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A w 2 x w w U Y U- a < LL a O _u J y V z 2 LU z /O/_^� aui m V Y w 1 c cc C a w n O d w w Z 2 z LU u u u Z ~ LL O O =) LU LLL LL O � Z Q z n+�o LLI W w cr m H t3 I Z w O L Y N r-I rt5 — C tD LL U a 4-J U (�o M W L- rj U `NN U O � •� Z GA ❑ a W O a = r c � 3 cr-a j O O tl) Ul aJ � O L O- O +T O Y u 0 E Q � � a O Q CL ++ a) W U1 u -0 t4 ro 1� a O 4� C aaj a O (A o E E O -0 O 0 a L O Ln � C •— u m O aj E nA L Q � L L cm C- E °i aJ 'O L' CL O �o c a) a •� a a � a CL aJ c 4�M u 2 .L HE E > L m t m C bA a) Y m ra �F C to A C m c L S a1 � W O_ a W L L 0 3 � a O q� E + ai O ai i a .O +' a Q MI 3 E O ai fU M Ln Q v- O O t O Q 41 C y a"' mL m O a °c CL LA T u O I4 /% m C O r a3 a) � E N aS y� Q t' fa } a_} u a �p a E -a E - . m I;r N FF,P,P--. -71 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax O 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Pilgrim's Pride-Marshville Date of Report: Sep 11, 2020 5901 West Marshville Blvd. Customer PO #: Marshville NC 28103 Customer ID: 17040005 Attention: George Chang, PE Report #: 2020-14707 Project ID: Marshville Storm Water Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-37446 Site: Outfall #1 8/31/2020 11:30 AM Water Yin-Pong Chang Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5.0 mg/L 09/02/2020 Residue Suspended (TSS) SM 2540 D 54.5 mg1L 09/01 /2020 pH SM 4500 s 8 6.7 units 09/09/2020 COD SM 5220D 57 mg/L 09/10/2020 Fecal Coliform SM 9222D MF 3000 Colonies/100mL 08/31/2020 Comment: Reviewed by: f Reporl #:: 2020.14707 Page 1 of 1 FPO"- -- --"q Environmental Chemists, Inc. 1-7- envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington 1-Iighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Pilgrim's QC - 2020-14707 LCS Parameter True value m lL Result mg%'L % True Value Limits % COD 1000 995 100 90-110 Fecal N/A N/A NIA NIA TSS 92.5 92.0 99 82.4-1 18 PH 7.00 6.99 100 90-1 10 OIL & GREASE 1 40.0 32.9 82 78-114 MS/MSD Parameter True Value m /L Recovery mg& % Recovery % Difference Limits % Recovery Limits Vo Difference COD 50.0 52154 104/108 4 80-120 520 Fecal NIA N/A N/A N/A N/A N/A TSS NIA N/A NIA NIA N/A NIA pH NIA NIA N/A NIA N/A N/A OIL & GREASE 40.0 35.3 88 N/A 78-114 < 18 DUPLICATE SAMPLES Parameter Results m91L %Difference Limits COD N/A N/A N/A < 10 Fecal NIA NIA N/A < 30 TSS 77.0 80.0 4 < 10 pH NIA N/A N/A < 10 OIL & GREASE NIA N/A NIA N/A Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info @Denvironmentalchemists.com BLANK Parameter Results mg/L Limit mg/L COD <l0 10 Fecal (Star# Control) 0 0 TSS <2.5 2.5 P11 N/A NIA OIL & GREASE <2.5 2.5 Environmental Chemist, Inc,, Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 I Client: i Y1 �S �rkNk Date: � 13eport Number:Ili Receipt of sample: Delivered UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Cor cted temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ID NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? 1,10 YES ---YES 10 NO 4. Were proper custody procedures (relinquished/received) followed? ;YES 10 NO 5. Were sample ID's listed on the COC? 10 NO 6, Were samples ID's listed on sample containers? YES 10 NO 7, Were collection date and time listed on the CDC? YES 1111 NO 8. Were tests to be performed listed on the COC? YES 10 NO 9. Did samples arrive in proper containers for each test? YES I ❑ NO 10, Did samples arrive in good condition for each test? YES ID NO 11. Was adequate sample volume availableT YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14, Were cyanide samples received at a pH >12? YE5 ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 w M 2 0 C p U w � aNw LL 0 u N 14 O N G E E d c m 'a /C ry LL V LL to 0 O a. a O Z a T rD 0 n LU Z o CL O C� E a t CO C C. C_ 'ra o IC Q. cc O d C L U t m 0 0 � LtJ Z w � Z ¢O O 0 w I. O U LU w } 0 U 0 Q. m d 7 o w �..� 3 V Z > IL y r o � N a c as U) LLI � o a 0 U W LL. W N �p a! LU y � � O a O U 3 a U) U) a3Hla Z CIHI X 13 O HOVN Q U EONH l!J Lu LEJ 9O5ZH X d,0H 3NON X H3eyynN ai evi E m 'llBw 4 auP0143 {0 JO d) d. C} 0. U' 0. CD 0. C7 0. 0 0. U a- U 0. C7 0- C7 Jauleluag el in U C7 U 0 U D U 0 U U' U C7 U CD U (D U C7 a;jsodwoo adRl aidweg a} a � N 3 C � C � � M 0 U Q M � C O '4 I u Q1 � 4t E m N � o m 16 N c a� E 0 0