WQ0014357_2018 Annual Report_20190201

Rogers, Michael
From: Thomas Mann <[e-mail]>
Sent: Friday, April 19, 2019 12:02 PM
To: Rogers, Michael
Cc: Rumford, Doug; bornholm [e-mail]; George Crouse; Garland Hilliard; Michael
Bogle; Ted Volskay; Barber, Jim
Subject: RE:WQ0014357 RE: [External] Route 211 Site 2018 Annual Treatment System Report
Permit No.WQ0014357
Attachments: Rt. 211 Treatment System WL Figure.pdf
CA r = External email.Do not click links or open attachments unless you verify.Send all suspicious email as an attachment to
«t310pam@nc gov
Mike—Please find attached figure displaying the infiltration galleries and the influent/effluent sampling locations inside
the treatment building.Thanks.
Tom
From: Rogers, Michael [mailto:[e-mail]]
Sent: Friday, April 12, 2019 3:17 PM
To: Thomas Mann
Cc: Rumford, Doug; [e-mail]; George Crouse; Garland Hilliard; Michael Bogle; Ted Volskay; Barber, Jim
Subject: WQ0014357 RE: [External] Route 211 Site 2018 Annual Treatment System Report Permit No. WQ0014357
Thomas-
I received the report. Thanks. Could you provide a revised site map showing the location of infiltration gallery and, if
possible, sampling points for influent/effluent. If this is a problem let me know.
Thanks.
From:Thomas Mann [mailto:[e-mail]]
Sent:Tuesday,January 29, 2019 2:22 PM
To: Rogers, Michael <[e-mail]>
Cc: Rumford, Doug<[e-mail]>; [e-mail]; George Crouse
<[e-mail]>; Garland Hilliard <[e-mail]>; Michael Bogle<[e-mail]>; Ted
Volskay<[e-mail]>; Barber,Jim <[e-mail]>
Subject: [External] Route 211 Site 2018 Annual Treatment System Report Permit No.WQ0014357
'`.External email.Do not click links or open attachments unless you verify.Send all suspicious email as an attachment to
� •ortsaamC�nc.gov.
Mike,
Good afternoon. Please find attached the 2018 Annual Treatment System Report for the Route 211 Site Permit No.
WO0014357. I will also mail a hard copy to you and Jim. If you have any comments or questions, please contact me.
Thanks.
Regards,
1

Tom
synTerra
Scr.ing and grow ing sink 1903
Thomas A. Mann, PE
SynTerra Corporation
148 River Street, Suite 220
Greenville, SC 29601
864-527-4617
tmann(asynterracorp.com
This e-mail might contain privileged or confidential information. If the e-mail was not intended for you, please:
(1) delete the e-mail and any attachments
(2) destroy any copies that might have been made
(3) do not use, copy, or distribute the contents in any form
(4) notify me by return e-mail or by calling 864-527-4617
No privilege is waived by inadvertent transmission. Thank you.
2

N
i
INFILTRATION
GALLERIES
05-MW-01 (MW-2)G, ....,„ t RT-MW-12 (MW-1)
NA "..` 434.99
�♦
— - r , \
♦...
- IW-03 43s
434.42
RT-MW-05 (MW-3) i ♦,,
432.97
05-MW-02
CARBON VESSELS 433.04
EFFLUENT
SAMPLE PORT P.
, ; I 1
INFLUENT
I
SAMPLE PORT
I I
I i
� I 1
INFI ION - �tT-PW-01
OA IES-
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=1 I C I I�I I�I I=1 I, 1=1 III I- I I I-I I I-I H �I I C-mI-E 11=1 I -I 1=1 1=1 11 11=
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-1 1=�1 I-II1 =I a I a 1=1 I I-1 1-1=1 1=1 1=1 11=1 11=1 I I-I 11=] �i 11-111E111-i l l-
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0 50 100 200 '�be
�._ Feet ilia, /?In
Legend 0 FIGURE 1
© EXTRACTION WELL S)/t1..( MONITORING LOCATIONS AND
e MONITORING WELL POTENTIOMETRIC MAP-
Source:Water levels measured December 2018,Moore County 2007 aerial,
FORMER SOURCE AREA and site surveys. SURFICIAL AQUIFER
This map is a product of SynTerra.Reasonable efforts have been made to ensure the
SURFACE WATER accuracy of this map.SynTena expressly disclaims any responsibility or liability with ROUTE 211 AREA
regard to the use of this map,and promotes and recommends the independent
"No GROUNDWATER SURFACE CONTOUR* verification of any data contained on this map by the user of this map product.
Created by:B.Russo on 06/222016 Edited by:A.Robinson 01/25/2019 ABERDEEN PESTICIDE DUMPS SITE
•Water elevations(ft msl)measured December2018. P9Syngenta.1053t04.01.Rt211 Downgradient1Figures1201e-01\Fig-0l-Monitor:rgLocabona.mnd MOORE COUNTY,NORTH CAROLINA

� .
Rogers, Michael
From: Thomas Mann <[e-mail]>
Sent: Tuesday, April 16, 2019 11:23 AM
To: Rogers, Michael
Cc: Rumford, Doug; [e-mail]; George Crouse; Garland Hilliard; Michael
Bogle; Ted Volskay; Barber, Jim
Subject: RE:WQ0014357 RE: [External] Route 211 Site 2018 Annual Treatment System Report
Permit No.WQ0014357
Cit! ..>t, External email.Do not click links or open attachments unless you verify.Send all suspicious email as an attachment to:.
Mike—
We will develop a figure showing the influent/effluent sample ports inside the treatment building as well as the location
of the infiltration gallery. I will send the figure to you when it is completed.Thanks.
Tom
From: Rogers, Michael [mailto:[e-mail]]
Sent: Friday, April 12, 2019 3:17 PM
To: Thomas Mann
Cc: Rumford, Doug; [e-mail]; George Crouse; Garland Hilliard; Michael Bogle; Ted Volskay; Barber, Jim
Subject: WQ0014357 RE: [External] Route 211 Site 2018 Annual Treatment System Report Permit No. WQ0014357
Thomas-
I received the report. Thanks. Could you provide a revised site map showing the location of infiltration gallery and, if
possible, sampling points for influent/effluent. If this is a problem let me know.
Thanks.
From:Thomas Mann [mailto:[e-mail]]
Sent:Tuesday,January 29, 2019 2:22 PM
To: Rogers, Michael <[e-mail]>
Cc: Rumford, Doug<[e-mail]>; [e-mail];George Crouse
<[e-mail]>; Garland Hilliard <[e-mail]>; Michael Bogle <[e-mail]>;Ted
Volskay<[e-mail]>; Barber,Jim <[e-mail]>
Subject: [External] Route 211 Site 2018 Annual Treatment System Report Permit No.WQ0014357
`External email.Do not click links or open attachments unless you verify.Send all suspicious email as an attachment
r,-
m nc. ov .
Mike,
Good afternoon. Please find attached the 2018 Annual Treatment System Report for the Route 211 Site Permit No.
WO0014357. I will also mail a hard copy to you and Jim. If you have any comments or questions, please contact me.
Thanks.
1

Regards,
Tom
synTerra
Set%ing and groM ins since I903
Thomas A. Mann, PE
SynTerra Corporation
148 River Street, Suite 220
Greenville, SC 29601
864-527-4617
tmann2svnterracorp.com
This e-mail might contain privileged or confidential information. If the e-mail was not intended for you, please:
(1) delete the e-mail and any attachments
(2) destroy any copies that might have been made
(3) do not use, copy, or distribute the contents in any form
(4) notify me by return e-mail or by calling 864-527-4617
No privilege is waived by inadvertent transmission. Thank you.
2

Rogers, Michael
From: Rogers, Michael
Sent: Friday, April 12, 2019 3:17 PM
To: 'Thomas Mann'
Cc: Rumford, Doug; [e-mail]; George Crouse; Garland Hilliard; Michael
Bogle; Ted Volskay; Barber,Jim
Subject: WQ0014357 RE: [External] Route 211 Site 2018 Annual Treatment System Report Permit
No.WQ0014357
Thomas-
I received the report. Thanks. Could you provide a revised site map showing the location of infiltration gallery and, if
possible, sampling points for influent/effluent. If this is a problem let me know.
Thanks.
From:Thomas Mann [mailto:[e-mail]]
Sent:Tuesday,January 29, 2019 2:22 PM
To: Rogers, Michael<[e-mail]>
Cc: Rumford, Doug<[e-mail]>; [e-mail];George Crouse
<[e-mail]>; Garland Hilliard <[e-mail]>; Michael Bogle <[e-mail]>;Ted
Volskay<[e-mail]>; Barber,Jim <[e-mail]>
Subject: [External] Route 211 Site 2018 Annual Treatment System Report Permit No. WQ0014357
P : External email. Do not click links or open attachments unless you verify.Send all suspicious email as an attachment to
rtkspamPnc.Rov
Mike,
Good afternoon. Please find attached the 2018 Annual Treatment System Report for the Route 211 Site Permit No.
WQ0014357. I will also mail a hard copy to you and Jim. If you have any comments or questions, please contact me.
Thanks.
Regards,
Tom
synTerra
Scr ing and grossing since 1993
Thomas A. Mann, PE
SynTerra Corporation
148 River Street, Suite 220
Greenville, SC 29601
864-527-4617
tmannsynterracorp.com
1

This e-mail might contain privileged or confidential information. If the e-mail was not intended for you, please:
(1) delete the e-mail and any attachments
(2) destroy any copies that might have been made
(3) do not use, copy, or distribute the contents in any form
(4) notify me by return e-mail or by calling 864-527-4617
No privilege is waived by inadvertent transmission. Thank you.
2

Greenville Office Charlotte Office
148 River Street, Suite 220 10806 Reames Road, Suite A
Greenville. SC 29601 Te r ra Charlotte. NC 28269
864.421.9999s y 980.312.5998
Fax: 864,421.9909 Fax [phone]
January 29, 2019
Mr. Mike Rogers
UIC Program
NC Division of Water Resources
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2018 Annual Report
Groundwater Remediation Permit •. WQ0014357
Aberdeen Pesticide Dumps Site-Route • -
Aberdeen, North Carolina
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2018 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide DumsOite.
Information provided in this letter report includes: St l)0-03
• Analytical monitoring requirements summary (Table 1); FEB
• Influent and effluent analytical results summary (Tables 2 and 3);
• Monitoring well analytical results summary (Table 4);
• Water levels and groundwater concentrations (Figure 1); Re,
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratorydata reports (Attachments).
Y P ( )
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (June 26, 2018 and December 18, 2018) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2018 and experienced minimal downtime. The system
operates 24 hours per day and a total of 517,741 gallons (based upon the monthly
inspection logs dated between December 19, 2017 to December 19, 2018) of
groundwater were treated. Groundwater extraction rates averaged approximately 1,418
gpd during the monitoring period. The treatment system removal efficiency was greater
than 95% (see Tables 2 and 3).
www.synterracorp.com

Greenville Office Charlotte Office
148 River Street,Suite 220 10806 Reames Road, Suite A
Greenville,SC 29601 Terra Charlotte, NC 28269
864.421.9999 980 312 5998
Fax:
Fax: [phone] Fax [phone]
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), and one upgradient well, MW-1 (RT-MW-12), were
sampled on December 18, 2018 and analyzed for SW-846 8081A pesticides. Analytical
results are summarized in Table 4. Water levels were collected on December 18, 2018 and are
shown of Figure 1 along with corresponding detectable groundwater pesticide concentrations
for each well. Copies of the treatment system influent and effluent analytical reports and
the MW-1, MW-2 and MW-3 analytical report are included with the completed GW-59
forms provided as attachments.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section III and IV of the Site Groundwater Remediation
Permit issued October 13, 2016.
If you require additional copies of the enclosed materials or have any questions, please
contact me at(864) 527-4617.
Sincerely,
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Electronic cc:
Jim Barber—NC DWR Fayetteville Garland Hilliard—Olin
Doug Rumford—NCDEQ Michael Bogle, Esq. -WBD
Jon Bornholm—USEPA Ted Volskay-SynTerra
George Crouse-Syngenta
www.synterracorp.com

Route 211 Treatment System
2018 Annual Operating Report
SynTerra Corporation
January 2019
Table 1
Analytical Monitoring Requirements
Groundwater Extraction and Treatment System
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Frequency
(Permit No.
Location Parameters of Analysis WQ0014357)
Influent TCL Pesticides&pH Semi-annually
(RT-PW-01) (Jan.-June,July-Dec.)
Effluent TCL Pesticides&pH Semi-annually
(Jan.-June,July-Dec.)
MW-1 TCL Pesticides Annually
(RT-MW-12) &Water Level
MW-2 TCL Pesticides Annually
(05-MW-01) &Water Level
MW-3 TCL Pesticides Annually
(RT-MW-05) &Water Level

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/26/18 06/26/18
Pesticides(ug/L)
Aldrin < 0.080 < 0.0016
alpha-BHC 0.19 J < 0.0024
alpha-Chlordane 0.17 JP < 0.0024
beta-BHC 4.3 < 0.0028
p,p-DDD < 0.20 < 0.0040
p,p-DDE < 0.20 < 0.0040
p,p-DDT < 0.21 < 0.0042
delta-BHC 8.9 < 0.0027
Dieldrin < 0.21 < 0.0042
Endosulfan I < 0.17 < 0.0034
Endosulfan II < 0.60 < 0.012
Endosulfan Sulfate < 0.23 < 0.0046
Endrin < 0.32 < 0.0065
Endrin Aldehyde < 0.80 < 0.016
Endrin Ketone < 0.20 < 0.0040
gamma-BHC 0.11 J < 0.0016
gamma-Chlordane < 0.28 < 0.0056
Heptachlor < 0.080 < 0.0016
Heptachlor Epoxide 0.17 J < 0.0018
Methoxychlor < 1.2 < 0.024
Toxaphene 17.0 J < 0.24
Total Pesticides 34.17 0.0083
System Removal Efficiency: 99.98%
Notes:
Influent pH was 5.35 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Since all effluent concentrations were ND,average detection limit of
all constituents divided by half was used for calculation.

Route 211 Treatment System
2018 Annual Operating Report
SynTerra Corporation
January 2019
Table 3
Treatment System Monitoring Results And
Treatment Removal Efficiency (July - December 2018)
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Period July - December 2018
Sample Name Influent Effluent
Date Sampled 12/18/18 12/18/18
Pesticides (ug/L)
Aldrin < 0.043 < 0.0021
alpha-BHC 0.18 J < 0.0032
beta-BHC 5.0 < 0.0036
gamma-BHC (Lindane) 0.13 J < 0.0021
alpha-Chlordane 0.27 P < 0.0032
gamma-Chlordane 0.18 J < 0.0075
p,p-DDD < 0.11 < 0.0054
p,p-DDE 0.16 JP < 0.0054
p,p-DDT < 0.11 < 0.0056
delta-BHC 21.0 < 0.0036
Dieldrin 0.13 JP < 0.0057
Endosulfan I < 0.091 < 0.0046
Endosulfan II < 0.32 < 0.016
Endosulfan Sulfate < 0.120 < 0.0062
Endrin < 0.17 < 0.0087
Endrin Aldehyde < 0.43 < 0.021
Endrin Ketone < 0.110 < 0.0054
Heptachlor < 0.043 < 0.0021
Heptachlor Epoxide < 0.049 < 0.0025
Methoxychlor < 0.64 < 0.032
Toxaphene < 6.4 < 0.32
Total pesticides 33.5 0.01
System Removal Efficiency: 99.97%
Notes:
Influent pH was 4.74
J-estimated value;P- RPD>40%;V-RPD>100%
Only measurable concentrations are used for removal efficiency.
Since all effluent concentrations were ND,average detection limit of
all constituents divided by half was used for calculation.
Permit specified removal efficiency:95%

Route 211 Treatment System
2018 Annual Operating Report
SynTerra Corporation
January 2019
Table 4
Monitoring Well Analytical Results Summary
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Sample Name MW-1 (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)
Sample Event Annual Annual Annual
Date Sampled 12/18/18 12/18/18 12/18/18
Pesticides (ug/L)
Aldrin < 0.0021 < 0.0021 < 0.0021
alpha-BHC < 0.0032 < 0.0031 < 0.0031
beta-BHC < 0.0036 < 0.0035 < 0.0035
gamma-BHC (Lindane) < 0.0021 < 0.0021 < 0.0021
alpha-Chlordane < 0.0032 < 0.0031 < 0.0031
gamma-Chlordane < 0.0074 < 0.0072 < 0.0072
p,p-DDD < 0.0053 < 0.0051 < 0.0051
p,p-DDE < 0.0053 < 0.0051 < 0.0051
p,p-DDT < 0.0055 < 0.0054 < 0.0054
delta-BHC < 0.0036 < 0.0035 < 0.0035
Dieldrin < 0.0056 < 0.0055 < 0.0055
Endosulfan I < 0.0045 < 0.0044 < 0.0044
Endosulfan II < 0.016 < 0.015 < 0.015
Endosulfan Sulfate < 0.0061 < 0.0060 < 0.0060
Endrin < 0.0085 < 0.0083 < 0.0083
Endrin Aldehyde < 0.021 < 0.021 < 0.021
Endrin Ketone < 0.0053 < 0.0051 < 0.0051
Heptachlor < 0.0021 < 0.0021 < 0.0021
Heptachlor Epoxide < 0.0024 < 0.0024 < 0.0024
Methoxychlor < 0.032 < 0.031 < 0.031
Toxaphene < 0.32 < 0.31 < 0.31
MW-1 (pH=4.24);MW-2(pH=4.05);MW-3 (pH=4.29)
J-estimated value
P-RPD>40%
V-RPD>100%

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SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION .
EN
COMPLIANCE REPORT FORM RALEIGR1636MAIL,NCSERVICE 27699C-16TER36 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE: Sept. 30,2021
Permit Name (if different): Non-Discharge W00014357 UIC
Facility Address: NC Highway Route 211 NPDES
(street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City)
ac Tom Mann (State) (zip) 864 527-4617 Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone#: ( )
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter:6.0 in. Check One: © Influent (98)
Screened Interval: 16.07 ft. to 40.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: NA ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 12/18/2018 Date sample analyzed: 12/27/2018
Field analysis: pH 4.74 , Specific Conductance 60 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 32.0 °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total _ mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable _
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations.
Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
G W-59
}i * Thawta4-A. Maviv 1725/2019
Rev. 03/2000 Signature of Permittee(or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT Y ENVIRONMENT, NATURAL S RESOURCES
_ to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:Sept. 30,2021
Non-Discharge WQ0014357 UIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (Stale) (Zip) County X
Contact Person: Tom Mann Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): NA For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuringpoint. ® Effluent (99)
P P colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 12/18/2018 Date sample analyzed: 12/27/2018
Field analysis: pH 5.13 , Specific Conductance 60 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 25.1 °C, Odor none Appearance Clear Certification No. NC Lab Certification#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100mI Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total_ mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Protect Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
..
GW-59 ; ' ''" Th wyt A. Mc ' 1/25/2019
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURA RESOURCES
to: WATER QUALITY DIVISIOOS
N,GROUNDWATER SECTION •
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: WQ0014357 EXPIRATION DATE:Sept. 30,2021
Permit Name (if different): Non Discharge UIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) Ted Volskay
(City) z County X
[phone] Lagoon Remediation: Infiltration Gallery
Contact Person: (state) ( ;v) Telephone #:
Well Location/Site Name: No. of Wells to be Sam led: 4 Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-Mw-12(Mw-1( For Groundwater Treatment Systems Other:
Well Depth: 20.50 ft. Well Diameter: 2.0 in. Check One: 0 Influent (98)
Screened Interval: 10 70 ft. to 20.50 ft ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 10.62 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.18 ft. above land surface. Relative M.P. Elevation in ft.: 445.61
Gallons of water pumped/bailed before sampling: 5.0 Date sample collected: 12/18/2018 Date sample analyzed: 12/27/2018
Field analysis: pH 4.24 , Specific Conductance 40 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 16.4 °C, Odor none Appearance Clear Certification No. NC Certification No.521
1 PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
7�rtcrv�a4-A. Ma* 1/25/2019
GW-59
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mall Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION .
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:Sept.30,2021
Permit Name (if different): Non-Discharge W00014357 UIC
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
( Tom Mann (Stale) (Zip)
Contact Person: Telephone #: [phone] Lagoon X Remediation: Infiltration Gallery
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): 05-MW-01(MW-2) For Groundwater Treatment Systems Other:
Well Depth: 37.52 ft. Well Diameter:4.0 in. Check One: 0 Influent (98)
Screened Interval:22.67 ft.to 37.52 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level:28.95 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 3.22 ft. above land surface. Relative M.P. Elevation in ft.: 454.40
Gallons of water pumped/bailed before sampling: 17.0 Date sample collected: 12/18/2018 Date sample analyzed: 12/27/2018
Field analysis: pH 4.05 , Specific Conductance 40 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 19.9 °C, Odor None Appearance Clear Certification No. NC Certification 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method# =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations.
Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
Th ina s•A. H aut vt, 1/2 5/2 019
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION . '
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:Sept. 30,2021
Non-Discharge WQ0014357 UIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) Tom Mann (State) (Zip) 864 527-4617 Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone #: ( )
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-Mw-05(Mw-3) For Groundwater Treatment Systems Other:
Well Depth: 24.57 ft. Well Diameter:2.0 in. Check One: 0 Influent (98)
Screened Interval: 14.57 ft. to 24.57 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 16.62 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.)is: 2.67 ft. above land surface. Relative M.P. Elevation in ft.: 449.59
Gallons of water pumped/bailed before sampling: 4.0 Date sample collected: 12/18/2018 Date sample analyzed: 12/27/2018
Field analysis: pH 4.29 , Specific Conductance 30 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 18.3 ,,C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWG(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations.
Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
Tw artiw t,a4-A. M 1/25/2019
GW-59
he>Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

I) 0o/471-35�
Greenville Office Charlotte Office
148 River Street,Suite 220 10806 Reames Road,Suite A
Greenville,SC 29601 syrire rra Charlotte, NC 28269
1.999
864.42 980.312.5999
4.421
Fax: .9909
July 14, 2017
Mr. Mike Rogers
DECEIVED/NCDEQ!DWR
UIC Program JUL 2 4 2017
NC Division of Water Resources
1636 Mail Service Center Water Quality Regional
Operations Section
Raleigh, North Carolina 27699-1636
RE: 2017 Semiannual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site -Route 211 Area
Aberdeen, North Carolina
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2017 Semiannual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
• Analytical monitoring requirements (Table 1);
• Monitoring events analytical results summary table (Table 2);
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratory data reports; and
• Influent and effluent analytical results.
The treatment system, which operates 24 hours per day, was inspected monthly in
accordance with the permit. The treatment system has performed as designed and
experienced no unscheduled downtime during this reporting period. Influent and
effluent samples were collected on June 14, 2017. The treatment system, which includes
bag filtration and carbon adsorption, achieved a 99.99% removal efficiency on August 9,
2016 which exceeded the 95% removal efficiency specified by the permit.
Approximately 520,515 gallons of groundwater was extracted and treated from January
28, 2016 to June 27, 2016. Groundwater extraction rates averaged approximately 2.41
gpm or 3,470 gpd during the monitoring period.
www.synterracorp.com

2017 Semiannual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
July 14,2017
Page Two
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. One upgradient well, MW-1 (RT-MW-
12), and two sidegradient wells, MW-2 and MW-3 (05-MW-01 and RT-MW-05,
respectively), are required to be sampled annually for TCL pesticide analysis. These
wells will be sampled in the second half of 2017 and the results will be provided in the
2017 annual operating report.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section III and IV of the Site Groundwater Remediation
Permit issued October 13, 2016.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
SynTerra Corporation
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Attachments:
GW-59 Forms
Analytical reports
Electronic cc:
Jim Barber—NC DWR Fayetteville
Jon Bornholm—USEPA
Doug Rumford—NCDEQ
George Crouse -Syngenta
Garland Hilliard—Olin
Michael Bogle, Esq. - WCS&R
Ted Volskay-SynTerra

Table 1
Analytical Monitoring Requirements
Groundwater Extraction And Treatment System
Route 211 Area Semiannual Operating Report
Aberdeen, North Carolina
Location Parameters of Analysis Monitoring Frequency
(Permit No.WQ0014357)
Influent TCL Pesticides&pH Semiannually
(Jan. -June,July-Dec.)
Effluent TCL Pesticides &pH Semiannually
(Jan. -June,July-Dec.)
MW-1 TCL Pesticides, pH Annually
(RT-MW-12) &Water Level (July-Dec.)
MW-2 TCL Pesticides, pH Annually
(05-MW-01) &Water Level (July-Dec.)
MW-3 TCL Pesticides, pH Annually
(RT-MW-05) &Water Level (July-Dec.)

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/14/17 06/14/17
Pesticides(ug/L)
Aldrin < 0.080 < 0.0016
alpha-BHC 0.069 < 0.0024
alpha-Chlordane < 0.0024 < 0.0024
beta-BHC 2.4 < 0.0027
p,p-DDD 0.067 < 0.0040
p,p-DDE 0.060 < 0.0040
p,p-DDT < 0.050 V < 0.0042
delta-BHC 7.0 < 0.0027
Dieldrin < 0.0042 < 0.0042
Endosulfan I 0.044 < 0.0034
Endosulfan II < 0.012 < 0.012
Endosulfan Sulfate < 0.0046 < 0.0046
Endrin < 0.0065 < 0.0065
Endrin Aldehyde < 0.050 V < 0.016
Endrin Ketone < 0.004 < 0.0040
gamma-BHC 0.062 < 0.0016
gamma-Chlordane 0.085 < 0.0056
Heptachlor < 0.002 < 0.0016
Heptachlor Epoxide 0.036 P < 0.0018
Methoxychlor 0.064 JP < 0.024
Toxaphene 7.7 < 0.24
Total Pesticides 17.69 0.0083
System Removal Efficiency: 99.95%
Notes:
Influent pH was 5.35 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Since all effluent concentrations were ND,average detection limit of
all constituents divided by half was used for calculation.

,
SUBMIT FORM ON YELLOW PAPER
��ONLY
' -it fAl ! WATER TMENT QUALITOY DIVISION,GROUNDWATER ENVIRONMENT& AL SECTIIONRCES
GROUNDWATER QUALITY MONITORING: ,.,.:
COMPLIANCE REPORT FORM ^r° _ _ RA163L IGILH NC R
`•rr' RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY_INFOFIMATIQN Please Print Clearly or Type
Route 211 Area PERMIT#: EXPIRATION DATE:Sept.30,2021
Facility Name: Non-Discharge WQ0014357 UIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
Wveeq TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
ICly) Mato) tun Lagoon X Remediation:Infiltration Gallery
Contact Person: Ted Volskay Telephone #: [phone]
Well Location/Site Name:. RT-PW-01 to treatment system No. of Wells to be Sam led: 4 Spray Field Remediation:
p Ilrom Vormal
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.0 in. Check One: El Influent (98)
Screened Interval: 1607 ft. to 40.51 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/14/2017 Date sample analyzed: 06/19/2017 _
Field analysis: pH 5.35 , Specific Conductance 87 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.8 °C, Odor none Appearance clear Certification No. NC Lab cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/1
Coliform: MF Fecal /1 00m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/ -
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N _..-_ mg/I Mn - Manganese mg/ TCL Pesticides : method # = 8081A
method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A. Mann, P.E., Project Manager
—
P _or Au-
th ized nt)Name and Title-Please print or type
17---
‘72b1-7
GW-59
Signature at Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mall GROUNDWATER QUALITY MONITORING: Original WATDEPER
QUALITYMENT OF ENVIRONMENT,GROUNDWATER NATURAL RESOURCES
.;, `Y;'#�• 1636 MAIL SERVICECENTER SECTION
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Route 211 Area PERMIT#: EXPIRATION DATE:Sept.30,2021
Facility Name: W00014357
Permit Name (if different): Non Discharge TIC_
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(city) (slate) (Zip) County
Contact Person: Telephone #: X
Ted Volskay [phone] Lagoon Remediation:Infiltration Gallery
Treatment sysl.discharge to infiltration gallery 4 Spray Field Remediation:
Well Location/Site Name:. No. of Wells to be Sampled:(horn Pc.mll)
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One:0 Influent (98)
Screened Interval: ft.to ft. El Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft.above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: . Date sample collected: 06/14/2017 Date sample analyzed: 06/19/2017
Field analysis: pH 5.44 , Specific Conductance S9 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 20.7 "C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/1
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/ Zn -Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance._ uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable _
TKN as N __ _ mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
method # _
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly OEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and Imprisonment for knowing violations. Tho as A. Mann, P.E., Project Manager
Pennine (or Authorize gen me and Title-Please print or type /
GW 59 � `7/��ul—]
Signature of Permittee(or Authorized Agent) (Uate)
Rev. 03/2000

tiff eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17001 •717-656-2300•Fax:[phone] •www.LancasterLabs.com
ANALYTICAL RESULTS
Prepared by: Prepared for:
Eurofins Lancaster Laboratories Environmental Synterra Corporation
2425 New Holland Pike Suite 220
Lancaster,PA 17601 148 River Street
Greenville SC 29601
Report Date: June 29,2017
Project: Rte 211 Treatment System,NC
Submittal Date: 06/15/2017
Group Number: 1813697
PO Number: 1053.04.01
State of Sample Origin: NC
Lancaster Labs
Client Sample Description (LL)#
Effluent Grab Groundwater 9050064
Influent Grab Groundwater 9050065
The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory Sample
Analysis Record.
Regulatory agencies do not accredit laboratories for all methods,analytes,and matrices. Our current scopes of
accreditation can be viewed at http://www.eurofinsus.com/environment-testing/laboratories/eurofins-Lancaster-
laboratories-environmental/resources/certifications/. To request copies of prior scopes of accreditation,contact
your project manager.
Electronic Copy To Synterra Corporation Attn:Ted Volskay
Respectfully Submitted,
V-1).1-40k
1
Lyssa M. Longenecker
Specialist
[phone]
Page 1 of 9

. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 9050064
Rt 211 Treatment System, NC LL Group # 1813697
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/14/2017 12:04 by TV Synterra Corporation
Suite 220
Submitted: 06/15/2017 09:30 148 River Street
Reported: 06/29/2017 09:40 Greenville SC 29601
211EF
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8O81B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 N.D. 0.0024 1
10589 Beta BHC 319-85-7 N.D. 0.0027 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0024 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0056 1
10589 p,p-DDD 72-54-8 N.D. 0.0040 1
10589 p,p-DDE 72-55-9 N.D. 0.0040 1
10589 p,p-DDT 50-29-3 N.D. 0.0042 1
10589 Delta BHC 319-86-8 N.D. 0.0027 1
10589 Dieldrin 60-57-1 N.D. 0.0042 1
10589 Endosulfan I 959-98-8 N.D. 0.0034 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0046 1
10589 Endrin 72-20-8 N.D. 0.0065 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0040 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0018 1
10589 Methoxychlor 72-43-5 N.D. 0.024 1
10589 Toxaphene 8001-35-2 N.D. 0.24 1
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 171680011A 06/19/2017 17:50 Andrea L Jones _
11120 Pesticide Waters Update SW-846 3510C 1 171680011A 06/19/2017 00:15 Nadia Bernabe
IV Ext
Page 2 of 9

tiff eurofins
, Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 9050065
Rt 211 Treatment System, NC LL Group # 1813697
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/14/2017 12:07 by TV Synterra Corporation
Suite 220
Submitted: 06/15/2017 09:30 148 River Street
Reported: 06/29/2017 09:40 Greenville SC 29601
211IN
CAT Dilution
No. Analysis Name CAS Number Result Method Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ughl ugh].
10589 Aldrin 309-00-2 N.D. 0.080 50
10589 Alpha BHC 319-84-6 0.069 0.0024 1
10589 Beta BHC 319-85-7 2.4 0.14 50
10589 Gamma BHC - Lindane 58-89-9 0.062 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0024 1
10589 Gamma Chlordane 5103-74-2 0.085 0.0056 1
10589 p,p-DDD 72-54-8 0.067 0.0040 1
10589 p,p-DDE 72-55-9 0.060 0.0040 1
10589 p,p-DDT 50-29-3 N.D. V 0.050 1
10589 Delta BHC 319-86-8 7.0 0.14 50
10589 Dieldrin 60-57-1 N.D. 0.0042 1
10589 Endosulfan I 959-98-8 0.044 0.0034 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0046 1
10589 Endrin 72-20-8 N.D. 0.0065 1
10589 Endrin Aldehyde 7421-93-4 N.D. V 0.050 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0040 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 0.036 P 0.0018 1
10589 Methoxychlor 72-43-5 0.064 JP 0.024 1
10589 Toxaphene 8001-35-2 7.7 0.24 1
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 171680011A 06/19/2017 18:16 Morgan P Good 50
10589 OC Pesticides in Water SW-846 8081E 1 171680011A 06/22/2017 17:36 Andrea L Jones 1
11120 Pesticide Waters Update SW-846 3510C 1 171680011A 06/19/2017 00:15 Nadia Bernabe 1
IV Ext
Page 3 of 9

titieurofins
j Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1813697
Reported: 06/29/2017 09:40
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise specified
in the method.
All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless otherwise noted
on the Analysis Report.
Method Blank
Analysis Name Result MDL
ug/1 ug/1
Batch number: 171680011A Sample number(s) : 9050064-9050065
Aldrin N.D. 0.0016
Alpha BHC N.D. 0.0024
Beta BHC N.D. 0.0027
Gamma BHC - Lindane N.D. 0.0016
Alpha Chlordane N.D. 0.0024
Gamma Chlordane N.D. 0.0056
p,p-DDD N.D. 0.0040
p,p-DDE N.D. 0.0040
p,p-DDT N.D. 0.0042
Delta BHC N.D. 0.0027
Dieldrin N.D. 0.0042
Endosulfan I N.D. 0.0034
Endosulfan II N.D. 0.012
Endosulfan Sulfate N.D. 0.0046
Endrin N.D. 0.0065
Endrin Aldehyde N.D. 0.016
Endrin Ketone N.D. 0.0040
Heptachlor N.D. 0.0016
Heptachlor Epoxide N.D. 0.0018
Methoxychlor N.D. 0.024
Toxaphene N.D. 0.24
LCS/LCSD
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/1 ug/1 ug/1 ug/1
Batch number: 171680011A Sample number(s) : 9050064-9050065
Aldrin 0.100 0.0936 94 28-119
Alpha BHC 0.0980 0.109 111 47-132
Beta BHC 0.0980 0.104 106 56-125
Gamma BHC - Lindane 0.0980 0.108 110 51-132
Alpha Chlordane 0.100 0.0979 98 53-126
Gamma Chlordane 0.100 0.108 108 53-130 I
1 p,p-DDD 0.196 0.229 117 42-148
p,p-DDE 0.198 0.208 105 51-129
p,p-DDT 0.196 0.211 108 40-145
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P######is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission group.
Page 4 of 9

. eurofins
•
Lancaster Laboratories Analysis Report
L= v)ronrentai
2425 New Holland Pike,Lancaster.PA 17601 • 717.656.2300 •Fax:[phone] • www.LancasterLabs.corn
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1813697
Reported: 06/29/2017 09:40
LCS/LCSD (continued)
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/1 ug/1 ug/1 ug/1
Delta BHC 0.0980 0.110 112 49-140
Dieldrin 0.194 0.196 101 54-126
Endosulfan I 0.0980 0.0878 90 40-138
Endosulfan II 0.200 0.185 92 54-124
Endosulfan Sulfate 0.198 0.200 101 41-133
Endrin 0.196 0.199 102 35-143
Endrin Aldehyde 0.198 0.199 100 40-135
Endrin Ketone 0.198 0.194 98 44-136
Heptachlor 0.0980 0.0968 99 38-135
Heptachlor Epoxide 0.100 0.103 103 56-132
Methoxychlor 0.984 1.03 105 39-143
MS/MSD
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Analysis Name Unspiked MS Spike MS MSD Spike MSD MS MSD MS/MSD RPD RPD
Conc Added Conc Added Conc %Rec %Rec Limits Max
ug/1 ug/1 ug/1 ug/1 ug/1
Batch number: 171680011A Sample number(s) : 9050064-9050065 UNSPK: P053469
Aldrin N.D. 0.100 0.0847 0.100 0.0944 85 94 28-119 11 30
Alpha BHC N.D. 0.0980 0.0973 0.0980 0.106 99 109 47-132 9 30
Beta BHC N.D. 0.0980 0.0955 0.0980 0.103 97 105 56-125 7 30
Gamma BHC - Lindane N.D. 0.0980 0.0998 0.0980 0.107 102 109 51-132 7 30
Alpha Chlordane N.D. 0.100 0.0872 0.100 0.0977 87 98 53-126 11 30
Gamma Chlordane N.D. 0.100 0.107 0.100 0.111 107 111 53-130 3 30
p,p-DDD N.D. 0.196 0.210 0.196 0.229 107 117 67-123 9 30
p,p-DDE N.D. 0.198 0.186 0.198 0.204 94 103 51-129 9 30
p,p-DDT N.D. 0.196 0.196 0.196 0.218 100 111 66-119 11 30
Delta BHC N.D. 0.0980 0.102 0.0980 0.109 104 111 76-126 7 30
Dieldrin N.D. 0.194 0.179 0.194 0.198 92 102 54-126 10 30
Endosulfan I N.D. 0.0980 0.0793 0.0980 0.0898 81 92 40-138 12 30
Endosulfan II N.D. 0.200 0.171 0.200 0.187 85 93 54-124 9 30
Endosulfan Sulfate N.D. 0.198 0.182 0.198 0.196 92 99 41-133 8 30
Endrin N.D. 0.196 0.185 0.196 0.200 94 102 35-143 8 30
Endrin Aldehyde N.D. 0.198 0.186 0.198 0.194 94 98 40-135 4 20
Endrin Ketone N.D. 0.198 0.184 0.198 0.196 93 99 44-136 6 30
Heptachlor N.D. 0.0980 0.0878 0.0980 0.0982 90 100 38-135 11 30
Heptachlor Epoxide N.D. 0.100 0.0919 0.100 0.101 92 101 56-132 9 30
Methoxychlor N.D. 0.984 0.967 0.984 1.03 98 105 39-143 6 30
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P######is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission group.
Page 5 of 9

tit eurofins
Lancaster Laboratories Analysis Report
Environmentai
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1813697
Reported: 06/29/2017 09:40
Surrogate Quality Control
Surrogate recoveries which are outside of the QC window are confirmed
unless attributed to dilution or otherwise noted on the Analysis Report.
Analysis Name: OC Pesticides in Water
Batch number: 171680011A
Tetrachloro-m-xylene Decachlorobiphenyl
9050064 113 87
9050065 87 50
Blank 113 48
LCS 107 57
MS 97 26*
MSD 103 33
Limits: 29-129 32-149
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P######is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission group.
Page 6 of 9

Routine Monitoring Report Review (MRR) Checklist
Permit No.: sal&. 0 D 14- 3 *;-
Permittee/Facility Name: c t6e,ta, &Lop
Report Name and Date: 20 - ct y-wvt, Q.l R c�
Reviewer: SW-,,,i,.G,'
Date Reviewed: 8/ 2 474 / 20 I
1. BIMS: Permit issued date: )v /i 3 /2 b t (o Expiration date: cl / 2L 2 / .
If Expired, check with Permittee if they want to renew.
2. BIMS: Log report in Events Tab. Select-> `Compliance Schedule Met' and enter name and
date of report, and date we received. Also, note that a Monitoring Report Review was
completed and inserted into report. -/
3. BIMS: For 5I reports- has Injection Event Report (IER) been received and info entered into
BIMS (Yes or No). If No, check file to see if we have received and then enter into
BIMS. If never received, then request from Consultant and CC Permittee via email. After
receipt of IERs from these parties, enter into BIMS.
4. BIMS: Check Wells Tab and see if GW-ls/GW-30s (if applicable) have been entered:
(Yes or No). If No and well status is still `proposed', then check file to see if we
have received GW-1 s and then enter into BIMS. If not received, then request from consultant
and CC Permittee. After receipt from these parties, enter as-built well construction into
BIMS; and well abandonment data, if applicable.
5. Do a quick review of report to see if there are any obvious impacts from injection activities by
reading Summary and Conclusions/Recommendation Section, and monitoring data tables.
Compare pre-injection levels of sulfate, iron,phosphate, etc. to post injection levels and note
this below. Also, note if there are any spikes in daughter products. If there are no impacts
evident, indicate 'No impacts from injection evident'. NOTE: The groundwater quality at
the site must be monitored until concentrations meet pre-injection levels or 2L standards
before the permit can eventually be Completed in BIMS, and a Completion Letter Sent to
Permittee.
NOTES: ,t
e(rer4JA.,0-v1-Cy ?S ./
6. When this Monitoring Report Review is complete, securely insert inside cover of
monitoring report and file.
MRR(Rev. 7-14-2017)

Greenville Qffice Charlotte Office
148 River Street, Suite 220 10806 Reames Road, Suite A
Greenville, SC 29601 Terra Charlotte, NC 28269
1.9999 980.312.5998
Fax: 8
Fax: [phone] Fax: [phone]
January 23, 2018
Mr. Mike Rogers
UIC Program ENE-
NC Division of Water Resources
n�-: U U
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2017 Annual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site -Route 211 Area
Aberdeen, North Carolina
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2017 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
• Analytical monitoring requirements summary (Table 1);
• Influent and effluent analytical results summary (Tables 2 and 3);
• Monitoring well analytical results summary (Table 4);
• Water levels and groundwater concentrations (Figure 1);
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratory data reports (Attachments).
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (June 14, 2017 and December 19, 2017) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2017 and experienced minimal downtime. The system
operates 24 hours per day and a total of 824,690 gallons (based upon the monthly
inspection logs dated between January 27 to December 19, 2017) of groundwater were
treated. Groundwater extraction rates averaged approximately 2,530 gpd during the
monitoring period. The treatment system removal efficiency was greater than 95% (see
Tables 2 and 3).
www.synterracorp.com

1 1
Greenville Qffice Charlotte Office
148 River Street,Suite 220 10806 Reames Road,Suite A
Greenville, SC 29601 Terra Charlotte, NC 28269
1.9999 980.312.5998
Fax: [phone].421.9909 Fax: [phone]
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), and one upgradient well, MW-1 (RT-MW-12), were
sampled on December 19, 2017 and analyzed for SW-846 8081A pesticides. Analytical
results are summarized in Table 4. Water levels were collected on December 19, 2017 and are
shown of Figure 1 along with corresponding detectable groundwater pesticide concentrations
for each well. Copies of the treatment system influent and effluent analytical reports and
the MW-1, MW-2 and MW-3 analytical report are included with the completed GW-59
forms provided as attachments.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section III and IV of the Site Groundwater Remediation
Permit issued October 13, 2016.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
a
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Electronic cc:
Jim Barber—NC DWR Fayetteville Garland Hilliard—Olin
Doug Rumford—NCDENR Michael Bogle, Esq. -WCS&R
Jon Bornholm—USEPA Ted Volskay-SynTerra
George Crouse -Syngenta
www.synterracorp.com

Route 211 Treatment System
2017 Annual Operating Report
SynTerra Corporation
January 2018
Table 1
Analytical Monitoring Requirements
Groundwater Extraction and Treatment System
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Frequency
(Permit No.
Location Parameters of Analysis WQ0014357)
Influent TCL Pesticides & pH Semi-annually
(RT-PW-01) (Jan.-June, July-Dec.)
Effluent TCL Pesticides & pH Semi-annually
(Jan.-June, July- Dec.)
MW-1 TCL Pesticides Annually
(RT-MW-12) & Water Level
MW-2 TCL Pesticides Annually
(05-MW-01) & Water Level
MW-3 TCL Pesticides Annually
(RT-MW-05) & Water Level

,
Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/14/17 06/14/17
Pesticides (ug/L)
Aldrin < 0.080 < 0.0016
alpha-BHC 0.069 < 0.0024
alpha-Chlordane < 0.0024 < 0.0024
beta-BHC 2.4 < 0.0027
p,p-DDD 0.067 < 0.0040
p,p-DDE 0.060 < 0.0040
p,p-DDT < 0.050 V < 0.0042
delta-BHC 7.0 < 0.0027
Dieldrin < 0.0042 < 0.0042
Endosulfan I 0.044 < 0.0034
Endosulfan II < 0.012 < 0.012
Endosulfan Sulfate < 0.0046 < 0.0046
Endrin < 0.0065 < 0.0065
Endrin Aldehyde < 0.050 V < 0.016
Endrin Ketone < 0.004 < 0.0040
gamma-BHC 0.062 < 0.0016
gamma-Chlordane 0.085 < 0.0056
Heptachlor < 0.002 < 0.0016
Heptachlor Epoxide 0.036 P < 0.0018
Methoxychlor 0.064 JP < 0.024
Toxaphene 7.7 < 0.24
Total Pesticides 17.69 0.0083
System Removal Efficiency: 99.95%
Notes:
Influent pH was 5.35 s.u.
J-estimated value
P- RPD>40%
V-RPD>100%
Since all effluent concentrations were ND, average detection limit of
all constituents divided by half was used for calculation.

Route 211 Treatment System
2017 Annual Operating Report
SynTerra Corporation
January 2018
Table 3
Treatment System Monitoring Results And
Treatment Removal Efficiency (July - December 2017)
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Period July - December 2017
Sample Name Influent Effluent
Date Sampled 12/19/17 12/19/17
Pesticides (ug/L)
Aldrin 0.095 P < 0.0017
alpha-BHC 0.054 < 0.0025
beta-BHC 1.80 < 0.0051 V
gamma-BHC (Lindane) 0.45 < 0.0017
alpha-Chlordane < 0.15 < 0.0025
gamma-Chlordane 0.14 < 0.0058
p,p-DDD < 0.13 < 0.0041
p,p-DDE 0.099 P < 0.0041
p,p-DDT < 0.064 V < 0.0043
delta-BHC 2.2 < 0.0028
Dieldrin 0.16 < 0.0044
Endosulfan I 0.048 < 0.0036
Endosulfan II 0.21 < 0.012
Endosulfan Sulfate < 0.024 < 0.0048
Endrin 0.10 P < 0.0067
Endrin Aldehyde 0.33 JP < 0.017
Endrin Ketone < 0.020 < 0.0041
Heptachlor < 0.0082 < 0.0017
Heptachlor Epoxide 0.094 P < 0.0019
Methoxychlor 0.41 J < 0.025
Toxaphene 12.0 < 0.25
Total pesticides 17.2 0.01
System Removal Efficiency: 99.95%
Notes:
Influent pH was 5.31
J-estimated value;P-RPD>40%;V-RPD>100%
Only measurable concentrations are used for removal efficiency.
Since all effluent concentrations were ND, average detection limit of
all constituents divided by half was used for calculation.
Permit specified removal efficiency: 95%

Route 211 Treatment System
2017 Annual Operating Report
Syn Terra Corporation
January 2018
Table 4
Monitoring Well Analytical Results Summary
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Sample Name MW-1 (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)
Sample Event Annual Annual Annual
Date Sampled 12/19/17 12/19/17 12/19/2017
Pesticides (ug/L)
Aldrin < 0.0017 < 0.0017 < 0.0017
alpha-BHC < 0.0025 < 0.0025 < 0.0025
beta-BHC < 0.0028 0.0074 JP < 0.0029
gamma-BHC (Lindane) < 0.0017 < 0.0017 < 0.0017
alpha-Chlordane < 0.0025 < 0.0025 < 0.0025
gamma-Chlordane < 0.0059 < 0.006 < 0.0059
p,p-DDD < 0.0042 < 0.0042 < 0.0042
p,p-DDE < 0.0042 < 0.0042 < 0.0042
p,p-DDT < 0.0044 < 0.0044 < 0.0044
delta-BHC < 0.0028 < 0.0028 < 0.0029
Dieldrin < 0.0044 < 0.0044 < 0.0045
Endosulfan I < 0.0036 < 0.0036 < 0.0036
Endosulfan II < 0.013 < 0.013 < 0.013
Endosulfan Sulfate < 0.0049 < 0.0049 < 0.0049
Endrin < 0.0068 < 0.0068 < 0.0069
Endrin Aldehyde < 0.017 < 0.017 < 0.017
Endrin Ketone < 0.0042 < 0.0042 < 0.0042
Heptachlor < 0.0017 < 0.0017 < 0.0017
Heptachlor Epoxide < 0.0019 < 0.0019 < 0.0019
Methoxychlor < 0.025 < 0.025 < 0.025
Toxaphene < 0.25 0.35 J < 0.25
MW-1 ( pH=4.57); MW-2 (pH=4.70); MW-3 (pH=4.87)
J-estimated value
P-RPD>40%
V-RPD>100%

N
ti
beta-BHC 0.00741P ug/I
toxaphene 0.35J u: I
05-MW-01 (MW-2)0
430.90 RT-MW-12 (MW-1)
432.11
--a—n--?�--'�"~ice,—'
RT-MW-05 (MW-3) Q , % r... - +
429.54 �'� � '
,k w�.. - /` N
aT�WA1 i ..
Po
0
0 50 100 200 1.1bOrNI
�� Feet yee/)
Legend 0 FIGURE 1
© EXTRACTION WELL MONITORING LOCATIONS AND
MONITORING WELL synTerra POTENTIOMETRIC MAP-
FORMER SOURCE AREA Source:Water levels measured December2017,Moore County2007 aerial,
and site surveys SURFICIAL AQUIFER
SURFACE WATER This map is a product of SynTerra.Reasonable efforts have been made to ensure the
accuracy of this map.SynTerra expressly disclaims any responsibility or liability with ROUTE 211 AREA
regard to the use of this map,and promotes and recommends the independent
GROUNDWATER SURFACE CONTOUR° verification of any data contained on this map by the user of this map product.
Created by.B.Russo on 06/22/2016 ABERDEEN PESTICIDE DUMPS SITE
*Water elevations(ft msl)measured December 2017. P iSyngenta 1053104 01. Rt 211 DowngrediennFigures12018-011Fig-gt-MorntoringLocations mxd MOORE COUNTY,NORTH CAROLINA

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mall Original
DEPARTMENT Y ENVIRONMENTO , NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]-
FACILITY INF_QPMATION Please Print Clearly or Type
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021
WQ0014357 -
Permit Name (if different): Non Discharge UIC -
Facility Address: NC Highway Route 211 NPDES
Aberdeen t'ireci7 NC 28315 TYPE OF PERMITTED OPERATION BEING MONITORED
(cnyi -__— — (stave) (bpi County Moore
. X
Ted Voiskay [phone] Lagoon Remediation: Infiltration Gallery
Contact Person: Telephone #:
Well Location/Site Name: _RT-Pw-o1 to treatment system No. of Wells to be Sampled:
a Spray Field Remediation:
p tt,om Permiu
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): _ RT-PW-01 ' For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6•0 in. Check One: 0 Influent (98)
Screened Interval: 16.07 ft. to 40.51 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point (M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/14/2017 Date sample analyzed: 06/19/2017
Field analysis: pH 5.35 , Specific Conductance 87 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.8 °C, Odor, none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /1 00m Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/ Ca - Calcium _ mg/I
Chloride mg/ Cd - Cadmium mg/I
Arsenic mg/ Chromium: Total mg/I
Grease and Oils mg/ Cu - Copper mg/I
Phenol mg/ Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/I (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia ____ mg/ Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N mg/ Mn - Manganese mg/I TCL Pesticides : method # = 8081A
method it =.
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A. Mann, P.E., Project Manager
P or Auth ized nt)Name and Title-Please print or type
...-- '7/6/1l.10
GW-59 •Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mall Original DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone] -
FACILITY INFORMATION Please Print Clearly or Type
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE. Sept.30,2021
Permit Name (if different): Non-Discharge WQ0014357 UIC
Facility Address: NC Highway Route 211 NPDES —_.
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 Moore
County
(City) (state) (Zip) Lagoon X Remediation: Infiltration Gallery
Contact Person: Ted Volskay Telephone #: [phone] g
Well Location/ Site Name: -Treatment syst.discharge t°infiltration gallery No. of Wells to be Sampled: ' Spray Field Remediation:
(Item Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft, Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06/14/2017 Date sample analyzed: 06/19/2017
Field analysis: pH 5.44 , Specific Conductance 89 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 2U.7 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc - mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic _ mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper _ mg/I
Phenol __ mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report)
Specific Conductance _ uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N .. mg/I Mn - Manganese mg/I TCL Pesticides •: method # = 8081A
method #
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false Information,
Including the possibility of fines and Imprisonment for knowing violations. 1 ho-nes A. Mann, P.E., Project Manager
Pennine.(or Authorized gen me and Title-Please print or type
1 ,s-yv .7/6/9\017
GW-59 Signature of Per ittee(or Authorized Agent) Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
-- 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:septa 30,2021
Non-Discharge WQ0014357 UIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (ZIP) County X
Tom Mann [phone] Lagoon Remediation: Infiltration Gallery
Contact Person: Telephone #:
Well Location/ Site Name: No. of Wells to be Sampled: Spray Field Remediation:
(ffom Peftn1t) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter:6.0 in. Check One: 0 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: NA ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 12/19/2017 Date sample analyzed: 01/10/2018
Field analysis: pH 5.31 , Specific Conductance 60 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 23.8 °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC _ _ mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method # = 6061A
: method # _
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
t .1 .A ti Permittee(or Authorized Agent)Name and Title-Please print or type
1�' T ho-n'wt -A. M G,vl t't, 1/2 3/2 018
G W 59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mall OriginalDEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to:
WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: WQ0014357 EXPIRATION DATE: Sept:30,2021
Permit Name (if different): Non DischargeUIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED '
(City) (Slate) (Zip) County X
Contact Person: Tom Mann Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): NA For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 12/19/2017 Date sample analyzed: 01/10/2018
Field analysis: pH 5.11 , Specific Conductance 70 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 23.5 °C, Odor none Appearance Clear Certification No. NC Lab Certification#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/ I
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
£„ Thoww -A. Ma.vt.vt. 1/23/2018
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH, NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type '
PERMIT#: EXPIRATION DATE: Sept.30,2021
Facility Name: Route 211 Area g WQ0014357
Permit Name (if different):
Non-Dischar e UIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (Zip)
County X
Contact Person: Ted Volskay Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/ Site Name: No. of Wells to be Sampled: a Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(fromRT-Mw-12(MW-1)
Permit): For Groundwater Treatment Systems Other:
Well Depth: 20.50 ft. Well Diameter: 2.0 in. Check One: 0 Influent (98)
Screened Interval: 1070 ft. to 20.50 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 13.50 ft. below measuring point.
colloidal concentrations.
Measuring Point(M.P.) is: 2.18 ft. above land surface. Relative M.P. Elevation in ft.: 445.61
Gallons of water pumped/bailed before sampling: 3.5 Date sample collected: 12/19/2017 Date sample analyzed: 01/10/2018
Field analysis: pH 4.57 , Specific Conductance 30 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
17.7none Clear Certification No. NC Certification No.521
Temp. °C, Odor Appearance
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance _ uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
` a: . ) Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 T?wm � vy aA. Mawl. 1/23/2018
Rev. 03/2000 Signature of Permittee(or Authorized Agent) (Date)

GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type .
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021
Permit Name (if different): Non-Discharge WQ0014357 UIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (Zip) County X
Tom Mann 864 527-4617 Lagoon Remediation: Infiltration Gallery
Contact Person: Telephone #: ( )
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): 05-MW-01(MW-2) For Groundwater Treatment Systems Other:
Well Depth: 37.52 ft. Well Diameter:4.0 in. Check One: ❑ Influent (98)
Screened Interval:22.67 ft. to 37.52 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 23.50 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 3.22 ft. above land surface. Relative M.P. Elevation in ft.: 454.40
Gallons of water pumped/bailed before sampling: 27.5 Date sample collected: 12/19/2017 Date sample analyzed: 01/10/2018
Field analysis: pH 4.70 , Specific Conductance 40 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 20.2 °C, Odor None Appearance Clear Certification No. NC Certification 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury _ ____ _ mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method # = 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
ThQmak A. Ma vwt. 1/23/2018
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021
Non-Discharge WQ0014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen (Street) NC 28315Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (Zip) County X
Contact Person: Tom Mann Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (from Permit) Rotary Distributor _ Land Application of Sludge
Well Identification Number(from Permit): RT-Mw-05(Mw-3) For Groundwater Treatment Systems Other:
Well Depth: 24.57 ft. Well Diameter:2.0 in. Check One: 0 Influent (98)
Screened Interval: 14.57 ft. to 24.57 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 20.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.67 ft. above land surface. Relative M.P. Elevation in ft.: 449.59
Gallons of water pumped/bailed before sampling: 2.5 Date sample collected: 12/19/2017 Date sample analyzed: 01/10/2018
Field analysis: pH 4.87 , Specific Conductance 20 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 18.5 °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
G W 59 7�t ovvt alb A. M avt iti 172372 01 8
Rev. 03/2000 Signature of Permittee(or Authorized Agent) (Date)

tiff' eurofins
Lancaster Laboratories :
Environmental
•
2425 New Holland Pike.Lancaster.PA 17601•717-656-2300•Fax:711i56-6266•www.Eurofin5US comfLancLaIxEnv
ANALYSIS REPORT
Prepared by: Prepared for:
Eurofins Lancaster Laboratories Environmental Synterra Corporation
2425 New Holland Pike Suite 220
Lancaster, PA 17601 148 River Street
Greenville SC 29601
Report Date: January 17, 2018 14:48
Project: Rte 211 Treatment System, NC
Account#: 12819
Group Number: 1889721
PO Number: 1053.04.01
State of Sample Origin: NC
Regulatory agencies do not accredit laboratories for all methods, analytes, and matrices. Our current
scopes of accreditation can be viewed at http://www.eurofinsus.com/environment-
testing/laboratories/eurofins-lancaster-laboratories-environmental/resources/certifications/ . To request
copies of prior scopes of accreditation, contact your project manager.
Electronic Copy To Synterra Corporation Attn: Ted Volskay
Respectfully Submitted,
Lyssa M. Longenecker
Specialist
[phone]
Page 1 of 15

tiff eurofins •
Lancaster Laboratorie, �!'"' "
a Environmental -.v
2425 New Monand Pike,Lancaster.PA 17601•717b56-2300•Fax:[phone]•www.EurafnsUS.comllanclassEnv
SAMPLE INFORMATION
Client Sample Description Sample Collection ELLE#
Date/Time
RT-MW-12 (MW-1) Grab Groundwater 12/19/2017 14:37 9380218
Effluent Grab Groundwater 12/19/2017 15:44 9380219
C2-C3 Grab Groundwater 12/19/2017 15:58 9380220
C1-C2 Grab Groundwater 12/19/2017 15:51 9380221
05-MW-01(MW-2) Grab Groundwater 12/19/2017 13:55 9380222
RT-MW-05(MW-3) Grab Groundwater 12/19/2017 15:09 9380223
Influent Grab Groundwater 12/19/2017 15:33 9380224
The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory
Sample Analysis Record.
Page 2 of 15

ti'• eurgfins .
Lancaster Laboraf. Analysis Report
Eririrnr,m 3nt,7i
2625 New Holland Pike,Lancaster.PA 17601.711356-2300•Fax:717456b166.www.EurollnsUS.conalancLabsEnv
Sample Description: RT-MW-12 (MW-1)Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380218
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 14:37
CAT
No. Analysis Name CAS Number Method Dilution
Result Detection Limit Factor
Pesticides SW-846 8081 B ug/I ug/I
10589 Aldrin 309-00-2 N.D. D1 0.0017 1
10589 Alpha BHC 319-84-6 N.D. D1 0.0025 1
10589 Beta BHC 319-85-7 N.D. D1 0.0028 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D1 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. D1 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. D1 0.0059 1
10589 p,p-DDD 72-54-8 N.D. D2 0.0042 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0042 1
10589 p,p-DDT 50-29-3 N.D. ZD2 0.0044 1
10589 Delta BHC 319-86-8 N.D. D1 0.0028 1
10589 Dieldrin 60-57-1 N.D. D2 0.0044 1
10589 Endosulfan I 959-98-8 N.D. D1 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. D2 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0049 1
10589 Endrin 72-20-8 N.D. D2 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. D2 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0042 1
10589 Heptachlor 76-44-8 N.D. D1 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0019 1
10589 Methoxychlor 72-43-5 N.D. D2 0.025 1
10589 Toxaphene 8001-35-2 N.D. D2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 11:26 Anita M Dale 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Page 3 of 15

tiff eurofins.
Lancaster Labora :I Analysis Report
, 7
2425 New Holland Pike.Lancaster.PA 17601•717-56-2300.Fax:[phone]•www.EurotlnsUS coMLanctaesEnv
Sample Description: Effluent Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380219
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 15:44
CAT Method Dilution
No. Analysis Name CAS Number Result Detection Limit Factor
Pesticides SW-846 8081 B ug/1 ug/I
10589 Aldrin 309-00-2 N.D. D1 0.0017 1
10589 Alpha BHC 319-84-6 N.D. D1 0.0025 1
10589 Beta BHC 319-85-7 N.D. VD2 0.0051 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D1 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. D1 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. D2 0.0058 1
10589 p,p-DDD 72-54-8 N.D. D2 0.0041 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0041
1
10589 p,p-DDT 50-29-3 N.D. ZD2 0.0043 1
10589 Delta BHC 319-86-8 N.D. D1 0.0028 1
10589 Dieldrin 60-57-1 N.D. D2 0.0044 1
10589 Endosulfan I 959-98-8 N.D. D1 0.0036 1
10589 Endosulfan II 3 32 1 3-6 5-9 N.D. D2 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0048 1
10589 Endrin 72-20-8 N.D. D2 0.0067 1
10589 Endrin Aldehyde 7421-93-4 N.D. D2 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0041 1
10589 Heptachlor 76-44-8 N.D. D1 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0019 1
10589 Methoxychlor 72-43-5 N.D. D2 0.025 1
10589 Toxaphene 8001-35-2 N.D. D2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 11:39 Anita M Dale 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Page 4 of 15

tiff. eurofins•
Lancaster Laboratorit Analysis Report
FIl`iir!?!'rrlt'r?t.1i
1
2425 New Holland Pike.Lancaster.PA 17601•717-656-2300•Fax [phone]•wwr.EurofinsUS comALancLatnEnv
Sample Description: C2-C3 Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WIN 9380220
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 15:58
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides SW-846 8081 B ughl ugil
10589 Aldrin 309-00-2 N.D. D2 0.0017 1
10589 Alpha BHC 319-84-6 N.D. D1 0.0025 1
10589 Beta BHC 319-85-7 0.012 D1 0.0028 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D1 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. D2 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. D2 0.0059 1
10589 p,p-DDD 72-54-8 N.D. D2 0.0042 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0042 1
10589 p,p-DDT 50-29-3 N.D. ZD2 0.0044 1
10589 Delta BHC 319-86-8 0.0086 D1 0.0028 1
10589 Dieldrin 60-57-1 N.D. D2 0.0044 1
10589 Endosulfan I 959-98-8 N.D. D1 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. D2 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0049 1
10589 Endrin 72-20-8 N.D. D2 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. D2 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0042 1
10589 Heptachlor 76-44-8 N.D. D2 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0019 1
10589 Methoxychlor 72-43-5 N.D. D2 0.025 1
10589 Toxaphene 8001-35-2 N.D. D2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 11:53 Anita M Dale 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Pape 5 of 15

tiff eurofins
Lancaster Laborato6-, Analysis Report
Fr1LIronnt ritAl
r
2425 New Holland Pike,Lancaster.PA 17601•717-656-2300•Fax:[phone]•www.EurofinsUS cornlLancLabsEnv
Sample Description: C1-C2 Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380221
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 15:51
CAT Method Dilution
No. Analysis Name CAS Number Result
Detection Limit Factor
Pesticides SW-846 8081 B ug/I ug/l
10589 Aldrin 309-00-2 0.027 PD2 0.0016 1
10589 Alpha BHC 319-84-6 0.013 D1 0.0025 1
10589 Beta BHC 319-85-7 0.44 D1 0.014 5
10589 Gamma BHC-Lindane 58-89-9 0.010 D1 0.0016 1
10589 Alpha Chlordane 5103-71-9 0.061 PD2 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.076 D1 0.0058 1
10589 p,p-DDD 72-54-8 N.D. D2 0.021
5
10589 p,p-DDE 72-55-9 0.045 JPD2 0.021 5
10589 p,p-DDT 50-29-3 N.D. ZVD2 0.028 5
10589 Delta BHC 319-86-8 0.48 D1 0.014 5
10589 Dieldrin 60-57-1 0.070 JD2 0.022 5
10589 Endosulfan I 959-98-8 0.030 JD1 0.018 5
10589 Endosulfan II 33213-65-9 0.090 JD2 0.062 5
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.024 5
10589 Endrin 72-20-8 0.045 JPD2 0.033 5
10589 Endrin Aldehyde 7421-93-4 N.D. D1 0.082 5
10589 Endrin Ketone 53494-70-5 N.D. D2 0.021 5
10589 Heptachlor 76-44-8 N.D. D2 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 0.018 PD1 0.0019 1
10589 Methoxychlor 72-43-5 0.17 JD2 0.12 5
10589 Toxaphene 8001-35-2 4.8 D2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 173550039A 01/10/2018 12:06 Anita M Dale 1
10589 OC Pesticides in Water SW-846 8081E 1 173550039A 01/10/2018 12:20 Anita M Dale 5
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Paae 6 of 15

titi eurofins•
Lancaster Laboratcr Analysis Report
1
2425 New Holland Pike,Lancaster.PA 17601•717-656-2300•Fax:[phone]•wwv.EuroflnsUS.com/LancLabsEnv
Sample Description: 05-MW-01(MW-2) Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380222
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 13:55
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides SW-846 8081 B ugh ug/l
10589 Aldrin 309-00-2 N.D. D2 0.0017 1
10589 Alpha BHC 319-84-6 N.D. D1 0.0025 1
10589 Beta BHC 319-85-7 0.0074 JPD2 0.0028 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D1 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. D1 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. D1 0.0059 1
10589 p,p-DDD 72-54-8 N.D. D2 0.0042 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0042 1
10589 p,p-DDT 50-29-3 N.D. ZD2 0.0044 1
10589 Delta BHC 319-86-8 N.D. D1 0.0028 1
10589 Dieldrin 60-57-1 N.D. D2 0.0044 1
10589 Endosulfan I 959-98-8 N.D. D2 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. D2 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0049 1
10589 Endrin 72-20-8 N.D. D2 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. D2 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0042 1
10589 Heptachlor 76-44-8 N.D. D2 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0019 1
10589 Methoxychlor 72-43-5 N.D. D2 0.025 1
10589 Toxaphene 8001-35-2 0.35 JD2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 12:33 Anita M Dale 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Paae 7 of 15

titi eurQfins
Lancaster Laborator - Analysis Report
Eri I ,l~r,,,."t,t)
2025 New Holland Pike.Lancaster.PA 17601•717 4 56-2306•Fax:[phone]•wwww.EUIOTinsUS.comQLancLanaEnv
Sample Description: RT-MW-05(MW-3)Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380223
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 15:09
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides SW-846 8081 B ugh ugh
10589 Aldrin 309-00-2 N.D. D1 0.0017 1
10589 Alpha BHC 319-84-6 N.D. D1 0.0025 1
10589 Beta BHC 319-85-7 N.D. D2 0.0029 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D1 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. D2 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. D1 0.0059 1
10589 p,p-DDD 72-54-8 N.D. D2 0.0042 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0042 1
10589 p,p-DDT 50-29-3 N.D. ZD2 0.0044 1
10589 Delta BHC 319-86-8 N.D. D1 0.0029 1
10589 Dieldrin 60-57-1 N.D. D2 0.0045 1
10589 Endosulfan I 959-98-8 N.D. D2 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. D2 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0049 1
10589 Endrin 72-20-8 N.D. D2 0.0069 1
10589 Endrin Aldehyde 7421-93-4 N.D. D2 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0042 1
10589 Heptachlor 76-44-8 N.D. D2 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0019 1
10589 Methoxychlor 72-43-5 N.D. D2 0.025 1
10589 Toxaphene 8001-35-2 N.D. D2 0.25 1
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 12:47 Anita M Dale 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Page 8 of 15

tiff eurpfins,
Lancaster Labora:cr Analysis Report
2425 New Holland Pike,Lancaster.PA 17601•717-656-2300•Fan:717-56-6766•www.EuroinsUS.coMlancLabsEnv
Sample Description: Influent Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9380224
ELLE Group#: 1889721
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 12/21/2017 08:45
Collection Date/Time: 12/19/2017 15:33
CAT
No. Analysis Name CAS Number Method Dilution
Result Detection Limit Factor
Pesticides SW-846 8081 B ug/l ug/l
10589 Aldrin 309-00-2 0.095 PD2 0.0082 5
10589 Alpha BHC 319-84-6 0.054 D1 0.012 5
10589 Beta BHC 319-85-7 1.8 D1 0.14 50
10589 Gamma BHC-Lindane 58-89-9 0.045 D2 0.0082 5
10589 Alpha Chlordane 5103-71-9 N.D. D2 0.15 5
10589 Gamma Chlordane 5103-74-2 0.14 D1 0.029 5
10589 p,p-DDD 72-54-8 N.D. D2 0.13 5
10589 p,p-DDE 72-55-9 0.099 PD2 0.020 5
10589 p,p-DDT 50-29-3 N.D. ZVD2 0.064 5
10589 Delta BHC 319-86-8 2.2 D1 0.14 50
10589 Dieldrin 60-57-1 0.16 D2 0.022 5
10589 Endosulfan I 959-98-8 0.048 D2 0.018 5
10589 Endosulfan II 33213-65-9 0.21 D2 0.061 5
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.024 5
10589 Endrin 72-20-8 0.10 PD2 0.033 5
10589 Endrin Aldehyde 7421-93-4 0.33 JPD2 0.082 5
10589 Endrin Ketone 53494-70-5 N.D. D2 0.020 5
10589 Heptachlor 76-44-8 N.D. D2 0.0082 5
10589 Heptachlor Epoxide 1024-57-3 0.094 PD1 0.0094 5
10589 Methoxychlor 72-43-5 0.41 JD2 0.12 5
10589 Toxaphene 8001-35-2 12 D2 1.2 5
Z=The response for a target analyte(s)in the continuing
calibration verification standard is outside the QC acceptance
limits. Since the response is high indicating increased
sensitivity,and the target analyte(s)is not detected in the
sample,the data is reported.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/10/2018 13:14 Anita M Dale 5
10589 OC Pesticides in Water SW-846 8081B 1 173550039A 01/11/2018 21:49 Anita M Dale 50
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 173550039A 12/22/2017 16:09 Kate E Lutte 1
Paae 9 of 15

. eurQfins,
Lancaster Laboratorii Analysis Report
, Env,ror,niPntal
,
2a25 New Holland Pike.Lancaster.PA 17601.711-656-2300.Fax:[phone]•www.EurolinsUS comM1alcLabsEnv
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1889721
Reported: 01/17/2018 14:48
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations,to demonstrate precision and accuracy at a
batch level,a LCS/LCSD was performed,unless otherwise specified in the method.
All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless otherwise noted on the Analysis Report.
Method Blank
Analysis Name Result MDL
ugh! ug/I
Batch number: 173550039A Sample number(s):9380218-9380224
Aldrin N.D. 0.0016
Alpha BHC N.D. 0.0024
Beta BHC N.D. 0.0027
Gamma BHC-Lindane N.D. 0.0016
Alpha Chlordane N.D. 0.0024
Gamma Chlordane N.D. 0.0056
p,p-DDD N.D. 0.0040
p,p-DDE N.D. 0.0040
p,p-DDT N.D. 0.0042
Delta BHC N.D. 0.0027
Dieldrin N.D. 0.0042
Endosulfan I N.D. 0.0034
Endosulfan II N.D. 0.012
Endosulfan Sulfate N.D. 0.0046
Endrin N.D. 0.0065
Endrin Aldehyde N.D. 0.016
Endrin Ketone N.D. 0.0040
Heptachlor N.D. 0.0016
Heptachlor Epoxide N.D. 0.0018
Methoxychlor N.D. 0.024
Toxaphene N.D. 0.24
LCS/LCSD
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/I ug/I ug/I ug/l
Batch number: 173550039A Sample number(s):9380218-9380224
Aldrin 0.100 0.0870 0.100 0.0602 87 60 28-119 36* 30
Alpha BHC 0.0980 0.0944 0.0980 0.0658 96 67 47-132 36* 30
Beta BHC 0.0980 0.0889 0.0980 0.0647 91 66 56-125 32* 30
Gamma BHC-Lindane 0.0980 0.0937 0.0980 0.0665 96 68 51-132 34* 30
Alpha Chlordane 0.100 0.0990 0.100 0.0678 99 68 53-126 37* 30
Gamma Chlordane 0.100 0.101 0.100 0.0700 101 70 53-130 36* 30
p,p-DDD 0.196 0.197 0.196 0.126 101 64 42-148 44* 30
p,p-DDE 0.198 0.172 0.198 0.110 87 55 51-129 45* 30
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P###1 #is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission
group.
Page 10 of 15

tiff eurpfins
Lancaster Laboratorie Analysis Report
► Environmental
2425 New Holland Pike.Lancaster,PA 17601•717456-2300.Fax:[phone]•www.EurofinsUS.com(la*CLaHsEnv
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1889721
Reported: 01/17/2018 14:48
LCS/LCSD (continued)
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/I ug/l ug/I ug/I
p,p-DDT 0.196 0.223 0.196 0.155 114 79 40-145 36* 30
Delta BHC 0.0980 0.0915 0.0980 0.0655 93 67 49-140 33* 30
Dieldrin 0.194 0.179 0.194 0.118 92 61 54-126 41* 30
Endosulfan I 0.0980 0.0795 0.0980 0.0652 81 67 40-138 20 30
Endosulfan II 0.200 0.179 0.200 0.116 89 58 54-124 43* 30
Endosulfan Sulfate 0.198 0.186 0.198 0.118 94 60 41-133 45* 30
Endrin 0.196 0.186 0.196 0.118 95 60 35-143 45* 30
Endrin Aldehyde 0.198 0.173 0.198 0.128 87 65 40-135 30* 20
Endrin Ketone 0.198 0.199 0.198 0.131 101 66 44-136 41* 30
Heptachlor 0.0980 0.0894 0.0980 0.0630 91 64 38-135 35* 30
Heptachlor Epoxide 0.100 0.0957 0.100 0.0658 96 66 56-132 37* 30
Methoxychlor 0.984 0.952 0.984 0.634 97 64 39-143 40* 30
Surrogate Quality Control
Surrogate recoveries which are outside of the QC window are confirmed unless
attributed to dilution or otherwise noted on the Analysis Report. For dual
column analyses,the surrogate(at least one surrogate for multi-surrogate
tests)must be within the acceptance limits on at least one of the two
columns.
Analysis Name:OC Pesticides in Water
Batch number: 173550039A
Tetrachloro-m-xylene-D1 Decachlorobiphenyl-D1 Tetrachloro-m-xylene-D2 Decachlorobiphenyl-D2
9380218 70 99 72 74
9380219 80 94 68 64
9380220 81 89 70 67
9380221 96 69 70 47
9380222 74 48 61 34
9380223 83 43 70 31*
9380224 79 45 58 31*
Blank 80 33 67 23*
LCS 85 47 72 34
LCSD 59 19* 47 14*
Limits: 29-129 32-149 29-129 32-149
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
' (2)The unspiked result was more than four times the spike added.
P#1144 is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission
group. 1
Page 11 of 15

Environmental Analysis Request/Chain of Custody
•ti For Eurofins Lancaster Laboratories Environmental use only d
tiff eurofins + 1 c�v c� 2 Y _ (� � ��. � �� "�,�
Lancaster Laboratories Acct.# l� '19 Group# I °cl i3 i Sample# r 3 S o d i `4- 1 COC
Environmental
Client Information Ma ix Analysis Requested For Lab Use Only
Client: -�- Acct.#: El Preservation Codes FSC: __
.5r P I f.3(-1 ��t ,r'/,/ • SCR#
ProjedtName/#: / y7 Ty PWSID#: H 'c a v� 1 Preservation Codes
y cd H=HCI T=Thlosulfate
R-1 f^— i
i LI� TF ,/7ntlr.yf ✓X.5�ZFt ' 2 j
Project Manager: P.O.#: ❑ 0 N=HNO3 B=NaOH
L �1 S=H2SO4 O=Other
tAi.s of
Sampler: C / Quote#: c E ? I Remarks
T Vr r� d 5 v !v
n is��r l /44a��� E w c n " ! , .
State where samples were c II ted: For Compliance: 'fl a „\
AI(_- I Yes ❑ No [ ' Cl) IZ z o cc ,
Collected a E Ela :: y V 4:3 II _
Sample Identification ;n o = t° �- o ��
Date Time 0 V cn O t- s ~
W '12 I—Iti1 l,tI _i e rat vLi -- 1) l,J17//-7 , /a?'7 - )C" 1- �
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('-,l c_ '2 /71/3/l 7 /5_S) X 0I a-. X
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V 7._kl/1IA) —0 T (M.6) --7) 14.14/17 150 ci k- K Z :7 .
i S 3 K. ry
. 4$%- -4�-------
Turns ,,ad Time(TAT) Requested(please circle) Relinq by to Time Received Date Time
J$tctnd Rush C.� )8 - �1,2"i ����� ��,�e �/ +(�1//7 (�`c-Y0
Re nqulshed by Date Time Received by Date Time
(Rush TAT Is subject to laboratory approval and surcharge.) �'� 1, v. /
?7_ /.e`/ I/- /Z00 t`-eS /./2,I7 /z o
Date results are needed: Rein wished by Date Time Received by Date Time
E-mail address: Relinquished by
Date Time Received by Date Time
Data Package Options(circle if required)
Type I (EPA Level 3 Relinquished by Date Time Receiv d by % �/ TI
Equivalent/non-CLP) Type VI(Raw Data Only) /)- V
T e III Reduced non CLP NJ DKQP TX TRRP 13 EDD Required? Yes No Relinquishhee by Commercial Carrier:
YP ( ) If yes,format: UPS . FedEx Other
NYSDEC Category A or B MA MCP CT RCP Site Specific QC(MS/MSD/Dup)? Yes No Temperature upon receipt Z:7°C
(If yes,indicate QC sample and submit triplicate sample volume.)
Eurofins Lancaster Laboratories Environmental,LLC•2425 New Holland Pike,Lancaster, PA 17601 •717-656-2300
The white copy should accompany samples to Eurofins Lancaster Laboratories Environmental.The yellow copy should be retained by the client. 7044 0216
Page 12 of 15

eurofins Sample Administration Doc Log ID: 204503
Lancaster Laboratori s Receipt Documentation Log I1111111111111111111111111111111liii 1111
(environmental
Group Number(s): 1889721
Client: SY JTERRA CORP
Delivery and Receipt Information
Delivery Method: UPS Arrival Timestamp: 12/21/2017 8:45
Number of Packages: 1 Number of Projects: 1
State/Province of Origin: NC
Arrival Condition Summary
Shipping Container Sealed: Yes Sample IDs on COC match Containers: Yes
Custody Seal Present: Yes Sample Date/Times match COC: Yes
Custody Seal Intact: Yes VOA Vial Headspace>_6mm: N/A
Samples Chilled: Yes Total Trip Blank Qty: 0
Paperwork Enclosed: Yes Air Quality Samples Present: No
Samples Intact: Yes
Missing Samples: No
Extra Samples: No
Discrepancy in Container Qty on COC: No
Unpacked by Wendy Wakeley(1669)at 09:11 on 12/21/2017
Samples Chilled Details
Thermometer Types: DT=Digital(Temp. Bottle) IR=Infrared(Surface Temp) All Temperatures in °C.
Cooler# Thermometer ID Corrected Temp Therm.Type Ice Type Ice Present? Ice Container Elevated Temp?
1 32170023 2.7 IR Wet Y Bagged N
Page 1 of 1 2425 New Holland Pike T 717-656-2300
Lancaster, PA 17605-2425 F 717-656-2681
Pape 13 of 15 www.LancasterLabs.com

tiff eurofins
Lancaster Laboratories' Environmental Explanation of Symbols and Abbreviations
The followi,,g define common symbols and abbreviations used in reporting technical data:
BMQL Below Minimum Quantitation Level mg milligram(s)
C degrees Celsius mL milliliter(s)
cfu colony forming units MPN Most Probable Number
CP Units cobalt-chloroplatinate units N.D. non-detect
F degrees Fahrenheit ng nanogram(s)
g gram(s) NTU nephelometric turbidity units
IU International Units pg/L picogram/liter
kg kilogram(s) RL Reporting Limit
L liter(s) TNTC Too Numerous To Count
lb. pound(s) pg microgram(s)
m3 cubic meter(s) pL microliter(s)
meq milliequivalents umhos/cm micromhos/cm
< less than
> greater than
ppm parts per million-One ppm is equivalent to one milligram per kilogram (mg/kg)or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter(mg/I), because one liter of water has a weight
very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported on an
as-received basis.
Analytical test results meet all requirements of the associated regulatory program (i.e., NELAC (TNI), DoD, and ISO 17025) unless
otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the
collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved,the test results will be
meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held
responsible for sample integrity, however, unless sampling has been performed by a member of our staff.
This report shall not be reproduced except in full,without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR Part 136 Table II as"analyze immediately"are not performed within
15 minutes.
WARRANTY AND LIMITS OF LIABILITY- In accepting analytical work, we warrant the accuracy of test results for the sample as submitted.
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Page 1s4�or 15

eurofins
Lancaster Laborator Data Qualifiers
"Environmental
y � i
Qualifier Definition
C Result confirmed by reanalysis
D1 Indicates for dual column analyses that the result is reported from column 1
D2 Indicates for dual column analyses that the result is reported from column 2
E Concentration exceeds the calibration range
J(or G, I,X) Estimated value>=the Method Detection Limit(MDL or DL)and<the Limit of Quantitation(LOQ or RL)
P Concentration difference between the primary and confirmation column>40%. The lower result is reported.
U Analyte was not detected at the value indicated
✓ Concentration difference between the primary and confirmation column>100%. The reporting limit is raised
due to this disparity and evident interference.
W The dissolved oxygen uptake for the unseeded blank is greater than 0.20 mg/L.
Z Laboratory Defined-see analysis report
Additional Organic and Inorganic CLP qualifiers may be used with Form 1 reports as defined by the CLP methods.
Qualifiers specific to Dioxin/Furans and PCB Congeners are detailed on the individual Analysis Report.
Page 15 of 15

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January 20, 2017
RECEIVED/NCDFCmWR
Mr. Mike Rogers JAN 26 2017
UIC Program Water Quality Regional
NC Division of Water Resources Operations Section F
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
il
RE: 2016 Annual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site - Route 211 Area
Aberdeen, North Carolina
A
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2016 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
i
• Analytical monitoring requirements summary (Table 1);
• Influent and effluent analytical results summary (Tables 2 and 3);
• Monitoring well analytical results summary (Table 4); Ie
• Water levels and groundwater concentrations (Figure 1);
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratory data reports (Attachments).
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (August 9, 2016 and December 15, 2016) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2016 and experienced minimal downtime. The system
operates 24 hours per day and a total of 930,460 gallons (based upon the monthly
inspection logs dated between January 28 to December 14, 2016) of groundwater were
treated. Groundwater extraction rates averaged approximately 2,900 gpd during the
f
INNOVATE 148 River Street, Suite 220 Greenville, SC 29601 [phone] Fax [phone] www.synterracorp.com is
Si

2016 Annual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
January 2017
Page Two
monitoring period. The treatment system removal efficiency was greater than 95% (see
Tables 2 and 3).
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), and one upgradient well, MW-1 (RT-MW-12), were
sampled on December 14, 2016 and analyzed for SW-846 8081A pesticides. Analytical
results are summarized in Table 4. Water levels were collected on December 14, 2016 and are
shown of Figure 1 along with corresponding detectable groundwater pesticide concentrations
for each well. Copies of the treatment system influent and effluent analytical reports and
the MW-1, MW-2 and MW-3 analytical report are included with the completed GW-59
forms provided as attachments.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section III and IV of the Site Groundwater Remediation
Permit issued October 13, 2016.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Electronic cc:
Jim Barber—NC DWR Fayetteville Garland Hilliard—Olin
Doug Rumford—NCDENR Michael Bogle, Esq. -WCS&R
Jon Bornholm—USEPA Ted Volskay -SynTerra
George Crouse -Syngenta
INNOVATE 148 River Street, Suite 220 Greenville, SC 29601 [phone] Fax[phone] www synterracorp corn

Route 211 Treatment System
2016 Annual Operating Report
SynTerra Corporation
January 2017
Table 1
Analytical Monitoring Requirements
Groundwater Extraction and Treatment System
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Frequency
(Permit No.
Location Parameters of Analysis WQ0014357)
Influent TCL Pesticides & pH Semi-annually
(RT-PW-01) (Jan.-June,July-Dec.)
Effluent TCL Pesticides & pH Semi-annually
(Jan.-June, July- Dec.)
MW-1 TCL Pesticides Annually
(RT-MW-12) & Water Level
MW-2 TCL Pesticides Annually
(05-MW-01) & Water Level
MW-3 TCL Pesticides Annually
(RT-MW-05) & Water Level

Route 211 Treatment System
2016 Annual Operating Report
SynTerra Corporation
January 2017
Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency (January - June 2016)
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 08/09/16 08/09/16
Pesticides (ug/L)
Aldrin < 0.016 < 0.0016
alpha-BHC 0.13 < 0.0025
alpha-Chlordane < 0.25 < 0.0025
beta-BHC 4.8 < 0.0028
p,p-DDD < 0.0410 < 0.0041
p,p-DDE < 0.041 < 0.0041
p,p-DDT 0.19 P < 0.0043
delta-BHC 4.5 < 0.0028
Dieldrin 0.21 P 0.0046 JP
Endosulfan I 0.10 < 0.0035
Endosulfan II 0.12 JP < 0.012
Endosulfan Sulfate < 0.047 < 0.0048
Endrin 0.32 < 0.0067
Endrin Aldehyde < 0.16 < 0.016
Endrin Ketone < 0.041 < 0.0041
gamma-BHC 0.076 J < 0.0016
gamma-Chlordane 0.057 < 0.0084
Heptachlor < 0.016 < 0.0016
Heptachlor Epoxide < 0.019 < 0.0019
Methoxychlor < 0.24 < 0.025
Toxaphene 22 < 0.25
Total Pesticides 32.45 0.0046
System Removal Efficiency: 99.99%
Notes:
Influent pH was 5.07 s.u.
J-estimated value
P- RPD>40%
V-RPD>100%
Only measurable concentrations are used for removal efficiency.
Permit specified removal efficiency:95%

Route 211 Treatment System
2016 Annual Operating Report
SynTerra Corporation
January 2017
Table 3
Treatment System Monitoring Results And
Treatment Removal Efficiency (July - December 2016)
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Period July - December 2016
Sample Name Influent Effluent
Date Sampled 12/15/16 12/15/16
Pesticides (ug/L)
Aldrin 0.018 < 0.0016
alpha-BHC 0.011 < 0.0024
beta-BHC 0.36 < 0.0028
gamma-BHC (Lindane) 0.0086 < 0.0016
alpha-Chlordane < 0.0025 < 0.0024
gamma-Chlordane 0.11 < 0.0057
p,p-DDD < 0.0042 < 0.0041
p,p-DDE 0.015 J < 0.0041
p,p-DDT < 0.0095 V < 0.0042
delta-BHC 0.53 < 0.0028
Dieldrin 0.017 P < 0.0043
Endosulfan I 0.012 < 0.0035
Endosulfan II < 0.013 < 0.012
Endosulfan Sulfate < 0.0049 < 0.0047
Endrin 0.082 < 0.0066
Endrin Aldehyde < 0.024 V < 0.016
Endrin Ketone < 0.0042 < 0.0041
Heptachlor < 0.0017 < 0.0016
Heptachlor Epoxide 0.014 < 0.0019
Methoxychlor < 0.036 V < 0.024
Toxaphene 5.1 < 0.24
Total pesticides 6.3 0.01
System Removal Efficiency: 99.87%
Notes:
Influent pH was not measured
J-estimated value; P- RPD>40%;V - RPD>100%
Only measurable concentrations are used for removal efficiency.
Since all effluent concentrations were ND,average detection limit of
all constituents divided by half was used for calculation.
Permit specified removal efficiency:95%

•
Route 211 Treatment System
2016 Annual Operating Report
SynTerra Corporation
January 2017
Table 4
Monitoring Well Analytical Results Summary
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Sample Name MW-1 (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)
Sample Event Annual Annual Annual
Date Sampled 12/14/16 12/14/16 12/14/2016
Pesticides (ug l.,)
Aldrin < 0.0017 < 0.0017 < 0.0016
alpha-BHC < 0.0025 < 0.0025 < 0.0025
beta-BHC < 0.0029 0.024 < 0.0028
gamma-BHC (Lindane) < 0.0017 < 0.0017 < 0.0016
alpha-Chlordane < 0.0025 0.006 J < 0.0025
gamma-Chlordane 0.027 P 0.012 J < 0.0058
p,p-DDD < 0.0042 < 0.0042 < 0.0041
p,p-DDE < 0.0042 < 0.0042 < 0.0041
p,p-DDT < 0.0044 < 0.0044 < 0.0043
delta-BHC < 0.0029 < 0.0028 < 0.0028
Dieldrin < 0.0045 < 0.0044 < 0.0044
Endosulfan I < 0.0036 < 0.0036 < 0.0035
Endosulfan II < 0.013 < 0.01 < 0.012
Endosulfan Sulfate < 0.0049 < 0.0049 < 0.0048
Endrin < 0.0068 < 0.0068 < 0.0067
Endrin Aldehyde < 0.017 < 0.02 < 0.016
Endrin Ketone < 0.0042 < 0.004 < 0.0041
Heptachlor < 0.0017 < 0.0017 0.0021 JP
Heptachlor Epoxide < 0.0019 < 0.0019 < 0.0019
Methoxychlor < 0.025 < 0.025 < 0.025
Toxaphene < 0.25 < 0.25 < 0.25
MW-1 (pH=4.91);MW-2 (pH=4.95);MW-3(pH=5.07)
J-estimated value
P-RPD>40%
V-RPD>100%

A.:=° N
beta-BHC 0.024 ugh! InMa
a-chlordane 0.006 3 ugh! i
g-chlordane 0.012 3 ugh
05-MW-01 (MW-2)
433.28 T-MW-12 (MW-1)
,* 433.95
—_,t x x-.-_,,.
j+' gamla-cholane 0.027 P ug/ _
X/
11
RT-MW-05 (MW-3) e
431.89
w
Heptachlor 0 CX)21 JP u1-/I Ui P.
tT
50 100 200 1ber4,
�� Feet e
0/2
Legend FIGURE 1
© EXTRACTION WELL 0MONITORING LOCATIONS AND
MONITORING WELL synTerra POTENTIOMETRIC�
FORMERSOURCEAREA MAP-
Source:Water levels measured December 2016,Moore County 2007 aerial, SURFICIAL AQUIFER
- and site surveys
�i SURFACE WATER This map is a product of SynTerra.Reasonable efforts have been made to ensure the
accuracy of this map.SynTerra expressly disclaims any responsibility or liability with ROUTE 211 AREA
regard to the use of this map,and promotes and recommends the independent
GROUNDWATER SURFACE CONTOUR* verification of any data contained on this map by the user ofthis map prndvrt
Created by B.Russo on 06/222016 ABERDEEN PESTICIDE DUMPS SITE
*Water elevations(ft msl)measured December 2016. plsyngenta 1053104 01 Rt 211 Downgradient1Figares12017-011Fig-01-fdonitoringl_ocahnns mxd MOORE COUNTY,NORTH CAROLINA

GROUNDWATER QUALITY MONITORING: Mail Original: DEPARTMENT Y ENVIRONMENTN, NATURAL S RESOURCES
WATER QUALITY DIVISION,GROUNDWATER SECTION
EN
COMPLIANCE REPORT FORM RALEIGH1636MAIL, NCSERVICE 27699C-16TER36 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021
Facility Name: WQ0014357
Permit Name (if different): Non Discharge UIC
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) (State) (zip) La oon X Remediation: Infiltration Gallery
Contact Person: Ted Volskay Telephone #: [phone] g
Well Location/Site Name: No. of Wells to be Sampled: ° Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number (from Permit): RT-MW-12(Mw-1)
) Other:
For Groundwater Treatment Systems y
Well Depth: 20.50 ft. Well Diameter: 2.0 in.
p Check One: ❑ Influent (98)
Screened Interval: 1070 ft. to 20.50 1t. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 11.66 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.18 ft. above land surface. Relative M.P. Elevation in ft.: 445.61
Gallons of water pumped/bailed before sampling: 4.3 Date sample collected: 12/14/2016 Date sample analyzed: 12/23/2016
Field analysis: pH 4.91 , Specific Conductance 40 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 17.6 °C, Odor none Appearance Clear Certification No. NC Certification No.521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X _(1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/1 Mn - Manganese mg/ TCL Pesticides : method # = 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 :_
Thonwt A. Mavuvt, 1/20/2017
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: WQ0014357 EXPIRATION DATE:Sept.30,2021
Non DischargeUIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) (State) (zip) La oon X Remediation: Infiltration Gallery
Contact Person: Tom Mann Telephone #: [phone] g
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): 05-MW-01(MW-2) For Groundwater Treatment Systems Other:
Well Depth: 37.52 ft. Well Diameter:4.0 in. Check One: 0 Influent (98)
Screened Interval:22.67 ft. to 37.52 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 21.12 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 3.22 ft. above land surface. Relative M.P. Elevation in ft.: 454.40
Gallons of water pumped/bailed before sampling: 12.5 Date sample collected: 12/14/2016 Date sample analyzed: 01/12/2017
Field analysis: pH 4.95 , Specific Conductance 50 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 19.7 °C, Odor None Appearance Clear Certification No. NC Certification 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/ Ca - Calcium mg/
Chloride _ mg/ Cd - Cadmium mg/
Arsenic mg/ Chromium: Total mg/
Grease and Oils mg/ Cu - Copper mg/
Phenol mg/ Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/ Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/ Mn - Manganese mg/ TCL Pesticides : method #= 8061A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true, accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
RESET Thetv+,aIKA. Mavwt. 1/20/2017
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER -
COMPLIANCE REPORT FORM RALEIGH, NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: w00014357 Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021 •
Non-Discharge UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (Zip) COUnty X
Lagoon Remediation: Infiltration Gallery
Contact Person: Tom Mann Telephone #: [phone]
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
P (from Permit)
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RI-Mw-os(Mw-3) For Groundwater Treatment Systems Other:
Well Depth: 24.57 ft. Well Diameter:2.0 in. Check One: 0 Influent (98)
Screened Interval: 1457 ft. to 24.57 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 17.7 ft. below measuring point. colloidal concentrations. •
Measuring Point (M.P.) is: 2.67 ft. above land surface. Relative M.P. Elevation in ft.: 449.59
Gallons of water pumped/bailed before sampling: 33 Date sample collected: 12/14/2016 Date sample analyzed: 12/23/2016
Field analysis: pH 5.07 , Specific Conductance 30 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. 18.5 °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N _ mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8061A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
Thovna k A. M ayt,vv 1/2 0/2 017
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

Mail Original DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH, NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021
Facility Name: W00014357
Permit Name (if different): Non Discharge UIC
Facility Address: NC Highway Route 211 NPDES
•
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) Ted Volskay (state) (z°)
Contact Person: Telephone #: [phone] Lagoon X Remediation: Infiltration Gallery
Well Location/ Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled:(from Permit) Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.0 in. Check One: 0 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 08/09/2016 Date sample analyzed: 08/17/2016
Field analysis: pH 5.44 , Specific Conductance 89 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.6 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/1
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
Thon'ta -A. Mauve, 1/20/2017
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER _
COMPLIANCE REPORT FORM RALEIGH, NC 27699-1636 Phone:[phone]
•
FACILITY INFORMATION Please Print Clearly or Type
Facility Name. WQ0014357 Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021 .
Permit Name (if different): Non DischargeUIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (S1eet) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(city) (Slate) (Zip) County X
Tom Mann 864 527-4617 Lagoon Remediation: Infiltration Gallery
Contact Person: Telephone #: ( )
Well Location/ Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p (ffom Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other: •
Well Depth: 40.51 ft. Well Diameter:6.0 in. Check One: D Influent (98)
Screened Interval:1607 ff. to 40.51 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: NA ft. below measuring point. colloidal concentrations.
Measuring Point (M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 12/15/2016 Date sample analyzed: 01/08/2016
Field analysis: pH NA , Specific Conductance NA uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. NA °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance _ uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method # = 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 , ,`"` Tho-nwu-A. Mavuv 1/20/2017
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM RAL GH SERVICE CENTER
LEIGH, NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE: Sept.30,2021 .
Permit Name (if different): Non-Discharge WQ0014357 UIC
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (State) (Zip) County x
Ted Volskay 864 527-4637 Lagoon Remediation: Infiltration Gallery
Contact Person: Telephone #: ( )
Well Location/ Site Name: Tre'''"i i ''''9e'°'°`''''''''a°P" No. of Wells to be Sampled: ' Spray Field Remediation:
(Irom Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. ID Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 08/09/2016 Date sample analyzed: 08/16/2016
Field analysis: pH 5.44 , Specific Conductance 89 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.6 °C, Odor _ none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method # = 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true, accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 ` ,a`":"'• :,` Thoncu-A. Mca.wn. 1/20/2017
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

GROUNDWATER QUALITY MONITORING: Mall Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
`0--- 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH, NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: WQ0014357 Route 211 Area PERMIT#: EXPIRATION DATE:Sept.30,2021
Non-DischargeUIC
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES
•
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) State) (Zip) County X
Contact Person: Tom Mann Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
(
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
(from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): NA For Groundwater Treatment Systems Other: -
Well Depth: ft. Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 12/15/2016 Date sample analyzed: 12/23/2016
Field analysis: pH NA , Specific Conductance NA uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. NA °C, Odor none Appearance Clear Certification No. NC Lab Certification#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method # = 8081A
. : method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true, accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 : 1, .'"„ -, Thom A. Maw, 1/20/2017
Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

eurofins
Lancaster LaboratorieE Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717.656-2300 •Fax.[phone] • www.LancasterLabs.cow
ANALYTICAL RESULTS
Prepared by: Prepared for:
Eurofins Lancaster Laboratories Environmental Synterra Corporation
2425 New Holland Pike Suite 220
Lancaster,PA 17601 148 River Street
Greenville SC 29601
Report Date: January 13,2017
Project: Rte 211 Treatment System,NC
Submittal Date: 12/16/2016
Group Number: 1745758
PO Number: 1053.04.01
State of Sample Origin: NC
Lancaster Labs
Client Sample Description (LL)#
Effluent Grab Groundwater 8750460
MW-1 (RT-MW-12)Grab Groundwater 8750461
MW-2(05-MW-01)Grab Groundwater 8750462
MW-3 (RT-TW-05)Grab Groundwater 8750463
Influent Grab Groundwater 8750464
The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory Sample
Analysis Record.
Regulatory agencies do not accredit laboratories for all methods,analytes,and matrices. Our current scopes of
accreditation can be viewed at http://www.eurofmsus.com/environment-testing/laboratories/eurofins-lancaster-
laboratories-environmental/resources/certifications/. To request copies of prior scopes of accreditation,contact
your project manager.
Electronic Copy To Synterra Corporation Attn:Ted Volskay
Respectfully Submitted,
+464..
Lyssa M Longenecker
Specialist
[phone]
Page 1 of 11

titi eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 8750460
Rt 211 Treatment System, NC LL Group # 1745758
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/15/2016 09:21 by TM Synterra Corporation
Suite 220
Submitted: 12/16/2016 10:00 148 River Street
Reported: 01/13/2017 13:49 Greenville SC 29601
211EF
CAT Dilution
Analysis Name CAS Number Method
No. y Result Detection Limit Factor
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 N.D. 0.0024 1
10589 Beta BHC 319-85-7 N.D. 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0024 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0057 1
10589 p,p-DDD 72-54-8 N.D. 0.0041 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10589 p,p-DDT 50-29-3 N.D. 0.0042 1
10589 Delta BHC 319-86-8 N.D. 0.0028 1
10589 Dieldrin 60-57-1 N.D. 0.0043 1
10589 Endosulfan I 959-98-8 N.D. 0.0035 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0047 1
10589 Endrin 72-20-8 N.D. 0.0066 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.024 1
10589 Toxaphene 8001-35-2 N.D. 0.24 1
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 163550022A 12/23/2016 07:39 Andrea L Jones 1
11120 Pesticide Waters Update SW-846 3510C 1 163550022A 12/20/2016 22:35 Karen L Beyer 1
IV Ext
Pape 2 of 11

4: eurofins
1 Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-1 (RT-MW-12) Grab Groundwater LL Sample # WW 8750461
Rt 211 Treatment System, NC LL Group # 1745758
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/14/2016 15:30 by TM Synterra Corporation
Suite 220
Submitted: 12/16/2016 10:00 148 River Street
Reported: 01/13/2017 13:49 Greenville SC 29601
211-1
CAT
No. Analysis Name CAS Number Method Dilution
Result Detection Limit Factor
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0017 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 N.D. 0.0029 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.027 P 0.0059 1
10589 p,p-DDD 72-54-8 N.D. 0.0042 1
10589 p,p-DDE 72-55-9 N.D. 0.0042 1
10589 p,p-DDT 50-29-3 N.D. 0.0044 1
10589 Delta BHC 319-86-8 N.D. 0.0029 1
10589 Dieldrin 60-57-1 N.D. 0.0045 1
10589 Endosulfan I 959-98-8 N.D. 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
10589 Endrin 72-20-8 N.D. 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0042 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 163550022A 12/23/2016 08:19 Andrea L Jones 1
11120 Pesticide Waters Update SW-846 3510C 1 163550022A 12/20/2016 22:35 Karen L Beyer 1
IV Ext
Page 3 of 11

.'. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717.656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-2 (05-MW-01) Grab Groundwater LL Sample # WW 8750462
Rt 211 Treatment System, NC LL Group # 1745758
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/14/2016 14:30 by TM Synterra Corporation
Suite 220
Submitted: 12/16/2016 10:00 148 River Street
Reported: 01/13/2017 13:49 Greenville SC 29601
211-2
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0017 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 0.024 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
10589 Alpha Chlordane 5103-71-9 0.0060 J 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.012 J 0.0059 1
10589 p,p-DDD 72-54-8 N.D. 0.0042 1
10589 p,p-DDE 72-55-9 N.D. 0.0042 1
10589 p,p-DDT 50-29-3 N.D. 0.0044 1
10589 Delta BHC 319-86-8 N.D. 0.0028 1
10589 Dieldrin 60-57-1 N.D. 0.0044 1
10589 Endosulfan I 959-98-8 N.D. 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
10589 Endrin 72-20-8 N.D. 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0042 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 163550022A 01/12/2017 06:01 Lisa A Reinert 1
11120 Pesticide Waters Update SW-846 3510C 1 163550022A 12/20/2016 22:35 Karen L Beyer 1
IV Ext
Page 4 of 11

4 eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717.656.2300 •Fax:[phone] • www.LancasterLabs.com I
Sample Description: MW-3 (RT-TW-05) Grab Groundwater LL Sample # WW 6750463
Rt 211 Treatment System, NC LL Group # 1745758
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/14/2016 16:00 by TM Synterra Corporation
Suite 220
Submitted: 12/16/2016 10:00 148 River Street
Reported: 01/13/2017 13:49 Greenville SC 29601
211-3
CAT Dilution
Analysis Name CAS Number Method
No. �' Result Detection Limit Factor
Pesticides/PCBs SW-846 8081B ug/1 ug/l
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 N.D. 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0058 1
10589 p,p-DDD 72-54-8 N.D. 0.0041 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10589 p,p-DDT 50-29-3 N.D. 0.0043 1
10589 Delta BHC 319-86-8 N.D. 0.0028 1
10589 Dieldrin 60-57-1 N.D. 0.0044 1
10589 Endosulfan I 959-98-8 N.D. 0.0035 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 N.D. 0.0067 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 0.0021 JP 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 163550022A 12/23/2016 08:45 Andrea L Jones 1
11120 Pesticide Waters Update SW-846 3510C 1 163550022A 12/20/2016 22:35 Karen L Beyer 1
IV Ext
Page 5 of 11

• •
t• eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 8750464
Rt 211 Treatment System, NC LL Group # 1745758
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/15/2016 09:20 by TM Synterra Corporation
Suite 220
Submitted: 12/16/2016 10:00 148 River Street
Reported: 01/13/2017 13:49 Greenville SC 29601
211IN
CAT Dilution
Analysis Name CAS Number Method
No. Result Detection Limit Factor
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 0.018 0.0017 1
10589 Alpha BHC 319-84-6 0.011 0.0025 1
10589 Beta BHC 319-85-7 0.36 0.014 5
10589 Gamma BHC - Lindane 58-89-9 0.0086 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.11 0.0059 1
10589 p,p-DDD 72-54-8 N.D. 0.0042 1
10589 p,p-DDE 72-55-9 0.015 J 0.0042 1
10589 p,p-DDT 50-29-3 N.D. V 0.0095 1
1058E Delta BHC 319-86-8 0.53 0.014 5
10589 Dieldrin 60-57-1 0.017 P 0.0045 1
10589 Endosulfan I 959-98-8 0.012 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
10589 Endrin 72-20-8 0.082 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. V 0.024 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0042 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 0.014 0.0019 1
10589 Methoxychlor 72-43-5 N.D. V 0.036 1
10589 Toxaphene 8001-35-2 5.1 0.25 1
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 163550022A 01/08/2017 21:32 Lisa A Reinert 5
10589 OC Pesticides in Water SW-846 8081B 1 163550022A 01/12/2017 06:14 Lisa A Reinert 1
11120 Pesticide Waters Update SW-846 3510C 1 163550022A 12/20/2016 22:35 Karen L Beyer 1
IV Ext
Pane 6 of 11

ti . eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1745758
Reported: 01/13/2017 13:49
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise specified
in the method.
All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless otherwise noted
on the Analysis Report.
Method Blank
Analysis Name Result MDL
ug/1 ug/1
Batch number: 163550022A Sample number(s) : 8750460-8750464
Aldrin N.D. 0.0016
Alpha BHC N.D. 0.0024
Beta BHC N.D. 0.0027
Gamma BHC - Lindane N.D. 0.0016
Alpha Chlordane N.D. 0.0024
Gamma Chlordane N.D. 0.0056
p,p-DDD N.D. 0.0040
p,p-DDE N.D. 0.0040
p,p-DDT N.D. 0.0042
Delta BHC N.D. 0.0027
Dieldrin N.D. 0.0042
Endosulfan I N.D. 0.0034
Endosulfan II N.D. 0.012
Endosulfan Sulfate N.D. 0.0046
Endrin N.D. 0.0065
Endrin Aldehyde N.D. 0.016
Endrin Ketone N.D. 0.0040
Heptachlor N.D. 0.0016
Heptachlor Epoxide N.D. 0.0018
Methoxychlor N.D. 0.024
Toxaphene N.D. 0.24
LCS/LCSD
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/1 ug/1 ug/1 ug/1
Batch number: 163550022A Sample number(s) : 8750460-8750464
Aldrin 0.102 0.0564 0.102 0.0863 55 85 28-119 42* 30
Alpha BHC 0.100 0.0597 0.100 0.0918 60 92 47-132 42* 30
Beta BHC 0.102 0.0603 0.102 0.0952 59 93 56-125 45* 30
Gamma BHC - Lindane 0.100 0.0601 0.100 0.0906 60 91 51-132 41* 30
Alpha Chlordane 0.102 0.0597 0.102 0.0890 59 87 53-126 39* 30
Gamma Chlordane 0.103 0.0623 0.103 0.0980 60 95 53-130 45* 30
p,p-DDD 0.198 0.128 0.198 0.191 65 97 42-148 40* 30
p,p-DDE 0.204 0.122 0.204 0.183 60 90 51-129 40* 30
p,p-DDT 0.198 0.119 0.198 0.180 60 91 40-145 41* 30
*-Outside of specification
(I)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P######is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission group.
Pape 7 of 11

%% eu roll ns
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1745758
Reported: 01/13/2017 13 :49
LCS/LCSD (continued)
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/1 ug/1 ug/1 ug/1
Delta BHC 0.102 0.0599 0.102 0.0907 59 89 49-140 41* 30
Dieldrin 0.198 0.119 0.198 0.182 60 92 54-126 42* 30
Endosulfan I 0.100 0.0565 0.100 0.0839 57 84 51-118 39* 30
Endosulfan II 0.203 0.116 0.203 0.172 57 85 54-124 39* 30
Endosulfan Sulfate 0.201 0.119 0.201 0.176 59 87 41-133 38* 30
Endrin 0.200 0.117 0.200 0.167 59 83 35-143 35* 30
Endrin Aldehyde 0.207 0.117 0.207 0.171 57 82 40-135 37* 20
Endrin Ketone 0.204 0.127 0.204 0.192 62 94 44-136 41* 30
Heptachlor 0.100 0.0568 0.100 0.0869 57 87 38-135 42* 30
Heptachlor Epoxide 0.102 0.0605 0.102 0.0916 59 90 56-132 41* 30
Methoxychlor 0.994 0.563 0.994 0.835 57 84 39-143 39* 30
Surrogate Quality Control
Surrogate recoveries which are outside of the QC window are confirmed
unless attributed to dilution or otherwise noted on the Analysis Report.
Analysis Name: OC Pesticides in Water
Batch number: 163550022A
Tetrachloro-m-xylene Decachlorobiphenyl
8750460 34 40
8750461 86 85
8750462 95 84
8750463 67 65
8750464 98 88
Blank 81 68
LCS 56 53
LCSD 81 69
Limits: 29-129 32-149
'-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
P######is indicative of a Background or Unspiked sample that is batch matrix QC and was not performed using a sample from this submission group.
Pape 8 of 11

Greenville Office Charlotte Office
148 River Street,Suite 220 10806 Reames Road, Suite A
Greenville, SC 29601 Terra Charlotte, NC 28269
1.9999 980.312.5998
Fax: [phone].421.9909 Fax: [phone]
August 6, 2018
Capes suonered0 ieuol6a8
Mr. Mike Rogers kneno.eleM
UIC Program g`OZ Q
NC Division of Water Resources
1636 Mail Service Center
HMO/0303N/O3AI30321
Raleigh, North Carolina 27699-1636
RE: 2018 Semiannual Report
RECEIVED/NCDEQ/DWR
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site- Route 211 Area AUG fl
Aberdeen, North Carolina 7 201$
Water Quality
Regional Operations Section
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2018 Semiannual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
• Analytical monitoring requirements summary (Table 1);
• Influent and effluent analytical results summary (Tables 2);
• Completed copies of NCDEQ Division of Water Quality, Groundwater Section form
GW-59 and analytical laboratory data reports (Attachments);
• Influent and effluent analytical results.
The treatment system, which operates 24 hours per day, was inspected monthly in
accordance with the permit. The treatment system has performed as designed and
experienced no unscheduled downtime during this reporting period. Influent and
effluent samples were collected on June 26, 2018. The treatment system, which includes
bag filtration and carbon adsorption, achieved a 99.98% removal efficiency which
exceeded the 95% removal efficiency specified by the permit. Approximately 300,000
gallons of groundwater was extracted and treated from January 30, 2018 to June 26,
2018. Groundwater extraction rates averaged approximately 1.42 gpm or 2,040 gpd
during the monitoring period.
www.synterracorp.com

Greenville Office Charlotte Office
148 River Street,Suite 220 10806 Reames Road,Suite A
Greenville,SC 29601 Terra Charlotte, NC 28269
Fax: 1.9999 980.312.5998
Fax: [phone] Fax: [phone]
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. One upgradient well, MW-1 (RT-MW-
12), and two sidegradient wells, MW-2 and MW-3 (05-MW-01 and RT-MW-05,
respectively), are required to be sampled annually for TCL pesticide analysis. These
wells will be sampled in the second half of 2018 and the results will be provided in the
2018 annual operating report.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section III and IV of the Site Groundwater Remediation
Permit issued October 13, 2016.
If you require additional copies of the enclosed materials or have any questions, please
contact me at(864) 527-4617.
Sincerely,
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Electronic cc:
Jim Barber-NC DWR Fayetteville Garland Hilliard-Olin
Doug Rumford-NCDEQ Michael Bogle, Esq. - WCS&R
Jon Bornholm-USEPA Ted Volskay-SynTerra
George Crouse -Syngenta
www.synterracorp.com

Table 1
Analytical Monitoring Requirements
Groundwater Extraction And Treatment System
Route 211 Area Semiannual Operating Report
Aberdeen, North Carolina
Location Parameters of Analysis Monitoring Frequency
(Permit No.WQ0014357)
Influent TCL Pesticides &pH Semiannually
(Jan. -June,July-Dec.)
Effluent TCL Pesticides&pH Semiannually
(Jan.-June,July-Dec.)
MW-1 TCL Pesticides,pH Annually
(RT-MW-12) &Water Level (July-Dec.)
MW-2 TCL Pesticides, pH Annually
(05-MW-01) &Water Level (July-Dec.)
MW-3 TCL Pesticides, pH Annually
(RT-MW-05) & Water Level (July -Dec.)

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/26/18 06/26/18
Pesticides(ug/L)
Aldrin < 0.080 < 0.0016
alpha-BHC 0.19 J < 0.0024
alpha-Chlordane 0.17 JP < 0.0024
beta-BHC 4.3 < 0.0028
p,p-DDD < 0.20 < 0.0040
p,p-DDE < 0.20 < 0.0040
p,p-DDT < 0.21 < 0.0042
delta-BHC 8.9 < 0.0027
Dieldrin < 0.21 < 0.0042
Endosulfan I < 0.17 < 0.0034
Endosulfan II < 0.60 < 0.012
Endosulfan Sulfate < 0.23 < 0.0046
Endrin < 0.32 < 0.0065
Endrin Aldehyde < 0.80 < 0.016
Endrin Ketone < 0.20 < 0.0040
gamma-BHC 0.11 J < 0.0016
gamma-Chlordane < 0.28 < 0.0056
Heptachlor < 0.080 < 0.0016
Heptachlor Epoxide 0.17 J < 0.0018
Methoxychlor < 1.2 < 0.024
Toxaphene 17.0 J < 0.24
Total Pesticides 34.17 0.0083
System Removal Efficiency: 99.98%
Notes:
Influent pH was 5.35 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Since all effluent concentrations were ND, average detection limit of
all constituents divided by half was used for calculation.

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
EXPIRATION DATE:Sept.30.2021
PERMIT#:
Facility Name: Route 211 AreaUIC
Permit Name (if different): Non-Discharge W00014357
Facility Address: NC Highway Route 211 NPDES
ts'"°"t TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(Gay) Ted Volskay (Stale) (Zip)
Contact Person: Telephone#: [phone] Lagoon X Remediation:Infiltration Gallery
Well Location/Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled:Morn Permit) Spray Held Remediation:
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other
Well Depth: 40.51 ft. Well Diameter: 6•° n. Check One: El Influent (98)
Screened Interval: 1607 ft to 40.51 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/26/2018 Date sample analyzed: 06/29/2018
Field analysis: pH 5.58 , Specific Conductance 90 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp.18.9 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K- Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method #=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
inducing the possibility of fines and imprisonment for knowing violations. Thoma A. Mann, P.E., Project Manager
Per ' uihoriz Age ame and Title-Please print or type
GW-59 L^'.--- y2.4118
Rev. 0312000 Signature o Pem+ittee(or Authorized Agent) (Date)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPWATER
MENT QUALITY
OF ENVIRONMENT, &NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL COMPLIANCE REPORT FORM RALEIGH,NC SERVICE 699 1636R Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area
PERMIT#: EXPIRATION DATE:Sept 30,2021
g
Non-Dischar e W(00014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
(si.eu TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
start Ted Volskay tswtol taus 86a)527 4637 Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone#:
Well Location/Site Name:T1Cd'1i1e'''"s'd'"haga 0 nri'°ar'Onya''ery No of Wells to be Sampled: ° Spray Field Remediation:
t1ipnf Po^""1 Rotary Distributor _ Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06/26/2018 Date sample analyzed: 06/29/2018
Field analysis: pH 5.56 , Specific Conductance 75 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.3 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/1 Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium._. mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
. method# _
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A Mann, P.E.,�]�P�ro�ject Manager
Permits 'zed Age t)Na� wv "e•Please print or type V
_ -7M-i
1
GW-59 Signature of ermittee(or thorized Agent) (Date)
Rev. 03/2000

tiff eurofins
Lancaster Laboratorie, n.. `i..,
Environmental
2426 New Holland Pike,Lancaster.PA 17601•717456-2300•Fax:[phone]•wwv.Euro5nsUS comlLanclabsEnv
ANALYSIS REPORT
Prepared by: Prepared for:
Eurofins Lancaster Laboratories Environmental Synterra Corporation
2425 New Holland Pike Suite 220
Lancaster, PA 17601 148 River Street
Greenville SC 29601
Report Date: July 09, 2018 17:30
Project: Rte 211 Treatment System, NC
Account#: 12819
Group Number: 1959742
PO Number: 1053.04.01
State of Sample Origin: NC
To view our laboratory's current scopes of accreditation please go to
http://www.eurofi nsus.com/envi ronment-testing/laboratories/eu rofi ns-lancaster-laboratories-
environmental/resources/certifications/ . Historical copies may be requested through your project
manager.
Electronic Copy To Synterra Corporation Attn: Thomas Mann
Electronic Copy To Synterra Corporation Attn: Mark McDade
Electronic Copy To Synterra Corporation Attn:Ted Volskay
Respectfully Submitted,
Lyssa M. Longenecker
Specialist
[phone]
Page 1 of 11

titi eurofins
Lancaster Laboratories,
Environmental
2425 New Holland Pike,Lancaster.PA 17601•717-066-2.100•Fax.[phone]•www.EuroOnsUScOmJLancLabaEnv
SAMPLE INFORMATION
Client Sample Description Sample Collection ELLE#
Date/Time
Effluent Grab Groundwater 06/26/2018 09:40 9679482
Carbon-1/Carbon-2 Grab Groundwater 06/26/2018 09:35 9679483
Influent Grab Groundwater 06/26/2018 09:30 9679484
The specific methodologies used in obtaining the enclosed analytical results are indicated on the Laboratory
Sample Analysis Record.
Page 2 of 11

EFFLUENT

SUBMIT FORM ON YELLOW PAPER ONLY
Mail,Qriginal DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: { '�a� to' WATER1636 IL QUALITY
SERVICE DIVISION,
ROUNDWATER SECTION
COMPLIANCE REPORT FORM '``" ` " RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Non-Discharge W00014357 UlC
Permit Name (if different): --
Facility Address: NC Highway Route 211 NPDES
(sheet) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 Moore
County
(city) 'Stahl) (ciu) _Lagoon X Remediation: Infiltration Gallery
Ted volskay
Contact Person: Telephone #: [phone]
Well Location/ Site Name: rreatmencsYs,mscharptovNiitrauungallery No. of Wells to be Sampled: ^ Spray Field Remediation:(trom PermO) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): - Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06/30/2015 Date sample analyzed: 06/20/2014
Field analysis: pH 4.75 , Specific Conductance 90 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 18.3 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium _ mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method It. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true.accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A. Mann, P.E., Project Manager
Perrnin a(or Author ed A ant)Name and Title•Please print or type
7/.5GW-59 Signal a of Permitlee(or Authorized Agent) ( ate)
Rev. 03/2000

SUBMI I FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: ,,,„, .41; toy WATER QUALITY DIVISION,GROUNDWATER SECTION
t+ rl',, 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM "; RALEIGH, NC 27699-1636 Pfione:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE,June 30,2016
Non-Discharge WQ0014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
tsireei) TYPE OF PERMITTED. OPERATION BEING MONITORED
Aberdeen NC 28315 COUnty Moore
fa` Torn Mann tsi`'r@I alp) __Lagoon __.X__Remediation: Infiltration Gallery
Contact Person: Telephone #:_�864)527-4617
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation: _
{rrom remit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): NA For Groundwater Treatment Systems Other: ___ _
Well Depth: ft. Well Diameter: in.
p - Check One: ❑ Influent
(98)
Screened Interval: _ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level:_ ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.)is: ft.above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 12/30/2015 Date sample analyzed: 01/07/2015
Field analysis: pH 4.35 , Specific Conductance 110 uMhos Laboratory Name: eurot ns(Lancaster Labs)(Pennsylvania)
Temp. 20.5 °C, Odor none Appearance Clear Certification No. NC Lab Certification#521
PARAMETERS (Samples for metals were collected unfiltered YES _.._.__.NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m Nitrate (NO3) as N mg/I Pb - Lead_. mg/I
Coliform: MF Total /100m Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen, mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/ Ca - Calcium mg/I _
Chloride mg/ Cd - Cadmium mg/I
Arsenic mg/ Chromium: Total mg/I
Grease and Oils mg/ Cu - Copper mg/I -
Phenol mg/ Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/I (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X _(1) No _(0)
Total Ammonia mg/ Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/ Mn - Manganese mg/I TCL Pesticides : method #= 8081A
: method #
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th+mas A. Mann P. ., Project Manager
Permit: e .r Author( d Ajar{ E
err'f Name and Title-Please print or type //(fila:t6i.
GW-59 V\--OV L ✓,`'`'...
Signature of Perm,tee(or Authorized Agent) (Dale)
Rev. 03/2000

. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 7951155
Rt 211 Treatment System, NC LL Group # 1573603
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/30/2015 09:07 by TM Synterra Corporation
Suite 220
Submitted: 07/01/2015 10:00 148 River Street
Reported: 07/14/2015 13:05 Greenville SC 29601
211-E
CAT Dilution
No. Analysis Name CAS NumberResult Method
na s
Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/i
00177 Aldrin 309-00-2 0.0034 J 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 0.017 0.0028 1
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 N.D. 0.0033 1
00177 Gamma Chlordane 5103-74-2 N.D. 0.0059 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 N.D. 0.0042 1
00177 p,p-DDT 50-29-3 N.D. 0.0044 1
00177 Delta BHC 319-86-8 N.D. 0.014 1
00177 Dieldrin 60-57-1 N.D. 0.0044 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 N.D. 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
00177 Endrin 72-20-8 N.D. 0.0068 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0042 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
00177 Methoxychlor 72-43-5 N.D. 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/07/2015 02:26 Lisa A Reinert 1
11118 Pesticide Screen Waters SW-846 3510C 1 151830009A 07/02/2015 19:35 Karen L Beyer 1
Ext
Page 3 of 8

. eurofins
j Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 -Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 8195135
Rt 211 Treatment System, NC LL Group # 1621136
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/30/2015 11:29 by TV Synterra Corporation
Suite 220
Submitted: 01/05/2016 10:05 148 River Street
Reported: 01/12/2016 11:39 Greenville SC 29601
211EF
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 0.048 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
10589 Alpha Chlordane 5103-71-9 0.0080 JP 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.0084 J 0.0057 1
10589 p,p-DDD 72-54-8 N.D. 0.0041 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10589 p,p-DDT 50-29-3 N.D. 0.0043 1
10589 Delta BHC 319-86-8 0.030 P 0.0028 1
10589 Dieldrin 60-57-1 0.0087 J 0.0043 1
10589 Endosulfan I 959-98-8 N.D. 0.0035 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 N.D. 0.0066 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
General Sample Comments
State of North Carolina Lab Certification No. 521
The temperature of the temperature blank bottle(s) upon receipt at the
lab was 6.7 C using a digital thermometer. The sample bottles were then
measured using an IR thermometer and were recorded at 7.2-7.8 C.
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 160060027A 01/07/2016 19:56 Lisa A Reinert 1
11120 Pesticide Waters Update SW-846 3510C 1 160060027A 01/06/2016 01:00 Sherry L Morrow 1
IV Ext
Page 3 of 12

Rogers, Michael
From: Slusser, Thomas
Sent: Monday, July 27, 2015 8:31 AM
To: Rogers, Michael
Subject: FW: Route 211 Site 2015 Semiannual Treatment System Report
Attachments: 2015 Treatment System Semiannual Report- Complete.pdf
Happy Monday, buddy!
Thomas Slusser, L.G.
Pre-Regulatory Landfill Unit I NCDENR Division of Waste Management
ph#: 919-707-8331 I [e-mail]
Mailing Address: 1646 Mail Service Center I Raleigh I NC 27699-1646
Physical Address: 217 West Jones Street I Raleigh I NC 27603
http://www.wastenotnc.org/web/wm/sf/ihs/ihsoldlf
t-1 N:IIJ Cr 17'PSJ)c)11c1t'11CC'ri7.'111ci f'[)Itl tJii acjc/1c'SS mar be sillwC-1 to/Vic'.A,?-J1 ii ,iina Public AC2Y'Iti.: L./t "alri 22;..1 Jl.1171,
From: [e-mail] [mailto:[e-mail]]
Sent: Friday, July 24, 2015 1:04 PM
To: Slusser, Thomas
Cc: [e-mail]; Rumford, Doug; [e-mail]; [e-mail]; [e-mail]
Subject: Route 211 Site 2015 Semiannual Treatment System Report
Thomas,
Good afternoon. Please find attached the 2015 Semiannual Treatment System Report for the Route 211 Site. If you have
any comments or questions, please contact me. Thanks.
Regards,
Tom
synTerra
Scars inz;and 1;rors ing iith:,! tow;
Thomas A. Mann, PE
SynTerra Corporation
148 River Street, Suite 220
Greenville, SC 29601
864-527-4617
[e-mail]
This e-mail might contain privileged or confidential information. If the e-mail was not intended for you, please:
(1) delete the e-mail and any attachments
(2) destroy any copies that might have been made
(3) do not use, copy, or distribute the contents in any form
(4) notify me by return e-mail or by calling 864-527-4617
No privilege is waived by inadvertent transmission. Thank you.
1

synTerra
July 24, 2015
Mr. Thomas Slusser
NCDENR, Division of Water Quality
Aquifer Protection, Underground Injection Control Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2015 Semiannual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site -Route 211 Area
Aberdeen, North Carolina
Dear Mr. Slusser:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2015 Semiannual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
L' Analytical monitoring requirements (Table 1);
C Monitoring events analytical results summary table(Table 2);
0 Influent and effluent analytical results; and
Lj Completed copies of NCDENR Division of Water Quality, Groundwater Section form GW-
59 and analytical laboratory data reports.
The treatment system, which operates 24 hours per day, was inspected monthly in
accordance with the permit. The treatment system has performed as designed and
experienced no unscheduled downtime during this reporting period. Influent and
effluent samples were collected on June 30, 2015. The treatment system, which includes
bag filtration and carbon adsorption, achieved a 99.79% removal efficiency which
exceeded the 95% removal efficiency specified by the permit. Approximately 599,473
gallons of groundwater was extracted and treated from January 28, 2015 to June 29,
INNOVATE 148 River Street,Suite 220 Greenville,SC 29601 [phone] Fax[phone] www.synterracorp.com

2015 Semiannual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
July 24,2015
Page Two
2015. Groundwater extraction rates averaged approximately 2.74 gpm or 3,944 gpd
during the monitoring period.
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. One upgradient well, MW-1 (RT-MW-
12), and two sidegradient wells, MW-2 and MW-3 (05-MW-01 and RT-MW-05,
respectively), are required to be sampled annually for TCL pesticide analysis. These
wells will be sampled in the second half of 2015 and the results will be provided in the
2015 annual operating report.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
SynTerra Corporation
Thomas A. Mann, P.E.
Attachments:
GW-59 Forms
Analytical reports
Electronic cc:
Jon Bornholm—USEPA James Cashwell—Olin
Doug Rumford —NCDENR Michael Bogle, Esq. - WCS&R
George Crouse-Syngenta Ted Volskay-SynTerra
INNOVATE 148 River Street, Suite 220 Greenville,SC 29601 [phone] Fax[phone] www.synterracorp.com

Table 1
Analytical Monitoring Requirements
Groundwater Extraction And Treatment System
Route 211 Area Semiannual Operating Report
Aberdeen, North Carolina
LocationParameters of Analysis Monitoring Frequency
(Permit No. WQ0014357)
Semiannually
Influent TCL Pesticides &pH
(Jan. -June,July-Dec.)
Effluent TCL Pesticides & pH Semiannually
(Jan. -June,July-Dec.)
TCL Pesticides, pH Annually
&Water Level (July-Dec.)
TCL Pesticides, pH Annually
1 1 &Water Level (July -Dec.)
TCL Pesticides, pH Annually
1 &Water Level (July -Dec.)

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/30/15 06/30/15
Pesticides(ug/L)
Aldrin 0.28 0.0034 J
alpha-BHC 0.047 < 0.0025
alpha-Chlordane 0.074 P < 0.0033
beta-BHC 2.8 0.017
p,p-DDD < 0.0042 < 0.0042
p,p-DDE 0.025 < 0.0042
p,p-DDT < 0.024 V < 0.0044
delta-BHC 6.0 < 0.014
Dieldrin 0.055 P < 0.0044
Endosulfan I 0.019 < 0.0036
Endosulfan II 0.096 < 0.013
Endosulfan Sulfate < 0.0048 < 0.0049
Endrin < 0.027 V < 0.0068
Endrin Aldehyde 0.094 P < 0.017
Endrin Ketone < 0.012 V < 0.0042
gamma-BHC 0.043 < 0.0017
gamma-Chlordane 0.08 < 0.0059
Heptachlor < 0.0017 < 0.0017
Heptachlor Epoxide < 0.030 V < 0.0019
Methoxychlor 0.20 P < 0.025
Toxaphene < 0.25 < 0.25
Total Pesticides 9.81 0.020
System Removal Efficiency: 99.79%
Notes:
Influent pH was 5.07 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable influent and effluent concentrations used.
Permit specified removal efficiency:95%

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT
ON, SECTIAL OURCES
10: WATER QUALITY DIVISION,GROUNDWATER SECTION
,i t;,. 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC27699-1636 Phone:(_919)733-3221
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area
PERMIT#:: EXPIRATION DATE:June 30,2016
g W00014357
Non-Discharge UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Is:M^,I TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 Moore
Piz) (Stoic) izqu County X
Contact Person;.Ted Volskay Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/ Site Name: RT-Pw-o1 to treatment system No. of Wells to be Sampled: a Spray Field Remediation:
p ttram rrrmit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.0 in. Check One: 0 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft, ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point (M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/30/2015 Date sample analyzed: 06/20/2014
Field analysis: pH 5-07 , Specific Conductance 90 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 18 0 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD , mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia __ mg/1 Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
. : method #
t certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A. Mann, P.E., Project Manager
Perrnitt e(or Authorix Agerr)Name and Title-Please print or type
7/6746 15-
GW-59 11......---
Signature of Permitte.(or Ault'or ed Agent) t (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: MaitOriginal DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
r t0: WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM it - 1636 MAIL SERVICE CENTER
RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
EXPIRATION DATE:June 30,2016
PERMIT#:
Facility Name: Route 211 Area g
Non-Dischar e W00014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen '"`4Q'' NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(cdY) (s,aic) (flu) County X
Contact Person: Ted vo,skay Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/ Site Name: r"'atrren`zY'` arr;na-a.«°rust'"°Ga"Y No. of Wells to be Sampled: 4 Spray Field Remediation:
p thorn Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: 0 Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE; Values should reflect dissolved and
Depth to Water Level: ft. below measuring point, colloidal concentrations.
Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06/30/2015 Date sample analyzed: 06/20/2014
Field analysis: pH_4•75 — , Specific Conductance 90 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 18.3 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N _ mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method #_
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWI(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A, Mann, P.E., Project Manager
Permitt a(or Autho ed Arent)
�Na_me and Title-Please print or type
. 1‘-t ..__,......__, VI
G W 59 Signal e of Permittee(or Authorized Agent) ( ate)
Rev. 03/2000

•
= eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 •717456.2300•Fax:[phone] •www.LancasterLabs.eom
ANALYTICAL RESULTS
Prepared by: Prepared for:
Eurofins Lancaster Laboratories Environmental Synterra Corporation
2425 New Holland Pike Suite 220
Lancaster,PA 17601 148 River Street
Greenville SC 29601
July 14,2015
Project: Rte 211 Treatment System,NC
Submittal Date: 07/01/2015
Group Number: 1573603
PO Number: 1053.04.01
State of Sample Origin: NC
Client Sample Description Lancaster Labs(LL)#
Influent Grab Groundwater 7951154
Effluent Grab Groundwater 7951155
The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.
Regulatory agencies do not accredit laboratories for all methods,analytes,and matrices. Our scopes of
accreditation can be viewed at http://www.eurofinsus.com/environment-testing/laboratories/eurofins-
lancaster-laboratories-environmental/resources/certifications/.
ELECTRONIC Synterra Corporation Attn: Ted Volskay
COPY TO
Respectfully Submitted.
2a-VAL JttilArrl/
Melanie uszynski
Specialist
[phone]
Page 1 of 8

%- eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 7951154
Rt 211 Treatment System, NC LL Group # 1573603
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/30/2015 08:58 by TM Synterra Corporation
Suite 220
Submitted: 07/01/2015 10:00 148 River Street
Reported: 07/14/2015 13:05 Greenville SC 29601
211-I
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 0.28 0.0083 5
00177 Alpha BHC 319-84-6 0.047 0.0025 1
00177 Beta BHC 319-85-7 2.8 0.28 100
00177 Gamma BHC - Lindane 58-89-9 0.043 0.0017 1
00177 Alpha Chlordane 5103-71-9 0.074 P 0.0025 1
00177 Gamma Chlordane 5103-74-2 0.076 0.0058 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 0.025 0.0042 1
00177 p,p-DDT 50-29-3 N.D. V 0.024 1
00177 Delta BHC 319-86-8 6.0 0.28 100
00177 Dieldrin 60-57-1 0.055 P 0.0044 1
00177 Endosulfan I 959-98-8 0.019 0.0036 1
00177 Endosulfan II 33213-65-9 0.096 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
00177 Endrin 72-20-8 N.D. V 0.027 1
00177 Endrin Aldehyde 7421-93-4 0.094 P 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. V 0.012 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. V 0.030 1
00177 Methoxychlor 72-43-5 0.20 P 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
The % difference for the calibration verification standard is outside the
+/- 15% criteria for the analyte(s) listed below. Since the average of the
% difference values meets the criteria, the results are reported.
This applies to the following analyte(s) :
methoxychlor
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/07/2015 02:13 Lisa A Reinert 1
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/11/2015 00:58 Lisa A Reinert 5
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/11/2015 01:23 Lisa A Reinert 100
11118 Pesticide Screen Waters SW-846 3510C 1 151830009A 07/02/2015 19:35 Karen L Beyer 1
Ext
Page 2 of 8

.
t
•
•
. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 7951155
Rt 211 Treatment System, NC LL Group # 1573603
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/30/2015 09:07 by TM Synterra Corporation
Suite 220
Submitted: 07/01/2015 10:00 148 River Street
Reported: 07/14/2015 13:05 Greenville SC 29601
211-E
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 0.0034 J 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 0.017 0.0028 1
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 N.D. 0.0033 1
00177 Gamma Chlordane 5103-74-2 N.D. 0.0059 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 N.D. 0.0042 1
00177 p,p-DDT 50-29-3 N.D. 0.0044 1
00177 Delta BHC 319-86-8 N.D. 0.014 1
00177 Dieldrin 60-57-1 N.D. 0.0044 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 N.D. 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
00177 Endrin 72-20-8 N.D. 0.0068 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0042 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
00177 Methoxychlor 72-43-5 N.D. 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/07/2015 02:26 Lisa A Reinert 1
11118 Pesticide Screen Waters SW-846 3510C 1 151830009A 07/02/2015 19:35 Karen L Beyer
Ext
Page 3 of 8

. 1 ,
,e. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1573603
Reported: 07/14/2015 13:05
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.
All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.
Laboratory Compliance Quality Control
Blank Blank Report LCS LCSD LCS/LCSD RPD
Analysis Name Result MDL Units %REC %REC Limits RPD Max
Batch number: 151830009A Sample number(s) : 7951154-7951155
Aldrin N.D. 0.0016 ug/1 61 61 24-141 0 30
Alpha BHC N.D. 0.0024 ug/1 75 75 55-141 0 30
Beta BHC N.D. 0.0027 ug/1 77 76 57-141 1 30
Gamma BHC - Lindane N.D. 0.0016 ug/1 77 76 58-140 2 30
Alpha Chlordane N.D. 0.0024 ug/1 72 72 54-135 0 30
Gamma Chlordane N.D. 0.0056 ug/1 74 74 53-138 0 30
p,p-DDD N.D. 0.0040 ug/1 86 85 52-144 0 30
p,p-DDE N.D. 0.0040 ug/1 78 77 49-144 2 30
p,p-DDT N.D. 0.0042 ug/1 84 86 51-142 3 30
Delta BHC N.D. 0.0027 ug/1 80 77 55-141 3 30
Dieldrin N.D. 0.0042 ug/1 76 75 58-133 1 30
Endosulfan I N.D. 0.0034 ug/1 63 64 50-126 2 30
Endosulfan II N.D. 0.012 ug/1 73 74 55-132 1 30
Endosulfan Sulfate N.D. 0.0046 ug/1 65 76 54-139 16 30
Endrin N.D. 0.0065 ug/1 74 76 35-143 2 30
Endrin Aldehyde N.D. 0.016 ug/1 70 73 50-131 4 20
Endrin Ketone N.D. 0.0040 ug/1 75 77 50-143 3 30
Heptachlor N.D. 0.0016 ug/1 76 75 38-135 1 30
Heptachlor Epoxide N.D. 0.0018 ug/1 73 75 56-140 3 30
Methoxychlor N.D. 0.024 ug/1 83 86 49-148 4 30
Toxaphene N.D. 0.24 ug/1
Surrogate Quality Control
Surrogate recoveries which are outside of the QC window are confirmed
unless attributed to dilution or otherwise noted on the Analysis Report.
Analysis Name: OC Pesticides in Water
Batch number: 151830009A
Tetrachloro-m-xylene Decachlorobiphenyl
7951154 58 67
7951155 65 80
Blank 99 107
LCS 64 73
LCSD 64 68
Limits: 39-138 32-149
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
Page 4 of 8

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syfferra
January 20, 2015
Mr. Thomas Slusser
NCDENR, Division of Water Quality
Aquifer Protection, Underground Injection Control Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2014 Annual Report
Groundwater Remediation Pe*nit No. WQ0014357
Aberdeen Pesticide Dumps Site - Route 211 Area
Aberdeen, North Carolina
Dear Mr. Slusser:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2014 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report indudes:
• Analytical monitoring requirements summary (Table 1);
• Influent and effluent analytical results summary (Tables 2 and 3);
• Monitoring well analytical results summary (Table 4);
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratory data reports (Attachments).
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (June 25, 2014 and December 16, 2014) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2014 and experienced minimal downtime. The system
operates 24 hours per day and a total of 987,713 gallons of groundwater were treated
during the reporting period (January 27, 2014 to December 16, 2014). Groundwater
extraction rates averaged approximately 3,058 gpd during the monitoring period. The
treatment system removal efficiency was greater than 95% (see Tables 2 and 3).
INNOVATE 148 River Street,Suite 220 Greenville, SC 29601 [phone] Fax[phone] www.synterracorp.corn

2014 Annual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
January 2015
Page Two
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), were sampled on December 16, 2014 and analyzed for SW-
846 8081A pesticides. The water table was below the pump intake on the one
upgradient well, MW-1 (RT-MW-12), so a representative groundwater sample could not
be collected. Analytical results are summarized in Table 4. Copies of the treatment
system influent and effluent analytical reports and the MW-2 and MW-3 analytical
report are induded with the completed GW-59 forms provided as attachments.
Information provided in this submittal is intended to fulfill the annual reporting
requirements described in Section IV, items 1 - 4 and 13, of the Site Groundwater
Remediation Permit issued January 25, 2007.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
jam �
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Attachments:
GW-59 Forms
Analytical reports
Electronic cc:
Jon Bornholm-USEPA James Cashwell-Olin
Doug Rumford-NCDENR Michael Bogle, Esq. -WCS&R
George Crouse-Syngenta Ted Volskay-SynTerra
INNOVATE 148 River Street, Suite 220 Greenville, SC 29601 [phone] Fax[phone] www.synterracorp.com

Route 211 Treatment System
2014 Annual Operating Report
SynTerra Corporation
January 2015
Table 1
Analytical Monitoring Requirements
Groundwater Extraction and Treatment System
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Frequency
(Permit No.
Location Parameters of Analysis WQ0014357)
Influent TCL Pesticides &pH Semi-annually
(RT-PW-01) (Jan.-June,July- Dec.)
Effluent TCL Pesticides & pH Semi-annually
Gan.-June,July- Dec.)
MW-1 TCL Pesticides, pH Annually
(RT-MW-12) &Water Level
MW-2 TCL Pesticides, pH Annually
(05-MW-01) & Water Level
MW-3 TCL Pesticides, pH Annually
(RT-MW-05) &Water Level

Route 211 Treatment System
2014 Annual Operating Report
SynTerra Corporation
January 2015
Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency (January - June 2014)
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event Approximate Treatment
Sample Name Influent Effluent Removal Efficiency
Date Sampled 06/18/14 06/18/14 [(Inf-Eff)/Infl x 100
Pesticides(ug/L)
Aldrin 0.25 < 0.0017 * 99.7%
alpha-BHC 0.11 < 0.0025 * 98.86%
alpha-Chlordane 0.20 < 0.0025 * 99.4%
beta-BHC 3.2 0.049 98.47%
p,p-DDD 0.055 < 0.0042 * 96.2%
p,p-DDE 0.043 < 0.0042 * 95.1%
p,p-DDT < 0.039 < 0.0044 * NA
delta-BHC 7.1 0.066 99.07%
Dieldrin 0.12 0.0088 J 92.7%
Endosulfan I 0.026 < 0.0036 * 93.1%
Endosulfan II < 0.01 < 0.013 * NA
Endosulfan Sulfate < 0.0470 < 0.0049 * NA
Endrin 0.083 < 0.0068 * 95.9%
Endrin Aldehyde < 0.050 < 0.017 * NA
1 Endrin Ketone 0.011 J < 0.0042 * 80.9%
gamma-BHC < 0.002 < 0.0017 * NA
gamma-Chlordane 0.16 < 0.0059 * 98.2%
Heptachlor < 0.0016 < 0.0017 * NA
Heptachlor Epoxide < 0.050 < 0.0023 * NA
Methoxychlor < 0.14 < 0.025 * NA
Toxaphene < 0.24 < 0.25 * NA
Total Pesticides 11.65 0.30 * 97.4%
System Removal Efficiency: 97.4%
Notes:
Influent pH was 5.25 s.u.
J-estimated value
NA-Not Applicable(Influent concentration below detection limit)
(*) Efficiency calculations assume 1/2 detection limit.
Permit specified removal efficiency:95%

Route 211 Treatment System
2014 Annual Operating Report
SynTerra Corporation
January 2015
Table 3
Treatment System Monitoring Results And
Treatment Removal Efficiency (July - December 2014)
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Period July - December 2014 Approximate Treatment
Sample Name Influent Effluent Removal Efficiency
Date Sampled 12/16/14 12/16/14 [(Inf-Eff)/Inf] x 100(14°1e 1)
Pesticides (ug/L)
Aldrin < 0.0017 0.0021 J NA
alpha-BHC 0.037 < 0.0025 96.62%
beta-BHC 2.0 0.012 99.70%
gamma-BHC(Lindane) 0.026 < 0.0017 96.73%
alpha-Chlordane 0.14 0.0053 J 98.11%
gamma-Chlordane 0.084 < 0.0059 96.49%
p,p-DDD < 0.12 < 0.0042 NA
p,p-DDE < 0.0043 < 0.0042 NA
p,p-DDT 0.065 P, < 0.0044 96.62%
delta-BHC 0.99 0.0098 99.51%
Dieldrin 0.070 P < 0.0045 96.79%
Endosulfan I 0.042 < 0.0036 95.71%
Endosulfan II 0.16 < 0.013 95.94%
Endosulfan Sulfate < 0.069 < 0.0049 NA
Endrin 0.12 < 0.0068 97.17%
Endrin Aldehyde < 0.017 < 0.017 NA
Endrin Ketone 0.033 < 0.0042 93.64%
Heptachlor < 0.055 < 0.0017 NA
Heptachlor Epoxide < 0.13 < 0.0019 NA
Methoxychlor 0.12 P < 0.025 89.58%
Toxaphene 4.4 < 0.25 97.16%
System Removal Efficiency: 96.41%
Notes:
Note 1: Effluent is 1/2 detection limit if nondetect.
Influent pH was 5.54 s.u.
J-estimated value
NA-Not Applicable(Influent concentration below method detection limit)
Permit specified removal efficiency:95%

Route 211 Treatment System
2014 Annual Operating Report
SynTerra Corporation
January 2015
Table 4
Monitoring Well Analytical Results Summary
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Sample Name MW-i (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)
Sample Event Annual Annual Annual
Date Sampled 12/16/14 12/16/14 12/16/2014
Pesticides (ug/L)
Aldrin < 0.0017 < 0.0017
alpha-BHC < 0.0025 < 0.0025
beta-BHC 0.25 < 0.0028
gamma-BHC(Lindane) < 0.0017 < 0.0017
alpha-Chlordane 0.021 < 0.0025
gamma-Chlordane 0.012 J < 0.0058
p,p-DDD < 0.030 < 0.0041
p,p-DDE < 0.0041 < 0.0041
p,p-DDT Note 1 < 0.0043 < 0.0043
delta-BHC 0.0066 J < 0.0028
Dieldrin 0.021 < 0.0044
Endosulfan I < 0.0036 < 0.0036
Endosulfan II 0.026 < 0.012
Endosulfan Sulfate < 0.0048 < 0.0048
Endrin 0.012 JP < 0.0067
Endrin Aldehyde < 0.017 < 0.017
Endrin Ketone < 0.0041 < 0.0041
Heptachlor < 0.0017 < 0.0017
Heptachlor Epoxide 0.004 JP < 0.0019
Methoxychlor 0.025 JP < 0.025
Toxaphene 0.7: J < 0.25
Note 1: A representative groundwater sample could not be collected because water
table was below the sampling pump intake.
MW-2 (05-MW-01) pH=5.25
MW-3 (RT-MW-05) pH=5.40

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ATTACHMENTS
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MONITORING WELLS
(MW-1, MW-2, MW-3)
•
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~ SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES •
GROUNDWATER QUALITY MONITORING: ;:4 ':�-x't! to. WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM :•- ::1'; . 1636 MAIL SERVICE CENTER
RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Non-Discharge WQ0014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen ($1v1) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (Siaie) (Zip) COUnty X
Contact Person: Tom Mann Telephone #: [phone] Lagoon Remediation:Infiltration Gallery
Veil Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
IT(O"'P""'"1 Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): 05-MW-01(MW-2) For Groundwater Treatment Systems Other:
Well Depth: 37.52 ft. Well Diameter:4.0 in. Check One: 0 Influent (98)
Screened Interval:22.67 ft. to 37.52 ft. NOTE: Values should reflect dissolved and
2s.a7 El Effluent (99)
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 3.22 ft. above land surface. Relative M.P. Elevation in ft.: 454.40
Gallons of water pumped/bailed before sampling: 22.0 Date sample collected; 12/16/2014 Date sample analyzed: 12/30/2014
Field analysis: pH 5.25 , Specific Conductance 130 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.3 °C, Odor None Appearance Clear Certification No. NC Certification 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/ Other(Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/ Ca - Calcium mg/
Chloride mg/ Cd - Cadmium mg/
Arsenic mg/ Chromium: Total mg/
Grease and Oils mg/ Cu - Copper mg/
Phenol mg/ Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/ (Specify test and method#.Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/ Mg Magnesium mg/ VOC (example) method #= Not Applicable
TKN as N mg/ Mn - Manganese mg/ TCL Pesticides method#= 8081A
: method#=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. 7h mas A. Mann, P.E., Project Manager
Perini e(or Aulh �
ent)Name and Tine-Please print or type
GW-59 `INA. - `A 1�01 ..
Signature of Permiltee(or Authorized Agent) (Date)
Rev. 03/2000

• SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail OrIgInal DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
DIVISION,
�r t" '' -' `." . 1636 MAIILUALITY SERVICE CENTER GROUNDWATER SECTION
COMPLIANCE REPORT FORM RALEIGH.NC276ss-1636 Phone:[phone]
FACILJTY INFORMATION Please Print Clearly or Type
PERMIT#: EXPIRATION DATE:June 30,2016
Facility Name: Route 211 Area Non-Discharge WQ0014357 UIC
, Permit Name (if different). NPDES
Facility Address: NC Highway Route 211
• Aberdeen (strew) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) (Slate) (Zip) County
[phone] Lagoon X Remediation: Infiltration Gallery
Contact Person: Tom Mann Telephone#:
Well Location/Site Name: No. of Wells to be Sampled: Spray Field Remediation:
p dranPermin Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Rr-Mw-os(Mw3) For Groundwater Treatment Systems Other:
Well Depth: 24.57 ft. Well Diameter:2.0 in. Check One: ❑ Influent (98)
Screened Interval: 14.5' ft, to 24.57 ft. ❑ Effluent (99) NOTE; Values should reflect dissolved and
Depth to Water Level: 22.99 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.67 ft. above land surface. Relative M.P. Elevation in ft.: 449.59
Gallons of water pumped/bailed before sampling: 0.80 Date sample collected: 12/16/2014 Date sample analyzed: 12/23/2014
Field analysis: pH 5.40 , Specific Conductance 70 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 17.2 °C, Odor None Appearance Clear Certification No. NC Certification No.521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/ Ca - Calcium mg/
Chloride mg/ Cd - Cadmium mg/
Arsenic mg/ Chromium: Total mg/
Grease and Oils mg/ Cu - Copper mg/
Phenol mg/ Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/ Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/ Mn - Manganese mg/ TCL Pesticides : method#= 8081A
: method#_
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. omas A. Mann, P.E., Project Manager
Permit ee or Autho ed A fin)Name and Title-Please print or type
/I 2-12,0/5-
G W 59 Signa ure of P mittee(or Authorized Agent) r (Date)
Rev. 03/2000

: eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-2 (05-MW-01) Grab Groundwater LL Sample # WW 7717228
Rt 211 Treatment System, NC LL Group # 1526684
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/16/2014 15:15 by TV Synterra Corporation
Suite 220
Submitted: 12/18/2014 08:00 148 River Street
Reported: 01/07/2015 14:50 Greenville SC 29601
M2---
As Received
CAT As Received Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 N.D. 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 0.25 0.014 5
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 0.021 0.0025 1
00177 Gamma Chlordane 5103-74-2 0.012 J 0.0058 1
00177 p,p-DDD 72-54-8 N.D. 0.030 1
00177 p,p-DDE 72-55-9 N.D. 0.0041 1
00177 p,p-DDT 50-29-3 N.D. 0.0043 1
00177 Delta BHC 319-86-8 0.0066 J 0.0028 1
00177 Dieldrin 60-57-1 0.021 0.0044 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 0.026 0.012 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
00177 Endrin 72-20-8 0.012 JP 0.0067 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0041 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 0.0043 JP 0.0019 1
00177 Methoxychlor 72-43-5 0.025 JP 0.025 1
00177 Toxaphene 8001-35-2 0.78 J 0.25 1
Target analytes were detected in the method blank associated
with the samples as noted on the QC Summary. The following
corrective action was taken:
The sample was re-extracted outside the method required holding
time and the QC is compliant. All results are reported from the
first trial. Similar results were obtained in both trials.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/30/2014 06:03 Jamie L Brillhart 1
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/30/2014 06:17 Jamie L Brillhart 5
1 11118 Pesticide Screen Waters SW-846 3510C 1 143540015A 12/22/2014 16:00 Kelli M Barto 1
Ext
Pape_4 of 10

.:: eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-3 (RT-MW-05) Grab Groundwater LL Sample # WW 7717229
Rt 211 Treatment System, NC LL Group # 1526684
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/16/2014 16:00 by TV Synterra Corporation
Suite 220
Submitted: 12/18/2014 08:00 148 River Street
Reported: 01/07/2015 14:50 Greenville SC 29601
M3---
As Received
CAT As Received Dilution
Analysis Name CAS Number Method
No. y Result Detection Limit Factor
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 N.D. 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 N.D. 0.0028 1
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
00177 Gamma Chlordane 5103-74-2 N.D. 0.0058 1
00177 p,p-DDD 72-54-8 N.D. 0.0041 1
00177 p,p-DDE 72-55-9 N.D. 0.0041 1
00177 p,p-DDT 50-29-3 N.D. 0.0043 1
00177 Delta BHC 319-86-8 N.D. 0.0028 1
00177 Dieldrin 60-57-1 N.D. 0.0044 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 N.D. 0.012 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
00177 Endrin 72-20-8 N.D. 0.0067 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0041 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
00177 Methoxychlor 72-43-5 N.D. 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
The recovery for the sample surrogate(s) is outside the QC
acceptance limits as noted on the QC Summary. The following
corrective action was taken:
The sample was re-extracted outside the method required holding
time and the QC is compliant. All results are reported from the
first trial. Similar results were obtained in both trials.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/23/2014 21:03 Jamie L Brillhart 1
11118 Pesticide Screen Waters SW-846 3510C 1 143540015A 12/22/2014 16:00 Kelli M Barto 1
Ext
Page 5 of 10

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INFLUENT
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SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original WATDEPER
MENT QUALITY
OF ENVIRONMENTN, LS CTION RESOURCES
•
da 'i.'•.~:fi0: WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM 'ir# �" '' RAL6EGH,NC276991636 SERVICE CENTER Phone:[phone]
FACILITY INFORMATION. Please Print Clearly or Type -
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Non-Discharge W00014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen (s"`P'1 NC 28315Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(City) ($lace) (Zip) County X
Contact Person: Ted Volskay Telephone#: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled: a Spray Field Remediation:
(Iron permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.0 in. Check One: x❑ Influent (98)
Screened Interval: 16.07 ft. to 40.51 ft, ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/18/2014 Date sample analyzed: 06/20/2014
Field analysis: pH 5.25 , Specific Conductance NA uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 17.9 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/ Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m Phosphorus: Total as P mg/ Zn -Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/ Al - Aluminum mg/ Other(Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/ Ca - Calcium mg/
Chloride mg/ Cd - Cadmium mg/
Arsenic mg/ Chromium: Total mg/
Grease and Oils mg/ Cu - Copper mg/
Phenol mg/ Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/ Hg - Mercury mg/ (Specify test and method#.Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No _(0)
Total Ammonia mg/ Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/ Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Perm tee(or Autho zed ent)Name and Title-Please print or type
GW-59 1
Signature of Pe miitee(or Authorized Agent) 7 (Dale)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original AT RTMENT OF ENVIRONMENTN, SATURAL SECTION
•
-`. to: WATER QUALITY DIVISION,GROUNDWATER SECTION
'` 1 `:r 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Facility Name: Non-Discharge WQ0014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
Aberdeen (spec) NC 28315 TYPE OF PERMITTED OPERATION BEING MONITORED
County Moore
tcoY) (slam) pi La(boon X Remediation:Infiltration Gallery
Contact Person: Tom MannTelephone #: [phone] g
Spray Field Remediation:
Well Location/Site Name: No. of Wells to be Sampled'p (tr.,Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter:6.0 in. Check One: ® Influent (98) `
Screened Interval:1607 ft. to 40.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: NA ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 12/16/2014 Date sample analyzed: 12/30/2014
Field analysis: pH 5.54 , Specific Conductance 140 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 20.2 °C, Odor None Appearance Clear Certification No. NC Certification No.521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn -Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total . mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#.Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method#= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method #_
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th mas A. Mann, P.E., Project Manager
Permit a or Authori ed Act)Name and Title-Please print or type l I
A 2/2.0
G W 59 Signe ure of P rmitt a(or Authorized Agent) (Date)
Rev. 03/2000

•
ti; eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 7504293
Rt 211 Treatment System, NC LL Group # 1483033
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/18/2014 13:35 by TV Synterra Corporation
Suite 220
Submitted: 06/19/2014 08:10 148 River Street
Reported: 06/25/2014 12:44 Greenville SC 29601
211IN
As Received
CAT As Received Method Dilution
No. Analysis Name CAS Number Result Detection Limit Factor
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 0.25 0.0081 5
00177 Alpha BHC 319-84-6 0.11 0.0024 1
00177 Beta BHC 319-85-7 3.2 0.14 50
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
00177 Alpha Chlordane 5103-71-9 N.D. 0.16 1
00177 Gamma Chlordane 5103-74-2 0.16 0.028 5
00177 p,p-DDD 72-54-8 0.055 0.0040 1
00177 p,p-DDE 72-55-9 0.043 0.0040 1
00177 p,p-DDT 50-29-3 N.D. 0.039 1
00177 Delta BHC 319-86-8 7.1 0.14 50
00177 Dieldrin 60-57-1 0.12 0.0043 1
00177 Endosulfan I 959-98-8 0.026 0.0035 1
00177 Endosulfan II 33213-65-9 N.D. 0.012 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0047 1
00177 Endrin 72-20-8 0.083 0.0065 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.050 1
00177 Endrin Ketone 53494-70-5 0.011 J 0.0040 1
00177 Heptachlor 76-44-8 N.D. 0.0016 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.050 1
00177 Methoxychlor 72-43-5 N.D. 0.14 1
00177 Toxaphene 8001-35-2 N.D. 0.24 1
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
LaboratorySampleAnalysis Anal sis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 141700010A 06/20/2014 10:47 Lisa A Reinert 1
00177 OC Pesticides in Water SW-846 8081A 1 141700010A 06/24/2014 01:27 Lisa A Reinert 5
00177 OC Pesticides in Water SW-846 8081A 1 141700010A 06/24/2014 01:52 Lisa A Reinert 50
11118 Pesticide Screen Waters SW-846 3510C 1 141700010A 06/19/2014 17:30 Seth A Farrier 1
Ext
Page 3 of 7

s eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 7717226
Rt 211 Treatment System, NC LL Group # 1526684
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/16/2014 13:30 by TV Synterra Corporation
Suite 220
Submitted: 12/18/2014 08:00 148 River Street
Reported: 01/07/2015 14:50 Greenville SC 29601
INFT-
As Received
CAT As Received Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 N.D. 0.0017 1
00177 Alpha BHC 319-84-6 0.037 0.0026 1
00177 Beta BHC 319-85-7 2.0 0.058 20
00177 Gamma BHC - Lindane 58-89-9 0.026 0.0017 1
00177 Alpha Chlordane 5103-71-9 0.14 0.0026 1
00177 Gamma Chlordane 5103-74-2 0.084 0.0060 1
00177 p,p-DDD 72-54-8 N.D. 0.12 1
00177 p,p-DDE 72-55-9 N.D. 0.0043 1
00177 p,p-DDT 50-29-3 0.065 P 0.0044 1
00177 Delta BHC 319-86-8 0.99 0.058 20
00177 Dieldrin 60-57-1 0.070 P 0.0045 1
00177 Endosulfan I 959-98-8 0.042 0.0037 1
00177 Endosulfan II 33213-65-9 0.16 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.069 1
00177 Endrin 72-20-8 0.12 0.0069 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 0.033 0.0043 1
00177 Heptachlor 76-44-8 N.D. 0.055 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.13 1
00177 Methoxychlor 72-43-5 0.12 P 0.026 1
00177 Toxaphene 8001-35-2 4.4 0.26 1
Reporting limits were raised due to interference from the sample matrix.
P - Concentration difference between the primary and confirmation column >40%.
The lower result is reported.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/30/2014 05:08 Jamie L Brillhart 1
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/30/2014 22:13 Jamie L Brillhart 20
11118 Pesticide Screen Waters SW-846 3510C 1 143540015A 12/22/2014 16:00 Kelli M Barto 1
Ext
Page 2 of 10

•
•
EFFLUENT
•
. , •. •

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail9rngtna! DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES '
+�° ` `i:.t�. WATER 1636 MAIILUALITY DIVISION,SERVICE CENTER GROUNDWATER SECTION
COMPLIANCE REPORT FORM . RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT#: EXPIRATION DATE:June 30,2016
Facility Name: Route 211 Area UIC
Permit Name (if different): Non-Discharge W00014357
Facility Address: NC Highway Route 211 NPDES
Aberdeen (Street) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
Contact Person: Ted Volskay Telephone#: [phone] Lagoon
(City) (Stale) (Zip) County X
Remediation:Infiltration Gallery
Well Location/Site Name: Treatment syst discharge t°infiltration gallery No. of Wells to be Sampled: " Spray Field Remediation:
(irom 6crmlt) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE; Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06118)2014 Date sample analyzed: 06/20/2014
Field analysis: pH 5.41 , Specific Conductance NA uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 18.5 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other(Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method #
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
P nie i{�arre(or Authors d A t)Name and Title-Please print or type
G W 59 Signature of Permittee(or Authorized Agent) t ate)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
M
GROUNDWATER QUALITY MONITORING: 71IOriginal DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES '
' _+to: 1636 MAIILUSERVICE CENTER GROUNDWATER SECTION
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type -
EXPIRATION DATE:June 30,2016
PERMIT#:
Facility Name: Route 211 AreaUIC
Permit Name (if different): Non-Discharge WQ0014357
NPDES
NC Highway Route 211
Facility Address: TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen Sveep NC 28315 Moore
(CM (State) (Zip) County X
Contact Person: Tom Mann Telephone#: [phone] Lagoon Remediation:Infiltration Gallery
Spray Field Remediation:
Well Location/Site Name: No. of Wells to be Sampled:p (from Perm't) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): NA For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. El Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 12/16/2014 Date sample analyzed: 12/23/2014
Field analysis: pH 5.74 , Specific Conductance 160 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.7 °C,Odor none Appearance Clear Certification No. NC Lab Certification#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note: Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium - mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#.Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method if= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method#= 8081A
: method#=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Tho as A. Mann, P.E., Project Manager
Permits or Authorizeden N me and Title-Please print or type
G W 59 Si nature of Permittee(or Authorized A ent V017-01(
(Date)
9 9 )
Rev. 03/2000

tie: eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 7504292
Rt 211 Treatment System, NC LL Group # 1483033
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/18/2014 13:30 by TV Synterra Corporation
Suite 220
Submitted: 06/19/2014 08:10 148 River Street
Reported: 06/25/2014 12:44 Greenville SC 29601
211EF
As Received
CAT As Received Dilution
Analysis Name CAS Number Method
No. y Result Detection Limit Factor
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 N.D. 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 0.049 0.0029 1
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
00177 Gamma Chlordane 5103-74-2 N.D. 0.0059 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 N.D. 0.0042 1
00177 p,p-DDT 50-29-3 N.D. 0.0044 1
00177 Delta BHC 319-86-8 0.066 0.0029 1
00177 Dieldrin 60-57-1 0.0088 J 0.0045 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 N.D. 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
00177 Endrin 72-20-8 N.D. 0.0068 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0042 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.0023 1
00177 Methoxychlor 72-43-5 N.D. 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 141700010A 06/20/2014 10:35 Lisa A Reinert 1
11118 Pesticide Screen Waters SW-846 3510C 1 141700010A 06/19/2014 17:30 Seth A Farrier 1
Ext
Page 2 of 7

.: eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 7717230
Rt 211 Treatment System, NC LL Group # 1526684
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/16/2014 13:40 by TV Synterra Corporation
Suite 220
Submitted: 12/18/2014 08:00 148 River Street
Reported: 01/07/2015 14:50 Greenville SC 29601
EFFT-
As Received
CAT As Received Dilution
Analysis Name CAS Number Method
No. Result Detection Limit Factor '..
Pesticides/PCBs SW-846 8O81A ug/1 ug/1
00177 Aldrin 309-00-2 0.0021 J 0.0017 1
00177 Alpha BHC 319-84-6 N.D. 0.0025 1
00177 Beta BHC 319-85-7 0.012 0.0029 1
00177 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
00177 Alpha Chlordane 5103-71-9 0.0053 J 0.0025 1
00177 Gamma Chlordane 5103-74-2 N.D. 0.0059 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 N.D. 0.0042 1
00177 p,p-DDT 50-29-3 N.D. 0.0044 1
00177 Delta BHC 319-86-8 0.0098 0.0029 1
00177 Dieldrin 60-57-1 N.D. 0.0045 1
00177 Endosulfan I 959-98-8 N.D. 0.0036 1
00177 Endosulfan II 33213-65-9 N.D. 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
00177 Endrin 72-20-8 N.D. 0.0068 1
00177 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. 0.0042 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
00177 Methoxychlor 72-43-5 N.D. 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
Target analytes were detected in the method blank associated
with the samples as noted on the QC Summary. The following
corrective action was taken:
The sample was re-extracted outside the method required holding
time and the QC is compliant. All results are reported from the
first trial. Similar results were obtained in both trials.
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 143540015A 12/23/2014 21:17 Jamie L Brillhart 1
11118 Pesticide Screen Waters SW-846 3510C 1 143540015A 12/22/2014 16:00 Kelli M Barto 1
Ext
Page 6 of 10

tiff eurofins
Lancaster Laboratorit Environmental Analysis ysis Report/�i
2425 New NOItan4 Pike.Lancaster,PA 1/601•2114156-2500•Faa:1174554 S•mom Eurafina0S.co1LancLabaEnv
Sample Description: Effluent Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9679482
ELLE Group#: 1959742
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 06/27/2018 09:30
Collection Date/Time: 06/26/2018 09:40
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides SW-846 8081 B ug/I ug/I
10589 Aldrin 309-00-2 N.D. D1 0.0016 1
10589 Alpha BHC 319-84-6 N.D. D2 0.0024 1
10589 Beta BHC 319-85-7 N.D. VD2 0.0028 1
10589 Gamma BHC-Lindane 58-89-9 N.D. D2 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. D2 0.0024 1
10589 Gamma Chlordane 5103-74-2 N.D. D1 0.0056 1
10589 p,p-DDD 72-54-8 N.D. D1 0.0040 1
10589 p,p-DDE 72-55-9 N.D. D2 0.0040 1
10589 p,p-DDT 50-29-3 N.D. D1 0.0042 1
10589 Delta BHC 319-86-8 N.D. D2 0.0027 1
10589 Dieldrin 60-57-1 N.D. D1 0.0042 1
10589 Endosulfan I 959-98-8 N.D. D2 0.0034 1
10589 Endosulfan II 33213-65-9 N.D. D1 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. D2 0.0046 1
10589 Endrin 72-20-8 N.D. D2 0.0065 1
10589 Endrin Aldehyde 7421-93-4 N.D. D1 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. D2 0.0040 1
10589 Heptachlor 76-44-8 N.D. D2 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. D1 0.0018 1
10589 Methoxychlor 72-43-5 N.D. D1 0.024 1
10589 Toxaphene 8001-35-2 N.D. D1 0.24 1
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081 B 1 181790012A 07/06/2018 09:43 Lisa A Reinert 1
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 181790012A 06/29/2018 01:00 Sherry L Morrow 1
Page 3 of 11

%.: eurofins
Lancaster Laboratorie Analysis Report
Environmental
2425 New Moils.M Pike.Lancaster.PA 12501.217456-2300.Fax:71/456i166.ww.EuronnsUS comfLancLabsEnv
Sample Description: Carbon-1/Carbon-2 Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9679483
ELLE Group#: 1959742
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 06/27/2018 09:30
Collection Date/Time: 06/26/2018 09:35
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides SW-846 8081 B ug/I ug/I
10589 Aldrin 309-00-2 0.41 D1 0.033 20
10589 Alpha BHC 319-84-6 0.11 JD1 0.049 20
10589 Beta BHC 319-85-7 2.6 D1 0.056 20
10589 Gamma BHC-Lindane 58-89-9 0.070 JD1 0.033 20
10589 Alpha Chlordane 5103-71-9 0.12 JPD2 0.049 20
10589 Gamma Chlordane 5103-74-2 0.16 JD2 0.11 20
10589 p,p-DDD 72-54-8 N.D. D1 0.082 20
10589 p,p-DDE 72-55-9 N.D. D1 0.082 20
10589 p,p-DDT 50-29-3 N.D. D2 0.085 20
10589 Delta BHC 319-86-8 5.1 D1 0.14 50
10589 Dieldrin 60-57-1 0.11 JPD1 0.087 20
10589 Endosulfan I 959-98-8 N.D. D2 0.070 20
10589 Endosulfan II 33213-65-9 N.D. D2 0.24 20
10589 Endosulfan Sulfate 1031-07-8 N.D. D1 0.095 20
10589 Endrin 72-20-8 N.D. D2 0.13 20
10589 Endrin Aldehyde 7421-93-4 N.D. D1 0.33 20
' 10589 Endrin Ketone 53494-70-5 N.D. D2 0.082 20
10589 Heptachlor 76-44-8 N.D. D2 0.033 20
10589 Heptachlor Epoxide 1024-57-3 0.14 JD2 0.038 20
10589 Methoxychlor 72-43-5 N.D. D1 0.49 20
10589 Toxaphene 8001-35-2 12 JD2 4.9 20
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081 B 1 181790012A 07/06/2018 08:24 Lisa A Reinert 20
10589 OC Pesticides in Water SW-846 8081B 1 181790012A 07/06/2018 08:40 Lisa A Reinert 50
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 181790012A 06/29/2018 01:00 Sherry L Morrow 1
Page 4 of 11

%% eurofins
Lancaster Labor<
Environmental Analysis Report
2425 New No6aM Pike.Lancaster,PA 17601.217.654.2300.Fax,2124561166.wawa EurofnaUS coMLswCLebaEnv
Sample Description: Influent Grab Groundwater Synterra Corporation
Rt 211 Treatment System, NC ELLE Sample#: WW 9679484
ELLE Group#: 1959742
Project Name: Rte 211 Treatment System, NC Matrix: Groundwater
Submittal Date/Time: 06/27/2018 09:30
Collection Date/Time: 06/26/2018 09:30
CAT Method Dilution
No. Analysis Name CAS Number Result Detection Limit Factor
Pesticides SW-846 8081 B ug/l ugn
10589 Aldrin 309-00-2 N.D. D1 0.080 50
10589 Alpha BHC 319-84-6 0.19 JD1 0.12 50
10589 Beta BHC 319-85-7 4.3 D1 0.14 50
10589 Gamma BHC-Lindane 58-89-9 0.11 JD1 0.080 50
10589 Alpha Chlordane 5103-71-9 0.17 JPD2 0.12 50
10589 Gamma Chlordane 5103-74-2 N.D. D1 0.28 50
10589 p,p-DDD 72-54-8 N.D. D2 0.20 50
10589 p,p-DDE 72-55-9 N.D. D1 0.20 50
10589 p,p-DDT 50-29-3 N.D. D2 0.21 50
10589 Delta BHC 319-86-8 8.9 D1 0.27 100
10589 Dieldrin 60-57-1 N.D. D1 0.21 50
10589 Endosulfan I 959-98-8 N.D. D2 0.17 50
10589 Endosulfan II 33213-65-9 N.D. D2 0.60 50
10589 Endosulfan Sulfate 1031-07-8 N.D. D1 0.23 50
10589 Endrin 72-20-8 N.D. D1 0.32 50
10589 Endrin Aldehyde 7421-93-4 N.D. D1 0.80 50
10589 Endrin Ketone 53494-70-5 N.D. D2 0.20 50
10589 Heptachlor 76-44-8 N.D. D2 0.080 50
10589 Heptachlor Epoxide 1024-57-3 0.17 JD2 0.092 50
10589 Methoxychlor 72-43-5 N.D. D1 1.2 50
10589 Toxaphene 8001-35-2 17 JD2 12 50
Sample Comments
State of North Carolina Lab Certification No.521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 181790012A 07/06/2018 08:56 Lisa A Reinert 50
10589 OC Pesticides in Water SW-846 8081B 1 181790012A 07/06/2018 09:11 Lisa A Reinert 100
11120 Pesticide Waters Update IV Ext SW-846 3510C 1 181790012A 06/29/2018 01:00 Sherry L Morrow 1
Page 5 of 11

tiff eurofins
Lancaster Laboratorie . A
Environmental nalysis Report
2425 Hew I4 II.0 Pihe,Lancaster.PA 17601•217456-2300•Pac 717456E766•www.EurofnsUS.conaancLab,Env
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1959742
Reported: 07/09/2018 17:30
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these situations,to demonstrate precision and accuracy at a
batch level,a LCS/LCSD was performed,unless otherwise specified in the method.
All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless otherwise noted on the Analysis Report.
Method Blank
Analysis Name Result MDL
ug/I ug/I
Batch number 181790012A Sample number(s):9679482-9679484
Aldrin N.D. 0.0016
Alpha BHC N.D. 0.0024
Beta BHC N.D. 0.0027
Gamma BHC-Lindane N.D. 0.0016
Alpha Chlordane N.D. 0.0024
Gamma Chlordane N.D. 0.0056
p,p-DDD N.D. 0.0040
p,p-DDE N.D. 0.0040
p,p-DDT N.D. 0.0042
Delta BHC N.D. 0.0027
Dieldrin N.D. 0.0042
Endosulfan I N.D. 0.0034
Endosulfan II N.D. 0.012
Endosulfan Sulfate N.D. 0.0046
Endrin N.D. 0.0065
Endrin Aldehyde N.D. 0.016
Endrin Ketone N.D. 0.0040
Heptachlor N.D. 0.0016
Heptachlor Epoxide N.D. 0.0018
Methoxychlor N.D. 0.024
Toxaphene N.D. 0.24
LCS/LCSD
An
alysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCSILCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/I ug/I ug/I ug/I
Batch number:1 81 790 01 2A Sample numbers:9679482-9679484
P
Aldrin 0.100 0.0847 0.100 0.0868 85 87 28-119 2 30
Alpha BHC 0.102 0.0942 0.102 0.0982 92 96 47-132 4 30
Beta BHC 0.100 0.0879 0.100 0.0932 88 93 56-125 6 30
Gamma BHC-Lindane 0.102 0.0924 0.102 0.0954 91 94 51-132 3 30
Alpha Chlordane 0.100 0.0946 0.100 0.0994 95 99 53-126 5 30
Gamma Chlordane 0.100 0.129 0.100 0.0999 129 100 53-130 25 30
p,p-DDD 0.204 0.198 0.204 0.212 97 104 42-148 7 30
p,p-DDE 0.200 0.181 0.200 0.195 90 98 51-129 8 30
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
Page 6 of 11

%% eurofins
Lancaster Laboratori,' Analysis Report
Environmental
2425 New MOAnd Pike,Lancaster,PA 17601•111456.2300•Fate 711456.6166•weenEurofinSUS conelalclabsEnr
Quality Control Summary
Client Name: Synterra Corporation Group Number: 1959742
Reported: 07/09/2018 17:30
LCS/LCSD (continued)
Analysis Name LCS Spike LCS LCSD Spike LCSD LCS LCSD LCS/LCSD RPD RPD
Added Conc Added Conc %REC %REC Limits Max
ug/I ug/I ug/I ug/I
p,p-DDT 0.204 0.204 0.204 0.217 100 106 40-145 6 30
Delta BHC 0.100 0.0899 0.100 0.0956 90 96 49-140 6 30
Dieldrin 0.204 0.194 0.204 0.202 95 99 54-126 4 30
Endosulfan I 0.102 0.0854 0.102 0.0906 84 89 40-138 6 30
Endosulfan II 0.200 0.178 0.200 0.185 89 93 54-124 4 30
Endosulfan Sulfate 0.202 0.186 0.202 0.204 92 101 41-133 9 30
Endrin 0.202 0.194 0.202 0.206 96 102 35-143 6 30
Endrin Aldehyde 0.202 0.179 0.202 0.187 89 93 40-135 4 20
Endrin Ketone 0.200 0.199 0.200 0.210 99 105 44-136 6 30
Heptachlor 0.102 0.0890 0.102 0.0924 87 91 38-135 4 30
Heptachlor Epoxide 0.100 0.0939 0.100 0.0985 94 98 56-132 5 30
Methoxychlor 1.02 1.12 1.02 1.20 110 117 39-143 6 30
Surrogate Quality Control
Surrogate recoveries which are outside of the QC window are confirmed unless
attributed to dilution or otherwise noted on the Analysis Report.
Analysis Name:OC Pesticides in Water
Batch number: 181790012A
Tetrachloro-m-xylene-D1 Decachlorobiphenyl-D1 Tetrachloro-m-xylene-D2 Decachlorobiphenyl-D2
9679482 64 48 53 40
9679483 92 97 64 82
9679484 95 71 60 64
Blank 76 82 67 73
LCS 80 85 70 77
LCSD 79 92 71 81
Limits: 29-129 32-149 29-129 32-149
*-Outside of specification
(1)The result for one or both determinations was less than five times the LOQ.
(2)The unspiked result was more than four times the spike added.
Page 7 of 11

Environmental Analysis Request/Chain of Custody -
y a
�!e u rofi n s ., For Eurofins Lancaster
(Labora or' s Environmental use only c 1 ��
~• Lancaster Laboratories Acct.# 12619 Group# \�( ` I—N ple#_C�•C�' ? [c 2- -I COC 3
Environmental Sam
Client Information Matrix Analysis Requested For Lab Use Only
Client: Acct.#: Preservation Codes FSC: )) ]�-�
s ❑ `i ❑ SCR# _tr/ 3(J
Project Na a/#: PWSID#: N -C ,,a) n L Preservation Codes
P o
H=HCI T=Thiosulfate
Project Manager:, P.O.#: ❑ 0 U) '` Sy y N=HNO3 t3=NaOH
T;�,� 1 / I S/ , .- U is, S=H2SO4 O=Other
Sampler: vr: �c Quote#: E. ❑ E _ Remarks
ter.._......
t E a� cn e r
Slate where samples w For Compliance: )));
N.
Yes No 0 d0 z �p ` st
y. �
Collected °- CI * ��
Sample Identification 13 E o '�° « 0 4'ti
r Date Time 0 0 0 3 O 1— -- ,
('.v / (.:,,y_ •- I f C i l4io.', ".2.. 4-12di8-C>�l ,�5 i K
Turnaround_,Time(TAT)Requested please circle) Rell q hed by Date Time Received bye ,i Date Time
tandard Rush �✓/ ,��S f fj /l U �5/� �/'/ d C'r 47'
(Rush TAT is su tact to laboratory approval and surcharge.) ellnqulshed y/ r ,. Date Time ecelved by Date Time
f d
Date results are needed: Relinquished by ate Time Received by Date Time
E-mail address: Relinquished by ate Time Received by Date Time
Data Package Options(circle if required)
Type I (EPA Level 3 Relinquished by Date Time Received by�� ,, �% Date IPP
Type VI(Raw Data Only) ,/!///,72--, ,„17/i
EquivalenUnon-CLP) t�/
Type III(Reduced non-CLP) NJ DKQP TX TRRP-13 EDD Required? ���Ye No Relinquis;he by Commercial Carrier:
If yes,format: UPS FedEx Other
'
NYSDEC Category A or B MA MCP CT RCP Site Specific QC(MS/MSD/Dup)? Yes Node Temperature upon receipt °C
(If yes,indicate QC sample and submit triplicate sample ume.)
Eurofins Lancaster Laboratories Environmental,LLC•2425 New Holland Pike,Lancaster,PA 17601 •717-656-2300
The white copy should accompany samples to Eurofins Lancaster LLaeborattories Environmental.The yellow copy should be retained by the client. 7044 0216

Doc Log ID: 220204
, ,w. eurafins Sample Administration
Lancaster Lahoiatories Receipt Documentation Log IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
i Environmental Group Number(s):
Client: SynTerra Corp.
I497L(Z
Delivery and Receipt Information
Delivery Method: UPS Arrival Timestamp: 06/27/2018 9:30
Number of Packages: 1 Number of Projects: 1
State/Province of Origin: NC
Arrival Condition Summary
Shipping Container Sealed: Yes Sample IDs on COC match Containers: Yes
Custody Seal Present: Yes Sample Date/Times match COC: Yes
Custody Seal Intact: Yes VOA Vial Headspace z 6mm: N/A
Samples Chilled: Yes Total Trip Blank Qty: 0
Paperwork Enclosed: Yes Air Quality Samples Present: No
Samples Intact: Yes
Missing Samples: No
Extra Samples: No
Discrepancy in Container Qty on COC: No
Unpacked by Nicole Reiff(25684) at 09:48 on 06/27/2018
Samples Chilled Details
Thermometer Types: DT =Digital(Temp. Bottle) IF?=Infrared (Surface Temp) All Temperatures in°C.
Cooler# Thermometer ID Corrected Temp Therm,Tyoe Ice Type Ice Present? Ice Container Flevated Temp?
1 DT146 0.8 DT Wet Y Loose N
2425 New Holland Pike T 717-656-2300
Page 1 of 1 Lancaster, PA 17605-2425 F 717-656-2681
www.LancasterLabs.com
Page 9 of 11

eurofins
Lancaster Laboratories Explanation of Symbols and Abbreviations
Environmental
The following defines common symbols and abbreviations used in reporting technical data:
BMQL Below Minimum Quantitation Level mL milliliter(s)
C degrees Celsius MPN Most Probable Number
cfu colony forming units N.D. non-detect
CP Units cobalt-chloroplatinate units ng nanogram(s)
F degrees Fahrenheit NTU nephelometric turbidity units
g gram(s) pg/L picogram/liter
IU International Units RL Reporting Limit
kg kilogram(s) TNTC Too Numerous To Count
L liter(s) pg microgram(s)
lb. pound(s) pL microliter(s)
m3 cubic meter(s) umhos/cm micromhos/cm
meq milliequivalents MCL Maximum Contamination Limit
mg milligram(s)
< less than
> greater than
ppm parts per million-One ppm is equivalent to one milligram per kilogram (mg/kg)or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter(mg/I), because one liter of water has a weight
very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported on an
as-received basis.
Analytical test results meet all requirements of the associated regulatory program(i.e.,NELAC(TNI), DoD,and ISO 17025)unless
otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the
collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved,the test results will be
meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held
responsible for sample integrity, however, unless sampling has been performed by a member of our staff.
This report shall not be reproduced except in full,without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR Part 136 Table II as"analyze immediately"are not performed within
15 minutes.
WARRANTY AND LIMITS OF LIABILITY-In accepting analytical work,we warrant the accuracy of test results for the sample as submitted.
THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR
IMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR
PARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES
ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL, CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT
LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS OF(A)THE NEGLIGENCE(EITHER SOLE OR
CONCURRENT)OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND(B)WHETHER EUROFINS LANCASTER
LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by
Eurofins Lancaster Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and
Eurofins Lancaster Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by
client.
Page610 01 11

tiff eurofins
Lancaster Laborator Data Qualifiers
Environmental
Qualifier Definition
C Result confirmed by reanalysis
D1 Indicates for dual column analyses that the result is reported from column 1
D2 Indicates for dual column analyses that the result is reported from column 2
E Concentration exceeds the calibration range
K1 Initial Calibration Blank is above the QC limit and the sample result is ND
K2 Continuing Calibration Blank is above the QC limit and the sample result is ND
K3 Initial Calibration Verification is above the QC limit and the sample result is ND
K4 Continuing Calibration Verification is above the QC limit and the sample result is ND
J(or G, I,X) Estimated value>=the Method Detection Limit(MDL or DL)and<the Limit of Quantitation(LOQ or RL)
P Concentration difference between the primary and confirmation column>40%. The lower result is reported.
U Analyte was not detected at the value indicated
✓ Concentration difference between the primary and confirmation column>100%. The reporting limit is raised
due to this disparity and evident interference.
W The dissolved oxygen uptake for the unseeded blank is greater than 0.20 mg/L.
Z Laboratory Defined-see analysis report
Additional Organic and Inorganic CLP qualifiers may be used with Form 1 reports as defined by the CLP methods.
Qualifiers specific to Dioxin/Furans and PCB Congeners are detailed on the individual Analysis Report.
Page 11 of 11

RECEIVEDINCDEQIDWR
syne T rra AUG 242016
Water Quality Regional
August 18, 2016 Operations Section
Mr. Mike Rogers
NCDENR, Division of Water Quality
Aquifer Protection, Underground Injection Control Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2016 Semiannual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
Aberdeen, North Carolina
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2016 Semiannual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
Analytical monitoring requirements(Table 1);
0 Monitoring events analytical results summary table(Table 2);
Completed copies of NCDENR Division of Water Quality,Groundwater Section form GW-
59 and analytical laboratory data reports; and
0 Influent and effluent analytical results.
The treatment system, which operates 24 hours per day, was inspected monthly in
accordance with the permit. The treatment system has performed as designed and
experienced no unscheduled downtime during this reporting period. Influent and
effluent samples were collected on June 27 (73.7%) and resampled on August 4 (93.8%)
due to lower than expected removal efficiency. Carbon was replaced with new virgin
carbon in all three carbon vessels on August 8, 2016 and the system was restarted. The
treatment system, which includes bag filtration and carbon adsorption, achieved a
99.99% removal efficiency on August 9, 2016 which exceeded the 95% removal
INNOVATE 148 River Street,Suite 220 Greenville,SC 29601 [phone] Fax[phone] www.synterracorp.com

2016 Semiannual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
August 18,2016
Page Two
efficiency specified by the permit. Approximately 520,515 gallons of groundwater was
extracted and treated from January 28, 2016 to June 27, 2016. Groundwater extraction
rates averaged approximately 2.41 gpm or 3,470 gpd during the monitoring period.
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. One upgradient well, MW-1 (RT-MW-
12), and two sidegradient wells, MW-2 and MW-3 (05-MW-01 and RT-MW-05,
respectively), are required to be sampled annually for TCL pesticide analysis. These
wells will be sampled in the second half of 2016 and the results will be provided in the
2016 annual operating report.
If you require additional copies of the enclosed materials or have any questions, please
contact me at(864) 527-4617.
Sincerely,
SynTerra Corporation
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Attachments:
GW-59 Forms
Analytical reports
Electronic cc:
Jon Bornholm-USEPA Garland Hilliard-Olin
Doug Rumford-NCDENR Michael Bogle, Esq. -WCS&R
George Crouse-Syngenta Ted Volskay-SynTerra
INNOVATE 148 River Street, Suite 220 Greenville, SC 29601 [phone] Fax[phone] www.synterracorp.com

Table 1
Analytical Monitoring Requirements
Groundwater Extraction And Treatment System
Route 211 Area Semiannual Operating Report
Aberdeen, North Carolina
Location Parameters of Analysis Monitoring Frequency
(Permit No. WQ0014357)
Influent TCL Pesticides&pH Semiannually
(Jan. -June,July-Dec.)
Effluent TCL Pesticides&pH Semiannually
(Jan. -June,July-Dec.)
MW-1 TCL Pesticides, pH Annually
(RT-MW-12) &Water Level (July-Dec.)
MW-2 TCL Pesticides,pH Annually
(05-MW-01) &Water Level (July-Dec.)
MW-3 TCL Pesticides,pH Annually
(RT-MW-05) &Water Level (July-Dec.)

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 08/09/16 08/09/16
Pesticides(ug/L)
Aldrin < 0.016 < 0.0016
alpha-BHC 0.13 < 0.0025
alpha-Chlordane < 0.25 < 0.0025
beta-BHC 4.8 < 0.0028
p,p-DDD < 0.0410 < 0.0041
p,p-DDE < 0.041 < 0.0041
p,p-DDT 0.19 P < 0.0043
delta-BHC 4.5 < 0.0028
Dieldrin 0.21 P 0.0046 JP
Endosulfan I 0.10 < 0.0035
Endosulfan II 0.12 JP < 0.012
Endosulfan Sulfate < 0.047 < 0.0048
Endrin 0.32 < 0.0067
Endrin Aldehyde < 0.16 < 0.016
Endrin Ketone < 0.041 < 0.0041
gamma-BHC 0.076 J < 0.0016
gamma-Chlordane 0.057 < 0.0084
Heptachlor < 0.016 < 0.0016
Heptachlor Epoxide < 0.019 < 0.0019
Methoxychlor < 0.24 < 0.025
Toxaphene 22 < 0.25
Total Pesticides 32.45 0.0046
System Removal Efficiency: 99.99%
Notes:
Influent pH was 5.44 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable influent and effluent concentrations used.
Permit specified removal efficiency:95%

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 08/04/16 08/04/16
Pesticides(ug/L)
Aldrin < 0.0082 < 0.0016
alpha-BHC 0.13 0.0045 JP
alpha-Chlordane 0.25 P 0.035
beta-BHC 5.8 0.16
p,p-DDD < 0.020 < 0.0180
p,p-DDE 0.078 JP < 0.0041
p,p-DDT 0.17 P < 0.017 P
delta-BHC 4.6 0.13 P
Dieldrin 0.20 P 0.027
Endosulfan I 0.095 0.007 J
Endosulfan II 0.40 0.028
Endosulfan Sulfate < 0.0240 < 0.0048
Endrin 0.30 0.025
Endrin Aldehyde < 0.082 < 0.016
Endrin Ketone < 0.079 J < 0.0041
gamma-BHC 0.095 < 0.0026 V
gamma-Chlordane 0.20 0.220 P
Heptachlor < 0.0082 < 0.0016
Heptachlor Epoxide < 0.0094 0.0069 JP
Methoxychlor 0.30 JP < 0.025
Toxaphene 22 1.5
Total Pesticides 34.70 2.16
System Removal Efficiency: 93.78%
Notes:
Influent pH was 5.37 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable influent and effluent concentrations used.
Permit specified removal efficiency:95%

Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Event
Sample Name Influent Effluent
Date Sampled 06/27/16 06/27/16
Pesticides(ug/L)
Aldrin 0.17 < 0.0017
alpha-BHC 0.055 0.0098
alpha-Chlordane < 0.003 < 0.0025
beta-BHC 3.1 0.45
p,p-DDD < 0.0041 < 0.0042
p,p-DDE 0.018 < 0.0042
p,p-DDT < 0.037 V < 0.007 V
delta-BHC 1.9 0.30
Dieldrin 0.11 P 0.058
Endosulfan I 0.037 0.013
Endosulfan II < 0.012 0.066
Endosulfan Sulfate < 0.0048 < 0.0048
Endrin < 0.0067 0.031 P
Endrin Aldehyde 0.053 V < 0.017
Endrin Ketone < 0.0041 0.0098 J
gamma-BHC 0.048 0.0075 J
gamma-Chlordane 0.13 P 0.061
Heptachlor < 0.0017 < 0.0017
Heptachlor Epoxide 0.090 P 0.035 P
Methoxychlor 0.20 V < 0.025
Toxaphene 15 J 4.4
Total Pesticides 20.66 5.44
System Removal Efficiency: 73.67%
Notes:
Influent pH was 5.16 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable influent and effluent concentrations used.
Permit specified removal efficiency:95%

r
SUBMI I FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016 •
Permit Name (if different): Non Discharge WQ0014357 UIC
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) (Slate) (Zip) LagoonLagoon X Remediation: Infiltration Gallery
Ted Volskay Person: Telephone #: (864)
Well Location/Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled: a Spray Field Remediation:
p (from Permtt) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.° in. Check One: C3 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 08/09/2016 Date sample analyzed: 08/17/2016
Field analysis: pH 5.44 , Specific Conductance 89 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.6 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/1
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method#= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
-
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT#: EXPIRATION DATE:June 30,2016
Facility Name: Route 211 Area UIC
Permit Name (if different): •
Non-Discharge W00014357
Highway Route 211 NC Hi •
Facility Address: 9 Y NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 Moore
(Gry) (Slate) (Zip) County X
Contact Person: Ted Volskay Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
Well Location/Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled: 4 Spray Field Remediation:
P (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.° in. Check One: 0 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 08/04/2016 Date sample analyzed: 08/12/2016
Field analysis: pH 5.37 , Specific Conductance 84 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 25.9 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Originalo: WATDEPER
QUALITMENT Y
OF ENVIRONMENT GROUNDWATER
L OURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type .
FacilityName:
Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Non-Discharge WQ0014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211 •
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) Ted Volskay (State) (Zip)
Contact Person: [phone] Lagoon X Remediation: Infiltration Gallery
Telephone #:
Well Location/ Site Name: RT-PW-01 to treatment system No. of Wells to be Sampled: a Spray Field Remediation:
p (tram Perm t) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other:
Well Depth: 40.51 ft. Well Diameter: 6.0 in. Check One: 0 Influent (98)
Screened Interval: 1607 ft. to 40.51 ft, 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.45 ft. above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/27/2016 Date sample analyzed: 07/08/2016
Field analysis: pH 5.16 , Specific Conductance 91 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.1 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method#= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
G W 59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mall Originalo: WATDEPER
QUALITMENT Y
OF ENVIRONMENT GROUNDWATER
L OURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Permit Name (if different): Non-Discharge WQ0014357 UIC
Facility Address: NC Highway Route 211 NPDES .
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City)
Ted Volskay (State) (Zip) 864 527-4637 Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone#: ( >
Well Location/Site Name: Treatment syst.discharge to infiltration gallery No. of Wells to be Sampled:(�om Pcrm�) Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 08/09/2016 Date sample analyzed: 08/16/2016
Field analysis: pH 5.44 , Specific Conductance 89 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.6 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/1
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/1 Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type .
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Permit Name (if different): Non-Discharge W00014357 UIC
NC Highway Route 211 NPDES .
Facility Address: (Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 Moore
(City) (slate) (Zip) County X
Ted Volskay [phone] lagoon Remediation: Infiltration Gallery
Contact Person: Telephone#:
Well Location/ Site Name: Treatment syst.discharge to infiltration gallery No. of Wells to be Sampled: ° Spray Field Remediation:
p (from Permit) Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 08/04/2016 Date sample analyzed: 08/12/2016
Field analysis: pH 5.37 , Specific Conductance 84 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 25.9 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/1 Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
GW-59 Signature of Permittee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES -
GROUNDWATER QUALITY MONITORING: to: WATER QUALITY DIVISION,GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH,NC 27699-1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name. Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
•
Permit Name (if different): Non-Discharge W00014357 UIC
Facility Address: NC Highway Route 211 NPDES
(Street) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) Ted Volskay (Slate) (Zip) [phone] Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone #:
Well Location/Site Name: Treatmenteyst discharge to infiltration gallery No. of Wells to be Sampled:
(from Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): Not Applicable For Groundwater Treatment Systems Other:
Well Depth: ft. Well Diameter: in. Check One: ❑ Influent (98)
Screened Interval: ft. to ft. ® Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: 06/27/2016 Date sample analyzed: 07/12/2016
Field analysis: pH 5.16 , Specific Conductance 91 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 19.1 °C, Odor _ none Appearance clear Certification No. NC Lab vertu 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method#. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method #= 8081A
. : method #=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. Mann, P.E., Project Manager
Permittee(or Authorized Agent)Name and Title-Please print or type
G W-59
Rev. 03/2000 Signature of Permittee(or Authorized Agent) (Date)

ti: eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656.2300 •Fax:[phone] • www.LancasterLabs.com
Partial Report
Sample Description: Effluent Grab Groundwater LL Sample # WW 8517494
Rt 211 Treatment System, NC LL Group # 1693003
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 08/09/2016 08:55 by TM Synterra Corporation
Suite 220
Submitted: 08/10/2016 09:25 148 River Street
Reported: 08/17/2016 17:18 Greenville SC 29601
211EF
CAT Dilution
Analysis Name CAS Number Method
No. �' Result Detection Limit Factor
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 N.D. 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0016 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0084 1
10589 p,p-DDD 72-54-8 N.D. 0.0041 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10589 p,p-DDT 50-29-3 N.D. 0.0043 1
10589 Delta BHC 319-86-8 N.D. 0.0028 1
10589 Dieldrin 60-57-1 0.0046 JP 0.0044 1
10589 Endosulfan I 959-98-8 N.D. 0.0035 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 N.D. 0.0067 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
Sample Comments
State of North Carolina Lab Certification No. 521
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 162240002A 08/16/2016 01:27 Jamie L Brilihart 1
Sample Description: Influent Grab Groundwater LL Sample # WW 8517495
Rt 211 Treatment System, NC LL Group # 1693003
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 08/09/2016 09:00 by TM Synterra Corporation
Suite 220
Submitted: 08/10/2016 09:25 148 River Street
Reported: 08/17/2016 17:18 Greenville SC 29601
211IN
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Reference ID:
1693003170816171851

- eurofins
Lancaster Laboratories Analysis Report
- vi
- nronmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656.2300 •Fax:[phone] • www.LancasterLabs.com
Partial Report
Sample Description: Influent Grab Groundwater LL Sample # WW 8517495
Rt 211 Treatment System, NC LL Group # 1693003
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 08/09/2016 09:00 by TM Synterra Corporation
Suite 220
Submitted: 08/10/2016 09:25 148 River Street
Reported: 08/17/2016 17:18 Greenville SC 29601
211IN
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.016 10
10589 Alpha BHC 319-84-6 0.13 0.024 10
10589 Beta BHC 319-85-7 4.8 0.28 100
10589 Gamma BHC - Lindane 58-89-9 0.076 J 0.016 10
10589 Alpha Chlordane 5103-71-9 N.D. 0.25 10
10589 Gamma Chlordane 5103-74-2 N.D. 0.057 10
10589 p,p-DDD 72-54-8 N.D. 0.041 10
10589 p,p-DDE 72-55-9 N.D. 0.041 10
10589 p,p-DDT 50-29-3 0.19 P 0.042 10
10589 Delta BHC 319-86-8 4.5 0.28 100
10589 Dieldrin 60-57-1 0.21 P 0.043 10
10589 Endosulfan I 959-98-8 0.10 0.035 10
10589 Endosulfan II 33213-65-9 0.12 JP 0.12 10
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.047 10
10589 Endrin 72-20-8 0.32 0.066 10
10589 Endrin Aldehyde 7421-93-4 N.D. 0.16 10
10589 Endrin Ketone 53494-70-5 N.D. 0.041 10
10589 Heptachlor 76-44-8 N.D. 0.016 10
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.019 10
10589 Methoxychlor 72-43-5 N.D. 0.24 10
10589 Toxaphene 8001-35-2 22 2.4 10
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No. 521
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 162240002A 08/17/2016 10:14 Jamie L Brillhart 10
10589 OC Pesticides in Water SW-846 8081B 1 162240002A 08/17/2016 10:28 Jamie L Brillhart 100
Reference ID:
1693003170816171851

. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 8510286
Rt 211 Treatment System, NC LL Group # 1691366
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 08/04/2016 13:17 by TV Synterra Corporation
Suite 220
Submitted: 08/05/2016 10:00 148 River Street
Reported: 08/16/2016 14:38 Greenville SC 29601
TSEFF
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 0.0045 JP 0.0025 1
10589 Beta BHC 319-85-7 0.16 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. V 0.0026 1
10589 Alpha Chlordane 5103-71-9 0.035 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.22 P 0.0057 1
10589 p,p-DDD 72-54-8 N.D. 0.018 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10589 p,p-DDT 50-29-3 0.017 P 0.0043 1
10589 Delta BHC 319-86-8 0.13 P 0.0028 1
10589 Dieldrin 60-57-1 0.027 0.0043 1
10589 Endosulfan I 959-98-8 0.0067 J 0.0035 1
10589 Endosulfan II 33213-65-9 0.028 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 0.025 0.0066 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.016 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 Heptachlor Epoxide 1024-57-3 0.0069 JP 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 1.5 0.25 1
The recovery for a target analyte(s) in the Laboratory Control
Spike(s) is outside the QC acceptance limits as noted on the QC
Summary. Dieldrin was detected in the method blank associated
with the sample as noted on the QC summary. The client was
contacted and the data reported.
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 162220004A 08/12/2016 17:49 Jamie L Brillhart 1
11120 Pesticide Waters Update SW-846 3510C 1 162220004A 08/09/2016 23:20 Karen L Beyer 1
IV Ext

.' eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs corn
Sample Description: Influent Grab Groundwater LL Sample # WW 8510287
Rt 211 Treatment System, NC LL Group # 1691366
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 08/04/2016 13:25 by TV Synterra Corporation
Suite 220
Submitted: 08/05/2016 10:00 148 River Street
Reported: 08/16/2016 14:38 Greenville SC 29601
TSINF
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0082 5
10589 Alpha BHC 319-84-6 0.13 0.012 5
10589 Beta BHC 319-85-7 5.8 0.14 50
10589 Gamma BHC - Lindane 58-89-9 0.095 0.0082 5
10589 Alpha Chlordane 5103-71-9 0.25 P 0.012 5
10589 Gamma Chlordane 5103-74-2 0.20 0.029 5
10589 p,p-DDD 72-54-8 N.D. 0.020 5
10589 p,p-DDE 72-55-9 0.078 JP 0.020 5
10589 p,p-DDT 50-29-3 0.17 P 0.021 5
10589 Delta BHC 319-86-8 4.6 0.14 50
10589 Dieldrin 60-57-1 0.20 P 0.022 5
10589 Endosulfan I 959-98-8 0.095 0.018 5
10589 Endosulfan II 33213-65-9 0.40 0.061 5
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.024 5
10589 Endrin 72-20-8 0.30 0.033 5
10589 Endrin Aldehyde 7421-93-4 N.D. 0.082 5
10589 Endrin Ketone 53494-70-5 0.079 J 0.020 5
10589 Heptachlor 76-44-8 N.D. 0.0082 5
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0094 5
10589 Methoxychlor 72-43-5 0.30 JP 0.12 5
10589 Toxaphene 8001-35-2 22 1.2 5
The recovery for a target analyte(s) in the Laboratory Control
Spike(s) is outside the QC acceptance limits as noted on the QC
Summary. Dieldrin was detected in the method blank associated
with the sample as noted on the QC summary. The client was
contacted and the data reported.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 162220004A 08/12/2016 18:02 Jamie L Brillhart 5
10589 OC Pesticides in Water SW-846 8081B 1 162220004A 08/14/2016 14:17 Jamie L Brillhart 50
11120 Pesticide Waters Update SW-846 3510C 1 162220004A 08/09/2016 23:20 Karen L Beyer 1
IV Ext

tieti eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike.Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Effluent Grab Groundwater LL Sample # WW 8449954
Rt 211 Treatment System, NC LL Group # 1676915
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/27/2016 14:13 by TV Synterra Corporation
Suite 220
Submitted: 06/28/2016 09:35 148 River Street
Reported: 07/22/2016 16:46 Greenville SC 29601
211EF
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 80818 ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0017 1
10589 Alpha BHC 319-84-6 0.0098 0.0025 1
10589 Beta BHC 319-85-7 0.45 0.014 5
10589 Gamma BHC - Lindane 58-89-9 0.0075 J 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.061 0.0058 1
10589 p,p-DDD 72-54-8 N.D. 0.0042 1
10589 p,p-DDE 72-55-9 N.D. 0.0042 1
10589 p,p-DDT 50-29-3 N.D. V 0.0070 1
10589 Delta BHC 319-86-8 0.30 0.014 5
10589 Dieldrin 60-57-1 0.058 0.0044 1
10589 Endosulfan I 959-98-8 0.013 0.0036 1
10589 Endosulfan II 33213-65-9 0.066 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 0.031 P 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
10589 Endrin Ketone 53494-70-5 0.0098 J 0.0042 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 0.035 P 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 4.4 0.25 1
Target analytes were detected in the method blank associated
with the samples as noted on the QC Summary. The following
corrective action was taken:
The sample was re-extracted outside the method required holding
time and the QC is compliant. All results are reported from the
first trial. Similar results were obtained in both trials.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 161810021A 07/12/2016 21:46 Lisa A Reinert 1
10589 OC Pesticides in Water SW-846 8081B 1 161810021A 07/12/2016 22:00 Lisa A Reinert 5
11120 Pesticide Waters Update SW-846 3510C 1 161810021A 06/30/2016 03:30 Sherry L Morrow 1
IV Ext

i
s
. eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 8449957
Rt 211 Treatment System, NC LL Group # 1676915
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/27/2016 14:30 by TV Synterra Corporation
Suite 220
Submitted: 06/28/2016 09:35 148 River Street
Reported: 07/22/2016 16:46 Greenville SC 29601
211IN
CAT Dilution
AnalysisNameCAS Number Result Method
No. Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 0.17 0.0017 1
10589 Alpha BHC 319-84-6 0.055 0.0025 1
10589 Beta BHC 319-85-7 3.1 0.071 25
10589 Gamma BHC - Lindane 58-89-9 0.048 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.13 P 0.0058 1
10589 p,p-DDD 72-54-8 N.D. 0.0041 1
10589 p,p-DDE 72-55-9 0.018 0.0041 1
10589 p,p-DDT 50-29-3 N.D. V 0.037 1
10589 Delta BHC 319-86-8 1.9 0.071 25
10589 Dieldrin 60-57-1 0.11 P 0.0044 1
10589 Endosulfan I 959-98-8 0.037 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 N.D. 0.0067 1
10589 Endrin Aldehyde 7421-93-4 N.D. V 0.053 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 0.090 P 0.0019 1
10589 Methoxychlor 72-43-5 N.D. V 0.20 1
10589 Toxaphene 8001-35-2 15 J 6.2 25
Reporting limits were raised due to interference from the sample matrix.
Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch* Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 161810021A 07/08/2016 05:07 Lisa A Reinert 1
10589 OC Pesticides in Water SW-846 8081E 1 161810021A 07/12/2016 23:36 Lisa A Reinert 25
11120 Pesticide Waters Update SW-846 3510C 1 161810021A 06/30/2016 03:30 Sherry L Morrow 1
IV Ext

Rogers, Michael
From: [e-mail]
Sent: Wednesday, January 20, 2016 10:17 AM
To: Rogers, Michael
Cc: Rumford, Doug; [e-mail]; [e-mail]; Hilliard, Garland E
CERG; [e-mail]; [e-mail]
Subject: Route 211 Site 2015 Annual Treatment System Report
Attachments: Final 2015 Treatment System Annual Report- Complete.pdf
Mike,
Good morning. Please find attached the 2015 Annual Treatment System Report for the Route 211 Site. If you have any
comments or questions, please contact me. Thanks.
Regards.
Tom
C
s y nTerra
Scnin+g and grokving since 1991
Thomas A. Mann, PE
SynTerra Corporation
148 River Street, Suite 220
Greenville, SC 29601
864-527-4617
[e-mail]
This e-mail might contain privileged or confidential information. If the e-mail was not intended for you, please:
(1) delete the e-mail and any attachments
(2) destroy any copies that might have been made
(3) do not use, copy, or distribute the contents in any form
(4) notify me by return e-mail or by calling 864-527-4617
No privilege is waived by inadvertent transmission. Thank you.
1

synTerra
January 20, 2016
Mr. Mike Rogers
NCDENR, Division of Water Quality
Aquifer Protection, Underground Injection Control Program
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: 2015 Annual Report
Groundwater Remediation Permit No. WQ0014357
Aberdeen Pesticide Dumps Site - Route 211 Area
Aberdeen, North Carolina
Dear Mr. Rogers:
On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2015 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
• Analytical monitoring requirements summary (Table 1);
• Influent and effluent analytical results summary (Tables 2 and 3);
• Monitoring well analytical results summary (Table 4);
• Completed copies of NCDENR Division of Water Quality, Groundwater Section
form GW-59 and analytical laboratory data reports (Attachments).
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (June 30, 2015 and December 30, 2015) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2015 and experienced minimal downtime. The system
operates 24 hours per day and a total of 1,110,388 gallons (based upon the monthly
inspection dates between January 28 to December 9, 2015) of groundwater were treated.
Groundwater extraction rates averaged approximately 3,525 gpd during the monitoring
period. The treatment system removal efficiency was greater than 95% (see Tables 2 and
3).
INNOVATE 148 River Street, Suite 220 Greenville. SC 29601 (8641 421-9999 Fax[phone] www.synterracorp.com

2015 Annual Report
Groundwater Remediation Permit No.WQ0014357
Aberdeen Pesticide Dumps Site-Route 211 Area
January 2016
Page Two
Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), and one upgradient well, MW-1 (RT-MW-12), were
sampled on December 30, 2015 and analyzed for SW-846 8081A pesticides. Analytical
results are summarized in Table 4. Copies of the treatment system influent and effluent
analytical reports and the MW-2 and MW-3 analytical report are included with the
completed GW-59 forms provided as attachments.
Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Section IV, items 1 - 4 and 13, of the Site Groundwater
Remediation Permit issued January 25, 2007.
If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].
Sincerely,
tviaA,
rzyvvy.,...,
Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation
Attachments:
GW-59 Forms
Analytical reports
Electronic cc:
Jon Bornholm—USEPA Garland Hilliard—Olin
Doug Rumford—NCDENR Michael Bogle, Esq. - WCS&R
George Crouse- Syngenta Ted Volskay-SynTerra
INNOVATE 148 River Street,Suite 220 Greenville,SC 29601 [phone] Fax[phone] www.synterracorp.com

Route 211 Treatment System
2015 Annual Operating Report
SynTerra Corporation
January 2016
Table 1
Analytical Monitoring Requirements
Groundwater Extraction and Treatment System
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Frequency
(Permit No.
Location Parameters of Analysis WQ0014357)
Influent TCL Pesticides &pH Semi-annually
(RT-PW-01) (Jan.-June, July- Dec.)
Effluent TCL Pesticides & pH Semi-annually
(Jan.-June,July- Dec.)
MW-1 TCL Pesticides, pH Annually
(RT-MW-12) &Water Level
MW-2 TCL Pesticides, pH Annually
(05-MW-01) &Water Level
MW-3 TCL Pesticides, pH Annually
(RT-MW-05) &Water Level

Route 211 Treatment System
2015 Annual Operating Report
SynTerra Corporation
January 2016
Table 2
Treatment System Monitoring Results And
Treatment Removal Efficiency (January - June 2015)
Route 211 Area Semi-Annual Operating Report
Aberdeen, North Carolina
Sample Name Influent Effluent
Date Sampled 06/30/15 06/30/15
Pesticides(ug/L)
Aldrin 0.28 0.0034 J
alpha-BHC 0.047 < 0.0025
alpha-Chlordane 0.074 P < 0.0033
beta-BHC 2.8 0.017
p,p-DDD < 0.0042 < 0.0042
p,p-DDE 0.025 < 0.0042
p,p-DDT < 0.024 V < 0.0044
delta-BHC 6.0 < 0.014
Dieldrin 0.055 P < 0.0044
Endosulfan I 0.019 < 0.0036
Endosulfan II 0.096 < 0.013
Endosulfan Sulfate < 0.0048 < 0.0049
Endrin < 0.027 V < 0.0068
Endrin Aldehyde 0.094 P < 0.017
Endrin Ketone < 0.012 V < 0.0042
gamma-BHC 0.043 < • 0.0017
gamma-Chlordane 0.08 < 0.0059
Heptachlor < 0.0017 < 0.0017
Heptachlor Epoxide < 0.030 V < 0.0019
'Methoxychlor 0.20 P < 0.025
Toxaphene < 0.25 < 0.25
Total Pesticides 9.81 0.020
System Removal Efficiency: 99.79%
Notes:
Influent pH was 5.07 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable concentrations are used for removal efficiency.
Permit specified removal efficiency:95%

Table 3
Treatment System Monitoring Results And
Treatment Removal Efficiency (July - December 2015)
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Monitoring Period July - December 2015
Sample Name Influent Effluent
Date Sampled 12/30/15 12/30/15
Pesticides(ug/L)
Aldrin < 0.0083 < 0.0016
alpha-BHC 0.24 < 0.0025
beta-BHC 4.9 0.048
gamma-BHC(Lindane) 0.130 < 0.0016
alpha-Chlordane 0.19 P 0.0080 JP
gamma-Chlordane 0.170 < 0.0084 J
p,p-DDD < 0.021 < 0.0041
p,p-DDE < 0.0210 < 0.0041
p,p-DDT < 0.04 V < 0.0043
delta-BHC 23 0.0300 P
Dieldrin 0.120 P 0.0087 J
Endosulfan I 0.062 < 0.0035
Endosulfan II 0.14 P < 0.012
Endosulfan Sulfate < 0.024 < 0.0048
Endrin 0.15 < 0.0066
Endrin Aldehyde 0.210 JP < 0.016 ,
Endrin Ketone 0.033 JP < 0.0041
Heptachlor < 0.008 < 0.0016
Heptachlor Epoxide < 0.10 P < 0.0019
Methoxychlor 0.24 JP < 0.025
Toxaphene < 1.2 < 0.25
Total pesticides 29.6 0.09
System Removal Efficiency: 99.68%
Notes:
Influent pH was 4.82 s.u.
J-estimated value
P-RPD>40%
V-RPD>100%
Only measurable concentrations are used for removal efficiency.
Permit specified removal efficiency:95%

Route 211 Treatment System
2015 Annual Operating Report
SynTerra Corporation
January 2016
Table 4
Monitoring Well Analytical Results Summary
Route 211 Area Annual Operating Report
Aberdeen, North Carolina
Sample Name MW-1 (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)
Sample Event Annual Annual Annual
Date Sampled 12/30/15 12/30/15 12/30/2015
Pesticides (ug/L)
Aldrin < 0.0017 < 0.0016 < 0.0017
alpha-BHC < 0.0025 0.012 < 0.0026
beta-BHC < 0.0028 1.2 < 0.0029
gamma-BHC (Lindane) < 0.0017 0.013 < 0.0017
alpha-Chlordane < 0.0025 0.079 P < 0.0026
gamma-Chlordane < 0.0059 0.050 < 0.0061
p,p-DDD < 0.0042 < 0.038 V < 0.0043
p,p-DDE < 0.0042 < 0.0041 < 0.0043
p,p-DDT < 0.0044 < 0.014 V < 0.0045
delta-BHC < 0.0028 0.16 < 0.0029
Dieldrin < 0.0044 0.186 < 0.0046
Endosulfan I < 0.0036 0.015 P < 0.0037
Endosulfan II < 0.0130 0.12 < 0.013
Endosulfan Sulfate < 0.0049 < 0.0048 < 0.005
Endrin < 0.0068 < 0.007 < 0.007
Endrin Aldehyde < 0.0170 0.11 P < 0.017
Endrin Ketone < 0.0042 0.015 JP < 0.0043
Heptachlor < 0.0017 < 0.0016 < 0.0017
Heptachlor Epoxide < 0.0019 0.044 < 0.002
Methoxychlor < 0.025 0.092 P < 0.026
Toxaphene < 0.25 < 0.25 < 0.26
MW-1 (RT-MW-12)pH=3.57
MW-2(05-MW-01)pH=4.33
MW-3(RT-MW-05)pH=3.97
J-estimated value
P-RPD>40%
V-RPD>100%

ATTACHMENTS

MONITORING WELLS
(MW-1, MW-2, MW-3)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
4, , ,.,,„„t0' WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM V 1636 MAIL SERVICE CENTER
RALEIGH,NC 27699-1636 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
Route 211 Area PERMIT it: EXPIRATION DATE: June 30 2016
Facility Name: Non-Discharge WQ0014357 UIC_
Permit Name (if different):
Facility Address: NC Highway Route 211 NPDES_ — _-
Aberdeen (Sveei) NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(CkyY tsratea >,5) County __.
Contact Person: Ted Volskay Telephone #: [phone] Lagoon X Remediation: Infiltration Gallery
Well Location!Site Name: No. of Wells to be Sampled: ' Spray Field _._.._..._._Remediation:
r°mrcrmuy Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-MW-12(rMW-1) For Groundwater Treatment Systems Other:
Well Depth: 20.50 ft. Well Diameter: 2.° in. Check One: ❑ Influent (98)
Screened Interval: 107D ft. to 20.50 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 12.05 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 2.18 ft.above land surface. Relative M.P. Elevation in ft.: 445.61
Gallons of water pumped/bailed before sampling: 4.5 Date sample collected: 12/30/2015 Date sample analyzed: 01/07/2015
Field analysis: pH 3.57 , Specific Conductance 30 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
Temp. __�6 6 °C, Odor none Appearance Clear Certification No. NC Certification No.521
E.ARAMETERS (Samples for metals were collected unfiltered YES _NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead . mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/ _
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils _ mg/I Cu - Copper mg/ -
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate ____ mg/I Fig - Mercury mg/ (Specify test and method It. Attach lab report)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes x (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/ VOC (example) : method # = Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method it = 8081A
: method it=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thomas A. ann, P.E., Project Manager
R r Auth ized Age )Name and Title-Please print or type /
GW 59 Signal rL�dt Permrttee(or Authorized Agent) (Date)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
•
GROUNDWATER QUALITY MONITORING: Mail Original DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES
to: WATER QUALITY DIVISION,GROUNDWATER SECTION
k ,., ' 1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM r° ::.``,, RALEIGH, NC27699-1636 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name:
Route 211 Area PERMIT#: EXPIRATION DATE:Jut 30,2o16
Non-Discharge W00014357 UIC_.__.._.__.__
Permit Name (if different): NPDES — —_
Facility Address: NC Highway Route 211 -.
(time') TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(City) Tom Mann (Sta1C) (T�"' [phone] Lagoon __X_Remediation: Infiltration Gallery
Contact Person: Telephone #:
Well Location/Site Name:....._.... No. of Wells to be Sampled: Spray Field Remediation:
tir¢m Perxnrti Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): 05-MW-01(MW-2) For Groundwater Treatment Systems Other:
Well Depth: 37.52 ft. Well Diameter:4.0 in. Check One: 0 Influent (98)
Screened Interval:22.67 ft.to 37.52 __ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level:21.74 _ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.) is: 3.22 ft. above land surface. Relative M.P. Elevation in ft.: 454.40
Gallons of water pumped/bailed before sampling: 31.0 Date sample collected: 12/29/2015 Date sample analyzed: 01/07/2015
Field analysis: pH 4.33 , Specific Conductance 80 .__._ .- Mhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania)
__
Temp. 19.3 °C, Odor None Appearance Clear Certification No. NC Certification 521
PARAMETERS(Samples for metals were collected unfiltered _YES NO and field acidified YES NO)
COD __ mg/I Nitrite (NO2) as N mg/I Ni Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/1
Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn - Zinc ._ mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/1
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mg/I ----
Phenol mg/I Fe - Iron_ — mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No _______(0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable
TKN as N _. mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8081A
: method 4 _
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ,(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Tomas A. Mann, P.E., Project Manager
Perm erne(or Auth ized {Agent)Name and Title-Please print or type
\A,UL/V•••-•, r \'4,p\„„,-....._____„,... VIC( -(-)16'
GW-59 Signal'ure of Permittee for Authorized Agent) t Dale)
Rev. 03/2000

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Origina DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: , � H i) WATER QUALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM ,. 1636 MAIL SERVICE CENTER
RALEIGH,NC 276 99-1 6 36 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Route 211 Area PERMIT#: EXPIRATION DATE:June 30,2016
Non-Discharge W00014357 UIC
Permit Name (if different): NPDES
Facility Address: NC Highway Route 211
`""°"`) TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(city) Tom Mann (Stale) (`�P' [phone] __Lagoon ____X___Remediation: Infiltration Gallery
Contact Person: Telephone #: ,.
Well Location/Site Name: No. of Wells to be Sampled:{iram Spray Field Remediation;
p Pcr ir)
Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): aT-Mw-0S(Mw-3)
) For Groundwater Treatment Systems Other:
Well Depth: 24.57 ft. Well Diameter:2.0 in. Check One: ❑ Influent (98)
Screened Interval:14" ft. to 24.57 ft. 0 Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 18.52 ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.)is: 2.67 _ ft.above land surface. Relative M.P. Elevation in ft.: 449.59
Gallons of water pumped/bailed before sampling: 3.0 ___ Date sample collected: 12/30/2015 _ Date sample analyzed: 01/07l'2015
Field analysis: pH 3.97 _ , Specific Conductance 20 uMhos Laboratory Name: eurofins(Lancaster Labs)(Pennsylvania) ^
None NC Certification No. 521
Temp. 1" °C, Odor Appearance Clear Certification No.
PARAMETERS (Samples for metals were collected unfiltered _._YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC___ mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium _ mg/ VOC (example) : method #= Not Applicable
TKN as N mg/I Mn - Manganese mg/ TCL Pesticides : method #= 8081A
: method#=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory,lam aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Thcmas A. Mann, P.E., Project Manager
P (or Authorir d Agent)Marne and Title•Please punt or type I
GW-59 Signature of a mittee(or Autho ed Agent) • (pare)
Rev. 03/2000

ti eurofins
1 Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-1 (RT-MW-12) Grab Groundwater LL Sample # WW 8195136
Rt 211 Treatment System, NC LL Group # 1621136
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/30/2015 10:20 by TV Synterra Corporation
Suite 220
Submitted: 01/05/2016 10:05 148 River Street
Reported: 01/12/2016 11:39 Greenville SC 29601
211M1
CAT Method Dilution
No. Analysis Name CAS Number -Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ugh]. ug/1
10589 Aldrin 309-00-2 N.D. 0.0017 1
10589 Alpha BHC 319-84-6 N.D. 0.0025 1
10589 Beta BHC 319-85-7 N.D. 0.0028 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. 0.0025 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0059 1
10589 p,p-DDD 72-54-8 N.D. 0.0042 1
10589 p,p-DDE 72-55-9 N.D. 0.0042 1
10589 p,p-DDT 50-29-3 N.D. 0.0044 1
10589 Delta BHC 319-86-8 N.D. 0.0028 1
10589 Dieldrin 60-57-1 N.D. 0.0044 1
10589 Endosulfan I 959-98-8 N.D. 0.0036 1
10589 Endosulfan II 33213-65-9 N.D. 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0049 1
10589 Endrin 72-20-8 N.D. 0.0068 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0042 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0019 1
10589 Methoxychlor 72-43-5 N.D. 0.025 1
10589 Toxaphene 8001-35-2 N.D. 0.25 1
General Sample Comments
State of North Carolina Lab Certification No. 521
The temperature of the temperature blank bottle(s) upon receipt at the
lab was 6.7 C using a digital thermometer. The sample bottles were then
measured using an IR thermometer and were recorded at 7.2-7.8 C.
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 160060027A 01/07/2016 20:10 Lisa A Reinert 1
11120 Pesticide Waters Update SW-846 3510C 1 160060027A 01/06/2016 01:00 Sherry L Morrow 1
IV Ext
Page 4 of 12

•
. l: eurafins
1 Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster.PA 17601 • 717.656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: MW-2 (05-MW-01) Grab Groundwater LL Sample # WW 8195137
Rt 211 Treatment System, NC LL Group # 1621136
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/29/2015 19:36 by TV Synterra Corporation
Suite 220
Submitted: 01/05/2016 10:05 148 River Street
Reported: 01/12/2016 11:39 Greenville SC 29601
211M2
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081E ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0016 1
10589 Alpha BHC 319-84-6 0.012 0.0025 1
10589 Beta BHC 319-85-7 1.2 0.070 25
10589 Gamma BHC - Lindane 58-89-9 0.013 0.0016 1
10589 Alpha Chlordane 5103-71-9 0.079 P 0.0025 1
10589 Gamma Chlordane 5103-74-2 0.050 0.0057 1
10589 p,p-DDD 72-54-8 N.D. V 0.038 1
10589 p,p-DDE 72-55-9 N.D. 0.0041 1
10569 p,p-DDT 50-29-3 N.D. V 0.014 1
10569 Delta BHC 319-86-8 0.16 0.0028 1
10589 Dieldrin 60-57-1 0.086 0.0043 1
10589 Endosulfan 959-98- 0.015 P 1
10589 Endosulfan II 33213-65-9 0.12 0.012 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
10589 Endrin 72-20-8 N.D. 0.0066 1
10589 Endrin Aldehyde 7421-93-4 0.11 P 0.016 1
10589 Endrin Ketone 53494-70-5 0.015 JP 0.0041 1
10589 Heptachlor 76-44-8 N.D. 0.0016 1
10589 H ptachlor Epoxide 1024-57-3 0.044. 0 0419 1
10589 Methoxychlor 72-43-5 0.092 P 0.025 1
10589 Toxaphene 6001-35-2 N.D. 0.25 1
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
The temperature of the temperature blank bottle(s) upon receipt at the
lab was 6.7 C using a digital thermometer. The sample bottles were then
measured using an IR thermometer and were recorded at 7.2-7.8 C.
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 160060027A 01/07/2016 20:37 Lisa A Reinert
10589 OC Pesticides in Water SW-846 8081B 1 160060027A 01/07/2016 20:51 Lisa A Reinert
11120 Pesticide Waters Update SW-846 3510C 1 160060027A 01/06/2016 01:00 Sherry L Morrow
IV Ext
Page 5 of 12

t eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656.2300 •Fax:[phone] - www.LancasterLabs.com
Sample Description: MW-3 (RT-MW-05) Grab Groundwater LL Sample # WW 8195138
Rt 211 Treatment System, NC LL Group # 1621136
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/30/2015 10:57 by TV Synterra Corporation
Suite 220
Submitted: 01/05/2016 10:05 148 River Street
Reported: 01/12/2016 11:39 Greenville SC 29601
211M3
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0017 1
10589 Alpha BHC 319-84-6 N.D. 0.0026 1
10589 Beta BHC 319-85-7 N.D. 0.0029 1
10589 Gamma BHC - Lindane 58-89-9 N.D. 0.0017 1
10589 Alpha Chlordane 5103-71-9 N.D. - 0.0026 1
10589 Gamma Chlordane 5103-74-2 N.D. 0.0061 1
10589 p,p-DDD 72-54-8 N.D. 0.0043 1
10589 p,p-DDE 72-55-9 N.D. 0.0043 1
10589 p,p-DDT 50-29-3 N.D. 0.0045 1
10589 Delta BHC 319-86-8 N.D. 0.0029 1
10589 Dieldrin 60-57-1 N.D. 0.0046 1
10589 Endosulfan I 959-98-8 N.D. 0.0037 1
10589 Endosulfan II 33213-65-9 N.D. 0.013 1
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.0050 1
10589 Endrin 72-20-8 N.D. 0.0070 1
10589 Endrin Aldehyde 7421-93-4 N.D. 0.017 1
10589 Endrin Ketone 53494-70-5 N.D. 0.0043 1
10589 Heptachlor 76-44-8 N.D. 0.0017 1
10589 Heptachlor Epoxide 1024-57-3 N.D. 0.0020 1
10589 Methoxychlor 72-43-5 N.D. 0.026 1
10589 Toxaphene 8001-35-2 N.D. 0.26 1
General Sample Comments
State of North Carolina Lab Certification No. 521
The temperature of the temperature blank bottle(s) upon receipt at the
lab was 6.7 C using a digital thermometer. The sample bottles were then
measured using an IR thermometer and were recorded at 7.2-7.8 C.
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081B 1 160060027A 01/07/2016 20:24 Lisa A Reinert 1
11120 Pesticide Waters Update SW-846 3510C 1 160060027A 01/06/2016 01:00 Sherry L Morrow 1
IV Ext
Page 6 of 12

INFLUENT

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail Original
o. DEPAWATRT ENT QUALITY DIVISION,
ENVIRONMENT S NATURAL SECTION
-4'' 1636 MAIL SERVICECENTER
GROUNDWATER SECTION
COMPLIANCE REPORT FORM RALEIGR,NC 27699.1636 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT#: EXPIRATION DATE:June 30,2016
Facility Name: Route 211 Area UIC
Permit Name (if different): Non-Discharge WQ0014357
Facility Address: NC Highway Route 211 NPDES
Aberdeen (street, NC 28315 Moore TYPE OF PERMITTED OPERATION BEING MONITORED
(COy) (st ) (zip) County X
Contact Person: Ted voiskay Telephone #: [phone] Lagoon Remediation: Infiltration Gallery
,,w
Well Location/ Site Name: RT-PW-°1 to treatment system No. of Wells to be Sampled: ^ Spray Field Remediation:
p lirem°°""i') Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems - Other: _ ______._.__.-.....__._. ,
Well Depth: 4°.51 ft. Well Diameter: 6.0 in. Check One: D Influent (98)
Screened Interval: 16_07 ft. to 4°.51 ft. ❑ Effluent (99) NOTE: Values should reflect dissolved and
Depth to Water Level: 22.05 ft. below measuring point. colloidal concentrations.
Measuring Point (M.P.) is: 2.45 ft.above land surface. Relative M.P. Elevation in ft.: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 06/30/2015 Date sample analyzed: 06i20/2014
Field analysis: pH 5.07 Specific Conductance 90 uMhos Laboratory Name: Lancaster(Pennsylvania)
Temp. 18.0 °C, Odor none Appearance clear Certification No. NC Lab Cert#521
PARAMETERS (Samples for metals were collected unfiltered _YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/ Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/ Pb - Lead mg/I
Coliform: MF Total /100m1 Phosphorus: Total as P mg/ Zn - Zinc mg/F
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/ Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/ Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/
TOC mg/I Ca - Calcium mg/
Chloride mg/I Cd - Cadmium mg/
Arsenic mg/I Chromium: Total mg/
Grease and Oils mg/I Cu - Copper mg/ --
Phenol mg/I Fe - Iron mg/ ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/ (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/ Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg Magnesium mg/ VOC (example) method # = Not Applicable
TKN as N mg/I Mn Manganese mg/ TCL Pesticides : method # = 8081A
: method #.=
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWO(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Th masA. Mann, P.E., Project Manager
Pe tin a or Auihoriz Ago )Name and Title-Please print or type
Ic 20 is-
GW 59 Signature of Perrnitte (or Aut or ed Agent) (Date)
Rev. 03/2000

SUBMIT i:ORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: MaitOriginal DEPARTMENT OF ENVIRONMENT& NATURAL.RESOURCES
rito. 1636 MAWATER OUSERVICE CENTER ALITY DIVISION,GROUNDWATER SECTION
COMPLIANCE REPORT FORM RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT#: EXPIRATION DATE:June 3U,2016 _
Facility Name: Route 211 Area Non-Dischargewo0014357
Permit Name (if different):
UIC
Facility Address: NC Highway Route 211 NPDES
(Sheep TYPEQF PERMITTED OPERATION BEING MONITORED
Aberdeen NC 28315 County Moore
(t a`r( Tom Mann (Slate)
(zip) 864 527 4617 Lagoon X Remediation: Infiltration Gallery
Contact Person: Telephone #: ( )
Well Location/ Site Name: No. of Wells to be Sampled: Spray Field __Remediation: __
p '°"'r°"""t Rotary Distributor Land Application of Sludge
Well Identification Number(from Permit): RT-PW-01 For Groundwater Treatment Systems Other: _
Well Depth: 40.51 ft. Well Diameter:6.0 in. Check One: ® Influent (98)
Screened Interval:1607 ft.to 40.51 ft. ❑ Effluent (99) NOTE; Values should reflect dissolved and
Depth to Water Level: NA ft. below measuring point. colloidal concentrations.
Measuring Point(M.P.)is: 2-45 ft.above land surface. Relative M.P. Elevation in ft,: 450.53
Gallons of water pumped/bailed before sampling: NA Date sample collected: 12/30/2015 Date sample analyzed: 01/07/2015
Field analysis: pH 4.82 Specific Conductance 110 uMhos Laboratory Name; eurofins(Lancaster Labs)(Pennsylvania)
Temp. 20.7 °C, Odor None Appearance Clear Certification No. NC Certification No. 521
PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO)
COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I
Coliform: MF Total /1 00m1 Phosphorus: Total as P mg/I Zn - Zinc mg/I
(Note:Use MPN method for highly turbid samples) Orthophosphate mg/I Ammonia Nitrogen mg/I
Dissolved Solids: Total mg/I Al - Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) units Ba - Barium mg/I
TOC mg/I Ca - Calcium mg/I __
Chloride mg/I Cd - Cadmium mg/I
Arsenic mg/I Chromium: Total mg/I
Grease and Oils _.. mg/I Cu - Copper mg/I
Phenol mg/I Fe - Iron mg/I ORGANICS: (GC,GC/MS,HPLC)
Sulfate mg/I Hg - Mercury mg/I (Specify test and method #. Attach lab report.)
Specific Conductance uMhos K - Potassium mg/I Report Attached? Yes X (1) No (0)
Total Ammonia mg/I Mg - Magnesium mg/I VOC (example) : method # = Not Applicable _
TKN as N mg/I Mn - Manganese mg/I TCL Pesticides : method # = 8081A
: method # =
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced
using approved methods of analysis by a North Carolina DWQ(formerly DEM)certified laboratory.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations. Tkiomas A. Mann, P.E., Project Manager
aed t (or Auth zed Aenl)Name and Title-Please print or type '
GW-59 \11IW�f /� �r !� yf -(JIILl.
Signature at Permittee(or Authorized Agent) (Date)
Rev. 03/2000

eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717 656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 7951154
Rt 211 Treatment System, NC LL Group # 1573603
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 06/30/2015 08:58 by TM Synterra Corporation
Suite 220
Submitted: 07/01/2015 10:00 148 River Street
Reported: 07/14/2015 13:05 Greenville SC 29601
211-I
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081A ug/1 ug/1
00177 Aldrin 309-00-2 0.28 0.0083 5
00177 Alpha BHC 319-84-6 0.047 0.0025 1
00177 Beta BHC 319-85-7 2.6 0.28 100
00177 Gamma BHC - Lindane 58-89-9 0.043 0.0017 1
00177 Alpha Chlordane 5103-71-9 0.074 P 0.0025 1
00177 Gamma Chlordane 5103-74-2 0.076 0.0058 1
00177 p,p-DDD 72-54-8 N.D. 0.0042 1
00177 p,p-DDE 72-55-9 0.025 0.0042 1
00177 p,p-DDT 50-29-3 N.D. V 0.024 1
00177 Delta BHC 319-86-8 6.0 0.28 100
00177 Dieldrin 60-57-1 0.055 P 0.0044 1
00177 Endosulfan I 959-98-8 0.019 0.0036 1
00177 Endosulfan II 33213-65-9 0.096 0.013 1
00177 Endosulfan Sulfate 1031-07-8 N.D. 0.0048 1
00177 Endrin 72-20-8 N.D. V 0.027 1
00177 Endrin Aldehyde 7421-93-4 0.094 P 0.017 1
00177 Endrin Ketone 53494-70-5 N.D. V 0.012 1
00177 Heptachlor 76-44-8 N.D. 0.0017 1
00177 Heptachlor Epoxide 1024-57-3 N.D. V 0.030 1
00177 Methoxychlor 72-43-5 0.20 P 0.025 1
00177 Toxaphene 8001-35-2 N.D. 0.25 1
The % difference for the calibration verification standard is outside the
+/- 15% criteria for the analyte(s) listed below. Since the average of the
% difference values meets the criteria, the results are reported.
This applies to the following analyte(s) :
methoxychlor
General Sample Comments
State of North Carolina Lab Certification No. 521
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/07/2015 02:13 Lisa A Reinert 1
00177 OC Pesticides in Water SW-846 8061A 1 151830009A 07/11/2015 00:58 Lisa A Reinert 5
00177 OC Pesticides in Water SW-846 8081A 1 151830009A 07/11/2015 01:23 Lisa A Reinert 100
11118 Pesticide Screen Waters SW-846 3510C 1 151830009A 07/02/2015 19:35 Karen L Beyer 1
Ext
Page 2 of 8

lit
y.1 eurofins
Lancaster Laboratories Analysis Report
Environmental
2425 New Holland Pike,Lancaster,PA 17601 • 717-656-2300 •Fax:[phone] • www.LancasterLabs.com
Sample Description: Influent Grab Groundwater LL Sample # WW 8195139
Rt 211 Treatment System, NC LL Group # 1621136
Account # 12819
Project Name: Rte 211 Treatment System, NC
Collected: 12/30/2015 11:45 by TV Synterra Corporation
Suite 220
Submitted: 01/05/2016 10:05 148 River Street
Reported: 01/12/2016 11:39 Greenville SC 29601
211IN
CAT Method Dilution
No. Analysis Name CAS Number Result Factor
Detection Limit
Pesticides/PCBs SW-846 8081B ug/1 ug/1
10589 Aldrin 309-00-2 N.D. 0.0083 5
10589 Alpha BHC 319-84-6 0.24 0.012 5
10589 Beta BHC 319-85-7 4.9 0.56 200
10589 Gamma BHC - Lindane 58-89-9 0.13 0.0083 5
10589 Alpha Chlordane 5103-71-9 0.19 P 0.012 5
10589 Gamma Chlordane 5103-74-2 0.17 0.029 5
10589 p,p-DDD 72-54-8 N.D. 0.021 5
10589 p,p-DDE 72-55-9 N.D. 0.021 5
10589 p,p-DDT 50-29-3 N.D. V 0.040 5
10589 Delta BHC 319-86-8 23 0.56 200
10589 Dieldrin 60-57-1 0.12 P 0.022 5
10589 Endosulfan I 959-98-8 0.062 0.018 5
10589 Endosulfan II 33213-65-9 0.14 P 0.062 5
10589 Endosulfan Sulfate 1031-07-8 N.D. 0.024 5
10589 Endrin 72-20-8 0.15 0.033 5
10589 Endrin Aldehyde 7421-93-4 0.21 JP 0.083 5
10589 Endrin Ketone 53494-70-5 0.033 JP 0.021 5
10589 Heptachlor 76-44-8 N.D. 0.0083 5
10589 Heptachlor Epoxide 1024-57-3 0.10 P 0.0095 5
10589 Methoxychlor 72-43-5 0.24 JP 0.12 5
10589 Toxaphene 8001-35-2 N.D. 1.2 5
Reporting limits were raised due to interference from the sample matrix.
General Sample Comments
State of North Carolina Lab Certification No. 521
The temperature of the temperature blank bottle(s) upon receipt at the
lab was 6.7 C using a digital thermometer. The sample bottles were then
measured using an IR thermometer and were recorded at 7.2-7.8 C.
All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Laboratory Sample Analysis Record
CAT Analysis Name Method Trial# Batch# Analysis Analyst Dilution
No. Date and Time Factor
10589 OC Pesticides in Water SW-846 8081E 1 160060027A 01/07/2016 21:19 Lisa A Reinert 5
10589 OC Pesticides in Water SW-846 8081B 1 160060027A 01/07/2016 21:46 Lisa A Reinert 200
11120 Pesticide Waters Update SW-846 3510C 1 160060027A 01/06/2016 01:00 Sherry L Morrow 1
IV Ext
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