NC0051161_Non-Compliance Notification_20200803

August 3, 2020
Via FedEx/Email
Mr. Ron Boone
Winston Salem Regional Office - DWR
North Carolina Department of Environmental Quality
450 West Hanes Mill Rd, Suite 300
Winston Salem, NC 27105
Reference: Written Report for 07/30/20 Verbal Notification
Plantation Pipe Line— Greensboro Tank Farm
NPDES Permit NCD051161
Dear Mr. Boone,
NC Department of
Environmental Quality
Received
AUG 0 4 2020
Winston-Salem
Regional Office
Per Section E.6 (a) of the current NPDES permit, enclosed is the follow up written report for the
verbal notification provided on 7/30/20 regarding the monthly sample result for total suspended
solids (TSS) above permit effluent limits. As discussed with Ms. Graznak during the verbal
notification, Kinder Morgan collected additional compliance samples on July 30, 2020 and
discussed the original TSS analytical results with PACE laboratories. These actions/ discussions
resulted in the following conclusions:
• The initial report by PACE laboratories of the sample collected on 7/15/20 resulted in a
TSS value of 146 mg/L. Since there was no apparent TSS problem during sample collection
and since results were not in line with historical sampling results, Kinder Morgan
requested a QA/QC review by the laboratory.
After review of the QA/QC data and the additional testing results from the original
sample (although out of hold time), the laboratory rejected the original result for TSS of
146 mg/L and reissued the analytical report (attached).
• On July 30, 2020 following the verbal notification to the Winston-Salem Regional office,
an additional setof compliance samples were collected and sentto R&A Laboratories and
PACE for TS5 analysis. The analytical results for these samples reflect TSS levels of 8.20
mg/I and 7.57 mg/L respectively. These results are in line with historical records. The
analytical reports are attached for your review.
P. O. BOX 18306
GREENSBORO, NORTH CAROLINA 27419 D;g,!_S�! 'Y
6907-A WEST MARKET STREET 7■i1A
GREENSBORO, NORTH CAROLINA 27409

PPL Greensboro Tank Farm
Written Report for 7/30/20 Verbal Notification
Page 2
Since the laboratory has rejected the TSS analytical result from the 07/15/20 sampling event due
to lab error, there was no exceedance of the permitted effluent limit for TSS. Kinder Morgan
wishes to withdraw the original verbal notification of permit limit exceedance forTSS.
Kinder Morgan will report the TSS results of the 7/30/20 sampling in the upcoming DMR report
for July 2020.
Please do not hesitate to contact Johnny Tapia at [phone] if you have any comments or
questions. Thank you in advance for your assistance with this matter.
Sincerely,
i my Stamey
perations Manager
Plantation Pipe Line
Attachments
cc:
Johnny Tapia, EHS
EHSDS
_+ P. O. BOX 18306
GREENSBORO, NORTH CAROLINA 27419 a [°
6907-A WEST MARKET STREET Dig €a Safe'+
V
``''GREENSBORO, NORTH CAROLINA 27409

ANALYTICAL REPORT
aceAnalytical®
-� NaEonal centerlor Tasliny 8lm:a.'a August 03, 2020
Revised Report
Alc
aSs
SWE Inc. -Raleigh NC
4Cn
Sample Delivery Group: L1240064
Samples Received: 07/16/2020
Sr
Project Number: 4305-19-001
Description: PLANTATION
6Qc
[GI
Report To: Claudia Irvin / Michael Pfeifer
3201 Spring Forest Road
A,I
Raleigh, NC 27616
9Sc
Entire Report Reviewed By: -
Tom Mellette
Project Manager
Results relate only to the items tested or wlibra Led and are reported as rounded values. This lest report shall not be
customer, results relate to
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
S&ME Inc. -Raleigh NC 4305-19-001 L1240064 08103/2009:51 1of14

TABLE OF CONTENTS ONE LAB. NATIONWIDE.
Tc: "Fable of Contents
Ss: Sample Summary
3
d RI
Cn: Case Narrative
4
5
aSs
Sr: Sample Results
OUTFALL 002 L1240064-01
5
4
Cn
Qc: Quality Control Summary
6
Gravimetric Analysis by Method 2540 D-2011
6
SSr
Wet Chemistry by Method 1664B
8
6Qc
Wet Chemistry by Method 2130 B-2011
9
Wet Chemistry by Method 420.4
10
Gl
Volatile Organic Compounds (GC/MS) by Method 624.1
11
Gl: Glossary of Terms
12
FAl
Sc Sample Chain of Custody
14
9SC
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
S&ME Inc. - Raleigh NC 4305-19-001 L1240064 08/03/2009:51 2of 14

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
OUTFALL 002 L1240064-01 WW
Collected by
Gary Simcox
Collected date/time
07I152013:45
Received dateltime
07/16/2008:45
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
dateltime
dateltime
Gravimetric Analysis by Method 2540 D-2011
WG1511180
1
07/1620 05:55
07A82010:34
TH
Mt. Juliet, TN
Gravimetric Analysis by Method 2540 D-2011
WG1517891
1
0713012016:30
07/3012016:54
MMF
Mt. Juliet, TN
Wet Chemistry by Method 1664B
WGI512957
1
07/212017:32
07232000:00
DLH
Mt. Juliet, TN
Wet Chemistry by Method 2130 B-2011
WGI510216
1
07116/2016:58
071162016:58
KPS
Mt. Juliet, TN
Wet Chemistry by Method 420.4
WGI512572
1
071212013:36
0722/2011:36
BAM
Mt, Juliet, TN
Volatile Organic Compounds)GC/MS) by Method 624.1
WGI511379
1
07/18202139
07AS2021:39
ADM
Mt. Juliet, TN
ACCOUNT: PROJECT: SOO: DATE/TIME: PAGE:
5&ME Inc. -Raleigh NC 4305-19-001 L1240064 08/03/2009:51 3of14

k r,.,. . ds,� C ., 3r ,:aa�....�:4. ,<}at •P, r:..ufh�°".,�. ,a,;� „-.�,1 ,<r,dt,�'?'x ,.r.:.. z:: `it'e ,m„ mk:;. ,,. �� �-.vd�5�'. �.
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
G�Gyt ' L
Tom Mellette
Project Manager
Report Revision Histo
Level II Report -Version is 07/23/2019:26
Level II Report -Version 2: 07/3112018:23
Project Narrative
All data points lead to the value of146mg/I was an erroneous result due to a lab error.
The analysis for TSS was reanalyzed due to the value of 146 mg/L being outside of the historical range. This analysis was done
in duplicate and yielded results of19 mg/L and 20.4 mg/L. These values are much more in line with historical data however this
analysis was completed beyond the 7 day hold time.
ACCOUNT: PROJECT: SDG: DATE/rIME: PAGE:
S&ME Inc. -Raleigh NC 4305-19-001 L1240064 08/03/2009:51 4of14

10
OUTFALL 002 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected dale/time. 07115/20 13:45 L1240064
Gravimetric Analysis by Method 2540 D-2011
--
Result Qualifier
RDL
Dilution Analysis Batch
Analyte ugfl
ugll
date/time
Suspended Solids 146000 R
25000
1 07/181202010:34 WG1511180
Suspended Solids 19600 Q
10000
1 07/30120201654 WGIS17891
Wet Chemistry by Method 1664B
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte ugll
ugll
date/time
TPH -Oil&Grease NO
5440
1
0723/202000:00
WG1512957
Wet Chemistry by Method 2130 B-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte NTU
NTU
date/time
Turbidity 6.02
0.400
1
07A6202016:58
WGI510216
Wet Chemistry by Method 420.4
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ugfl
ugll
date/time
Total Phenol by 4AAP
NO
40.0
1
0722/202011:36
WG1512572
Volatile Organic Compounds
(GC/MS) by Method 624.1
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date/time
Benzene
ND
1.00
1
07/181202021:39
WG1511379
Ethylbenzene
ND
1.00
1
07ABI202021:39
WGI511379
Toluene
ND
1.00
1
07118202021:39
WGI511379
Xylenes, Total
NO
3.00
1
07/181202021:39
WG1511379
Methyl tert-butyl ether
NO
1.00
1
07/18/202021:39
WG1511379
Naphthalene
NO
5.00
1
07118/202021:39
WG1511379
(S)Toluene-d8
110
80.0-120
07481202021.39
WG1511379
(S)4-Bromofluorobenzene
105
80.0-120
071781202021,39
WG1511379
P 1,2-Dichloroethone-d4
108
70.0-130
0717WO2021.39
WGIS11379
ACCOUNT: PROJECT: SDG: DATE/NME: PAGE:
5&ME Inc. - Raleigh NC 4305-19-001 L1240064 08/032009:51 5cF14

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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Feld Spikes, Reid Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit
Rea.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) -Analyzes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported..
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analyzes in the sample are higher than the highest limit of concentration that the
Dilution
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target% recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sam pie analysis will target all analytes recovered or
duplicated within these ranges.
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Original Sample
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative If applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyze, the result in this column may state "ND" (Not Detected) or"BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest valuethat the laboratory could detect
or reportfor this analyze.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Quality Control
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
Summary (Qc)
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (So)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
Sample Summary (Ss)
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
JS
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P7
RPD value not applicable for sample concentrations less than 5 times the reporting limit
Q
Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
R
Rejected: Results have been rejected by the lab and should not be used.
Is .
7C
eSs
QCn
5Sr
aQC
Al
aJC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
S&MElnc.-Raleigh NC 4305-19-001 L1240064 08/03/2009:51 12 of

ACCREDITATIONS i LOCATIO S ONE LAB. NATIONWIDE.
Pace National
- Accreditation is
tale �CCI"edlt ffons
Alabama
40660
Alaska
1T026
Arizona
AZ0612
Arkansas
88-0469
California
2932
Colorado
TN00003
Connecticut
PH-0197
Florida
E87487
Georgia
NELAP
Georgia
923
Idaho
TN00003
Illinois
200008
Indiana
C-TN-01
Iowa
364
Kansas
E-10277
Kentuckyt8
90010
Ksntucky2
16
Louisiana
A130792
Louisiana'
LA180010
Maine
TN0002
Maryland
324
Massachusetts
M-TN00.3
Michigan
9958
Minnesota
047-999-395
Mississippi
TN00003
Missouri
340
Montana
CERT0086
1 hird Party Federal Acciedita'Lions
One phone call,
Hon design is the design of ourlabomlorycampus. The model is can
iample Integrity. Ourfocus on premium quality and prompt service t
s reported In the attached report.
scope of accreditation held by Pace National.
Nebraska
Nevada
New Hampshire
New Jersey—NELAP
New Mexico'
Newyork
North Carolina
North Carolina'
North Carolina'
North Dakota
Ohio—VAP
Oklahoma
Oregon
Pennsylvania
Rhode Island
South Carolina
South Dakota
Tennessee"
Texas
Texas °
Utah
Vermont
Virginia
Washington
WestVirginla
Wisconsin
Wyoming
unit of contact, one laboratory. No other lab Is as
e to the collective totals of the network
e to accelerated productivity. decreasing
us to be YOUR LAB OF CHOICE.
- - NE-OS-15-05 _--
TN-03-2002-34
2975
TN002
We
11742
Env375
DW21704
41
R-140
CL0069
9915
TN200002
68-02979
LA000356
84004
me
2006
T104704245-IB45
LAB0152
TN00003
VF2006
460132
C847
233
9980939910
A21A
A2LA— ISO 17025
1461.01
AIHA4AP,LLC EMLAP
100789
A21A— ISO 170255
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
'Dunking Water 2 Underground Stooge Tanks'Aquatk Toxicity 4Chemicaftcrobiological °Mold 6Wamewater Na Accreditation not applicable
Ow LI r Locations
Pace National has sbty4ourclient support centers that provide sample pickup andlorthe delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
FL
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ACCOUNT: PROJECT: SDG: DATEMME:
S&ME Inc. -Raleigh NC 430549-001 L1240064 08/032009:51
PAGE:
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r a Ysax av R n R + &1 r i 77Cd
For: S&ME, Inc.
8646 W. Market Street Suite 105
Greensboro, NC 27409
Attn: Claudia Irving
Report of Analysis
7/31/2020
MWYPj Jp+++
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o 01
CIE:M NC 1134 y:
NC#37701
ii.OFA �/RgCtpP 5�r��j
Client Sample ID: Outfall 002 - Plantation - 4305-19-001 Lab Sample ID: 85386-01
Site: S&ME Inc Collection Date: 7/30/2020 13:30
Parameter Method Result Units -Rep Limit Analyst Analysis Date/Time
Total Suspended Solids SM 2450 D-2011 8.20 mg/L 5 AW 7/30/2020
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] v .randalabs.com Page 1

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S&ME Inc. -Raleigh NC
Sample Delivery Group: L1245193
Samples Received: 07/31/2020
Project Number: 4305-19-001
Description: Plantation
Report To: Claudia Irvin / Michael Pfeifer
3201 Spring Forest Road
Raleigh, NC 27616
Entire Report Reviewed By:
� I
r
Tom Mellette
Project Manager
Results relate only to the Items tested or calibrated and are reported as founded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by pare
Analyilal National is performed per guidance provided In laboratory standard operating procedures ENV-SOP-MTJL 0067and
ENV-SOP-14TJL-0068. Where Sampling conducted by the customer, results relate to the accuracy of the Information provided,
and as the samples are received.
I 6 �•,:rn.,,.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
S&ME Inc. - Raleigh NC 4305-19-001 L124S193 OW03/2009:33 101`9

TABLE OF CONTENTS ONE LAB. NATIONWIDE. 1
Te: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
OUTFALL 002 L1245193-01 5
Qc: Quality Control Summary 6
Gravimetric Analysis by Method 2540 D-2011 6
GI: Glossary of Terms 7
Sc: Sample Chain of Custody 9
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
5&ME Inc. -Raleigh NC 4305-19-001 L1245193 08/03/2009.33 2of9

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SAMPLE SUMMARY ONE • •
OUTFALL 002 L1245193-01 WW
Method Batch
Gravlmetric Analysis by Method 2540 D-2011 WGI518467
Collected by
Collected datehime
Received date/time
Gary Simcox
07/3012013:30
07/31/2009:00
Dilution Preparation
Analysis
Analyst Location
date/time
datettime
1 07/3112015:26
07/3112016:30
TH Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATEITIME:
S&MElnc.-Raleigh NC 4305-19-001 L1245193 08/03/200933
PAGE:
3 of

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FT,
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
c
are within established criteria except where addressed in this case narrative, a non-conformance form
a
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
SSr
6
QC
Tom Mellette
Project Manager
-
9Sc
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
S&MElnc.-Raleigh NC 4305-19-001 L1245193 08103/2009.33 4of9

OUTFALL 002 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 07/30/20 13: 30 L1245193
Gravimetric Analysis by Method 2540 D-2011
Result
Analyte ug/I
Suspended Solids 7570
Qualifier RDL Dilution Analysis Batch
ug/I dateitime
J4 3580 1 07/31202016:30 WG1518467
Tc
3Ss
4Cn
6QC
7 GI
Al
9SC
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
S&ME Inc. -Raleigh NC 4305-19-001 L1245193 08/03/2009:33 50f9

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GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The Information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer -Information that maybe provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Feld Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy ofthis information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit
RDL
Reported Detection Limit
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Analyte
reported.
ffthe sample matrix contains an interfering material, the sample preparation volume or weightvalues differ from the
Dilution
standard, or if concentrations of analyses in the sample are higher than the highest limit of concentration thatthe
laboratory can accurately report, the sample may be diluted for analysis. If a value differentthan 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value thatthe laboratory has historically determined as normal
Limits
for the method and analyze being reported. Successful QC Sample analysis will target all analyses recovered or
duplicated within these ranges.
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)from a quality control
Original Sample
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is preserrL a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyze, the result in this column may state "ND" (Not Detected) or"BDL"
Result
(Below Detectable Levels). The information In the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest voluethat the laboratory could detect
or report for this analyze.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion aboutthe included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from thefeld or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis,
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J4
The associated batch QC was outside the established quality control range for accuracy.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT: SDG: DATErTME: PAGE:
S&ME Inc. -Raleigh NC 4305-19-001 L1245193 08/03120 09 33 7of9

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
s
Pace National is the only environmental laboratory accredited7certifed to support your work nationwide from one location. One phone call, one point of contact,
one laboratory. No other lab Is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective totals ofthe network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conductveto accelerated productivity, decreasing
lum-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR
LAB OF CHOICE.
' Not all certifications held bythe laboratory are applicable to the results reported in the attached report.
' Accreditation Is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
ETC]
`;late AccredltciLions
Alabama 40660
Nebraska
NEOS-15-05
SS
Alaska 17-026
Nevada
TWG3-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TN002
Cn
California 2932
New Mexico'
n/a
Colorado TN00003
New York
11742
s
Connecticut PH-0197
North Carolina
Env375
S r
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina
41
6
Georgia' 923
North Dakota
R-140
QC
Idaho TN00003
Ohlo—VAP
CL0069
Illinois 20000E
Oklahoma
9915
7G
Indiana C-TN-01
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhedelsland
LA000356
Kentucky" 90010
Southcarollna
84004
Kentucky z 16
South Dakota
We
Louisiana A130792
Tennessee"
2006
5
Louisiana' LA180010
Texas
T1047042454845
SC
Maine TN0002
Texas'
LAB0152
Maryland 324
Utah
TN00003
Massachusetts M-TN003
Vermont
Vr2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Vlrghma
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A21A
hhd PartV, Federal Accieditations
A2LA— ISO 17025 1461.01
AIHA-LAPJ-C EMLAP
100789
A2LA— ISO 17025s 1461.02
DOD
1461.01
Canada 146101
USDA
P330-15-00234
EPA—Crypto TN00003
'Drinking Water' Underground Storage Tanks 3 Aquatic Toxicity 4ChemicaYMlcroblological sMold
`Wastewater n/a Accreditation net applicable
C)LII" I OCFILIOIIS
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. Ifyou would like assistance from one of our supPort offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
S&ME Inc. -Raleigh NC 4305-19-001 L1245193 08/03/2009:33 8of9

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