WQ0015102_Annual Reports (2014/2015)_20160809

)�- 0 1, 5' AA)A)L4 41— i��a1-1
Rogers, Michael
From: Wang. Shuying
Sent: Tuesday, August 09. 2016 8.32 AM
To: Rogers, Michael
Cc: Watts, Debra; Wang, Shuying
Subject: FW. Annual Reports
Attachments: Annual Report for 2014.pdf:.Annual Report for 2015.pdf
Good Morning Michael,
For your record and review, I am forwarding two annual reports (2014 and 2015) for WQ0015102 !, w-hich was
requested from Permittee during WSRO biannual compliance review.
If you have any questions; you � may directly contact Flora D'Souza, Shield Engineering, Inc., the operator or consultant of
the permittee or me.
Shuying Wang, P.G.
Hydrogeologist
NC
Phone:: 14r, 6-9
Fax:
Emaii: 5tiil�i;l°_lb'e.lE dnCGEi
Vvinston-SalEr, f:� ._-1._..
From: Flora D'Souza[mailto:[e-mail]
Sent: Monday; August OS, 2016 5:13 PM
To: Wang, Shuying <shuving.v„[e-mail],,,>
Subject; Annual Reports

Flora J. D'Souza, CHMM
Project Manager
Shield Engineering, Inc.
4301 Taggart Creek Road
Charlotte, NC 28208
Phone: [phone]
Cell: (7D4) 519-5054
Fax: [phone]
www.shieldengineering.com
This message is intended only for the use of the addressee and may contain information that is PRIVILEGED and CONFIDENTIAL,
and/or may contain ATTORNEY WORK PRODUCT. If you are not the intended recipient, you are hereby notified that any
dissemination of this communication is strictly prohibited. If you have received this communication in error, please erase all copies of
the message and its attachments and notify us immediately. Thank you.

. ___ * T
kS11IEL_D_
GINEERING, INC.
August 8, 2016
Ms. Shuying Wang, P.G.
NCDEQ — Winston-Salem Regional Office
Division of Water Resources
450 W Hanes Mill Road, Suite 300
Winston-Salem, NC 27105
Ref: Annual Report for 2015
Groundwater Remediation Non -discharge Permit WQ0015102
Hill Oil Co. — Walser's Service
6419 N. NC Highway 150
Lexington, Davidson County, North Carolina
Shield Project 1990018
Dear Ms. Wang:
Shield Engineering, Inc. (Shield) is pleased to submit this annual report summarizing the effluent
discharged into the injection well during 2015. Based on the Non -discharge Permit WQ0015102,
the annual report should contain the following:
• Volume and injection pressures of effluent discharged into the injection well
• The summary results of related groundwater, influent, and effluent monitoring
• Isoconcentration and water level contour maps
The Air Sparge (AS), Soil Vapor Extraction (SVE), and Groundwater Recovery System (GRS) was
installed and commenced operation on January 28, 1999. The Air Sparge system includes two 2-inch
diameter sparge wells (AI-1 and AI-2). The Groundwater Recovery System includes one vapor
enhanced groundwater dual phase recovery well (VERW-1). Treated groundwater is discharged in
an injection well (MW-3).
Approximately 54,891 gallons of groundwater was treated and discharged into the injection well
during 2015. The summary of GRS data, analytical results, and mass of total contaminants removed
are presented in Table 1. The mass of BTEX (benzene, toluene, ethylbenzene, and total xylenes)
contaminants removed is presented in Table 2. Injection pressures were not recorded during 2015
because the system was originally designed with a high level shut off float inside the injection well
and pressure gauges were not required. However, due to the high level shut off float continually
shutting the system down when the groundwater inside the injection well reached the high level, the
float has since been removed and the injection well sealed. Shield plans to install a pressure gauge
to the system in August 2016 and will begin recording pressures to the injection well at that time.
4301 Taggart Creek Road Telephone [phone]
www. shieidengineenng.com
Chadotte, NC 28206 Fax [phone]

6
Walser's Service
Lexington, Davidson County, North Carolina August 8, 2016
Annual Report for 2015 Page 2
Site wide sampling is conducted in monitoring wells MW-1, MW-2, and MW-4 through MW-9
during May and November each year and MW-1 is also sampled in February and August with semi-
annual active remediation monitoring reports being submitted to the NCDEQ Winston-Salem
Regional Office in June and December. Groundwater and influent and effluent laboratory data for
2015 was presented in the June 30, 2015 and December 17, 2015 Active Remediation Monitoring
Reports. As shown in Table 3 — Summary of Historical Analytical Results, generally the only
constituent above the 15A NCAC 21, Groundwater Standards (2L Standards) during 2015 was
naphthalene and only in monitoring wells MW-1 and MW-2 with the exception of total xylenes in
MW-1 in February and May 2015. Attached are Figure 4 (Groundwater Elevation Contour Map)
and Figure 5 (Naphthalene Isoconcentration Map) from the December 17, 2015 Active Remediation
Monitoring Report.
If you should have any questions, please contact the undersigned at [phone].
Respectfully yours,
Shield Engineering, Inc.
Flora J. D'Souza, CHMM
Project Manager
cc; Mr. Mayne Hill, Hill Oil Company
Mr. Michael Rogers, NCDEQ
HAProjects\1999\1990018 Walsees\Annual Reports\Annual report for 2015.doc
t
v i1, L
David A. Stoner, P, 3.L C)
Senior Principal r,, D
Registered, NC# 1427�''`��+i
*SHIELD

TABLE 1; Summary of GRS Data and An *Iytic3 I Results-Grnundw air r Recovery S,,stero
Walser i Service
Highway ISO Lexi.%tar, NC
NCDENR GW[014876
DATE
SAMPLE
LOCATION
BENZENE
TOLUENE
ETHYL-
BENZENE
XVLENES
TOTAL, BTEX
MTBE
V PH CS -Cs
Aliphad,,,
VPH C9.Cl1
Allplisdes
VPI-I C9-CIO
Aromatics
ESTIMATED
TOTAL
GALLONS
TREATED
MASS Of TOTAL s rEx
REMOVED (lb/day)
0 1 (1 K.F99
A F
$600
9900
550
4100
2305O
ND
1 1foll
NO
610
NA
NA
EFF
96
70
41
29
236
F
14000
11000
3100
NA
NA
I wo
-,mfi
930
9400
49330
NO
ti2000
12000
1201
NA
NA
I10
52
NO
ND1
162
20
1 "iflo
1700
500
NA
NA
MOO
41000
2700
1 1 R000
-RD"Oo
600
11 ()O()G
10000
11
NA
NA
FYI`
I 10
95
2 t
o(I
322
49
R?V,.
I MO
NA
NA
0/25199
I \1 1",
4600
76GJ
lOo
2500
15190
N 0
72000
11000
660
A230.7
NA
; FF
U
R4
to
48
225
NO
6600
i 000
550
NA
NA
04!09IY9
INF.
201)00
310
21100
16000
39330
ND
X0()O0
2Ci100
0400
NA
EFF
SS
i5
12
40
)42
ND
05 D 0
WOO
.510
—1101(11)
NA
NA
(14120!99
INF.
21000
36000
2100
12000
71100
74D
Xwo
24000
5900
i 1 169'3
NA
EFF
130
61
1
61
3s
94
320
-, 1
171�0
1400
512
NA
NA
05/1 W99
INF
18000
37000
2500
150DO
72300
ND
71,000
29000
A900
119860
NA
EFF
60
17
(13
AIR
22
4700
MOO
730
NA
NA
061091,99
INF.
21000
3901,11)
114000
79300
290
66000
22000
3900
2722R.4
NA
EFF.
9
36
24
10
99
1. 1 D
29DO
NO
2,qL)
NA
00.11
97121/99
INF
ll000
200oo
.1100
7.3000
3 7 t 00
t50
I 10 DOO
2RO000
220000
57722,5
NA
EFF.
q
II
53
193
NO
1400
700
250
NA
0340
OX/06/94
INF
R200
14000
1300
15000
39500
NO
32000
170,10
4900
93783,0
NA
F.FF,
45
12
9
24
89
26
13000
11000
3700
N A
0,520
(1141,11.199
EFF
NA
NA
NA
NA
NA
NA
2700
500
120
NA
NA
09116)99
INF.6600
12000
RIO
9400
28920
NO
24000
12000
4300
1147152
NA
EFF,49
36
14D
47
132
NO
21300
250
100
NA
0 101
)012U99
INF.
4200
�500
920
$700
22220
NO
20000 1
8400
5600
139940,0
NA
EFF
43
44
17
81
185
12
2700
640
300
NA
0. 133
11/11199
INF.
5900
11000
040
9JR0
28140
NO
26000
10000
4900
14 10?79
NA
Err
NO
NO
NO
ND
NO
NO
NO
ND
NO
NA
0012
1212 t"
INF,
4100
22000
1400
22000
.51700
NO
90000
92000
79000
1490241
NA
EFF.
ND
NO
ND
NO
NO
NO
ND
NO
NO
NA
01,0115
ol"Woo
INF
5610
1 '> ") (-r,
1100
1 Out)
IR900
NO
2! o0o
13000
11000
149119.5
NA
Err
ND
NO
NI)
NO
NO
NO
ND
NO
NA
0.0006
wrl-'i1.' rent 4p,,WAr,wl ':t,,pi,,,.20l5`.i'le,,,%:,,,:,n41,,C.;i(1);,1;�,An,uaI,p12115s1s h., 1 oI 10

TABLE]: S....,y eFGRS Dah and Aaslylical RmIfs-G,—d—w Reca—y Ssa —
W als,"s 5—iee
I-lf-h ay 150 U.i,gi— NC
NCDENR GWINN141176
DATE,
SAMPLE
LOCATION
BENZENE
TOLUENEETOYL
BENZENE
XYLENES
TOTAL BTEX
MTBF.
/fI CS-CX
Aliphmics
VPN C9-C12
Aliphatic,
VP"C9-CIO
A..mtks
ESTIMATED
TOTAL
.GALLONS
TREATED
MASS OF TOTAL BTE.X
REMOVED 04/day)
02/23!00
INF
S900
13000
1500
Hoop
31460
`:D
31f300
IS000
R200
1541173
NA
EFF
ND
ND
\0
ND
ND
VD
230
ND
NO
NA
004'
0/1014)
INF.
7300
11000
1400
10000
<9700
UO
0000
15000
9000
156635.3
NA
EFF
ND
NO
1.110
ND
ND
VD
41�)
NO
ND
NA
0.031
04/12.910
INF
6201
29000
44FJ
29000
67603
\11
95009
97000
59000
159560.3
NA
EFF
ND
ND
ND
ND
ND
`:D
1900
ND
ND
NA
QOS7
05/30/00
INF,
r:;!0
1000
71Cnr
21700
ND
3i00D
15000
9500
16 ?ORS 7
NA
EFF
NU
N)
NO
ND
ND
NO
2400
NO
ND
NA
000
66;2 t'00
INT
4900
95J0
910
6400
21710
50
32000
12000
7100
167116.8
NA
FFF.
NO
NO
NO
ND
NO
NO
960
ND
NO
NA
0031
n.nX,'00
1yr
ti600
F600
12e0
7F00
24200
210
49000
15000
6700
1691700
NA
F.FF
N,)
ND
NO
ND
ND
NO
2?CO
\D
NO
NA
02,29i00
I\F.
4100
790n
790
3300
IR190
NO
20000
15000
6200
173926.4
NA
EFF,
I2
ND
NO
ND
1.2
ND
i609
ND
ND
NA
0019
09i2)1!00
INF
4300
7900
720
5100
17920
95
24000
""1
5400
176A 75 1
NA
EFF
NO
ND
NO
ND
ND
ND
;200
';D
NO
NA
0014
10/23/00
INF
2000
6800
?9P
5.1
157"
59
21000
10000
6000
179307.0
NA
EFF.
.51
ND
ND
ND
51
ND
lA00
ND
ND
NA
0,002
I IIOX!00
INF
3700
7300
790
5ToD
17490
110
37000
11000
14000
179335 0
NA
EFF.
16
ND
ND
ND
16
NO
4400
ND
ND
NA
0,009
12/f141,00
INF
4100
11000
1200
A400
24700
110
33000
13000
9500
179859 0
NA
EFF.
23
1.3
`[,
NO
24,3
ND
2100
NO
ND
NA
0. 00414
61/36101
1NF.
4900
11000
1100
9000
25200
ND
33D00
10000
11000
1R4199 1
NA
EFF.
70
ND
',D
140
?0
ND
2300
NO
ND
NA
0 01 714
02n7101
fNF
5700
12000
1100
940A
27200
120
231,00
NO
66M
196920.9
NA
EFF
NO
ND
`:D
ND
ND
ND
1600
NO
ND
NA
009961
03/27/01
INF
6400
12060
1104
7800
2A300
110
76000
NO
l; 10i1
206401
NA
EFF
24
I I
NO
ND
25.1
ND
1400
NO
ND
NA
0,09016
04/24;01
fNF
1600
9100
790
6600
200NO
67
22000
NO
6000
2�"OJI
NA
EFF
51
39
1.1
27
94,9
NO
1600
1140
ND
NA
005324
09/23/01
INF
4i90
1;'i00
530
69U0
24330
ND
20000
6000
3300
222930.1
NA
EFF.
ND
ND
ND
N'D
NO
ND
4100
230
NO
NA
0:'14186
11 >111'p;11n 14 .14, K r A71"orI K, ;01; l—,i�e ar01.f 1'...'70,1,-A-,.., ,613 s's P,re 2M'IU

TABLE I: Summary e(GRS Oats and Aaal)•tical Results-Gr4unNater Recovery System
Walser'. Servkr
HiBMtay 130 Luin0t4a. NC
NCDENR GWIAI4976
DATE
SAMFLL
LOCATION
BENZENE
TOLUENE
ETHYL-
BENZENE
XVLENES
TOTALRTEX
MIRE
VPHCS-CA
Aliphatirs
VPHC9-Cl2
Aliphatics
VPHC9-CI8
Arenutics
ES I I MA,m)
TOTAL
GALLONS
THE 7 D
MASS OF TOTAL STEX
REMOVED(Ib/day)
06/22101
INF
4600
79ii0
630
4790
17830
ND
IRn00
r5000
2806
227042.7
NA
EFF,
15
6..9
35
49
174.8
NO
5100
lift
NO
NA
0,2142
(1707101
INF.
5000
9900
FPO
6900
21690
S0
32000
96M
3900
2229126
NA
EFF.
76
4.1
35
40
155.1
1 NO
6300
W
75
1 NA
03134
O8114/01
INF.
3700
R300
940
6100
19040
NO
26000
83M
4700 1
23302R.0
NA
EFF,
NO
1.2
2R
28
5R,2
NO
5300
450
ND
NA
0,2559
0911 till
INF,
4100
9100
9A0
6100
20280
NO
25000
7F90
5900
2155502
NA
EFF.
41
3.3
17
32
113 3
NO
45n-)
360
NO
NA
0.2622
10110/01
INF,
33
75
9.2
47
1632
NO
1900n
7100
4600
237992.7
NA
EFF.
NO
NO
NO
25
25
ND
'1800
170
NO
NA
DOW
111011/91
INF.
7700
720J
900
.5000
15900
69
19000
7900
5300
259971,7
NA
EFF.
30
16
12
IS
SR6
6.9
3100
ND
NO
1 NA
01976
01014102
(NF.
3400
990n
1700
9500
24500
A6
23000
10000
4R00
2646195
NA
EFF
NO
NO
NO
NO
NO
ND
2700
no
NO
NA
0.0366
01/28102
MF
2400
two
2900
15000
.33300
NO
33000
+2000
1"00
266519.1
NA
V
NO
NO
NO
NO
NO
ND
1700
176
ND
NA
00220
02175/02
IMF .
3300
16000
4100
'loop
46400
ND
34000
.31000
15n00
267079,3
NA
Err.
21
26
23
24
76.6
NO
2600
340
)6
NA
00077
01/2A/02
NF.
2900
9100
1600
13000
26500
ND
20000
11000
9100
270300.1
NA
EFF
i R
2 (,
9 6
14
442
NO
1500
ND
NO
NA
0 0229
04/E3102
MF.
2000
Ao00
1800
12000
23900
NO
24000
1MOO
10000
272909.1
NA
EFF.
22
14
19
1!
619
*,D
460
VO
NO
NA
0.0197
OS/20102
INF,
2700
11000
1900
14000
29600
ND
27000
14000
1!OOn
274800,0
NA
EFF.
27
I.F
20
12
60.8
ND
1000
NO
ND
NA
(10114
06/25102
INF..
4900
Flo
5800
11310
ND
23000
17000
7400
2742829
NA
EFF,
15
a
NO
I
61.9
ND
1100
ND
NO
NA
00148
07116102
INF
r'('p
5800
IIN)
6100
14900
NO
I ND
NO
9900
287430,6
NA
EFF,
30
NO
26
56
5.5
850
ND
ND
NA
00540
081I2i02
NF.
1600
4000
820
4300
10720
55
NO
ND
!?Oo
7119214
NA
EFF.
21
3.2
NO
12
362
ND
R30
VD
`:D
NA
00900
09125102
INF.
1100
2740
400
3800
8000
ND
I1000
6X00
i 00
)29A 10,2
NA
EFF,
22
64
ND
ND
2R,1
ND
930
140
ND
NA
0,0270
,:1'n, 11,+VM 90061 N 8 T+ fl -2' 1 \I:Icraiinn and lr.l:-i:,q an -A,. —I rpr 201 i x1. P.g, ? of 10

TABLE I: S.—y of GRS Dan and AW) lic.l Reudb-Gro-d-- Rrm.very Syetem
Walser'. Service
likhvny 150 Lexingrnn, NC
NCDENR G3VI R 14976
DATE
SAMPLE
LOCATION
BENZENE
TOLUENE
ETHYL-
BENZENE
XYLENES
TOTAL BTF..X
MTSE
VPH C5-CA
Aliphark,
VPH C9-Cl2
AliphRtln
VPH C9-CIO
A,.—.ke
ESTIMATED
TOTAL
GALLONS
TREATED
MASS OF TOTAL BTEX
REMOVED(lb/dn3)
WWII?
INF.
1400
.:'-90
140
1500
5790
ND
\D
NO
11000
340131.2
NA
EFF.
NO
26
ND
12
14.6
NU
7 G
'60
.3,,
NA
0.0166
1112110E
INF
1100
1900
:20
1700
4R20
ND
6500
2R00
2700
35RI00 2
NA
F.FF.
NU
26
NU
25
276
NO
900
220
NO
NA
0.0266
12/16/03
INF
900.
2000
340
2500
51,40
NO
ND
4100
161622 2
NA
EFF
10
NO
21
33
NO
S50
NO
NO
NA
0,11000
01712/03
INF
1000
AAr,,;7
670
4400
10670
NO
9800
NO
6900
375824.1
NA
ErE
f9
2,3
NO
1I
3.1.3
NO
660
NO
ND
NA
0.0467
02W!03
I\f
1000
3900
410
3100
$410
ND
i0000
NO
4000
3119811.0
NA
EFF.
19
7.2
ND
f4
40.2
NO
610
*:0
NCI
NA
0.0273
0401103
IN
761
17f0
240
110
1410
7
47,10
9:?0G
UC0
4!91903
NA
EfF.
1-.2
NO
NO
NO
i.2,
1.11
590
560
NO
NA
0,0114
04/24703
INF
620
1$f
180
1540
4140
NO
4300
91100
1200
4176979
NA
EFF.
11
2.2
ND
ND
3.7
ND
440
300
NO
NA
0.0221
06/05/03
INF.
3n0
17Ud
220
I670
7970
NO
3600
7200
I700
447(,"A
NA
EFF.
ND
1.9
NO
4
5 A
ND
540
2"
NO
NA
0.0151
06/2V03
INF.
+'3
1900
270
i A'
4430
NO
31.11
6700
1400
455426 9
NA
EFF.
I s
3.4
NO
41
9.9
NO
490
230
ND
NA
00151
07/21/03
fNF.
430
1700
270
4530
NO
4100
11000
1500
455712.0
NA
EF'F.
NU
22
NO
s
'7 4
NO
510
330
NO
NA
0.0004
09/30!03
f:1 F.
6R0
2.500
no
2270
5740
NO
1900
moo
1200
194097,4
NA
EFF.
7..0
..11
ND
10
17.7
ND
910
410
.300
NA
0.0295
10/IV03
fNF,
150
600
76
AM,
1426
ND
NO
6400
ND
5077920
NA
EFF
IA
NO
ND
ID
1,4
NO
2200
970
270
NA
0110
11120103
E\F
550
NO
ND
1900
2450
NO
6600
4600
2400
515102.0
NA
EFF
2.1
62
ND
NO
9,1
ND
13000
4600
1300
NA
00050
12/04103
INF
7R0
290fi
260
1900
5R40
NO
17000
13000
6400
5253974
NA
EFF
ND
NO
ND
ND
NO
NO
9900
3700
NO
NA
00356
01/211I04
1N F.
440
1700
140
1500
3780
ND
6600
6700
NO
545912.0
NA
CFF.
ND
NO
NO
NO
ND
NO
2600
1400
510
NA
0.0117
02/11104
INF
430
2100
260
IRf70
4590
M1
6500
A100
ND
549009,0
NA
rrf
NO
NCl
NO
ND
NO
NO
6400
1100
1500
NA
000�7

TABLE. 1: Summary n1CRS Data and An.h.l cal Resalf.-Crnandoa;er R...... y Spsfcm
W.1ser's Service
150 Wi.g1m NC
NCDENR GN'1414876
1) 1TF
SAMPLE
LOCATION
BENZENE
TOLUENE
ETHVL
BENZENE
XYLENES
TOTAL RTEX
MTRE
VPH C5-CA
Aliphafics
VPH C9.02
Aiiphalias
VPH C9-C10
Arnmaf{es
ESTIMATED
TOTAL
GALLONS
TREATED
MASS OF TOTAL BTEX
REMOVED (IMdq)
Uiz5/0t
INF.
600
3?0q
400
2700
1400
NO
15000
15000
7200
5550242
NA
EFF,
NO
ND
ND
20
20
ND
2900
2200
Rao
NA
0.0019
0410M4
INF
590
11?011
.110
2000
6200
ND
10000
RA00
3A00
561975.2
NA
EFF
I NO
NO
I ND
ND
ND
NO
2600
1700
100
NA
0.0167
05/86/04
INF,
G60
2300
250
IR00
3010
NO
7100
6400
1000
566659 2
NA
EFF.
NO
NO
ND
NO
NO
ND
2900
2900
NO
NA
0.0095
06/22W
INF,
2.00
11,000
1,400
7.900
22.900
NO
24000
21,000
9,5DO
568,175 20
NA
EFF
ND
4.2
NO
12.4
166
NO
950
900
430
NA
00055
Rr9/2007
INF.
ND
16 5
NO
NO
16 5
NO
t39
462
329
574,732 20
NA
E Ff.
14
NO
It
212
NO
523
76R.
420
NA
000003
9/6/2007
IN
2n6
;sni''
211
1390
4,307
ND
4970
6R50
1790
N75nR3
NA
EFF,
ND
5
ND
10
15.0
ND
124
4"
251
NA
00004
I It 1/7009
INF,
430
6300
R60
4700
12.290
ND
20000
1.3001
N00
57S.214
Na
EFF
ND
2
ND
7.2
92
ND
550
2S0
120
NA
00001
2121/200R
iNf
294
3950
374
2260
6,76R
NO
7400
I110n
2450
57.5 4R3
NA
CI°F.
NO
NO
NO
NO
ND
ND
IR'.
275
126
NA
00007
5%201200A
INF,
209
2530
277
2240
5.256
1 NO
33R0
62110
12"
580,9R?
NA
EFF,
49.4
492
435
$00
1,0949
ND
i? :;
28110
539
NA
00052
(V10/200R
fNF.
256
4<.30
545
5160
10,192
ND
NA
NA
NA
592.455
NA
EFF.
NO
NO
FJI)
NO
NO
ND
NA
NA
NA
NA
O.0060
7/79/2009
POR
100
79w
?63
2260
5,743
NO
509.0
15800
1720
J91.445
NA
EFF,
20.7
315
27.9
2343
59?.9
I,R
441
12400
160
NA
0. 00p0
9!12!200R
IN'F,
86..2
090
124
1177
2,717.2
NO
2SR0
6580
1190
591704
NA
EFF..
ND
NO
NO
ND
NO
NO
NO
NO
NO
NA
00001
10/21/2008
1NF,
93 5
1620
164
1390
3,2679
NO
3130
5RR0
1120
S91,A59
NA
EFF.
i9
294
265
277
616.5
2.3
519
1330
264
NA
00001
2!24/2009
IN,
99 4
1290
144
927
2,459.4
NO
2250
4920
719
592,254
NA
EFF.
NO
NO
6;p
ND
NO
ND
NO
NO
NO
NA
00002
31f9/2009
INF,
6
96.6
11 5
146
260A
ND
532
1?60
137
594.691
NA
EFF
NO
NO
NO
ND
NO
ND
ND
NO
NO
NA
00002
11-109
INF.
696
364
95.9
411
939 3
7.$
20R0
5460
921
.194,711
NA
EFF,
ND
NO
ND
NU
ND
^iD
ND
NO
NO
NA
00000
r1,..,.r.;.':::d:lvW,;::".:Anm:nlR::1:m1.:Aum;n;kp,r1.2n::itf:l�vn;-:;,nan<I!nr.,:n-U,n,.Ar:nval rr.8f$_ x- R a}e 1 of 10

TABLE L• Smnmary aF GR5 Data and A-13Iial Re,a1n-Groundsate r Rt-N, Sy,rem
Wal,er', Srrvke
2liph-y 150 4cxingt"n, NC _
NCDENR G W I814R76
DATE
SAMPLE
LOCATION
RENI,F.NF.
TOLI;ENE
ETHYL-
BENZENE
X\'LENES
TOTAL BTEX
M7.BE
VPH CS-CR
Aliphatic,
VPH C9-CI1
Aliphatic,
VP11 C9-C10
Aramalic,
ESTIMATED
TOTAL
GALLONS
TREATED
MASS OF TOTAL RTEX
REMOVED (Iblday)
5/711009
IM
ND
11]
ND
I9.0
115
NI)
59F
14J0
232
G00,104
NA
E:FF
ND
NO
NO
ND
ND
J:D
NO
NO
NO
NA
-
0.0001
6/30/1009
IMF
ND
14.5
1.1
31.3
N?
306
106
NO
614,349
NA
EFT
NO
ND I
ND
ND
NO
P+D
NO
NO
ND
NA
0.0001
711412004
INF
12
20.1
1,9
21..9
45
ND
1730
3130
197
617,SR1
NA
E'.FF,
ND
ND
ND
NO
ND
ND
ND
NO
ND
NA
00001
W15/2009
INF
i3.'
194r!
20)
1420
3.695
A5
ND
ND
ND
630.561
NA
'IF
NO
NO
NU
NO
NO
NO
NO
NO
ND
NA
0.0093
Nl3072009
I10
17i?
231
2050
4,167
3.1
NO
139
NO
639.350
NA
EFF,
NO
NO
ND
NO
ND
NO
NO
ND
NO
NA
00085
I0/14/2009
FI4E
11A
10.2
933
22.15
N.
210
2670
";21
643,711
NA
EFF.
ND
NDN(.?
NO
NO
NU
NO
2fi9
114
NA v
0.000"
1111112009
INF,
!9;.
560
140
1464
2.26E
66
1260
2930
514
651,448
NA
EFF,
�di
I166
NU
NO
ND
NO
ND
NO
NO
NA
00077
12115/1009
INF.
'.9 !
96R
141
1220
2,408 1
ND
!940
5130
ROG
666.379
NA
EFF.
NO
ND
NO
NO
NO
NO
NO
ND
NO
NA
0.004
I 119/2010
INF.
50>
1440
85.7
609
2, 185.2
3.5
2560
7910
91A
672,024
NA
E.FF.
ND
ND
ND
ND
NO
I NO
NO
ND
NO
NA
00029
215!2010
INF.
3k,:
3.4
39,2
79.8
077
N'D
228
NO
680.103
NA
EFF,.
NO
ND
ND
NO
NO
NO
ND
ND
NO
NA
90003
3lf R/2010
INF,
17
2A.7
33
32.9
666
NO
ND
155
NO
684,471
NA
EFF.
NO
NO
NU
NU
NO
ND
NU
NO
NO
NA
00001
4;22/201D
FlIV
97,2
17.0
194
907
2,948.2
3,7
592
1370
225
695A'11
NA
EFF.
ND
ND
NO
NO
NO
NO
NO
NO
NO
NA
0.OD77
$/12/2010
fNF.
1.7
28,(,
2,S
259
59
NO
NO
NO
NO
699,965
NA
EFF
NO
NO
NO
ND
NO
NO
ND
NO
ND
NA
0.0001
6/22/2010
fN'F.
NU
10
1.2
99
21.1
NO
NO
NO
ND
707.837
NA
FF E
NI)
ND
NO
NO
NO
NO
NO
NO
NO
NA
00000
Si1R71A10
INF
IIR
1440
181
1242
7.981
, 1
2710
11700
1300
714,013
NA
6FF.
NJ)
ND
NO
NO
NO
NU
NI.)
NO
ND
NA
0,0043
N!I I/30f0
INF
"I r.9
230
34
2A1
563.9
16
444
1650
12$
715,R04
NA
EFF.
NU
ND
NO
NO
NI:)
`-
ND
NO
NA
is iu706
I I'�"n; o;;J 010,!:Jq:!n;x•d'nea%•1Nv:oa'R;:oNWAnrx•;Ia.on"r:-1"13u(I,;�adnn:n,d I," :!I Un:x.Amnml rr! 2915'], . "ae a of 10

TABLE I: Summary of GRS Dal, and Analytical Resu11s-Gronadlealer Recovery System
Walser's Service
Hlyh—y 150 Lexi,etnn, NC
NCDENR GWIM14A76
DATE
SAMPLE
LOCA1"ION
BENZENE
TOLUENE
ETHYL-
BENZENE
XYLENCS
TOTAL BTE%
MTRE
VP11C5•CR
,Aliyhalics
VPHC9-C11
Aliplwics
VPHC9-CIO
A,—Vir_s
ESTIMATED
TOTAL
GALLONS
7R 'AT D
MASS OF TOTAL STEX
REMOVED (lb/day)
92812010
2_>2G
2?5
2014
4,649
31
2950
9390
'140
121642
NA
ND
Ni)
NO
NO
NO
ND
NO
ND
NO
NA
00063 -
10/2612010
INF
"1
2420
290
IA56
4,'21
NU
4540
17300
NO
726,119
NA
EFF.
NO
NO
NC,
5.2
NO
I NO
NO I
NO
NO
i NA
A00:35
1212912010
INF,
141
30,80
566
4300
9,9R7
NO
NO
23906
NO
726,119
NA
EFF
ND
74
11
II
195
NO
ND
155
NO
NA
000U0
112112011
INF,
75.1
1610
12R
135)
3,166.3
ND
2500
9930
1170
730,953
NA
FFF.
1:0
0..5
NO
1.5
2..0
111)
NO
201
NO
NA
0,0047
7/9/2011
INF
rj
2260
IR3
2105
4,622.3
NO
NO
23000
ND
736.i 5x
VA
EFF.
kD
ND
NO
1.4
1.4
NO
103
IR2
ND
NA
0,0143
.119.17011
INF.
3 9
R3,2
1,9
906
1916
NI)
ND
1610
ND
;44,69?
NA
EFF
NO
NO
ND
ND
NO
ND
NO
ND
NO
NA
000115
4PI 2011
it: P,
:47
2930
316
2227
5.62n
ND
.5950
161.00
1490
157 194
NA
EFF.
NO
ND
NO
NO
NO
NO
209
152
NO
NA
00122
5!19!2011
-NF
64
1340
119
I245
2.755
^dp
'470
11000
1470
761,913
NA
EFF.
NO
ND
NO
ND
\D
N)
NO
NO
ND
NA
00061
f,/1612011
INF.
106
553
13.7
1 121
937
f 069
1520
1 4141
761
771,1)77
NA
EFF.
NO
NO
ND
NO
ND
ND
73 2
67,3
NO
NA
0,0020
7127;2011
INF
2.1
36R.'
4 2
64,7
110
0,61
IFR
310
33.R
790.19?
NA
ND
?:D
NO
NO
ND
7R.6
t7.4
NO
NA
0,0002
A1301011
INF
13A
30R,
2767
6,336
2,1
$210
11400
2220
785.449
NA
EFF.
ND
D
\D
ND
ND
ND
ND
ND
N A
0071,
9!1912011
INF,
357
1
669
,711
NO
2.790
3990
NO
7a2, 7; r�
NA
EFF.
D
tU
>'I)
I ND
NO
NO
ND
NO
NO
NA
1) 003 5
10/2612011
IV
F.
7M,
71
610
1,496
ND
3420
9910
1170
798.13F
NA
EFF
ND
ND
ND
ND
ND
NO
NO
ND
NO
NA
0.0029
11/1712(111
INF.
_ K, 7.
2330
755
1498
41722
ND
3660
6S70
995
F04.528
NA
EFF.
ND
052
NO
NO
NO
ND
NO
NO
NO
NA
0
1211912011
TNF.
7r,9
1530
16A
1184
2,952A
ND
2231
571U
8"4
911.342
NA
EFF.
NO
0.52
ND
NO
NO
NO
ND
139,
ND
NA
000V
1/1212012
NF,
144
Irf•i1
394
363
RRI R
NO
327
1400
234
R19,049
NA
EFF
NO
?12
NO
NO
ND
NO
NO
NO
ND
NA
(10024
2l14/I012
INF.
NO
NO
44
6.5
NO
692
I93
ND
F27,94(,,
NA
EFF
ND
I1'
NO
ND
NO
NO
NDNDvA
INF,
64.6
1650
IGI
1271
3,141
ND
�ND
$390
1010
F4G244EFF
NU
0.52
ND
ND
ND
NU
52.9
ND
NA
U.U13R
4 ,,,,,..a:-) lA`19ar19tV;kw,.YA nelli!c;.,nVv.f,;,,IR.P,1n.2i;13i1iereh•1-dI-d'.1:If0,4n-Ae-drp,2)15O1 rnce7,(IP

TABLE I: Summary of GRS Wt...d Analyria.l Resnirs-G rnundw.rer Recovery Si v—
W.Iser'. Service
- Hi;hw.y ISO Lc.igfo., NC
NCDENR CWIM14816
DATE
SAMPLE
LOCATION
BENZENE
TOLUENE
ETHYL-
BENZENE
XYLENES
TOTAL BTEX
MTBE
VPII CS•C8
Alipharks
VPH C9-C12
Aliphatic,
VPH C9-CIO
A—vk,
ESTIMATED
TOTAL
GALLONS
TREATED
MASS OF TOTAL BTEX
REMOVED(Ibld.y)
4118/2412
INF
SO4
1550
!i)
14RI
3.241
NO
1270
R620
1140
950.996
NA
F.FT
_!N1
\D
ND
ND
NO
NO
NO
NO
51.5
ND
NA
0.0119
S11712012
:.; ^.
1710
.'hG
1078
4,039
ND
2741)
5160
1030
A72,9R7
NA
i f b
ND
NO
^NE,
NO
ND
ND
NU
.52.9
ND
NA
0.0163
6714/261?
INY
AS
IR50
"5
2345
4559
NU
225
4R9
96.1
RAI.02
NA
EF'E
ND
ND
Nli
NO
ND
NU
NO
NO
ND
NA
0.0111
71 411017
INF.
526
17'G
...11
19"2
3976
ND
60(10
6600
.1400
P93944
NA
LFF.
NU
ND
-..__\D
ND
NU
NO
NU
ND
ND
NA
0. 0106
9A5/2012
INF.
26
719
-N 7
62R
1445
ND
1150
7510
257
u96,576
nla
EF'F',
NO
ND
NO
NO
NU
NO
ND
NO
NI)
NA
O9ou }V�
9/1112012
INF
0 52
I S
i t
149
32
ND
ND
NO
I NO
905,533
NA
EFF
ND
ND
ND
ND
NU
ND
NO
NO
NO
NA
00001
I oil 5/2RI2
INF.
37e
1220
146
105"
3.456
ND
2960
5070
AA7
911,455
NA
EFF
vu
NO
NO
ND
NO
NO
ND
ND
NU
NA
0.0029
11/2R/2011
D 3
R37
103
007
I.R70
ND
!674
4650
9RR
917.114
NA
EFF
':I)
ND
ND
ND
NO
NO
?all
NO
ND
NA.
00025
1211912412
INF.
53
tAU
199
199
403
ND
359
8A1
230
923.541
NA
EFF.
7:D
ND
NU
ND
ND
ND
ND
ND
ND
NA
0.0010
1/241261.1
INF
6R
224
25.'3
106
562
NU
794
IA5
6i9
933,179
NA
EFF.
ND
ND
VU
NU
ND
ND
ND
NU
NO
NA
0,0013
2/19/2013
INF.
39,14
1510
:17
1352
3,079
NU
3060
5520
1400
942.164
NA
EFF,
NO
ND
NTJ
ND
NO
NU
NO
NO
NO
NA
(10099
3/2712013
FNF,
51. 3.
1960
210
1544
3,767
NO
4350
7530
NO
956,453
NA
EFF,
NO
NO
NO
ND
NO
NO
ND
NO
NO
NA
00125
411712013
INF.
2).8
v
920
7).9
A)I
1.615
ND
3R70
3850tNO
971,dR2
NA
EFF.
NO
NO
NO
NO
ND
ND
NU
NU
NA _
0,0096
5/27/2013
INF.
29
1200
A3A
M10
2,323
ND
3060
4880
9944943
NA
EFT'.
NO
ND
ND
NU
ND
ND
ND
NU
NA
0.0130
6!IV2013
INF
25.4
F3R
64.4
70S
1.633
ND
I610
2250IA0S,414
NA
EF7
NO
NFl
NU
NO
NO
ND
NU
ND
NA
0!1772013
INF
12.6
429
3' A
436
910
NO
A42
1990
1,019,976
Nn
EFF
NU
ND _
NO
NO
NU
NO
NO
ND
NO
NA
f)
872XR611
h'F
1090
91.1
67R
1,973
ND
(109
799
NO
1,023,501
NA
FFF
N:(I
NO
ND
ND
ND
ND
[iD
ND
ND
NA
r10(,1'f
P%.! ,,I1,,A i490AIAWai-,.RAnnmu k<pnr+.aemcd RCIfOO-2u15\I[Izvxdrm.ad In!:^(I'llara.nnmra! rpi 2.'t i )b P.gr. .f 61 ! 0

TABLE]: Summary of GRS D.I. and ,Ana I)licsl RrxuRs-G ranndsv al<r Recovery System
Welser's Se"ite
high—) 150 L<zington, NC
NCDENR CWIN14816
DATE
SAMPLE
LOCATION
BENZENE
TOLUENE
ETHYL
BENZENE
XYLENES
TOTAL B'FEX
MTBE
VPH C5d;8
Aliphatin
VPH C9-Cl2
ARphatl<s
VPH C9-CIO
AremfOrs
ESTIMATED
TOTAL
GALLONS
TREATED
MASS OF TOTAL STEX
REMOVED(Ihldvy)
9/14/2013
INF
14 7
7127
40,9
1440
2,233
ND
i,38
2410
565
1,036,499
NA
FFF
NO
ND
ND
NO
NO
NO
NO
ND
NA
0fmo
10/2412013
INF,
4.4 }
1740
199
1943
.3,916
NU
915
1390
ND
1,046.757
NA
EFF.
NO
NU
NO
ND
NO
ND
NO
I NO
ND
NA
00112
11119/2013
INF.
19 R
$2,5
106
R'_9
1. 80
NO
19217
2840
NO
1.055,451
NA
EFF.
NO
NO
ND
ND
NO
ND
ND
NO
NO
NA
0,0050
12/1711013
INF.
151
600
(1.5
648
1,329
ND
1:110
.5671)
1320
I f163,258
NA
EFF
ND
W,
NO
ND
NO
NO
NO
NA
000?I
l 1111"014
INF.
9,7
121r
145
1336
2,701
114C+
2430
7420
1750
1,061.19P
NA
EFF.
NI)
ND
ND
NC)
NO
ND
NO
NO
N❑
NA
00055
' 1.71014
INF.
2.p
105
U.6
1023
224
NO
249
1 4.69
159
1,074,006
NA
EFF..
NO
NO
ND
NO
ND
ND
ND
NO
ND
NA
00002
3116/1014
INF.
3' S
128E
216
1535
3,069
ND
368E
5360
117E
L;?'7,566
NA
If F
ND
NO
ND
NO
NO
ND
NO
NO
NO
NA
00025
4r29:2014
}F
305
107E
125
811
2,097
NO
2750
31170
503
1.182.1194
NA
FF
NO
NO
f4O
ND
ND
ND
ND
ND
ND
NA
0.0027
c%21/701/
INF.
NO
901
661
1042
2,014
NO
'Afk)
I100
510
I092,160
NA
EFF,
NO
NU
NO
ND
ND
ND
NO
ND
NA
0.0069
612412014
INF.
26.3,
9)5
11j
71a
1.908
NO
NO
3126
1240
1,107,874
NA
EFF.
NO
ND
NO
rari
Nf)
NO
NO
NO
NO
NA
00072
7123;2014
INF..
16.5
691
!A..1
563
1,34o
NO
1360
2120
NO
1J IIi,913
NA
CFF.
ND
ND
ND
NO
NO
ND
ND
NO
NO
NA
00035
872012014
INF,
NO
3 4
09
16,7
21
NO
NO
52.5
NO
1.12009
NA
EFF
ND
NO
ND
ND
NO
NO
NU
NO
NO
NA
0,0001
9I2312014
INF,
24,4
1130
174
1 1140.
2.472
NO
200
40a0
654
1,139,691
NA
EFF
NO
ND
NO
NO
NO
NO
NC)
NU
NO
NA
0,0063
1012912014
NE
.33,R
1920
314
2019
C287
NO
5760
74RO
1220
1,150, 539
NA
F.FF
NO
ND
NO
ND
ND
ND
NO
NO
ND
NA
0.0108
11/14/2014
1\F
.32.4
189E
101
2057
41R0
NO
.100
7700
1880
1,150,765
NA
ET I"
NO
NO
NO
NO
NO
NO
ND
ND
NO
NA
O.Onnv
12/I6i2014
NF.
2.1
76.8
124
110.A
202
ND
NO
612
NO
1.)53,207
VA
1,22/2015
EFF I
lNF
ND
I8.3
NO
727
NO I
109
NO
672
ND
1,526
ND
ND
NO
SIB
NO
1400
NO
NO 1
NA
1.160.673
0,0002
NA
EFF.
ND
NO
NO
NO
NO
ND
ND
NO
ND
NA
010026
2/18/2015
INF.
26.0
740
64.5
798
1,619
NO
1290
4p"a,
635
1,166,702
NA
EFF.
ND
NO
N1)
NO
NO
NO
ND
NO
NO _
NA
0. 0032
3125/20t5
INF,
19.3
F07
II7
1010
1,973
ND
2230
154E
615
1,175.342
NA
EFF,
ND
NO
NO
ND
NO
NO
lls
56.3
I) I)
NA
00041
4II4/1015
INF.
35
l oo
210
1229
3.064
NO
437n
460E
1010
1.180.202
NA
FFF:
ND
NO
NO
NU
NO
ND
10"
"7
ND
NA
0.0062
5R7l1015
INF
231
I)RE
159
1164
2.731
ND
235E
1140
NO
1,1911460
NA
EFF,
NC)
rdD
NO
Np
NO
ND
146
64.9
NO
NA
0 )054
111!";;"C !.;I V99119WII)!.4 NF,.1,'x:Azl Rx'7.nr1-26151!'J v;n i:fn.- -4:0 Daly!-Arinux1 /rl N)i 5 xi, rage 9 of 10

TABLE. 1: Summary ofGRS D.I. and A nalrtlol Rc,ulrs•GrnttnAsnrer Recovery System
Walser', Servlee
Highway I50 LeArigron, NC
NCDENR GWIM14876
DATE
SAMPLE
LOCATION
gE,V ZENE
TOLUENE
ETHYL
BENZENE
XVLENES
TOTAL OTEX
MTBE
VPH C5-"
Alipballcs
VPII C9-C12
Aliphatic,
VPH C9-C)0
Aromatics
ESTIMATED
TOTAL
GALLONS
TRE4TED
MASS OF TOTAL BTEX
REMOVED(Ibiday)
W2112015
INF
903
1.664
NO
85n
ND
ND
1,195,775
NA
:f!
ND
ND
NO
NO
ND
67
NO
NO
NA
0001
7R917015
1•41
:I I
IJ3d
3t2
2054
4337
NO
4370
9560
NO
1.191.9n5
NA
EFF
\11
ND
ND
ND
NO
NO
76
%4
NO
NA
91(Itz015
INF
I•IRO
I38
101
3,235
NO
4010
6800
NO
1,198,394
NA
FFF.
VD
ND
NO
r;D
NO
NO
713
54.7
NO
NA
0,0012
913012015
FNF
1;
b'6
62
615
1,301
r4r)
1440
1000
70R
1,201.42R
NA
EFF
NO
ND
NO
NO
NO
ND
NO
NA
0.0009
10l291,2013
INF
307
1190
I9
1302
2.652
NO
34f.t1
3210
1300
1104,066
NA
EFF
ND
ND
NO
ND
NO
NO
653
NO
NO
NA
00021
I11I9110I5
I�f
_.
'<54
91;
s9
_..___.'
1307
2.313
ND
_'Si0
WO
1410
1705,064
NA
1) r
NO
NO
v
NO
ND
NO
123
58.3
NO
VA
0.0017
12;ISit01"
f1F
10.2
761
n-
1051
I,9R1
tip
2100
2390
1150
208.1'R
NA
EFF 1
NO
ND
NO
NO
ND
5U
103
NO
ND
NA
00Ui4
MTDE - Methyl Tertiary Bunyl Elher
IPE • Leopropyl F.thev
ND - Non Detect - Concentrations Mlow laboratory minimum quartifteation limit
NA - Not available or not analysed
ppb - Results are in pans {w billion
a - Flow meter moved i I'Mienc Number of gallons treated are boxed on the rcadin8s lion the eRluem flow miter.
Bl'EX-pcnsene. Toluene, E.th-vlbenaene. and Xylenea
VPH -Volatile Pctroieum Hydrocarbons
V31190-System retested for VPH
(Avmge iota) BTEX u&IL) (g 1 1,000.000) (1 LJ 02642 gall (Gallium T—ted) (0.0022046 Ibs/g) ^ Pounds of Comaminamo
Ponds of CG)roaminants I Dar of 0pmtiona m Pounds per Day
See analwtcal dale In, adAAional analyAril results
L!'•a 7-C1Wom:...md Rrymvtnmvr.,l 11wit-.201514:Izw0 —t IrVkVA DAI-All—lrs
P!20 1� `, Page 100 14

TABLE2
WAISER .S SERVICE
MASS OF BTEX CONTAMINANTS REMOVED -GROUNDWATER RECOVERY SYSTEM
Date
Gallons
Treated
Influent
Effluent
Total BTEX
Days
BETX Contaminants
Removed (lbs)
Pounds prr
Day
623!2002
3482.9
13310
61.8
13248.2
26
03850
0,014E
7/162002
9147.7
i4900
56
14844
21
1,1331
0.0540
8/122002
24490.8
10720
36.2
1068i.8
27
2,1834
0,0909
92512002
17888.8
8000
284
79716
44
1;1899
0,0270
1012511002
IC341,0
5790
14.6
57-5 4
30
0.4984
O.O166
1H2112002
I?949.0
4920
27,6
4792A
27
0.7178
0.0266
12/16/2002
3522,0
5640
33
5607.0
25
0,1648
0.0066
V122003
14201.9
10670
33.3
106367
27
1,2605
0.0467
2i202003
12986,9
9410
402
8369,8
39
0.9070
0.0233
4/11/2003
305693
3410
12
3408,8
50
0,8695
0.0174
4124t2003
83176
4140
3.3
4136,7
13
0.28? 1
0.0221
6/512003
19975.9
3970
5.8
39642
42
0.6608
0,0157
62412003
7753,1
4430
8,8
4421,2
19
0.2860
0.0151
72112003
285.1
4530
7.4
4522,6
27
00108
0,0004
9/30/2003
42385.4
5740
1 i 7
57223
71
2.0239
0.0285
IWI/2003
9694,6
1426
1.4
1424.6
21
0,1152
0.0055
1120/2003
7390,0
2450
83
24417
30
0,1506
0,0050
12142003
10215.4
5840
0
5840
14
0497E
0.0356
1/28/2004
20414.6
3780
0
3780
55
0,6439
0.0117
2+112004
31970
4590
0
4590
0.7224
OOO87
3252004
6815.2
7400
20
7380
43
04197
0,(H)98
4113.2004
61 fl 0
6200
0
6200
19
03182
0.0167
5162004
4683.0
5010
0
5010
23
0,1958
00085
6,222007
1517,0
22900
42
22896
53
0,2898
0.0055
9/92007
6557.0
80,8
21.2
60
120
0,0033
0 00003
9/62007
455.0
4307
15
4292
37
0.0163
00004
1/3112008
131.3
12.290
9,2
12281
147
0,0135
0.0001
2/222008
269.0
676E
0
6768
22
0,01.52
0,0007
5120200E
5077.0
525E
1084.9
4171
34
0,1767
0.0052
6/102008
1472.O
10,192
0
10192
21
0,1252
0,0060
7282008
89899
5,747
597S
5149
48
03863
0,0080
9/122008
259,0
2,7272
0
2727
46
0:0059
0,0001
10/7112008
155.0
3,26 7.E
616.5
2651.
39
0.0034
0.0001
2/24;<009
395.0
_45c4
0
2459
40
0 (YJ81
00002
3I192009
2436.9
260.1
0
260
23
0.0053
0 (M2
'1612009
19,9
939.3
0
939
18
0.0002
0.000(1
5/72009
5393.2
37.6
0
38
31
0,0017
00001
61302009
14244.7
31.3
0
31.3
- 54
0.0037
0MOi
7/14/2009
3532,4
45
0
45
14
0.0011
0.0001
82SP-009
12680,3
3.695
0
3645
42
0,39I0
0,0093
91302009
8788.2
4,167
0
4167
36
03056
000R5
10/14/2009
6354,6
229.5
0
228,5
14
OOf21
0,0009
122009
11743.5
2,266
0
2266
29
02221
0.0077
122/152009
8930.7
2,408,1
0
2408.1
33
0.1795
00054
V192010
56455
2,185.2
0
21852
35
(1,i029
0,0029
2/52010
8078.E
79,8
0
79.8
17
0.0054
0 0003
3/182010
4368.2
66,6
0
66 5
41
0,0024
0.0001
422/2010
11000,1
2,9482
0
29482
35
02706
0,0077
5/122010
4494,E
5v.
0
59
20
0.0022
0,0001
622R010
7871,4
30
0
29,5
41
0.0019
0,0000
728/2010
6176,3
'2,981
0
2981
36
0,1536
0,0043
8/112010
;790,6
563.9
0
364
14
0.0084
0 000E
912R2010,
7837.9
4,6480
0
4648
48
0.3040
00N+3
IOQ612010
2478
4,721,0
5,2
4716
28
00975
0.0035
12/292010
0
8.987.0
19S
896E
64
0.0000
0.0000
1127i'oi1
5205
3.166.3
2
3164
29
0.1374
0.0047
2/9!2(ti1
4934 1
4,622.3
14
4621
13
0.1864
0.014:.
M::('+ojxcts�".a 9l55ti9fN:1 I. N'abe1 ;v%J E4 "" a',, Ri-[F U.l An, ..'p, 201;,a

TABLE2
WALSER'S SERVICE
MASS OF BTEX CONTAMINANTS REMOVED - GROUNDWATER RECOVERY SYSTEM
Date
Gallons
Treated
Influent
Effluent
Total BTEX
Days
BETX Contaminants
Removed (lbs)
Pounds per
Dev
3/9/2011
8523,8
1856
0
185.6
28
0,0132
0.0005
4/27/2011
12711.9
5,620,0
0
5620
49
0,5961
0.0122
5/19/2011
6419
2.769.0
0
2768
22
0.1483
0,0067
6/16/2011
7263,5
937.0
0
937
28
0,0368
0.0020
7/27/2011
9716
110,0
0
110
41
0,0089
0.0002
9/30/2011
4656,3
6,336,0
0
6336
34
O.2462
0,0072
9/29/2011
7289.9
1.7110
0
1711
30
0,1041
0,0035
1026/201 i
5999 i
1,496.,0
0
1496
27
0,0749
0.0029
11/17/2011
5.79C,.
4,372.0
0..52
4371
22
0.2112
0.0096
12/19/2011
68l4,2
2952,9
0
2952.9
32
0,1679
0.0052
1/122012
7706.9
881,8
0
RR1.8
24
0.0567
00024
2/14/2012
87970
6,5
0
6.5
33
0.0005
OOOOO
3202012
18398.0
3,146,E
0
31466
35
0,4831
00138
4/18/2012
12741,9
3.241.4
0
3241.4
29
0.344E
00119
5/17/2012
14000.E
4.039.4
0
4039.4
29
0A719
0.0163
6/142012
8185.6
4,559
0
4559
28
0,3114
0,0111
7/242012
127715
3,976
0
3976
40
0,4237
0.0106
8/15!2012
2632,3
1445
(t
1445
22
0.0317
0.0014
9/11,12012
8956.6
32
0
32
27
0,0024
0,000)
10/25/2012
5922,7
2,456
0
2456
44
0.1214
0.0028
1128/2012
5658.9
1,870
0
187C
34
00883
0.0026
12/192012
6427.0
403
0
403
21
0,0216
0.0010
1/242013
9638,0
562
0
562
36
0,0452
O,0013
2/19/2013
89850
3,079
0
3079
26
01308
0.0089
3272013
142890
3,767
C.
3767
36
0A492
0,0125
4117/2013
150290
1,615
0
1615
21
0,2025
_0.0096
5/2212013
234610
2.323
0
2323
35
0,4548
0,0J30
6/252013
10471,0
1.633
0
16333
24
0.1427
00059
7/17/2013
14462.0
910
0
910
22
0.1098
0,0050
9/29/2013
3625,0
1,873
0
1973
42
0.05E7
0.0013
9/24/2013
12987,0
2.233
0
2233
0,2420
0,0090
1024/2013
10269.0
3,916
0
3916
30
03356
0.0112
11/19/2013
8724,0
1,790
0
1780
26
0.1296
0.0050
12/172013
7777.0
1328
0
1329
28
0.0862
0,0031
1/132014
6530.0
2.701
0
2701
27
0.1472
Q.0055
2/172014
4217,.0
224
0
224
35
0,0079
0.0002
3126,'2014
3561.0
3.069
0
3069
37
0.0912
0.0025
4,12912014
532S.0
2,097
0
2097
34
0,0932
00027
5/222014
9266,0
2,014
0
2014
23
0,1551
0.0068
6/24/2014
15714,0
1,808
0
i808
33
0,2371
0.0072
723/2014
907910
1.348
0
1349
29
0,1021
0,0035
91202014
11955.0
21
0
21
28
0.0021
0,0001
923/2014
10?820
2.472
0
2472
34
0,2224
0,0065
1029/2014
10848,0
4,296
0
4296
36
0.3880
0 0108
1 1/242014
226.0
4.280
0
4280
26
0,0081
0 003
1211(-42014
2442.0
202
')
202
22
0.0041
0,0002
122/2015
7466,0
1,525
0
1525
37
0.0950
(1,0026
2/ 18/2015
60290
1.692
0
1692
27
0.0951
3;.52015
8640,0
1,973
0
1973
35
0.1422
0 004
4/14!2015
486C,O
3,064
0
30E4
20
0,1243
0.0062
527/2015
10258,0
2,731
0
2731
47
0,2338
0,0054
6122/2015
5315,0
1.664
0
1664
0.07-18
0,0028
7/292013
18200
4.337
(1
4337
37
0.0659
0,001R
8120M15
999.0
1235
0
3235
22
O.0270
0.00)2
9i30/2015
28340
1.301
0
1301
41
O.03OR
0,0009
10'2Rl2015
2638.0
2,652
0
2652
28
00584
0.0021
I I/I R12015
1798,0
2,313
0
2313
21
0.0347
0.0017
12l152015
2234,0
1,981
0
1981
27
00369
1;0014
total:
27.4173
--_�-
Arerage:
0.2394
0.0077
Notes:
A,age laal U?ES ug:Li lS'LUW.Ut)U)taL%024:_eal)iOallnnr. 7rcaed)(0002:0lG tlrs/e)=Prwn,h ofCMpiNrrNgrtlF
.oAr :. , o,nam6rsn!r' i Days of Cperwk-- N-,& pr, Day
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ME)
11:Ck)I.
Rll
ND
Nil
ND
Nil
ND
Nil
vil"n)
ND
Mil
via
RD
):f)
1P
11,
it%111i)
MU
RD
RD
Nil
ND
>
NT)
OfT61J
III
NO
N73
40
'I'll
ND
St,
VP
N„
ail
Nil
RE=
ME)
01;11f
NI,
RD
ND
RD
NO
MD
Ni)
i„1L1)
NU
Ni3
a7>
Nt7
131
MI)
OIrDYII
11
17
NO
0
Ni)
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I
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NYf
- ME,
M)1
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ND
RD
NO
I I,I I+OV
1!
4.1
RO
No
*I
NT)
Of?ILOD
XI1
,Nt)
ND
ND
RD
NO
lIMI'm
NI,
AT,
ND
ND
MD
aT)
04DIN1 _
It,
a i
No,
Nn
RD
wt)
tl—V
NY)
No,
Nil
ND
rill
Fi)
O)d.47 - 1
NO
las I
NO
NU
Mil
'a,
114U07
MD
N1
NP
RD
NU
NEIP
Df1D)Oi
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aY)
NO
RD
-. Nil
NRl
1191A)
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RY)
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11,
Not,
}
OibHN
?.11
Nil
RD
ND
\Yt
)tif
RD
firl 7
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Nl)
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RTt
NO
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tillOn
NT)
D$06"
ND
NT)
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xv
ME)
NTf
)Will"
MO
W
RD
ND
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9)
p
"W"
?Ys
NO
Nil
Nt)
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RT3 1
ig
!l.)i.4V
NU
W
xU
RD
Nil
4li
DVl$:FO
aD
N(i
ND
Nn
RD
li!Y)'ID
RD
N$)
RD
-NU
RD
NO
5
0)'N'11
wt)
NU
RD
Nil
wt, -
NL $
II4,rII
NO
N7l
MP
wt,
RDND
W
RD
NII
RV
M)
l,Y1rl:
ID
N,
RD
vp 1
Im
Nil
MO
D11d+,)
a7)
N1l
IV
No;
at,
MP
Nn
NU
11)
NY)
ND
NO
Nil I
Mi
Nft
ND
Rh
!f.D
NO
`
o, l—,
tin
MD
. )
Nt)
ND
ND
NTl-
bN13,11
Nil
W.
ND
Nil
NO
W.,
6
iviLi3
NO i
WD
Nil 1
ai)
NE,
wt
\:)
Naf:s:
I a±TRt —dqh—, bci.l H.,
.,i^I: xi,np,op)l tint;
I. u&I - ♦l µ"nNrom,+tr i:kc
S NO _ Nrn dtletl; nl ; . •Mvc IAt +u;MM Anrt,bn Ilrni: ip<cii:ru in iac 4trnrz+) ac,
D N��1r„nPNIIrN.:..,:m t•ur.ed ro..n. v«.
O. fdm= Conrfminnm i .--.A .. p.tv.,rei ::Ou tii Dt C) Alxumrr- mtl I:nmt- ve Ae:i.,n' [>weD Anvil IWI r:.?rcli.r )niv i, 7
...r •,Ip,icnal.'mN�;+:•..I :NN , .t.o. wn-Enatftm..oesnt, ArM.-n,,-,aYicnea. SnT61', anc :l'LcswsouMt
r.. _yct..•9f<::?9JOfJ lv,e.e!arN..u:,iew�sNvt,e: A•to�. R,Sv.:t�rN-.•i:K 4Aw �a
^i}

._ b.
._ , .
...
,, ... ,,
,. ,
w__
.i 'i - 1
"^ �
,. �
e- E ..
.. -
.. �..
.,
� e
� �
;, h
,.x�
�
'�� _ � �. _
o�
a
n;

ecuEplAnoN 0 MW-4
SUPPLY WFCLL evl�oikc v N*
Ln (57.01)
Ln
MW9
(57,41)�
Mw-2 0AI-1
Li 557.10)
0
MW-1
m (56.82f)
$ ©ER®1
Vf1DE
Mw-8
(56.80) AI-2
ID
a
iO 0
! MW-5
(56.92)
(56.79) 0` S6 d
IY
LEGEND
APPROX. LOCATION OF BEDROCK MONITORING WELL
(DATA NOT USED IN CONTOURING)
® APPROX. LOCATION OF VAPOR EXTRACTION/GROUNDWATER
RECOVERY WELL (VERW)
APPROX. LOCATION OF INJECTION WELL
APPROX. LOCATION OF AIR INJECTION WELL (AI)
® APPROX. LOCATION OF SUPPLY WELL
(it) FEET
(56.32) RELATIVE GROUNDWATER ELEVATION Qf)
ISOCONTOUR UNE ((f)
APPROXIMATE GROUNDWATER FLOW DIRECTION
NOTES: I— DEPTHS TO GROUNDWATER MEASURED ON 11/18/15.
2- GROUNDWATER CONTOUR INTERVALS = AS SHOWN.
3- ALL LOCATIONS ARE APPROXIMATE.
i;\PROJE C i $t iY9H\ 199DO1 ti lYAl4FRS1F IC.tJRFSIARMR ,)F( MIS MAPC nWC,
I
/-DRAINAGE DITCH
10
O .
GRAVEL DRIVE
x ;
WELL
new 6©
(56.%)
�eAtz/swe-2
/uu/swe-I
ceAPW C scaLE
+0 20
SCAU; I.
c b'

SUPPLY WELL
SW-1/W-I
MW-4
(ND)
MW-4s I
(ND)
1
�jj ) MW•1
FOR
E� '3 (� I VERW- tom
Mw-8 4 SERVICE ` (NS1.0 �' 1
INC) 0 b��
AI-2
Ill 1
O
yk ©MW-5
w 0 w (ND)
(ND)
LEGEND
i0 AYI'KUA. LUE:AIIUN 0h GKUUNOWAILR MONITORING WELL
APPROX. LOCATION OF BEDROCK MONITORING WELL
(DATA NOT USED IN CONTOURING)
® APPROX. LOCATION OF VAPOR EXTRACTION/GROUNDWATER
RECOVERY WELL (VERW)
APPROX. LOCATION OF INJECTION WELL
APPROX. LOCATION OF AIR INJECTION WELL (AI)
Q APPROX. LOCATION OF SUPPLY WELL
(ppb) PARTS PER OIL'_ION
(40.1) NAPHTHALENE CONCENTRATION (ppb)
— — NAPHTHALENE CONCENTRATION ISOPLETH
OF SURICAL AOUIFER (ppb)
(ND) LESS THAN THE METHOD DETECTION LIMITS
SPECIFIED IN THE LABORATORY REPORT
(NS) NOT SAMPLED
NOTES: I- ON O8� 80/t5 AND DWATER 1/ 8/15. COLLECTED
2- ISOCONCENTRATION CONTOURS AS SHOWN.
3- ALL LOCATIONS ARE APPROXIMATE.
I
1:1PROJECTS%1999',199001R WAI SFRSIFIGIIRF4;L1RLtR npr 7ni5 AAAOS I)WG
;DRAINAGE DITCH
0, ;
N
GRAVEL DRIVE
x,
WELL.
0612/ ®-2
r`
/8374/SWS-I
0AAP111C SCALE
0 10 20 40
SCALE: 1' 40'

SUBMIT FORM ON YF_L I OW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• ,
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company, Inc. - WalSer's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Hiahwav 150N
TYPE OF PERMITTED OPERATION BEING MONITORED
NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ® Remediation: GrOUndWater
Contact Person: Flora D'Souza/Shield Enaineerina, Inc
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected:
11/18/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: _min.
pH 7.26 units Temp. NM °C
DRY at
Depth to Water Level: NM ft. below measuring point
Screened Interval:
33 ft. to 63
ft. Spec. Cond. NMµMhos
time ofsampling,
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: El
YES El NO
LABORATORY INFORMATION
Date sample analyzed: 11/19/15 - 11/24/15
Laboratory Name: Pace
Analytical Seryi
r � Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved
COD NA
and colloidal concentrations.
Nitrite N/tIe
tom,_ ?/ O
mg/I
(NOz) as
Nmmn0
a�t � Pb J ead ND mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
p � lw - Zinc NA mg/I
Coliform: MF Total NA /100m1
Phosphorus: Total as P
NA mg/I
ESSI�
0/7
(Note: Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
Al -Aluminum
NA mg/I
Aliphatic (C05-CO8) = 0.125 mg/1
pH (when analyzed) NA units
Ba - Barium
NA mg/I
Aliphatic (C09-C12) = 0.0583 mg/1
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Arsenic NA mg/i
Chromium: Total
NA mg/I
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MAnFP VPH
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 10.4886 mg/L Effluent Total VOCs: 0.1833 mg/L VOC Removal% 98.25%
Flora D'Souza/Shield Enaineerina, Proiect Manaaer
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007

APPENDIX A

/7PaceAnalytical
wwwpacelabs.00m
race Anaryucai services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 04, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S
Pace Project No.: 92276745
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 26

laceAnalXical-
wwwpacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92276745
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 26

/_ i�alceAnalytical
www.pacelabs.com
Pace Analytical Jervices, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: WALSER'S
Pace Project No.: 92276745
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92276745001 INFLUENT MADEP VPH
ZDO
5
PASI-C
SM 6200B
CAH
63
PASI-C
92276745002 EFFLUENT MADEP VPH
ZDO
5
PASI-C
EPA 200.7
CDF
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc Page 3 of 26

1,71ace Analytical
www.pacelabs.com
race AlidlyucGl avf vlbrl, ."'.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
WALSER'S
92276745
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92276745001
INFLUENT
MADEP VPH
Aliphatic (C05-008)
2820
ug/L
1000
11/20/15 12:08
N2
MADEP VPH
Aliphatic (C09-C12)
3400
ug/L
1000
11/20/15 12:08
N2
MADEP VPH
Aromatic (C09-C10)
1410
ug/L
1000
11/20/15 12:08
N2
SM 6200B
Benzene
25.4
ug/L
5.0
11/24/15 08:17
SM 6200B
1,2-Dibromoethane (EDB)
6.1
ug/L
5.0
11/24/15 08:17
SM 6200B
Ethylbenzene
65.9
ug/L
5.0
11/24/15 08:17
SM 6200B
Isopropylbenzene (Cumene)
6.3
ug/L
5.0
11/24/15 08:17
SM 6200B
Naphthalene
135
ug/L
20.0
11/24/15 08:17
SM 6200B
n-Propylbenzene
7.6
ug/L
5.0
11/24/15 08:17
SM 6200B
Toluene
915
ug/L
5.0
11/24/15 08:17
SM 6200B
1,2,4-Trimethylbenzene
301
ug/L
5.0
11/24/15 08:17
SM 6200B
1,3,5-Trimethylbenzene
89.3
ug/L
5.0
11/24/15 08:17
SM 6200B
m&p-Xylene
867
ug/L
10.0
11/24/15 08:17
SM 6200B
o-Xylene
440
ug/L
5.0
11/24/15 08:17
92276745002
EFFLUENT
MADEP VPH
Aliphatic (C05-008)
125
ug/L
50.0
11/19/15 19:47
N2
MADEP VPH
Aliphatic (C09-C12)
58.3
ug/L
50.0
11/19/15 19:47
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 26

/ a eAnalytical
www.pacelabs.com
race Anaryucai services, uw.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92276745
Method:
MADEP VPH
Description:
VPH NC Water
Client:
Shield
Date:
December 04, 2015
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 26

/�laceAnalytical"
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92276745
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: December 04, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 26

�IaceAnalXical
www.pacelabs.com
race Anayticai services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92276745
Method: SM 6200B
Description: 6200B MSV
Client: Shield
Date: December 04, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

�-aceAnalytical
www.pacelabs.com
9800 Kincey Ave Suite 100
Huntersville, NC 28078
(704 )875-9092
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92276745
Sample: INFLUENT Lab ID: 92276745001 Collected: 11/18/15 13:12 Received: 11/18/15 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1 -Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 12/04/2015 04:49 PM
Analytical Method: MADEP VPH
2820 ug/L
3400 ug/L
1410 ug/L
102
%
101
%
Analytical Method:
SM 6200B
25.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
6.1
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
65.9
ug/L
ND
ug/L
6.3
ug/L
1000
20
11/20/1512:08
1000
20
11/20/1512:08
1000
20
11/20/1512:08
70-130
20
11/20/1512:08
460-00-4
70-130
20
11/20/1512:08
460-00-4
5.0
10
11/24/15 08:17
71-43-2
5.0
10
11/24/15 08:17
108-86-1
5.0
10
11/24/15 08:17
74-97-5
5.0
10
11/24/15 08:17
75-27-4
5.0
10
11/24/15 08:17
75-25-2
50.0
10
11/24/15 08:17
74-83-9
5.0
10
11/24/15 08:17
104-51-8
5.0
10
11/24/15 08:17
135-98-8
5.0
10
11/24/15 08:17
98-06-6
5.0
10
11/24/15 08:17
56-23-5
5.0
10
11/24/15 08:17
108-90-7
10.0
10
11/24/15 08:17
75-00-3
5.0
10
11/24/15 08:17
67-66-3
10.0
10
11/24/15 08:17
74-87-3
5.0
10
11/24/15 08:17
95-49-8
5.0
10
11/24/15 08:17
106-43-4
10.0
10
11/24/15 08:17
96-12-8
5.0
10
11/24/15 08:17
124-48-1
5.0
10
11/24/15 08:17
106-93-4
5.0
10
11/24/15 08:17
74-95-3
5.0
10
11/24/15 08:17
95-50-1
5.0
10
11/24/15 08:17
541-73-1
5.0
10
11/24/15 08:17
106-46-7
5.0
10
11/24/15 08:17
75-71-8
5.0
10
11 /24115 08:17
75-34-3
5.0
10
11/24/15 08:17
107-06-2
5.0
10
11/24/15 08:17
75-35-4
5.0
10
11/24/15 08:17
156-59-2
5.0
10
11/24/15 08:17
156-60-5
5.0
10
11/24/15 08:17
78-87-5
5.0
10
11/24/15 08:17
142-28-9
5.0
10
11/24/15 08:17
594-20-7
5.0
10
11/24/15 08:17
563-58-6
5.0
10
11/24/15 08:17
10061-01-5
5.0
10
11/24/15 08:17
10061-02-6
5.0
10
11/24/15 08:17
108-20-3
5.0
10
11/24/15 08:17
100-41-4
20.0
10
11/24/15 08:17
87-68-3
5.0
10
11/24/15 08:17
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
N2
N2
Page 8 of 26

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ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92276745
Sample: INFLUENT Lab ID: 92276745001 Collected: 11/18/15 13:12 Received: 11/18/15 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Methylene Chloride
ND
ug/L
20.0
10
11/24/15 08:17
75-09-2
Methyl-tert-butyl ether
ND
ug/L
5.0
10
11/24/15 08:17
1634-04-4
Naphthalene
135
ug/L
20.0
10
11/24/15 08:17
91-20-3
n-Propylbenzene
7.6
ug/L
5.0
10
11/24/15 08:17
103-65-1
Styrene
ND
ug/L
5.0
10
11/24/15 08:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
10
11/24/15 08:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
5.0
10
11/24/15 08:17
79-34-5
Tetrachloroethene
ND
ug/L
5.0
10
11/24/15 08:17
127-18-4
Toluene
915
ug/L
5.0
10
11/24/15 08:17
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
20.0
10
11/24/15 08:17
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
20.0
10
11/24/15 08:17
120-82-1
1, 1, 1 -Trichloroethane
ND
ug/L
5.0
10
11/24/15 08:17
71-55-6
1,1,2-Trichloroethane
ND
ug/L
5.0
10
11/2411508:17
79-00-5
Trichloroethene
ND
ug/L
5.0
10
11/24/15 08:17
79-01-6
Trichlorofluoromethane
ND
ug/L
10.0
10
11/24/15 08:17
75-69-4
1,2,3-Trichloropropane
ND
ug/L
5.0
10
11/24/15 08:17
96-18-4
1,2,4-Trimethylbenzene
301
ug/L
5.0
10
11/24/15 08:17
95-63-6
1,3,5-Trimethylbenzene
89.3
ug/L
5.0
10
11/24/15 08:17
108-67-8
Vinyl chloride
ND
ug/L
10.0
10
11/24/15 08:17
75-01-4
m&p-Xylene
867
ug/L
10.0
10
11/24/15 08:17
179601-23-1
o-Xylene
440
ug/L
5.0
10
11/24/15 08:17
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
10
11/24/15 08:17
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
10
11/24/15 08:17
460-00-4
Toluene-d8(S)
100
%
70-130
10
11/24/15 08:17
2037-26-5
Date: 12/04/2015 04:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 26

�Iace Analytical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92276745
Sample: EFFLUENT Lab ID: 92276745002 Collected: 11/18/15 13:22 Received: 11/18/15 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
200.7 MET ICP
Lead
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1 -Dichloroethane
1,2-Dichloroethane
1, 1 -Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1 -Dichloropropene
cis- 1,3-Dichloropropene
trans- 1,3-Dichloropropene
Date: 12/04/2015 04:49 PM
Analytical Method: MADEP VPH
125
ug/L
50.0
1
11/19/1519:47
N2
58.3
ug/L
50.0
1
11/19/1519:47
N2
ND
ug/L
50.0
1
11/19/1519:47
N2
102
%
70-130
1
11/19/1519:47
460-00-4
99
%
70-130
1
11/19/1519:47
460-00-4
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND
ug/L
5.0
1 12/01/1517:30
12/02/1512:43
7439-92-1
Analytical Method: SM 6200B
ND
ug/L
0.50
1
11/23/1518:38
71-43-2
ND
ug/L
0.50
1
11/23/1518:38
108-86-1
ND
ug/L
0.50
1
11/23/1518:38
74-97-5
ND
ug/L
0.50
1
11/23/1518:38
75-27-4
ND
ug/L
0.50
1
11/23/1518:38
75-25-2
ND
ug/L
5.0
1
11/23/1518:38
74-83-9
ND
ug/L
0.50
1
11 /23/15 18:38
104-51-8
ND
ug/L
0.50
1
11/23/1518:38
135-98-8
ND
ug/L
0.50
1
11/23/1518:38
98-06-6
ND
ug/L
0.50
1
11/23/1518:38
56-23-5
ND
ug/L
0.50
1
11/23/1518:38
108-90-7
ND
ug/L
1.0
1
11123/1518:38
75-00-3
ND
ug/L
0.50
1
11/23/1518:38
67-66-3
ND
ug/L
1.0
1
11/23/1518:38
74-87-3
ND
ug/L
0.50
1
11/23/1518:38
95-49-8
ND
ug/L
0.50
1
11/23/1518:38
106-43-4
ND
ug/L
1.0
1
11/23/1518:38
96-12-8
ND
ug/L
0.50
1
11/23/1518:38
124-48-1
ND
ug/L
0.50
1
11/23/1518:38
106-93-4
ND
ug/L
0.50
1
11/23/1518:38
74-95-3
ND
ug/L
0.50
1
11/23/1518:38
95-50-1
ND
ug/L
0.50
1
11/23/1518:38
541-73-1
ND
ug/L
0.50
1
11/23/1518:38
106-46-7
ND
ug/L
0.50
1
11/23/1518:38
75-71-8
ND
ug/L
0.50
1
11/23/1518:38
75-34-3
ND
ug/L
0.50
1
11/23/1518:38
107-06-2
ND
ug/L
0.50
1
11/23/1518:38
75-35-4
ND
ug/L
0.50
1
11/23/1518:38
156-59-2
ND
ug/L
0.50
1
11/2311518:38
156-60-5
ND
ug/L
0.50
1
11/23/1518:38
78-87-5
ND
ug/L
0.50
1
11/23/1518:38
142-28-9
ND
ug/L
0.50
1
11/23/1518:38
594-20-7
ND
ug/L
0.50
1
11/23/1518:38
563-58-6
ND
ug/L
0.50
1
11/23/1518:38
10061-01-5
ND
ug/L
0.50
1
11/23/1518:38
10061-02-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 26

�PaceAnalytical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92276745
Sample: EFFLUENT Lab ID: 92276745002 Collected: 11/18/15 13:22 Received: 11/18/15 15:40 Matrix: Water
Parameters Results Units Report Limit DF . Prepared Analyzed CAS No. Qual
6200E MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 12/04/2015 04:49 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100
%
100
%
101
%
0.50
1
11 /23/15 18:38
108-20-3
0.50
1
11 /23/15 18:38
100-41-4
2.0
1
11/23/1518:38
87-68-3
0.50
1
11 /23/15 18:38
98-82-8
2.0
1
11/23/1518:38
75-09-2
0.50
1
11 /23/15 18:38
1634-04-4
2.0
1
11/23/1518:38
91-20-3
0.50
1
11 /23/15 18:38
103-65-1
0.50
1
11 /23/15 18:38
100-42-5
0.50
1
11 /23/15 18:38
630-20-6
0.50
1
11 /23/15 18:38
79-34-5
0.50
1
11 /23/15 18:38
127-18-4
0.50
1
11 /23/15 18:38
108-88-3
2.0
1
11/23/1518:38
87-61-6
2.0
1
11/23/15 18:38
120-82-1
0.50
1
11/23/1518:38
71-55-6
0.50
1
11/23/1518:38
79-00-5
0.50
1
11/23/1518:38
79-01-6
1.0
1
11/23/1518:38
75-69-4
0.50
1
11/23/1518:38
96-18-4
0.50
1
11 /23/15 18:38
95-63-6
0.50
1
11/23/15 18:38
108-67-8
1.0
1
11/23/1518:38
75-01-4
1.0
1
11 /23/15 18:38
179601-23-1
0.50
1
11/23/1518:38
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11 /23/15 18:38 17060-07-0
11/23/1518:38 460-00-4
11/23/1518:38 2037-26-5
Page 11 of 26

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QUALITY CONTROL DATA
Project:
WALSER'S
Pace Project No.:
92276745
QC Batch:
GCV/10098 Analysis Method: MADEP VPH
QC Batch Method:
MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92276745001, 92276745002
METHOD BLANK: 1610358
Matrix:
Water
Associated Lab Samples: 92276745001, 92276745002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
ug/L
ND
50.0
11/19/15 14:45 N2
Aliphatic (C09-C12)
ug/L
ND
50.0
11/19/15 14:45 N2
Aromatic (C09-C10)
ug/L
ND
50.0
11/19/15 14:45 N2
4-Bromofluorobenzene (FID) (S)
%
106
70-130
11/19/15 14:45
4-Bromofluorobenzene (PID) (S)
%
104
70-130
11/19/15 14:45
LABORATORY CONTROL SAMPLE & LCSD:
1610359
1610360
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
352
345
117
115
70-130 2 25 N2
Aliphatic (C09-C12)
ug/L
300
337
343
112
114
30-130 2 25 N2
Aromatic (C09-C10)
ug/L
100
97.6
95.9
98
96
70-130 2 25 N2
4-Bromofluorobenzene (FID) (S)
%
107
103
70-130
4-Bromofluorobenzene (PID) (S)
%
105
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 26

/�e Analytical
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r�
race Analytical aennces, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
QC Batch: MPRP/20142 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92276745002
METHOD BLANK: 1617332 Matrix: Water
Associated Lab Samples: 92276745002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 12/02/1511:57
LABORATORY CONTROL SAMPLE: 1617333
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 478 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617334 1617335
MS MSD
92276507007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 519 469 104 94 70-130 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617338 1617339
MS MSD
92277478003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L 12.7 500 500 489 450 95 88 70-130 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
QC Batch: MSV/34404 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92276745002
METHOD BLANK: 1613565
Associated Lab Samples: 92276745002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
11/23/15 16:58
1,1,1-Trichloroethane
ug/L
ND
0.50
11/23/15 16:58
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
11/23/15 16:58
1,1,2-Trichloroethane
ug/L
ND
0.50
11/23/15 16:58
1,1-Dichloroethane
ug/L
ND
0.50
11/23/15 16:58
1,1-Dichloroethene
ug/L
ND
0.50
11/23/15 16:58
1,1-Dichloropropene
ug/L
ND
0.50
11/23/15 16:58
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/23/15 16:58
1,2,3-Trichloropropane
ug/L
ND
0.50
11/23/15 16:58
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/23/15 16:58
1,2,4-Trimethylbenzene
ug/L
ND
0.50
11/23/15 16:58
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
11/23/15 16:58
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/23/15 16:58
1,2-Dichlorobenzene
ug/L
ND
0.50
11/23/15 16:58
1,2-Dichloroethane
ug/L
ND
0.50
11/23/15 16:58
1,2-Dichloropropane
ug/L
ND
0.50
11/23/15 16:58
1,3,5-Trimethylbenzene
ug/L
ND
0.50
11/23/15 16:58
1,3-Dichlorobenzene
ug/L
ND
0.50
11/23/15 16:58
1,3-Dichloropropane
ug/L
ND
0.50
11/23/15 16:58
1,4-Dichlorobenzene
ug/L
ND
0.50
11/23/15 16:58
2,2-Dichloropropane
ug/L
ND
0.50
11/23/15 16:58
2-Chlorotoluene
ug/L
ND
0.50
11/23/15 16:58
4-Chlorotoluene
ug/L
ND
0.50
11/23/15 16:58
Benzene
ug/L
ND
0.50
11/23/15 16:58
Bromobenzene
ug/L
ND
0.50
11/23/15 16:58
Bromochloromethane
ug/L
ND
0.50
11/23/15 16:58
Bromodichloromethane
ug/L
ND
0.50
11/23/15 16:58
Bromoform
ug/L
ND
0.50
11/23/15 16:58
Bromomethane
ug/L
ND
5.0
11/23/15 16:58
Carbon tetrachloride
ug/L
ND
0.50
11/23/15 16:58
Chlorobenzene
ug/L
ND
0.50
11/23/15 16:58
Chloroethane
ug/L
ND
1.0
11/23/15 16:58
Chloroform
ug/L
ND
0.50
11/23/15 16:58
Chloromethane
ug/L
ND
1.0
11/23/15 16:58
cis- 1,2-Dichloroethene
ug/L
ND
0.50
11/23/15 16:58
cis- 1,3-Dichloropropene
ug/L
ND
0.50
11/23/15 16:58
Dibromochloromethane
ug/L
ND
0.50
11/23/15 16:58
Dibromomethane
ug/L
ND
0.50
11/23/15 16:58
Dichlorodifluoromethane
ug/L
ND
0.50
11/23/15 16:58
Diisopropyl ether
ug/L
ND
0.50
11/23/15 16:58
Ethylbenzene
ug/L
ND
0.50
11/23/15 16:58
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 26

1�laceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
METHOD BLANK: 1613565
Associated Lab Samples: 92276745002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/23/15 16:58
Isopropylbenzene (Cumene)
ug/L
ND
0.50
11/23/15 16:58
m&p-Xylene
ug/L
ND
1.0
11/23/15 16:58
Methyl-tert-butyl ether
ug/L
ND
0.50
11/23/15 16:58
Methylene Chloride
ug/L
ND
2.0
11/23/15 16:58
n-Butylbenzene
ug/L
ND
0.50
11/23/15 16:58
n-Propylbenzene
ug/L
ND
0.50
11/23/15 16:58
Naphthalene
ug/L
ND
2.0
11/23/15 16:58
o-Xylene
ug/L
ND
0.50
11/23/15 16:58
sec-Butylbenzene
ug/L
ND
0.50
11/23/15 16:58
Styrene
ug/L
ND
0.50
11/23/15 16:58
tert-Butylbenzene
ug/L
ND
0.50
11/23/15 16:58
Tetrachloroethene
ug/L
ND
0.50
11/2311516:58
Toluene
ug/L
ND
0.50
11/23/15 16:58
trans-1,2-Dichloroethene
ug/L
ND
0.50
11/2311516:58
trans-1,3-Dichloropropene
ug/L
ND
0.50
11/23/15 16:58
Trichloroethene
ug/L
ND
0.50
11/23/15 16:58
Trichlorofluoromethane
ug/L
ND
1.0
11/23/15 16:58
Vinyl chloride
ug/L
ND
1.0
11/23/15 16:58
1,2-Dichloroethane-d4 (S)
%
97
70-130
11/23/15 16:58
4-Bromofluorobenzene (S)
%
100
70-130
11/23/15 16:58
Toluene-d8 (S)
%
101
70-130
11/23/15 16:58
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1613566
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
53.8
108
60-140
1,1,1-Trichloroethane
ug/L
50
48.8
98
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
60-140
1,1,2-Trichloroethane
ug/L
50
48.7
97
60-140
1,1-Dichloroethane
ug/L
50
46.7
93
60-140
1,1-Dichloroethene
ug/L
50
49.6
99
60-140
1, 1 -Dichloropropene
ug/L
50
50.0
100
60-140
1,2,3-Trichlorobenzene
ug/L
50
46.5
93
60-140
1,2,3-Trichloropropane
ug/L
50
48.6
97
60-140
1,2,4-Trichlorobenzene
ug/L
50
46.5
93
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.4
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
48.5
97
60-140
1,2-Dibromoethane (EDB)
ug/L
50
50.2
100
60-140
1,2-Dichlorobenzene
ug/L
50
48.6
97
60-140
1,2-Dichloroethane
ug/L
50
43.0
86
60-140
1,2-Dichloropropane
ug/L
50
47.1
94
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.6
97
60-140
1,3-Dichlorobenzene
ug/L
50
49.7
99
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 26

ceAnalytical
www.pacelabs.com
race Anaiyucai oennces, inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
LABORATORY CONTROL SAMPLE:
Parameter
1613566
Units
Spike
Conc.
1,3-Dichloropropane
ug/L
50
1,4-Dichlorobenzene
ug/L
50
2,2-Dichloropropane
ug/L
50
2-Chlorotoluene
ug/L
50
4-Chlorotoluene
ug/L
50
Benzene
ug/L
50
Bromobenzene
ug/L
50
Bromochloromethane
ug/L
50
Bromodichloromethane
ug/L
50
Bromoform
ug/L
50
Bromomethane
ug/L
50
Carbon tetrachloride
ug/L
50
Chlorobenzene
ug/L
50
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis- 1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Diisopropyl ether
ug/L
50
Ethylbenzene
ug/L
50
Hexachloro-1,3-butadiene
ug/L
50
Isopropylbenzene (Cumene)
ug/L
50
m&p-Xylene
ug/L
100
Methyl -tent -butyl ether
ug/L
50
Methylene Chloride
ug/L
50
n-Butylbenzene
ug/L
50
n-Propylbenzene
ug/L
50
Naphthalene
ug/L
50
o-Xylene
ug/L
50
sec-Butylbenzene
ug/L
50
Styrene
ug/L
50
tert-Butylbenzene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans- 1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl chloride
ug/L
50
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
Result
LCS
% Rec
% Rec
Limits
46.7
93
60-140
49.6
99
60-140
47.2
94
60-140
47.0
94
60-140
47.9
96
60-140
50.4
101
60-140
46.5
93
60-140
50.8
102
60-140
53.4
107
60-140
40.6
81
60-140
31.8
64
60-140
52.9
106
60-140
48.8
98
60-140
53.7
107
60-140
49.5
99
60-140
33.1
66
60-140
48.6
97
60-140
50.4
101
60-140
46.1
92
60-140
50.1
100
60-140
38.4
77
60-140
49.6
99
60-140
47.3
95
60-140
46.0
92
60-140
51.9
104
60-140
96.7
97
60-140
50.6
101
60-140
50.0
100
60-140
49.0
98
60-140
46.6
93
60-140
47.8
96
60-140
46.9
94
60-140
48.8
98
60-140
50.3
101
60-140
41.0
82
60-140
45.5
91
60-140
47.8
96
60-140
50.1
100
60-140
50.4
101
60-140
48.0
96
60-140
47.8
96
60-140
49.0
98
60-140
97
70-130
104
70-130
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 26

1�e Analytical
www.pacelabs.com
race Analytical aernces, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1613567
MS
92276745002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1613568
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.4
22.4
107
112
60-140
4
1, 1, 1 -Trichloroethane
ug/L
ND
20
20
21.8
22.3
109
111
60-140
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.7
23.3
109
116
60-140
7
1,1,2-Trichloroethane
ug/L
ND
20
20
20.3
21.2
102
106
60-140
4
1,1-Dichloroethane
ug/L
ND
20
20
20.9
21.5
104
107
60-140
3
1,1-Dichloroethene
ug/L
ND
20
20
23.3
24.0
116
120
60-140
3
1,1-Dichloropropene
ug/L
ND
20
20
22.9
23.2
114
116
60-140
1
1,2,3-Trichlorobe nzene
ug/L
ND
20
20
20.1
20.6
101
103
60-140
2
1,2,3-Trichloropropane
ug/L
ND
20
20
19.6
21.1
98
106
60-140
7
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.5
20.5
102
103
60-140
0
1,2,4-Trimethylbenzene
ug/L
ND
20
20
21.7
21.9
109
110
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
17.2
19.3
86
97
60-140
12
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.6
21.8
103
109
60-140
5
1,2-Dichlorobenzene
ug/L
ND
20
20
21.1
21.4
105
107
60-140
1
1,2-Dichloroethane
ug/L
ND
20
20
18.5
19.1
92
95
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
20.1
20.8
101
104
60-140
3
1,3,5-Trimethylbenzene
ug/L
ND
20
20
21.6
21.8
108
109
60-140
1
1,3-Dichlorobenzene
ug/L
ND
20
20
21.6
22.0
108
110
60-140
2
1,3-Dichloropropane
ug/L
ND
20
20
19.9
20.8
100
104
60-140
4
1,4-Dichlorobe nzene
ug/L
ND
20
20
21.6
21.9
108
110
60-140
1
2,2-Dichloropropane
ug/L
ND
20
20
20.3
21.2
101
106
60-140
4
2-Chlorotoluene
ug/L
ND
20
20
21.3
20.8
107
104
60-140
2
4-Chlorotoluene
ug/L
ND
20
20
21.2
21.5
106
108
60-140
1
Benzene
ug/L
ND
20
20
22.1
22.5
110
112
60-140
2
Bromobenzene
ug/L
ND
20
20
20.1
20.4
100
102
60-140
1
Bromochloromethane
ug/L
ND
20
20
21.9
23.0
110
115
60-140
5
Bromodichloromethane
ug/L
ND
20
20
20.3
21.6
101
108
60-140
6
Bromoform
ug/L
ND
20
20
14.7
16.0
73
80
60-140
8
Bromomethane
ug/L
ND
20
20
19.7
17.8
99
89
60-140
10
Carbon tetrachloride
ug/L
ND
20
20
21.8
22.6
109
113
60-140
4
Chlorobenzene
ug/L
ND
20
20
21.3
21.7
107
109
60-140
2
Chloroethane
ug/L
ND
20
20
24.5
25.3
123
126
60-140
3
Chloroform
ug/L
ND
20
20
21.4
22.6
107
113
60-140
5
Chloromethane
ug/L
ND
20
20
18.0
18.7
90
93
60-140
4
cis- 1,2-Dichloroethene
ug/L
ND
20
20
21.3
22.0
106
110
60-140
3
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.3
20.5
97
103
60-140
6
Dibromochloromethane
ug/L
ND
20
20
17.3
18.9
86
95
60-140
9
Dibromomethane
ug/L
ND
20
20
20.8
21.3
104
107
60-140
3
Dichlorodifluoromethane
ug/L
ND
20
20
17.7
18.5
89
93
60-140
4
Diisopropyl ether
ug/L
ND
20
20
21.1
22.3
106
111
60-140
5
Ethylbenzene
ug/L
ND
20
20
21.2
21.5
106
107
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
20.5
21.3
102
106
60-140
4
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.1
23.4
116
117
60-140
1
m&p-Xylene
ug/L
ND
40
40
43.2
43.5
108
109
60-140
1
Methyl-tert-butyl ether
ug/L
ND
20
20
21.2
22.5
106
112
60-140
6
Methylene Chloride
ug/L
ND
20
20
20.6
22.3
103
112
60-140
8
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 26

eAnalytical
www.pacelabs.com
race mnaiyucai aervices, nw.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1613567
1613568
MS
MSD
92276745002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
21.9
22.2
110
111
60-140
1
n-Propylbenzene
ug/L
ND
20
20
21.4
21.2
107
106
60-140
1
Naphthalene
ug/L
ND
20
20
19.9
21.3
100
107
60-140
7
o-Xylene
ug/L
ND
20
20
20.8
20.8
104
104
60-140
0
sec-Butylbenzene
ug/L
ND
20
20
22.3
22.2
111
111
60-140
0
Styrene
ug/L
ND
20
20
21.3
21.9
107
109
60-140
3
tert-Butylbenzene
ug/L
ND
20
20
18.5
18.4
93
92
60-140
0
Tetrachloroethene
ug/L
ND
20
20
21.0
20.6
105
103
60-140
2
Toluene
ug/L
ND
20
20
21.0
21.3
105
107
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.5
23.4
113
117
60-140
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
19.3
20.3
96
102
60-140
5
Trichloroethene
ug/L
ND
20
20
21.0
21.3
105
107
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
24.8
24.6
124
123
60-140
1
Vinyl chloride
ug/L
ND
20
20
23.4
24.0
117
120
60-140
3
1,2-Dichloroethane-d4 (S)
%
96
98
70-130
4-Bromofluorobenzene(S)
%
101
102
70-130
Toluene-d8 (S)
%
100
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 26

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
QC Batch: MSV/34408 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92276745001
METHOD BLANK: 1613637
Associated Lab Samples: 92276745001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
11/24/15 08:00
1,1,1-Trichloroethane
ug/L
ND
0.50
11/24/15 08:00
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
11/24/15 08:00
1,1,2-Trichloroethane
ug/L
ND
0.50
11/24/15 08:00
1. 1 -Dichloroethane
ug/L
ND
0.50
11/24/15 08:00
1,1-Dichloroethene
ug/L
ND
0.50
11/24/15 08:00
1,1-Dichloropropene
ug/L
ND
0.50
11/24/15 08:00
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/24/15 08:00
1,2,3-Tiichloropropane
ug/L
ND
0.50
11/24/15 08:00
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/24/15 08:00
1,2,4-Trimethylbenzene
ug/L
ND
0.50
11/24/15 08:00
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
11/24/15 08:00
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/24/15 08:00
1,2-Dichlorobenzene
ug/L
ND
0.50
11/24/15 08:00
1,2-Dichloroethane
ug/L
ND
0.50
11/24/15 08:00
1,2-Dichloropropane
ug/L
ND
0.50
11/24/15 08:00
1,3,5-Trimethylbenzene
ug/L
ND
0.50
11/24/15 08:00
1,3-Dichlorobenzene
ug/L
ND
0.50
11/24/15 08:00
1,3-Dichloropropane
ug/L
ND
0.50
11/24/15 08:00
1,4-Dichlorobenzene
ug/L
ND
0.50
11/24/15 08:00
2,2-Dichloropropane
ug/L
ND
0.50
11/24/15 08:00
2-Chlorotoluene
ug/L
ND
0.50
11/24/15 08:00
4-Chlorotoluene
ug/L
ND
0.50
11/24/15 08:00
Benzene
ug/L
ND
0.50
11/24/15 08:00
Bromobenzene
ug/L
ND
0.50
11/24/15 08:00
Bromochloromethane
ug/L
ND
0.50
11/24/15 08:00
Bromodichloromethane
ug/L
ND
0.50
11/24/15 08:00
Bromoform
ug/L
ND
0.50
11/24/15 08:00
Bromomethane
ug/L
ND
5.0
11/24/15 08:00
Carbon tetrachloride
ug/L
ND
0.50
11/24/15 08:00
Chlorobenzene
ug/L
ND
0.50
11/24/15 08:00
Chloroethane
ug/L
ND
1.0
11/24/15 08:00
Chloroform
ug/L
ND
0.50
11/24/15 08:00
Chloromethane
ug/L
ND
1.0
11/24/15 08:00
cis-1,2-Dichloroethene
ug/L
ND
0.50
11/24/15 08:00
cis- 1,3-Dichloropropene
ug/L
ND
0.50
11/24/15 08:00
Dibromochloromethane
ug/L
ND
0.50
11/24/15 08:00
Dibromomethane
ug/L
ND
0.50
11/24/15 08:00
Dichlorodifluoromethane
ug/L
ND
0.50
11/24/15 08:00
Diisopropyl ether
ug/L
ND
0.50
11/24/15 08:00
Ethylbenzene
ug/L
ND
0.50
11/24/15 08:00
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 26

�,IaceAnalytical-
wwwpacelabs.com
race Anaiyucai services, III(;.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
METHOD BLANK: 1613637
Associated Lab Samples: 92276745001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/24/15 08:00
Isopropylbenzene (Cumene)
ug/L
ND
0.50
11/24/15 08:00
m&p-Xylene
ug/L
ND
1.0
11/24/15 08:00
Methyl-tert-butyl ether
ug/L
ND
0.50
11/24/15 08:00
Methylene Chloride
ug/L
ND
2.0
11/24/15 08:00
n-Butylbenzene
ug/L
ND
0.50
11/24/15 08:00
n-Propylbenzene
ug/L
ND
0.50
11/24/15 08:00
Naphthalene
ug/L
ND
2.0
11/24/15 08:00
o-Xylene
ug/L
ND
0.50
11/24/15 08:00
sec-Butylbenzene
ug/L
ND
0.50
11/24/15 08:00
Styrene
ug/L
ND
0.50
11/24/15 08:00
tert-Butylbenzene
ug/L
ND
0.50
11/24/15 08:00
Tetrachloroethene
ug/L
ND
0.50
11/24/15 08:00
Toluene
ug/L
ND
0.50
11/24/15 08:00
trans-1,2-Dichloroethene
ug/L
ND
0.50
11/24/15 08:00
trans-1,3-Dichloropropene
ug/L
ND
0.50
11/24/15 08:00
Trichloroethene
ug/L
ND
0.50
11/24/15 08:00
Trichlorofluoromethane
ug/L
ND
1.0
11/24/15 08:00
Vinyl chloride
ug/L
ND
1.0
11/24/15 08:00
1,2-Dichloroethane-d4 (S)
%
99
70-130
11/24/15 08:00
4-Bromofluorobenzene (S)
%
100
70-130
11/24/15 08:00
Toluene-d8 (S)
%
99
70-130
11/24/15 08:00
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1613638
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.5
109
60-140
1,1,1-Trichloroethane
ug/L
50
48.9
98
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
52.3
105
60-140
1,1,2-Trichloroethane
ug/L
50
49.7
99
60-140
1,1-Dichloroethane
ug/L
50
47.0
94
60-140
1, 1 -Dichloroethene
ug/L
50
50.3
101
60-140
1, 1 -Dichloropropene
ug/L
50
49.7
99
60-140
1,2,3-Trichlorobenzene
ug/L
50
45.7
91
60-140
1,2,3-Trichloropropane
ug/L
50
50.9
102
60-140
1,2,4-Trichlorobe nzene
ug/L
50
45.4
91
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.1
98
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
52.0
104
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.4
103
60-140
1,2-Dichlorobenzene
ug/L
50
48.2
96
60-140
1,2-Dichloroethane
ug/L
50
44.1
88
60-140
1,2-Dichloropropane
ug/L
50
47.2
94
60-140
1,3,5-Trimethylbenzene
ug/L
50
47.9
96
60-140
1,3-Dichlorobenzene
ug/L
50
49.4
99
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 26

17 ceAnalytical
www.pacelabs.com
race Analytical Services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
LABORATORY CONTROL SAMPLE:
Parameter
1613638
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
47.6
95
60-140
1,4-Dichlorobenzene
ug/L
50
50.1
100
60-140
2,2-Dichloropropane
ug/L
50
40.4
81
60-140
2-Chlorotoluene
ug/L
50
46.2
92
60-140
4-Chlorotoluene
ug/L
50
47.2
94
60-140
Benzene
ug/L
50
50.2
100
60-140
Bromobenzene
ug/L
50
45.6
91
60-140
Bromochloromethane
ug/L
50
52.1
104
60-140
Bromodichloromethane
ug/L
50
52.9
106
60-140
Bromoform
ug/L
50
41.2
82
60-140
Bromomethane
ug/L
50
33.9
68
60-140
Carbon tetrachloride
ug/L
50
52.7
105
60-140
Chlorobenzene
ug/L
50
49.1
98
60-140
Chloroethane
ug/L
50
45.5
91
60-140
Chloroform
ug/L
50
49.1
98
60-140
Chloromethane
ug/L
50
34.0
68
60-140
cis-1,2-Dichloroethene
ug/L
50
49.0
98
60-140
cis- 1,3-Dichloropropene
ug/L
50
49.6
99
60-140
Dibromochloromethane
ug/L
50
46.5
93
60-140
Dibromomethane
ug/L
50
50.0
100
60-140
Dichlorodifluoromethane
ug/L
50
36.9
74
60-140
Diisopropyl ether
ug/L
50
50.6
101
60-140
Ethylbenzene
ug/L
50
48.0
96
60-140
Hexachloro-1,3-butadiene
ug/L
50
43.2
86
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.2
104
60-140
m&p-Xylene
ug/L
100
97.6
98
60-140
Methyl-tert-butyl ether
ug/L
50
51.6
103
60-140
Methylene Chloride
ug/L
50
49.9
100
60-140
n-Butylbenzene
ug/L
50
47.2
94
60-140
n-Propylbenzene
ug/L
50
45.6
91
60-140
Naphthalene
ug/L
50
49.0
98
60-140
o-Xylene
ug/L
50
47.5
95
60-140
sec-Butylbenzene
ug/L
50
48.0
96
60-140
Styrene
ug/L
50
50.8
102
60-140
tert-Butylbenzene
ug/L
50
40.6
81
60-140
Tetrachloroethene
ug/L
50
45.5
91
60-140
Toluene
ug/L
50
48.0
96
60-140
trans-1,2-Dichloroethene
ug/L
50
49.9
100
60-140
trans-1,3-Dichloropropene
ug/L
50
49.9
100
60-140
Trichloroethene
ug/L
50
47.9
96
60-140
Trichlorofluoromethane
ug/L
50
47.3
95
60-140
Vinyl chloride
ug/L
50
49.6
99
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 26

!` ceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1613795
MS
92276750009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1613796
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.4
22.5
112
112
60-140
0
1, 1, 1 -Trichloroethane
ug/L
ND
20
20
22.8
22.9
114
115
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.3
21.1
106
105
60-140
1
1,1,2-Trichloroethane
ug/L
ND
20
20
21.3
20.9
106
104
60-140
2
1, 1 -Dichloroethane
ug/L
ND
20
20
22.0
21.5
110
108
60-140
2
1, 1 -Dichloroethene
ug/L
ND
20
20
24.6
24.2
123
121
60-140
2
1, 1 -Dichloropropene
ug/L
ND
20
20
23.9
23.5
120
118
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.0
20.7
105
104
60-140
1
1,2,3-Trichloropropane
ug/L
ND
20
20
21.3
20.4
106
102
60-140
4
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.0
20.8
105
104
60-140
1
1,2,4-Trimethylbenzene
ug/L
ND
20
20
23.1
22.1
116
111
60-140
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
19.1
18.7
95
93
60-140
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.5
21.1
107
106
60-140
2
1,2-Dichlorobenzene
ug/L
ND
20
20
21.9
21.3
109
106
60-140
3
1,2-Dichloroethane
ug/L
ND
20
20
19.6
19.2
97
95
60-140
2
1,2-Dichloropropane
ug/L
ND
20
20
21.1
20.7
105
104
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
22.9
22.0
115
110
60-140
4
1,3-Dichlorobenzene
ug/L
ND
20
20
22.6
21.9
113
110
60-140
3
1,3-Dichloropropane
ug/L
ND
20
20
20.9
20.2
105
101
60-140
3
1,4-Dichlorobenzene
ug/L
ND
20
20
22.9
22.0
114
110
60-140
4
2,2-Dichloropropane
ug/L
ND
20
20
22.4
22.1
112
110
60-140
1
2-Chlorotoluene
ug/L
ND
20
20
21.8
21.1
109
106
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
22.3
21.8
112
109
60-140
2
Benzene
ug/L
ND
20
20
23.0
22.4
115
112
60-140
3
Bromobenzene
ug/L
ND
20
20
21.4
20.4
107
102
60-140
5
Bromochloromethane
ug/L
ND
20
20
23.0
22.4
115
112
60-140
3
Bromodichloromethane
ug/L
ND
20
20
21.5
21.4
107
107
60-140
0
Bromoform
ug/L
ND
20
20
15.7
15.8
79
79
60-140
1
Bromomethane
ug/L
ND
20
20
19.9
20.3
99
101
60-140
2
Carbon tetrachloride
ug/L
ND
20
20
22.9
23.3
115
116
60-140
1
Chlorobenzene
ug/L
ND
20
20
22.5
22.1
112
111
60-140
2
Chloroethane
ug/L
ND
20
20
24.6
24.1
123
120
60-140
2
Chloroform
ug/L
ND
20
20
22.6
22.4
113
112
60-140
1
Chloromethane
ug/L
ND
20
20
19.2
18.0
96
90
60-140
6
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.6
22.2
113
111
60-140
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.6
20.7
103
104
60-140
1
Dibromochloromethane
ug/L
ND
20
20
18.8
18.7
94
94
60-140
0
Dibromomethane
ug/L
ND
20
20
21.5
21.0
108
105
60-140
2
Dichlorodifluoromethane
ug/L
ND
20
20
19.1
18.8
95
94
60-140
1
Diisopropyl ether
ug/L
ND
20
20
22.7
22.4
113
112
60-140
1
Ethylbenzene
ug/L
ND
20
20
22.2
21.8
111
109
60-140
2
Hexachloro-1,3-butadiene
ug/L
ND
20
20
20.9
20.7
105
103
60-140
1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.9
23.4
120
117
60-140
2
m&p-Xylene
ug/L
ND
40
40
45.1
44.4
113
111
60-140
2
Methyl-tert-butyl ether
ug/L
ND
20
20
22.4
22.3
112
111
60-140
1
Methylene Chloride
ug/L
ND
20
20
22.1
21.3
110
107
60-140
3
Results presented on
this page are in
the units indicated by the
"Units" column except where
an alternate
unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 26

171aceAnalXical
www.pacelabs.com
Pace Analytical 5ennces, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92276745
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1613795
1613796
MS
MSD
92276750009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
n-Butylbenzene
ug/L
ND
20
20
22.9
22.4
115
112
60-140
2
n-Propylbenzene
ug/L
ND
20
20
22.4
21.9
112
109
60-140
2
Naphthalene
ug/L
ND
20
20
21.6
21.3
108
107
60-140
1
o-Xylene
ug/L
ND
20
20
21.4
20.9
107
104
60-140
2
sec-Butylbenzene
ug/L
ND
20
20
23.3
22.7
117
113
60-140
3
Styrene
ug/L
ND
20
20
22.3
21.6
111
108
60-140
3
tert-Butylbenzene
ug/L
ND
20
20
19.4
18.8
97
94
60-140
3
Tetrachloroethene
ug/L
ND
20
20
21.7
21.4
109
107
60-140
2
Toluene
ug/L
ND
20
20
22.0
21.5
110
107
60-140
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.7
23.4
119
117
60-140
1
trans-1,3-Dichloropropene
ug/L
ND
20
20
20.3
20.4
102
102
60-140
1
Trichloroethene
ug/L
ND
20
20
22.1
21.6
111
108
60-140
2
Trichlorofluoromethane
ug/L
ND
20
20
24.4
24.2
122
121
60-140
1
Vinyl chloride
ug/L
ND
20
20
24.7
24.5
123
123
60-140
1
1,2-Dichloroethane-d4(S)
%
98
98
70-130
4-Bromofluorobenzene (S)
%
102
101
70-130
Toluene-d8 (S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 26

74�eAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALIFIERS
Project: WALSER'S
Pace Project No.: 92276745
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 26

��aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WALSER'S
92276745
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92276745001
INFLUENT
MADEP VPH
GCV/10098
92276745002
EFFLUENT
MADEP VPH
GCV/10098
92276745002
EFFLUENT
EPA 200.7
MPRP/20142 EPA 200.7 ICP/18170
92276745001
INFLUENT
SM 6200B
MSV/34408
92276745002
EFFLUENT
SM 6200B
MSV/34404
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/04/2015 04:49 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 26

ceAnaVtcal
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1
Company Shield Engineering Repo" To. Flora D'Souza Attention. Flora D'Souza
Address 4301 Taggart Creek Road Copy To Company Name Shield Engineering
Charlotte. NC 28208
Address. 4301 Taggart Creek Road, Charlotte, NC 28
Regulatory Agency
Email To fdsouza shielden ineerin .com
Purchase Order No. 1990018-70
Pace Quote Reference.
UST - Underground Stora a Tank
Phone [phone] Fax
Client Project ID. WALSER'S
Pace Project Manager nicole. asiorowski acela
State I Location
Requested Due DaterTAT 10 Da Default
Container Order Number
Pace Profile #
North Carolina
Request
Analysis
Flltered
M
a'
Z
MATRIX CODE
COLLECTED
z
Preservatives
>
Ormlung wmw OW
o
U
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P'.4-1 P
SAMPLE ID
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START
END
V
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¢
One Character per box. W,a WP
A.Z. 0.9 I , •) '°" AR
pOT
Sample Ids must be unique T„:u. Ts
x
w
w
°
„'
„
o
R
0
O
10
W
/�
i
o
a
0
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2
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DATE
TIME
DATE
TIME
Q
c
ry
__
z
U
M
m
z
m
z
m
f
o
m
o
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cc
1
INFLUENT
WT
V
I
X
X
VC]
2
EFFLUENT
VYT
X
X
X
CA
3
4
5
It
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINQUISpED BY I AFFILIATION
DATE
TIME
A C TE B i AFFI.
DATE
TIME
SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
c
D
m
u
0
c
o
T>
c
PRINT Name of SAMPLER: 1 n i
1
WO.■:
SIGNATURE of -SAMPLER
DATE Signed: I
9 22 7 6 7 45
W
N}

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IMI
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company Inc. - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Highway 150N
TYPE OF PERMITTED OPERATION BEING MONITORED
NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
"'`
`
❑ Spray Field ® Remediation: GroUndWater
Contact Person: Flora D'Souza/Shield Enaineerina.
Inc_ Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's_ Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 10/28/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft•
Well Diameter: 4 in.
pH 6.01 units Temp. NM °C
DRY at
time ofsampling,
Depth to Water Level: _NMft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NMµMhos
Measuring Point is _NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/30/15 - 11/5/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/1
Pb - Lead ND mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100m1
Phosphorus: Total as P
NA mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/l
Aliphatic (C .Mzftl
pH (when analyzed) NA units
Ba - Barium
NA mg/I
w
TOC NA mg/I
Ca - Calcium
NA mg/I
PEC 0 12015
Chloride NA mg/I
Cd - Cadmium
NA mg/I
11-10
Arsenic NA mg/I
Chromium: Total
NA mg/I
I F
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPL
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/1
VOC , method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I VPH method # MADFP VPH
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
NA mg/I
, method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 11.0291 mg/L Effluent Total VOCs: 0.0653 mg/L VOC Removal% 99.4%
Flora D'Souza/Shield Enoineerino, Proiect Manager
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007

APPENDIX A

7?4eAnalXical
www.pacelabs.com
Pace Analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 06, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSERS 67389
Pace Project No.: 92273972
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 22

i- aceAnalytical
www.pacelabs.com
Face Analytical Jervices, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSERS 67389
Pace Project No.: 92273972
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia[VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 22

�laceAnalXical
www.pacelabs.com
face Analytical ,ervlces, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
WALSERS 67389
92273972
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92273972001
INFLUENT
MADEP VPH
ZDO
5
PASI-C
SM 6200B
CAH
63
PASI-C
92273972002
EFFLUENT
MADEP VPH
ZDO
5
PASI-C
EPA200.7
CDF
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 22

/ , aceAnalytical
www.pacelabs.com
race /Anaryucai services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Project: WALSERS 67389
Pace Project No.: 92273972
Lab Sample ID
Method
92273972001
MADEP VPH
MADEP VPH
MADEP VPH
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
92273972002
MADEP VPH
SUMMARY OF DETECTION
Client Sample ID
Parameters
INFLUENT
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Benzene
1,2-Dibromoethane (EDB)
Ethylbenzene
Isopropylbenzene (Cumene)
Naphthalene
n-Propylbenzene
Toluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m&p-Xylene
o-Xylene
EFFLUENT
Aliphatic (C05-008)
Result
3400
3210
1300
30.7
10.1
129
7.7
175
14.6
1190
154
106
661
641
65.3
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Report Limit Analyzed
250 11/03/1511:31 N2
250 11/03/1511:31 N2
250 11/03/1511:31 N2
2.5
11/05/15 05:25
2.5
11/05/15 05:25
2.5
11/05/15 05:25
2.5
11/05/15 05:25
10.0
11/05/15 05:25
2.5
11/05/15 05:25
5.0
11/05/15 20:08
2.5
11/05/15 05:25
2.5
11/05/15 05:25
5.0
11/05/15 05:25
2.5
11/05/15 05:25
50.0 11/02/1519:40 N2
Qualifiers
Page 4 of 22

I I
eAnalytica(
www.pacelabs.com
race mnaryacar our vices, uw.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSERS 67389
Pace Project No.: 92273972
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: November 06, 2015
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 22

1//4eAnalytical
www.pacelabs.com
race Nnaryucai aervices, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
PROJECT NARRATIVE
Project: WALSERS 67389
Pace Project No.: 92273972
Method: EPA 200.7
Description: 2003 MET ICP
Client: Shield
Date: November 06, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/19933
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92273535002,92273764001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1596294)
• Lead
• MSD (Lab ID: 1596295)
• Lead
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 22

�yaceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSERS 67389
Pace Project No.: 92273972
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: November 06, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/34145
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92274322003
M1: Matrix spike recovery exceeded QC limits
• MS (Lab ID: 1598649)
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Trichlorofluoromethane
• Vinyl chloride
• MSD (Lab ID: 1598650)
• 2,2-Dichloropropane
• Chloromethane
• Dichlorodifluoromethane
• Trichlorofluoromethane
• Vinyl chloride
Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 22

r Ike Analical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSERS 67389
Pace Project No.: 92273972
Method: SM 6200B
Description: 6200B MSV
Client: Shield
Date: November 06, 2015
QC Batch: MSV/34145
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92274322003
R1: RPD value was outside control limits.
• MSD (Lab ID: 1598650)
• 2,2-Dichloropropane
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 22

171keAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
ANALYTICAL RESULTS
Project: WALSERS 67389
Pace Project No.: 92273972
Sample: INFLUENT Lab ID: 92273972001 Collected: 10/28/15 15:00 Received: 10/29/15 14:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1, 3-Dichloroprope ne
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 11/06/2015 04:28 PM
Analytical Method: MADEP VPH
3400 ug/L
3210 ug/L
1300 ug/L
94
%
95
%
Analytical Method:
SM 6200B
30.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
10.1
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
129
ug/L
ND
ug/L
7.7
ug/L
250
5
11/03/15 11:31
250
5
11/03/1511:31
250
5
11/03/1511:31
70-130
5
11/03/1511:31
460-00-4
70-130
5
11/03/1511:31
460-00-4
2.5
5
11/05/15 05:25
71-43-2
2.5
5
11/05/15 05:25
108-86-1
2.5
5
11/05/15 05:25
74-97-5
2.5
5
11/05/15 05:25
75-27-4
2.5
5
11/05/15 05:25
75-25-2
25.0
5
11/05/15 05:25
74-83-9
2.5
5
11/05/15 05:25
104-51-8
2.5
5
11/05/15 05:25
135-98-8
2.5
5
11/05/15 05:25
98-06-6
2.5
5
11/05/15 05:25
56-23-5
2.5
5
11/05/15 05:25
108-90-7
5.0
5
11/05/15 05:25
75-00-3
2.5
5
11/05/15 05:25
67-66-3
5.0
5
11/05/15 05:25
74-87-3
2.5
5
11/05/15 05:25
95-49-8
2.5
5
11/05/15 05:25
106-43-4
5.0
5
11/05/15 05:25
96-12-8
2.5
5
11/05/15 05:25
124-48-1
2.5
5
11/05/15 05:25
106-93-4
2.5
5
11/05/15 05:25
74-95-3
2.5
5
11/05/15 05:25
95-50-1
2.5
5
11/05/15 05:25
541-73-1
2.5
5
11/05/15 05:25
10646-7
2.5
5
11/05/15 05:25
75-71-8
2.5
5
11/05/15 05:25
75-34-3
2.5
5
11/05/15 05:25
107-06-2
2.5
5
11/05/15 05:25
75-35-4
2.5
5
11/05/15 05:25
156-59-2
2.5
5
11/05/15 05:25
156-60-5
2.5
5
11/05/15 05:25
78-87-5
2.5
5
11/05/15 05:25
142-28-9
2.5
5
11/05/15 05:25
594-20-7
2.5
5
11/05/15 05:25
563-58-6
2.5
5
11/05/15 05:25
10061-01-5
2.5
5
11/05/15 05:25
10061-02-6
2.5
5
11/05/15 05:25
108-20-3
2.5
5
11/05/15 05:25
100-41-4
10.0
5
11/05/15 05:25
87-68-3
2.5
5
11/05/15 05:25
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
N2
N2
Page 9 of 22

��e Analytical
www.pacelabs.com
race mnaiyuca, services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSERS 67389
Pace Project No.: 92273972
Sample: INFLUENT Lab ID: 92273972001 Collected: 10/28/15 15:00 Received: 10/29/15 14:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV
Methylene Chloride
Methyl4ert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobe nzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 11/06/2015 04:28 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
175
ug/L
14.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1190
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
154
ug/L
106
ug/L
ND
ug/L
661
ug/L
641
ug/L
101 %
97 %
105 %
10.0
5
11/05/15 05:25
75-09-2
2.5
5
11/05/15 05:25
1634-04-4
10.0
5
11/05/15 05:25
91-20-3
2.5
5
11/05/15 05:25
103-65-1
2.5
5
11/05/15 05:25
100-42-5
2.5
5
11/05/15 05:25
630-20-6
2.5
5
11/05/15 05:25
79-34-5
2.5
5
11/05/15 05:25
127-18-4
5.0
10
11/05/15 20:08
108-88-3
10.0
5
11/05/15 05:25
87-61-6
10.0
5
11/05/15 05:25
120-82-1
2.5
5
11/05/15 05:25
71-55-6
2.5
5
11/05/15 05:25
79-00-5
2.5
5
11/05/15 05:25
79-01-6
5.0
5
11/05/15 05:25
75-69-4
2.5
5
11/05/15 05:25
96-18-4
2.5
5
11/05/15 05:25
95-63-6
2.5
5
11/05/15 05:25
108-67-8
5.0
5
11/05/15 05:25
75-01-4
5.0
5
11/05/15 05:25
179601-23-1
2.5
5
11/05/15 05:25
95-47-6
70-130 5
70-130 5
70-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/05/15 05:25 17060-07-0
11/05/15 05:25 460-00-4
11/05/15 05:25 2037-26-5
Page 10 of 22

171keAnalytical
www.pacelabs.com
race Hnaryucm aeivicaa, -'.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSERS 67389
Pace Project No.: 92273972
Sample: EFFLUENT
Lab ID: 92273972002 Collected.
10/28/15 14:00 Received:
10/29/15 14:05 Matrix: Water
Parameters
Results
Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-008)
65.3
ug/L
50.0
1
11/02/15 19:40
N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
11/02/15 19:40
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
11/02/15 19:40
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
94
%
70-130
1
11/02/15 19:40
460-00-4
4-Bromofluorobenzene (PID) (S)
92
%
70-130
1
11/02/15 19:40
460-00-4
200.7 MET ICP
Analytical Method:
EPA 200.7 Preparation Method:
EPA 200.7
Lead
ND
ug/L
5.0
1 10/30/15 20:30 11/05/15 19:21
7439-92-1
6200E MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
11/05/15 04:19
71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/05/15 04:19
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/05/15 04:19
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
11/05/15 04:19
75-27-4
Bromoform
ND
ug/L
0,50
1
11/05/15 04:19
75-25-2
Bromomethane
ND
ug/L
5.0
1
11/05/15 04:19
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/05/15 04:19
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/05/15 04:19
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
11/05/15 04:19
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/05/15 04:19
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
11/05/15 04:19
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/05/15 04:19
75-00-3
Chloroform
ND
ug/L
0.50
1
11/05/15 04:19
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/05/15 04:19
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/05/15 04:19
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/05/15 04:19
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/05/15 04:19
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/05/15 04:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
11/05/15 04:19
106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/05/15 04:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
11/05/15 04:19
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
11/05/15 04:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
11/05/15 04:19
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/05/15 04:19
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/05/15 04:19
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/05/15 04:19
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/05/15 04:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/05/15 04:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
11/05/15 04:19
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/05/15 04:19
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/05/15 04:19
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/05/15 04:19
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/05/15 04:19
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
1
11/05/15 04:19
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
11/05/15 04:19
10061-02-6
Date: 11/06/2015 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 22

�aceAnalytical
www.pacelabs.com
race Anaryucai services, rnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSERS 67389
Pace Project No.: 92273972
Sample: EFFLUENT
Parameters
6200E MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 11/06/2015 04:28 PM
ANALYTICAL RESULTS
Lab ID: 92273972002 Collected: 10/28/15 14:00 Received: 10/29/15 14:05 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100
%
119
%
106
%
0.50
1
11/05/15 04:19
108-20-3
0.50
1
11/05/15 04:19
100-41-4
2.0
1
11/05/15 04:19
87-68-3
0.50
1
11/05/15 04:19
98-82-8
2.0
1
11/05/15 04:19
75-09-2
0.50
1
11/05/15 04:19
1634-04-4
2.0
1
11/05/15 04:19
91-20-3
0.50
1
11/05/15 04:19
103-65-1
0.50
1
11/05/15 04:19
100-42-5
0.50
1
11/05/15 04:19
630-20-6
0.50
1
11/05/15 04:19
79-34-5
0.50
1
11/05/15 04:19
127-18-4
0.50
1
11/05/15 04:19
108-88-3
2.0
1
11/05/15 04:19
87-61-6
2.0
1
11/05/15 04:19
120-82-1
0.50
1
11/05/15 04:19
71-55-6
0.50
1
11/05/15 04:19
79-00-5
0.50
1
11/05/15 04:19
79-01-6
1.0
1
11/05/15 04:19
75-69-4
0.50
1
11/05/15 04:19
96-18-4
0.50
1
11/05/15 04:19
95-63-6
0.50
1
11/05/15 04:19
108-67-8
1.0
1
11/05/15 04:19
75-01-4
1.0
1
11/05/15 04:19
179601-23-1
0.50
1
11/05/15 04:19
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
11/05/15 04:19 17060-07-0
11/05/15 04:19 460-00-4
11/05/15 04:19 2037-26-5
Page 12 of 22

I�Palbe Anal ical
www.pacelabs.com
Face Analytical ,erVlces, mc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
QC Batch: GCV/10035 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92273972001, 92273972002
METHOD BLANK: 1596544
Matrix:
Water
Associated Lab Samples: 92273972001, 92273972002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
ug/L
ND
50.0
11/02/15 14:08 N2
Aliphatic (C09-C12)
ug/L
ND
50.0
11/02/15 14:08 N2
Aromatic (C09-C10)
ug/L
ND
50.0
11/02/15 14:08 N2
4-Bromofluorobenzene (FID) (S)
%
100
70-130
11/02/15 14:08
4-Bromofluorobenzene (PID) (S)
%
98
70-130
11/02/15 14:08
LABORATORY CONTROL SAMPLE & LCSD:
1596545
1596546
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
317
314
106
105
70-130 1 25 N2
Aliphatic (C09-C12)
ug/L
300
327
337
109
112
30-130 3 25 N2
Aromatic (C09-C10)
ug/L
100
99.0
98.1
99
98
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
103
103
70-130
4-Bromofluorobenzene (PID) (S)
%
101
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 22

�,FalceAnalytical'�
www,pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
QC Batch: MPRP/19933
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92273972002
METHOD BLANK: 1596290
Matrix: Water
Associated Lab Samples: 92273972002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0
11/05/1517:57
LABORATORY CONTROL SAMPLE: 1596291
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Lead ug/L
500 489
98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1596292 1596293
MS MSD
92273535002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Lead ug/L ND
500 500 472
467 94 93 70-130 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1596294 1596295
MS MSD
92273764001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 101 84.0 20 17 70-130 19 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 22

/ �, ceAnalytical
www.pacelabs.com
race Analytical services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
QC Batch: MSV/34145
QC Batch Method: SM 6200B
Associated Lab Samples: 92273972001, 92273972002
Analysis Method:
Analysis Description:
SM 6200B
6200B MSV
METHOD BLANK: 1598647
Matrix: Water
Associated Lab Samples: 92273972001,
92273972002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
11/05/15 02:55
1,1,1-Trichloroethane
ug/L
ND
0.50
11/05/15 02:55
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
11/05/15 02:55
1,1,2-Trichloroethane
ug/L
ND
0.50
11/05/15 02:55
1,1-Dichloroethane
ug/L
ND
0.50
11/05/15 02:55
1,1-Dichloroethene
ug/L
ND
0.50
11/05/15 02:55
1,1-Dichloropropene
ug/L
ND
0.50
11/05/15 02:55
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/05/15 02:55
1,2,3-Trichloropropane
ug/L
ND
0.50
11/05/15 02:55
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/05/15 02:55
1,2,4-Trimethylbenzene
ug/L
ND
0.50
11/05/15 02:55
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
11/05/15 02:55
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/05/15 02:55
1,2-Dichlorobenzene
ug/L
ND
0.50
11/05/15 02:55
1,2-Dichloroethane
ug/L
ND
0.50
11/05/15 02:55
1,2-Dichloropropane
ug/L
ND
0.50
11/05/15 02:55
1,3,5-Trimethylbenzene
ug/L
ND
0.50
11/05/15 02:55
1,3-Dichlorobenzene
ug/L
ND
0.50
11/05/15 02:55
1,3-Dichloropropane
ug/L
ND
0.50
11/05/15 02:55
1,4-Dichlorobenzene
ug/L
ND
0,50
11/05/15 02:55
2,2-Dichloropropane
ug/L
ND
0.50
11/05/15 02:55
2-Chlorotoluene
ug/L
ND
0.50
11/05/15 02:55
4-Chlorotoluene
ug/L
ND
0.50
11/05/15 02:55
Benzene
ug/L
ND
0.50
11/05/15 02:55
Bromobenzene
ug/L
ND
0.50
11/05/15 02:55
Bromochloromethane
ug/L
ND
0.50
11/05/15 02:55
Bromodichloromethane
ug/L
ND
0,50
11/05/15 02:55
Bromoform
ug/L
ND
0.50
11/05/15 02:55
Bromomethane
ug/L
ND
5.0
11/05/15 02:55
Carbon tetrachloride
ug/L
ND
0.50
11/05/15 02:55
Chlorobenzene
ug/L
ND
0.50
11/05/15 02:55
Chloroethane
ug/L
ND
1.0
11/05/15 02:55
Chloroform
ug/L
ND
0.50
11/05/15 02:55
Chloromethane
ug/L
ND
1.0
11/05/15 02:55
cis-1,2-Dichloroethene
ug/L
ND
0.50
11/05/15 02:55
cis-1,3-Dichloropropene
ug/L
ND
0.50
11/05/15 02:55
Dibromochloromethane
ug/L
ND
0.50
11/05/15 02:55
Dibromomethane
ug/L
ND
0.50
11/05/15 02:55
Dichlorodifluoromethane
ug/L
ND
0.50
11/05/15 02:55
Diisopropyl ether
ug/L
ND
0.50
11/05/15 02:55
Ethylbenzene
ug/L
ND
0.50
11/05/15 02:55
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 22

�aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
METHOD BLANK: 1598647
Matrix:
Water
Associated Lab Samples: 92273972001,
92273972002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/05/15 02:55
Isopropylbenzene(Cumene)
ug/L
ND
0.50
11/05/15 02:55
m&p-Xylene
ug/L
ND
1.0
11/05/15 02:55
Methyl-tert-butyl ether
ug/L
ND
0.50
11/05/15 02:55
Methylene Chloride
ug/L
ND
2.0
11/05/15 02:55
n-Butylbenzene
ug/L
ND
0.50
11/05/15 02:55
n-Propylbenzene
ug/L
ND
0.50
11/05/15 02:55
Naphthalene
ug/L
ND
2.0
11/05/15 02:55
o-Xylene
ug/L
ND
0.50
11/05/15 02:55
sec-Butylbenzene
ug/L
ND
0.50
11/05/15 02:55
Styrene
ug/L
ND
0.50
11/05/15 02:55
tert-Butylbenzene
ug/L
ND
0.50
11/05/15 02:55
Tetrachloroethene
ug/L
ND
0.50
11/05/15 02:55
Toluene
ug/L
ND
0.50
11/05/15 02:55
trans-1,2-Dichloroethene
ug/L
ND
0.50
11/05/15 02:55
trans-1,3-Dichloropropene
ug/L
ND
0.50
11/05/15 02:55
Trichloroethene
ug/L
ND
0.50
11/05/15 02:55
Trichlorofluoromethane
ug/L
ND
1.0
11/05/15 02:55
Vinyl chloride
ug/L
ND
1.0
11/05/15 02:55
1,2-Dichloroethane-d4 (S)
%
99
70-130
11/05/15 02:55
4-Bromofluorobenzene (S)
%
91
70-130
11/05/15 02:55
Toluene-d8 (S)
%
104
70-130
11/05/15 02:55
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1598648
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
53.6
107
60-140
1,1,1-Trichloroethane
ug/L
50
53.3
107
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
54.5
109
60-140
1,1,2-Trichloroethane
ug/L
50
47.0
94
60-140
1,1-Dichloroethane
ug/L
50
53.2
106
60-140
1,1-Dichloroethene
ug/L
50
52.7
105
60-140
1,1-Dichloropropene
ug/L
50
51.8
104
60-140
1,2,3-Trichlorobenzene
ug/L
50
59.2
118
60-140
1,2,3-Trichloropropane
ug/L
50
54.0
108
60-140
1,2,4-Trichlorobenzene
ug/L
50
56.2
112
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.7
105
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
58.1
116
60-140
1,2-Dibromoethane (EDB)
ug/L
50
57.0
114
60-140
1,2-Dichlorobenzene
ug/L
50
52.1
104
60-140
1,2-Dichloroethane
ug/L
50
46.4
93
60-140
1,2-Dichloropropane
ug/L
50
50.0
100
60-140
1,3,5-Trimethylbenzene
ug/L
50
52.0
104
60-140
1,3-Dichlorobenzene
ug/L
50
52.9
106
60-140
Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 22

; 4ceAnalyficalo
www.pacelabs.com
face Analytical ,ervices, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
LABORATORY CONTROL SAMPLE:
1598648
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,3-Dichloropropane
ug/L
50
53.5
107
60-140
1,4-Dichlorobenzene
ug/L
50
50.8
102
60-140
2,2-Dichloropropane
ug/L
50
45.6
91
60-140
2-Chlorotoluene
ug/L
50
50.6
101
60-140
4-Chlorotoluene
ug/L
50
49.6
99
60-140
Benzene
ug/L
50
53.2
106
60-140
Bromobenzene
ug/L
50
48.6
97
60-140
Bromochloromethane
ug/L
50
54.7
109
60-140
Bromodichloromethane
ug/L
50
55.6
111
60-140
Bromoform
ug/L
50
46.7
93
60-140
Bromomethane
ug/L
50
52.0
104
60-140
Carbon tetrachloride
ug/L
50
53.7
107
60-140
Chlorobenzene
ug/L
50
51.6
103
60-140
Chloroethane
ug/L
50
54.9
110
60-140
Chloroform
ug/L
50
51.6
103
60-140
Chloromethane
ug/L
50
69.4
139
60-140
cis-1,2-Dichloroethene
ug/L
50
52.2
104
60-140
cis- 1,3-Dichloropropene
ug/L
50
51.1
102
60-140
Dibromochloromethane
ug/L
50
55.8
112
60-140
Dibromomethane
ug/L
50
53.0
106
60-140
Dichlorodifluoromethane
ug/L
50
68.6
137
60-140
Diisopropyl ether
ug/L
50
54.4
109
60-140
Ethylbenzene
ug/L
50
50.9
102
60-140
Hexachloro-1,3-butadiene
ug/L
50
63.8
128
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.0
104
60-140
m&p-Xylene
ug/L
100
102
102
60-140
Methyl-tert-butyl ether
ug/L
50
55.6
111
60-140
Methylene Chloride
ug/L
50
53.5
107
60-140
n-Butylbenzene
ug/L
50
51.2
102
60-140
n-Propylbenzene
ug/L
50
50.8
102
60-140
Naphthalene
ug/L
50
60.1
120
60-140
o-Xylene
ug/L
50
51.9
104
60-140
sec-Butylbenzene
ug/L
50
50.9
102
60-140
Styrene
ug/L
50
55.1
110
60-140
tert-Butylbenzene
ug/L
50
43.2
86
60-140
Tetrachloroethene
ug/L
50
51.2
102
60-140
Toluene
ug/L
50
49.1
98
60-140
trans- 1,2-Dichloroethene
ug/L
50
51.7
103
60-140
trans-1,3-Dichloropropene
ug/L
50
51.3
103
60-140
Trichloroethene
ug/L
50
48.7
97
60-140
Trichlorofluoromethane
ug/L
50
59.3
119
60-140
Vinyl chloride
ug/L
50
62.8
126
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluene-d8 (S)
%
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 22

1laceAnalyfical'
www.pacelabs.com
I-aCe Analytical Services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1598649
MS
92274322003 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1598650
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
<0.25
20
20
23.6
23.4
118
117
60-140
1
1,1,1-Trichloroethane
ug/L
<0.25
20
20
24.8
24.6
124
123
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
<0.25
20
20
22.8
22.7
114
113
60-140
1
1,1,2-Trichloroethane
ug/L
<0.25
20
20
23.0
22.7
115
114
60-140
1
1,1-Dichloroethane
ug/L
<0.25
20
20
23.6
23.9
118
119
60-140
1
1, 1 -Dichloroethene
ug/L
<0.25
20
20
25.2
24.6
126
123
60-140
3
1, 1 -Dichloropropene
ug/L
<0.25
20
20
24.4
24.0
122
120
60-140
1
1,2,3-Trichlorobenzene
ug/L
<1.0
20
20
24.2
22.8
121
114
60-140
6
1,2,3-Trichloropropane
ug/L
<0.25
20
20
22.8
22.9
114
114
60-140
0
1,2,4-Trichlorobenzene
ug/L
<1.0
20
20
24.0
21.6
120
108
60-140
11
1,2,4-Trimethylbenzene
ug/L
<0.25
20
20
24.8
23.7
124
118
60-140
5
1,2-Dibromo-3-chloropropane
ug/L
<0.50
20
20
24.3
23.3
122
116
60-140
5
1,2-Dibromoethane (EDB)
ug/L
<0.25
20
20
24.8
24.4
124
122
60-140
2
1,2-Dichlorobenzene
ug/L
<0.25
20
20
23.0
22.9
115
114
60-140
1
1,2-Dichloroethane
ug/L
<0.25
20
20
20.4
20.3
101
101
60-140
0
1,2-Dichloropropane
ug/L
<0.25
20
20
23.5
22.8
117
114
60-140
3
1,3,5-Trimethylbenzene
ug/L
<0.25
20
20
24.4
23.8
122
119
60-140
3
1,3-Dichlorobenzene
ug/L
<0.25
20
20
23.6
22.8
118
114
60-140
3
1,3-Dichloropropane
ug/L
<0.25
20
20
23.6
23.6
118
118
60-140
0
1,4-Dichlorobenzene
ug/L
<0.25
20
20
22.7
21.7
114
109
60-140
4
2,2-Dichloropropane
ug/L
<0.25
20
20
26.9
11.6
135
58
60-140
80 M1,R1
2-Chlorotoluene
ug/L
<0.25
20
20
24.0
23.3
120
116
60-140
3
4-Chlorotoluene
ug/L
<0.25
20
20
23.7
22.7
118
114
60-140
4
Benzene
ug/L
<0.25
20
20
23.7
22.9
119
115
60-140
3
Bromobenzene
ug/L
<0.25
20
20
24.2
23.2
121
116
60-140
4
Bromochloromethane
ug/L
<0.25
20
20
23.7
23.8
119
119
60-140
0
Bromodichloromethane
ug/L
<0.25
20
20
23.9
23.4
119
117
60-140
2
Bromoform
ug/L
<0.25
20
20
19.3
19.2
96
96
60-140
0
Bromomethane
ug/L
<0.50
20
20
22.8
22.3
114
112
60-140
2
Carbon tetrachloride
ug/L
<0.25
20
20
25.2
24.6
126
123
60-140
2
Chlorobenzene
ug/L
<0.25
20
20
23.5
23.2
118
116
60-140
1
Chloroethane
ug/L
<0.50
20
20
26.1
25.9
130
129
60-140
1
Chloroform
ug/L
<0.25
20
20
22.8
23.0
114
115
60-140
1
Chloromethane
ug/L
<0.50
20
20
36.9
34.8
184
174
60-140
6 M1
cis-1,2-Dichloroethene
ug/L
<0.25
20
20
23.1
22.9
116
114
60-140
1
cis- 1, 3-Dich loropropene
ug/L
<0.25
20
20
25.7
21.6
128
108
60-140
17
Dibromochloromethane
ug/L
<0.25
20
20
23.4
23.3
117
117
60-140
0
Dibromomethane
ug/L
<0.25
20
20
22.7
22.5
114
112
60-140
1
Dichlorodifluoromethane
ug/L
<0.25
20
20
35.0
32.1
175
160
60-140
9 M1
Diisopropyl ether
ug/L
<0.25
20
20
22.9
23.5
115
117
60-140
2
Ethylbenzene
ug/L
<0.25
20
20
24.2
23.7
121
118
60-140
2
Hexachloro-1,3-butadiene
ug/L
<1.0
20
20
28.1
24.0
141
120
60-140
16 M1
Isopropylbenzene (Cumene)
ug/L
<0.25
20
20
24.2
23.5
121
117
60-140
3
m&p-Xylene
ug/L
<0.50
40
40
48.2
46.8
121
117
60-140
3
Methyl-tert-butyl ether
ug/L
<0.25
20
20
23.1
23.5
115
117
60-140
2
Methylene Chloride
ug/L
<1.0
20
20
22.7
22.9
113
114
60-140
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 22

F/71aceAnalyfical'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS 67389
Pace Project No.: 92273972
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1598649
1598650
MS
MSD
92274322003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
<0.25
20
20
25.4
21.3
127
106
60-140
18
n-Propylbenzene
ug/L
<0.25
20
20
24.6
23.3
123
117
60-140
5
Naphthalene
ug/L
<1.0
20
20
25.2
24.0
126
120
60-140
5
o-Xylene
ug/L
<0.25
20
20
23.6
23.9
118
119
60-140
1
sec-Butylbenzene
ug/L
<0.25
20
20
24.6
22.8
123
114
60-140
7
Styrene
ug/L
<0.25
20
20
24.2
22.9
121
115
60-140
6
tert-Butylbenzene
ug/L
<0.25
20
20
20.7
19.9
103
99
60-140
4
Tetrachloroethene
ug/L
<0.25
20
20
24.1
23.0
120
115
60-140
5
Toluene
ug/L
<0.25
20
20
25.0
24.2
125
121
60-140
3
trans- 1,2-Dichloroethene
ug/L
<0.25
20
20
23.9
23.7
120
118
60-140
1
trans- 1,3-Dichloropropene
ug/L
<0.25
20
20
25.4
22.0
127
110
60-140
14
Trichloroethene
ug/L
<0.25
20
20
23.2
22.2
116
111
60-140
4
Trichlorofluoromethane
ug/L
<0.50
20
20
29.1
28.6
145
143
60-140
2 M1
Vinyl chloride
ug/L
<0.25
20
20
30.5
29.1
152
146
60-140
5 M1
1,2-Dichloroethane-d4 (S)
%
97
98
70-130
4-Bromofluorobenzene(S)
%
101
100
70-130
Toluene-d8 (S)
%
103
105
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc..
Page 19 of 22

17PaceAnalj cal
www pacelabs.00m
race Anaryn Cal Dervrces, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: WALSERS 67389
Pace Project No.: 92273972
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 22

.1aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WALSERS 67389
92273972
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92273972001
INFLUENT
MADEP VPH
GCV/10035
92273972002
EFFLUENT
MADEP VPH
GCV/10035
92273972002
EFFLUENT
EPA 200.7
MPRP/19933 EPA 200.7 ICP/17975
92273972001
INFLUENT
SM 6200B
MSV/34145
92273972002
EFFLUENT
SM 6200B
MSW34145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2015 04:28 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 22

i .PaceAnaJytical
CHAIN-OF-CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Pa e : 1 Of 1
Company Shield Engineering Report To: Flora D'Souza Attention: Flora D'Souza
Address 4301 Taggart Creek Road Copy To: Company Name: Shield Engineering
Charlotte, NC 28208
Address: .4301 Taggart Creek Road, Charlotte,.NcFa'sii)R8"Jlaf
Email To fdsouza shielden ineerin .com
Purchase Order No. 1990018-55 -
Pace Quote Reference:
UST - Underground Storage Tank
Phone [phone] JFax
Client Project ID: WALSERS
Pace Project Manager. Herrin ,.Kevin
�l�lF+wi i` aX iBinlr(fStato7 (wca8onbs)fia'f 7tdti?ii,r.?- 4.
Requested Due Dale/TAT: 10 Da Default
Container Order Number. 67389
Pace Profile B:
North Carolina
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SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
OilDIVISION
OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date 1/31/2018
Facility Name: Hill Oil Company, Inc. - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Hiahwav_ 150N
TYPE OF PERMITTED OPERATION BEING MONITORED
Lexnaton` NC 27295
County Davidson
❑ Lagoon El Remediation: Infiltration
9 Gallery
❑ Spray Field ® Remediation: GroUndWater
Contact Person. Flora D'Souza/Shield F_naineedna. Inc.
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Wals is Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 9/30/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: _min.
pH 5.73 units Temp. NM OC
DRY at
time ofsampling,
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NM µMhos
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/3/15 - 10/8/15
Laboratory Name: Pare Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead ND mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100mi
Phosphorus: Total ap. NA mg/I
(Note Use MPN method for highly turbid samples)
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/1
AIj- I i Il� NA mg/I
Aliphatic C05-008 0.0768 m /1
p � ) - 9
pH (when analyzed) NA units
�C B arium
NA mg/I
TOC NA mg/I
OgRjt ,_,,, ►
NA mg/I
Chloride NA mg/I
NA mg/I
Arsenic NA mg/I
fl 0 rh omium: Total
NA mg/1
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? IR Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I VPH method # MADFP VPH
(Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I ,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 4.7055 mg/L Effluent Total VOCs: 0.0768 mg/L VOC Removal% 98.37 �o
Flora D'Souza/Shield Enaineerina. Proiect Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007

APPENDIX A

Iac
eAnalytical
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Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
October 08, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on October 01, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 27

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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
WALSER'S 1990018-70
92270127
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92270127001
INFLUENT
MADEP VPH
ZDO
5
PASI-C
SM 6200B
CAH
63
PASI-C
92270127002
EFFLUENT
MADEP VPH
ZDO
5
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
WALSER'S 1990018-70
92270127
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92270127001
INFLUENT
MADEP VPH
Aliphatic (C05-008)
1440
ug/L
500
10/08/15 03:29
N2
MADEP VPH
Aliphatic (C09-C12)
1000
ug/L
500
10/08/15 03:29
N2
MADEP VPH
Aromatic (C09-C10)
708
ug/L
500
10/08/15 03:29
N2
SM 6200B
Benzene
17.5
ug/L
2.5
10/06/15 08:05
SM 6200B
1,2-Dibromoethane (EDB)
9.6
ug/L
2.5
10/06/15 08:05
SM 6200B
Ethylbenzene
62.0
ug/L
2.5
10/06/15 08:05
SM 6200B
Isopropylbenzene (Cumene)
4.1
ug/L
2.5
10/06/15 08:05
SM 6200B
Naphthalene
132
ug/L
10.0
10/06/15 08:05
SM 6200B
n-Propylbenzene
6.2
ug/L
2.5
10/06/15 08:05
SM 6200B
Toluene
606
ug/L
2.5
10/06/15 08:05
SM 6200B
1,2,4-Trimethylbenzene
41.3
ug/L
2.5
10/06/15 08:05
SM 6200B
1,3,5-Trimethylbenzene
63.8
ug/L
2.5
10/06/15 08:05
SM 6200B
m&p-Xylene
204
ug/L
5.0
10/06/15 08:05
SM 6200B
o-Xylene
411
ug/L
2.5
10/06/15 08:05
92270127002
EFFLUENT
MADEP VPH
Aliphatic (C05-008)
76.8
ug/L
50.0
10/08/15 01:59
N2
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: October 08. 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 27

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Pace Analytical Services, Inc.
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: October 08, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 27

aceA IXical
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PROJECT NARRATIVE
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: October 08, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: MSV/33665
L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: 1574795)
• Hexachloro-1,3-butadiene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/33640
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92270188002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1573642)
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1573643)
• Hexachloro-1,3-butadiene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 27

(��raceAnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: October 08, 2015
QC Batch: MSV/33665
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92270356021
MO: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 1574796)
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1574797)
• Hexachloro-1,3-butadiene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 8 of 27

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ANALYTICAL RESULTS
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: INFLUENT Lab ID: 92270127001 Collected: 09/30/15 13:00 Received: 10/01/15 14:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
.�3rIr17Pi6y9
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 10/08/2015 04:17 PM
Analytical Method: MADEP VPH
1440 ug/L
1000 ug/L
708 ug/L
96 %
96 %
Analytical Method: SM 6200B
17.5
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
9.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
62.0
ug/L
ND
ug/L
4.1
ug/L
500
10
10/08/15 03:29
500
10
10/08/15 03:29
500
10
10/08/15 03:29
70-130
10
10/08/15 03:29 460-00-4
70-130
10
10/08/15 03:29 460-00-4
N2
N2
N2
2.5
5
10/06/15 08:05
71-43-2
2.5
5
10/06/15 08:05
108-86-1
2.5
5
10/06/15 08:05
74-97-5
2.5
5
10/06/15 08:05
75-27-4
2.5
5
10/06/15 08:05
75-25-2
25.0
5
10/06/15 08:05
74-83-9
2.5
5
10/06/15 08:05
104-51-8
2.5
5
10/06/15 08:05
135-98-8
2.5
5
10/06/15 08:05
98-06-6
2.5
5
10/06/15 08:05
56-23-5
2.5
5
10/06/15 08:05
108-90-7
5.0
5
10/06/15 08:05
75-00-3
2.5
5
10/06/15 08:05
67-66-3
5.0
5
10/06/15 08:05
74-87-3
2.5
5
10/06/15 08:05
95-49-8
2.5
5
10/06/15 08:05
106-43-4
5.0
5
10/06/15 08:05
96-12-8
2.5
5
10/06/15 08:05
124-48-1
2.5
5
10/06/15 08:05
106-93-4
2.5
5
10/06/15 08:05
74-95-3
2.5
5
10/06/15 08:05
95-50-1
2.5
5
10/06/15 08:05
541-73-1
2.5
5
10/06/15 08:05
106-46-7
2.5
5
10/06/15 08:05
75-71-8
2.5
5
10/06/15 08:05
75-34-3
2.5
5
10/06/15 08:05
107-06-2
2.5
5
10/06/15 08:05
75-35-4
2.5
5
10/06/15 08:05
156-59-2
2.5
5
10/06/15 08:05
156-60-5
2.5
5
10/06/15 08:05
78-87-5
2.5
5
10/06/15 08:05
142-28-9
2.5
5
10/06/15 08:05
594-20-7
2.5
5
10/06/15 08:05
563-58-6
2.5
5
10/06/15 08:05
10061-01-5
2.5
5
10/06/15 08:05
10061-02-6
2.5
5
10/06/15 08:05
108-20-3
2.5
5
10/06/15 08:05
100-41-4
10.0
5
10/06/15 08:05
87-68-3 L3
2.5
5
10/06/15 08:05
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 27

/�� laceAnalXical'
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1
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Sample: INFLUENT Lab ID: 92270127001 Collected: 09/30/15 13:00 Received: 10/01/15 14:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Methylene Chloride
ND
ug/L
10.0
5
10/06/15 08:05
75-09-2
Methyl -tent -butyl ether
ND
ug/L
2.5
5
10/06/15 08:05
1634-04-4
Naphthalene
132
ug/L
10.0
5
10/06/15 08:05
91-20-3
n-Propylbenzene
6.2
ug/L
2.5
5
10/06/15 08:05
103-65-1
Styrene
ND
ug/L
2.5
5
10/06/15 08:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
2.5
5
10/06/15 08:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
2.5
5
10/06/15 08:05
79-34-5
Tetra chloroethene
ND
ug/L
2.5
5
10/06/15 08:05
127-18-4
Toluene
606
ug/L
2.5
5
10/06/15 08:05
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
10.0
5
10/06/15 08:05
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
10.0
5
10/06/15 08:05
120-82-1
1,1,1-Trichloroethane
ND
ug/L
2.5
5
10/06/15 08:05
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.5
5
10/06/15 08:05
79-00-5
Trichloroethene
ND
ug/L
2.5
5
10/06/15 08:05
79-01-6
Trichlorofluoromethane
ND
ug/L
5.0
5
10/06/15 08:05
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.5
5
10/06/15 08:05
96-18-4
1,2,4-Trimethylbenzene
41.3
ug/L
2.5
5
10/06/15 08:05
95-63-6
1,3,5-Trimethylbenzene
63.8
ug/L
2.5
5
10/06/15 08:05
108-67-8
Vinyl chloride
ND
ug/L
5.0
5
10/06/15 08:05
75-01-4
m&p-Xylene
204
ug/L
5.0
5
10/06/15 08:05
179601-23-1
o-Xylene
411
ug/L
2.5
5
10/06/15 08:05
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
5
10/06/15 08:05
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
5
10/06/15 08:05
460-00-4
Toluene-d8 (S)
100
%
70-130
5
10/06/15 08:05
2037-26-5
Date: 10/08/2015 04:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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�aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Sample: EFFLUENT Lab ID: 92270127002 Collected: 09/30/15 14:00 Received: 10/01/15 14:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
200.7 MET ICP
Lead
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Date: 10/08/2015 04:17 PM
Analytical Method: MADEP VPH
76.8
ug/L
50.0
1
10/08/15 01:59
N2
ND
ug/L
50.0
1
10/08/15 01:59
N2
ND
ug/L
50.0
1
10/08/15 01:59
N2
100
%
70-130
1
10/08/15 01:59
460-00-4
101
%
70-130
1
10/08/15 01:59
460-00-4
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND
ug/L
5.0
1 10/05/15 19:00
10/07/15 08:27
7439-92-1
Analytical Method: SM 6200B
ND
ug/L
0.50
1
10/03/15 00:33
71-43-2
ND
ug/L
0.50
1
10/03/15 00:33
108-86-1
ND
ug/L
0.50
1
10/03/15 00:33
74-97-5
ND
ug/L
0.50
1
10/03/15 00:33
75-27-4
ND
ug/L
0.50
1
10/03/15 00:33
75-25-2
ND
ug/L
5.0
1
10/03/15 00:33
74-83-9
ND
ug/L
0.50
1
10/03/15 00:33
104-51-8
ND
ug/L
0.50
1
10/03/15 00:33
135-98-8
ND
ug/L
0.50
1
10/03/15 00:33
98-06-6
ND
ug/L
0.50
1
10/03/15 00:33
56-23-5
ND
ug/L
0.50
1
10/03/15 00:33
108-90-7
ND
ug/L
1.0
1
10/03/15 00:33
75-00-3
ND
ug/L
0.50
1
10/03/15 00:33
67-66-3
ND
ug/L
1.0
1
10/03/15 00:33
74-87-3
ND
ug/L
0.50
1
10/03/15 00:33
95-49-8
ND
ug/L
0.50
1
10/03/15 00:33
106-43-4
ND
ug/L
1.0
1
10/03/15 00:33
96-12-8
ND
ug/L
0.50
1
10/03/15 00:33
124-48-1
ND
ug/L
0.50
1
10/03/15 00:33
106-93-4
ND
ug/L
0.50
1
10/03/15 00:33
74-95-3
ND
ug/L
0.50
1
10/03/15 00:33
95-50-1
ND
ug/L
0.50
1
10/03/15 00:33
541-73-1
ND
ug/L
0.50
1
10/03/15 00:33
106-46-7
ND
ug/L
0.50
1
10/03/15 00:33
75-71-8
ND
ug/L
0.50
1
10/03/15 00:33
75-34-3
ND
ug/L
0.50
1
10/03/15 00:33
107-06-2
ND
ug/L
0.50
1
10/03/15 00:33
75-35-4
ND
ug/L
0.50
1
10/03/15 00:33
156-59-2
ND
ug/L
0.50
1
10/03/15 00:33
156-60-5
ND
ug/L
0.50
1
10/03/15 00:33
78-87-5
ND
ug/L
0.50
1
10/03/15 00:33
142-28-9
ND
ug/L
0.50
1
10/03/15 00:33
594-20-7
ND
ug/L
0.50
1
10/03/15 00:33
563-58-6
ND
ug/L
0.50
1
10/03/15 00:33
10061-01-5
ND
ug/L
0.50
1
10/03/15 00:33
10061-02-6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Sample: EFFLUENT Lab ID: 92270127002 Collected: 09/30/15 14:00 Received: 10/01/15 14:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 10/08/2015 04:17 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
102 %
101 %
101 %
0.50
1
10/03/15 00:33
108-20-3
0.50
1
10/03/15 00:33
100-41-4
2.0
1
10/03/15 00:33
87-68-3
0.50
1
10/03/15 00:33
98-82-8
2.0
1
10/03/15 00:33
75-09-2
0.50
1
10/03/15 00:33
1634-04-4
2.0
1
10/03/15 00:33
91-20-3
0.50
1
10/03/15 00:33
103-65-1
0.50
1
10/03/15 00:33
100-42-5
0.50
1
10/03/15 00:33
630-20-6
0.50
1
10/03/15 00:33
79-34-5
0.50
1
10/03/15 00:33
127-18-4
0.50
1
10/03/15 00:33
108-88-3
2.0
1
10/03/15 00:33
87-61-6
2.0
1
10/03/15 00:33
120-82-1
0.50
1
10/03/15 00:33
71-55-6
0.50
1
10/03/15 00:33
79-00-5
0.50
1
10/03/15 00:33
79-01-6
1.0
1
10/03/15 00:33
75-69-4
0.50
1
10/03/15 00:33
96-18-4
0.50
1
10/03/15 00:33
95-63-6
0.50
1
10/03/15 00:33
108-67-8
1.0
1
10/03/15 00:33
75-01-4
1.0
1
10/03/15 00:33
179601-23-1
0.50
1
10/03/15 00:33
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
10/03/15 00:33 17060-07-0
10/03/15 00:33 460-00-4
10/03/15 00:33 2037-26-5
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QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
QC Batch: GCV/9947 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92270127001, 92270127002
METHOD BLANK: 1575172
Associated Lab Samples: 92270127001, 92270127002
Parameter
Units
Aliphatic (C05-CO8)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
10/07/15 22:28 N2
ND
50.0
10/07/15 22:28 N2
ND
50.0
10/07/15 22:28 N2
97
70-130
10/07/15 22:28
97
70-130
10/07/15 22:28
LABORATORY CONTROL SAMPLE & LCSD: 1575173
Spike
Parameter Units Conc.
Aliphatic (C05-CO8) ug/L 300
Aliphatic (CO9-Cl2) ug/L 300
Aromatic (C09-C10) ug/L 100
4-Bromofluorobenzene (FID) (S) %
4-Bromofluorobenzene (PID) (S) %
1575174
LCS
LCSD
LCS
LCSD
% Rec
Result
Result
% Rec
% Rec
Limits
302
294
101
98
70-130
289
287
96
96
30-130
104
100
104
100
70-130
98
98
70-130
111
110
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD RPD Qualifiers
3 25 N2
1 25 N2
4 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 27

A�ace Analytical
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Pace Analytical Services, Inc.
9800 Kincey Ave- Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
WALSER'S 1990018-70
Pace Project No.:
92270127
QC Batch:
MPRP/19718 Analysis Method: EPA 200.7
QC Batch Method:
EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples:
92270127002
METHOD BLANK: 1574735
Associated Lab Samples: 92270127002
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1574736
Parameter Units
Lead ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/07/15 07:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 452 90 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1574737 1574738
MS MSD
92270216002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 436 449 87 90 70-130 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1574739 1574740
MS MSD
92270258002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L 0.010 500 500 445 493 87 96 70-130 10
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 10/08/2015 04:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 27

/�acmnalXica(
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I
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
QC Batch: MSV/33640 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92270127002
METHOD BLANK: 1573640
Associated Lab Samples: 92270127002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
10/02/15 23:44
1,1,1-Trichloroethane
ug/L
ND
0.50
10102/1523:44
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
10/02/15 23:44
1,1,2-Trichloroethane
ug/L
ND
0.50
10/02/15 23:44
1,1-Dichloroethane
ug/L
ND
0.50
10/02/15 23:44
1,1-Dichloroethene
ug/L
ND
0.50
10/02/15 23:44
1,1-Dichloropropene
ug/L
ND
0.50
10/02/15 23:44
1,2,3-Trichlorobenzene
ug/L
ND
2.0
10/02/15 23:44
1,2,3-Trichloropropane
ug/L
ND
0.50
10/02/15 23:44
1,2,4-Trichlorobenzene
ug/L
ND
2.0
10/02/15 23:44
1,2,4-Trimethylbenzene
ug/L
ND
0.50
10/02/15 23:44
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
10/02/15 23:44
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
10/02/15 23:44
1,2-Dichlorobenzene
ug/L
ND
0.50
10/02/15 23:44
1,2-Dichloroethane
ug/L
ND
0.50
10/02/15 23:44
1,2-Dichloropropane
ug/L
ND
0.50
10/02/15 23:44
1,3,5-Trimethylbenzene
ug/L
ND
0.50
10/02/15 23:44
1,3-Dichlorobenzene
ug/L
ND
0.50
10/02/15 23:44
1,3-Dichloropropane
ug/L
ND
0.50
10/02/15 23:44
1,4-Dichlorobenzene
ug/L
ND
0.50
10/02/15 23:44
2,2-Dichloropropane
ug/L
ND
0.50
10/02/15 23:44
2-Chlorotoluene
ug/L
ND
0.50
10/02/15 23:44
4-Chlorotoluene
ug/L
ND
0.50
10/02/15 23:44
Benzene
ug/L
ND
0.50
10/02/15 23:44
Bromobenzene
ug/L
ND
0.50
10/02/15 23:44
Bromochloromethane
ug/L
ND
0.50
10/02/15 23:44
Bromodichloromethane
ug/L
ND
0.50
10/02/15 23:44
Bromoform
ug/L
ND
0.50
10/02/15 23:44
Bromomethane
ug/L
ND
5.0
10/02/15 23:44
Carbon tetrachloride
ug/L
ND
0.50
10/02/15 23:44
Chlorobenzene
ug/L
ND
0.50
10/02/15 23:44
Chloroethane
ug/L
ND
1.0
10/02/15 23:44
Chloroform
ug/L
ND
0.50
10/02/15 23:44
Chloromethane
ug/L
ND
1.0
10/02/15 23:44
cis-1,2-Dichloroethene
ug/L
ND
0.50
10/02/15 23:44
cis-1,3-Dichloropropene
ug/L
ND
0.50
10/02/15 23:44
Dibromochloromethane
ug/L
ND
0.50
10/02/15 23:44
Dibromomethane
ug/L
ND
0.50
10/02/15 23:44
Dichlorodifluoromethane
ug/L
ND
0.50
10/02/15 23:44
Diisopropyl ether
ug/L
ND
0.50
10/02/15 23:44
Ethylbenzene
ug/L
ND
0.50
10/02/15 23:44
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 27

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QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
METHOD BLANK: 1573640
Associated Lab Samples: 92270127002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
10/02/15 23:44
Isopropylbenzene (Cumene)
ug/L
ND
0.50
10/02/15 23:44
m&p-Xylene
ug/L
ND
1.0
10/02/15 23:44
Methyl-tert-butyl ether
ug/L
ND
0.50
10/02/15 23:44
Methylene Chloride
ug/L
ND
2.0
10/02/15 23:44
n-Butylbenzene
ug/L
ND
0.50
10/02/15 23:44
n-Propylbenzene
ug/L
ND
0.50
10/02/15 23:44
Naphthalene
ug/L
ND
2.0
10/02/15 23:44
o-Xylene
ug/L
ND
0.50
10/02/15 23:44
sec-Butylbenzene
ug/L
ND
0.50
10/02/15 23:44
Styrene
ug/L
ND
0.50
10/02/15 23:44
tert-Butylbenzene
ug/L
ND
0.50
10/02/15 23:44
Tetrachloroethene
ug/L
ND
0.50
10/02/15 23:44
Toluene
ug/L
ND
0.50
10/02/15 23:44
trans-1,2-Dichloroethene
ug/L
ND
0.50
10/02/15 23:44
trans-1,3-Dichloropropene
ug/L
ND
0.50
10/02/15 23:44
Trichloroethene
ug/L
ND
0.50
10/02/15 23:44
Trichlorofluoromethane
ug/L
ND
1.0
10/02/15 23:44
Vinyl chloride
ug/L
ND
1.0
10/02/15 23:44
1,2-Dichloroethane-d4 (S)
%
101
70-130
10/02/15 23:44
4-Bromofluorobenzene (S)
%
100
70-130
10/02/15 23:44
Toluene-d8 (S)
%
101
70-130
10/02/15 23:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1573641
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
50.7
101
60-140
1, 1, 1 -Trichloroethane
ug/L
50
55.2
110
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.5
103
60-140
1,1,2-Trichloroethane
ug/L
50
50.2
100
60-140
1, 1 -Dichloroethane
ug/L
50
53.3
107
60-140
1,1-Dichloroethene
ug/L
50
53.8
108
60-140
1, 1 -Dichloropropene
ug/L
50
52.5
105
60-140
1,2,3-Trichlorobenzene
ug/L
50
47.4
95
60-140
1,2,3-Trichloropropane
ug/L
50
47.7
95
60-140
1,2,4-Trichlorobe nzene
ug/L
50
47.9
96
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.1
104
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
51.8
104
60-140
1,2-Dibromoethane (EDB)
ug/L
50
52.1
104
60-140
1,2-Dichlorobenzene
ug/L
50
50.6
101
60-140
1,2-Dichloroethane
ug/L
50
46.5
93
60-140
1,2-Dichloropropane
ug/L
50
50.2
100
60-140
1,3,5-Trimethylbenzene
ug/L
50
52.9
106
60-140
1,3-Dichlorobenzene
ug/L
50
50.4
101
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 27

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QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
LABORATORY CONTROL SAMPLE:
Parameter
1573641
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
50.5
101
60-140
1,4-Dichlorobenzene
ug/L
50
49.9
100
60-140
2,2-Dichloropropane
ug/L
50
49.5
99
60-140
2-Chlorotoluene
ug/L
50
51.7
103
60-140
4-Chlorotoluene
ug/L
50
51.0
102
60-140
Benzene
ug/L
50
52.8
106
60-140
Bromobenzene
ug/L
50
50.5
101
60-140
Bromochloromethane
ug/L
50
53.4
107
60-140
Bromodichloromethane
ug/L
50
51.0
102
60-140
Bromoform
ug/L
50
49.4
99
60-140
Bromomethane
ug/L
50
45.9
92
60-140
Carbon tetrachloride
ug/L
50
54.1
108
60-140
Chlorobenzene
ug/L
50
50.2
100
60-140
Chloroethane
ug/L
50
45.9
92
60-140
Chloroform
ug/L
50
50.0
100
60-140
Chloromethane
ug/L
50
55.5
111
60-140
cis- 1,2-Dichloroethene
ug/L
50
51.6
103
60-140
cis- 1,3-Dichloropropene
ug/L
50
51.6
103
60-140
Dibromochloromethane
ug/L
50
51.6
103
60-140
Dibromomethane
ug/L
50
51.6
103
60-140
Dichlorodifluoromethane
ug/L
50
46.0
92
60-140
Diisopropyl ether
ug/L
50
55.2
110
60-140
Ethylbenzene
ug/L
50
52.1
104
60-140
Hexachloro-1,3-butadiene
ug/L
50
67.8
136
60-140
Isopropylbenzene (Cumene)
ug/L
50
56.3
113
60-140
m&p-Xylene
ug/L
100
103
103
60-140
Methyl-tert-butyl ether
ug/L
50
53.8
108
60-140
Methylene Chloride
ug/L
50
49.1
98
60-140
n-Butylbenzene
ug/L
50
54.6
109
60-140
n-Propylbenzene
ug/L
50
52.8
106
60-140
Naphthalene
ug/L
50
50.7
101
60-140
o-Xylene
ug/L
50
51.8
104
60-140
sec-Butylbenzene
ug/L
50
56.2
112
60-140
Styrene
ug/L
50
53.2
106
60-140
tert-Butylbenzene
ug/L
50
44.8
90
60-140
Tetrachloroethene
ug/L
50
49.9
100
60-140
Toluene
ug/L
50
51.7
103
60-140
trans- 1,2-Dichloroethene
ug/L
50
52.4
105
60-140
trans-1,3-Dichloropropene
ug/L
50
50.6
101
60-140
Trichloroethene
ug/L
50
51.2
102
60-140
Trichlorofluoromethane
ug/L
50
55.2
110
60-140
Vinyl chloride
ug/L
50
56.9
114
60-140
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene(S)
%
102
70-130
Toluene-d8 (S)
%
99
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 27

aceMalytical
/ www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1573642
1573643
MS
MSD
92270188002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.9
20.7
105
104
60-140
1
1,1,1-Trichloroethane
ug/L
ND
20
20
26.1
24.7
130
123
60-140
6
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.3
22.0
111
110
60-140
1
1,1,2-Trichloroethane
ug/L
ND
20
20
21.7
21.5
109
108
60-140
1
1,1-Dichloroethane
ug/L
ND
20
20
24.7
23.7
124
119
60-140
4
1,1-Dichloroethene
ug/L
ND
20
20
26.0
25.1
130
126
60-140
3
1,1-Dichloropropene
ug/L
ND
20
20
25.3
23.8
126
119
60-140
6
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.3
18.4
101
92
60-140
10
1,2,3-Trichloropropane
ug/L
ND
20
20
20.8
20.7
104
104
60-140
0
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.0
19.3
105
96
60-140
9
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.6
22.2
113
111
60-140
2
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.1
19.8
106
99
60-140
7
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.2
22.2
111
111
60-140
0
1,2-Dichlorobenzene
ug/L
ND
20
20
22.0
21.3
110
107
60-140
3
1,2-Dichloroethane
ug/L
ND
20
20
20.6
20.0
103
99
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
22.5
21.9
113
109
60-140
3
1,3,5-Trimethylbenzene
ug/L
ND
20
20
23.5
22.7
117
114
60-140
3
1,3-Dichlorobenzene
ug/L
ND
20
20
22.5
21.7
112
108
60-140
4
1,3-Dichloropropane
ug/L
ND
20
20
21.6
21.8
108
109
60-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
22.3
21.5
111
108
60-140
3
2,2-Dichloropropane
ug/L
ND
20
20
23.9
21.0
119
105
60-140
13
2-Chlorotoluene
ug/L
ND
20
20
22.5
21.8
113
109
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
22.9
22.2
114
111
60-140
3
Benzene
ug/L
ND
20
20
24.3
23.1
121
116
60-140
5
Bromobenzene
ug/L
ND
20
20
22.1
21.8
111
109
60-140
1
Bromochloromethane
ug/L
ND
20
20
23.8
22.5
119
112
60-140
6
Bromodichloromethane
ug/L
ND
20
20
22.2
21.2
111
106
60-140
5
Bromoform
ug/L
ND
20
20
19.6
18.2
98
91
60-140
7
Bromomethane
ug/L
ND
20
20
23.1
21.3
115
107
60-140
8
Carbon tetrachloride
ug/L
ND
20
20
25.3
24.5
127
123
60-140
3
Chlorobenzene
ug/L
ND
20
20
22.4
22.1
112
111
60-140
1
Chloroethane
ug/L
ND
20
20
22.9
21.9
114
110
60-140
4
Chloroform
ug/L
ND
20
20
23.6
22.2
117
110
60-140
6
Chloromethane
ug/L
ND
20
20
24.0
24.2
120
121
60-140
1
cis- 1,2-Dichloroethene
ug/L
ND
20
20
23.5
22.7
118
114
60-140
4
cis- 1,3-Dichloropropene
ug/L
ND
20
20
21.6
20.0
108
100
60-140
8
Dibromochloromethane
ug/L
ND
20
20
20.9
20.2
105
101
60-140
3
Dibromomethane
ug/L
ND
20
20
22.3
21.3
111
106
60-140
4
Dichlorodifluoromethane
ug/L
ND
20
20
19.5
22.5
97
113
60-140
14
Diisopropyl ether
ug/L
ND
20
20
24.6
23.3
123
117
60-140
5
Ethylbenzene
ug/L
ND
20
20
23.3
23.3
116
116
60-140
0
Hexachloro-1,3-butadiene
ug/L
ND
20
20
33.9
28.6
170
143
60-140
17 M1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
24.8
24.9
124
124
60-140
1
m&p-Xylene
ug/L
ND
40
40
46.1
45.3
115
113
60-140
2
Methyl-tert-butyl ether
ug/L
ND
20
20
23.5
22.5
118
112
60-140
5
Methylene Chloride
ug/L
ND
20
20
21.6
20.3
108
101
60-140
6
Results presented on
this page are in
the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF
LABORATORY ANALYSIS
This
report shall
not be reproduced, except in full,
Date: 10/08/2015 04:17 PM
without
the written consent of Pace
Analytical
Services, Inc..
Page 18 of 27

ace Analytical
www.p"labs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1573642
1573643
MS
MSD
92270188002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
23.4
22.6
117
113
60-140
4
n-Propylbenzene
ug/L
ND
20
20
23.9
23.2
120
116
60-140
3
Naphthalene
ug/L
ND
20
20
22.2
19.0
111
95
60-140
16
o-Xylene
ug/L
ND
20
20
23.0
22.7
115
114
60-140
1
sec-Butylbenzene
ug/L
ND
20
20
25.1
24.4
125
122
60-140
3
Styrene
ug/L
ND
20
20
22.5
22.5
112
113
60-140
0
tert-Butylbenzene
ug/L
ND
20
20
19.7
19.3
98
96
60-140
2
Tetra chloroethene
ug/L
ND
20
20
22.7
22.3
114
112
60-140
2
Toluene
ug/L
ND
20
20
23.6
23.3
118
116
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.6
23.6
123
118
60-140
4
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.5
19.9
107
100
60-140
7
Trichloroethene
ug/L
ND
20
20
23.4
22.8
117
114
60-140
2
Trichlorofluoromethane
ug/L
ND
20
20
26.7
26.4
133
132
60-140
1
Vinyl chloride
ug/L
ND
20
20
26.6
26.7
133
133
60-140
0
1,2-Dichloroethane-d4 (S)
%
101
99
70-130
4-Bromofluorobenzene (S)
%
101
101
70-130
Toluene-d8 (S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 27

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
QC Batch: MSV/33665 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92270127001
METHOD BLANK: 1574794
Associated Lab Samples: 92270127001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
10/06/15 04:46
1,1,1-Trichloroethane
ug/L
ND
0.50
10/06/15 04:46
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
10/06/15 04:46
1,1,2-Trichloroethane
ug/L
ND
0.50
10/06/15 04:46
1,1-Dichloroethane
ug/L
ND
0.50
10/06/15 04:46
1,1-Dichloroethene
ug/L
ND
0.50
10/06/15 04:46
1, 1 -Dichloropropene
ug/L
ND
0.50
10/06/15 04:46
1,2,3-Trichlorobe nzene
ug/L
ND
2.0
10/06/15 04:46
1,2,3-Trichloropropane
ug/L
ND
0.50
10/06/15 04:46
1,2,4-Trichlorobe nzene
ug/L
ND
2.0
10/06/15 04:46
1,2,4-Trimethylbenzene
ug/L
ND
0.50
10/06/15 04:46
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
10/06/15 04:46
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
10/06/15 04:46
1,2-Dichlorobenzene
ug/L
ND
0.50
10/06/15 04:46
1,2-Dichloroethane
ug/L
ND
0.50
10/06/15 04:46
1,2-Dichloropropane
ug/L
ND
0.50
10/06/15 04:46
1,3,5-Trimethylbenzene
ug/L
ND
0.50
10/06/15 04:46
1,3-Dichlorobenzene
ug/L
ND
0.50
10/06/15 04:46
1,3-Dichloropropane
ug/L
ND
0.50
10/06/15 04:46
1,4-Dichlorobenzene
ug/L
ND
0.50
10/06/15 04:46
2,2-Dichloropropane
ug/L
NO
0.50
10/06/15 04:46
2-Chlorotoluene
ug/L
ND
0.50
10/06/15 04:46
4-Chlorotoluene
ug/L
ND
0.50
10/06/15 04:46
Benzene
ug/L
ND
0.50
10/06/15 04:46
Bromobenzene
ug/L
ND
0.50
10/06/15 04:46
Bromochloromethane
ug/L
ND
0.50
10/06/15 04:46
Bromodichloromethane
ug/L
ND
0.50
10/06/15 04:46
Bromoform
ug/L
ND
0.50
10/06/15 04:46
Bromomethane
ug/L
ND
5.0
10/06/15 04:46
Carbon tetrachloride
ug/L
ND
0.50
10/06/15 04:46
Chlorobenzene
ug/L
ND
0.50
10/06/15 04:46
Chloroethane
ug/L
ND
1.0
10/06/15 04:46
Chloroform
ug/L
ND
0.50
10/06/15 04:46
Chloromethane
ug/L
ND
1.0
10/06/15 04:46
cis-1,2-Dichloroethene
ug/L
ND
0.50
10/06/15 04:46
cis- 1,3-Dichloropropene
ug/L
ND
0.50
10/06/15 04:46
Dibromochloromethane
ug/L
ND
0.50
10/06/15 04:46
Dibromomethane
ug/L
ND
0.50
10/06/15 04:46
Dichlorodifluoromethane
ug/L
ND
0.50
10/06/15 04:46
Diisopropyl ether
ug/L
ND
0.50
10/06/15 04:46
Ethylbenzene
ug/L
ND
0.50
10/06/15 04:46
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 27

I�YaceAnalXical
/ wwwpacelabs.com
i
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
METHOD BLANK: 1574794
Associated Lab Samples: 92270127001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
10/06/15 04:46
Isopropylbenzene (Cumene)
ug/L
ND
0.50
10/06/15 04:46
m&p-Xylene
ug/L
ND
1.0
10/06/15 04:46
Methyl-tert-butyl ether
ug/L
ND
0.50
10/06/15 04:46
Methylene Chloride
ug/L
ND
2.0
10/06/15 04:46
n-Butylbenzene
ug/L
ND
0.50
10/06/15 04:46
n-Propylbenzene
ug/L
ND
0.50
10/06/15 04:46
Naphthalene
ug/L
ND
2.0
10/06/15 04:46
o-Xylene
ug/L
ND
0.50
10/06/15 04:46
sec-Butylbenzene
ug/L
ND
0.50
10/06/15 04:46
Styrene
ug/L
ND
0.50
10/06/15 04:46
tert-Butylbenzene
ug/L
ND
0.50
10/06/15 04:46
Tetrachloroethene
ug/L
ND
0.50
10/06/15 04:46
Toluene
ug/L
ND
0.50
10/06/15 04:46
trans-1,2-Dichloroethene
ug/L
ND
0.50
10/06/15 04:46
trans-1,3-Dichloropropene
ug/L
ND
0.50
10/06/15 04:46
Trichloroethene
ug/L
ND
0.50
10/06/15 04:46
Trichlorofluoromethane
ug/L
ND
1.0
10/06/15 04:46
Vinyl chloride
ug/L
ND
1.0
10/06/15 04:46
1,2-Dichloroethane-d4 (S)
%
97
70-130
10/06/15 04:46
4-Bromofluorobenzene (S)
%
101
70-130
10/06/15 04:46
Toluene-d8 (S)
%
99
70-130
10/06/15 04:46
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1574795
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.3
109
60-140
1,1,1-Trichloroethane
ug/L
50
59.6
119
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
57.9
116
60-140
1,1,2-Trichloroethane
ug/L
50
54.8
110
60-140
1, 1 -Dichloroethane
ug/L
50
57.2
114
60-140
1, 1 -Dichloroethene
ug/L
50
58.2
116
60-140
1, 1 -Dichloropropene
ug/L
50
58.3
117
60-140
1,2,3-Trichlorobenzene
ug/L
50
54.5
109
60-140
1,2,3-Trichloropropane
ug/L
50
52.8
106
60-140
1,2,4-Trichlorobenzene
ug/L
50
54.9
110
60-140
1,2,4-Trimethylbenzene
ug/L
50
56.6
113
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
59.4
119
60-140
1,2-Dibromoethane (EDB)
ug/L
50
57.5
115
60-140
1,2-Dichlorobenzene
ug/L
50
55.2
110
60-140
1,2-Dichloroethane
ug/L
50
49.0
98
60-140
1,2-Dichloropropane
ug/L
50
54.9
110
60-140
1,3,5-Trimethylbenzene
ug/L
50
57.2
114
60-140
1,3-Dichlorobenzene
ug/L
50
55.3
111
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 27

aceAnalXical
/ www.pacelabs.com
1
i
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1574795
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,3-Dichloropropane
ug/L
50
56.0
112
60-140
1,4-Dichlorobenzene
ug/L
50
54.3
109
60-140
2,2-Dichloropropane
ug/L
50
51.4
103
60-140
2-Chlorotoluene
ug/L
50
55.5
111
60-140
4-Chlorotoluene
ug/L
50
55.8
112
60-140
Benzene
ug/L
50
58.4
117
60-140
Bromobenzene
ug/L
50
55.3
111
60-140
Bromochloromethane
ug/L
50
57.2
114
60-140
Bromodichloromethane
ug/L
50
55.8
112
60-140
Bromoform
ug/L
50
52.8
106
60-140
Bromomethane
ug/L
50
53.8
108
60-140
Carbon tetrachloride
ug/L
50
59.4
119
60-140
Chlorobenzene
ug/L
50
55.3
111
60-140
Chloroethane
ug/L
50
51.8
104
60-140
Chloroform
ug/L
50
54.1
108
60-140
Chloromethane
ug/L
50
58.3
117
60-140
cis- 1,2-Dichloroethene
ug/L
50
55.7
111
60-140
cis-1,3-Dichloropropene
ug/L
50
55.8
112
60-140
Dibromochloromethane
ug/L
50
55.5
111
60-140
Dibromomethane
ug/L
50
55.9
112
60-140
Dichlorodifluoromethane
ug/L
50
50.5
101
60-140
Diisopropyl ether
ug/L
50
59.1
118
60-140
Ethylbenzene
ug/L
50
57.5
115
60-140
Hexachloro-1,3-butadiene
ug/L
50
75.4
151
60-140 LO
Isopropylbenzene (Cumene)
ug/L
50
62.5
125
60-140
m&p-Xylene
ug/L
100
114
114
60-140
Methyl-tert-butyl ether
ug/L
50
58.1
116
60-140
Methylene Chloride
ug/L
50
53.2
106
60-140
n-Butylbenzene
ug/L
50
58.7
117
60-140
n-Propylbenzene
ug/L
50
57.3
115
60-140
Naphthalene
ug/L
50
60.2
120
60-140
o-Xylene
ug/L
50
57.2
114
60-140
sec-Butylbenzene
ug/L
50
60.8
122
60-140
Styrene
ug/L
50
58.6
117
60-140
tert-Butylbenzene
ug/L
50
48.7
97
60-140
Tetrachloroethene
ug/L
50
54.6
109
60-140
Toluene
ug/L
50
57.3
115
60-140
trans-1,2-Dichloroethene
ug/L
50
56.7
113
60-140
trans-1,3-Dichloropropene
ug/L
50
55.1
110
60-140
Trichloroethene
ug/L
50
55.8
112
60-140
Trichlorofluoromethane
ug/L
50
59.1
118
60-140
Vinyl chloride
ug/L
50
62.7
125
60-140
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene(S)
%
103
70-130
Toluene-d8 (S)
%
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 27

Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
aceAnalytical
wwwpacelabs.com
1
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1574796
1574797
MS
MSD
92270356021
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD
Qua[
1,1,1,2-Tetrachloroethane
ug/L
<0.50
20
20
20.6
21.0
103
105
60-140
2
1,1,1-Trichloroethane
ug/L
<0.50
20
20
25.3
25.0
127
125
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
<0.50
20
20
23.5
22.7
117
114
60-140
3
1,1,2-Trichloroethane
ug/L
<0.50
20
20
22.5
21.7
112
109
60-140
4
1, 1 -Dichloroethane
ug/L
<0.50
20
20
24.0
24.2
120
121
60-140
1
1, 1 -Dichloroethene
ug/L
<0.50
20
20
25.3
25.6
126
128
60-140
1
1,1-Dichloropropene
ug/L
<0.50
20
20
24.9
24.6
125
123
60-140
1
1,2,3-Trichlorobenzene
ug/L
<2.0
20
20
21.5
19.9
108
100
60-140
8
1,2,3-Trichloropropane
ug/L
<0.50
20
20
21.5
20.9
108
105
60-140
3
1,2,4-Trichlorobenzene
ug/L
<2.0
20
20
21.3
21.0
107
105
60-140
1
1,2,4-Trimethylbenzene
ug/L
<0.50
20
20
23.4
23.2
117
116
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
<1.0
20
20
22.0
19.9
110
99
60-140
10
1,2-Dibromoethane (EDB)
ug/L
<0.50
20
20
23.1
22.9
115
114
60-140
1
1,2-Dichlorobenzene
ug/L
<0.50
20
20
21.7
22.0
109
110
60-140
1
1,2-Dichloroethane
ug/L
<0.50
20
20
19.9
19.9
99
99
60-140
0
1,2-Dichloropropane
ug/L
<0.50
20
20
23.1
22.7
115
113
60-140
2
1,3,5-Trimethylbenzene
ug/L
<0.50
20
20
23.6
23.6
118
118
60-140
0
1,3-Dichlorobenzene
ug/L
<0.50
20
20
22.3
22.8
111
114
60-140
2
1,3-Dichloropropane
ug/L
<0.50
20
20
22.5
22.3
113
111
60-140
1
1,4-Dichlorobenzene
ug/L
<0.50
20
20
21.9
22.1
110
110
60-140
1
2,2-Dichloropropane
ug/L
<0.50
20
20
19.5
19.9
98
100
60-140
2
2-Chlorotoluene
ug/L
<0.50
20
20
22.1
23.5
110
117
60-140
6
4-Chlorotoluene
ug/L
<0.50
20
20
22.7
23.2
113
116
60-140
2
Benzene
ug/L
<0.50
20
20
24.6
24.6
123
123
60-140
0
Bromobenzene
ug/L
<0.50
20
20
22.3
23.0
112
115
60-140
3
Bromochloromethane
ug/L
<0.50
20
20
23.6
23.1
118
116
60-140
2
Bromodichloromethane
ug/L
<0.50
20
20
21.4
22.0
107
110
60-140
2
Bromoform
ug/L
<0.50
20
20
18.5
18.7
92
93
60-140
1
Bromomethane
ug/L
<5.0
20
20
26.0
25.5
130
128
60-140
2
Carbon tetrachloride
ug/L
<0.50
20
20
24.1
24.7
121
123
60-140
2
Chlorobenzene
ug/L
<0.50
20
20
22.8
22.9
114
115
60-140
0
Chloroethane
ug/L
<1.0
20
20
22.0
22.7
110
113
60-140
3
Chloroform
ug/L
<0.50
20
20
23.2
22.6
116
113
60-140
3
Chloromethane
ug/L
<1.0
20
20
24.6
24.7
123
124
60-140
1
cis- 1,2-Dichloroethene
ug/L
<0.50
20
20
23.1
23.0
115
115
60-140
0
cis-1,3-Dichloropropene
ug/L
<0.50
20
20
21.3
21.1
107
106
60-140
1
Dibromochloromethane
ug/L
<0.50
20
20
20.5
20.4
102
102
60-140
0
Dibromomethane
ug/L
<0.50
20
20
22.3
22.3
111
112
60-140
0
Dichlorodifluoromethane
ug/L
<0.50
20
20
22.8
22.7
114
113
60-140
1
Diisopropyl ether
ug/L
<0.50
20
20
23.8
23.5
118
117
60-140
1
Ethylbenzene
ug/L
<0.50
20
20
23.9
24.1
119
120
60-140
1
Hexachloro-1,3-butadiene
ug/L
<2.0
20
20
30.6
30.0
153
150
60-140
2 MO
Isopropylbenzene (Cumene)
ug/L
<0.50
20
20
25.5
25.2
128
126
60-140
1
m&p-Xylene
ug/L
<1.0
40
40
47.4
47.5
118
118
60-140
0
Methyl-tert-butyl ether
ug/L
160
20
20
186
185
129
125
60-140
0
Methylene Chloride
ug/L
<2.0
20
20
20.3
19.9
101
99
60-140
2
Results presented on this page are in
the units indicated by the "Units" column except where
an alternate
unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 27

laceAnalyiical
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I
QUALITY CONTROL DATA
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1574796 1574797
Parameter
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
92270356021
Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
ug/L
<0.50
20
20
22.7
22.9
113
115
60-140
1
ug/L
<0.50
20
20
23.7
23.9
119
119
60-140
1
ug/L
<2.0
20
20
26.2
22.4
131
112
60-140
16
ug/L
<0.50
20
20
23.7
23.6
119
118
60-140
1
ug/L
<0.50
20
20
24.7
25.0
124
125
60-140
1
ug/L
<0.50
20
20
23.3
23.5
116
117
60-140
1
ug/L
<0.50
20
20
20.1
20.0
101
100
60-140
1
ug/L
<0.50
20
20
22.9
22.9
114
115
60-140
0
ug/L
<0.50
20
20
24.5
24.2
122
121
60-140
1
ug/L
<0.50
20
20
24.1
24.1
121
120
60-140
0
ug/L
<0.50
20
20
20.5
20.7
102
103
60-140
1
ug/L
<0.50
20
20
23.9
23.8
119
119
60-140
0
ug/L
<1.0
20
20
26.5
25.9
133
130
60-140
2
ug/L
<1.0
20
20
27.3
28.0
137
140
60-140
2
%
97
96
70-130
%
101
100
70-130
%
102
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 24 of 27

aceAnalXical
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I
QUALIFIERS
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/08/2015 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 27

�IaceAnalytical
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i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WALSER'S 1990018-70
Pace Project No.: 92270127
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92270127001
INFLUENT
MADEP VPH
GCV/9947
92270127002
EFFLUENT
MADEP VPH
GCV/9947
92270127002
EFFLUENT
EPA 200.7
MPRP/19718 EPA 200.7
92270127001
INFLUENT
SM 6200B
MSV/33665
92270127002
EFFLUENT
SM 6200B
MSV/33640
Date: 10/08/2015 04:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/17770
Page 26 of 27

CHAIN -OF -CUSTODY / Analytical Request Document N
aceAnalytlpl The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
a -
Section A Section 8 Section C
Required Client Information: Required Project information: Invoice Information: Page: 1 Of
company: Shield Engineering Report To: Flora D'Souza Attentions Flora O'Souza
Address. 4301 Taggart Creek Road Copy To: Company Name: Shield Engineering
Charlotte, NC 28208
Address. 4301 Taggart Creek Road, Charlotte, N
Regulatory Agency :ar.>
Email To: fdsouza shielden ineerin .com
Purchase Order No. 1990018-70
Pace Quote Reference:
UST - Underground Storage Tank
Phone [phone] Fax
Client Project ID: WALSER'S
Pace Project Manager: Matt 6rainard
State I Location
Requested Due Date/TAT: 10 Day Default
Container Order Number.
Pace Profile
North Carolina
'-"Requested
Anal
sis
Filtered
M
-
.,.
a
Z
MATRIX com
0
v
COLLECTED
Z
Preservatives
>-
pr'mkmg Water Ow
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$
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wma Wr
Waarewm« Ww
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SAMPLE ID Pr�.n P
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�
=
START
END
}
oa
One Character per box, W'P. WP'
w
w
a
a
b
LFm—s'
3m.4
c
a
xt
Sample Ids must be unique T- '.TS
w
w
U10
v
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reF
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W
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u.
$
0
=
d
N
k
DATE
TIME
DATE
TIME
y
O
a
C
N
S
Z
S
2
2
Z
.4.
O
C
1
INFLUENT
WY11'�Pl'.5-
'J�
X
X
" 2'*
EFFLUENT
WT
X
X
X
OO
3
4
6
7
8
9
_. 10
11
12
-: ADDITIONAL, COMMENTS -
REUNQUISNEDiiY1AFFILIATION i'
.DATE'.
;=T1ME
••,ACCEPTEDSYfAFFILIATION.-
DATE
TIME.
$AMPLECONDITIONS
SAMPLER NAME AND SIGNATURE m
PRINT Name ofSAMPLER: �t� v N�
(vli/ ( tC�Ot �iit
J ��`��r�
a } w n�
W�v
n SIGNATURE of SAMPLER: DATE Signed:
O u o e
1_
/ 1- rL 8 U U N Y
lI � II� ■� � � I�'� I "�� �I� f
9227OIZI

ci MKAIT F00kj r1N VPI I rIUV PAPER nNI Y
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1 /31 /2018
Facility Name: Hill Oil Company Inc - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Highway 15ON
TYPE OF PERMITTED OPERATION BEING MONITORED
NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
= > "^r''
❑ Spray Field ® Remediation: GroUndWater
Contact Person: Flora D'Souza/Shield Enaineedna. Inc.
__ Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: fig_
❑ Water Source Heat Pump ❑ Other:
from Permit
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 8/20/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: min.
pH 5.98 units Temp. NM C
DRY at
time ofsampling,
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to eft. Spec. Cond. NMµMhos
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft. Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 8/24/15 - 8/31/15
Laboratory Name: Pace Analytical
Services Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/I
Nitrite (NOZ) as N
NA mg/I Pb - Lead ND mg/I
Coliform: MF Fecal NA /100m1
Nitrate (NO3) as N
NA mg/I Zn - Zinc NA mg/I
Coliform: MF Total NA /100mi
Phosphorus: Total as P
NA mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I Aliphatic (C05-CO8) = 0.0713 m9/1
pH (when analyzed) NA units
RF^��`e "Barium
NA m9/I Aliphatic (C09-C12) = 0.0547 mg/1
TOC NA mg/I
1� l ! Calcium
NA mg/I
Chloride NA mg/I
SEP 2 9 (XW�admium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA rng/I DWR SEC IKt Nu - Co fr
'
NA mg/I ORGANICS: (by GC, GC/MS, HPLC)
14FORMIATION
Phenol NA mg/I
PROCESS! U
e - ron
NA mg/I (Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I VOC , method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I VPH method # MADFP VPH
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
NA mg/I method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 14.55;i3mg/L Effluent Total VOCs: u• I co mg/L VOL; Removal /o UZ7• 1 � /u
GW-59 Rev.1/2007

APPENDIX A

/71aceAnalytical
www.pacelabs.com
race ranaiyucai services, uic.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(7 04 )875-9092
August 31, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSERS
Pace Project No.: 92264544
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on August 21, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 22

/71ac'eAnalytical
www.pacelabs.com
race �naiyucai oei vwaa, ow.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Project: WALSERS
Pace Project No.: 92264544
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 22

171aceAnalytical'
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race Anaiyticai services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
WALSERS
92264544
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92264544001
INFLUENT
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAN
63
PASI-C
92264544002
EFFLUENT
MADEP VPH
BFW
5
PASI-C
EPA 200.7
JDA
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 3 of 22

�71aceAnalytical
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I
rave hnmyu�ai om rwca, uw.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: WALSERS
Pace Project No.: 92264544
Lab Sample ID
Method
92264544001
MADEP VPH
MADEP VPH
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 62006
SM 6200B
92264544002
MADEP VPH
MADEP VPH
Client Sample ID
Parameters
INFLUENT
Aliphatic (C05-008)
Aliphatic (C09-C12)
Benzene
1,2-Dibromoethane (EDB)
Ethylbenzene
Isopropylbenzene (Cumene)
Naphthalene
Toluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m&p-Xylene
o-Xylene
EFFLUENT
Aliphatic (C05-008)
Aliphatic (C09-C12)
Result
Units
Report Limit
Analyzed
4010
ug/L
1250
08/24/1519:33
N2
6800
ug/L
1250
08/24/1519:33
N2
36.2
ug/L
2.5
08/28/15 20:10
7.2
ug/L
2.5
08/28/15 20:10
238
ug/L
2.5
08/28/15 20:10
12.8
ug/L
2.5
08/28/15 20:10
141
ug/L
10.0
08/28/15 20:10
1480
ug/L
6.2
08/31/15 11:50
264
ug/L
2.5
08/28/15 20:10
83.1
ug/L
2.5
08/28/15 20:10
958
ug/L
5.0
08/28/15 20:10
523
ug/L
2.5
08/28/15 20:10
71.3
ug/L
50.0
08/24/1514:18
N2
54.7
ug/L
50.0
08/24/1514:18
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 4 of 22

% la eAnalytical
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race M1141YLIUGI OCI-W., "".
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Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSERS
Pace Project No.: 92264544
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: August 31, 2015
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 5 of 22

/�IaceAnalXical
www.pacelabs.com
i
PROJECT NARRATIVE
Project: WALSERS
Pace Project No.: 92264544
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: August 31, 2015
race Anaryucai aervices, mc.
9600 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 200.7_ All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 22

/�00,
ace Analytical
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race rna�y u�m oci vwca, uw.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSERS
Pace Project No.: 92264544
Method: SM 6200B
Description: 6200B MSV
Client: Shield
Date: August 31, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 22

race Anaiyucat services, inc.
® 9800 Kincey Ave. Suite 100
laceAnalyfical Huntersville, NC 28078
www.pacelabs.com [phone]
r
ANALYTICAL RESULTS
Project: WALSERS
Pace Project No.: 92264544
Sample: INFLUENT
Lab ID: 92264544001 Collected:
08/20/15 13:00
Received: 08/21/15 14:42 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
VPH NC Water
Analytical Method: MADEP VPH
Aliphatic (C05-008)
4010
ug/L
1250
25
08/24/15 19:33
N2
Aliphatic (C09-C12)
6800
ug/L
1250
25
08/24/15 19:33
N2
Aromatic (C09-C10)
ND
ug/L
1250
25
08/24/15 19:33
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
90
%
70-130
25
08/24/15 19:33
460-00-4
4-Bromofluorobenzene (PID) (S)
74
%
70-130
25
08/24/15 19:33
460-00-4
6200E MSV
Analytical Method:
SM 6200B
Benzene
36.2
ug/L
2.5
5
08/28/15 20:10
71-43-2
Bromobenzene
ND
ug/L
2.5
5
08/28/15 20:10
108-86-1
Bromochloromethane
ND
ug/L
2.5
5
08/28/15 20:10
74-97-5
Bromodichloromethane
ND
ug/L
2.5
5
08/28/15 20:10
75-27-4
Bromoform
ND
ug/L
2.5
5
08/28/15 20:10
75-25-2
Bromomethane
ND
ug/L
25.0
5
08/28/15 20:10
74-83-9
n-Butylbenzene
ND
ug/L
2.5
5
08/28/15 20:10
104-51-8
sec-Butylbenzene
ND
ug/L
2.5
5
08/28/15 20:10
135-98-8
tert-Butylbenzene
ND
ug/L
2.5
5
08/28/15 20:10
98-06-6
Carbon tetrachloride
ND
ug/L
2.5
5
08/28/15 20:10
56-23-5
Chlorobenzene
ND
ug/L
2.5
5
08/28/15 20:10
108-90-7
Chloroethane
ND
ug/L
5.0
5
08/28/15 20:10
75-00-3
Chloroform
ND
ug/L
2.5
5
08/28/15 20:10
67-66-3
Chloromethane
ND
ug/L
5.0
5
08/28/15 20:10
74-87-3
2-Chlorotoluene
ND
ug/L
2.5
5
08/28/15 20:10
95-49-8
4-Chlorotoluene
ND
ug/L
2.5
5
08/28/15 20:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
5
08/28/15 20:10
96-12-8
Dibromochloromethane
ND
ug/L
2.5
5
08/28/15 20:10
124-48-1
1,2-Dibromoethane (EDB)
7.2
ug/L
2.5
5
08/28/15 20:10
106-93-4
Dibromomethane
ND
ug/L
2.5
5
08/28/15 20:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
2.5
5
08/28/15 20:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.5
5
08/28/15 20:10
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.5
5
08/28/15 20:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
2.5
5
08/28/15 20:10
75-71-8
1,1-Dichloroethane
ND
ug/L
2.5
5
08/28/15 20:10
75-34-3
1,2-Dichloroethane
ND
ug/L
2.5
5
08/28/15 20:10
107-06-2
1, 1 -Dichloroethene
ND
ug/L
2.5
5
08/28/15 20:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.5
5
08/28/15 20:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.5
5
08/28/15 20:10
156-60-5
1,2-Dichloropropane
ND
ug/L
2.5
5
08/28/15 20:10
78-87-5
1,3-Dichloropropane
ND
ug/L
2.5
5
08/28/15 20:10
142-28-9
2,2-Dichloropropane
ND
ug/L
2.5
5
08/28/15 20:10
594-20-7
1,1-Dichloropropene
ND
ug/L
2.5
5
08/28/15 20:10
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
2.5
5
08/28/15 20:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.5
5
08/28/15 20:10
10061-02-6
Diisopropyl ether
ND
ug/L
2.5
5
08/28/15 20:10
108-20-3
Ethylbenzene
238
ug/L
2.5
5
08/28/15 20:10
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
10.0
5
08/28/15 20:10
87-68-3
Isopropylbenzene (Cumene)
12.8
ug/L
2.5
5
08/28/15 20:10
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 22

laeAnalytical
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i
r-aceAnaryucm aefvices, uic.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSERS
Pace Project No.: 92264544
Sample: INFLUENT
Parameters
6200B MSV
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobe nzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/31/2015 04:53 PM
ANALYTICAL RESULTS
Lab ID: 92264544001 Collected: 08/20/15 13:00 Received: 08/21/15 14:42 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
141
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1480
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
264
ug/L
83.1
ug/L
ND
ug/L
958
ug/L
523
ug/L
102 %
100 %
100 %
10.0 5
2.5 5
10.0 5
2.5 5
2.5 5
2.5 5
2.5 5
2.5 5
6.2 12.5
10.0 5
10.0 5
2.5 5
2.5 5
2.5 5
5.0 5
2.5 5
2.5 5
2.5 5
5.0 5
5.0 5
2.5 5
70-130 5
70-130 5
70-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
08/28/15 20:10
75-09-2
08/28/15 20:10
1634-04-4
08/28/15 20:10
91-20-3
08/28/15 20:10
103-65-1
08/28/15 20:10
100-42-5
08/28/15 20:10
630-20-6
08/28/15 20.10
79-34-5
08/28/15 20:10
127-18-4
08/31 /15 11:50
108-88-3
08/28/15 20:10
87-61-6
08/28/15 20:10
120-82-1
08/28/15 20:10
71-55-6
08/28/15 20:10
79-00-5
08/28/15 20:10
79-01-6
08/28/15 20:10
75-69-4
08/28/15 20:10
96-18-4
08/28/15 20:10
95-63-6
08/28/15 20:10
108-67-8
08/28/15 20:10
75-01-4
08/28/15 20:10
179601-23-1
08/28/15 20:10
95-47-6
08/28/15 20:10 17060-07-0
08/28/15 20:10 460-00-4
08/28/15 20:10 2037-26-5
Qual
Page 9 of 22

17P`4ceAnalytical
www.pacelabs.com
rater-- ... yu -aai rasa,uw.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSERS
Pace Project No.: 92264544
Sample: EFFLUENT
Lab ID: 92264544002 Collected:
08/20/15 12:00 Received:
08/21/15 14:42 Matrix:
Water
Parameters
Results
Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-008)
71.3
ug/L
50.0
1
08/24/15 14:18
N2
Aliphatic (C09-C12)
54.7
ug/L
50.0
1
08/24/15 14:18
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
08/24/15 14:18
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
91
%
70-130
1
08/24/15 14:18
460-00-4
4-Bromofluorobenzene (PID) (S)
78
%
70-130
1
08/24/15 14:18
460-00-4
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
ND
ug/L
5.0
1 08/24/15 19:45 08/26/15 20:48
7439-92-1
6200E MSV
Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
08/28/15 17:41
71-43-2
Bromobenzene
ND
ug/L
0.50
1
08/28/15 17:41
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
08/28/15 17:41
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
08/28/1517,41
75-27-4
Bromoform
ND
ug/L
0.50
1
08/28/15 17:41
75-25-2
Bromomethane
ND
ug/L
5.0
1
08/28/15 17:41
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
08/28/15 17:41
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
08/28/15 17:41
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
08/28/15 17:41
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
08/28/15 17:41
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
08/28/15 17:41
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/28/1517A1
75-00-3
Chloroform
ND
ug/L
0.50
1
08/28/15 17:41
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/28/15 17:41
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
08/28/15 17:41
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
08/28/15 17:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
08/28/15 17:41
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
08/28/15 17:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
08/28/15 17:41
106-93-4
Dibromomethane
ND
ug/L
0.50
1
08/28/15 17:41
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
08/28/15 17:41
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
08/28/15 17:41
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
08/28/15 17:41
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
08/28/15 17:41
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
08/28/15 17:41
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
08/28/15 17:41
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
08/28/15 17:41
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
0.50
1
08/28/15 17:41
156-59-2
trans- l,2-Dichloroethene
ND
ug/L
0.50
1
08/28/15 17:41
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
08/28/15 17:41
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
08/28/15 17:41
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
08/28/15 17:41
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
08/28/15 17:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
08/28/15 17:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
08/28/15 17:41
10061-02-6
Date: 08/31/2015 04:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 22

171ace Analytical
www.pacelabs.com
race Anaryucai services, inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: WALSERS
Pace Project No.: 92264544
Sample: EFFLUENT Lab ID: 92264544002 Collected: 08/20/15 12:00 Received. 08/21/15 14:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
6200B MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-13romofluorobenzene (S)
Toluene-d8 (S)
Date: 08/31/2015 04:53 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
100 %
100 %
0.50
1
08/28/15 17:41
108-20-3
0.50
1
08/28/15 17:41
100-41-4
2.0
1
08/28/15 17 A 1
87-68-3
0.50
1
08/28/15 17:41
98-82-8
2.0
1
08/28/15 17:41
75-09-2
0.50
1
08/28/15 17:41
1634-04-4
2.0
1
08/28/15 17:41
91-20-3
0.50
1
08/28/15 17:41
103-65-1
0.50
1
08/28/15 17:41
100-42-5
0.50
1
08/28/15 17:41
630-20-6
0.50
1
08/28/15 17:41
79-34-5
0.50
1
08/28/15 17:41
127-18-4
0.50
1
08/28/15 17:41
108-88-3
2.0
1
08/28/15 17:41
87-61-6
2.0
1
08/28/15 17:41
120-82-1
0.50
1
08/28/15 17:41
71-55-6
0.50
1
08/28/15 17:41
79-00-5
0.50
1
08/28/15 17.41
79-01-6
1.0
1
08/28/15 17:41
75-69-4
0.50
1
08/28/15 17:41
96-18-4
0.50
1
08/28/15 17:41
95-63-6
0.50
1
08/28/15 17:41
108-67-8
1.0
1
08/28/15 17:41
75-01-4
1.0
1
08/28/15 17:41
179601-23-1
0.50
1
08/28/15 17:41
95-47-6
70-130
1
08/28/15 17:41
17060-07-0
70-130
1
08/28/15 17:41
460-00-4
70-130
1
08/28/15 17:41
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 22

171aceAnalyfical'
www.pacelabs.com
1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
QC Batch: GCV/9774 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92264544001, 92264544002
METHOD BLANK: 1539883 Matrix: Water
Associated Lab Samples: 92264544001, 92264544002
Parameter
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
Blank
Units
Result
ug/L
ND
ug/L
ND
ug/L
ND
%
89
%
76
Reporting
Limit Analyzed Qualifiers
50.0
08/24/1511:40 N2
50.0
08/24/1511:40 N2
50.0
08/24/1511:40 N2
70-130
08/24/1511:40
70-130
08/24/1511:40
LABORATORY CONTROL SAMPLE & LCSD:
1539884
1539885
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
297
258
99
86
70-130
14 25 N2
Aliphatic (C09-C12)
ug/L
300
341
352
114
117
30-130
3 25 N2
Aromatic (C09-C10)
ug/L
100
85.6
86.0
86
86
70-130
0 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
92
70-130
4-Bromofluorobe nzene (PID) (S)
%
84
80
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31/2015 04:53 PM without the written consent of Pace Analytical Services, Inc.
Page 12 of 22

laeAnalXical
( www.pacelabs.com
i
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
QC Batch: MPRP/19322 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92264544002
METHOD BLANK: 1540438
Associated Lab Samples: 92264544002
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1540439
Parameter Units
Lead ug/L
race Analytical aervlces, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/26/1519:48
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 467 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1540440 1540441
MS MSD
92264560001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 449 448 89 89 70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1540442 1540443
MS MSD
92264511001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 452 467 90 93 70-130 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 22

_ll�laceAnalytical
www.pacelabs.com
i
j
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
QC Batch: MSV/33167 Analysis Method: SM 62006
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92264544001, 92264544002
METHOD BLANK: 1544222
Associated Lab Samples: 92264544001, 92264544002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
08/28/15 17:24
1,1,1-Trichloroethane
ug/L
ND
0.50
08/28/15 17:24
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
08/28/15 17:24
1,1,2-Trichloroethane
ug/L
ND
0.50
08/28/15 17:24
1,1-Dichloroethane
ug/L
ND
0.50
08/28/15 17:24
1,1-Dichloroethene
ug/L
ND
0.50
08/28/15 17:24
1,1-Dichloropropene
ug/L
ND
0.50
08/28/15 17:24
1,2,3-Trichlorobenzene
ug/L
ND
2.0
08/28/15 17:24
1,2,3-Trichloropropane
ug/L
ND
0.50
08/28/15 17:24
1,2,4-Trichlorobenzene
ug/L
ND
2.0
08/28/15 17:24
1,2,4-Trimethylbenzene
ug/L
ND
0.50
08/28/15 17:24
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
08/28/15 17:24
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
08/28/15 17:24
1,2-Dichlorobenzene
ug/L
ND
0.50
08/28/15 17:24
1,2-Dichloroethane
ug/L
ND
0.50
08/28/15 17:24
1,2-Dichloropropane
ug/L
ND
0.50
08/28/15 17:24
1,3,5-Trimethylbenzene
ug/L
ND
0.50
08/28/15 17:24
1,3-Dichlorobenzene
ug/L
ND
0.50
08/28/15 17:24
1,3-Dichloropropane
ug/L
ND
0.50
08128/1517:24
1,4-Dichlorobenzene
ug/L
ND
0.50
08/28/15 17:24
2,2-Dichloropropane
ug/L
ND
0.50
08/28/15 17:24
2-Chlorotoluene
ug/L
ND
0.50
08/28/15 17:24
4-Chlorotoluene
ug/L
ND
0.50
08/28/15 17:24
Benzene
ug/L
ND
0.50
08/28/15 17:24
Bromobenzene
ug/L
ND
0.50
08/28/15 17:24
Bromochloromethane
ug/L
ND
0.50
08/28/15 17:24
Bromodichloromethane
ug/L
ND
0.50
08/28/15 17:24
Bromoform
ug/L
ND
0.50
08/28/15 17:24
Bromomethane
ug/L
ND
5.0
08/28/15 17:24
Carbon tetrachloride
ug/L
ND
0.50
08/28/15 17:24
Chlorobenzene
ug/L
ND
0.50
08/28/15 17:24
Chloroethane
ug/L
ND
1.0
08/28/15 17:24
Chloroform
ug/L
ND
0.50
08/28/15 17:24
Chloromethane
ug/L
ND
1.0
08/28/15 17:24
cis-1,2-Dichloroethene
ug/L
ND
0.50
08/28/15 17:24
cis-1,3-Dichloropropene
ug/L
ND
0.50
08/28/15 17:24
Dibromochloromethane
ug/L
ND
0.50
08/28/15 17:24
Dibromomethane
ug/L
ND
0.50
08/28/15 17:24
Dichlorodifluoromethane
ug/L
ND
0.50
08/28/15 17:24
Diisopropyl ether
ug/L
ND
0.50
08/28/15 17:24
Ethylbenzene
ug/L
ND
0.50
08/28/15 17:24
Qualifiers
race Analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 22

/�aceAna,(Xical
www.pacelabs.com
race Analytical aervices, MU.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
METHOD BLANK: 1544222
Associated Lab Samples: 92264544001, 92264544002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
08/28/15 17:24
Isopropylbenzene (Cumene)
ug/L
ND
0.50
08/28/15 17:24
m&p-Xylene
ug/L
ND
1.0
08/28/15 17:24
Methyl-tert-butyl ether
ug/L
ND
0.50
08/28/15 17:24
Methylene Chloride
ug/L
ND
2.0
08/28/15 17:24
n-Butylbenzene
ug/L
ND
0.50
08/28/15 17:24
n-Propylbenzene
ug/L
ND
0.50
08/28/15 17:24
Naphthalene
ug/L
ND
2.0
08/28/15 17:24
o-Xylene
ug/L
ND
0.50
08/28/15 17:24
sec-Butylbenzene
ug/L
ND
0.50
08/28/15 17:24
Styrene
ug/L
ND
0.50
08/28/15 17:24
tert-Butylbenzene
ug/L
ND
0.50
08/28/15 17:24
Tetrachloroethene
ug/L
ND
0.50
08/28/15 17:24
Toluene
ug/L
ND
0.50
08/28/15 17:24
trans-1,2-Dichloroethene
ug/L
ND
0.50
08128/1517:24
trans-1,3-Dichloropropene
ug/L
ND
0.50
08/28/15 17:24
Trichloroethene
ug/L
ND
0.50
08/28/15 17:24
Trichlorofluoromethane
ug/L
ND
1.0
08/28/15 17:24
Vinyl chloride
ug/L
ND
1.0
08/28/15 17:24
1,2-Dichloroethane-d4 (S)
%
103
70-130
08/28/15 17:24
4-Bromofluorobenzene (S)
%
98
70-130
08/28/15 17:24
Toluene-d8 (S)
%
99
70-130
08/28/15 17:24
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1544223
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.2
104
60-140
1, 1, 1 -Trichloroethane
ug/L
50
48.3
97
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
52.2
104
60-140
1,1,2-Trichloroethane
ug/L
50
49.4
99
60-140
1, 1 -Dichloroethane
ug/L
50
46.3
93
60-140
1,1-Dichloroethene
ug/L
50
48.3
97
60-140
1,1-Dichloropropene
ug/L
50
49.6
99
60-140
1,2,3-Trichlorobe nzene
ug/L
50
57.5
115
60-140
1,2,3-Trichloropropane
ug/L
50
48.9
98
60-140
1,2,4-Trichlorobenzene
ug/L
50
58.1
116
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.5
105
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
62.3
125
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.2
106
60-140
1,2-Dichlorobenzene
ug/L
50
53.6
107
60-140
1,2-Dichloroethane
ug/L
50
45.3
91
60-140
1,2-Dichloropropane
ug/L
50
47.8
96
60-140
1,3,5-Trimethylbenzene
ug/L
50
52.4
105
60-140
1,3-Dichlorobenzene
ug/L
50
52.8
106
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 22

eAnalytical
www.pacelabs.com
r
race Analytical services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
LABORATORY CONTROL SAMPLE:
Parameter
1544223
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
50.7
101
60-140
1,4-Dichlorobenzene
ug/L
50
51.1
102
60-140
2,2-Dichloropropane
ug/L
50
50.7
101
60-140
2-Chlorotoluene
ug/L
50
49.6
99
60-140
4-Chlorotoluene
ug/L
50
51.4
103
60-140
Benzene
ug/L
50
49.9
100
60-140
Bromobenzene
ug/L
50
50.7
101
60-140
Bromochloromethane
ug/L
50
51.5
103
60-140
Bromodichloromethane
ug/L
50
51.5
103
60-140
Bromoform
ug/L
50
55.1
110
60-140
Bromomethane
ug/L
50
55.8
112
60-140
Carbon tetrachloride
ug/L
50
50.9
102
60-140
Chlorobenzene
ug/L
50
49.6
99
60-140
Chloroethane
ug/L
50
44.2
88
60-140
Chloroform
ug/L
50
47.3
95
60-140
Chloromethane
ug/L
50
44.7
89
60-140
cis- 1,2-Dichloroethene
ug/L
50
48.0
96
60-140
cis-1,3-Dichloropropene
ug/L
50
51.1
102
60-140
Dibromochloromethane
ug/L
50
53.5
107
60-140
Dibromomethane
ug/L
50
51.1
102
60-140
Dichlorodifluoromethane
ug/L
50
41.0
82
60-140
Diisopropyl ether
ug/L
50
49.5
99
60-140
Ethylbenzene
ug/L
50
48.3
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
58.2
116
60-140
Isopropylbenzene (Cumene)
ug/L
50
54.0
108
60-140
m&p-Xylene
ug/L
100
99.0
99
60-140
Methyl-tert-butyl ether
ug/L
50
49.0
98
60-140
Methylene Chloride
ug/L
50
49.7
99
60-140
n-Butylbenzene
ug/L
50
53.7
107
60-140
n-Propylbenzene
ug/L
50
50.0
100
60-140
Naphthalene
ug/L
50
61.6
123
60-140
o-Xylene
ug/L
50
50.5
101
60-140
sec-Butylbenzene
ug/L
50
53.6
107
60-140
Styrene
ug/L
50
53.0
106
60-140
tert-Butylbenzene
ug/L
50
44.5
89
60-140
Tetrachloroethene
ug/L
50
48.8
98
60-140
Toluene
ug/L
50
47.9
96
60-140
trans-1,2-Dichloroethene
ug/L
50
49.9
100
60-140
trans-1,3-Dichloropropene
ug/L
50
52.2
104
60-140
Trichloroethene
ug/L
50
45.9
92
60-140
Trichlorofluoromethane
ug/L
50
42.3
85
60-140
Vinyl chloride
ug/L
50
43.8
88
60-140
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene(S)
%
102
70-130
Toluene-d8(S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 22

OD
/ aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1544224
1544225
MS
MSD
92264544002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.6
21.5
108
108
60-140
0
1,1,1-Trichloroethane
ug/L
ND
20
20
23.1
22.8
115
114
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.6
22.4
118
112
60-140
5
1,1,2-Trichloroethane
ug/L
ND
20
20
21.9
20.2
110
101
60-140
8
1, 1 -Dichloroethane
ug/L
ND
20
20
22.4
21.6
112
108
60-140
4
1,1-Dichloroethene
ug/L
ND
20
20
24.2
23.4
121
117
60-140
3
1,1-Dichloropropene
ug/L
ND
20
20
24.6
23.3
123
116
60-140
6
1,2,3-Trichlorobe nzene
ug/L
ND
20
20
24.1
22.0
121
110
60-140
9
1,2,3-Trichloropropane
ug/L
ND
20
20
21.1
19.4
106
97
60-140
9
1,2,4-Trichlorobe nzene
ug/L
ND
20
20
23.6
23.1
118
115
60-140
2
1,2,4-Trimethylbenzene
ug/L
ND
20
20
23.1
22.6
115
113
60-140
2
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
23.1
21.4
115
107
60-140
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.2
21.8
116
109
60-140
6
1,2-Dichlorobenzene
ug/L
ND
20
20
23.4
22.2
117
111
60-140
5
1,2-Dichloroethane
ug/L
ND
20
20
20.4
20.0
101
99
60-140
2
1,2-Dichloropropane
ug/L
ND
20
20
21.6
21.1
108
105
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
24.0
22.9
120
115
60-140
4
1,3-Dichlorobenzene
ug/L
ND
20
20
23.4
22.9
117
114
60-140
2
1,3-Dichloropropane
ug/L
ND
20
20
22.7
21.2
114
106
60-140
7
1,4-Dichlorobenzene
ug/L
ND
20
20
22.2
21.7
110
108
60-140
2
2,2-Dichloropropane
ug/L
ND
20
20
21.3
21.0
107
105
60-140
1
2-Chlorotoluene
ug/L
ND
20
20
23.0
21.8
115
109
60-140
5
4-Chlorotoluene
ug/L
ND
20
20
23.2
22.4
116
112
60-140
4
Benzene
ug/L
ND
20
20
23.8
22.9
118
113
60-140
4
Bromobenzene
ug/L
ND
20
20
22.3
21.3
112
107
60-140
5
Bromochloromethane
ug/L
ND
20
20
23.5
22.7
117
114
60-140
3
Bromodichloromethane
ug/L
ND
20
20
22.1
21.8
110
109
60-140
1
Bromoform
ug/L
ND
20
20
19.8
19.1
99
95
60-140
4
Bromomethane
ug/L
ND
20
20
16.4
18.6
82
93
60-140
13
Carbon tetrachloride
ug/L
ND
20
20
24.0
23.4
120
117
60-140
2
Chlorobenzene
ug/L
ND
20
20
22.7
21.7
113
108
60-140
5
Chloroethane
ug/L
ND
20
20
22.4
22.4
112
112
60-140
0
Chloroform
ug/L
ND
20
20
22.5
21.5
112
107
60-140
4
Chloromethane
ug/L
ND
20
20
18.8
19.4
94
97
60-140
3
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.6
22.0
113
110
60-140
3
cis- 1,3-Dichloropropene
ug/L
ND
20
20
21.0
20.5
105
102
60-140
2
Dibromochloromethane
ug/L
ND
20
20
20.2
19.9
101
99
60-140
2
Dibromomethane
ug/L
ND
20
20
21.8
22.1
109
111
60-140
2
Dichlorodifluoromethane
ug/L
ND
20
20
21.4
20.6
107
103
60-140
4
Diisopropyl ether
ug/L
ND
20
20
22.5
21.8
112
109
60-140
3
Ethylbenzene
ug/L
ND
20
20
22.3
21.8
112
109
60-140
2
Hexachloro-1,3-butadiene
ug/L
ND
20
20
28.0
25.8
140
129
60-140
8
Isopropylbenzene (Cumene)
ug/L
ND
20
20
24.9
23.6
125
118
60-140
5
m&p-Xylene
ug/L
ND
40
40
45.7
43.8
114
110
60-140
4
Methyl-tert-butyl ether
ug/L
ND
20
20
21.4
20.9
107
104
60-140
2
Methylene Chloride
ug/L
ND
20
20
22.3
21.1
111
105
60-140
6
Results presented on this page are in the units indicated by the
"Units" column except where an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31/2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 22

�-IaceAnalX cal
www.pacelabs.com
race Hnaryucai services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSERS
Pace Project No.: 92264544
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1544224
MS
92264544002
Spike
Parameter
Units
Result
Cone.
n-Butylbenzene
ug/L
ND
20
n-Propylbenzene
ug/L
ND
20
Naphthalene
ug/L
ND
20
o-Xylene
ug/L
ND
20
sec-Butylbenzene
ug/L
ND
20
Styrene
ug/L
ND
20
tert-Butylbenzene
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
Toluene
ug/L
ND
20
trans- 1,2-Dichloroethene
ug/L
ND
20
trans- 1,3-Dichloropropene
ug/L
ND
20
Trichloroethene
ug/L
ND
20
Trichlorofluoromethane
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
MSD
Spike
Cone.
1544225
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
20
23.3
22.6
116
113
60-140
3
20
23.3
22.3
116
111
60-140
4
20
24.4
22.6
122
113
60-140
8
20
23.2
22.1
116
110
60-140
5
20
24.6
23.4
123
117
60-140
5
20
23.8
23.0
119
115
60-140
3
20
20.0
19.5
100
97
60-140
3
20
22.7
21.6
114
108
60-140
5
20
22.6
21.7
113
109
60-140
4
20
24.2
23.4
121
117
60-140
3
20
20.8
20.1
104
100
60-140
4
20
22.0
21.0
110
105
60-140
5
20
21.9
21.3
110
107
60-140
3
20
22.0
22.4
110
112
60-140
2
97
97
70-130
99
102
70-130
100
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 18 of 22

117FalceAnalytical"
� www.pacefabs.com
race r+naryucai aeivices, lilt..
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: WALSERS
Pace Project No.: 92264544
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 22

1"71ace Analytical
www.pacelabs.com
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
race Anaryucat services, inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
WALSERS
92264544
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92264544001
INFLUENT
MADEP VPH
GCV/9774
92264544002
EFFLUENT
MADEP VPH
GCV/9774
92264544002
EFFLUENT
EPA 200.7
MPRP/19322 EPA 200.7 ICP/17370
92264544001
INFLUENT
SM 6200B
MSV/33167
92264544002
EFFLUENT
SM 6200B
MSV/33167
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/31 /2015 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 22

.�� Sample Condition Upon Receipt SCUR Page 1 of 2*
I'meAnalylical
Document Number: Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersviile Quality Office
Client Name. S � % e I (� • Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client[--]�no
Co ercial❑ ace Other
Custody Seal on Cooler/Box Present: ❑ yes Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble V❑ip \ ubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun 140 Type of Ice: et Blue None Samples on ice, cooling process has begun
Tamn Cnrrnrtinn Factor 01 No Correction
G
p•�
Corrected Cooler Tem (/ tom- C
Biological Tissue is Frozen: Yes N
N/A
Date and Initials of person examining
contents:
Temp should be above frei-zing to 6°C
Comments:
Chain of Custody Present:
s No
❑NIA
1.
Chain of Custody Filled Out:
es P No
❑N/A
2.
Chain of Custody Relinquished:
es PKo
ON/A
3.
Sampler Name & Signature on COC:
es ON
❑NIA
4.
Samples Arrived within Hold Time:
DY/es ONo
t IA
5.
Short Hold Time Analysis <72hr :
❑Yes o
6.
Rush Turn Around Time Requested:
❑Yes o
❑N/A
7.
Sufficient Volume:
es No
ON/A
$•
Correct Containers Used:
Yes o
ON/A
9.
-Pace Containers Used:
es
N/A
Containers Intact:
21es ❑No
❑NIA
Filtered volume received for Dissolved tests
❑Yes
21<A
11,
Sample Labels match COC:
es ❑No
❑N/A
12. NU
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
s [—
C�AUA
13.
All containers needing preservation are found to be In
❑ es ❑No
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, W -DRO (water)
s ❑No
Samples checked for dechlorination:
❑Yes ❑No
14.
Headspace in VOA Vials >6mm :
OYes o
❑NIA
15.
Trip Blank Present:
Yes No
❑NIA
16. T�
/ n (� N
Trip Blank Custody Seals Present
Yes ONo
ON/A
Pace Trip Blank Lot # if purchased): ----
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time: g z� �~ `'
Comments/Resolution: ��r, n ('' :, k- -n r_WIC 0 j'n emit of - 1�t��-� i1Yr"iV
SCURF Review: Date:
SRF Review: AQ Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
Incorrect containers)
WO#:92264544
11111111111111111111111111
92264544
Page 21 of 22

�,rceayrrar CHAIN -OF -CUSTODY 7 Analytical Request Document
- The Chain -of Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
iection A Section a Section c
tequired Client Information: Required Project Information: Invoice information: P.,. 1 Of t
;ompany: Shield Engineering Report To: Flora D'Souza Aneniion: Flora D'Sotrza
Wdress: 4301 Taggart Creek Road Copy To: company Name: Shield Engineering
charlotte, NC 28208
Address 4301 Taggart Creek,Road. Charlotte,. N(
?mall To: fdsouza shieiden ineerin .com
Purchase Order No. 1990018-55
Pate tie Reference:
UST - Underground Storage Tank
'hone: 04 394-6913 Fax
Client Project I0: WALSERS
Pace Project Manager. Herring.Kevin
Zequested Due Date/TAT: 10 Da Default
Container Order Number. 67359
Pace Profile V. ;ry
North Carolina
a.
f
�fk r•�rru.r
esf"
MATWX cone
,°�
.COLLECTED
z
Preservatives
.
Domar9 W.t. DW
��.,
$
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O
Vi" vrr
W.A. WNr WW
SAMPLE ID S bd o
K
START
ENDCA
'
.
One Character per hox. Wb. wD
(A,7- 0-91, -) Air AR
mar OT
z
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Sample Ids must tw unique m— Ts
X
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mZ
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=
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'
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pp>.
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DATE
TIME
DATE
TIME •
+'
x
x
X.
Z
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2
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Influent
V✓ T
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PRINT Name of SAMPLER
$
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SIGNATURE of SAMPLER (
DAT�Signod;
�'
$
f t / i�
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P2CBM2lyt f
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page : 1 Of
Company Shield Engineering Report To: James Gamertsfelder Attention: James Gamertsfelder
Address. 4301 Taggart Creek Road Copy To Company N amei Shield Engineering
Charlotte, NC 28208
.
Address: 4301 Taggart Creek Road, Charlotte, N
Regulatory Agency
Email To [e-mail]
Purchase Order No. 1001288
Pace Quote Reference:
UST - Underground Storage Tank
Phone [phone] IFax
Client Project ID. Sandy Plains SVE
Pace Project Manager: Brainard, Matthew
State / Location
Requested Due DaterTAT 10 Da Default
Container Order Number
Pace Profiles!:
North Carolina
Requested
Analysis
Filtered
Y/N
d
a
Z
°
o
COLLECTED
Preservatives
>
MATRIX CODE
U
Z
Drinking Water DW
a
Water WT
m
U
Waste Water vM
Product P
SAMPLE ID sowsood sr
ou
>
d
:^,
¢
�
START
END
m
N
►`-'
=
Z
}
c
on
One Character per box. WIPe WP
w
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Z
°
(A-Z. Other Or 9!, 1 Air AR
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w
F
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m
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Sample Ids must be unique Tissue rs
o
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m
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to
z
_=
O
N
t
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Q
m
F
Q
Q
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DATE
TIME
DATE
TIME
Q
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N
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U
=
t0
Z
N
Z
N
O
0
N
1
SVE
AR
G
8/28/2015
1100
1
1
X
2
3
4
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS ==RELINQUISHED
BY AFFILIATION
DATE
TIME
ACCEPTED BY! AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
c
1p
U
=_
o
v
d z
>
c
PRINT Name of SAMPLER:
Jeff Nicholson
M
w
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d m
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E Z
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SIGNATURE of SAMPLER:
DATE Signed:
� 2
U U
N }

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company Inc. - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Hiahwav 15ON
TYPE OF PERMITTED OPERATION BEING MONITORED
Lexinaton ` NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
_..
❑ Spray Field ® Remediation: GroUndWater
Contact Person: Flora D'Souza/Shield Enaineerina. Inc.
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 7/29/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: 4 in.
pH 5.71 units Temp. NM OC
DRY at
time of
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NM µMhos
sampling,
Measuring Point is _. NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling: NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 8/03/15 - 8/10/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead ND mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100mi
Phosphorus: Total as P
NA mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I n
Al - Aluminum
NA mg/I
Aliphatic (C05-CO8) = 0.076 mg/1
pH (when analyzed) NA units
�' Ba - Barium
NA mg/I
Aliphatic (C09-C12) = 0.0504 mg/1
TOC NA mg/ I o
C Ca -Calcium
NA mg/I
t
Chloride NA mg/I v �
w Cd - Cadmium
NA mg/I
Arsenic NA mg/I p 'Ili—
Chromium: Total
NA mg/I
Grease and Oils NA mg/I m z
r" Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I z
c.n Fe - Iron
NA mg/I (Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I c
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos :q
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MADFP VPH
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 18.1421 mg/L Effluent Total VOCs: 0.1264 mg/L VOC Removal% 99-3%
Flora D'Souza/Shield Enoineerina. Proiect Manaaer
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007

APPENDIX A

` �IaceAnalytical
I wwwpacelabs.com
I
I
August 10, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Dear Ms. D'Souza:
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 30, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page t of 29

/71aceAnalytical
/ wwwpacelabs com
1
I
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 29

��aceAnalXkal
wwwpacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92261208001 INFLUENT MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
92261208002 EFFLUENT MADEP VPH
BFW
5
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 3 of 29

Pace Analytical Services, Inc.
®
laceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpacelabs.com
1
[phone]
SUMMARY OF DETECTION
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92261208001
INFLUENT
MADEP VPH
Aliphatic (C05-CO8)
4370
ug/L
1250
08/10/15 14:34 N2
MADEP VPH
Aliphatic (C09-C12)
8560
ug/L
1250
08/10/15 14:34 N2
SM 6200B
Benzene
41.3
ug/L
2.5
08/05/15 06:53
SM 6200B
1,2-Dibromoethane (EDB)
9.6
ug/L
2.5
08/05/15 06:53
SM 6200B
Ethylbenzene
312
ug/L
2.5
08/05/15 06:53
SM 6200B
Isopropylbenzene (Cumene)
20.2
ug/L
2.5
08/05/15 06:53
SM 6200B
Naphthalene
263
ug/L
10.0
08/05/15 06:53
SM 6200B
n-Propylbenzene
43.0
ug/L
2.5
08/05/15 06:53
SM 6200B
Toluene
1930
ug/L
10.0
08/05/15 19:49
SM 6200B
1,2,4-Trimethylbenzene
410
ug/L
2.5
08/05/15 06:53
SM 6200B
1,3,5-Trimethylbenzene
129
ug/L
2.5
08/05/15 06:53
SM 6200B
m&p-Xylene
1320
ug/L
5.0
08/05/15 06:53
SM 6200B
o-Xylene
734
ug/L
2.5
08/05/15 06:53
92261208002
EFFLUENT
MADEP VPH
Aliphatic (C05-CO8)
76.0
ug/L
50.0
08/04/15 19:14 N2
MADEP VPH
Aliphatic (C09-C12)
50.4
ug/L
50.0
08/04/15 19:14 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Page 4 of 29

aceAnalXical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: August 10, 2015
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9701
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1525407)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
- Aromatic (C09-C10)
• EFFLUENT (Lab ID: 92261208002)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCS (Lab ID: 1525408)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc . Page 5 of 29

Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
�IaceA1a��!^�' Huntersville, NC 28078
www.pacelabs.com [phone]
i
PROJECT NARRATIVE
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: August 10, 2015
Analyte Comments:
QC Batch: GCV/9701
N2: The lab does not hold TNI accreditation for this parameter.
• LCS (Lab ID: 1525408)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1525409)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
QC Batch: GCV/9719
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1529723)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• INFLUENT (Lab ID: 92261208001)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCS (Lab ID: 1529724)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1529725)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 29

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I
PROJECT NARRATIVE
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: August 10, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 29

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I
I
PROJECT NARRATIVE
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: August 10, 2015
Pace Analytical liervlceS, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/32803
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92261155008
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1523369)
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1523370)
• Hexachloro-1,3-butadiene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 29

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Sample: INFLUENT Lab ID: 92261208001 Collected: 07/29/15 11:00 Received: 07/30/15 13:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromod ich loromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1 -Dichloroethane
1,2-Dichloroethane
1, 1 -Dichloroethene
cis- 1,2-Dichloroethene
trans-1,2-Dich loroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 08/10/2015 04:07 PM
Analytical Method: MADEP VPH
4370
ug/L
8560
ug/L
ND
ug/L
103
%
94
%
Analytical Method:
SM 6200B
41.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
9.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
312
ug/L
ND
ug/L
20.2
ug/L
1250
25
08/10/1514:34
1250
25
08/10/1514:34
1250
25
08/10/1514:34
70-130
25
08/10/1514:34
460-00-4
70-130
25
08/10/1514:34
460-00-4
2.5
5
08/05/15 06:53
71-43-2
2.5
5
08/05/15 06:53
108-86-1
2.5
5
08/05/15 06:53
74-97-5
2.5
5
08/05/15 06:53
75-27-4
2.5
5
08/05/15 06:53
75-25-2
25.0
5
08/05/15 06:53
74-83-9
2.5
5
08/05/15 06:53
104-51-8
2.5
5
08/05/15 06:53
135-98-8
2.5
5
08/05/15 06:53
98-06-6
2.5
5
08/05/15 06:53
56-23-5
2.5
5
08/05/15 06:53
108-90-7
5.0
5
08/05/15 06:53
75-00-3
2.5
5
08/05/15 06:53
67-66-3
5.0
5
08/05/15 06:53
74-87-3
2.5
5
08/05/15 06:53
95-49-8
2.5
5
08/05/15 06:53
106-43-4
5.0
5
08/05/15 06:53
96-12-8
2.5
5
08/05/15 06:53
124-48-1
2.5
5
08/05/15 06:53
106-93-4
2.5
5
08/05/15 06:53
74-95-3
2.5
5
08/05/15 06:53
95-50-1
2.5
5
08/05/15 06:53
541-73-1
2.5
5
08/05/15 06:53
106-46-7
2.5
5
08/05/15 06:53
75-71-8
2.5
5
08/05/15 06:53
75-34-3
2.5
5
08/05/15 06:53
107-06-2
2.5
5
08/05/15 06:53
75-35-4
2.5
5
08/05/15 06:53
156-59-2
2.5
5
08/05/15 06:53
156-60-5
2.5
5
08/05/15 06:53
78-87-5
2.5
5
08/05/15 06:53
142-28-9
2.5
5
08/05/15 06:53
594-20-7
2.5
5
08/05/15 06:53
563-58-6
2.5
5
08/05/15 06:53
10061-01-5
2.5
5
08/05/15 06:53
10061-02-6
2.5
5
08/05/15 06:53
108-20-3
2.5
5
08/05/15 06:53
100-41-4
10.0
5
08/05/15 06:53
87-68-3
2.5
5
08/05/15 06:53
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
N2
N2
N2
Page 9 of 29

/�IaceAnalytical
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I
1
ANALYTICAL RESULTS
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: INFLUENT Lab ID: 92261208001 Collected: 07/29/15 11:00 Received: 07/30/15 13:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
6200B MSV
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobe nzene
1,2,4-Trichlorobenzene
1, 1,1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/10/2015 04:07 PM
Analytical Method: SM 6200B
ND ug/L
ND ug/L
263 ug/L
43.0 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
1930 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
410 ug/L
129 ug/L
ND ug/L
1320 ug/L
734 ug/L
89 %
101 %
97 %
10.0
5
08/05/15 06:53
75-09-2
2.5
5
08/05/15 06:53
1634-04-4
10.0
5
08/05/15 06:53
91-20-3
2.5
5
08/05/15 06:53
103-65-1
2.5
5
08/05/15 06:53
100-42-5
2.5
5
08/05/15 06:53
630-20-6
2.5
5
08/05/15 06:53
79-34-5
2.5
5
08/05/15 06:53
127-18-4
10.0
20
08/05/1519:49
108-88-3
10.0
5
08/05/15 06:53
87-61-6
10.0
5
08/05/15 06:53
120-82-1
2.5
5
08/05/15 06:53
71-55-6
2.5
5
08/05/15 06:53
79-00-5
2.5
5
08/05/15 06:53
79-01-6
5.0
5
08/05/15 06:53
75-69-4
2.5
5
08/05/15 06:53
96-18-4
2.5
5
08/05/15 06:53
95-63-6
2.5
5
08/05/15 06:53
108-67-8
5.0
5
08/05/15 06:53
75-01-4
5.0
5
08/05/15 06:53
179601-23-1
2.5
5
08/05/15 06:53
95-47-6
70-130 5
70-130 5
70-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .
08/05/15 06:53 17060-07-0
08/05/15 06:53 460-00-4
08/05/15 06:53 2037-26-5
Page 10 of 29

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I
ANALYTICAL RESULTS
race Anaryucai cervices, in(;.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Sample: EFFLUENT Lab ID: 92261208002 Collected: 07/29/15 10:00 Received: 07/30/15 13:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
200.7 MET ICP
Lead
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1 -Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis- 1,2-Dichloroethene
trans- 1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Date: 08/10/2015 04:07 PM
Analytical Method: MADEP VPH
76.0
ug/L
50.0
1
08/04/1519:14
N2
50.4
ug/L
50.0
1
08/04/1519:14
N2
ND
ug/L
50.0
1
08/04/1519:14
N2
99
%
70-130
1
08/04/1519:14
460-00-4
98
%
70-130
1
08/04/1519:14
460-00-4
Analytical Method:
EPA 200.7 Preparation Method:
EPA 200.7
ND
ug/L
5.0
1 07/31/1518:00
08/03/1515:09
7439-92-1
Analytical Method:
SM 6200B
ND
ug/L
0.50
1
08/05/1514:34
71-43-2
ND
ug/L
0.50
1
08/05/1514:34
108-86-1
ND
ug/L
0.50
1
08/05/1514:34
74-97-5
ND
ug/L
0.50
1
08/05/1514:34
75-27-4
ND
ug/L
0.50
1
08/05/1514:34
75-25-2
ND
ug/L
5.0
1
08/05/1514:34
74-83-9
ND
ug/L
0.50
1
08/0511514:34
104-51-8
ND
ug/L
0.50
1
08/0511514:34
135-98-8
ND
ug/L
0.50
1
08/05/1514:34
98-06-6
ND
ug/L
0.50
1
08/0511514:34
56-23-5
ND
ug/L
0.50
1
08/05/1514:34
108-90-7
ND
ug/L
1.0
1
08/05/1514:34
75-00-3
ND
ug/L
0.50
1
08/05/1514:34
67-66-3
ND
ug/L
1.0
1
08/05/1514:34
74-87-3
ND
ug/L
0.50
1
08105/1514:34
95-49-8
ND
ug/L
0.50
1
08/05/1514:34
106-43-4
ND
ug/L
1.0
1
08/05/1514:34
96-12-8
ND
ug/L
0.50
1
08/05/1514:34
124-48-1
ND
ug/L
0.50
1
08/05/1514:34
106-93-4
ND
ug/L
0.50
1
08/05/1514:34
74-95-3
ND
ug/L
0.50
1
08/05/1514:34
95-50-1
ND
ug/L
0.50
1
08/05/1514:34
541-73-1
ND
ug/L
0.50
1
08/05/1514:34
106-46-7
ND
ug/L
0.50
1
08/05/1514:34
75-71-8
ND
ug/L
0.50
1
08/05/1514:34
75-34-3
ND
ug/L
0.50
1
08/05/1514:34
107-06-2
ND
ug/L
0.50
1
08/0511514:34
75-35-4
ND
ug/L
0.50
1
08/05/1514:34
156-59-2
ND
ug/L
0.50
1
08/05/1514:34
156-60-5
ND
ug/L
0.50
1
08/05/1514:34
78-87-5
ND
ug/L
0.50
1
08/05/1514:34
142-28-9
ND
ug/L
0.50
1
08/05/1514:34
594-20-7
ND
ug/L
0.50
1
08/05/1514:34
563-58-6
ND
ug/L
0.50
1
08/05/1514:34
10061-01-5
ND
ug/L
0.50
1
08/05/1514.34
10061-02-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 29

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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Sample: EFFLUENT Lab ID: 92261208002 Collected: 07/29/15 10:00 Received: 07/30/15 13:03 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
6200B MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trich loroetha ne
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/10/2015 04:07 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
101 %
99 %
100 %
0.50
1
08/05/15 14:34
108-20-3
0.50
1
08/05/15 14:34
100-41-4
2.0
1
08/05/15 14:34
87-68-3
0.50
1
08/05/15 14:34
98-82-8
2.0
1
08105/1514:34
75-09-2
0.50
1
08/05/15 14:34
1634-04-4
2.0
1
08/05/15 14:34
91-20-3
0.50
1
08/05/15 14:34
103-65-1
0.50
1
08/05/15 14:34
100-42-5
0.50
1
08/05/15 14:34
630-20-6
0.50
1
08/05/15 14:34
79-34-5
0.50
1
08/05/15 14:34
127-18-4
0.50
1
08/05/15 14:34
108-88-3
2.0
1
08/05/15 14:34
87-61-6
2.0
1
08/05/15 14:34
120-82-1
0.50
1
08/05/15 14:34
71-55-6
0.50
1
08/05/15 14:34
79-00-5
0.50
1
08/05/15 14:34
79-01-6
1.0
1
08/05/15 14:34
75-69-4
0.50
1
08/05/15 14:34
96-18-4
0.50
1
08/05/15 14:34
95-63-6
0.50
1
08/05/15 14:34
108-67-8
1.0
1
08/05/15 14:34
75-01-4
1.0
1
08/05/15 14:34
179601-23-1
0.50
1
08/05/15 14:34
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
08/05/15 14:34 17060-07-0
08/05/15 14:34 460-00-4
08/05/15 14:34 2037-26-5
Page 12 of 29

Pace Analytical Services, Inc.
®
aceAnalytical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QC Batch: GCV/9701
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH NC Water
Associated Lab Samples: 92261208002
METHOD BLANK: 1525407
Matrix: Water
Associated Lab Samples: 92261208002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aliphatic (C05-008)
ug/L
ND 50.0
08/04/15 17:29
N2
Aliphatic (C09-C12)
ug/L
ND 50.0
08/04/15 17:29
N2
Aromatic (C09-C10)
ug/L
ND 50.0
08/04/15 17:29
N2
4-Bromofluorobenzene (FID) (S)
%
103 70-130
08/04/15 17:29
4-Bromofluorobenzene (PID) (S)
%
99 70-130
08/04/15 17:29
LABORATORY CONTROL SAMPLE & LCSD:
1525408
1525409
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300 313 306
104 102
70-130
2 25 N2
Aliphatic (C09-C12)
ug/L
300 276 290
92 97
30-130
5 25 N2
Aromatic (C09-C10)
ug/L
100 94.4 96.9
94 97
70-130
3 25 N2
4-Bromofluorobenzene (FID) (S)
%
106 108
70-130
4-Bromofluorobenzene (PID) (S)
%
110 111
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 29

Pace Analytical Services, Inc
/ ®
aceAnalXical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpacelabs.com
1
i
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QC Batch: GCV/9719
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH
NC Water
Associated Lab Samples: 92261208001
METHOD BLANK: 1529723
Matrix: Water
Associated Lab Samples: 92261208001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aliphatic (C05-CO8)
ug/L
ND 50.0
08/10/15 14:07
N2
Aliphatic (C09-C12)
ug/L
ND 50.0
08/10/15 14:07
N2
Aromatic (C09-C10)
ug/L
ND 50.0
08/10/15 14:07
N2
4-Bromofluorobenzene (FID) (S)
%
96 70-130
08/10/15 14:07
4-Bromofluorobenzene (PID) (S)
%
88 70-130
08/10/15 14:07
LABORATORY CONTROL SAMPLE & LCSD:
1529724
1529725
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300 377 358
126 119
70-130
5 25 N2
Aliphatic (C09-C12)
ug/L
300 368 379
123 126
30-130
3 25 N2
Aromatic (C09-C10)
ug/L
100 98.3 99.2
98 99
70-130
1 25 N2
4-Bromofluorobe nzene (FID) (S)
%
104 96
70-130
4-Bromofluorobenzene (PID) (S)
%
100 92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 29

aceAnalytical
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i
i
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QC Batch: MPRP/19144
QC Batch Method: EPA 200.7
Associated Lab Samples: 92261208002
METHOD BLANK: 1523317
Associated Lab Samples: 92261208002
Parameter Units
Lead ug/L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/03/1513:49
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1523318
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 454 91 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1523319 1523320
MS MSD
92261010014 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 467 468 93 93 70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1523321 1523322
MS MSD
92260932001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Lead ug/L ND 500 500 467 462 93 92 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 29

aceAnalytical
/ wwwpacelabs.com
i
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QC Batch: MSV/32803 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92261208001
METHOD BLANK: 1523367
Associated Lab Samples: 92261208001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
08105/1501:19
1,1,1-Trichloroethane
ug/L
ND
0.50
08105/1501:19
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
08/05/15 01:19
1,1,2-Trichloroethane
ug/L
ND
0.50
08/05/15 01:19
1,1-Dichloroethane
ug/L
ND
0.50
08/05/15 01:19
1,1-Dichloroethene
ug/L
ND
0.50
08/05/15 01:19
1,1-Dichloropropene
ug/L
ND
0.50
08/05/15 01:19
1,2,3-Trichlorobenzene
ug/L
ND
2.0
08/05/15 01:19
1,2,3-Trichloropropane
ug/L
ND
0.50
08/05/15 01:19
1,2,4-Trichlorobe nzene
ug/L
ND
2.0
08/05/15 01:19
1,2,4-Trimethylbenzene
ug/L
ND
0.50
08/05/15 01:19
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
08/05/15 01:19
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
08/05/15 01:19
1,2-Dichlorobenzene
ug/L
ND
0.50
08/05/15 01:19
1,2-Dichloroethane
ug/L
ND
0.50
08/05/15 01:19
1,2-Dichloropropane
ug/L
ND
0.50
08/05/15 01:19
1,3,5-Trimethylbenzene
ug/L
ND
0.50
08/05/15 01:19
1,3-Dichlorobenzene
ug/L
ND
0.50
08/05/15 01:19
1,3-Dichloropropane
ug/L
ND
0.50
08/05/15 01:19
1,4-Dichlorobenzene
ug/L
ND
0.50
08/05/15 01:19
2,2-Dichloropropane
ug/L
ND
0.50
08/05/15 01:19
2-Chlorotoluene
ug/L
ND
0.50
08/05/15 01:19
4-Chlorotoluene
ug/L
ND
0.50
08/05/15 01:19
Benzene
ug/L
ND
0.50
08/05/15 01:19
Bromobenzene
ug/L
ND
0.50
08/05/15 01:19
Bromochloromethane
ug/L
ND
0.50
08/05/15 01:19
Bromodichloromethane
ug/L
ND
0.50
08/05/15 01:19
Bromoform
ug/L
ND
0.50
08/05/15 01:19
Bromomethane
ug/L
ND
5.0
08/05/15 01:19
Carbon tetrachloride
ug/L
ND
0.50
08/05/15 01:19
Chlorobenzene
ug/L
ND
0.50
08/05/15 01:19
Chloroethane
ug/L
ND
1.0
08/05/15 01:19
Chloroform
ug/L
ND
0.50
08/05/15 01:19
Chloromethane
ug/L
ND
1.0
08/05/15 01:19
cis-1,2-Dichloroethene
ug/L
ND
0.50
08/05/15 01:19
cis-1,3-Dichloropropene
ug/L
ND
0.50
08/05/15 01:19
Dibromochloromethane
ug/L
ND
0.50
08/05/15 01:19
Dibromomethane
ug/L
ND
0.50
08/05/15 01:19
Dichlorodifluoromethane
ug/L
ND
0.50
08/05/15 01:19
Diisopropyl ether
ug/L
ND
0.50
08/05/15 01:19
Ethylbenzene
ug/L
ND
0.50
08/05/15 01:19
Qualifiers
Pace Analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 29

1�laceA.nalXical
pacelabs.com
i
i
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
METHOD BLANK: 1523367
Associated Lab Samples: 92261208001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Hexachloro-1,3-butadiene
ug/L
ND
2.0
Isopropylbenzene (Cumene)
ug/L
ND
0.50
m&p-Xylene
ug/L
ND
1.0
Methyl-tert-butyl ether
ug/L
ND
0.50
Methylene Chloride
ug/L
ND
2.0
n-Butylbenzene
ug/L
ND
0.50
n-Propylbenzene
ug/L
ND
0.50
Naphthalene
ug/L
ND
2.0
o-Xylene
ug/L
ND
0.50
sec-Butylbenzene
ug/L
ND
0.50
Styrene
ug/L
ND
0.50
tent-Butylbenzene
ug/L
ND
0.50
Tetrachloroethene
ug/L
ND
0.50
Toluene
ug/L
ND
0.50
trans-1,2-Dichloroethene
ug/L
ND
0.50
trans-1,3-Dichloropropene
ug/L
ND
0.50
Trichloroethene
ug/L
ND
0.50
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl chloride
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
Analyzed
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
08/05/15 01:19
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1523368
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
60-140
1,1,1-Trichloroethane
ug/L
50
51.5
103
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
49.6
99
60-140
1,1,2-Trichloroethane
ug/L
50
45.8
92
60-140
1,1-Dichloroethane
ug/L
50
47.5
95
60-140
1,1-Dichloroethene
ug/L
50
54.9
110
60-140
1, 1 -Dichloropropene
ug/L
50
53.0
106
60-140
1,2,3-Trichlorobenzene
ug/L
50
49.3
99
60-140
1,2,3-Trichloropropane
ug/L
50
50.0
100
60-140
1,2,4-Trichlorobenzene
ug/L
50
48.2
96
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.5
105
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.5
107
60-140
1,2-Dibromoethane (EDB)
ug/L
50
52.5
105
60-140
1,2-Dichlorobenzene
ug/L
50
51.3
103
60-140
1,2-Dichloroethane
ug/L
50
40.1
80
60-140
1,2-Dichloropropane
ug/L
50
49.3
99
60-140
1,3,5-Trimethylbenzene
ug/L
50
53.1
106
60-140
1,3-Dichlorobenzene
ug/L
50
51.6
103
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 29

/�IaceAnalXical
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i
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
LABORATORY CONTROL SAMPLE:
1523368
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,3-Dichloropropane
ug/L
50
49.8
100
60-140
1,4-Dichlorobenzene
ug/L
50
48.9
98
60-140
2,2-Dichloropropane
ug/L
50
41.9
84
60-140
2-Chlorotoluene
ug/L
50
51.8
104
60-140
4-Chlorotoluene
ug/L
50
51.4
103
60-140
Benzene
ug/L
50
51.6
103
60-140
Bromobenzene
ug/L
50
49.5
99
60-140
Bromochloromethane
ug/L
50
48.0
96
60-140
Bromodichloromethane
ug/L
50
48.8
98
60-140
Bromoform
ug/L
50
46.6
93
60-140
Bromomethane
ug/L
50
49.4
99
60-140
Carbon tetrachloride
ug/L
50
57.8
116
60-140
Chlorobenzene
ug/L
50
50.7
101
60-140
Chloroethane
ug/L
50
44.3
89
60-140
Chloroform
ug/L
50
46.4
93
60-140
Chloromethane
ug/L
50
44.6
89
60-140
cis- 1,2-Dichloroethene
ug/L
50
47.8
96
60-140
cis- 1,3-Dichloropropene
ug/L
50
47.0
94
60-140
Dibromochloromethane
ug/L
50
48.5
97
60-140
Dibromomethane
ug/L
50
49.3
99
60-140
Dichlorodifluoromethane
ug/L
50
45.7
91
60-140
Diisopropyl ether
ug/L
50
45.2
90
60-140
Ethylbenzene
ug/L
50
51.8
104
60-140
Hexachloro-1,3-butadiene
ug/L
50
61.7
123
60-140
Isopropylbenzene (Cumene)
ug/L
50
58.3
117
60-140
m&p-Xylene
ug/L
100
104
104
60-140
Methyl-tert-butyl ether
ug/L
50
45.1
90
60-140
Methylene Chloride
ug/L
50
45.1
90
60-140
n-Butylbenzene
ug/L
50
54.5
109
60-140
n-Propylbenzene
ug/L
50
53.0
106
60-140
Naphthalene
ug/L
50
52.0
104
60-140
o-Xylene
ug/L
50
51.8
104
60-140
sec-Butylbenzene
ug/L
50
57.2
114
60-140
Styrene
ug/L
50
52.9
106
60-140
tert-Butylbenzene
ug/L
50
45.7
91
60-140
Tetrachloroethene
ug/L
50
52.7
105
60-140
Toluene
ug/L
50
49.5
99
60-140
trans-1,2-Dichloroethene
ug/L
50
49.2
98
60-140
trans- 1,3-Dichloropropene
ug/L
50
46.5
93
60-140
Trichloroethene
ug/L
50
49.6
99
60-140
Trichlorofluoromethane
ug/L
50
46.3
93
60-140
Vinyl chloride
ug/L
50
45.9
92
60-140
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene(S)
%
102
70-130
Toluene-d8 (S)
%
97
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 29

/,-IaceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1523369
1523370
MS
MSD
92261155008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
<0.50
20
20
21.4
21.5
107
107
60-140
0
1,1,1-Trichloroethane
ug/L
<0.50
20
20
22.6
22.6
113
113
60-140
0
1,1,2,2-Tetrachloroethane
ug/L
<0.50
20
20
21.2
21.6
106
108
60-140
2
1,1,2-Trichloroethane
ug/L
<0.50
20
20
20.7
19.9
103
100
60-140
4
1,1-Dichloroethane
ug/L
<0.50
20
20
21.0
20.7
105
104
60-140
1
1,1-Dichloroethene
ug/L
<0.50
20
20
25.0
25.0
125
125
60-140
0
1,1-Dichloropropene
ug/L
<0.50
20
20
24.4
23.8
122
119
60-140
2
1,2,3-Trichlorobenzene
ug/L
<2.0
20
20
20.5
21.8
103
109
60-140
6
1,2,3-Trichloropropane
ug/L
<0.50
20
20
22.0
22.2
110
111
60-140
1
1,2,4-Trichlorobe nzene
ug/L
<2.0
20
20
20.4
20.8
102
104
60-140
2
1,2,4-Trimethylbenzene
ug/L
<0.50
20
20
23.1
23.1
115
115
60-140
0
1,2-Dibromo-3-chloropropane
ug/L
<1.0
20
20
21.3
22.1
107
111
60-140
3
1,2-Dibromoethane (EDB)
ug/L
<0.50
20
20
22.7
22.3
113
112
60-140
2
1,2-Dichlorobenzene
ug/L
<0.50
20
20
22.2
22.2
111
111
60-140
0
1,2-Dichloroethane
ug/L
<0.50
20
20
17.4
17.5
87
87
60-140
0
1,2-Dichloropropane
ug/L
<0.50
20
20
21.1
21.3
106
106
60-140
1
1,3,5-Trimethylbenzene
ug/L
<0.50
20
20
23.4
23.7
117
118
60-140
1
1,3-Dichlorobenzene
ug/L
<0.50
20
20
22.3
22.5
111
113
60-140
1
1,3-Dichloropropane
ug/L
<0.50
20
20
21.6
21.1
108
105
60-140
2
1,4-Dichlorobenzene
ug/L
<0.50
20
20
21.8
21.5
109
107
60-140
1
2,2-Dichloropropane
ug/L
<0.50
20
20
17.0
16.5
85
83
60-140
3
2-Chlorotoluene
ug/L
<0.50
20
20
22.9
22.4
114
112
60-140
2
4-Chlorotoluene
ug/L
<0.50
20
20
22.8
22.6
114
113
60-140
1
Benzene
ug/L
<0.50
20
20
23.4
23.2
117
116
60-140
1
Bromobenzene
ug/L
<0.50
20
20
21.7
21.6
108
108
60-140
0
Bromochloromethane
ug/L
<0.50
20
20
21.4
20.6
107
103
60-140
4
Bromodichloromethane
ug/L
<0.50
20
20
20.8
20.5
104
102
60-140
2
Bromoform
ug/L
<0.50
20
20
18.1
18.0
90
90
60-140
0
Bromomethane
ug/L
<5.0
20
20
19.2
20.2
96
101
60-140
5
Carbon tetrachloride
ug/L
<0.50
20
20
25.2
25.1
126
126
60-140
0
Chlorobenzene
ug/L
<0.50
20
20
22.6
22.6
113
113
60-140
0
Chloroethane
ug/L
<1.0
20
20
21.2
20.4
106
102
60-140
4
Chloroform
ug/L
<0.50
20
20
20.7
20.8
103
104
60-140
1
Chloromethane
ug/L
<1.0
20
20
20.8
20.6
104
103
60-140
1
cis-1,2-Dichloroethene
ug/L
<0.50
20
20
21.1
20.8
105
104
60-140
1
cis- 1,3-Dichloropropene
ug/L
<0.50
20
20
19.6
19.1
98
96
60-140
2
Dibromochloromethane
ug/L
<0.50
20
20
19.5
19.9
98
99
60-140
2
Dibromomethane
ug/L
<0.50
20
20
21.6
21.3
108
106
60-140
1
Dichlorodifluoromethane
ug/L
<0.50
20
20
21.4
20.6
107
103
60-140
4
Diisopropyl ether
ug/L
<0.50
20
20
19.9
19.6
99
98
60-140
1
Ethylbenzene
ug/L
<0.50
20
20
22.9
22.9
115
114
60-140
0
Hexachloro-1,3-butadiene
ug/L
<2.0
20
20
28.8
28.2
144
141
60-140
2 M1
Isopropylbenzene (Cumene)
ug/L
<0.50
20
20
25.7
25.3
128
127
60-140
1
m&p-Xylene
ug/L
<1.0
40
40
45.9
45.1
115
113
60-140
2
Methyl-tert-butyl ether
ug/L
<0.50
20
20
19.4
19.4
97
97
60-140
0
Methylene Chloride
ug/L
<2.0
20
20
19.6
18.9
98
95
60-140
4
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 29

Analytical
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i
I
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1523369
1523370
MS
MSD
92261155008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
<0.50
20
20
23.7
23.9
119
120
60-140
1
n-Propylbenzene
ug/L
<0.50
20
20
23.8
23.8
119
119
60-140
0
Naphthalene
ug/L
<2.0
20
20
22.7
22.6
113
113
60-140
0
o-Xylene
ug/L
<0.50
20
20
22.5
22.5
113
113
60-140
0
sec-Butylbenzene
ug/L
<0.50
20
20
25.3
25.7
126
128
60-140
1
Styrene
ug/L
<0.50
20
20
22.2
22.4
111
112
60-140
1
tert-Butylbenzene
ug/L
<0.50
20
20
20.3
20.3
102
101
60-140
0
Tetrachloroethene
ug/L
<0.50
20
20
24.0
23.6
120
118
60-140
2
Toluene
ug/L
<0.50
20
20
22.7
21.8
114
109
60-140
4
trans-1,2-Dichloroethene
ug/L
<0.50
20
20
22.2
22.0
111
110
60-140
1
trans-1,3-Dichloropropene
ug/L
<0.50
20
20
19.2
18.9
96
94
60-140
2
Trichloroethene
ug/L
<0.50
20
20
22.7
22.4
113
112
60-140
1
Trichlorofluoromethane
ug/L
<1.0
20
20
21.7
21.6
108
108
60-140
0
Vinyl chloride
ug/L
<1.0
20
20
21.8
21.2
109
106
60-140
3
1,2-Dichloroethane-d4 (S)
%
89
89
70-130
4-Bromofluorobenzene(S)
%
100
101
70-130
Toluene-d8 (S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 29

ll�la eAnalytical
/ www.pacelabs.com
r
A
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QC Batch: MSV/32804 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92261208002
METHOD BLANK: 1523386
Associated Lab Samples: 92261208002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
08105/1514:17
1,1,1-Trichloroethane
ug/L
ND
0.50
08/05/15 14:17
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
08/05/15 14:17
1,1,2-Trichloroethane
ug/L
ND
0.50
08/05/15 14:17
1,1-Dichloroethane
ug/L
ND
0.50
08/05/15 14:17
1,1-Dichloroethene
ug/L
ND
0.50
08/0511514:17
1,1-Dichloropropene
ug/L
ND
0.50
08/05/15 14:17
1,2,3-Trichlorobe nzene
ug/L
ND
2.0
08/05/15 14:17
1,2,3-Trichloropropane
ug/L
ND
0.50
08/05/15 14:17
1,2,4-Trichlorobenzene
ug/L
ND
2.0
08/05/15 14:17
1,2,4-Trimethylbenzene
ug/L
ND
0.50
08/05/15 14:17
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
08/05/15 14:17
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
08/05/15 14:17
1,2-Dichlorobenzene
ug/L
ND
0.50
08/05/15 14:17
1,2-Dichloroethane
ug/L
ND
0.50
08/05/15 14:17
1,2-Dichloropropane
ug/L
ND
0.50
08/05/15 14:17
1,3,5-Trimethylbenzene
ug/L
ND
0.50
08/05/15 14:17
1,3-Dichlorobenzene
ug/L
ND
0.50
0810511514:17
1,3-Dichloropropane
ug/L
ND
0.50
08/05/15 14:17
1,4-Dichlorobenzene
ug/L
ND
0.50
08/05/15 14:17
2,2-Dichloropropane
ug/L
ND
0.50
08/05/15 14:17
2-Chlorotoluene
ug/L
ND
0.50
08/05/15 14:17
4-Chlorotoluene
ug/L
ND
0.50
08/05/15 14:17
Benzene
ug/L
ND
0.50
08/05/15 14:17
Bromobenzene
ug/L
ND
0.50
08/05/15 14:17
Bromochloromethane
ug/L
ND
0.50
08/05/15 14:17
Bromodichloromethane
ug/L
ND
0.50
08/05/15 14:17
Bromoform
ug/L
ND
0.50
08/05/15 14:17
Bromomethane
ug/L
ND
5.0
08/05/15 14:17
Carbon tetrachloride
ug/L
ND
0.50
08/05/15 14:17
Chlorobenzene
ug/L
ND
0.50
08/05/15 14:17
Chloroethane
ug/L
ND
1.0
08/05/15 14:17
Chloroform
ug/L
ND
0.50
08/05/15 14:17
Chloromethane
ug/L
ND
1.0
08/05/15 14:17
cis-1,2-Dichloroethene
ug/L
ND
0.50
08/05/15 14:17
cis- 1,3-Dichloropropene
ug/L
ND
0.50
08/05/15 14:17
Dibromochloromethane
ug/L
ND
0.50
08/05/15 14:17
Dibromomethane
ug/L
ND
0.50
08/05/15 14:17
Dichlorodifluoromethane
ug/L
ND
0.50
08/05/15 14:17
Diisopropyl ether
ug/L
ND
0.50
08/05/15 14:17
Ethylbenzene
ug/L
ND
0.50
08/05/15 14:17
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 29

1�7aceAnalXical
/ www.pacelabs.com
1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
METHOD BLANK: 1523386
Matrix:
Water
Associated Lab Samples: 92261208002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
08/05/15 14:17
Isopropylbenzene (Cumene)
ug/L
ND
0.50
08/05/15 14:17
m&p-Xylene
ug/L
ND
1.0
08/05/15 14:17
Methyl-tert-butyl ether
ug/L
ND
0.50
08/05/15 14:17
Methylene Chloride
ug/L
ND
2.0
08/05/15 14:17
n-Butylbenzene
ug/L
ND
0.50
08/05/15 14:17
n-Propylbenzene
ug/L
ND
0.50
08/05/15 14:17
Naphthalene
ug/L
ND
2.0
08/05/15 14:17
o-Xylene
ug/L
ND
0.50
08/05/15 14:17
sec-Butylbenzene
ug/L
ND
0.50
08/05/15 14:17
Styrene
ug/L
ND
0.50
08/05/15 14:17
tert-Butylbenzene
ug/L
ND
0.50
08/05/15 14:17
Tetrachloroethene
ug/L
ND
0.50
08/05/15 14:17
Toluene
ug/L
ND
0.50
08/05/15 14:17
trans- 1,2-Dichloroethene
ug/L
ND
0.50
08/05/15 14:17
trans-1,3-Dichloropropene
ug/L
ND
0.50
08/05/15 14:17
Trichloroethene
ug/L
ND
0.50
08/05/15 14:17
Trichlorofluoromethane
ug/L
ND
1.0
08105/1514:17
Vinyl chloride
ug/L
ND
1.0
08/05/15 14:17
1,2-Dichloroethane-d4 (S)
%
102
70-130
08/05/15 14:17
4-Bromofluorobenzene (S)
%
99
70-130
08/05/15 14:17
Toluene-d8 (S)
%
101
70-130
08/05/15 14:17
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1523387
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.4
109
60-140
1,1,1-Trichloroethane
ug/L
50
53.4
107
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.4
103
60-140
1,1,2-Trichloroethane
ug/L
50
50.8
102
60-140
1,1-Dichloroethane
ug/L
50
51.3
103
60-140
1,1-Dichloroethene
ug/L
50
55.1
110
60-140
1, 1 -Dichloropropene
ug/L
50
55.4
111
60-140
1,2,3-Trichlorobenzene
ug/L
50
56.1
112
60-140
1,2,3-Trichloropropane
ug/L
50
48.7
97
60-140
1,2,4-Trichlorobenzene
ug/L
50
54.0
108
60-140
1,2,4-Trimethylbenzene
ug/L
50
54.4
109
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
56.3
113
60-140
1,2-Dibromoethane (EDB)
ug/L
50
54.5
109
60-140
1,2-Dichlorobenzene
ug/L
50
53.0
106
60-140
1,2-Dichloroethane
ug/L
50
45.5
91
60-140
1,2-Dichloropropane
ug/L
50
51.0
102
60-140
1,3,5-Trimethylbenzene
ug/L
50
54.0
108
60-140
1,3-Dichlorobenzene
ug/L
50
53.1
106
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 29

'/7
aceAnalytical
www.pacelabs.com
I
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
LABORATORY CONTROL SAMPLE:
Parameter
1523387
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
52.0
104
60-140
1,4-Dichlorobenzene
ug/L
50
51.7
103
60-140
2,2-Dichloropropane
ug/L
50
52.1
104
60-140
2-Chlorotoluene
ug/L
50
54.0
108
60-140
4-Chlorotoluene
ug/L
50
53.5
107
60-140
Benzene
ug/L
50
52.8
106
60-140
Bromobenzene
ug/L
50
54.9
110
60-140
Bromochloromethane
ug/L
50
55.4
111
60-140
Bromodichloromethane
ug/L
50
53.7
107
60-140
Bromoform
ug/L
50
54.5
109
60-140
Bromomethane
ug/L
50
51.0
102
60-140
Carbon tetrachloride
ug/L
50
56.0
112
60-140
Chlorobenzene
ug/L
50
51.7
103
60-140
Chloroethane
ug/L
50
50.4
101
60-140
Chloroform
ug/L
50
53.7
107
60-140
Chloromethane
ug/L
50
50.1
100
60-140
cis- 1,2-Dichloroethene
ug/L
50
52.8
106
60-140
cis-1,3-Dichloropropene
ug/L
50
52.9
106
60-140
Dibromochloromethane
ug/L
50
55.7
111
60-140
Dibromomethane
ug/L
50
52.2
104
60-140
Dichlorodifluoromethane
ug/L
50
54.2
108
60-140
Diisopropyl ether
ug/L
50
52.4
105
60-140
Ethylbenzene
ug/L
50
51.3
103
60-140
Hexachloro-1,3-butadiene
ug/L
50
56.6
113
60-140
Isopropylbenzene (Cumene)
ug/L
50
58.5
117
60-140
m&p-Xylene
ug/L
100
105
105
60-140
Methyl-tert-butyl ether
ug/L
50
51.4
103
60-140
Methylene Chloride
ug/L
50
53.3
107
60-140
n-Butylbenzene
ug/L
50
56.0
112
60-140
n-Propylbenzene
ug/L
50
52.4
105
60-140
Naphthalene
ug/L
50
56.3
113
60-140
o-Xylene
ug/L
50
53.4
107
60-140
sec-Butylbenzene
ug/L
50
56.8
114
60-140
Styrene
ug/L
50
54.8
110
60-140
tert-Butylbenzene
ug/L
50
46.8
94
60-140
Tetrachloroethene
ug/L
50
51.5
103
60-140
Toluene
ug/L
50
51.2
102
60-140
trans- 1,2-Dichloroethene
ug/L
50
53.3
107
60-140
trans- 1,3-Dichloropropene
ug/L
50
53.6
107
60-140
Trichloroethene
ug/L
50
48.8
98
60-140
Trichlorofluoromethane
ug/L
50
53.0
106
60-140
Vinyl chloride
ug/L
50
53.4
107
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc. Page 23 of 29

laceAnalytical
ll�Huntersville,
www.pacelabs.com
l
i
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KineyAve. Suite 100
NC 28078078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1523388
1523389
MS
MSD
92261208002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.6
21.5
103
108
60-140
4
1,1,1-Trichloroethane
ug/L
ND
20
20
21.7
22.7
109
113
60-140
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.7
24.1
109
121
60-140
11
1,1,2-Trichloroethane
ug/L
ND
20
20
202
21.1
101
105
60-140
4
1,1-Dichloroethane
ug/L
ND
20
20
21.0
22.1
105
111
60-140
5
1,1-Dichloroethene
ug/L
ND
20
20
23.2
24.6
116
123
60-140
6
1,1-Dichloropropene
ug/L
ND
20
20
22.6
24.7
113
124
60-140
9
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.3
23.9
102
119
60-140
16
1,2,3-Trichloropropane
ug/L
ND
20
20
19.3
21.7
96
109
60-140
12
1,2,4-Trichlorobenzene
ug/L
ND
20
20
18.9
21.6
95
108
60-140
13
1,2,4-Trimethylbenzene
ug/L
ND
20
20
21.1
22.9
105
115
60-140
8
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.5
24.7
103
124
60-140
19
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.4
23.5
107
118
60-140
9
1,2-Dichlorobenzene
ug/L
ND
20
20
20.6
22.5
103
113
60-140
9
1,2-Dichloroethane
ug/L
ND
20
20
18.7
19.9
93
98
60-140
6
1,2-Dichloropropane
ug/L
ND
20
20
20.8
21.5
104
107
60-140
3
1,3,5-Trimethylbenzene
ug/L
ND
20
20
21.0
23.1
105
116
60-140
10
1,3-Dichlorobenzene
ug/L
ND
20
20
20.7
22.4
103
112
60-140
8
1,3-Dichloropropane
ug/L
ND
20
20
20.8
21.9
104
110
60-140
5
1,4-Dichlorobenzene
ug/L
ND
20
20
20.4
21.7
101
108
60-140
6
2,2-Dichloropropane
ug/L
ND
20
20
12.8
13.5
64
67
60-140
5
2-Chlorotoluene
ug/L
ND
20
20
21.5
23.1
107
116
60-140
7
4-Chlorotoluene
ug/L
ND
20
20
21.1
22.9
106
114
60-140
8
Benzene
ug/L
ND
20
20
21.9
23.1
110
115
60-140
5
Bromobenzene
ug/L
ND
20
20
21.7
23.4
108
117
60-140
8
Bromochloromethane
ug/L
ND
20
20
22.7
24.0
113
120
60-140
5
Bromodichloromethane
ug/L
ND
20
20
21.1
21.4
106
107
60-140
1
Bromoform
ug/L
ND
20
20
19.7
20.7
99
103
60-140
5
Bromomethane
ug/L
ND
20
20
13.3
14.0
67
70
60-140
5
Carbon tetrachloride
ug/L
ND
20
20
23.1
23.8
116
119
60-140
3
Chlorobenzene
ug/L
ND
20
20
20.6
21.8
103
109
60-140
6
Chloroethane
ug/L
ND
20
20
20.7
25.6
104
128
60-140
21
Chloroform
ug/L
ND
20
20
22.0
22.9
110
114
60-140
4
Chloromethane
ug/L
ND
20
20
19.0
18.8
95
94
60-140
1
cis- 1,2-Dichloroethene
ug/L
ND
20
20
21.7
22.7
108
113
60-140
4
cis-1,3-Dichloropropene
ug/L
ND
20
20
18.8
19.5
94
97
60-140
3
Dibromochloromethane
ug/L
ND
20
20
20.5
21.9
102
109
60-140
7
Dibromomethane
ug/L
ND
20
20
21.2
21.9
106
110
60-140
3
Dichlorodifluoromethane
ug/L
ND
20
20
23.7
25.5
119
128
60-140
7
Diisopropyl ether
ug/L
ND
20
20
21.3
22.0
107
110
60-140
3
Ethylbenzene
ug/L
ND
20
20
20.4
21.6
102
108
60-140
6
Hexachloro-1,3-butadiene
ug/L
ND
20
20
22.5
24.5
113
122
60-140
8
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.0
24.4
115
122
60-140
6
m&p-Xylene
ug/L
ND
40
40
41.2
43.9
103
109
60-140
6
Methyl-tert-butyl ether
ug/L
ND
20
20
20.7
21.6
103
108
60-140
5
Methylene Chloride
ug/L
ND
20
20
21.6
22.9
108
114
60-140
6
Results presented on this page are in
the units indicated
by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc . Page 24 of 29

1�7aceAnalXical
/ www.pacelabs.com
1
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1523388
1523389
MS
MSD
92261208002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
19.9
21.7
100
108
60-140
8
n-Propylbenzene
ug/L
ND
20
20
20.7
22.4
103
112
60-140
8
Naphthalene
ug/L
ND
20
20
21.0
25.4
105
127
60-140
19
o-Xylene
ug/L
ND
20
20
21.0
22.3
105
111
60-140
6
sec-Butylbenzene
ug/L
ND
20
20
21.8
23.6
109
118
60-140
8
Styrene,
ug/L
ND
20
20
21.3
22.5
107
112
60-140
5
tert-Butylbenzene
ug/L
ND
20
20
18.3
19.9
92
99
60-140
8
Tetrachloroethene
ug/L
ND
20
20
20.2
20.9
101
104
60-140
3
Toluene
ug/L
ND
20
20
21.0
21.9
105
109
60-140
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.1
23.2
111
116
60-140
5
trans-1,3-Dichloropropene
ug/L
ND
20
20
18.6
19.2
93
96
60-140
3
Trichloroethene
ug/L
ND
20
20
19.5
20.3
98
102
60-140
4
Trichlorofluoromethane
ug/L
ND
20
20
23.2
24.2
116
121
60-140
4
Vinyl chloride
ug/L
ND
20
20
23.0
23.8
115
119
60-140
4
1,2-Dichloroethane-d4 (S)
%
97
97
70-130
4-Bromofluorobenzene(S)
%
101
99
70-130
Toluene-d8 (S)
%
100
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 29

_�laceAnalXical
r
www.pacelabs.com
i
QUALIFIERS
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/10/2015 04:07 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 29

-11�lac
_eAnalytical
wwwpacelabs.com
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 1990018-55 WALSERS 67389
Pace Project No.: 92261208
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92261208001
INFLUENT
MADEP VPH
GCV/9719
92261208002
EFFLUENT
MADEP VPH
GCV/9701
92261208002
EFFLUENT
EPA 200.7
MPRP/19144 EPA 200.7
92261208001
INFLUENT
SM 6200B
MSV/32803
92261208002
EFFLUENT
SM 6200B
MSV/32804
Date: 08/10/2015 04:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Analytical
Batch
Page 27 of 29

► /�P�,CeAnalyticalSam
i
Client Name:
Condition Upon Receil
Document Number:
F-CHR-CS-003-rev.16
✓VV4111G1 IL 1\GVJOGM. 1-Y
CUR Page 1 of 2`
Issuing Authority:
Pace Huntersville Quality Office
Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS[:] USPS❑,��Cel'ent❑ Commercial❑ Pace Other s ;�
CustodySeal on Cooler/Box Present:
❑ no Seals intact: �es ❑ no
Packing Material: ❑ Bubble V❑p ❑ Bubble Bags None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ic Wet Blue None _ Samples on Ice, cooling process has begun
Temp Correction Factor T1401 No Correction
J_ '_ I- - -
Corrected Cooler Temp.: r -C
Biological Tissue is Frozen: Yes No N/A
Date and Initiaof peeq[lex �ning
contents: (}
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
es
❑No
❑N/A
1.
Chain of Custody Filled Out:
Y
❑No
❑NIA
2.
Chain of Custody Relinquished:
JdYes
❑No
❑NIA
3.
Sampler Name & Signature on COC:
Yes
❑No
❑NIA
4.
Samples Arrived within Hold Time:
AS
❑No
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Yes
No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
No
❑NIA
7.
Sufficient Volume:
Yes
❑No
❑NIA
8.
Correct Containers Used:
es
El No
❑NIA
9.
-Pace Containers Used:
es
❑No
❑NIA
Containers Intact:
Yes
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
PYes
❑No
❑NIA
11.
Sample Labels match COC:
Yes
❑No
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
Yes
❑No
❑NIA
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
XJYes
❑No
❑N/A
exceptions: VOA, coliform, Too, O&G, wt•DRO (water)
Yes
❑No
Samples checked for dechlorination:
6s
❑No
❑N/A
14.
Headspace in VOA Vials (>6mm):
Yes
❑No
11N�A
15.
Trip Blank Present:
❑Yes
❑No
N/A
46.
Trip Blank Custody Seals Present
❑Yes
❑No
W/A
ace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:1 Date: yl
SRF Review: Date: Df 3
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
WO#:92261208
1111111111111111111111
92261208
Page 28 of 29

rn
• N
CHAIN -OF=CUSTODY / Ana�ytical:'R6q.uest:Document N
The Chain of-CtJstody9s a LEGAL DOCUNIEIVT''g1i relevantfelds-mustbe'completed accurately. o,
Section 8 '^.`:Li>_ .. d
Re4ulrod Client Information: Required Project IrAortnaUon: Invoice]nformAlon:
page 1 Of 1
UST - Unde round Storage Tank
,,
.�+"'r3bcs c siatio"rYo'catPon"�ic+d 'z•
Company: Shield Engineering
Repon 70: Flora• D'SoUza
Att-0= FIG D�Souza,
Address: 4301 Taggart Creek Road
Copy To:
gompany Name Shield 'En' ineed '
Charlotte, NC 28208
Email To: fdsouza shielden ineerin .Corn
Purchase.Order No. 1990018-55 :
Address: • 01-- Tadgtirt CreekRoad;.-Chartotte,:N
Pace -OuReRefarenG
Phone: [phone] Fax
Requested Due Date/fAT:
Client Projea lo: WALSEf2S .
Pea P+�ie�z7e< ..'Herrin Kevin ,
10 Da Default
Container Order Number 67389 ?
Racd'PrQfmbaY14 44,
P2ii
ieaCedxaiaT
J71tu:Od
North
mo,
Carolina
�,t
SON i12A _
,tsrry
WA" MATRIX
W.I. p y
w WOO.- wwwr
SAMPLE ID 1d 011 a
One Character par -box. WIw wv
(AZ, 0-91,') Irr AR
Sample Ids musf be unique other oT
r u. ry
Influent
Efiluent
e`.
o'
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COLLECTED
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. SIGNATURE ofSAMPLM"
DATESIgned•
- f r
11

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company, Inc. - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 641q North Carolina HiahwaV 15ON
TYPE OF PERMITTED OPERATION BEING MONITORED
LeAnoton" NC 27295
County Davidson
El Lagoon El Remediation: Infiltration Gallery
`
❑ Spray Field ® Remediation: GrOUndWater
Contact Person: Flora D'Souza/Shield Enaineerina. Inc.
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: Nam_
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 6/22/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: 4 in.
pH 5.71 units Temp. NM OC
DRY at
Depth to Water Level. NM ft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NMµMhos
time ofsampling,
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/24/15 - 6/26/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead 0.0065 mg/1
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100m1
Phosphorus: Total as P
NA mg/1
(Note. Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds ."3L cent�atiori Uhits):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I
Aliphatic (C05-CO8) = O.bg7 tg l
pH (when analyzed) NA units
Ba - Barium
NA mg/I
Ji n 27 2015
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
`
Grease and Oils NA mg/1
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MAnFP VPH
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/1
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 2.8047 mg/L Effluent Total VOCs: 0.067 mg/L VOC Removal% 97.6%
Flora D'Souza/Shield Enaineerina. Proiect Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007

APPENDIX A

a
�aceAnalytilcal
wwwpacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 30, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S
Pace Project No.: 92255672
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on June 23, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 29

aceAnalytical
..pacelabs.ccm
1
Project: WALSER'S
Pace Project No.: 92255672
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 29

Pace Analytical Services, Inc.
,r nalyti^al
Cili Ha' I li
ace
9800 Kinsey Ave. Suite 100
078
Huntersville, NC 28078
wwwpacelabs.com
i
1
I
[phone]
SAMPLE ANALYTE COUNT
Project: WALSER'S
Pace Project No.: 92255672
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92255672001 INFLUENT
MADEP VPH
BFW
5 PASI-C
SM 6200B
CAH
63 PASI-C
92255672002 EFFLUENT
MADEP VPH
BFW
5 PASI-C
EPA 200.7
JMW
1 PASI-A
SM 6200B
CAH
63 PASI-C
REPORT OF LABORATORY ANALYSIS
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/71aceAnalXical'
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Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: WALSER'S
Pace Project No.: 92255672
Lab Sample ID Client Sample ID
92255672001
INFLUENT
MADEP VPH
Aliphatic (C09-C12)
SM 6200B
Benzene
SM 6200B
1,2-Dibromoethane (EDB)
SM 6200B
Ethylbenzene
SM 6200B
Isopropylbenzene (Cumene)
SM 6200B
Naphthalene
SM 6200B
n-Propylbenzene
SM 6200B
Toluene
SM 6200B
1,2,4-Trimethylbenzene
SM 6200B
1,3,5-Trimethylbenzene
SM 6200B
m&p-Xylene
SM 6200B
o-Xylene
92255672002
EFFLUENT
MADEP VPH
Aliphatic (C05-008)
EPA 200.7
Lead
Result
Units
Report Limit
Analyzed Qualifiers
850
ug/L
500
06/25/1510:06 N2
16.8
ug/L
1.2
06/26/15 06:51
7.2
ug/L
1.2
06/26/15 06:51
71.3
ug/L
1.2
06/26/15 06:51
4.9
ug/L
1.2
06/26/15 06:51
105
ug/L
5.0
06/26/15 06:51
7.6
ug/L
1.2
06/26/15 06:51
773
ug/L
2.5
06/26/1515:43
98.9
ug/L
1.2
06/26/15 06:51
67.0
ug/L
1.2
06/26/15 06:51
418
ug/L
2.5
06/26/15 06:51
385
ug/L
1.2
06/26/15 06:51
67.0
ug/L
50.0
06/25/15 09:12 N2
6.5
ug/L
5.0
06/26/15 22:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 29

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92255672
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: June 30, 2015
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9545
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1493381)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
EFFLUENT (Lab ID: 92255672002)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• INFLUENT (Lab ID: 92255672001)
• Aliphatic (C05-008)
• Aliphatic (C09-C 12)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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/�aceAnalytical"
/ www.pacelabs.com
i
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92255672
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: June 30, 2015
Analyte Comments:
QC Batch: GCV/9545
N2: The lab does not hold TNI accreditation for this parameter.
• INFLUENT (Lab ID: 92255672001)
• Aromatic (C09-C10)
• LCS (Lab ID: 1493382)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1493383)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C 10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 6 of 29

aceAnalytical
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PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92255672
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: June 30, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 7 of 29

aceAnalyticaI
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PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92255672
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: June 30, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/32299
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92255672002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1493890)
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1493891)
• Dichlorodifluoromethane
QC Batch: MSV/32319
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92255912006
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1495061)
• Dichlorodifluoromethane
- MSD (Lab ID: 1495062)
- Dichlorodifluoromethane
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc. Page 8 of 29

/�aceAnalytica(
www..pacelabs.com
i
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92255672
Method: SM 6200B
Description: 6200B MSV
Client: Shield
Date: June 30, 2015
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc Page 9 of 29

/�aceAnalytical
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r
i
Project: WALSER'S
Pace Project No.: 92255672
Sample: INFLUENT
Parameters
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans- l,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 06/30/2015 0105 PM
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92255672001 Collected:
06/22/15 12:00
Received: 06/23/15 15:21 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Analytical Method: MADEP VPH
ND ug/L
500
10
06/25/1510:06 N2
850 ug/L
500
10
06/25/1510:06 N2
ND ug/L
500
10
06/25/1510:06 N2
103
%
98
%
Analytical Method:
SM 62006
16.8
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
7.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
71.3
ug/L
ND
ug/L
4.9
ug/L
70-130 10
70-130 10
06/25/1510:06 460-00-4
06/25/1510.06 460-00-4
1.2
2.5
06/26/15 06:51
71-43-2
1.2
2.5
06/26/15 06:51
108-86-1
1.2
2.5
06/26/15 06:51
74-97-5
1.2
2.5
06/26/15 06:51
75-27-4
1.2
2.5
06/26/15 06:51
75-25-2
12.5
2.5
06/26/15 06:51
74-83-9
1.2
2.5
06/26/15 06:51
104-51-8
1.2
2.5
06/26/15 06:51
135-98-8
1.2
2.5
06/26/15 06:51
98-06-6
1.2
2.5
06/26/15 06:51
56-23-5
1.2
2.5
06/26/15 06:51
108-90-7
2.5
2.5
06/26/15 06:51
75-00-3
1.2
2.5
06/26/15 06:51
67-66-3
2.5
2.5
06/26/15 06:51
74-87-3
1.2
2.5
06/26/15 06:51
95-49-8
12
2.5
06/26/15 06:51
106-43-4
2.5
2.5
06/26/15 06:51
96-12-8
1.2
2.5
06/26/15 06:51
124-48-1
1.2
2.5
06/26/15 06:51
106-93-4
1.2
2.5
06/26/15 06:51
74-95-3
1.2
2.5
06/26/15 06:51
95-50-1
1.2
2.5
06/26/15 06:51
541-73-1
1.2
2.5
06/26/15 06:51
106-46-7
1.2
2.5
06/26/15 06:51
75-71-8
1.2
2.5
06/26/15 06:51
75-34-3
1.2
2.5
06/26/15 06:51
107-06-2
1.2
2.5
06/26/15 06:51
75-35-4
1.2
2.5
06/26/15 06:51
156-59-2
1.2
2.5
06/26/15 06:51
156-60-5
1.2
2.5
06/26/15 06:51
78-87-5
1.2
2.5
06/26/15 06:51
142-28-9
1.2
2.5
06/26/15 06:51
594-20-7
1.2
2.5
06/26/15 06:51
563-58-6
1.2
2.5
06/26/15 06:51
10061-01-5
1.2
2.5
06/26/15 06:51
10061-02-6
1.2
2.5
06/26/15 06:51
108-20-3
1.2
2.5
06/26/15 06:51
100-41-4
5.0
2.5
06/26/15 06:51
87-68-3
1.2
2.5
06/26/15 06:51
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .
Page 10 of 29

A_ ace Analytical
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[phone]
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92255672
Sample: INFLUENT Lab ID: 92255672001 Collected: 06/22/15 12:00 Received: 06/23/15 15:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6200B MSV
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 06/30/2015 03:05 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
105
ug/L
7.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
773
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98.9
ug/L
67.0
ug/L
ND
ug/L
418
ug/L
385
ug/L
100
%
102
%
100
%
5.0
2.5
06/26/15 06:51
75-09-2
1.2
2.5
06/26/15 06:51
1634-04-4
5.0
2.5
06/26/15 06:51
91-20-3
1.2
2.5
06/26/15 06:51
103-65-1
1.2
2.5
06/26/15 06:51
100-42-5
1.2
2.5
06/26/15 06:51
630-20-6
1.2
2.5
06/26/15 06:51
79-34-5
1.2
2.5
06/26/15 06:51
127-18-4
2.5
5
06/26/1515:43
108-88-3
5.0
2.5
06/26/15 06:51
87-61-6
5.0
2.5
06/26/15 06:51
120-82-1
1.2
2.5
06/26/15 06:51
71-55-6
1.2
2.5
06/26/15 06:51
79-00-5
1.2
2.5
06/26/15 06:51
79-01-6
2.5
2.5
06/26/15 06:51
75-69-4
1.2
2.5
06/26/15 06:51
96-18-4
1.2
2.5
06/26/15 06:51
95-63-6
1.2
2.5
06/26/15 06:51
108-67-8
2.5
2.5
06/26/15 06:51
75-01-4
2.5
2.5
06/26/15 06:51
179601-23-1
1.2
2.5
06/26/15 06:51
95-47-6
70-130 2.5
70-130 2.5
70-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
06/26/15 06:51 17060-07-0
06/26/15 06:51 460-00-4
06/26/15 06:51 2037-26-5
Page 11 of 29

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Project: WALSER'S
Pace Project No.: 92255672
Sample: EFFLUENT
Parameters
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
200.7 MET ICP
Lead
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1 -Dichloropropene
cis- 1,3-Dichloropropene
trans-1, 3-Dichloropropene
Date: 06/30/2015 03:05 PM
ANALYTICAL RESULTS
Lab ID: 92255672002 Collected: 06/22/15 13:00 Received: 06/23/15 15:21 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: MADEP VPH
67.0
ug/L
50.0
1
06/25/15 09:12
N2
ND
ug/L
50.0
1
06/25/15 09:12
N2
ND
ug/L
50.0
1
06/25/15 09:12
N2
106
%
70-130
1
06/25/15 09:12
460-00-4
100
%
70-130
1
06/25/15 09:12
460-00-4
Analytical Method:
EPA 200.7 Preparation Method: EPA 200.7
6.5
ug/L
5.0
1 06/24/15 16:15
06/26/15 22:52
7439-92-1
Analytical Method:
SM 6200B
ND
ug/L
0.50
1
06/25/15 03:15
71-43-2
ND
ug/L
0.50
1
06/25/15 03:15
108-86-1
ND
ug/L
0.50
1
06/25/15 03:15
74-97-5
ND
ug/L
0.50
1
06/25/15 03:15
75-27-4
ND
ug/L
0.50
1
06/25/15 03:15
75-25-2
ND
ug/L
5.0
1
06/25/15 03:15
74-83-9
ND
ug/L
0.50
1
06/25/15 03:15
104-51-8
ND
ug/L
0.50
1
06/25/15 03:15
135-98-8
ND
ug/L
0.50
1
06/25/15 03:15
98-06-6
ND
ug/L
0.50
1
06/25/15 03:15
56-23-5
ND
ug/L
0.50
1
06/25/15 03:15
108-90-7
ND
ug/L
1.0
1
06/25/15 03:15
75-00-3
ND
ug/L
0.50
1
06/25/15 03:15
67-66-3
ND
ug/L
1.0
1
06/25/15 03:15
74-87-3
ND
ug/L
0.50
1
06/25/15 03:15
95-49-8
ND
ug/L
0.50
1
06/25/15 03:15
106-43-4
ND
ug/L
1.0
1
06/25/15 03:15
96-12-8
ND
ug/L
0.50
1
06/25/15 03:15
124-48-1
ND
ug/L
0.50
1
06/25/15 03:15
106-93-4
ND
ug/L
0.50
1
06/25/15 03:15
74-95-3
ND
ug/L
0.50
1
06/25/15 03:15
95-50-1
ND
ug/L
0.50
1
06/25/15 03:15
541-73-1
ND
ug/L
0.50
1
06/25/15 03:15
106-46-7
ND
ug/L
0.50
1
06/25/15 03:15
75-71-8
M1
ND
ug/L
0.50
1
06/25/15 03:15
75-34-3
ND
ug/L
0.50
1
06/25/15 03:15
107-06-2
ND
ug/L
0.50
1
06/25/15 03:15
75-35-4
ND
ug/L
0.50
1
06/25/15 03:15
156-59-2
ND
ug/L
0.50
1
06/25/15 03:15
156-60-5
ND
ug/L
0.50
1
06/25/15 03:15
78-87-5
ND
ug/L
0.50
1
06/25/15 03:15
142-28-9
ND
ug/L
0.50
1
06/25/15 03:15
594-20-7
ND
ug/L
0.50
1
06/25/15 03:15
563-58-6
ND
ug/L
0.50
1
06/25/15 03:15
10061-01-5
ND
ug/L
0.50
1
06/25/15 03:15
10061-02-6
REPORT OF LABORATORY ANALYSIS
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Project: WALSER'S
Pace Project No.: 92255672
Sample: EFFLUENT
Parameters
6200B MSV
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 06/30/2015 0105 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92255672002 Collected: 06/22/15 13:00 Received: 06/23/15 15:21 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200E
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
102 %
99 %
0.50
1
06/25/15 03:15
108-20-3
0.50
1
06/25/15 03:15
100-41-4
2.0
1
06/25/15 03:15
87-68-3 M1
0.50
1
06/25/15 03:15
98-82-8
2.0
1
06/25/15 03:15
75-09-2
0.50
1
06/25/15 03:15
1634-04-4
2.0
1
06/25/15 03:15
91-20-3
0.50
1
06/25/15 03:15
103-65-1
0.50
1
06/25/15 03:15
100-42-5
0.50
1
06/25/15 03:15
630-20-6
0.50
1
06/25/15 03:15
79-34-5
0.50
1
06/25/15 03:15
127-18-4
0.50
1
06/25/15 03:15
108-88-3
2.0
1
06/25/15 03:15
87-61-6
2.0
1
06/25/15 03:15
120-82-1
0.50
1
06/25/15 03:15
71-55-6
0.50
1
06/25/15 03:15
79-00-5
0.50
1
06/25/15 03:15
79-01-6
1.0
1
06/25/15 03:15
75-69-4
0.50
1
06/25/15 03:15
96-18-4
0.50
1
06/25/15 03:15
95-63-6
0.50
1
06/25/15 03:15
108-67-8
1.0
1
06/25/15 03:15
75-01-4
1.0
1
06/25/15 03:15
179601-23-1
0.50
1
06/25/15 03:15
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
06/25/15 03:15 17060-07-0
O6/25/15 03:15 460-00-4
06/25/15 03:15 2037-26-5
Page 13 of 29

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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
QC Batch: GCV/9545 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92255672001, 92255672002
METHOD BLANK: 1493381
Associated Lab Samples: 92255672001, 92255672002
Parameter
Units
Aliphatic (C05-CO8)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
06/24/1516:59 N2
ND
50.0
06/24/1516:59 N2
ND
50.0
06/24/1516:59 N2
101
70-130
06/24/1516:59
95
70-130
06/24/1516:59
LABORATORY CONTROL SAMPLE & LCSD: 1493382
Spike
Parameter Units Conc.
Aliphatic (C05-CO8) ug/L 300
Aliphatic (C09-C12) ug/L 300
Aromatic (C09-C10) ug/L 100
4-Bromofluorobenzene (FID) (S) %
4-Bromofluorobenzene (PID) (S) %
1493383
LCS
LCSD
LCS
LCSD
% Rec
Max
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
296
303
99
101
70-130
2 25 N2
310
325
103
108
30-130
5 25 N2
94.1
95.7
94
96
70-130
2 25 N2
102
105
70-130
99
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 29

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i
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
QC Batch: MPRP/18823 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92255672002
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1493286
Matrix: Water
Associated Lab Samples: 92255672002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Lead ug/L
ND 5.0
06/26/15 21:18
LABORATORY CONTROL SAMPLE: 1493287
Spike
LCS
LCS
% Rec
Parameter Units
Conic.
Result
% Rec
Limits
Qualifiers
Lead ug/L
500
446
89
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1493288
1493289
MS
MSD
92255572005
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD Qual
Lead ug/L ND
500
500 483
446
97
89
70-130
8
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1493290
1493291
MS
MSD
92255694002
Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD Qual
Lead ug/L ND
500
500 453
455
91
91
70-130
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc .
Page 15 of 29

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
QC Batch: MSV/32299
QC Batch Method: SM 6200B
Associated Lab Samples: 92255672002
Analysis Method:
Analysis Description:
SM 6200B
6200B MSV
METHOD BLANK: 1493888
Matrix: Water
Associated Lab Samples: 92255672002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
06/25/15 02:59
1, 1, 1 -Trichloroethane
ug/L
ND
0.50
06/25/15 02:59
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
06/25/15 02:59
1,1,2-Trichloroethane
ug/L
ND
0.50
06/25/15 02:59
1,1-Dichloroethane
ug/L
ND
0.50
06/25/15 02:59
1,1-Dichloroethene
ug/L
ND
0.50
06/25/15 02:59
1,1-Dichloropropene
ug/L
ND
0.50
06/25/15 02:59
1,2,3-Trichlorobenzene
ug/L
ND
2.0
06/25/15 02:59
1,2,3-Trichloropropane
ug/L
ND
0.50
06/25/15 02:59
1,2,4-Trichlorobenzene
ug/L
ND
2.0
06/2511502:59
1,2,4-Trimethylbenzene
ug/L
ND
0.50
06/25/15 02:59
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
06/25/15 02:59
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
06/25/15 02:59
1,2-Dichlorobenzene
ug/L
ND
0.50
06/25/15 02:59
1,2-Dichloroethane
ug/L
ND
0.50
06/25/15 02:59
1,2-Dichloropropane
ug/L
ND
0.50
06/25/15 02:59
1,3,5-Trimethylbenzene
ug/L
ND
0.50
06/25/15 02:59
1,3-Dichlorobenzene
ug/L
ND
0.50
06/25/15 02:59
1,3-Dichloropropane
ug/L
ND
0.50
06/25/15 02:59
1,4-Dichlorobenzene
ug/L
ND
0.50
06/25/15 02:59
2,2-Dichloropropane
ug/L
ND
0.50
06/25/15 02:59
2-Chlorotoluene
ug/L
ND
0.50
06/25/15 02:59
4-Chlorotoluene
ug/L
ND
0.50
06/25/15 02:59
Benzene
ug/L
ND
0.50
06/25/15 02:59
Bromobenzene
ug/L
ND
0.50
06/25/15 02:59
Bromochloromethane
ug/L
ND
0.50
06/25/15 02:59
Bromodichloromethane
ug/L
ND
0.50
06/25/15 02:59
Bromoform
ug/L
ND
0.50
06/25/15 02:59
Bromomethane
ug/L
ND
5.0
06/25/15 02:59
Carbon tetrachloride
ug/L
ND
0.50
06/25/15 02:59
Chlorobenzene
ug/L
ND
0.50
06/25/15 02:59
Chloroethane
ug/L
ND
1.0
06/25/15 02:59
Chloroform
ug/L
ND
0.50
06/25/15 02:59
Chloromethane
ug/L
ND
1.0
06/25/15 02:59
cis-1,2-Dichloroethene
ug/L
ND
0.50
06/25/15 02:59
cis-1,3-Dichloropropene
ug/L
ND
0.50
06/25/15 02:59
Dibromochloromethane
ug/L
ND
0.50
06/25/15 02:59
Dibromomethane
ug/L
ND
0.50
06/25/15 02:59
Dichlorodifluoromethane
ug/L
ND
0.50
06/25/15 02:59
Diisopropyl ether
ug/L
ND
0.50
06/25/15 02:59
Ethylbenzene
ug/L
ND
0.50
06/25/15 02:59
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 29

/�aceAnalyticaI
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
METHOD BLANK: 1493888
Associated Lab Samples: 92255672002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
06/25/15 02:59
Isopropylbenzene (Cumene)
ug/L
ND
0.50
06/25/15 02:59
m&p-Xylene
ug/L
ND
1.0
06/25/15 02:59
Methyl-tert-butyl ether
ug/L
ND
0.50
06/25/15 02:59
Methylene Chloride
ug/L
ND
2.0
06/25/15 02:59
n-Butylbenzene
ug/L
ND
0.50
06/25/15 02:59
n-Propylbenzene
ug/L
ND
0.50
06/25/15 02:59
Naphthalene
ug/L
ND
2.0
06/25/15 02:59
o-Xylene
ug/L
ND
0.50
06/25/15 02:59
sec-Butylbenzene
ug/L
ND
0.50
06/25/15 02:59
Styrene
ug/L
ND
0.50
06/25/15 02:59
tert-Butylbenzene
ug/L
ND
0.50
06/25/15 02:59
Tetrachloroethene
ug/L
ND
0.50
06/25/15 02:59
Toluene
ug/L
ND
0.50
06/25/15 02:59
trans-1,2-Dichloroethene
ug/L
ND
0.50
06/25/15 02:59
trans-1,3-Dichloropropene
ug/L
ND
0.50
06/25/15 02:59
Trichloroethene
ug/L
ND
0.50
06/25/15 02:59
Trichlorofluoromethane
ug/L
ND
1.0
06/25/15 02:59
Vinyl chloride
ug/L
ND
1.0
06/25/15 02:59
1,2-Dichloroethane-d4 (S)
%
98
70-130
06/25/15 02:59
4-Bromofluorobenzene (S)
%
101
70-130
06/25/15 02:59
Toluene-d8 (S)
%
101
70-130
06/25/15 02:59
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1493889
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.5
103
60-140
1,1,1-Trichloroethane
ug/L
50
53.6
107
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.3
103
60-140
1,1,2-Trichloroethane
ug/L
50
48.9
98
60-140
1, 1 -Dichloroethane
ug/L
50
48.2
96
60-140
1, 1 -Dichloroethene
ug/L
50
51.7
103
60-140
1, 1 -Dichloropropene
ug/L
50
51.8
104
60-140
1,2,3-Trichlorobenzene
ug/L
50
51.1
102
60-140
1,2,3-Trichloropropane
ug/L
50
51.1
102
60-140
1,2,4-Trichlorobenzene
ug/L
50
50.7
101
60-140
1,2,4-Trimethylbenzene
ug/L
50
50.5
101
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.5
107
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.8
108
60-140
1,2-Dichlorobenzene
ug/L
50
49.0
98
60-140
1,2-Dichloroethane
ug/L
50
46.8
94
60-140
1,2-Dichloropropane
ug/L
50
48.5
97
60-140
1,3,5-Trimethylbenzene
ug/L
50
50.5
101
60-140
1,3-Dichlorobenzene
ug/L
50
49.4
99
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 29

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
LABORATORY CONTROL SAMPLE:
Parameter
1493889
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
48.7
97
60-140
1,4-Dichlorobenzene
ug/L
50
47.5
95
60-140
2,2-Dichloropropane
ug/L
50
49.2
98
60-140
2-Chlorotoluene
ug/L
50
49.5
99
60-140
4-Chlorotoluene
ug/L
50
48.6
97
60-140
Benzene
ug/L
50
49.3
99
60-140
Bromobenzene
ug/L
50
50.8
102
60-140
Bromochloromethane
ug/L
50
51.1
102
60-140
Bromodichloromethane
ug/L
50
51.9
104
60-140
Bromoform
ug/L
50
40.8
82
60-140
Bromomethane
ug/L
50
35.6
71
60-140
Carbon tetrachloride
ug/L
50
55.3
111
60-140
Chlorobenzene
ug/L
50
48.1
96
60-140
Chloroethane
ug/L
50
48.9
98
60-140
Chloroform
ug/L
50
51.2
102
60-140
Chloromethane
ug/L
50
42.4
85
60-140
cis- 1,2-Dichloroethene
ug/L
50
49.4
99
60-140
cis-1,3-Dichloropropene
ug/L
50
53.7
107
60-140
Dibromochloromethane
ug/L
50
53.6
107
60-140
Dibromomethane
ug/L
50
48.9
98
60-140
Dichlorodifluoromethane
ug/L
50
53.4
107
60-140
Diisopropyl ether
ug/L
50
50.9
102
60-140
Ethylbenzene
ug/L
50
49.8
100
60-140
Hexachloro-1,3-butadiene
ug/L
50
63.1
126
60-140
Isopropylbenzene (Cumene)
ug/L
50
54.0
108
60-140
m&p-Xylene
ug/L
100
99.9
100
60-140
Methyl-tert-butyl ether
ug/L
50
50.8
102
60-140
Methylene Chloride
ug/L
50
51.5
103
60-140
n-Butylbenzene
ug/L
50
52.1
104
60-140
n-Propylbenzene
ug/L
50
51.9
104
60-140
Naphthalene
ug/L
50
54.1
108
60-140
o-Xylene
ug/L
50
50.6
101
60-140
sec-Butylbenzene
ug/L
50
54.9
110
60-140
Styrene
ug/L
50
52.7
105
60-140
tert-Butylbenzene
ug/L
50
44.8
90
60-140
Tetrachloroethene
ug/L
50
47.2
94
60-140
Toluene
ug/L
50
48.2
96
60-140
trans- 1,2-Dichloroethene
ug/L
50
49.6
99
60-140
trans-1,3-Dichloropropene
ug/L
50
52.5
105
60-140
Trichloroethene
ug/L
50
47.4
95
60-140
Trichlorofluoromethane
ug/L
50
50.5
101
60-140
Vinyl chloride
ug/L
50
50.3
101
60-140
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
98
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 29

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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92255672
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1493890
1493891
MS
MSD
92255672002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.7
24.1
119
120
60-140
2
1,1,1-Trichloroethane
ug/L
ND
20
20
24.9
24.8
124
124
60-140
0
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
24.9
24.7
125
123
60-140
1
1,1,2-Trichloroethane
ug/L
ND
20
20
22.3
22.1
111
110
60-140
1
1,1-Dichloroethane
ug/L
ND
20
20
22.5
22.3
112
112
60-140
1
1, 1 -Dichloroethene
ug/L
ND
20
20
25.4
25.3
127
126
60-140
0
1,1-Dichloropropene
ug/L
ND
20
20
24.6
24.5
123
123
60-140
0
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.6
21.2
108
106
60-140
2
1,2,3-Trichloropropane
ug/L
ND
20
20
23.6
23.0
118
115
60-140
3
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.9
21.1
109
105
60-140
4
1,2,4-Trimethylbenzene
ug/L
ND
20
20
23.9
23.1
119
115
60-140
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
22.3
21.7
111
109
60-140
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
24.7
24.6
124
123
60-140
1
1,2-Dichlorobenzene
ug/L
ND
20
20
22.6
22.1
113
111
60-140
2
1,2-Dichloroethane
ug/L
ND
20
20
21A
21.5
107
108
60-140
1
1,2-Dichloropropane
ug/L
ND
20
20
23.0
23.0
115
115
60-140
0
1,3,5-Trimethylbenzene
ug/L
ND
20
20
23.8
23.0
119
115
60-140
3
1,3-Dichlorobenzene
ug/L
ND
20
20
23.1
22.8
116
114
60-140
2
1,3-Dichloropropane
ug/L
ND
20
20
22.1
22.5
110
112
60-140
2
1,4-Dichlorobenzene
ug/L
ND
20
20
22.7
21.6
113
108
60-140
5
2,2-Dichloropropane
ug/L
ND
20
20
25.4
25.0
127
125
60-140
1
2-Chlorotoluene
ug/L
ND
20
20
23.3
22.7
117
114
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
22.9
22.6
114
113
60-140
1
Benzene
ug/L
ND
20
20
23.4
23.7
116
117
60-140
1
Bromobenzene
ug/L
ND
20
20
23.9
22.9
120
115
60-140
4
Bromochloromethane
ug/L
ND
20
20
23.2
22.9
116
114
60-140
1
Bromodichloromethane
ug/L
ND
20
20
23.4
23.8
117
119
60-140
2
Bromoform
ug/L
ND
20
20
19.6
19.1
98
96
60-140
3
Bromomethane
ug/L
ND
20
20
11.9
12.6
60
63
60-140
6
Carbon tetrachloride
ug/L
ND
20
20
26.7
26.9
133
134
60-140
1
Chlorobenzene
ug/L
ND
20
20
22.7
23.1
113
116
60-140
2
Chloroethane
ug/L
ND
20
20
21.9
23.2
109
116
60-140
6
Chloroform
ug/L
ND
20
20
23.5
23.5
117
118
60-140
0
Chloromethane
ug/L
ND
20
20
19.6
21.9
98
110
60-140
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.5
22.7
112
113
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
24.0
23.8
120
119
60-140
1
Dibromochloromethane
ug/L
ND
20
20
23.3
23.6
116
118
60-140
1
Dibromomethane
ug/L
ND
20
20
22.1
22.3
111
112
60-140
1
Dichlorodifluoromethane
ug/L
ND
20
20
28.8
29.2
144
146
60-140
1 M1
Diisopropyl ether
ug/L
ND
20
20
23.6
23.6
118
118
60-140
0
Ethylbenzene
ug/L
ND
20
20
24.0
24.1
120
121
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
28.5
28.0
143
140
60-140
2 M1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
25.5
25.8
128
129
60-140
1
m&p-Xylene
ug/L
ND
40
40
47.8
47.9
120
120
60-140
0
Methyl-tert-butyl ether
ug/L
ND
20
20
22.7
22.6
113
113
60-140
0
Methylene Chloride
ug/L
ND
20
20
22.8
21.6
114
108
60-140
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 0105 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 29

r
aceAnalytical
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1
I
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1493890 1493891
Parameter
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
92255672002
Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
ug/L
ND
20
20
23.7
23.0
118
115
60-140
3
ug/L
ND
20
20
24.8
24.0
124
120
60-140
3
ug/L
ND
20
20
23.4
22.8
117
114
60-140
3
ug/L
ND
20
20
24.2
23.9
121
120
60-140
1
ug/L
ND
20
20
25.4
24.8
127
124
60-140
2
ug/L
ND
20
20
24.8
24.6
124
123
60-140
1
ug/L
ND
20
20
21.0
20.3
105
102
60-140
3
ug/L
ND
20
20
22.7
23.1
114
116
60-140
2
ug/L
ND
20
20
22.8
22.9
114
115
60-140
0
ug/L
ND
20
20
23.5
23.4
117
117
60-140
0
ug/L
ND
20
20
23.2
23.2
116
116
60-140
0
ug/L
ND
20
20
22.5
22.9
112
114
60-140
2
ug/L
ND
20
20
25.7
25.5
129
127
60-140
1
ug/L
ND
20
20
24.5
25.0
123
125
60-140
2
%
99
99
70-130
%
104
105
70-130
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc
Qual
Page 20 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
QC Batch: MSV/32319
Analysis Method:
SM 6200B
QC Batch Method: SM 6200B
Analysis Description:
6200E MSV
Associated Lab Samples: 92255672001
METHOD BLANK: 1495059
Matrix: Water
Associated Lab Samples: 92255672001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
06/26/15 04:55
1,1,1-Trichloroethane
ug/L
ND
0.50
06/26/15 04:55
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
06/26/15 04:55
1,1,2-Trichloroethane
ug/L
ND
0.50
06/26/15 04:55
1,1-Dichloroethane
ug/L
ND
0.50
06/26/15 04:55
1,1-Dichloroethene
ug/L
ND
0.50
06/26/15 04:55
1,1-Dichloropropene
ug/L
ND
0.50
06/26/15 04:55
1,2,3-Trichlorobenzene
ug/L
ND
2.0
06/26/15 04:55
1,2,3-Trichloropropane
ug/L
ND
0.50
06/26/15 04:55
1,2,4-Trichlorobenzene
ug/L
ND
2.0
06/26/15 04:55
1,2,4-Trimethylbenzene
ug/L
ND
0.50
06/26/15 04:55
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
06/26/15 04:55
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
06/26/15 04:55
1,2-Dichlorobenzene
ug/L
ND
0.50
06/26/15 04:55
1,2-Dichloroethane
ug/L
ND
0.50
06/26/15 04:55
1,2-Dichloropropane
ug/L
ND
0.50
06/26/15 04:55
1,3,5-Trimethylbenzene
ug/L
ND
0.50
06/26/15 04:55
1,3-Dichlorobenzene
ug/L
ND
0.50
06/26/15 04:55
1,3-Dichloropropane
ug/L
ND
0.50
06/26/15 04:55
1,4-Dichlorobenzene
ug/L
ND
0.50
06/26/15 04:55
2,2-Dichloropropane
ug/L
ND
0.50
06/26/15 04:55
2-Chlorotoluene
ug/L
ND
0.50
06/26/15 04:55
4-Chlorotoluene
ug/L
ND
0.50
06/26/15 04:55
Benzene
ug/L
ND
0.50
06/26/15 04:55
Bromobenzene
ug/L
ND
0.50
06/26/15 04:55
Bromochloromethane
ug/L
ND
0.50
06/26/15 04:55
Bromodichloromethane
ug/L
ND
0.50
06/26/15 04:55
Bromoform
ug/L
ND
0.50
06/26/15 04:55
Bromomethane
ug/L
ND
5.0
06/26/15 04:55
Carbon tetrachloride
ug/L
ND
0.50
06/26/15 04:55
Chlorobenzene
ug/L
ND
0.50
06/26/15 04:55
Chloroethane
ug/L
ND
1.0
06/26/15 04:55
Chloroform
ug/L
ND
0.50
06/26/15 04:55
Chloromethane
ug/L
ND
1.0
06/26/15 04:55
cis- 1,2-Dichloroethene
ug/L
ND
0.50
06/26/15 04:55
cis- 1,3-Dichloropropene
ug/L
ND
0.50
06/26/15 04:55
Dibromochloromethane
ug/L
ND
0.50
06/26/15 04:55
Dibromomethane
ug/L
ND
0.50
06/26/15 04:55
Dichlorodifluoromethane
ug/L
ND
0.50
06/26/15 04:55
Diisopropyl ether
ug/L
ND
0.50
06/26/15 04:55
Ethylbenzene
ug/L
ND
0.50
06/26/15 04:55
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc . Page 21 of 29

Pace Analytical Services, Inc.
®
/�aceAnalyfical
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
1
(704) 87 5-9092
QUALITY
CONTROL
DATA
Project: WALSER'S
Pace Project No.: 92255672
METHOD BLANK: 1495059
Matrix:
Water
Associated Lab Samples: 92255672001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Hexachloro-1,3-butadiene
ug/L
ND
2.0
06/26/15 04:55
Isopropylbenzene (Cumene)
ug/L
ND
0.50
06/26/15 04:55
m&p-Xylene
ug/L
ND
1.0
06/26/15 04:55
Methyl-tert-butyl ether
ug/L
ND
0.50
06/26/15 04:55
Methylene Chloride
ug/L
ND
2.0
06/26/15 04:55
n-Butylbenzene
ug/L
ND
0.50
06/26/15 04:55
n-Propylbenzene
ug/L
ND
0.50
06/26/15 04:55
Naphthalene
ug/L
ND
2.0
06/26/15 04:55
o-Xylene
ug/L
ND
0.50
06/26/15 04:55
sec-Butylbenzene
ug/L
ND
0.50
06/26/15 04:55
Styrene
ug/L
ND
0.50
06/26/15 04:55
tert-Butylbenzene
ug/L
ND
0.50
06/26/15 04:55
Tetrachloroethene
ug/L
ND
0.50
06/26/15 04:55
Toluene
ug/L
ND
0.50
06/26/15 04:55
trans- 1,2-Dichloroethene
ug/L
ND
0.50
06/26/15 04:55
trans- 1,3-Dichloropropene
ug/L
ND
0.50
06/26/15 04:55
Trichloroethene
ug/L
ND
0.50
06/26/15 04:55
Trichlorofluoromethane
ug/L
ND
1.0
06/26/15 04:55
Vinyl chloride
ug/L
ND
1.0
06/26/15 04:55
1,2-Dichloroethane-d4 (S)
%
100
70-130
06/26/15 04:55
4-Bromofluorobenzene (S)
%
102
70-130
06/26/15 04:55
Toluene-d8 (S)
%
101
70-130
06/26/15 04:55
LABORATORY CONTROL SAMPLE:
1495060
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
60-140
1,1,1-Trichloroethane
ug/L
50
50.6
101
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
51.4
103
60-140
1,1,2-Trichloroethane
ug/L
50
48.8
98
60-140
1,1-Dichloroethane
ug/L
50
45.6
91
60-140
1,1-Dichloroethene
ug/L
50
48.3
97
60-140
1, 1 -Dichloropropene
ug/L
50
48.2
96
60-140
1,2,3-Trichlorobenzene
ug/L
50
49.4
99
60-140
1,2,3-Trichloropropane
ug/L
50
51.7
103
60-140
1,2,4-Trichlorobenzene
ug/L
50
48.6
97
60-140
1,2,4-Trimethylbenzene
ug/L
50
48.4
97
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
52.4
105
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.8
108
60-140
1,2-Dichlorobenzene
ug/L
50
47.9
96
60-140
1,2-Dichloroethane
ug/L
50
46.6
93
60-140
1,2-Dichloropropene
ug/L
50
47.4
95
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.2
96
60-140
1,3-Dichlorobenzene
ug/L
50
48.4
97
60-140
Results presented on this
page are in the units
indicated by the "Units"
column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 0105 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 29

/�alceAnalytical'-
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i
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92255672
LABORATORY CONTROL SAMPLE:
Parameter
1495060
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
48.3
97
60-140
1,4-Dichlorobenzene
ug/L
50
46.3
93
60-140
2,2-Dichloropropane
ug/L
50
43.7
87
60-140
2-Chlorotoluene
ug/L
50
47.1
94
60-140
4-Chlorotoluene
ug/L
50
46.9
94
60-140
Benzene
ug/L
50
47.4
95
60-140
Bromobenzene
ug/L
50
49.6
99
60-140
Bromochloromethane
ug/L
50
49.6
99
60-140
Bromodichloromethane
ug/L
50
52.3
105
60-140
Bromoform
ug/L
50
41.5
83
60-140
Bromomethane
ug/L
50
37.4
75
60-140
Carbon tetrachloride
ug/L
50
53.7
107
60-140
Chlorobenzene
ug/L
50
47.9
96
60-140
Chloroethane
ug/L
50
41.9
84
60-140
Chloroform
ug/L
50
49.5
99
60-140
Chloromethane
ug/L
50
48.9
98
60-140
cis-1,2-Dichloroethene
ug/L
50
47.2
94
60-140
cis-1,3-Dichloropropene
ug/L
50
52.1
104
60-140
Dibromochloromethane
ug/L
50
54.3
109
60-140
Dibromomethane
ug/L
50
48.9
98
60-140
Dichlorodifluoromethane
ug/L
50
48.2
96
60-140
Diisopropyl ether
ug/L
50
50.0
100
60-140
Ethylbenzene
ug/L
50
48.3
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
57.7
115
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.6
105
60-140
m&p-Xylene
ug/L
100
97.1
97
60-140
Methyl-tert-butyl ether
ug/L
50
48.6
97
60-140
Methylene Chloride
ug/L
50
49.2
98
60-140
n-Butylbenzene
ug/L
50
48.3
97
60-140
n-Propylbenzene
ug/L
50
49.2
98
60-140
Naphthalene
ug/L
50
52.5
105
60-140
o-Xylene
ug/L
50
49.3
99
60-140
sec-Butylbenzene
ug/L
50
51.4
103
60-140
Styrene
ug/L
50
52.1
104
60-140
tert-Butylbenzene
ug/L
50
42.6
85
60-140
Tetrachloroethene
ug/L
50
45.9
92
60-140
Toluene
ug/L
50
47.2
94
60-140
trans-1,2-Dichloroethene
ug/L
50
46.5
93
60-140
trans-1,3-Dichloropropene
ug/L
50
52.4
105
60-140
Trichloroethene
ug/L
50
45.6
91
60-140
Trichlorofluoromethane
ug/L
50
48.3
97
60-140
Vinyl chloride
ug/L
50
45.5
91
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene(S)
%
106
70-130
Toluene-d8 (S)
%
99
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc
Page 23 of 29

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1
1
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92255672
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1495061
1495062
MS
MSD
92255912006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.1
23.6
116
118
60-140
2
1,1,1-Trichloroethane
ug/L
ND
20
20
24.8
25.2
124
126
60-140
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.2
23.1
111
116
60-140
4
1,1,2-Trichloroethane
ug/L
ND
20
20
21.8
21.9
109
110
60-140
1
1,1-Dichloroethane
ug/L
ND
20
20
22.2
22.4
111
112
60-140
1
1, 1 -Dichloroethene
ug/L
ND
20
20
24.8
25.1
124
125
60-140
1
1, 1 -Dichloropropene
ug/L
ND
20
20
24.3
24.7
122
123
60-140
1
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.7
21.2
104
106
60-140
2
1,2,3-Trichloropropane
ug/L
ND
20
20
22.4
23.1
112
116
60-140
3
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.7
21.3
104
106
60-140
3
1,2,4-Trimethylbenzene
ug/L
0.61
20
20
23.8
24.0
116
117
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.1
21.5
106
108
60-140
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.6
23.7
118
118
60-140
1
1,2-Dichlorobenzene
ug/L
ND
20
20
21.9
22.1
109
111
60-140
1
1,2-Dichloroethane
ug/L
ND
20
20
21.0
21.1
105
105
60-140
0
1,2-Dichloropropane
ug/L
ND
20
20
22.2
23.4
111
117
60-140
5
1,3,5-Trimethylbenzene
ug/L
ND
20
20
23.6
23.5
117
117
60-140
0
1,3-Dichlorobenzene
ug/L
ND
20
20
22.6
22.8
113
114
60-140
1
1,3-Dichloropropane
ug/L
ND
20
20
21.8
22.3
109
111
60-140
2
1,4-Dichlorobe nzene
ug/L
ND
20
20
21.9
22.0
110
110
60-140
0
2,2-Dichloropropane
ug/L
ND
20
20
24.9
25.0
124
125
60-140
0
2-Chlorotoluene
ug/L
ND
20
20
22.8
23.6
114
118
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
22.4
22.8
112
114
60-140
2
Benzene
ug/L
5.5
20
20
26.6
28.1
105
113
60-140
6
Bromobenzene
ug/L
ND
20
20
21.9
23.4
109
117
60-140
7
Bromochloromethane
ug/L
ND
20
20
22.6
23.3
113
117
60-140
3
Bromodichloromethane
ug/L
ND
20
20
22.5
23.5
113
117
60-140
4
Bromoform
ug/L
ND
20
20
18.8
19.4
94
97
60-140
3
Bromomethane
ug/L
ND
20
20
15.9
17.6
80
88
60-140
10
Carbon tetrachloride
ug/L
ND
20
20
26.1
27.4
131
137
60-140
5
Chlorobenzene
ug/L
ND
20
20
22.4
22.8
112
114
60-140
2
Chloroethane
ug/L
ND
20
20
23.1
23.3
116
116
60-140
1
Chloroform
ug/L
ND
20
20
23.0
23.5
115
118
60-140
2
Chloromethane
ug/L
ND
20
20
21.3
19.7
107
98
60-140
8
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.5
22.7
112
113
60-140
1
cis- 1,3-Dichloropropene
ug/L
ND
20
20
23.0
24.0
115
120
60-140
4
Dibromochloromethane
ug/L
ND
20
20
22.8
23.8
114
119
60-140
4
Dibromomethane
ug/L
ND
20
20
21.4
22.8
107
114
60-140
6
Dichlorodifluoromethane
ug/L
ND
20
20
28.8
28.7
144
144
60-140
0 M1
Diisopropyl ether
ug/L
0.55
20
20
23.5
24.0
115
117
60-140
2
Ethylbenzene
ug/L
0.93
20
20
23.9
24.7
115
119
60-140
3
Hexachloro-1,3-butadiene
ug/L
ND
20
20
27.9
26.7
139
134
60-140
4
Isopropylbenzene (Cumene)
ug/L
ND
20
20
24.9
25.4
125
127
60-140
2
m&p-Xylene
ug/L
2.7
40
40
48.3
50.2
114
119
60-140
4
Methyl-tert-butyl ether
ug/L
ND
20
20
22.5
22.8
111
112
60-140
1
Methylene Chloride
ug/L
ND
20
20
21.7
22.5
108
112
60-140
4
Results presented on this page are in
the units indicated by the
"Units" column
except where
an alternate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 29

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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92255672
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1495061
1495062
MS
MSD
92255912006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
22.8
22.7
114
114
60-140
0
n-Propylbenzene
ug/L
ND
20
20
24.1
24.3
121
122
60-140
1
Naphthalene
ug/L
ND
20
20
22.3
22.9
110
113
60-140
3
o-Xylene
ug/L
1.3
20
20
24.3
24.9
115
118
60-140
2
sec-Butylbenzene
ug/L
ND
20
20
24.9
24.9
125
125
60-140
0
Styrene
ug/L
ND
20
20
23.5
24.2
118
121
60-140
3
tert-Butylbenzene
ug/L
ND
20
20
20.4
20.9
102
104
60-140
2
Tetrachloroethene
ug/L
ND
20
20
22.6
22.6
113
113
60-140
0
Toluene
ug/L
8.4
20
20
29.2
30.6
104
111
60-140
5
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.1
23.5
115
117
60-140
2
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.4
23.8
112
119
60-140
6
Trichloroethene
ug/L
ND
20
20
22.1
22.8
110
114
60-140
3
Trichlorofluoromethane
ug/L
ND
20
20
25.0
25.5
125
128
60-140
2
Vinyl chloride
ug/L
ND
20
20
24.5
24.8
123
124
60-140
1
1,2-Dichloroethane-d4 (S)
%
97
97
70-130
4-Bromofluorobenzene (S)
%
103
103
70-130
Toluene-d8 (S)
%
98
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 25 of 29

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QUALIFIERS
Project: WALSER'S
Pace Project No.: 92255672
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/30/2015 03:05 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 29

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WALSER'S
Pace Project No.: 92255672
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92255672001
INFLUENT
MADEP VPH
GCV/9545
92255672002
EFFLUENT
MADEP VPH
GCV/9545
92255672002
EFFLUENT
EPA 200.7
MPRP/18823 EPA 200.7
92255672001
INFLUENT
SM 6200B
MSV/32319
92255672002
EFFLUENT
SM 6200B
MSV/32299
Date: 06/30/2015 03:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/16884
Page 27 of 29

-at,C; vrc,v('Um
Document Number: Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersviile Quality Office
Client Name: ► e l 011 • Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS[] USPS❑ Client❑ Commercial❑ KaZe Other ' • ,
Custody Seal on Cooler/Box Preseni;/�yes El no Seals intact: ��CJ yes ❑ nof4 77
ll Packing Material: Material: ❑ Bubble VDp ❑ Bubble Bags None Other
Thermometer Used: IR Gun T1401 Type of Ice: (yetl Blue None ❑ samples on ice, cooling process has begun
Tamn r'nrrarfinn Factor T1401 No Correction
r
Corrected Cooler Temp.: D •C
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No�U
Comments:
Date and Initials of of a mining
contents: v.� �D� _
Chbib Custody Present:
es ❑No
ON/A
1.
Chain of Custody Filled Out:
ZYes ❑No
❑NIA
2.
Chain of Custody Relinquished:
es ❑No
❑N/A
3.
Sampler Name & Signature on COC:
❑Yes ONo
❑N/A
4.
Samples Arrived within Hold Time:
es ❑No
❑N/A
5.
Short Hold Time Analysis <72hr :
❑Yes J26
❑NIA
6.
Rush Turn Around Time Requested:
❑Yes PNo
❑NIA
7, f fl QG
Sufficient Volume:
16yes ❑No
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
iiJYes ONo
Ples ❑No
ON/A
❑NIA
9.
Containers Intact:
Yes ❑No
❑NIA
10.
Filtered volume received for Dissolved tests
Yes ONo
ON/A
11.
Sample Labels match COC: es ONo ❑N/A
-Includes date/time/ID/Analysis Matrix:
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
Yes []No
/6Yes ONo
Yes []No
❑NIA
ON/A
13.
Samples checked for dechiorination:
Yes ONo
❑NIA
14.
Headspace in VOA Vials(>6mm):
XYes ONo
ON/A
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip --Blank Lot# if purchased):- ------ - ----
Oyes ❑No
❑Yes ❑No
------ ---- --
Nf
NIA
._. ----
16.
- . - - --- ----.__--....---- _._---- -- -- - --- ..._ --- ..-
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date: 2���'i�
SRF Review: (l Date: \Ui),�11�> 140 : 92 ((
Note: Whenever there is a discrepancy affecting North Carolina compliance W
samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp,Iii
incorrect containers) g22g5g72
Page 28 of 29

�aceAnaliical
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
—1-1 — aocuon is Section C
Required Client Information: Required Project Information: Invoice Information: Page: 1 Of
1
Company: Shield Engineering Report To: Flora D'Souza Attention: Flora D'Souza
Address: 4301 Taggart Creek Road Copy To: Company Name: Shield Engineering
Charlotte, NC 28208
Address: 4301 Taggart Creek Road, Charlotte, N
Regulatory Agency
Email To: [e-mail]
Purchase order No. 1990018-69
Pace Quote Reference:
UST - Undo round storage Tank
Phone: [phone] JFax
Client Project ID: WALSER'S
Pace Project Manager. Laura Coo er
" .State / Location
Requested Due DaterrAT. 10 Da Default
Container Order Number.
Pace Profile
North Carolina
Re
uested
Anal
Is
Filtered
YIN
-
o
Z
MATRIX CODE
o
V
COLLECTED
Preservatives>-
Dmk" Wala DIN
Water Wr
10U
m
2 4
Wasla Water NAY
Proaua P
SAMPLE ID �aitl
o
—
J
Z
}
aO
a
START
ENO
Ono Character per box. Wma WP
wQ
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(A-Z. 0,9 / -) A. AR
u
#
Y. OT
Sample Ids must be unique iS
nssue
V
x
w
w
Z
O
n
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na:
m
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Za
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DATE
DATE
TIME
N
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1
INFLUENT
WTI
t /LU
7 t
�T�I,M�E
12*,)
1
X
X
2
EFFLUENT
Wr
d-1A
iu0
X
X
X
3
4
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS.
REUNQUISHEDBY I AFFILIATION
DATE ,'.
TIME:,'
ACCEPTED BY/AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
�3
a
L—
SAMPLER NAME AND SIGNATURE
v
i
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8
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PRINT Name of SAMPLER:
!Nj 1 $ ri
$
SIGNATURE of SAMPLER:
DATE Signed: ^ /
A z
E z

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
,
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company Inc. - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Hia_hwav_ 15ON
_
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
NC 27295 County Davidson
"`'
❑ Spray Field ® Remediation: Groundwater
Contact Person: Flora D'Souza/Shield Enaineerina. Inc.
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from
Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 5/26/15
FIELD ANALYSES:
WAS
Well Depth: 63ft.
Well Diameter: 4 in.
pH 6.01 units Temp. NM °C
DRY at
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NM µMhos
time of
sampling,
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 5/28/15 - 6/4/15
Laboratory Name: Pace Analytical
Services
Certification No. 12 �\O�
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead 0.0157 mg/I
Coliform: MF Fecal NA /100m1
Nitrate (NOs) as N
NA mg/I
V �4
Zn -Zinc NA mg/ I ..,;111 �Q
�
Coliform: MF Total NA /100mi
Phosphorus: Total as P
NA mg/I
�e
(Notes Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Unitsr
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I
Aliphatic (C05-CO8) = 0.146 mg/I
pH (when analyzed) NA units
Ba - Barium
NA mg/I
Aliphatic (C09-C12) = 0.0649 mg/1
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MAnF=P VPH
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese
NA mg/I
, method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 8.8373 mg/L Effluent Total VOCs: 0.2109 mg/L VOC Removal% 97.6%
Flora D'Souza/Shield Enaineerina. Proiect Manaaer
Pernittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

SI IRMIT;:nPM r1NYFI I OW PAPFR ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
, •
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: Hill Oil Company Inc - Walser's Service
Non -Discharge W00015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Highway 15ON
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Lexinaton NC 27295 County Davidson
❑ Spray Field ® Remediation: GroUndWater
Contact Person: Flora D'Solva/Shield Enalneerana.
Inc. Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
_ No. of wells to be sampled: N_
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
le collected: 5/26/15
Date sample
p
FIELD ANALYSES:
WAS
Well Depth: 63ft.
Well Diameter: _4in.
pH 6.01 units Temp. NM OC
DRY at
time ofsampling,
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63 ft. Spec. Cond. NMµMhos
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES
❑ NO
INFORMATION
LABORATORY
Date sample analyzed: 5/28/15 - 6/4/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead 0.0157 mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100mi
Phosphorus: Total as P
NA mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I
Aliphatic (C05-CO8) = 0.146 mg/1
pH (when analyzed) NA units
Ba - Barium
NA mg/I
Aliphatic (C09-C12) = 0.0649 mg/I
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC , method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MADFP VPH
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 8.8373 mg/L Effluent Total VOCs: U.L I ua mg/L VOC Removal% a 1.0 70
GW-59 Rev.1/2007

APPENDIX A

aceAna1Xica1
www.pacelabs.com
June 08, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: Walser's
Pace Project No.: 92251627
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on May 27, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 26

1�;a'ceAna,(Xical
www-pacelabs.com
Project: Walser's
Pace Project No.: 92251627
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 26

_ , aceAnalytical
www.p"labs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Walser's
92251627
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92251627001
EFF
MADEP VPH
BFW
5
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
92251627002
INF
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 26

_ aceAnalytical
j www.pacelabs.com
Project: Walser's
Pace Project No.: 92251627
Lab Sample ID Client Sample ID
Method Parameters
92251627001
MADEP VPH
MADEP VPH
EPA 200.7
92251627002
MADEP VPH
MADEP VPH
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SM 6200B
SUMMARY OF DETECTION
EFF
Aliphatic (C05-008)
Aliphatic (C09-C12)
Lead
INF
Aliphatic (C05-008)
Aliphatic (C09-C12)
Benzene
Ethylbenzene
Isopropylbenzene (Cumene)
Naphthalene
n-Propylbenzene
Toluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m&p-Xylene
o-Xylene
Result Units
146
64.9
15.7
2350
3340
28.3
159
9.8
119
19.8
1380
191
76.4
729
435
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Report Limit
Analyzed
Qualifiers
50.0
05/28/1516:13
N2
50.0
05/28/1516:13
N2
5.0
05129/1518:57
1000
06/08/1515:51
N2
1000
06/08/1515:51
N2
6.2
06/04/15 22:49
6.2
06/04/15 22:49
6.2
06/04/15 22:49
25.0
06/04/15 22:49
6.2
06/04/15 22:49
6.2
06/04/15 22:49
6.2
06/04/15 22:49
6.2
06/04/15 22:49
12.5
06/04/15 22:49
6.2
06/04/15 22:49
Page 4 of 26

aceAna1Xica1
www.pacelabs.com
PROJECT NARRATIVE
Project: Walser's
Pace Project No.: 92251627
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: June 08, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9419
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1469423)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• EFF (Lab ID: 92251627001)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCS (Lab ID: 1469424)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 26

_ ;aceAnalyficaf'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Walser's
Pace Project No.: 92251627
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: June 08, 2015
Analyte Comments:
QC Batch: GCV/9419
N2: The lab does not hold TNI accreditation for this parameter.
• LCSD (Lab ID: 1469425)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
QC Batch: GCV/9476
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1478885)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
•INF (Lab ID:92251627002)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCS (Lab ID: 1478886)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1478887)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 26

1�;a'ceAnalXical'
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Walser's
Pace Project No.: 92251627
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: June 08, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

Pace Analytical Services, Inc.
aceAnalytical ® 9800 Kincey Ave. Suite100
Huntersville, NC 28078078
www.pacelabs.com
[phone]
PROJECT NARRATIVE
Project: Walser's
Pace Project No.: 92251627
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: June 08, 2015
General Information:
2 samples were analyzed for SM 620013. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/31990
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92251627001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1475541)
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1475542)
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 26

aceAnalytical
/ www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800KinceyAve . Suite100
Huntersville, NC 28078
[phone]
Project: Walser's
Pace Project No.: 92251627
Sample: EFF
Lab ID: 92251627001 Collected:
05/26/15 14:00 Received:
05/27/15 14:56 Matrix:
Water
Parameters
Results
Units Report Limit
DF Prepared
Analyzed
CAS No.
Qual
VPH NC Water
Analytical Method: MADEP VPH
Aliphatic (C05-008)
146
ug/L
50.0
1
05/28/15 16:13
N2
Aliphatic (C09-C12)
64.9
ug/L
50.0
1
05/28/15 16:13
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
05/28/15 16:13
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
101
%
70-130
1
05/28/15 16:13
460-00-4
4-Bromofluorobenzene (PID) (S)
80
%
70-130
1
05/28/15 16:13
460-00-4
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Lead
15.7
ug/L
5.0
1 05/28/1517:30
05/29/1518:57
7439-92-1
6200E MSV
Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
06/04/15 20:36
71-43-2
Bromobenzene
ND
ug/L
0.50
1
06/04/15 20:36
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
06/04/15 20:36
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
06/04/15 20:36
75-27-4
Bromoform
ND
ug/L
0.50
1
06/04/15 20:36
75-25-2
Bromomethane
ND
ug/L
5.0
1
06/04/15 20:36
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
06/04/15 20:36
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
06/04/15 20:36
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/04/15 20:36
75-00-3
Chloroform
ND
ug/L
0.50
1
06/04/15 20:36
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/04/15 20:36
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
06/04/15 20:36
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
06/04/15 20:36
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
06/04/15 20:36
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
06/04/15 20:36
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
06/04/15 20:36
106-93-4
Dibromomethane
ND
ug/L
0.50
1
06/04/15 20:36
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
06/04/15 20:36
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
06/04/15 20:36
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
06/04/15 20:36
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
06/04/15 20:36
75-71-8
M1
1,1-Dichloroethane
ND
ug/L
0.50
1
06/04/15 20:36
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
06/04/15 20:36
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
06/04/15 20:36
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
06/04/15 20:36
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
06/04/15 20:36
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
06/04/15 20:36
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
06/04/15 20:36
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
06/04/15 20:36
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
06/04/15 20:36
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
06/04/15 20:36
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
06/04/15 20:36
10061-02-6
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 06/08/2015 05:26 PM
without the written consent of Pace Analytical
Services, Inc..
Page 9 of 26

Pace Analytical Services, Inc.
® 9800 KinceyAve. Suite 100
aceAnalytical Huntersville, NC 28078
www.pacelabs.com [phone]
i
I
ANALYTICAL RESULTS
Project: Walser's
Pace Project No.: 92251627
Sample: EFF
Lab ID: 92251627001 Collected:
05/26/15 14:00
Received: 05/27/15 14:56 Matrix:
Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Diisopropyl ether
ND
ug/L
0.50
1
06/04/15 20:36
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
06/04/15 20:36
87-68-3 M1
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
06/04/15 20:36
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
06/04/15 20:36
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
06/04/15 20:36
1634-04-4
Naphthalene
ND
ug/L
2.0
1
06/04/15 20:36
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
103-65-1
Styrene
ND
ug/L
0.50
1
06/04/15 20:36
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
06/04/15 20:36
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
06/04/15 20:36
79-34-5
Tetra chloroethene
ND
ug/L
0.50
1
06/04/15 20:36
127-18-4
Toluene
ND
ug/L
0.50
1
06/04/15 20:36
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
06/04/15 20:36
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
06/04/15 20:36
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
06/04/15 20:36
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
06/04/15 20:36
79-00-5
Trichloroethene
ND
ug/L
0.50
1
06/04/15 20:36
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/04/15 20:36
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
06/04/15 20:36
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
06/04/15 20:36
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
06/04/15 20:36
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
06/04/15 20:36
179601-23-1
o-Xylene
ND
ug/L
0.50
1
06/04/15 20:36
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
06/04/15 20:36
17060-07-0
4-Bromofluorobenzene (S)
97
%
70-130
1
06/04/15 20:36
460-00-4
Toluene-d8 (S)
101
%
70-130
1
06/04/15 20:36
2037-26-5
Date: 06/08/2015 05:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 10 of 26

aceAnalyticaI
www.pacelabs.com
ANALYTICAL RESULTS
Project: Walser's
Pace Project No.: 92251627
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: INF Lab ID: 92251627002 Collected: 05/26/15 13:00 Received: 05/27/15 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloroprop ane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 06/08/2015 05:26 PM
Analytical Method: MADEP VPH
2350
ug/L
3340
ug/L
ND
ug/L
95
%
93
%
Analytical Method: SM 6200B
28.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
159
ug/L
ND
ug/L
9.8
ug/L
1000 20
1000 20
1000 20
70-130 20
70-130 20
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
62.5 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
12.5 12.5
6.2 12.5
12.5 12.5
6.2 12.5
6.2 12.5
12.5 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
6.2 12.5
25.0 12.5
6.2 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
06/08/15 15:51
O6/08/15 15:51
06/08/15 15:51
O6/08/15 15:51 460-00-4
06/08/15 15:51 460-00-4
O6/04/15 22:49
71-43-2
06/04/15 22:49
108-86-1
06/04/15 22:49
74-97-5
06/04/15 22:49
75-27-4
06/04/15 22:49
75-25-2
O6/04/15 22:49
74-83-9
O6/04/15 22:49
104-51-8
06/04/15 22:49
135-98-8
06/04/15 22:49
98-06-6
O6/04/15 22:49
56-23-5
O6/04/15 22:49
108-90-7
06/04/15 22:49
75-00-3
06/04/15 22:49
67-66-3
06/04/15 22:49
74-87-3
O6/04/15 22:49
95-49-8
O6/04/15 22:49
106-43-4
06/04/15 22:49
96-12-8
06/04/15 22:49
124-48-1
O6/04/15 22:49
106-93-4
06/04/15 22:49
74-95-3
O6/04/15 22:49
95-50-1
O6/04/15 22:49
541-73-1
06/04/15 22:49
106-46-7
06/04/15 22:49
75-71-8
O6/04/15 22:49
75-34-3
06/04/15 22:49
107-06-2
06/04/15 22:49
75-35-4
06/04/15 22:49
156-59-2
06/04/15 22:49
156-60-5
06/04/15 22:49
78-87-5
06/04/15 22:49
142-28-9
06/04/15 22:49
594-20-7
06/04/15 22:49
563-58-6
06/04/15 22:49
10061-01-5
O6/04/15 22:49
10061-02-6
06/04/15 22:49
108-20-3
06/04/15 22:49
100-41-4
06/04/15 22:49
87-68-3
06/04/15 22:49
98-82-8
N2
N2
N2
Page 11 of 26

�-;aceAnalyfica(
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Walser's
Pace Project No.: 92251627
Sample: INF Lab ID: 92251627002 Collected: 05/26/15 13:00 Received: 05/27/15 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Methylene Chloride
ND
ug/L
25.0
12.5
06/04/15 22:49
75-09-2
Methyl-tert-butyl ether
ND
ug/L
6.2
12.5
06/04/15 22:49
1634-04-4
Naphthalene
119
ug/L
25.0
12.5
06/04/15 22:49
91-20-3
n-Propylbenzene
19.8
ug/L
6.2
12.5
06/04/15 22:49
103-65-1
Styrene
ND
ug/L
6.2
12.5
06/04/15 22:49
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
6.2
12.5
06/04/15 22:49
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
6.2
12.5
06/04/15 22:49
79-34-5
Tetrachloroethene
ND
ug/L
6.2
12.5
06/04/15 22:49
127-18-4
Toluene
1380
ug/L
6.2
12.5
06/04/15 22:49
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
25.0
12.5
06/04/15 22:49
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
25.0
12.5
06/04/15 22:49
120-82-1
1,1,1-Trichloroethane
ND
ug/L
6.2
12.5
06/04/15 22:49
71-55-6
1,1,2-Trichloroethane
ND
ug/L
6.2
12.5
06/04/15 22:49
79-00-5
Trichloroethene
ND
ug/L
6.2
12.5
06/04/15 22:49
79-01-6
Trichlorofluoromethane
ND
ug/L
12.5
12.5
06/04/15 22:49
75-69-4
1,2,3-Trichloropropane
ND
ug/L
6.2
12.5
06/04/15 22:49
96-18-4
1,2,4-Trimethylbenzene
191
ug/L
6.2
12.5
06/04/15 22:49
95-63-6
1,3,5-Trimethylbenzene
76.4
ug/L
6.2
12.5
06/04/15 22:49
108-67-8
Vinyl chloride
ND
ug/L
12.5
12.5
06/04/15 22:49
75-01-4
m&p-Xylene
729
ug/L
12.5
12.5
06/04/15 22:49
179601-23-1
o-Xylene
435
ug/L
6.2
12.5
06/04/15 22:49
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
103
%
70-130
12.5
06/04/15 22:49
17060-07-0
4-Bromofluorobenzene (S)
96
%
70-130
12.5
06/04/15 22:49
460-00-4
Toluene-d8 (S)
100
%
70-130
12.5
06/04/15 22:49
2037-26-5
Date: 06/08/2015 05:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 26

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Project:
Walser's
Pace Project No.:
92251627
QC Batch:
GCV/9419 Analysis Method: MADEP VPH
QC Batch Method:
MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92251627001
METHOD BLANK: 1469423
Matrix:
Water
Associated Lab Samples: 92251627001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
ug/L
ND
50.0
05/28/15 20:12 N2
Aliphatic (C09-C12)
ug/L
ND
50.0
05/28/15 20:12 N2
Aromatic (C09-C10)
ug/L
ND
50.0
05/28/15 20:12 N2
4-Bromofluorobenzene (FID) (S)
%
105
70-130
05/28/15 20:12
4-Bromofluorobenzene (PID) (S)
%
80
70-130
05/28/15 20:12
LABORATORY CONTROL SAMPLE & LCSD:
1469424
Spike
Parameter
Units
Conc.
Aliphatic (C05-008)
ug/L
300
Aliphatic (C09-C12)
ug/L
300
Aromatic (C09-C10)
ug/L
100
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
1469425
LCS
LCSD
LCS
LCSD
% Rec Max
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
321
323
107
108
70-130 0 25 N2
277
278
92
93
30-130 0 25 N2
74.2
73.7
74
74
70-130 1 25 N2
106
100
70-130
84
79
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 26

aceAnalytical
www.pacelabs.com
Project: Walser's
Pace Project No.: 92251627
QC Batch: GCV/9476
QC Batch Method: MADEP VPH
Associated Lab Samples: 92251627002
METHOD BLANK: 1478885
Associated Lab Samples: 92251627002
Parameter
Units
Aliphatic (C05-008)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
QUALITY CONTROL DATA
Analysis Method: MADEP VPH
Analysis Description: VPH NC Water
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ND
50.0
06/08/1515:25 N2
ND
50.0
06/08/1515:25 N2
ND
50.0
06/08/1515:25 N2
98
70-130
06/08/1515:25
96
70-130
06/08/1515:25
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
1478886
1478887
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-008)
ug/L
300
290 279
97
93
70-130 4 25 N2
Aliphatic (C09-C12)
ug/L
300
275 266
92
89
30-130 3 25 N2
Aromatic (C09-C10)
ug/L
100
92.9 89.1
93
89
70-130 4 25 N2
4-Bromofluorobenzene (FID) (S)
%
104
100
70-130
4-Bromofluorobenzene (PID) (S)
%
105
101
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 26

;a'cceAnalyficalo
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walser's
Pace Project No.: 92251627
QC Batch: MPRP/18566 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92251627001
METHOD BLANK: 1469956 Matrix: Water
Associated Lab Samples: 92251627001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 05/29/1518:08
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1469957
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 476 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1469958 1469959
MS MSD
92251441001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 475 479 95 96 70-130 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1469960 1469961
MS MSD
92251714002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 452 445 90 89 70-130 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc . Page 15 of 26

aceAna lytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walser's
Pace Project No.: 92251627
QC Batch: MSV/31990 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Associated Lab Samples: 92251627001, 92251627002
METHOD BLANK: 1475539
Associated Lab Samples: 92251627001, 92251627002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
06/04/15 19:13
1,1,1-Trichloroethane
ug/L
ND
0.50
06/04/15 19:13
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
06/04/15 19:13
1,1,2-Trichloroethane
ug/L
ND
0.50
06/04/15 19:13
1,1-Dichloroethane
ug/L
ND
0.50
06/0411519:13
1,1-Dichloroethene
ug/L
ND
0.50
06104/1519:13
1,1-Dichloropropene
ug/L
ND
0.50
06/04/15 19:13
1,2,3-Trichlorobenzene
ug/L
ND
2.0
06/04/15 19:13
1,2,3-Trichloropropane
ug/L
ND
0.50
06/04/15 19:13
1,2,4-Trichlorobenzene
ug/L
ND
2.0
06/04/15 19:13
1,2,4-Trimethylbenzene
ug/L
ND
0.50
06/04/15 19:13
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
06/04/15 19:13
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
06/04/15 19:13
1,2-Dichlorobenzene
ug/L
ND
0.50
06/04/15 19:13
1,2-Dichloroethane
ug/L
ND
0.50
06/04/15 19:13
1,2-Dichloropropane
ug/L
ND
0.50
06/04/15 19:13
1,3,5-Trimethylbenzene
ug/L
ND
0.50
06/04/15 19:13
1,3-Dichlorobenzene
ug/L
ND
0.50
06/04/15 19:13
1,3-Dichloropropane
ug/L
ND
0.50
06/04/15 19:13
1,4-Dichlorobenzene
ug/L
ND
0.50
06/04/15 19:13
2,2-Dichloropropane
ug/L
ND
0.50
06/04/15 19:13
2-Chlorotoluene
ug/L
ND
0.50
06/0411519:13
4-Chlorotoluene
ug/L
ND
0.50
06/04/15 19:13
Benzene
ug/L
ND
0.50
06/04/15 19:13
Bromobenzene
ug/L
ND
0.50
06/0411519:13
Bromochloromethane
ug/L
ND
0.50
06/04/15 19:13
Bromodichloromethane
ug/L
ND
0.50
06/04/15 19:13
Bromoform
ug/L
ND
0.50
06/04/15 19:13
Bromomethane
ug/L
ND
5.0
06/04/15 19:13
Carbon tetrachloride
ug/L
ND
0.50
06/04/15 19:13
Chlorobenzene
ug/L
ND
0.50
06/04/15 19:13
Chloroethane
ug/L
ND
1.0
06/04/15 19:13
Chloroform
ug/L
ND
0.50
06/04/15 19:13
Chloromethane
ug/L
ND
1.0
06/04/15 19:13
cis-1,2-Dichloroethene
ug/L
ND
0.50
06/04/15 19:13
cis-1,3-Dichloropropene
ug/L
ND
0.50
06/04/15 19:13
Dibromochloromethane
ug/L
ND
0.50
06/04/15 19:13
Dibromomethane
ug/L
ND
0.50
06/04/15 19:13
Dichlorodifluoromethane
ug/L
ND
0.50
06/04/15 19:13
Diisopropyl ether
ug/L
ND
0.50
06/04/15 19:13
Ethylbenzene
ug/L
ND
0.50
06/0411519:13
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc..
Page 16 of 26

11!;a'ce Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walser's
Pace Project No.: 92251627
METHOD BLANK: 1475539
Matrix:
Water
Associated Lab Samples: 92251627001, 92251627002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
06/04/15 19:13
Isopropylbenzene (Cumene)
ug/L
ND
0.50
06/04/15 19:13
m&p-Xylene
ug/L
ND
1.0
06/04/15 19:13
Methyl-tert-butyl ether
ug/L
ND
0.50
06/04/15 19:13
Methylene Chloride
ug/L
ND
2.0
06/04/15 19:13
n-Butylbenzene
ug/L
ND
0.50
06/04/15 19:13
n-Propylbenzene
ug/L
ND
0.50
06/04/15 19:13
Naphthalene
ug/L
ND
2.0
06/04/15 19:13
o-Xylene
ug/L
ND
0.50
06/04/15 19:13
sec-Butylbenzene
ug/L
ND
0.50
06/04/15 19:13
Styrene
ug/L
ND
0.50
06104/1519:13
tert-Butylbenzene
ug/L
ND
0.50
06/04/15 19:13
Tetra chloroethene
ug/L
ND
0.50
06/04/1519:13
Toluene
ug/L
ND
0.50
06/04/15 19:13
trans-1,2-Dichloroethene
ug/L
ND
0.50
06/04/15 19:13
trans-1,3-Dichloropropene
ug/L
ND
0.50
06/04/15 19:13
Trichloroethene
ug/L
ND
0.50
06/04/15 19:13
Trichlorofluoromethane
ug/L
ND
1.0
06/04/15 19:13
Vinyl chloride
ug/L
ND
1.0
06/04/15 19:13
1,2-Dichloroethane-d4 (S)
%
98
70-130
06/04/15 19:13
4-Bromofluorobenzene (S)
%
103
70-130
06/04/15 19:13
Toluene-d8 (S)
%
100
70-130
06/04/15 19:13
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1475540
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
60-140
1,1,1-Trichloroethane
ug/L
50
50.6
101
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
53.6
107
60-140
1,1,2-Trichloroethane
ug/L
50
50.2
100
60-140
1,1-Dichloroethane
ug/L
50
50.0
100
60-140
1,1-Dichloroethene
ug/L
50
46.5
93
60-140
1,1-Dichloropropene
ug/L
50
53.1
106
60-140
1,2,3-Trichlorobenzene
ug/L
50
48.4
97
60-140
1,2,3-Trichloropropane
ug/L
50
52.9
106
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.9
100
60-140
1,2,4-Trimethylbenzene
ug/L
50
47.9
96
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
49.9
100
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.9
108
60-140
1.2-Dichlorobe nzene
ug/L
50
52.2
104
60-140
1,2-Dichloroethane
ug/L
50
48.1
96
60-140
1,2-Dichloropropane
ug/L
50
49.1
98
60-140
1,3,5-Trimethylbenzene
ug/L
50
47.7
95
60-140
1,3-Dichlorobenzene
ug/L
50
48.8
98
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 26

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walser's
Pace Project No.: 92251627
LABORATORY CONTROL SAMPLE:
1475540
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,3-Dichloropropane
ug/L
50
50.3
101
60-140
1,4-Dichlorobenzene
ug/L
50
48.9
98
60-140
2,2-Dichloropropane
ug/L
50
51.6
103
60-140
2-Chlorotoluene
ug/L
50
47.9
96
60-140
4-Chlorotoluene
ug/L
50
47.8
96
60-140
Benzene
ug/L
50
47.8
96
60-140
Bromobenzene
ug/L
50
47.1
94
60-140
Bromochloromethane
ug/L
50
54.3
109
60-140
Bromodichloromethane
ug/L
50
53.6
107
60-140
Bromoform
ug/L
50
44.4
89
60-140
Bromomethane
ug/L
50
55.9
112
60-140
Carbon tetrachloride
ug/L
50
62.8
126
60-140
Chlorobenzene
ug/L
50
49.5
99
60-140
Chloroethane
ug/L
50
47.9
96
60-140
Chloroform
ug/L
50
46.2
92
60-140
Chloromethane
ug/L
50
51.8
104
60-140
cis- 1,2-Dichloroethene
ug/L
50
51.0
102
60-140
cis-1,3-Dichloropropene
ug/L
50
56.6
113
60-140
Dibromochloromethane
ug/L
50
43.4
87
60-140
Dibromomethane
ug/L
50
53.0
106
60-140
Dichlorodifluoromethane
ug/L
50
55.4
111
60-140
Diisopropyl ether
ug/L
50
49.8
100
60-140
Ethylbenzene
ug/L
50
46.0
92
60-140
Hexachloro-1,3-butadiene
ug/L
50
52.8
106
60-140
Isopropylbenzene (Cumene)
ug/L
50
51.1
102
60-140
map-Xylene
ug/L
100
90.5
90
60-140
Methyl-tert-butyl ether
ug/L
50
48.6
97
60-140
Methylene Chloride
ug/L
50
53.2
106
60-140
n-Butylbenzene
ug/L
50
49.2
98
60-140
n-Propylbenzene
ug/L
50
44.3
89
60-140
Naphthalene
ug/L
50
52.3
105
60-140
o-Xylene
ug/L
50
48.0
96
60-140
sec-Butylbenzene
ug/L
50
49.5
99
60-140
Styrene
ug/L
50
55.5
111
60-140
tert-Butylbenzene
ug/L
50
41.6
83
60-140
Tetrachloroethene
ug/L
50
46.3
93
60-140
Toluene
ug/L
50
49.2
98
60-140
trans-1,2-Dichloroethene
ug/L
50
46.7
93
60-140
trans-1,3-Dichloropropene
ug/L
50
58.1
116
60-140
Trichloroethene
ug/L
50
46.8
94
60-140
Trichlorofluoromethane
ug/L
50
45.7
91
60-140
Vinyl chloride
ug/L
50
47.1
94
60-140
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
95
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate until Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 26

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Walser's
Pace Project No.: 92251627
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1475541
1475542
MS
MSD
92251627001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
18.8
20.8
94
104
60-140
10
1,1,1-Trichloroethane
ug/L
ND
20
20
22.5
24.7
113
124
60-140
9
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
24.7
24.5
123
122
60-140
1
1,1,2-Trichloroethane
ug/L
ND
20
20
22.5
23.3
113
116
60-140
3
1,1-Dichloroethane
ug/L
ND
20
20
23.1
24.5
115
122
60-140
6
1,1-Dichloroethene
ug/L
ND
20
20
22.7
24.3
114
121
60-140
7
1,1-Dichloropropene
ug/L
ND
20
20
25.4
27.1
127
135
60-140
6
1,2,3-Trichlorobenzene
ug/L
ND
20
20
22.5
21.4
112
107
60-140
5
1,2,3-Trichloropropane
ug/L
ND
20
20
22.9
22.0
115
110
60-140
4
1,2,4-Trichlorobe nzene
ug/L
ND
20
20
22.2
21.9
111
109
60-140
1
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.0
22.5
109
112
60-140
2
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.4
20.0
102
100
60-140
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.3
22.8
116
114
60-140
2
1,2-Dichlorobenzene
ug/L
ND
20
20
22.9
23.5
115
117
60-140
2
1,2-Dichloroethane
ug/L
ND
20
20
21.8
22.5
109
112
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
23.2
23.7
116
119
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
22.2
23.1
111
116
60-140
4
1,3-Dichlorobenzene
ug/L
ND
20
20
21.5
22.2
108
111
60-140
3
1,3-Dichloropropane
ug/L
ND
20
20
23.2
23.0
116
115
60-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
22.1
23.1
111
115
60-140
4
2,2-Dichloropropane
ug/L
ND
20
20
19.7
21.7
98
108
60-140
10
2-Chlorotoluene
ug/L
ND
20
20
22.4
23.9
112
119
60-140
6
4-Chlorotoluene
ug/L
ND
20
20
22.6
23.6
113
118
60-140
4
Benzene
ug/L
ND
20
20
22.0
22.9
108
112
60-140
4
Bromobenzene
ug/L
ND
20
20
22.2
22.7
111
113
60-140
2
Bromochloromethane
ug/L
ND
20
20
23.6
25.0
118
125
60-140
6
Bromodichloromethane
ug/L
ND
20
20
20.6
22.7
103
114
60-140
10
Bromoform
ug/L
ND
20
20
15.9
16.8
79
84
60-140
6
Bromomethane
ug/L
ND
20
20
19.1
22.6
95
113
60-140
17
Carbon tetrachloride
ug/L
ND
20
20
23.8
27.4
119
137
60-140
14
Chlorobenzene
ug/L
ND
20
20
22.4
23.0
112
115
60-140
3
Chloroethane
ug/L
ND
20
20
24.4
27.0
122
135
60-140
10
Chloroform
ug/L
ND
20
20
21.2
22.2
106
111
60-140
5
Chloromethane
ug/L
ND
20
20
25.7
27.3
129
136
60-140
6
cis-1,2-Dichloroethene
ug/L
ND
20
20
23.2
24.8
116
124
60-140
6
cis- 1,3-Dichloropropene
ug/L
ND
20
20
21.5
23.2
107
116
60-140
8
Dibromochloromethane
ug/L
ND
20
20
16.9
17.9
85
89
60-140
5
Dibromomethane
ug/L
ND
20
20
22.0
22.6
110
113
60-140
3
Dichlorodifluoromethane
ug/L
ND
20
20
29.6
31.2
148
156
60-140
5 M1
Diisopropyl ether
ug/L
ND
20
20
22.8
24.1
114
120
60-140
6
Ethylbenzene
ug/L
ND
20
20
21.2
22.2
105
110
60-140
4
Hexachloro-1,3-butadiene
ug/L
ND
20
20
28.2
30.2
141
151
60-140
7 M1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
22.6
23.6
113
118
60-140
4
m&p-Xylene
ug/L
ND
40
40
41.6
43.2
103
107
60-140
4
Methyl-tert-butyl ether
ug/L
ND
20
20
20.9
21.8
105
109
60-140
4
Methylene Chloride
ug/L
ND
20
20
23.6
25.8
118
129
60-140
9
Results presented on this page are in the units indicated by the
"Units" column except where an alternate unit is presented
to the right
of the result.
REPORT
OF
LABORATORY
ANALYSIS
This
report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM
without
the written consent of Pace Analytical
Services, Inc..
Page 19 of 26

/7;a'ce
Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walser's
Pace Project No.: 92251627
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1475541
MS
92251627001
Spike
Parameter
Units
Result
Conc.
n-Butylbenzene
ug/L
ND
20
n-Propylbenzene
ug/L
ND
20
Naphthalene
ug/L
ND
20
o-Xylene
ug/L
ND
20
sec- Butyl benzene
ug/L
ND
20
Styrene
ug/L
ND
20
tert-Butylbenzene
ug/L
ND
20
Tetrachloroethene
ug/L
ND
20
Toluene
ug/L
ND
20
trans- l,2-Dichloroethene
ug/L
ND
20
trans-1,3-Dichloropropene
ug/L
ND
20
Trichloroethene
ug/L
ND
20
Trichlorofluoromethane
ug/L
ND
20
Vinyl chloride
ug/L
ND
20
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MSD
Spike
Conc.
1475542
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
20
21.5
23.4
107
117
60-140
8
20
21.4
22.3
107
111
60-140
4
20
26.5
22.9
133
114
60-140
15
20
21.4
22.0
107
110
60-140
2
20
22.8
24.4
114
122
60-140
7
20
23.9
24.5
119
123
60-140
3
20
19.0
20.5
95
102
60-140
8
20
21.3
22.2
106
111
60-140
5
20
22.9
24.1
114
121
60-140
5
20
22.5
23.7
112
119
60-140
5
20
21.4
22.8
107
114
60-140
6
20
21.0
22.0
105
110
60-140
5
20
23.4
24.8
117
124
60-140
6
20
24.2
25.4
121
127
60-140
5
99
103
70-130
99
99
70-130
100
99
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 20 of 26

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: Walser's
Pace Project No.: 92251627
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 26

1�;a'ce AnalXical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huniersville, NC 28078
[phone]
Project:
Pace Project No.:
Walser's
92251627
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92251627001
EFF
MADEP VPH
GCV/9419
92251627002
INF
MADEP VPH
GCV/9476
92251627001
EFF
EPA 200.7
MPRP/18566 EPA 200.7 ICP/16654
92251627001
EFF
SM 6200B
MSV/31990
92251627002
INF
SM 6200B
MSV/31990
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/08/2015 05:26 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 26

• �P��ceAn��lytical'
Sample Condition Upon Recell
Document Number:
F-CHR-CS-003-rev.16
Client Name: ��G, , e 1,1
CUR Page 1 of 2` _
Issuing Authority:
Pace Huntersville Qualitv Office
Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Co mrfcial❑ ace Other
Custody Seal on Cooler/Box Present: ❑ ye no Seals intact: Elyes Elno
Packing Material: ❑ Bubble VQp Bubble Bags ❑ None Other
l
Thermometer Used: IR Gun r4l
Type of Ice W Blue None amples on ice, cooling process has begun
Temp Correction Factor To Correction
Corrected Cooler Temp.: D'S •C
Biological Tissue is Frozen: Yes No
Iq
Date and Initialg (gipe
J , r�rr eg _mi In
contents; %J o!
Temp should be above freezing to 6°C
Comments:
Chain of Custody❑ Present:
es e- ❑NIA
1.
Chain of Custody Filled Out:
04s fQo ❑N/A
2.
Chain of Custody Relinquished:
es No ❑N/A
3.
Sampler Name & Signature on COC:
es ao— ❑NIA
4,
Samples Arrived within Hold Time:
81es []No ClWk,5.
Short Hold Time Analysis <72hr):
OYes o 0_10K
6.
Rush Turn Around Time Requested:
❑Yes ❑N!A
7.
Sufficient Volume:
a es m-. ON/A
g.
Correct Containers Used:
es o ONIA
g.
-Pace Containers Used:
❑Yes o ONIA
Containers Intact:
ElYes ❑No ❑N/A
1
Filtered volume received for Dissolved tests
❑Yes
Sample Labels match COC:
es ONo ❑NIA
12.
-Includes date/time/ID/Analysis Matrix:
All contalners needing preservation have been checked.
❑Yes o/❑NIA
13,
All containers needing preservation are found to be in
❑Yes t�O ONIA
compliance with EPA recommendation.
exceptlons: VOA, coliform, TOC, O&G, WI-DRO (water)
Yes ONo
Samples checked for dechlorination:
❑Yes ❑No rA
14.
Headspace in VOA Vials >6mm :
❑Yes o N/A
Trip Blank Present:
OYes ONo Q /A
Trip Blank Custody Seals Present
Oyes ❑No ❑ IA
Pace Trip Blank Lot # if purchased):,-..,,, - -
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: kc I Date; I W®# : 92251627
SRF Review: �/` Date; I 5A451
Note: Whenever there is a d screpancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR 92251627
Certification Office ( i,e out of hold, incorrect preservative, out of temp,
Incorrect containers)
Page 23 of 26

CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Pa e : 1 Of 1
Company: Shield
Report To: Flora O'Souza
Attention:
Address: 4301 Taggart Creek Road
Copy To:
Company Name:
Charlotte. NC 28208
Address:
Regulatory
Ema11-. fdsouza shieldergineering.com
Purchase Order T:
Pace Quote:
Phone: [phone] Fax
Pror,,ect Name: Walser's
Pace Project Manager, laura.coop pacelaos.com,
State I Location
Requested Due Date:
Project, #:
Pace Profile #: ' ' t1 - j
NC
Requested
Analysis
Fill
red
IN
a
Z
MATRIX CODE
COLLECTED
o
Preservatives
}
D-" Water Dw
Watat WT
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waste WNaI Ww
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One Character per box. W'w WP
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(A-Z, 0-9 / . •) Duct OT
sample Ids must be unique T.— Ts
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6
7
8
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ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONOMONS
! �QQ
�TIIME�
SAMPLER NAME AND SIGNATURE
c
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PRINT Name of SAMPLER:
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SIGNATURE of SAMPLER:
DATE Signed:
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F��ceAn��Iyflcai• Sample Condition Upon Recei
Document Number:
F-CHR-CS-003-rev.16
Client Name:
Page 1 of 2* _
Issuing Authority:
Pace Huntersville Quality Office
* Page 2 of 2 Is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Co m6r-cial❑ ace Other
Custody Seal on Cooler/Box Present: ❑ ye no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble VDp Bubble Bags ❑ Noneja Other
l
Thermometer Used: IR Gun 140 Type of Ice W Blue None amples on ice, cooling process has begun
TPmn r nrrPCtinn Factor T1401 No Correction
Corrected Cooler Temp.: �'� •C
Temp should be above freezing to 6*C
Biological Tissue is Frozen: Yes No /A
Comments:
Date and Initlaj� gLper n ejc�mirtI
contents: ?f T- �'
Chain of Custody Present:
0 es
ON/A
1.
Chain of Custody Filled Out:
es g-/
ON/A
2,
Chain of Custody Relinquished:
14 es No
❑N/A
3.
Sampler Name & Signature on COC:
t4s fqo—
C7N/A
4.
Samples Arrived within Hold Time:
es [:]No
5.
Short Hold Time Analysis <72hr :
OYes o
O
6.
Rush Turn Around Time Requested:
OYes
ON/A
7.
Sufficient Volume:
es Qed
ON/A
8.
Correct Containers Used:
-Pace Containers Used:
es o
❑Yea �00
❑NIA
N/A
9,
Containers Intact:
Yes ❑No
O /A
1
Filtered volume received for Dissolved tests
Dyes o
Q /A
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
es ❑No
❑N/A
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes Floc ON/A
Oyes 0 ON/A
Yes ONo
13.
Samples checked for dechlorination:
❑Yes ONo
/A
14.
Heads ace in VOA Vials (>6mm):
❑Yes o
❑N/A
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # if purchased):
❑Yes ONo
❑Yes ❑No
R /A
❑ /A
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: DatelTime:
Comments/ Resolution:
SCURF Review: kc Date: �`�� W®# : 92251627
SRF Review: I I Date: 25
Note: Whenever there is a d screpancy affecting North Carolina compliance �I I II" II I'I'I I I III �II
samples, a copy of this form will be sent to the North Carolina DEHNR E12251627
Certification Office ( i.e out of hold, Incorrect preservative, out of temp,
Incorrect containers)
Page 25 of 26

CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Irtfornation: Pa e : 1 01 7
Company. Shield Report To. Flora D'Souza Attention:
Address: 4307 Taggart Creek Road Copy To: Company Name:
Charlotte, NC 2820E
Address:
R69ulartoryAgency
Email: fdsouza shieldengineering.com
Purchase Order #:
Page Quote:
I
Phone: [phone] lFax
Project Name: Walsees
Pace Project Manager laura.wopor pacelabs.com,
State I Location
Requested Due Date:
Project #:
Pace Profile It
NC
Requested
Analysis
Mltorad
/N
a
�
Z
tsarRuc cone
o
0
COLLECTED
o
Preservatives
}
N-9 Wager DW
W— WT
Wasi.Wal.r VA,=
m
s
O
V
Z
PAW— P
SAMPLE ID sa9sab SL
oa OL
()
START
END
O
V
w
o
One Character per box. W." WP
o
a
a
e
o
m
Sample Ids must be unique T.... Ts
x
n
U
o
p
x
c
m
=
'
a
`a
o
zz
DATE
TIME
DATE
TIME
m
=>=
x
x
z
z
2
0
f
1
EFF
WT
I
`"l
x
x
x
/v 1
2
INF
WT
�j"
I+
x
x
3
4
5
6
7
8
9
10
11
12
ADDIMONALCOMMENTS
RELINQUISHED BY/AFFILIATION
DATE
TIME
ACCEPTED BY/AFFILIATION
DATE
TIME
SAMPLE CONDEMNS
ll
SAMPLER NAME AND SIGNATURE
cc
U
PRINT Name of SAMPLER:
` y 3�
5
0
'^
,
o e?
m y
m m
SIGNATURE of SAMPLER:
DATE Signed:
I `1

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT &NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiratign Date: 1/31/2018
Facility Name: HIII Oil Company, Inc. - Walser's Service
Non -Discharge W00015102 C
Permit Name (if different):
NPDES
Facility Address: 6419 North Carolina HiahwaV 150N
lljOther
TYPE OF�RFgm) -OPERATION BEING MONITORED
Lexnoton NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ® Remediation: GroUndWater
Contact Person: Flora D'Souza/Shield Enaineerina.
Inc. Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name. Walser's Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 3/25/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: _4 in.
pH 5.98 units Temp. NM OC
DRY at
Depth to Water Level: ft. below measuring point
�M 9 P
Screened Interval: 33 ft.
to 63
ft. Sec. Cond. µ
p NM Mhos
time of
sampling,
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/30/15 - 4/03/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
n'q
2-
COD NA mg/I
Nitrite (NO2) as IN
NA rrWY U 5 Lead lab lost sample mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100m1
Phosphorus: Total as P
NA mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/1
Al - Aluminum
NA mg/I
Aliphatics (C05-008) = 0.118 m9/1
pH (when analyzed) NA units
Ba - Barium
NA mg/I
Aliphatic (C09-C-12) = 0.0563 mg/1
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Lab notified us of lost lead sample on 4/6/15
Arsenic NA mg/1
Chromium: Total
NA mg/I
Grease and Oils NA mg/1
Cu - Copper
NIA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/1
Mg - Magnesium
NA mg/I
VPH method # MAnFP VPH
(Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 8.8334 mg/L Effluent Total VOCs: 0.1743 mg/L VOC Removal% 98%
Flora D'Souza/Shield Enaineerina. Proiect Manaaer
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
so
MAY 2 4 2015

APPENDIX A

aceAnalytical
j www.pacelabs.com
April 17, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: Walsers
Pace Project No.: 92242825
Dear Ms. D'Souza:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 26, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Revised report issued on 4/17/15 to note missing metals result for sample 002.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 21

17;a'ce Analytical
www.pacelabs.com
i
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Walsers
Pace Project No.: 92242825
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 21

aceAnalytical
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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Walsers
92242825
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92242825001
Influent
MADEP VPH
BFW
5
PASI-C
SM 62006
CAH
63
PASI-C
92242826002
Effluent
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 21

1�;a'ce Analytical
www.pacelabs.com
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Walsers
92242825
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92242826001
Influent
MADEP VPH
Aliphatic (C05-008)
2230
ug/L
500
03/30/15 18:48
N2
MADEP VPH
Aliphatic (C09-C12)
3540
ug/L
500
03/30/15 18:48
N2
MADEP VPH
Aromatic (C09-C10)
615
ug/L
500
03/30/15 18:48
N2
SM 6200B
Benzene
19.3
ug/L
5.0
04/03/15 08:11
SM 6200B
Ethylbenzene
117
ug/L
5.0
04/03/15 08:11
SM 6200B
Isopropylbenzene (Cumene)
7.4
ug/L
5.0
04/03/15 08:11
SM 6200B
Methylene Chloride
28.4
ug/L
20.0
04/03/15 08:11
SM 6200B
Naphthalene
130
ug/L
20.0
04/03/15 08:11
SM 6200B
n-Propylbenzene
16.8
ug/L
5.0
04/03/15 08:11
SM 6200B
Toluene
807
ug/L
5.0
04/03/15 08:11
SM 6200B
1,2,4-Trimethylbenzene
210
ug/L
5.0
04/03/15 08:11
SM 6200B
1,3,5-Trimethylbenzene
82.5
ug/L
5.0
04/03/15 08:11
SM 6200B
m&p-Xylene
662
ug/L
10.0
04/03/15 08:11
SM 6200B
o-Xylene
368
ug/L
5.0
04/03/15 08:11
92242825002
Effluent
MADEP VPH
Aliphatic (C05-008)
118
ug/L
50.0
03/30/15 19:15
N2
MADEP VPH
Aliphatic (C09-C12)
56.3
ug/L
50.0
03/30/15 19:15
N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 21

1�;ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: Walsers
Pace Project No.: 92242825
Date: April 17, 2015
Effluent (Lab ID:92242825002)
• Due to laboratory error, no metals data is available to report for this sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 21

_ ;a'ce Analytical
www.pacelabs.com
PROJECT NARRATIVE
Project: Walsers
Pace Project No.: 92242825
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: April 17, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9135
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1422198)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• Effluent (Lab ID: 92242825002)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• Influent (Lab ID: 92242825001)
• Aliphatic (C05-008)
• Aliphatic (C09-1312)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 21

Pace Analytical Services, Inc.
aceAnalytical ® 9800 Kincey Ave. Suite Huntersville, NC 28078078
www.pacelabs.com [phone]
i
PROJECT NARRATIVE
Project: Walsers
Pace Project No.: 92242825
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: April 17, 2015
Analyte Comments
QC Batch: GCV/9135
N2: The lab does not hold TNI accreditation for this parameter.
• LCS (Lab ID: 1422199)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1422200)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 21

7 0
Pace Analytical Services, Inc.
aceAnalytical 9800 Kiney Ave. Suite 100
Huntersviile, NC 28078078
% www.pacelabs.com [phone]
i
PROJECT NARRATIVE
Project: Walsers
Pace Project No.: 92242825
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: April 17, 2015
General Information:
2 samples were analyzed for SM 62006. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/31032
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92242825002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1425933)
• Bromomethane
• MSD (Lab ID: 1425934)
• Bromomethane
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 21

1�;a ce AnalXical
www.pacelabs.com
r
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Walsers
Pace Project No.: 92242825
Sample: Influent Lab ID: 92242825001 Collected: 03/25/15 13:00 Received: 03/26/15 10.58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobe nzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
Isopropylbenzene (Cumene)
Date: 04/17/2015 04:10 PM
Analytical Method: MADEP VPH
2230
ug/L
3540
ug/L
615
ug/L
97
%
93
%
Analytical Method:
SM 6200B
19.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
117
ug/L
ND
ug/L
7.4
ug/L
500
10
03/30/15 18:48
500
10
03/30/15 18:48
500
10
03/30/15 18:48
70-130
10
03/30/15 18:48
460-00-4
70-130
10
03/30/15 18:48
460-00-4
5.0
10
04/03/15 08:11
71-43-2
5.0
10
04/03/15 08:11
108-86-1
5.0
10
04/03/15 08:11
74-97-5
5.0
10
04/03/15 08:11
75-27-4
5.0
10
04/03/15 08:11
75-25-2
50.0
10
04/03/15 08:11
74-83-9
5.0
10
04/03/15 08:11
104-51-8
5.0
10
04/03/15 08:11
135-98-8
5.0
10
04/03/15 08:11
98-06-6
5.0
10
04/03/15 08:11
56-23-5
5.0
10
04/03/15 08:11
108-90-7
10.0
10
04/03/15 08:11
75-00-3
5.0
10
04/03/15 08:11
67-66-3
10.0
10
04/03/15 08:11
74-87-3
5.0
10
04/03/15 08:11
95-49-8
5.0
10
04/03/15 08:11
106-43-4
10.0
10
04/03/15 08:11
96-12-8
5.0
10
04/03/15 08:11
124-48-1
5.0
10
04/03/15 08:11
106-93-4
5.0
10
04/03/15 08:11
74-95-3
5.0
10
04/03/15 08:11
95-50-1
5.0
10
04/03/15 08:11
541-73-1
5.0
10
04/03/15 08:11
106-46-7
5.0
10
04/03/15 08:11
75-71-8
5.0
10
04/03/15 08:11
75-34-3
5.0
10
04/03/15 08:11
107-06-2
5.0
10
04/03/15 08:11
75-35-4
5.0
10
04/03/15 08:11
156-59-2
5.0
10
04/03/15 08:11
156-60-5
5.0
10
04/03/15 08:11
78-87-5
5.0
10
04/03/15 08:11
142-28-9
5.0
10
04/03/15 08:11
594-20-7
5.0
10
04/03/15 08:11
563-58-6
5.0
10
04/03/15 08:11
10061-01-5
5.0
10
04/03/15 08:11
10061-02-6
5.0
10
04/03/15 08:11
108-20-3
5.0
10
04/03/15 08:11
100-41-4
20.0
10
04/03/15 08:11
87-68-3
5.0
10
04/03/15 08:11
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
N2
N2
Page 9 of 21

;aceAnalyfical"
wmv.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Project: Walsers
Pace Project No.: 92242825
Sample: Influent Lab ID: 92242825001 Collected: 03/25/15 13:00 Received: 03/26/15 10:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Methylene Chloride
28.4
ug/L
20.0
10
04/03/15 08:11
75-09-2
Methyl-tert-butyl ether
ND
ug/L
5.0
10
04/03/15 08:11
1634-04-4
Naphthalene
130
ug/L
20.0
10
04/03/15 08:11
91-20-3
n-Propylbenzene
16.8
ug/L
5.0
10
04/03/15 08:11
103-65-1
Styrene
ND
ug/L
5.0
10
04/03/15 08:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
10
04/03/15 08:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
5.0
10
04/03/15 08:11
79-34-5
Tetra chloroethene
ND
ug/L
5.0
10
04/03/15 08:11
127-18-4
Toluene
807
ug/L
5.0
10
04/03/15 08:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
20.0
10
04/03/15 08:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
20.0
10
04/03/15 08:11
120-82-1
1,1,1-Trichloroethane
ND
ug/L
5.0
10
04/03/15 08:11
71-55-6
1,1,2-Trichloroethane
ND
ug/L
5.0
10
04/03/15 08:11
79-00-5
Trichloroethene
ND
ug/L
5.0
10
04/03/15 08:11
79-01-6
Trichlorofluoromethane
ND
ug/L
10.0
10
04/03/15 08:11
75-69-4
1,2,3-Trichloropropane
ND
ug/L
5.0
10
04/03/15 08:11
96-18-4
1,2,4-Trimethylbenzene
210
ug/L
5.0
10
04/03/15 08:11
95-63-6
1,3,5-Trimethyl benzene
82.5
ug/L
5.0
10
04/03/15 08:11
108-67-8
Vinyl chloride
ND
ug/L
10.0
10
04/03/15 08:11
75-01-4
m&p-Xylene
662
ug/L
10.0
10
04/03/15 08:11
179601-23-1
o-Xylene
368
ug/L
5.0
10
04/03/15 08:11
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
100
%
70-130
10
04/03/15 08:11
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
10
04/03/15 08:11
460-00-4
Toluene-d8 (S)
99
%
70-130
10
04/03/15 08:11
2037-26-5
Date: 04/17/2015 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 21

aceAnalytical
/ www.pacelabs.com
i
ANALYTICAL RESULTS
Project: Walsers
Pace Project No.: 92242825
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Effluent Lab ID: 92242825002 Collected: 03/25/15 14.00 Received: 03/26/15 10:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 04/17/2015 04:10 PM
Analytical Method: MADEP VPH
118 ug/L
56.3 ug/L
ND ug/L
96
%
93
%
Analytical Method: SM 62006
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
50.0
1
03/30/1519:15
N2
50.0
1
03/30/1519:15
N2
50.0
1
03/3011519:15
N2
70-130
1
03/30/1519:15
460-00-4
70-130
1
03/30/1519:15
460-00-4
0.50
1
04/03/15 07:05
71-43-2
0.50
1
04/03/15 07:05
108-86-1
0.50
1
04/03/15 07:05
74-97-5
0.50
1
04/03/15 07:05
75-27-4
0.50
1
04/03/15 07:05
75-25-2
5.0
1
04/03/15 07:05
74-83-9
M1
0.50
1
04/03/15 07:05
104-51-8
0.50
1
04/03/15 07:05
135-98-8
0.50
1
04/03/15 07:05
98-06-6
0.50
1
04/03/15 07:05
56-23-5
0.50
1
04/03/15 07:05
108-90-7
1.0
1
04/03/15 07:05
75-00-3
0.50
1
04/03/15 07:05
67-66-3
1.0
1
04/03/15 07:05
74-87-3
0.50
1
04/03/15 07:05
95-49-8
0.50
1
04/03/15 07:05
106-43-4
1.0
1
04/03/15 07:05
96-12-8
0.50
1
04/03/15 07:05
124-48-1
0.50
1
04/03/15 07:05
106-93-4
0.50
1
04/03/15 07:05
74-95-3
0.50
1
04/03/15 07:05
95-50-1
0.50
1
04/03/15 07:05
541-73-1
0.50
1
04/03/15 07:05
106-46-7
0.50
1
04/03/15 07:05
75-71-8
0.50
1
04/03/15 07:05
75-34-3
0.50
1
04/03/15 07:05
107-06-2
0.50
1
04/03/15 07:05
75-35-4
0.50
1
04/03/15 07:05
156-59-2
0.50
1
04/03/15 07:05
156-60-5
0.50
1
04/03/15 07:05
78-87-5
0.50
1
04/03/15 07:05
142-28-9
0.50
1
04/03/15 07:05
594-20-7
0.50
1
04/03/15 07:05
563-58-6
0.50
1
04/03/15 07:05
10061-01-5
0.50
1
04/03/15 07:05
10061-02-6
0.50
1
04/03/15 07:05
108-20-3
0.50
1
04/03/15 07:05
100-41-4
2.0
1
04/03/15 07:05
87-68-3
0.50
1
04/03/15 07:05
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 21

Pace Analytical Services, Inc.
® 9800 KineyAve. Suite 100
aceAnalytical
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Walsers
Pace Project No.: 92242825
Sample: Effluent
Lab ID: 92242825002 Collected: 03/25/15 14:00
Received: 03/26/15 10:58 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method: SM 62006
Methylene Chloride
ND
ug/L
2.0
1
04/03/15 07:05
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/03/15 07:05
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/03/15 07:05
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/03/15 07:05
103-65-1
Styrene
ND
ug/L
0.50
1
04/03/15 07:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/03/15 07:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/03/15 07:05
79-34-5
Tetra chloroethene
ND
ug/L
0.50
1
04/03/15 07:05
127-18-4
Toluene
ND
ug/L
0.50
1
04/03/15 07:05
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
04/03/15 07:05
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/03/15 07:05
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/03/15 07:05
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/03/15 07:05
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/03/15 07:05
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/03/15 07:05
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/03/15 07:05
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/03/15 07:05
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/03/15 07:05
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/03/15 07:05
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/03/15 07:05
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/03/15 07:05
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
04/03/15 07:05
17060-07-0
4-Bromofluorobenzene (S)
104
%
70-130
1
04/03/15 07:05
460-00-4
Toluene-d8 (S)
98
%
70-130
1
04/03/15 07:05
2037-26-5
Date: 04/17/2015 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 21

aceAnalXical
~..pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
Project: Walsers
Pace Project No.: 92242825
QC Batch: GCV/9135
Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH
Analysis Description: VPH
NC Water
Associated Lab Samples: 92242825001, 92242825002
METHOD BLANK: 1422198
Matrix: Water
Associated Lab Samples: 92242825001, 92242825002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aliphatic (C05-CO8)
ug/L
ND 50.0
03/30/15 13:06
N2
Aliphatic (C09-C12)
ug/L
ND 50.0
03/30/15 13:06
N2
Aromatic (C09-C10)
ug/L
ND 50.0
03/30/15 13:06
N2
4-Bromofluorobenzene (FID) (S)
%
92 70-130
03/30/15 13:06
4-Bromofluorobenzene (PID) (S)
%
88 70-130
03/30/15 13:06
LABORATORY CONTROL SAMPLE & LCSD:
1422199
1422200
Spike LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-008)
ug/L
300 271 270
90 90
70-130 0 25 N2
Aliphatic (C09-C12)
ug/L
300 281 286
94 95
30-130 2 25 N2
Aromatic (C09-C10)
ug/L
100 85.4 85.8
85 86
70-130 0 25 N2
4-Bromofluorobenzene (FID) (S)
%
98 96
70-130
4-Bromofluorobenzene (PID) (S)
%
97 94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 21

aceAnalj cal
www.pacelabs.com
QUALITY CONTROL DATA
Project: Walsers
Pace Project No.: 92242825
QC Batch: MSV/31032
QC Batch Method: SM 6200B
Associated Lab Samples: 92242825001, 92242825002
Analysis Method:
Analysis Description:
SM 6200B
6200B MSV
METHOD BLANK: 1425931
Matrix: Water
Associated Lab Samples: 92242825001,
92242825002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
NO
0.50
04/03/15 05:43
1,1,1-Trichloroethane
ug/L
ND
0.50
04/0311505:43
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/03/15 05:43
1,1,2-Trichloroethane
ug/L
ND
0.50
04/03/15 05:43
1,1-Dichloroethane
ug/L
ND
0.50
04/03/15 05:43
1,1-Dichloroethene
ug/L
ND
0.50
04/03/15 05:43
1,1-Dichloropropene
ug/L
NO
0.50
04/03/15 05:43
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/03/15 05:43
1,2,3-Trichloropropane
ug/L
ND
0.50
04/03/15 05:43
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/03/15 05:43
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/03/15 05:43
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/03/15 05:43
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/03/15 05:43
1,2-Dichlorobenzene
ug/L
ND
0.50
04/03/15 05:43
1,2-Dichloroethane
ug/L
ND
0.50
04/03/15 05:43
1,2-Dichloropropane
ug/L
ND
0.50
04/03/15 05:43
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/03/15 05:43
1,3-Dichlorobenzene
ug/L
ND
0.50
04/03/15 05:43
1,3-Dichloropropane
ug/L
ND
0.50
04/03/15 05:43
IA-Dichlorobenzene
ug/L
ND
0,50
04/03/15 05:43
2,2-Dichloropropane
ug/L
ND
0.50
04/03/15 05:43
2-Chlorotoluene
ug/L
ND
0.50
04/03/15 05:43
4-Chlorotoluene
ug/L
ND
0.50
04/03/15 05:43
Benzene
ug/L
ND
0.50
04/03/15 05:43
Bromobenzene
ug/L
ND
0.50
04/03/15 05:43
Bromochloromethane
ug/L
ND
0.50
04/03/15 05:43
Bromodichloromethane
ug/L
ND
0.50
04/03/15 05:43
Bromoform
ug/L
ND
0.50
04/03/15 05:43
Bromomethane
ug/L
ND
5.0
04/03/15 05:43
Carbon tetrachloride
ug/L
ND
0.50
04/03/15 05:43
Chlorobenzene
ug/L
ND
0.50
04/03/15 05:43
Chloroethane
ug/L
ND
1.0
04/03/15 05:43
Chloroform
ug/L
ND
0.50
04/03/15 05:43
Chloromethane
ug/L
ND
1.0
04/03/15 05:43
cis-1,2-Dichloroethene
ug/L
ND
0.50
04/03/15 05:43
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/03/15 05:43
Dibromochloromethane
ug/L
ND
0.50
04/03/15 05:43
Dibromomethane
ug/L
ND
0.50
04/03/15 05:43
Dichlorodifluoromethane
ug/L
ND
0.50
04/03/15 05:43
Diisopropyl ether
ug/L
ND
0.50
04/03/15 05:43
Ethylbenzene
ug/L
ND
0.50
04/03/15 05:43
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 21

aceAnalXical
% www.pacelabs.com
QUALITY CONTROL DATA
Project: Walsers
Pace Project No.: 92242825
METHOD BLANK: 1425931
Associated Lab Samples: 92242825001. 92242825002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/03/15 05:43
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/03/15 05:43
m&p-Xylene
ug/L
ND
1.0
04/03/15 05:43
Methyl-tert-butyl ether
ug/L
ND
0.50
04/03/15 05:43
Methylene Chloride
ug/L
ND
2.0
04/03/15 05:43
n-Butylbenzene
ug/L
ND
0.50
04/03/15 05:43
n-Propylbenzene
ug/L
ND
0.50
04/03/15 05:43
Naphthalene
ug/L
ND
2.0
04/03/15 05:43
o-Xylene
ug/L
ND
0.50
04/03/15 05:43
sec -Butyl benzene
ug/L
ND
0.50
04/03/15 05:43
Styrene
ug/L
ND
0.50
04/03/15 05:43
tert-Butylbenzene
ug/L
ND
0.50
04/03/15 05:43
Tetra chloroethene
ug/L
ND
0.50
04/03/15 05:43
Toluene
ug/L
ND
0.50
04/03/15 05:43
trans-1,2-Dichloroethene
ug/L
ND
0.50
04/03/15 05:43
trans-1,3-Dichloropropene
ug/L
ND
0.50
04/03/15 05:43
Trichloroethene
ug/L
ND
0.50
04/03/15 05:43
Trichlorofluoromethane
ug/L
ND
1.0
04/03/15 05:43
Vinyl chloride
ug/L
ND
1.0
04/03/15 05:43
1,2-Dichloroethane-d4 (S)
%
105
70-130
04/03/15 05:43
4-Bromofluorobenzene (S)
%
103
70-130
04/03/15 05:43
Toluene -dB (S)
%
99
70-130
04/03/15 05:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1425932
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
50.6
101
60-140
1,1,1-Trichloroethane
ug/L
50
49.8
100
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
45.3
91
60-140
1,1,2-Trichloroethane
ug/L
50
47.7
95
60-140
1,1-Dichloroethane
ug/L
50
44.8
90
60-140
1,1-Dichloroethene
ug/L
50
45.9
92
60-140
1,1-Dichloropropene
ug/L
50
49.4
99
60-140
1,2,3-Trichlorobenzene
ug/L
50
53.4
107
60-140
1,2,3-Trichloropropane
ug/L
50
47.4
95
60-140
1,2,4-Trichlorobenzene
ug/L
50
55.6
111
60-140
1,2,4-Trimethylbenzene
ug/L
50
52.9
106
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
50.2
100
60-140
1,2-Dibromoethane (EDB)
ug/L
50
50.2
100
60-140
1,2-Dichlorobenzene
ug/L
50
49.3
99
60-140
1,2-Dichloroethane
ug/L
50
47.3
95
60-140
1,2-Dichloropropane
ug/L
50
47.5
95
60-140
1,3,5-Trimethylbenzene
ug/L
50
52.2
104
60-140
1,3-Dichlorobenzene
ug/L
50
49.0
98
60-140
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 21

_ aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
QUALITY CONTROL DATA
Project: Walsers
Pace Project No.: 92242825
LABORATORY CONTROL SAMPLE:
Parameter
1425932
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
47.4
95
60-140
1,4-Dichlorobenzene
ug/L
50
48.6
97
60-140
2,2-Dichloropropane
ug/L
50
46.7
93
60-140
2-Chlorotoluene
ug/L
50
49.6
99
60-140
4-Chlorotoluene
ug/L
50
46.6
93
60-140
Benzene
ug/L
50
47.2
94
60-140
Bromobenzene
ug/L
50
47.5
95
60-140
Bromochloromethane
ug/L
50
44.0
88
60-140
Bromodichloromethane
ug/L
50
47.1
94
60-140
Bromoform
ug/L
50
47.9
96
60-140
Bromomethane
ug/L
50
42.3
85
60-140
Carbon tetrachloride
ug/L
50
56.7
113
60-140
Chlorobenzene
ug/L
50
47.1
94
60-140
Chloroethane
ug/L
50
42.4
85
60-140
Chloroform
ug/L
50
42.1
84
60-140
Chloromethane
ug/L
50
46.0
92
60-140
cis-1,2-Dichloroethene
ug/L
50
45.9
92
60-140
cis-1,3-Dichloropropene
ug/L
50
49.0
98
60-140
Dibromochloromethane
ug/L
50
47.1
94
60-140
Dibromomethane
ug/L
50
48.4
97
60-140
Dichlorodifluoromethane
ug/L
50
47.6
95
60-140
Diisopropyl ether
ug/L
50
45.5
91
60-140
Ethylbenzene
ug/L
50
48.6
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
52.2
104
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.4
97
60-140
m&p-Xylene
ug/L
100
100
100
60-140
Methyl-tert-butyl ether
ug/L
50
45.5
91
60-140
Methylene Chloride
ug/L
50
58.1
116
60-140
n-Butylbenzene
ug/L
50
51.0
102
60-140
n-Propylbenzene
ug/L
50
47.1
94
60-140
Naphthalene
ug/L
50
50.7
101
60-140
o-Xylene
ug/L
50
49.3
99
60-140
sec-Butylbenzene
ug/L
50
47.9
96
60-140
Styrene
ug/L
50
50.4
101
60-140
tert-Butylbenzene
ug/L
50
47.7
95
60-140
Tetra chloroethene
ug/L
50
49.4
99
60-140
Toluene
ug/L
50
46.0
92
60-140
trans-1,2-Dichloroethene
ug/L
50
44.3
89
60-140
trans-1,3-Dichloropropene
ug/L
50
52.1
104
60-140
Trichloroethene
ug/L
50
49.7
99
60-140
Trichlorofluoromethane
ug/L
50
49.4
99
60-140
Vinyl chloride
ug/L
50
43.8
88
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 21

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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Walsers
Pace Project No.: 92242825
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1425933
1425934
MS
MSD
92242825002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conic.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
20.7
109
104
60-140
5
1,1,1-Trichloroethane
ug/L
ND
20
20
21.5
22.0
108
110
60-140
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.7
21.3
108
106
60-140
2
1,1,2-Trichloroethane
ug/L
ND
20
20
20.2
20.3
101
101
60-140
0
1,1-Dichloroethane
ug/L
ND
20
20
19.8
19.9
99
100
60-140
1
1,1-Dichloroethene
ug/L
ND
20
20
20.8
21.2
104
106
60-140
2
1,1-Dichloropropene
ug/L
ND
20
20
22.1
21.9
111
109
60-140
1
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.1
16.9
100
85
60-140
17
1,2,3-Trichloropropane
ug/L
ND
20
20
19.9
19.8
99
99
60-140
0
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.8
16.3
104
81
60-140
24
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.7
19.6
113
97
60-140
15
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
19.6
18.0
98
90
60-140
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.1
21.4
110
107
60-140
3
1,2-Dichlorobenzene
ug/L
ND
20
20
20.1
17.5
100
87
60-140
14
1,2-Dichloroethane
ug/L
ND
20
20
19.2
19.4
96
97
60-140
1
1,2-Dichloropropane
ug/L
ND
20
20
20.8
20.6
104
103
60-140
1
1,3,5-Trimethyl benzene
ug/L
ND
20
20
22.8
20.1
114
101
60-140
12
1,3-Dichlorobenzene
ug/L
ND
20
20
21.0
17.8
105
89
60-140
16
1,3-Dichloropropane
ug/L
ND
20
20
20.8
20.2
104
101
60-140
3
1,4-Dichlorobenzene
ug/L
ND
20
20
20.4
17.3
102
87
60-140
16
2,2-Dichloropropane
ug/L
ND
20
20
18.1
18.4
91
92
60-140
1
2-Chlorotoluene
ug/L
ND
20
20
22.0
19.3
110
97
60-140
13
4-Chlorotoluene
ug/L
ND
20
20
20.5
17.7
102
88
60-140
15
Benzene
ug/L
ND
20
20
21.6
21.2
107
105
60-140
2
Bromobenzene
ug/L
ND
20
20
21.3
18.7
106
94
60-140
13
Bromochloromethane
ug/L
ND
20
20
19.3
19.5
97
98
60-140
1
Bromodichloromethane
ug/L
ND
20
20
19.0
18.8
95
94
60-140
1
Bromoform
ug/L
ND
20
20
18.0
17.6
90
88
60-140
2
Bromomethane
ug/L
ND
20
20
11.5
11.2
57
56
60-140
3 M1
Carbon tetrachloride
ug/L
ND
20
20
23.3
23.8
117
119
60-140
2
Chlorobenzene
ug/L
ND
20
20
21.3
19.5
106
97
60-140
9
Chloroethane
ug/L
ND
20
20
18.5
20.3
92
101
60-140
9
Chloroform
ug/L
ND
20
20
17.6
18.5
88
92
60-140
5
Chloromethane
ug/L
ND
20
20
17.2
19.2
86
96
60-140
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.8
19.9
99
100
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.4
19.4
97
97
60-140
0
Dibromochloromethane
ug/L
ND
20
20
18.7
18.6
94
93
60-140
1
Dibromomethane
ug/L
ND
20
20
20.5
20.9
102
104
60-140
2
Dichlorodifluoromethane
ug/L
ND
20
20
21.8
23.0
109
115
60-140
6
Diisopropyl ether
ug/L
ND
20
20
19.1
18.9
96
95
60-140
1
Ethylbenzene
ug/L
ND
20
20
22.2
20.6
111
103
60-140
8
Hexachloro-1,3-butadiene
ug/L
ND
20
20
21.3
19.2
106
96
60-140
10
Isopropylbenzene (Cumene)
ug/L
ND
20
20
22.1
20.2
110
101
60-140
9
m&p-Xylene
ug/L
ND
40
40
44.2
41.0
110
102
60-140
8
Methyl-tert-butyl ether
ug/L
ND
20
20
18.6
18.7
93
93
60-140
0
Methylene Chloride
ug/L
ND
20
20
19.6
20.2
98
101
60-140
3
Results presented on this page are in the units Indicated by the "Units" column except where an ahemate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 21

aceAnalytica!
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Walsers
Pace Project No.: 92242825
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1425933
1425934
MS
MSD
92242825002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
21.3
18.1
106
91
60-140
16
n-Propylbenzene
ug/L
ND
20
20
21.0
18.9
105
94
60-140
11
Naphthalene
ug/L
ND
20
20
18.3
15.0
88
71
60-140
20
o-Xylene
ug/L
ND
20
20
22.2
20.0
111
100
60-140
10
sec-Butylbenzene
ug/L
ND
20
20
21.1
18.9
106
95
60-140
11
Styrene
ug/L
ND
20
20
22.4
18.2
112
91
60-140
21
tert-Butylbenzene
ug/L
ND
20
20
21.2
19.2
106
96
60-140
10
Tetra chloroethene
ug/L
ND
20
20
24.2
22.5
121
112
60-140
7
Toluene
ug/L
ND
20
20
20.8
20.2
104
101
60-140
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.9
19.8
99
99
60-140
0
trans- 1,3-Dichloropropene
ug/L
ND
20
20
19.8
19.7
99
98
60-140
1
Trichloroethene
ug/L
ND
20
20
21.6
21.6
108
108
60-140
0
Trichlorofluoromethane
ug/L
ND
20
20
21.4
23.1
107
116
60-140
8
Vinyl chloride
ug/L
ND
20
20
19.8
20.8
99
104
60-140
5
1,2-Dichloroethane-d4 (S)
%
95
96
70-130
4-Bromofluorobenzene(S)
%
102
102
70-130
Toluene-d8 (S)
%
98
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.
Page 18 of 21

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QUALIFIERS
Project: Walsers
Pace Project No.: 92242825
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/17/2015 04:10 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 21

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Walsers
Pace Project No.: 92242825
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92242825001
Influent
MADEP VPH
GCV/9135
92242825002
Effluent
MADEP VPH
GCV/9135
92242825001
Influent
SM 6200B
MSV/31032
92242825002
Effluent
SM 6200B
MSV/31032
Date: 04/17/2015 04:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
Page 20 of 21

172RAnaVicaf-
CHAIN-OF-CUSTODY I AnalyticaURequest: Document
The-Chain-of-;Crustoi yls-a LEGALDOCUMENT- All reievant-fieids-MUstber-orripltted accurately.
Section A Section a beet on p
R*c;uirod Client Infortnation: Required Project Information: —Involceitomatiorc Page I Of
Company: Shield Engineering Roport'ro. Flora DSoUza Attention: Flora Usouza,
Address: 4301 Taggart Creek Road Copy To: Co mO" Namc Shield Engineeri!m'
Charlotte. NC 28208
j;FWT.= - .4304 Ta`gart Creek,.Rbad,.,Charlotle,:N(
Email To: [e-mail]
PurchasaOrder No. 1990018-55
Pace Quote Pe(erepnoll:
UST - UndeMmund Storage Tank
ptlor,C [phone] 1 Fax
Client Project to WALSERS
P*e Proiect manager .'Herring:-XvAn
5F TA., 1) C %--.' 7x Z--Iili t "VII
Requested Due DaWTAT: 10 Day (Default )
Container Order Number. '67389
Pace Profile P.
North Carolina
givagr
...COLLECTED
Preservatives
.....
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"TRIX com
DO." W.W ow
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SAMPLE ID wsSL
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Ids must be TI.— TS
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PRINT Name of SAMPLER:
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Wo#:92242825 SIGREof
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92242825

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIR & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WAT ALITY-INFORMATION PROCESSING UNI
COMPLIANCE REPORT FORM
1617 MAI VICE CE ALEIGH, NC 27s99.1617 Phone: 919) 733J221
FACILITY INFORMATION Please Print Clearly or Type
r: ate: 1/3 /2018
Facility Name: Hill Oil CompanV, Inc. - Walser's Service
00015102
Permit Name (if different):
Facility Address. 6419 North Carolina Hiahwav 15ON
ITTED OPERATONITORED
ion: Infiltration Gallery
Eig
Lexinaton NC County Davidson
ion:Contact
Person: Flora D'Souza/Shield Eno neerina.
Inc. Telephone#: [phone]
tributor lication of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: NA
Heat Pump
from
Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 2/18/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: min.
pH 6.24 units Temp. NM °C
DRY at
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63
ft. Spec. Cond. NM µ Mhos
time of
sampling;
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here.
Samples for metals were collected unfiltered: ® YES
❑ NO and field acidified: ❑YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 2/23/15 - 2/26/15
Laboratory Name: Pace Analytical
Services
Certification No 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/1
Nitrite (NOZ) as N
NA mg/I
Pb - Lead 0.0155 mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform. MF Total NA /100m1
Phosphorus: Total as P
NA mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I
pH (when analyzed) NA units
Ba - Barium
NA mg/I
TOC NA mg/1
Ca - Calcium
NA mg/I
APR p g 201
Chloride NA mg/I
Cd - Cadmium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA mg/1
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 62006
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MADFP VPH
(Ammonia Nitrogen, NH3 as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/1
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 7.9278 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100%
GW-59 Rev. 1/2007

F."I w w , 1_ N l

aceAnalytical
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February 27, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S
Pace Project No.: 92238263
Dear Ms. D'Souza:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 1 of 26

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Project: WALSER'S
Pace Project No.: 92238263
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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SAMPLE ANALYTE COUNT
Project: WALSER'S
Pace Project No.: 92238263
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92238263001
INFLUENT
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
92238263002
EFFLUENT
MADEP VPH
BFW
5
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
92238263003
MW-1
SM 6200B
CAH
16
PASI-C
REPORT OF LABORATORY ANALYSIS
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/�;ace AnalXical
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SUMMARY OF DETECTION
Project:
Pace Project No.:
WALSER'S
92238263
Lab Sample ID
Client Sample ID
Method
Parameters
92238263001
INFLUENT
MADEP VPH
Aliphatic (C05-008)
MADEP VPH
Aliphatic (C09-C12)
MADEP VPH
Aromatic (C09-C10)
SM 6200B
Benzene
SM 6200B
1,2-Dibromoethane (EDB)
SM 6200B
Ethylbenzene
SM 6200B
Isopropylbenzene (Cumene)
SM 6200B
Naphthalene
SM 6200B
n-Propylbenzene
SM 6200B
Toluene
SM 6200B
1,2,4-Trimethylbenzene
SM 6200B
1,3,5-Trimethylbenzene
SM 6200B
m&p-Xylene
SM 6200B
o-Xylene
92238263002
EFFLUENT
EPA 200.7
Lead
92238263003
MW-1
SM 6200B
Ethylbenzene
SM 6200B
Isopropylbenzene (Cumene)
SM 6200B
Naphthalene
SM 6200B
m&p-Xylene
SM 6200B
o-Xylene
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Result
Units
Report Limit
Analyzed
1290
ug/L
500
02/23/1515:31 N2
4030
ug/L
500
02/23/1515:31 N2
635
ug/L
500
02/23/1515:31 N2
26.9
ug/L
2.5
02/26/15 17:03
3.0
ug/L
2.5
02126/1517:03
64.4
ug/L
2.5
02/26/15 17:03
5.4
ug/L
2.5
02/26/15 17:03
98.1
ug/L
10.0
02/26/15 17:03
7.2
ug/L
2.5
02/26/15 17:03
740
ug/L
2.5
02/26/15 17:03
162
ug/L
2.5
02/26/15 17:03
67.8
ug/L
2.5
02/26/15 17:03
455
ug/L
5.0
02/26/15 17:03
343
ug/L
2.5
02/26/15 17:03
15.5
ug/L
5.0
02/25/15 02:25
208
ug/L
2.0
02/26/15 00:02
15.1
ug/L
2.0
02/26/15 00:02
106
ug/L
4.0
02/26/15 00:02
727
ug/L
4.0
02/26/15 00:02
3.9
ug/L
2.0
02/26/15 00:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 4 of 26

aceAnalytica!
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PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92238263
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: February 27, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9031
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1396118)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• EFFLUENT (Lab ID: 92238263002)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• INFLUENT (Lab ID: 92238263001)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
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17;a'ce A nalytica I
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r
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92238263
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: February 27, 2015
Analyte Comments:
QC Batch: GCV/9031
N2: The lab does not hold TNI accreditation for this parameter.
• LCS (Lab ID: 1396119)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1396120)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
aceAnalytical 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92238263
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: February 27, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 7 of 26

Pace Analytical Services, Inc.
ZAnalyfical 9800KinceyAve. Suite100
` _Huntersville, NC 28078
wwwpacelabs.com [phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92238263
Method: SM 6200B
Description: 602 Volatiles by Method 6200
Client: Shield
Date: February 27, 2015
General Information:
1 sample was analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/30474
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92238010013
MO: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MSD (Lab ID: 1397031)
• Methyl-tert-butyl ether
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 26

aceAnalXical
ww�+w.pacelabs.arn
i
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92238263
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: February 27, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 26

_ _ 2ce Analytical
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Project: WALSER'S
Pace Project No.: 92238263
Sample: INFLUENT
Parameters
VPH NC Water
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200B MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis- 1,2-Dichloroethene
trans- 1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 02/27/2015 04:08 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
ANALYTICAL RESULTS
Lab ID: 92238263001 Collected: 02/18/15 14:00 Received: 02/19/15 15:11 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: MADEP VPH
1290 ug/L
4030 ug/L
635 ug/L
89
%
93
%
Analytical Method: SM 6200B
26.9
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
3.0
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
64.4
ug/L
ND
ug/L
5.4
ug/L
500
10
02/23/15 15:31
500
10
02/23/15 15:31
500
10
02/23/15 15:31
70-130
10
02/23/15 15:31
460-00-4
70-130
10
02/23/15 15:31
460-00-4
2.5
5
02/26/1517:03
71-43-2
2.5
5
02/2611517:03
108-86-1
2.5
5
02/26/1517:03
74-97-5
2.5
5
02126/1517:03
75-27-4
2.5
5
02126/1517:03
75-25-2
25.0
5
02/26/1517:03
74-83-9
2.5
5
02/26/1517:03
104-51-8
2.5
5
02/26/1517:03
135-98-8
2.5
5
02/26/1517:03
98-06-6
2.5
5
02/26/1517:03
56-23-5
2.5
5
02/26/1517:03
108-90-7
5.0
5
02/26/1517:03
75-00-3
2.5
5
02/26/1517:03
67-66-3
5.0
5
02/26/1517:03
74-87-3
2.5
5
02/26/1517:03
95-49-8
2.5
5
02/26/1517:03
106-43-4
5.0
5
02/26/1517:03
96-12-8
2.5
5
02/26/1517:03
124-48-1
2.5
5
02/26/1517:03
106-93-4
2.5
5
02/26/1517:03
74-95-3
2.5
5
02/2611517:03
95-50-1
2.5
5
02/26/1517:03
541-73-1
2.5
5
02/26/1517:03
106-46-7
2.5
5
02/26/1517:03
75-71-8
2.5
5
02/26/1517:03
75-34-3
2.5
5
02/26/1517:03
107-06-2
2.5
5
02/2611517:03
75-35-4
2.5
5
02/26/1517:03
156-59-2
2.5
5
02/26/1517:03
156-60-5
2.5
5
02/2611517:03
78-87-5
2.5
5
02/26/1517:03
142-28-9
2.5
5
02/26/1517:03
594-20-7
2.5
5
02/26/1517:03
563-58-6
2.5
5
02/26/15 17:03
10061-01-5
2.5
5
02/26/1517:03
10061-02-6
2.5
5
02/26/1517:03
108-20-3
2.5
5
02/26/1517:03
100-41-4
10.0
5
02/26/1517:03
87-68-3
2.5
5
02/26/1517:03
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N2
N2
N2
Page 10 of 26

aceAnalytical
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ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92238263
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Sample: INFLUENT Lab ID: 92238263001 Collected: 02/18/15 14:00 Received: 02/19/15 15:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Methylene Chloride
ND
ug/L
10.0
5
02/26/15 17:03
75-09-2
Methyl-tert-butyl ether
ND
ug/L
2.5
5
02/26/15 17:03
1634-04-4
Naphthalene
98.1
ug/L
10.0
5
02/26/15 17:03
91-20-3
n-Propylbenzene
7.2
ug/L
2.5
5
02/26/15 17:03
103-65-1
Styrene
ND
ug/L
2.5
5
02/26/15 17:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
2.5
5
02/26/15 17:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
2.5
5
02/26/15 17:03
79-34-5
Tetrachloroethene
ND
ug/L
2.5
5
02/26/15 17:03
127-18-4
Toluene
740
ug/L
2.5
5
02/26/15 17:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
10.0
5
02/26/15 17:03
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
10.0
5
02/26/15 17:03
120-82-1
1,1,1-Trichloroethane
ND
ug/L
2.5
5
02/26/15 17:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.5
5
02/26/15 17:03
79-00-5
Trichloroethene
ND
ug/L
2.5
5
02/26/15 17:03
79-01-6
Trichlorofluoromethane
ND
ug/L
5.0
5
02/26/15 17:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.5
5
02/26/15 17:03
96-18-4
1,2,4-Trimethylbenzene
162
ug/L
2.5
5
02/26/15 17:03
95-63-6
1,3,5-Trimethylbenzene
67.8
ug/L
2.5
5
02/26/15 17:03
108-67-8
Vinyl chloride
ND
ug/L
5.0
5
02/26/15 17:03
75-01-4
m&p-Xylene
455
ug/L
5.0
5
02126/1517:03
179601-23-1
o-Xylene
343
ug/L
2.5
5
02/26/15 17:03
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
5
02/26/15 17:03
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
5
02/26/15 17:03
460-00-4
Toluene-d8 (S)
100
%
70-130
5
02/26/15 17:03
2037-26-5
Date: 02/27/2015 04:08 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 26

_ ;a'ce Analytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92238263
Sample: EFFLUENT
Lab ID: 92238263002 Collected:
02/18/15 13:00 Received: 02/19/15 15:11 Matrix: Water
Parameters
Results
Units Report
Limit
DF Prepared
Analyzed
CAS No. Qual
VPH NC Water
Analytical Method: MADEP VPH
Aliphatic (C05-008)
ND
ug/L
50.0
1
02/23/15 13:19
N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
02/23/15 13:19
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
02/23/15 13:19
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
89
%
70-130
1
02/23/15 13:19
460-00-4
4-Bromofluorobenzene (PID) (S)
91
%
70-130
1
02/23/15 13:19
460-00-4
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Lead
15.5
ug/L
5.0
1 02/23/15 15:00
02/25/15 02:25
7439-92-1
6200E MSV
Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
02/26/15 15:38
71-43-2
Bromobenzene
ND
ug/L
0.50
1
02/26/15 15:38
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
02/26/15 15:38
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
02/26/15 15:38
75-27-4
Bromoform
ND
ug/L
0.50
1
02/26/15 15:38
75-25-2
Bromomethane
ND
ug/L
5.0
1
02/26/15 15:38
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
135-98-8
tent-Butylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
02/26/15 15:38
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
02/26/15 15:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
02/26/15 15:38
75-00-3
Chloroform
ND
ug/L
0.50
1
02/26/15 15:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
02/26/15 15:38
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
02/26/15 15:38
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
02/26/15 15:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
02/26/15 15:38
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
02/26/15 15:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
02/26/15 15:38
106-93-4
Dibromomethane
ND
ug/L
0.50
1
02/26/15 15:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
02/26/15 15:38
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
02/2611515:38
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
02/26/15 15:38
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
02/26/15 15:38
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
02/26/15 15:38
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
02/26/15 15:38
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
02/2611515:38
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
0.50
1
02/26/15 15:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
02/26/15 15:38
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
02/26/15 15:38
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
02/26/15 15:38
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
02/26/15 15:38
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
02/26/15 15:38
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
1
02/26/15 15:38
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
02/26/15 15:38
10061-02-6
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 02/27/2015 04:08 PM
without the written consent of Pace Analytical
Services, Inc..
Page 12 of 26

Pace Analytical Services, Inc.
9800KinceyAve. Suite100
172eAnalXical' Huntersville, NC 28078
www.pacelabs.com (704)8759092
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92238263
Sample: EFFLUENT
Lab ID: 92238263002 Collected:
02/18/15
13:00
Received: 02/19/15 15:11 Matrix:
Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Diisopropyl ether
ND
ug/L
0.50
1
02/26/15 15:38
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
02/26/15 15:38
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
02/26/15 15:38
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
02/26/15 15:38
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
02/26/15 15:38
1634-04-4
Naphthalene
ND
ug/L
2.0
1
02/2611515:38
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
103-65-1
Styrene
ND
ug/L
0.50
1
02/26/15 15:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
02126/1515:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
02/26/15 15:38
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
02/26/15 15:38
127-18-4
Toluene
ND
ug/L
0.50
1
02/26/15 15:38
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
02/26/15 15:38
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
02/26/15 15:38
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
02/26/15 15:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
02/26/15 15:38
79-00-5
Trichloroethene
ND
ug/L
0.50
1
02/26/15 15:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
02/26/15 15:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
02/26/15 15:38
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
02126/1515:38
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
02/26/15 15:38
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
02/26/15 15:38
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
02126/1515:38
179601-23-1
o-Xylene
ND
ug/L
0.50
1
02/26/15 15:38
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
02/26/15 15:38
17060-07-0
4-Bromofluorobenzene (S)
101
%
70-130
1
02/26/15 15:38
460-00-4
Toluene-d8 (S)
101
%
70-130
1
02/26/15 15:38
2037-26-5
Date: 02/27/2015 04:08 PM
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 26

1�;a'ce Analytical"
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ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92238263
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: MW-1 Lab ID: 92238263003 Collected: 02/18/15 12:00 Received: 02/19/15 15:11 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
602 Volatiles by Method 6200
Benzene
Chlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Diisopropyl ether
Ethylbenzene
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Naphthalene
Toluene
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 02/27/2015 04:08 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
208
ug/L
15.1
ug/L
ND
ug/L
106
ug/L
ND
ug/L
727
ug/L
3.9
ug/L
104 %
99 %
101 %
2.0
2
02/26/15 00:02
71-43-2
2.0
2
02/26/15 00:02
108-90-7
2.0
2
02/26/15 00:02
95-50-1
2.0
2
02/26/15 00:02
541-73-1
2.0
2
02/26/15 00:02
106-46-7
2.0
2
02/26/15 00:02
108-20-3
2.0
2
02/26/15 00:02
100-41-4
2.0
2
02/26/15 00:02
98-82-8
2.0
2
02/26/15 00:02
1634-04-4
4.0
2
02/26/15 00:02
91-20-3
2.0
2
02/26/15 00:02
108-88-3
4.0
2
02/26/15 00:02
179601-23-1
2.0
2
02/26/15 00:02
95-47-6
70-130
2
02/26/15 00:02
460-00-4
70-130
2
02/26/15 00:02
17060-07-0
70-130
2
02/26/15 00:02
2037-26-5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 14 of 26

17;alce Analytical
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
QC Batch: GCV/9031 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92238263001, 92238263002
METHOD BLANK: 1396118
Associated Lab Samples: 92238263001, 92238263002
Parameter
Units
Aliphatic (C05-008)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
02/23/1516:23 N2
ND
50.0
02/2311516:23 N2
ND
50.0
02/2311516:23 N2
85
70-130
02/23/1516:23
87
70-130
02/23/1516:23
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
1396119
1396120
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-008)
ug/L
300
238
254
79
85
70-130 7 25 N2
Aliphatic (C09-C12)
ug/L
300
278
306
93
102
30-130 10 25 N2
Aromatic (C09-C10)
ug/L
100
84.0
89.5
84
90
70-130 6 25 N2
4-Bromofluorobenzene (FID) (S)
%
90
90
70-130
4-Bromofluorobenzene (PID) (S)
%
95
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 26

aceAnalytical
j wwwpacelabs.com
Project: WALSER'S
Pace Project No.: 92238263
QC Batch: MPRP/17941
QC Batch Method: EPA 200.7
Associated Lab Samples: 92238263002
METHOD BLANK: 1396345
Associated Lab Samples: 92238263002
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1396346
Parameter Units
Lead ug/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 02/25/15 02:19
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 482 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1396347 1396348
MS MSD
92238263002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L 15.5 500 500 495 503 96 98 70-130 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1396349 1396350
MS MSD
92238124001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L NO 500 500 472 467 94 93 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 26

aceAnalytical
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
QC Batch: MSV/30474 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 602 by 6200E
Associated Lab Samples: 92238263003
METHOD BLANK: 1397028
Associated Lab Samples: 92238263003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2-Dichlorobenzene
ug/L
ND
1.0
02/25/15 18:23
1,3-Dichlorobenzene
ug/L
ND
1.0
02/25/15 18:23
1,4-Dichlorobenzene
ug/L
ND
1.0
02/25/15 18:23
Benzene
ug/L
ND
1.0
02/25/15 18:23
Chlorobenzene
ug/L
ND
1.0
02/25/15 18:23
Diisopropyl ether
ug/L
ND
1.0
02/25/15 18:23
Ethylbenzene
ug/L
ND
1.0
02125/1518:23
Isopropylbenzene (Cumene)
ug/L
ND
1.0
02/25/15 18:23
m&p-Xylene
ug/L
ND
2.0
02/25/15 18:23
Methyl-tert-butyl ether
ug/L
ND
1.0
02/25/15 18:23
Naphthalene
ug/L
ND
2.0
02/25/15 18:23
o-Xylene
ug/L
ND
1.0
02/25/15 18:23
Toluene
ug/L
ND
1.0
02/25/15 18:23
1,2-Dichloroethane-d4 (S)
%
101
70-130
02/25/15 18:23
4-Bromofluorobenzene (S)
%
96
70-130
02/25/15 18:23
Toluene-d8 (S)
%
99
70-130
02/25/15 18:23
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1397029
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dichlorobenzene
ug/L
50
50.2
100
60-140
1,3-Dichlorobenzene
ug/L
50
49.9
100
60-140
1,4-Dichlorobenzene
ug/L
50
49.3
99
60-140
Benzene
ug/L
50
49.3
99
60-140
Chlorobenzene
ug/L
50
48.5
97
60-140
Diisopropyl ether
ug/L
50
42.9
86
60-140
Ethylbenzene
ug/L
50
51.0
102
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.9
106
60-140
m&p-Xylene
ug/L
100
101
101
60-140
Methyl-tert-butyl ether
ug/L
50
40.8
82
60-140
Naphthalene
ug/L
50
51.7
103
60-140
o-Xylene
ug/L
50
49.4
99
60-140
Toluene
ug/L
50
48.0
96
60-140
1,2-Dichloroethane-d4(S)
%
99
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 26

1�;a'ce Analytical
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1397030 1397031
Parameter
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Chlorobenzene
Diisopropyl ether
Ethylbenzene
Isopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Naphthalene
o-Xylene
Toluene
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MS
MSD
92238010013
Spike
Spike
MS
MSD
MS
MSD
% Rec
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
ug/L
ND
20
20
16.1
13.3
80
66
60-140
19
ug/L
ND
20
20
16.4
13.3
82
67
60-140
21
ug/L
ND
20
20
16.3
13.5
81
67
60-140
19
ug/L
ND
20
20
16.1
13.5
80
67
60-140
18
ug/L
ND
20
20
15.9
13.0
79
65
60-140
20
ug/L
ND
20
20
15.1
12.5
76
62
60-140
19
ug/L
ND
20
20
16.4
13.7
82
69
60-140
18
ug/L
ND
20
20
17.1
14.0
85
70
60-140
20
ug/L
ND
40
40
32.8
27.2
82
68
60-140
19
ug/L
ND
20
20
13.3
11.1
64
53
60-140
18 MO
ug/L
ND
20
20
16.4
13.3
82
66
60-140
21
ug/L
ND
20
20
15.6
12.7
78
63
60-140
21
ug/L
ND
20
20
16.2
13.3
81
67
60-140
19
101
104
70-130
102
104
70-130
99
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc..
Page 18 of 26

;aceAnalytical"
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
QC Batch: MSV/30498 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92238263001, 92238263002
METHOD BLANK: 1398256
Associated Lab Samples: 92238263001, 92238263002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
NO
0.50
02/26/15 11:56
1,1,1-Trichloroethane
ug/L
NO
0.50
02/26/15 11:56
1,1,2,2-Tetrachloroethane
ug/L
NO
0.50
02/2611511:56
1,1,2-Trichloroethane
ug/L
NO
0.50
02/26/15 11:56
1,1-Dichloroethane
ug/L
ND
0.50
02/26/15 11:56
1,1-Dichloroethene
ug/L
NO
0.50
02/26/15 11:56
1,1-Dichloropropene
ug/L
NO
0.50
02/26/15 11:56
1,2,3-Trichlorobenzene
ug/L
NO
2.0
02/26/15 11:56
1,2,3-Trichloropropane
ug/L
ND
0.50
02/26/15 11:56
1,2,4-Trichlorobenzene
ug/L
ND
2.0
02/26/15 11:56
1,2,4-Trimethylbenzene
ug/L
NO
0.50
02/26/15 11:56
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
02/2611511:56
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
02/26/15 11:56
1,2-Dichlorobenzene
ug/L
NO
0.50
02/26/15 11:56
1,2-Dichloroethane
ug/L
ND
0.50
02/26/15 11:56
1,2-Dichloropropane
ug/L
ND
0.50
02/26/15 11:56
1,3,5-Trimethylbenzene
ug/L
ND
0.50
02/26/15 11:56
1,3-Dichlorobenzene
ug/L
ND
0.50
02/26/15 11:56
1,3-Dichloropropane
ug/L
NO
0.50
02/26/15 11:56
1,4-Dichlorobenzene
ug/L
ND
0.50
02/26/15 11:56
2,2-Dichloropropane
ug/L
NO
0.50
02/26/15 11:56
2-Chlorotoluene
ug/L
NO
0.50
02/2611511:56
4-Chlorotoluene
ug/L
NO
0.50
02/26/15 11:56
Benzene
ug/L
ND
0.50
02/26/15 11:56
Bromobenzene
ug/L
ND
0.50
02/26/15 11:56
Bromochloromethane
ug/L
NO
0.50
02/26/15 11:56
Bromodichloromethane
ug/L
ND
0.50
02/26/15 11:56
Bromoform
ug/L
NO
0.50
02/26/15 11:56
Bromomethane
ug/L
NO
5.0
02/26/15 11:56
Carbon tetrachloride
ug/L
NO
0.50
02/26/15 11:56
Chlorobenzene
ug/L
NO
0.50
02/26/15 11:56
Chloroethane
ug/L
ND
1.0
02/26/15 11:56
Chloroform
ug/L
NO
0.50
02/26/15 11:56
Chloromethane
ug/L
ND
1.0
02/26/15 11:56
cis- 1,2-Dichloroethene
ug/L
ND
0.50
02/26/15 11:56
cis-1,3-Dichloropropene
ug/L
ND
0.50
02/26/15 11:56
Dibromochloromethane
ug/L
NO
0.50
02126/1511:56
Dibromomethane
ug/L
NO
0.50
02/26/15 11:56
Dichlorodifluoromethane
ug/L
ND
0.50
02/26/15 11:56
Diisopropyl ether
ug/L
ND
0.50
02/26/15 11:56
Ethylbenzene
ug/L
ND
0.50
02/26/15 11:56
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 26

_ , aceAnalytical
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
METHOD BLANK: 1398256
Associated Lab Samples: 92238263001, 92238263002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
02/26/15 11:56
Isop ropylbenzene (Cumene)
ug/L
ND
0.50
02/26/15 11:56
m&p-Xylene
ug/L
ND
1.0
02/26/15 11:56
Methyl-tert-butyl ether
ug/L
ND
0.50
02/26/15 11:56
Methylene Chloride
ug/L
ND
2.0
02/26/15 11:56
n-Butylbenzene
ug/L
ND
0.50
02/26/15 11:56
n-Propylbenzene
ug/L
ND
0.50
02/26/15 11:56
Naphthalene
ug/L
ND
2.0
02/26/15 11:56
o-Xylene
ug/L
ND
0.50
02/26/15 11:56
sec-Butylbenzene
ug/L
ND
0.50
02/26/15 11:56
Styrene
ug/L
ND
0.50
02/26/15 11:56
tent-Butylbenzene
ug/L
ND
0.50
02/26/15 11:56
Tetrachloroethene
ug/L
ND
0.50
02/26/15 11:56
Toluene
ug/L
ND
0.50
02/26/15 11:56
trans-1,2-Dichloroethene
ug/L
ND
0.50
02/26/15 11:56
trans-1,3-Dichloropropene
ug/L
ND
0.50
02/26/15 11:56
Trichloroethene
ug/L
ND
0.50
02/26/15 11:56
Trichlorofluoromethane
ug/L
ND
1.0
02/26/15 11:56
Vinyl chloride
ug/L
ND
1.0
02/26/15 11:56
1,2-Dichloroethane-d4 (S)
%
103
70-130
02/26/15 11:56
4-Bromofluorobenzene (S)
%
97
70-130
02/26/15 11:56
Toluene-d8 (S)
%
101
70-130
02/26/15 11:56
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1398257
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.3
109
60-140
1,1,1-Trichloroethane
ug/L
50
51.8
104
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
50.4
101
60-140
1,1,2-Trichloroethane
ug/L
50
47.4
95
60-140
1,1-Dichloroethane
ug/L
50
46.5
93
60-140
1,1-Dichloroethene
ug/L
50
44.8
90
60-140
1,1-Dichloropropene
ug/L
50
52.0
104
60-140
1,2,3-Trichlorobenzene
ug/L
50
50.2
100
60-140
1,2,3-Trichloropropane
ug/L
50
49.2
98
60-140
1,2,4-Trichlorobenzene
ug/L
50
50.8
102
60-140
1,2,4-Trimethylbenzene
ug/L
50
50.7
101
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
55.0
110
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.1
102
60-140
1,2-Dichlorobenzene
ug/L
50
49.5
99
60-140
1,2-Dichloroethane
ug/L
50
46.9
94
60-140
1,2-Dichloropropane
ug/L
50
44.3
89
60-140
1,3,5-Trimethylbenzene
ug/L
50
50.0
100
60-140
1,3-Dichlorobenzene
ug/L
50
49.3
99
60-140
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 26

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
LABORATORY CONTROL SAMPLE:
1398257
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,3-Dichloropropane
ug/L
50
47.5
95
60-140
1,4-Dichlorobenzene
ug/L
50
48.5
97
60-140
2,2-Dichloropropane
ug/L
50
38.9
78
60-140
2-Chlorotoluene
ug/L
50
50.4
101
60-140
4-Chlorotoluene
ug/L
50
49.1
98
60-140
Benzene
ug/L
50
48.0
96
60-140
Bromobenzene
ug/L
50
49.4
99
60-140
Bromochloromethane
ug/L
50
47.6
95
60-140
Bromodichloromethane
ug/L
50
47.7
95
60-140
Bromoform
ug/L
50
42.2
84
60-140
Bromomethane
ug/L
50
52.8
106
60-140
Carbon tetrachloride
ug/L
50
57.8
116
60-140
Chlorobenzene
ug/L
50
47.5
95
60-140
Chloroethane
ug/L
50
42.7
85
60-140
Chloroform
ug/L
50
43.3
87
60-140
Chloromethane
ug/L
50
44.6
89
60-140
cis- 1,2-Dichloroethene
ug/L
50
48.3
97
60-140
cis-1,3-Dichloroprope ne
ug/L
50
50.4
101
60-140
Dibromochloromethane
ug/L
50
41.7
83
60-140
Dibromomethane
ug/L
50
49.5
99
60-140
Dichlorodifluoromethane
ug/L
50
45.9
92
60-140
Diisopropyl ether
ug/L
50
45.2
90
60-140
Ethylbenzene
ug/L
50
49.1
98
60-140
Hexachloro-1,3-butadiene
ug/L
50
49.3
99
60-140
Isopropylbenzene (Cumene)
ug/L
50
52.0
104
60-140
m&p-Xylene
ug/L
100
99.0
99
60-140
Methyl-tert-butyl ether
ug/L
50
41.5
83
60 140
Methylene Chloride
ug/L
50
49.5
99
60-140
n-Butylbenzene
ug/L
50
51.8
104
60-140
n-Propylbenzene
ug/L
50
49.0
98
60-140
Naphthalene
ug/L
50
51.6
103
60-140
o-Xylene
ug/L
50
48.0
96
60-140
sec-Butylbenzene
ug/L
50
51.9
104
60-140
Styrene
ug/L
50
53.2
106
60-140
tert-Butylbenzene
ug/L
50
50.6
101
60-140
Tetrachloroethene
ug/L
50
51.6
103
60-140
Toluene
ug/L
50
47.7
95
60-140
trans-1,2-Dichloroethene
ug/L
50
39.3
79
60-140
trans- 1,3-Dichloropropene
ug/L
50
51.4
103
60-140
Trichloroethene
ug/L
50
48.3
97
60-140
Trichlorofluoromethane
ug/L
50
49.3
99
60-140
Vinyl chloride
ug/L
50
42.6
85
60-140
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 26

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92238263
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1398258
MS
Parameter
1.1,1,2-Tetrachloroethane
1, 1. 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1, 2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethyl benzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
92238383007 Spike
Units Result Conc.
MSD
Spike
Conc.
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
20
20
ug/L
ND
40
40
ug/L
ND
20
20
ug/L
ND
20
20
1398259
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
21.5
21.2
107
106
60-140
1
22.5
22.8
112
114
60-140
1
21.6
22.2
108
111
60-140
3
20.7
20.4
104
102
60-140
1
21.5
20.9
108
105
60-140
3
20.4
20.9
102
105
60-140
2
23.9
23.5
119
117
60-140
2
21.2
22.0
106
110
60-140
4
20.1
20.7
100
104
60-140
3
21.4
21.9
107
110
60-140
2
22.5
22.7
113
113
60-140
1
18.5
20.7
93
104
60-140
11
20.4
21.3
102
106
60-140
4
21.3
21.7
106
108
60-140
2
20.3
20.4
102
102
60-140
0
19.7
19.8
99
99
60-140
1
22.8
22.6
114
113
60-140
1
21.4
21.3
107
106
60-140
1
20.9
20.9
104
104
60-140
0
21.5
21.5
107
107
60-140
0
15.0
15.2
75
76
60-140
1
21.7
22.1
108
110
60-140
2
21.7
21.8
109
109
60-140
1
21.9
21.4
110
107
60-140
3
22.2
21.7
111
109
60-140
2
21.2
21.3
106
106
60-140
0
18.3
18.8
91
94
60-140
3
15.3
15.8
77
79
60-140
3
27.9
26.7
140
134
60-140
4
23.4
24.0
117
120
60-140
3
21.8
21.1
109
105
60-140
3
20.8
20.9
104
104
60-140
0
19.5
19.0
97
95
60-140
2
21.0
19.4
105
97
60-140
8
21.8
21.6
109
108
60-140
1
19.1
19.3
96
96
60-140
1
16.5
16.6
82
83
60-140
1
20.4
20.3
102
101
60-140
1
21.6
21.9
108
109
60-140
1
20.7
20.5
103
103
60-140
1
22.4
21.9
112
109
60-140
3
24.1
25.3
120
127
60-140
5
23.2
22.7
116
113
60-140
2
45.4
42.7
114
107
60-140
6
18.4
18.1
92
91
60-140
2
21.1
21.0
105
105
60-140
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc..
Qua[
Page 22 of 26

_ 2ceAnalyfical'
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92238263
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1398258
1398259
MS
MSD
92238383007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
n-Buty[benzene
ug/L
ND
20
20
22.4
22.9
112
115
60-140
2
n-Propy[benzene
ug/L
ND
20
20
22.6
22.5
113
113
60-140
0
Naphthalene
ug/L
ND
20
20
20.9
22.1
104
110
60-140
6
o-Xylene
ug/L
ND
20
20
21.4
20.7
107
104
60-140
3
sec-Butylbenzene
ug/L
ND
20
20
23.4
23.4
117
117
60-140
0
Styrene
ug/L
ND
20
20
20.0
19.4
100
97
60-140
3
tert-Butylbenzene
ug/L
ND
20
20
22.7
22.7
114
114
60-140
0
Tetrachloroethene
ug/L
ND
20
20
23.6
22.3
118
111
60-140
6
Toluene
ug/L
ND
20
20
21.7
21.4
108
107
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.3
20.1
116
100
60-140
15
trans-1,3-Dichloropropene
ug/L
ND
20
20
19.9
19.8
100
99
60-140
1
Trichloroethene
ug/L
ND
20
20
21.2
21.1
106
105
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
23.2
22.9
116
114
60-140
1
Vinyl chloride
ug/L
ND
20
20
20.0
20.3
100
102
60-140
2
1,2-Dichloroethane-d4 (S)
%
98
98
70-130
4-Bromofluorobenzene(S)
%
103
101
70-130
Toluene-d8 (S)
%
101
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 26

I�ZAnalyticalo
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QUALIFIERS
Project: WALSER'S
Pace Project No.: 92238263
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
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Date: 02/27/2015 04:08 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 26

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: WALSER'S
Pace Project No.: 92238263
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92238263001
INFLUENT
MADEP VPH
GCV/9031
92238263002
EFFLUENT
MADEP VPH
GCV/9031
92238263002
EFFLUENT
EPA 200.7
MPRP/17941 EPA 200.7
92238263003
MW-1
SM 6200B
MSV/30474
92238263001
INFLUENT
SM 6200B
MSV/30498
92238263002
EFFLUENT
SM 6200B
MSV/30498
Date: 02/27/2015 04:08 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/16134
Page 25 of 26

/ .ZC Analyt al
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section 0 Section C I
Page : t_ Of 1
Required Client Information: Required Project Information: Invoice Information:
Company: Shield Engineering Report To: Flora D'Souza Attention: Flora D'Souza
Address: 4301 Taggart Creek Road Copy To: Company Name: Shield Engineering
Charlotte, NC 28208
address: 4301 Taggart Creek Road. Charlotte, N
Regulatory en
Email To: fdsouza shielden ineerin .com
Purchase Order No. 1990018
Pace Ouote Reference:
UST - Underground Storage Tank
Phone: [phone] JFax
Client Project ID: WALSER'S
Pace Project Manager. Laura Cooper
State I Location
Requested Due Oa:errAT: 10 Da Default
Container Order Number
Pace Profile a: i
North Carolina
Requested
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ADDITIONAL COMMENTS
RELINQUISHED I AFFLIATI N
DATE
71ME
ACCEPTED BY rAFFILIATION
DATE
TIME
SAMPLE CONDITIONS
IBY
9,00
SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER: r I\} t I� I
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SIGNATURE of SAMPLER:
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92238263

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRO qlMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUAL -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CEN RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Numb • Expl tin I�Date: 1 /31 /2018
Facility Name: Hill Oil Company, Inc. - Walser's Service
Non-Dis rge f 015102 UIC
Permit Name (if different):
NPD S
Facility Address: 6419 North Carolina Highway 150N
TYPE O PhKMI 17M OPERATION BEING MONITORED
Lex4natonNC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
-
❑ Spray Field ® Remediation: GrOUndWater
Contact Person: Flora D'Soliza_/Shield Enaineerina.
Inc. Telephone#:[phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
No. of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 1/22/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: 4 in.
pH 5.63 units Temp. NM OC
DRY at
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63
ft. Spec. Cond. NM µMhos
time ofsampling,
Measuring Point is NA ft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 1 /26/15 - 2/03/15
Laboratory Name: Pace Anal;rtical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD NA mg/l
Nitrite (NO2) as N
NA mg/I
Pb - Lead ND mg/1
Coliform: IMF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: IMF Total NA /100mi
Phosphorus: Total as P
NA mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
NA mg/I
Other'(Spg.Gify.,Gcmpoun& and Concentration Units):
Dissolved Solids: Total NA mg/I
Al - Aluminum
NA mg/I
pH (when analyzed) NA units
Ba - Barium
NA mg/I
►iAB A 4 9(11�i
TOC NA mg/I
Ca - Calcium
NA mg/I
Chloride NA mg/I
Cd - Cadmium
NA mg/1
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/1
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC , method # 6200B
Total Ammonia NA mg/1
Mg - Magnesium
NA mg/I
VPH method # MAnF=P VPH
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
NA mg/I
, method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 3.68604 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100%
GW-59 Rev.1/2007

APPENDIX A

��aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 05, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S
Pace Project No.: 92234783
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 23

1�laceAnalytical
i
www.pacelabs.com
I
Project: WALSER'S
Pace Project No.: 92234783
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 23

aceAnalXical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
WALSER'S
92234783
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92234783001
INFLUENT
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
92234783002
EFFLUENT
MADEP VPH
BFW
5
PASI-C
EPA 200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 23

aceAnalytical
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1
i
SUMMARY OF DETECTION
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
WALSER'S
92234783
Lab Sample ID
Client Sample ID
Method
Parameters
Result Units
Report Limit
Analyzed Qualifiers
92234783001
INFLUENT
MADEP VPH
Aliphatic (C05-008)
518 ug/L
250
01/29/15 17:17 N2
MADEP VPH
Aliphatic (C09-C12)
1400 ug/L
250
01/29/15 17:17 N2
SM 6200B
Benzene
18.3 ug/L
0.50
02/03/15 19:52
SM 6200B
1,2-Dibromoethane (EDB)
2.2 ug/L
0.50
02/03/15 19:52
SM 6200B
1,2-Dichloroethane
0.54 ug/L
0.50
02/03/15 19:52
SM 6200B
Ethylbenzene
108 ug/L
0.50
02/03/15 19:52
SM 6200B
Isopropylbenzene (Cumene)
6.9 ug/L
0.50
02/03/15 19:52
SM 6200B
Naphthalene
53.5 ug/L
2.0
02/03/15 19:52
SM 6200B
n-Propylbenzene
13.9 ug/L
0.50
02/03/15 19:52
SM 6200B
Toluene
727 ug/L
2.5
02/04/15 21:53
SM 6200B
1,2,4-Trimethylbenzene
112 ug/L
0.50
02/03/15 19:52
SM 6200B
1,3,5-Trimethylbenzene
53.7 ug/L
0.50
02/03/15 19:52
SM 6200B
m&p-Xylene
427 ug/L
5.0
02/04/15 21:53
SM 6200B
o-Xylene
245 ug/L
2.5
02/04/15 21:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 23

aceAnalXical
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l
I
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92234783
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: February 05, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/8947
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1377264)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• EFFLUENT (Lab ID: 92234783002)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCS (Lab ID: 1377265)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 23

Pace Analytical Services, Inc.
a
aceAnlXical ®
9800Hunte sv Ave. Suite 100
lle, C 28078
wwwpacelabs.com
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92234783
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: February 05, 2015
Analyte Comments:
QC Batch: GCW8947
N2: The lab does not hold TNI accreditation for this parameter.
• LCSD (Lab ID: 1377266)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
QC Batch: GCV/8957
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1378407)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• INFLUENT (Lab ID: 92234783001)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C 10)
• LCS (Lab ID: 1378408)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1378409)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
-Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 23

aceAnalXical
www-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92234783
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: February 05, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 23

1�laceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92234783
Method: SM 6200B
Description: 6200E MSV
Client: Shield
Date: February 05, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/30221
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92234783002
MO: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 1383356)
• Chloroethane
• Trichlorofluoromethane
• MSD (Lab ID: 1383357)
• Chloroethane
• Dichlorodifluoromethane
• Trichlorofluoromethane
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 23

aceAnalytical
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1
Project: WALSER'S
Pace Project No.: 92234783
Sample: INFLUENT
Parameters
►V1:J71 kiDAY =
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
[�Y�4�7-1 ��il►y�l
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobe nzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 02/05/2015 04:37 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92234783001 Collected: 01/22/15 13:00 Received: 01/23/15 14:56 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: MADEP VPH
518 ug/L
1400 ug/L
ND ug/L
88 %
82 %
Analytical Method: SM 6200B
18.3 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
2.2 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
0.54 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
108 ug/L
ND ug/L
6.9 ug/L
250
5
01/29/1517:17
250
5
01/29/1517:17
250
5
01/29/1517:17
70-130
5
01/29/1517:17
460-00-4
70-130
5
01/29/1517:17
460-00-4
0.50
1
02/03/15 19:52
71-43-2
0.50
1
02/03/15 19:52
108-86-1
0.50
1
02/03/15 19:52
74-97-5
0.50
1
02/03/15 19:52
75-27-4
0.50
1
02/03/15 19:52
75-25-2
5.0
1
02/03/15 19:52
74-83-9
0.50
1
02/03/15 19:52
104-51-8
0.50
1
02/03/15 19:52
135-98-8
0.50
1
02/03/15 19:52
98-06-6
0.50
1
02/03/15 19:52
56-23-5
0.50
1
02/03/15 19:52
108-90-7
1.0
1
02/03/15 19:52
75-00-3
0.50
1
02/03/15 19:52
67-66-3
1.0
1
02/03/15 19:52
74-87-3
0.50
1
02/03/15 19:52
95-49-8
0.50
1
02/03/15 19:52
106-43-4
1.0
1
02/03/15 19:52
96-12-8
0.50
1
02/03/15 19:52
124-48-1
0.50
1
02/03/15 19:52
106-93-4
0.50
1
02/03/15 19:52
74-95-3
0.50
1
02/03/15 19:52
95-50-1
0.50
1
02/03/15 19:52
541-73-1
0.50
1
02/03/15 19:52
106-46-7
0.50
1
02/03/15 19:52
75-71-8
0.50
1
02/03/15 19:52
75-34-3
0.50
1
02/03/15 19:52
107-06-2
0.50
1
02/03/15 19:52
75-35-4
0.50
1
02/03/15 19:52
156-59-2
0.50
1
02/03/15 19:52
156-60-5
0.50
1
02/03/15 19:52
78-87-5
0.50
1
02/03/15 19:52
142-28-9
0.50
1
02/03/15 19:52
594-20-7
0.50
1
02/03/15 19:52
563-58-6
0.50
1
02/03/15 19:52
10061-01-5
0.50
1
02/03/15 19:52
10061-02-6
0.50
1
02/03/15 19:52
108-20-3
0.50
1
02/03/15 19:52
100-41-4
2.0
1
02/03/15 19:52
87-68-3
0.50
1
02/03/15 19:52
98-82-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Qua[
N2
N2
N2
Page 9 of 23

aceAnalytical
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I
Project: WALSER'S
Pace Project No.: 92234783
Sample: INFLUENT
Parameters
6200E MSV
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrach loroetha ne
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trich loroethane
1,1,2-Trich loroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropa ne
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/05/2015 04:37 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92234783001 Collected: 01/22/15 13:00 Received: 01/23/15 14:56 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 6200B
ND ug/L
ND ug/L
53.5 ug/L
13.9 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
727 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
112 ug/L
53.7 ug/L
ND ug/L
427 ug/L
245 ug/L
105 %
102 %
100 %
2.0
1
02103/1519:52
75-09-2
0.50
1
02/03/15 19:52
1634-04-4
2.0
1
02/03/15 19:52
91-20-3
0.50
1
02/03/15 19:52
103-65-1
0.50
1
02/03/15 19:52
100-42-5
0.50
1
02/03/15 19:52
630-20-6
0.50
1
02/03/15 19:52
79-34-5
0.50
1
02/03/15 19:52
127-18-4
2.5
5
02/04/15 21:53
108-88-3
2.0
1
02/03/15 19:52
87-61-6
2.0
1
02/03/15 19:52
120-82-1
0.50
1
02/03/15 19:52
71-55-6
0.50
1
02/03/15 19:52
79-00-5
0.50
1
02/03/15 19:52
79-01-6
1.0
1
02/03/15 19:52
75-69-4
0.50
1
02/03/15 19:52
96-18-4
0.50
1
02/03/15 19:52
95-63-6
0.50
1
02/03/15 19:52
108-67-8
1.0
1
02/03/15 19:52
75-01-4
5.0
5
02/04/15 21:53
179601-23-1
2.5
5
02/04/15 21:53
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
02/03/15 19:52 17060-07-0
02/03/15 19:52 460-00-4
02/03/15 19:52 2037-26-5
Page 10 of 23

aceAnalytical
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Project: WALSER'S
Pace Project No.: 92234783
Sample: EFFLUENT
Parameters
VPH NC Water
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
200.7 MET ICP
Lead
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Date: 02/05/2015 04:37 PM
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92234783002 Collected: 01/22/15 14:00 Received: 01/23/15 14:56 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: MADEP VPH
ND ug/L
50.0
1
01/26/15 05:28
ND ug/L
50.0
1
01/26/15 05:28
ND ug/L
50.0
1
01/26/15 05:28
94 %
70-130
1
01/26/15 05:28
460-00-4
85 %
70-130
1
01/26/15 05:28
460-00-4
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
ND ug/L
5.0
1 01/26/15 15:20
01/27/15 05:06
7439-92-1
Analytical Method: SM 6200B
ND ug/L
0.50
1
02/03/15 16:13
71-43-2
ND ug/L
0.50
1
02/03/15 16:13
108-86-1
ND ug/L
0.50
1
02/03/15 16:13
74-97-5
ND ug/L
0.50
1
02/03/15 16:13
75-27-4
ND ug/L
0.50
1
02/03/15 16:13
75-25-2
ND ug/L
5.0
1
02/03/15 16:13
74-83-9
ND ug/L
0.50
1
02/03/15 16:13
104-51-8
ND ug/L
0.50
1
02/03/15 16:13
135-98-8
ND ug/L
0.50
1
02/03/15 16:13
98-06-6
ND ug/L
0.50
1
02/03/15 16:13
56-23-5
ND ug/L
0.50
1
02/03/15 16:13
108-90-7
ND ug/L
1.0
1
02/03/15 16:13
75-00-3
ND ug/L
0.50
1
02/03/15 16:13
67-66-3
ND ug/L
1.0
1
02/03/15 16:13
74-87-3
ND ug/L
0.50
1
02/03/15 16:13
95-49-8
ND ug/L
0.50
1
02/03/15 16:13
106-43-4
ND ug/L
1.0
1
02/03/15 16:13
96-12-8
ND ug/L
0.50
1
02/03/15 16:13
124-48-1
ND ug/L
0.50
1
02/03/15 16:13
106-93-4
ND ug/L
0.50
1
02/03/15 16:13
74-95-3
ND ug/L
0.50
1
02/03/15 16:13
95-50-1
ND ug/L
0.50
1
02/03/15 16:13
541-73-1
ND ug/L
0.50
1
02/03/15 16:13
106-46-7
ND ug/L
0.50
1
02/03/15 16:13
75-71-8
ND ug/L
0.50
1
02/03/15 16:13
75-34-3
ND ug/L
0.50
1
02/03/15 16:13
107-06-2
ND ug/L
0.50
1
02/03/15 16:13
75-35-4
ND ug/L
0.50
1
02/03/15 16:13
156-59-2
ND ug/L
0.50
1
02/03/15 16:13
156-60-5
ND ug/L
0.50
1
02/03/15 16:13
78-87-5
ND ug/L
0.50
1
02/03/15 16:13
142-28-9
ND ug/L
0.50
1
02/03/15 16:13
594-20-7
ND ug/L
0.50
1
02/03/15 16:13
563-58-6
ND ug/L
0.50
1
02/03/15 16:13
10061-01-5
ND ug/L
0.50
1
02/03/15 16:13
10061-02-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qua[
N2
N2
N2
Page 11 of 23

Pace Analytical Services, Inc.
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aceAnalXical Huntersville, NC 28078
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I
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92234783
Sample: EFFLUENT
Lab ID: 92234783002 Collected:
01/22/15
14:00
Received: 01/23/15 14:56 Matrix:
Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Diisopropyl ether
ND ug/L
0.50
1
02/03/15 16:13
108-20-3
Ethylbenzene
ND ug/L
0.50
1
02/03/15 16:13
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
2.0
1
02/03/15 16:13
87-68-3
Isopropylbenzene (Cumene)
ND ug/L
0.50
1
02/03/15 16:13
98-82-8
Methylene Chloride
ND ug/L
2.0
1
02/03/15 16:13
75-09-2
Methyl-tert-butyl ether
ND ug/L
0.50
1
02/03/15 16:13
1634-04-4
Naphthalene
ND ug/L
2.0
1
02/03/15 16:13
91-20-3
n-Propylbenzene
ND ug/L
0.50
1
02/03/15 16:13
103-65-1
Styrene
ND ug/L
0.50
1
02/03/15 16:13
100-42-5
1,1,1,2-Tetrachloroethane
ND ug/L
0.50
1
02/03/15 16:13
630-20-6
1,1,2,2-Tetrachloroethane
ND ug/L
0.50
1
02/03/15 16:13
79-34-5
Tetrachloroethene
ND ug/L
0.50
1
02/03/15 16:13
127-18-4
Toluene
ND ug/L
0.50
1
02/03/15 16:13
108-88-3
1,2,3-Trichlorobe nzene
ND ug/L
2.0
1
02/03/15 16:13
87-61-6
1,2,4-Trichlorobe nzene
ND ug/L
2.0
1
02/03/15 16:13
120-82-1
1,1,1-Trichloroethane
ND ug/L
0.50
1
02/03/15 16:13
71-55-6
1,1,2-Trichloroethane
ND ug/L
0.50
1
02/03/15 16:13
79-00-5
Trichloroethene
ND ug/L
0.50
1
02/03/15 16:13
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
1
02/03/15 16:13
75-69-4
1,2,3-Trichloropropane
ND ug/L
0.50
1
02/03/15 16:13
96-18-4
1,2,4-Trimethylbenzene
ND ug/L
0.50
1
02/03/15 16:13
95-63-6
1,3,5-Trimethylbenzene
ND ug/L
0.50
1
02/03/15 16:13
108-67-8
Vinyl chloride
ND ug/L
1.0
1
02/03/15 16:13
75-01-4
m&p-Xylene
ND ug/L
1.0
1
02/03/15 16:13
179601-23-1
o-Xylene
ND ug/L
0.50
1
02/03/15 16:13
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104 %
70-130
1
02/03/15 16:13
17060-07-0
4-Bromofluorobenzene (S)
100 %
70-130
1
02/03/15 16:13
460-00-4
Toluene-d8 (S)
100 %
70-130
1
02/03/15 16:13
2037-26-5
Date: 02/05/2015 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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1�laceAnalXica(
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
WALSER'S
Pace Project No.:
92234783
QC Batch:
GCV/8947 Analysis Method: MADEP VPH
QC Batch Method:
MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92234783002
METHOD BLANK: 1377264
Associated Lab Samples: 92234783002
Matrix: Water
Parameter
Units
Blank
Result
Aliphatic (C05-008)
ug/L
ND
Aliphatic (C09-C12)
ug/L
ND
Aromatic (C09-C10)
ug/L
ND
4-Bromofluorobenzene (FID) (S)
%
93
4-Bromofluorobenzene (PID) (S)
%
85
Reporting
Limit Analyzed Qualifiers
50.0
01125/1514:06 N2
50.0
01125/1514:06 N2
50.0
01/25/1514:06 N2
70-130
01/25/1514:06
70-130
01/25/1514:06
LABORATORY CONTROL SAMPLE & LCSD: 1377265
1377266
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
278
283
93
94
70-130 2 25 N2
Aliphatic (C09-C12)
ug/L
300
328
322
109
107
30-130 2 25 N2
Aromatic (C09-C10)
ug/L
100
94.5
95.6
95
96
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
96
95
70-130
4-Bromofluorobenzene (PID) (S)
%
92
90
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92234783
QC Batch: GCV/8957 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92234783001
METHOD BLANK: 1378407 Matrix: Water
Associated Lab Samples: 92234783001
Blank
Parameter Units Result
Aliphatic (C05-CO8) ug/L ND
Aliphatic (C09-C12) ug/L ND
Aromatic (C09-C10) ug/L ND
4-Bromofluorobe nzene (FID) (S) % 91
4-Bromofluorobenzene (PID) (S) % 83
LABORATORY CONTROL SAMPLE & LCSD: 1378408
Spike
Parameter Units Conc.
Aliphatic (C05-CO8) ug/L 300
Aliphatic (C09-C12) ug/L 300
Aromatic (C09-C10) ug/L 100
4-Bromofluorobenzene (FID) (S) %
4-Bromofluorobenzene (PID) (S) %
Reporting
Limit Analyzed Qualifiers
50.0
01/29/1514:40 N2
50.0
01 /29/15 14:40 N2
50.0
01/29/1514:40 N2
70-130
01/29/1514:40
70-130
01/29/1514:40
1378409
LCS
LCSD
LCS
LCSD
% Rec
Result
Result
% Rec
% Rec
Limits
259
256
86
85
70-130
274
289
91
96
30-130
86.8
87.0
87
87
70-130
94
90
70-130
90
86
70-130
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD RPD Qualifiers
1 25 N2
5 25 N2
0 25 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92234783
QC Batch: MPRP/17774 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92234783002
METHOD BLANK: 1377709
Associated Lab Samples: 92234783002
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE: 1377710
Parameter Units
Lead ug/L
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 01/27/15 04:18
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 473 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1377711 1377712
MS MSD
92234840004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L 15.3 500 500 451 459 87 89 70-130 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1377713 1377714
MS MSD
92234546001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L 5.4 500 500 465 463 92 92 70-130 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 23

/�WaceAnalXical-
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92234783
QC Batch: MSV/30221 Analysis Method: SM 6200B
QC Batch Method: SM 6200E Analysis Description: 6200E MSV
Associated Lab Samples: 92234783001, 92234783002
METHOD BLANK: 1383269
Associated Lab Samples: 92234783001, 92234783002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
02/03/15 13:25
1,1,1-Trichloroethane
ug/L
ND
0.50
02/03/15 13:25
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
02/03/15 13:25
1,1,2-Trichloroethane
ug/L
ND
0.50
02/03/15 13:25
1,1-Dichloroethane
ug/L
ND
0.50
02/03/15 13:25
1,1-Dichloroethene
ug/L
ND
0.50
02/03/15 13:25
1,1-Dichloropropene
ug/L
ND
0.50
02/03/15 13:25
1,2,3-Trichlorobenzene
ug/L
ND
2.0
02/03/15 13:25
1,2,3-Trichloropropane
ug/L
ND
0.50
02/0311513:25
1,2,4-Trichlorobenzene
ug/L
ND
2.0
02/03/15 13:25
1,2,4-Trimethylbenzene
ug/L
ND
0.50
02/03/15 13:25
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
02/03/15 13:25
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
02/03/15 13:25
1,2-Dichlorobenzene
ug/L
ND
0.50
02/03/15 13:25
1,2-Dichloroethane
ug/L
ND
0.50
02/03/15 13:25
1,2-Dichloropropane
ug/L
ND
0.50
02/03/15 13:25
1,3,5-Trimethylbenzene
ug/L
ND
0.50
02/0311513:25
1,3-Dichlorobenzene
ug/L
ND
0.50
02/03/15 13:25
1,3-Dichloropropane
ug/L
ND
0.50
02/03/15 13:25
1,4-Dichlorobenzene
ug/L
ND
0.50
02/03/15 13:25
2,2-Dichloropropane
ug/L
ND
0.50
02/03/15 13:25
2-Chlorotoluene
ug/L
ND
0.50
02/03/15 13:25
4-Chlorotoluene
ug/L
ND
0.50
02/03/15 13:25
Benzene
ug/L
ND
0.50
02/03/15 13:25
Bromobenzene
ug/L
ND
0.50
02/03/15 13:25
Bromochloromethane
ug/L
ND
0.50
02/03/15 13:25
Bromodichloromethane
ug/L
ND
0.50
02/03/15 13:25
Bromoform
ug/L
ND
0.50
02/03/15 13:25
Bromomethane
ug/L
ND
5.0
02/03/15 13:25
Carbon tetrachloride
ug/L
ND
0.50
02/03/15 13:25
Chlorobenzene
ug/L
ND
0.50
02/03/15 13:25
Chloroethane
ug/L
ND
1.0
02/03/15 13:25
Chloroform
ug/L
ND
0.50
02/03/15 13:25
Chloromethane
ug/L
ND
1.0
02/03/15 13:25
cis-1,2-Dichloroethene
ug/L
ND
0.50
02/03/15 13:25
cis- 1,3-Dichloroprope ne
ug/L
ND
0.50
02/03/15 13:25
Dibromochloromethane
ug/L
ND
0.50
02/03/15 13:25
Dibromomethane
ug/L
ND
0.50
02/03/15 13:25
Dichlorodifluoromethane
ug/L
ND
0.50
02/03/15 13:25
Diisopropyl ether
ug/L
ND
0.50
02/03/15 13:25
Ethylbenzene
ug/L
ND
0.50
02/03/15 13:25
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave- Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc. Page 16 of 23

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92234783
METHOD BLANK: 1383269
Matrix:
Water
Associated Lab Samples: 92234783001, 92234783002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
02/03/15 13:25
Isopropylbenzene (Cumene)
ug/L
ND
0.50
02/03/15 13:25
m&p-Xylene
ug/L
ND
1.0
02/03/15 13:25
Methyl-tert-butyl ether
ug/L
ND
0.50
02/03/15 13:25
Methylene Chloride
ug/L
ND
2.0
02/03/15 13:25
n-Butylbenzene
ug/L
ND
0.50
02/03/15 13:25
n-Propylbenzene
ug/L
ND
0.50
02/03/15 13:25
Naphthalene
ug/L
ND
2.0
02/03/15 13:25
o-Xylene
ug/L
ND
0.50
02/03/15 13:25
sec-Butylbenzene
ug/L
ND
0.50
02103/1513:25
Styrene
ug/L
ND
0.50
02/03/15 13:25
tert-Butylbenzene
ug/L
ND
0.50
02/03/15 13:25
Tetrachloroethene
ug/L
ND
0.50
02103/1513:25
Toluene
ug/L
ND
0.50
02/03/15 13:25
trans-1,2-Dichloroethene
ug/L
ND
0.50
02/03/15 13:25
trans-1,3-Dichloropropene
ug/L
ND
0.50
02/03/15 13:25
Trichloroethene
ug/L
ND
0.50
02/03/15 13:25
Trichlorofluoromethane
ug/L
ND
1.0
02/03/15 13:25
Vinyl chloride
ug/L
ND
1.0
02/03/15 13:25
1,2-Dichloroethane-d4 (S)
%
102
70-130
02/03/15 13:25
4-Bromofluorobenzene (S)
%
104
70-130
02/03/15 13:25
Toluene-d8 (S)
%
100
70-130
02/03/15 13:25
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1383270
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
53.0
106
60-140
1,1,1-Trichloroethane
ug/L
50
53.7
107
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.7
95
60-140
1,1,2-Trichloroethane
ug/L
50
52.7
105
60-140
1,1-Dichloroethane
ug/L
50
52.5
105
60-140
1,1-Dichloroethene
ug/L
50
52.3
105
60-140
1,1-Dichloropropene
ug/L
50
53.5
107
60-140
1,2,3-Trichlorobenzene
ug/L
50
48.5
97
60-140
1,2,3-Trichloropropane
ug/L
50
47.0
94
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.9
100
60-140
1,2,4-Trimethylbenzene
ug/L
50
48.7
97
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
45.1
90
60-140
1,2-Dibromoethane (EDB)
ug/L
50
50.6
101
60-140
1,2-Dichlorobenzene
ug/L
50
48.1
96
60-140
1,2-Dichloroethane
ug/L
50
53.4
107
60-140
1,2-Dichloropropane
ug/L
50
51.5
103
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.2
96
60-140
1,3-Dichlorobenzene
ug/L
50
47.0
94
60-140
Pace Analytical Services, Inc.
980o Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 23

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1
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92234783
LABORATORY CONTROL SAMPLE:
1383270
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
1,3-Dichloropropane
ug/L
50
48.8
98
60-140
1,4-Dichlorobenzene
ug/L
50
47.3
95
60-140
2,2-Dichloropropane
ug/L
50
53.9
108
60-140
2-Chlorotoluene
ug/L
50
47.4
95
60-140
4-Chlorotoluene
ug/L
50
47.2
94
60-140
Benzene
ug/L
50
53.3
107
60-140
Bromobenzene
ug/L
50
47.5
95
60-140
Bromochloromethane
ug/L
50
56.7
113
60-140
Bromodichloromethane
ug/L
50
51.8
104
60-140
Bromoform
ug/L
50
44.0
88
60-140
Bromomethane
ug/L
50
49.8
100
60-140
Carbon tetrachloride
ug/L
50
54.9
110
60-140
Chlorobenzene
ug/L
50
48.6
97
60-140
Chloroethane
ug/L
50
56.7
113
60-140
Chloroform
ug/L
50
49.0
98
60-140
Chloromethane
ug/L
50
49.7
99
60-140
cis-1,2-Dichloroethene
ug/L
50
54.4
109
60-140
cis- 1,3-Dich loropropene
ug/L
50
56.3
113
60-140
Dibromochloromethane
ug/L
50
50.9
102
60-140
Dibromomethane
ug/L
50
55.1
110
60-140
Dichlorodifluoromethane
ug/L
50
57.2
114
60-140
Diisopropyl ether
ug/L
50
53.0
106
60-140
Ethylbenzene
ug/L
50
48.5
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
48.4
97
60-140
Isopropylbenzene (Cumene)
ug/L
50
49.4
99
60-140
m&p-Xylene
ug/L
100
97.2
97
60-140
Methyl-tert-butyl ether
ug/L
50
52.8
106
60-140
Methylene Chloride
ug/L
50
55.5
111
60-140
n-Butylbenzene
ug/L
50
48.1
96
60-140
n-Propylbenzene
ug/L
50
46.0
92
60-140
Naphthalene
ug/L
50
45.9
92
60-140
o-Xylene
ug/L
50
47.7
95
60-140
sec-Butylbenzene
ug/L
50
46.3
93
60-140
Styrene
ug/L
50
52.0
104
60-140
tert-Butylbenzene
ug/L
50
37.6
75
60-140
Tetrachloroethene
ug/L
50
48.4
97
60-140
Toluene
ug/L
50
51.5
103
60-140
trans-1,2-Dichloroethene
ug/L
50
53.2
106
60-140
trans-1,3-Dichloropropene
ug/L
50
59.2
118
60-140
Trichloroethene
ug/L
50
50.1
100
60-140
Trichlorofluoromethane
ug/L
50
57.4
115
60-140
Vinyl chloride
ug/L
50
50.8
102
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluene-d8 (S)
%
103
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 23

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1
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92234783
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1383356
1383357
MS
MSD
92234783002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.6
22.7
108
113
60-140
5
1,1,1-Trichloroethane
ug/L
ND
20
20
24.0
24.8
120
124
60-140
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.4
20.9
102
104
60-140
2
1,1,2-Trichloroethane
ug/L
ND
20
20
22.7
23.0
113
115
60-140
1
1,1-Dichloroethane
ug/L
ND
20
20
23.8
24.2
119
121
60-140
2
1,1-Dichloroethene
ug/L
ND
20
20
24.5
25.3
122
127
60-140
3
1,1-Dichloropropene
ug/L
ND
20
20
24.6
25.2
123
126
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
19.5
20.7
97
104
60-140
6
1,2,3-Trichloropropane
ug/L
ND
20
20
20.5
21.1
102
105
60-140
3
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.4
21.3
102
107
60-140
4
1,2,4-Trimethylbenzene
ug/L
ND
20
20
21.4
22.0
107
110
60-140
3
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
18.0
18.7
90
93
60-140
4
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.0
22.4
110
112
60-140
2
1,2-Dichlorobenzene
ug/L
ND
20
20
20.8
21.4
104
107
60-140
3
1,2-Dichloroethane
ug/L
ND
20
20
23.7
23.5
118
118
60-140
0
1,2-Dichloropropane
ug/L
ND
20
20
22.2
22.6
111
113
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
21.0
21.8
105
109
60-140
4
1,3-Dichlorobenzene
ug/L
ND
20
20
20.3
21.0
101
105
60-140
4
1,3-Dichloropropane
ug/L
ND
20
20
21.3
21.2
107
106
60-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
20.3
21.0
101
105
60-140
4
2,2-Dichloropropane
ug/L
ND
20
20
23.1
23.0
115
115
60-140
0
2-Chlorotoluene
ug/L
ND
20
20
20.6
21.3
103
106
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
20.6
21.2
103
106
60-140
3
Benzene
ug/L
ND
20
20
24.2
24.3
121
121
60-140
0
Bromobenzene
ug/L
ND
20
20
20.3
21.0
102
105
60-140
3
Bromochloromethane
ug/L
ND
20
20
25.0
24.7
125
124
60-140
1
Bromodichloromethane
ug/L
ND
20
20
21.3
21.6
106
108
60-140
2
Bromoform
ug/L
ND
20
20
17.4
18.2
87
91
60-140
4
Bromomethane
ug/L
ND
20
20
18.2
18.3
91
92
60-140
0
Carbon tetrachloride
ug/L
ND
20
20
22.8
24.9
114
125
60-140
9
Chlorobenzene
ug/L
ND
20
20
20.9
21.5
105
107
60-140
3
Chloroethane
ug/L
ND
20
20
29.1
28.8
146
144
60-140
1 MO
Chloroform
ug/L
ND
20
20
22.0
21.9
110
110
60-140
0
Chloromethane
ug/L
ND
20
20
21.2
22.0
106
110
60-140
4
cis-1,2-Dichloroethene
ug/L
ND
20
20
24.1
24.2
121
121
60-140
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.6
23.0
113
115
60-140
2
Dibromochloromethane
ug/L
ND
20
20
19.3
20.1
96
100
60-140
4
Dibromomethane
ug/L
ND
20
20
23.0
23.6
115
118
60-140
3
Dichlorodifluoromethane
ug/L
ND
20
20
27.8
29.1
139
146
60-140
5 MO
Diisopropyl ether
ug/L
ND
20
20
23.4
23.4
117
117
60-140
0
Ethylbenzene
ug/L
ND
20
20
21.4
21.9
107
109
60-140
2
Hexachloro-1,3-butadiene
ug/L
ND
20
20
19.6
21.3
98
106
60-140
8
Isopropylbenzene (Cumene)
ug/L
ND
20
20
21.7
22.2
109
111
60-140
2
m&p-Xylene
ug/L
ND
40
40
43.0
44.4
107
111
60-140
3
Methyl-tert-butyl ether
ug/L
ND
20
20
22.9
22.9
115
114
60-140
0
Methylene Chloride
ug/L
ND
20
20
24.6
24.1
123
120
60-140
2
Results presented on this page are in
the units indicated by the
"Units" column
except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc. Page 19 of 23

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I
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92234783
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1383356
1383357
MS
MSD
92234783002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
20.5
21.4
102
107
60-140
4
n-Propylbenzene
ug/L
ND
20
20
20.5
21.0
103
105
60-140
2
Naphthalene
ug/L
ND
20
20
19.0
20.0
95
100
60-140
5
o-Xylene
ug/L
ND
20
20
21.1
21.1
105
106
60-140
0
sec-Butylbenzene
ug/L
ND
20
20
20.3
21.4
101
107
60-140
5
Styrene
ug/L
ND
20
20
22.5
22.7
113
114
60-140
1
tert-Butylbenzene
ug/L
ND
20
20
16.5
17.1
83
86
60-140
4
Tetrachloroethene
ug/L
ND
20
20
21.3
22.2
105
110
60-140
4
Toluene
ug/L
ND
20
20
22.9
23.1
114
116
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.1
24.4
120
122
60-140
1
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.8
23.3
114
116
60-140
2
Trichloroethene
ug/L
ND
20
20
22.2
22.6
111
113
60-140
2
Trichlorofluoromethane
ug/L
ND
20
20
28.5
29.5
143
147
60-140
3 MO
Vinyl chloride
ug/L
ND
20
20
24.0
24.9
120
124
60-140
4
1,2-Dichloroethane-d4 (S)
%
100
99
70-130
4-Bromofluorobenzene (S)
%
105
106
70-130
Toluene-d8 (S)
%
101
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc..
Page 20 of 23

'aceAnalXical
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I
QUALIFIERS
Project: WALSER'S
Pace Project No.: 92234783
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
N2 The lab does not hold TNI accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
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Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc.. Page 21 of 23

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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
WALSER'S
92234783
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92234783001
INFLUENT
MADEP VPH
GCV/8957
92234783002
EFFLUENT
MADEP VPH
GCV/8947
92234783002
EFFLUENT
EPA 200.7
MPRP/17774 EPA 200.7 ICP/16002
92234783001
INFLUENT
SM 6200B
MSV/30221
92234783002
EFFLUENT
SM 6200B
MSV/30221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2015 04:37 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 23

M
N
O
M
CHAIN -OF -CUSTODY / Analytical Request Document
3CeAn2tytiCa! The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
a
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page : 1 Of t
Company: Shield Engineering Report To: Flora D'Souza Attention: Flora D'Souza
Address 4301 Taggart Creek Road Copy To: Company Name: Shield Engineering
Charlotte, NC 28208
Address: 4301 Taqqart Creek Road, Charlotte, N
Regulatory Agency
Email To. [e-mail]
Purchase Order No. 1990018
Pace Quote Reference:
UST - Underground Storage Tank
Phone [phone] Fax
Client Project ID: WALSER'S
Paco Project Manager. Benjamin, Nicole
State t Location
Requested Due DaterrAT: 10 Da Default
Container Order Number.
Pace Profile #:
North Carolina
Requested
Analysis
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ADDITIONAL COMMENTS
RELINQUISHED BY/AFFILIATION
DATE
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ACCEPTED BYAFFILIATION
DATE
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SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
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DATE Signed: �� r—
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SUBMIT FORM ON YELLOW OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IM'617
(VISION OF WATER QUALITY -INFORM ATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 1/31/2018
Facility Name: HIII Oil Company, Inc. - Walser's Service
Non -Discharge WQ0015102 UIC
Permit Name (if different):
NPDES Other
Facility Address: 6419 North Carolina Hiahwav 15ON
TYPE OF PERMITTED OPERATION BEING MONITORED
NC 27295
County Davidson
❑ Lagoon ❑ Remediation: Infiltration Gallery
Slm�'
❑ Spray Field ® Remediation: GrOUndWater
Contact Person: Flora D'Souza/Shield Enaineerina. Inc.
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Walser's Service
Nom of wells to be sampled: NA
❑ Water Source Heat Pump ❑ Other:
from
Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): VERW-1
Date sample collected: 4/14/15
FIELD ANALYSES:
WAS
Well Depth: 63 ft.
Well Diameter: 4 in.
pH 6.29 units Temp. NM °C
DRY at
Depth to Water Level: NM ft. below measuring point
Screened Interval: 33 ft.
to 63
ft. Spec. Cond. NM µ Mhos
time of
sampling,
Measuring Point is Ngft. above land surface
Relative M.P. Elevation: NA ft.
Odor
check
Volume of water pumped/bailed before sampling:
NA gallons
Appearance
here:
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 4/17/15 - 4/26/15
Laboratory Name: Pace Analytical
Services
Certification No. 12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD NA mg/I
Nitrite (NO2) as N
NA mg/I
Pb - Lead 0.0052 mg/I
Coliform: MF Fecal NA /100ml
Nitrate (NO3) as N
NA mg/I
Zn - Zinc NA mg/I
Coliform: MF Total NA /100mi
Phosphorus: Total as P
NA mg/I
(Note. Use MPN method for highly turbid samples) r
Orthophosphate
NA mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total NA mg/I
,,q�( luminum
JUN 0 2 LU
NA mg/I
Aliphatic (C5-C8) = 0.107 mg/L
pH (when analyzed) NA units
a - Barium
NA mg/I
Aliphatic (C9-C12) = 0.0587 mg/L
TOC NA mg/I
DER SECT(f�Ca - Calcium
11
NA mg/I
Chloride NA mg/+,FORMATION PR" Cd - Cadmium
NA mg/I
Arsenic NA mg/I
Chromium: Total
NA mg/I
Grease and Oils NA mg/I
Cu - Copper
NA mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol NA mg/I
Fe - Iron
NA mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate NA mg/I
Hg - Mercury
NA mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance NA µMhos
K - Potassium
NA mg/I
VOC method # 6200B
Total Ammonia NA mg/I
Mg - Magnesium
NA mg/I
VPH method # MAnFP VPH
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
NA mg/I
,method #
TKN as N NA mg/I
Ni - Nickel
NA mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 13.4672 mg/L Effluent Total VOCs: 0.1657 mg/L VOC Removal% 98.77%
Flora D'Souza/Shield Enaineerina. Proiect Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

APPENDIX A

aceAnalXical
www.pacelabs.com
May 06, 2015
Ms. Flora D'Souza
Shield Engineering
4301 Taggart Creek Road
Charlotte, NC 28208
RE: Project: WALSER'S
Pace Project No.: 92245619
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Ms. D'Souza:
Enclosed are the analytical results for sample(s) received by the laboratory on April 15, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Revised report issued on 5/6/15 to include all VPH reportable compounds for sample 002.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 22

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: WALSER'S
Pace Project No.: 92245619
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
WALSER'S
92245619
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92245619001
EFF
MADEP VPH
BFW
5
PASI-C
EPA200.7
JMW
1
PASI-A
SM 6200B
CAH
63
PASI-C
92245619002
INF
MADEP VPH
BFW
5
PASI-C
SM 6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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SUMMARY OF DETECTION
Project:
WALSER'S
Pace Project No.:
92245619
Lab Sample ID
Client Sample ID
Method
Parameters
92245619001
EFF
MADEP VPH
Aliphatic (C05-008)
MADEP VPH
Aliphatic (C09-C12)
EPA 200.7
Lead
92245619002
INF
MADEP VPH
Aliphatic (C05-CO8)
MADEP VPH
Aliphatic (C09-C12)
MADEP VPH
Aromatic (C09-C10)
SM 6200B
Benzene
SM 6200B
1,2-Dibromoethane (EDB)
SM 6200B
Ethylbenzene
SM 6200B
Isopropylbenzene (Cumene)
SM 6200B
Naphthalene
SM 6200B
n-Propylbenzene
SM 6200B
Toluene
SM 6200B
1,2,4-Trimethylbenzene
SM 6200B
1,3,5-Trimethyl benzene
SM 6200B
m&p-Xylene
SM 6200B
o-Xylene
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Result Units Report Limit Analyzed
107
ug/L
50.0
04/26/15 21:43
N2
58.7
ug/L
50.0
04/26/15 21:43
N2
5.2
ug/L
5.0
04/17/15 18:28
4370
ug/L
500
04/26/15 22:10
N2
4600
ug/L
500
04/26/15 22:10
N2
1010
ug/L
500
04/26/15 22:10
N2
35.0
ug/L
2.5
04/22/15 04:16
8.4
ug/L
2.5
04/22/15 04:16
210
ug/L
2.5
04/22/15 04:16
12.9
ug/L
2.5
04/22/15 04:16
89.4
ug/L
10.0
04/22/15 04:16
30.4
ug/L
2.5
04/22/15 04:16
1590
ug/L
6.2
04/22/1515:03
195
ug/L
2.5
04/22/15 04:16
87.1
ug/L
2.5
04/22/15 04:16
764
ug/L
5.0
04/22/15 04:16
465
ug/L
2.5
04/22/15 04:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 4 of 22

Ice Analytical
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PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92245619
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: May 06, 2015
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
2 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: GCV/9260
R1: RPD value was outside control limits.
• LCSD (Lab ID: 1443760)
• Aliphatic (C05-008)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: GCV/9260
N2: The lab does not hold TNI accreditation for this parameter.
• BLANK (Lab ID: 1443758)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92245619
Method: MADEP VPH
Description: VPH NC Water
Client: Shield
Date: May 06, 2015
Analyte Comments
QC Batch: GCV/9260
N2: The lab does not hold TNI accreditation for this parameter.
• EFF (Lab ID: 92245619001)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
•INF (Lab ID:92245619002)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C 10)
• LCS (Lab ID: 1443759)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
• LCSD (Lab ID: 1443760)
• Aliphatic (C05-CO8)
• Aliphatic (C09-C12)
• Aromatic (C09-C10)
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92245619
Method: EPA 200.7
Description: 200.7 MET ICP
Client: Shield
Date: May 06, 2015
General Information:
1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 7 of 22

* / ) 7 0
aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: WALSER'S
Pace Project No.: 92245619
Method: SM 6200B
Description: 6200B MSV
Client: Shield
Date: May 06, 2015
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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i
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92245619
Sample: EFF
Lab ID: 92245619001 Collected:
04/14/15 14:00 Received: 04/15/15 15:46 Matrix: Water
Parameters
Results
Units Report Limit
DF Prepared
Analyzed
CAS No.
Qual
VPH NC Water
Analytical Method: MADEP VPH
Aliphatic (C05-008)
107
ug/L
50.0
1
04/26/15 21:43
N2
Aliphatic (C09-C12)
58.7
ug/L
50.0
1
04/26/15 21:43
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
04/26/15 21:43
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
95
%
70-130
1
04/26/15 21:43
460-00-4
4-Bromofluorobenzene (PID) (S)
94
%
70-130
1
04/26/15 21:43
460-00-4
200.7 MET ICP
Analytical Method:
EPA 200.7 Preparation Method: EPA 200.7
Lead
6.2
ug/L
5.0
1 04/16/1514:55
04/17/1518:28
7439-92-1
6200E MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
04/22/15 01:15
71-43-2
Bromobenzene
ND
ug/L
0.50
1
04/22/15 01:15
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
04/22/15 01:15
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
04/22/15 01:15
75-27-4
Bromoform
ND
ug/L
0.50
1
04/22/15 01:15
75-25-2
Bromomethane
ND
ug/L
5.0
1
04/22/15 01:15
74-83-9
n-Butylbenzene
ND
ug/L
0,50
1
04/22/15 01:15
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
04/22/15 01:15
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
04/22/15 01:15
108-90-7
Chloroethane
ND
ug/L
1.0
1
04/22/15 01:15
75-00-3
Chloroform
ND
ug/L
0.50
1
04/22/15 01:15
67-66-3
Chloromethane
ND
ug/L
1.0
1
04/22/15 01:15
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
04/22/15 01:15
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
04/22/15 01:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
04/22/15 01:15
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
04/22/15 01:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
04/22/15 01:15
106-93-4
Dibromomethane
ND
ug/L
0.50
1
04/22/15 01:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
04/22/15 01:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
04/22/15 01:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
04/22/15 01:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
04/22/15 01:15
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
04/22/15 01:15
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
04/22/15 01:15
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
04/22/15 01:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
04/22/15 01:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
04/22/15 01:15
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
04/22/15 01:15
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
04/22/15 01:15
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
04/22/15 01:15
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
04/22/15 01:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
04/22/15 01:15
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
1
04/22/15 01:15
10061-02-6
REPORT OF LABORATORY ANALYSIS
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except in full,
Date: 05/06/2015 11:26 AM
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Page 9 of 22

Pace Analytical Services, Inc.
® 9800 Kincey Ave. Suite 100
1!;ace Analytical Huntersville, NC 28078
i www.pacelabs.com [phone]
i
ANALYTICAL RESULTS
Project: WALSER'S
Pace Project No.: 92245619
Sample: EFF
Lab ID: 92245619001 Collected:
04/14/15 14:00
Received: 04/15/15 15 46 Matrix:
Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200E MSV
Analytical Method: SM 6200B
Diisopropyl ether
ND
ug/L
0.50
1
04/22/15 01:15
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
04/22/15 01:15
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
04/22/15 01:15
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
04/22/15 01:15
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
04/22/15 01:15
1634-04-4
Naphthalene
ND
ug/L
2.0
1
04/22/15 01:15
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
103-65-1
Styrene
ND
ug/L
0.50
1
04/22/15 01:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
04/22/15 01:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
04/22/15 01:15
79-34-5
Tetra chloroethene
ND
ug/L
0.50
1
04/22/15 01:15
127-18-4
Toluene
ND
ug/L
0.50
1
04/22/15 01:15
108-88-3
1,2,3-Trichlorobe nzene
ND
ug/L
2.0
1
04/22/15 01:15
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
04/22/15 01:15
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
04/22/15 01:15
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
1
04/22/15 01:15
79-00-5
Trichloroethene
ND
ug/L
0.50
1
04/22/15 01:15
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
04/22/15 01:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
04/22/15 01:15
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
04/22/15 01:15
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
04/22/15 01:15
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
04/22/15 01:15
179601-23-1
o-Xylene
ND
ug/L
0.50
1
04/22/15 01:15
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
04/22/15 01:15
17060-07-0
4-13romofluorobenzene (S)
97
%
70-130
1
04/22/15 01:15
460-00-4
Toluene-d8 (S)
98
%
70-130
1
04/22/15 01:15
2037-26-5
Date: 05/06/2015 11:26 AM
REPORT OF LABORATORY ANALYSIS
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Project: WALSER'S
Pace Project No.: 92245619
Sample: INF
Parameters
VPH NC Water
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
6200E MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Date: 05/06/2015 11:26 AM
Pace Analytical Services, Inc.
9800 KinceyAve Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92245619002 Collected: 04/14/15 15:06 Received: 04/15/15 15:46 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: MADEP VPH
4370 ug/L
4600 ug/L
1010 ug/L
98
%
98
%
Analytical Method: SM 6200B
35.0
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
8.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
210
ug/L
ND
ug/L
12.9
ug/L
500
10
04/26/15 22:10
500
10
04/26/15 22:10
500
10
04/26/15 22:10
70-130
10
04/26/15 22:10
460-00-4
70-130
10
04/26/15 22:10
460-00-4
2.5
5
04/22/15 04:16
71-43-2
2.5
5
04/22/15 04:16
108-86-1
2.5
5
04/22/15 04:16
74-97-5
2.5
5
04/22/15 04:16
75-27-4
2.5
5
04/22/15 04:16
75-25-2
25.0
5
04/22/15 04:16
74-83-9
2.5
5
04/22/15 04:16
104-51-8
2.5
5
04/22/15 04:16
135-98-8
2.5
5
04/22/15 04:16
98-06-6
2.5
5
04/22/15 04:16
56-23-5
2.5
5
04/22/15 04:16
108-90-7
5.0
5
04/22/15 04:16
75-00-3
2.5
5
04/22/15 04:16
67-66-3
5.0
5
04/22/15 04:16
74-87-3
2.5
5
04/22/15 04:16
95-49-8
2.5
5
04/22/15 04:16
106-43-4
5.0
5
04/22/15 04:16
96-12-8
2.5
5
04/22/15 04:16
124-48-1
2.5
5
04/22/15 04:16
106-93-4
2.5
5
04/22/15 04:16
74-95-3
2.5
5
04/22/15 04:16
95-50-1
2.5
5
04/22/15 04:16
541-73-1
2.5
5
04/22/15 04:16
106-46-7
2.5
5
04/22/15 04:16
75-71-8
2.5
5
04/22/15 04:16
75-34-3
2.5
5
04/22/15 04:16
107-06-2
2.5
5
04/22/15 04:16
75-35-4
2.5
5
04/22/15 04:16
156-59-2
2.5
5
04/22/15 04:16
156-60-5
2.5
5
04/22/15 04:16
78-87-5
2.5
5
04/22/15 04:16
142-28-9
2.5
5
04/22/15 04:16
594-20-7
2.5
5
04/22/15 04:16
563-58-6
2.5
5
04/22/15 04:16
10061-01-5
2.5
5
04/22/15 04:16
10061-02-6
2.5
5
04/22/15 04:16
108-20-3
2.5
5
04/22/15 04:16
100-41-4
10.0
5
04/22/15 04:16
87-68-3
2.5
5
04/22/15 04:16
98-82-8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
N2
N2
N2
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WALSER'S
Pace Project No.: 92245619
Sample: INF Lab ID: 92245619002 Collected: 04/14/15 15:06 Received: 04/15/15 15:46 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Methylene Chloride
ND
ug/L
10.0
5
04/22/15 04:16
75-09-2
Methyl-tert-butyl ether
ND
ug/L
2.5
5
04/22/15 04:16
1634-04-4
Naphthalene
89.4
ug/L
10.0
5
04/22/15 04:16
91-20-3
n-Propylbenzene
30.4
ug/L
2.5
5
04/22/15 04:16
103-65-1
Styrene
ND
ug/L
2.5
5
04/22/15 04:16
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
2.5
5
04/22/15 04:16
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
2.5
5
04/22/15 04:16
79-34-5
Tetra chloroethene
ND
ug/L
2.5
5
04/22/15 04:16
127-18-4
Toluene
1590
ug/L
6.2
12.5
04/22/1515:03
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
10.0
5
04/22/15 04:16
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
10.0
5
04/22/15 04:16
120-82-1
1,1,1-Trichloroethane
ND
ug/L
2.5
5
04/22/15 04:16
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.5
5
04/22/15 04:16
79-00-5
Trichloroethene
ND
ug/L
2.5
5
04/22/15 04:16
79-01-6
Trichlorofluoromethane
ND
ug/L
5.0
5
04/22/15 04:16
75-69-4
1,2,3-Trichloropropane
ND
ug/L
2.5
5
04/22/15 04:16
96-18-4
1,2,4-Trimethylbenzene
195
ug/L
2.5
5
04/22/15 04:16
95-63-6
1,3,5-Trimethylbenzene
87.1
ug/L
2.5
5
04/22/15 04:16
108-67-8
Vinyl chloride
ND
ug/L
5.0
5
04/22/15 04:16
75-01-4
m&p-Xylene
764
ug/L
5.0
5
04/22/15 04:16
179601-23-1
o-Xylene
465
ug/L
2.5
5
04/22/15 04:16
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
5
04/22/15 04:16
17060-07-0
4-Bromofluorobenzene (S)
98
%
70-130
5
04/22/15 04:16
460-00-4
Toluene-d8 (S)
97
%
70-130
5
04/22/15 04:16
2037-26-5
Date: 05/06/2015 11:26 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
QC Batch: GCV/9260
QC Batch Method: MADEP VPH
Associated Lab Samples: 92245619001, 92245619002
Analysis Method:
Analysis Description:
MADEP VPH
VPH NC Water
METHOD BLANK: 1443758
Matrix: Water
Associated Lab Samples: 92245619001, 92245619002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
ug/L
ND
50.0
04/26/15 19:32 N2
Aliphatic (C09-C12)
ug/L
ND
50.0
04/26/15 19:32 N2
Aromatic (C09-C10)
ug/L
ND
50.0
04/26/15 19:32 N2
4-Bromofluorobenzene (FID) (S)
%
99
70-130
04/26/15 19:32
4-Bromofluorobenzene (PID) (S)
%
97
70-130
04/26/15 19:32
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
1443759
1443760
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
Aliphatic (C05-008)
ug/L
300
223
300
74
100
70-130
29 25 N2,R1
Aliphatic (C09-C12)
ug/L
300
253
375
84
125
30-130
39 25 N2,R1
Aromatic (C09-C10)
ug/L
100
83.8
119
84
119
70-130
35 25 N2,R1
4-Bromofluorobenzene (FID) (S)
%
96
98
70-130
4-Bromofluorobenzene (PID) (S)
%
97
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
QC Batch: MPRP/18289 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92245619001
METHOD BLANK: 1436374 Matrix: Water
Associated Lab Samples: 92245619001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 04/1711517:49
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1436375
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 480 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1436376 1436377
MS MSD
92245140002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 468 474 94 95 70-130 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1436378 1436379
MS MSD
92245262002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 484 479 97 96 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
QC Batch: MSV/31308
QC Batch Method: SM 6200B
Associated Lab Samples: 92245619001, 92245619002
Analysis Method:
Analysis Description:
SM 6200B
6200B MSV
METHOD BLANK: 1439866
Matrix: Water
Associated Lab Samples: 92245619001,
92245619002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
04/22/15 00:25
1,1,1-Trichloroethane
ug/L
ND
0.50
04/22/15 00:25
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
04/22/15 00:25
1,1,2-Trichloroethane
ug/L
ND
0.50
04/22/15 00:25
1,1-Dichloroethane
ug/L
ND
0.50
04/22/15 00:25
1,1-Dichloroethene
ug/L
ND
0.50
04/22/15 00:25
1,1-Dichloropropene
ug/L
ND
0.50
04/22/15 00:25
1,2,3-Trichlorobenzene
ug/L
ND
2.0
04/22/15 00:25
1,2,3-Trichloropropane
ug/L
ND
0.50
04/22/15 00:25
1,2,4-Trichlorobenzene
ug/L
ND
2.0
04/22/15 00:25
1,2,4-Trimethylbenzene
ug/L
ND
0.50
04/22/15 00:25
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
04/22/15 00:25
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
04/22/15 00:25
1,2-Dichlorobenzene
ug/L
ND
0.50
04/22/15 00:25
1,2-Dichloroethane
ug/L
ND
0.50
04/22/15 00:25
1,2-Dichloropropane
ug/L
ND
0.50
04/22/15 00:25
1,3,5-Trimethylbenzene
ug/L
ND
0.50
04/22/15 00:25
1,3-Dichlorobenzene
ug/L
ND
0.50
04/22/15 00:25
1,3-Dichloropropane
ug/L
ND
0.50
04/22/15 00:25
1,4-Dichlorobenzene
ug/L
ND
0.50
04/22/15 00:25
2,2-Dichloropropane
ug/L
ND
0.50
04/22/15 00:25
2-Chlorotoluene
ug/L
ND
0.50
04/22/15 00:25
4-Chlorotoluene
ug/L
ND
0.50
04/22/15 00:25
Benzene
ug/L
ND
0.50
04/22/15 00:25
Bromobenzene
ug/L
ND
0.50
04/22/15 00:25
Bromochloromethane
ug/L
ND
0.50
04/22/15 00:25
Bromodichloromethane
ug/L
ND
0.50
04/22/15 00:25
Bromoform
ug/L
ND
0.50
04/22/15 00:25
Bromomethane
ug/L
ND
5.0
04/22/15 00:25
Carbon tetrachloride
ug/L
ND
0.50
04/22/15 00.25
Chlorobenzene
ug/L
ND
0.50
04/22/15 00.25
Chloroethane
ug/L
ND
1.0
04/22/15 00:25
Chloroform
ug/L
ND
0.50
04/22/15 00:25
Chloromethane
ug/L
ND
1.0
04/22/15 00:25
cis-1,2-Dichloroethene
ug/L
ND
0.50
04/22/15 00:25
cis-1,3-Dichloropropene
ug/L
ND
0.50
04/22/15 00:25
Dibromochloromethane
ug/L
ND
0.50
04/22/15 00:25
Dibromomethane
ug/L
ND
0.50
04/22/15 00:25
Dichlorodifluoromethane
ug/L
ND
0.50
04/22/15 00:25
Diisopropyl ether
ug/L
ND
0.50
04/22/15 00:25
Ethylbenzene
ug/L
ND
0.50
04/22/15 00:25
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 22

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
METHOD BLANK: 1439866
Associated Lab Samples: 92245619001, 92245619002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
04/22/15 00:25
Isopropylbenzene (Cumene)
ug/L
ND
0.50
04/22/15 00:25
m&p-Xylene
ug/L
ND
1.0
04/22/15 00:25
Methyl-tert-butyl ether
ug/L
ND
0.50
04/22/15 00:25
Methylene Chloride
ug/L
ND
2.0
04/22/15 00:25
n-Butylbenzene
ug/L
ND
0.50
04/22/15 00:25
n-Propylbenzene
ug/L
ND
0.50
04/22/15 00:25
Naphthalene
ug/L
ND
2.0
04/22/15 00:25
o-Xylene
ug/L
ND
0.50
04/22/15 00:25
sec-Butylbenzene
ug/L
ND
0.50
04/22/15 00:25
Styrene
ug/L
ND
0.50
04/22/15 00:25
tert-Butylbenzene
ug/L
ND
0.50
04/22115 00:25
Tetra chi oroethene
ug/L
ND
0.50
04/22/15 00:25
Toluene
ug/L
ND
0.50
04/22/15 00:25
trans-1,2-Dichloroethene
ug/L
ND
0.50
04/22/15 00:25
trans-1,3-Dichloropropene
ug/L
ND
0.50
04/22/15 00:25
Trichloroethene
ug/L
ND
0.50
04/22/15 00:25
Trichlorofluoromethane
ug/L
ND
1.0
04/22/15 00:25
Vinyl chloride
ug/L
ND
1.0
04/22/15 00:25
1,2-Dichloroethane-d4 (S)
%
102
70-130
04/22/15 00:25
4-Bromofluorobenzene (S)
%
100
70-130
04/22/15 00:25
Toluene-d8 (S)
%
99
70-130
04/22/15 00:25
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1439867
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.3
103
60-140
1,1,1-Trichloroethane
ug/L
50
45.1
90
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
48.3
97
60-140
1,1,2-Trichloroethane
ug/L
50
45.4
91
60-140
1,1-Dichloroethane
ug/L
50
43.5
87
60-140
1,1-Dichloroethene
ug/L
50
41.4
83
60-140
1,1-Dichloropropene
ug/L
50
46.6
93
60-140
1,2,3-Trichlorobenzene
ug/L
50
42.2
84
60-140
1,2,3-Trichloropropane
ug/L
50
51.2
102
60-140
1,2,4-Trichlorobenzene
ug/L
50
43.9
88
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.7
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
55.6
111
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.2
98
60-140
1,2-Dichlorobenzene
ug/L
50
48.5
97
60-140
1,2-Dichloroethane
ug/L
50
45.2
90
60-140
1,2-Dichloropropane
ug/L
50
44.3
89
60-140
1,3,5-Trimethyl benzene
ug/L
50
48.7
97
60-140
1,3-Dichlorobenzene
ug/L
50
48.1
96
60-140
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 22

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QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
LABORATORY CONTROL SAMPLE:
Parameter
1439867
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
49.5
99
60-140
1,4-Dichlorobenzene
ug/L
50
47.4
95
60-140
2,2-Dichloropropane
ug/L
50
41.7
83
60-140
2-Chlorotoluene
ug/L
50
49.8
100
60-140
4-Chlorotoluene
ug/L
50
49.4
99
60-140
Benzene
ug/L
50
44.4
89
60-140
Bromobenzene
ug/L
50
49.6
99
60-140
Bromochloromethane
ug/L
50
44.1
88
60-140
Bromodichloromethane
ug/L
50
45.5
91
60-140
Bromoform
ug/L
50
42.5
85
60-140
Bromomethane
ug/L
50
34.0
68
60-140
Carbon tetrachloride
ug/L
50
48.5
97
60-140
Chlorobenzene
ug/L
50
47.2
94
60-140
Chloroethane
ug/L
50
41.6
83
60-140
Chloroform
ug/L
50
40.3
81
60-140
Chloromethane
ug/L
50
43.7
87
60-140
cis-1,2-Dichloroethene
ug/L
50
43.7
87
60-140
cis-1,3-Dichloropropene
ug/L
50
47.1
94
60-140
Dibromochloromethane
ug/L
50
50.5
101
60-140
Dibromomethane
ug/L
50
45.3
91
60-140
Dichlorodifluoromethane
ug/L
50
46.4
93
60-140
Diisopropyl ether
ug/L
50
43.6
87
60-140
Ethylbenzene
ug/L
50
46.8
94
60-140
Hexachloro-1,3-butadiene
ug/L
50
49.8
100
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.9
98
60-140
m&p-Xylene
ug/L
100
93.7
94
60-140
Methyl-tert-butyl ether
ug/L
50
43.9
88
60-140
Methylene Chloride
ug/L
50
46.7
93
60-140
n-Butylbenzene
ug/L
50
45.4
91
60-140
n-Propylbenzene
ug/L
50
47.7
95
60-140
Naphthalene
ug/L
50
44.8
90
60-140
o-Xylene
ug/L
50
47.6
95
60-140
sec-Butylbenzene
ug/L
50
48.8
98
60-140
Styrene
ug/L
50
49.5
99
60-140
tert-Butylbenzene
ug/L
50
46.2
92
60-140
Tetra chloroethene
ug/L
50
48.0
96
60-140
Toluene
ug/L
50
43.2
86
60-140
trans-1,2-Dichloroethene
ug/L
50
42.5
85
60-140
trans-1,3-Dichloropropene
ug/L
50
49.8
100
60-140
Trichloroethene
ug/L
50
43.1
86
60-140
Trichlorofluoromethane
ug/L
50
45.6
91
60-140
Vinyl chloride
ug/L
50
41.9
84
60-140
1,2-Dichloroethane-d4(S)
%
103
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 22

17;ace Ana lytica I
www.paceiabs.com
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1439868
1439869
MS
MSD
92245969009
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.5
23.0
118
115
60-140
2
1,1,1-Trichloroethane
ug/L
ND
20
20
21.9
21.8
110
109
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.3
20.8
112
104
60-140
7
1,1,2-Trichloroethane
ug/L
ND
20
20
21.3
20.2
107
101
60-140
6
1,1-Dichloroethane
ug/L
ND
20
20
21.1
20.6
105
103
60-140
2
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.4
107
107
60-140
0
1,1-Dichloropropene
ug/L
ND
20
20
23.3
23.7
116
118
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
19.1
17.4
95
87
60-140
9
1,2,3-Trichloropropane
ug/L
ND
20
20
22.8
22.3
114
112
60-140
2
1,2,4-Trichlorobenzene
ug/L
ND
20
20
19.9
18.6
99
93
60-140
6
1,2,4-Trimethylbenzene
ug/L
ND
20
20
23.3
23.5
116
117
60-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
22.6
22.7
113
114
60-140
1
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.2
21.3
111
106
60-140
4
1,2-Dichlorobenzene
ug/L
ND
20
20
22.8
23.1
114
116
60-140
1
1,2-Dichloroethane
ug/L
ND
20
20
20.2
19.5
101
98
60-140
4
1,2-Dichloropropane
ug/L
ND
20
20
21.3
20.4
107
102
60-140
4
1,3,5-Trimethylbenzene
ug/L
ND
20
20
23.3
23.3
117
116
60-140
0
1,3-Dichlorobenzene
ug/L
NO
20
20
22.7
22.7
113
113
60-140
0
1,3-Dichloropropane
ug/L
ND
20
20
22.4
21.9
112
110
60-140
2
1,4-Dichlorobenzene
ug/L
ND
20
20
22.1
22.6
110
113
60-140
2
2,2-Dichloropropane
ug/L
ND
20
20
18.0
18.4
90
92
60-140
2
2-Chlorotoluene
ug/L
ND
20
20
23.5
23.9
117
119
60-140
2
4-Chlorotoluene
ug/L
ND
20
20
23.3
23.6
116
118
60-140
1
Benzene
ug/L
ND
20
20
21.6
21.7
108
108
60-140
0
Bromobenzene
ug/L
ND
20
20
23.0
23.0
115
115
60-140
0
Bromochloromethane
ug/L
ND
20
20
20.4
20.2
102
101
60-140
1
Bromodichloromethane
ug/L
NO
20
20
20.1
20.0
100
100
60-140
0
Bromoform
ug/L
ND
20
20
18.4
17.8
92
89
60-140
4
Bromomethane
ug/L
ND
20
20
14.8
17.5
74
88
60-140
17
Carbon tetrachloride
ug/L
NO
20
20
23.6
23.7
118
119
60-140
1
Chlorobenzene
ug/L
ND
20
20
22.7
22.2
114
111
60-140
2
Chloroethane
ug/L
ND
20
20
20.4
20.2
102
101
60-140
1
Chloroform
ug/L
NO
20
20
19.1
19.1
95
96
60-140
0
Chloromethane
ug/L
ND
20
20
22.2
22.3
111
111
60-140
0
cis-1,2-Dichloroethene
ug/L
NO
20
20
20.6
20.8
103
104
60-140
1
cis-1,3-Dichloropropene
ug/L
NO
20
20
20.9
20.1
104
101
60-140
3
Dibromochloromethane
ug/L
ND
20
20
20.2
19.9
101
99
60-140
2
Dibromomethane
ug/L
NO
20
20
20.7
20.1
104
100
60-140
3
Dichlorodifluoromethane
ug/L
NO
20
20
25.4
25.7
127
128
60-140
1
Diisopropyl ether
ug/L
ND
20
20
20.2
19.7
101
99
60-140
2
Ethylbenzene
ug/L
ND
20
20
22.6
22.5
113
113
60-140
0
Hexachloro-1,3-butadiene
ug/L
ND
20
20
22.9
20.6
114
103
60-140
10
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.6
23.1
118
116
60-140
2
m&p-Xylene
ug/L
ND
40
40
45.6
45.4
114
113
60-140
1
Methyl-tert-butyl ether
ug/L
ND
20
20
19.9
18.9
99
94
60-140
5
Methylene Chloride
ug/L
ND
20
20
18.9
18.5
95
93
60-140
2
Results presented on this page are in
the units indicated by the
"Units" column except where an alternate
unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc. Page 18 of 22

_ aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: WALSER'S
Pace Project No.: 92245619
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1439868
MS
92245969009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1439869
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
20.8
20.6
104
103
60-140
1
n-Propylbenzene
ug/L
ND
20
20
23.3
23.2
116
116
60-140
0
Naphthalene
ug/L
ND
20
20
20.5
19.3
102
96
60-140
6
o-Xylene
ug/L
ND
20
20
22.3
22.2
111
111
60-140
0
sec-Butylbenzene
ug/L
ND
20
20
23.6
23.1
118
115
60-140
2
Styrene
ug/L
ND
20
20
23.1
23.0
116
115
60-140
0
tert-Butyl benzene
ug/L
ND
20
20
22.1
21.2
111
106
60-140
4
Tetra chloroethene
ug/L
ND
20
20
23.7
24.0
118
120
60-140
1
Toluene
ug/L
ND
20
20
21.4
21.0
107
105
60-140
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.9
21.0
105
105
60-140
1
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.7
20.2
108
101
60-140
7
Trichloroethene
ug/L
ND
20
20
21.5
21.4
107
107
60-140
0
Trichlorofluoromethane
ug/L
ND
20
20
23.5
23.6
117
118
60-140
1
Vinyl chloride
ug/L
ND
20
20
20.9
21.9
105
109
60-140
5
1,2-Dichloroethane-d4 (S)
%
98
96
70-130
4-Bromofluorobenzene (S)
%
98
98
70-130
Toluene-d8 (S)
%
99
97
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc..
Page 19 of 22

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: WALSER'S
Pace Project No.: 92245619
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
N2 The lab does not hold TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 22

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
WALSER'S
92245619
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92245619001
EFF
MADEP VPH
GCV/9260
92245619002
INF
MADEP VPH
GCV/9260
92245619001
EFF
EPA 200.7
MPRP/18289 EPA 200.7 ICP/16421
92245619001
EFF
SM 6200B
MSV/31308
92245619002
INF
SM 6200B
MSV/31308
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/06/2015 11:26 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 22

CHAIN -OF -CUSTODY / Analytical Request Document
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Section A Section 8 Section C
Required Client Information: Required Project Information: Invoice Information: Page : 1 Qf 1
Company Shield Report To Flora D'Souza Attention.
Address 4301 Taggart Creek Road Copy To Company Name
Charlotte. NC 28208
Address
Regulatory Agency
Email fdsouza@shieldengineenng com
Purchase Order S
Pace Ouote-
Phone [phone] JFax
Project Name Walser's
Pace Project Manager ]aura coope
pacelabs.com,
State I Location
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