WQ0004268_Monitoring - 03-2020_20200424

GW-59A COMPLIANCE REPORT FORM Permit # WQ0004268
(Submit one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. ( 4/30/2020 ) Will this monitoring report (GW-59 and GW-59A)
YES
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the wellie�i�tjpt�„qu ) and
��
explain the problems encountered in obtaining the required information. (( jj-- �1 \`// M— ��f
APR 2 4 2020
nyw
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, u ji$
YES
NO
*
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Region ce or guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is `NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
1.) pH <6.5 at monitoring wells R1 — R9.
2.) R-2 (12.4 mg/L), R-5 (13.1 mg/L) & R-8 (16.2 mg/L) exceed 10 mg/L Nitrate nitrogen level
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
ES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Please refer to the data in the attached spreadsheet.
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YE
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility.ffilymato do so may subject the permittee to a Notice of Violation
fines, and/or penalties.
Land application occurred In MV16 t -9 sprayfields were la ber+27, 2019.
There is no facility discharging in o t ese la oons for quite some time
tark 't 9 0
g
The person completing this portion (GW--59A) of the monitoring repo{,r and submit this
form with GW-59 forms for required wells to the address provided at � e top V � rrent GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
,r �l 411412020
Signature of Permittee (or Authorized Agent) Date

Murphy Brown - Elliot & Rowan Tracts, Turkey, NC. Permit # WQ0004268
Groundwater Quality'
MW-1
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
CI
COD
NO,-N
NH ,- N
Total-P
TDS
SO
TOC
ft.
' C
Std. Units
umhos/cm
MPN/100 ml
- mg/ L--
Nov-17
27.00
19.7
4.3
NT
<I
200.0
25
0.53
c0.045
0.045
330
<2.9
5.40
Mar-18
27.10
17.7
4.6
NT
<I
177.0
46
0.48
<0.20
1.390
328
<5.0
1.80
Jul48
28.20
19.1
4.8
NT
<1
163.0
74
0.52
<0.20
1.090
358
<5.0
2.00
Nov-18
24.20
18.4
5.9
NT
<1
95.0
<20
3.46
<0.02
0.070
369
107.0
2.00
Mar-19
23.40
17.2
5.5
NT
<1
74.0
<20
3.17
<0.02
<0.04
285
79.0
1.90
Jul-19
24.90
20-4
7.9
NT
<1
77.0
<20
0.26
<0.20
0.120
398
136.0
2.40
Nov-19
24.00
18.5
6.4
NT
<1
103.0
27
8.23
<020
0.180
373
90.0
3.40
Mar-20
23.30
19.4
5.2
NT
<1
7Z0
<20
7.36
<0.20
0.190
321
75.0
2.90
Mean
25.3
18.8
5.6
NT
<I
120.8
43.0
3.0
<0.20
1.4
345.3
97.4 1
2.7
Min
23.3
17.2
4.3
NT
<1
74.0
<10
0.3
<0.02
<0.04
285.0
<2.9 1
1.8
Max
28.2
20.4
7.9
NT
41 1
200.0
74.0 1
8.2
<0.20
1.4 1
398.0 1
136.0 1
5.4
GWStds. I
1
1
6.5-8.5
1
250
1
10
1.5
1
500 1
250
MW-2
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,- N
NH ,- N
Total-P
TDS
SO.
TOC
ft.
' C
Sid. Units
umhos/cm
NIPN/100 ml
- mg/ L-
Nov-17
11.00
20.0
5.5
NT
<t
83.0
<10
0.27
0.30
<0.025
150
9.7
3.80
Mar-18
10.50
15.0
7.3
NT
<1
84.0
<20
0.13
0.30
0.11
208
11.0
2.80
Jul-18
11.30
18.1
5.3
NT
<1
85.0
<20
0.10
0.30
<0.04
223
11.0
2.50
Nov-18
9.80
19.7
4.7
NT
<1
6&0
<20
c0.02
<0.02
<0.04
185
15.0
2.60
Mar-19
9.10
14.9
5.2
NT
<1
43.0
<20
0.28
<0.02
<0.04
153
18.0
2.90
Jul-19
9.60
19.3
6.3
NT
<1
33.0
<20
<0.02
<0.02
0.04
141
23.0
3.10
Nov-19
10.40
1995
5.9
NT
<1
32.0
<20
<0.02
<0.02
0.04
133
23.0
3.30
Mar-20
9.30
16-6
5.6
NT
<1
3&0
<20
0.23
<0.2
0.07
162
1 20.0
3.10
Mean
10.1
17.9
5.7
NT
<1
58.0
<20
0.19
0.30
0.07
169.4
16.3
3.0
Min
9.1
14.9
4.7
NT
<1
32.0
<10
<0.12
<0.02
<0.025
133.0
9.7
2.5
Max
11.3
20.0
7.3
NT
<i
85.0
13
0.28
0.3
0.11
223.0
23.0
3.8
GW Stds.
6.5-8.5
250
10
1.5
500
250
MW-3
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,- N
N=
Total-P
TDS
SO.
TOC
ft.
C
Sid. Units
umhos/cm
MPN/100 ml
- mg/ L--__
Nov-17
6.00
19.0
6.2
NT
<I
140.0
29
0.049
0.07
0.33
400
5790
2.10
18-Mar
3.30
14.2
5.4
NT
<I
183.0
<20
<0.02
<0.20
0.18
786
64.0
0.70
Jul-18
4.80
19.2
5.4
NT
<1
155.0
<20
0.03
<0.20
0.22
738
62.0
0.50
Nov-18
4.30
18.4
5.0
NT
<1
132.0
<0.5
<0.02
<0.20
0.31
480
56.0
<0.5
Mar-19
1.80
13.1
4.9
NT
<1
181.0
<20
0.05
<0.20
0.36
553
65.0
<0.5
Jul-19
3.10
21.2
5.5
NT
<7
155.0
<20
<0.02
<0.20
0.46
499
57.0
1.00
Nov-19
4.70
19.3
5.7
NT
<1
78.0
<20
0.02
<0.20
0.49
304
40.0
0.50
Mar-20
3.20
15.4
6.3
NT
<7
139.0
<20
<0.02
<0.2
0.67
251
51.0
0980
Mean
3.9
17.5
5.5
NT
<I
145.4 1
29.0 1
0.04 4
0.07
0.38
501.4
56.5
0.93
Min
1.8
13.1
4.9
NT
<I
78.0
<0.5
<0.02
<0.2
0.2
251.0
40.0
<0.5
Max
6.0
1 21.2
6.3
NT
<1
183.0
29.0 1
0.05 1
0.07 10.671
786.0
65.0
2.1
GWStds.
6.5-8.5
250
1
10 1
1.5 1
1
500
250
R-1
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,-N
NH,-N
Total-P
TDS
SO.
TOC
g.
C
Std. Units
umhos/cm
MPN/100 ml
- mg/ L--
Nov-17
8.00
19.1
5.1
NT
<I
56.0
68
<0.20
0.076
3.30
94
17.0
7.50
hlar-18
5.40
13.0
4.8
NT
<I
32.0
<20
<0.02
<0. 20
0.64
152
16.0
0.7
Jul-18
7.20
22.3
4.8
NT
<1
14.0
31
<0.02
<0.20
0.96
101
1990
0.60
Nov-18
5.40
17.9
C3
NT
<1
50.0
120
0.03
0.2
0.96
101
19.0
0.60
Mar-19
4.80
12.1
4.3
NT
<1
3Z0
<20
0.12
<0.2
0.51
143
16.0
0.60
Jul-19
5.90
25.3
4.0
NT
<1
76.0
<20
0.07
<0.2
1.52
189
16.0
2.60
Nov-19
6.70
20.5
5.1
NT
<1
32-0
120
<0.02
<0.2
0.71
121
20.0
0.60
Mar-20
5,20
152
4.8
NT
<5
27.0
<20
0.09
<0.20
0.69
142
16.0
1.30
Mean
6.1
18.2
4.6
NT
<I
40.5
39.9
8
0.14
1.16
130.4
17.4
1.8
Min
4.8
12.1
4.0
NT
<I
14.0
<20
%
<0.02
<0.045
0.51
94.0
16.0
0.6
Max
8.0
25.3
5.1
NT
<5
76.0
120.0 1
0.12
0.20
3.3
189.0 1
20.0
7.5
GWStds.
6.5.8.5 1
250
110
1.5
500 1
250
R-2
Sample Data
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO, N
NH ,- N
Total-P
TDS
SO
TOC
ft,
' C
Sid. Units
umhos/cm
MPN/100 ml
- mg/ L-
Nov-17
7.50
19.8
4.6
NT
<I
39.0
<10
<0.20
<0.045
0.03
50
13.0
0.55
18-Mar
5.50
13.6
4.1
NT
c1
31.0
<20
0.43
<0.20
0.41
115
23.0
1.40
Jul-18
6.30
24.6
4.9
NT
<1
8.0
<20
1.59
<0.20
0.08
56
12.0
1.00
Nov-18
5.30
19.9
4.2
NT
<1
12.0
<20
8.85
<0.20
0.10
104
17.0
0.80
Mar-19
4.50
13.9
4.1
NT
<1
10.0
<20
11.7
<0.20
0.08
125
16.0
0.80
Jul-19
5.80
25.2
4.3
NT
<1
14.0
24
0.22
<0.2
0.15
87
14.0
0.50
Nov-19
6.30
214
4.6
NT
<1
15.0
23
11.7
<0.2
0.23
115
6.0
1.10
Mar-20
520
16.8
4.4
NT
<5
12.0
<20
12.4
<0.2
0.17
149
11.0
1.10
Mean
5.8
19.4
4.4
NT
<1
17.6
23.5 1
6.7
<0.14
0.16
100.1 1
14.0
0.9
Min
4.5
13.6
4.1
NT
<1
8.0
<10
<0.2
<0.045
0.03
<50
6.0
0.5
Max
7.5
25.2
4.9
NT
<5
39.0
24.0
12.4
<0.20
0.41
149.0
23.0
1.4
GWStds.
6.5-8.5
250
10
1.5
500
250

R-3
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,-N
NH,-N
I Total-P
TDS
SO
TOC
ft.
C
Std. Units
umhos/cm
MPN/100 ml
Nov-17
8.50
19.4
4.2
NT
<i
120 0
<10
1.10
0.045
<O 025
- -
54.0
1 80
Mar-18
7-60
14.0
4.2
NT
<1
108.0
<20
1.13
<0.20
0.360
-
49.0
0.90
Jut-18
8.20
20.2
4.3
NT
<1
108.0
<20
1.68
<0.20
0.050
274
44.0
0.70
Nov-18
720
18.8
3.7
NT
<1
116.0
<20
0.27
<0.20
0.100
250
28.0
1.30
Mar-19
6.70
13.4
4.0
NT
<1
93.0
<20
4.59
<0.20
<0.040
266
39.0
1.10
Jul-19
8.50
21.0
4.2
NT
<1
98.0
<20
0.06
<0.20
0.230
234
53.0
0.90
Nov-19
8.00
19.8
4.6
NT
<1
650
<20
5.33
<0.20
0.470
205
49.0
120
Mar-20
6.90
15.2
4.5
NT
<5
480
<20
5.31
<0.20
0.110
216
45.0
1.40
Mean
7.7
17.7
4.2
NT
<1
94.5
<20
2.43
0.05
0.22
248.4
45.1
1.2
Min
6.7
13.4
3.7
NT
<1
48.0
<10
0.06
<0.045
<0 .025
205.0
28.0
0.7
Max
8.5
21.0
4.6
NT
<5
120.0
28
5-3 1
0.05 1
0.47
292.0
54.0 1
.8
GWStd
1
1
6.5 -8.5
250
10 1
1.5 1
500
250
R-4
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO, N
NH,-N
Total-P
TDS
SO
TOC
ft.
' C
Std. Units
umhos/cm
MPN/100 ml
- mg/ L-
Nov-17
7.00
20.5
4.5
NT
<1
66.0
<10
<0.20
<0.045
1.40
130
16.0
1.50
M ar-18
7.00
14.1
4.4
NT
<1
82.0
<20
0.080
<0.20
0.60
238
15.0
1.20
Jul-18
7.80
21.6
4.3
NT
<1
89.0
<20
0.08
<0.20
0.14
230
11.0
0.80
Nov-18
7.10
20.1
4.1
NT
<1
85.0
<20
<0.02
<0.20
0.41
219
12.0
1.60
Mar-19
5.10
12.5
4.3
NT
<1
58.0
22.0
1.60
<0.20
0.90
136
10.0
2.10
Jul-19
7.50
23.2
4.5
NT
<1
80.0
<20
0.03
<0.20
0.45
178
11.0
1.80
Nov-19
8.10
21.4
5.0
NT
<1
78.0
3&0
1.17
<0.20
1.15
174
13.0
2.00
Mar-20
6.80
15.8
4.6
NT
<5
63.0
20.0
2.36
<0.20
0.29
190
19.0
2.10
Mean
7.1
18.7
4.5
NT
<1
75.1
25.7
0.89
<0.20
0.67
186.9
13.4
1.6
Min
5.1
12.5
4.1
NT
<1
58.0
<10
<0.025
<0.045
0.14
130.0
10.0
0.8
Max
8.1
23.2
5.0
NT
<5
1 89.0
35.0
1 2.36
1 <0.20
1.4
238.0
19.0
2.1
GW Side.
6.5- 8.5
250
1 10
1 1.5
500
250
R-5
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO, N
NH,-N
Total-P
TDS
SO
TOC
ft.
' C
Std. Units
umhos/cm
MPN/100 ml
- mg/ L-
Nov-17
7.50
20.6
4.6
NT
<1
5&0
17.0
2.40
<0.045
0.10
150
24.0
1 1.70
Mar-18
5.60
13.1
4.9
NT
<1
21.0
<20
1.18
<0.20
0.41
108
21.0
1.50
Jul-18
5.70
24.8
4.9
NT
<1
1&0
<20
1.64
<0.20
0.07
82
18.0
1.20
Nov-18
SAO
19.9
4.6
NT
<1
30.0
<20
1.84
<0.20
0.08
140
15.0
1.20
Mar-19
4.40
12.8
4.4
NT
<1
51.0
<20
20.00
<0.20
<0.04
231
10.0
0.90
Jui-19
5.70
26.1
4.7
NT
<1
36.0
<20
0.40
<0.20
0.21
161
13.0
1.50
Nov-19
6.60
21.9
4.9
NT
<1
29.0
<20
12.90
<0.20
0.04
172
12.0
1.30
Mar-20
5.50
15S
5.1
NT
<5
31.0
<20
13.10
.0. 00
-0. 15
184
14.0
1.40
Mean
5.9
19.4
4.8
NT
<1 1
34.0
19.6
6.7
<0.20
0.15
153.5
15.9
1.3
Min
4.4
12.8
4.4
NT
<1
18.0
<10
0.4
<0.045
<0.04
82.0
10.0
0.9
Max
7.5
26.1
5.1
NT
<5 1
56.0
17.0
20.0 1
<0.2
0.41
231.0
24.0
1.7
GW Stds.
6.5 - 8.5
1
1
250
10 1
1.5
500
250
R-6
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO, N
NH,-N
Total-P
TDS
SO
TOC
ft.
C
Std. Units
umhoskm
MPN/100 ml
- mg/ L-
Nov-17
9.50
20.2
5.1
PIT
<1
120.0
12.0
0.16
6.1
0.074
220
29.0
4.80
Nlar-18
7.00
14.6
5.1
NT
<1
102.0
24.0
OS3
0.9
0.240
330
52.0
8.20
Jul-18
7.30
2067
5.1
NT
<1
91.0
43.0
0.05
3.3
0.10
250
34.0
1260
Nov-18
7.50
20.3
4.8
NT
<1
640
4&0
<0.02
1.0
0.23
255
39.0
17.00
Mar-19
6.60
14.4
4.9
NT
<7
47.0
78.0
0.41
0.5
0.11
240
28.0
20.80
Jul-19
720
22.0
5.3
NT
<1
42.0
84.0
<0.02
0.5
0.24
251
32.0
29.90
Nov-19
7.80
21.4
5.3
NT
<1
47.0
62.0
0.11
1.1
0.23
201
30.0
20.70
Mar-20
7.10
16.3
5.4
NT
<5
44.0
45.0
3.62
<0.02
0.29
256
39.0
13.40
Mean
7.5
18.7
5.1
NT
<1
69.6
49.5
0.6
1.7
0.2
250.4
35.4
15.9
Min
6.6
14.4
4.8
NT
<I
42.0
12.0
<0.A
111
0.1
261.0
28.0
4.6
Max
9.5
22.0
5.4
NT
<5
120.0
84.0
3.6
6.1
0.3
330.0
52.0
29.11
GWStds.
6.5-8.5 1
1
1
250
10
1.5
500
250
R-7
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO, N
NH ,- N
Total-P
TDS
SO
TOC
ft.
' C
Std. Units
umhoa/cm
MPN/100 ml
- mg/ L-
Nov-17
9.00
16.8
4.2
NT
<1
110.0
17
0.28
0.061
0.150
180
13.0
4.20
Mar-18
4.50
14.0
4.3
NT
<1
179.0
<20
0.09
<0.20
0.320
379
9.0
3.00
Jul-18
6.80
20.0
4.4
NT
<7
152.0
50
<0.02
<0.20
1.10
320
140
4.40
Nov-18
5.60
19.2
4.1
NT
<1
146.0
<20
<0.02
<0.20
<0.04
293
14.0
3.20
Mar-19
4.00
13.5
4.4
NT
<1
112.0
<20
0.48
<0.20
0.04
240
16.0
3.20
Jul-19
8.20
20S
5.1
NT
<1
106.0
<20
<0.02
<0.20
0.11
227
17.0
3.70
Nov-19
7.20
20.6
5.0
NT
<1
124.0
<20
0.05
<0.20
0.07
226
13.0
4.00
Mar-20
4.80
16.1
4.9
NT
<5
110.0
<20
0.08
<0.20
0.14
272
22.0
4.30
Mean
6.3
17.6
4.5
NT
<1
129.9
23.4 1
0.13
0.06 1
0.28
267.1
14.8
3.75
Min
4.0
13.5
4.1
NT
<1
106.0
<20
<0.02
0.06
<0.025
180.0
9.0
3.0
Max
9.0
20.9
5.1
NT
<5
179.0
50.0
0.48
<0.20
1.1
379.0
22.0
4.4
GWStds.
6.5.8.5
250 1
10 1
1.5 1
1
500
250

R-8
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,- N
NH,- N
Total-P
TDS
SO
TOC
ft.
C
Std. Units
umhos/cm
MPN/100 ml
- mg/ L-
Nov-17
11.00
21.0
4.1
NT
<1
9.6
10
17.0
0.150
0.089
120
20.0
1,00
Nlar-18
6,40
14.7
4.5
NT
<1
To
<20
17.5
<0.2
0.130
178
15.0
0.60
Jul-18
6.80
23.1
5.1
NT
<1
12.0
<20
14.3
<0.2
0.14
155
15.0
0.50
Nov-18
6,90
20.4
5.2
NT
<1
10.0
<20
1.55
<0.2
0.10
118
15.0
<0.5
Mar-19
4.40
13.6
5.0
NT
<7
9.0
<20
14.4
<0.2
<0.04
132
16.0
-0.5
Jul-19
8.00
24.8
5.9
NT
<1
13.0
<20
09"
<0.2
0.32
126
17.0
<0.5
Nov-19
7.50
22.3
5.8
NT
<7
9.0
120
14.7
<0.2
0.12
168
12.0
0.70
Mar-20
5.80
16.3
6.4
NT
<5
100
<20
16.2
<0.2
0.16
165
14.0
0.90
Mean
7.1
19.5
5.3
NT
<1
10.0
1 18.8
12.0
0.19
0.15
145.3
15.5
0.65
Min
4.4
13.6
4.1
NT
<1
7.0
<10
0.44
<0.045
<0.025
118.0
12.0
<0.5
Max
11.0
24.8
6.4
NT
<5
13.0
10.0
17.5
0.15
0.32
178.0
20.0
1.00
GWStds.
6.5-8.5
250
10
1.5
500
250
R-9
Sample Date
DTW
Field Temp.
Field pH
EC
Fecal
Coliform
Cl
COD
NO,-N
NH,- N
Total-P
TDS
SO
TOC
ft.
C
Std. Units
um in
MPN/100 ml
- mg/ L-
Nov-17
11.50
19.7
4.2
NT
<1
59.0 1
12
0.79
-0.045
0.03
180
66.0
5.20
Mar-18
8.00
14.6
4.7
NT
<1
<5
20
1.43
<0.20
0.60
74
26.0
1,30
Jul-18
9.10
23.0
4.6
NT
<7
9.0
22
0.31
<0.20
0.99
111
30.0
1.40
Nov-18
9.60
19.8
4.0
NT
<1
14.0
41
0.48
<0.20
1.02
156
22.0
1.20
Mar-19
7.90
13.9
4.1
NT
<1
6.0
38
7.20
<0.20
0,49
112
20.0
1.20
Jul-19
8.80
26.0
C0
NT
<1
6.0
35
0.17
<0.20
1.07
124
18.0
1.70
Nov-19
10.40
22.1
4.9
NT
<1
9.0
29
9.24
<0.20
0943
121
17.0
1.20
Mar-20
8.50
17.2
4.9
NT
<5
6.0
20
6.00
<0.20
0.36
106 1
21.0
1.00
Mean
9.2
19.5
4.4
NT
<1
15.6
27.1
3.20
<0.18
0.63
123.0
27.5
1.8
Min
7.9
13.9
4.0
NT
<I
<5
12.0
0.17
<0.045
0.03
74.0
17.0
1.00
Max
11.5
26.0
4.9
NT
<5
59.0
41.0
9.2
<0.20
1.07
180.0
66.0
5.2
GWStds.
6.5-8.5
250
10
1.5
1.1
156.0
30.0
1.8
niu -
not much ground -ter standards.
�hoslcm = micromhos per centimete r, mg/L= parts per million, NT= Not Tested
DTbV = depth to groundwater, Field Temp.= field temperature; EC= electrical conductivity; Cl= chloride; COD= chemical oxygen demand; NO.- N = nitrate-nitroge n; NH,-N = ammonia- nitrogen, Total-P = Total Phcspho rus; TDS = tots I dissolved
soli ds, SO, = total sulfa te; and TOC = total organic carbon
Ile, NC, ENCO Laboratories, Cary, NC, and Enviromental Chemists, Inc.
Iliot & Rowan Tracts- Turkey. NC
wndw der Quality'

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (199 b8 County Sampson
(City) (state)
(zip)
❑■ Spray Field ❑ Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 1
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2
in.
pH 00400: 5.20 units Temp. 000lo: 19.4 oC
DRY at
Depth to Water Level 82546: 23.3 ft. below measuring point Screened Interval:
ft. to
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 1
/100mL
Nitrate (NO3) as N 00620 7.36
mg/L Zn - Zinc 01092 mg/L
Coliform: IMF Total 31504
/100mL
Phosphorus: Total as P 00665 0,19
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 7030o 321
mg/L
Al -Aluminum olim
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 2.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 77
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 75
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
�
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
PO Box 856, Warsaw NC sIff t�8
County Sampson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (State)
(zip)
A Spray Field ❑Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 2
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 19.75 ft.
Well Diameter: 2
in.
pH 00400: 5.6 units Temp. 000lo: 16.6 °C
DRY at
Depth to Water Level 82546: 9.3 ft. below measuring point Screened Interval:
ft. to _ft.
Spec. Cond. 000sa: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335 < 20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 1
/100mL
Nitrate (NO3) as N 00620 0.23
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.07
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 162
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 3.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 38
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 20
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
320
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
•
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (s`lOA8 County Sampson
(City) (Slate)
(Zip)
0 Spray Field 0 Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 3
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 17 ft.
Well Diameter: 2
in.
pH 00400: 6.3 units Temp. 000lo: 15.4 eC
DRY at
Depth to Water Level 82546: 3.2 ft. below measuring point Screened Interval:
ft. to —
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: Slight Sulfur
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Reddish / Brown
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335 < 20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.67
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 251
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 0.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 139
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 51
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 9 Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017
.2a.216

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
• •
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge W00004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
PO Box 856, Warsaw NC (sln3 8
County Sampson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(Oily) (State)
(Zip)
0 Spray Field El Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R1
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2
in.
pH 00400: 4.8 units Temp. 000lo: 15.2 eC
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval:
ft. to _ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 3 ft, above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan / Brown
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 0.09
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.69
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 142
mg/L
Al - Aluminum o1105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 27
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 16
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese o1055
uglL ,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
vZv
GW-59 Rev.05-02-2017

RI IRMIT FORM ON YFI.I.OW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
181T MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (sIgst68 County Sampson
(city) (state)
(zip)
❑■ Spray Field ❑ Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled: 12
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R2
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 4A units Temp. 000lo: 16.8 nC
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: ft. to
_ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan Tint
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 12.4
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.17
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 149
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 12
mg/L
Cd - Cadmium 01027
1
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 11
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? X Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L Voc Kemoval io
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
�?O-3 o
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
"
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (19A8 County Sampson
(City) (Slate)
(Zip)
0 Spray Field El Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled: 12
❑ Water Source Heat Pump ❑ Other:
from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R3
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2 in.
pH 00400: 4.5 units Temp. 000lo: 15.2 oC
DRY at
Depth to Water Level 82546: 6.9 ft. below measuring point Screened Interval: ft. to
_ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan Tint
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335 < 20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 5.31
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.11
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 216
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.4
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 48
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 45
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
26
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
•
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1817 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
PO Box 856, Warsaw NC (s'YgA8
County Sampson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(City) (State)
(Gip)
X Spray Field D Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled: 12
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R4
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 0040o: 4.6 units Temp. 000lo: 15.8 oC
DRY at
Depth to Water Level azsas: 6.8 ft. below measuring point Screened Interval: ft. to
_ft.
Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan Tint
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists,
Inc.
Certification No. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 20
mg/L
Nitrite (NO2) as N 00615 0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 2.36
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.29
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 190
mg/L
Al -Aluminum o11o5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 2.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 63
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen: NH3asN: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4130/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Po Box 856, Warsaw NC (sl�f�a County Sampson
(City) (State)
(Zip)
ME Spray Field El Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R5
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 17 ft.
Well Diameter: 2
in.
pH 00400: 5.1 units Temp. 000lo: 15.6 OC
DRY at
Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval:
ft. to
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan Tint
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020-3131/2020
Laboratory Name: Environmental
Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 13.1
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.15
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 184
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.4
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 31
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 14
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 < 0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; N1­13as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017
re
Agent)
'///y/_2d20

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (S ggS8 County Sampson
(City) (slate)
(zip)
❑■ Spray Field ❑ Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R6
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2.
in.
pH 00400: 5.4 units Temp. 000lo: 16.3 oC
DRY at
Depth to Water Level 82546: 7.1 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Yellow / Tan
here: ❑
Samples for metals were collected unfiltered: ❑ YES ❑
NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental
Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335 45
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 3.62
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 0.29
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 256
mg/L
Al -Aluminum ol1o5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 13.4
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 44
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 39
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 9 Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn -Manganese 01055
ug/L
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017
zv

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��&117
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (Iyg�' B County Sampson
(Gly) (31ate)
(Zip)
9 Spray Field El Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled: 12
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R7
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000io: 16.1 oC
DRY at
Depth to Water Level 82546: 4.8 ft. below measuring point Screened Interval: ft. to
—
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists,
Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 0.08
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.14
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 703oo 272
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 4.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 110
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 22
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese oio55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge WQ0004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (�'gA8 County Sampson
(City) (sidle)
(zip)
9 Spray Field ❑ Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R8
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2
in.
pH 00400: 6.4 units Temp. 000lo: 16.3 oC
DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval:
ft. to
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: Slight Sulfur
check
Volume of water pumped/bailed before sampling:
5
gallons
Appearance Tan Tint
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental
Chemists, Inc. Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335 <20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 uglL
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 16.2
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.16
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 165
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 0.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 10
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 14
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH,asN; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 4/30/2023
Facility Name: Murphy Brown Elliot & Rowan Tracts
Non -Discharge W00004268 UIC
Permit Name (if different): Murphy Brown WWIS
NPDES Other
Facility Address: PO Box 856, Warsaw NC
28398
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
PO Box 856, Warsaw NC (18ff `68 County Sampson
(City) (Slate)
(zip)
X Spray Field El Remediation:
Contact Person: David Nordin
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Elliot and Rowan sites
No. of wells to be sampled:
12
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - R9
Date sample collected: 3/20/2020
FIELD ANALYSES:
WAS
Well Depth: 17 ft.
Well Diameter: 2
in.
pH 00400: 4.90 units Temp. 000lo: 17.2 oC
DRY at
Depth to Water Level 82546: 8.5 ft. below measuring point Screened Interval:
ft. to —
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
4 (dry)
gallons
Appearance Tan / Brown / Turbid
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/20/2020 - 3/31/2020
Laboratory Name: Environmental Chemists, Inc.
Certification No. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 20
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616 < 5
/100mL
Nitrate (NO3) as N 00620 6.0
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.38
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 106
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.0
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 21
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese o1055
uglL ,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
David Nordin, Director of Environmental Compliance
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.05-02-2017

Smithfield Hog Productions - Warsaw Date of Report;___ Apr 09 2020__ _
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID:
20-11812 Site: MW-1
Test
Collect Date/Time
3/20/2020 9:50 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Color
Color
Clear
03/20/2020
Depth to water, ft.
Depth to water, Ft.
23.3 feet
03/20/2020
Sulfate
EPA 300.0
75 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
321 mg/L
03/20/2020
Temperature
SI41 2550 B
19.4 C
03/20/2020
Chloride
SM 4500 Cl E
77 mg/L
04/04/2020
pH
SM 4500 H B
5.2 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.19 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
2.9 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
7.36mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
7.36 mg/L
04/08/2020
Report # 2020-04795 Pano i H ,

3 E'i).virUC�.E'.111
ANALYTICAL & CONSULTING CHEMISTS
nvironmental Chemists, Inca
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab s 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
inforenvironmen talchemists.com
Smithfield Hog Productions -Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11815 Site: MW-2 3/20/2020 10:20 AM Water Client
Test Method Results Date Analyzed
Color
Color
Clear
03/20/2020
Depth to water, ft.
Depth to Water, Ft.
9.3 feet
03/20/2020
Sulfate
EPA 300.0
20 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
162 mg/L
03/23/2020
Temperature
SM 2550 B
16.6 C
03/20/2020
Chloride
SM 4500 Cl E
38 mg/L
04/04/2020
pH
SM 4500 H B
5.6 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.07 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
3.1 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL 03/20/2020
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/21 /2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.23 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
0.23 mg/L
04/08/2020
Report #:. 2020-04795 Paqe 2 of 12

nvironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 8 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
info(! ;environmentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID:
20-11816 Site: MW-3
Test
Collect Date/Time
3/20/2020 10:30 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Color
color
Reddish/Brown
03/20/2020
Depth to water, ft.
Depth to water, Ft.
3.2 feet
03/20/2020
Sulfate
EPA 300.0
51 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
Slight Sulfur
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 c
251 mg/L
03/23/2020
Temperature
SM 2550 B
15.4 C
03/20/2020
Chloride
SM 4500 Cl E
139 mg/L
04/04/2020
pH
SM 4500 H B
6.3 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.67 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
0.8 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/21/2020
Nitrate+ N itrite-N itrogen
EPA 353.2
< 0.02 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
04/08/2020
Report # 2020-04795 Paqe 3 of 12

ANALYTICAL & CONSULTING CHEMISTS
E vironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab m 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infor:environtnentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report:_ Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11817 Site: R-1 3/20/2020 12:14 PM Water Client
Test
Method
Results
Date Analyzed
Color
Color
Tan/Brown
03/20/2020
Depth to water, ft.
Depth to water, Ft.
5.2 feet
03/20/2020
Sulfate
EPA 300.0
16 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
Sne 2540 c
142 mg/L
03/23/2020
Temperature
SM 2550 B
15.2 C
03/20,12020
Chloride
SM 4500 Cl E
27 mg/L
04/04/2020
pH
SM 4500 H B
4.8 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.69 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOG)
SM 5310 B
1.3 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL 03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2
< 0.02 mg/L
03/21 /2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.09 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
0.09 mg/L
04/08/2020
Report # 2020-04795 Gana c �f 19

= enyiroch�m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Law/Fax
info Lenvironmentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
20-11818 Site: R-2 3/20/2020 11:59 AM Water Client
Test
Color
Depth to water, ft.
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
Chloride
pH
Total Phosphorus
COD
Total Organic Carbon (TOC)
Fecal Coliform
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
Nitrate+Nitrite-Nitrogen
Nitrate Nitrogen
Method
Results Date Analyzed
Color
Tan Tint
03/20/2020
Depth to water, Ft.
5.2 feet
03/20/2020
EPA 300.0
11 mg/L
03/23/2020
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Qualitative
None
03/20/2020
SM 2540 C
149 mg/L
03/23/2020
SM 2550 B
16.8 C
03/20/2020
SM 4500 cl E
12 mg/L
04/04/2020
SM 4500 H B
4.4 units
03/20/2020
SM 4500 P F
0.17 mg/L
04/06/2020
SM 5220D
<20 mg/L
03/24/2020
SM 5310 B
1.1 mg/L
03/23/2020
SM 9222D MF
<5 Colonies/100mL
03/20/2020
EPA 353 2 < 0.02 mg/L 03/21/2020
EPA 353.2 12.4 mg/L 04/04/2020
Subtraction Method 12.4 mg/L 04/08/2020
Report # 2020-04795 Page 5 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental eists9Inc®
6602 Windmill Way, Wilmington, NC 2840.5 a 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 s 252.473.5702 Lab/Fax
2 55-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info(n,environmentalchernists.com
Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11819 Site: R-3 3/20/2020 11:46 AM Water Client
Test Method Results Date Analyzed
Color
Color
Tan Tint
03/20/2020
Depth to water, ft.
Depth to water. Ft.
6.9 feet
03/20/2020
Sulfate
EPA 300-0
45 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
216 mg/L
03/23/2020
Temperature
SM 2550 B
15.2 C
03/20/2020
Chloride
SM 4500 Cl E
48 mg/L
04/04/2020
pH
SM 4500 H B
4.5 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.11 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
1.4 m /L
g.
/23
03, �„/202Q
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
5.31 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
5.31 mg/L
04/08/2020
Report #:: 2020-04795 Page 6 of 12

Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office B-6 x 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11820 Site: R-4 3/20/2020 11:34 AM Water Client
Test Method Results Date Analyzed
Color
color
Tan Tint
03/20/2020
Depth to water, fit.
Depth to water, Ft.
6.8 feet
03/20/2020
Sulfate
EPA 300.0
19 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 c
190 mg/L
03/23/2020
Temperature
SM 2550 B
15.8 C
03/20/2020
Chloride
SM 4500 cl E
63 mg/L
04/04/2020
pH
SM 4500 H B
4.6 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.29 mg/L
04/06/2020
COD
SM 5220D
20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
2.1 mg/L
03/2312020
Fecal Coliform
SM 92220 MF
<5 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
<0.02mg/L
03/21/2020
Nitrate+ N itrite-N itrogen
EPA353.2
2.36mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
2.36 mg/L
04/08/2020
Report # 2020-04795 Page 7 of 12

nvirenmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 m 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, INC 28540 s 910.347.5843 Lab/Fax
[e-mail]
Smithfield Hog Productions-1/i/iarsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11821 Site: R-5 3/20/2020 11:23 AM Water Client
Test Method Results Date Analyzed
Color
color
Tan Tint
03/20/2020
Depth to water, ft.
Depth to water, Ft.
5.5 feet
03,120/2020
Sulfate
EPA 300.0
14 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 c
184 mg/L
03/23/2020
Temperature
SM 2550 B
15.6 C
03/20/2020
Chloride
SM 4500 Cl E
31 mg/L
04/04/2020
pH
SM 4500 H B
5.1 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.15 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
1.4 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
< 0.02 mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA353.2
13.1 mg/L
04/04/2020
Nitrate Nitrogen
subtraction Method
13.1 mg/L
04/08/2020
Report # 2020-04795 Page 8 of 12

evxr0Ghenat
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inca
6602 Windmill Way, Wilmington, NC 28405 9 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Smithfield Hog Productions -Warsaw
Date of Report: Apr 09, 2020
Post Office Box 856
Customer PO #:
Warsaw NC 28398
Customer ID: 08110011
Attention: Kraig Westerbeek
Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-11822 Site: R-6
3/20/2020
11:12 AM Water Client
Test
Method
Results Date Analyzed
Color
color
Yellow/Tan
03/20/2020
Depth to water, ft.
Depth to water, Ft-
7.1 feet
03/20/2020
Sulfate
EPA 300.0
39 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
256 mg/L
03/23/2020
Temperature
SM 2550 B
16.3 C
03/20/2020
Chloride
SM 4500 Cl E
44 mg/L
04/04/2020
pH
SM 4500 H B
5.4 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.29 mg/L
04/06/2020
COD
SM 5220D
45 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
13.4 mg/L
03!23/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA353.2
< 0.02 mg/L
03/21/2020
Nitrate+ N itrite-N itrogen
EPA353.2
3.62mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
3.62 mg/L
04/08/2020
Report # 2020-04795 — ---- — Page 9 of 12

ANALYTICAL & CONSULTING CHEMISTS
Environmental Ce , Inc.
6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A VVilmulgton Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
info@eiiviroj-,mentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
20-11823 Site: R-7 3/20/2020 10:58 AM Water Client
Test Method Results Date Analyzed
Color
Color
Clear
03/20/2020
Depth to water, ft.
Depth to water, Ft.
4.8 feet
03/20/2020
Sulfate
EPA 300.0
22 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
272 mg/L
03/23/2020
Temperature
SM 2550 B
16.1 C
03/20/2020
Chloride
SM 4500 Cl E
110 mg/L
04/04/2020
pH
SM 4500 H B
4.9 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.14 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 8
4.3 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/1 OOmL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
< 0.02 mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.08 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
0.08 mg/L
04/08/2020
Report #: 2020-04795 Page 10 of 12

T en�v�roc�emyY°
ANALYTICAL & CONSULTING CHEMISTS
Im
nvironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Ivlanteo, NC 27954 s 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
info genvironmentalchemists.com
Smithfield Hog Productions - Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-11824 Site: R-8 3/20/2020 10:45 AM Water Client
Test Method Results Date Analyzed
Color
color
Tan Tint
03/20/2020
Depth to water, ft.
Depth to Water. Ft.
5.8 feet
03/20/2020
Sulfate
EPA 300.0
14 mg/L
03/23/2020
Ammonia Nitrogen
EPA350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
03/20/2020
Odor
Qualitative
Slight Sulfur
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 C
165 mg/L
03/23/2020
Temperature
SM 2550 B
16.3 C
03/20/2020
Chloride
SM 4500 CI E
10 mg/L
04/04/2020
pH
SM 4500 H B
6.4 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.16 mg/L
04/06/2020
COD
SM 5220D
<20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
0.9 mg/L
03,123/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL
03,120/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
16.2 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
16.2 mg/L
04/08/2020
Report 9: 2020-04795 Page 11 of 12

�n�ira�chem
ANALYTICAL & CONSULTING CHEMISTS
nviro mental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info@envir(-)nrnentalchemists.com
Smithfield Hog Productions -Warsaw Date of Report: Apr 09, 2020
Post Office Box 856 Customer PO #:
Warsaw NC 28398 Customer ID: 08110011
Attention: Kraig Westerbeek Report #: 2020-04795
Project ID: Del Monte -Monitoring Wells
Lab ID Sample ID:
20-11825 Site: R-9
Collect Date/Time Matrix Sampled by
3/20/2020 12:30 PM Water Client
Test Method Results Date Analyzed
Color
Color
Tan/Brown/Turb
03/20/2020
Depth to water, ft.
Depth to water, Ft.
8.5 feet
03/20/2020
Sulfate
EPA 300.0
21 mg/L
03/23/2020
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
04/06/2020
Gallons bailed before sampling
Gallons Baited before sampling
4 (dry) gallons
03/20/2020
Odor
Qualitative
None
03/20/2020
Total Dissolved Solids (TDS)
SM 2540 c
106 mg/L
03/23/2020
Temperature
SM 2550 B
17.2 C
03/20/2020
Chloride
SM 4500 Cl E
6 mg/L
04/04/2020
pH
SM 4500 H B
4.9 units
03/20/2020
Total Phosphorus
SM 4500 P F
0.38 mg/L
04/06/2020
COD
SM 5220D
20 mg/L
03/24/2020
Total Organic Carbon (TOC)
SM 5310 B
1.0 mg/L
03/23/2020
Fecal Coliform
SM 9222D MF
<5 Colonies/100mL
03/20/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2
<0.02mg/L
03/21/2020
Nitrate+Nitrite-Nitrogen
EPA 353.2
6.00 mg/L
04/04/2020
Nitrate Nitrogen
Subtraction Method
6.00 mg/L
04/08/2020
Comment:
Reviewed by:
Report # : 2020-04795 Page 12 of 12

Date: '/j4/
knalyst:
Certifleation q 94
Facility Name: __
PermitM: �:.�%'—fit' f�` t.l�sea Vj0. r)(DO LlZi,
pH
Reference Method: SM4500 H+B -2011 Instrument lD A"O.W o
Calibration Time ( Ca! Butler 4 0 s u.
Cal Buffer 10 0 s u Check Buffer 7.0 s.u.
Comments
"pH check butTer must read within t 0.1 pH units of the buffer's true value.
4 su buffer Lod#/: Ricca 2901791 Exp 1220 7 su buffer Lot#/: Ricca 2809744 Exit 7120 10 su buffer Lot#: Ricca 2905A94 Exit I Of20
Sample location
Sample Collection
Time
Sample Analysis
Time♦
pH Result
s.0
Do- Post -analysis Buffer
Check value s.u.
Comments/Data Qualifiers
► Post analysis buffer check is (equired when performing analyses at multiple sarApling locations and must be within ; O 1 units of the butler's rue value
All pH values in pH units (i.e., s.u.)_ Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s.u.
Total Residual Chlorine (TRC)
Reference Method: SM 4500 Ct-G2011: Hach 8167 HR: ( Please circle aitolicable Method Instrument ID:
Daily Check
Post -analysis
Check Std.
Time check
Sample
Sample
Sample
TRC Result
Standard Result
(when analyzing
Standard
Location
Collection
Analysis
µg/L or mg/L
Comments/Data Qualifiers
µg/L or mg/L
at multiple sites
Analyzed
Time
Time
FRC Daily Check Standard fnic value pgfL or mg/L acceptance range µg/L or me1L
Check standards must recover within f 10% of the check standard's true value
Annual Calibration Curve Verification Date:
Reagent Blank Value: (When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
Reference Method:SM 45000 G,•2011 Instrument ID:
Calibration/
Verification
Time
Calibration variable
Meter reading
or % efficiency
after calibration
• Post -analysis calibration
verification (when necessary)
I
Comments
Temperature
Barometric
Pressure
Theoretical
Value ill
Calculated
Value m
I lie this row when performing a verification instead of
calibration
SampieL anon
Sample Collection
Time
Sample Analysis
Time
DO reading
m
CommentslDataQuaJifiers
i
• When performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed
if sample is measured dtrectIv in the ,cream and/or url only ume anah&d wnuld he recorded with it note that they are mcasurcd in iitu ur immediately
Temperature
Reference Method: SM 2550 B-2010 Instrument ID:"4z4f a
Sample Location
Sample
Collection
Time
'Sample
Analysis
Time
Temperature
'C
i Comments/Data Qualifiers
Irv.
*lo
rl ,o it
/`- V t /(.4
t
p9w- s Pt r
I /o>w �,.�
ray, n: f
r-
, L ,:impl: is ;ncasurod dircctK n the stream at'fdror tin ioe onK tithe anah./cd �sould he r.n>rded. eth a not, that thcc x,� rn„tsur_d in situ :r nrimcdiatcK
annual Verification Date 1/2020
Field Personnel Note:
DOC.QA.t01
Rev 07/2019

Certification # 94
Date: Facility Name:.L'O j�j�yt�2y���� — •7 gA1 �-G'\fir GA C�
knalyst: Permit#:
pH
Reference Method: SM4500 H+B -2011 Instrument ID:
Calibration, Time Cal Buffer C su. Cal Buffer 10.0 s U. Check Buffer 7.0 s u. Comments
"pH check buffer must read within t 0 1 pH units of the butler's true value.
4 su butler Lot#/: Ricca 2901791 Exv l2/20 7 Sul buffer Lot; / Ricca 2809744 Exn 7/20 10 Sul buffer Lot#: Ricca 2905A94 Exo 10/20
Sample location
Sample Collection
Sample Analysis
pH Result
►Post -analysis Buffer
Comments/Data Qualifiers
Time*
Time*
s,u
Check value s.u.
t
/i
j/5� 1rL 3
Oil
% f q
►;Post analysts butter cneck is requirea when performmg analyses at muatpie sampling iocanons ana must oe wimm = D ! units DI me Du Iicr s u uc vatuc
All pH values in pH units (i.e., s.u.). Record all data to the nearest 0.01 s.u. and report to the nearest 0.1 s.u.
Total Residual Chlorine (TRC)
Referenre Merhnri• CM 3iM!•1�:7ni t • W—h R167 HR- I PirAce circle annlicahle Methrxi Instnument ID -
Daily Check
Standard Result
µg/t, or mg/L
Post -analysis
Check Std.
(when analyzing at multiple sites)
Time check
Standard
Analyzed
Sample
Location
Sample
Collection
Time
Sample
Analysis
Time
TRC Result
µl3n or mg/L
Cornments/Data Qua! itiets
i
i
TRC Daily Check Standard frue value AWL or mg/L acceptance range pg/L or ntg/L
Check standards must recover within* 10% of the check standard's true value
Annual Calibration Curve Verification Date:
Reagent Blank Value: —(When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared)
Dissolved Oxygen (DO)
R.-c rn kA-Ii A-QXA AGM rl !: _')AI I 1—tnirnnnt Irt.
Calibration/
Verification
rime
Calibration variable
Meter reading
or%efficiency
after calibration
• Post -analysis calibration
verification (when necessary)
Comments
Temperature
Barometric
Barometric
Theoretical
Value m L
Calculated
Value m
IIlse this row when performing a verificution instead of
Sample Location
Sample Collection
Time
Sample Analysis
"rime
DO reading
m
Comments/Data Qualifiers
• When performing analyses at mukipie locations. the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed.
it'sampie is measured directly in Inc ,t.,cani and/or on9nc. only Imicanah zed would Iv recorded with a note that they are measured in situ or onniediatek
Temperature
Reference Method SM 2550 R-2010 Instrument ID -
Sample Location
Sample
Collection
Time
'Sample
analysis
Time
Temperature
°C
Comments/DataQualifiers
i it I, 7
J4Y rL,S
A. Irl-Z &I
I Jf- !j1143t
A-1 V&j
urt% t;ni sn.d tad •,t�r,ud �� rcc��rdcd. •.� nth note slut thee .u� m�.nurui m u! �,r i�nmcdr: I�te
knnual Verification Date 1/2020
Personnel Note:
DOC.QA.001
Rev 0712019

Environmental Chemist, inc., Wilmington, NC lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392,0223
Sample Receipt Checklist
Client-�---�}
Date: O /a0__...._Report Number - {}—(�'
Receipt of sample:
Delivered
❑ YES ❑ NO
❑ YES
N/A UPS ❑ EedEx ❑ Other ❑
1 Were custody seals
❑ NO N/A present on the cooler?
2. if custody seals were presunbroken?
Original temperature upon receipt J-3_oC ent, were they intact/
How temperature taken:
❑ Temperature Blank Corrected temperature upon receipt oC
IR Gun ID: Thomas Traceable
S/N 192511657 Against Bottles —�—
❑ YES Cl NO
Gun
Correct Factor 'C:
3. If temperature of 'e
iwas
12 YES ❑ NO
P o ect Mgon
cooler cee exceeded 6 C r
4. Were proper custod f g /GA notified?
YES ❑ NO
5• Were sam le ID's listed
p Y procedures (relinquished/received) followed?
YES ❑ NO
on the COC?
6. Were samples ID's listed
YES ❑ NO
on sample containers?
7. Were collection date
YES ❑ NO
t`
and time lised on the COC?
8• Were tests to be
YES ❑ NO
performed listed on the COC?
9. Did samples arrive in
YES ❑ NO
proper containers for each test?
10. Did samples arrive in
YE5 ❑ NO
good condition for each test?
11. Was adequate
YES ❑ NO
sample voiurne available?'
12. Were camp;es received
YES ❑ NO
within proper holding time far requested
13. Were acid presetests?
rved
YES 0 NO
❑ YES I:]
samples received at a pH of <2?
14. Were cyanide samples received at a
NO
YES ❑ NO
pH >12?
15. Were sulfide samples received at a pH >9?
YES Ci NO
16. Were NH3/TK1VJphenol received at a chlorine residual of <0.5 m/�? **
17. Were Sulfide/Cyanide
received at a chlorine residual
" TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
" Bacteria samples are
checked for Chlorine at time of analysis and recorded on the benchsheet
rvation;
(Must be completed for
Fadding
any ample(s) incorrectly y preserved or with headspace)
were
cle oneH250a
received incorrectly preserved and were adjusted accordingly
HNO3
ofrvation:
HCI NaOH
Note:
If more than one preservative is needed, notate in comments below
customer service immediately for incorrectly preserved samples.
Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who
Volatiles Sample(s)
was notified, date and time:
were received with headspace
COMMENTS:
-vC l�ra.ill7[,.

6602 Windmill Way , NC
ton
ENVIRONMENTAL CHEMISTS' I N C OFFICE: 910-392-02 311FAX[phone]
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled By• SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a
m
a
M
r
$
�
s
" a
�',
= E
"
Uj
z
PRESERVATION
ANALYSIS REQUESTED
D to
Time
Temp
Z
z
e
N
m
o
_.
x
o
z
=
W
o
MW:
�cf.
C
P
� t '
X
Chloride, NO2,TDS,Sulfate
G
G
.r
Depth to water: �. 6
C
P
" `'�°
X
NH3,NO3,Total P, COD
G
G
Gallons bailed:
C
P
X
TOC
G
G
pH (field): 1
C
P
I
X
I
IFecal Coliform
G
G
Depth ter:
C
P
G
G
Color: �''�
C
P
G
G
Odor:
C
P
G
G
C�
P
G
G
C
P
G
G
Total of 12 wells due march, july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Date7ime
1.
1.
2.
Temperature when ReceiveC: 1; Accepted: V
Delivered By e - Received By:
Comments:
mple Requested:_
Time:
TURNAROUND: 1

a m
13602 Windmill Way
ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910-3 2-02 31ImingtonFAX 92-4 24 s
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO: (c)�
REPORT TO: Kraig Westerbeek
PHONEIFAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
&
a
w
�,
E° i2
U
C
qq°
V
r E
V
a
J .Z
PRESERVATION
ANALYSIS REQUESTED
Clete,
Time
Temp
z
Z
U
=
c�V
2
o
-
0
Z
o
�
W
O
MW: Z-
W t•
!� �-�
P� .� .
C
P
X
Chloride, NO2,TDS,Sulfate
G
G
to water: ®�"
C
P
p
j� ia,�
X
le�Depth
NH3,NO3,Total P, COD
G
G
Gallons bailed:
C
P
X
TOC
G
G
pH field): Jr
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color: C Q
C
P
G
G
Odor: Am a�
C
P
G
G
C
P
G
G
C
P
G
G
Total of 12 wells due march, July, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Daterrime
Received By:
Date/Time
2.
I emperaiure when Received c;: 1, .J Accepted: � _ �ieje t cf: ���.,�' Resample Requested: _
Delivered By: F _ � -
�Z .� Received By: � <.�""' � Date: -2-0-14) Time
Comments:_ ____ __ J TURNAROUND:

6602 Windmill Way on, NC 2
44� min
ENVIRONMENTAL, CHEMISTS, INC OFFICE: 910-3 2-02 3'IFAX910-392-44245
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Prod udtion-Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:•.. (irTr�
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
p
Collection
a
a
�_
E `o
U
_
L o
oa
V
o
= E
"
m
dt=
J z
PRESERVATION
ANALYSIS REQUESTED
Date,,
Time
Temp
z
°z
U
o
m
"
o
i
o
�-
w
o
MW: 3
60�
'7r
C
P
X
Chloride, NO2,TDS,Sulfate
G
G
e•
Depth to water:
C
P
f'
X
NH3,NO3,Total P, COD
G
G8
Gallons bailed:
C
P
X
TOC
G
G
pH (field): '
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color:
G
G
Odor: 6 b �,''� Jb
C
P
G
G
C
P
G
G
C
P
_T1
G
G
Total of 12 wells due march, julyy november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Tom erature wh n R
d °C
o ecelve � Accepted:" Re to : � r i_Resample Requested:_
Delivered By: — - Received BY: Date: ,� ° a "� ,. �•-
0 �,o —Time:
�,M.,.—•.
Comments: _____ TURNAROUND: , —

4=0
Analytical & Consulting Chemisj's
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
rn] I FrTIr)H AN[) PHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28406
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME;
PO NO:
REPORT TO: Kraig Westerbeek
PHONEIFAX:
COPY TO:
email:
Sampled Bv: SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
&
9�
U
E
ca
2
t;
0 8
E
W
r a 1
4)
C
E
M
9 W
03 M
z
PRESERVATION
ANALYSIS REQUESTED
D4te
Time
Temp
T�l
0
z
3".
x
z
0
0
MW:
C
P
x
Chloride, NO2,TDS,Sulfate
G
Ga
Depth to water:
C
P
Z'
x
NH3,NO3,Total P, COD
G
G
Gallons bailed:
C
P
X
TOC
G
I G
pH (field): Q_
x
Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color.- -A,, Life Jj 0
C
'P
G
G
Odor: Ad
C
P_
G
G
C
P
G
C
P
G
G
Total of 12 wells due march, july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
2.
Temperature when Receivqd"C.. Accepted: V Resample Requested:
Delivered By: Received By: Date: Time:
TURNAROUND:

ton, NC
ming
4 k .
ENVIRONMENTAL CHEMISTS, IN � OFFICE: 910'392-02231FAX[phone]
Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:'''.
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
K
F
a
s
YI
C 8
0
_
C (7
o
0 "
C
9 E
°
W
a
-'
PRESERVATION
ANALYSIS REQUESTED
Cl to
Time
Temp
z
a
v
"o
o
o
MW:
�i
' C
C
P
t
X
Chloride, NO2,TDS,Suifate
NH3,1\103,Total P, COD
G
G
Depth to water: to
C
P
I
ix
-
G
G
Gallons bailed:
C
P
X
TOC
G
G
pH field :!
C
P
JXJ
IFecal Coliform
G
G
De water:
C
P
G
G
Color: Id ; N
C
P
G
G
Odor: A
C
P
G
G
C
P
G
G
C
P
G
G
Total of 12 wells due march, july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Datefrime
1.
2.
Temperature when Received "C: Accepted: Re' ted: &`1` Resample Requested: _
Delivered By: Received By: I` —Date:2-_" __ Time:s_ u �
Comments:" ` ' TURNAROUND:

6602 Windmill Way
QM on
ENVIRONMENTAL CHEMISTS, -IN �.B OFFICE: 910-392-02 31tFAX 9t10 392-4424 5
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
_
CONTACT NAME:
PO NO: ., -
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled Dy: _ SAMPLE TYPE: I = Influent, E = Effluent, W = Well ST = Stream SO = Soil SL = Sludge Other:
Sample Identification
Collection
a
N
2
$ o
`o
a
0'
c�
`a xn
" s
®w
m
z
PRESERVATION
ANALYSIS REQUESTED
Pat
Time
Temp
i
s
�,
x__
o
0
0
o
A
MW: I`" �
!I Yt
�"� '�
C
P
16111
X
Chloride, NO2,TDS,Sultate
G
G
r,
Depth to water:
C
P
`r
X
NH3,NO3,Total P, COD
G
G
,,.
Gallons bailed: >
C
P
X
TOC
G
G
pH field):° 7 F
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
G
G
s�
Color: "
C
P
G
G
Odor: oi -
C
P
G
G
C
P
G
G
C
P
G
G
Total of 12 wells due march, jul', november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
12.
"r ,.. �_ r,_
_� �,._9 A. 9
acantivaturewilvik rswa;eovea u:
_ _ Accepted: — eject", �<
Resample Requested:
Delivered By:
Received By: t�s
Date .. .-2 Time:
Comments: --a
""
___ TURNAROUND:

6602 Windmill Way Wilmington, NC 28405
41� ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
ICOPY TO: lemail:
Sampled By: i
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
CL
a
CL
E
a
CD
0
a
E
0
0
aPRESERVATION
8 (M
2 E
U
ca
a) n
z
ANALYSIS REQUESTED
[)at
Time
Temp
W
0
z
0
W
z
x
0
4
z
W X
MW
C
P
X
Chloride, NO2,TDS,Sulfate
G
ou
22L to water: d
C
P
x
NH3,NO3,Total P, COD
G
I G
Gallons bailed:
C
P
x
TOC
G
G
pH {field):
C
P_
I
I
Ix
I Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color:
C
P
G
G
Odor: AM
C
P
G
G
C
P
G
G
C
G
Total of 12 wells due march, july, noVernber: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date[Time
Received By:
Date/Time
1.
[2-
I emperature when H-eceived-IC: s Accepted:_ V 'R ' ed: Resample Requested:
e,,
Delivered By:, Received By: Date: Time: -:0,
Comments: —TURNAROUND:

4M
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS. DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sam Sampled By: SAMPLE TYPE: I = Influprit F = Ffflijant W � Wall Q-r — cr—..., en 4z-;l Q1 421 .4 ^6ti
Sample Identification
Collection
CL
E
M
(n
0 w
CL
E a
0
0
0
0 0.
I —
2 E
0
LU
M
J
z
PRESERVATION
ANALYSIS REQUESTED
Dpte,,
Time
Temp
0
z
0
0
z
X
0
z
0
W
w
0
Mw: it
a
I I i%
C
P
r
x
Chloride, NO2,TDS,Sulfate
G
G
rr
Depth to water: G
C
P
x
NH3,1\103jotal P, COD
G _
G
Gallons bailed:
C—
I P
X
-
TOC
G
pH (field):
C
—G
P
x
Fecal Coliform
G
G
De wo titer:
C
G
G
Color: f,.j
C
P
G
G
Odor: ,fit w-
C
P
G
G
C
P
G
G
C P—
G G
Total of 12 wells due march july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer Relinquished By: Date/Time Received By: Datefrime
1.
2.
Temperature when 0--h-4 A
Accepted:_Kejecte
Resample Requested:
;'61
Delivered By:- C Received BY: Time:
Comments: Date: Aw A,
TURNAROUND:

ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-02 3'IFAX 910 392-44245
44W
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN ni: ri j-4:zTnny
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO: 7A)
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled By:_
SAMPLE TYPE: I = Influent. F = Fffluenf W = We!! CT -- Cfream Cn _ Sail - _ ci..A,.e r%f
Sample Identification
Collection
a
a
°
E
M
CL o
o
d
0
o"
w
o rn
Ea
oc
w
a
PRESERVATION
ANALYSIS REQUESTED
to
Time
Temp
w
i
�
x
x
¢o
ao
MW:
S
• �'�
C
P
�,%� ✓
X
Chloride, NO2,TDS,Sulfiate
I a
G
G
Depth to water: a?
X
INI-13,1\103jotal P, COD
G
G
�s
Gallons bailed:
C
P
X
TOC
G
G
�-
pH (field):
C
P
X
Fecal Coliform
G
G
Depth o water:
C
P
G
G
Color: a. ,J LA4G
G
Odor:
C
P
G
G
C
P
G
G
C
P
J—
G
G
Total of 12 wells due march,
july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,19
Transfer
Relinquished By:
DatefTime
Received By:
Date/Time
1.
2.
Temnerafurs%whesn Re ceiverfor'•
� e___-`-'-
- - - - - ...__ ... ... p...._ nucepicu: a Jepled: Resample Requested:
Delivered By:_- r Received B � , • ' '"7 � �.;" .
Date: Time: - "
Comments:— _ TURNAROUND:

4=0
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Smithfield Hog Produr;tion-Warsaw
PROJECT NAME: Del Monte Facility
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
Sampled By:-- SAMPLE TYPE: I = Influent. E = Effluent. W = Well- ST = Stream_ qO = Snit Al = Shidna rlthar-
Sample Identification
Collection
N
•m
E
C
c o
a•
C
W
z
PRESERVATION
ANALYSIS REQUESTED
[
Time
Temp
zt
,o
a
~
x
o
MW:
TV►
a, y
d
t It.
C
P
`
X
Chloride, NO2,TDS,Su1fate
G
G
as
Depth to water: �9
G
P
X
NH3,NO3,Total P, COD
G
G�
Gallons bailed: ��
C
P
X
TOC
G
G
pH field): e9•
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color:
G
G
Odor: A ""
C
P
G
G
G
G
C
P
G
G
Total of 12 wells due march,
july' november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2.
Temnerature whAn Panekivael
ar•---------
-
- - ----- --� - ,. _9jectea f� Resample Requested:
Delivered By: . �✓ .. Received By: �� " Date: ) Time:
Comments.--- — -- TURNAROUND:

Analytical & Consulting Chemists
4W
ENVIRONMENTAL. CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION ANn rHAIN n1l: i-I MTnnv
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Smithfield Hog Production -Warsaw
PROJECT NAME: Del Monte Facility
eo
REPORT NO:#
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO: Kraig Westerbeek
PHONE/FAX:
COPY TO:
email:
arllp_ Ed By: SAMPLE TYPE: I = Influont_ IF = Ef font W - Wnll CT - Stranm Cn _ Q-H c1 _ c1..a... n+§ ,
Sample Identification
Collection
a
"
E
N
Q o
W ^
s O
c a
"
a
o
E
"
m M
M
-
PRESERVATION
ANALYSIS REQUESTED
Time
Temp
W
z
z
ME
_at
_
°
as
o
MW:
X
Chloride, NO2,TDS,Sulfate
G j
G
Depth to water:
C
P
65
L
X
;,
�-
NH3,NO3,Total P, COD
G
G
Gallons bailed:
C
P
X
TOC
G
G
pH (field): 6. .�
C
P
X
Fecal Coliform
G
G
Depth to water:
C
P
G
G
Color: „ra m �►"
C
P
G
G
Odor: �w
C
P
G
G
C P
G G
C P
G G
july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8,R9
Relinquished By: Date/Time Received By: Date/Time
or, / r
Total of 12 wells due march,
Transfer
f.
2.
TemnP_raturea wh an A anaiunrl
electea:�41 ,: Resample Requested: --
Delivered By: Received By �:-;' �- - _ ,, ,...
Comments w Date: " _ LO .., .a. Time: '
-.—TURNAROUND:---

i
ton, NC 28405
ENVIRONMENTAL CHEMISTS, I N C OFFIC6602 E: 910-392-0223ndmill Way'ImingFAX 910-92-4424
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Smithfield Hog Production -Warsaw PROJECT NAME: Del Monte Facility REPORT NO: :>20
ADDRESS:
CONTACT NAME:
PO NO:
PHONE/FAX:
REPORT TO: Kraig Westerbeek
COPY TO: email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Collection PRESERVATION
Sample Identification a o "'
a CL ° c o r E o o a o w ANALYSIS REQUESTED
ate Time Temp U " z °_ z x o
MW: z
/ •�.
C
P
r
h
X
Chloride, NO2,TDS,Sulfate
G
G
40
Depth to water:
C
P
/ . i
X
1
..
NH3,NO3,Total P, COD
G
G
Gallons bailed:
C
P
X
TOC
G
G
pH (field):
C
P
X Fecal Coliform
Received By: Da te/T
G
G
Depth to water:
C
P
G
G
Color: �6'D
C
P
.
G
G
Odor:
C
P
G
G
C
P
G
G
C
P
G
G
Total of'12 wells due march,
Transfer
july, november: MW1,2,3,R1,R2A,R3,R4,R5A,R6,R7,R8;R9
Relinquished By; I
Date/Time
1.
2.
Temperature when Received'°C: _. ` Accepted:_`.
Delivered By: ''cl—_ Received
Ime