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HomeMy WebLinkAboutWQ0006317_Monitoring - 03-2020_20200428FIORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page i of Permit No.: WQ0006317 Facility Name: Colonial Pipeline - Greensboro Junction WWTF County: Guilford Month: March Year: 2020 PPI: 001 Flow Measuring Point: ❑Influent ❑Effluent ❑✓ No flow generated Parameter Monitoring Point: [:]Influent❑✓ Effluent ❑Groundwater Lowering ❑Surface water Parameter Code 10 50050 00310 00916 00940 31616 00927 00610 00625 00620 00600 00556 00400 00665 00931 00929 70300 > @ ` Q 1= O O E ._ U 0 O 7 m E 7 is U d t U R O li O U E N R O E a s C ccto a� rn Y o �°Z R Z C 2 0) H O Z N ott _ o _ w 7 L 1- O 0. O Q O O N W cnv a o "6 f6 =_ H N O N o 24-hr hrs GPD mg/L mg/L mg/L #/100 mL mg/L mg/L mg/L mg/L mg/L mg/L su mg/L Ratio mg/L mg/L 1 0 2 06:30 8 0 3 06:30 8 0 4 06:30 8 0 5 06:30 8 1 0 6 06:30 8 0 7 0 8 0 9 06:30 8 0 10 06:30 8 0 11 06:30 4 0 12 06:30 8 0 13 06:30 8 0 14 0 15 0 16 06:30 8 0 17 06:30 8 0 181 06:30 8 1 0 19 06:30 8 0 <68 3.63 323 <20 5.45 12.8 40.1 1.7 0.533 36.1 7.56 0.269 48 619 2050 20 06:30 8 0 21 0 22 0 23 06:30 8 0 24 06:30 8 0 25 06:30 8 0 26 06:30 8 0 27 06:30 8 0 28 0 29 0 30 06:30 8 0 31 06:30 8 0 Average: 0 0.00 3.63 323.00 1.00 5.45 12.80 40.10 1.70 0.53 36.10 0.27 48.00 619.00 2,050.00 Daily Maximum: 0 68.00 3.63 323.00 20.00 5.45 12.80 40.10 1.70 0.53 36.10 7.56 0.27 48.00 619.00 2,050.00 Daily Minimum: 0 68.00 3.63 323.00 20.00 5.45 12.80 40.10 1.70 0.53 36.10 7.56 0.27 48.00 619.00 2,050.00 Sampling Type: Estimate Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Calculated Grab Grab Monthly Limit: 7,140 Daily Limit: Sample Frequency: Monthly 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year 3 X Year Per Event 3 X Year 3 X Year 3 X Year 3 X Year FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _,::�&_ of Sampling Person(s) Certified Laboratories Name: Faron D. Leigh Name: Analytical Environmental Services Name: Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑s compliant [:]Non-com pliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Faron D. Leigh Permittee: Colonial Pipeline Company Certification No.: 14891 Signing official: Brian L. Smith Grade: Phone Number: 336-669-7903 Signing Officials Title: Operations Manager Has the ORC changed since the previous NDMR? Dyes ❑� No Phone Number: 703-517-3051 Permit Expiration: 1/31/2025 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ? L1- F,ORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page ,7 of Z_ Permit No.: W00006317 Facility Name: Colonial Pipeline - Greensboro Junction WWTF County: Guilford Month: March Year: 2020 PPI: 001 Flow Measuring Point: ❑Influent ❑Effluent ❑� No flow generated Parameter Monitoring Point: ❑Influent ❑� Effluent ❑Groundwater Lowering ❑Surface Water Parameter Code —► 00530 NDVOC p U~ w O C O E aJ ~ U a v m R c ;a N N a C N a d o = a CL o f o U 24-hr hrs mg/L Yes/No 1 2 06:30 8 3 06:30 8 4 06:30 8 5 06:30 8 6 06:30 8 7 8 9 06:30 8 10 06:30 8 11 06:30 4 12 06:30 8 13 06:30 8 14 15 16 06:30 8 17 06:30 8 18 06:30 8 19 06:30 8 119 P 20 06:30 8 21 22 231 06:30 8 24 06:30 8 25 06:30 8 26 06:30 8 27 06:30 8 28 29 30 06:30 8 31 06:30 8 Average: 119.00 0 Daily Maximum: 119.00 0 Daily Minimum: 119.00 0 Sampling Type: Grab Grab Monthly Limit: Daily Limit: Sample Frequency: 3 X Year 3 X Year FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page __�tof Sampling Person(s) 11 Certified Laboratories Name: Faron D. Leigh 11 Name: Analytical Environmental Services Name: II Name: Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? 71Compliant ❑Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Faron D. Leigh Permittee: Colonial Pipeline Company Certification No.: 14891 Signing Official: Brian L. Smith Grade: Phone Number: 336-669-7903 Signing Official's Title: Operations Manager Has the ORC changed since the previous NDMR? ❑Yes [ONO Phone Number: 703-517-3051 Permit Expiration: 1/31/2025 z D Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted Is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _/—of Permit No.: 111116317 Facility Name: Colonial Pipeline• •. • • . 1 1 Field Name: • irrigation occur �� •Area (acres): Area (acres): Area (acres): this facility? Cover Crow p ■ • Hourlyat •. 1 • '. 1 • '. Hourly Rate (in): ...F Field Irrigated?p ■ Ii .. •. p ■ •Field Irrigated?■ • .. ■ ■ • FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page-12-of--o2,, Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? []Compliant ❑Non -Compliant OCompliant []Non -Compliant []Compliant ❑Non-Compilant QCompliant ❑Non -Compliant Compliant ❑Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Faron D. Leigh Permittee: Colonial Pipeline Company Certification No.: 14891 Signing Official: Brian L. Smith Grade: Phone Number: 336-669-7903 Signing Official's Title: Operationsw Manager Has the ORC changed since the previous NDAR-1? dyes ❑� No Phone Number: 703-517-3051 Permit Exp.: 1/31/25 ZZ q /Zo/ Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my Inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted Is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and Imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 III r, G«-59A COMPLIANCE REPORT FORM Permit #1 Q pain 3j (Submit one each nrunitorin,, period with GR-59 Ji)rms./ 1 Enter date monitoring results were due. Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO , skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office, 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. if the answer to question 7 is ",NO" contact the Regional Office within 90 days, an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facilit Failure to do so may sub'ect the permittee to a Notice of Violation fines, and/or penalties. APR 2 8 2020 g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A ' true d complete to the best of my knowledge. - yIz-o/ow Signature of Permittee (or Authorized Agent) Date GkN-59.S 12i8/2003 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: nff,"'617 o IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge WQ0006317 UIC NPDES Other Permit Name (if different): Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Upgradient of Fields 2-6 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 4� _ FIELD ANALYSES: WAS Well Depth: 21.20 ft. Well Diameter: 2 in. pH 5- u7 s Temp. �s. a °C DRY at Depth to Water Level: =ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: Z�gallons Appearance here: ElSamples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal < oZ /100ml Nitrate (NO3) as IN Z�j mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P (f. /�% mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total �cl 7 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride Jyr 12f mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia -4 • mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3as N; Ammonia Ni rogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Brian L. Smith - Operations Manager ,f'errnittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.1/2007 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 3/19/2020 12:45:00 PM Lab ID: 20031,97-001 Matrix: Aqueous Analyses Result Reporting Limit Qual Units Dilution BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 2-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH n-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH n-Propylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Chloroethane BRL 1.0 ug/L 294654 1 03/24/2020 19:28 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,1-Dichloroethene BRL 0.50 z. ug/L 294654 1 03/24/2020'19:28 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/24/2020 19:28 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1, 1 -Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Chloroform BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Benzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Dibromomethane BRL 0.50 ug/L, 294654 1 03/24/2020 19:28 ZH Trichloroethene BRL 0.50 ug/L. 294654 1 03/24/2020 19:28 ZH Bromodichloromethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Toluene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Dibromochloromethane BRL 0.50 ug/L, 294654 I 03/24/2020 19:28 ZH 1,2-Dibromoethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Bromoform BRL LO ug/L 294654 1 03/24/2020 19:28 ZH Styrene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,2,3-Trichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Isopropylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH Bromobenzene BRL 0.50 ug/L 294654 1 03/24/202019.28 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 l 03/24/2020 19:28 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 19:28 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L. 294654 1 03/24/2020 19:28 ZH Qualifiers: ' Value exceeds maximum cont4minant level E Estimated (value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value 1 Estimated value detected below Reporting Limit Page 10 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 3/19/2020 12:45:00 PM Lab ID: 20031,97-001 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Sun: Dibromofluoromethane 106 Surr: Toluene-d8 100 Surr: 4-Bromofluorobenzene 104 Total Phosphorus E365.1 Phosphorus, Total (As P) 0.197 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 307 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 8.09 Nitrogen, Nitrate (As N) 1.70 Hydrogen Ion (pH) by SM4500 H+ B pH 5.88 Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) BRL METALS, TOTAL SW6010D Cadmium BRL Chromium 0.0102 Lead BRL Zinc 0.0849 Qualifiers: • Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in die associated method blank > Greater than Result value (SW5030B) 0.50 ug/L 294654 1 03/24/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 0.50 u9/L 294654 1 03/24/202019:28 ZH 1.0 ug/L 294654 1 03/24/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 1.0 ug/L 294654 1 03124/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 0.50 ug/L 294654 1 03/24/202019:28 ZH 2.0 ug/L 294654 1 03/24/202019:29 ZH 76.4-125 %REC 294654 1 03/24/202019:28 ZH 78.3-116 %REC 294654 1 03/24/202019:28 ZH 64-125 %REC 294654 1 03/24/202019:28 ZH (E365.1) 0.050 mg/L 294601 1 03/26/202017:25 GO 10 m9/L 294241 1 03/23/202014:00 NN (E350.1) 0.200 m9/L 294636 1 03/26/2020 13 : 17 TL 1.00 mg/L R421345 1 03/20/202014:13 AS 0.250 mg/L R421345 1 03/20/202014:13 AS 0.0100 H pH Units R421432 1 03/23/20201520 SK 20 H Cotonies/100 R421502 10 03/23/202013:37 MH ml (SW3010A) 0.0050 mg/L 294456 1 03/24/202014:40 AJ 0.0100 mg/L 294456 1 03/24/202014:40 AJ 0.0100 mg/L 294456 1 03/24/202014:40 AJ 0.0200 mg/L 294456 1 03/24/202014:40 AJ E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix Narr See case narrative F Analyzed in the lab which is a deviation from the method < Less than Result value 1 Estimated value detected below Reporting Limit Page 11 of 49 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge W00006317 UIC Permit Name (if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Upgradient of Fields 2-6 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: '::�13/9^ate FIELD ANALYSES: WAS Well Depth: 25.20 ft. Well Diameter: 2 in. pH �l�units Temp. � °C DRY at Depth to Water Level: 2' 2ft. below measuring point Screened Interval: 18 ft. to 23 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 1.75 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: __771 -Z ,S gallons Appearance here: ❑ Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: EYES ❑ NO LABORATORY INFORMATION Date sample analyzed: e,3^a/J f ��ry O3^ 07� Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N 3, mg/I Zn - Zinc mg/I yZ1 Coliform: MF Total /100ml O Phosphorus: Total as P �. / mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate m /I g Other (Specify Compounds ( p fy pounds and Concentration Units): Dissolved Solids: Total mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia 0 . r� tl mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Aqent) Name and Title - Please print or Noe Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.1/2007 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: 3/19/2020 12:30:00 PM Lab ID: 20031,97-002 Matrix: Aqueous Reporting Dilution .analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 2-Chlorotoluene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH n-Butylbenzene BRL 0.50 ug/L 294654 t 03/25/2020 16:18 ZH n-Propylbenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Chloroethane BRL 1.0 ug/L 294654 1 03/25/2020 16:18 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1, 1 -Dichloroethene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/25/2020 16:18 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,1-Dichloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/25/202016:18 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Chloroform BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Benzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Dibromomethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Trichloroethee BRL 0.50 ug/L 294654 I 03/25/2020 16:18 ZH Bromodichloromethane BRL 0.50 ug/L 294654 1 03/25/2020 1& 18 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Toluene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/25/2020 16 18 ZH Dibromochloromethane BRL 0.50 ug✓L 294654 1 03/25/2020 16:18 ZH 1,2-Dibromoethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1, 1. 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Bromoform BRL 1.0 ug/L 294654 1 03/25/2020 16:18 ZH Styrene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,2,3-Trichloropropane BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH lsopropylbenzene BRL 0.50 ug/L 294654 1 03/25/20201618 ZH Bromobenzene BRL 0.50 ug/L 294654 1 03/2 5/2020 16 18 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/25/2020 16:18 ZH Qualifiers: • Value exceeds maximum contaminant level E Estimated (value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Nan See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value 1 Estimated value detected below Reporting Limit Page 12 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: 3/19/2020 12:30:00 PM Lab ID: 2003L97-002 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchlD Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D sec-Butylbenzene BRL 1,3-Dichiorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surr: Dibromofluoromethane 123 Surr: Toluene-d8 97.8 Surr: 4-Bromofluorobenzene 109 Total Phosphorus E365.1 Phosphorus, Total (As P) 0.139 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 221 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 34.3 Nitrogen, Nitrate (As N) 3.02 Hydrogen Ion (pH) by SM4500 H+ B pH 6.08 Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) 16 METALS, TOTAL SW6010D Cadmium BRL Chromium BRL Lead BRL Zinc 0.0343 Qualifiers. ' Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value (SW5030B) 0.50 ug/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/25/202016:18 ZH 1.0 ug/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/251202016:18 ZH 1.0 ug/L 294654 1 03/25/202016:18 ZH 0.50 u9/L 294654 1 03/25/202016:18 ZH 0.50 ug/L 294654 1 03/25/202016:18 ZH 2.0 ug/L 294654 1 03/25/202016:18 ZH 76.4-125 %REC 294654 1 03/25/202016:18 ZH 78.3-116 %REC 294654 1 03/25/202016:18 ZH 64-125 %REC 294654 1 03/25/202016:18 ZH (E365.1) 0.050 mg/L 294601 1 03/26/202017.26 GO 10 mg/L 294241 1 03/23/202014:00 NN (E350.1) 0.200 mg/L 294636 1 03/26/202013:19 TL 1.00 mg/L R421345 1 03/20/202014:29 AS 0.250 mg/L R421345 1 03/20/202014:29 AS 0.0100 H pH Units R421432 1 03/23/2020 15:26 SK 4 H Colottiesnoo R421502 2 03/23/202013:37 MH ml (SW3010A) 0.0050 mg/L 294456 1 03/24/202014:43 AJ 0.0100 mg/L 294456 1 03/24/202014:43 AJ 0.0100 mg/L 294456 1 03/24/202014:43 Al 0.0200 mg/L 294456 1 03/24/202014.43 AJ E Estimated (value above quantization range) S Spike Recovery outside limits due to matrix Narr See case narrative F Analyzed in the lab which is a deviation from the method < Less than Result value J Estimated value detected below Reporting Limit Page 13 of 49 SUBMIT FORM ON YFLLOW PAPER ONLY miff DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ��Z617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge W00006317 UIC NPDES Other Permit Name (if different): Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Downgradient of Fields 7-11 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-5A Date sample collected: FIELD ANALYSES: WAS Well Depth: 27.70 ft. Well Diameter: 2 in. pH ,�units Temp. a.4(// °C DRY at Depth to Water Level: / , ft. below measuring point Screened Interval: 8 ft. to 28 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 1.21 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: _gallons Appearance here: ❑ Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: of - a?e -,hr* Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal 4 oZ6� /100m1 Nitrate (NO3) as N mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 6 ?/0 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate m /l g Other (Specify Compounds ( p y pounds and Concentration Units): Dissolved Solids: Total A7 5 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia .4 m. a�mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.112007 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-5 Project Name: Greensboro Collection Date: 3/19/2020 1:15:00 PM Lab ID: 2003L97-004 Matrix: Aqueous Analyses Result Reporting Limit Qual Units Batchlt) Dilution Factor Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 2-Chlorotoluene BRL 0.50 u8/L 294654 1 03/24/2020 20:09 ZH n-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH n-Propylbenzene BRL 0.50 us/L 294654 1 03/24/2020 20:09 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Chloroethane BRL 1.0 ug/L 294654 1 03/24/2020 20:09 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH I,1-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/24/2020 20:09 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1, 1 -Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Chloroform BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Benzene BRL 0.50 119/L 294654 1 03/24/2020 20:09 ZH Dibromomethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Trichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Bromodichloromethane BRL 0.50 ug/L. 294654 1 03/24/2020 20:09 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Toluene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Dibromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 112-Dibromoethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Bromoform BRL 1.0 ag/L 294654 1 03/24/2020 20:09 ZH Styrene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,2,3-Trichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Isopropylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Bromobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Qualifiers: • Value exceeds maximum contaminant level E Estimated (value above quamitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 16 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-5 Project Name: Greensboro Collection Date: 3/19/2020 1:15:00 PM Lab ID: 20031,97-004 Matrix: Aqueous Reporting Dilution Analyses Rcsult Qual Units BatchlU Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) sec-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,3-Dichlorobenzene BRL 0.50 U19/1- 294654 1 03/24/2020 20:09 ZH 1,4-Dichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 4-Isopropyltoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,2-Dichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH 1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 294654 1 03/24/2020 20:09 ZH 1,2,4-Trichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Naphthalene BRL 1.0 ug/L 294654 1 03/24/2020 20:09 ZH Hexachlorobutadiene BRL 0.50 us/L 294654 1 03/24/2020 20:09 ZH 1,2,3-Trichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:09 ZH Xylenes, Total BRL 2.0 ug/L 294654 1 03/24/2020 20:09 ZH Sun: Dibromofluoromethane 104 76.4-125 %REC 294654 1 03/24/2020 20:09 ZH Sun: Toluene-d8 99.6 78.3-116 %REC 294654 1 03/24/2020 20:09 ZH Sun: 4-Bromofluorobenzene 104 64-125 %REC 294654 1 03/24/2020 20:09 ZH Total Phosphorus E365.1 (E365.1) Phosphorus, Total (As P) 0.710 0.050 mg/L 294601 1 03/26/2020 17:28 GO Residue, Dissolved (TDS) by SN12540C Residue, Dissolved (TDS) 105 10 mg/L 294241 1 03/23/2020 14:00 NN Nitrogen, Ammonia (as N) E350.1 (E350.1) Nitrogen, Ammonia (As N) BRL 0.200 mg/L 294636 1 03/26/2020 13:21 TL Inorganic Anions by IC EPA 300.0 Chloride 2.28 1.00 mg/L R421345 1 03/20/202015:42 AS Nitrogen, Nitrate (As N) 0.480 0.250 mg/L R421345 1 03/20/2020 15:42 AS Hydrogen Ion (pH) by SM4500 H+ B pH 6.38 0.0100 H pH Units R421432 1 03/23/2020 15:30 SK Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) BRL 20 H Colonies/too R421502 10 03/23/2020 13:37 MH m1 Qualifiers: • Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC cenified B Analyte detected in the associated method blank > Greater than Result value E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix Narr See case narrative F Analyzed in the lab which is a deviation from the method < Less than Result value J Estimated value detected below Reporting Limit Page 17 of 49 SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: NVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge WQ0006317 UIC NPDES Other Permit Name (if different): Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery '' X1 Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Downgradient of Fields 2-6 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-6 / Date sample collected: C%� /Y '0l2 FIELD ANALYSES: WAS Well Depth: 20.80 ft. Well Diameter: 2 in. pH 41,&units Temp. a_°C DRY at Depth to Water Level: .4. V.-ft. below measuring point Screened Interval: 4 ft. to 17 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: FL. _gallons Appearance here: ❑ Sam les for metals were collected unfiltered: ®YES ❑ NO and field acidified: ®YES El NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NOz) as N mg/I Pb - Lead mg/I Coliform: MF Fecal A L—/100ml Nitrate (NO3) as N 1r-, �, mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P f. �/ mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total lu mg/I AI - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/1 Cd - Cadmium mg/1 Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia ' mg/1 Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3as N; Ammonia NitroglTn, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.1/2007 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-6 Project Name: Greensboro Collection Date: 3/19/2020 1:00:00 PM Lab ID: 2003L97-005 Matrix: Aqueous Analyses Result Reporting Limit Qual Units Dilution BatchID Factor Date:kn:fhzcd Analyst Volatile Organic Compounds by GC/NIS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 2-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH n-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH n-Propylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Chloroethane BRL 1.0 ug/L 294654 1 03/24/2020 20:29 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,1-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/24/2020 20:29 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,1-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/202020:29 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Chloroform BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1, 1, 1 -Trichloroethane BRL 0.50 119/1. 294654 1 03/24/2020 20:29 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Benzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Dibromomethane BRL 0.50 ug/[, 294654 1 03/24/2020 20:29 ZH Trichloroethee BRL 0.50 ug/L 294654 1 03/24/2020 2029 ZH Bromodichloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Toluene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Dibromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2-Dibromoethane BRL 0.50 u9& 294654 1 03/24/2020 20:29 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 l 03/24/2020 20:29 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Bromoform BRL 1.0 ug/L 294654 1 03/24/2020 20:29 ZH Styrene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2,3-Trichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Isopropylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Bromobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Qualifien: . Value exceeds maximum contaminant level E Estimated (value above quantization range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Anslyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 18 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-6 Project Name: Greensboro Collection Date: 3/19/2020 1:00:00 PM Lab ID: 2003L97-005 Matrix: Aqueous Reporting Dilution Analyses Kesult Qual Units BatcbID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) sec-Butylbenzene BRL 0.50 ug(L 294654 1 03/24/2020 20:29 ZH 1,3-Dichlorobenzene BRL 0.50 ug(L 294654 1 03/24/2020 20:29 ZH 1,4-Dichlorobenzene BRL 0.50 us/L 294654 1 03/24/2020 20:29 ZH 4-Isopropyltoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2-Dichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2-Dibromo-3-chloropropane BRL 1.0 ug/L 294654 1 03/24/2020 20:29 ZH 1,2,4-Trichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Naphthalene BRL 1.0 ug(L 294654 1 03/24/2020 20:29 ZH Hexachlorobutadiene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH 1,2,3-Trichlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:29 ZH Xylenes, Total BRL 2.0 ug/L 294654 1 03/24/2020 20:29 ZH Surr: Dibromofluoromethane 109 76.4-125 %REC 294654 1 03/24/2020 20:29 ZH Surr: Toluene-d8 100 78.3-116 %REC 294654 1 03/24/2020 20:29 ZH Surr: 4-Bromofluorobenzene 107 64-125 iREC 294654 1 03/24/2020 20:29 ZH Total Phosphorus E365.1 (E365.1) Phosphorus, Total (As P) 1.01 0.050 mg/L 294601 1 03/26/2020 17:29 GO Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 392 10 mg/L 294241 1 03/23/2020 14:00 NN Nitrogen, Ammonia (as N) E350.1 (E350.1) Nitrogen, Ammonia (As N) BRL 0.200 mg/L 294636 1 03/26/2020 13:23 TL Inorganic Anions by IC EPA 300.0 Chloride 58.8 10.0 mg/L R421345 10 03/21/2020 05:36 AS Nitrogen, Nitrate (As N) BRL 0.250 mg/L R421345 1 03/20/2020 16:14 AS Hydrogen Ion (pH) by SM4500 H+ B pH 6.22 0.0100 H pH Units R421432 1 03/23/2020 15:38 SK Fecal Coliform (MF) SM9222D Fecal Coliform, WF) BRL 20 H Coloniesnoo R421502 10 03/23/2020 13:37 ME 1111 Qualifiers: • Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix Nan See case narrative F Analyzed in the lab which is a deviation from the method < Las than Result value J Estimated value detected below Reporting Limit Page 19 of 49 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge WQ0006317 UIC Permit Name (if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED Greensboro NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Downgradient of Fields 7-17 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7 Date sample collected: �� ��' v�2 FIELD ANALYSES: WAS Well Depth: 26.13 ft. Well Diameter: 2 in. p pH AI,;, Temp. / °C DRY at Depth to Water Level: ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 3 ft. above land surfaces Relative M.P. Elevation: ft. Odor check �� Volume of water pumped/bailed before sampling: Zd. i �-_gallons Appearance here: ❑ Sam les for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: era -,ArJ ?L-h ell/i3-a� Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal <Pz'�F /100ml Nitrate (NO3) as N <j�r, �mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P A t7 % mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total9 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia _mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen: NHaas N; Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Brian L. Smith - Operations Manager Permittee (or Authorized Aqent) Name and Title - Please print or Noe GW-59 Rev.1/2007 'S 1 a.f.._ 'ln knalytical Environmental Services, Inc "Ate; ✓ s-ivicu Client: Colonial Pipeline Client Sample ID: MW-7 Project Name: Greensboro Collection Date: 3/19/2020 1:30:00 PM Lab ID: 20031,97-006 Matrix: Aqueous Analyses Result Reporting Limit Qua[ Units Dilution BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 2-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH n-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH n-Propylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Chloroethane BRL 1.0 ug/L 294654 1 03/24/2020 20:50 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1, 1 -Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/24/2020 20:50 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,1-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Chloroform BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Benzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Dibromomethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Trichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Bromodichloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Toluene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Dibromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,2-Dibromoethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Bromoform BRL 1.0 ug/L 294654 1 03/24/2020 20:50 ZH Styrene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,2,3-Trichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Isopropylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Bromobenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 l 03/24/2020 20:50 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 20:50 ZH Qualifren: " Value exceeds maximum contaminant level E Estimated (value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Nan See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value 1 Estimated value detected below Reporting Limit Page 20 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-7 Project Name: Greensboro Collection Date: 3/19/2020 1:30:00 PM Lab ID: 2003L97-006 Matrix: Aqueous Analyses Result Reporting Qual Units BatchID Dilution DateAnalyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surr: Dibromofluoromethane 115 Surr: Toluene-d8 100 Surr: 4-Bromofluorobenzene 107 Total Phosphorus E365.1 Phosphorus, Total (As P) 1.07 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved JDS) 89 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA300.0 Chloride 15.1 Nitrogen, Nitrate (As N) BRL Hydrogen Ion (pH) by SM4500 H+ B pH 5.72 Fecal Coliform (NIF) SM9222D Fecal Coliform, (MF) BRL Qualifiers: . Value exceeds maximum contaminant level BRL Below reporting limit * Holding times for preparation or analysis exceeded * Analyte not NELAC certified * Analyte detected in the associated method blank > Greater than Result value (SW5030B) 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 0.50 ugIL 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1.0 119/L 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 1.0 ug/L 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 0.50 ug/L 294654 1 03/24/2020 20:50 ZH 2.0 Ug/L 294654 1 03/24/2020 20:50 ZH 76.4-125 9/oREC 294654 1 03/24/2020 20:50 ZH 78.3-116 %REC 294654 1 03/24/2020 20:50 ZH 64-125 %REC 294654 1 03/24/2020 20:50 ZH (E365.1) 0,050 ing/L 294601 1 03/26/2020 17:30 GC 10 1119/1, 294241 1 03/23/2020 14:00 NN (E350.1) 0.200 ing/L 294636 1 03/26/2020 13:25 TL 1.00 mg/L R421345 1 03/20/2020 15:01 AS 0.250 mg[L R421345 1 03/20/2020 15:01 AS 0.0100 H pH Units R421432 1 03/23/2020 15:39 SK 20 H col,miesnoo R421502 10 03/23/2020 13:37 MH nil E Estimated (value above quantitation range) S Spike Recovery outside limits due to matrix Narr See case narrative F Awlyzed in the lab which is a deviation from the method I Less than Result value J Estrinated value detected below Reporting Limit Page 21 of 49 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone. (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 01-31-2025 Facility Name: Colonial Pipeline Company Non -Discharge WQ0006317 UIC Permit Name (if different): NPDES Other Facility Address: 411 Gallimore Dairy Road TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro "` NC 27409 County Guilford © Spray Field ❑ Remediation: Contact Person: Faron D. Leigh Telephone#: 336-669-7903 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Upgradient of Fields 7-17 No. of wells to be sampled: 6 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: FIELD ANALYSES: WAS Well Depth: 31.0 ft. Well Diameter: 2 in, pH units Temp. 10, �K °C DRY at p ft. below measuring point Depth to Water Level: ,f, Screened Interval: 13 ft. to 33 ft. Spec. Cond. µMhos time of sampling, Measuring Point is 2.22 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: FL, tgallons Appearance here: ❑ Samples for metals were collected unfiltered: ®YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 4;-,& ��— ' / c� Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as IN � /3 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P e57 mg/I (Note: Use MPN method for highly turbidsamples)Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total / mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # 8260 Total Ammonia 4&4 mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.1/2007 91 u.__'lA knalytical Environmental Services, Inc Client: Colonial Pipeline Client Sample ID: MW-9 Project Name: Greensboro Collection Date: 3/19/2020 12:15:00 PM Lab ID: 20031,97-007 Matrix: Aqueous Analyses Result Reporting Limit Qual Units Dilution B:+tch[U Factor Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW503013) 1,2-Dichloropropane BRL 0.50 U91L 294654 1 03/24/2020 21:10 ZH 2,2-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 2-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH n-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH n-Propylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Dichlorodifluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Chloromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Vinyl chloride BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Bromomethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Chloroethane BRL 1.0 119/1. 294654 1 03/24/2020 21:10 ZH Trichlorofluoromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,1-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Methylene chloride BRL 5.0 ug/L 294654 1 03/24/2020 21:10 ZH trans-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1, 1 -Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH cis-1,2-Dichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Bromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Chloroform BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,2-Dichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,1-Dichloropropee BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Carbon tetrachloride BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Benzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Dibromomethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Trichloroethene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Bromodichloromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,1,2-Trichloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Toluene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,3-Dichloropropane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Dibromochloromethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,2-Dibromoethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Tetrachloroethene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Chlorobenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Ethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Bromoform BRL 1.0 ug/L 294654 1 03/24/2020 21:10 ZH Styrene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,2,3-Trichloropropane BRL 0.50 ug/l. 294654 1 03/24/2020 21:10 ZH Isopropylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Bromobenzene BRL 0.50 ug/L 294654 l 03/24/2020 21:10 ZH 4-Chlorotoluene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,3,5-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH tert-Butylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 1,2,4-Trimethylbenzene BRL 0.50 ug/L 294654 1 03/24/2020 21:10 ZH Qualifiers: . Value exceeds maximum contaminant level E Estimated (value above quantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 22 of 49 Analytical Environmental Services, Inc Date: 31-Mar-20 Client: Colonial Pipeline Client Sample ID: MW-9 Project Name: Greensboro Collection Date: 3/19/2020 12:15:00 PM Lab ID: 20031,97-007 Matrix: Aqueous Reporting Dilution lnalyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Sun: Dibromofluoromethane 105 Surr: Toluene-d8 101 Surr: 4-Bromofluorobenzene 104 Total Phosphorus E365.1 Phosphorus, Total (As P) BRL Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 41 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 3.77 Nitrogen, Nitrate (As N) 1.13 Hydrogen Ion (pH) by SM4500 H+ B pH 5.05 Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) BRL (SW5030B) 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 0.50 u9/L 294654 1 03/24/2020 21:10 ZH 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 0.50 119/L 294654 1 03/24/2020 21:10 ZH 1.0 ug/L 294654 1 03/24/2020 21:10 ZH 0.50 119/L 294654 1 03/24/2020 21:10 ZH 1.0 119/L 294654 1 03/24/2020 21:10 ZH 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 0.50 ug/L 294654 1 03/24/2020 21:10 ZH 2.0 u9/L 294654 1 03/24/2020 21:10 ZH 76.4-125 %REC 294654 1 03/24/2020 21:10 ZH 78.3-116 %REC 294654 1 03/24/2020 21:10 ZH 64-125 %REC 294654 1 03/24/2020 21:10 ZH (E365.1) 0.050 mg/L 294601 1 03/26/202017:34 GO 10 mg/L 294241 1 03/23/202014:00 NN (E350.1) 0.200 mg/L 294636 1 03/26/202013:27 TL 1.00 mg/L R421345 1 03/20/202016:30 AS 0.250 mg/L R421345 1 03/20/202016:30 AS 0.0100 H pH Units R421432 1 03/23/2020 15:42 SK 20 H Colonies/1o0 R421502 10 03/23/202013:37 MH mil Qualifiers: ' Value exceeds maximum contaminant level E Estimated (value above quantization range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Narr See case narrative N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method B Analyte detected in the associated method blank < Less than Result value > Greater than Result value 1 Estimated value detected below Reporting Limit Page 23 of 49