WQ0000020_Monitoring (Report)_20200817

& DUKE
'r° ENERGY
May 22, 2020
NCDEQ Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
RE:
Duke Energy Progress, LLC. Permit WQ0000020, Asheville Airport Fills
April 2020 Groundwater and Surface Water Analytical Results
Dear Sir or Madam:
410 S. Wilmington Street.
Raleigh, NC 27601
Mailing Address
Mail Code NC 15
Raleigh, NC 27601
MENVED
NCDEQ/IIWR
17 AUG 2020
Non -Discharge
Permitting Unit
Attached are the results from the most recent semi-annual groundwater monitoring sampling event
conducted in April 2020 for the wells near the Area I, III and IV structural fills at the Asheville Regional
Airport. These results include the four additional wells installed in 2018 near Area I fill. Also attached are
the quarterly 'surface' water sampling results from locations near the Area I fill. The results from these
sampling events are included on the GW59CCR forms per permit WQ0000020, dated September 2, 2015.
As these structural fill sampling events are not part of an NPDES permit, these forms were slightly modified
and are not signed.
Area I groundwater monitoring wells and 'surface'water samples were collected on April 6 - 8, 2020. Area
III and IV groundwater monitoring wells were sampled between April 7 - 9, 2020.
Note that results for well MW-7A4 continue to show elevated conductivity, TDS, arsenic, sulfate,
manganese, nickel & selenium. Duke Energy voluntarily sampled wells MW2A4, MW5A4, MW5DA4,
MW6A4, MW7A4 and MW9A4 (wells along Ferncliff Park Drive) for nitrate (as N) and fecal coliform. The
results do not indicate any sanitary sewer influence and Duke Energy will not sample for these
constituents going forward. Duke Energy will continue semi-annual sampling of the groundwater
monitoring wells for Area I, III and IV, per above -referenced permit.
Per our prior letter to DEQ (March 2, 2015 to Mr. Brett Laverty), DEP requests that DEQ continue to
contact MSD directly regarding leachate quantity and quality for Area III and Area IV leachate discharges.
If you have any questions or need any clarification regarding the information provided, feel free to contact
me at [e-mail] or at 919-546-7863 at your convenience.
Respectfully submitted,
Jahn Toepfer, P.E.
Lead Engineer, Duke Energy EHS CCP
Waste & Groundwater Programs

May 22, 2020
Page 2
Attachments
cc: Mr. G. Landon Davidson
NCDENR/Asheville Regional Office
2090 U.S. 70 Highway
Swannanoa, NC 28778
cc: Mr. Matt Hanchey— NC20
Mr. Ed Sullivan - EC13K
Mr. Ryan Czop— EC13K
Mr. John Toepfer — NC15
Ms. Teresa Williams —Asheville Plant
Ms. Tina Woodward — EC13K
Mr. Jeremy Pruett — EC13K
Ms. Bryson Sheetz — EC13K
Mr. Bryan Moeller—EC13K
Mr. Matt Pickett —Asheville Plant
Ms. Kathy Webb — SynTerra Corporation
Mr. James McNash - Geosyntec
Mr. Michael Reisman — Asheville Airport
Asheville Regional Airport
61 Terminal Drive, Suite 1
Fletcher, NC 28732
2

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Analytical Laboratory Page 1 of50
* ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J20030214
ASHEVILLE AIRPORT - AIRPORT FILL AREA I SW - (IN-HOUSE)
B Allison, F Holt,B Moeller, T Hunsucker,H Seaton
Lab Contact: �{py Peggy Kendall Phone: [phone]
Report Authorized By: - Date: 4/22/2020
(Signature) f*
y Kendall
Program Comments:
Please contact the Program Manager (Peggy Kendall) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions: Page 2 of 50
Collection
Sample ID Plant/Station Date and Time Collected By Sample Description
2020006510
Asheville Airport
06-Apr-20
4:12 PM
Haley Seaton
ASA_SW-2-A1
2020006543
Asheville Airport
06-Apr-20
3:15 PM
Haley Seaton
ASA_SW-3-A1
2020006544
Asheville Airport
06-Apr-20
1:30 PM
Haley Seaton
ASA_SW-4C-A1
2020006545
Asheville Airport
06-Apr-20
3:00 PM
Haley Seaton
ASA_SW-5-A1
2020006546
Asheville Airport
06-Apr-20
3:30 PM
Haley Seaton
ASA_SW-6-A1
2020006547
Asheville Airport
06-Apr-20
1:16 PM
Haley Seaton
ASA_SW-8-A1
2020006548
Asheville Airport
06-Apr-20
1:40 PM
Haley Seaton
ASA_SW-9-A1
2020006549
Asheville Airport
06-Apr-20
2:35 PM
Haley Seaton
ASA_SW-413-A1
2020006550
Asheville Airport
06-Apr-20
4:40 PM
Haley Seaton
ASA_FTB-20200406-1640
2020006552
Asheville Airport
06-Apr-20
4:40 PM
Josh Stowe
ASA_EB-20200406-1640
2020006553
Asheville Airport
06-Apr-20
4:40 PM
Josh Stowe
ASA_FB-20200406-1640
11 Total Samples

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. Yes 0 No
All laboratory QA/QC requirements are acceptable. Yes No
Report Sections Included:
d❑ Job Summary Report
© Sample Identification
❑ Technical Validation of Data Package
Analytical Laboratory Certificate of Analysis
91 Analytical Laboratory QC Report
Page 3 of 50
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
d❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 4/22/2020

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-2-Al
Collection Date: 04/06/2020 04:12 PM
Analyse Result Units Qualifiers RDL DF
TOTALALKALINITY - 92004016
Total Alkalinity as CaCO3
13.7
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
13.7
mg/L
INORGANIC N BY IC -
g2004O36
Chloride
16
mg/L
Fluoride
< 0.1
mg/L
Sulfate
1.2
mg/L
MERCURY J COLD VAPOR IN
WATER -
1 8
Mercury (Hg)
< 0.05
ug/L
Mercuf v Dissolved cold vapor) in Water it
r dl - 020040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED)
- 020040150
Aluminum (AI)
0.013
mg/L
Barium (Ba)
0.060
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
6.64
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.584
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
3.08
mg/L
Manganese (Mn)
0.228
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.46
mg/L
Sodium (Na)
6.59
mg/L
Strontium (Sr)
0.060
mg/L
Zinc (Zn)
< 0.005
mg/L
Sample #: 2020006510
Matrix: GW WW
Page 4 of 50
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 15:46
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:46
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:46
PARMSTR
1
10
EPA 300.0
04/17/2020 12:09
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 12:09
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 12:09
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:21
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:21
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.1
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:13
DMFRANC

Certificate of Laboratory Analysis Page 5 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-2-A1 Sample #: 2020006510
Collection Date: 04/06/2020 04:12 PM Matrix: GW WW
Analyte Result Units Qualifiers
TOTAL RECOVERABLE METALS BY ICP - Q20040152
Aluminum (Al)
0.024
mg/L
Barium (Ba)
0.060
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
6.51
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.875
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
3.02
mg/L
Manganese (Mn)
0.224
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.43
mg/L
Sodium (Na)
6.55
mg1L
Strontium (Sr)
0.060
mg/L
Total Hardness (Ca and Mg)
28.7
mg/L
(CaCO3)
Zinc (Zn)
0.005
mg/L
RDL
DF
Method
Analysis Date/Time
Analyst
0.01
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.01
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.01
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.1
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.066
1
EPA 200.7
04/09/2020 11:28
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:28
MHALL3
TOTAL RECOVERABLE_ METALS BY ICP-MS (DISSOLVED) - 020040151
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
0.2
1
EPA 200.8
04/08/2020 20:03
CWSPEN3
0.3
1
EPA 200.8
04/08/2020 20:03
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-2-A1
Collection Date: 04/06/2020 04:12 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040153
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL DISSOLVED SOLIDS - 020040123
TDS
84.0
mg/L
25
Total Suspended Solids - Low RL 2.5
- Q2 040148
TSS
< 2.5
mg/L
2.5
Page 6 of 50
Sample #: 2020006510
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 EPA 200.8
04/09/2020 00:51
CWSPEN3
1 SM2540C
04107/202010:16
GBSINGL
1 SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-3-A1
Collection Date: 04/06/2020 03:15 PM
Analyse Result Units Qualifiers RDL
TOTAL ALKALINITY - 020040160
Total Alkalinity as CaCO3
23.8
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
23.8
mg/L
INORGANIC IONS BY IC - 020040365
Chloride
14
mg/L
Fluoride
< 0.1
mg/L
Sulfate
3.0
mg/L
MERCURY {COLD VAPOR} IN WATER - Q20040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved scold vapor} in Water (Filtered)
- Q20040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP DISSOLVED - 020040150
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
0.048
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
8.95
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.162
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
3.79
mg/L
Manganese (Mn)
0.264
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.57
mg/L
Sodium (Na)
6.09
mg/L
Strontium (Sr)
0.088
mg/L
Zinc (Zn)
< 0.005
mg/L
Page 7 of 50
Sample #: 2020006543
Matrix: GW WW
DF Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 15:52
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:52
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:52
PARMSTR
0.5
5
EPA 300.0
04/17/2020 12:47
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 12:47
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 12:47
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:23
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:14
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.1
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:18
DMFRANC

Certificate of Laboratory Analysis Page 8 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-3-Al
Collection Date: 04/06/2020 03:15 PM
Analyse
Result
Units
Qualifiers RDL
TOTAL RECOVERABLE METALS
BY ICP - Q20040152
Aluminum (AI)
0.122
mg/L
0.01
Barium (Ba)
0.050
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Calcium (Ca)
8.58
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
0.789
mg/L
0.01
Lithium (Li)
< 0.005
mg/L
0.005
Magnesium (Mg)
3.71
mg/L
0.01
Manganese (Mn)
0.284
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
1.55
mg/L
0.1
Sodium (Na)
6.01
mglL
0.05
Strontium (Sr)
0.084
mg/L
0.005
Total Hardness (Ca and Mg)
36.7
mg/L
0.066
(CaCO3)
Zinc (Zn)
0.006
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
DISSOLVED
- 02 40151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006543
Matrix: GW WW
DF
Method
Analysis Daterrime
Analyst
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.7
04/09/2020 11:41
MHALL3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3
1
EPA 200.8
04/08/2020 20:11
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-3-A1
Collection Date: 04/06/2020 03:15 PM
Analyse Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040153
Antimony (Sb) < 1
ug/L
1
Arsenic (As) < 1
ug/L
1
Beryllium (Be) < 1
ug/L
1
Cadmium (Cd) < 1
ug/L
1
Cobalt (Co) < 1
ug/L
1
Lead (Pb) < 1
ug/L
1
Molybdenum (Mo) < 1
ug/L
1
Selenium (Se) < 1
ug/L
1
Thallium (TI) Low Level < 0.2
ug/L
0.2
Vanadium (V) Low Level < 0.3
ug/L
0.3
TOTAL DISSOLVED SOLIDS - Q20040123
TDS 86.0
mg/L
25
Total Suspended Solids - Low RL 2.5 - Q20040148
TSS 3.7
mg/L
2.5
Sample #: 2020006543
Matrix: GW WW
Page 9 of 50
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
EPA 200.8
04/09/2020 00:16
CWSPEN3
1
SM2540C
04/07/202010:17
GBSINGL
1
SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4C-A1
Collection Date: 04/06/2020 01:30 PM
Sample #: 2020006544
Matrix: GW WW
Page 10 of 50
Analyte
Result
Units
Qualifiers RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - Q20040160
Total Alkalinity as CaCO3
25.2
mg/L
5
1
SM 2320B-2011
04/08/2020 15:56
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/08/2020 15:56
PARMSTR
Alkalinity, Bicarbonate
25.2
mg/L
5
1
SM 2320B-2011
04/08/2020 15:56
PARMSTR
INORGANIC IONS BY IC - 020040365
Chloride
2.4
mg/L
0.1
1
EPA 300.0
04/17/2020 11:12
GHUTCHI
Fluoride
< 0.1
mg/L
0.1
1
EPA 300.0
04/17/2020 11:12
GHUTCHI
Sulfate
7.9
mg/L
0.1
1
EPA 300.0
04/17/2020 11:12
GHUTCHI
MERCURY f COLD V
IN WATER - Q200401
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 12:26
DMFRANC
Mercury Dissolved (cold v
porl in Water (Filtered)
- Q20040167
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 11:23
DMFRANC
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED) -
Q20040150
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Barium (Ba)
0.023
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Boron (B)
0.119
mg/L
0.05
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Calcium (Ca)
6.99
mg/L
0.05
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Iron (Fe)
0.812
mg/L
0.01
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Lithium (Li)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Magnesium (Mg)
3.58
mg/L
0.01
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Manganese (Mn)
0.363
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Potassium (K)
1.10
mg/L
0.1
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Sodium (Na)
2.76
mg/L
0.05
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Strontium (Sr)
0.066
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:22
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4C-A1
Collection Date: 04/06/2020 01:30 PM
Analyse Result Units
TOTAL RECOVERABLE METALS BY ICP - Q20040152
Sample #: 2020006544
Matrix: GW WW
Page 11 of 50
Qualifiers RDL DF Method Analysis Date/Time Analyst
Aluminum (AI)
0.036
mg/L
0.01
1
EPA 200.7
04/09/2020 11:46
MHALL3
Barium (Ba)
0.021
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Boron (B)
0.113
mg/L
0.05
1
EPA 200.7
04/09/2020 11:46
MHALL3
Calcium (Ca)
6.16
mg/L
0.05
1
EPA 200.7
04/09/2020 11:46
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Iron (Fe)
0.836
mg/L
0.01
1
EPA 200.7
04/09/2020 11:46
MHALL3
Lithium (Li)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Magnesium (Mg)
3.33
mg/L
0.01
1
EPA 200.7
04/09/2020 11:46
MHALL3
Manganese (Mn)
0.327
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Potassium (K)
1.03
mg/L
0.1
1
EPA 200.7
04/09/2020 11:46
MHALL3
Sodium (Na)
2.64
mg/L
0.05
1
EPA 200.7
04/09/2020 11:46
MHALL3
Strontium (Sr)
0.055
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
Total Hardness (Ca and Mg)
29.1
mg/L
0.066
1
EPA 200.7
04/09/2020 11:46
MHALL3
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 11:46
MHALL3
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
- 020040151
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Selenium (Se)
2.10
ug/L
1
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/08/2020 20:19
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/08/2020 20:19
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4C-A1
Collection Date: 04/06/2020 01:30 PM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS -
Q20040153
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
2.11
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL DISSOLVED SOLIDS - Q20040123
TDS
55.0
mg/L
25
Total Suspended Solids - Low
RL 2.5 - Q2004014�
TSS
< 2.5
mg/L
2.5
Page 12 of 50
Sample #: 2020006544
Matrix: GW WW
DF Method Analysis DatefTime Analyst
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 EPA 200.8
04/09/2020 00:59
CWSPEN3
1 SM2540C
04/07/202010:18
GBSINGL
1 SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis Page 13 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA_SW-5-Al Sample #: 2020006545
Collection Date: 04/06/2020 03:00 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040160
Total Alkalinity as CaCO3
99.9
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
99.9
mg/L
INORGANIC IONS BY IC - 020040365
Chloride
17
mg/L
Fluoride
< 0.1
mg/L
Sulfate
1.3
mg/L
MERCURY (COLD VAPOR) IN WATER - 020040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved (cold vapor) in Water (Filtered) - Q20040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED) - 020040150
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
0.071
mg/L
Boron (B)
0.194
mg/L
Calcium (Ca)
31.6
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
3.37
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
7.89
mg/L
Manganese (Mn)
1.50
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
2.46
mg/L
Sodium (Na)
6.46
mg/L
Strontium (Sr)
0.458
mg/L
Zinc (Zn)
< 0.005
mg/L
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 15:59
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:59
PARMSTR
5
1
SM 2320B-2011
04/08/2020 15:59
PARMSTR
0.5
5
EPA 300.0
04/17/2020 13:24
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 13:24
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 13:24
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:28
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:25
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/0812020 15:27
DMFRANC
0.1
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:27
DMFRANC

Certificate of Laboratory Analysis Page 14 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA_SW-5-Al Sample #: 2020006545
Collection Date: 04/06/2020 03:00 PM Matrix: GW_WW
Analyse
Result
Units Qualifiers
TOTAL RECOVERABLE METAL
P - Q20040152
Aluminum (Al)
0.345
mg/L
Barium (Ba)
0.086
mg/L
Boron (B)
0.194
mg/L
Calcium (Ca)
30.8
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
8.88
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
7.76
mg/L
Manganese (Mn)
1.88
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
2.46
mg/L
Sodium (Na)
6.40
mg/L
Strontium (Sr)
0.458
mg/L
Total Hardness (Ca and Mg)
109
mg/L
(CaCO3)
Zinc (Zn)
0.006
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
(DISSOLVED) 02004015
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
1.43
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
2.97
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
RDL
DF
Method
Analysis Date/Time
Analyst
0.01
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.01
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.01
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.1
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.05
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.066
1
EPA 200.7
04/09/2020 11:50
MHALL3
0.005
1
EPA 200.7
04/09/2020 11:50
MHALL3
1
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
1
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
0.2
1
EPA 200.8
04/08/2020 20:28
CWSPEN3
0.3
1
EPA 200.8
04/08/2020 20:28
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-5-Al
Collection Date: 04/06/2020 03:00 PM
Analyse Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040153
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
2.24
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
3.97
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL DISSOLVED SOLIDS -
Q20040123
TDS
145
mg/L
25
Total Suspended Solids - Low RL 2.5 - Q20040148
TSS
16
mg/L
2.5
Sample #: 2020006545
Matrix: GW WW
Page 15 of 50
DF
Method
Analysis DatelTime
Analyst
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
EPA 200.8
04/09/2020 01:07
CWSPEN3
1
SM2540C
04107/202010:19
GBSINGL
1
SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis Page 16 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA_SW-6-Al Sample #: 2020006546
Collection Date: 04/06/2020 03:30 PM Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis DatelTime
Analyst
TOTAL ALKALINITY - 020040160
Total Alkalinity as CaCO3
55.2
mg/L
5
1
SM 2320B-2011
04/08/2020 16:03
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/08/2020 16:03
PARMSTR
Alkalinity, Bicarbonate
55.2
mg/L
5
1
SM 2320B-2011
04/08/2020 16:03
PARMSTR
INORGANIC IONS BY IC - Q20040365
Chloride
5.8
mg/L
0.1
1
EPA 300.0
04/17/2020 13:43
GHUTCHI
Fluoride
< 0.1
mg/L
0.1
1
EPA 300.0
04/17/2020 13:43
GHUTCHI
Sulfate
1.6
mg/L
0.1
1
EPA 300.0
04/17/2020 13:43
GHUTCHI
MERCURY COLD V IN WATER - Q2004016,8
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 12:30
DMFRANC
Mercury Dissolved (cold vapor) in Water (Filtered)
- Q2004016
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 11:27
DMFRANC
TOTAL RECOVERABLE METALS BY ICP DISSOLVED - Q2 040150
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Barium (Ba)
0.019
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Calcium (Ca)
15.8
mg/L
0.05
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Iron (Fe)
0.075
mg/L
0.01
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Lithium (Li)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Magnesium (Mg)
4.50
mg/L
0.01
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Manganese (Mn)
1.14
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Potassium (K)
1.91
mg/L
0.1
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Sodium (Na)
2.76
mg/L
0.05
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Strontium (Sr)
0.077
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 15:31
DMFRANC

Certificate of Laboratory Analysis Page 17of50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-6-A1 Sample #: 2020006546
Collection Date: 04/06/2020 03:30 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP - 020040152
Aluminum (Al)
0.030
mg/L
0.01
Barium (Ba)
0.019
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Calcium (Ca)
15.3
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
1.52
mg/L
0.01
Lithium (Li)
< 0.005
mg/L
0.005
Magnesium (Mg)
4.37
mg/L
0.01
Manganese (Mn)
1.10
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
1.84
mg/L
0.1
Sodium (Na)
2.67
mg/L
0.05
Strontium (Sr)
0.075
mg/L
0.005
Total Hardness (Ca and Mg)
56.3
mg/L
0.066
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVEDI
020040151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
1.20
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.7
04/09/2020 11:55
MHALL3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3
1
EPA 200.8
04/08/2020 20:36
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-6-Al
Collection Date: 04/06/2020 03:30 PM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY
ICP-MS - Q20040153
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
1.13
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL DISSOLVED SOLIDS - Q20040123
TDS
85.0
mg/L
25
Total Suspended Solids - Low RL 2.5 - 020040148
TSS
3.3
mg/L
2.5
Page 18 of 50
Sample #: 2020006546
Matrix: GW WW
DF Method Analysis Daterrime Analyst
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 EPA 200.8
04/09/2020 01:16
CWSPEN3
1 SM2540C
04/07/202010:19
GBSINGL
1 SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis Page 19 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-8-Al Sample #: 2020006547
Collection Date: 04/06/2020 01:16 PM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q20040160
Total Alkalinity as CaCO3
459
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
459
mg/L
INORGANIC IONS BY IC - Q20040365
Chloride
3.7
mg/L
Fluoride
0.53
mg/L
Sulfate
27
mg/L
MERCURY (COLD VAPOR) IN WATER - 020040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved cold vapor) in Water Filtered
- 020040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED) - Q20040150
Aluminum (Al)
0.017
mg/L
Barium (Ba)
0.263
mg/L
Boron (B)
1.23
mg/L
Calcium (Ca)
147
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
20.1
mg/L
Lithium (Li)
0.048
mg/L
Magnesium (Mg)
28.5
mg/L
Manganese (Mn)
6.26
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
4.69
mg/L
Sodium (Na)
7.07
mg/L
Strontium (Sr)
2.45
mg/L
Zinc (Zn)
< 0.005
mg/L
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 16:06
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:06
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:06
PARMSTR
1
10
EPA 300.0
04/17/2020 14:21
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 14:21
GHUTCHI
1
10
EPA 300.0
04/17/2020 14:21
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:32
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:30
DMFRANC
0.01
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.05
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.5
10
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.01
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.01
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.1
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.05
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC
0.005
1
EPA 200.7
04/09/2020 08:25
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-8-A1
Collection Date: 04/06/2020 01:16 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP - 020040152
Aluminum (AI)
0.523
mg/L
0.01
Barium (Ba)
0.279
mg/L
0.005
Boron (B)
1.23
mg/L
0.05
Calcium (Ca)
146
mg/L
0.5
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
25.6
mg/L
0.01
Lithium (Li)
0.047
mg/L
0.005
Magnesium (Mg)
28.1
mg/L
0.01
Manganese (Mn)
6.13
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
4.67
mg/L
0.1
Sodium (Na)
6.94
mg/L
0.05
Strontium (Sr)
2.47
mg/L
0.005
Total Hardness (Ca and Mg)
480
mg/L
0.066
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS IDISSOLVEDi_
020040151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
364
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
10.5
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
92.4
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006547
Matrix: GW WW
Page 20 of 50
DF
Method
Analysis Daterrime
Analyst
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
10
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.7
04/09/2020 11:59
MHALL3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3
1
EPA 200.8
04/08/2020 20:44
CWSPEN3

Certificate of Laboratory Analysis Page21 of50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-8-Al Sample #: 2020006547
Collection Date: 04/06/2020 01:16 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040153
Antimony (Sb) < 1
ug/L
1
Arsenic (As) 470
ug/L
1
Beryllium (Be) < 1
ug/L
1
Cadmium (Cd) < 1
ug/L
1
Cobalt (Co) 10.8
ug/L
1
Lead (Pb) < 1
ug/L
1
Molybdenum (Mo) 99.4
ug/L
1
Selenium (Se) < 1
ug/L
1
Thallium (TI) Low Level < 0.2
ug/L
0.2
Vanadium (V) Low Level 0.423
ug/L
0.3
TOTAL DISSOLVED SOLIDS - Q20040123
TDS 523
mg/L
25
Total Suspended Solids - Low RL 2.5 - Q20040148
TSS 69
mg/L.
2.5
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
EPA 200.8
04/09/2020 01:24
CWSPEN3
1
SM2540C
04/071202010:20
GBSINGL
1
SM2540D
04/08/2020 06:40
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-9-A1
Collection Date: 04/06/2020 01:40 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040160
Total Alkalinity as CaCO3
17.3
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
17.3
mg/L
INORGANIC IONS BY IC - Q20040365
Chloride
16
mg/L
Fluoride
< 0.1
mg/L
Sulfate
1.9
mg/L
MERCURY LD VAPORi IN WATER - Q20040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved (cold vapor)
in Water (Filtered)
- Q20040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP DISSOLVED - 020 40150
Aluminum (AI)
< 0.01
mg/L
Barium (Be)
0.058
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
7.77
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.415
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
3.43
mg/L
Manganese (Mn)
0.291
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.59
mg/L
Sodium (Na)
6.81
mg/L
Strontium (Sr)
0.065
mg/L
Zinc (Zn)
0.022
mg/L
Sample #: 2020006548
Matrix: GW WW
Page 22 of 50
Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/08/2020 16:11
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:11
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:11
PARMSTR
0.5
5
EPA 300.0
04/17/2020 14:58
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 14:58
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 14:58
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:14
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:32
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.1
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:40
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-9-Al
Collection Date: 04/06/2020 01:40 PM
Analyse Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP - 020040152
Aluminum (Al)
0.157
mg/L
0.01
Barium (Ba)
0.057
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Calcium (Ca)
7.45
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
0.861
mg/L
0.01
Lithium (Li)
40.005
mg/L
0.005
Magnesium (Mg)
3.30
mg/L
0.01
Manganese (Mn)
0.278
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
1.52
mg/L
0.1
Sodium (Na)
6.61
mg/L
0.05
Strontium (Sr)
0.063
mg/L
0.005
Total Hardness (Ca and Mg)
32.2
mglL
0.066
(CaCO3)
Zinc (Zn)
0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED) -
Q20040151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006548
Matrix: GW WW
Page 23 of 50
DF
Method
Analysis Daterrime
Analyst
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.7
04/09/2020 12:04
MHALL3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3
1
EPA 200.8
04/08/2020 20:53
CWSPEN3

Certificate of Laboratory Analysis Page 24 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-9-A1
Sample #:
2020006548
Collection Date: 04/06/2020 01:40 PM
Matrix:
GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040153
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/09/2020 01:32
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040123
TDS
68.0
mg/L
25
1
SM2540C
04/07/202010:21
GBSINGL
Total Suspended Solids - Low RL 2
- 02004014
TSS
<2.5
mg/L
2.5
1
SM2540D
04/08/202006:41
GBSINGL

Certificate of Laboratory Analysis Page 25 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4B-A1 Sample #: 2020006549
Collection Date: 04/06/2020 02:35 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q20040160
Total Alkalinity as CaCO3
51.2
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
51.2
mg/L
INORGANIC IONS BY IC -
Q20040365
Chloride
14
mg/L
Fluoride
< 0.1
mg/L
Sulfate
9.0
mg/L
MERCURY f COLD VAPORI IN WATER - Q20040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved (cold vaQor) in Water (Filtered) - Q20040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP DISSOLVED - 020040150
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
0.044
mg/L
Boron (B)
0.146
mg/L
Calcium (Ca)
15.1
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
2.36
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
7.01
mg/L
Manganese (Mn)
0.840
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.94
mg/L
Sodium (Na)
5.66
mg/L
Strontium (Sr)
0.170
mg/L
Zinc (Zn)
0.009
mg/L
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 16:15
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:15
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:15
PARMSTR
0.5
5
EPA 300.0
04/17/2020 15:17
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 15:17
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 15:17
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:35
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:34
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.1
1
EPA 200.7
04/080020 15:45
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:45
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4B-A1
Collection Date: 04/06/2020 02:35 PM
Analyte
Result
Units
Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP - Q200401
52
Aluminum (AI)
0.024
mg/L
0.01
Barium (Ba)
0.041
mg/L
0.005
Boron (B)
0.140
mg/L
0.05
Calcium (Ca)
14.2
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
2.36
mg/L
0.01
Lithium (Li)
< 0.005
mg/L
0.005
Magnesium (Mg)
6.63
mg/L
0.01
Manganese (Mn)
0.786
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
1.80
mg/L
0.1
Sodium (Na)
5.31
mg/L
0.05
Strontium (Sr)
0.161
mg/L
0.005
Total Hardness (Ca and Mg)
62.7
mg/L
0.066
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
[DISSOLVED)
- Q20040151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
2.74
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006549
Matrix: GW WW
Page 26 of 50
DF
Method
Analysis Daterrime
Analyst
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.7
04/09/2020 12:08
MHALL3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3
1
EPA 200.8
04/08/2020 21:01
CWSPEN3

Certificate of Laboratory Analysis Page 27 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA SW-4131-Al Sample #: 2020006549
Collection Date: 04/06/2020 02:35 PM Matrix: GW WW
Analyse
Result
Units Qualifiers
RDL
DF
TOTAL RECOVERABLE METALS BY ICP-MS - 020040153
Antimony (Sb)
< 1
ug/L
1
1
Arsenic (As)
< 1
ug/L
1
1
Beryllium (Be)
< 1
ug/L
1
1
Cadmium (Cd)
< 1
ug/L
1
1
Cobalt (Co)
2.60
ug/L
1
1
Lead (Pb)
< 1
ug/L
1
1
Molybdenum (Mo)
< 1
ug/L
1
1
Selenium (Se)
< 1
ug/L
1
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
TOTAL DISSOLVED SOLIDS -
Q20040123
TDS
107
mg/L
25
1
Total Suspended Solids - Low RL 2.5 - Q20040148
TSS
< 2.5
mg/L
2.5
1
Method Analysis Daterfime Analyst
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
EPA 200.8
04/09/2020 02:06
CWSPEN3
SM2540C
04/07/202010:21
GBSINGL
SM2540D
04/08/2020 06:41
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA FTB-20200406-1640 Filter Blank
Collection Date: 04/06/2020 04:40 PM
Analyte
Result
Units Qualifiers
RDL
Mercury Dissolved ;cold vapor)
in Water (Filtered) - 020040167
Mercury (Hg)
< 0.05
ug/L
0.05
TOTAL RECOVERABLE METALS
BY ICP {DISSOLVED)
- Q2Q040150
Aluminum (AI)
< 0.01
mg/L
0.01
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Calcium (Ca)
< 0.05
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
< 0.01
mg/L
0.01
Lithium (Li)
< 0.005
mg/L
0.005
Magnesium (Mg)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS
BY ICP-MS
LVED - 200401 1
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Page 28 of 50
Sample #: 2020006550
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 EPA 245.1
04/08/2020 11:36
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.7
04/08/2020 15:49
DMFRANC
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3
1 EPA 200.8
04/08/2020 21:09
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA_EB-20200406-1640 Equipment Blank
Collection Date: 04/06/2020 04:40 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040160
Total Alkalinity as CaCO3
< 5
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
< 5
mg/L
INORGANIC IONS BY IC - Q20040365
Chloride
< 0.1
mg/L
Fluoride
< 0.1
mg/L
Sulfate
< 0.1
mg/L
MERCURY (COLD VAPOR) IN WATER - 020040168
Mercury (Hg)
< 0.05
ug/L
Mercury Dissolved (cold vapor) in Water (Filtered)
- 020040167
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP !DISSOLVED) - Q20040150
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
< 0.005
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
< 0.05
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Lithium (Li)
< 0.005
mg/L
Magnesium (Mg)
< 0.01
mg/L
Manganese (Mn)
< 0.005
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
< 0.1
mg/L
Sodium (Na)
< 0.05
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
< 0.005
mg/L
Sample #: 2020006552
Matrix: GW WW
Page 29 of 50
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/08/2020 16:18
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:18
PARMSTR
5
1
SM 2320B-2011
04/08/2020 16:18
PARMSTR
0.1
1
EPA 300.0
04/17/2020 15:36
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 15:36
GHUTCHI
0.1
1
EPA 300.0
04/17/2020 15:36
GHUTCHI
0.05
1
EPA 245.1
04/08/2020 12:37
DMFRANC
0.05
1
EPA 245.1
04/08/2020 11:39
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.01
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.1
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.05
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC
0.005
1
EPA 200.7
04/08/2020 15:54
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA EB-20200406-1640 Equipment Blank
Collection Date: 04/06/2020 04:40 PM
Analyse
Result
Units
Qualifiers RDL
TOTAL RECOVERABLE METALS BY
ICP - Q20040152
Aluminum (AI)
< 0.01
mg/L
0.01
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Calcium (Ca)
< 0.05
mg/L
0.05
Chromium (Cr)
< 0.005
mg/L
0.005
Copper (Cu)
< 0.005
mg/L
0.005
Iron (Fe)
< 0.01
mg/L
0.01
Lithium (Li)
< 0.005
mg/L
0.005
Magnesium (Mg)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Nickel (Ni)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
Strontium (Sr)
< 0.005
mg/L
0.005
Total Hardness (Ca and Mg)
< 0.066
mg/L
0.066
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY
ICP-MS (DISSOLVED)
- 020040151
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006552
Matrix: GW WW
Page 30 of 50
DF
Method
Analysis Daterrime
Analyst
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.7
04/09/2020 12:13
MHALL3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3
1
EPA 200.8
04/08/2020 21:43
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA_EB-20200406-1640
Equipment Blank
Collection Date: 04/06/2020
04:40 PM
Analyse
Result Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS - 020040153
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2020006552
Matrix: GW WW
Page 31 of 50
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3
1
EPA 200.8
04/09/2020 02:15
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Page 32 of 50
Site: ASA_FB-20200406-1640 Field Blank
Sample #: 2020006553
Collection Date: 04/06/2020 04:40 PM
Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - Q2004016
Total Alkalinity as CaCO3
< 5
mg/L
5
1
SM 2320E-2011
04/08/2020 17:18
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/08/2020 17:18
PARMSTR
Alkalinity, Bicarbonate
< 5
mg/L
5
1
SM 2320B-2011
04/08/2020 17:18
PARMSTR
INORGANIC IONS BY IC - 020040365
Chloride
< 0.1
mg/L
0.1
1
EPA 300.0
04/17/2020 15:55
GHUTCHI
Fluoride
< 0.1
mg/L
0.1
1
EPA 300.0
04/17/2020 15:55
GHUTCHI
Sulfate
< 0.1
mg/L
0.1
1
EPA 300.0
04/17/2020 15:55
GHUTCHI
MERCURY (COLD VAPORS IN WATER
- 020040168
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 12:39
DMFRANC
Mercury Dissolved (cold vapor) in
Water (Filtered)
- Q20040167
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/08/2020 11:52
DMFRANC
TOTAL RECOVERABLE METALS BY ICP (DISSOLVED) -_ Q20040150
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Barium (Ba)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Calcium (Ca)
< 0.05
mg/L
0.05
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Lithium (Li)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Magnesium (Mg)
< 0.01
mg/L
0.01
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Potassium (K)
< 0.1
mg/L
0.1
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Sodium (Na)
< 0.05
mg/L
0.05
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/08/2020 16:19
DMFRANC

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA FB-20200406-1640 Field Blank
Collection Date: 04/06/2020 04:40 PM
Analyse Result Units
TOTAL RECOVERABLE METALS BY ICP - Q20040152
Page 33 of 50
Sample #: 2020006553
Matrix: GW WW
Qualifiers RDL DF Method Analysis Date/Time Analyst
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/09/2020 12:17
MHALL3
Barium (Ba)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/09/2020 12:17
MHALL3
Calcium (Ca)
< 0.05
mg/L
0.05
1
EPA 200.7
04/09/2020 12:17
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/09/2020 12:17
MHALL3
Lithium (Li)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Magnesium (Mg)
< 0.01
mg/L
0.01
1
EPA 200.7
04/09/2020 12:17
MHALL3
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Potassium (K)
< 0.1
mg/L
0.1
1
EPA 200.7
04/09/2020 12:17
MHALL3
Sodium (Na)
< 0.05
mg/L
0.05
1
EPA 200.7
04/09/2020 12:17
MHALL3
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
Total Hardness (Ca and Mg)
< 0.066
mg/L
0.066
1
EPA 200.7
04/09/2020 12:17
MHALL3
(CaCO3)
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/09/2020 12:17
MHALL3
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
- Q20040151
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/08/2020 22:18
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/08/2020 22:18
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Site: ASA FB-20200406-1640 Field Blank
Collection Date: 04/06/2020 04:40 PM
Analyse
Result
Units Qualifiers
RDL
DF
TOTAL RECOVERABLE METALS BY ICP-MS - Q20Q40153
Antimony (Sb)
< 1
ug/L
1
1
Arsenic (As)
< 1
ug/L
1
1
Beryllium (Be)
< 1
ug/L
1
1
Cadmium (Cd)
< 1
ug/L
1
1
Cobalt (Co)
< 1
ug/L
1
1
Lead (Pb)
< 1
ug/L
1
1
Molybdenum (Mo)
< 1
ug/L
1
1
Selenium (Se)
< 1
ug/L
1
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
Sample #: 2020006553
Matrix: GW WW
Page 34 of 50
Method
Analysis Datelrime
Analyst
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3
EPA 200.8
04/09/2020 02:23
CWSPEN3

Certificate of Laboratory Analysis Page 35 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040160 ALK CarbBicarb TOTAL ALKALINITY
Duplicate # 1
Parent Sample: J20030214 -- 2020006510
Parameter
Measured
Final
Units:
Dil
Limit Ranae
RPD Qualifier
Alkalinity, Bicarbonate
13.7
13.7
mg/L
1
0 - 20%
0 -
Alkalinity, Carbonate
0
0
mg/L
1
0- 20%
0
Total Alkalinity as CaCO3
13.7
13.7
mg/L
1
0 - 20%
0
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike % Recovery LCL UCL
Qualifier
Total Alkalinity as CaCO3
106
106
mg/L
1
105 101 85 115

Certificate of Laboratory Analysis Page 36 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040365 Dionex
INORGANIC IONS BY IC
Blank # 1
Parameter
Measured
Final
Units:
DiI RDL
Relative Concentration
Chloride
0
0
mg/L
1 0.1
< 112 RDL
Fluoride
0
0
mg/L
1 0.1
< 1/2 RDL
Sulfate
0
0
mg/L
1 0.1
< 1/2 RDL
LCS # 1
ualifier
Parameter
Measured
Final
Units:
Dil
Soike
% Recovent LCL
UCL
Qualifier
Chloride
5.06
5.06
mg/L
1
5
101 90
110
Fluoride
4.79
4.79
mg/L
1
5
95.9 90
110
Sulfate
5.18
5.18
mg/L
1
5
104 90
110
MS # 1
Parent Sample:
J20030214
-- 2020006544
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery LCL
UCL
Qualifier
Chloride
4.56
4.56
mg/L
1
2
106 80
120
-
Fluoride
2.02
2.02
mg/L
1
2
101 80
120
-
Sulfate
9.83
9.83
mg/L
1
2
96.7 80
120
-
MSD # 1
Parent Sample:
J20030214
-- 2020006544
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery LCL
UCL
RPD Qualifier
Chloride
4.65
4.65
mg/L
1
2
ill 80
120
4.25 -
Fluoride
2.21
2.21
mg/L
1
2
110 80
120
9.15 -
Sulfate
9.9
9.9
mg/L
1
2
100 80
120
3.7 -

Certificate of Laboratory Analysis Page 37 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040168 HG 245.1 MERCURY (COLD VAPOR) IN WATER
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Mercury (Hg)
-0.001
-0.001
ug/L
1
0.05
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
%Recovezv LCL
UCL Qualifier
Mercury (Hg)
2.02
2.02
ug/L
1
2
101 85
115 -
MS # 1
Parent Sample:
J20030214 -- 2020006548
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL Qualifier
Mercury (Hg)
0.969
0.969
ug/L
1
1
95.4 70
130
MSD # 1
Parent Sample:
J20030214 -- 2020006548
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL RPD Qualifier
Mercury (Hg)
0.98
0.98
ug/L
1
1
96.5 70
130 1.15

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040167 HG 245.1 Dissolved Mercury Dissolved (cold vapor) in Water (Filtered)
Blank # 1
Parameter Measured Final
Mercury (Hg) -0.003 -0.003
LCS # 1
Parameter Measured Final
Mercury (Hg) 2.05 2.05
MS # 1
Parameter
Measured
Final
Mercury (Hg)
0.95
0.95
MSD # 1
Parameter
Measured
Final
Mercury (Hg)
0.946
0.946
Units: Dil RDL Relative Concentration
ug/L 1 0.05 < 112 RDL
Page 38 of 50
ualifier
Units:
Dil
Spike
% Recovery LCL
UCL Qualifier
ug/L
1
2
102 85
115 -
Parent Sample:
J20030214 -- 2020006543
Units:
Dil
Spike
% Recovery LCL
UCL Qualifier
ug/L
1
1
95.6 70
130
Parent Sample:
J20030214 -- 2020006543
Units:
Dil
Spike
% Recovery LCL
UCL RPD Qualifier
ug/L
1
1
95.2 70
130 0.419 -

Certificate of Laboratory Analysis Page 39 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040150 ICP_DIS_TRM TOTAL RECOVERABLE METALS BY ICP (DISSOLVED)
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Aluminum (AI)
0.000558
0.000558
mg/L
1
0.01
< 1/2 RDL
Barium (Ba)
-0.000421
-0.000421
mg/L
1
0.005
< 1/2 RDL
Boron (B)
-0.000635
-0.000635
mg/L
1
0.05
< 1/2 RDL
Calcium (Ca)
-0.0048
-0.0048
mg/L
1
0.05
< 1/2 RDL
Chromium (Cr)
-0.000093
-0.000093
mg/L
1
0.005
< 1/2 RDL
Copper (Cu)
-0.000141
-0.000141
mg/L
1
0.005
< 1/2 RDL
Iron (Fe)
-0.00398
-0.00398
mg/L
1
0.01
< 112 RDL
Lithium (Li)
0.000098
0.000098
mg/L
1
0.005
< 1/2 RDL
Magnesium (Mg)
-0.0053
-0.0053
mg/L
1
0.01
< 1/2 RDL
Manganese (Mn)
-0.000441
-0.000441
mg/L
1
0.005
< 112 RDL
Nickel (Ni)
-0.000007
-0.000007
mg/L
1
0.005
< 112 RDL
Potassium (K)
0.00663
0.00663
mg/L
1
0.1
< 1/2 RDL
Sodium (Na)
-0.0116
-0.0116
mg/L
1
0.05
< 1/2 RDL
Strontium (Sr)
-0.000384
-0.000384
mg/L
1
0.005
< 1/2 RDL
Zinc (Zn)
-0.00115
-0.00115
mg/L
1
0.005
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5.22
5.22
mg/L
1
5
104
85
115
Barium (Ba)
5.23
5.23
mg/L
1
5
105
85
115
Boron (B)
5.15
5.15
mg/L
1
5
103
85
115
Calcium (Ca)
5.24
5.24
mg/L
1
5
105
85
115
Chromium (Cr)
5.13
5.13
mg/L
1
5
103
85
115 -
Copper (Cu)
5.15
5.15
mg/L
1
5
103
85
115 -
Iron (Fe)
5.26
5.26
mg/L
1
5
105
85
115 -
Lithium (Li)
5.11
5.11
mg/L
1
5
102
85
115 -
Magnesium (Mg)
5.15
5.15
mg/L
1
5
103
85
115 -
Manganese (Mn)
5.26
5.26
mg/L
1
5
105
85
115 -
Nickel (Ni)
5.23
5.23
mg/L
1
5
105
85
115 -
Potassium (K)
5.11
5.11
mg/L
1
5
102
85
115 -
Sodium (Na)
5.11
5.11
mg/L
1
5
102
85
115 -
Strontium (Sr)
5.08
5.08
mg/L
1
5
102
85
115 -
Zinc (Zn)
5.19
5.19
mg/L
1
5
104
85
115 -
LCSD # 1
Parameter
Measured
Final
Units:
Dil
Spike
'/o Recove, %r.
LCL
UCL
RPD Qualifier
Aluminum (AI)
5.26
5.26
mg/L
1
5
105
85
115
0.801
Barium (Ba)
5.26
5.26
mg/L
1
5
105
85
115
0.515
Boron (B)
5.17
5.17
mg/L
1
5
103
85
115
0.446
Calcium (Ca)
5.26
5.26
mg/L
1
5
105
85
115
0.438

Certificate of Laboratory Analysis Page 40 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040150 ICP_DIS_TRM TOTAL RECOVERABLE METALS BY ICP (DISSOLVED)
LCSD # 1
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery
LCL
UCL
RPD Qualifier
Chromium (Cr)
5.16
5.16
mg/L
1
5
103
85
115
0.505 -
Copper (Cu)
5.17
5.17
mg/L
1
5
103
85
115
0.388 -
Iron (Fe)
5.29
5.29
mg/L
1
5
106
85
115
0.531 -
Lithium (Li)
5.16
5.16
mg/L
1
5
103
85
115
1.05 -
Magnesium (Mg)
5.18
5.18
mg/L
1
5
104
85
115
0.638 -
Manganese (Mn)
5.29
5.29
mg/L
1
5
106
85
115
0.55 -
Nickel (Ni)
5.26
5.26
mg/L
1
5
105
85
115
0.534 -
Potassium (K)
5.12
5.12
mg/L
1
5
102
85
115
0.0978 -
Sodium (Na)
5.13
5.13
mg/L
1
5
103
85
115
0.351 -
Strontium (Sr)
5.11
5.11
mg/L
1
5
102
85
115
0.668 -
Zinc (Zn)
5.21
5.21
mg/L
1
5
104
85
115
0.403 -
LCS # 2
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5.18
5.18
mg/L
1
5
104
85
115
Barium (Ba)
5.18
5.18
mg/L
1
5
104
85
115 -
Boron (B)
5.11
5.11
mg/L
1
5
102
85
115 -
Calcium (Ca)
5.2
5.2
mg/L
1
5
104
85
115 -
Chromium (Cr)
5.1
5.1
mg/L
1
5
102
85
115 -
Copper (Cu)
5.12
5.12
mg/L
1
5
102
85
115 -
Iron (Fe)
5.23
5.23
mg/L
1
5
105
85
115 -
Lithium (Li)
5.12
5.12
mg/L
1
5
102
85
115 -
Magnesium (Mg)
5.12
5.12
mg/L
1
5
102
85
115 -
Manganese (Mn)
5.23
5.23
mg/L
1
5
105
85
115 -
Nickel (Ni)
5.2
5.2
mg/L
1
5
104
85
115 -
Potassium (K)
5.07
5.07
mg/L
1
5
101
85
115 -
Sodium (Na)
5.08
5.08
mg/L
1
5
102
85
115 -
Strontium (Sr)
5.05
5.05
mg/L
1
5
101
85
115 -
Zinc (Zn)
5.14
5.14
mg/L
1
5
103
85
115 -
LCSD # 2
Parameter
Measured
Final
Units:
Dil
Saike
% Recove+v
LCL
UCL
RPD Qualifier
Aluminum (AI)
5.37
5.37
mg/L
1
5
107
85
115
3.49 -
Barium (Ba)
5.33
5.33
mg/L
1
5
107
85
115
2.95 -
Boron (B)
5.22
5.22
mg/L
1
5
104
85
115
2.09 -
Calcium (Ca)
5.36
5.36
mg/L
1
5
107
85
115
2.94 -
Chromium (Cr)
5.24
5.24
mg/L
1
5
105
85
115
2.65 -
Copper (Cu)
5.25
5.25
mg/L
1
5
105
85
115
2.68 -
Iron (Fe)
5.39
5.39
mg/L
1
5
108
85
115
2.88 -
Lithium (Li)
5.24
5.24
mg/L
1
5
105
85
115
2.47 -

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040150 ICP_DIS_TRM TOTAL RECOVERABLE METALS BY ICP (DISSOLVED)
LCSD # 2
Parameter
Measured
Final
Units:
Dil
Sgike
% Recover
LCL
UCL
Magnesium (Mg)
5.27
5.27
mg/L
1
5
105
85
115
Manganese (Mn)
5.38
5.38
mg/L
1
5
108
85
115
Nickel (Ni)
5.34
5.34
mg/L
1
5
107
85
115
Potassium (K)
5.22
5.22
mg/L
1
5
105
85
115
Sodium (Na)
5.22
5.22
mg/L
1
5
104
85
115
Strontium (Sr)
5.19
5.19
mg/L
1
5
104
85
115
Zinc (Zn)
5.3
5.3
mg/L
1
5
106
85
115
Page 41 of 50
RPD Qualifier
2.91
2.94
2.79
3.05
2.64
2.85
3.01 -

Certificate of Laboratory Analysis Page 42 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level I1 QC Summary
Q20040152 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentr
to ion
Qualifier
Aluminum (AI)
0.00233
0.00233
mg/L
1
0.01
< 1/2 RDL
Barium (Ba)
0.000551
0.000551
mg/L
1
0.005
< 1/2 RDL
Boron (B)
0.00254
0.00254
mg/L
1
0.05
< 1/2 RDL
Calcium (Ca)
0.00354
0.00354
mg/L
1
0.05
< 112 RDL
Chromium (Cr)
0.000073
0.000073
mg/L
1
0.005
< 1/2 RDL
Copper (Cu)
0.000672
0.000672
mg/L
1
0.005
< 1/2 RDL
Iron (Fe)
0.0012
0.0012
mg/L
1
0.01
< 1/2 RDL
Lithium (Li)
0.000672
0.000672
mg/L
1
0.005
< 1/2 RDL
Magnesium (Mg)
0.00112
0.00112
mg/L
1
0.01
< 1/2 RDL
Manganese (Mn)
0.000554
0.000554
mg/L
1
0.005
< 1/2 RDL
Nickel (Ni)
0.000782
0.000782
mg/L
1
0.005
< 1/2 RDL
Potassium (K)
-0.0116
-0.0116
mg/L
1
0.1
< 1/2 RDL
Sodium (Na)
0.000773
0.000773
mg/L
1
0.05
< 1/2 RDL
Strontium (Sr)
0.000621
0.000621
mg/L
1
0.005
< 1/2 RDL
Zinc (Zn)
0.00176
0.00176
mg/L
1
0.005
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5
5
mg/L
1
5
99.9
85
115 -
Barium (Ba)
5.04
5.04
mg/L
1
5
101
85
115 -
Boron (B)
4.95
4.95
mg/L
1
5
98.9
85
115 -
Calcium (Ca)
5
5
mg/L
1
5
99.9
85
115 -
Chromium (Cr)
4.96
4.96
mg/L
1
5
99.1
85
115 -
Copper (Cu)
4.93
4.93
mg/L
1
5
98.6
85
115 -
Iron (Fe)
5.01
5.01
mg/L
1
5
100
85
115 -
Lithium (Li)
4.93
4.93
mg/L
1
5
98.7
85
115 -
Magnesium (Mg)
4.92
4.92
mg/L
1
5
98.4
85
115 -
Manganese (Mn)
5.01
5.01
mg/L
1
5
100
85
115 -
Nickel (Ni)
5.01
5.01
mg/L
1
5
100
85
115 -
Potassium (K)
4.91
4.91
mg/L
1
5
98.1
85
115 -
Sodium (Na)
4.94
4.94
mg/L
1
5
98.7
85
115 -
Strontium (Sr)
4.95
4.95
mg/L
1
5
99
85
115 -
Zinc (Zn)
4.98
4.98
mg/L
1
5
99.7
85
115 -
MS # 1
Parent Sample:
J20030214 -- 2020006510
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5.18
5.18
mg/L
1
5
103
70
130
Barium (Ba)
5.32
5.32
mg/L
1
5
105
70
130
Boron (B)
5.14
5.14
mg/L
1
5
103
70
130
Calcium (Ca)
11.6
11.6
mg/L
1
5
102
70
130

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040152 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
MS # 1
Parameter
Measured
Final
Units:
Chromium (Cr)
5.14
5.14
mg/L
Copper (Cu)
5.12
5.12
mg/L
Iron (Fe)
6.1
6.1
mg/L
Lithium (Li)
5.14
5.14
mg/L
Magnesium (Mg)
8.03
8.03
mg/L
Manganese (Mn)
5.42
5.42
mg/L
Nickel (Ni)
5.18
5.18
mg/L
Potassium (K)
6.58
6.58
mg/L
Sodium (Na)
11.7
11.7
mg/L.
Strontium (Sr)
5.18
5.18
mg/L
Zinc (Zn)
5.16
5.16
mg/L
MSD # 1
Parameter
Measured
Final
Units:
Aluminum (AI)
5
5
mg/L
Barium (Ba)
5.13
5.13
mg/L
Boron (B)
4.98
4.98
mg/L
Calcium (Ca)
11.5
11.5
mg/L
Chromium (Cr)
4.95
4.95
mg/L
Copper (Cu)
4.92
4.92
mg/L
Iron (Fe)
5.91
5.91
mg/L
Lithium (Li)
4.95
4.95
mg/L
Magnesium (Mg)
7.89
7.89
mg/L
Manganese (Mn)
5.25
5.25
mg/L
Nickel (Ni)
4.98
4.98
mg/L
Potassium (K)
6.4
6.4
mg/L
Sodium (Na)
11.6
11.6
mg/L
Strontium (Sr)
5
5
mg/L
Zinc (Zn)
4.97
4.97
mg/L
Page 43 of 50
Parent Sample: J20030214 -- 2020006510
Dil S ike % Recovery LCL UCL Qualifier
1 5 103 70 130
1 5 102 70 130
1 5 104 70 130
1 5 103 70 130
1 5 100 70 130
1 5 104 70 130
1 5 104 70 130 -
1 5 103 70 130 -
1 5 104 70 130 -
1 5 102 70 130 -
1 5 103 70 130 -
Parent Sample: J20030214 -- 2020006510
Dil Soike % Recovery LCL UCL RPD Qualifier
1 5 99.6 70 130 3.38
1 5 101 70 130 3.5 -
1 5 99.5 70 130 3.16 -
1 5 99.8 70 130 1.14 -
1 5 99 70 130 3.9
1 5 98.4 70 130 4.04
1 5 101 70 130 3.2
1 5 99 70 130 3.9
1 5 97.4 70 130 1.76
1 5 101 70 130 3.24
1 5 99.6 70 130 3.9
1 5 99.4 70 130 2.76
1 5 100 70 130 1.6
1 5 98.8 70 130 3.61
1 5 99.3 70 130 3.75 -

Certificate of Laboratory Analysis Page 44 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040151 IMS_DIS_TRM TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Blank # 1
Parameter
Measured
Final
Units:
ail
RDL
Relative Concen r tio
Qualifier
Antimony (Sb)
0.023
0.023
ug/L
1
1
< 1/2 RDL
Arsenic (As)
0.022
0.022
ug/L
1
1
< 1/2 RDL
Beryllium (Be)
0.013
0.013
ug/L
1
1
< 1/2 RDL
Cadmium (Cd)
-0.003
-0.003
ug/L
1
1
< 1/2 RDL
Cobalt (Co)
0.001
0.001
ug/L
1
1
< 1/2 RDL
Lead (Pb)
0.003
0.003
ug/L
1
1
< 1/2 RDL
Molybdenum (Mo)
0.015
0.015
ug/L
1
1
< 1/2 RDL
Selenium (Se)
0.041
0.041
ug/L
1
1
< 1/2 RDL
Thallium (TI) Low Level
0.057
0.057
ug/L
1
0.2
< 1/2 RDL
Vanadium (V) Low Level
0.066
0.066
ug/L
1
0.3
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
allM
%Recovery
LCL
UCL
Qualifier
Antimony (Sb)
49.1
49.1
ug/L
1
50
98.2
85
115
Arsenic (As)
50.5
50.5
ug/L
1
50
101
85
115
-
Beryllium (Be)
49
49
ug/L
1
50
97.9
85
115
-
Cadmium (Cd)
49
49
ug/L
1
50
97.9
85
115
-
Cobalt (Co)
50.5
50.5
ug/L
1
50
101
85
115
-
Lead (Pb)
49.1
49.1
ug/L
1
50
98.2
85
115
-
Molybdenum (Mo)
49.6
49.6
ug/L
1
50
99.1
85
115
-
Selenium (Se)
48.9
48.9
ug/L
1
50
97.8
85
115
-
Thallium (TI) Low Level
47.8
47.8
ug/L
1
50
95.7
85
115
-
Vanadium (V) Low Level
48.2
48.2
ug/L
1
50
96.5
85
115
-
LCSD # 1
Parameter
Measured
Final
Units:
Dil
SoiLg
% Recovery
LCL
UCL
RPD
Qualifier
Antimony (Sb)
48.6
48.6
ug/L
1
50
97.2
85
115
1.07
Arsenic (As)
50.6
50.6
ug/L
1
50
101
85
115
0.129
Beryllium (Be)
43.3
43.3
ug/L
1
50
86.5
85
115
12.4
-
Cadmium (Cd)
48.8
48.8
ug/L
1
50
97.7
85
115
0.229
Cobalt (Co)
50
50
ug/L
1
50
100
85
115
0.917
Lead (Pb)
49.2
49.2
ug/L
1
50
98.5
85
115
0.254
Molybdenum (Mo)
49.4
49.4
ug/L
1
50
98.8
85
115
0.37
-
Selenium (Se)
44
44
ug/L
1
50
88
85
115
10.5
-
Thallium (TI) Low Level
47.7
47.7
ug/L
1
50
95.4
85
115
0.216
-
Vanadium (V) Low Level
49.2
49.2
ug/L
1
50
98.5
85
115
2.04
-
LCS # 2
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery
LCL
UCL
Qualifier
Antimony (Sb)
47.7
47.7
ug1L
1
50
95.4
85
115

Certificate of Laboratory Analysis Page 45 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040151 IMS DIS_TRM
TOTAL RECOVERABLE
METALS BY ICP-MS
(DISSOLVED)
LCS # 2
Parameter
Measured
Final
Units:
Dil
Soike
% Recover v
LCL
UCL
Qualifier
Arsenic (As)
49.1
49.1
ug/L
1
50
98.2
85
115
Beryllium (Be)
48.2
48.2
ug/L
1
50
96.4
85
115
-
Cadmium (Cd)
47.6
47.6
ug/L
1
50
95.3
85
115
-
Cobalt (Co)
48.6
48.6
ug/L
1
50
97.1
85
115
-
Lead (Pb)
48.3
48.3
ug/L
1
50
96.6
85
115
-
Molybdenum (Mo)
48.4
48.4
ug/L
1
50
96.9
85
115
-
Selenium (Se)
47
47
ug/L
1
50
94
85
115
-
Thallium (TI) Low Level
46.6
46.6
ug/L
1
50
93.3
85
115
-
Vanadium (V) Low Level
48.2
48.2
ug/L
1
50
96.3
85
115
-
LCSD # 2
Parameter
Measured
Final
Units:
Dil
agM
% Recovery
LCL
UCL
RPD Qualifier
Antimony (Sb)
49.6
49.6
ug/L
1
50
99.1
85
115
3.83
Arsenic (As)
50.2
50.2
ug/L
1
50
100
85
115
2.24
Beryllium (Be)
48.7
48.7
ug/L
1
50
97.5
85
115
1.12
Cadmium (Cd)
49.4
49.4
ug/L
1
50
98.7
85
115
3.52
Cobalt (Co)
50.1
50.1
ug/L
1
50
100
85
115
3.11 -
Lead (Pb)
50.2
50.2
ug/L
1
50
100
85
115
3.85 -
Molybdenum (Mo)
50
50
ug/L
1
50
100
85
115
3.16 -
Selenium (Se)
49.4
49.4
ug/L
1
50
98.8
85
115
4.99 -
Thallium (TI) Low Level
48.4
48.4
ug/L
1
50
96.7
85
115
3.64 -
Vanadium (V) Low Level
49.5
49.5
ug/L
1
50
99.1
85
115
2.8 -

Certificate of Laboratory Analysis Page 46 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040153 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentratio0
Qualifier
Antimony (Sb)
-0.02
-0.02
ug/L
1
1
< 1/2 RDL
Arsenic (As)
-0.007
-0.007
ug/L
1
1
< 1/2 RDL
Beryllium (Be)
0.02
0.02
ug/L
1
1
< 112 RDL
Cadmium (Cd)
-0.002
-0.002
ug/L
1
1
< 1/2 RDL
Cobalt (Co)
0.005
0.005
ug/L
1
1
< 1/2 RDL
Lead (Pb)
0.005
0.005
ug/L
1
1
< 1/2 RDL
Molybdenum (Mo)
0.009
0.009
ug/L
1
1
< 1/2 RDL
Selenium (Se)
-0.015
-0.015
ug/L
1
1
< 1/2 RDL
Thallium (TI) Low Level
0.039
0.039
ug/L
1
0.2
< 112 RDL
Vanadium (V) Low Level
-0.019
-0.019
ug/L
1
0.3
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovent
LCL
UCL
Qualifier
Antimony (Sb)
48
48
ug/L
1
50
96
85
115
Arsenic (As)
46.4
46.4
ug/L
1
50
92.8
85
115
-
Beryllium (Be)
47.7
47.7
ug/L
1
50
95.5
85
115
-
Cadmium (Cd)
48.7
48.7
ug/L
1
50
97.3
85
115
-
Cobalt (Co)
47.3
47.3
ug/L
1
50
94.6
85
115
-
Lead (Pb)
48.5
48.5
ug/L
1
50
97.1
85
115
-
Molybdenum (Mo)
48.8
48.8
ug/L
1
50
97.7
85
115
-
Selenium (Se)
44.9
44.9
ug/L
1
50
89.7
85
115
-
Thallium (TI) Low Level
47.2
47.2
ug/L
1
50
94.3
85
115
-
Vanadium (V) Low Level
48.6
48.6
ug/L
1
50
97.3
85
115
-
MS # 1
Parent Sample:
J20030214
-- 2020006543
Parameter
Measured
Final
Units:
Dil
Spike
% Recover
LCL
UCL
Qualifier
Antimony (Sb)
49
49
ug/L
1
50
97.9
70
130
Arsenic (As)
47.4
47.4
ug/L
1
50
94.7
70
130
Beryllium (Be)
48.2
48.2
ug/L
1
50
96.3
70
130
Cadmium (Cd)
49.6
49.6
ug/L
1
50
99.1
70
130
-
Cobalt (Co)
47.9
47.9
ug/L
1
50
94.1
70
130
-
Lead (Pb)
49.7
49.7
ug/L
1
50
99.3
70
130
-
Molybdenum (Mo)
50.2
50.2
ug/L
1
50
100
70
130
-
Selenium (Se)
45.1
45.1
ug/L
1
50
89.6
70
130
-
Thallium (TI) Low Level
48.1
48.1
ug/L
1
50
96.1
70
130
-
Vanadium (V) Low Level
50.4
50.4
ug/L
1
50
100
70
130
-
MSD # 1
Parent Sample:
J20030214
-- 2020006543
Parameter
Measured
Final
Units:
Dil
Spike
% Recovef:
LCL
UCL
RPD Qualifier
Antimony (Sb)
47.8
47.8
ug/L
1
50
95.6
70
130
2.37

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040153 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
MSD # 1
Parameter
Measured
Final
Units:
Arsenic (As)
46
46
ug/L
Beryllium (Be)
46.6
46.6
ug/L
Cadmium (Cd)
48
48
ug/L
Cobalt (Co)
46.8
46.8
ug/L
Lead (Pb)
48.1
48.1
ug/L
Molybdenum (Mo)
48.6
48.6
ug/L
Selenium (Se)
44.9
44.9
ug/L
Thallium (TI) Low Level
46.8
46.8
ug/L
Vanadium (V) Low Level
49.3
49.3
ug/L
Page 47 of 50
Parent Sample:
J20030214 -- 2020006543
Dil
Spike
% Recovery LCL
UCL
RPD Qualifier
1
50
92 70
130
2.91
1
50
93 70
130
3.4
1
50
95.9 70
130
3.25
1
50
92 70
130
2.29
1
50
96 70
130
3.31
1
50
97 70
130
3.16
1
50
89.3 70
130
0.362
1
50
93.4 70
130
2.86
1
50
98.3 70
130
2.14

Certificate of Laboratory Analysis Page 48 of 50
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040123 TDS
TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter
Measured
Final
Units:
DiI
RDL
Relative Concentratio
Qualifier
TDS
7
mg/L
1
25
< 112 RDL
Blank # 2
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
TDS
6
mg/L
1
25
< 1/2 RDL
Duplicate # 1
Parent Sample:
J20030035 --
2020005649
Parameter
Measured
Final
Units:
Dil
Limit Ranr a
RPD Qualifier
TDS
839
mg/L
1
0 - 10%
0.119 -
Duplicate # 2
Parent Sample:
J20030265 --
2020006794
Parameter
Measured
Final
Units:
Dil
it Ranm a
RPD Qualifier
TDS
506
mg/L
1
0 - 10%
2.4
Duplicate # 3
Parent Sample:
J20030265 -- 2020006797
Parameter
Measured
Final
Units:
Dil
Limit Ran•ip
RPD Qualifier
TDS
345
mg/L
1
0 - 10%
0.578 -
LCS # 1
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery LCL
UCL
Qualifier
TDS
993
mg/L
1
1000
99.3 90
110
-

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030214
Level II QC Summary
Q20040148 TSS_LL Total Suspended Solids - Low RL 2.5
Page 49 of 50
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
TSS 0.1 mg/L 1 2.5 < 1/2 RDL

0
LO
0
0
rn
\a
.,..-14"..1 4-13

A„
I

Sample ID's & Descriptions:
Sample ID
Plant/Station
Collection
Date and Time
Collected By
Sample Descripth
2020006502
Asheville Airport
07-Apr-20
12:03 PM
Haley Seaton
ASA_MW-1A-A1
2020006530
Asheville Airport
07-Apr-20
11:18 AM
Haley Seaton
ASA_MW-2A-A1
2020006531
Asheville Airport
08-Apr-20
9:45 AM
Josh Stowe
ASA_MW-4A-A1
2020006532
Asheville Airport
07-Apr-20
1:18 PM
Haley Seaton
ASA_MW-5-A1
2020006533
Asheville Airport
07-Apr-20
10:35 AM
Haley Seaton
ASA_MW-6-A1
2020006534
Asheville Airport
07-Apr-20
1:00 PM
Josh Stowe
ASA_MW-7-A1
2020006535
Asheville Airport
07-Apr-20
11:55 AM
Josh Stowe
ASA_MW-8-A1
2020006536
Asheville Airport
07-Apr-20
9:50 AM
Josh Stowe
ASA_MW-9-A1
2020006537
Asheville Airport
08-Apr-20
9:55 AM
Josh Stowe
ASA_FD-2020040
2020006538
Asheville Airport
07-Apr-20
4:40 PM
Connor Zahora
ASA_FB-20200407-
2020006539
Asheville Airport
07-Apr-20
4:40 PM
Connor Zahora
ASA_EB-20200407-
11 Total Samples
Page 2 of 41

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals ® Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable.❑ Yes ❑ No
Report Sections Included:
Job Summary Report
❑ Sample Identification
d❑ Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
d❑ Analytical Laboratory QC Report
Page 3 of 41
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
© Chain of Custody
© Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 4/22/2020

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-1A-A1
Collection Date: 04/07/2020 12:03 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q
Total Alkalinity as CaCO3
17.3
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
17.3
mg/L
INORGANIC IONS BY IC -
Q20040189
Chloride
1A
mg/L
Sulfate
0.22
mg/L
MERCURY COLD VAPOR
IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040256
Aluminum (AI)
0.174
mg/L
Barium (Ba)
0.019
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
3.37
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.111
mg/L
Magnesium (Mg)
2.00
mg/L
Manganese (Mn)
0.006
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.858
mg/L
Sodium (Na)
2.57
mg/L
Strontium (Sr)
0.037
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
- 020040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS - 020040188
TDS
37.0
mg/L
Sample #: 2020006502
Matrix: GW WW
Page 4 of 41
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/09/2020 18:08
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:08
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:08
PARMSTR
0.1
1
EPA 300.0
04/09/2020 12:25
BGN9034
0.1
1
EPA 300.0
04/09/2020 12:25
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:21
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.1
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:09
DMFRANC
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 20:13
CWSPEN3
25
1
SM2540C
04/09/202010:44
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-1A-A1
Collection Date: 04/07/2020 12:03 PM
Analyse Result Units Qualifiers RDL
Total Susn ended Solids -Low RL 2.5 - 020040178
TSS 6.7 mg/L 2.5
Page 5 of 41
Sample #: 2020006502
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 SM2540D 04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-2A-A1
Collection Date: 04/07/2020 11:18 AM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040198
Total Alkalinity as CaCO3
16.6
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
16.6
mg/L
INORGANIC IONS BY IC -
Q2004018
Chloride
9,7
ma/L
Sulfate
< 0.1
mg/L
MERCURY ICOLD VAPOR)
IN WATER - 020040243
Mercury (Hg)
0.11
ug/L
TOTAL. RECOVERABLE METALS BY ICP - Q2004025
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
0.040
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
6.16
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Magnesium (Mg)
2.48
mg/L
Manganese (Mn)
0.048
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.07
mg/L
Sodium (Na)
3.45
mg/L
Strontium (Sr)
0.068
mg/L
Zinc (Zn)
0.012
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS - ❑20040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS - Q20040188
TDS
46.0
mg/L
Page 6 of 41
Sample #: 2020006530
Matrix: GW WW
Method Analysis Datefrime Analyst
5
1
SM 2320B-2011
04/09/2020 18:15
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:15
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:15
PARMSTR
0.1
1
EPA 300.0
04/09/2020 13:25
BGN9034
0.1
1
EPA 300.0
04/09/2020 13:25
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:23
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.1
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:23
DMFRANC
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
1
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 19:39
CWSPEN3
25
1
SM2540C
04/09/202010:46
GBSINGL

Certificate of Laboratory Analysis Page 7 of41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-2A-A1 Sample #: 2020006530
Collection Date: 04/07/2020 11:18 AM Matrix: GW WW
Analyse. Result Units Qualifiers RDL DF Method Analysis Daterrime Analyst
Total Suspended Solids - Low RL 2.5 - Q20040178
TSS < 2.5 mg/L 2.5 1 SM2540D 04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
Page 8 of41
This
report shall not be reproduced,
except in full.
Order # J20030210
Site: ASA MW-4A-A1
Sample #: 2020006531
Collection Date: 04/08/2020 09:45 AM
Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - g2004O299
Total Alkalinity as CaCO3
17.6
mg/L
5
1
SM 2320B-2011
04/15/2020 18:33
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320E-2011
04/15/2020 18:33
PARMSTR
Alkalinity, Bicarbonate
17.6
mg/L
5
1
SM 2320E-2011
04/15/2020 18:33
PARMSTR
INORGANIC IONS BY IC - Q20040265
Chloride
1.8
ma/L
0.1
1
EPA 300.0
04/14/2020 18:53
BGN9034
Sulfate
1.2
mg/L
0.1
1
EPA 300.0
04/14/2020 18:53
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 12:25
DMFRANC
T TAL RECOVERABLE METALS BY IC - Q20040256
Aluminum (AI)
0.070
mg/L
0.01
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Barium (Ba)
0.029
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Calcium (Ca)
0.248
mg/L
0.05
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Iron (Fe)
2.42
mg/L
0.01
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Magnesium (Mg)
0.235
mg/L
0.01
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Manganese (Mn)
1.16
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Potassium (K)
0.939
mg/L
0.1
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Sodium (Na)
6.48
mg/L
0.05
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
Zinc (Zn)
0.010
mg/L
0.005
1
EPA 200.7
04/15/2020 13:27
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS -
0200402 2
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Cobalt (Co)
34.7
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
Vanadium (V) Low Level
0.389
ug/L
0.3
1
EPA 200.8
04/17/2020 20:22
CWSPEN3
TOTAL DISSOLVED SOLIDS - Q20040250
TDS
< 25
mg/L
25
1
SM2540C
04/14/2020 10:54
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-4A-Al
Collection Date: 04/08/2020 09:45 AM
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - Q20040246
TSS < 2.5 mg/L 2.5
Sample #: 2020006531
Matrix: GW WW
Page 9 of 41
DF Method Analysis Date/Time Analyst
1 SM2540D 04/14/2020 09:42 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-5-Al
Collection Date: 04/07/2020 01:18 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY-- Q.20040198
Total Alkalinity as CaCO3
< 5
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
< 5
mg/L
INORGANIC IONS BY IC - Q2004 180
Chloride
2.2
mg/L
Sulfate
0.19
mg/L
MERCURY (COLD VAPOR)
IN WATER - g2004O243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q2004925
Aluminum (AI)
0.152
mg/L
Barium (Ba)
0.017
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
0.300
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.138
mg/L
Magnesium (Mg)
0.630
mg/L
Manganese (Mn)
0.043
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.580
mg/L
Sodium (Na)
2.21
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
0.007
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
- Q20040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS
- Q20040188
TDS
< 25
mg/L
Sample #: 2020006532
Matrix: GW WW
Page 10 of 41
Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/09/2020 18:18
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:18
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:18
PARMSTR
0.1
1
EPA 300.0
04/09/2020 15:33
BGN9034
0.1
1
EPA 300.0
04/09/2020 15:33
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:27
DMFRANC
0.01
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.05
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.05
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.01
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.01
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.1
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.05
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
0.005
1
EPA 200.7
04/15/2020 14:05
DMFRANC
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 20:30
CWSPEN3
25
1
SM2540C
04/09/202010:46
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-5-A1
Collection Date: 04/07/2020 01:18 PM
Analyte Result Units Qualifiers RDL DF
Total Suspended Solids -Low RL 2.5 - Q20040178
TSS 3.1 mg/L 2.5 1
Sample #: 2020006532
Matrix: GW WW
Page 11 of 41
Method Analysis Date/Time Analyst
SM2540D 04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-6-A1
Collection Date: 04/07/2020 10:35 AM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q20040
Total Alkalinity as CaCO3
11.7
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
11.7
mg/L
INORGANIC IONS BY IC - Q
4 180
Chloride
15
mall -
Sulfate
0.25
mg/L
MERCURY ICOLD VAPORa IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS
BY ICP - 020040256
Aluminum (Al)
0.031
mg/L
Barium (Ba)
0.047
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
5.53
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.682
mg/L
Magnesium (Mg)
2.69
mg/L
Manganese (Mn)
0.020
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.09
mg/L
Sodium (Na)
5.53
mg/L
Strontium (Sr)
0.071
mg/L
Zinc (Zn)
0.010
mg/L
TOTAL RECOVERABLE METALS
BY ICP-M3
- Q20040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS -
Q20040188
TDS
53.0
mg/L
Sample #: 2020006533
Matrix: GW WW
Page 12 of 41
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/09/2020 18:21
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:21
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:21
PARMSTR
0.3
3
EPA 300.0
04/09/2020 18:33
BGN9034
0.1
1
EPA 300.0
04/09/2020 18:33
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:30
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.1
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:31
DMFRANC
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 21:54
CWSPEN3
25
1
SM2540C
04109/202010:47
GBSINGL

Certificate of Laboratory Analysis Page 13 of41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-6-A1 Sample #: 2020006533
Collection Date: 04/07/2020 10:35 AM Matrix: GW WW
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - a20040178
TSS < 2.5 mg/L 2.5
DF Method
1 SM2540D
Analysis Date/Time Analyst
04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
Page 14of41
This report shall not be reproduced,
except in full.
Order # J20030210
Site: ASA_MW-7-Al
Sample #: 2020006534
Collection Date: 04/07/2020 01:00 PM
Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis DatefTime
Analyst
TOTAL ALKALINITY - Q200407
Total Alkalinity as CaCO3
9.40
mg/L
5
1
SM 2320B-2011
04/09/2020 18:24
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320E-2011
04/09/2020 18:24
PARMSTR
Alkalinity, Bicarbonate
9.40
mg/L
5
1
SM 2320E-2011
04/09/2020 18:24
PARMSTR
INORGANIC IONS BY IC - Q20040180
Chloride
14
ma/L
0.3
3
EPA 300.0
04/09/2020 18:48
BGN9034
Sulfate
0.16
mg/L
0.1
1
EPA 300.0
04/09/2020 18:48
BGN9034
MERCURY (COLD VAPOR) IN WATER - 020040243
Mercury (Hg)
40.05
ug/L
0.05
1
EPA 245.1
04/13/2020 12:32
DMFRANC
TOTAL REQ0VERABLE METALS BY ICP - 02004025
Aluminum (AI)
0.020
mg/L
0.01
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Barium (Ba)
0.036
mglL
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Calcium (Ca)
2.69
mg/L
0.05
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Iron (Fe)
0.013
mg/L
0.01
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Magnesium (Mg)
1.86
mg/L
0.01
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Manganese (Mn)
0.061
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Potassium (K)
1.21
mg/L
0.1
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Sodium (Na)
6.88
mg/L
0.05
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Strontium (Sr)
0.031
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
Zinc (Zn)
0.006
mg/L
0.005
1
EPA 200.7
04/15/2020 13:36
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS
- Q20040262
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2020 20:38
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040188
TDS
44.0
mg/L
25
1
SM2540C
04109/202010:47
GBSINGL

Certificate of Laboratory Analysis Page 15 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-7-A1 Sample #: 2020006534
Collection Date: 04/07/2020 01:00 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
Total Suspended Solids - Low RL 2.5 - Q20040178
TSS < 2.5 mg/L 2.5 1 SM2540D 04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-8-A1
Collection Date: 04/07/2020 11:55 AM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040198
Total Alkalinity as CaCO3
< 5
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
< 5
mg/L
INORGANIC IONS BY IC -
22904 1180
Chloride
55
mg/L
Sulfate
0.26
mg/L
MERCURY (COLD VAPOR)
IN WATER - 02004Q243
Mercury (Hg)
0.10
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040256
Aluminum (AI)
0.618
mg/L
Barium (Ba)
0.516
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
1.70
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Magnesium (Mg)
4.58
mg/L
Manganese (Mn)
1.81
mg/L
Nickel (Ni)
0.007
mg/L
Potassium (K)
2.91
mg/L
Sodium (Na)
24.0
mg/L
Strontium (Sr)
0.032
mg/L
Zinc (Zn)
0.043
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
- Q20040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
18.9
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS - 020040188
TDS
113
mg/L
Sample #: 2020006535
Matrix: GW WW
Page 16 of 41
Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/09/2020 18:27
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:27
PARMSTR
5
1
SM 2320B-2011
04/09/2020 18:27
PARMSTR
1.1
11
EPA 300.0
04/09/2020 19:18
BGN9034
0.1
1
EPA 300.0
04/09/2020 19:18
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:34
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.1
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:48
DMFRANC
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 20:47
CWSPEN3
25
1
SM2540C
04/09/202010:47
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-8-Al
Collection Date: 04/07/2020 11:55 AM
Analyte Result Units Qualifiers RDL
Total Suspended Solids -Low RI-2.5 - Q20040178
TSS < 2.5 mg/L 2.5
Sample #: 2020006535
Matrix: GW WW
DF Method
Page 17 of 41
Analysis Date/Time Analyst
04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-9-Al
Collection Date: 04/07/2020 09:50 AM
Sample #: 2020006536
Matrix: GW WW
Page 18 of 41
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Daterrime
Analyst
TOTAL ALKALINITY - 02004019
Total Alkalinity as CaCO3
38.9
mg/L
5
1
SM 2320B-2011
04/09/2020 18:30
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/09/2020 18:30
PARMSTR
Alkalinity, Bicarbonate
38.9
mg/L
5
1
SM 2320B-2011
04/09/2020 18:30
PARMSTR
INORGANIC IONS BY I
- 02004018
Chloride
28
mg/L
0.6
6
EPA 300.0
04/09/2020 19:03
BGN9034
Sulfate
23
mg/L
0.6
6
EPA 300.0
04/09/2020 19:03
BGN9034
MERCURY (COLD VAPOR IN WATER - 020040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 12:36
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - Q20040256
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Barium (Ba)
0.034
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Calcium (Ca)
7.61
mg/L
0.05
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Iron (Fe)
0.134
mg/L
0.01
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Magnesium (Mg)
5.22
mg/L
0.01
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Manganese (Mn)
4.81
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Potassium (K)
7.80
mg/L
0.1
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Sodium (Na)
22.3
mg/L
0.05
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Strontium (Sr)
0.068
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 13:52
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040262
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Cobalt (Co)
1.07
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Molybdenum (Mo)
3.26
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2020 21:29
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040188
TDS
148
mg/L
25
1
SM2540C
04109/202010:48
GBSINGL

Certificate of Laboratory Analysis Page 19of41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA MW-9-Al Sample #: 2020006536
Collection Date: 04/07/2020 09:50 AM Matrix: GW WW
Analyse Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
Total Suspended Solids - Low RL 2.5 - Q20040178
TSS < 2.5 mg/L 2.5 1 SM2540D 04/09/2020 06:57 GBSINGL

Certificate of Laboratory Analysis Page 20 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA FD-20200408-1 Duplicate
Collection Date: 04/08/2020 09:55 AM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q20040299
Total Alkalinity as CaCO3
17.1
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
17.1
mg/L
INORGANIC IONS BY IC - 020040265
Chloride
1.7
ma/L
Sulfate
1.0
mg/L
MERCURY (COLD VAPOR) IN
WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - 020040256
Aluminum (AI)
0.070
mg/L
Barium (Ba)
0.030
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
0.241
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
2.28
mg/L
Magnesium (Mg)
0.239
mg/L
Manganese (Mn)
1.19
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.979
mg/L
Sodium (Na)
5.83
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
0.006
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040262
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
36.5
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
0.361
ug/L
TOTAL DISSOLVED SOLIDS
-_020040280
TDS
37.0
mg/L
Sample #: 2020006537
Matrix: GW WW
Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/15/2020 18:37
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:37
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:37
PARMSTR
0.1
1
EPA 300.0
04/14/2020 19:08
BGN9034
0.1
1
EPA 300.0
04/14/2020 19:08
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:39
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.01
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.1
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.05
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
0.005
1
EPA 200.7
04/15/2020 13:57
DMFRANC
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
1
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
0.2
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
0.3
1
EPA 200.8
04/17/2020 21:37
CWSPEN3
25
1
SM2540C
04/15/202010:40
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA FD-20200408-1 Duplicate
Collection Date: 04/08/2020 09:55 AM
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - Q20040277
TSS < 2.5 mg/L 2.5
Page 21 of 41
Sample #: 2020006537
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 SM2540D 04/15/2020 07:35 GBSINGL

Certificate of Laboratory Analysis Page 22 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA_FB-20200407-1640 Field Blank Sample #: 2020006538
Collection Date: 04/07/2020 04:40 PM Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Daterrime
Analyst
TOTAL ALKALINITY - Q2994019$
Total Alkalinity as CaCO3
< 5
mg/L
5
1
SM 2320E-2011
04/09/2020 18:34
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 232OB-2011
04/09/2020 18:34
PARMSTR
Alkalinity, Bicarbonate
< 5
mg/L
5
1
SM 2320B-2011
04/09/2020 18:34
PARMSTR
INORGANIC IONS BY IC - 020040180
Chloride
< 0.1
mg/L
0.1
1
EPA 300.0
04/09/2020 17:18
BGN9034
Sulfate
< 0.1
mg/L
0.1
1
EPA 300.0
04/09/2020 17:18
BGN9034
MERCURY VAPOR) IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 12:54
DMFRANC
TOTAL RECOVERABLE METALS
BY ICP - Q20040256
Aluminum (Al)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Barium (Ba)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Calcium (Ca)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Magnesium (Mg)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Potassium (K)
< 0.1
mg/L
0.1
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Sodium (Na)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:01
DMFRANC
TOTAL RECOVERABLE METALS
BY ICP-MS - a2004O262
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2020 21:45
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2020 21:45
CWSPEN3

Certificate of Laboratory Analysis Page 23 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Site: ASA EB-20200407-1640 Equipment Blank Sample #: 2020006539
Collection Date: 04/07/2020 04:40 PM Matrix: GW WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - Q20040198
Total Alkalinity as CaCO3
< 5
mg/L
5
1
SM 2320B-2011
04/09/2020 18:37
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/09/2020 18:37
PARMSTR
Alkalinity, Bicarbonate
< 5
mg/L
5
1
SM 2320B-2011
04/09/2020 18:37
PARMSTR
INORGANIC IONS BY IC - Q20040180
Chloride
< 0.1
mg/L
0.1
1
EPA 300.0
04/09/2020 17:33
BGN9034
Sulfate
< 0.1
mg/L
0.1
1
EPA 300.0
04/09/2020 17:33
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 12:56
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - Q20040256
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Barium (Ba)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Calcium (Ca)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/1512020 14:19
DMFRANC
Magnesium (Mg)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Potassium (K)
< 0.1
mg/L
0.1
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Sodium (Na)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 14:19
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040262
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2020 22:28
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2020 22:28
CWSPEN3

Certificate of Laboratory Analysis Page 24 of41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040198 ALK CarbBicarb TOTAL ALKALINITY
Duplicate # 1
Parent Sample: J20030210 -- 2020006502
Parameter
Measured
Final
Units:
Dil
Limit Ranee
RPD Qualifier
Alkalinity, Bicarbonate
17.5
17.5
mg/L
1
0 - 20%
0.861
Alkalinity, Carbonate
0
0
mg/L
1
0- 20%
0
Total Alkalinity as CaCO3
17.5
17.5
mg/L
1
0 - 20%
0.861
LCS # 1
Parameter
Measured
Final
Units:
Dil
Saike % Recovery LCL UCL
Qualifier
Total Alkalinity as CaCO3
104
104
mg/L
1
105 99.3 85 115

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040299 ALK_CarbBicarb TOTAL ALKALINITY
Duplicate # 1
Parameter
Measured
Final
Units:
Alkalinity, Bicarbonate
12.3
12.3
mg/L
Alkalinity, Carbonate
0
0
mg/L
Total Alkalinity as CaCO3
12.3
12.3
mg/L
LCS # 1
Parameter
Measured
Final
Units:
Total Alkalinity as CaCO3
105
105
mg/L
Page 25 of 41
Parent Sample: J20030212 -- 2020006508
Dil
Limit Rami
RPD Qualifier
1
0 - 20%
0.244
1
0-20%
0
1
0 - 20%
0.244
Dil
Spike % Recovery LCL UCL
Qualifier
1
105 99.9 85 115

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040180 Dionex INORGANIC IONS BY IC
Blank # 1
Page 26 of 41
Parameter
Measured
Final
Units:
D11
RDL
Relative Concentration
Qualifier
Chloride
0
0
mg/L
1
0.1
< 1/2 RDL
Sulfate
0
0
mg/L
1
0.1
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
Chloride
4.87
4.87
mg/L
1
5
97.3 90
110
Sulfate
4.89
4.89
mg/L
1
5
97.9 90
110
MS # 1
Parent Sample:
J20030210
-- 2020006502
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
Chloride
3.54
3.54
mg/L
1
2
97.7 80
120
Sulfate
2.05
2.05
mg/L
1
2
91.9 80
120
MSD # 1
Parent Sample:
J20030210
-- 2020006502
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
RPD Qualifier
Chloride
3.57
3.57
mg/L
1
2
98.9 80
120
1.22
Sulfate
2.08
2.08
mg/L
1
2
93 80
120
1.24

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040265 Dionex INORGANIC IONS BY IC
Blank # 1
LCS # 1
MS # 1
MSD # 1
Parameter Measured Final
Chloride 0 0
Sulfate 0 0
Parameter Measured Final
Chloride 4.88 4.88
Sulfate 4.92 4.92
Parameter Measured Final
Chloride 3.87 77.3
Sulfate 6.32 126
Parameter Measured Final
Chloride 3.88 77.6
Sulfate 6.37 127
Page 27 of 41
Units:
Dil
RDL
Relative Concentration
Qualifier
mg/L
1
0.1
< 1/2 RDL
mg/L
1
0.1
< 1/2 RDL
Units:
Dil
Saike
% Recovery LCL
UCL
Qualifier
mg/L
1
5
97.5 90
110
-
mg/L
1
5
98.4 90
110
-
Parent Sample:
J20040249
-- 2020009798
Units:
Dil
Saike
% Recovery LCL
UCL
Qualifier
mg/L
20
40
101 80
120
-
mg/L
20
40
99.1 80
120
Parent Sample:
J20040249
-- 2020009798
Units:
Dil
Soike
% Recovery LCL
UCL
RPD Qualifier
mg/L
20
40
102 80
120
0.775
mg/L
20
40
102 80
120
2.62 -

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040243 HG 245.1 MERCURY (COLD VAPOR) IN WATER
Blank # 1
Parameter Measured Final
Mercury (Hg) -0.013 -0.013
Blank # 2
Parameter Measured Final
Mercury (Hg) -0.009 -0.009
LCS # 1
Parameter Measured Final
Mercury (Hg) 2 2
LCS # 2
Units: Dil RDL Relative Concentration
ug/L 1 0.05 < 1/2 RDL
Units: Dil RDL Relative Concentration
ug/L 1 0.05 < 1/2 RDL
Units: Dil Sgike % Recovery LCL UCL
ug/L 1 2 100 85 115
Page 28 of 41
ualifier
ualifier
Qualifier
Parameter
Measured
Final
Units:
Dil
Soike
% Recover LCL
UCL Qualifier
Mercury (Hg)
1.99
1.99
ug/L
1
2
99.5 85
115
MS # 1
Parent Sample:
J20020127 -- 2020004467
Parameter
Measured
Final
Units:
Dil
Soike
% Recove3_}. LCL
UCL Qualifier
Mercury (Hg)
0.695
13.9
ug/L
20
20
71 70
130
MSD # 1
Parent Sample:
J20020127 -- 2020004467
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery LCL
UCL RPD Qualifier
Mercury (Hg)
0.694
13.9
ug/L
20
20
70.9 70
130 0.211 -

Certificate of Laboratory Analysis
This report shah not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040256 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Page 29 of 41
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Aluminum (AI)
0.00127
0.00127
mg/L
1
0.01
< 1/2 RDL
Barium (Ba)
-0.000342
-0.000342
mg/L
1
0.005
< 1/2 RDL
Boron (B)
0.00185
0.00185
mg/L
1
0.05
< 1/2 RDL
Calcium (Ca)
0.00489
0.00489
mg/L
1
0.05
< 1/2 RDL
Chromium (Cr)
-0.000759
-0.000759
mg/L
1
0.005
< 1/2 RDL
Copper (Cu)
-0.000821
-0.000821
mg/L
1
0.005
< 112 RDL
Iron (Fe)
-0.00144
-0.00144
mg/L
1
0.01
< 1/2 RDL
Magnesium (Mg)
-0.00116
-0.00116
mg/L
1
0.01
< 1/2 RDL
Manganese (Mn)
-0.000319
-0.000319
mg/L
1
0.005
< 1/2 RDL
Nickel (Ni)
-0.000402
-0.000402
mg/L
1
0.005
< 1/2 RDL
Potassium (K)
-0.0095
-0.0095
mg/L
1
0.1
< 1/2 RDL
Sodium (Na)
-0.000327
-0.000327
mg/L
1
0.05
< 1/2 RDL
Strontium (Sr)
-0.000339
-0.000339
mg/L
1
0.005
< 1/2 RDL
Zinc (Zn)
-0.000526
-0.000526
mg/L
1
0.005
< 112 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery
LCL
UCL Qualifier
Aluminum (Al)
4.96
4.96
mg/L
1
5
99.3
85
115
Barium (Ba)
4.92
4.92
mg/L
1
5
98.4
85
115
Boron (B)
5.14
5.14
mg/L
1
5
103
85
115
Calcium (Ca)
5.21
5.21
mg/L
1
5
104
85
115
Chromium (Cr)
5.22
5.22
mg/L
1
5
104
85
115
Copper (Cu)
5.08
5.08
mg/L
1
5
102
85
115
Iron (Fe)
5.07
5.07
mg/L
1
5
101
85
115
Magnesium (Mg)
5.12
5.12
mg/L
1
5
102
85
115 -
Manganese (Mn)
5.18
5.18
mg/L
1
5
104
85
115 -
Nickel (Ni)
5.09
5.09
mg/L
1
5
102
85
115 -
Potassium (K)
5.13
5.13
mg/L
1
5
103
85
115 -
Sodium (Na)
5.09
5.09
mg/L
1
5
102
85
115
Strontium (Sr)
4.77
4.77
mg/L
1
5
95.5
85
115
Zinc (Zn)
5.23
5.23
mg/L
1
5
105
85
115
MS # 1
Parent Sample:
J20030210 -- 2020006502
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5.27
5.27
mg/L
1
5
102
70
130 -
Barium (Ba)
5.08
5.08
mg/L
1
5
101
70
130 -
Boron (B)
5.27
5.27
mg/L
1
5
105
70
130 -
Calcium (Ca)
8.65
8.65
mg/L
1
5
106
70
130 -
Chromium (Cr)
5.38
5.38
mg/L
1
5
108
70
130 -
Copper (Cu)
5.23
5.23
mg/L
1
5
105
70
130 -

Certificate of Laboratory Analysis Page 30 of41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040256 ICP_TRM TOTAL RECOVERABLE
METALS BY
ICP
MS # 1
Parent Sample:
J20030210
-- 2020006502
Parameter
Measured
Final
Units:
Dil
Soike
° Recover
LCL
UCL
Qualifier
Iron (Fe)
5.34
5.34
mg/L
1
5
105
70
130
-
Magnesium (Mg)
7.18
7.18
mg/L
1
5
104
70
130
-
Manganese (Mn)
5.36
5.36
mg/L
1
5
107
70
130
-
Nickel (Ni)
5.23
5.23
mg/L
1
5
105
70
130
-
Potassium (K)
6.13
6.13
mg/L
1
5
105
70
130
-
Sodium (Na)
7.77
7.77
mg/L
1
5
104
70
130
-
Strontium (Sr)
4.83
4.83
mg/L
1
5
95.8
70
130
-
Zinc (Zn)
5.38
5.38
mg/L
1
5
108
70
130
-
MSD # 1
Parent Sample:
J20030210
-- 2020006502
Parameter
Measured
Final
Units:
DiI
Saike
% Recovery
LCL
UCL
RPD Qualifier
Aluminum (Al)
5.23
5.23
mg/L
1
5
101
70
130
0.685 -
Barium (Ba)
5.02
5.02
mg/L
1
5
100
70
130
1.27 -
Boron (B)
5.27
5.27
mg/L
1
5
105
70
130
0.114 -
Calcium (Ca)
8.72
8.72
mg/L
1
5
107
70
130
0.852 -
Chromium (Cr)
5.36
5.36
mg/L
1
5
107
70
130
0.317 -
Copper (Cu)
5.2
5.2
mg/L
1
5
104
70
130
0.518 -
Iron (Fe)
5.33
5.33
mg/L
1
5
104
70
130
0.3 -
Magnesium (Mg)
7.23
7.23
mg/L
1
5
105
70
130
0.597 -
Manganese (Mn)
5.33
5.33
mg/L
1
5
106
70
130
0.58 -
Nickel (Ni)
5.21
5.21
mg/L
1
5
104
70
130
0.422 -
Potassium (K)
6.14
6.14
mg/L
1
5
106
70
130
0.13 -
Sodium (Na)
7.82
7.82
mg/L
1
5
105
70
130
0.603 -
Strontium (Sr)
4.97
4.97
mg/L
1
5
98.7
70
130
2.94 -
Zinc (Zn)
5.36
5.36
mg/L
1
5
107
70
130
0.279 -
MS # 2
Parent Sample:
J20030210
-- 2020006532
Parameter
Measured
Final
Units:
Dil
5nike
% Recovery
LCL
UCI,
Qualifier
Aluminum (AI)
5.22
5.22
mg/L
1
5
101
70
130
-
Barium (Ba)
4.97
4.97
mg/L
1
5
99.1
70
130
-
Boron (B)
5.31
5.31
mg/L
1
5
106
70
130
-
Calcium (Ca)
5.68
5.68
mg/L
1
5
108
70
130
-
Chromium (Cr)
5.41
5.41
mg/L
1
5
108
70
130
-
Copper (Cu)
5.24
5.24
mg/L
1
5
105
70
130
-
Iron (Fe)
5.38
5.38
mg/L
1
5
105
70
130
-
Magnesium (Mg)
5.9
5.9
mg/L
1
5
105
70
130
-
Manganese (Mn)
5.41
5.41
mg/L
1
5
107
70
130
-
Nickel (Ni)
5.23
5.23
mg/L
1
5
105
70
130
-
Potassium (K)
5.9
5.9
mg/L
1
5
106
70
130
-
Sodium (Na)
7.4
7.4
mg/L
1
5
104
70
130
-

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040256 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
MS # 2
Parameter
Measured
Final
Units:
Strontium (Sr)
4.81
4.81
mg/L
Zinc (Zn)
5.42
5.42
mg/L
MSD # 2
Parameter
Measured
Final
Units:
Aluminum (Al)
5.27
5.27
mg/L
Barium (Ba)
4.99
4.99
mg/L
Boron (B)
5.37
5.37
mg/L
Calcium (Ca)
5.71
5.71
mg/L
Chromium (Cr)
5.45
5.45
mg/L
Copper (Cu)
5.27
5.27
mg/L
Iron (Fe)
5.41
5.41
mg/L
Magnesium (Mg)
5.92
5.92
mg/L
Manganese (Mn)
5.45
5.45
mg/L
Nickel (Ni)
5.25
5.25
mg/L
Potassium (K)
5.92
5.92
mg/L
Sodium (Na)
7.41
7.41
mg/L
Strontium (Sr)
4.87
4.87
mg/L
Zinc (Zn)
5.46
5.46
mg/L
Page 31 of 41
Parent Sample:
J20030210 -- 2020006532
Dil
Sgike
% Recover v LCL
UCL
Qualifier
1
5
96.1 70
130
-
1
5
108 70
130
-
Parent Sample:
J20030210
-- 2020006532
Dil
Sgike
% Recovery LCL
UCL
RPD Qualifier
1
5
102 70
130
0.877
1
5
99.4 70
130
0.321
1
5
107 70
130
1.18
1
5
108 70
130
0.597
1
5
109 70
130
0.626
1
5
105 70
130
0.438
1
5
105 70
130
0.519
1
5
106 70
130
0.288
1
5
108 70
130
0.645
1
5
105 70
130
0.515
1
5
107 70
130
0.355 -
1
5
104 70
130
0.0811 -
1
5
97.4 70
130
1.32 -
1
5
109 70
130
0.661 -

Certificate of Laboratory Analysis Page 32 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040262 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
Parameter
Measured
Final
Units:
DiI
RDL
Relative Concentration
Qualifier
Antimony (Sb)
-0.046
-0.046
ug/L
1
1
< 1/2 RDL
Arsenic (As)
-0.005
-0.005
ug/L
1
1
< 1/2 RDL
Beryllium (Be)
-0.003
-0.003
ug/L
1
1
< 1/2 RDL
Cadmium (Cd)
0
0
ug/L
1
1
< 1/2 RDL
Cobalt (Co)
0
0
ug/L
1
1
< 1/2 RDL
Lead (Pb)
0
0
ug/L
1
1
< 112 RDL
Molybdenum (Mo)
-0.012
-0.012
ug/L
1
1
< 1/2 RDL
Selenium (Se)
-0.276
-0.276
ug/L
1
1
< 1/2 RDL
Thallium (TI) Low Level
0.017
0.017
ug/L
1
0.2
< 1/2 RDL
Vanadium (V) Low Level
0.034
0.034
ug/L
1
0.3
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
1i1
Soike
% Recover:
LCL
UCL
Qualifier
Antimony (Sb)
46.9
46.9
ug/L
1
50
93.8
85
115
Arsenic (As)
46.9
46.9
ug/L
1
50
93.8
85
115
Beryllium (Be)
46.9
46.9
ug/L
1
50
93.8
85
115
Cadmium (Cd)
47.9
47.9
ug/L
1
50
95.8
85
115
Cobalt (Co)
48
48
ug/L
1
50
96
85
115
Lead (Pb)
48.5
48.5
ug/L
1
50
96.9
85
115
Molybdenum (Mo)
48.6
48.6
ug/L
1
50
97.1
85
115
Selenium (Se)
45.9
45.9
ug/L
1
50
91.8
85
115
Thallium (TI) Low Level
47.6
47.6
ug/L
1
50
95.2
85
115
Vanadium (V) Low Level
47.5
47.5
ug/L
1
50
95.1
85
115
MS # 1
Parent
Sample:
J20030210
-- 2020006530
Parameter
Measured
Final
Units:
Dil
Soike
% Recover •
LCL
UCL
Qualifier
Antimony (Sb)
48.3
48.3
ug/L
1
50
96.7
70
130
-
Arsenic (As)
46.7
46.7
ug/L
1
50
93.3
70
130
-
Beryllium (Be)
47.6
47.6
ug/L
1
50
95.1
70
130
-
Cadmium (Cd)
47.9
47.9
ug/L
1
50
95.8
70
130
-
Cobalt (Co)
47.6
47.6
ug/L
1
50
94.2
70
130
-
Lead (Pb)
48.9
48.9
ug/L
1
50
97.7
70
130
-
Molybdenum (Mo)
49
49
ug/L
1
50
98
70
130
-
Selenium (Se)
46.2
46.2
ug/L
1
50
92.9
70
130
-
Thallium (TI) Low Level
48.3
48.3
ug/L
1
50
96.5
70
130
-
Vanadium (V) Low Level
48.8
48.8
ug/L
1
50
97.4
70
130
-
MSD # 1
Parent
Sample:
J20030210
-- 2020006530
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery
LCL
UCL
RPD Qualifier
Antimony (Sb)
49.5
49.5
ug/L
1
50
99
70
130
2.35 -

Level II QC Summary
Q20040262 IMS_TRM
MSD # 1
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
TOTAL RECOVERABLE METALS BY ICP-MS
Parameter
Measured
Final
Units:
Dil
Spike
Arsenic (As)
48.4
48.4
ug/L
1
50
Beryllium (Be)
48.5
48.5
ug/L
1
50
Cadmium (Cd)
49.6
49.6
ug/L
1
50
Cobalt (Co)
49.4
49.4
ug/L
1
50
Lead (Pb)
50
50
ug/L
1
50
Molybdenum (Mo)
50.2
50.2
ug/L
1
50
Selenium (Se)
47.8
47.8
ug/L
1
50
Thallium (TI) Low Level
49.4
49.4
ug/L
1
50
Vanadium (V) Low Level
50
50
ug/L
1
50
MS # 2
Parameter
Measured
Final
Units:
Dil
Spike
Antimony (Sb)
49.5
49.5
ug/L
1
50
Arsenic (As)
47.5
47.5
ug/L
1
50
Beryllium (Be)
49
49
ug/L
1
50
Cadmium (Cd)
48.9
48.9
ug/L
1
50
Cobalt (Co)
48.8
48.8
ug/L
1
50
Lead (Pb)
50
50
ug/L
1
50
Molybdenum (Mo)
49.9
49.9
ug/L
1
50
Selenium (Se)
47.6
47.6
ug/L
1
50
Thallium (TI) Low Level
49.1
49.1
ug/L
1
50
Vanadium (V) Low Level
49.8
49.8
ug/L
1
50
MSD # 2
Parameter
Measured
Final
Units:
Dil
Spike
Antimony (Sb)
48.4
48.4
ug/L
1
50
Arsenic (As)
46.9
46.9
ug/L
1
50
Beryllium (Be)
46.1
46.1
ug/L
1
50
Cadmium (Cd)
48.5
48.5
ug/L
1
50
Cobalt (Co)
48
48
ug/L
1
50
Lead (Pb)
48.8
48.8
ug/L
1
50
Molybdenum (Mo)
48.8
48.8
ug/L
1
50
Selenium (Se)
45.7
45.7
ug/L
1
50
Thallium (TI) Low Level
48.1
48.1
ug/L
1
50
Vanadium (V) Low Level
48.3
48.3
ug/L
1
50
Page 33 of 41
Parent Sample: J20030210 -- 2020006530
Y. Recover•,
LCL
UCL
RPD Qualifier
96.7
70
130
3.54 -
97
70
130
2.06 -
99.1
70
130
3.47 -
97.7
70
130
3.6 -
99.9
70
130
2.26 -
100
70
130
2.47 -
96
70
130
3.3 -
98.8
70
130
2.34 -
99.8
70
130
2.39 -
Parent Sample:
J20030210
-- 2020006533
% Recover v
LCL
UCL
Qualifier
99.1
70
130
94.9
70
130
97.3
70
130
-
97.6
70
130
-
96.6
70
130
-
99.8
70
130
-
99.9
70
130
-
95.8
70
130
-
98.2
70
130
-
99.2
70
130
-
Parent Sample: J20030210 -- 2020006533
% Recover,
LCL
UCL
RPD Qualifier
96.8
70
130
2.25 -
93.7
70
130
1.31 -
91.7
70
130
6.01 -
96.9
70
130
0.814 -
94.9
70
130
1.78 -
97.5
70
130
2.39 -
97.6
70
130
2.36 -
91.9
70
130
4.11 -
96.1
70
130
2.08 -
96.4
70
130
2.94 -

Certificate of Laboratory Analysis
Page 34of41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040188 TDS
TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentratoo
Qualifier
TDS
2
mg/L
1
25 < 1/2 RDL
Blank # 2
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
7
mg/L
1
25 < 1/2 RDL
Blank # 3
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
4
mg/L
1
25 < 1/2 RDL
Duplicate # 1
Parent Sample:
J20030022 --
2020005591
Parameter
Measured
Final
Units:
Dil
LLmit Rance
RPD Qualifier
TDS
315
mg/L
1
0 - 10%
1.6
Duplicate # 2
Parent Sample:
J20030022 --
2020005594
Parameter
Measured
Final
Units:
Dil
Limit Rtn�,,e
RPD Qualifier
TDS
303
mg/L
1
0 - 10%
1.31 -
Duplicate # 3
Parent Sample:
J20030141 --
2020006117
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD Qualifier
TDS
101
mg/L
1
0 - 10%
0 -
Duplicate # 4
Parent Sample:
J20030178 --
2020006299
Parameter
Measured
Final
Units:
Dil
Limit Rani,, e
RPD Qualifier
TDS
421
mg/L
1
0 - 10%
0.476 -
Duplicate # 5
Parent Sample:
J20030210 -- 2020006502
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD Qualifier
TDS
40
mg/L
1
0 - 10%
7.79 -
LCS # 1
Parameter
Measured
Final
Units:
Dil
Soike % Recovery LCL
UCL
Qualifier
TDS
992
mglL
1
1000 99.2 90
110

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Page 35 of 41
Level 11 QU Nummary
Q20040250 TDS TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
TDS 1 mg/L 1 25 < 1/2 RDL
Blank # 2
Parameter
Measured
Final
TDS
0
Duplicate # 1
Parameter
Measured
Final
TDS
26
Duplicate # 2
Parameter
Measured
Final
TDS
1480
Duplicate # 3
Parameter
Measured
Final
TDS
488
Duplicate # 4
Parameter
Measured
Final
TDS
429
LCS # 1
Parameter Measured Final
TDS 979
Units:
Dil
RDL
Relative Concentration
Qualifier
mg/L
1
25
< 1/2 RDL
Parent Sample:
J20030210 -- 2020006531
Units:
Dil
Limit Ram RPD Qualifier
mg/L
1
0 - 10% 8 -
Parent Sample:
J20040216 -- 2020009536
Units:
Dil
Limit RanaRPD Qualifier
mg/L
1
0 - 10% 0.673 -
Parent Sample:
J20040216 -- 2020009537
Units:
Dil
Limit Ran,RPD Qualifier
mg/L
1
0 - 10% 1.42 -
Parent Sample:
J20040216 -- 2020009538
Units:
Dil
Limit RantRPD Qualifier
mg/L
1
0 - 10% 0.928
Units:
Dil
Soike
% Recover; LCL
UCL Qualifier
mg/L
1
1000
97.9 90
110

Certificate of Laboratory Analysis Page 36of41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040280 TDS TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter Measured
Final
Units:
Dil
RDL
Relative Concentratwo
Qualifier
TDS
3
mg/L
1
25
< 1/2 RDL
Blank # 2
Parameter Measured
Final
Units:
Dil
RDL
Relative Concentratio
Qualifier
TDS
3
mg/L
1
25
< 1/2 RDL
Duplicate # 1
Parent Sample:
J20030210 --
2020006537
Parameter Measured
Final
Units:
Dil
Limit Ranee
RPD
Qualifier
TDS
34
mg/L
1
0 - 10%
8.45
-
Duplicate # 2
Parent Sample:
J20030213 --
2020006509
Parameter Measured
Final
Units:
Dil
Limit Ranee
RPD
Qualifier
TDS
68
mg/L
1
0 - 10%
15
R1
Duplicate # 3
Parent Sample:
J20030213 --
2020006570
Parameter Measured
Final
Units:
Dil
j_imit Ranee
RPD
Qualifier
TDS
31
mg/L
1
0 -10%
9.23
-
Duplicate # 4
Parent Sample:
J20030213 --
2020006571
Parameter Measured
Final
Units:
Dil
Limit Ranee
RPD
Qualifier
TDS
71
mg/L
1
0 - 10%
1.4
LCS # 1
Parameter Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
TDS
993
mg/L
1
1000
99.3 90
110
Qualifiers:
R1 Relative Percent Difference exceeded method acceptance
limits.

Certificate of Laboratory Analysis Page 37 of 41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040178 TSS_LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
TSS 0 mg/L 1 2.5 < 1/2 RDL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040246 TSS_LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter Measured Final
TSS 0
Duplicate # 1
Parameter Measured Final
TSS 0.4
LCS # 1
LCSD # 1
Parameter Measured Final
TSS 45.2
Page 38 of 41
Units: Dil RDL Relative Concentratio Qualifier
mg/L 1 2.5 < 1/2 RDL
Parent Sample: J20030206 -- 2020006487
Units: MI Limit Ramle RPD Qualifier
mg/L 1 120 R
Units: Dig Spike % Recovery LCL UCL
mg/L 1 50 90.4 90 110
Parameter Measured Final Units: Dil Spike % Recovery LCL UCL
TSS 50.8 mg/L 1 50 102 90 110
Qualifiers:
R % RPD indeterminate due to low concentration in the parent sample.
Qualifier
RPD Qualifier
11.7 -

Certificate of Laboratory Analysis Page 39 of41
This report shall not be reproduced, except in full.
Order # J20030210
Level II QC Summary
Q20040277 TSS_LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
TSS 0 mg/L 1 2.5 < 1/2 RDL

Page 40 of 41
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Page 41 of 41

GROUNDWATER QUALITY MONITORING 0lAA'IiMEIROF F3MpONMUITALQUALIIY
COMPLIANCE REPORT FORM blwvvi aFwaTFA g11ALNY-INF R TION FROCEMNIG UNIT
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IMAh noted on the reportarc for reference only.

DUKE Analytical Laboratory Page 1 of34
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J20030212
ASHEVILLE AIRPORT - AIRPORT FILL AREA III - (IN-HOUSE)
B Allison, F Holt,B Moeller, T Hunsucker,H Seaton
Lab Contact: Peggy Kendall
Phone: [phone]
Report Authorized By: a,i.- ate: 4/22/2020
(Signature) P"."
Peg 14d,11
Program Comments:
Per Josh Stowe, the collection time for ASA_MW-7-A3 was 12:00, omitted on the COC.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 2 of 34
Collection
Sample ID
Plant/Station
Date and Time
Collected By
Sample Description
2020006508
Asheville Airport
08-Apr-20
4:25 PM
Josh Stowe
ASA_MW-1-A3
2020006555
Asheville Airport
08-Apr-20
3:22 PM
Haley Seaton
ASA_MW-2-A3
2020006556
Asheville Airport
08-Apr-20
1:59 PM
Haley Seaton
ASA_MW-3-A3
2020006557
Asheville Airport
08-Apr-20
12:37 PM
Haley Seaton
ASA_MW-4-A3
2020006558
Asheville Airport
08-Apr-20
10:28 AM
Haley Seaton
ASA_MW-5-A3
2020006559
Asheville Airport
07-Apr-20
2:55 PM
Haley Seaton
ASA_MW-6-A3
2020006560
Asheville Airport
08-Apr-20
12:00 PM
Josh Stowe
ASA_MW-7-A3
2020006561
Asheville Airport
08-Apr-20
Haley Seaton
ASA_FD-20200408-1
2020006562
Asheville Airport
08-Apr-20
2:00 PM
Haley Seaton
ASA_FB-20200408-1400
9 Total Samples

Page 3 of 34
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable.
Report Sections Included:
❑ Job Summary Report
d❑ Sample Identification
© Technical Validation of Data Package
Analytical Laboratory Certificate of Analysis
S6 Analytical Laboratory QC Report
0 Yes ❑ No
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
0 Chain of Custody
W] Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 4/22/2020

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-1-A3
Collection Date: 04/08/2020 04:25 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 0200402
Total Alkalinity as CaCO3 12.3
Alkalinity, Carbonate < 5
Alkalinity, Bicarbonate 12.3
INORGANIC IONS BY IC - Q20040265
Chloride 2.0
Sulfate 1.2
MERCURY (COLD VAPORI IN WATER - Q20040243
mg/L
mg/L
mg/L
mg/L
mg/L
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040257
Aluminum (AI)
3.28
mg/L
Barium (Ba)
0.052
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
3.59
mg/L
Chromium (Cr)
0.010
mg/L
Copper (Cu)
0.011
mg/L
Iron (Fe)
3.43
mg1L
Magnesium (Mg)
2.09
mg/L
Manganese (Mn)
0.181
mg/L
Nickel (Ni)
0.011
mg/L
Potassium (K)
2.87
mg/L
Sodium (Na)
2.40
mg/L
Strontium (Sr)
0.035
mg/L
Zinc (Zn)
0.059
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS
- 020040263
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
3.04
ug/L
Lead (Pb)
1.05
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
3.29
ug/L
TOTAL DISSOLVED SOLIDS - Q20040224
TDS
34.0
mg/L
Sample #: 2020006508
Matrix: GW WW
Page 4 of 34
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/15/2020 18:27
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:27
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:27
PARMSTR
0.1
1
EPA 300.0
04/14/2020 15:24
BGN9034
0.1
1
EPA 300.0
04/14/2020 15:24
BGN9034
0.05
1
EPA 245.1
04/13/2020 12:59
DMFRANC
0.01
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.05
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.05
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.01
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.01
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.1
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.05
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
0.005
1
EPA 200.7
04/15/2020 17:35
DMFRANC
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
0.2
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
0.3
1
EPA 200.8
04/15/2020 02:19
CWSPEN3
25
1
SM2540C
04/131202011:26
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-1-A3
Collection Date: 04/08/2020 04:25 PM
Analyse Result Units Qualifiers RDL DF
Total Suspended Solids -Low RL 2.5 - 020040246
TSS 65 mg/L 2.5 1
Sample #: 2020006508
Matrix: GW WW
Page 5 of 34
Method Analysis Date/Time Analyst
SM2540D 04/14/2020 09:42 GBSINGL

Certificate of Laboratory Analysis Page 6 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA_MW-2-A3 Sample #: 2020006555
Collection Date: 04/08/2020 03:22 PM Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Daterrime
Analyst
TOTAL ALKALINITY - 020040299
Total Alkalinity as CaCO3
6.69
mg/L
5
1
SM 2320B-2011
04/15/2020 18:40
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/15/2020 18:40
PARMSTR
Alkalinity, Bicarbonate
6.69
mg/L
5
1
SM 2320B-2011
04/15/2020 18:40
PARMSTR
INORGANIC IONS BY IC - t7200402§5
Chloride
0.85
mg/L
0.1
1
EPA 300.0
04/14/2020 16:08
BGN9034
Sulfate
0.25
mg/L
0.1
1
EPA 300.0
04/14/2020 16:08
BGN9034
MERCURY (COLD VAPOR) IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 13:01
DMFRANC
TOTAL RECOVERABLE METALS
BY ICE - Q2 0402 7
Aluminum (AI)
0.017
mg/L
0.01
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Barium (Ba)
0.008
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Calcium (Ca)
0.384
mg/L
0.05
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Magnesium (Mg)
0.438
mg/L
0.01
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Manganese (Mn)
0.025
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Potassium (K)
0.521
mg/L
0.1
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Sodium (Na)
2.25
mg/L
0.05
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Strontium (Sr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
Zinc (Zn)
0.009
mg/L
0.005
1
EPA 200.7
04/15/2020 17:48
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040263
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/15/2020 01:45
CWSPEN3
TOTAL DISSOLVED SOLIDS -
Q20040224
TDS
< 25
mg/L
25
1
SM2540C
04/1312020 11:26
GBSINGL

Certificate of Laboratory Analysis Page 7 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-2-A3 Sample #: 2020006555
Collection Date: 04/08/2020 03:22 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL
Total Suspended Solids -Low RL 2.5 - Q20040246
TSS < 2.5 mg/L 2.5
DF
1
Method Analysis Date/Time Analyst
SM2540D 04/14/2020 09:43 GBSINGL

Certificate of Laboratory Analysis Page 8 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-3-A3 Sample #: 2020006556
Collection Date: 04/08/2020 01:59 PM Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - Q20040299
Total Alkalinity as CaCO3
5.28
mg/L
5
1
SM 2320B-2011
04/15/2020 18:43
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320E-2011
04/15/2020 18:43
PARMSTR
Alkalinity, Bicarbonate
5.28
mg/L
5
1
SM 2320E-2011
04/15/2020 18:43
PARMSTR
INORGANIC IONS BY I_C-Q20040265
Chloride
0.59
mg/L
0.1
1
EPA 300.0
04/14/2020 16:23
BGN9034
Sulfate
0.31
mg/L
0.1
1
EPA 300.0
04/14/2020 16:23
BGN9034
MERCURY (COLD VAPORI
IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 13:03
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - 020040257
Aluminum (AI)
2.35
mg/L
0.01
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Barium (Ba)
0.028
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Calcium (Ca)
0.508
mg/L
0.05
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Copper (Cu)
0.009
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Iron (Fe)
2.30
mg/L
0.01
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Magnesium (Mg)
1.21
mg/L
0.01
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Manganese (Mn)
0.065
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Potassium (K)
1.34
mg/L
0.1
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Sodium (Na)
1.57
mg/L
0.05
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Strontium (Sr)
0.009
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
Zinc (Zn)
0.016
mg/L
0.005
1
EPA 200.7
04/15/2020 17:53
DMFRANC
TOTAL RECOVERABLE
METALS BY ICP-MS - 020040263
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Cobalt (Co)
1.12
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
Vanadium (V) Low Level
2.03
ug/L
0.3
1
EPA 200.8
04/15/2020 02:28
CWSPEN3
TOTAL DISSOLVED SOLIDS - Q20040224
TDS
< 25
mg/L
25
1
SM2540C
04/13/2020 11:27
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-3-A3
Collection Date: 04/08/2020 01:59 PM
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - Q20040246
TSS 130 mg/L 2.5
Page 9 of 34
Sample #: 2020006556
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 SM2540D 04/14/2020 09:43 GBSINGL

Certificate of Laboratory Analysis Page 10 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-4-A3 Sample #: 2020006557
Collection Date: 04/08/2020 12:37 PM Matrix: GW_WW
Analyse
Result
Units
Qualifiers RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - 020040299
Total Alkalinity as CaCO3
20.4
mg/L
5
1
SM 2320B-2011
04/15/2020 18:47
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/15/2020 18:47
PARMSTR
Alkalinity, Bicarbonate
20.4
mg/L
5
1
SM 2320B-2011
04/16/2020 18:47
PARMSTR
INORGANIC IONS BY IC - 020040265
Chloride
0.96
mg/L
0.1
1
EPA 300.0
04/14/2020 16:38
BGN9034
Sulfate
< 0.1
mg/L
0.1
1
EPA 300.0
04/14/2020 16:38
BGN9034
MERCURY (COLD VAPORI IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 13:05
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - ❑29040257
Aluminum (AI)
0.014
mg/L
0.01
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Barium (Ba)
0.012
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Calcium (Ca)
4.70
mg/L
0.05
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Iron (Fe)
0.052
mg/L
0.01
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Magnesium (Mg)
1.75
mg/L
0.01
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Manganese (Mn)
0.025
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Potassium (K)
1.29
mg/L
0.1
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Sodium (Na)
1.58
mg/L
0.05
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Strontium (Sr)
0.033
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 17:57
DMFRANC
TOTAL RECOVERABLE METALS BY ICP-MS - 02004026
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/15/2020 02:36
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040224
TDS
31.0
mg/L
25
1
SM2540C
04/13/202011:28
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-4-A3 Sample M 2020006557
Collection Date: 04/08/2020 12:37 PM Matrix: GW WW
Page 11 of 34
Analyte Result Units Qualifiers RDL DF Method Analysis Daterrime Analyst
Total Suspended Solids - Low RL 2.5 - 020040246
TSS 4.8 mg/L 2.5 1 SM2540D 04/14/2020 09:44 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-5-A3
Collection Date: 04/08/2020 10:28 AM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040299
Total Alkalinity as CaCO3
9.59
mg/L
Alkalinity, Carbonate
< 5
mg/L.
Alkalinity, Bicarbonate
9.59
mg/L
INORGANIC IONS BY IC -
Q20040265
Chloride
0.62
mg/L
Sulfate
0.15
mg/L
MERCURY (COLD VAPORI IN
WATER - Q200_4.0243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q2004025�
Aluminum (AI)
0.410
mg/L
Barium (Ba)
0.013
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
1.22
mg/L
Chromium (Cr)
< 0.005
mg/L
Capper (Cu)
< 0.005
mg/L
Iron (Fe)
0.271
mg/L
Magnesium (Mg)
1.13
mg/L
Manganese (Mn)
0.024
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.920
mg/L
Sodium (Na)
1.42
mg/L
Strontium (Sr)
0.008
mg/L
Zinc (Zn)
0.006
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS - 020040263
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
0.311
ug/L
TOTAL DISSOLVED SOLIDS
- 020040224
TDS
< 25
mg/L
Page 12 of 34
Sample #: 2020006558
Matrix: GW WW
Method Analysis Datefrime Analyst
5
1
SM 2320B-2011
04/15/2020 18:50
PARMSTR
5
1
SM 2320B-2011
04/15/2620 18:50
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:50
PARMSTR
0.1
1
EPA 300.0
04/14/2020 16:53
BGN9034
0.1
1
EPA 300.0
04/14/2020 16:53
BGN9034
0.05
1
EPA 245.1
04/13/2020 13:08
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.1
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:02
DMFRANC
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
0.2
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
0.3
1
EPA 200.8
04/15/2020 02:44
CWSPEN3
25
1
SM2540C
04/13/202011:28
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-5-A3
Collection Date: 04/08/2020 10:28 AM
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - 020040246
TSS 4.7 mg/L 2.5
Sample #: 2020006558
Matrix: GW WW
DF Method
1 SM2540D
Page 13 of 34
Analysis Date/Time Analyst
04/14/2020 09:44 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-6-A3
Collection Date: 04/07/2020 02:55 PM
Analyte Result Units Qualifiers RDL DF
TOTAL ALKALINITY - Q20040299
Total Alkalinity as CaCO3 9.95 mg/L
Alkalinity, Carbonate < 5 mg/L
Alkalinity, Bicarbonate 9.95 mg/L
INORGANIC IONS BY IC - g20040181
Chloride 0.50 mg/L
Sulfate 0.13 mg/L
MERCURY [COLD VAPOR! IN WATER - 220040243
Mercury (Hg) < 0.05 ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040257
Aluminum (AI)
0.040
mg/L
Barium (Ba)
0.006
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
1.78
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.015
mg/L
Magnesium (Mg)
0.960
mg/L
Manganese (Mn)
0.006
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.611
mg/L
Sodium (Na)
1.02
mg/L
Strontium (Sr)
0.009
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE METALS
BY ICP-MS
- Q20040263
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DISSOLVED SOLIDS - Q20040188
TDS
< 25
mg/L
Page 14 of 34
Sample #: 2020006559
Matrix: GW WW
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/15/2020 18:53
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:53
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:53
PARMSTR
0.1
1
EPA 300.0
04/09/2020 14:57
BGN9034
0.1
1
EPA 300.0
04/09/2020 14:57
BGN9034
0.05
1
EPA 245.1
04/13/2020 13:10
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.1
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:06
DMFRANC
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
1
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
0.2
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
0.3
1
EPA 200.8
04/15/2020 02:53
CWSPEN3
25
1
SM2540C
04/09/202010:48
GBSINGL

Certificate of Laboratory Analysis Page 15 of 34
This report shall not be reproduced, except in full.
Order# J20030212
Site: ASA MW-6-A3 Sample #: 2020006559
Collection Date: 04/07/2020 02:55 PM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
Total Suspended Solids - Low RL 2.5 - 020040178
TSS < 2.5 mg/L 2.5 1 SM2540D 04/09/2020 06:58 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-7-A3
Collection Date: 04/08/2020 12:00 PM
Analyse Result Units Qualifiers RDL OF
TOTAL ALKALINITY - 020040299
Total Alkalinity as CaCO3
9.41
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
9.41
mg/L
INORGANIC IONS BY IC -
Q2094Q265
Chloride
0.89
mg/L
Sulfate
0.31
mg/L
MERCURY tCOLD VAPORY
IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - 020040257
Aluminum (AI)
9.59
mg/L
Barium (Ba)
0.064
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
1.47
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
7.53
mg/L
Magnesium (Mg)
4.36
mg/L
Manganese (Mn)
0.852
mg/L
Nickel (Ni)
0.021
mg/L
Potassium (K)
3.04
mg/L
Sodium (Na)
1.39
mg/L
Strontium (Sr)
0.020
mg/L
Zinc (Zn)
0.076
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040263
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
9.06
ug/L
Lead (Pb)
4.24
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
0.249
ug/L
Vanadium (V) Low Level
4.36
ug/L
TOTAL DISSOLVED SOLIDS - Q20040224
TDS
27.0
mg/L
Page 16 of 34
Sample #: 2020006560
Matrix: GW WW
Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/15/2020 18:56
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:56
PARMSTR
5
1
SM 2320B-2011
04/15/2020 18:56
PARMSTR
0.1
1
EPA 300.0
04/14/2020 18:08
BGN9034
0.1
1
EPA 300.0
04/14/2020 18:08
BGN9034
0.05
1
EPA 245.1
04/13/2020 13:12
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.1
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:10
DMFRANC
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
1
1
EPA 200.8
04115/202014:49
CWSPEN3
0.2
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
0.3
1
EPA 200.8
04/15/2020 14:49
CWSPEN3
25
1
SM2540C
04113/202011:29
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA MW-7-A3
Collection Date: 04/08/2020 12:00 PM
Analyse Result Units Qualifiers RDL
Total Suspended Solids- Low RL 2.5 - 020040246
TSS 170 mg/L 2.5
DF
1
Sample #: 2020006560
Matrix: GW WW
Page 17 of 34
Method Analysis Date/Time Analyst
SM2540D 04/14/2020 09:45 GBSINGL

Certificate of Laboratory Analysis Page 18 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA_FD-20200408-1 Duplicate Sample #: 2020006561
Collection Date: 04/08/2020 Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - 02004029
Total Alkalinity as CaCO3
9.50
mg/L
5
1
SM 2320E-2011
04/15/2020 19:00
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320E-2011
04/15/2020 19:00
PARMSTR
Alkalinity, Bicarbonate
9.50
mg/L
5
1
SM 2320B-2011
04/15/2020 19:00
PARMSTR
INORGANIC IONS BY I
- Q20040265
Chloride
0.62
mg/L
0.1
1
EPA 300.0
04/14/2020 18:23
BGN9034
Sulfate
0.15
mg/L
0.1
1
EPA 300.0
04/14/2020 18:23
BGN9034
MERCURY (COLD VAPOR IN WATER - 02004024
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/13/2020 13:26
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - Q20040257
Aluminum (AI)
0.424
mg/L
0.01
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Barium (Ba)
0.013
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Calcium (Ca)
1.24
mg/L
0.05
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Iron (Fe)
0.277
mg/L
0.01
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Magnesium (Mg)
1.15
mg/L
0.01
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Manganese (Mn)
0.023
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Potassium (K)
0.938
mg/L
0.1
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Sodium (Na)
1.44
mg/L
0.05
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Strontium (Sr)
0.007
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/15/2020 18:15
DMFRANC
TOTAL RECOVERABLE
METALS BY ICP-MS - Q20040263
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/15/2020 03:09
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040224
TDS
< 25
mg/L
25
1
SM2540C
04/13/2020 11:29
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA_FD-20200408-1 Duplicate
Collection Date: 04/08/2020
Analyse Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - Q20040246
TSS 5.9 mg/L 2.5
DF
1
Sample #: 2020006561
Matrix: GW WW
Page 19 of 34
Method Analysis Date/Time Analyst
SM2540D 04/14/2020 09:45 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Site: ASA FB-20200408-1400 Field Blank
Collection Date: 04/08/2020 02:00 PM
Analyse Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040299
Total Alkalinity as CaCO3
< 5
mg/L
Alkalinity, Carbonate
< 5
mg/L
Alkalinity, Bicarbonate
< 5
mg/L
INORGANIC IONS BY IC -
Q20040265
Chloride
< 0.1
mg/L
Sulfate
< 0.1
mg/L
MERCURY {COLD VAPORI
IN WATER - Q20040243
Mercury (Hg)
< 0.05
ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040257
Aluminum (AI)
< 0.01
mg/L
Barium (Ba)
< 0.005
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
< 0.05
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Magnesium (Mg)
< 0.01
mg1L
Manganese (Mn)
< 0.005
mg1L
Nickel (Ni)
< 0.005
mg1L
Potassium (K)
< 0.1
mg1L
Sodium (Na)
< 0.05
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
< 0.005
mg1L
TOTAL RECOVERABLE METALS BY ICP-MS
- 020040263
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
Sample M 2020006562
Matrix: GW WW
Page 20 of 34
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/15/2020 19:03
PARMSTR
5
1
SM 2320B-2011
04/15/2020 19:03
PARMSTR
5
1
SM 2320B-2011
04/15/2020 19:03
PARMSTR
0.1
1
EPA 300.0
04/14/2020 18:38
BGN9034
0.1
1
EPA 300.0
04/14/2020 18:38
BGN9034
0.05
1
EPA 245.1
04/13/2020 13:28
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.01
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.1
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.05
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
0.005
1
EPA 200.7
04/15/2020 18:19
DMFRANC
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
1
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
0.2
1
EPA 200.8
04/15/2020 03:18
CWSPEN3
0.3
1
EPA 200.8
04/15/2020 03:18
CWSPEN3i I

Certificate of Laboratory Analysis Page21 of34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040299 ALK CarbBicarb
TOTAL
ALKALINITY
Duplicate # 1
Parent Sample: J20030212 --
2020006508
Parameter Measured
Final
Units:
Dil
Limit Ran(
RPD Qualifier
Alkalinity, Bicarbonate 12.3
12.3
mg/L
1
0 - 20%
0.244
Alkalinity, Carbonate 0
0
mg/L
1
0- 20%
0
Total Alkalinity as CaCO3 12.3
12.3
mg/L
1
0 - 20%
0.244 -
LCS # 1
Parameter Measured
Final
Units:
Dil
Spike % Recovery LCL UCL
Qualifier
Total Alkalinity as CaCO3 105
105
mg/L
1
105 99.9 85 115
-

Certificate of Laboratory Analysis Page 22 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040181
Dionex
INORGANIC
IONS BY IC
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentratio
Qualifier
Chloride
0
0
mg/L
1
0.1
< 1/2 RDL
Sulfate
0
0
mg/L
1
0.1
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
DiI
Soike
% Recove,,y
LCL
UCL
Qualifier
Chloride
1.92
1.92
mg/L
1
2
96
90
110
Sulfate
1.91
1.91
mg/L
1
2
95.5
90
110
MS # 1
Parent Sample:
J20040176
-- 2020009363
Parameter
Measured
Final
Units:
Dil
Soike
% Recovers
LCL
UCL
Qualifier
Chloride
2.87
143
mg/L
50
100
96.4
80
120
Sulfate
5.69
285
mg/L
50
100
97.2
80
120
MSD # 1
Parent Sample:
J20040176
-- 2020009363
Parameter
Measured
Final
Units:
DiI
Spike
% Recovery
LCL
UCL
RPD Qualifier
Chloride
2.85
142
mg/L
50
100
95.6
80
120
0.875
Sulfate
5.68
284
mg/L
50
100
96.4
80
120
0.811

Certificate of Laboratory Analysis Page 23 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040265 Dionex INORGANIC IONS BY IC
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
Chloride 0 0 mg/L 1 0.1 < 1/2 RDL
Sulfate 0 0 mg/L 1 0.1 < 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Sgike
% Recove, v LCL
UCL Qualifier
Chloride
4.88
4.88
mg/L
1
5
97.5 90
110
Sulfate
4.92
4.92
mg/L
1
5
98.4 90
110
MS # 1
Parent Sample:
J20040249 -- 2020009798
Parameter
Measured
Final
Units:
Dil
Sgike
% Recove, v LCL
UCL Qualifier
Chloride
3.87
77.3
mg/L
20
40
101 80
120
Sulfate
6.32
126
mg/L
20
40
99.1 80
120
MSD # 1
Parent Sample:
J20040249 -- 2020009798
Parameter
Measured
Final
Units:
Dil
Sgike
% Recove, v LCL
UCL RPD Qualifier
Chloride
3.88
77.6
mg/L
20
40
102 80
120 0.775 -
Sulfate
6.37
127
mg/L
20
40
102 80
120 2.62
MS # 2
Parent Sample:
J20030212 -- 2020006508
Parameter
Measured
Final
Units:
Dil
Sgike
% Recover_;: LCL
UCL Qualifier
Chloride
3.93
3.93
mg/L
1
2
95.5 80
120
Sulfate
3.12
3.12
mg/L
1
2
94.7 80
120
MSD # 2
Parent Sample:
J20030212 -- 2020006508
Parameter
Measured
Final
Units:
Dil
Sgike
% Recovery LCL
UCL RPD Qualifier
Chloride
3.98
3.98
mg/L
1
2
98 80
120 2.58
Sulfate
3.18
3.18
mg/L
1
2
97.7 80
120 3.07

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Level 1I QC Summary
Q20040243 HG 245.1 MERCURY (COLD VAPOR) IN WATER
Blank # 1
Parameter
Measured
Final
Mercury (Hg)
-0.013
-0.013
Blank # 2
Parameter
Measured
Final
Mercury (Hg)
-0.009
-0.009
LCS # 1
LCS # 2
Parameter Measured Final
Mercury (Hg) 2 2
Parameter Measured Final
Mercury (Hg) 1.99 1.99
MS # 1
Parameter Measured Final
Mercury (Hg) 0.695 13.9
MSD # 1
Parameter Measured Final
Mercury (Hg) 0.694 13.9
Page 24 of 34
Units:
Dil
12L
Relative Concentratio
Qualifier
ug/L
1
0.05
< 112 RDL
Units:
Dil
RDL
Relative Concentration
Qualifier
ug/L
1
0.05
< 1/2 RDL
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
ug/L
1
2
100 85
115
Units:
Dil
Spike
% Recover,. LCL
UCL
Qualifier
ug/L
1
2
99.5 85
115
Parent Sample:
120020127
-- 2020004467
Units:
Dil
Spike
%Recover y LCL
UCL
Qualifier
ug/L
20
20
71 70
130
-
Parent Sample:
J20020127
-- 2020004467
Units:
Dil
Spike
% Recovery. LCL
UCL
RPD Qualifier
ug/L
20
20
70.9 70
130
0.211 -

Certificate of Laboratory Analysis Page 25 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040257 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Aluminum (AI)
0.000376
0.000376
mg/L
1
0.01
< 1/2 RDL
Barium (Ba)
-0.00012
-0.00012
mg/L
1
0.005
< 1/2 RDL
Boron (B)
0.0015
0.0015
mg/L
1
0.05
< 1/2 RDL
Calcium (Ca)
0.0104
0.0104
mg/L
1
0.05
< 1/2 RDL
Chromium (Cr)
-0.000181
-0.000181
mg/L
1
0.005
< 1/2 RDL
Copper (Cu)
-0.000334
-0.000334
mg/L
1
0.005
< 1/2 RDL
Iron (Fe)
-0.000775
-0.000775
mg/L
1
0.01
< 112 RDL
Magnesium (Mg)
0.000136
0.000136
mg/L
1
0.01
< 1/2 RDL
Manganese (Mn)
-0.000232
-0.000232
mg/L
1
0.005
< 112 RDL
Nickel (Ni)
-0.000296
-0.000296
mg/L
1
0.005
< 1/2 RDL
Potassium (K)
0.0321
0.0321
mg/L
1
0.1
< 1/2 RDL
Sodium (Na)
0.00233
0.00233
mg/L
1
0.05
< 1/2 RDL
Strontium (Sr)
-0.000351
-0.000351
mg/L
1
0.005
< 1/2 RDL
Zinc (Zn)
-0.000047
-0.000047
mg/L
1
0.005
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Aluminum (AI)
4.8
4.8
mg/L
Barium (Ba)
4.81
4.81
mg/L
Boron (B)
5.52
5.52
mg/L
Calcium (Ca)
5.65
5.65
mg/L
Chromium (Cr)
5.63
5.63
mg/L
Copper (Cu)
5.46
5.46
mg/L
Iron (Fe)
5.32
5.32
mg/L
Magnesium (Mg)
5.47
5.47
mg/L
Manganese (Mn)
5.56
5.56
mg/L
Nickel (Ni)
5.22
5.22
mg/L
Potassium (K)
5.64
5.64
mg/L
Sodium (Na)
5.37
5.37
mg/L
Strontium (Sr)
4.72
4.72
mg/L
Zinc (Zn)
5.63
5.63
mg/L
MS # 1
Parameter
Measured
Final
Units:
Aluminum (AI)
7.88
7.88
mg/L
Barium (Ba)
5.03
5.03
mg/L
Boron (B)
5.61
5.61
mg/L
Calcium (Ca)
9.36
9.36
mg/L
Chromium (Cr)
5.76
5.76
mg/L
Copper (Cu)
5.58
5.58
mg/L
Qualifier
Dil
Saike
% Recovery LCL
UCL Qualifier
1
5
96 85
115
1
5
96.2 85
115
1
5
110 85
115
1
5
113 85
115
1
5
113 85
115
1
5
109 85
115
1
5
106 85
115
1
5
109 85
115
1
5
111 85
115
1
5
105 85
115
1
5
113 85
115
1
5
107 85
115
1
5
94.4 85
115
1
5
113 85
115
Parent Sample:
J20030212 -- 2020006508
Dil
Soike
% Recovery LCL
UCL Qualifier
1
5
92 70
130
1
5
99.5 70
130
1
5
112 70
130
1
5
116 70
130
1
5
115 70
130
1
5
111 70
130

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040257 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
MS # 1
Parameter
Measured
Final
Iron (Fe)
8.72
8.72
Magnesium (Mg)
7.65
7.65
Manganese (Mn)
5.88
5.88
Nickel (Ni)
5.33
5.33
Potassium (K)
8.6
8.6
Sodium (Na)
7.93
7.93
Strontium (Sr)
4.87
4.87
Zinc (Zn)
5.78
5.78
lu ty 11F:IEI
Parameter
Measured
Final
Aluminum (AI)
7.77
7.77
Barium (Ba)
4.92
4.92
Boron (B)
5.41
5.41
Calcium (Ca)
9.25
9.25
Chromium (Cr)
5.65
5.65
Copper (Cu)
5.49
5.49
Iron (Fe)
8.47
8.47
Magnesium (Mg)
7.49
7.49
Manganese (Mn)
5.76
5.76
Nickel (Ni)
5.17
5.17
Potassium (K)
8.48
8.48
Sodium (Na)
7.88
7.88
Strontium (Sr)
4.76
4.76
Zinc (Zn)
5.67
5.67
Page 26 of 34
Parent Sample:
J20030212 -- 2020006508
Units:
ail
Soike
% Recovery LCL
UCL
Qualifier
mg/L
1
5
106 70
130
mg/L
1
5
111 70
130
-
mg/L
1
5
114 70
130
-
mg/L
1
5
106 70
130
-
mg/L
1
5
114 70
130
-
mg/L
1
5
111 70
130
-
mg/L
1
5
96.8 70
130
-
mg/L
1
5
114 70
130
-
Parent Sample:
120030212 --
20201106508
Units-
Mil
Soikr3
% Recovery LCL
UCL
RPD Qualifier
mg/L
1
5
89.8 70
130
1.38 -
mg/L
1
5
97.4 70
130
2.09 -
mg/L
1
5
108 70
130
3.67 -
mg/L
1
5
113 70
130
1.18 -
mg/L
1
5
113 70
130
1.96 -
mg/L
1
5
110 70
130
1.7 -
mg/L
1
5
101 70
130
2.97 -
mg/L
1
5
108 70
130
2.13 -
mg/L
1
5
111 70
130
2.13 -
mg/L
1
5
103 70
130
2.97 -
mg/L
1
5
112 70
130
1.3 -
mg/L
1
5
110 70
130
0.671 -
mg/L
1
5
94.5 70
130
2.37 -
mg/L
1
5
112 70
130
1.99 -

Certificate of Laboratory Analysis Page 27 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040263 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Antimony (Sb)
-0.043
-0.043
ug/L
1
1
< 1/2 RDL
Arsenic (As)
0.025
0.025
ug/L
1
1
< 1/2 RDL
Beryllium (Be)
-0.027
-0.027
ug/L
1
1
< 1/2 RDL
Cadmium (Cd)
0.002
0.002
ug/L
1
1
< 1/2 RDL
Cobalt (Co)
0.001
0.001
ug/L
1
1
< 1/2 RDL
Lead (Pb)
-0.002
-0.002
ug/L
1
1
< 112 RDL
Molybdenum (Mo)
0.032
0.032
ug/L
1
1
< 1/2 RDL
Selenium (Se)
-0.111
-0.111
ug/L
1
1
< 1/2 RDL
Thallium (TI) Low Level
0.072
0.072
ug/L
1
0.2
< 1/2 RDL
Vanadium (V) Low Level
0.076
0.076
ug/L
1
0.3
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery
LCL
UCL
Qualifier
Antimony (Sb)
49.9
49.9
ug/L
1
50
99.7
85
115
Arsenic (As)
54.8
54.8
ug/L
1
50
110
85
115
Beryllium (Be)
49.7
49.7
ug/L
1
50
99.4
85
115
Cadmium (Cd)
50
50
ug/L
1
50
100
85
115
Cobalt (Co)
52.1
52.1
ug/L
1
50
104
85
115
Lead (Pb)
49.8
49.8
ug/L
1
50
99.6
85
115
Molybdenum (Mo)
50.9
50.9
ug/L
1
50
102
85
115
Selenium (Se)
50.1
50.1
ug/L
1
50
100
85
115
Thallium (TI) Low Level
49.2
49.2
ug/L
1
50
98.3
85
115
Vanadium (V) Low Level
49
49
ug/L
1
50
98.1
85
115
MS # 1
Patent Sample:
120030-' I
202(K)06555
Parameter
Measured
Final
Units
Dil
Soike
% Recovery
LCL
UCL
Qualifier
Antimony (Sb)
51.5
51.5
ug/L
1
50
103
70
130
Arsenic (As)
56.1
56.1
ug/L
1
50
112
70
130
Beryllium (Be)
53.4
53.4
ug/L
1
50
107
70
130
Cadmium (Cd)
52.4
52.4
ug/L
1
50
105
70
130
Cobalt (Co)
53.9
53.9
ug/L
1
50
107
70
130
Lead (Pb)
51.7
51.7
ug/L
1
50
103
70
130
-
Molybdenum (Mo)
52.4
52.4
ug/L
1
50
105
70
130
-
Selenium (Se)
50.1
50.1
ug/L
1
50
100
70
130
-
Thallium (TI) Low Level
51
51
ug/L
1
50
102
70
130
-
Vanadium (V) Low Level
51.6
51.6
ug/L
1
50
103
70
130
-
MSD # 1
Parent Sample:
J20030212
-- 2020006555
Parameter
Measured
Final
Units:
Dil
Soike
% Recover,;
LCL
UCL
RPD Qualifier
Antimony (Sb)
50.5
50.5
ug/L
1
50
101
70
130
1.86 -

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040263 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
MSD it 1
Parameter
Measured
Final
Units:
Arsenic (As)
54.3
54.3
ug/L
Beryllium (Be)
50.5
50.5
ug/L
Cadmium (Cd)
51.1
51.1
ug/L
Cobalt (Co)
52.6
52.6
ug/L
Lead (Pb)
50.4
50.4
ug/L
Molybdenum (Mo)
51.4
51.4
ug/L
Selenium (Se)
48.8
48.8
ug/L
Thallium (TI) Low Level
49.7
49.7
ug/L
Vanadium (V) Low Level
50
50
ug/L
Page 28 of 34
Parent Sample:
J20030212 -- 2020006555
Dil
Soike
% Recove, s LCL
UCL
RPD Qualifier
1
50
108 70
130
3.25
1
50
101 70
130
5.65
1
50
102 70
130
2.62
1
50
105 70
130
2.38
1
50
101 70
130
2.6
1
50
103 70
130
1.92
1
50
97.7 70
130
2.6
1
50
99.3 70
130
2.44
1
50
99.7 70
130
3.18

Certificate of Laboratory Analysis Page 29 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040188 TDS
TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
TDS
2
mg/L
1
25
< 1/2 RDL
Blank # 2
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
TDS
7
mg/L
1
25
< 1/2 RDL
Blank # 3
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
TDS
4
mg/L
1
25
< 1/2 RDL
Duplicate # 1
Parent Sample:
J20030022 --
2020005591
Parameter
Measured
Final
Units:
Dil
Limit Ranee
RPD
Qualifier
TDS
315
mg/L
1
0 - 10%
1.6
Duplicate # 2
Parent Sample:
J20030022 --
2020005594
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
303
mg/L
1
0 - 10%
1.31
Duplicate # 3
Parent Sample:
J20030141 --
2020006117
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
101
mg/L
1
0 - 10%
0
Duplicate # 4
Parent Sample:
J20030178 --
2020006299
Parameter
Measured
Final
Units:
Dil
Limit Ranr;e
RPD
Qualifier
TDS
421
mg/L
1
0 - 10%
0.476
-
Duplicate # 5
Parent Sample:
J20030210 --
2020006502
Parameter
Measured
Final
Units:
Dil
Limit Ram_ a
RPD
Qualifier
TDS
40
mg/L
1
0 - 10%
7.79
LCS # 1
Parameter
Measured
Final
Units:
Dil
Soike
% Recovery LCL
UCL
Qualifier
TDS
992
mg/L
1
1000
99.2 90
110

Certificate of Laboratory Analysis
Page 30 of 34
This report shall not be
reproduced, except in full.
Order #
J20030212
Level II QC Summary
Q20040224 TDS
TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
4
mg/L
1
25 < 1/2 RDL
Blank # 2
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentratio
Qualifier
TDS
2
mg/L
1
25 < 1/2 RDL
Blank # 3
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
9
mg/L
1
25 < 1/2 RDL
Duplicate # 1
Parent Sample:
J20030019 -- 2020005579
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
777
mg/L
1
0 - 10%
0.513
-
Duplicate # 2
Parent Sample:
J20030085 -- 2020005849
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
12500
mg/L
1
0 - 10%
0.318
-
Duplicate # 3
Parent Sample:
J20030085 -- 2020005850
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
334
mg/L
1
0 - 10%
6.1
Duplicate # 4
Parent Sample:
J20030212 -- 2020006508
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
34
mg/L
1
0 - 10%
0
Duplicate # 5
Parent Sample:
J20030212 -- 2020006555
Parameter
Measured
Final
Units:
Dil
Limit Ram:
RPD
Qualifier
TDS
12
mg/L
1
0 - 10%
8
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike % Recovery LCL
UCL
Qualifier
TDS
983
mg/L
1
1000 98.3 90
110

Certificate of Laboratory Analysis Page 31 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040178 TSS_LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration
TSS 0 mg/L 1 2.5 < 1/2 RDL
Qualifier

Certificate of Laboratory Analysis Page 32 of 34
This report shall not be reproduced, except in full.
Order # J20030212
Level II QC Summary
Q20040246 TSS LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative
tatio
Qualifier
TSS
0
mg/L
1
2.5
< 1/2 RDL
Duplicate # I
Parent
Sample:
J20030206 --
2020006487
Parameter
Measured
Final
Units:
Dil
Limit Ramie
RPD
Qualifier
TSS
0.4
mg/L
1
120
R
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL
Qualifier
TSS
45.2
mg/L
1
50
90.4
90
110
LCSD # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL
RPD
Qualifier
TSS
50.8
mg/L
1
50
102
90
110
11.7
-
Qualifiers:
R % RPD indeterminate due to low concentration in the parent sample.

Page 33 of 34
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
Iff wV nC i Oulte Energy Analytical Laboratories
Anal ical Laboratory Use Dnl
ENERGY. Mall Code MG03A2 (Building 74051
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Page 34 of 34
IL Irnl Ive CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
V NI'% . i DuAa EmMy Analyllcal Labaralodaa
_
ENERGY. Mail Cod. M003A1 (Building T405)
i 13339 N&Vera Fairy Rd i
iHumanwla, .... —1.
i (00,
0 014TS•51 0 I
Far: f ,�,RSd0...._.._
I)Pro uNama: wW� 2^onallo:
ASHEVILLE AIRPORT FILL PROJECT AREA 01 990.9TS325T
3xllant p"ll Coda:
TiM HUNSUCNER, g7RY N MOELLER, 3A]
HALEYSFJITONI'�'L111" Tw_�`'•�
I
LAB USE ONLY I
i
i
"Lab ID
i
202000050S1
2020000555!
2020006550�
2 OON537 i
20200005561
20200065M
I
2020006561•
20200065M
j
"Sample DescrlOon or ID
.A3
1 -11 IN lilt
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4
�
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Ij mmft,_L1i��
�0©00
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ffitt 2PMSlZRA"MW©00
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DISTRIBUTION
Al. to LAB, COPY toCUENT
3A"1Y1?0
45
2000 mL
mit"uaaNdTurnaround
N4�
.r Dap
"w
'QUsw • Add Cost Will
Ap*

DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Vendor QC Data Review
Summary Report
Order Number: J20030231
Project Name: ASHEVILLE - AIRPORT FILL AREA IV - (VENDOR)
Customer Name(s): B Allison, B Moeller, T Hunsucker,H Seaton
Lab Contact: Peggy Kendall Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please review all vendor data for case narratives with explanations of quality control failures and data qualifiers.
4-20-2020
Page 1 of 35
Any analytical tests or individual analytes within a test flagged with a qualifier indicate a deviation from the method quality
system or quality control requirement. Certified vendor results and QC qualifiers can be found in the vendor lab final report.
This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory.
Vendor Data Review Criteria:
This vendor data package has been reviewed at the Duke Analytical Laboratory for the following applicable criteria:
• Required QC samples collected and analyzed
• Required tests performed for all samples
• Vendor Laboratory utilized required test methods for all analyses
• Vendor Laboratory met all requested Reporting Limits (RL)
• QC Results reviewed for outlying recovery values
Case Narrative:
The samples were taken directly to the vendor laboratory after sample collection.
Note: Sample ASA_MW-9-A4 was run at a 2X dilution due to limited sample volume.

PaceAnalytical
www.pacelabs.com
April 08, 2020
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg.7405 MG30A2
Huntersville, NC 28078
RE: Project: J20030231
Pace Project No.: 92472725
Dear Program Manager:
Pace Aaa11UUtv2!%&rvices, LLC
9���� 1Z�UU11ke. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 07, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
GCS
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
cc: Program Manager, Duke Energy
REPORT OF LABORATORY ANALYSIS
T N I This report shall not be reproduced, except in full,
C. ¢A without the written consent of Pace Analytical Services, LLC. Page 1 of 15
a0RAY0

aceAnalXical
www.pacolabs.com
Project: J20030231
Pace Project No.: 92472725
Pace AjatvtiG &rvices, LLC
90QQ�ti�c/e. Suite 100
yHuntersville, NC 28078
[phone]
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

ceAnalytical
www.pacelabs.cam
Project: J20030231
Pace Project No.: 92472725
Lab ID Sample ID
92472725001 2020006593
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 04/07/2015:00 04/0712016:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace AaaMi%&rvices, LLC
GP�9Q&i&,;&J3te. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 15

aceAnalytical
www.pacolabi.com
SAMPLE ANALYTE COUNT
Project: J20030231
Pace Project No.: 92472725
Pace Aaal�dicalkrvices, LLC
�a�6i8°e. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92472725001 2020006593 SM 9222D-2006 ECH 1 PASI-A
EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A
PASI-A = Pace Analytical Services -Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

PaceAnalytical
www.pacelabs.com
Project: J20030231
Pace Project No.: 92472725
Lab Sample ID Client Sample ID
Method Parameters
92472725001 2020006593
EPA 353.2 Rev 2.0 1993 Nitrogen, Nitrate
SUMMARY OF DETECTION
Result Units
0.88 mg/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace AaaMi%&rvices, LLC
20apiawke. Suite 100
Huntersville, NC 28078
[phone]
Report Limit Analyzed
0.040 04/07/20 23:15
Qualifiers
Page 5 of 15

aceAnalytical
www.pacolabs.com
PROJECT NARRATIVE
Project: J20030231
Pace Project No.: 92472725
Method: SM 9222D-2006
Description: MBIO 9222D Fecal Coliform AVL
Client: Duke Energy
Date: April 08, 2020
Pace Aaatrdi%&rvices, LLC
90gB6i�cM,te. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for SM 9222D-2006 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with SM 9222D-2006 with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

aceAnalytical
www.pacelabs.com
PROJECT NARRATIVE
Project: J20030231
Pace Project No.: 92472725
Method: EPA 353.2 Rev 2.01993
Description, 353.2 Nitrogen, N021NO3 unpres
Client: Duke Energy
Date: April 08, 2020
Pace Aaat�dical�ervices, LLC
(�Q�Cigc e. Suite 100
9Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 353.2 Rev 2.0 1993 by Pace Analytical Services Asheville. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

aceAnalytical
www.pacolabs.com
Project: J20030231
Pace Project No.: 92472725
Sample: 2020006593
Parameters
MBIO 9222D Fecal Coliform AVL
Fecal Coliforms
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Date: 04/08/2020 03:22 PM
Pace A3aN!%&rvices, LLC
9p%g�c&'te. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92472725001 Collected: 04/07/20 15:00 Received: 04/07/20 16:20 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No.
Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Asheville
ND CFU/100 mL 2.0 2 04/07/20 16:58 04/08/20 15:07
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
0.88 mg/L 0.040 1 04/07/20 23:15 14797-55-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
Page 8 of 15

aceAnalytical
www.pacelabs.com
Project: J20030231
Pace Project No.: 92472725
QC Batch: 534885
QC Batch Method: SM 9222D-2006
Associated Lab Samples: 92472725001
METHOD BLANK: 2854462
Associated Lab Samples: 92472725001
Parameter Units
Fecal Coliforms CFU/100 mL
QUALITY CONTROL DATA
Analysis Method: 5M 9222U-2uuo
Analysis Description: 9222D Fecal Coliform(MF) - AVL
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 04/08/2015:07
Pace ApaMig&rvices, LLC
npI�i�c /3NSe. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 2854463
92472686002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Fecal Coliforms CFU/100 mL ND ND 25
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2020 03:22 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

1*�2 8
aceAnalytical
www.pacelabs.com
Project: J20030231
Pace Project No.: 92472725
QC Batch: 534924
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92472725001
METHOD BLANK: 2854603
Associated Lab Samples: 92472725001
Parameter Units
Nitrogen, Nitrate
mg/L
LABORATORY CONTROL SAMPLE: 2854604
Parameter Units
Nitrogen, Nitrate mg/L
Pace ArM5011rices, LLC
ftgg iTcgffte. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services - Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.040 04/07/20 23:02
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1.5 1.6 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2854605 2854606
MS MSD
92472683001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qua[
Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.4 100 95 90-110 5 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2020 03:22 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: J20030231
Pace Project No.: 92472725
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Anat�di5V&rvices, LLC
g
19 0 "1iiiU2cake. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/08/2020 03:22 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

2aceAnalyfical'
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J20030231
Pace Project No.: 92472725
Pace ArMIM&rvices, LLC
Opagl�igcff:ie. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92472725001
2020006593
SM 9222D-2006
534885 SM 9222D-2006
92472725001
2020006593
EPA 353.2 Rev 2.0 1993
534924
Date: 04/08/2020 03:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
534886
Page 12 of 15

4-20-2020
Page 14 of 35
Document Name: Oocument Revised: February 7, 2018
Pa eiaf2
f� Sample Condition Upon Recelpt(SCUR) issuing Authority:
J dCeflf)oVicai ` Document No.:
F•CAR-CS•033•Rev.06 Pace Carolinas Quality Office
Laboratory receiving sa ples: Raleigh[] Mechanicsville( —I
Ashevi)lei Eden❑ Greenwood ❑ Huntersville ❑ ��
Client Name:
0�:92472
ene� Project q: 1����I�����
Courier: ❑Fed Ex —]UPS S Client �12'172❑ Commercial ❑Pace ❑Other:_ 9247
Custody Seal Present? []yes /[fNo Seals intact? [-]Yes �t'Jo
natellnitlals Person Examining Conlenls.—s-l—�
BIOIOgi[al nswe rruac—
Packing Material: ❑Bubble wrap ❑Bubble Bags ,None ❑ Other []Yes []No UN/A
Thermometer: �3Tv �� Type of ice: Aiwet []Blue❑Ilona
❑lfi Gun ID: / t
Cooler Temp ('C): Correction Factor: Add/Subtract ('C) - 0 r U Temp should be above freezing to VC
Cooler Temp Corrected ('C): 3, _ ❑Simples outof temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil Z N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? D'dud nzlHas all and Puerto Rico)?n source
(internationally,,
❑Noionally
icl
❑Yes ❑No_ _._ - - Comments/Discre ancY-
Chain of Ctistod Presets u? — _L
Yes nNo N/A
1.
Samples Arrived within Hold Time?
Yes No N/A
2.
Short Hold Time Anal sis 02 hr. ?
Yes rJNo N/A
3.
Rush Turn Around Time_ Requested?
Yes ONO ❑N/A
4•
Sufficient Volume?
Yes ONO I1N/A
5.
Correct Containers Used?
Yes ONO DN/A
.-._ r-r_...
G•
Containers intact?
dlyes
Nu N/A
7.
Dissolved analysis: Samples Field Filtered?
yes
No N A
B.
Sample Labels Match COC?
Yes
❑No ❑N/A
9,
-includes Date/Time/ID/Analysis Matrix:—
r
/
I eads pace in VOA Vials .S•Gmm)?
Yes
_ No
N/A
10.
Trip Blank Present?
Dyes
ONO L
IN/A
11.
Trip Blank Custody Seals Present?
No
N/A
Field Data Required? ❑Yes alto
COMMENTS/SAMPLE DI CREPANCY
c-e l
��lf`�•.r, r� �.�L
6r
Lot 10 of split containers: — -- -
CLIENT NOTIFICATION/RESOLUTION
Person contacted: - _
Project Manager SCURF Review: --
Project Manager SRF Review'
Date/Time:
Date: — - -
Date:
Page 13 of 15

4-20-2020
Page 15 of 35
Document Name: Document Revised: February 7, 2018
/.-Sample_Condition_Upon Receipt(SCUR) Page 1 of 2 ace�l�ral/Ircal` Document No� I Issuing Authority:
P-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project �j �24727 ��
verified and within the acceptance range for preservation WO —
samples, pM: KLHI out Date: 04/16/20
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLlig CLIENT: 92—Duke Ener
**Bottom half of box Is to list number of bottle
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pH Adjustment
Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Cate preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 0
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of loss loom will ee Senr.10 the Noun Laroima Vr.neYn Lernncauon vlmv p.r.
Out of hold, Incorrect preselvalive, mot of temp, incnrrect containers.
Page 14 of 15

a-20-2020
Page 16 of 35
f`UAI I nr f I ICTnnV DG!`nDn Amin AMAI VSIS RF[SIIFST F()RM

aceAnalytical 00
www.pacelabs.com
April 10, 2020
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg. 7405 MG30A2
Huntersville, NC 28078
RE: Project: J20030231
Pace Project No.: 92473057
Dear Program Manager:
Pace AaaNi%&rvices, LLC
Offiglllgc&fte. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 09, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
cc: Program Manager, Duke Energy
p PCCREp`�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
!q �Y without the written consent of Pace Analytical Services, LLC. Page 1 of 19
00RATO

aceAnalytical
J www.pacelabs.com
Project: J20030231
Pace Project No.: 92473057
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Arrmi%&rvices, LLC
ogagKigc&/�e. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 19

PaceAnalytical
www.pacelabs.com
SAMPLE SUMMARY
Project: J20030231
Pace Project No.: 92473057
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92473057001
2020006588
Water
04/09/20 09:25
04/09/20 11:52
92473057002
2020006589
Water
04/09/20 08:59
04/09/20 11:52
92473057003
2020006590
Water
04/09/20 09:39
04/09/20 11:52
92473057004
2020006591
Water
04/09/2010:42
04/09/20 11:52
92473057005
2020006592
Water
04109/2010:50
04/09/20 11:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace A4gMi%&rvices, LLC
pgog�iig cgke. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19

1001
PaceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace AnaM!% Services, LLC
098a "wke. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
J20030231
92473057
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92473057001
2020006588
SM 9222D-2006
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
92473057002
2020006589
SM 922213-2006
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
92473057003
2020006590
SM 9222D-2006
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
92473057004
2020006591
SM 9222D-2006
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
92473057005
2020006592
SM 9222D-2006
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

1�;a'ceAnalydca(
www.pacolabs.com
I
Project: J20030231
Pace Project No.: 92473057
Lab Sample ID
Method
Client Sample ID
Parameters
92473057002
2020006589
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
92473057003
2020006590
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
92473057004
2020006591
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
92473057005
2020006592
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
Pace AaaMical&rvices, LLC
ma8 nmv- Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Result
Units
Report Limit
Analyzed Qualifiers
3.8
mg/L
0.040
04/10/20 00:17
1.0
mg/L
0.040
04/10/20 00:22
0.64
mg/L
0.040
04/10/20 00:23
1.0
mg/L
0.040
04/10/20 00:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 19

,�_aiceAnalyfical
www.pacelabs.com
PROJECT NARRATIVE
Project: J20030231
Pace Project No.: 92473057
Method: SM 9222D-2006
Description: MBIO 9222D Fecal Coliform AVL
Client: Duke Energy
Date: April 10, 2020
Pace ARaMi5a &rvices, LLC
0089K299f349e. Suite 100
��JJ Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for SM 9222D-2006 by Pace Analytical Services Asheville. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with SM 9222D-2006 with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 19

PaceAnalytical
www.pacolabs.com
PROJECT NARRATIVE
Project: J20030231
Pace Project No.: 92473057
Method: EPA 353.2 Rev 2.0 1993
Description: 353.2 Nitrogen, NO2/NO3 unpres
Client: Duke Energy
Date: April 10, 2020
Pace Aaat 1%2!% rvices, LLC
09694� V19e. Suite 100
Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for EPA 353.2 Rev 2.0 1993 by Pace Analytical Services Asheville. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 19

*1007
PaceAnalytical
www.pacelabstam
ANALYTICAL RESULTS
Pace A2aMi%&rvices, LLC
190K2+'$c6r13lge. Suite 100
Huntersville, NC 28078
[phone]
Project: J20030231
Pace Project No.: 92473057
Sample: 2020006588 Lab ID: 92473057001 Collected: 04/09/20 09:25 Received: 04/09/20 11:52 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 04/09/20 16:43 04/10/20 16:00
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate ND mg/L 0.040 1 04/10/20 00:18 14797-55-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

25ceAnalyfical'
www.pacelabs.com
ANALYTICAL RESULTS
Pace A3aMi5V&rvices, LLC
0A8glPigc& fte. Suite 100
Huntersville, NC 28078
[phone]
Project: J20030231
Pace Project No.: 92473057
Sample: 2020006589 Lab ID: 92473057002 Collected: 04/09/20 08:59 Received: 04/09/20 11:52 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 922213-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services -Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 04/09/20 16:43 04/10/20 16:00
353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate 3.8 mg/L 0.040 1 04/10/20 00:17 14797-55-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: J20030231
Pace Project No.: 92473057
Pace AraaMi%&rvices, LLC
o�Qg IfZi�c�ke. Suite 100
a9 Huntersville, NC 28078
[phone]
Sample: 2020006590 Lab ID: 92473057003 Collected: 04/09/20 09:39 Received: 04/09/20 11:52 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 04/09/20 16:43 04/10/20 16:00
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate 1.0 mg/L 0.040 1 04/10/20 00:22 14797-55-8
Date: 04/10/2020 11:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: J20030231
Pace Project No.: 92473057
Pace A Jat 15V&rvices, LLC
Ogagg iff34�e. Suite 100
Huntersville, NC 28078
[phone]
Sample: 2020006591 Lab ID: 92473057004 Collected: 04/09/20 10:42 Received: 04/09/20 11:52 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services -Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 04/09/20 16:43 04/10/20 16:00
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate 0.64 mg/L 0.040 1 04/10/20 00:23 14797-55-8
Date: 04/10/2020 11:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

/ Pace Aaat� %2%ervices, LLC
00 e. Suite 100
PaceAnalytical �����
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: J20030231
Pace Project No.: 92473057
Sample: 2020006592 Lab ID: 92473057005 Collected: 04/09/20 10:50 Received: 04/09/20 11:52 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006
Pace Analytical Services - Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 04/09/20 16:43 04/10/20 16:00
353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate 1.0 mg/L 0.040 1 04/10/20 00:24 14797-55-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

0i
FaceAnalytical
www.paceiabs.com
QUALITY CONTROL DATA
Project: J20030231
Pace Project No.: 92473057
UL; hatch: 535465 Analysis Method: SM 9222D-2006
QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) -AVL
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92473057001, 92473057002, 92473057003, 92473057004, 92473057005
METHOD BLANK: 2857261 Matrix: Water
Associated Lab Samples: 92473057001, 92473057002, 92473057003, 92473057004, 92473057005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 04/10/20 16:00
SAMPLE DUPLICATE: 2857262
Parameter
Fecal Coliforms
92473057002
Units Result
CFU/100 mL ND
Dup
Result
ND
Pace AagMi%&rvtces, LLC
§ag i2gc6fkre. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD RPD Qualifiers
25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

aceAnalyticai®
www.pacelabs.com
QUALITY CONTROL DATA
Project: J20030231
Pace Project No.: 92473057
QC Batch: 535487 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92473057001, 92473057002, 92473057003, 92473057004, 92473057005
METHOD BLANK: 2857325 Matrix: Water
Associated Lab Samples: 92473057001, 92473057002, 92473057003, 92473057004, 92473057005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 04/10/20 00:08
Pace Aaal%krvices, LLC
0§Qg isac��e. Suite 100
�J Huntersville, NC 28078
[phone]
LADUKHI UM %,UIN I rRUL ommr�--�.
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2857327 2857328
MS MSD
92473041001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/L 1.7 1.5 1.5 3.2 3.1 97 95 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 19

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: J20030231
Pace Project No.: 92473057
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Aaa:M!% ervices, LLC
Pgag I gcgke. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/10/2020 11:54 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 19

r4oloon
FaceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J20030231
Pace Project No.: 92473057
Pace Aaatvs!5V&rvices, LLC
098gKiQcsfI3,gre. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92473057001
2020006588
SM 9222D-2006
535465
SM
9222D-2006
92473057002
2020006589
SM 9222D-2006
535465
SM
9222D-2006
92473057003
2020006590
SM 9222D-2006
535465
SM
9222D-2006
92473057004
2020006591
SM 9222D-2006
535465
SM
9222D-2006
92473057005
2020006592
SM 9222D-2006
535465
SM
9222D-2006
92473057001
2020006588
EPA 353.2 Rev 2.0 1993
535487
92473057002
2020006589
EPA 353.2 Rev 2.0 1993
535487
92473057003
2020006590
EPA 353.2 Rev 2.0 1993
535487
92473057004
2020006591
EPA 353.2 Rev 2.01993
535487
92473057005
2020006592
EPA 353.2 Rev 2.0 1993
535487
Date: 04/10/2020 11:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
535466
535466
535466
535466
535466
Page 16 of 19

4-20-2020
- 33 of 35
} Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recelpt(SCUR) Page 1 of 2
r�eeAnalytleai Document No,: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville R] Eden[] Greenwood ❑ Huntersville (-I Raleigh❑ Mechanicsville❑
SampleCondlflDn Client Name: wog : 92473057
Upon Recdpt
Project
Courier: 4edEx ❑UPS LAUSPS ]Client
❑ Commercial ❑Pace ❑OLher:_ 92473067
Custody Seal Present? VJYes ❑No Seals Intact? OYes ❑No
Date/Initials Person Examining Content ' /-J0
Packing Material: ❑Bubble Wrap ❑Bubble Bags }None ❑ Other Biological Tissue Frozen?
Thermometer: []Yes []No ®N/A
W IR Gun ID: 3--10F> Type of Ice. ENO Elul- Dion-!
Cooler Temp (°C): U ? Correction Factor: Add/Subtract (°C) —
� Temp should be above freezing to VCCooler Temp Corrected (°C): q I %?
❑Samples out of temp criteria. Samples oil Ice, coaling process
has begun
USDA Regulated Soil (N N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes No including ilawail and Puerto Rico)? ❑Yes No
Chain of Custody Present? 91Yes___01`10 ❑N/A L 1,
Samples Arrived within Hold Time?
]Yes
❑No
N/A
2.
Short Hold Time Analysis 472 hr.)?
Ves
QNo
QN1A
3.
Rush Turn Around Time Requested?
Sufficient Volume?
Yes NNo.
JQyes ❑No
NJA
❑NJA
4.
5.
Correct Containers Used?
-Pace Containers Used?
E4Yes
(QYes
[]No
ONO
❑N/A
❑N/A
6.
Containers intact?
-
XYe, ❑No
N A
7.
Dissolved analysis: Saniles Field Filtered?
[]Yes[IN.N/A
_S_.
Sample Labels Match CDC?
Pes
❑Nu
❑N/A 1
9.
-Includes Date/Time/ID/Analysis Matrix:/ j
Headspace in VOA Vials (>5-13mm)? [:]Yes []NO _26_N/A 10. Y_ _
Trip Blank Present? ❑Yes ❑No WN/A 11.
Trip Blank Custody Seals Present? ❑Yes ❑No N/A
CON-11 TENTS/SAMPLE DISCREPANCY Fleid Data Required! Oyes ONO
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: _ _— _ Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: _ Date:
Page 17 of 19

.- aceAralytical
4-20-2020
Page 34 of 35
Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No,: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
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Project # I
Wo#:92473057
PM: KLH1 Due Oatat 04/20/20
CLIENT: 92—Duke Enor
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Tittle preservation Amount of Preservative Lot If
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will to sent to the North Carolina DEHNR Certification office {i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 18 of 19

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DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J20030213
Project Name: ASHEVILLE AIRPORT - AIRPORT FILL AREA IV - (IN-HOUSE)
Customer Name(s): B Allison, F Holt,B Moeller, T Hunsucker,H Seaton
Customer Address:
Lab Contact: Peggy Kendall Phone: [phone]
ReportAuthorized By: 1
(Signature) �Wynd,11
WaVDate:
e
Program Comments:
4/24/2020
Note: Per Haley Seaton, the collection time for ASA_MW-1AR-A4 was 12:45 (not indicated on the COC).
Data Flags & Calculations:
Page 1 of 34
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Sample ID
2020006509
2020006570
2020006571
2020006572
2020006573
2020006574
2020006575
2020006576
2020006577
9 Total Samples
Plant/Station
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Asheville Airport
Collection
Date and Time
09-Apr-20
12:45 PM
09-Apr-20
9:25 AM
09-Apr-20
8:59 AM
09-Apr-20
9:39 AM
09-Apr-20
10:42 AM
09-Apr-20
10:50 AM
07-Apr-20
3:00 PM
09-Apr-20
09-Apr-20
9:45 AM
Collected By
Josh Stowe
Josh Stowe
Haley Seaton
Haley Seaton
Haley Seaton
Josh Stowe
JAS
Josh Stowe
Haley Seaton
Page 2 of 34
Sample Description
ASA MW-IAR-A4
ASA MW-2-A4
ASA MW-5-A4
ASA MW-5D-A4
ASA MW-6-A4
ASA MW-7-A4
ASA MW-9-A4
ASA FD-20200409-1
ASA FB-20200409-945

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals © Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable.
F./I Yes 11 No
Report Sections Included:
d❑ Job Summary Report
Sample Identification
d❑ Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
0 Analytical Laboratory QC Report
Page 3 of 34
❑ Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
© Chain of Custody
d❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 4/24/2020

Certificate of Laboratory Analysis Page 4 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Sw Sample #: 2020006509
Site: ASA_MW-1AR-A4
Collection Date: 04/09/2020 12:45 PM Matrix: GW_WW -
I Result Units Qualifiers RDL DF Method Analysis Daterrime Analyst
Ana yte
TOTAL ALKALINITY - Q20040325
Total Alkalinity as CaCO3
Alkalinity, Carbonate
Alkalinity, Bicarbonate
INORGANIC IONS BY IC
Chloride
Sulfate
MERCURY (COLD VAPOR)
Mercury (Hg)
TOTAL RECOVERAB E
36.8
< 5
36.8
- 20 40298
0.81
1.8
IN WATER--- Q2 0403
< 0.05
METALS BY ICP - 42 040331
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
Aluminum (Al)
0.063
mg/L
Barium (Ba)
0.007
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
3.85
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.079
mg/L
Magnesium (Mg)
1.06
mg/L
Manganese (Mn)
0.284
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
2.00
mg/L
Sodium (Na)
12.1
mg/L
Strontium (Sr)
0.035
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE
METALS BY ICP-MS - 020040345
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
c 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
8.87
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level 0.457
ug/L
TOTAL DISSOLVED SOLIDS - Q20040280
TDS
79.0
mg/L
5
1
SM 2320B-2011
04/16/2020 18:24
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:24
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:24
PARMSTR
0.1
1
EPA 300.0
04/15/2020 19:09
BGN9034
0.1
1
EPA 300.0
04/15/2020 19:09
BGN9034
0.05
1
EPA 245.1
04/15/2020 12:56
DMFRANC
0.01
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.05
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.05
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.01
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.01
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.1
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.05
1
EPA 200.7
04117/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
0.005
1
EPA 200.7
04/17/2020 14:59
MHALL3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
0.2
1
EPA 200.8
04/22/2020 19:49
CWSPEN3
0.3
1
EPA 200.8
04/221202019:49
CWSPEN3
25
1
SM2540C
04/15/202010:41
GBSINGL

Certificate of Laboratory Analysis Page 5 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA_MW-1AR-A4 f Sample #: 2020006509
Collection Date: 04/09/2020 12:45 PM Matrix: GW WW
Analyse Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
Total Suspended Solids - Low RL 2 5 - ❑20040246
TSS < 2.5 mg/L 2.5 1 SM2540D 04/14/2020 09:42 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-2-A4
Collection Date: 04/09/2020 09:25 AM
Analyse Result Units Qualifiers RDL
TOTAL ALKALINI - [-2004 325
Total Alkalinity as CaCO3
Alkalinity, Carbonate
Alkalinity, Bicarbonate
I N 0 R GARK IONS BY IC -
Chloride
Sulfate
_MERCURY IC LD VAPO
Mercury (Hg)
TOTAL RECOVE BLE
11.9
< 5
11.9
4 0040228
3.4
0.20
1 IN W TER - Q2004030
< 0.05
ETALS BY ICP - Q20040331
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
Aluminum (Al)
0.034
mg/L
Barium (Ba)
0.019
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
1.52
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Magnesium (Mg)
1.30
mg/L
Manganese (Mn)
0.018
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
0.864
mg/L
Sodium (Na)
2.54
mg/L
Strontium (Sr)
0.014
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE
ETALS BY ICP-MS - ❑ 00040345
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (MO)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
TOTAL DI SOLVED SOLIDS - Q20040280
TDS
34.0
mg/L
Sample #: 2020006570
Matrix: GW_WW
Page 6 of 34
DF Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/16/2020 18:32
PARMSTR
5
1
SM 2320B-2011
04/1612020 18:32
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:32
PARMSTR
0.1
1
EPA 300.0
04/16/2020 17:06
BGN9034
0.1
1
EPA 300.0
04/16/2020 17:06
BGN9034
0.05
1
EPA 245.1
04/1512020 12:58
DMFRANC
0.01
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/1712020 15:12
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.01
1
EPA 200.7
04117/2020 15:12
MHALL3
0.01
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.1
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:12
MHALL3
1
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
1
1
EPA 200.8
04122/2020 19:06
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
1
1
EPA 200.8
04/221202019:06
CWSPEN3
1
1
EPA 200.8
04122/2020 19:06
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
1
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
1
1
EPA 200.8
04/221202019:06
CWSPEN3
0.2
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
0.3
1
EPA 200.8
04/22/2020 19:06
CWSPEN3
25
1
SM2540C
04115/202010:42
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-5-A4
Collection Date: 04/09/2020 08:59 AM
Analyte Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - 020040246
TSS < 2.5 mg/L 2.5
Sample #: 2020006571
Matrix: GW WW
Page 9 of 34
DF
Method
Analysis Daterrime
Analyst
1
SM2540D
04/14/2020 09:46
GBSINGL

Certificate of Laboratory Analysis Page 10 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA_MW-5D-A4 Sample #: 2020006572
Collection Date: 04/09/2020 09:39 AM Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Daterrime
Analyst
TOTAL ALKALINITY - Q20040325
Total Alkalinity as CaCO3
38.6
mg/L
5
1
SM 2320B-2011
04/16/2020 18:38
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/16/2020 18:38
PARMSTR
Alkalinity, Bicarbonate
38.6
mg/L
5
1
SM 2320E-2011
04/16/2020 18:38
PARMSTR
INORGANIC IONS BY IC
- Q20040298
Chloride
0.79
mg/L
0.1
1
EPA 300.0
04/16/2020 17:22
BGN9034
Sulfate
0.15
mg/L
0.1
1
EPA 300.0
04/16/2020 17:22
BGN9034
MERCURY (COLD VAPOR)
IN WATER - 020040305
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/15/2020 13:03
DMFRANC
TOTAL RECOVERABLE
METALS BY ICP - 220040331
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/17/2020 15:21
MHALL3
Barium (Ba)
0.024
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/17/2020 15:21
MHALL3
Calcium (Ca)
8.51
mg/L
0.05
1
EPA 200.7
04/17/2020 15:21
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/17/2020 15:21
MHALL3
Magnesium (Mg)
1.89
mg/L
0.01
1
EPA 200.7
04/17/2020 15:21
MHALL3
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Potassium (K)
1.40
mg/L
0.1
1
EPA 200.7
04/17/2020 15:21
MHALL3
Sodium (Na)
6.74
mg/L
0.05
1
EPA 200.7
04/17/2020 15:21
MHALL3
Strontium (Sr)
0.108
mg/L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
Zinc (Zn)
< 0.005
mg1L
0.005
1
EPA 200.7
04/17/2020 15:21
MHALL3
TOTAL RECOVERABLE
METALS BY ICP-MS - Q20040345
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
Vanadium (V) Low Level
0.610
ug/L
0.3
1
EPA 200.8
04/22/2020 20:06
CWSPEN3
TOTAL DISSOLVED SOLIDS - ❑2004 2
TDS
74.0
mg/L
25
1
SM2540C
04/15/202010:44
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-5D-A4
Collection Date: 04/09/2020 09:39 AM
Analyte Result Units Qualifiers RDL
Total Suspended Solids - Low RL 2.5 - 020040246
TSS < 2.5 mg/L 2.5
Page 11 of 34
Sample #: 2020006572
Matrix: GW WW
DF Method Analysis Date/Time Analyst
1 SM2540D 04/14/2020 09:47 GBSINGL

Certificate of Laboratory Analysis Page 12 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-6-A4 Sample #: 2020006573
Collection Date: 04/09/2020 10:42 AM Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - 020040325
Total Alkalinity as CaCO3
15.8
mg/L
5
1
SM 2320B-2011
04/16/2020 18:42
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/16/2020 18:42
PARMSTR
Alkalinity, Bicarbonate
15.8
mg/L
5
1
SM 2320E-2011
04/16/2020 18:42
PARMSTR
INORGANIC IONS BY IC - 020040298
Chloride
3.4
mg/L
0.1
1
EPA 300.0
04/15/2020 22:38
BGN9034
Sulfate
0.75
mg/L
0.1
1
EPA 300.0
04/15/2020 22:38
BGN9034
MERCURY [COLD VAPORI IN WATER - Q20040305
Mercury (Hg)
0.08
ug/L
0.05
1
EPA 245.1
04/15/2020 13:05
DMFRANC
TOTAL RECOV BLE METALS BY ICP - 02 40331
Aluminum (AI)
< 0.01
mg/L
0.01
1
EPA 200.7
04/17/2020 15:25
MHALL3
Barium (Ba)
0.032
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/17/2020 15:25
MHALL3
Calcium (Ca)
3.63
mg/L
0.05
1
EPA 200.7
04/17/2020 15:25
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/17/2020 15:25
MHALL3
Magnesium (Mg)
1.44
mg/L
0.01
1
EPA 200.7
04/17/2020 15:25
MHALL3
Manganese (Mn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Potassium (K)
1.06
mg/L
0.1
1
EPA 200.7
04/17/2020 15:25
MHALL3
Sodium (Na)
2.98
mg/L
0.05
1
EPA 200.7
04/17/2020 15:25
MHALL3
Strontium (Sr)
0.037
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:25
MHALL3
TOTAL RECOVERABLE METALS BY ICP-MS - Q20040345
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/22/2020 20:14
CWSPEN3
TOTAL DISSOLVED SOLIDS - Q20040280
TDS
41.0
mg/L
25
1
SM2540C
04/151202010:44
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-6-A4
Collection Date: 04/09/2020 10:42 AM
Analyse Result Units Qualifiers RDL
Total Suspended Solids- Low RI-2.5 - Q20040246
TSS < 2.5 mg/L 2.5
Sample #: 2020006573
Matrix: GW WW
Page 13 of 34
DF
Method
Analysis Date/Time
Analyst
1
SM2540D
04/14/2020 09:47
GBSINGL

Certificate of Laboratory Analysis Page 14 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA_MW-7-A4 Sample #: 2020006574
Collection Date: 04/09/2020 10:50 AM Matrix: GW_WW
Analyse
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - 020040325
Total Alkalinity as CaCO3
< 5
mg/L
5
1
SM 2320E-2011
04/16/2020 18:45
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320E-2011
04/16/2020 18:45
PARMSTR
Alkalinity, Bicarbonate
< 5
mg/L
5
1
SM 232OB-2011
04/16/2020 18:45
PARMSTR
INORGANIC IONS BY IC - 020040298
Chloride
6.0
mg/L
0.5
5
EPA 300.0
04/15/2020 21:02
BGN9034
Sulfate
480
mg/L
5
50
EPA 300.0
04/15/2020 21:02
BGN9034
MERCURY LD VAPOR IN WATER
- Q20040305
Mercury (Hg)
0.29
ug/L
0.05
1
EPA 245.1
04/15/2020 13:07
DMFRANC
TOTAL REC VERABLE METALS BY
I P - Q20040331
Aluminum (AI)
20.1
mg/L
0.01
1
EPA 200.7
04/17/2020 15:30
MHALL3
Barium (Ba)
0.089
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/17/2020 15:30
MHALL3
Calcium (Ca)
39.6
mg/L
0.05
1
EPA 200.7
04/17/2020 15:30
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Iron (Fe)
< 0.01
mg/L
0.01
1
EPA 200.7
04/17/2020 15:30
MHALL3
Magnesium (Mg)
70.2
mg/L
0.01
1
EPA 200.7
04/17/2020 15:30
MHALL3
Manganese (Mn)
4.99
mg1L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Nickel (Ni)
0.901
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Potassium (K)
1.66
mg/L
0.1
1
EPA 200.7
04/17/2020 15:30
MHALL3
Sodium (Na)
6.25
mg/L
0.05
1
EPA 200.7
04/17/2020 15:30
MHALL3
Strontium (Sr)
0.008
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
Zinc (Zn)
0.053
mg/L
0.005
1
EPA 200.7
04/17/2020 15:30
MHALL3
TOTAL RECOVERABLE METALS BY
ICP-MS -
Q20040345
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Arsenic (As)
116
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Beryllium (Be)
2.42
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Cadmium (Cd)
1.20
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Cobalt (Co)
207
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Selenium (Se)
24.1
ug/L
1
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/23/2020 13:59
CWSPEN3
TOTAL DISSOLVED SOLIDS - 020040280
TDS
1170
mg/L
25
1
SM2540C
04/15/202010:45
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-7-A4
Collection Date: 04/09/2020 10:50 AM
Analyse Result Units Qualifiers RDL
Total Suspended Solids -Low RI-2.5 - Q20040246
TSS < 2.5 mg/L 2.5
Sample #: 2020006574
Matrix: GW WW
DF Method
1 SM2540D
Page 15 of 34
Analysis Date/Time Analyst
04/14/2020 09:47 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-9-A4
Collection Date: 04/07/2020 03:00 PM
Analyte Result Units Qualifiers RDL
TOTAL ALKALINITY - Q20040325
Total Alkalinity as CaCO3 37.2 mg1L
Alkalinity, Carbonate < 5 mg/L
Alkalinity, Bicarbonate 37.2 mg/L
INORGANIC IONS BY IC - Q200401 1
Chloride 0.67 mglL
Sulfate 0.10 mg/L
MERCURY C LID V O 1 IN WAT - 020040305
Mercury (Hg) < 0.05 ug/L
TOTAL RECOVERABLE METALS BY ICP - Q200403 1
Aluminum (AI)
0.019
mg/L.
Barium (Ba)
0.008
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
7.45
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
0.012
mg/L
Magnesium (Mg)
2.05
mg/L
Manganese (Mn)
< 0.005
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
1.49
mg/L
Sodium (Na)
6.70
mg/L
Strontium (Sr)
0.078
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE METALS BY ICP-MS -
C120040345
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
0.570
ug/L
TOTAL DISSOLVED SOLIDS - Q20040188
TDS
70.0
mg/L
Page 16 of 34
Sample #: 2020006575
Matrix: GW WW
DF Method Analysis Daterrime Analyst
5
1
SM 2320B-2011
04/16/2020 18:48
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:48
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:48
PARMSTR
0.1
1
EPA 300.0
04/09/2020 15:13
BGN9034
0.1
1
EPA 300.0
04/09/2020 15:13
BGN9034
0.05
1
EPA 245.1
04/15/2020 12:49
DMFRANC
0.01
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.01
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.01
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.1
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:34
MHALL3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
0.2
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
0.3
1
EPA 200.8
04/22/2020 20:31
CWSPEN3
25
1
SM2540C
04/09/202010:49
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA MW-9-A4
Collection Date: 04/07/2020 03:00 PM
Analyte Result Units Qualifiers RDL DF
Total Suspended Solids -Low RL 2.5 - Q20040178
TSS < 2.5 mg/L 2.5 1
Page 17 of 34
Sample #: 2020006575
Matrix: GW WW
Method Analysis Date/Time Analyst
SM2540D 04/09/2020 06:58 GBSINGL

Certificate of Laboratory Analysis Page 18 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA_FD-20200409-1 Duplicate Sample #: 2020006576
Collection Date: 04/09/2020 Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
TOTAL ALKALINITY - 020040325
Total Alkalinity as CaCO3
37.2
mg/L
5
1
SM 2320E-2011
04/16/2020 18:51
PARMSTR
Alkalinity, Carbonate
< 5
mg/L
5
1
SM 2320B-2011
04/16/2020 18:51
PARMSTR
Alkalinity, Bicarbonate
37.2
mg/L
5
1
SM 2320B-2011
04/16/2020 18:51
PARMSTR
INORGANIC IONS BY IC
- Q20040298
Chloride
0.80
mg/L
0.1
1
EPA 300.0
04/15/2020 23:59
BGN9034
Sulfate
1.8
mg/L
0.1
1
EPA 300.0
04/15/2020 23:59
BGN9034
MERCURY (COLD VAPOR}
IN WATER - ❑20040305
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
04/15/2020 13:09
DMFRANC
TOTAL RECOVERABLE METALS BY ICP - 020040331
Aluminum (AI)
0.070
mg/L
0.01
1
EPA 200.7
04/17/2020 15:39
MHALL3
Barium (Ba)
0.007
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Boron (B)
< 0.05
mg/L
0.05
1
EPA 200.7
04/17/2020 15:39
MHALL3
Calcium (Ca)
3.87
mg/L
0.05
1
EPA 200.7
04/17/2020 15:39
MHALL3
Chromium (Cr)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Copper (Cu)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Iron (Fe)
0.082
mg/L
0.01
1
EPA 200.7
04/17/2020 15:39
MHALL3
Magnesium (Mg)
1.07
mg/L
0.01
1
EPA 200.7
04/17/2020 15:39
MHALL3
Manganese (Mn)
0.298
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Nickel (Ni)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Potassium (K)
1.99
mg/L
0.1
1
EPA 200.7
04/17/2020 15:39
MHALL3
Sodium (Na)
12.2
mg/L
0.05
1
EPA 200.7
04/17/2020 15:39
MHALL3
Strontium (Sr)
0.035
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
Zinc (Zn)
< 0.005
mg/L
0.005
1
EPA 200.7
04/17/2020 15:39
MHALL3
TOTAL RECOVERABLE METALS BY ICP-MS - 020040345
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Molybdenum (Mo)
8.77
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
Vanadium (V) Low Level
0.453
ug/L
0.3
1
EPA 200.8
04/22/2020 20:39
CWSPEN3
TOTAL DISSOLVED SOLIDS - Q20040280
TDS
66.0
mg/L
25
1
SM2540C
04115/202010:45
GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA_FD-20200409-1 Duplicate
Collection Date: 04/09/2020
Analyse Result Units Qualifiers RDL DF
Total Suspended Solids -Low RL 2.5 - 020040246
TSS < 2.5 mg/L 2.5 1
Sample #: 2020006576
Matrix: GW WW
Page 19 of 34
Method Analysis Date/Time Analyst
SM2540D 04/14/2020 09:48 GBSINGL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Site: ASA FB-20200409-945 Field Blank
Collection Date: 04/09/2020 09:45 AM
Analyte Result Units Qualifiers RDL DF
TOTAL ALKALINITY - 020040325
Total Alkalinity as CaCO3 < 5 mg/L
Alkalinity, Carbonate < 5 mg/L
Alkalinity, Bicarbonate < 5 mg/L
INORGANIC IONS BY IC - Q20940298
Chloride < 0.1 mg/L
Sulfate < 0.1 mg/L
MERCURY ICOLD VAPOR) IN WATER - Q20040305
Mercury (Hg) < 0.05 ug/L
TOTAL RECOVERABLE METALS BY ICP - Q20040331
Aluminum (Al)
< 0.01
mg/L
Barium (Ba)
< 0.005
mg/L
Boron (B)
< 0.05
mg/L
Calcium (Ca)
< 0.05
mg/L
Chromium (Cr)
< 0.005
mg/L
Copper (Cu)
< 0.005
mg/L
Iron (Fe)
< 0.01
mg/L
Magnesium (Mg)
< 0.01
mg/L
Manganese (Mn)
< 0.005
mg/L
Nickel (Ni)
< 0.005
mg/L
Potassium (K)
< 0.1
mg/L
Sodium (Na)
< 0.05
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE METALS BY ICP-M - Q20040345
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
Sample #: 2020006577
Matrix: GW WW
Page 20 of 34
Method Analysis Date/Time Analyst
5
1
SM 2320B-2011
04/16/2020 18:55
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:55
PARMSTR
5
1
SM 2320B-2011
04/16/2020 18:55
PARMSTR
0.1
1
EPA 300.0
04/15/2020 21:34
BGN9034
0.1
1
EPA 300.0
04/15/2020 21:34
BGN9034
0.05
1
EPA 245.1
04/15/2020 13:12
DMFRANC
0.01
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.01
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.01
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.1
1
EPA 200.7
04/17/2020 16:43
MHALL3
0.05
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
0.005
1
EPA 200.7
04/17/2020 15:43
MHALL3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
1
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
0.2
1
EPA 200.8
04/22/2020 20:47
CWSPEN3
0.3
1
EPA 200.8
04/22/2020 20:47
CWSPEN3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040325 ALK CarbBicarb TOTAL ALKALINITY
Page 21 of 34
Duplicate # 1
Parent Sample:
J20030213 -- 2020006509
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
Alkalinity, Bicarbonate
37.2
37.2
mg/L
1
0 - 20%
1.08
Alkalinity, Carbonate
0
0
mg/L
1
0- 20%
0
-
Total Alkalinity as CaCO3
37.2
37.2
mg/L
1
0 - 20%
1.08
-
Duplicate # 2
Parent Sample:
J20040190 -- 2020009425
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
Alkalinity, Bicarbonate
0
0
mg/L
1
0- 20%
0
Alkalinity, Carbonate
116
116
mg/L
1
0 - 20%
0.782
Total Alkalinity as CaCO3
94.7
94.7
mg/L
1
0 - 20%
0.657
LCS # 1
Parameter
Measured
Final
Units:
Dil
Sgike
% Recovery LCL
UCL
Qualifier
Total Alkalinity as CaCO3
105
105
mg/L
1
105
100 85
115
LCS # 2
Parameter
Measured
Final
Units:
Dil
Saike
% Recovery LCL
UCL
Qualifier
Total Alkalinity as CaCO3
105
105
mg/L
1
105
100 85
115

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040181 Dionex INORGANIC IONS BY IC
Blank # 1
Page 22 of 34
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Chloride
0
0
mg/L
1
0.1
< 1/2 RDL
Sulfate
0
0
mg/L
1
0.1
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
Chloride
1.92
1.92
mg/L
1
2
96 90
110
-
Sulfate
1.91
1.91
mg/L
1
2
95.5 90
110
-
MS # 1
Parent Sample:
J20040176
-- 2020009363
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
Chloride
2.87
143
mg/L
50
100
96.4 80
120
Sulfate
5.69
285
mg1L
50
100
97.2 80
120
MSD # 1
Parent Sample:
J20040176
-- 2020009363
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery LCL
UCL
RPD Qualifier
Chloride
2.85
142
mg/L
50
100
95.6 80
120
0.875
Sulfate
5.68
284
mg/L
50
100
96.4 80
120
0.811

Certificate of Laboratory Analysis Page 23 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040298 Dionex INORGANIC IONS BY IC
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
Chloride 0 0 mg/L 1 0.1 < 112 RDL
Sulfate 0 0 mg/L 1 0.1 < 1/2 RDL
LCS # 1
Parameter Measured Final
Chloride 2.06 2.06
Sulfate 2.05 2.05
MS # 1
Parameter
Measured
Final
Chloride
2.78
2.78
Sulfate
3.68
3.68
MSD # 1
Parameter Measured Final
Chloride 2.78 2.78
Sulfate 3.67 3.67
Units:
Dil
Spike
% Recovery LCL
UCL Qualifier
mg/L
1
2
103 90
110
mg/L
1
2
102 90
110
Parent Sample:
J20030213 -- 2020006509
Units:
Dil
Spike
% Recovery LCL
UCL Qualifier
mg/L
1
2
98.8 80
120
mg/L
1
2
96.1 80
120
Parent Sample:
J20030213 -- 2020006509
Units:
Dil
Spike
% Recovery LCL
UCL RPD Qualifier
mg/L
1
2
98.5 80
120 0.304
mg/L
1
2
96 80
120 0.156

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040305 HG 245.1 MERCURY (COLD VAPOR) IN WATER
Blank # 1
LCS # 1
h% (.MlmI
MSD # 1
Parameter Measured Final
Mercury (Hg) -0.009 -0.009
Parameter Measured Final
Mercury (Hg) 2.08 2.08
Parameter Measured Final
Mercury (Hg) 0.993 0.993
Parameter Measured Final
Mercury (Hg) 0.999 0.999
Page 24 of 34
Units:
Dil
RDL
Relative Concentratio
Qualifier
ug/L
1
0.05
< 1/2 RDL
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
ug/L
1
2
104 85
115
Parent Sample:
J20030213
-- 2020006575
Units:
Dil
Spike
% Recovery LCL
UCL
Qualifier
ug/L
1
1
98.1 70
130
-
Parent Sample:
J20030213
-- 2020006575
Units:
Dil
Spike
% Recovery LCL
UCL
RPD Qualifier
ug/L
1
1
98.7 70
130
0.61

Certificate of Laboratory Analysis Page 25 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040331 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Aluminum (AI)
0.000776
0.000776
mg/L
1
0.01
< 1/2 RDL
Barium (Ba)
-0.000053
-0.000053
mg/L
1
0.005
< 112 RDL
Boron (B)
0.000525
0.000525
mg/L
1
0.05
< 1/2 RDL
Calcium (Ca)
0.00291
0.00291
mg/L
1
0.05
< 1/2 RDL
Chromium (Cr)
-0.000012
-0.000012
mg/L
1
0.005
< 1/2 RDL
Copper (Cu)
-0.000916
-0.000916
mg/L
1
0.005
< 1/2 RDL
Iron (Fe)
-0.000881
-0.000881
mg/L
1
0.01
< 1/2 RDL
Magnesium (Mg)
-0.000163
-0.000163
mg/L
1
0.01
< 1/2 RDL
Manganese (Mn)
-0.000475
-0.000475
mg/L
1
0.005
< 1/2 RDL
Nickel (Ni)
0.000057
0.000057
mg/L
1
0.005
< 1/2 RDL
Potassium (K)
0.0138
0.0138
mg/L
1
0.1
< 1/2 RDL
Sodium (Na)
-0.000518
-0.000518
mg/L
1
0.05
< 1/2 RDL
Strontium (Sr)
-0.000062
-0.000062
mg/L
1
0.005
< 1/2 RDL
Zinc (Zn)
0.000324
0.000324
mg/L
1
0.005
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
5.08
5.08
mg/L
1
5
102
85
115
Barium (Ba)
5.09
5.09
mg/L
1
5
102
85
115
Boron (B)
4.95
4.95
mg/L
1
5
99
85
115
Calcium (Ca)
5.07
5.07
mg/L
1
5
101
85
115
Chromium (Cr)
5.01
5.01
mg/L
1
5
100
85
115
Copper (Cu)
5
5
mg/L
1
5
99.9
85
115
Iron (Fe)
5.05
5.05
mg/L
1
5
101
85
115
Magnesium (Mg)
5.02
5.02
mg/L
1
5
100
85
115
Manganese (Mn)
5.07
5.07
mg/L
1
5
101
85
115
Nickel (Ni)
5.05
5.05
mg/L
1
5
101
85
115
Potassium (K)
4.98
4.98
mg/L
1
5
99.5
85
115 -
Sodium (Na)
4.97
4.97
mg/L
1
5
99.5
85
115 -
Strontium (Sr)
4.98
4.98
mg/L
1
5
99.5
85
115 -
Zinc (Zn)
5.03
5.03
mg/L
1
5
101
85
115 -
MS # 1
Parent Sample:
J20030213 -- 2020006509
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL Qualifier
Aluminum (AI)
4.98
4.98
mg/L
1
5
98.4
70
130 -
Barium (Ba)
5.01
5.01
mg/L
1
5
100
70
130 -
Boron (B)
4.93
4.93
mg/L
1
5
98.3
70
130 -
Calcium (Ca)
8.68
8.68
mg/L
1
5
96.7
70
130 -
Chromium (Cr)
4.9
4.9
mg/L
1
5
98
70
130 -
Copper (Cu)
4.87
4.87
mg/L
1
5
97.4
70
130 -

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040331 ICP_TRM TOTAL RECOVERABLE METALS BY ICP
MS # 1
Parameter
Measured
Final
Iron (Fe)
5.02
5.02
Magnesium (Mg)
5.94
5.94
Manganese (Mn)
5.22
5.22
Nickel (Ni)
4.92
4.92
Potassium (K)
6.83
6.83
Sodium (Na)
16.6
16.6
Strontium (Sr)
4.95
4.95
Zinc (Zn)
4.89
4.89
MSD # 1
Parameter
Measured
Final
Aluminum (AI)
5.18
5.18
Barium (Ba)
5.18
5.18
Boron (B)
5.09
5.09
Calcium (Ca)
8.85
8.85
Chromium (Cr)
5.08
5.08
Copper (Cu)
5.06
5.06
Iron (Fe)
5.22
5.22
Magnesium (Mg)
6.13
6.13
Manganese (Mn)
5.41
5.41
Nickel (Ni)
5.12
5.12
Potassium (K)
7
7
Sodium (Na)
16.7
16.7
Strontium (Sr)
5.1
5.1
Zinc (Zn)
5.08
5.08
Page 26 of 34
Parent Sample:
J20030213 -- 2020006509
Units:
Dil
Soike
% Recovery
LCL
UCL
Qualifier
mg/L
1
5
98.9
70
130
mg/L
1
5
97.6
70
130
mg/L
1
5
98.8
70
130
mg/L
1
5
98.4
70
130
mg/L
1
5
96.7
70
130
mg/L
1
5
89.3
70
130
-
mg/L
1
5
98.4
70
130
-
mg/L
1
5
97.7
70
130
-
Parent Sample:
]20030213
-- 2020005509
alai :
Dil
Snike
% Recovery
ILL
UCL
RPD Qualifier
mg1L
1
5
102
70
130
3.86
mg1L
1
5
104
70
130
3.45
mg/L
1
5
102
70
130
3.35
mg/L
1
5
100
70
130
1.88
mg/L
1
5
102
70
130
3.67
mg1L
1
5
101
70
130
3.83 -
mg/t_
1
5
103
70
130
3.87 -
mglL
1
5
101
70
130
3.1 -
mg/L
1
5
102
70
130
3.46
mg/L
1
5
102
70
130
4
mg/L
1
5
99.9
70
130
2.36
mg/L
1
5
92.8
70
130
1.05
mg/L
1
5
101
70
130
2.92
mg/L
1
5
102
70
130
3.91

Certificate of Laboratory Analysis Page 27 of 34
This report shall not be reproduced, except in full.
Order# J20030213
Level II QC Summary
Q20040345 IMS_TRM TOTAL RECOVERABLE METALS BY ICP-MS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL
Relative Concentration
Qualifier
Antimony (Sb)
0.047
0.047
ug/L
1
1
< 1/2 RDL
Arsenic (As)
0.011
0.011
ug/L
1
1
< 1/2 RDL
Beryllium (Be)
0.034
0.034
ug/L
1
1
< 1/2 RDL
Cadmium (Cd)
0
0
ug/L
1
1
< 1/2 RDL
Cobalt (Co)
0.006
0.006
ug/L
1
1
< 1/2 RDL
Lead (Pb)
-0.001
-0.001
ug/L
1
1
< 1/2 RDL
Molybdenum (Mo)
0.009
0.009
ug/L
1
1
< 1/2 RDL
Selenium (Se)
-0.01
-0.01
ug/L
1
1
< 1/2 RDL
Thallium (TI) Low Level
0.026
0.026
ug/L
1
0.2
< 1/2 RDL
Vanadium (V) Low Level
-0.031
-0.031
ug/L
1
0.3
< 1/2 RDL
LCS # 1
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL
Qualifier
Antimony (Sb)
48.9
48.9
ug/L
1
50
97.7
85
115
Arsenic (As)
52.5
52.5
ug/L
1
50
105
85
115
Beryllium (Be)
50.9
50.9
ug/L
1
50
102
85
115
Cadmium (Cd)
49.6
49.6
ug/L
1
50
99.2
85
115
Cobalt (Co)
51.4
51.4
ug/L
1
50
103
85
115
Lead (Pb)
49.1
49.1
ug/L
1
50
98.3
85
115
Molybdenum (Mo)
51.1
51.1
ug/L
1
50
102
85
115
Selenium (Se)
50
50
ug/L
1
50
100
85
115
Thallium (TI) Low Level
48.7
48.7
ug/L
1
50
97.4
85
115
Vanadium (V) Low Level
49.3
49.3
ug/L
1
50
98.5
85
115
MS # 1
Parent Sample:
J20030213
-- 2020006570
Parameter
Measured
Final
Units:
Dil
an&
% Recovery
LCL
UCL
Qualifier
Antimony (Sb)
49.6
49.6
ug/L
1
50
99.1
70
130
Arsenic (As)
51.1
51.1
ug/L
1
50
102
70
130
Beryllium (Be)
50.7
50.7
ug/L
1
50
101
70
130
Cadmium (Cd)
50
50
ug/L
1
50
100
70
130
Cobalt (Co)
51.1
51.1
ug/L
1
50
101
70
130
Lead (Pb)
49.4
49.4
ug/L
1
50
98.7
70
130
Molybdenum (Mo)
50.9
50.9
ug/L
1
50
102
70
130
Selenium (Se)
50.3
50.3
ug/L
1
50
101
70
130
Thallium (TI) Low Level
48.9
48.9
ug/L
1
50
97.6
70
130
Vanadium (V) Low Level
49.8
49.8
ug/L
1
50
99.4
70
130
-
MSD # 1
Parent Sample:
J20030213
-- 2020006570
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LCL
UCL
RPD Qualifier
Antimony (Sb)
50.3
50.3
ug/L
1
50
100
70
130
1.33

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Page 28 of 34
Level II QC Summary
Q20040345 IMS_TRM TOTAL RECOVERABLE METALS
BY ICP-MS
MSD # 1
Parent
Sample:
J20030213
-- 2020006570
Parameter
Measured
Final
Units:
Dil
Spike
% Recovery
LC
UCL
RPD Qualifier
Arsenic (As)
52.6
52.6
ug/L
1
50
105
70
130
2.79 -
Beryllium (Be)
52.7
52.7
ug/L
1
50
105
70
130
3.9 -
Cadmium (Cd)
50.9
50.9
ug/L
1
50
102
70
130
1.72 -
Cobalt (Co)
52.5
52.5
ug/L
1
50
104
70
130
2.74 -
Lead (Pb)
50.7
50.7
ug/L
1
50
101
70
130
2.7 -
Molybdenum (Mo)
52.3
52.3
ug/L
1
50
105
70
130
2.8 -
Selenium (Se)
50.5
50.5
ug/L
1
50
101
70
130
0.28 -
Thallium (TI) Low Level
50.4
50.4
ug/L
1
50
101
70
130
3.09 -
Vanadium (V) Low Level
51.1
51.1
ug/L
1
50
102
70
130
2.49 -

Certificate of Laboratory Analysis
Page 29 of 34
This report shall not be
reproduced, except in full.
Order #
J20030213
Level II QC Summary
Q20040188 TDS
TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
2
mg/L
1
25 < 1/2 RDL
Blank # 2
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
7
mg/L
1
25 < 1/2 RDL
Blank # 3
Parameter
Measured
Final
Units:
Dil
RDL Relative Concentration
Qualifier
TDS
4
mg/L
1
25 < 1/2 RDL
Duplicate # 1
Parent Sample:
J20030022 --
2020005591
Parameter
Measured
Final
Units:
Dil
Limit Ramie
RPD
Qualifier
TDS
315
mg/L
1
0 - 10%
1.6
Duplicate # 2
Parent Sample:
J20030022 --
2020005594
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
303
mg/L
1
0 - 10%
1.31
-
Duplicate # 3
Parent Sample:
J20030141 --
2020006117
Parameter
Measured
Final
Units:
Dil
Limit Range
RPD
Qualifier
TDS
101
mg/L
1
0 - 10%
0
-
Duplicate # 4
Parent Sample:
J20030178 --
2020006299
Parameter
Measured
Final
Units:
Dil
Limit Ran(Le
RPD
Qualifier
TDS
421
mg1L
1
0 - 10%
0.476
-
Duplicate # 5
Parent Sample:
J20030210 --
2020006502
Parameter
Measured
Final
Units:
Dil
Limit Rance
RPD
Qualifier
TDS
40
mg/L
1
0 - 10%
7.79
-
LCS # 1
Parameter
Measured
Final
Units:
Dil
Sgike %Recoveia LCL
UCL
Qualifier
TDS
992
mg/L
1
1000 99.2 90
110
-

Certificate of Laboratory Analysis
Page 30 of 34
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040280 TDS TOTAL DISSOLVED SOLIDS
Blank # 1
Parameter Measured
Final
Units: Dil RDL Relative Concentratio
Qualifier
TDS
3
mg/L 1 25 < 1/2 RDL
Blank # 2
Parameter Measured
Final
Units: DiI RDL Relative Concentration
Qualifier
TDS
3
mg/L 1 25 < 1/2 RDL
Duplicate # 1
Parent Sample:
J20030210 --
2020006537
Parameter Measured
Final
Units: Dil
Limit Ranu
RPD
Qualifier
TDS
34
mg/L 1
0 - 10%
8.45
-
Duplicate # 2
Parent Sample:
J20030213 --
2020006509
Parameter Measured
Final
Units: Dil
Limit Range
RPD
Qualifier
TDS
68
mg/L 1
0 - 10%
15
R1
Duplicate # 3
Parent Sample:
J20030213 --
2020006570
Parameter Measured
Final
Units: Dil
Limit Ranee
RPD
Qualifier
TDS
31
mg/L 1
0 - 10%
9.23
-
Duplicate # 4
Parent Sample:
J20030213 --
2020006571
Parameter Measured
Final
Units: Di
Limit Ra
RPD
Qualifier
TDS
71
mg/L 1
0 - 10%
1.4
LCS # 1
Parameter Measured
Final
Units: Dil Spike % Recovws LCL
UCL
Qualifier
TDS
993
mg/L 1 1000 99.3 90
110
-
Qualifiers:
R1 Relative Percent
Difference exceeded method acceptance limits.

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040178 TSS_LL Total Suspended Solids - Low RL 2.5
Page 31 of 34
Blank # 1
Parameter Measured Final Units: Dil RDL Relative Concentration Qualifier
TSS 0 mg/L 1 2.5 < 1/2 RDL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J20030213
Level II QC Summary
Q20040246 TSS_LL Total Suspended Solids - Low RL 2.5
Blank # 1
Parameter Measured Final
TSS 0
Duplicate # 1
Parameter Measured Final
TSS 0.4
LCS # 1
Parameter Measured Final
TSS 45.2
LCSD # 1
Parameter Measured Final
TSS 50.8
Page 32 of 34
Units:
Dil
RDL
Relative Concentration
Qualifier
mg/L
1
2.5
< 1/2 RDL
Parent Sample:
J20030206 -- 2020006487
Units:
DilLimit
Ranta
RPD
Qualifler
mg/L
1
120
R
Units:
Dil
Spike
%Recovery LCL
UCL
Qualifier
mg/L
1
50
90.4 90
110
Units:
Dil
Spike
% Recovery LCL
UCL
'RPD
Qualifier
mg/L
1
50
102 90
110
11.7
-
Qualifiers:
R % RPD indeterminate due to low concentration in the parent sample.

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