NCG030145_DMR_20200406

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted /6/b2242 RECpj J 0 CERTIFICATE OF COVERAGENO. NCG030145 SAMPLE COLLECTION YEAR: 2020 APR 1 4 2020
FACILITY NAME: Newton Instruments SAMPLE PERIOD Jan-June❑July-Dec CENT
COUNTY: Granville or®Monthly1 March 2020 DWR RAL FILES
PERSON COLLECTING SAMPLES: Geoffrey Murphrev DISCHARGING TO CLASS❑ORW®HQW❑Trout❑PNA SECTIO, !
LABORATORY: : Pace Analytical Lab Cert.#: 40 ❑Zero-flow❑Water Supply❑SA
Comments on sample collection or analysis: Monthly sampling ❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 34
Part A:Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?2
Non-Polar
Outfall No. Date Sample 24-hour rainfall Total Suspended pH, O&G/Total Total Toxic
1 Standard Copper Lead Zinc
Collected amount, Solids units Petroleum Organics'
(mo/dd/yr) Inches Hydrocarbons
Benchmarks===> - - 100 mg/L 6.0—9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L
001 03/03/20 0.2 11.4 mg/L 8.0 0.0042 mg/L 0,0025 mg/L 0.0457 mg/L <4.8 mg/L Not Detected
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit,Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor
manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan mayso certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Permit Date:11/1/2017-10/31/2022 SWU-245,last revised 10/25/2012
Page 1 of 3

,
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name(Print name)
Title(Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND, or other similar non-numerical
format. When results are below the applicable limits, they must be reported in the format,"<XX mg/L",where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2,or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
n No discharge this period?2
Outfall No. Date Sample 24-hour rainfall
Collected) amount, Non-polar O&G/TPH by
(mo/dd/yr) Inches3 EPA 1664(SGT-HEM) Total Suspended Solids pH
Benchmarks===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0—9.0 SU
Footnotes from Part A also apply to this Part B
*See General Permit text,Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2,or Tier 3 responses. See General Permit text.
Permit Date:11/1/2017-10/31/2022 SWU-245,last revised 10/25/2012
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL?YES ® NO E
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE?YES ® NO❑
REGIONAL OFFICE CONTACT NAME: John Holley
Mail an original and one copy of this DMR, including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period
in the case of"No Discharge"reports)to:
Division of Water Quality
Attn:DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or
those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate, and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
J —43---
V/‘7. c."1..26,-)
(Signature of Peicittee) (Date)
Permit Date:11/1/2017-10/31/2022 5WU-245,last revised 10/25/2012
Page 3 of 3

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacalabs.com [phone]
March 17, 2020
Mr. Pete Dressel
Piedmont Geologic
6003 Chapel Hill Road
Suite 109
Raleigh, NC 27607
RE: Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Dear Mr. Dressel:
Enclosed are the analytical results for sample(s) received by the laboratory on March 04, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Jonathan Murphrey,Piedmont Geologic
4e#7„
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aceAnalytical Huntersville.NC 28078
www.pacelabs.com
[phone]
CERTIFICATIONS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Pace Analytical Services Charlotte
9800 Kincey Ave.Ste 100, Huntersville,NC 28078 South Carolina Certification#:99006001
Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#: E87627
North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84
North Carolina Field Services Certification#:5342 VirginiaNELAP Certification#:460221
North Carolina Wastewater Certification#:12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222
North Carolina Drinking Water Certification#:37712
Pace Analytical Services Eden
205 East Meadow Road Suite A,Eden,NC 27288 North Carolina Wastewater Certification#:633
North Carolina Drinking Water Certification#:37738 VirginiaNELAP Certification#:460025
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
aeAnalytical Huntersville,NC 28078
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[phone]
SAMPLE SUMMARY
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Lab ID Sample ID • Matrix Date Collected Date Received
92467868001 OUTFALL 001 Water 03/03/20 13:15 03/04/20 09:16
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalyticai 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.eom [phone]
SAMPLE ANALYTE COUNT
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92467868001 OUTFALL 001 SM 2540D-2011 AMI 1 PASI-E
EPA 1664E HH 1 PASI-C
EPA 608.3 SEM 31 PASI-C
EPA 200.7 Rev 4.4 1994 RDT 12 PASI-A
EPA 245.1 Rev 3.0 1994 SOO 1 PASI-A
EPA 625.1 PKS 62 PASI-C
EPA 624.1 SAS 31 PASI-C
EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A
SM 4500-CN-E-2011 CJH1 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aeAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Sample: OUTFALL 001 Lab ID: 92467868001 Collected: 03/03/20 13:15 Received: 03/04/20 09:16 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D-2011
Total Suspended Solids 11.4 mg/L 2.5 2.5 1 03/05/20 13:22
Field Data Analytical Method:
Collected By GM 1 03/03/20 13:15
Collected Date 03/03/20 1 03/03/20 13:15
Collected Time 13:15 1 03/03/20 13:15
pH 8.0 Std.Units 1 03/03/20 13:15
HEM,Oil and Grease Analytical Method:EPA 1664E
Oil and Grease ND mg/L 4.8 1.2 1 03/17/20 09:13
608 PCB Pest RVE Analytical Method:EPA 608.3 Preparation Method:EPA 608.3
Aldrin ND ug/L 0.050 0.022 1 03/10/20 12:53 03/11/20 16:02 309-00-2
alpha-BHC ND ug/L 0.050 0.019 1 03/10/20 12:53 03/11/20 16:02 319-84-6
beta-BHC ND ug/L 0.050 0.014 1 03/10/20 12:53 03/11/20 16:02 319-85-7
delta-BHC ND ug/L 0.050 0.020 1 03/10/20 12:53 03/11/20 16:02 319-86-8
gamma-BHC(Lindane) ND ug/L 0.050 0.012 1 03/10/20 12:53 03/11/20 16:02 58-89-9
Chlordane(Technical) ND ug/L 0.50 0.14 1 03/10/20 12:53 03/11/20 16:02 57-74-9
alpha-Chlordane ND ug/L 0.050 0.0090 1 03/10/20 12:53 03/11/20 16:02 5103-71-9
gamma-Chlordane ND ug/L 0.050 0.017 1 03/10/20 12:53 03/11/20 16:02 5103-74-2
4,4'-DDD ND ug/L 0.050 0.0069 1 03/10/20 12:53 03/11/20 16:02 72-54-8
4,4'-DDE ND ug/L 0.050 0.0064 1 03/10/20 12:53 03/11/20 16:02 72-55-9
4,4'-DDT ND ug/L 0.050 0.018 1 03/10/20 12:53 03/11/20 16:02 50-29-3
Dieldrin ND ug/L 0.050 0.0073 1 03/10/2012:53 03/11/20 16:02 60-57-1
Endosulfan I ND ug/L 0.050 0.0094 1 03/10/20 12:53 03/11/20 16:02 959-98-8
Endosulfan II ND ug/L 0.050 0.0065 1 03/10/20 12:53 03/11/20 16:02 33213-65-9
Endosulfan sulfate ND ug/L 0.050 0.0091 1 03/10/20 12:53 03/11/20 16:02 1031-07-8
Endrin ND ug/L 0.050 0.0089 1 03/10/20 12:53 03/11/20 16:02 72-20-8
Endrin aldehyde ND ug/L 0.050 0.013 1 03/10/20 12:53 03/11/20 16:02 7421-93-4
Endrin ketone ND ug/L 0.050 0.0062 1 03/10/20 12:53 03/11/20 16:02 53494-70-5
Heptachlor ND ug/L 0.050 0.016 1 03/10/20 12:53 03/11/20 16:02 76-44-8
Heptachlor epoxide ND ug/L 0.050 0.0097 1 03/10/20 12:53 03/11/20 16:02 1024-57-3
Methoxychlor ND ug/L 0.15 0.033 1 03/10/20 12:53 03/11/20 16:02 72-43-5
PCB-1016(Aroclor 1016) ND ug/L 0.50 0.22 1 03/10/20 12:53 03/11/20 16:02 12674-11-2
PCB-1221 (Arodor 1221) ND ug/L 0.50 0.32 1 03/10/20 12:53 03/11/20 16:02 11104-28-2
PCB-1232(Arodor 1232) ND ug/L 0.50 0.21 1 03/10/20 12:53 03/11/20 16:02 11141-16-5
PCB-1242(Aroclor 1242) ND ug/L 0.50 0.44 1 03/10/20 12:53 03/11/20 16:02 53469-21-9
PCB-1248(Arodor 1248) ND ug/L 0.50 0.34 1 03/10/20 12:53 03/11/20 16:02 12672-29-6
PCB-1254(Aroclor 1254) ND ug/L 0.50 0.24 1 03/10/20 12:53 03/11/20 16:02 11097-69-1
PCB-1260(Arodor 1260) ND ug/L 0.50 0.30 1 03/10/20 12:53 03/11/20 16:02 11096-82-5
Toxaphene ND ug/L 0.50 0.19 1 03/10/20 12:53 03/11/20 16:02 8001-35-2
Surrogates
Tetrachloro-m-xylene(S) 78 % 10-130 1 03/10/20 12:53 03/11/20 16:02 877-09-8
Decachlorobiphenyl(S) 84 % 10-130 1 03/10/20 12:53 03/11/20 16:02 2051-24-3
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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ANALYTICAL RESULTS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Sample: OUTFALL 001 Lab ID: 92467868001 Collected: 03/03/20 13:15 Received: 03/04/20 09:16 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Antimony ND ug/L 5.0 3.0 1 03/13/20 02:24 03/15/20 22:11 7440-36-0
Arsenic ND ug/L 10.0 4.7 1 03/13/20 02:24 03/15/20 22:11 7440-38-2
Beryllium ND ug/L 1.0 0.20 1 03/13/20 02:24 03/15/20 22:11 7440-41-7
Cadmium ND ug/L 1.0 0.40 1 03/13/20 02:24 03/15/20 22:11 7440-43-9
Chromium 1.1J ug/L 5.0 1.0 1 03/13/20 02:24 03/15/20 22:11 7440-47-3
Copper 4.2J ug/L 5.0 2.1 1 03/13/20 02:24 03/15/20 22:11 7440-50-8
Lead 2.5J ug/L 5.0 1.6 1 03/13/20 02:24 03/15/20 22:11 7439-92-1
Nickel 3.6J ug/L 5.0 0.90 1 03/13/20 02:24 03/15/20 22:11 7440-02-0
Selenium ND ug/L 10.0 4.7 1 03/13/20 02:24 03/15/20 22:11 7782-49-2
Silver ND ug/L 5.0 2.5 1 03/13/20 02:24 03/15/20 22:11 7440-22-4
Thallium ND ug/L 10.0 2.6 1 03/13/20 02:24 03/15/20 22:11 7440-28-0
Zinc 45.7 ug/L 10.0 3.9 1 03/13/20 02:24 03/15/20 22:11 7440-66-6
245.1 Mercury Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method:EPA 245.1 Rev 3.0 1994
Mercury ND ug/L 0.20 0.10 1 03/06/20 14:55 03/11/20 13:36 7439-97-6
625 RVE Analytical Method:EPA625.1 Preparation Method:EPA625.1
Acenaphthene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 83-32-9
Acenaphthylene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 208-96-8
Anthracene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 120-12-7
Benzidine ND ug/L 50.0 3.3 1 03/10/20 11:27 03/11/20 04:08 92-87-5
Benzo(a)anthracene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 56-55-3
Benzo(a)pyrene ND ug/L 5.0 1.8 1 03/10/20 11:27 03/11/20 04:08 50-32-8
Benzo(b)fluoranthene ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 191-24-2
Benzo(k)fluoranthene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.0 1.2 1 03/10/20 11:27 03/11/20 04:08 101-55-3
Butylbenzylphthalate ND ug/L 5.0 1.9 1 03/10/20 11:27 03/11/20 04:08 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.0 2.8 1 03/10/20 11:27 03/11/20 04:08 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 10.0 1.3 1 03/10/20 11:27 03/11/20 04:08 111-91-1
bis(2-Chloroethyl)ether ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 111-44-4
2-Chloronaphthalene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 91-58-7
2-Chlorophenol ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 7005-72-3
Chrysene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 218-01-9
Dibenz(a,h)anthracene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 53-70-3
1,2-Dichlorobenzene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 106-46-7
3,3'-Dichlorobenzidine ND ug/L 10.0 2.7 1 03/10/20 11:27 03/11/20 04:08 91-94-1
2,4-Dichlorophenol ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 120-83-2
Diethylphthalate ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 84-66-2
2,4-Dimethylphenol ND ug/L 10.0 1.5 1 03/10/20 11:27 03/11/20 04:08 105-67-9
Dimethylphthalate ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 131-11-3
Di-n-butylphthalate ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 10.0 4.5 1 03/10/20 11:27 03/11/20 04:08 534-52-1
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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aceAnalytical 9800 Kincey Ave. Suite 100
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_ Huntersville,NC 28078
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ANALYTICAL RESULTS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Sample: OUTFALL 001 Lab ID: 92467868001 Collected: 03/03/20 13:15 Received: 03/04/20 09:16 Matrix:Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method:EPA625.1 Preparation Method:EPA625.1
2,4-Dinitrophenol ND ug/L 50.0 7.3 1 03/10/20 11:27 03/11/20 04:08 51-28-5
2,4-Dinitrotoluene ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 121-14-2
2,6-Dinitrotoluene ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 606-20-2
Di-n-octylphthalate ND ug/L 5.0 2.2 1 03/10/20 11:27 03/11/20 04:08 117-84-0
1,2-Diphenylhydrazine ND ug/L 5.0 1.3 1 03/10/20 11:27 03/11/20 04:08 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/L 5.0 2.0 1 03/10/20 11:27 03/11/20 04:08 117-81-7
Fluoranthene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 206-44-0
Fluorene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 86-73-7
Hexachloro-1,3-butadiene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 87-68-3
Hexachlorobenzene ND ug/L 5.0 1.3 1 03/10/20 11:27 03/11/20 04:08 118-74-1
Hexachlorocyclopentadiene ND ug/L 10.0 2.4 1 03/10/20 11:27 03/11/20 04:08 77-47-4
Hexachloroethane ND ug/L 5.0 1.3 1 03/10/20 11:27 03/11/20 04:08 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 193-39-5
Isophorone ND ug/L 10.0 1.3 1 03/10/20 11:27 03/11/20 04:08 78-59-1
Naphthalene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 91-20-3
Nitrobenzene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 98-95-3
2-Nitrophenol ND ug/L 5.0 1.7 1 03/10/20 11:27 03/11/20 04:08 88-75-5
4-Nitrophenol ND ug/L 10.0 9.4 1 03/10/20 11:27 03/11/20 04:08 100-02-7
N-Nitrosodimethylamine ND ug/L 5.0 1.8 1 03/10/20 11:27 03/11/20 04:08 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 5.0 1.3 1 03/10/20 11:27 03/11/20 04:08 621-64-7
N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 03/10/20 11:27 03/11/20 04:08 86-30-6
Pentachlorophenol ND ug/L 10.0 2.8 1 03/10/20 11:27 03/11/20 04:08 87-86-5
Phenanthrene ND ug/L 5.0 1.4 1 03/10/20 11:27 03/11/20 04:08 85-01-8
Phenol ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 108-95-2
Pyrene ND ug/L 5.0 1.5 1 03/10/20 11:27 03/11/20 04:08 129-00-0
1,2,4-Trichlorobenzene ND ug/L 5.0 1.6 1 03/10/20 11:27 03/11/20 04:08 120-82-1
2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 03/10/20 11:27 03/11/20 04:08 88-06-2
Surrogates
Nitrobenzene-d5(S) 93 % 10-120 1 03/10/20 11:27 03/11/20 04:08 4165-60-0
2-Fluorobiphenyl(S) 79 % 15-120 1 03/10/20 11:27 03/11/20 04:08 321-60-8
Terphenyl-d14(S) 91 % 11-131 1 03/10/20 11:27 03/11/20 04:08 1718-51-0
Phenol-d6(S) 44 % 10-120 1 03/10/20 11:27 03/11/20 04:08 13127-88-3
2-Fluorophenol(S) 32 % 10-120 1 03/10/20 11:27 03/11/20 04:08 367-12-4
2,4,6-Tribromophenol(S) 21 % 10-137 1 03/10/20 11:27 03/11/20 04:08 118-79-6
624 Volatile Organics Acrolein Analytical Method: EPA 624.1
Acrolein ND ug/L 5.0 3.8 1 03/06/20 15:33 107-02-8 M1
Acrylonitrile ND ug/L 5.0 1.5 1 03/06/20 15:33 107-13-1
Benzene ND ug/L 1.0 0.38 1 03/06/20 15:33 71-43-2
Bromodichloromethane ND ug/L 2.0 0.24 1 03/06/20 15:33 75-27-4
Bromoform ND ug/L 2.0 0.40 1 03/06/20 15:33 75-25-2
Bromomethane ND ug/L 2.0 1.2 1 03/06/20 15:33 74-83-9
Carbon tetrachloride ND ug/L 2.0 0.29 1 03/06/20 15:33 56-23-5
Chlorobenzene ND ug/L 2.0 0.37 1 03/06/20 15:33 108-90-7
Chloroethane ND ug/L 2.0 1.4 1 03/06/20 15:33 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 0.73 1 03/06/20 15:33 110-75-8
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aeAnalyt
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ical Huntersville,NC 28078
i www.pacelabs.com
[phone]
I
ANALYTICAL RESULTS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Sample: OUTFALL 001 Lab ID: 92467868001 Collected: 03/03/20 13:15 Received: 03/04/20 09:16 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Acrolein Analytical Method:EPA 624.1
Chloroform ND ug/L 2.0 0.58 1 03/06/20 15:33 67-66-3
Chloromethane ND ug/L 2.0 0.73 1 03/06/20 15:33 74-87-3
Dibromochloromethane ND ug/L 2.0 0.32 1 03/06/20 15:33 124-48-1
1,1-Dichloroethane ND ug/L 2.0 0.51 1 03/06/20 15:33 75-34-3
1,2-Dichloroethane ND ug/L 2.0 0.34 1 03/06/20 15:33 107-06-2
trans-1,2-Dichloroethene ND ug/L 2.0 0.42 1 03/06/20 15:33 156-60-5
1,2-Dichloropropane ND ug/L 2.0 0.27 1 03/06/20 15:33 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 0.33 1 03/06/20 15:33 10061-01-5
trans-1,3-Dichloropropene ND ug/L 2.0 0.41 1 03/06/20 15:33 10061-02-6
Ethylbenzene ND ug/L 1.0 0.28 1 03/06/20 15:33 100-41-4
Methylene Chloride ND ug/L 2.0 0.24 1 03/06/20 15:33 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.34 1 03/06/20 15:33 79-34-5
Tetrachloroethene ND ug/L 2.0 0.28 1 03/06/20 15:33 127-18-4
Toluene ND ug/L 1.0 0.44 1 03/06/20 15:33 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 0.35 1 03/06/20 15:33 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 0.31 1 03/06/20 15:33 79-00-5
Trichloroethene ND ug/L 2.0 0.36 1 03/06/20 15:33 79-01-6
Vinyl chloride ND ug/L 2.0 0.72 1 03/06/20 15:33 75-01-4
Surrogates
4-Bromofluorobenzene(S) 100 % 70-130 1 03/06/20 15:33 460-00-4
Toluene-d8(S) 99 % 70-130 1 03/06/20 15:33 2037-26-5
1,2-Dichloroethane-d4(S) 102 % 70-130 1 03/06/20 15:33 17060-07-0
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method:EPA 420.4 Rev 1.0 1993
Phenol ND mg/L 0.020 0.0050 1 03/10/20 09:35 03/10/20 13:58 108-95-2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E-2011 Preparation Method:SM 4500-CN-E-2011
Cyanide ND mg/L 0.0080 0.0060 1 03/11/20 14:00 03/11/20 19:07 57-12-5
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalyticalx
9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 528761 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92467868001
METHOD BLANK: 2824182 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 03/05/20 13:17
LABORATORY CONTROL SAMPLE: 2824183
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 248 99 90-110
SAMPLE DUPLICATE: 2824184
92467901001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 28.8 27.8 4 25
SAMPLE DUPLICATE: 2824185
92467865001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 34.8 35.8 3 25
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
x
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 530850 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92467868001
METHOD BLANK: 2834448 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 1.3 03/17/20 09:01
LABORATORY CONTROL SAMPLE: 2834449
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 33.6 84 78-114
MATRIX SPIKE SAMPLE: 2834450
35536353002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 1.2U 38.5 7.3 19 78-114 M1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
s 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529003 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Associated Lab Samples: 92467868001
METHOD BLANK: 2825220 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury ug/L ND 0.20 0.10 03/11/20 12:58
LABORATORY CONTROL SAMPLE: 2825221
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 2.5 2.5 100 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2825222 2825223
MS MSD
92467528027 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.6 2.4 102 97 70-130 5 20
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2825224 2825225
MS MSD
92467868001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.5 100 100 70-130 0 20
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite Huntersville,NC 2607878
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 530258 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92467868001
METHOD BLANK: 2831905 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony ug/L ND 5.0 3.0 03/15/20 21:04
Arsenic ug/L ND 10.0 4.7 03/15/20 21:04
Beryllium ug/L ND 1.0 0.20 03/15/20 21:04
Cadmium ug/L ND 1.0 0.40 03/15/20 21:04
Chromium ug/L ND 5.0 1.0 03/15/20 21:04
Copper ug/L ND 5.0 2.1 03/15/20 21:04
Lead ug/L ND 5.0 1.6 03/15/20 21:04
Nickel ug/L ND 5.0 0.90 03/15/20 21:04
Selenium ug/L ND 10.0 4.7 03/15/20 21:04
Silver ug/L ND 5.0 2.5 03/15/20 21:04
Thallium ug/L ND 10.0 2.6 03/15/20 21:04
Zinc ug/L ND 10.0 3.9 03/15/20 21:04
LABORATORY CONTROL SAMPLE: 2831906
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Antimony ug/L 500 502 100 85-115
Arsenic ug/L 500 473 95 85-115
Beryllium ug/L 500 492 98 85-115
Cadmium ug/L 500 488 98 85-115
Chromium ug/L 500 483 97 85-115
Copper ug/L 500 491 98 85-115
Lead ug/L 500 502 100 85-115
Nickel ug/L 500 492 98 85-115
Selenium ug/L 500 494 99 85-115
Silver ug/L 250 232 93 85-115
Thallium ug/L 500 477 95 85-115
Zinc ug/L 500 505 101 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE 2831907 2831908
MS MSD
92467745001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 525 532 104 106 70-130 1 20
Arsenic ug/L ND 500 500 496 500 99 100 70-130 1 20
Beryllium ug/L ND 500 500 506 511 101 102 70-130 1 20
Cadmium ug/L ND 500 500 507 515 101 103 70-130 2 20
Chromium ug/L ND 500 500 504 508 100 101 70-130 1 20
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical g 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.ctml [phone]
I
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2831907 2831908
MS MSD
92467745001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Copper ug/L 0.014 500 500 509 512 99 100 70-130 0 20
mg/L
Lead ug/L ND 500 500 507 514 101 102 70-130 1 20
Nickel ug/L 0.0073 500 500 502 508 99 100 70-130 1 20
mg/L
Selenium ug/L ND 500 500 531 536 106 107 70-130 1 20
Silver ug/L ND 250 250 240 240 96 96 70-130 0 20
Thallium ug/L ND 500 500 445 454 89 90 70-130 2 20
Zinc ug/L 0.19 mg/L 500 500 724 733 107 109 70-130 1 20
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2831909 2831910
MS MSD
92467867003 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 532 531 106 106 70-130 0 20
Arsenic ug/L ND 500 500 497 498 99 100 70-130 0 20
Beryllium ug/L ND 500 500 511 518 102 103 70-130 1 20
Cadmium ug/L ND 500 500 519 523 104 105 70-130 1 20
Chromium ug/L 12.3 500 500 508 517 99 101 70-130 2 20
Copper ug/L 16.2 500 500 524 523 102 101 70-130 0 20
Lead ug/L ND 500 500 518 524 103 104 70-130 1 20
Nickel ug/L 23.8 500 500 530 535 101 102 70-130 1 20
Selenium ug/L ND 500 500 545 549 109 110 70-130 1 20
Silver ug/L ND 250 250 240 243 96 97 70-130 1 20
Thallium ug/L ND 500 500 476 481 95 96 70-130 1 20
Zinc ug/L 334 500 500 843 866 102 106 70-130 3 20
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
71aceAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529029 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV with Acrolein
Associated Lab Samples: 92467868001
METHOD BLANK: 2825384 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1-Trichloroethane ug/L ND 2.0 0.35 03/06/20 14:24
1,1,2,2-Tetrach loroetha ne ug/L ND 2.0 0.34 03/06/20 14:24
1,1,2-Trichloroethane ug/L ND 2.0 0.31 03/06/20 14:24
1,1-Dichloroethane ug/L ND 2.0 0.51 03/06/20 14:24
1,2-Dichloroethane ug/L ND 2.0 0.34 03/06/20 14:24
1,2-Dichloropropane ug/L ND 2.0 0.27 03/06/20 14:24
2-Chloroethylvinyl ether ug/L ND 5.0 0.73 03/06/20 14:24
Acrolein ug/L ND 5.0 3.8 03/06/20 14:24
Acrylonitrile ug/L ND 5.0 1.5 03/06/20 14:24
Benzene ug/L ND 1.0 0.38 03/06/20 14:24
Bromodichloromethane ug/L ND 2.0 0.24 03/06/20 14:24
Bromoform ug/L ND 2.0 0.40 03/06/20 14:24
Bromomethane ug/L ND 2.0 1.2 03/06/20 14:24
Carbon tetrachloride ug/L ND 2.0 0.29 03/06/20 14:24
Chlorobenzene ug/L ND 2.0 0.37 03/06/20 14:24
Chloroethane ug/L ND 2.0 1.4 03/06/20 14:24
Chloroform ug/L ND 2.0 0.58 03/06/20 14:24
Chloromethane ug/L ND 2.0 0.73 03/06/20 14:24
cis-1,3-Dichloropropene ug/L ND 2.0 0.33 03/06/20 14:24
Dibromochloromethane ug/L ND 2.0 0.32 03/06/20 14:24
Ethylbenzene ug/L ND 1.0 0.28 03/06/20 14:24
Methylene Chloride ug/L ND 2.0 0.24 03/06/20 14:24
Tetrachloroethene ug/L ND 2.0 0.28 03/06/20 14:24
Toluene ug/L ND 1.0 0.44 03/06/20 14:24
trans-1,2-Dichloroethene ug/L ND 2.0 0.42 03/06/20 14:24
trans-1,3-Dichloropropene ug/L ND 2.0 0.41 03/06/20 14:24
Trichloroethene ug/L ND 2.0 0.36 03/06/20 14:24
Vinyl chloride ug/L ND 2.0 0.72 03/06/20 14:24
1,2-Dichloroethane-d4(S) % 104 70-130 03/06/20 14:24
4-Bromofluorobenzene(S) % 102 70-130 03/06/20 14:24
Toluene-d8(S) % 100 70-130 03/06/20 14:24
LABORATORY CONTROL SAMPLE: 2825385
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 19.9 99 70-130
1,1,2,2-Tetrachloroethane ug/L 20 21.2 106 60-140
1,1,2-Trichloroethane ug/L 20 20.9 104 70-130
1,1-Dichloroethane ug/L 20 19.8 99 70-130
1,2-Dichloroethane ug/L 20 20.0 100 49-155
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
A
7119 eAnalytical 9800 Kincey Ave. Suite100 Huntersville,NC 28078078
www.pacelabs.com
[phone]
I
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
LABORATORY CONTROL SAMPLE: 2825385
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,2-Dichloropropane ug/L 20 20.3 102 35-165
2-Chloroethylvinyl ether ug/L 40 40.2 101 1-225
Acrolein ug/L 100 100 100 60-140
Acrylonitrile ug/L 100 90.4 90 60-140
Benzene ug/L 20 20.5 103 65-135
Bromodichloromethane ug/L 20 21.8 109 65-135
Bromoform ug/L 20 21.1 106 70-130
Bromomethane ug/L 20 29.2 146 15-185
Carbon tetrachloride ug/L 20 20.8 104 70-130
Chlorobenzene ug/L 20 21.5 107 65-135
Chloroethane ug/L 20 18.8 94 40-160
Chloroform ug/L 20 20.3 101 70-135
Chloromethane ug/L 20 16.4 82 1-205
cis-1,3-Dichloropropene ug/L 20 20.5 103 25-175
Dibromochloromethane ug/L 20 21.0 105 70-135
Ethylbenzene ug/L 20 20.4 102 60-140
Methylene Chloride ug/L 20 19.3 97 60-140
Tetrachloroethene ug/L 20 20.8 104 70-130
Toluene ug/L 20 20.4 102 70-130
trans-1,2-Dichloroethene ug/L 20 21.0 105 70-130
trans-1,3-Dichloropropene ug/L 20 21.6 108 50-150
Trichloroethene ug/L 20 21.0 105 65-135
Vinyl chloride ug/L 20 19.5 97 5-195
1,2-Dichloroethane-d4(S) % 97 70-130
4-Bromofluorobenzene(S) % 101 70-130
Toluene-d8(S) % 99 70-130
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2825386 2825387
MS MSD
92467868001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
1,1,1-Trichloroethane ug/L ND 20 20 22.1 23.1 111 115 52-162 4 36
1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.2 23.4 106 117 46-157 10 61
1,1,2-Trichloroethane ug/L ND 20 20 21.5 23.5 107 117 52-150 9 45
1,1-Dichloroethane ug/L ND 20 20 22.9 24.0 114 120 59-155 5 40
1,2-Dichloroethane ug/L ND 20 20 20.5 22.3 102 111 49-155 8 49
1,2-Dichloropropane ug/L ND 20 20 22.9 24.4 115 122 1-210 6 55
2-Chloroethylvinyl ether ug/L ND 40 40 42.0 43.5 105 109 1-305 3 71
Acrolein ug/L ND 100 100 35.8 37.8 36 38 40-160 5 60 M1
Acrylonitrile ug/L ND 100 100 97.4 112 97 112 40-160 14 60
Benzene ug/L ND 20 20 24.0 24.4 120 122 37-151 2 61
Bromodichloromethane ug/L ND 20 20 23.2 26.2 116 131 35-155 12 56
Bromoform ug/L ND 20 20 19.8 23.0 99 115 45-169 15 42
Bromomethane ug/L ND 20 20 30.1 30.4 150 152 1-242 1 61
Carbon tetrachloride ug/L ND 20 20 23.9 25.5 119 127 70-140 6 41
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
_ Huntersville,NC 28078078
www.pacelabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2825386 2825387
MS MSD
92467868001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Chlorobenzene ug/L ND 20 20 22.7 22.8 114 114 37-160 0 53
Chloroethane ug/L ND 20 20 21.8 21.9 109 109 14-230 0 78
Chloroform ug/L ND 20 20 22.0 24.3 110 121 51-138 10 54
Chloromethane ug/L ND 20 20 20.3 21.0 101 105 1-273 4 60
cis-1,3-Dichloropropene ug/L ND 20 20 23.0 24.6 115 123 1-227 7 58
Dibromochloromethane ug/L ND 20 20 20.9 22.0 105 110 53-149 5 50
Ethylbenzene ug/L ND 20 20 22.3 22.6 112 113 37-162 1 63
Methylene Chloride ug/L ND 20 20 22.9 22.9 114 115 1-221 0 28
Tetrachloroethene ug/L ND 20 20 22.9 22.9 114 114 64-148 0 39
Toluene ug/L ND 20 20 21.9 23.5 109 118 47-150 7 41
trans-1,2-Dichloroethene ug/L ND 20 20 22.8 25.4 114 127 54-156 10 45
trans-1,3-Dichloropropene ug/L ND 20 20 21.7 24.1 108 120 17-183 11 86
Trichloroethene ug/L ND 20 20 22.5 23.4 113 117 70-157 4 48
Vinyl chloride ug/L ND 20 20 25.6 26.5 128 133 1-251 4 66
1,2-Dichloroethane-d4(S) % 94 100 70-130
4-Bromofluorobenzene(S) % 100 99 70-130
Toluene-d8(S) % 100 103 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
s
7aceAnalytical 9800 Kincey Ave. Suite100
Huntersville,NC 28078078
www.pacslabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529440 Analysis Method: EPA 608.3
QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Associated Lab Samples: 92467868001
METHOD BLANK: 2827709 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
4,4'-DDD ug/L ND 0.050 0.0069 03/11/20 17:44
4,4'-DDE ug/L ND 0.050 0.0064 03/11/20 17:44
4,4'-DDT ug/L ND 0.050 0.018 03/11/20 17:44
Aldrin ug/L ND 0.050 0.022 03/11/20 17:44
alpha-BHC ug/L ND 0.050 0.019 03/11/20 17:44
alpha-Chlordane ug/L ND 0.050 0.0090 03/11/20 17:44
beta-BHC ug/L ND 0.050 0.014 03/11/20 17:44
Chlordane(Technical) ug/L ND 0.50 0.14 03/11/20 17:44
delta-BHC ug/L ND 0.050 0.020 03/11/20 17:44
Dieldrin ug/L ND 0.050 0.0073 03/11/20 17:44
Endosulfan I ug/L ND 0.050 0.0094 03/11/20 17:44
Endosulfan II ug/L ND 0.050 0.0065 03/11/20 17:44
Endosulfan sulfate ug/L ND 0.050 0.0091 03/11/20 17:44
Endrin ug/L ND 0.050 0.0089 03/11/20 17:44
Endrin aldehyde ug/L ND 0.050 0.013 03/11/20 17:44
Endrin ketone ug/L ND 0.050 0.0062 03/11/20 17:44
gamma-BHC(Lindane) ug/L ND 0.050 0.012 03/11/20 17:44
gamma-Chlordane ug/L ND 0.050 0.017 03/11/20 17:44
Heptachlor ug/L ND 0.050 0.016 03/11/20 17:44
Heptachlor epoxide ug/L ND 0.050 0.0097 03/11/20 17:44
Methoxychlor ug/L ND 0.15 0.033 03/11/20 17:44
PCB-1016(Arodor 1016) ug/L ND 0.50 0.22 03/11/20 17:44
PCB-1221 (Arodor 1221) ug/L ND 0.50 0.32 03/11/20 17:44
PCB-1232(Arodor 1232) ug/L ND 0.50 0.21 03/11/20 17:44
PCB-1242(Arodor 1242) ug/L ND 0.50 0.44 03/11/20 17:44
PCB-1248(Arodor 1248) ug/L ND 0.50 0.34 03/11/20 17:44
PCB-1254(Arodor 1254) ug/L ND 0.50 0.24 03/11/20 17:44
PCB-1260(Arodor 1260) ug/L ND 0.50 0.30 03/11/20 17:44
Toxaphene ug/L ND 0.50 0.19 03/11/20 17:44
Decachlorobiphenyl(S) % 109 10-130 03/11/20 17:44
Tetrachloro-m-xylene(S) % 67 10-130 03/11/20 17:44
LABORATORY CONTROL SAMPLE: 2827710
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4,4'-DDD ug/L 0.25 0.30 120 31-141
4,4'-DDE ug/L 0.25 0.27 107 30-145
4,4'-DDT ug/L 0.25 0.29 117 25-160
Aldrin ug/L 0.25 0.19 77 42-140
alpha-BHC ug/L 0.25 0.24 96 37-140
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 30

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
/f9 e Analytical Huntersville,NC 28078
www.pacelabs.can
[phone]
I
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No: 92467868
LABORATORY CONTROL SAMPLE: 2827710
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
alpha-Chlordane ug/L 0.25 0.25 100 45-140
beta-BHC ug/L 0.25 0.32 128 17-147
delta-BHC ug/L 0.25 0.27 108 19-140
Dieldrin ug/L 0.25 0.27 110 36-146
Endosulfan I ug/L 0.25 0.27 106 45-153
Endosulfan II ug/L 0.25 0.27 107 1-202
Endosulfan sulfate ug/L 0.25 0.28 113 26-144
Endrin ug/L 0.25 0.29 117 30-147
Endrin aldehyde ug/L 0.25 0.25 100 50-148
Endrin ketone ug/L 0.25 0.31 125 70-130
gamma-BHC(Lindane) ug/L 0.25 0.25 100 32-140
gamma-Chlordane ug/L 0.25 0.21 84 45-140
Heptachlor ug/L 0.25 0.21 85 34-140
Heptachlor epoxide ug/L 0.25 0.26 106 37-142
Methoxychlor ug/L 0.75 0.81 109 46-130
Decachlorobiphenyl(S) % 88 10-130
Tetrachloro-m-xylene(S) % 78 10-130
LABORATORY CONTROL SAMPLE: 2827739
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
PCB-1016(Arodor 1016) ug/L 5 4.9 98 50-140
PCB-1260(Arodor 1260) ug/L 5 4.6 91 8-140
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827711 2827712
MS MSD
2629706001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
4,4'-DDD ug/L <0.050 0.25 0.25 0.86 0.81 344 326 31-141 5 39 M1
4,4'-DDE ug/L <0.050 0.25 0.25 0.33 0.31 132 124 30-145 7 35
4,4'-DDT ug/L <0.050 0.25 0.25 17.3 17.3 6930 6910 25-160 0 42 M1
Aldrin ug/L <0.050 0.25 0.25 0.18 0.19 73 75 42-140 3 35
alpha-BHC ug/L <0.050 0.25 0.25 0.18 0.19 72 77 37-140 6 36
alpha-Chlordane ug/L <0.050 0.25 0.25 0.42 0.40 170 160 45-140 6 35 M1
beta-BHC ug/L <0.050 0.25 0.25 0.36 0.38 142 153 17-147 7 44 M1
delta-BHC ug/L <0.050 0.25 0.25 0.18 0.21 72 84 19-140 14 52
Dieldrin ug/L <0.050 0.25 0.25 0.66 0.60 263 242 36-146 8 49 M1
Endosulfan I ug/L <0.050 0.25 0.25 0.31 0.29 124 117 45-153 6 28
Endosulfan II ug/L <0.050 0.25 0.25 1.1 1.0 443 416 1-202 6 53 M1
Endosulfan sulfate ug/L <0.050 0.25 0.25 1.0 1.0 417 399 26-144 4 38 M1
Endrin ug/L <0.050 0.25 0.25 6.1 6.2 2440 2480 30-147 1 48 M1
Endrin aldehyde ug/L <0.050 0.25 0.25 1.1 1.0 440 417 50-150 5 30 M1
Endrin ketone ug/L <0.050 0.25 0.25 4.1 3.6 1640 1420 20-150 14 30 M1
gamma-BHC(Lindane) ug/L <0.050 0.25 0.25 0.20 0.21 81 82 32-140 1 39
Results presented on this page are in the units indicated by the"units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 30

Pace Analytical Services,LLC
s
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827711 2827712
MS MSD
2629706001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
gamma-Chlordane ug/L <0.050 0.25 0.25 0.66 0.54 265 217 45-140 20 35 M1
Heptachlor ug/L <0.050 0.25 0.25 0.28 0.33 112 130 34-140 15 43
Heptachlor epoxide ug/L <0.050 0.25 0.25 0.94 0.97 377 388 37-142 3 26 M1
Methoxychlor ug/L <0.15 0.75 0.75 3.6 3.1 478 419 10-130 13 30 M1
Decachlorobiphenyl(S) % 203 127 10-130 SO
Tetrachloro-m-xylene(S) % 74 87 10-130
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827740 2827741
MS MSD
2629706001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
PCB-1016(Arodor 1016) ug/L <0.50 5 5 3.1 2.7 62 54 50-140 14 36
PCB-1260(Arodor 1260) ug/L <0.50 5 5 2.5 2.0 50 41 8-140 21 38
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 30

Pace Analytical Services,LLC
aceAnalytical 9800 Kinceyt Ave. Suite 100
liG 11 Huntersville,NC 28078
www.pacelabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529438 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92467868001
METHOD BLANK: 2827701 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/L ND 5.0 1.6 03/11/2000:25
1,2-Dichlorobenzene ug/L ND 5.0 1.4 03/11/20 00:25
1,2-Diphenylhydrazine ug/L ND 5.0 1.3 03/11/20 00:25
1,3-Dichlorobenzene ug/L ND 5.0 1.4 03/11/20 00:25
1,4-Dichlorobenzene ug/L ND 5.0 1.5 03/11/20 00:25
2,4,6-Trichlorophenol ug/L ND 10.0 1.4 03/11/20 00:25
2,4-Dichlorophenol ug/L ND 5.0 1.5 03/11/20 00:25
2,4-Dimethylphenol ug/L ND 10.0 1.5 03/11/20 00:25
2,4-Dinitrophenol ug/L ND 50.0 7.3 03/11/20 00:25
2,4-Dinitrotoluene ug/L ND 5.0 1.7 03/11/20 00:25
2,6-Dinitrotoluene ug/L ND 5.0 1.7 03/11/20 00:25
2-Chloronaphthalene ug/L ND 5.0 1.4 03/11/20 00:25
2-Chlorophenol ug/L ND 5.0 1.4 03/11/20 00:25
2-Nitrophenol ug/L ND 5.0 1.7 03/11/2000:25
3,3'-Dichlorobenzidine ug/L ND 10.0 2.7 03/11/20 00:25
4,6-Dinitro-2-methylphenol ug/L ND 10.0 4.5 03/11/20 00:25
4-Bromophenylphenyl ether ug/L ND 5.0 1.2 03/11/20 00:25
4-Chloro-3-methylphenol ug/L ND 5.0 2.8 03/11/20 00:25
4-Chlorophenylphenyl ether ug/L ND 5.0 1.5 03/11/20 00:25
4-Nitrophenol ug/L ND 10.0 9.4 03/11/20 00:25
Acenaphthene ug/L ND 5.0 1.4 03/11/20 00:25
Acenaphthylene ug/L ND 5.0 1.5 03/11/20 00:25
Anthracene ug/L ND 5.0 1.6 03/11/20 00:25
Benzidine ug/L ND 50.0 3.3 03/11/20 00:25
Benzo(a)anthracene ug/L ND 5.0 1.5 03/11/20 00:25
Benzo(a)pyrene ug/L ND 5.0 1.8 03/11/20 00:25
Benzo(b)fluoranthene ug/L ND 5.0 1.7 03/11/20 00:25
Benzo(g,h,i)perylene ug/L ND 5.0 1.6 03/11/20 00:25
Benzo(k)fluoranthene ug/L ND 5.0 1.5 03/11/20 00:25
bis(2-Chloroethoxy)methane ug/L ND 10.0 1.3 03/11/20 00:25
bis(2-Chloroethyl)ether ug/L ND 5.0 1.7 03/11/20 00:25
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 2.0 03/11/20 00:25
Butylbenzylphthalate ug/L ND 5.0 1.9 03/11/20 00:25
Chrysene ug/L ND 5.0 1.4 03/11/20 00:25
Di-n-butylphthalate ug/L ND 5.0 1.6 03/11/20 00:25
Di-n-octylphthalate ug/L ND 5.0 2.2 03/11/20 00:25
Dibenz(a,h)anthracene ug/L ND 5.0 1.6 03/11/20 00:25
Diethylphthalate ug/L ND 5.0 1.6 03/11/20 00:25
Dimethylphthalate ug/L ND 5.0 1.4 03/11/20 00:25
Fluoranthene ug/L ND 5.0 1.6 03/11/20 00:25
Fluorene ug/L ND 5.0 1.4 03/11/20 00:25
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 20 of 30

Pace Analytical Services,LLC
'S
ac Anal tical 9800 Kincey Ave. Suite 0100
78
I�GH IY�!� Huntersville,NC 28078
www.pacslabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
METHOD BLANK: 2827701 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Hexachloro-1,3-butadiene ug/L ND 5.0 1.6 03/11/20 00:25
Hexachlorobenzene ug/L ND 5.0 1.3 03/11/20 00:25
Hexachlorocyclopentadiene ug/L ND 10.0 2.4 03/11/20 00:25
Hexachloroethane ug/L ND 5.0 1.3 03/11/20 00:25
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 1.7 03/11/20 00:25
Isophorone ug/L ND 10.0 1.3 03/11/20 00:25
N-Nitroso-di-n-propylamine ug/L ND 5.0 1.3 03/11/20 00:25
N-Nitrosodimethylamine ug/L ND 5.0 1.8 03/11/20 00:25
N-Nitrosodiphenylamine ug/L ND 10.0 1.4 03/11/20 00:25
Naphthalene ug/L ND 5.0 1.6 03/11/20 00:25
Nitrobenzene ug/L ND 5.0 1.5 03/11/20 00:25
Pentachlorophenol ug/L ND 10.0 2.8 03/11/20 00:25
Phenanthrene ug/L ND 5.0 1.4 03/11/20 00:25
Phenol ug/L ND 5.0 1.5 03/11/20 00:25
Pyrene ug/L ND 5.0 1.5 03/11/20 00:25
2,4,6-Tribromophenol(S) % 60 10-137 03/11/20 00:25
2-Fluorobiphenyl(S) % 62 15-120 03/11/20 00:25
2-Fluorophenol(S) % 43 10-120 03/11/20 00:25
Nitrobenzene-d5(S) % 66 10-120 03/11/20 00:25
Phenol-d6(S) % 42 10-120 03/11/20 00:25
Terphenyl-d14(S) % 76 11-131 03/11/20 00:25
LABORATORY CONTROL SAMPLE: 2827702
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,2,4-Trichlorobenzene ug/L 50 27.5 55 44-142
1,2-Dichlorobenzene ug/L 50 30.1 60 32-129
1,2-Diphenylhydrazine ug/L 50 34.6 69 25-150
1,3-Dichlorobenzene ug/L 50 29.7 59 1-172
1,4-Dichlorobenzene ug/L 50 31.3 63 20-124
2,4,6-Trichlorophenol ug/L 50 30.6 61 37-144
2,4-Dichlorophenol ug/L 50 30.8 62 1-191
2,4-Dimethylphenol ug/L 50 28.7 57 32-119
2,4-Dinitrophenol ug/L 250 207 83 1-181
2,4-Dinitrotoluene ug/L 50 39.0 78 39-139
2,6-Dinitrotoluene ug/L 50 35.4 71 50-158
2-Chloronaphthalene ug/L 50 30.0 60 60-118
2-Chlorophenol ug/L 50 32.8 66 23-134
2-Nitrophenol ug/L 50 34.2 68 29-182
3,3'-Dichlorobenzidine ug/L 100 72.2 72 1-262
4,6-Dinitro-2-methylphenol ug/L 100 88.0 88 1-181
4-Bromophenylphenyl ether ug/L 50 32.1 64 53-127
4-Chloro-3-methylphenol ug/L 100 65.8 66 22-147
4-Chlorophenylphenyl ether ug/L 50 28.9 58 25-158
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 30

Pace Analytical Services,LLC
aceAnalytical x 9800 Kinsey Ave. Suite 100
Huntersville,NC 28078
www.paeNsbs.eom [phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
LABORATORY CONTROL SAMPLE: 2827702
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
4-Nitrophenol ug/L 250 140 56 1-132
Acenaphthene ug/L 50 31.1 62 47-145
Acenaphthylene ug/L 50 31.9 64 33-145
Anthracene ug/L 50 36.5 73 1-166
Benzidine ug/L 100 30.9J 31 10-130
Benzo(a)anthracene ug/L 50 40.3 81 33-143
Benzo(a)pyrene ug/L 50 41.1 82 17-163
Benzo(b)fluoranthene ug/L 50 41.5 83 24-159
Benzo(g,h,i)perylene ug/L 50 36.3 73 1-219
Benzo(k)fluoranthene ug/L 50 43.6 87 11-162
bis(2-Chloroethoxy)methane ug/L 50 29.7 59 33-184
bis(2-Chloroethyl)ether ug/L 50 31.3 63 12-158
bis(2-Ethylhexyl)phthalate ug/L 50 51.8 104 8-158
Butylbenzylphthalate ug/L 50 51.3 103 1-152
Chrysene ug/L 50 40.0 80 17-168
Di-n-butylphthalate ug/L 50 44.7 89 1-118
Di-n-octylphthalate ug/L 50 52.5 105 4-146
Dibenz(a,h)anthracene ug/L 50 37.2 74 1-227
Diethylphthalate ug/L 50 37.5 75 1-114
Dimethylphthalate ug/L 50 33.7 67 1-112
Fluoranthene ug/L 50 38.0 76 26-137
Fluorene ug/L 50 31.1 62 59-121
Hexachloro-1,3-butadiene ug/L 50 26.4 53 24-116
Hexachlorobenzene ug/L 50 33.4 67 1-152
Hexachlorocydopentadiene ug/L 50 26.5 53 25-150
Hexachloroethane ug/L 50 30.7 61 40-113
Indeno(1,2,3-cd)pyrene ug/L 50 37.5 75 1-171
Isophorone ug/L 50 31.2 62 21-196
N-Nitroso-di-n-propylamine ug/L 50 31.7 63 1-230
N-Nitrosodimethylamine ug/L 50 28.6 57 25-150
N-Nitrosodiphenylamine ug/L 50 36.0 72 25-150
Naphthalene ug/L 50 30.6 61 21-133
Nitrobenzene ug/L 50 30.3 61 35-180
Pentachlorophenol ug/L 100 84.2 84 14-176
Phenanthrene ug/L 50 36.2 72 54-120
Phenol ug/L 50 25.0 50 5-112
Pyrene ug/L 50 42.6 85 52-115
2,4,6-Tribromophenol(S) % 84 10-137
2-Fluorobiphenyl(S) • % 61 15-120
2-Fluorophenol(S) % 59 10-120
Nitrobenzene-d5(S) % 64 10-120
Phenol-d6(S) % 45 10-120
Terphenyl-d14(S) % 78 11-131
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC Page 22 of 30

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
f www.pacelabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827703 2827704
MS MSD
35534979001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
1,2,4-Trichoorobenzene ug/L 1.6U 50 50 34.9 34.8 70 70 44-142 0 30
1,2-Dichlorobenzene ug/L 1.4U 50 50 33.6 33.5 67 67 32-129 0 30
1,2-Diphenylhydrazine ug/L 1.3U 50 50 39.2 41.5 78 83 25-150 6 30
1,3-Dichlorobenzene ug/L 1.4U 50 50 32.3 32.8 65 66 1-172 2 30
1,4-Dichlorobenzene ug/L 1.5U 50 50 34.1 34.4 68 69 20-124 1 30
2,4,6-Trichlorophenol ug/L 1.4U 50 50 17.8 21.8 36 44 37-144 20 30 M1
2,4-Dichlorophenol ug/L 1.5U 50 50 30.4 32.5 61 65 1-191 6 30
2,4-Dimethylphenol ug/L 1.5U 50 50 39.4 37.0 79 74 32-119 6 30
2,4-Dinitrophenol ug/L 7.3U 250 250 67.5 75.5 27 30 1-181 11 30
2,4-Dinitrotoluene ug/L 1.7U 50 50 42.4 42.9 85 86 39-139 1 30
2,6-Dinitrotoluene ug/L 1.7U 50 50 40.9 40.6 82 81 50-158 1 30
2-Chloronaphthalene ug/L 1.4U 50 50 35.0 34.8 70 70 60-118 0 30
2-Chlorophenol ug/L 1.4U 50 50 28.2 29.9 56 60 23-134 6 30
2-Nitrophenol ug/L 1.7U 50 50 27.7 30.8 55 62 29-182 10 30
3,3'-Dichlorobenzidine ug/L 2.7U 100 100 81.5 88.6 82 89 1-262 8 30
4,6-Dinitro-2-methylphenol ug/L 4.5U 100 100 35.9 45.6 36 46 1-181 24 30
4-Bromophenylphenyl ether ug/L 1.2U 50 50 36.2 39.5 72 79 53-127 8 30
4-Chloro-3-methylphenol ug/L 2.8U 100 100 82.4 79.8 82 80 22-147 3 30
4-Chlorophenylphenyl ether ug/L 1.5U 50 50 37.1 36.9 74 74 25-158 0 30
4-Nitrophenol ug/L 9.4U 250 250 40.5 51.5 16 21 1-132 24 30
Acenaphthene ug/L 1.4U 50 50 36.4 35.2 73 70 47-145 3 30
Acenaphthylene ug/L 1.5U 50 50 37.1 36.0 74 72 33-145 3 30
Anthracene ug/L 1.6U 50 50 38.4 41.0 77 82 1-166 7 30
Benzidine ug/L 3.3U 100 100 40.5J 31.6J 41 32 10-130 30
Benzo(a)anthracene ug/L 1.5U 50 50 43.0 45.9 86 92 33-143 7 30
Benzo(a)pyrene ug/L 1.8U 50 50 43.3 46.3 87 93 17-163 7 30
Benzo(b)fluoranthene ug/L 1.7U 50 50 42.7 45.5 85 91 24-159 6 30
Benzo(g,h,i)perylene ug/L 1.6U 50 50 44.1 47.4 88 95 1-219 7 30
Benzo(k)fluoranthene ug/L 1.5U 50 50 44.5 46.9 89 94 11-162 5 30
bis(2- ug/L 1.3U 50 50 39.1 36.1 78 72 33-184 8 30
Chloroethoxy)methane
bis(2-Chloroethyl)ether ug/L 1.7U 50 50 38.6 37.1 77 74 12-158 4 30
bis(2-Ethylhexyl)phthalate ug/L 2.0U 50 50 42.0 44.5 84 89 8-158 6 30
Butylbenzylphthalate ug/L 1.9U 50 50 42.0 44.3 84 89 1-152 6 30
Chrysene ug/L 1.4U 50 50 42.2 45.5 84 91 17-168 8 30
Di-n-butylphthalate ug/L 1.6U 50 50 40.7 44.1 81 88 1-118 8 30
Di-n-octylphthalate ug/L 2.2U 50 50 41.9 46.1 84 92 4-146 10 30
Dibenz(a,h)anthracene ug/L 1.6U 50 50 45.0 48.7 90 97 1-227 8 30
Diethylphthalate ug/L 1.6U 50 50 37.3 38.1 75 76 1-114 2 30
Dimethylphthalate ug/L 1.4U 50 50 36.9 37.0 74 74 1-112 0 30
Fluoranthene ug/L 1.6U 50 50 39.3 42.7 79 85 26-137 8 30
Fluorene ug/L 1.4U 50 50 36.9 36.7 74 73 59-121 1 30
Hexachloro-1,3-butadiene ug/L 1.6U 50 50 34.7 35.2 69 70 24-116 1 30
Hexachlorobenzene ug/L 1.3U 50 50 37.0 40.6 74 81 1-152 9 30
Hexachlorocydopentadiene ug/L 2.4U 50 50 32.1 33.5 64 67 25-150 4 30
Hexachloroethane ug/L 1.3U 50 50 32.0 32.7 64 65 40-113 2 30
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 30

Pace Analytical Services,LLC
3
ace /final, ,kcal 9800 l ncey Ave. Suite 0100
78
_ /111 �/( Huntersville,NC 28078
www.pacelabs.com
[phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827703 2827704
MS MSD
35534979001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Indeno(1,2,3-cd)pyrene ug/L 1.7U 50 50 44.6 47.7 89 95 1-171 7 30
Isophorone ug/L 1.3U 50 50 40.2 37.4 80 75 21-196 7 30
N-Nitroso-di-n-propylamine ug/L 1.3U 50 50 42.0 39.6 84 79 1-230 6 30
N-Nitrosodimethylamine ug/L 1.8U 50 50 33.9 31.0 68 62 25-150 9 30
N-Nitrosodiphenylamine ug/L 1.4U 50 50 36.9 39.3 74 79 25-150 6 30
Naphthalene ug/L 1.6U 50 50 36.4 35.6 73 71 21-133 2 30
Nitrobenzene ug/L 1.5U 50 50 42.0 39.5 84 79 35-180 6 30
Pentachlorophenol ug/L 2.8U 100 100 29.1 27.1 29 27 14-176 7 30
Phenanthrene ug/L 1.4U 50 50 37.2 40.2 74 80 54-120 8 30
Phenol ug/L 1.5U 50 50 21.0 21.2 42 42 5-112 1 30
Pyrene ug/L 1.5U 50 50 40.4 42.2 81 84 52-115 4 30
2,4,6-Tribromophenol(S) % 49 62 10-137
2-Fluorobiphenyl(S) % 77 78 15-120
2-Fluorophenol(S) % 36 42 10-120
Nitrobenzene-d5(S) % 87 83 10-120
Phenol-d6(S) % 41 41 10-120
Terphenyl-d14(S) % 78 83 11-131
Results presented on this page are in the units indicated by the"Units.'column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 24 of 30

Pace Analytical Services,LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacslebs.com
[phone]
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529285 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92467868001
METHOD BLANK: 2827020 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Phenol mg/L ND 0.020 0.0050 03/10/20 13:30
LABORATORY CONTROL SAMPLE: 2827021
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Phenol mg/L 0.05 0.046 93 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827022 2827023
MS MSD
92467445001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Phenol mg/L ND 0.05 0.05 0.049 0.046 96 92 90-110 5 10
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2827024 2827025
MS MSD
92467960001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Phenol mg/L 0.029 0.05 0.05 0.075 0.077 91 95 90-110 3 10
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 30

Pace Analytical Services,LLC
a 9800 Kincey Ave, Suite 100
711eAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
i
QUALITY CONTROL DATA
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
QC Batch: 529719 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 4500CNE Cyanide,Total
Associated Lab Samples: 92467868001
METHOD BLANK: 2829238 Matrix: Water
Associated Lab Samples: 92467868001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L ND 0.0080 0.0060 03/11/20 18:35
LABORATORY CONTROL SAMPLE: 2829239
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Cyanide mg/L 0.1 0.095 95 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2829240 2829241
MS MSD
92468005002 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.092 0.093 84 85 80-120 1 10
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2829242 2829243
MS MSD
92467880004 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.10 0.10 97 95 80-120 2 10
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 26 of 30

Pace Analytical Services,LLC
3 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
www.pacelabs.com
[phone]
QUALIFIERS
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services-Asheville
PASI-C Pace Analytical Services-Charlotte
PASI-E Pace Analytical Services-Eden
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 30

Pace Analytical Services,LLC
/+ /+
s 9800 Kincey Ave. Suite 100
_ aceAnalytical Huntersville,NC 28078
www.pacelabs.com [phone]
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NEWTON INSTRUMENTS 2012
Pace Project No.: 92467868
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92467868001 OUTFALL 001 SM 2540D-2011 528761
92467868001 OUTFALL 001
92467868001 OUTFALL 001 EPA 1664E 530850
92467868001 OUTFALL 001 EPA 608.3 529440 EPA 608.3 529772
92467868001 OUTFALL 001 EPA 200.7 Rev 4.4 1994 530258 EPA 200.7 Rev 4.4 1994 530267
92467868001 OUTFALL 001 EPA 245.1 Rev 3.0 1994 529003 EPA 245.1 Rev 3.0 1994 529072
92467868001 OUTFALL 001 EPA 625.1 529438 EPA 625.1 529604
92467868001 OUTFALL 001 EPA 624.1 529029
92467868001 OUTFALL 001 EPA 420.4 Rev 1.0 1993 529285 EPA 420.4 Rev 1.0 1993 529497
92467868001 OUTFALL 001 SM 4500-CN-E-2011 529719 SM 4500-CN-E-2011 529887
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/17/2020 03:09 PM without the written consent of Pace Analytical Services,LLC. Page 28 of 30

en
CHAIN-OF-CUSTODY Analytical Request Document .wau 1 lo# ; 92467866 Nwtberw o
/193ceAnalitical'
W
Chain-of-Custody is a LEGAL DOCUMENT-Complete all relevent fields 1 a:
Company: Billing Information: II (I' II II III III I II 'II 1
Piedmont Geologic (.
same Conta 92467868
Address: 6003-145 Chapel Hill Rd, Raleigh,NC 27607 I
U. 1. 3 '.'1 1�3 zit.'l I I U l 1_.I
Report To: Email To: ••Preservative T (2) (3) (4) hydroxide,(5)zinc tcetate,
JonathE n Mur hre yodi m bisulfate,
(8)sodium
Mosul ,(9)h hydrochloric(A ascorbicsodium acid,
P y jmurphrey e( piedmontgeologie.com (6)methanol,(7)sodium bisulfate, sodium thiosulfate,(9)hexane,(A) (B)ammonium svfate,
Copy To: Site Collection Info/Address: (C)ammcnium hydroxide,(D)TSP,(U)Unpreserved,(0)Other
Anatyse5 Lab Profile/Line: -
Customer Project Nam!/Number. State: County/City: Time Zone Collected: . Lab Sample-Receipt Chect.listn
Newton Instruments/2012 NC / Butner [ 1 PT[ PAT[ 1 CT (I ET
Phone: 919 d54 9700 Site/Facility ID N: Custody Seam Dteesent//*..tact r�j NA
( ) Site F ty Compliance Monitoring? -Custody Siyaat:ures prea nt Y�rJNA
Email: lmvprreKaidxemolllgeWogicmn [ ] Yes ( ]No _ collector Signature Prei ent NA
otrles intact -(H NA
Collected By(print): Purchase Order#: DINPWS ID it: correct Hottl'en CP ri NA
(7 �Y ti(fiZ ( e'1 Quote U: DW Location Code: .. - rA Sufficient Volume N NA
C.lea - -Sampler, Received on Ice N NA
��.y(signature: Turnaround Date Required: Immediately Packed on Ice: _ VQA - tieadapnee;Aeceptalla N NA
( Yes [ ]No Z USDA Beguleted Soi1a 5 N lFf.
. c O .:.Sareplea in NolOigg Time. CD N}ice
Sam osal: Rush: Field Filtered(if applicable): I, Residual Chlorine Preaeut Y N
[4 Depose as appropria+s ;Return [ (Same Day [ )Next Day ( I Yes 'Q'
[ 1 No to v :+�v � "§ � Cl ships:
[ I Archive: ; 1 2 Day ( ]3 Day ( )4 Day ( ]5 Day ro , CV ? ' (V `r in Semple pit A ce sb •2.3 g43�N NA.
[ I Holdi (Expedite Charges Apply) Analysis:_ -- �O �. f�;, ;a• m *' pit'Strips:
�3 �
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`� O .r] a_ - .Sit3 3de ?resent Y.N ®
•Matrix Codes(Insert n Matrix box below):Drinking Water(OW),Ground Water(GW),Wastewater(WW), a N O I- 5 • r + (Y.. Leid"Acetate Stripe: '
Product(P),Soil/Soli/(SL),Oil(01),Wipe(WP(,Air(AR),Tissue(TS),Bioassay(B),Vapor(V),Other(OT) co Ea , H 1-- m n •
Camp/ Collected(or Res if of :ccx m' •`i. CD Lis LAB.USE Sample Y.
Customer Sample ID Matrix• Composite End .b. > p ` Lab >< / cormlanto,
PGrab Composite Start) CI Cms W -- U m Cl) _m. a of
Cl) = m 0 r a, at m ,c L.
Date Time Date Time t-- 0 > la_ ' U a. .-'c.
Outfall-00' GW Grab 3/3/ao /3/5 — — 15
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Customer Remarks/Sc ecial Conditions/Possible Hazards: TYPeot Ice(lied ^(.We1 :Blue ;, Dry None', SHORT+ (;QSP ESENT(<72 hours): Y- N/A Lab Sample Temperal ue Info:
Packing Material L(sed;•/ t ili Tracking if: Temp Blank Received: Y N NA
1 td - g. Therm[IV: 9l tOV'.
• , . ---- Cooler i Temp Up.n Receipt c'oC '
Radchem-sample(s)screened(<500 rpm): '1 61 NA S'ampies received via t Copier l Therm Cvs:Factor-Q.1 oC_
FEDEX. LIPS Client.' Courier r t! — Cooler 1 Correctec Temp T.' oC
Relin ed by/Comp y:(Signature) Date� e: Received by/Company:(Signature) Date/Time: MTIL.LA6 E ONLY Comments:
Rel. �` �� ql� �r 3�y�Zo 041 ' .
quished Com Lure) Date/lime. R e y/ mpa y:(Sign Date/Time;
9 Template: . Trio Blank Receiveq Y N NA '
3-y-2' /"J •3 f_ 3/4he 1 I 1 l 39 Prelogin: HCL McOH TSP " Other
R quished by/Comp ny:(Signature) Date/Time: R ' e Company:(Signature) Date/Time:
PM: Non Confurmance(s: Page'_
PB: ;'y YES J NO . of:

Document Name: Document issued:March 14,2019
Bottle IdentUicatlon Form IBIF) Page 1 of 1
/74Y- 3C8Alt8V,'Cdl Document No.: Issuing Authority:
F-CAR•CS-043-Rev.00 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project# WO# : 92467868
verified and within the acceptance range for preservation
samples. PM: TIH Due Date: 03/18/20
Exceptions:VOA,Coilform,IOC,Oil and Grease,DRO/9015(water)DOC,LLHg i CLIENT: 92—PIED GEOL
**Bottom half of box is to fist number of bottle L
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot g
adjusted added
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office;!.e.
Out of hold,incorrect preservative,out of temp,incorrect containers.
Page 30 of 30