): &) ,-el
Temperature at time of collection °C : e `-
Method of transport to PACE: VA-h}
Note: Rinse containers with the sample before filling. Pack sample In loose Ice.
REMARKS
Samples must be received at PACE at or below 4°C. Sample shordd not be frozen.
-'T"—'-'—"'
SAMPLE CUSTODY
collected by:
SIGNATURE DA
Relinquished by:
-0
t Is3e,
�- rTillrr SIGNATURE DATE AND TIME
---
FOR OFFICE USE ONLY
PRO,
ACODE:
SAWPLE
Recelved by:
t-'� ri--ee
09 Pninr IOHAT RE HATE AND TIME
Recelved at PACE by:
�u 0I 13GD,
- Va l z;
FITDIr SIGNATURE - DATE AND TIME
Sample tomporaturn' ulwn mcelpt at PACE C):

;acieAnalyfical"'
www.pacelabs.com
FII Inc. Charlotte
9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
1
I4ttn: Project Management
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9322170
Client Project ID: C. dubia Full Range- IT
Lab Sample No: 93935906 Project Sample Number: 9322170-001 Date Collected: 07/23/01 11:20
.lient Sample ID: IT COMPOSITE EFFLUENT Matrix: Water Date Received: 07/25/01 11:20
'Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
'C.dubia Full -range Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Full -range Chronic NOEC<45, No units 07/25/01 JGJ
Date: 08/10/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
o�&� a
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9322170
Client Project ID: C. dubia Full Range- IT
i
Lab Sample No: 93940708 Project Sample Number: 9322170-002 Date Collected: 07/26/01 16:47
Client Sample ID: 2ND IT COMPOSITE EFFLUENT Matrix: Water Date Received: 07/28/01 16:47
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Full -range Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Full range Chronic No units 07/25/01 JGJ
Date: 08/10/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,y AC[pA
c
Page: 2
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

1 i �
�i
ace Analyical'
www.pacelabs.com
tent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia
I
acility IT NPDES#: NC
iLaboratory Performing Test PACE Anal t' 1 Services, Ing
'49nawre of Operator in Responsible Charge ignature Lab Supe or
Sample Information
Collection Start Date
Grab
Composite (Duration)
-- Hardness (mg/L)
Spec. Cond. (umhos/cm)
Chlorine (mg/L)
Sample Temp. at Receipt
I
?ntrol
i
Effluent%
J
Sample 1
Sample 2
Control
7\23\01
7\26\01
24
25
42
84
90
129
0
0
0.3 C
74 C
Pipe# 1001
Comments:
.0
Pace Analytical Services, Inc.
54 Ravenscroll Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Countv Mecklenbu
Test
Information'
Treatment
pH Initial
pH Final
D.O. Initial
D.O.'Final
Temp. Initial
Temp. Final
Start Date
7125401
End Date
8111o1
Start Time
15:15
End Time
9:00
Start
Renew
Renew2
Start
Renewt
Renew2
100
100
100
Control
Control
Control
7.3
7.3
7.5
7.8
7.7
7.9
7.8
8.0
8.0
7.6
8.1
8.1
8.7
9.0
8.5
8.5
8.1
8.0
8.8
7.4
8.4
8.8
8.1
8.4
24.7
24.9
25.3
24.8
24.4
25.0
24.7
24.8
24.9
25.0
24.7
24.7
Organism # Chronic Test Results
1 2 3 4 5 R 7 A a '1n 11 41) _
# Youngs
19
19
18
18
20
19
17
15
22
17
NA
NA
18.4
Adult
f live (Dlead
L
L
L
L
L
L
L
L
L
L
NA
NA
1 2 3 4 5 R 7 R a 1n 11 in _
# Young
8
14
L
17
L
17
L
11
L
11
L
11
L
7
L
8
L
9
L
NA
NA
NA
NA
11.3
%Re
38.6
Adult
(Clive (Dlead
L
1 2 3 4 5 6 7 8 A 1 n mo,r,
# Young
19
9
15
12
12
8
16
18
17
11
13.7
Adult
%Red
fLlive IDlead
L
L
L
L
L
L
L
L
L
L
25.5
,fluent%
' � 7
Iuent%
#Young
Adult
90
I
(llive IDlead
#Young
Effluent%
I
95
Adult
(Clive IDlead
went%
100
1 2 3 4 1.9 R 7 A a 1 n
11
9
1 9
20
9
8
10
7
16
10
1o.9
L
L
D
L
L
L
L
L
L
L
%Red
140.71
1 2 3 4 5 R 7 A a 1 n ----
7
9
1 10
1 8
1 7
9
9
5
13
8
8.5
L
L
L
I L
I L
I L
I D
L
L
L
%Red
153.8
1 2 3 4 5 R 7 A a -in ----
# Young
15
7
11
7
8
6
7
7
6
9
8.3
Adult
(Clive (Dlead
L
L
L
L
L
L
L
L
L
L
%Red
54.9
IL ATT: Environmental Sciences Branch Should use highest test
Div. of Water Quality concentration or highest
TO; N.C.DENR concentration with 0.0. > 5.0
� mg/L
1621 Mail Service Center % Reduction from Control
Raleigh, NC 27699-1621 Reproduction Mean
-laboratory Certification IDs
IC Wastewater 40
` AC Drinking Water 37712
I
Final Control Mortality % 0
% Control with 3rd Brood 100
Control Reproduction CV 10.3
48 Hour Mortality
Iwc
•, 0 0 10 0 0 10
Significant? NO
Final Mortality Significant @ no coot.
0 % None
Reproduction Analysis:
Reproduction LOEC= >100 NOEC= <45
Method: Steel's Many One Rank Test
Normal Distrib? No
Method: Kolmogorov d
Statistic:
1.112 Critical:
1.035
Non -Parametric Analysis (if applicable):
Method:
Effluent%
Rank Sum Critical Sum
45
59.0
75.0
65
69.0
75.0
90
64.5
75.0
95
55.0
75.0
100
55.5
75.0
Overall Analysis:
Result = PASS/FAIL
or
Test LOEC= 45
%: NOEC=
<45 %
Chronic Value =
<45
%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 9,9030

-- ' �- — �`_-_ A(:2UATIC TOXICOLOGY LABO,� "TORY
CHAIN -OF -CUSTODY AND FIELD ANt`YSIS FORM
CLIENT/ FACILITY NAME:
PURCHASE ORDER #:
i C D T
COUNTY: 6 " , i
STATE: C-
NPUES PERMIT #: Sl
OUTFALL I PIPE #:
PACE ANALYTICALSERVICES
54 RAVENSCROFT DRIVE
ASHEVILLE, NC 28801
M"IE: [phone]
FAX: [phone]
INFORMATION ON THIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please check the appropriate lest typo and species required.)
TestIf a Species
Acute, circle the appropriate test duration: 24 48 96 hours Cedodaphnia dubla (Water flea)
Chronic, 7-days X Plinepha/es pimme/as (Fathead minnow)
Pass / Fail, dilution required: Daphnia pulex
Full Range Definillve, dilutions required: Cyprinodon vadegafus (Sheepshead minnow)
Other, specify: Menida beryfkna (Inland silverside)
RMysidopsls behis (Mysid shrirnp)
Other, specify:
SAMPLE -TYPE
Composite sample Sample Infoimatlon
Start dale: ` /2G v /
Start time: / () 0
End date: /2� r t
End llrne:
Sarnples per hour: `3
Chilled during collection?:
yes
If chilled, specify temperature:
I C f 4 0 C-
Grab sample
Dale: Tin �]
(Note: Rlnse containers with Ilia sample before filling. Pack sample In loose Ice.
Samples must be received at PACE at or below 4°C. Sample should not be frozen.
REMARKS
SAMPLE CUSTODY
Sample collected by:
effluent Sample location: (after chloflnadon, above outfall, at weir, outfall, etc.)
".,A-1 A- r—
ApproxIniate volume collected for testing:
L"Az E)cc I b>�
Number of cons filled for testing:
Total residual chlorine (mg/L):
N/ .
Temperature at time of collection (*C):
�4 I • V
Method of transport to PACE:
A
�rLT�r
inur SIGNATURE DAr NU TIME
Relinquished by:
C
n71Nr SIGNATURE DATE AND TIME
Rel/nqulshed to PACE by:
^�
MINT 6H7NA 11111E DATE AND TIME
FOR OFFICE USE ONLY
1PROJECT :
'4
ACODE:
SAMPLE
Received by:
rniNr SIGNAT E DATE AND TIME
Received at PACE by:
Twi%A5a'r��C 28 jo)
mlNT 6IGNATURE DATE AND TIME
Sample temperature upon necelpt at PACE (' Q:
/ Z/O
6--lac-

__ _. __,_ I A`._�•rl�-.-J.xfl{,��OCs-�E=ADv~—='TGr=c�r ' - - ---�
C}-IAIN .
-OF-CUSTODY AND FIELD ANt,,.YSIS FORM
1
PACE ANALYTICAL SERVICE
54 RAVENSCROFT DRIVE
ASHEVR- E, NC 28801
PttONE: [phone]
FAX: [phone]
INFORMATION ON THIS FORM IS REQUIRED
TEST REWUIREM ENTS (Please check the appropriate test type and species required.)
BY STATE AND FEDERAL AGENCIES.
Test f e Species
Acute, circle the appropriate test duration: 24 48 96 hours ' Cerfodaphnia dubla (Water flea)
Chronic,d
Pass /Fail,dilution required: Plmephales promelas (Fathead rninnmv)
Fulldilution
Other,
Range Definitive, dilutions required: Daphnis pulex
Cyprinodon vadegafuminnow)
s (Sheepshead ow)
Other, specify:Manida beryf5ne (Inland silverside)
Mysldopsis behis (Mysld shrlrnp)
Other, specify:
SAMPLE TYPE
Composite sample Sample Information
Start dale: IStart lime: 1.2 t/.71
End date: /sp pf End Ulna: 1.2 vy
Samples per hour:
Chiiled'durin collecllorn?: �s
If chilled, specify temperature: leiro y oe.
Semple location: (after chlorination, above Rutfa11. at weir, effluent outfall, sec.)
Approxitnate volume collected for testis ; q It
Number of containers filled for testincy�Q
Total realdual chlorine (mgfl: N� -
Tern rature at time or coilectlon °C
Grab ate: - ° Method of transport to PACE:
Date: Time: C"
Note: Rinse containers with 01e sample before filling. Pack sample In loose ice.
i
REMARKS Samples must be received at PACE at or below 4°C. Sample shotild not be frozen.
SAMPLE CUSTODY
LIU-
MINYuy:
SIGNAWFIE DATE AHD TIME
FOR 0FFICE USE ONLY
PROJECT f
ACO(.IE:
SAMPLE N '� C
Recelverl
by:
Recolverl
MINT SIONATt DALE AND TIME
at PACE by:
MINI GIONArunE DALE AND IIME
SanMTh temperature upon rece/pt at PACEQ:
n• .3

ace Analytical "'
www.pacelahs.com
f�. _ Inc. Charlotte
9800 Kincey Ave.
(Suite 100
`Huntersville, NC 28078
i
.Attn: Project Management
Phone: [phone]
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9322706
Client Project ID: C.dubia Full Range Chronic -IT
Lab Sample No: 93953834 Project Sample Number: 9322706-001 Date Collected: 08/13/01 13:17
,Client Sample ID: COMPOSITE EFFLUENT Matrix: Water Date Received: 08/15/01 13:17
i
f
-Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Full -range Chronic NC Prep/Method: EPA.600/4-91/002 / EPA 600/4.91/002
j C.dubia Full -range Chronic NOEC<65R No units 08/15/01 JGJ
Date: 08/23/01
- Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Y Accp..
\C 1
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

ace Analytical''
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax., 828.254.4618
Lab Project Number: 9322706
Client Project ID: C.dubia Full Range Chronic -IT
Lab Sample No: 93957314 Project Sample Number: 9322706-002 Date Collected: 08/16/01 10:14
_ Client Sample ID: 2ND COMPOSITE EFFLUENT Matrix: Water Date Received: 08/18/01 10:14
1
j
'arameters. Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
'!C.dubia Full -range Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Full -range Chronic No units 08/15/01 JGJ
Date: 08/23/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
neiac.=
Page: 2
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

I,
aceAnalyticafr
�ffluent Aquatic TH1 *6flEff Form/Phase II Chronic Cerioda
_I hnia P
Facility IT Corp. NPDES#:NC Pipe#
Laboratory Performing Test PACE Anal}cbical Services_ Tnr• C
! Signature of Operator in Responsible Charge
- Sample Information
Collection Start Date
Grab
_-i Composite (Duration)
Hardness (mg/L)
Spec. Cond. (µmhos/cm)
Chlorine (mg/L)
Sample Temp. at Receipt
Signature
Sample 1
Sample 2
Control
8\13\01
8\16\01
24 hr
23.5 hr
45
75
74
128
0.00
0.00
1.7 C
1.6 C
Pace Analytical Services, Inc.
54 Ravenscroli Drive
Asheville, NC 28801
Phone: [phone], 76
Fax: [phone]
County Guilford
,�Qjomments.
The organism in replicate 10 was m
Test
Information'
Start Date
9115101
End
8122101
Date
Start Time
14:23
End T,me
8:50
Treatment
pH Initial
pH Final
D. 0. Initial
D.O. Final
Temp. Initial
Temp. Final
Start
Renewt
Renew2
Startr79
Renew
too
100
100
Control
Contri
6.9
6.3
6.6
7.6
7.5
7.4
7.7
6.9
7.5
7.3
7.8
7.8
7.6
7.9
8.1
7.6
8.3
7.8
7.5
8.2
7.6
24.7
25.1
24.9
24.8
25.3
25.0
24.6
24.7
24.7
24.6
24.7
24.7
Organism 9 Chronic Test Results
1 2 3 4 5 6 7 8 9 10 11 12
Control #Young
Adult
(Clive (Dlead
30
25
24
25
25
9
28
29
33
13
NA
NA
24.1
L
L
L
L
L
L
L
L
L
L
NA
NA
1 1 2 3 4 5 6 7 8 9 10 11 12 n
i Effluent% EL).Y,,
ung
ult
Dlead
25
27
23
23
23
20
28
26
31
-
NA
NA
25.1
L
L
L
L
L
L
L
L
L
-� 1 17 9 A c c I - -
24
22
22
19
23
24
24
19
22
27
Final Control Mortality % 0
% Control with 3rd Brood 90
Control Reproduction CV 31.1
48 Hour Mortality
IwC
0 0 10 0 0 10
Significant? No
Final Mortality Significant @ no conc.
0 % x
trnuenmo
Reproduction Analysis:
-
65
Adult
(Clive (plead
Reproduction LOEC= >100 NOEC= 100
- 1
2
3
4
5
6
7
8
9
10 mean
Meth d
j Effluent% #Young
Ad u It
90 ILlive (plead
o Bonferronl t
Normal Distrib? Yes Method Kolmogrovo D
. Statistic: 0.844 Critical: 1.035
1 2 3 4 5 6 7 8 9 10 mean N P
Effluent% #Young
Adult
, 95 (Clive (plead
Effluent%
# Young
Adult
- 100
(L)ive (plead
21
21
19
17
21
22
20
8
10
13
17.z
L
L
L
L
L
L
L
D
L
D
2%86
13
20
15
18
9
9
9
18
4
11
12.6
L
L
L
L
L I
L
I L
L
L
D
47e7
_on- arametnc Analysis (If appllcableY
Method:
Effluent% Rank Sum Critical Sum
1 2 3 4 5 6 7 8 9 10 mean 45
65
90
95
MAIL ATT: Environmental Sciences Branch Should use highest test 100
_ Div. of Water Quality concentration or highest
TO. N.C.DENR concentration with D.O. >5.0 Overall Analysis:
mg/L Result = PASS/FAIL or
1621 Mail Service Center •' % Reduction from Control Test LOEC- 90 % ' _ °
Raleigh, NC 27699-1621 Reproduction Mean - NOEC 65 /o
Chronic Value = 76.5 %
18
20
17
14
18
2
3
3
2
10
1a.7
L
L
L
L
L
D
D
L
L
L
SSe6
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laborat Certification IDs
NC Wastewater 40 TN Drinking Water 02980
_ NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

AQUATIC TOXICOLOGY LABORATORY
CHAIN-OF-CUSTOIDY AND FIELD ANALYSIS FORM
CLIENT / FACILITY NAME: PURCHASE ORDER #:
-r 7- L o i••
COUNTY: ti _ STATE:
NPDES PERMIT #: OUTFALL / PIPE #:
PACE ANALYTICAL_ SERVICES, INC.
54 RAVENSCROFF DRIVE
ASIiEVILLE, NC 28801
PHONE: [phone]
FAX: [phone]
INFORMATION ON THIS FORM IS REQUIRED
BY S rATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please check gio appropriate lost typo and species required.)
Test t e Specles
Acute, circle the appropriate test duration: 2.1 48 96 hours erlodaphnia dubla (Water flea)
Chronic, 7-days Plmephales pmrnelas (Fathead rninnow)
Pass / Fail, dilution required: Daplinla pulex
Full Range Definitive, dilutions required: — Cyprinodon variegafus (Sheepshead minnow)
Other, specify: Manias beryfflna (Inland silverside)
Mysldopsls bahia (Mysid shrlinp)
Other, specify:
SAMPLE TYPE
Composite sample Sample int`ormatlon
Start date: 13ok
i Start time: 1.00
End dat Z 114I
1 End time: 1 t p
Samples per hour: Li
Chilled during collection?:
f S
If chilled, specify temperature:
T c s p 4 o,.,
Sarnple locatlon: (after chlorination, above outrall, at weir, effluent outfall, etc.)
ApproxlnTale volurne collected for testing: OWL R a, a'h
Number of containers filled for testing: b Vl Q
Total residual chlorine (mg/L): N
Tern ralure at lime of collection 'C : N I k; } -r el
Grab sampleQ Method of transport to PACE: -e d ` Ex i
Date: Tinge:
Mote: Rinse containers with the sample before filling. Pack sample In Loose Ice.
REMARKS Samples must be received at PACE at or below 4'C. Sample should not be frozen.
SAMPLE CUSTODY
collected by: FOR OFFICE USE ONLY PROJECT #:
11 ��,µ�D l ACODE: SAMPLE #: L t*c `•tTc� (�' DU
MINT k I SIG NAI URE nnrc A/+n nut;
Relinquished by:
- MIN
J
SIGTIAlI1RE � DATE AND TIME
Relinquished to PACE by:
fT11Nr
61+irU lUllE�-- DAZE AND TIME
Received by:
MINT MOHAi URE DATE AND TIME
Received at PACE by:
MINT SIGNATURE DATE AND TIME
Sample temperature upon tDcelpt at PACE (' Q:
a.��rin57-e od +�..�C1�_� �(��Q4?X

AQUATIC TOXICOLOGY LABORATORY
CHAIN -OF -CUSTODY AND FIELD ANALYSIS FORM
CLIENT / FACILITY NAME: —' PURCHASE ORDER #:
-7 T- Co t2 P
COUNTY: - &t i % /'(1 _ STATE: 1V0,4k cero rrla
NPDES PERMIT #•
PACE ANALYTICAL SERVICES, INC.
54 RAVENSCROFT DRrVE
ASI IEViLLE, NC 288oi
Pt "IE: [phone]
FAX: [phone]e
l OUT FALL / PIPE #: INFORMATION ON THIS FORM IS REQUIRED
BY S rATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please check the appropriate test typo and species required.)
Test t e Species
Acute, circle the appropriate test duration: 24 48 96 hours Cedodaphnia dubla (Water flea)
Chronic, 7-days Plmephales pronrelas (Fathead rAnnow)
Pass / Fall, dilution required: Daplinla puler
Full Range Definitive, Dilutions required: i ^ Cyprinodon vadegatus (Sheepshead minnow)
Other, specify: Men1da beryfna (Inland silverside)
Mysidops/s bahia (Mysld shrimp)
Other, specify:
SAMPLE TYPE
Composite sample Sample inlbfmadort
Start dale: 8 /
Start lime: /�—
End date: p
End time: /p j d
Samples per hour:
Chilled during collection?:
�S
If chilled, specify temperature:
l t Ee) qOC.
Sample locallat: (after chlwlf'frfu a above outfall, at weir, eent outfall, etc.)
f f /lcQ,�f `)' q v Ic
Approximate volurne collected for testing:
14 /; • .ti,
Number of containers filled for testing:
Total residual chlorine (mg/L):
A)/�(
Temperature at time of collection (°C):
� U . -3
Method of transport to PACE:
�
Grab sample
'16 1—) I
Date: t
(Vote: Rinse containers witiT the sample before filling. Pack .sample In loose Ice.
Samples must be received at PACE at or below 4°C. Sample should trot be frozen.
REMARKS
SAMPLE CUSTODY
Sample collected by:
I,���
MINT SIGNATURE DATE AND 71ME
Relinquished by: _
MINT SIGNATURE DAT AND TIME
Relinquished to PACE by:
vniNI FHINAIURE DATE AND TIME
FOR OFFICE USE ONLY
PROJECT Ir:C
ACODE:
SAMPLE IF:
L
Received by: zi
L &A LI�L 1 ��5 - J-
MINT A IGNATURE DATE AND TIME
Recelved at PACE by:
`5� (
MINT SIGNATURE DATE Ar1D TIME
Sample ternperatutTe upon tecelpt at PACE (' q: /

ce Analytical o
www.pacelabs.com
PpSI Inc. Charlotte
9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
�I
'Attu: Project Management
Phone: [phone]
Lab Sample No: 93966711
Client Sample ID: IT COMPOSITE EFFLUENT
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9323011
Client Project ID: C. dubia Pass/Fail-IT
Project Sample Number: 9323011-001 Date Collected: 08/20/01 09:10
Matrix: Water Date Received: 08/22/01 09:10
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Pass/Fail Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Pass/Fail Chronic FAIL No units 08/22/01 JGJ
Date: 09/04/01
Laboratory Certification IN
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,p ACCOgO'
l'
it 3C;
Page: I
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

laceAnalyficaf"
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9323011
Client Project ID: C. dubia Pass/Fail-IT
Lab Sample No: 93966729 Project Sample Number: 9323011-002 Date Collected: 08/23/01 09:10
Client Sample ID: 2ND IT COMPOSITE EFFLUENT Matrix: Water Date Received: 08/25/01 09:10
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Pass/Fail Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Pass/Fail Chronic No units 08/22/01 JGJ
Date: 09/04/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
a
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
y �Cppgp
Page: 2
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

Facility: IT
Pace Analytical Services, Inc.
Analytical rM Asheville. NC 28801
www.pacR f kIft b Toxicity Report AT-1 Form Chronic Pass/Fail and Acute LC50 Phone: [phone]
Date 9\4\01 Fax: [phone]
fVrUt:69 NU uu86860 Pipe #
l-aooratory I-errorming lest PACE An I Y 1
County Guilford
a v I rvl c In
Comments
,SrTest Failed Fisher's Exact Test due to 100%
gn lure of Operato m Res sl Charge
mortality.
i ure of Labor y upervisor
Samples Not Aerated Unless Otherwise Noted
Environmental Sciences Branch Chronic Test Results
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR Calculated t
1621 Mail Service Center
Raleigh, North Carolina 27699-1621 Tabular t
North Carolina Cerrodaohnra Chronic Pass/Fail Reproduction Toxicity Test
Reduction 70.c
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# YoungProduced
26
24
20
fE22
25
8
18
17
23
23
% Mortality
Avg. Reprod.
Control
Control
Adult (L)ive (D)ead
L
L
L
L
fD±
L
L
L
L
L
8130
22.30
Effluent%
90
Treatment 2
Treatment 2
6.60
TREATMENT 2 ORGANISMS
1
2
3
4
5
6
7
8
9
10
11
12
Control CV
17.3
PASS FAIL
# Youn Produced
7
6
4
4
ED
5
7
6
7
7
$
12
%control organisms
X
Adult (L)ive (D)ead
D
D
D
D
D
D
D
D
D
D
D
producing 3rd brood
91.7
Check One
1st 1St 2nd
pH Control 7.6 8.0 7.8 7.6 7.6E77
Treatment 7.2 7.4 7.6 7.7 7,2
S E S E S E
t n t n t n
a d a d a d
r r r
t t t
1St 1St 2nd
D.O Control 8.4 8.3 8.0 7.8 7.7F72
Treatment 8.1 8.1 8.8 7.5 8 9
LC50/A t Toxicity Test
(Mortality expressed as % , combinin° renlinsta l
LC50= % Method of Determination
95% Confidence Moving Avg. Probit
% - % Spearman Other
Organism Tested: Ce%/
abQratory Certification IDS
IC Wastewater 40
NC Drinking Water 37712
8\22\01
Collection Start Data
Sample 8\20\01 sample 2
8123\01
4.
Sampel Type/Duration
N
Grab Comp.
H c
Sample
X
°x
m °x
=
3.75 hr
2
rn
N
in
0 R
Sample
X
o'
2
za nr
Hardness (mg/I)
ffA
43
.
Spec. Cond. (umhos)
_IS
137
Chlorine (mg/p
C59
080
Sample temp. at receipt
1.1
Concentration Note: Please
Complete This
Mortality Section also'
dubia (Test Duration (Hours)-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
start/end start/end
Control
High
Conc.
r
Laboratory Certification IDS.
TN Drinking Water 02980
SC Environmental 99030

AQUATIC TOXICOLOGY LABORATORY
CHAIN -OF -CUSTODY AND FIELD ANALYSIS FORM
CLIENT / FA/ FACILITY N ME: PURCHASE ORDER #:
'1%C.Ott V SC�.YS
COUNTY: STATE: ;0 �[ ✓v ,�
NPDES PERMIT #: OUTFALL / PIPE #:
PACE ANALYTICAL SERVICES, INC.
54 RAVENSCROFT DRIVE
ASHEVILLE, NC 213WI
P1lONE: [phone]
FAX: [phone]
INFORMATION ON THIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please check the appropriate lost typo and species required,)
Test f e Species
Acute, circle the appropriate test duration: 24 48 96 hours Ceriodaphrria duble (Water flea)
Chronic, 7 days Pjmephales piume/as (Fathead minnow)
Pass / Fail, dilution required: Daphnfa pulex
__ Full Range Definitive, dilutions roquired: Cypfinodon vadegafus (Sheepshead minnow)
Other, specify: Monida lerylfins (Ireland silverside)
Mys/dopsfs behis (Mysld shrlrnp)
Other, specify:
SAMPLE TYPE
Composite sample Sample /nfbimatlon
Start_ date: R 12-3 of
time: / D 70
Ed
End dale: $ f2� of
tlrno: p 3�
Samples per (Tour: q
Chilled during collection?: Tl e
S
If chilled, specify temperature:
u ,- O Trt•o `
Sarnple location: (after chlorination, above outfall, at weir, effluent outfall, etc.)
-77-}-w IC
ApproArnate volume collected for testing:
Nurnber of corTtalners filled for testing: 0
Total residual chlorine (rnglQ: ^/
Tern rature at time of collection °C :
Grab sample Method of transport to PACE: r
Date: I Irne:
Note: Rinse containers with tire sample before filling. Pack sample Irr Iooze Ice.
REMARKS
,w�KS Samples must be received at PACE at or below 4'C. Sample should Trot be frozen.
,
SAMPLE CUSTODY
Sample collected by:.
MINT SIGNATURE DATE AND TIME
Relinquished by:
NIN7 l ) SIGNAIUNE DATE ANU TIME
FOR OFFICE USE ONLY
PROJECT 1) 'j
ACODE:
SAMPLE #:C '' -
cl
Rece/ved by:
I - I --F
MINT 6RTNATUNE DATE AND TIME
ReAnqulshad to PACE by: Rece/ved at PACE by:
rTIINI CKMATURE DATE AND TIME MINT 610r1ATunE DATE AND TIME
Sample temperature upon receipt at PACE (' Q: ✓ / o�

AQUA•rIC TOXICOLOGY LABORATORY
CHAIN -OF -CUSTODY AND FIELD ANALYSIS FORM
CLIENT / FACILITY NAME: .__. PURCHASE ORDER #:
,=..T
COUNTY: A utr Orc STATE: &j �6vn�i1-�tt
NPDES PERMIT #•
PACE ANALYTICAL SERVICES, INC.
54 RAVENSCROFT DRIVE
ASHEVILLE, NC 28MI
PI TONE: [phone]
FAX: [phone]
r OUT FALL I PIPE #: INFORMATION ON THIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please clock lire appropriate test typo arid species required.)
Test f pe Specles
Acute, circle tho appropriate test duration: 24 48 96 hours Ceriodaphnia dubia (Water flea)
Chronic, 7-days Phnephales prorne/as (Fathead rnlnnow)
Pass / Fail, dilution required: Daphrila pulex
_ Full Range Definitive, dilutions required: Cyprinodon variegatus (Sheepshead minnow)
Other, specify: Menials beryNna (Inland silverside)
RMysidopsls bahis (Mysld shilinp)
Other, specify:
SAMPLE TYPE
Composite sample Samnle Infoimatlon
St; o
EnI Id1
Slart lline: )0.
End lime: �5T
Samples per hour: N
Chilled during collection?: e5
If chilled, specify temparalure: 'fir
G
Semple location: (after chlorination, above outfall, at weir, effluent outfall, etc.)
U fT J ue.;� 'T-A+�'��
Approximate volume collected for testing:
O 1)
Nurnber of containers filled for testing:
0 "-(?
Total residual chlorine (mg,/L):
) A
Temperature at time of collection (°C):
;--) O , G C.Method
of transport to PACE:
Ve <<
Grab sample CJ
Date: Tirne;
Note: Rinse containers with lire sample before filling. Pack sample In loose Ice.
REMARKS
Samples must be received at PACE at or below 4°C. Sample should tot be frozen.
SAMPLE CUSTODY
Sample collected by:
MINT 1 SICIUAIURE DATE AND TIME
Relinquished by:
MINT
SIGNATURE DATE AND TIME
Relinquished to PACE by:
L
T77RII
SKINAIURE DATE AND TIME
FOR OFFICE USE ONLY
PROJECT #: C.I
ACODE:
SAMPLE
Received by.
C� ,VV( �Liz
MINT SIGNATURE DATE AND TIME
Received ,ait PACE by:
L12
MINT SIGNAIURE DATE AND TIME
Sam le temperature upon tacelpt at PACE (0 Q:

ace Analytical "'
www.pacelabs.com
r )I Inc. Charlotte
9100 Kinsey Ave.
Suite 100
— Huntersville, NC 28078
Pace Analytical Services, Inc.
54 Aavenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax., 828.254.4618
Lab Project Number: 9323553
Client Project ID: C.dubia Full Range -IT
-'Attn: Project Management
Phone: [phone]
Lab Sample No: 93988665 Project Sample Number: 9323553.001 Date Collected: 09/17/01 09:40
,Client Sample ID: IT COMPOSITE EFFLUENT Matrix: Water Date Received: 09/18/01 09:40
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Full -range Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Full -range Chronic NOEC<45X No units 09/19/01 JGJ
Date: 10/01/01
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
\M AC[ON
0
ndac
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

Pace Analytical Services, Inc.
eacieAnalyticafm A R vine, C Drive
Asheville, NC 28801
Phone:[phone]
www. pace/abs. com Fax: [phone]
F
Lab Project Number: 9323553
Client Project ID: C.dubia Full Range -IT
Lab Sample No: 93991651 Project Sample Number: 9323553-002 Date Collected: 09/20/01 10:51
Client Sample ID: IT 2ND COMPOSITE EFFLUENT Matrix: Water Date Received: 09/22/01 10:51
--'Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Bioassay
C.dubia Full -range Chronic NC Prep/Method: EPA 600/4-91/002 / EPA 600/4-91/002
C.dubia Full -range Chronic No units 09/19/01 JGJ
Date: 10/01/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Page: 2
REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
This report shall not be reproduced, except in full, TN Drinking Water 02980
without the written consent of Pace Analytical Services, Inc.
SC Environmental 99030
,M �CC09
Meiact.

i
7eaceAnalyficafm
ti www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9323553
Client Project ID: C.dubia Full Range -IT
Lab Sample No: 93993467 Project Sample Number: 9323553-003 Date Collected: 09/17/01 14:08
client Sample ID: 1ST SAMPLE METALS Matrix: Water Date Received: 09/19/01 14:07
-,>arameters
Results
Units
Report Limit
Analyzed
CAS No.
Metals
ICP Metals, trace -level
Prep/Method:
EPA 3010 /
EPA 200.7
Aluminum
23.
mg/l
0.25
09/28/01
07:48
TRW
7429-90-5
Antimony
ND
mg/l
0.010
09/28/01
07:48
TRW
7440-36-0
Arsenic
ND
mg/l
0.010
09/28/01
07:48
TRW
7440-38.2
Barium
0.33
mg/l
0.0050
09/28/01
07:48
TRW
7440-39-3
Beryllium
ND
mg/l
0.0020
09/28/01
07:48
TRW
7440-41-7
Boron
ND
mg/l
0.010
09/28/01
07:48
TRW
7440-42-8
Cadmium
0.0028
mg/1
0.0010
09/28/01
07:48
TRW
7440-43-9
Calcium
11.
mg/l
0.10
09/28/01
07:48
TRW
7440-70-2
Chromium
0.052
mg/l
0.0050
09/28/01
07:48
TRW
7440-47-3
Cobalt
0.017
mg/l
0.0050
09/28/01
07:48
TRW
7440-48-4
Copper
0.055
mg/l
0.0050
09/28/01
07:48
TRW
7440-50-8
Iron
27.
mg/l
0.020
09/28/01
07:48
TRW
7439-89.6
Lead
ND
mg/l
0.010
09/28/01
07:48
TRW
7439-92-1
Magnesium
14.
mg/l
0.10
09/28/01
07:48
TRW
7439.95-4
Manganese
0.73
mg/l
0.0050
09/28/01
07:48
TRW
7439-96-5
_ •lybdenum
ND
mg/l
0.0050
09/28/01
07:48
TRW
7439-98-7
rckel
0.027
mg/l
0.0050
09/28/01
07:48
TRW
7440-02-0
Potassium
7.3
mg/l
0.50
09/28/01
07:48
TRW
7440-09-7
Selenium
ND
mg/l
0.020
09/28/01
07:48
TRW
7782-49-2
Silicon
48.
mg/l
0.10
09/28/01
07:48
TRW
7440-21-3
Silver
0.0091
mg/l
0.0020
09/28/01
07:48
TRW
7440-22-4
Sodium
5.6
mg/l
0.25
09/28/01
07:48
TRW
7440-23.5
Thallium
ND
mg/l
0.020
09/28/01
07:48
TRW
7440-28-0
Tin
ND
mg/l
0.010
09/28/01
07:48
TRW
7440.31-5
Titanium
1.5
mg/l
0.0050
09/28/01
07:48
TRW
7440-32-6
Vanadium
0.072
mg/l
0.0050
09/28/01
07:48
TRW
7440-62-2
Zinc
0.11
mg/l
0.010
09/28/01
07:48
TRW
7440-66-6
l I Date Digested
09/27/01
Date: 10/01/01
Laboratory certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
`O4M •«OyQ'
IC
Ftnote Reg Limit
Page: 3
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

;aceAnalyfical..
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9323553
Client Project ID: C.dubia Full Range -IT
Lab Sample No: 93993475 Project Sample Number: 9323553-004 Date Collected: 09/21/01 14:08
Client Sample ID: 2ND SAMPLE METALS Matrix: Water Date Received: 09/22/01 14:07
Darameters
Results
Units
Report Limit
Analyzed
CAS No. Ftnote Reg Limit
Hetals
ICP Metals, trace -level
Prep/Method:
EPA 3010 /
EPA 200.7
Aluminum
40.
mg/l
0.25
09/28/01
08:01
TRW
7429-90-5
Antimony
ND
mg/l
0.010
09/28/01
08:01
TRW
7440-36-0
Arsenic
ND
mg/l
0.010
09/28/01
08:01
TRW
7440-38-2
Barium
0.58
mg/l
0.0050
09/28/01
08:01
TRW
7440-39.3
_ Beryllium
ND
mg/l
0.0020
09/28/01
08:01
TRW
7440-41-7
Boron
ND
mg/l
0.010
09/28/01
08:01
TRW
7440-42-8
'- Cadmium
0.0061
mg/l
0.0010
09/28/01
08:01
TRW
7440-43-9
Calcium
16.
mg/l
0.10
09/28/01
08:01
TRW
7440-70-2
1 Chromium
0.11
mg/l
0.0050
09/28/01
08:01
TRW
7440-47-3
Cobalt
0.033
mg/1
0.0050•
09/28/01
08:01
TRW
7440-48-4
Copper
0.088
mg/l
0.0050
09/28/01
08:01
TRW
7440-50-8
Iron
51.
mg/l
0.020
09/28/01
Oa:01
TRW
7439-89-6
j Lead
ND
mg/l
0.010
09/28/01
08:01
TRW
7439-92-1
' Magnesium
24.
mg/l
0.10
09/28/01
08:01
TRW
7439-95-4
";nganese
1.5
mg/l
0.0050
09/28/01
08:01
TRW
7439-96-5
�lybdenum
ND
mg/1
0.0050
09/28/01
08:01
TRW
7439-98-7
'._ Nickel
0.067
mg/l
0.0050
09/28/01
08:01
TRW
7440-02-0
Potassium
11.
mg/1
0.50
09/28/01
08:01
TRW
7440.09-7 -
Selenium
ND
mg/l
0.020
09/28/01
08:01
TRW
7782-49-2
Silicon
55.
mg/l
0.10
09/28/01
08:01
TRW
7440-21-3
Silver
0.0055
mg/l
0.0020
09/28/01
08:01
TRW
7440-22-4
- Sodium
9.4
mg/l
0.25
09/28/01
08:01
TRW
7440.23-5
, Thallium
ND
mg/l
0.020
09/28/01
08:01
TRW
7440.28-0
Tin
ND
mg/l
0.010
09/28/01
08:01
TRW
7440-31.5
Titanium
2.4
mg/l
0.0050
09/28/01
08:01
TRW
7440-32-6
Vanadium
0.14
mg/l
0.0050
09/28/01
08:01
TRW
7440-62-2
Zinc
0.19
mg/l
0.010
09/28/01
08:01
TRW
7440-66-6
Date Digested
09/27/01
Date: 10/01/01
f Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
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REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
This report shall not be reproduced, except in full, TN Drinking Water 02980SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.
,N �CCOq
nelac

ace Analytical tM
F luent Aquatic Toxic t� ge"Po- ��orm/Phase II Chronic Ceriodaphnia
I
Facility IT NPDES#:NC 0086860 Pipe#
_aboratory Performing Test PACE Analytical Services, Inc. FTh_--1:nism
ents:
in
--� Signature at Operator n Responsible Charge ignatur 741111,
b S er ¢or I.
ilample Information
Collection Start Date
Grab
Composite (Duration)
r- Hardness (mg/L)
Spec. Cond. (umhos/cm)
jChlorine (mg/L)
Sample Temp. at Receipt
�,ontrol
'_ffluent%
Effluent%
I
65
aaluuumualaallnuau
Ilnlll1111HIall
IM011
IIIIIIIIIIIIIIIIIIIIIIIIIIII
I V�III
IUII�INgllllllllllll
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®IW�IUWIIUWWWIY
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville. NC 28801
Phone: [phone]
Fax: [phone]
County Guilford
8 of the 65°% was killed.
Test
Information'
Start Date
9119to 1
Eno
9126101
Date
Start Time
15:55
End
Time
10:40
Start
Renewl
Renewl
Start
Renewl
Renewl
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. Initial
Temp. Final
100
100
100
Control
Control
Control
7.5
7.5
7.5
7.6
7.6
7.5
7.7
7.7
7.7
7.8
7.5
T5
8.9
8.3
8.5
8.1
7.7
8.3
7.6
7.0
7.4
1 7.1
7.3
7.3
24.4
24.7
24.6
24.4
24.7
F 24.6
24.7
24.4
24.6
24.7
24.8 1
24.5
Organism # I Chronic Test Results
1 2 3 4 5 6 7 8 9 10 11 19 moan
# Young
27
20
20 i21
25
20
23
25
24
21
NA
NA
22.6
Adult
ILlive tDlead
L
L
D
L
L
I L
L
L
L
L
NA
NA
1 2 3 4 5 6 7 8 9 10 11 19 mean
# Young
1
1
18
9
L
15
L
13
L
22
L
20
L
1 21
L
11 1
D
18
L
25
L
1 NA
NA
I NA
NA
1 17.2
%Re
23.s
Adult
ILlive (Dlead
L
1 2' 3 4 5 6- 7 8 9 10 mean
# Young
F1o.7
18
6
3
10
7
8
14
11
19
°6Retl
Adult
(Clive tDlead
L
L
L
L
D I
L
I L
I
I L
I L
1 52.7
Final Control Mortality % 0
% Control with 3rd Brood 90
Control Reproduction CV 11.3
48 Hour Mortality
rnnTrni lwC
0 0 10 0 0 10
Significant? No
Final Mortality Significant @ no conc.
0 % X
Reproduction Analysis:
Reproduction LOEC= >100 NOEC= 100
1 2 3 4 5 6 7 8 9 10 mean Method: Bonferroni It Test
_ffluent% #Young
Adult
QC ILlive (Dlead
Normal Distrib? Yes Method Kolmogrovo D
Statistic: 0.688 Critical: 1.035
I 1 2 3 4 5 6 7 8 9 10 mean Non -Parametric Analysis (if apDlicable)-
'
Effluent/o -- o # Young
Adult
95 Wive (Dlead
14
2
7
8
13
2
2
4
8
8
6.8
L
D
L
L
L
L
L
L
L
L
%Red
69.9
Method:
Effluent°% Rank Sum Critical Sum
1 2 3 4 5 6 7 8 9 10 mean 45
'-ffluent% # Young
Adult
100 (Clive (D)ead
11
4
1 1
1 3
7
2
3
2
1 5
1 8
4.6
L
L
L
L
L
L
L
L
L
L
%Red
7s.6
3
1 i
2
4
7
5
4
5
5
2
3.8
L
D
L
L
L
L
L
L
L
L
%Red
83.2
'MAIL ATT: Environmental Sciences Branch
Div. of Water Quality
TO: N.C.DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Should use highest test
concentration or highest
concentration with D.C. > 5.0
m c; L
-- % Reduction from Control
Reproduction Mean
b5
90
95
100
Overall Analysis:
Result = PASS/FAIL or
Test LOEC= 45 %: NOEC= <45 %
Chronic Value = <45 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
c .cco,o
nelk
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

PACE ANALTI'ICAL SERVICE..
CHAIN-OF-CUSTOIDY AND FIELD ANi4LY513 FORM
CLIEN T� / F�ACILI TY NAME: ^�
JT C.urp, L 0 n2e-vsbo rD PURCHASE ORDER #:
COUNTY: �(�( E'L7rC STATE:
NPDF_S PERMIT #: OUTFALL / PIPE #: -
54 RAVENSCROFT DRiVE
ASHEViLLE.14C 28801
r I KNIE: [phone]
FAX: [phone]
INFORMATION ON I I IIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.
TEST REQUIREMENTS (Please check the appropriate lost type and species required.)
Test f e Species
Acute, circle the appropriate lest duration: 24 48 96 hours Cerlodaphnin dubia (Water Ilea)
Chronic, 7-days PlntePllales Prolnelas (Faliiead minnow)
Pass / Fail, dilution required: Daphnls pulex
iK Full Range Definitive, dilutions required: Cyptinodorr variegafus (Sheepshead minnow)
Other, specify: �,Menkfa beryKna (Inland silverside)
Mysidopsis bahin (Mysid shrimp)
Outer, specify:
SAMPLE TYPE
Composite sample Sample lnforntatlail
Start dale: !'t _ p t
End date:
5lalt time:
End it I I: tl fl
Samples per hour.
Chilled during collection?: Vp.
If chilled, specify temperature:
Grab s-itnple
Date: Time:
Sample location: (after chlorination, above outfall, at weir, effluent outfall, etc.)
Approximate volume collected for testing:
Number of containers filled for testing:
Total residual chlorine (mg/1-):
Temperature at time of collectiotl °C :
Method of tlnnsport to PACE:
Note: Rinse containers will, lire sample bTrrDre filling. Pack sample IT) loose Ice.
Samples must be recrived at PACE at or below A°C. Sample should not be frozen.
REMARKS
SAMPLE CUSTODY
Sample collected by: _ FOR OFFICE USE ONLY PROJECT;
ACODE: SAMPLE ff: - e
n1111T stanATllnE DATE AIID TIME
Refin(julshed by: Rocelved by:
L
rnnir 3IDNAI UDE Ell 6 � /v 6 Llk�—
���
DATE AIID TIME MINT NATunE DATE AND TIME
RoJingtrlshod to PAC._ by: Received at PACE_ by:
- rr-
r Intl rIAIIHIF DATE AND TIME PfIINT 61ONArUNE DATE AND TIME
Sample tomperatur>3 upon face! t PACE (` C): l r

AQUATIC TOXICOLOGY -LA -- ---- - sG TORY
CHAIN-OF-CUSTOIDY AND FIELD ANALYSIS FORM
CLIENT / FACILITY NAME: PURCHASE ORDER #:
COUNTY: G`,J-STATE: _
WDF_S PERMIT #: OUTFALI
PACE ANALYTICAL SERVICES
54 RAVENSCROFT ORIVE
ASHEVILLE. NC 28801
PHONE: [phone]
FAX: [phone]
.1 PIPE #. INFORMATION ON THIS FORM IS REQUIRED
BY STATE AND FEDERAL AGENCIES.TEST REQUIREMENTS (Please check the appropriate test typo and species required.)
Test f e Species
Acute, circle the appropriate tort duration: 24 413 96 hours Cedodsplrnia dullin (Water Ilea)
Chronic, 7-days Pimeplra/es promolas (Fathead minnow)
Pass I Fail, dilution required: Daphnia pu/ex
Full Range Definitive, dilutions required: Cyprinodon vadegntus (Sheepshead minnow)
Other, spocify: Menida beryfflna (Inland silverside)
Mysidopsis bahia (Mysid shrimp)
Other, specify:
SAMPLE TYPE
Composite sample Sample /nfoimatlo►1
Start date: o
Start lime:C�-
End date: ogLL, /D.
End line: o v,�
Samples per hour:
Chilled during collection?:
If chilled, specify temperature:
Sample location: (after chlorination, above outfall, at weir, effluent outlall, etc.)
ApproArnate volutne collected for testing:
Number of containers filled for testln :
Total residual chlorine (mg/L):
Temperature at time of collection (°C):
Grab same/e Method of transport to PACE:
Time:
rate:
Note: Rinse containers with tile sample before filling. Pack sample In loose Ice.
RESamples must be received at PACE at or below 4'C. Sample should not be frozen.
MARKS
SAMPLE CUSTODY
Sample cal/acted by: FOR OFFICE USE ONLY PROJECT aR:
4-CE ACODE: SAMPLE:
f11RlT SIOIr}IV E �' nATF Ann nuc
Relinquished by:
E-
PrimSIGNATURE
GATE AND TIME
Relingtilshod to PACE by:
I URE DATE AND
Received by:
I �1163s-- I
MINT 61ONAIURE DATE AND TIME
Received al PACE by:
Kart�S�i�C1vi IlF E���'Vm')� Zz 101 ► 3�D
MINT BRTNAr RE DATE AND IIME
Sample lemperatiula upon ilacelpt at PACE (' C): /
r

1 �KaceAnalytical rM
I www.pacelabs.com
IT Corporation
- 2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Keith Ogden
Phone: [phone] x224
_- Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746988 Project Sample Number: 9225030.001 Date Collected: 08/01/01 17:00
Client Sample ID: SAMPLE 1 (T-1 SOLID) Matrix: Soil Date Received: 08/03/01 11:25
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
Metals
Trace ICP Metals, TCLP Leach. Prep/Method: EPA 1311 / EPA 6010
Date Digested 08/06/01
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
ND
mg/l
0.025
0.7
08/10/01
Barium
1.0
mg/l
0.025
0.7
08/10/01
Cadmium
ND
mg/l
0.0050
0.7
08/10/01
Chromium
ND
mg/1
0.010
0.7
08/10/01
Lead
ND
mg/l
0.025
0.7
08/10/01
Selenium
ND
mg/l
0.025
0.7
08/10/01
Silver
NO
mg/l
0.010
0.7
08/10/01
Date Digested
08/08/01
Mercury, CVAAS, TCLP Leachate
Prep/Method:
EPA 7470 /
EPA 7470
Mercury
NO
mg/l
0.00020
0.7
08/09/01
Volatile Organics, TCLP Leach. Prep/Method: EPA 1311 / EPA 8260
Date Leached 0.00
Wet Chemistry
Percent Moisture
Percent Moisture
-- Flash Point, Closed Cup
Date: 08/17/01
Laborao v Certificationt r IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
Method: X Moisture
26.4 Y,
Prep/Method: EPA 1010 / EPA 1010
RWF 7440-38-2
RWF 7440-39.3
RWF 7440-43-9
RWF 7440-47-3
RWF 7439-92-1
RWF 7782-49-2
RWF 7440-22-4
DJR 7439-97-6
0.7 08/08/01 LYS
0.7 08/10/01 LBG
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
KY Drinking Waver 90090
VA Drinking Water 213
FL NELAP E87627

� I
i
aceAnalyticafm
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746988 Project Sample Number: 9225030-001 Date Collected: 08/01/01 17:00
Client Sample ID: SAMPLE 1 (T-1 SOLID) Matrix: Soil Date Received: 08/03/01 11:25
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
Flash Point >180 deg F 0.7 08/13/01 CBJ
pH
pH
GUMS Semivolatiles
Semivolatile Organics, TCLP
1,4-Dichlorobenzene
2.4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane'
2-Methylphenol (o-Cresol).
3&4-Methylphenol
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date Extracted
GC Semi vol atiles
Pesticides, TCLP Leachate
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Tetrachloro-m-xylene (S)
Date: 08/17/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Prep/Method: EPA 9045 / EPA 9045
7.73 units
Prep/Method:
EPA 3510 / EPA 8270
NO
mg/l
0.75
NO
mg/l
0.013
NO
mg/l
0.050
NO
mg/l
0.013
NO
mg/l
0.30
ND
mg/l
20.
ND
mg/l
20.
NO
mg/l
0.20
NO
mg/l
10.
ND
mg/l
0.50
ND
mg/l
40.
ND
mg/l
0.20
53
X
51
X
88
X
21
X
27
X
63
X
Prep/Method:
EPA 3510 /
EPA 8081
NO
mg/l
0.00050
ND
mg/1
0.00050
NO
mg/l
0.00050
NO
mg/l
0.00050
NO
mg/1
0.00050
ND
mg/l
0.00050
ND
mg/l
0.00050
75
X
0.7 08/16/01 CDE
0.7 08/15/01 19:30 DHJ 106-46-7
0.7 08/15/01 19:30 DHJ 121-14-2
0.7 08/15/01 19:30 DHJ 87-68-3
0.7 08/15/01 19:30 DHJ 118 74-1
0.7 08/15/01 19:30 DHJ 67-72-1
0.7 08/15/01 19:30 DHJ 95 48-7
0.7 08/15/01 19:30 DHJ
0.7 08/15/01 19:30 DHJ 98.95-3
0.7 08/15/01 19:30 DHJ 87-86-5
0.7 08/15/01 19:30 DHJ 110-86-1
0.7 08/15/01 19:30 DHJ 95-95-4
0.7 08/15/01 19:30 DHJ 88.06-2
1.0 08/15/01 19:30 DHJ 4165-60-0
1.0 08/15/01 19:30 DHJ 321-60-8
1.0 08/15/01 19:30 DHJ 1718.51-0
1.0 08/15/01 19:30 DHJ 13127-88-3
1.0 08/15/01 19:30 DHJ 367-12-4
1.0 08/15/01 19:30 DHJ
08/13/01
0.7
08/10/01
TSG
58-89-9
0.7
08/10/01
TSG
57-74-9
0.7
08/10/01
TSG
72-20-8
0.7
08/10/01
TSG
76-44-8
0.7
08/10/01
TSG
1024-57-3
0.7
08/10/01
TSG
72-43-5
0.7
08/10/01
TSG
8001.35-2
1.0
08/10/01
TSG
877-09-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. Inc.
1
Page: 2
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

ace Analytical TM
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suile 100
Huntersville. NC 28078
Phone: [phone]
Fax: [phone]
i
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746988 Project Sample Number: 9225030-001 Date Collected: 08/01/01 17:00
Client Sample ID: SAMPLE 1 (T-1 SOLID) Matrix: Soil Date Received: 08/03/01 11:25
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
Decachlorobiphenyl (S) 110 % 1.0 08/10/01 TSG 2051-24-3
Date Extracted 08/09/01
GUMS Volatiles
Volatile Organics, TCLP Leach.
Prep/Method:
EPA 8260 /
EPA 8260
Benzene -
ND
mg/l
0.020
2-Butanone (MEK)
ND
mg/l
0.40
Carbon tetrachloride
NO
mg/l
0.020
Chlorobenzene
ND
mg/l
0.020
Chloroform
NO
mg/l
0.020
1.2-Dichloroethane
NO
mg/l
0.020
1.1-Dichloroethene
ND
mg/l
0.020
Tetrachloroethene
0.073
mg/l
0.020
Trichloroethene
0.051
mg/l
0.020
Vinyl chloride
NO
mg/l
0.020
Toluene-d8 (S)
89
X
4-Bromofluorobenzene (S)
101
X
Dibromofluoromethane (S)
127
X
1.2-Dichloroethane-d4 (S)
120
X
Date: 08/17/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
0.7 08/10/01 21:19 RWS 71.43-2
0.7 08/10/01 21:19 RWS 78-93-3
0.7 . 08/10/01 21:19 RWS 56-23-5
0.7 08/10/01 21:19 RWS 108-90.7
0.7 08/10/01 21:19 RWS 67-66-3
0.7 08/10/01 21:19 RWS 107-06-2
0.7 08/10/01 21:19 RWS 75-35-4
0.7 08/10/01 21:19 RWS 127-18-4
0.7 08/10/01 21:19 RWS 79-01-6
0.7 08/10/01 21:19 RWS 75-01-4
1.0 68/10/01 21:19 RWS 2037-26-5
1.0 08/10/01 21:19 RWS 460-00-4
1.0 08/10/01 21:19 RWS 2
1.0 08/10/01 21:19 RWS 17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.
Page: 3
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

aceAnalytical'M
www.pacelabs.com
Pace Analytical Services. Inc.
9800 Kincey Avenue. Suite 101
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746996 Project Sample Number: 9225030-002 Date Collected: 08/01/01 17:05
Client Sample ID: SAMPLE 2 (SPENT CAR) Matrix: Soil Date Received: 08/03/01 11:25
Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit
Metals
Trace ICP Metals, TCLP Leach. Prep/Method: EPA 1311 / EPA 6010
Date Digested
Trace ICP Metals, TCLP Leach. Prep/Method: EPA 3010 / EPA 6010
Arsenic NO mg/1 0.025
- Barium 0.68 mg/l 0.025
Cadmium NO mg/l 0.0650
1 Chromium ND mg/l 0.010
Lead NO mg/l 0.025
Selenium 0.034 mg/l 0.025
Silver NO mg/l 0.010
Date Digested
Mercury, CVAAS, TCLP Leachate Prep/Method: EPA 7470 / EPA 7470
Mercury NO mg/1 0.00020
Volatile Organics, TCLP Leach. Prep/Method: EPA 1311 / EPA 8260
Date Leached 0.00
Wet Chemistry
Percent Moisture
Percent Moisture
!--I Flash Point. Closed Cup
Flash Point
_i
pH
pH
GUMS Semivolatiles
Semivolatile Organics, TCLP
1,4-Dichlorobenzene
Date: 08/17/01
Laboratory Certification IDs
NC Wastewater 12
- NC Drinking Water 37706
Sc 99006
Method: % Moisture
43.3 %
Prep/Method: EPA 1010 / EPA 1010
>180 deg F
Prep/Method: EPA 9045 / EPA 9045
7.49 units
Prep/Method: EPA 3510 / EPA 8270
NO mg/l 0.75
08/06/01
0.6 08/10/01
0.6 08/10/01
0.6 08/10/01
0.6 08/10/01
0.6 08/10/01
0.6 08/10/01
0.6 08/10/01
08/08/01
0.6 08/09/01
0.6 08/08/01
0.6 08/10/01
0.6 08/13/01
0.6 08/16/01
RWF 7440-38-2
RWF 7440-39-3
RWF 7440-43-9
RWF 7440-47-3
RWF 7439.92-1
RWF 7782-49-2
RWF 7440-22-4
DJR 7439-97-6
LYS
LBG
CBJ
COE 1
0.6 08/15/01 20:09 DHJ 106-46-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. Inc.
Page: 4
Laboratory Certification IDs
KY Drinking Water 90090
VA Drinking Water 213
FL NELAP E87627

Pace Analytical Services, Inc.
e Analytical 'M 9800 Kincey Avenue. Suite 1051
Huntnlersvrlle, NC 2807878
www.pacelabs.com Phone: [phone]
Fax: [phone]
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746996 Project Sample Number: 9225030-002 Date Collected: 08/01/01 17:05
Client Sample ID: SAMPLE 2 (SPENT CAR) / Matrix: Soil Date Received: 08/03/01 11:25
Parameters
Results
Units
Report Limit
Dilution Analyzed
CAS No. Ftnote Reg Limit
2,4-Dinitrotoluene
NO
mg/l
0.013
0.6
08/15/01
20:09
DHJ
121.14-2
Hexachloro-1.3-butadiene
NO
mg/l
0.050
0.6
08/15/01
20:09
DHJ
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
0.6
08/15/01
20:09
DHJ
118-74-1
Hexachloroethane
NO
mg/l
0.30
0.6
08/15/01
20:09
DHJ
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
20.
0.6
08/15/01
20:09
'DHJ
95-48-7
3&4-Methylphenol
NO
mg/l
20.
0.6
08/15/01
20:09
DHJ
Nitrobenzene
NO
mg/l
0.20
0.6
08/15/01
20:09
DHJ
98-95-3
Pentachlorophenol
NO
mg/l
10.
0.6
08/15/01
20:09
DHJ
87-86-5
Pyridine
NO
mg/l
0.50
0.6
OB/15/01
20:09
DHJ
110-86.1
2,4,5-Trichlorophenol
NO
mg/l
40.
0.6
08/15/01
20:09
DHJ
95-95-4
2,4,6-Trichlorophenol
NO
mg/l
0.20
0.6
08/15/01
20:09
DHJ
88-06.2
Nitrobenzene-d5 (S)
52
X
1.0
08/15/01
20:09
DHJ
4165-60-0
2-Fluorobiphenyl (S)
43
X
1.0
08/15/01
20:09
DHJ
321-60-8
Terphenyl-d14 (S)
99
X
1.0
08/15/01
20:09
DHJ
1718-51-0
Phenol-d6 (S)
19
X
1.0
08/15/01
20:09
DHJ
13127-88-3
2-Fluorophenol (S)
32
X
1.0
08/15/01
20:09
DHJ
367.12-4
2,4,6-Tribromophenol (S)
52
X
1�0
08/15/01
20:09
DHJ
Date Extracted
08/13/01
GC Semivolatiles
Pesticides, TCLP Leachate
Prep/Method:
EPA 3510 /
EPA 8081
gamma-BHC (Lindane)
NO
mg/l
0.00050
0.6
08/10/01
TSG
58-89-9
Chlordane (Technical)
NO
mg/l
0.00050
0.6
08/10/01
TSG
57-74-9
Endrin
NO
mg/l
0.00050
0.6
'08/10/01
TSG
72-20-8
Heptachlor
NO
mg/l
0.00050
0.6
08/10/01
TSG
76-44-8
Heptachlor epoxide
NO
mg/l
0.00050
0.6
08/10/01
TSG
1024-57-3
Methoxychlor
NO
mg/l
0.00050
0.6
08/10/01
TSG
72-43-5
Toxaphene
NO
mg/l
0.00050
0.6
08/10/01
TSG
8001-35-2
Tetrachloro-m-xylene (S)
77
%
1.0
08/10/01
TSG
877-09-8
Decachlorobiphenyl (S)
95
X
1.0
08/10/01
TSG
2051-24-3
Date Extracted
08/09/01
GUMS Vol ati l es
Volatile Organics, TCLP Leach
Benzene
Date: 08/17/01
Laboratory Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
Prep/Method: EPA 8260 / EPA 8260
ND mg/l 0.020 0.6 08/10/01 21:52 RWS 71-43-2
Page: 5
REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
KY Drinking Water 90090
This report shall not be reproduced, except in full, VA Drinking Water 213
without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

aceAnalytical m
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 9225030
Client Project ID: SLS-Greensboro 010305-107535
Lab Sample No: 921746996 Project Sample Number: 9225030-002 Date Collected: 08/01/01 17:05
Client Sample ID: SAMPLE 2 (SPENT CAR) Matrix: Soil Date Received: 08/03/01 11:25
Parameters
Results
Units
Report Limit
Dilution
Analyzed
CAS No. Ftnote Reg Limit
2-Butanone (MEK)
ND
mg/l
0.40
0.6
08/10/01
21:52
RWS
78-93-3
Carbon tetrachloride
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
56-23.5
Chlorobenzene
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
108-90-7
Chloroform
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
67-66-3
1.2-Dichloroethane
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
107-06-2
1.1-Dichloroethene
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
75-35-4
Tetrachloroethene
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
127-18-4
Trichloroethene
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
79-01-6
Vinyl chloride
ND
mg/l
0.020
0.6
08/10/01
21:52
RWS
75-01-4
Toluene-d8 (S)
84
X
1.0
08/10/01
21:52
RWS
2037-26-5
4-Bromofluorobenzene (S)
98
%
1.0
08/10/01
21:52
RWS
460-00-4
Dibromofluoromethane (S)
138
%
1.0
08/10/01
21:52
RWS
2
1.2-Dichloroethane-d4 (S)
130
%
1.0
08/10/01
21:52
RWS.
17060-07-0 2
Date: 08/17/01 Page: 6
Laboratory Certification IDs LaboratoryCertification IDs
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627

r�aceAnaiyticai
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Valt atrix Codes 4-,
MATRIX CODE
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SAM PLE I D
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OIL OL
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Pace Project No.:
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SAMPLE
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2ceAnalyfical­
IT Corporation
2200 Gateway Centre Boulevard
Suite 205
Morrisville, NC 27560
Attn: Mr. Charles Bertz
Phone: [phone]
Lab Sample No: 921523924
Client Sample ID: SAMPLE-1
Parameters
GC Volatiles
Lab Project Number: 9221512
Client Project ID: SLS-Greensboro/010305
k
Project Sample Number: 9221512-001 Date Collected: 03/22/01 10:30
Matrix: Water Date Received: 03/22/01 14:30
Results Units PRL Dilution Analyzed Analyst CAS# Ftnote Limit
Halogen. & Aromatic Vol. Orgs.
Method: EPA 601/602
Prep Method:
EPA 601/602
Dichlorodiflucromethane
ND
ug/l
1.0
1.0
03/23/01
KST
75-71-8
Chloromethane
ND
ug/l
2.0
1.0
03/23/01
KST
74-87-3
Vinyl chloride
ND
ug/l
1.0
1.0
03/23/01
KST
75-01-4
Bromomethane
ND
ug/l
1.0
1.0
03/23/01
KST
74-83-9
Chloroethane
ND
ug/1
1.0
1.0
03/23/01
KST
75-00-3
Trichlorofluoromethane
ND
ug/l
1.0
1.0
03/23/01
KST
75-69-4
1,1-Dichloroethene
ND
ug/1
1.0
1.0
03/23/01
KST
75-35-4
Methylene chloride
ND
ug/l
2.0
1.0
03/23/01
KST
75-09-2
trans-1,2-Dichloroethene
ND
ug/l
1.0
1.0
03/23/01
KST
156-60-5
1,1-Dichloroethane
ND
ug/1
1.0
1.0
03/23/01
KST
75-34-3
Chloroform
ND
ug/l
1.0
1.0
03/23/01
KST
67-66-3
1,1,1-Trichloroethane
ND
ug/l
1.0
1.0
03/23/01
KST
71-55-6
Carbon tetrachloride
ND
ug/l
1.0
1.0
03/23/01
KST
56-23-5
1,2-Dichloroethane
ND
ug/l
1.0
1.0
03/23/01
KST
107-06-2
Trichloroethene
ND
ug/l
1.0
1.0
03/23/01
KST
79-01-6
1,2-Dichloropropane
ND
ug/l
1.0
1.0
03/23/01
KST
78-87-5
Bromodichloromethane
ND
ug/l
1.0
1.0
03/23/01
KST
75-27-4
cis-1,3-Dichloropropene
ND
ug/l
1.0
1.0
03/23/01
KST
10061-01-5
trans-1,3-Dichloropropene
ND
ug/l
1.0
1.0
03/23/01
KST
10061-02-6
1,1,2-Trichloroethane
ND
ug/l
1.0
1.0
03/23/01
KST
79-00-5
Tetrachloroethene
54.
ug/l
1.0
1.0
03/23/01
KST
127-18-4
Dibromochloromethane
ND
ug/l
1.0
1.0
03/23/01
KST
124-48-1
Bromoform
ND
ug/1
1.0
1.0
03/23/01
KST
75-25-2
1,1,2,2-Tetrachloroethane
ND
ug/l
1.0
1.0
03/23/01
KST
79-34-5
Methyl-tert-butyl ether
ND
ug/l
1.0
1.0
03/23/01
KST
1634-04-4
Diisopropyl ether
ND
ug/l
1.0
1.0
03/23/01
KST
108-20-3
Benzene
2.1
ug/l
1.0
1.0
03/23/01
KST
71-43-2
Date: 03/26/01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1

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MATRIX CODE w w Preservatives
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