HomeMy WebLinkAboutNCG030427_DMR_20191022Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 SAMPLE COLLECTION YEAR Zv/y
FACILITY NAME GKN Driveline SAMPLE PERIOD Q Jan -June Q July -Dec
COUNTY Alamance or r-� Monthly' (month)
PERSON COLLECTING SAMPLES Ricky Hiatt DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY Pace Analytical Lab Cert. # 12,40 R-EGEIVED ❑Zero -flow ❑Water Supply ❑SA
_
Comments on sample collection or analysis: MAR 10 2020 ❑Other
CENTRAL FILES
DVVR SECTIGN
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 —>
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks
_
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
0,10
3 ,/ ,� 1�
S:'
u,vor"l`
��,��s�;
v v��I��/
i►� ��/�
N�
Vvl lLlolJ 2—
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormmw�ate/r PollutionPrevention Plan."
/�/, /i,/ //' �
Name (Print name)
'ro C, , - /--
Title (Print tit e)
Sl nature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period ?2
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L°
Parameter Code
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
® A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
® 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
® TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES Q NO
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES E]NO 0
REGIONAL OFFICE CONTACT NAME:
Mail an original copv of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signatdre of Permittee
Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3
aceAnalytical
www.pacelabs.com
November 06, 2019
Ricky Hiatt
GKN Driveline
1067 Trollingwood Hawfield Rd.
Mebane, NC 27302
RE: Project: Monthly Stormwater
Pace Project No.: 92450868
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Dear Ricky Hiatt:
Enclosed are the analytical results for sample(s) received by the laboratory on October 23, 2019.
This report is a summary of the results based upon our understanding of your data quality objectives.
Please contact us if itemized quality control results are needed. These results relate only to the
samples included in this report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Dave Bruce, GKN Driveline
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 13
aceAnalytical
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Project: Monthly Stormwater
Pace Project No.: 92450868
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13
aceAnalXical
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
Pace Project No.:
Monthly Stormwater
92450868
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92450868001
Outfall 001
EPA 1664B
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
GAW
34
PASI-C
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
92450868002
Outfall 002
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
GAW
34
PASI-C
SM 2540D-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
EPA 420.4 Rev 1.0 1993
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13
Pace Analytical Services, LLC
aceAnalXical 9800 KineyAveSuite 100
Huntersville, NC 28078078
www.pacelabs.com
(704)875-9092
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 001
Lab ID: 92450868001
Collected: 10/22/19 14:25
Parameters
Results
Units
Report Limit
DF Qualifiers
Oil and Grease
11.3
mg/L
5.0
1
Aldrin
ND
ug/L
0.050
1
alpha-BHC
ND
ug/L
0.050
1
beta-BHC
ND
ug/L
0.050
1
delta-BHC
ND
ug/L
0,050
1
gamma-BHC (Lindane)
ND
ug/L
0.050
1
Chlordane (Technical)
ND
ug/L
0.50
1
alpha -Chlordane
ND
ug/L
0.050
1
gamma -Chlordane
ND
ug/L
0.050
1
4,4'-DDD
ND
ug/L
0.050
1
4,4'-DDE
ND
ug/L
0.050
1
4,4'-DDT
ND
ug/L
0.050
1
Dieldrin
ND
ug/L
0.050
1
Endosulfan I
ND
ug/L
0.050
1
Endosulfan II
ND
ug/L
0.050
1
Endosulfan sulfate
ND
ug/L
0.050
1
Endrin
ND
ug/L
0.050
1
Endrin aldehyde
ND
ug/L
0.050
1
Heptachlor
ND
ug/L
0.050
1
Heptachlor epoxide
ND
ug/L
0.050
1
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
Toxaphene
ND
ug/L
0.50
1
Tetrachloro-m-xylene (S)
71
%
10-130
1
Decachlorobiphenyl (S)
52
%
10-130
1
Copper
5.9
ug/L
5.0
1
Lead
ND
ug/L
5.0
1
Zinc
84.5
ug/L
10.0
1
Acenaphthene
ND
ug/L
5.0
1
Acenaphthylene
ND
ug/L
5.0
1
Anthracene
ND
ug/L
5.0
1
Benzo(a)anthracene
ND
ug/L
5.0
1
Benzo(a)pyrene
ND
ug/L
5.0
1
Benzo(b)fluoranthene
ND
ug/L
5.0
1
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
Benzo(k)fluoranthene
ND
ug/L
5.0
1
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
Butylbenzylphthalate
ND
ug/L
5.0
1
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
2-Chloronaphthalene
ND
ug/L
5.0
1 L2
2-Chlorophenol
ND
ug/L
5.0
1
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
Date: 11 /06/2019 05:10 PM
without the written consent of Pace Analytical Services, LLC. Page 4 of 13
1�;a'ceAnalytical"
www.pacelabs.com
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 001
Parameters
Lab ID: 92450868001
Results Units
Collected: 10/22/19 14:25
Report Limit DF
Chrysene
ND
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
ND
ug/L
5.0
1
Diethylphthalate
ND
ug/L
5.0
1
2,4-Dimethylphenol
ND
ug/L
10.0
1
Dimethylphthalate
ND
ug/L
5.0
1
Di-n-butylphthalate
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
2,4-Dinitrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
ND
ug/L
5.0
1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
Di-n-octylphthalate
ND
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
Fluoranthene
ND
ug/L
5.0
1
Fluorene
ND
ug/L
5.0
1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
Hexachloroethane
ND
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
Isophorone
ND
ug/L
10.0
1
Naphthalene
ND
ug/L
5.0
1
Nitrobenzene
ND
ug/L
5.0
1
2-Nitrophenol
ND
ug/L
5.0
1
4-Nitrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
Pentachlorophenol
ND
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
ND
ug/L
5.0
1
Pyrene
ND
ug/L
5.0
1
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5 (S)
41
%
10-120
1
2-Fluorobiphenyl (S)
37
%
15-120
1
Terphenyl-d14 (S)
43
%
11-131
1
Phenol-d6 (S)
22
%
10-120
1
2-Fluorophenol (S)
17
%
10-120
1
2,4,6-Tribromophenol (S)
25
%
10-137
1
Benzene
ND
ug/L
1.0
1
Bromodichloromethane
ND
ug/L
2.0
1
Bromoform
ND
ug/L
2.0
1
Bromomethane
ND
ug/L
2.0
1
Carbon tetrachloride
ND
ug/L
2.0
1
Chlorobenzene
ND
ug/L
2.0
1
Chloroethane
ND
ug/L
2.0
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2019 05:10 PM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 5 of 13
1�;a'ce Analytical
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 001
Parameters
Lab ID: 92450868001
Results Units
Collected: 10/22/19 14:25
Report Limit DF
Chloroform
ND
ug/L
2.0
1
Chloromethane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
1,2-Dichloroethane
ND
ug/L
2.0
1
1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
1,2-Dichloropropane
ND
ug/L
2.0
1
cis- 1,3-Dichloropropene
ND
ug/L
2.0
1
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
Ethylbenzene
ND
ug/L
1.0
1
Methylene Chloride
ND
ug/L
2.0
1
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
Tetrachloroethene
ND
ug/L
2.0
1
Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
1,12-Trichloroethane
ND
ug/L
2.0
1
Trichloroethene
ND
ug/L
2.0
1
Trichlorofluoromethane
ND
ug/L
2.0
1
Vinyl chloride
ND
ug/L
2.0
1
4-Bromofluorobenzene (S)
102
%
70-130
1
Toluene-d8 (S)
102
%
70-130
1
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
Total Suspended Solids
3.4
mg/L
2.5
1
pH at 25 Degrees C
5.9
Std. Units
0.10
1
Phenol
ND
mg/L
0.020
1
Date: 11/06/2019 05:10 PM
HS
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 6 of 13
aceAnalytical
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 002
Parameters
Lab ID: 92450868002
Results Units
Collected: 10/22/19 14:35
Report Limit DF
Oil and Grease
ND
mg/L
5.0
1
Aldrin
ND
ug/L
0.050
1
alpha-BHC
ND
ug/L
0.050
1
beta-BHC
ND
ug/L
0.050
1
delta-BHC
ND
ug/L
0.050
1
gamma-BHC (Lindane)
ND
ug/L
0.050
1
Chlordane (Technical)
ND
ug/L
0.50
1
alpha -Chlordane
ND
ug/L
0.050
1
gamma -Chlordane
ND
ug/L
0.050
1
4,4'-DDD
ND
ug/L
0.050
1
4,4'-DDE
ND
ug/L
0.050
1
4,4'-DDT
ND
ug/L
0.050
1
Dieldrin
ND
ug/L
0.050
1
Endosulfan 1
0.070
ug/L
0.050
1
Endosulfan II
ND
ug/L
0.050
1
Endosulfan sulfate
ND
ug/L
0.050
1
Endrin
ND
ug/L
0.050
1
Endrin aldehyde
ND
ug/L
0.050
1
Heptachlor
ND
ug/L
0.050
1
Heptachlor epoxide
ND
ug/L
0.050
1
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
Toxaphene
ND
ug/L
0.50
1
Tetrachloro-m-xylene (S)
64
%
10-130
1
Decachlorobiphenyl (S)
50
%
10-130
1
Copper
5.9
ug/L
5.0
1
Lead
ND
ug/L
5.0
1
Zinc
41.8
ug/L
10.0
1
Acenaphthene
ND
ug/L
5.0
1
Acenaphthylene
ND
ug/L
5.0
1
Anthracene
ND
ug/L
5.0
1
Benzo(a)anthracene
ND
ug/L
5.0
1
Benzo(a)pyrene
ND
ug/L
5.0
1
Benzo(b)fluoranthene
ND
ug/L
5.0
1
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
Benzo(k)fluoranthene
ND
ug/L
5.0
1
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
Butylbenzylphthalate
ND
ug/L
5.0
1
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
2-Chloronaphthalene
ND
ug/L
5.0
1 L2
2-Chlorophenol
ND
ug/L
5.0
1
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /06/2019 05:10 PM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 7 of 13
aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 002
Lab ID: 92450868002
Collected: 10/22/19 14:35
Parameters
Results
Units
Report Limit
DF
Chrysene
ND
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
ND
ug/L
5.0
1
Diethylphthalate
ND
ug/L
5.0
1
2,4-Dimethylphenol
ND
ug/L
10.0
1
Dimethylphthalate
ND
ug/L
5.0
1
Di-n-butylphthalate
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
2,4-Dinitrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
ND
ug/L
5.0
1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
Di-n-octylphthalate
ND
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
Fluoranthene
ND
ug/L
5.0
1
Fluorene
ND
ug/L
5.0
1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
Hexachloroethane
ND
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
Isophorone
ND
ug/L
10.0
1
Naphthalene
ND
ug/L
5.0
1
Nitrobenzene
ND
ug/L
5.0
1
2-Nitrophenol
ND
ug/L
5.0
1
4-Nitrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
Pentachlorophenol
ND
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
ND
ug/L
5.0
1
Pyrene
ND
ug/L
5.0
1
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5 (S)
36
%
10-120
1
2-Fluorobiphenyl (S)
33
%
15-120
1
Terphenyl-d14 (S)
40
%
11-131
1
Phenol-d6 (S)
14
%
10-120
1
2-Fluorophenol (S)
6
%
10-120
1 SO
2,4,6-Tribromophenol (S)
12
%
10-137
1
Benzene
ND
ug/L
1.0
1
Bromodichloromethane
ND
ug/L
2.0
1
Bromoform
ND
ug/L
2.0
1
Bromomethane
ND
ug/L
2.0
1
Carbon tetrachloride
ND
ug/L
2.0
1
Chlorobenzene
ND
ug/L
2.0
1
Chloroethane
ND
ug/L
2.0
1
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Date: 11/06/2019 05:10 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13
aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92450868
Sample: Outfall 002
Lab ID: 92450868002
Collected: 10/22/19 14:35
Parameters
Results
Units
Report Limit
DF
Chloroform
ND
ug/L
2.0
1
Chloromethane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
1,2-Dichloroethane
ND
ug/L
2.0
1
1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
1,2-Dichloropropane
ND
ug/L
2.0
1
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
Ethylbenzene
ND
ug/L
1.0
1
Methylene Chloride
ND
ug/L
2.0
1
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
Tetrachloroethene
ND
ug/L
2.0
1
Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
1,1,2-Trichloroethane
ND
ug/L
2.0
1
Tdchloroethene
ND
ug/L
2.0
1
Trichlorofluoromethane
ND
ug/L
2.0
1
Vinyl chloride
ND
ug/L
2.0
1
4-Bromofluorobenzene (S)
100
%
70-130
1
Toluene-d8 (S)
103
%
70-130
1
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
Total Suspended Solids
6.3
mg/L
2.5
1
pH at 25 Degrees C
6.0
Std. Units
0.10
1
Phenol
ND
mg/L
0.020
1
Date: 11/06/2019 05:10 PM
HS
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 9 of 13
aceAnalytical
—pace/abs.00m
I
QUALIFIERS
Project: Monthly Stormwater
Pace Project No.: 92450868
I�]�yI;IrIC7:69
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
IS-1 7_yt017:71_:9
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
HS Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/06/2019 05:10 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13
Document Name:
Document Revised: February 7, 2018
v
aceAnalytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Client Name:
❑ Commercial ❑Pace ❑Other:
Custody Seat Present? ❑Yes ❑No Sealslntact? (—]Yes
Huntersville 11 Raleigh[] Mechanicsville❑
Project#: � W0# : 92450868
Client II 1 IIU I11 11111 II 1 it 111
92450868
[—]No /
Date/initials Person Examining Contents: � 10— 6 T-
Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No ❑N/A
❑IR Gun ID: 92TO49 Type of Ice: []Wet ❑Blue []None
Cooler Temp ('C): Correction Factor: Add/Subtract (°C) 0.0
Temp should be above freezing to 6°C
Cooler Temp Corrected (*C): / []Samples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Boll (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States. CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
M.— I- — inrludino Hawaii and PuPrin Rirnl? MYes MNo
Comm ents/Discrepan :
Chain of Custody Present?
❑Yes
No
❑N/A
1.
Samples Arrived within Hold Time?
❑Yes
ONO
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
I]No
Q N/A
3.
Rush Turn Around Time Requested?
Yes
ONO
❑N/A
4.
Sufficient volume? _
(3Ves
❑No
N/A
S.
6.
Correct Containers Used? (ayes ONO ❑N/A
-Pace Containers Used? Oyes ONO ❑N/A
Containers Intact?
[fYes
ONO
❑N/A
7.
Dissolved znalysis: Samples Nei,, riltered?
❑Yes
No
❑N/A
g.
Sample Labels Match COC?
-Ltc'udes Date/Time/10/Analysis Matrix:
❑Yes
ONO
[-]N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
ONO
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
OYes
ONO
ONO
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes [:]No
I
✓ JL �� 1 t
r I
°.vtfn-���.� ['lc•t�. � cL Inr�;�•'s/��-�° r,^ v,��c� C. f •<. _)�,. n, � er.�� (.,
-- -- . ............ --- _ _ _
f 41-C 1 Lot 10 of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: L. Ira, Date/Time: (C.'
Project Manager SCURF Review: 1 Date: lC' LI I
Project Manager SRF Review: f�. Date:
C ,
e 11 of 13
Document name.
Document Revised: February 7, 2018
,� aceAnalyticaj
Sample Condition Upon RecelptlSCUR)
Page 1 of 2
Document No.:
Issuing Authority:
j
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box Is to list number of bottle
Project # r WO # : 92450868
PM: IM
CLIENT: 92-GKN
t
Due Date: 11/06/19
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date p •r.servation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there is a discrepancy artecnng Norm caroma COMP nanie,dIr)P;", a wNy U. uu� U�,,,
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 12 of 13
f"? CHAIN -OF -CUSTODY / Analytical Request Document
Parek.alyfrar
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Pa e : 1 Of
Company GKN Dnvehne- Al...an- Report 10. Ricky Hutt Alteniton.
Address 1007 T-lli--odd Hnwlmlds Rd Copy To Companv Nnm.:
Mebane, NC 27302
--_
Addmsl
Rcoulatory Ane.-y
[mall
Purchase Older 1:
Pace OUOte
Phn�c (y19J215-1 C05 Fa.
Project Name. Monthly Sformvwer
Pace Project Manener nvwtim Dranard(nlpaeelabs corn
Stale I Location
Roqu.e:fitl Due Date.
Project #-
Pace Profile p A804.`.
NC
Requested
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ADDITIONAL COMMENTS
RELINQUISHED BY IAFFILIATION
DATE
TIME
ACCEPT Y I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
SAMPLER NAME AND SIGNATURE
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