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NCG060095_Monitoring_20200116
For guidance on filling out this form, please visit: htt1�://portal.ncde.nr.orItiveh/wdlwsisii/rl dU eSSw#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0/ or Certificate of Coverage No.: N/C/G/ 0/ 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: Date of Inspection: 9 ® n t� Time of Inspection: 3113T Total Event Precipitation (inches): I . Ll . n Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). ........................... .......... ...._............................ ..... ............. .......... .......... . .. .. .......... A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. .......... _ ........ .............. ..... . ........ ............ ............ ...... .................... ......... ......... ............ By this signature rI certify that this report is accurate and complete to the best of my knowledge: (Signature df Permittee or Designee) 1. 9esor4ption: t '.l Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that V occur within the outfall drainage area: �? (east \d N k Ella rotj 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: r j- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Ao Page 1 of 2 S WU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: b 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes Eo 8. Is there an oil sheen in the stormwater discharge? Yes nNo 9. Is there evidence of erosion or deposition at the outfall? Yes &No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 For guidance on filling out this form, please visit: pdessN.y#tab-4 Permit No.: N/C/G / 0 / 6 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 6/ 0/ 0/ 9/ 5/ Facility Name: Goulston Technologies, Inc. County: Union Phone No. 704-296-6427 Inspector: _ LLO, ryl�r Date of Inspection: i — 1 Time of Inspection: 3 o Total Event Precipitation (inches): 1 . q t Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be perfonned during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this si nature, I certify that this report is accurate and complete to the best of my knowledge: �2,z z� of Permittee or 1. � 1�m� �c��G►r . Structure (pipe, ditch, etc.) pipe Receiving Stream: Bearskin Creek Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 1y. r 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): nog Page 1 of 2 SWU-242-20120613 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe (\( Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-20120613 January 13, 2020 Attention: Lily Kay North Carolina Department of Environmental Quality Division of Energy, Mineral & Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Dear Lily, Results from the roof run off stormwater sampling requested during our October 22, 2019 Compliance Evaluation Inspection are attached. The pH for both samples was 6.9. Please feel free to contact me at ymckinney goulston.com or 704-296-6427 if there are any questions or if additional information is needed. � su�' r-1.\ Veronica McKinney Human Resources Ma ager 700 N. Johnson St. I Monroe, NC 28110, USA P.O. Box 5025 1 Monroe, NC 28111-5025, USA PHONE 704-289-6464 1 FAx 704-296-6400 1 www.gouiston.com aceAnalytical- www.pacelabs.com t January 07, 2020 John McTaggart Goulston Technologies 700 N. Johnson Street Monroe, NC 28110 RE: Project: RAINWATER ROOF DISCHARGE Pace Project No.: 92458747 Dear John McTaggart: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 26, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Ms. Sally Duncan, Goulston Technologies Veronica McKinney, Goulston Technologies John McTaggart pECRp� �9BORaio% REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 aceAnalytical www.pacelab$.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 aeeAnalytieal j www.pacelabs.com f t SAMPLE ANALYTE COUNT Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92458747001 RAIN WATER ROOF DISCHARGE A EPA 1664E HH 1 PASI-C SM 2540D-2011 CJL 1 PASI-A SM 5220D-2011 LEF 1 PASI-A 92458747002 RAIN WATER ROOF DISCHARGE B EPA 1664E HH 1 PASI-C SM 2540D-2011 CJL 1 PASI-A SM 5220D-2011 LEF 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 12 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RAIN WATER ROOF DISCHARGE A Parameters Lab ID: 92458747001 Collected: 12/23/19 15:35 Results Units Report Limit DF Received: 12/26/19 11:45 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/06/20 13:30 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND mg/L 2.5 1 12/27/19 15:52 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/31/1912:01 12/31/19 15:48 Sample: RAIN WATER ROOF Lab ID: 92458747002 Collected: 12/23/19 15:35 Received: 12/26/19 11:45 Matrix: Water DISCHARGE B Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/06/20 13:35 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids ND mg/L 2.5 1 12/27/19 15:53 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/31/19 12:01 12/31/19 15:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalyfical www.pacelabs.com QUALITY CONTROL DATA Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 QC Batch: 517897 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92458747001, 92458747002 METHOD BLANK: 2772436 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 01/06/20 13:24 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2772437 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 37.6 94 78-114 MATRIX SPIKE SAMPLE: 2772438 92458866001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 5.3 40 44.9 99 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 aceAnalytical www.pacelabs.com i QUALITY CONTROL DATA Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 517022 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92458747001, 92458747002 METHOD BLANK: 2769232 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/27/19 15:49 LABORATORY CONTROL SAMPLE: 2769233 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 254 102 90-110 SAMPLE DUPLICATE: 2769234 92458634003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 830 1070 25 SAMPLE DUPLICATE: 2769235 92458746001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 69.0 70.0 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /07/2020 03:58 PM without the written consent of Pace Analytical Services, I.I.C. Page 6 of 12 aceAnalyticaiIV www.pacelabs.com i QUALITY CONTROL DATA Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 QC Batch: 517274 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92458747001, 92458747002 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2770044 Matrix: Water Associated Lab Samples: 92458747001, 92458747002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 12/31/19 15:42 LABORATORY CONTROL SAMPLE: 2770045 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 744 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2770046 2770047 MS MSD 92458595001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 138 100 100 234 238 96 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2770048 2770049 MS MSD 2626933001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 28.2 100 100 138 122 109 94 90-110 12 R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 aceAnalytical www.pacelabs.com t QUALIFIERS Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /07/2020 03:58 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: RAIN WATER ROOF DISCHARGE Pace Project No.: 92458747 Lab ID Sample ID QC Batch Method 92458747001 RAIN WATER ROOF DISCHARGE EPA 1664B A 92458747002 RAIN WATER ROOF DISCHARGE EPA 1664E B 92458747001 RAIN WATER ROOF DISCHARGE SM 2540D-2011 A 92458747002 RAIN WATER ROOF DISCHARGE SM 2540D-2011 B 92458747001 RAIN WATER ROOF DISCHARGE SM 5220D-2011 A 92458747002 RAIN WATER ROOF DISCHARGE SM 5220D-2011 B Date: 01/07/2020 03:58 PM Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch Analytical Method 517897 517897 517022 517022 517274 SM 5220D-2011 517274 SM 5220D-2011 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 517467 517467 Page 9 of 12 Document Name: Document Revised: February 7, 2018 ' i ,81ce lyflCal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No,: Issuing Authority: j F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood Huntersvi�e0 WOMMINMEM Client Name: +' f / Project #: C_i7('(/(Sr 0A Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client ❑ Commercial ]P e []Other; Custody Seal Present? MY— o� Seals Intact? ❑Yes QNo Date/initials Person Examining Contents: CJ E2� ?racking Material: ❑Bubble Wrap �26ubble Bags ;None U Other Biological Tissue f ozen? Thermometer, / Dyes ❑No �EfN/A �IR Gun ID; 921058 Type of Ice: Wet ❑Blue ❑Nrine Cooler Temp (°C): — Correction Factor: Add/Subtract ('C) Q.d°C Cooler Temp Corrected ('C): ` ` Temp should be above freezing to 6'C []Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated So1112-N/A,water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, (—lYes r INo Inehidina Hnwaii and Puarta Rirnl) MY— ntdm Ralelgh❑ Mechanicsville❑ ,.. Chair of Custody Preseni7 Yeess ©NoLiN/A :Comments/Discrepancy: 1. -I I Samples Arrived within Hold Time? QYes []NO []N/A 2. Short Hold Time Analysis (t72 hr.)? Des No ❑N/A 3. Rush Turn Around Time Requested? C)Y�es ®IVO ❑N/A 4. Sufficient Volume? t yes ('"t CJN/A S. 6. Correct Containers Used? !fYes 7,;No ❑N/A -Pace.ContainersUsed? Qie5 ]No ❑N/A Containers Intact? Yes ONo ❑N/A 7. Dissolved analysis: Samples Field Filtered? [ jYes (]Now ❑N/A Is. Sample Labels Match COC? f[j4es ❑No -Includes Date/Time/ID/Anaiysis Matrix`. ❑N/A 9. ` Headspace in VOA Vials (>5-6mm)? ❑yes No IA" 10, Trip Blank Present? Trip Blank Custody Seals Present? ❑yes ❑Yes CjNo " QN/g ❑No " �N//A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: C Project Manager SCURF Review: 13,71. V 7/ Project Manager SRF Review: s Date/Time: FleldData Required? Des QNo Date: Date Page 10 of 12 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 n A aCeAnalyfical Document No.: Issuing Authority: ,t f-CAR-CS-033-Rev,05 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle .p 2 - N H D U z t Y' -g 0) V W2 2 2 d S v a t,a '.. A Z v 2 w N v y a S 2 4 Z .+ x d z v O N 2 v z y. w ar aZr Rl N .Ta, , S a a V N 4 ?. M Q a. Z Ss to \ z u u N a a i O N O ¢ p —0 �tl C n c O Ot vO a Q z ._. O Z fitly o y V x c c A n D D j C S Z � u U S N S S N r1 n, y, y p^�, 6 = m j u 'a 'G v v_ u s �EE O T �. j = Q .x"- aJ _. .� •� nr E .c w a a a n a —° G° E E E E d .a E d N d O Q O d O 6 n va N a 4 u E J E J E J E _m r1 E E J E J E a Q `v 4 a` E .� v J E m �I E > E > E J E 4) 3 ffi *3 J E J E .J E J o E J E v5 rNl O N O CD .° L W vn O ul H ryLA 'i y} "{ rl = ry vOi N �, O N+M.. `z^ 6 O O .N-i O N u0i O O O •QQ��� A E a a M N r tN-. M N ct U a O i T W 7 M v` rl V1 M 4 M S Q E- Ol O Ol 0. m = 4 Y V p iV 4 M p�p (�� 0. a M . M 0. M m 0. Com 0. v la 4 V' Q t'1 4 0 4 t7 4 t7 4 W Ct U >>A 0 0 O i �,. i In N ro l9 4 J > l7 cc m m Go 2 � i 3 i� 5 N\N 'I b _. \N\ "\N 7 v g rr 10 F—* 11 — 12 -N I L 1 H Ad'ustment Log for Preserved Samples Sample t0 Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot It Note: wnenevertnere Is a discrepancy arteCUrtg wortn t.aronna [ompnence bampIcn, u wpp v, —1 —•,., ..,,, .,c wn. w u�c rvv,.w .,o,..,,,,a �..,,,,,...�, ,.•-. 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