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HomeMy WebLinkAboutWQ0019504_Renewal Application_20200901Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0019504 Applicant/Permittee City of Belmont Applicant/Permittee Address PO Box431 Belmont, NC 28012 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name City of Belmont DCAR County Gaston Fee Category Minor Fee Amount 0 Is this a complete application?* r Yes r No Complete App Date 09/01/2020 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * Zach Key Email Address* zachkey@usbiosolids.com electronic subntttal, confirmation of receipt, and other correspondence. Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3369577871 O Modification - Minor G Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00019504 Fbs Current Existing perrrit number Applicant/Permittee * City of Belmont Applicant/Permittee Address* PO Box431 Belmont, NC 28012 Facility Name * City of Belmont DCAR Please provide comments/notes on your current submittal below. This is a permit renewal package for Permit WQ0019504 for the City of Belmont"s Water Treatment Plant. This is for the renewal of the distribution and land application of class A water treatment plant residuals. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) Belmont WTP 2020 Land Application Permit Renewal.pdf 1.84MB Upload only 1 RCFdocurrent (less than 250 W). NLfliple documents rust be corrbined into one RDFfile unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date Is filled inautonaticallyonce subnitted. P4 Box 146 Ronda, NC 28670 336-777-6909 www.usbiosolids.com Tuesday, September 1, 2020 North Carolina Department of Environmental Quality Division of Water Resources Water Quality Permitting Section Non -Discharge Permitting Unit 512 N. Salisbury Street Raleigh, NC 27064 Reference: City of Belmont Water Treatment Plant Permit Renewal WQ0019504 US Biosolids, Inc. is assisting the City of Belmont, NC in preparing this renewal package for its distribution/land application of Alum residuals; Permit No. WQ0019504 from the Water Treatment Plant. There have been no changes in the process or the way the residuals are handled since the last issue of permit WQ0019054. The residuals are stored in a 400,000-gallon concrete clarifier tank till the residuals are distributed through land application. Your attention in the review of this permit renewal application is greatly appreciated. Please contact me with any questions or concerns at zachkey@usbiosolids.com or at 336-957-7871. Sincerely, 3-;.A --� Zach Key US Biosolids, Inc. CITY OF BELMONT WATER TREATMENT PLANT PERMIT RENEWAL PERMIT No. WQ0019504 FOR DISTRIBUTION/LAND APPLICATION OF ALUM RESIDUALS State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T A 100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant_ shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting.4ection's Non -Discharge Permitting Unit website General -- This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T . 1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ❑ Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ The project name should be consistent on the plans, specifications, etc. ❑ The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ if this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification' . ......... ..... . Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage, adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ❑ List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page I of 3 D. Program Information (All Application Packages) ❑ Provide a narrative explaining the following: ❑ How the materials will be handled and transported from where the residuals were produced to where it will be treated. ❑ How the residuals will be processed/treated (attach process flow diagram). ❑ How leachate collection will be handled. ❑ Where the residuals will be stored until processed. ❑ How the final product will be distributed (packaging, bulk, etc.) ❑ What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ❑ Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ❑ Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ❑ Name and address of the person who prepared the residual that is sold or given away. ❑ A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ❑ A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ❑ Information on all applicable setbacks in accordance with 15A NCAC 02T .1 108(b). ❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC. 02T 1 108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1 104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN -- NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 l p4(a}. G. Environmental Assessments (May be Required — See 15A NCAC I C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T . I 110 and include at a minimum: ❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ❑ Maintenance schedules, may include equipments calibration, maintenance of signs, etc. ❑ Safety measures; may include safety training program, manuals, signs, etc. ❑ Spill response plan; including control, containment, remediation, emergency contact information, etc. ❑ Inspection plan including the following information; ❑ Names and titles of personnel responsible for conducting the inspections. ❑ Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ❑ Sampling and monitoring plan including the following information; ❑ Names and titles of personnel responsible for conducting the sampling and monitoring. ❑ Detailed description of monitoring procedures including parameters to be monitored. ❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, Flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: By Courier/Special Delivery: 1617 MAIL SERVICE CENTER 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 807-6464 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06- l6 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 1. APPLICANT INFORMATION: 1. Applicant's name: City of Belmont Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Adrian Miller Title: City Manatrer Applicant's mailing address: PO Box 431_ City: NC Zip: 28012 Telephone number: (704) 825-5586 Email Address: amillerc cityofbelmont.org 2. Consultant's name: Zach Key License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: US Biosolids.lne.) Consultant's mailing address: 958 Hoots Road City: Roaring River State: NC Zip:28669 Telephone number: (336) 957-7871 Email Address: zachkey (_usbiosolids.com 3. Fee submitted: $0.00 (See Instruction B) H. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W 0�4_. 019504 Date of most -recently issued permit: 916.-2015 Date of most -recently certified Attachment A (if different than the permit): 9-16-2015 Ill. FACILITY INFORMATION: I. Name of residuals processing facility: City of Belmont WTP City: Belmont State: NC Zip: 28012 Coordinates: Latitude: 35" 14' 32.35" Longitude: 81' O1' 0O600" Datum: WGS84 Level of accuracy: f0.01 Method of measurement: MAP County where facility is located: Gaston 2. Facility contact (person familiar with residuals preparation): Name: Josue Title: Superintendent Mailing address: PO Box 431 City: Belmont State: NC Zip: 28012 Telephone number: (704) 901-2077 E-mail address: iroy@cityofbelmont.org FORM: DCAR 06-16 Page I of 3 3. Is the residual process facility also the generator? ® Yes: ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 365+days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: I . Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); Given away through land application Note: Sulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added per 1.0 d ton of residuals d ton Not Mixed with other materials 3. Approximate amounts of the residuals received and processed at the facility: 23.21 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 23.3 l dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): 400,000 gallon concrete tank 6. Does the facility have a stormwater management plan? ❑ Yes; ® No Explain whether the treatment and storage areas are under roof or how storm water runoff will be handled: AI I storm water that mixes with the residuals are sent to the WWTP for rocessing V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals .Source Certification and all associated documentation. RSC 06-16.doc I=ORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) Wiest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and bate: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A N A 02T .0 105, ® Yes ❑ No. Explain, I• _ _ AdriAn Miller _ City Manama (Signature Authority's Name — PLEASE PRINT) (Title) _� attest that this application for C .4 of, ""i__ wT (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specificaliv granted in the permit. Further. any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I al$o understand that if all required parts of this application are not completed and that if all rcquired supporting information and attachments arc not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation. or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed 510.000 as well as civiVpenalties up to $25.000 per violation. Signature: r _ Date: FORM: ❑CAR 06-16 Page 3 of City of Belmont Water Treatment Plant The residuals are generated from particles from the treatment of water from the Catawba River. The raw water that is pumped from the Catawba River is added with liquid alum and pre -caustic to bind sediments that are pumped with the raw water from the river. These particles are removed from the water by filters and sent to the clarifier. Once the residuals reach the clarifier, they settle to then bottom of the clarifier by gravity. Once the clarifier is nearing full, a land application/distribution event is planned. The supernatant water is removed from the top of the residuals and sent to the sanitary sewer system before the land application/distribution event. The remaining alum residuals are then pumped out and used as a soil amendment. These residuals are stored at the facility site until distribution. The storage time is greater than 365 days. The distribution is handled by an experienced private contractor, Southern Soil Builders, Inc. The contractor will provide pumps and tanker trucks to the facility on a timely basis. The residuals will be loaded into the tankers from the clarifier and then transported to suitable application sites in the area. Cropland, pasture and hay land are available to receive the material, which is used as a suitable soil amendment. The common limiting factor in the use of this product is commonly the amount of PAN (plant available nitrogen) that the crop on the field can hold. Caution should be used, as the amount of residuals that can be applied before pooling or runoff starts can happen before the maximum amount of nitrogen levels have been reached. Marketability Statement: The product will be given to local landowners who desire the material as a soil amendment. The amount of residuals to be land applied per year is approximately 25 dry tons. These residuals can be beneficial to soils and plants and the improved soil physical properties are the results of the addition of organic matter and plant nutrients. Destinations for these residuals are local landowners and farmers that have. sufficient amount of land to handle a bulk distribution of the alum residuals; a field or combination of fields of around 25 acres are desired. Product Information: Residuals produced from: City of Belmont Water Treatment Plant Mailing Address: P4 Box 4301 Belmont, NC 28012 Facility Address: 205 N Tenth Street Belmont, INC 28012 (704)901-2077 • This product contains plant nutrients such as nitrogen and aluminum and can be used as a soil amendment. This material has been processed in accordance with EPA guidelines. Chemical composition of this product is such that it does not exceed pollutant ceiling concentrations • This material shall not be applied to any site that is: o frozen, snow-covered, or flooded 0 100 feet of any public or private water supply source (including wells) 0 100 feet of surface waters (streams, rivers, wetlands) 0 25 feet of water diversions (ditches) 0 Within a 100-year flood plain unless incorporated within 24 hours 0 During a measurable precipitation event (0.01 inch per hour) or within 24 hours of a rainfall event of 0.5 inches 0 Slope greater than 10% 0 Has a vertical separation of the bedrock less than one foot 0 If vertical separation of seasonal water table is less than one foot 0 Then does not have an established vegetative cover unless incorporated • If soil pH is less than 6.0, lime shall be added to maintain at least 6.0 unless an agronomist provides information indication otherwise • Residual stockpile for more than 14 days shall be covered For current analysis and appropriate loading rates for farmland application, contact: US Biosolids, Inc. 958 Hoots Road Roaring River, NC 28669 Phone (336) 957-7871 zachkey@usbiosolids.con Application of this material to the land is prohibited except in the accordance with the instructions on this label and all applicable setbacks as in accordance with 15A NCAC 2T .1108(b). Use of this material should conform to the recommendations of the current analysis and loading rates. Operation and Maintenance Plan City of Belmont Water Treatment Plant Permit No. WQ0019504 In accordance to the requirements as issued by the North Carolina Department of Environmental and Natural Resources using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T .1 10, the City of Belmont and US Biosolids, Inc. is implementing this Operation and Maintenance Plan, The Class A distribution program from the City of Belmont will be conducted from the Water Treatment facility, located at 205 N Tenth Street Belmont, NC. Residuals will be removed and given away to local farmers to be used as a soil amendment. The residuals will be removed on as needed bases; as fluctuation in the output of the plant will vary with changing economic conditions. The day to day operation of the running of the Water Treatment will be conducted by the City of Belmont. The operations of the distribution program will be conducted by Southern Soil Builders, Inc. A label shall be provided to every recipient of the residual material, in addition to this label, the ORC will make sure every recipient is educated in the proper use of the residuals. Prior to distributing these residuals to local farmers, the following sampling conditions must be met (as is outlined in greater detail in the sampling plan attached to this Operation and Maintenance Plan). Toxicity Characteristics Leaching Procedure (TCLP) will be conducted once per permit cycle. An analysis of the parameters will be conducted annually if a distribution event takes place. A fecal coliform test shall be conducted as required in 15A NCAC 027T .110b chapters (a) and (b) to show that the density of the fecal coliform is less than 1,000 MPN per gram of total solids, each year a distribution event takes place These samples will be collected by the ORC or his/her designee and transported to an approved lab the same day the samples are taken, as in accordance to 15A NCAC 02B .0505. The samples must be taken in a matter to ensure a representative sample of the residuals has been taken. To prevent any spills and or safety issues from occurring the flowing will take place during a distribution event. In the unlikely event of a spill consult the spill control plan immediately. 1. Access to the facility will be controlled with a locked gate and signs to prevent any unauthorized entry into the complex; this gate will be lock at the end of each day. 2. All pumps and hose will be checked at the start of each day for leaks or loose fittings. 3. All tanker valves are closed prior to loading and lids are closed prior to transport. 4. All dump trailers or dump trucks gates are tightly fastened and do not leak prior to transport. 5. All on road equipment is check as per DOT regulations for any safety or mechanical hazards or issues. 6. All equipment is secured at the end of each working day to prevent any tampering or unauthorized use. The fields should be inspected daily by the ORC or the BORC for compliance with the conditions that is outline in then permit. The inspection should consist of (but not limited to): 1. All required set -backs and buffers are in compliance 2. All required record keeping of truck and fields sheets are maintained and properly filled out so accurate records of the volume and locate of residuals are keep. 3. All public access points are controlled (signs posted, gates closed) 4. Make sure all fields are turned over to the ORC and the City of Belmont so records and be reviewed by NCDEQ and an annual report can be constructed. If any issues or violations are discovered, the ORC, Belmont Water Treatment Plant and the Mooresville Regional Office should be contacted as soon as safely possible. SPILL CONTROL PLAN- US BiosoIids Inc. CITY OF BELMONT-WATER TREATMENT PLANT In the event of a spill, the following should be taken IMMEDITALY. 1. Make sure all personal and bystanders are safe; if not, contact emergency services without delay. 2. Halt the source of the spill- overturned truck, leaking valve, ruptured tank, 3. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill. 4. Cleanup. Employ vacuum trucks, dump trucks, and loaders to remove as much of the spilled material as possible. Use straw to soak -up the remaining material. Dispose of the same in a landfill. 5. Flush the roadways with water if needed. If the spill occurred on a tillable area, till the same into the soil and spread lime if necessary. If a spill occurs on private property, final clean-up should be to the satisfaction of the owner. 6. Notification. (This should be done as soon as safely possible.) US Biosolids, Inc. Main Office (336) 777-6909 City of Belmont Water Treatment Plant (704) 901-2077 NCDEQ, Mooresville Regional Office (704) 663-1699 County/City Emergency Services (Sheriff, Fire Dept.) 911 7. Reporting. The project manager shall detail how the spill occurred and all action that was taken. A written report shall be given to the Asheville regional office as soon as possible, and within 24 hours of the spill, or next working day. 8. Spill Prevention. The easiest way to clean a spill is to prevent one. A. Ensure loading personal watch the vehicle being loaded. B. Ensure all valves and lids are closed. C. Inspect all seals and replace if necessary. State of North Carolina DWK Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supportin2 documentation For more information, visit the Water Quality Permitting Section's Non-Dischar e Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 1 l-I5, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC I I-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: ❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Ma,p_Gui_dan,ce_for Residuals Land, Application Pen -pits". ❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06- l6 Page I of I Dlvlslon of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): I. Facility Name: City of Belmont Water Treatment Plant 2. Facility permit holder is: ❑' Federal, ❑ State, tR Local Government, or ❑ Private. Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Joseph Roy, Superintendent Complete mailing address: PO Box 431 City: Belmont State: NC Zip: 28012 Telephone number: (704) 901-2077 E-mail address: Troy@cityofbelmontorg 4. Facility physical address: 205 N 1011 Street City: Belmont State: NC Zip: 28012 Coordinates: Latitude: 350 14' 32.35" Longitude: 81 ° 01' 06.00" Datum: WGS84 Level of accuracy: 0.01 Method of measurement: MAP 5. Purpose of the facility: [] treatment of municipal wastewater, 0 treatment of 100% domestic wastewater, . treatment of potable water, 0 treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes No 7. Facility permitted/design flow: 10 MGD and facility average daily flow: 2 MGD 8. Average amount of residuals being generated at this facility 14.66 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 400,000 gal [on concrete tank Type and volume of residuals storage (i.e., outside of residuals treatment units): 11. RESIDUALS QUALITY INFORMATION (See Instruction C.): I . Specify if residuals are regulated under: El 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1 102(6) as: El Biological [@ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: City of Belmont WTP € Status Maximum Dry Tons Per Year Facility Permit Holder Facility Name County Permit Number Code" Current a Proposed R City of Belmont City of Belmont WTP Gaston WQ0019504 200 200 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) s The amount of residuals currently permitted for distribution. land application. or disposal (i.e. not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ❑ no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: El yes Q no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 03-14-2016 Passed corrosivity test: 0 yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: M yes ❑ no. Flashpoint: 183 OF (> 140°F) Passed reactivity test: 0 yes Ono. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/0 Result (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 NDN o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND IJ-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0,008 NDN Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 7-25-2016 Parameter Ceiling Concentration Limits (ClossA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 10 Cadmium 85 39 2 Copper 4,300 1,500 49 Lead 840 300 14 Mercury 57 17 0.4 Molybdenum 75 n/a 5 Nickel 420 420 14 Selenium 100 100 5 Zinc 7,500 2,800 102 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/k9d Nickel (mg/kg) [] > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 [] > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 0.87 %. b. Fill in the following table with the results of the latest analyses (i.e... on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint AnaE tical and Date of analysis: 7-25-2016 Parameter Result (mg/kg) Aluminum 119000 Ammonia -Nitrogen 10300 Calcium 1410 Magnesium 800 Nitrate -Nitrite Nitrogen 2 pH (Standard Unit) 6.39 Phosphorus 2170 Potassium 1450 Sodium 328 Total Kjeldahl Nitrogen 28700 c. Using the results listed in [tern II. 5b. above, calculate the sodium adsorption ration (SAR): 0.11 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): E default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Default for Alum Residuals e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN ("mg/kgj (mg/kg) Surface 12512 13387 Injection/Incorporation 17662 18898 6. Other Pollutants Determ ination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Patho2en Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: El A fecal coliform density that is demonstrated to be less than 1,000 MPN per grate of total dry solids, or ❑ A salmonella sp, density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): 0 Alternative 1 [ 15A NCAC 02T. 1106(b)(3)(A)] - Time/Temperature Compliance. 0 Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)] -Alkaline Treatment. ❑ Alternative 3 (15A NCAC 02T.1 106(b)(3)(C)] -Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.1 I06(b)(3)(D)] -No Prior Testing for Enteric Virus/Viable Helm inth Ova. El Alternative 5 [15A NCAC 02T.1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, [] heat drying, ❑ heat treatment, thermophilic aerobic digestion, ❑ beta ray irradiation, [] gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: El Alternative I [15A NCAC 02T.] 106(c)(1)] - Fecal Coliform Density Demonstration. [] Alternative 2 j 15A NCAC 02T.1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion ❑ air drying, ❑ anaerobic digestion, composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [ 15A NCAC 02T.1 106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: El Alternative I [15A NCAC 02T. 1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T. 1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T. 1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ED Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.1 107(a)(10)] - Incorporation. rl Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1 107(b)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: for animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 J a 4� t= =i Q X Q � U C c O E aj m +� v Cam!] a O 00 N V Z +r o O � V L *' c� ?> Z No O E m 0 N_ C [G Q. m A m � 7 CD CD I V U J]DL Q U U C7 C7 0 {6 a � o o m c m JC m U O r LL m m m c m m 7 W m 4 � c n io o o m a - E o m c LL cy m .100 E W U m r U W ;%1 0 m U O. Q v m J a r 0 = m m a V C b vi mm m J b O � W L ai 0 GU o x a E �o n m E Em = = a � m `m L ,c Co o w- U a m � ID C CD LL U C 'rJ cn m 8.0 OO O n a, my 3 � om n T m m E c� m �y c � o 3 m 0 m LL a 0 Quantitative Justification for Residuals Production Rate: In the 7 years since the last permit was issued, the City of Belmont Water Treatment Plant has produced 14.66 Dry Tons per year. This is less than the 200 dry tons currently allowed by permit WQ0019504, This will allow any growth that the Water Treatment Plant may occur during the next permit cycle. CITY OF BELMONT WTP SAMPLING PLAN Annually, if a distribution event occurs, grab samples are collected from the clarifier. Samples from the clarifier will be combined to form individual grab samples to be sent to a laboratory for analysis. If a distribution event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for fecal coliform analysis, nutrient analysis, and a TCLP test. These tests will be taken by Zach Key of US Biosolids, Inc. All samples apart from the composite residual sample will be taken to Statesville Analytical, the composite residual sample will be sent to Waypoint Laboratory. All samples taken will be taken in the same condition as the residuals are to be land applied. Fecal Coliform is gathered in seven (7) individual samples and tested to meet the requirements of [503.32(b)(2)j. This requirement is for the geometric mean fecal coliform density of the samples be less than one thousand (1,000) MPN per gram. These samples will be placed in 250ml containers and placed on ice, in a cooler for transport to the laboratory before 1600 hours (4pm) the same day the samples are obtained. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, %total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will be collected in a non -breakable container, at least one quart in size. This sample will be taken from the clarifier. A Toxicity Characteristics Leaching Procedure (TCLP) test with ignitability, reactivity, and corrosivity will be collected in two separate, one gallons jugs. This test will be conducted on a frequency as outlined in the permit. Page: i of 2 Report Number: 16-210-0203 Account Number: 46381 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743.9401 ° FaK 804-271-6446 ANALYTICAL www.waypointanalytical.corn Send To: Southern Soil Builders Project : Belmont WTP Dennis Key NC Cert##257 958 Hoots Road Roaring River. NC 28669 REPORT OF ANALYSIS Date Sampled: 7/25/2016 13:56:00 Lab Number : 58594 Date Received: 07/28/2016 00:00 Sample Id : Belmont WTP Date Reported: 08/05/2016 Total Solids * 0.87 8700 1010 JM 07/28/2016 1,929 SM-2540G Moisture " 99.13 100.0 JM 07/28/2016 15 29 SM-254OG Total Kjeldahl Nitrogen 2.87 28700 10.0 JM 08/04/2016 10:55 SM-4500-NH3C-TKN Total Phosphorus 0.22 2170 100 KM 07/29/2016 13:00 SW 6010C Total Potassium 0.15 1450 100 KM 07/29/2016 13:00 SW 6010C Total Sulfur 0.69 6930 100 KM 07/29/2016 13:00 SW 6010C Total Calcium 0.14 1410 100 KM 07/29/2016 13:00 SW 6010C Total Magnesium 0.23 2260 100 KM 07/29/2016 13:00 SW 6010C Total Sodium 0.03 328 100 KM 07/29/2016 13:00 SW 6010C Total Iron 28500 100 KM 07/29/2016 13:00 SW 6010C Total Aluminum 119000 100 KM 07/29/2016 13:00 SW 6010C Total Manganese 800 5 KM 07/29/2016 13:00 SW 6010C Total Copper 49 5 KM 07/29/2016 13:00 SW 6010C Total Zinc 102 5 KM 07/29/2016 13:00 SW 6010C Ammonia Nitrogen 1.03 10300 10.0 JM 07/29/2016 08.30 SM-4500-NH3C Organic N 1.84 18400 0.001 JM 08/05/2016 08:40 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 07/29/2016 09:00 SM-450ONO3F All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9OW reports anu :et:er; am 70; ?: ie e­4;usrve ana contiderrtral use of uur CueuiS. and may not be repiooucea tit wbote or part, nor may any reference be made /idft�l to the work the results, or the company in any advertising, nears refeaze or other public announcements without obtaining our pnor vrmten aidhonzahon Debbie Holt Laboratory Supervisor Page: 2 of 2 Report Number: 16-210-0203 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number: 58594 Sample Id : Belmont WTP Waypoint(2) ANALYTICAL Project: Belmont WTP NC Cert#257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/25/2016 13:56:00 Date Received: 07/28/2016 00:00 Date Reported: 08/05/2016 Total Cadmium <2.0 2.0 KM 07/29/2016 13:00 SW 6010C Total Chromium 105 5 KM 07/29/2016 13:00 SW 6010C Total Nickel 14 5 KM 07/29/2016 13:00 SW 6010C Total Lead 14 5 KM 07/29/2016 13:00 SW 6010C Total Arsenic 10.0 3.0 KM 07/29/2016 13:00 SW 6010C Total Mercury <0.4 0.4 KKM 08/02/2016 15:30 SW-7471B Total Selenium <5.0 5.0 KM 07/29/2016 13:00 SW 6010C pH (Standard Units) * 6.39 2.00 JM 07/29/2016 09:00 SW-9045D Total Molybdenum <5 5 KM 07/29/2016 13:00 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Na". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "P", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exc usfoe and conlidenlial use of our clientsand may not be reproduced in Whole or part, nor may any reference be made to the cork. the results, or the company in any advertising. news release or other public announcements without oblaining our prior written authorization Debbie Holt Laboratory Supervisor PAN Mineralization as decimal ITotal dry tons/year Acres Applied on 1 25.7 Rate 0.4 TKN NH3 28700 10300 NO3 2 NO2 0 % Solids 0.0087 1 12.73 PAN Surface 125121mg1kg 25.024 lbs/dry ton 318.5555 Ibs total PAN 12.39516 lbs PAN/acre PAN Injection 176621mg/kg 1 35.324 lbs/dry ton 449.6745 Ibs total PAN 17.49706 Ibs PAN/acre Dry Tonsl1000 gal. 0.036279 1st year PAN Surface Ibs. 318.55552 1st year PAN Injected Ibs. Ibs.lacre Surface 12.39515fi42 Ibs.lacre Injected 17.49708304 MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 mg/kg x .002 MR(TKN-NH3) + 1(NH3)+NO3+NO2 mg/kg x .002 =mglkg =lbsldry ton =mglkg =lbsldry ton 1000 X 8.34 X %solids X sp. gravi "=dry tons/ 1000gai." 2000 Sodium Absorption Ratio Na(Mg/L) Ca(MgIL) Ma{Mg/L1 Na: Sodium (MgIL) Equivalent weight: 23 2.85 1 12.26 19.66 Ca., Calcium (MgIL) Equivalent weight: 20 Mg : Magnesium (MgJL) Equivalent weight: 12 Na (ME) Ca (ME) 1 Mg (ME) 0.123913 0 613 1 638333 Milli Equivalent = MgIL 1 Equivalent weight The amour amount of E SAR= Na Milli Equivalentl[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power Permitting � SAR = 0.116792 (From MgJL entered above) SAR= 0 113137 (From ME entered below) Na (ME) 1 Ca (ME) 1 Mg (ME) 0.12 0.61 1.64 laceAnalyticais I wwwpacelabs.com Project: 160314-15-08 Pace Project No.: 92290089 Sample: 160314-15-08 Parameters 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Arodor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Arodor 1248) PCB-1254 (Arodor 1254) PCB-1260 (Arodor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury 8270 MSSV TCLP Sep Funnel 1,4-Di chlorobenzene 2,4-Dinitrotoluene Date: 03/29/2016 04:40 PM Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92290089001 Collected: 03/14/16 11:15 Received: 03/15/16 10:00 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 0312611614:00 ND ug/L 1.0 1 03/28/1612:50 03/28/1619:13 58-89-9 ND ug/L 6.0 1 03/28/1612:50 03128/1619:13 57-74-9 NO ug/L 1.0 1 03/28/1612:50 03128/1619:13 72-20-8 ND ug/L 1.0 1 03/28/1612:50 03/28/1619:13 1024-57-3 NO ug/L 2000 1 03/28/1612:50 03/28/1619:13 72-43-5 NO ug/L 6.0 1 03128/1612:50 03/28/1619:13 8001-35-2 51 % 10-138 1 0312811612:50 03/28/1619:13 2051-24-3 215 % 10-110 1 0312811612:50 03/28/1619:13 877-09-8 S5 Analytical Method: EPA 8082 Preparation Method: EPA 3510 NO ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 12674-11-2 NO ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 11104-28-2 ND ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 11141-16-5 NO ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 53469-21-9 ND ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 12672-29-6 ND ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 11097-69-1 ND ug/L 5.0 1 03/18/16 09:07 03/18/16 20:47 11096-82-5 16 % 10-132 1 03/18/16 09:07 03/18/16 20:47 2051-24-3 Analytical Method: EPA 8151 Preparation Method: EPA 3510 ND mg/L 0.010 1 03/24/16 12:55 03/26/16 01:27 94-75-7 ND mg1L 0.010 1 03/24/16 12:55 03/26/16 01:27 93-72-1 95 % 42-142 1 03/24/16 12:55 03/26/16 01:27 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 03/22/16 0100 Initial pH: 6.7; Final pH: 5 NO mg/L 0.050 1 03/23/16 03:00 03/23/16 14:00 7440-38-2 ND mg/L 0.25 1 03/23/16 03:00 03/23/16 14:00 7440-39-3 ND mglL 0.0050 1 03/23116 03:00 03/23/16 14:00 7440-43-9 ND mg1L 0.025 1 03/23/16 03:00 03/23/16 14:00 7440-47-3 ND mg/L 0.025 1 03/23/16 03:00 03/23/16 14:00 7439-92-1 ND mglL 0.10 1 03/23/16 03:00 03/23/16 14:00 7782-49-2 ND mg/L 0.025 1 03/23/16 03:00 03/23/16 14:00 7440-22-4 Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 03/22/16 03:00 Initial pH: 6.7, Final pH: 5 NO mg/L 0.00020 1 03/23/1611:00 03/23/1614:17 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate MethodlDate: EPA 1311; 03/26/16 14:00 NO ug/L 500 10 03128/1611:25 03/29/1611:25 106-46-7 ND ug/L 500 10 03/28/1611:25 03/29/1611:25 121-14-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: 160314-15-08 Pace Project No.: 92290089 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersviile, NC 28078 (704)875-9092 Sample: 160314-15-08 Parameters Lab IQ: 92290089001 Results Units Collected: 03/14/16 11:15 Report Limit DF Received: 03/15/16 10:00 Matrix: Water Prepared Analyzed GAS No. Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 03/26/16 14:00 Hexachloro-1,3-butadiene ND ug/L 500 10 03/28/16 11:25 03129/1611:25 87-68-3 Hexachlorobenzene ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 118-74-1 Hexachloroethane ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 Nitrobenzene ND ug/L 500 10 03128/1611:25 03/2911611:25 98-95-3 Pentachlorophenol ND ug/L 1000 10 03/28/16 11:25 03129/1611:25 87-86-5 Pyridine ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 110-86-1 2,4,5-Trichlorophenol ND ug/L 500 10 03/28/16 11:25 03/29/16 11:25 95-95-4 2,4,6-Trichlorophenol ND ug/L 500 10 03/28/16 11:25 03/29/16 11 :25 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 12-102 10 03/28/16 11:25 03/29/16 11:25 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 13-107 10 03/28/16 11:25 03/29/16 11:25 321-60-8 S4 Terphenyl-d14 (S) 0 % 21-132 10 03/28/16 11:25 03/29/16 11:25 1718-51-0 S4 Phenol-d6 (S) 0 % 10-110 10 03/28/16 11:25 03/29/16 11:25 13127-88-3 S4 2-Fluorophenol (S) 0 % 10-110 10 03/28/16 11:25 03/29/16 11:25 367-12-4 S4 2,4,6-Tribromophenol (S) 0 % 27-108 10 03/28/16 11:25 03/29/16 11:25 118-79-6 S4 8260 MSV TCLP Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 03/16/16 10A2 Benzene ND ug/L 100 20 03/22/16 00:48 71-43-2 2-Butanone (MEK) ND ug/L 200 20 03/22/16 00:48 78-93-3 Carbon tetrachloride ND ug/L 100 20 03/22/16 00:48 56-23-5 Chlorobenzene ND ug/L 100 20 03/22/16 00:48 108-90-7 Chloroform ND ug/L 100 20 03/22/16 00:48 67-66-3 1,4-Dichlorobenzene ND ug/L 100 20 03/22/16 00:48 106-46-7 1,2-Dichloroethane ND ug/L 100 20 03/22/16 00:48 107-06-2 1,1-Dichloroethene ND ug/L 100 20 03/22/16 00:48 75-35-4 Tetrachloroethene ND ug/L 100 20 03/22/16 00:48 127-18-4 Trichloroethene ND ug/L 100 20 03/22/16 00:48 79-01-6 Vinyl chloride ND ug/L 100 20 03/22/16 00:48 75-01-4 Surrogates 1,2-Dichloroethane-d4(S) 100 % 70-130 20 0312211600:48 17060-07-0 Toluene-d8 (S) 101 % 67-135 20 03/22/16 00:48 2037-26-5 4-Bromofluorobenzene (S) 101 % 70-130 20 03/22/16 00:48 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 96.6 % 0.10 1 03/24/16 11:39 1010 Flash point,Closed Cup Analytical Method: EPA 1010 Flashpoint 183 deg F 70.0 1 03/27/16 12:15 9D45 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 5.8 Std. Units 0.10 1 03/18/16 14:35 H6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2016 04:40 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 aceAnalXical r xnvw.Pacelebs.crom ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 160314-15-08 Pace Project No.: 92290089 Sample: 160314-15-08 Lab ID: 92290089001 Collected: 03/14/16 11:15 Received: 03/15/16 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9095 Paint Filter Liquid Test Analytical Method: EPA 9095 Free Liquids FAIL 1.0 1 03/17/16 14:40 733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/L 0.010 1 03/21/16 21:04 734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/L 1.0 1 03/21/16 18:20 Date: 03/29/2016 04:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 27