NC0088919_Toxicity Reduction Evaluation Progress Report_20140730

TE uest _
E'A
R
' ENVIRONMENTAL CONSULTANTS; P.C. , .. �i ` . .
-July 30; 2014
W. Corey Basinger - Regional Supervisor
Sur.`face�Water-Protection Section =Winston=Salem. Regional Office°
Division of Water Quality.
585 Waughtown Street
Winston-Salem; NC:27107-2241
Re:, Toxicity Reduction. Evaluation Progress Report'
Former Coliseum -Shelf ='Quality Oil. Company, LLC
NPDES Permit No. NC0088919
NCDWM-UST Incident No.: 15260. -
Terraquest Project No':: 01195
Dear Mr. Basinger:'
On' behalf ofthe permitee,: Quality Oil, Company,'.LLC,Terraquest'Environmental Consultants) P.C.. ,
hereby submits this Toxicity Reduction Evaluation Progress Report in acco_ rd'ance'.with the Special
Order,by-Consent EMC SOC VVQ S-12=004..
,Section 2 (a) 2)'of the "SOC states the following:
"scope`. of ' the THE ' work' should ` consider but, is not . limited. , to: effluent
characterization/identification/confirmation of suspected toxicants, 'evaluation of point source,
contributionsto".toxicity, pretreatment bench scale treatabilitystudies,,toxicity so_urce reduction
strategies":
As'requirdd, consideration to each of those- items'throughbut the ;latest testing quarter that
ended. in�June.2014 per Section 2'(a) 3) ofahe'SOC follows:
effluent characterization%identification/confirmation of suspected toxicants:
During the April, May, June 2014 discharge quarter; weekly inspection Sr,
of the subject treatment'
...system were performed by'either the ORC Or. backup ORC.for routine maintenance and oversight
as requiire&by the permit and.also-to'"investigate the source,or situationthat might be causing_
the toxicity to Ceriodaphnia.Dubia. No finite'toxicant was identified throughout the period:
Routine maintenance activities including'general'cleaning and the -replacement of pohethylene-
bag filters was conducted with site"visits made on 4/7/14,- 4/.14/14, 4/21/14;'4/28/14,•5/5/14,1'
5/12/14, 5/19%14; 5/27/14, 6/4/14;,6/9/14;.6/10/14;'6/16/14, 6/23/146nd;6/30/14. Associated
checklists are enclosed.
100 E. Ruffin Street • Mebane, North -Carolina 27302
Telephone [phone] • Facsirdle (919), 56&9095
Www.terraquestpe.com

Page t
C: Basinger.
7/30/14.
Monthly system. sariiples`were collected from, the treatment.system's influent; after air. stripper,'
after first carbon filter, and effluent port locations. Those samples were submitted to'an.NG
certified laboratory for analysis of the VOCs that are the subject of both the -•site's 'remediation
and of the,TRE. No toxicants are apparent. 'The analytical results -are similar to histdrical results.
La,b.re,po.rts for April;-May,,,and.June,2014;are included for reference.
evaluation of point source contributions to toxicity: .
Terraquest has reviewed possible contributors of toxicants at thi,s'site., No new information is
available and the.,toxicant remains undefined.:As noted,, recent analytical data:mimics.historical",-
results:
pretreatment bench seale.treatability studies:
Consideration was provided to bench sale treatability studies,'however, at this time there are, no:
suspected toxicants nor have Terraquest;:DWQ,or several third parties been able,".to'discern a
way to discover the,toxicant., Study of the contaminants involved:at the site will continue.
toxicitvsource.reduction strategies:
Consideration to toxicityreducti'on was given, however, .the toxicity.source.'has not: been.
identified: =Terraquest- recommends continued 'remediation of the subject contaminant_ plume
while'attention -is paid to -possible sources of the toxicity. .
To: date,=the, toxicanf,to ;C. "Dubia,remains unclear. In compliance with the SOC, Terraquest has.
considered the items set forth'in Section 2 (a),2),of.the SQC;:however, those .considerati6ns have.
not produced a 'solution to the toxicity at this time. The evaluation of toxicity will. continue...
Y g vided an :solutions..:ent';
Notethat Terraquest,and Quality are workin with theAquaticToxicolb6.'Branch and have s
_them samples, for analysis. To date, that has not pro y,

100 'E: Ruffin .Street . Mebane, North Carolina 27302
Telephone [phone] _.Facsimile (919) 563=9095
wwW.terraquestpc.co m

TERRA uest
ENVIRONMENTAL CONSULTANTS, P.C.
Inspector
Coliseum Shell System Inspection Checklist
Q=Uality Oil
jrLint
//`6 / Date of Inspection /
�h
across sep elem.
on P
before filter
after filter
Vacuum pressure
N
__ / S' r J J
z�
2CD
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
-v 5-1� IleL
added coolant "'
9
scfm .21
3 7
2 /0 ` oco gallons
Q y hours
Zo) C 1 Z— hours
OK ✓' Comments:
OK Temp
Change coolant / L'
` �Ib deg. F
OWS Condition OK Comments:
OWS transfer pump lam' �)e `ws ` JK Comments:
AST Blower Operation J OK ' Comments:
jt �!'l
AST transfer pump APw �r�sf�'re' J�e rlLG OK Comments:
Bag filters dirty? ots Some Minimal None Didn't check
Changed bag ^J IQ/ No
Changed sand / Yes /6 C_ # bags
Comments & Observations: �V�%` ��`t ��'�� J-p— `T i r`1 �` " L Cr,, �/ �[- � J J ! r � ff
Change coolant / L'
` �Ib deg. F
OWS Condition OK Comments:
OWS transfer pump lam' �)e `ws ` JK Comments:
AST Blower Operation J OK ' Comments:
jt �!'l
AST transfer pump APw �r�sf�'re' J�e rlLG OK Comments:
Bag filters dirty? ots Some Minimal None Didn't check
Changed bag ^J IQ/ No
Changed sand / Yes /6 C_ # bags
Comments & Observations: �V�%` ��`t ��'�� J-p— `T i r`1 �` " L Cr,, �/ �[- � J J ! r � ff

TERRA uest
ENVIRONMENTAL CONSVLTAN19, P.C.
Inspector OL16
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection " Z3I �_`
'acro'sspSeepp eellein.
bn LRP
before filt`perq
aftergfilter
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump 4,01kz-
scfm MR 1� /*ram
Z I q qI 4�•�`� gallons
lot t J u, hours
hours
OK v/ Comments:
OK v Temp deg. F
added coolant MD Change coolant 1VO
OWS Condition
OK
Comments:
M^JOIs�
OWS transfer pump
OK ✓
Comments:
_
IJ h q
t�r 2o•S
OK
Comments:
AST Blower Operation p,j dl;(r IS •S
AST transfer pump
OK
Comments:
Bag filters dirty? Lots Some Minimal
None
Didn't check
Changed bag Z
b/No
SGA e_ Setv,o( Cal'rvt Oyer
l
Changed sand
Yes /
# bags
Comments & Observations:
$ j�e ti.� V-V-AAl k 04-tN q. k
)LA-3 4eof a«y Z (�Ws I Ix C1j rl� ea:S- / r-P cc r-C. 0 (X /l/tS -MAI I(. -J(L/ 5 f Lk A Q \ l e c�l.c -e j C� %Sc� l t
pL0�0` f12 - Oh C1 CA r CD!- jmSSOf z 011'�-y 1 -wl� w, L,

ENVIRONMENTAL CONSULTANTS, P.G.
Inspector W
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection 1
across sep'elem.
on LRP
before filter
afterfilter:'
I�
Vacuum pressure
1
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
scfm
gallons
hours
hours
OK NZ Comments:
OK NZ Temp
ti_deg. F
added coolant
Change coolant
OWS Condition
r--' e—
OK _\Z
Comments:
OWStransfer pump ��
OK11
Comments:
AST Blower Operation
OK Y
Comments:
AST transfer pump
OKNZ
Comments:
Bag filters dirty? Lots Some Minimal
None
Didn't check
/ r
Ci``�GLwQ[jL ee��p�
Changed bag
No
kZ
Changed sand
Yes
# bags
Comments & Observations:
wmpw�
6 LA
vim. «. �r
r Cq r 4 r
C® 1
-1N re Slur
ck,- co, / nE-SSf

TERRAcmuest
ElIVIROIIl.1ElRAL CONSVLTA117S, P.C.
Inspector
Coliseum Shell System Inspection Checklist
ii°ty Lail
Date of Inspection
acrosstp elem. o before filter after filter "
vadose sparge
scfm q r'�
Totalizer Reading
gallons
hours
LRP run hours
AST blower run hours
L� d hours
Control Panel
OK Comments:
Liquid Ring Pump
OK V Temp ��
deg. F
added coolant �1 Change coolant
Iq (. i
p
G�"
SZ F�, { L4
OWS Condition
1
OK ✓ Comments:
OK_ QAL„r`-&ommen s
OWStransferpump
AST Blower Operation
OK l/ Comments:
AST transfer pump
Bag filters dirty? Lots
OK ✓ Comments:
Some Minimal None Etcheck
Changed bag
Yes/�F)
Changed sand
Ye's / t�o bags
cpb," //)� rJ
Comments Comments & Observations:
Jo-

Coliseum Shell System Inspection Checklist
TERRAnest
ENVIRONMZZI
am•-,k`
Inspector
=lity Oil
Date of Inspection
1�10A
across sep elem. on LRP before filter afterfilter
'acuum pressure
r
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
2C J! Cso scfm
xl� gallons
hours
U r
hours
OK Comments:
OK Temp J2 deg. F
added coolant /V-b
Change coolant 410
OK ✓
Comments:
OK
Comments:
OK "
Comments:
/
OK
Comments:
Bag filters dirty? Lots Some Minimal None Didn't check
Changed bag x Z�_ es No
Changed sand
Yes / (lye% # bags
Comments & Observations:
olk
C��Ai✓�Y9 ow i �( �E sTkf �-��

TERRA Uest
ENVIRONMENTAL GONSULTANTS� P.C.
InspectorUree;4-10%-
I
Coliseum Shell System Inspection Checklist
Uality Coil
• L jj /(�
Date of inspection
across sep elem.
on LRP
before filter
after filter
Vacuum pressure
vadose sparge
scfm
Totalizer Reading
I V gallons
l �[ hours
LRP run hours
AST blower run hours
20! 4 hours
Control Panel
OK Comments:
Liquid Ring Pump
OKNZ Temp
added coolant_ Change coolant
OWS Condition
OKNZ Comments:
OWS transfer pump
OK \/ Comments:
AST Blower Operation
OK\Z Comments:
AST transfer pump
OK Z Comments:
Bag filters dirty? Lots
Some Minimal None Didn't check
Changed bag
Yes/ No
Changed sand
Yes `Jo
Comments & Observations:
# bags
_deg. F

TERRA ueSt
ENVIRONMENTAL CONSULTANTS. P.C.
Inspector
across sep elem.
m
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changed sand
Comments & Observations:
Coliseum Shell System inspection Checklist
Luality Oil
Date of Inspection q
on LRP before filter after filter
scfm
gallons
hours
f-� hours
OK V f— Comments:
OK Nelle, Temp deg. F
added coolant Change coolant_
OK V Comments:
OKV Comments:
OK V Comments:
OK V--*' Comments:
Some Minimal None Didn't check
Yes No
Yes No # bags

TERRA ue�t
ENVIRONMENTAL CONSULTANTS. P.C. ►'//A �.,{r r
Inspector (-,(
Coliseum Shell System Inspection Checklist
uality tail
Date of Inspection
ve z
„&l
vadose sparge
�{
Z
scfmp
gj 'r0-0
Totalizer Reading
gallons
C J U z
LRP run hours
1
G� 6
hours
/
hours
AST blower run hours
✓
Comments:
Control Panel
OK
Temp
(� deg. F
Liquid Ring Pump �'
l S
a
OK
added coolant
/VD Change coolant
Al"
OWS Condition
OK
Comments:
OWS transfer pump
OK
Comments:
✓
AST Blower Operation)
t�
I,/S w{ v,,
a/( 0 Q
OK
/
/
Comments:
AST transfer pump
OK '
Comments:
Minimal None Didn'tchec
(
L
7
Bag filters dirty.
Lots
Some
Yes/ o
Changed bag
Changed sand
Yes /
o
/
# bags
dl' rW,0_d� oaf 4 a C-
Comments & Observations:
ICDI � 0-11l CIWII

TePJIA uest
ENVIRONMENTA CONSULTANTS. P.C.
C> YL-
Inspector 7
vadose spa rge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS 'Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty?
across sep elem.
Coliseum Shell System Inspection Checklist
q uality Oil
mllllri�olili 5--l-
Date of Inspection
AAl -
on LRP before filter after filter
CJ
Co
scfm
q00gallons
WT, hours
hours
OK Comments'.
OK Temp deg. F
added coolant A112
Change coolant
OK
Comments:
OK
Comments:
OK
Comments:
OK-
Comments:
Minimal None
Didn't check
Lots Some
,,-/' -7 rl.-Zv N.

TERRA uest
_ �IN -ft-
ENVIRONMENTAL oNSVLTANTSS/, P.C.
Inspector
Coliseum Shell System Inspection Checklist
uality Gail
Date of Inspection
across sep elem. on LRP before filter after filter
acuum pressure
vC-2
vadose sparge Zf Z
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
scfm
1, -7()/ gallons
/g/
Z 7 1 • hours
I9 z
z —7 • hours
OK Comments:
OK ✓ Temp
added coolant
OK
OWS Condition
OWS transfer pump
OK
l�
AST Blower Operation
OK
✓/
AST transfer pump
OK
Bag filters dirty? Lots
Some Minimal
None
Changed bag
5es) No
Changed sand
Yes l�
/�
kft AcC %J (6
Comments & observations:
Change coolant A0
Comments:
Comments:
Comments:
Comments:
Didn't check
deg. F
# bags (r
Cu4�G-G� 1(5T-- �4CFSCW6-- �«T� ��
cv �aOGt,� - �" Tim l i �c 6C w e.
Cry •c �� (� QL cad Ga—°c/ m w CO /Z� ci(C w( Cissu L� LJ
I �
aq�f
C'�l b '� r 15- t

TERRA Iluest,
ENVIRONMENTAL CONSULTANTS, P.C. U
Inspector
Coliseum Shell Svstern Inspection Checklist
Uality
Oil
=
$/Y
Date of Inspection
across sep elem.
on LRP
bef&efilter
after filter
7o
-7 C)
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
added coolant
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer purhp
Bag filters dirty? Lots
Changed bag
Changed sand
Comments & Observations:
scfm
009( 1, �OD gallons
C?O hours
0/
hours
OK Comments:
OK V"� Temp deg. F
Change coolant
OK- Comments:
OK- Comments:
OK- Comments:
OK Comments:
G�5 Minimal None Didn't check
a/No
Yes /&) .# bags

Coliseum Shell System Inspection Checklist
TERRA nest uaiity Oil
ENvIRONMENTALCO SVLTANTS•P.C. ,
Date of inspection �r
Inspector
across sep elem.
on LRP
bef&6 filter
after filter
Vacuum pressure
vadosesparge
scfm
z 0�
Totalizer Reading
/ / gallons
LRP run hours
C f 0/ 0, hours
AST blower run hours
5
% / Z hours
Control Panel
OK NeComments:
Liquid Ring Pump K� P `9 t t
(�
CL `i E2 �1C OK� Temp r' �/ deg. F
added coolant
AA2 Change coolant AIV
1 OWS Condition
OK v**" Comments:
OWS transfer pump
OK Comments:
AST Blower Operation
OK ✓ Comments:
/ Comments:
ASTtransferpump
OK
Bag filters dirty? Lot Some
Minimal None Didn't check
Changed bag
>( 2- 9/ No
Changed sand
Yes / Q& # bags
s
�'sL"ff �. 4"
Comments &Observations:
14,r
� ix, ' -0,,µ A%� STO-
A 12. c/
wf/ Co a, %r /rfSDY
%a r^'Z•,�- ! L�tlPa. k Lz e/
._
2 l ✓`l s'!

i -
TEi�RA nest
ENVIRONMENTAL CONSVLTANTS. P.C.
�
Inspector __66
jlort_
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection //7 /
across sep elem.
on LRP
before filter
after filter
z,. a
- 2 C,
Vacuum pressure
- c
t�A l f
vadose sparge
sdm
Totalizer Reading
gallons
LRP run hours
�-7 / 1/0 • hours
%� 3 ' hours
AST blower run hours
Control Panel
OK Comments:
Liquid Ring Pump
OK Temp 15y deg. F
added coolant
Change coolant
1 OWS Condition
/
OK " Comments:
OWS transfer pump
OK Comments:
AST Blower Operation
OK Comments:
AST transfer pump
OK v Comments:
Bag filters dirty? Lots Some
Minimal None idn't check '
Changed bag
Yes/ N9
Changed sand
Yes /® # bags
Comments & Observations:
a , &-y 01 /(—L) Vc� C

TERRA uest
ENVIRONMENTAL CONSUMANTS, P.G.
Inspector
Coliseum Shell System Inspection Checklist
Date of Inspection]
acrosssepelein:
66LRP
beforefilter` "
'afterfilteP"
Vacuum pressure
rtoe It
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
ASTtransfer pump
Bag filters dirty? Lots
Changed bag
Changed sand
7-.2 • .S— S.
c
gallons
jhours
hours
OK_v Comments:
�i OKV Temp
added coolant Change coolant_
OK JZ Comments:
OK `V/ Comments:
OK Comments:
OK\ Comments:
Some Minimal None
Ye No"
Ye No # bags
_deg. F

As m Woz, �# E Lei r%,. j
L•A•6 S•C•I•E N•C•E•5
12065 Lebanon Rd.
Mt. Juliet, Tt! 37122
1615) 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Ryan Kerins
TerraQuest Environmental Consultants BC
100 East Ruffin Street
Ifebane, NC 27302
Report Summary
Friday April 18, 2014
Report Number: L692310
Samples Receiveci: 04/OS/14
Client Project: 01195
Description: -Col .: iseum Shell
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If.you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By: gmmw
lYt
JiM4Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660; CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010 KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN502, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910 NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-029ig, IA Lab 4364, EPA- TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures. 060302, 060303, and 060304.
Page 1 of 24

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
OESC
1-800-767-5859
Fax [phone]
l•A•:a 9•C.7•e•N•C-E-S
Tax I.D. 62-0814289
=
Est. 1970
REPORT
OF ANALYSIS
Ryan Kerins
April 18,2014
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
ESC Sample $
L692310-01
Date Received April 06, 2014
Description Coliseum Shell
Site ID 472NSTON-SALE)•!, NC
Sample ID INFLUENT
Project 4 01195
Collected By Andy Wrenn
Collection Date 04/07/14 11:01
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Volatile Organics
Acetone
BDL
1000
ug/1
6200B-1997
04/18/14
2(
Acrolein
BDL
1000
ug/1
6200B-1997
04/15/14
2(
Acrylonitrile
BDL
200
ug/1
6200B-1997
04/15/14
2(
Benzene
24.
20.
ug/1
620OB-1997
04/15/14
2(
Bromobenzene
BDL
20.
ug/1
6200B-1997
04/15/14
2(
Bromodichloromethane
BDL
20.
ug/1
62008-1997
04/15/14
2(
Bromoform
BDL
20.
ug/1
6200B-1997
04/15/14
2(
Bzomomethane
BDL
100
ug/1
6200B-1997
04/15/14
2(
n-Butylbenzene
BDL
20.
ug/1
6200B-1997
04/15/14
2(
sec-Butylbenzene
BDL
20.
ug/1
620013-1997
04/15/14
2(
tert-Butylbenzene
BDL
20.
ug/1
6200B-1997
04/15/14
2(
Carbon tetrachloride
BDL
20.
ug/1
6200B-1997
04/15/14
21
Chlorobanzene
BDL
20.
ug/1
6200B-1997
04/15/14
21
Chlorodibromdmethane
BDL
BDL
20.
100
ug/1
ug/1
6200E-1997
6200E-1997
04/15/14
04/15/14
21
21
Chloroethane
Chloroform
BDL
100
ug/1
6200B-1997
04/15/14
21
Chloromethane
BDL
50.
ug/1
6200B-1997
04/15/14
21
2-Chlorotoluene
BDL
BDL
20.
20.
ug/1
ug/1
6200E-1997
6200E-1997
04/15/14
04/15/14
21
21
4-Chlorotoluene
1,2-Dibromo=3-Chloropropane
BDL
100
ug/1
6200B-1997
04/15/14
21
1,2-Dibromoethane
BDL
20.
ug/1
6200E-1997
04/15/14
21
Dibromomethane
BDL
20.
ug/l
6200E-1997
04/15/14
21
1,2-Dichlorobenzene
BDL
20.
ug/1
6200E-1997
04/15/14
21
1,3-Dichlorobenzene
BDL
BDL
20.
20.
ug/1
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
21
21
1,4-Dichlorobenzene
Dichlorodifluoromethane
BDL
100
ug/1
.
6200B-1997
04/15/14
21
1,1-Dichloroethane
BDL
BDL
20.
20.
ug/1
ug/1
620.OB-1997
620OB-1997
04/15/14
04/15/14
21
21
1,2-Dichloroethane
1,1-Dichloroethene
BDL
20.
ug/1
620OB-1997
04/15/14
21
cis-1,2-Dichloroethene
BDL
20.
ug/1
6200B-1997
04/15/14
Z
trans-1,2-Dichloroethene
BDL
20.
ug/1
6200B-1997
04/15/14
21
1,2-Dichloropropane
BDL
20.
ug/1
620OB-1997
04/15/14
2i
1,1-Dichloropropene
BDL
BDL
20.
20.
ug/1
ug/1
620DB-1997
6206E-1997
04/15/14
04/15/14
2i
2
1,3-Dichloropropane
2,2-Dichloropropane
BDL
20.
ug/1
6200B-1997
04/15/14
2
Di -isopropyl ether
37.
20.
ug/1
620OB-1997
04/15/14
2
Ethylbecizene
BDL
20.
ug/1
6200B-1997
04/15/14
2
Hexachloro-1,3-butadiene
BDL
20.
ug/1
6200E-1997
04/15/14
2
Isopropylbenzene
BDL
20.
ug/1
6200E-1997
04/15/14
2
p-Isopropyltoluene
BDL
20.
200
ug/1
ug/1
6200B-1997
6200E-1997
04/15/14
04/15/14
2
2
2-Butanone (MEK)
Methylene Chloride
BDL
BDL
100
ug/1
6200E-1997
04/15/14
2
4-Pfethyl-2-pentanone (MIRK)
BDL
200
ug/1
6200E-1997
04/15/14
2
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 2 of 24

,r
.YOUR-.L- ES-.*(`6-,CH'O10E
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street_
14ebane, NC 27302
Date Received
April 081 2014
Description
Coliseum Shell
Sample ID
INFLUENT
Collected By
Andy Wrenn
Collection Date :
04/07/14 11:01
12065 Lebanon Rd.
Mt. Juliet, T17 37122
1615) 758-5858
1-800-767-5859
Fax (615) '758-5859
Tax I.D. 62-0814289
Est. 1970
April 18,2014
ESC Sample 4 : L692310-01
Site ID WiNSTON-SALEM, NC
Project $ 01195
Parameter. Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether
1700
20.
ug/1
620OB-1997
04/15/14
20
Naphthalene
BDL
100
ug/1
6200E-1997
04/15/14
20
n-Propylbenzene
BDL
20.
ug/1
620OB-1997
04/15/14
20
Styrene
BDL
20.
ug/1
620OB-1991
04/15/14
20
1,1,1,2-Tetrachl6roethane
BDL
20.
ug/l
620OB-1997
04/15/14
20
1,1,2,2-Tetrachloroethane
BDL
20.
ug/1
620OB-1997
04/15/14
20
Tetrachloroethene
BDL
20.
ug/l
620OB-1997
04/15/14
20
Toluene
BDL
100
ug/1
6200E-1997
04/15/14
20
1,2,3-Trichlorobenzene
BDL
20.
ug/l
620OB-1997
04/15/14
20
1,2,4-Trichlorobenzene
BDL
20.
ug/1
620OB-1997
04/15/14
20
1,1,1-Trichloroethane
BDL
20.
ug/1
620OB-1997
04/15/14
20
1,1,2-Trichloroethane
BDL
20.
ug/1
620OB-1997
04/15/14
20
Trichloroethene
BDL
20.
ug/l
620OB-1997
04/15/14
20
Trichlorofluoromethane
BDL
100
ug/1
620OB-1997
04/15/14
20
1;2,3-Trichloiopropane
BDL
50.
ug/l
620OB-1997
04/15/14
20
1,2,4-Trimethylbenzene
44.
20.
ug/1
620OB-1997
04/15/14
20
1,3,5-Trimethylbenzene
BDL
20.
ug/1
620OB-1997
04/15/14
20
Vinyl chloride
BDL
20.
ug/l
620OB-1997
04/15/14
20
o-Xylene
44.
20.
ug/l
620OB-1997
04/15/14
20
msp-Xylenes
64.
40.
ug/l
6200E-1997
04/15/14
20
Surrogate Recovery
Toluene-d8
99.9
% Rec.
6200E-1997
04/15/14
20
Dibromofluoromethane
109.
% Rec.
6200E-1997
04/15/14
20
a,a,a-Trifluorotoluene
99.6
� Rec.
620OB-1997
04/15/14
20
4-Bromofluorobenzene
99.0
% Rec.
6200E-1997
04/15/14
20
SAL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 3 of 24

*ESC
)
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
REPORT
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received April 08, 2014
Description Coliseum Shell
Sample ID AFTER AST
Collected By Andy Wrenn
Collection Date : 04/07/14 10:09
Parameter Result
OF ANALYSIS
Det. Limit
Est. 1970
April 18,2014
ESC Sample # L692310-02
Site ID : WINSTON-SALEN,
Project 4 : 01195
Units Method Date
NC
Dil.
Volatile Organics
Acetone
BDL
50.
ug/l
6200E-1997
04/15/14
1
Acrolein
BDL
50.
ug/1
6200B-1997
04/15/14
1
Acrylonitrile
BDL
10.
ug/1
6200B-1997
04/15/14
1
Benzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Bromobenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Bromodichloromethane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Bromoform
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Bromomethane
BDL
5.0
ug/l
6200B-1997
04/15/14
1
n-Butylbenzene
BDL
1.0
ug/l
620013-1997
04/15/14
1
sac-Butylbenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
tort-Butylbenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Carbon tetrachloride
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Chlorobenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Chlorodibromomethane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Chlorcethane
BDL
5.0
ug/l
6200B-1997
04/15/14
1
Chloroform
BDL
5.0
ug/l
6200B-1997
04/15/14
1
Chloromethane
BDL
2.5
ug/l
6200B-1997
0,4/15/14
1
2-Chlorotoluene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
4-Chlorotoluene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,2-Dibromo-3-Chloropropane
BDL
5.0
ug/l
6200B-1997
04/15/14
1
1,2-Dibromoethane
BDL
1.0
ug/l
62008-1997
04/15/14
1
Dibromomethane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
112-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,3-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
114-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Dichlorodifluoromethane
BDL
5.0
ug/i
6200B-1997
04/15/14
1
1,1-Dichloroethane
BDL
1.0
ug/1
6200B=1997
04/15/14
1
1,2-Dichloroethane
BDL
1.0
ug/1
6200B-1997
04/15/14
1
1,1-Dichloroethene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
cis-1,2-Dichloroethene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
trans-1,2-Dichloroethene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,2-Dichloropropane
BDL
1.0
ug/1
6200B-1997
04/15/14
1
1,1-Dichloropropene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
1,3-Dichloropropane
BDL
1.0
ug/1
6200B-1997
04/15/14
1
2,2-Dichloropropane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Di -isopropyl ether
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Ethylbenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Hexachloro-1,3-butadiene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Isopropylbenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
p-Isopropyltoluene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
2-Butanone (MEK)
BDL
10.
ug/1
6200B-1997
04/15/14
1
Methylene Chloride
BDL
5.0
ug/l
6200B-1997
04/15/14
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
620013-1997
04/15/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 4 of 24

WA;13 O F•>C H 016 E:
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received April 08, 2014
Description Coliseum Shell
Sample ID AFTER AST
Collected By Andy Wrenn
Collection Date : 04/07/14 10:09
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L692310-02
Site ID : WINSTON-SALEM, NC
Project # 01195
Parameter Result Det. Limit Units Method Date Dil.
Methyl tert-butyl ether
1.6
1.0
ug/1
620OB-1997
04/15/14 1
Naphthalene
BDL
5.0
ug/1
620OB-1997
04/15/14 1
n-Propylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
Styrene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
1,1,I,2-Tetrachloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14 1
04/15/14 1
1,1,2,2-Tetrachloioethane
BDL
1.0
ug/1
620OB-1997
Tetrachloroethene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
Toluene
BDL
5.0
ug/1
620OB-2997
04/15/14 1
1;2,3-Trichlorobenzene
BDL
1.D
ug/1
620OB-1997
04/15/14 1
1,214-Trichloiobenzene
BDL
1.0
ug/l
6200E-1997
09/15/14 1
1,1,1-Trichloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14 1
1,1,2-Trichloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14 1
Trichloroethene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
Trichlorofluoromethane
BDL
5.0
ug/1
620OB-1997
04/15/14 1
1,2,3-Trichloropropane
BDL
2.5
ug/1
6200B-1997
04/15/14 1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
6200B-1997
04/15/14 1
Vinyl chloride
BDL
1.0
ug/1
620OB-1997
04/15/14 1
o-Xylene
BDL
1.0
ug/1
620DB-1997
04/15/14 1
m&p-Xylenes
BDL
2.0
ug/1
620OB-1997
04/15/14 1
Surrogate Recovery
Toluene-d8
98.8
% Rec.
620OB-1997
04/15/14 1
Dibromofluoromethane
112.
% Rec.
6200E-1997
04/15/14 1
a,a,a-Trifluorotoluene
98.6
% Rec.
620OB-1997
04/15/14 1
4-Bromofluorobenzene
102.
& Rec.
6200E-1997
04/15/14 1
BDL - Below Detection Limit
Dot. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 5 of 24

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
OESC
1-800-767-5859
Fax [phone]
L-A-41 S'C•I•E:•N•C•E-8
Tax I.D. 62-0814289
Est. 1970
REPORT
OF ANALYSIS
April
18,2019
Ryan Kerins
Terraguest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
ESC Sample Q
L692310-03
Date Received April 08, 2014
Description Coliseum Shell
Site ID WINSTON-SALEM, NC
Sample ID AFTER 1ST CARBON
Project 9 01195
Collected By Andy Wrenn
Collection Date 04/07/14 10:13
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Volatile Organics
BDL
50.
ug/1
6200B-1997
04/15/14
1
Acetone
Acrolein
BDL
50.
10.
ug/1
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
1
1
Acrylonitrile
BDL
BDL
1.0
ug/ l
6200B-1997
04/15/14
1
Benzene
BDL
1.0
ug/1
6200B-1997
04/15/19
1
Bromobenzene
Bromodichloromethane
BDL
1.0
ug/1
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
1
1
Bromoform
BDL
BDL
1.0
5.0
ug/1
6200B-1997
04/15/14
1
Bromomethane
BDL
1.0
ug/1
6200B-1997
04/15/14
1
n-Butylbenzene
BDL
1.0
ug/1
62008-1997
04/15/14
1
sec-Butylbenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
text-Butylbenzene
Carbon tetrachloride
BDL
1.0
ug/l
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
1
1
Chlorobenzene
BDL
BDL
1.0
1.0
ug/1
6200B-1997
04/15/14
1
Chlorodibromomethane
BDL
5.0
ug/1
6200s-1997
04/15/14
1
Chloroethane
BDL
5.0
ug/1
6200B-1997
04/15/14
1
Chloroform
Chloromethane
BDL
2.5
ug/1
ug/1
6200B-1997
6200B-1997
09/15/14
04/15/14
1
1
2-Chlorotoluene
BDL
BDL
1.0
1.0
ug/1
6200B-1997
04/15/19
1
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
BDL
5.0
ug/1
ug/l
6200E-1997
6200B-1997
04/15/14
04/15/14
1
1
1,2-Dibromoethane
BDL
BDL
1.0
1.0
ug/1
6200B-1997
04/15/14
1
Dibromomethane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,2-Diohlorobenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
1,3-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
BDL
5.0
ug/1
ug/1
6200B-1997
620OB-1997
04/15/14
04/15/14
1
1
1,1-Dichloroethane
BDL
BDL
1.0
1.0
ug/1
6200B-1997
04/15/14
1
1,2-Dichloroethane
BDL
1.0
ug/1
6200B-1997
04/15/14
1
1,1-Dichloroethene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
cis=1,2-Dichloroethene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
trans-1,2-Dichloroethene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,2-Dichloropropane
BDL
1.0
ug/1
6200B-1997
09/15/19
1
1,1-Dichloropropene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,3-Dichloropropane
BDL
1.0
ug/l
6200B-1997
04/15/14
1
2,2-Dichloropropane
Di -isopropyl ether
BDL
1.0
ug/1
ug/1
6200B-1997
620OB-1997
04/15/24
04/15/14
1
1
Ethylbenzene
Hexachloro-1,3-butadiene
BDL
BDL
1.0
1.0
1.0
ug/1
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
1
1
Isopropylbenzene
BDL
BDL
1.0
ug/1
620DB-1997
04/15/14
1
p-Isopropyltoluena
(MEK)
BDL
10.
ug/1
6200B-9/15/14
1997
0
1
2-Butanone
Methylene Chloride
BDL
5.0
ug/l
ug/1
6200B-1997
6200B-1997
04/15/14
04/15/14
1
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 6 0£ 24

U.UR.LAgO 06F=C`Ii 010E
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received
April 08, 2014
Description
Coliseum Shell
Sample ID
AFTER 1ST CARBON
Collected By
Andy Wrenn
Collection Date
04/07/14 10:13
12065 Lebanon Rd.
Ht. Juliet, Tit 37122
[phone]
1-800-767-5859
Fax [phone]
Tax Y.D. 62-0814289
Est. 1970
April 18,2014
ESC Sample f : L692310-03
Site ID WINSTON-SALEM, NC
Project # 01195
Parameter Result Det. Limit Units Method Date . Dil.
Methyl tert-butyl ether
BDL
1.0
5.0
ug/l
ug/l
620OB-1997
6200B-1997
04/15/14 1
04/15/14 1
Naphthalene
n-Propylbenzene
BDL
BDL
1.0
ug/l
620013-1997
04/15/14 1
Styrene
BDL
1.0
ug/l
6200B-1997
04/15/14 1
1,1,1,2-Tetrachloroethane
BDL
1.0
1.0
ug/1
ug/1
620OB-1997
620OB-1997
04/15/14 1
04/15/14 1
1,1,2,2-Tetrachloroethane
Tetrachloroethene
BDL
BDL
1.0
ug/l
620OB-1997
04/15/14 1
Toluene
BDL
5.0
ug/l
6200B.-1997
04/15/14 1
1,2,3-Trichlorobenzene
BDL
BDL
1.0
1.0
ug/1
ug/1
620OB-1997
620OB-1997
04/15/14 1
04/15/14 1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
BDL
1.0
ug/l
620OB-1997
04/15/14 1
1,1,2-Trichloroethane
BDL
1.0
1.0
ug/l
ug/1
620OB-1997
620OB-1997
04/15/14 1
04/15/14 1
Trichloroethene
Trichlorofluoromethane
BDL
BDL
5.0
ug/1
620OB=1997
04/15/14 1
1,2,3-Trichloropropane
BDL
2.5
1.0
ug/1
ug/1
6200B-1997
6200B=1997
04/15/14 1
04/15/14 1
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
BDL
BDL
1.0
ug/1
62003-1997
04/15/14 1
Vinyl chloride
BDL
1.0
ug/1
620OB-1997
04/15/14 1
o-Xylene
BDL
1.0
ug/1
620OB-1997
04/15/14 1
m&p-Xylenes
BDL
2.0
ug/l
620OB-1997
04/15/14 1
Surrogate Recovery
Toluene-d8
99.8
% Rec.
6200E-1997
04/15/14 1
Dib;omofluoromethane
109.
97.1
% Rec.
% Rec.
6200E-1997
620OB-1997
04/15/14 1
04/15/14 1
a,a,a-Trifluorotoluene
4-Bromofluorobenzene
101.
% Rec.
620OB-1997
04/15/14 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 7 of 24

s-
YO t7 R�L'11.8`D•'F •CH O 1 C,E'
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, T11 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18, 2014
ESC Sample f : L692310-04
Date Received April OB, 2014
Description Coliseum Shell
Site
ID WINSTON-SALEM,
NC
Sample ID EFFLUENT
Project # 01195
Collected By Andy Wrenn
Collection Date 04/07/14 11:05
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
NOEL - C.dubia
12.5
%
1002.0
04/08/14
1
ALK
46000
20000
ug/1
310.2
04/10/14
1
Hardness, Total (mg/L as CaCO3)
45000
30000
ug/1
130.1
04/11/14
1
Lead
BDL
5.0
ug/1
6010C
04/11/14
1
volatile Organics
Acetone
BDL
50.
ug/l
620OB-1997
04/15/14
1
Acrolein
BDL
50.
ug/l
620OB-1997
04/15/14
1
Acrylonitrile
BDL
10.
ug/1
620OB-1997
04/15/14
1
Benzene
BDL
1.0
ug/1
620OB-1997'
04/15/14
1
Bromobenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Bromodichloromethane
BDL
1.0
ug/1
620013-1997
04/15/14
1
Bromoform
BDL
1.0
ug/1
620OB-1997
04/15/16
1
Bromomethane
BDL
5.0
ug/1
6200E-1997
04/15/14
1
n-Butylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
sec-Butylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
text-Butylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Carbon tetrachloride
BDL
1.0
ug/1
62DOB-1997
04/15/14
1
Chlorobenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Chlorodibromomethane
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Chloroethane
BDL
5.0
ug/1
620OB-1997
04/15/14
1
Chloroform
BDL
5.0
ug/1
620OB-1997
04/15/14
1
Chloromethane
BDL
2.5
ug/1
620OB-1997
04/15/14
1
2-Chlorotoluene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
4-Chlorotoluene
BDL
BDL
1.0
5.0
ug/1
ug/1
620OB-1997
620OB-1997
04/15/14
04/15/14
1
1
1,2-Dibromo-3-Chloropropane
1,2-Dibxomoethane
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Dibromomethane
BDL
1.0
ug/1
62DOB-1997
04/15/14
1
1,2-Dichlorobenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,3-Dichlorobenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,4-Dichlorobenzene
BDL
1.0
5.0
ug/1
ug/1
620OB-1997
620OB-1997
04/15/14
04/15/14
1
1
Dichlorodifluoromethane
1,1-Dichloroethane
BDL
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,2-Dichloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,1-Dichloroethene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
cis-1,2-Dichloroethene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
trans-1,2-Dichloroethene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,2-Dichloropropane
BDL
1.0
1.0
ug/1
ug/1
620OB-1997
620OB-1997
04/15/14
04/15/14
1
1
1,1-Dichloropropane
1,3-Dichloropropane
BDL
BDL
1.0
ug/1
620OB-1997
04/15/14
1
2,2-Dichloropropane
BDL
1.0
ug/1
6200E-1997
04/15/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 8 of 24

•4
YO Lt R'" fiA' B • 'G. F'.0 H O 1 C E
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TH 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18, 2014
ESC Sample 4 : L692310-04
Date Received April 08, 2014
Description Coliseum Shell
Site
ID WINSTON-SALEM;
NC
Sample ID EFFLUENT
Project 4 01195
Collected By Andy .Wrenn
Collection Date : 04/07/14 11:05
Parameter
Result
Det. Limit
Units
Method
Date .
Dil.
Di -isopropyl ether
BDL
1.0
ug/l
620OB-1597
04/15/14
1
Ethylbenzene
BDL
1.0
ug/1
6200B-1997
04/15/14
1
Hexachloro=l,3-butadiene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
Isopropylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
p-Isopropyltoluene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
2-Butanone (MEK)
BDL
10.
ug/l
620OB-1997
04/15/14
1
Methylene Chloride
BDL
5.0
ug/l
620OB-1997
04/15/14
1
4-Methyl-2-pentanone_ (MIBK)
BDL
10.
ug/1
620OB-1997
04/15/14
1
Methyl tert-butyl ether
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Naphthalene
BDL
5.0
ug/1
620OD-1997
04/15/14
1
n-Propylbenzene
BDL
1.0
ug/l
620OB-1997
04/15/19
1
Styrene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/l
620OB-1997
04/15/14
1
Tetrachloroethene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
Toluene
BDL
5.0
ug/1
620OB-1997
04/15/14
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
1,1,1-Trichloroethane
BDL
1.0
ug/l
620OB-1997
04/15/14
1
1,1,2=Trichloroethane
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Trichloroethene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
Trichlorofluoromethane
BDL
5.0
ug/1
620OB-1997
04/15/14
1
1,2,3-Trichloropropane
BDL
2.5
ug/1
620OB-1997
04/15/14
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
6200B-1997
04/15/14
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
620OB-1997
04/15/14
1
Vinyl chloride
BDL
1.0
ug/l
620OB-1997
04/15/14
1
o-Xylene
BDL
1.0
ug/l
620OB-1997
04/15/14
1
m&p-Xylenes
BDL
2.0
ug/l
6200E-1997
04/15/14
1
Surrogate Recovery
Toluene-d6
97.3
% Rec.
6200E-1997
04/15/14
1
Dibromofluorornethane
110.
% Rec.
6200E-1997
04/15/14
1
a,a,a-Trifluorotoluene
100.
% Rec.
620OB-1997
04/15/14
1
4-Bromofluorobenzene
102.
% Rec.
620OB-1997
04/15/14
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 M 25 Revised: 04/18/14 08:44
Page 9 of 24

}
.YG0R°L'796"C. F•`C H 0 1 C E.
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
April 16, 2014
ESC Sample 8 : L692310-05
Date Received
April 08, 2014
Description
Coliseum Shell
Site
ID 19INSTON-SALEM,
NC
Sample ID
LRP STACK
Project #
01195
Collected By
Andy Wrenn
Collection Date
04/07/14 10:52
Parameter
Casa
1401 Wght
RDL1
RDL2
ppbv
uq/m3
Method
Date
Dil.
Benzene
71-43-2
78.1
92.1
16.0
160
51.0
600
1200
8200
3800
31000
M18-Mod
MIS -Mod
04/11/14
04/12/14
80
800
Toluene
Ethylbenzene
108-88-3
100-41-4
106
16.0
69.0
320
1400
1418-Mod
04/11/14
04/11/14
80
80
m&p-Xylene
1330-20-7
95-47-6
106
106
32.0
16.0
140.
69.0
830
300
3600
1300
M18-14od
1416-Mod
04/11/14
80
o-Xylene
Methyl tart -butyl
ether
1634-04-4
88.1
160.
580.
15000
54000
120000
1418-Mod
M18-Mod
04/12/14
04/11/14
800
80
TPH (GC/1-IS) Low Fraction
8006-61-9
101
4000
17000
28000
98.2
% Rec.
M18-Mod
04/11/14
80
1,4-Bromofluorobenzene
460-00-4
RDL1 - ppbv , RDL2 - ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 10 of 24

J,M -a
YOUR `L"AB'=:C "F•7C Ha 1 CEO
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax (61S) 758-5859
Tax I.D. 62-8814289
Est. 1970
April 18,2014
ESC Sample $ : L692310-66
Date Received April 08, 2014
Description Coliseum Shell
Site ID WINSTON-SALEbi, NC
Sample ID EFFLUENT
Project � 01195
Collected By Andy Wrenn
Collection Date 04/07/14 11:05
Parameter Result Det. Limit Units Method Date Dil.
Suspended Solids BDL 2.5 mg/l 2540 D-2011 04/10/14 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 11 of 24

YGLR-i:a-.
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18,2014
ESC Sample $ : L692310-07
Date Received April 10, 2014
Description Coliseum Shell
Site ID VIINSTQN-SALEbf, NC
Sample ID EFFLUENT
Project $ s 01195
Collected By Andy Wrenn
Collection Date 04/09/14 14:28
Parameter Result Det. Limit Units Method Date Dil,
ALK 49200 20000 ug/1 310.2 04/15/14 1
Hardness, Total (mg/L as CaCO3) 49000 30000 ug/1 130.1 04/14/14 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/17/14 16:25 Revised: 04/18/14 08:44
Page 12 of 24

Attachment A
List of Analytes with QC Qualifiers
Sample Work. Sample Run
Number Group Type Analyte ID Qualifier
L692310-01 NG716142 SAMP 1,2,4-Trimethylbenzene R2904832 V3
WG716142 SAMP o-Xylene R2904832 V3
lIG716142 SAMP m&p-Xylenes R2904832 V3
Page 13 of 24

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
V3 (ESC) - Additional QC Info: The internal standard exhibited poor recovery
due to sample matrix interference. The analytical results will be biased
high. BDL results will be unaffected.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 14 of 24

Summary of Remarks For Samples Printed
04/18/14 at 08:44:11
TSR Signing Reports: 350
R5 - Desired TAT
No emails. Report all air samples in ppb by vol & acetone at 50ppb. Report TSS in mg/L.
Sample: L692310-01 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/15/14 00:00 APT Date: 04/17/14 16:25
Sample: L692310-02 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/15/14 00:00 RPT Date: 04/17/14 16:25
Sample: L692310-03 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/15/14 00:00 RPT Date: 04/11/14 16:25
Sample: L692310.-04 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/16/14 00:00 RPT Date: 04/11/14 16:25
Sample: L692310-05 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/15/14 00:00 RPT Date: 04/17/14 16:25
Sample: L692310706 Account: TURENV Received: 04/08/14 07:00 Due Date: 04/15/14 00:00 RPT Date: 04/17/14 16:25
Use TSS container from -04
Sample: L692310-07 Account: TURENV Received: 04/10/14 09:45 Due Date: 04/17/14 00:00 RPT Date: 04/17/14 16:25

12065 Lebanon Rd.
Ift. Juliet, T11 37122
[phone]
1-800-767-5859
OESC Fax [phone]
L-A- 13 Tax I.D. 62-0814289
02.111TUIPTIME Est. 1970
TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street Quality Assurance Report
Level II
Mebane, 11C 27302 April 18, 2014
L692310
Analyte
Result units
% Rae Limit Batch Date Analyzed
—3) :5
Benzene
< .2 ppb
WG715458 04/10/14 12:05
OL_4' .05
FnT,p-Xylene
< .4 ppb
WG715450 04/10/14 12:05
o-Xylene
< .2 ppb.
WG715458 04/10/14 1205
1,4-Bromofluozobenzene
t Rec.
92.90 60-140 W015458 04/10/14 12:05
. .. ... .....
Vet�l tert-butyl ether.
< .2 ppb
WG715684 04/11/14 14:27
7
L 4.27
1,4-Bromofluorobenzene
t Rec.
103.0 60-140 WG715684 04/11/14 14:27
ard.-12:39
.B
Hardness, Total (mg/L as CaCO3)
< 30 . ...... . ..
Y.G715798 04/14/14 15:01
. . . .. .......... .
..7
1,1,1,2-Tetrachloroothane
< .001 Mg/l
NG716142 04/15/14 11:57
1,1,1-Trichloroethane
< .001 mg/l
NG716142 04/15/1 ' 4 11:57
., NX "MI
3 X.
.... .... ..
2 q L
1:57
2,1,2-Trichloroothane
< .001 mg/1
5-1
1,1-Dichloroothane
< .001
WG716142 04/15/14 11:57
- al:57
1,1-Dichloropropene
< .001 mg/1
VIG116142 04/15/14 11:57
1,2,3-Trichlorobenzone
< .001 mg/1
WG716142 04/15/14 11:57
7.192;::04 1 : 5 7
1,2,4-Trichlorobenzone
< .001 mg/1
WG716142 04115/14 11:57
ld,4-Trimethylbenzene
< .001 mg/l
VG71614204115/14 11:57
T 117 1:57
1,2-Dibromoethane
DOI mg/1
WG716142 04/15/14 11:57
2-Dic,lorobenzene
< .001 mg/1
WG716142 04/15/14 11:57
p T7 I!
... ... ..
1,2-Dichloropxopane
< .001
WG716142 04/15/14 11:57
1,3i5-Trimethylbenzene
.4 .001 mg/l
WG716142 04/15/14 11:57
0
7
1,3-Dichloropropane
< .001 mg/1
NG716142 04/15/14 11:57
1(4-Dichlorobenzene
< .001 mg/1
WG716142 04115114 11:57
2-Butanone (MEK)
.01 mg/1
Tis/14 11:57
WG716142 04 15
2-Chlorotoluene
< .001 mg/1
WG716142 04/15/14 11:57
Z.R-
19 Z�
-- . - 1'. - * ., '�1:57
T.
4-Methyl-2-pentanone (MIBK)
< .01
WG716142 04/15/14 11;57
Acetone
< .05 mg/1
WG716142 04/15/14 11;57
-D�7
Uj� T4­11:57
—VOR
Ylli57
Benzene
mg/1
WGY716192 04/15/14
Bromobenzone
< .001 m5l1
WG716142 C4/I5/14 11:57
RML —
Bromoform
< DOI mg/I
WG716142 04/15/14 11:57
�romomathane
< .005
WG716142 04/15114 11:57
77i.
-57
Chlorobenzene
< .001 mg/l
WG716142 04/15/14 11:57
• Performance of this Analyto is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 15 of 24

TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street
Mebane, TIC 27302
QualityAssurance Report
Level II
L692310
12065 Lebanon Rd.
Mt. Juliet, TH 37122
[phone].
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est, 1970
April 18, 2014
[�x�aliaY�tdxy 92�nIc`.
Analyte Result Units 6 Rea Limit" Batch Date Analyzed
-_ - - /1 _._---------{- WG716142 04/15/14 11:57,
-pra 1be51z_en�--'="--- -- - -
,.001
y ram_
=_< .09i,_ ter..- ,�Yn`'•1'� _.:c,..-�-��`=� =���
- 1 • 7
=<�G7161A2n09"a6%1"9�1 .5
by d�.....:...`.�--
Naphthalene
< .005 mg/1
WG716142 04/15/14 11:57
o Xylene
1
.00mg/1
5/1
WG716142 09/1 9 11:57
- _
..sue-- ._
.Iso za �koluene. _--..�,_ ��..�<�.:_.�.�..-=:"=er.-,k�;0o1�:=
P.Y
�c - _ - - - _ --
,:�� - = -
- - xs, %2j: ..�.-�>_" - �-�-;t:=- -- -
'hl9T.:�,._,.-`-.--<�--c-f�:=_=s-;_._�=_._._._a�.zt-�°.Z.:K::-;av;°--<wG...
-
T 2:='0 1 .1'4?-11:57
..
1' 4' / _
-~WG716142
.W-�p —_::._.�.__r-=.:--=-----._,_.r...-�..,__:::_,:�,,.
sec-Butylbenzene
_ _
< .001 mg/1
04/15/114 11:57
Serene
< .001 mg/1
WG716142 04/15/14 11:57
_ - —w'4^.t
-"e"But - - -
C 1lbenzeha`'x,._
�r """i�'-��-�=�•-- - - - - - �ry;�_'hGf
-
61'42`�04/: 5%X_4`11:57
.x_ -..,.�
Tetrachloroethene
_
< .001 mg/1
WG716142 04/15/14 11:57
Toluene
< .005 mg/1
WG716142 04/15/14 11:57
��:�'
_ P'-.=--,-..,,., _�_-.-..,-,-.-.�.:...,,
�.�:•: >.=T �� - -- - - - - - �:�.�.-r
:-...r-..._ _ ._ _,-.,-�:,.,.gC•.-�=.._..:.-.�_..r...-_:.,: �s�..:.._.-,� .;:ter...,,•. _,.�.-,�_..
- e'.:WG716292=0�'15/ 9�11:57
., ,��.-
Trichloroethene
_
<':001 mg/l
WG716142 04/15/14 11:57
Trichloiofluoromethane
< .005 mg/1
NG716142 04/15/14 11:57
1-c tolde; - hG7 6' :47�57
_vin
4-Bremofluorobenzene
Rec. 100.0 71-126
WG716142 04/15/14 11:57
Dibromofluoromethane
Rec. 110.0 78.3-121
NG716142 04/15/14 11:57
,215�•191:579o1yn� 1
a,a,a-Trifluorotoluene
% Rec. 98.20 85-114
WG716142 04/15/14 11:57
.Y7.5�.'O-�`_,K.}.y-s.:'_a`2� %'..� _ _ _ - _ 1 _ _ _�5' �d'=°I2 : 92
�__ „-�:�si' �,;::a�, .,: :.,.__..-... ... ;=- .:..>..-...�_, .. ...,•,._. „9;.- ....,:��c_. _.___.. -`=.``fizz-;-s.- ..-_,_._..�, - �s,.
4-Bromofluorobenzene % Rec. 98.10 71-126 WG716143 04/15/14 12:42
Dibromofluoromethane 8 Rec. 105.0 78.3-121 WG716143 04/15/14. 12:42
_ __ 1 2.42
�10 .:Lrt -=�� .f i _ �s6s 7.1:6J,L:-O_!- 4,-
..........
a,a,a-Trifluorotoluene % Rec. 94:00 85-114 WG716143 04/15/14 12:42
%„Dqp�"��dtig
Analyte Units Result Duplicate RPD Limit Ref Samp Batch
320=� 5163
_
Suspended Solids mg/1 32.8^ 33.6 2.41 5 L692336-01 NG715163
- - 6 .;:.�:=•�: - �?2 - �L 9219 'Ah>`-=�-.WG 1562 �-90;0_:, 0:_ 7., 7 Hardness, Total.(mg/L as CaCO3) mg/1 120. 122. 1.65 20 L692386-01 WG715460
�5460
,
,.---_._4- �..4,_.4.:.,...:...�..._.s.,-;.,�,,.r._:.•_cltaeJ_.---..._� .___..— __ _.-;;:�e:..,w_.._..__...-•"=`=,.`'i-_--::_-._'... ...........
:_.._.....:._�.._—'-----..:..-:_._._�_
Hardness, Total (mg/L as CaCO3) zq VT '!�2/1 # 78.0 YYti> 90.0;4 14.3t : _ 20 L692563-002 WG715798
=.=117.s-__.ts-ti 2 53 > ,.. s 2p :_-L692272n03s WG5798
+ Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytea with QC Qualifiers.
Page 16 of 24

Teri:aQuest Environmental Consultants PC
Ryan Kerins,
100 East Ruffin Street
Mebane, RC 27302
Quality Assurance Report
Level II
L692310
12065 Lebanon Rd.
Mt. Juliet, TIT 37122
[phone]
1=800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18, 2014
Analyte
is+ LabgYatary Cbntrol<<§atnple_j
units Ifnown Val' Result
Pk Rae Limit.
Batch
Benzene
b _...__3.75 3.26
_., Ya:;a� •.�__,_,__,.__
86.9 70 ^130
as'ra,::_..:,....:._t.__,-....:.t o=i30``c:
WG715458
._._.:`.F7G715958
.5 0.01
1,9-eromofluorobenzehe
- ,......-.____,.__..mac..
0 --.
ear- - ....:...............,....-.......--_..
75 3.62 9b 3
,ethyl tert-butyl ether p.G7i5684
- 6.5 70 130 W
>75 va. v
106.0 60-190 WG715689
1,4-Bromofluorobenzene��
5460
$ardness Total (mg/L as CaCO3) mq/1 200 201. _ __- = 798
101. 85-115 WGy�
._.. - 192
- - - DWG 6
- - ry0.024>6rK j98.4 74.2-12
1,1,1,2-Tetrachloroethane mg/1 025 0.0234 93.5 73.2-123 WG716142
1,1 1-Trichlorcethane m4�1u_ _ _ _ _ _ _ _6142
- 1=a ` _. .
?EZi�,.�STeCYachlcxo �a(!._.:,..,..:.,-., :-......, �-' - 77.7-iisl WG716142
1,1,2-Trichloroethane mg/1 025 0.0239 �95.5
1 chIsroethane mg/1 _ .025 _ 0.0232 93.0_ 70.7-126 _ WG716142
, - _ _ _ - ;;^r--•-- -- -- -- - 67:8-129'< _ - '-WG�6142
39'- 5 _ ,L-:..x�., ..mot R.,...,
.' :z.: .-...r._a, ...,.e-r..
chlozoet,one..:�;T_:�.,...:.,....,-.,:-_.�.:+:-:>"�<-_:.,_�..,..; ...�:w.,n,. , .::
0.0217 87.0 73.1-125 WG716142
1,1-Dichloropropene mg/1 .025 64.9-135 WG716142
1,2, 3-Trichlorobenzene 0.0218 111. _
.._._.__.,.�..-..c..,':i71'3'B :-1.21•• r,"s,.,`WG716142
1,2,4-Trichlorobenzene
lbanzene
mg 1
m /1 .025 0.0233 931
-
7$u123
WG716142
1,2, 4-Trimath
..�.•�-. - -- - --=:°'4"- - - - i�s«- - - =6 �.`1-'2'=='--`r►1G7�6192
i,2-Dibromoethane
mg/1 .025 0.0257
78.4-117
NGIL6142
103.
mg/1 .025 0.0257 103.
_ _78.4-124
- WG716142
1,2=Dichlorobenzene i1�29'+�-=_
�Y2�b�chloYoeth3n�;7,�-;;;a:,v _::.-'<: •. =..::r. .•... -~` 76.5-119~�
2•:WG716192
WG716142
mg/1 .025 0.0231 92.3
1,2-Dichloropropane
tag/1 025 0.0241
_.,_�5.6;124
WG716142
1 3,5-Trimethylbenzena
ter_____ .. ..
_ `.-... ;96.5
.._. ,:,-:,,.,_<, •,...�,.-. - --- 0
_."._,-ti025 :__,,_-:;:._ ae:^ OF025.0: _; y'_a.,:.z_J.;_ s :c_ _ti':;.
=-T-tly8=128s'-6192
=" --
1�3-Uichloren_�epei-,^,_s'?:-.c:r=c_::.t2:a.__==_m9f?=<.s: %:•s_;;u----......_.. ---
0.0221 88.5
77.4-117
WG716142
1,3-Dichloropzopane
mg/1 .025
mg/1 0.0241 96.4
142
1 4-Dichlorobenzene
'
_025
..:... .. 47133:t
:.,._-_.._..-........_.__ .......:.. - -
F)G71 192
2-eutanone (AIEK)
.094
m9/1 .125 0.0979 77.9
93.0
55-149
74.7-122
YiG716142
WG716142
2-Chlorotoluene
mg/1„ .025 N :_ 0.0232. ... _
.r-,: ,. �_t=c:c:,_,�,91v3.,r-:.E.c"^`=" :-:: 7.7: 5�,, 2 Q';� �, :r :.._.... 142
/,; .-...w..<w...
.,........._:_.._ ..
(MIBK) mg%1 .125
70. -133
HG716142
Ncetone
anone
cetone mg/1 .125 0.0979 77.9 _ :_..;._.35.6Y163--- WG71614
- -- - -- - - -- _-- - _ - _ _ �2••130:<„==a 6142
AcYylonit'til:e.:'�z.� _w;->`a.;-; :;�.:_ _.�:_••;:`:'-�;:.;:;=_,:: 9_=::_':=;._-:..._. ---- 0.021786.7 74.8-121 14G716192
Benzene mg/1 025 _
m /1 .025 :..,.,.,0 0229.._..:....._4-.:..: _,;;..;89 7 •::, <a,:,:;: 77
Bzomobenzene y g,...,«,.._.:..--<..... - _
.5 116 WG716142
_ - 3'3'6142
0 1 ro ethdnees; _ _._,...._...:....:.-...... - _ _
Bromoform mq/1 .025 0.0235 96.2 49.9-162 WG716142
Bromomethane m /1 .025 0.0215 86.2 99.9-162 WG716142
- - - --,.>:..r;��.;,_:a��70:2x�23<-"'.:-'�S��1G�16142
Chlorobenzene mg/1 .025 0.0227 90.7 78.1119 WG7
16142
Chlorodibromomethane mg .025 0.0230 92.2 74-121 WG716142
Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 17 of 24
Page 17 of 24

12065 Lebanon Rd.
Mt. Juliet, TN 37222
[phone]
1-800-767-5859.
OESC. Fax [phone]
L-A•13 0-c•I-M•N•.C-M-S
Tax I.D. 62-0814289
Est. 1970
TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street Quality Assurance Report
Level It
Vebane, NC 27302 April 18, 2014
L692310
F. Lhboras%XyCont'co1;Sainple
Analyte Units Known Val Result
4 Ree
Limit Batch
Cho a e._.,._:,_:,;,. ..,:..,..,_x.,..-;-,.,•_. •....:_;':02 -'^"` ,-c`�w -•• -6192
1 koe� n .._.....: .:.. ..._ �..,:::_,z>.:.... •::,>: � ,,-_. 5:�:.>.�U., it`"=`_0..0290�::-'-_- - --::.__�_-._.__,
Chloroform mg/1 .025 0.0243
97.0
76-121 UG716142
Chloromethane mg/l .025 0.0205=
82.1s
61.5-129 WG716142
. ^T ; „J _
o ^`4-
.z �"�•- - .�hG716142
6i �_ ,:..:7..
Di -isopropyl ether mg/1 .025 0.0215
86.1
65.6-132 NG716142
Di_bromomethane mq/1 .025 0.0245
97.9
79.5-118 _' NG116142
_
ichloYodifl't oin9�h'age2-� '�=i�':'� - /6142
n
BEhylbenzeneu- mg/1 .025 v 0.0222
88.7-
78.6-122 WG716142
Hexachlore-1,3-butadiene mg/1 .025 0.0248
99.4
64.7-129 NG716142
a250_` =96142
Iso ro lh��ene- _ - - ;i: _ ==°lag �:.- - -- 30�. -959r_._�_��__._=...-
- �89.2...-78.8-121
map-Xylenes mg/l .05 0.0446
WG716142
!:ethyl tent -butyl ether Mg/1 .025 0.0264
.106.
71.2-126 WG716142
. sv, Y 2� w �u0:0249
.-.025--
1614z
n-Butylbenzene mg/102b
97.6
97.b
76.2-126 WG716142
n-Propylbenzene mq/1 .025 _
90.0_
-
78:2-122- NG716142
�4 y;y _ r _ _0.6225 _ y a
--....... - - _ _ _ - = g>W'-4 128 6:' G736192
a hEha'T' ts� = - w989'S,: 4 N 6 r',�
�..� ._tip._. _ .:. ,>. .N...,:,zc:.=...,,..-:-..., a--.'__-'__}>z+. ..< ... :..> ._�,. �:E•,..:...-� .. -... _
o-Xylene mg/1 .025 0.0235
93.8
77.6-122 WG716142
a=Zsooroovltoluene ma/l .025 0.0240
99.1
74-131 WG716142
Styrene mg/1 .025 0.0225 90.2 au.4-12b nG/1bviz
tart-ButlbenzeneV mg/1 .025. 0.0238 95.0 75.3-126 WG716142
= v-; �.�•:- r �: ..�� _- - - =;� ysii`-� - _ "'`�'; ��;r'= - - '���`s�%',. ' - _ " 2=6=Z2 � =�:'= h�'GT16192
Toluene ma/l -.025 l 0.0215 66.2 79.7-216 UG716142
2-Dichloreethene m(j/1 -.025 0.0219 87.5 12.6-121 WG716142
--- - o- --- - - _ - -_ /:�"='�� -- :025'n„��• _i�'ra^',T•,'.,a':^,:-<0�0
ofluoromethane --" g/l .025 ' 0.0210 h 84.0 �63.5-135 WG716142
I ride ma/1 .025 0.0224 89.7 65.9-128 WG716142
Dibromofluoromethane 108.0 76.3-121 WG716142
Toluene-0
`.. 1 ... ...: ,
98.30 88.5-111 WG716142
ar:ar_d�TY� uo ..9..to�-Uelle', - - =.z,A� - -- - - - . w. - ,: -E�:._:r=.m,-_�___>�:.--__�...���.:.z.��sx�6142
Acrolein mcr/1 .125 0,126 102. 10-190 NG716143
Toluene-d8 101.0 88.5-111 WG716143
0 - - - - - _ - •--�'���- - - --- -- - - �95�60�-. _ 5r" '14'�=�_r=;?'c=' 'Gi 6143 .agh-Tlifluoratoluene.. ...,-. <.r:..::_ ....r,_,,..m._,_,.._ = - -- _-= •.. : ��'�:=,m;a,.:;? - - --------- - 'T.$...7:- -° - - �'`- -
�; J.aAara,�,i?xy; CsAE;�g�'4S�P1sG�Pl�Cate
Analvte Units Result Per 8Rec Limit .RPDLimit Batch
t'8- - _ - -- - - - - --
- 'L'
- --- - - - -_ -- - - - - - - 715 � .,
.,: �p.::_.._... _...._,-.,-n✓r_._:_.__ „_-i'-4-:..,. �g:A:�;:d:.�.�..5...:-.-_t...._....-_.-'_..::�a:c..a=.. =,L,v .:zV.._.__' ._.:... 5163
_
�wG7i5684
th �:-, ertR t 1'?et Y.r• - ::3.:55: - 0 - 2.::' __._.. ......_.
Toluene ~ .- ppb 3.64 3.66 97.0 70-130 0.480 25 WG715684
1,4-Bromofluorobenzene 104.0 60-140 110715684
Hardness, Total (mg/L as CaCO3) mg/l 207. 207. Y104. 85-115 0.0 20 W0715460
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 18 of 24

12065 Lebanon Rd.
Mt. Juliet,
uliet, T11 31122
[phone]
1-800-767-5859
OESC Fax [phone]
L-A-P Tax I.D. 62-0814289
Est. 1970
TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street Quality Assurance Report
Level II
Mebane, NC 27302 April 18, 2014
L692310
Anal to
*01".S
Units Result Ref %Rec Limit RPD Limit Batch
Coji 5798
1,1,1,2-Tetrachloroethane W,/1 0.0237 0.0246 95.0 74.2-124 3:81 20 WG716142
6142
231 0.0231 92.0 70.7-122 0.100 20 WG716142
1;1,2,2-Tetrachloroethane
:1,1,2-Tricbloroethane
mg/10.0235 0.0239 94.0 77.7-118 1.76 20 WG716142
. .........
i.t,20. �ZW 716142
�0-232,Fd NffM�:;�
8.43 20 WG716142
I,I-Dichloroethene
mg/1 0.0219 0.0239 67.8-129
63.0 73.1-125 5.14 20 WG716142
6142
95.0 3.51 20
5.02 20 NG716142
108. 69.7--136
-- I F- Zdd 6142 . . . . . . . . . . . . .
93.0 65.4-128 4.09 20 WG716142
76.6-121 0.600 20 WG716142
93.0
U42
..........
oroo ane,
mg/l 0.0234 68.8-124 0.0900 20 WG716142
90.0 76.5-119 2.92 20 WG716142
i * , 7 -k- -RI Z 6142
qgj 4 Q,
. , - _-- �-.R,--
_w�
P. .11 -. - i:5
9 . 7.0 10.8-128 2.08 20 WG716142
90.0 77.4-117 1.57 20 JIG716142
6142
92.0 62.4-133 5.56 20 WG716142
55-149 O.B20 20 WG716142
77.0
. . . . . . . . . . . . . . 142
. . . . . . . . . . .... .........
.......... ....
. . . .
mg/1 0.0229 0.0228 92.0 77.5-120 0.450 20 WG716142
4-Methyl-2-pentanone (HIBK)
mg/1 0.111 0.108 89.0 70.5-133 2.75 20 WG716142
6142
0974 ....... .... .. ------
0.118 93.0 55.2-130 1.22 20 WG716142
Acrylonitrile
Benzene
-,- '--'
Mg/l 0.117
-_- mg/l 0.0211 0.0217 84.0 74.8-121 2.75 20 W0716142
,
pi %, 0=43 ;r< _A... :=;;T$==:_r:':.: ._.
6
0.0233 90.0 75.1-116 3.05 20 NG71 142
XV
thane B.
Bromoform.
mg/1 0.0226
mg/l 0.0234 0.0235 94.0 67.5-130 0.210 20 KG716142
• 116142
20 WG716142
Cbon tetrachloride
Carbon
mg/1 0.0206 0.0214�rr 82.0 10.2-123
mg/1 0.0227 0.0227 91.0 18.1-119 0:140 20 WG716142
Chlorobenzene w4--'IN F-3 %--K K� 16142
--u ji623-2
-0 20 WG716142
Chloroethane
.02;U0.0240 9�0 61.7-135 6.94
-/1 0.0234 0.0243 94.0 76-121 .3.38. 20 NG716142
'Ti:4:,-2-6ichlorcethena
mg/l 0.0221 U.UZZU Ut) . U
mg/l 0.0206 0.0215 $2.0
J-1- --
65.6-132 4.41
-- I --------
20 WG716142
)I-is?propyl ether 16142
...
.. . .........6.36,
)ichlorodiflooromethane
mg/1 0,0210 0.0229 84.0
j. 3 6`
20 WG716142
20 WG716142
,thylbenzene mqr/l 0.0219 0.0222 88.0 78.8-122 1.29
47
0 _-Iff 16142
MY �SEEY�dr-q Oil-
............ Mj7/1 6.0242 D.0250 97.0
78.6-132 3.14
20 WG716142
Esoprqpylbenzene
rk&p-Xylenes
mg/l 0.0439 0.0446 08.0
;-2 ­',
78.8-121 1.65
v--*-,-ajV �37
20 NG716142
'��7X6142
24
0.0240
4716142
qethylene Chloride
a-Butylbenzene
mg/1
mg/1 - 0-0 224 -
44
WG716142
6142
7 0226
Ed'n' NG716142
4
0.02 0
Naphthalene
a-Xylene
mg/1
mg/l 022 6 -0. 02
NG716142
6142
mg/1 0.0232
wG716142
sec7Butylbenzene
Styrene
mg/I 0.0222 0.0225 89.0
--I
80.4-126 1. 7
WG716142
-2
.. ........ ...... -,-- -0
023 0 1 8
71`%�,:rQ. .3 . ...... ....
.�6142
Performance of ilUs Analyte is outside of established.criteria.
For additional information,
please see Attachment A 'List of Analytes with
QC: Qualifiers.'
Page 19 of 24

12065 Lebanon Rd.
Mt. Juliet, Ttd 37122
[phone]
1-800-767-5859
Fax [phone]
L•A B S•C•I-E•N'•C-V-S
Tax I.D. 62-0814289
Est. 1970
Terra Quest Environmental Consultants PC -
Ryan Kerins
100 East Ruffin Street - Quality Assurance Report
Level II
Mebane, IiC 27302 April 18, 2614
L692310
I"' ' Labozafozy oittro� mplxe bupl cater
Analyte Units Result Ref $Rec Limit RPD Limit Batch
- - - 6192
- r_ _ ;=�;. . 1__RY0 -i �s 'b2 • --`83%t0.-
,T_gk��i7,ozyat�e"nea'<:�., 4.� _:�3c;�,Fps>��-�:F�v�r:-fi�mq[._<_�.T..02-
Toluene mg/l 0.0211 0.0215 84.0 79.7-116 1.86 20 WG716142
trans-1,2-Dichloroethene mg/1 0,0204 0.0219 82.0 72.6-121 6.80 20 WG716142
13..5.., ~;-
142
6.63 2WG716142Trichlorofluoromethane mg/l 0:0197 0.0210 79.0
Vinyl chloride mg/1 0.0210 0.0224 84.0 _ -65y 99-128 6.69 _ 20 WG716142
G7 6142
6 :71:�126:e -
�8roin�-`'6�liidYobe$�ene.=;=-_- '98: 0.,-�5i''-�...�.,xs=`�s>_.=�e.��-
Dibromofluoromathane Y � »108.0'� 78.3-121 WG716142
Toluene-d8 101.0 88.5-111 WG716142
- - -- -- - - - - --- -'S'•- - wit.142
-
--8�
- :it-�- �=a�;�-� �:=.�=;rt=--'r`�� =a=�;��j__•-' 8�69�*,...-^ -
a T.ri'fluoro. � e _ .b �,. r.,... . _ =� �� _ _..� �- •.: t
Acrolein mg/1 0.135 -0.126 108 .10-190 - 6.62 28 1 F.G_716143
__.sv_���.1$•.�:::�_:��� �.
6143
Dibromofluoromethane 107.0 78.3-121 ~ WG716143
Toluerte-d8 - _ _ _ _ _ _ 99.90 8 -�8�5 111 WG7161 3
-- ---- - a:,�s;- ;-=^^, ' _ - ..-.sz=•s _ _s :.�r- t '- ---' - -- - :. �: - - -- - - - - =r'-1-�16,143
Analyte Units MS Res Ref Res TV 0 Rec Limit_ Ref Same Batch
._�-._v._..:.---�' , ,.,!-., _ =�'�• • Ss:>;:=:--_`%L 921 .L�.b�i:'=�':?�3G 1562
5._,..•.x,._.:�>,:.,:..��:��._,�---t_�=:--_:::.r�-:=t.,-,.:<r; -- �9',4�'Db066.'�3>�: #0':'• ..:5��2 _. _�...�.�..---ti=--��>
Hardness, Total (mg/L as CaCO3) mq/1 202. 45.0 150 _ 100. 80-120 L692310-04 WG715460
^,,..-^,:s• _•t;+.:_,a_�___-.-:a�`�,� `:,-^•_-'�,_.E. _ _ _ _ - _ _-rJ:y._$':�. _ _ _ ___ r_v:�ee ,s:;fl +�..�T'-�'3
�_''•':a.�`.-.,�-:!'3'`i4i•_ - .-4i`��.- _ - __::>:,::5;:ivi3.. . •=_a",ti�->= -.... _..:s �.x� `v::.. - - ti'S�:C.. ._u�,._.: `_>.a':e%9:d".=FS't:= ': `:i _
Hardness, Total4�(mg/L as CaCO3) mg/l 215.1 88.4 150 L 84.0 80-120 L692563-01 WG715798
1_9-a-Tri rhlnrnnrnnwna m /1 0.0238 0.0 .025 95.0 . .61.4-1ZU LUIWJ/'L-U3 .- hV/101yL
0.0235 0.0 .025 94.0 57.4-137 La9Z3IZ-U3 Mvr1o19Z
0.0241 0.0 .025 96.0 57.3-136 L692372-03_ WG716142
1,2-Dichlorobenzene mg/1 0.0253 0.0 UZ5 LUU. du.Z-143 LONZ012-va nm,loiya
1,2-Dichloroethans mg/1 0.0233 0.0 .025 93.0 _ 60-126 _ _ _1:692372-03 NG716142
- >•• - °0 2 ,0=0; - t02 •0:,•=-�G�.;r2•-I2 ':.i592372?0�;y�=h 7 6142
•1•-2�Pich1 r9 0 �.R - =-��„ :LP��°:.�-0. 2. 1;;=_- ,>.a::_ - ,:.. Sw...,=:�,�a,:.-.:•.:.s:.,_n _.�.y.�.>��_�s.��..�,��._.., .
1;3,5-Trimethylbenzene mg/k 0:0245 -1 0.0-`'-.025 •; 96.0-,, •63.6-132 L692372703, WG716142
1.3-Dichlorobenzene mq/1 0.0251 0.0 .025 100. 63.1-131 L692372-03 WG716142
1,4-Dichlorobenzene mgll U.ueas U.0 .U<:, --------
2,2-Dichloropropane mg/1 0.0240 0.0 .025 96.0 50.5-144, L692372-03 _=WG716142
- - =. _ - --i-_ a-= "iv` : 4 x.L'69232=Q ^- h0 6142
2c$utaiiboe*. K.= u ice'- - _/lz =._ _0101 _ xO Q0.�337,_<12Srt 7
2-Chlorotoluena mg/k 0.0233 0.0 .025 93.0 63.6-228 L692372-03 NG716142
4=Chlorotoluena _ _ m%/1 0.0234 _ 0.0 .025 94.0 65.7-127 L692372-03 NG716142
sB40;L5923
Aliy2zpenarsoE�'S?}IB?i) x ':•_`"' [9YFr' :Ol4_>`;Q10 ;'r= .._ _� �- s: .__,._„g _.�,.,.
Acetone mg/1 0.102 0.00559 125 77:0 10-130 L692372-03 WG716142
Acryionitrile mq/1 O.I21 0:0 _125 _6 97 0_ti`R___= 49.4-133 L692372-03 __ WG716142
-s; - -- - - _ --- - - - _ -=_ - - ,5 {3 L'-'-3•' `rL6923. 2s_03:.,•-=,SiG716142
;..r-; .�; _ - - 2 3=;•0: -�:025..:x,:.�89:0.,� 3 2 .r :....
Bromobenzene � mg/1 0.0231 0.0 .025 92.0 63.9-124 L692372-03> YWG716142'
• Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 20 of 24

12065 Lebanon Rd.
Mt. Juliet, TM 37122
[phone]
OESC 1-800-767-5859
Fax [phone]
(--A•13 9•C-I-E•N-C-M-s Tax I.D. 62-0814289
Est. 1970
TerraQuest Environmental Consultants PC
Ryan Xerins
100 East Ruffin Street Quality Assurance Report
Level II
Mebane, NC 27302 April 18, 2014
L692310
Ma�i�il��S-1 ke n
Analyte Units MS Res Ref Res TV 4 Rec Limit Ref Samp Batch
142
rgmo i hioFoma _. =N,_w r_6 0224 rt"_< ,,
_.�..�,�_...._._._tha-.e.':':-:z•ss::=,;:_�_.:°t;�:''._�_mg/l__;,._,,::--'�.::. ___�.... ..,. s2,-.a':_-
Bromoform mg/1 0.0237 0.0 .025 95.0- 59.5-134 L692372-03 WG716142
Bromomethane ag/1 0�0214 0.0 .025 86.0 41.7-155 L692372-03 WG716142
:gip 5'>`F. 794-i692r0 ;.'t�G7 6142
87:._ ?;asz.., ���_ ..' _..-3i_
...:,�.��-.,"s
Chlorohenzene mg/1 0.0228 0.0 .025 91.0 _, 67-125" ~• L692372-03 WG716142
Chlorodibromomathana mq/1-0;0231: 0.0 _- .025 92.0 �64.3-1254vY L692372-03 3_rNG716142
s,k. •t `- - _ _ :ya5s :3}n 1 OxD233r -.0 O4> z 025^930 x , _- 51 5 136, < ; 7692372 03= :FiG736142
CtiloY$efh'eng'Y'r:-.=•"%'=;-3�;?.,;._.�r-r.,........._..r-„_.._.:......,,:z..a,., �x".:k�-;, r
Chloroform mg/1 0.0238 0.0 .025 95.0 63--129 L692372-03 WG716142
Chloromethane mg/l 0.0207 0.0 .025 81_0 - 92.9-135 - L692372-03 WG716142
N.c1716142
- ..-_0_o__ -"
Di -isopropyl ether mg/1 0.0208 0.0 .025 83.0 56.9-136 L692372-03 WG716142
Dibromomethan_e m /l 0.0246 0.0 .025 98.0 69.2-124 L692372-03 WG716142
- k;i: _ -f'" ems,::40'6 �' =L892 7203 `wWG716192
3.9 s:r''=`�5-_'.....02,3�. .-.93i4, 6 -133� -
Ii1cLh'�oipii£f`3uo=oliigtiLatlec==`� �s:.,�;.._,<�Q. ,�t:_s�.:,.. `
Ethylbenzene mg/1 0.0223 0.0 .025 w 89.0 55.1-133 L692372-03 WG716142
mg/1 _ 0.0293 0.0 .025 97.0 55.1-136 L692372-03 .-.._ WG716142
Hexachloro^1, 3-butadisne _ _ _ _ = zr �_ _ -- - _' r. -- -- G7 6142
`"'''- =�'i'e.?^w°6 18`tl'91`^".�^:L692372r.03�cc�
"saolb'e"ciiise?=1L...,.
m&p-Xylenes mq�l 0.0450 0.00 .05 90.1 61.7-133 'L692372-U3 WG716142
57.7-134
Methyl tart -butyl
ether mg/1 00262 OTO _F�025 Y 100. :,L692372-03 ..--+ _ WG716192
0=._ 22 _L6.923T2=03:_; :WG716142
- - Q�025.1=z,- c0 : �:yQ25 .=a, _ _....._...r. -
eth'leneiCiilozida-, ;_ _r_::'r -> _ a:z:.mT<: s'��__< .s_P�.$ �, - - _ WG716142
'k w _ _ mg/1 0.0238 0.0 .025 95.0 62.7-140 L692372 03
n-Butylbenzene
n-Propylbenzens mg/1 `0:0233 0.0 .025 93.0 Jr_65.9-1311-L692372-03 WG716142
sl. a 98`'.Q SB 125 9 3.�2 03;' = r.VjGJ}61
,�._ 42
i!a .htha en..9,:-=" s' ?: ?:';`_'::_c:' ;?;s :' Si)!4�1_:..:..,b . .::: Qt �...._...:s .. ..
p - ~ M_..- mg/l 0.0239 0.00 .025 95.6 63.3-130 L692372-03 WG116142
o-Xylene 025 100. 63.2-139 L_692372-03 WG716142
-LSO ropyltoluene mg/1...,. _ _ _ - =63?2 139 G716142
0.025 --
.' ,
01'02952 ...O d* F Q25 i r;98'.0 - " 692322 U3 = 3,
Styrene
1.lbenzene... 2..�.._..:.:-_.6...r_.,::_..._ - <_. w.. ...... .. :. . a . _....:.._. .y
Styrene 1 mg/1 0.0225 0.0 .025 90.0 66.6-133 L692372-03 WG716192
tert-Butylbenzene mg/l 0.0240 0.0 `025 - 96.0 _ - 63.3-134_ _ L692372-03 NG716142
- - - yY- - F -- _- - = 93=139 t :;�23Z2' 3_'°: •. IG 16192
1'=c..e::k:0#0230`t,:_.9:0::._.;... ,..0.25T-, 2•c0 `=:' `,.,,.-'{--�...,.. ----
T`eabharoethene.;,::,:; ngJ._,,:_...,....--- -..... _ 2 _
Toluene mg/1 0.0214 0.0 .025 86.0 61.4-130 L692372-03 WG716142
trans^1,2-Dichlorcethene mg/1 0.0217 0.0 .025 87.0 56.5-129 L692372 03 t WG716142
L -
r , � : ".;� ..":'::: �372�z-��. :EG71619z
a: r_::.,:.:- :.:;:::xT;?.m f11;;::Q,Q3- _.OLO..,'> c. _ x:•-.:...'rv_=.._.vim,. 9r...
- ,._. -
Triehlorofluoromethane mg/1 0.0207 0:0 .025 83.0 47.8-137 L692372-03 WG716142
Vinyl 0716142
chloride m�/1 0.02�21 0 0 .025„ T88.0 ^_yt4Yz' 97.8-137L69237�^„ 2-03 _ ;.. G716192
97.7� 72r126`'':
4=_�zomo_robenzgR�_.c;: =` 5:;s:c:a:::�•_!; = ,x...._ t:=:'•;;t :;_'d":':.. a. ..... rio „ . -
Dibromofluoromethana w 9.0 88.3 111 �WG726142
99.20 88.5-111
WG7161 2
Toluene-d8::...... - - 6142
ache_�:T�zi-filuorotolusne--,...:....... i ,.,_...:_. �:...._...._....::...._._.__._..-..
w
ma/1 0.116 0.0 .125-._94.0,-_-10^200 L692510-09 WG716143
Dibromofluorometnane 99.30 88.5-111 WG716143
Toluene-d8 - _ -�: = "-ti:i`.' _ wG7i6143
Analyte Units MSD Ref %Rea Limit RPD Limit Ref Samp Hatch
- - - - -- - 5627
- - - -- - - -- - - fi;- 5a1`25.�-
sT
e,
v:
Hardness Total (m'/L aslCaCO3)` m /1 200. 202. 103. 80-120 0.995 20 L692310-04 WG715460
- -- - - 'W 71 79
•:.�::y - f�01G - 2 �3 - - �69 56
- -469
�20 �L
- - - - -1202 �0.
Hardness; Total~ (mg/LJas,CaCO3)� i�mg/l� 216. 415. 85.1 �..60
- - - - - -s.'-- - L692372 p3 'S; YWG7�6142
-- - ----- "- ,..,�..�•;r�;' --- - 'r0 45�:i9.7:9*''=y'•5^�=64T128=�a_�:,40,�470r,`,;:?tiQ--.%i'%............:._..__.,..,-�.....'3.,m_W
'`1�2=TAtYsehl'oYoehS'ne;:_;:.;<'029 0. 2..=:..._
1,1,1-Trichloroethane mq/1 0.0226 0.0232 90.2 58.7-134 ^2.82 20 L692372-03 W016142
* Performance of this Analyte is -outside of established criteria.
For additional information, please see Attachment R 'List of Analytes with QC Qualifiers.'
Page 21 of 24

TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street
Mebane, tiC 27302
Quality Assurance Report
Level II
L692310
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18, 2014
Analyte
�Matz�3t�S'"ika�Du
R
Units MSD Ref &ReC Limit RPD limit Ref Samp Batch
�16142
1,1,2-Trichloroethane
mg/1 0.0241 0.0233 96.4 66.3-125 3.27 20 L692372-03 FiG716142
Il-Dic- K^ } 58.5-132 2.10 20 L6923772-03 WG716142
1hloroethane mg/10;0230 0.0235 91.9
-Sl D:�C ZSSE 'eb -^,,t`. y �?� ? 2�E5' 0:$' 3 x i'�1�U� ° r432 : s :LL2� 2 o-3 6h2 4 ``• ✓` 6141
11 Dich propene
.. , :'�0 . .:s.:,..
mg/1 0.0219 0.0224 85.6 57.3-136 0.220 20 L692372-03 WGI16142
1,2,3_Tfichlorobenzene/1 0.0� 274 0.0268 110. 59.1-138 2.25_ 23.7 L692372-03__- '_ WG716142
,: , - 16142
Q23tk,$93: ri, t 03Zr : r
2t3`rT=692872-
1 t3-1-oYo 74�ana.r.::c., Sxh_ Y
1,2,4-Trichlorobanzena
x�14§�1x�0d298='=0
mg%1 0.0285 0.0273 114. 63.6-143 4.99 21.9 L592372-03 WG716142
1:2:4-Trimethvlbenzene
ma/1 0.0234 0.0235 93.5 57.9-137 __. 0.62020L692372=03 WG716142
1,2-Dibromoethane mg/1 u.uZei u.
1.2-Dichlorobenzene mg/l 0.0255 0.
,
0
Q
0'
3 67.1-125 2.09 20
68.2-123 0.970 20
.2
WGI16142
68.6^123 0.270 20 L692372-03 WG71614-2
50 9=1 - Y500: 27 9. `L692332=03_ N: G716142
22.4-138 1.56 2-1 L692372-03 WG716142
4-Methyl-2-pentanone (MIBK) mg'/1 0.117 0.114 93.9
60.8-140 2.89
25.1
L692372-03
WG716142
Acetone
mg/l 0.102 0.102 76.9
10-130 0.210
27.9
L692372-03
NG716142
_ - - _ _ - --''49'9�1 3s.: u3'25;3= 9 3 =03i? ;' iG 16142
�
m' L:s`::r.0 12 :121 a :.2201' 3 _ vir w _ r... e
': s _?:'':='.'e�_..... .. ti ,� _M....:,::... '- ::F,'^': `4�3.81
Benzene
mg/L 0.0219 0.0223 85.7
54.3-133
20
L692372-03
WG716142
Bromobenzene
mg/L _0.0228 0.0231 91.3
63.9-124 1.38
20
L692372-03
WG716142
@4omodichloromethane•�:.:,ti=_ �' =�-_ �-<<� ' ::=; m9�')•: �:t:.=._0 � P225"�;:.0:0224;_::i'90.1 �''.=:-'�:__ _ ::= 63: 9: 121!:'", �_.. ...
_
a.� 0�'�xw�_-_�.....,
G716142
Bromoform
_
mg/1 0.0291 0.0237 96.2
59.5-139 1.50
20.5
L692372-03
NG716142
Bromomethane mg/1 0.0225 0.0214 90.1 41.7^155 5.23 •21.9 L692372-03 NG716142
-. ;x: - - •j_ _ _ Pb3_i1=a f16142
b:. �=�b.:lo,�:.--- _ _ aTJ..--:4}0� ....__. ..r__ _u=... -- - :.�-_�.
- _ ,.4° '.,.7.=3 _•::, 20 92 d
� •� �
Chloro6enzene
mg/1 0.0222 0.0228 88.7
67-125� 2.60
20
L692372-03
WG716142
Chlorodibromomethana
m /1 0.0232 0.6231 92.9 64.3-125 0.640
._. .:...__ -
20.8 L692372-03
=L692372r03r-
NG716142
- G.�6142
Chleroethane:_;:::�:ar,-:.:..+.�>i�t�,-,-:..-
_.d�..:.;�:�:��..=�..-::.,,.?.....,.,,.._:.,,�_- M_,:..�:
0 02 O..0233.;r:9
~mg/1
-�--
.4
Q-�=;
:.._.�..-.M,._.....:t�fi..Z
Chloroform '
0.0238 0.6238 95.3
63-129 0.230
20
L692372-03
WG716142
Chloromethane -
mg/l 0.0198 0.0202 _79.3
- -- -
_ _ ;-`.90i0
1F"•;>c.0_0225;;`;
42.4_135 1.72
- _-- -
_ ^:::;; ` 59'c2r124i 1764
20
z '�-: i'<L6
;.--. 0
L692372-03
3 3=03':`
92_�...=-....-
WG716142
.WG. i6142
cis_i :......;:_:: <�S .0 .0229
Di -isopropyl ether mg/1 0.02�09 0.0208 83:5
56.9-136 0.290
20
L692372-03
-
NG716142
Dibromometbane
mg/1 0.0246 0.6246 98.6
68:2-124 0.100
20
L692_372-03
6142
WG71-6142
?ichlorodiflu¢rometane,:_:a
'•._`°?' ':.:..:...:..:.`.
_
Ethylben2ene mg/1 0.0216 0.0223 86.2
61.4-133 3.34
20
L692372-03
WG716142
Hexachloro-1,3-butadiene mg/1 0.0239 0.0243 95.5 55.1--1-136. 1.72 23.6 L692372-03
- - '--'m •i� ::0 0250.:.,,.0.025�..:.��0: ,....;�665E,�141'Y=,
�..._�}._.-gs;S��t:-.ir:�:Etr�;�:',='"t;::�?;��?=*.....�.•?:z,-a..,-,.. _:::,..
WG716142
16142
-.�.
.. 4P..Pp
map-Xylenes
mg/l 0.0439 0.0450 87.8
61.7-133 2.58
20
L692372-03
WG716142
Math 1 tert-butyl ether mcq/1 0.0268 0.0262 107.
_ -�
- 5-":=0': 251'- :Y 7::0':;'s
e tiyl'ene' Chloride' ';=:=:_`:�':_`-_ `^�=':�_:':.�sr�: �<;0;02 3=.:_ 0 ..._: �,.-...
57.7-134 2.04
:`:=:SBi'122%%0:810_;=.20_::L692372,03:;:>:.=WGT16142
= _. ._...__._......-----
20
..- _.. .
L692372-03 NG716142
.
n-Butylbenzene
_=;:;;mgT�
mg/l 0.0235 0.0238 93.9
62.7-140 1.19
20.3
L692372-03
WG716142
n-Pro lbenzene mg/l 0.0225 0.0233 90.1 65.9-131 3.55 20 L692372-03
�.. �'. , .; _,_........,...: ......... ......_... -411""`:I;IEC-- -
7aPhtha�,eng,:,s::=:,::�:,rx::,_:.:_�,:.:.:._..:-,..... •m%��:��:QZ�.r��0�45�:,e;>102:1��;�;_:i::?,�_-_.;_----_--- ----- �..�..
NG716142
Gil 6142
-:..r.
o-Xylena
• : mg/1/l-:0.0237 0.0239 94.8
63.3-130 0.790
20
I.692372-03
WG716142
ma/1 0.0247 0.0253 98.9
63.2-139 2.44
_20.4
_L692372-03NG716142
-Y..-. •-_•- ---� -
tert-Butylbenzene mg/l:a 0.0239
... 2 3 =:00O230::,:
1:°.0=--2-:•s..`..._:
------ - .
0.0240 95.5 63.3-234 0.580 21
89;2;-`=ems _s:t 53a139.:='" :3s28 20 = y°L692372e03
L692372-03 UG716142
?�-HG716142
Tetzachlokoath'eha-:,':='::-:'t_
.
0.0205
__...._...._�-
0.0214 82.0
_ ._.....
61.4-130
4.19 20
L692372-03 NG716142
Toluene
trans-1,2-Dichloroethene
mg/1
mg/1-
0.0210
0.0217 84.1
56.5-129
3.24 20
L692372-03 lIG716142
.:.::••:,.•-:..::.::;-�:;:-:;:::�-�::_:::�:'_��7,i,::;c>;�:.02�::_O;�I23.3'=�:90::8:=:=.�::';�;`:941'-1A9,��:::�;2�'+i3_:.:�`:_20,.,_.`:'-.L6g2
Z_:03`-:_<'�:-:hG716142
Trichlorofluoromethane
mg/l
0.0202
0.0207 81.0
49.67145
2.36 21.2
L692372-03 WG716142
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment A 'List of Analytes with QC Qualifiers.'
Page 22 of 24

12065 Lebanon Rd.
Mt. Juliet, TH 37122
[phone]
OESC 1-800-767-5859
Fax [phone]
L•A•6 S•C•1.•�•tJ•C•E•s Tax I.P. 62-0814289
Est. 1970
TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street Quality Assurance Report
Level II
N.ebane, NC 27302 April 18, 2014
L692310
;_13aeYtk,�S;pilce;t�Tp1'�'cate
Anal to Units MSD Ref 4cRec Limit RPD Limit Ref Samn Batch
yL-9 3 2 b.. =.........
'-x•- — - - -�c:-�c_<.�._ti :.-:-s—;,-._x� v--- -- - - ----��?-'-s-;- _ -_ _---`.7�8= 37.��€3 _. 6=r�:;.'ZO.=')', 6 2---_.,t 16142
Vi;(iy1_,ch_ 5�1�1e' �;. �� ���:�.�_:{�--_..z_-::�._3�.==m9/,1�,a� 0 �92�9� �•� G'J0221 f,_��=�^-`�=_��i4__.,,�_,_-�_.�_�.LL.-.._.__u.,_ .�_,.._�
4-Bromofluorobenzene 91.70 71-126 WG716142
Dibromofluoromethane 108.0 78.3-121 - iiG716142
s.._ 6142
a,a,aiflu'== 99 60 85 114 NG716142
a,s,e-Trifluorotoluene� � -
>;. `ra s-L 0�9 ',27s l - 692510=09=v=,c.WG 6143
.18>>T;105:�.'-a 10200w'T...w.,s.�,�»_.'.�-,.;,..-.,��
_
4-Bromofluorobenzene 100.0 71-126 WG716143
Dibromo£luoromethane, 110.0 78T3-121 - _ _ _- VIG716143
- x- n.. '. :3 x: - - 7:-ice: <.i =-s GT 6143
frmxa a
..._..,. a-Tri£luorotoluena -�._.: - : •z....- - -------- - - 94.10 85-114 WG716143
Batch number /Run number / Sample number cross reference
NG7151631 R2903332: L692310-06
WG715331: R2903389: L692310-04
WG715458: R2903628: L692310-05
V,G715627: R2903886 R2904785: L692310-04
WG715684: R2903920: L692310-05
42G715460: R2903943: L692310-04
WG715798: R2904461: L692310-07
NG115797: R2904772: L692310-07
NG716142: R2904832: L692310-01 02 03 04
WG716143: R2904860: L692310-01 02 03 04
TIG715192: R2905502: L692310-04
* + Calculations are performed prior to rounding of reported values.
+ Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 23 of 24

�wESC
L•A•t3 S•c•1•M•N•G��•8
TerraQuest Environmental Consultants PC
Ryan Kerins
100 East Ruffin Street
Mebane, NC 27302
Quality Assurance Report
bevel II
L692310
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix D of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the In" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery; expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control"._ If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 24 of 24
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-761-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 18, 2014

:::•:;
�4ynt�i�et'.�
,�
�
chainof•custcdy
Page of
yo
iiWW
Prepared by:. _... _—..
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Analytical Report 484686
for.
Tefraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Coliseum Shell
13-MAY-14
Collected By: Client
XIENCO
Laboratories q
Florida Testing Services, LLCFJIA
( A4w-'imoq��v`
6017 Financial Dr., Norcross, GA 30071
Ph: [phone] Fax: [phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (T104704215-14-167TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code: AZ0O0989):- Arizona (AZ0758)
Final 1.000

10 s
Florida Testing Services, LLC
13-MAY-14
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 484686
Coliseum Shell
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 484686. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 484686 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Eben Buchanan
Project Manager
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 2 of 24 Final 1.000

P CIA
• Sam le Cross Reference 484686 �, -�
\�9 PJIA
Florida Testing Services, LLc Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id
Matrix
Date Collected Sample Depth
Lab Sample Id
Influent
W
05-05-1411:21
484686-001
After AST
W
05-05-14 11:16
484686-002
After 1st GAC
W
05-05-14 11:09
484686-003
Effluent
W
05-05-1410:58
484686-004
Version: 1.%
Page 3 of 24 Final 1.000

PUR�
Flagging Criteria V'� PJ�°
Florida Testing Services, LLC
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the 'T' qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by mlmerous States and Agencies.
A Small Business and Minority States Company that delivers SERVICE and QUALITY
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd, Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone
Fax
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Page 4 of 24 Final 1.000

Certificate of Analytical Results 484686 �a
rau
Florida Testing services, LLC
Terraquest Environmental
Consultants,
P.C.,
Mebane, NC
Coliseum
Shell
Sample.Id: Influent
Matrix:
Ground Water
Date Received: 05.06.14 10.50
Lab Sample Id: 484686-001
Date Collected: 05.05.14
11.21
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM6200B PREP
Tech: JOL
% Moisture:
Analyst: MLA
Date Prep:
05.07.14
06.35
Seq Number: 940303
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
05.07.14 11.12
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
05.07.14 11.12
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
05.07.1411.12
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
05.07.1411.12
U
1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
05.07.14 11.12
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
05.07.14 11.12
U
1
1,1-Dichloropropene
563-58-6
U
0.500"
0.0600
ug/L
05.07.14 11.12
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
05.07.14 11.12
U
1
1,2,3-Tihchloropropane
96-18-4
U
1.00
0.138
ug/L
05.07.14 11.12
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
05.07.14 11.12
U
1
1,2,4-Trimethylbenzene
95-63-6
50.0
0.500
0.103
ug/L
05.07.1411.12
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
05.07.14 11.12
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
05.07.14 11.12
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
05.07.1411.12
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
05.07.1411.12
U
1
1,3,5-Trimethylbenzene
108-67-8
11.6
0.500
0.0870
ug/L
05.07.1411.12
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0990
ug/L
05.07.14 11.12
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
05.07.14 11.12
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
05.07.14 11.12
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
05.07.1411.12
U
1
2-Butanone (MEK)
78-93-3
101
20.0
0.378
ug/L
05.07.14 11.12
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
05.07.14 11.12
U
1
2-Hexanone
591-78-6
24.5
0.400
0.352
ug/L
05.07.1411.12
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
05.07.14 11.12
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
05.07.14 11.12
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
05.07.14 11.12
U
.1
Acetone
67-64-1
113
2.00
0.352
ug/L
05.07.1411.12
1
Benzene
71-43-2
19.9
0.500
0.119
ug/L
05.07.1411.12
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
05.07.1411.12
U
1
Bromochloromethane
74-97-5
U
0.500,
0.112
ug/L
05.07.14 11.12
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
05.07.1411.12
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
05.07.14 11.12
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L.
05.07.1411.12
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
05.07.14 11.12
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
05.07.1411.12
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L,
05.07.1411.12
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
05.07.1411.12
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
05.07.14 11.12
U
I
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
05.07.1411.12
U
1
Page 5 of 24 Final 1.000

i ®
Certificate
of
Analytical Results 484686
Ida Testing Services, LLC
Terraquest Environmental Consultants,
P.C.,
Mebane, NC
Coliseum
Shell
Sample Id: Influent
Matrix:
Ground Water
Date Received: 05.06.14 10.50
Lab Sample Id: 484686-001
Date Collected: 05.05.14
11.21
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM6200B PREP
Tech: JOL
% Moisture:
Analyst: MLA
Date Prep: 05.07.14
06.35
Seq Number: 940303
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
. Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
05.07.1411.12
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
05.07.1411.12
U
1
Dichlorodifluoroinethane
75-71-8
U
1.00
0.0670
ug/L
05.07.1411.12
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
05.07.1411.12
U
1
Ethylbenzene
100-41-4
20.0
0.500
0.0920
ug/L
05.07.1411.12
I
Isopropyl ether
108-20-3
28.5
0.500
0.0920
ug/L
05.07.14 11.12
1
Isopropylbenzene
98-82-8
0.780
0.500
0.0980
ug/L
05.07.14 11.12
1
Methyl tert-butyl ether (MTBE)
1634-04-4
915
25.0
8.45
ug/L
05.07.14 11.43
D
50
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
05.07.14 11.12
U
1
Naphthalene
91-20-3
55.7
2.00
0.0940
ug/L
05.07.1411.12
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
05.07.14 11.12
U
1
n-Propylbenzene
103-65-1
3.39
1.00
0.0650
ug/L
05.07.1411.12
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
05.07.14 11.12
U
I
Styrene
100-42-5
U
0.500
0.0740
ug/L,
05.07.1411.12
U
1
tert-Butylbenzene
98-06-6
0.620
0.500
0.0890
ug/L
05.07.14 11.12
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
05.07.14 11.12
U
1
Toluene
108-88-3
120
25.0
2.85
ug/L
05.07.1411.43
D
50
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
05.07.14 11.12
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
05.07.14 11.12
U
1
Tichloroethene
79-01-6
U
0.500
0.139
ug/L
05.07.14 11.12
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
05.07.1411.12
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
05.07.14 11.12
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
05.07.14 11.12
U
1
m,p-Xylenes
179601-23-1
80.6
1.00
0.176
ug/L
05.07.1411.12
1
o-Xylene
95-47-6
49.5
0.500
0.122
ug/L
05.07.1411.12
1
Surrogate
Cas Number
Recovery
Units
Limits Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
108
%
65-134
05.07.14 11.12
4-Bromofluorobenzene
460-00-4
108
%
60-148
05.07.1411.12
Toluene-D8
2037-26-5
108
%
87-114
05.07.1411.12
Page 6 of 24 Final 1.000

Certificate of Analytical Results 484686
PJIA
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST
Lab Sample Id: 484686-002
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 940303
Parameter Cas Number
Matrix: Ground Water
Date Collected: 05.05.14 11.16
Date Prep: 05.07.14 06.35
Result RL MDL
Units
Date Received:05.06.14 10.50
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
05.07.14 10.43
U 1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
05.07.1410.43
U 1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
05.07.1410.43
U 1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
05.07.1410.43
U 1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
05.07.14 10.43
U 1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
05.07.14 10.43
U 1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
05.07.14 10.43
U 1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
05.07.14 10.43
U 1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
05.07.1410.43
U 1
1,2,4-Trichlorobenzene
120-82-1
U,
1.00
0.0690
ug/L
05.07.14 10.43
U 1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
05.07.1410.43
U 1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
05.07.14 10.43
U 1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
05.07.14 10.43
U 1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
05.07.14 10.43
U 1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
05.07.1410.43
U 1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
05.07.14 10.43
U 1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
05.07.14 10.43
U 1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
05.07.14 10.43
U 1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
05.07.14 10.43
U 1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
05.07.14 10.43
U 1
2-Butanone (MEK)
78-93-3
7.49
20.0
0.378
ug/L
05.07.1410.43
J 1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
05.07.14 10.43
U 1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
05.07.1410.43
U 1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
05.07.14 10.43
U 1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
05.07.14 10.43
U 1
4-Methyl-2-pentanone (MI13K)
108-10-1
U
0.400
0.253
ug/L
05.07.14 10.43
U 1
Acetone
67-64-1
31.8
2.00
0.352
ug/L
05.07.14 10.43
1
Benzene
71-43-2
U
0.500
0.119
ug/L
05.07.14 10.43
U 1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
05.07.1410.43
U 1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
05.07.1410.43
U 1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
05.07.1410.43
U 1
Bromofonn
75-25-2
U
2.00
0.159
ug/L
05.07.1410.43
U 1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
05.07.1410.43
U 1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
05.07.14 10.43
U 1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
05.07.1410.43
U 1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
05.07.1410.43
U 1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
05.07.14 10.43
U 1
Chloroform
67-66-3
U
0.500
0.172
ug/L
05.07.1410.43
U 1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
05.07.1410.43
U 1
Page 7 of 24 Final 1.000

p[Cgp°
Certificate of Analytical Results 484686
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST Matrix: Ground Water Date Received:05.06.14 10.50
Lab Sample Id: 484686-002 Date Collected: 05.05.14 11.16
Analytical Method: VOCs by GUMS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 940303
Parameter Cas Number
Date Prep: 05.07.14 06.35
Result RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
05.07.14 10.43
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
05.07.14 10.43
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
05.07.1410.43
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
05.07.1410.43
U
I
Etylbenzene
100-41-4
U
0.500
0.0920
ug/L
05.07.14 10.43
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
05.07.14 10.43
U
1 ,
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L.
05.07.1410.43
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
05.07.14 10.43
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
05.07.14 10.43
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
05.07.14 10.43
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
05.07.14 10.43
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
05.07.14 10.43
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L,
05.07.14 10.43
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
05.07.14 10.43
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
05.07.14 10.43
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
05.07.14 10.43
U
I
Toluene
108-88-3
U
0.500
0.0570
ug/L
05.07.1410.43
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L:
05.07.14 10.43
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
05.07.14 10.43
U
1
Tichloroethene
79-01-6
U
0.500
0.139
ug/L,
05.07.14 10.43
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
05.07.1410.43
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
05.07.14 10.43
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
05.07.14 10.43
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
05.07.1410.43
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
05.07.14 10.43
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
107
%
65-134
05.07.14 10.43
4-Bromofluorobenzene
460-00-4
110
%
60-148
05.07.14 10.43
Toluene-D8
2037-26-5
110
%
87-114
05.07.1410.43
Page 8 of 24 Final 1.000

yVem.w
�V�WCertificate of Analytical Results 484686 / ri-
- � ..-
Terraquest Environmental Consultants, P.C.; Mebane, NC
Coliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water Date Received: 05.06.14 10.50
Lab Sample Id: 484686-003 Date Collected: 05.05.14 11.09
Analytical Method: VOCs by GC/MS by SM6200B
Tech: 70L
Analyst: MLA
Seq Number: 940303
Parameter Cas Number
Prep Method: SM6200B PREP
% Moisture:
Date Prep: 05.07.14 06.35
Result RL NIDL Units Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
05.07.14 10.16
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
05.07.14 10.16
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
05.07.1410.16
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
05.07.14 10.16
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
05.07.1410.16
U
1
1,1-Dichloroethee
75-35-4
U
0.500
0.104
ug/L
05.07.1410.16
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
05.07.14 10.16
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
05.07.14 10.16
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
05.07.1410.16
U
1
1,2-,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
05.07.14 10.16
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
05.07.14 10.16
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
05.07.14 10.16
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
05.07.1410.16
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
05.07.1410.16
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
05.07.1410.16
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
05.07.1410.16
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
05.07.14 10.16
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
05.07.14 10.16
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
05.07.14 10.16
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
05.07.1410.16
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
05.07.14 10.16
OF
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
05.07.14 10.16
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
05.07.1410.16
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
05.07.14 10.16
U
1
4-1sopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
05.07.14 10.16
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
05.07.14 10.16
U
1
Acetone
67-64-1
9.96
2.00
0.352
ug/L
05.07.1410.16
1
Benzene
71-43-2
U
0.500
0.119
ug/L
05.07.14 10.16
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
05.07.1410.16
U
1
Bromochlorometbane
74-97-5
U
0.500
0.112
ug/L
05.07.14 10.16
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
05.07.1410.16
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
05.07.1410.16
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
05.07.1410.16
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
05.07.14 10.16
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
05.07.1410.16
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L .
05.07.14 10.16
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L.
05.07.1410.16
U
1
Chloroform
67-66-3
0.900
0.500-
0.172
ug/L
05.07.1410.16
1
Chloromethane
74-87-3
U
0.500
.0.0850
ug/L
05.07.1410.16
U
I
Page 9 of 24 Final 1.000

Certificate of Analytical Results 484686`'BQR'
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water Date Received: 05.06.14 10.50
Lab Sample Id: 484686-003 Date Collected: 05.05.14 11.09
Analytical Method: VOCs by GUMS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 940303
Parameter Cas Number
Prep Method: SM6200B PREP
% Moisture:
Date Prep: 05.07.14 06.35
Result RL MDL Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
05.07.1410.16
U
1
cis- 1, 3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
05.07.1410.16
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
05.07.1410.16
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
05.07.1410.16
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
05.07.1410.16
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
05.07.14 10.16
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
05.07.14 10.16
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
1.46
0.500
0.169
ug/L
05.07.14 10.16
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
05.07.14 10.16
U
I
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
05.07.14 10.16
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
05.07.14 10.16
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L,
05.07.14 10.16
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
05.07.1410.16
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L,
05.07.1410.16
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
05.07.14 10.16
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
05.07.14 10.16
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
05.07.1410.16
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
05.07.14 10.16
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
05.07.1410.16
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
05.07.14 10.16
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
05.07.1410.16
U
I
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
05.07.14 10.16
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
05.07.14 10.16
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
05.07.1410.16
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L,
05.07.1410.16
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
106
%
65-134
05.07.1410.16
4-Bromofluorobenzene
460-00-4
109
%
60-148
05.07.14 10.16
Toluene-D8
2037-26-5
109
%
87-114
05.07.1410.16
Page 10 of 24 Final 1.000

Pu W
Certificate of Analytical Results 484686,eoR
, �KaL
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:05.06.14 10.50
Lab Sample Id: 484686-004 Date Collected: 05.05.14 10.58
Analytical Method: TSS by SM2540D
Tech: ANS
Analyst: ANS
Seq Number: 940584
Parameter
Total Suspended Solids
% Moisture:
SUB: E871002
Cas Number Result RL NIDL Units Analysis Date Flag Dil
U 4.00 3.50 me/L 05.12.14 09.41 U 1
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR % Moisture:
Analyst: 4150 Date Prep: 05.12.14 11.14
Seq Number: 940652
Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil
Lead 7439-92-1
U 0.0100 0.00330 mg/L 05.12.1415.04 U
Page 11 of 24
Final 1.000

P�CgFO
Certificate of Analytical Results 484686
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:05.06.14 10.50
Lab Sample Id: 484686-004 Date Collected: 05.05.14 10.58
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 940303
Parameter Cas Number
Date Prep:
Result
05.07.14 06.35
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
05.07.1409.48
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
05.07.14 09.48
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
05.07.14 09.48
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
05.07.14 09.48
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
05.07.14 09.48
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
05.07.14 09.48
U
1
I,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
05.07.14 09.48
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
05.07.14 09.48
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
05.07.14 09.48
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
05.07.14 09.48
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
05.07.14 09.48
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
05.07.14 09.48
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
05.07.14 09.48
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
05.07.14 09.48
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
05.07.14 09.48
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L.
05.07.14 09.48
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
05.07.1409.48
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
05.07.14 09.48
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
05.07.14 09.48
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
05.07.14 09.48
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
05.07.14 09.48
OF
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L,
05.07.14 09.48
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
05.07.1409.48
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
05.07.14 09.48
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
05.07.14 09.48
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
05.07.14 09.48
U
1
Acetone
67-64-1
1.34
2.00
0.352
ug/L
05.07.14 09.48
J
1
Benzene
71-43-2
U
0.500
0.119
ug/L
05.07.14 09.48
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
05.07.14 09.48
U
1
Bromochlorornethane
74-97-5
U
0.500
0.112
ug/L
05.07.14 09.48
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
05.07.14 09.48
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
05.07.14 09.48
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
05.07.14 09.48
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
05.07.14 09.48
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L,
05.07.14 09.48
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
05.07.14 09.48
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
05.07.14 09.48
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
05.07.14 09.48
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
05.07.14 09.48
U
1
Page 12 of 24 Final 1.000

3 pCCNo u J
Certificate of Analytical Results 484686 k'4e
r�,tu
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent
Matrix:
Ground Water
Date Received:05.06.14 10.50
Lab Sample Id: 484686-004
Date Collected: 05.05.14
10.58
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM6200B PREP
Tech: JOL
%
Moisture:
Analyst: MLA
Date Prep:
05.07.14 06.35
Seq Number: 940303
Parameter
Cas Number
Result
RL
NIDL
Units
Analysis Date
Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
05.07.14 09.48
U
I .
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
05.07.14 09.48
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
05.07.14 09.48
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
05.07.14 09.48
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
05.07.14 09.48
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
05.07.14 09.48
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
05.07.14 09.48
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
05.07.14 09.48
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
05.07.14 09.48
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
05.07.14 09.48
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
05.07.14 09.48
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
05.07.14 09.48
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
05.07.14 09.48
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
05.07.14 09.48
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
05.07.14 09.48
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
05.07.14 09.48
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
05.07.14 09.48
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
05.07.14 09.48
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
05.07.14 09.48
U
I
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
05.07.14 09.48
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
05.07.14 09.48
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
05.07.14 09.48
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
05.07.14 09.48
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
05.07.14 09.48
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
05.07.14 09.48
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
101
%
65-134
05.07.14 09.48
4-Bromofluorobenzene
460-00-4
110
%
60-148
05.07.14 09.48
Toluene-D8
2037-26-5
111
%
87-114
05.07.14 09.48
Page 13 of 24 Final 1.000

�F
QC Summary 484686 fl��
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method: TSS by SM2540D
Seq Number: 940584
Matrix:
Water
MB Sample Id: 940584-1-BLK
LCS Sample Id:
940584-1-BKS
LCSD Sample Id: 940584-1-BSD
B Spike
Parameter M
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Fla g
Result Amount
Result %Ree
Result %Rec
Limit Date
Total Suspended Solids <3.50 100
96.0 96
95.0 95
80-120 1 10 mg/L 05.12.14 09:41
Analytical Method: TSS by SM2540D
Seq Number: 940584
Parent Sample Id: 484839-001
Parameter Parent
Result
Total Suspended Solids 272
Analytical Method: TSS by SM2540D
Seq Number: 940584
Parent Sample Id: 484874-001
Parameter Parent
Result
Total Suspended Solids <3.50
Matrix: Water
MD Sample Id: 484839-001 D
MD %RPD RPD Units Analysis Flag
Result Limit Date
288 6 10 mg/L 05.12.14 09:41
Matrix: Water
MD Sample Id: 484874-001 D
MD %RPD RPD Units Analysis Flag
Result Limit Date
<3.50 0 10 mg/L 05.12.14 09:41 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
940652
Matrix:
Water
Date Prep: 05.12.14
MB Sample Id:
655237-1-BLK
LCS Sample Id:
655237-1-BKS
LCSD Sample Id: 655237-1-BSD
Parameter
M B Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
0.970 97
0.991 99
80-120 2 20 mg/L 05.12.1414:42
Analytical Method: Lead by SW-846 6010C
Seq Number: 940652 Matrix: Ground Water
Parent Sample Id: 484845-003 MD Sample Id: 484845-003 D
Parameter Parent MD
Result Result
Lead <0.00330 <0.00330
Prep Method: SW3010A
Date Prep: 05.12.14
%RPD RPD Units Analysis Flag
Limit Date
0 20 mg/L 05.12.1414:47 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
940652
Matrix:
Ground Water
Date Prep: 05.12.14
Parent Sample Id:
484845-003
MS Sample Id:
484845-003 S
MSD Sample Id: 484845-003 SD
Parameter
Parent Spike
MS MS
MSD MSD Limits
%RPD RPD Units Analysis
Flag
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
0.975 98
0.955 96 80-120
2 20 mg/L 05.12.1414:49
Page 14 of 24 Final 1.000

s
Florida Testing Services, LLC
Analytical Method:
Seq Number:
MB Sample Id:
Parameter
QC Summary 484686
Terraquest Environmental Consultants, P.C.
Coliseum Shell
VOCs by GUMS by SM6200B
940303 Matrix: Water
655073-1-BLK LCS Sample Id: 655073-1-BKS
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1, 3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyholuene
4-Methyl-2-pentanone (MMK)
Acetone
Benzene
Bromobenzene
Bromoehloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
ME
Spike
LCS
LCS
LCSD
LCSD
Result
Amount
Result
%Ree
Result
%Rec
<0.190
25.0
24.1
96
23.2
93
<0.0760
25.0
22.2
89
21.3
85
<0.0700
25.0
28.1
112
28.4
114
<0.113
25.0
27.8
ill
26.8
107
<0.121
25.0
24.8
99
23.5
94
<0.104
25.0
23.8
95
20.8
83
<0.0600
25.0
25.4
102
24.1
96
<0.118
25.0
25.2
101
25.2
101
<0.138
25.0
23.3
93
26.0
104
<0.0690
25.0
24.2
97
24.1
96
<0.103
25.0
27.5
110
26.8
107
<0.180
25.0
25.1
100
24.8
99
<0.0940
25.0
25.4
102
24.9
100
<0.0900
25.0
23.8
95
23.3
93
<0.122
25.0
27.2
109
26.5
106
<0.0870
25.0
27.0
108
26.1
104
<0.0980
25.0
25.9
104
24.7
99
<0.133
25.0
26.6
106
26.2
105
<0.0670
25.0
24.9
100
24.1
96
<0.0970
25.0
24.1
96
23.0
92
<0.378
50.0
43.7
87
55.6
ill
<0.0880
25.0
27.3
109
26.1
104
<0.352
50.0
57.7
115
60.9
122
<0.0900
25.0
28.5
114
27.5
110
<0.0890
25.0
26.5
106
25.2
101
<0.253
50.0
50.9
102
53.9
108
<0.352
50.0
41.4
83
43.1
86
<0.119
25.0
25.6
102
24.2
97
<0.132
25.0
28.4
114
27.3
109
<0.112
25.0
23.5
94
22.7
91
<0.124
25.0
25.1
100
24.4
98
<0.159
25.0
24.6
98
24.3
97
<0.0970
25.0
21.3
85
20.1
80
<0.0990
25.0
22.0
88
20.7
83
<0.105
25.0
24.7
99
23.6
94
<0.177
25.0
24.5
98
23.8
95
<0.0420
25.0
21.5
86
21.5
86
<0.172
25.0
23.9
96
23.1
92
<0.0850
25.0
20.5
82
20.2
81
<0.114
25.0
24.4
98
23.6
94
<0.100
25.0
25.0
100
24.5
98
<0.0670
25.0
23.7
95
22.6
90
<3.00
1000
679
68
780
78
<0.0920
25.0
25.9
104
24.8
99
<0.0920
25.0
27.0
108
26.2
105
<0.0980
25.0
26.9
108
25.6
102
<0.169
50.0
40.7
81
39.0
78
<0.190
25.0
25.5
102
24.0
96
<0.0940
25.0
23.3
93
24.0
96
<0.0600
25.0
29.1
116
28.2
113
<0.0650
25.0
28.4
114
27.0
108
<0.0920
25.0
27.0
108
26.0
104
rau
Prep Method:
SM620OB_PREP
Date Prep:
05.07.14
LCSD Sample Id: 655073-1-BSD
Limits
%RPD
RPD
Units
Analysis
Limit
Date
75-127
4
20
ug/L
05.07.14 07:27
62-128
4
20
ug/L
05.07.14 07:27
77-129
1
20
ug/L
05.07.14 07:27
86-120
4
20
ug/L
05.07.14 07:27
82-114
5
20
ug/L
05.07.14 07:27
73-123
13
22
ug/L
05.07.14 07:27
83-125
5
20
ug/L
05.07.14 07:27
57-127
0
20
ug/L
05.07.14 07:27
79-118
11
20
ug/L
05.07.14 07:27
59-125
0
20
ug/L
05.07.14 07:27
84-118
3
20
ug/L
05.07.14 07:27
83-126
1
20
ug/L
05.07.14 07:27
89-126
2
20
ug/L
05.07.14 07:27
56-133
2
20
ug/L
05.07.14 07:27
79-127
3
20
ug/L
05.07.14 07:27
86-118
3
20
ug/L
05.07.14 07:27
90-126
5
20
ug/L
05.07.14 07:27
85-121
2
20
ug/L
05.07.14 07:27
88-121
3
20
ug/L
05.07.14 07:27
76-126
5
20
ug/L
05.07.14 07:27
66-133
24
20
ug/L
05.07.14 07:27
80-128
4
20
ug/L
05.07.14 07:27
70-130
5
20
ug/L
05.07.14 07:27
82-130
4
20
ug/L
05.07.14 07:27
80-128
5
20
ug/L
05.07.14 07:27
74-129
6
20
ug/L
05.07.14 07:27
51-143
4
21
ug/L
05.07.14 07:27
81-123
6
20
ug/1-
05.07.14 07:27
84-114
4
20
ug/L
05.07.14 07:27
89-127
3
20
ug/L
05.07.14 07:27
70-129
3
20
ug/L
05.07.14 07:27
73-140
1
20
ug/L
05.07.14 07:27
53-143
6
20
ug/L
05.07.14 07:27
66-136
6
20
ug/L
05.07.14 07:27
88-118
5
20
ug/L
05.07.14 07:27
73-139
3
20
ug/L
05.07.14 07:27
70-123
0
20
ug/L
05.07.14 07:27
72-118
3 _
20
ug/L
05.07.14 07:27
65-125
1
20
ug/L
05.07.14 07:27
85-125
3 .
20
ug/L
05.07.14 07:27
92-126
2
20
ug/L
05.07.14 07:27
48-143 ,
5
20
ug/L
05.07.14 07:27
61-133
14
20
ug/L
05.07.14 07:27
87-123
4
20
ug/L
05.07.14 07:27
77-125
3
20
ug/L
05.07.14 07:27
82-115
5
20
ug/L
05.07.14 07:27
53-149
4
20
ug/L
05.07.14 07:27
75-119
6
20
ug/L
05,07.14 07:27
52-116
3
20
ug/L
05.07.14 07:27
83-130
3
20
ug/L
05.07.14 07:27
84-122
5
20
ug/L
05.07.14 07:27
86-120
4
20
ug/L
05.07.14 07:27
Flag
F
Page 15 of 24 Final 1.000

QC Summary 484686
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method:
VOCs by GUMS by SM6200B
Prep Method:
SM6200B_PREP
Seq Number:
940303
Matrix:
Water
Date Prep:
05.07.14
MB Sample Id:
655073-1-BLK
LCS Sample
Id:
655073-1-BKS
LCSD Sample Id:
655073-1-BSD
MB
Spike
LCS
LCS
LCSD
LCSD
Limits %RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
25.6
102
24.7
99
85-123
4
20
ug/L
05.07.14 07:27
tert-Butylbenzene
<0.0890
25.0
26.2
105
25.1
100
79-126
4
20
ug/L
05.07.14 07:27
Tetrachloroethene (PCE)
<0.0540
25.0
24.5
98
23.3
93
64-131
5
20
ug/L
05.07.14 07:27
Toluene
<0.0570
25.0
25.9
104
24.5
98
89-116
6
20
ug/L
05.07.14 07:27
trans-1,2-Dichloroethene
<0.188
25.0
22.1
88
20.4
82
78-118
8
20
ug/L
05.07.14 07:27
trans-1,3-Dichloropropene <0.110
25.0
27.9
112
27.4
110
86-127
2
20
ug/L
05.07.14 07:27
Trichloroethene
<0.139
25.0
24.7
99
23.5
94
82-119
5
20
ug/L
05.07.14 07:27
Trichlorofluoromethane
<0.0540
25.0
18.0
72
18.9
76
46-144
5
20
ug/L
05.07.14 07:27
Vinyl Acetate
<0.720
25.0
25.4
102
25.8
103
58-141
2
20
ug/L
05.07.14 07:27
Vinyl Chloride
<0.0810
25.0
24.1
96
23.3
93
76-122
3
20
ug/L
05.07.14 07:27
m,p-Xylenes
<0.176
50.0
50.3
101
48.3
97
90-125
4
20
ug/L
05.07.14 07:27
o-Xylene
<0.122
25.0
25.6
102
24.3
97
86-119
5
20
ug/L
05.07.14 07:27
MB
MB
LCS
LCS
LCSD
LCSD
Limits
Units
Analysis
Surrogate
%Rec
Flag
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
104
99
102
65-134
%
05.07.14 07:27
4-Bromofluorobenzene
109
110
110
70-130
%
05.07.14 07:27
Toluene-D8
110
110
109
87-114
%
05.07.14 07:27
Page 16 of 24 Final 1.000

C_~j
® QC Summary 484686 �; ��
4� 1 ft"OV
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method: VOCs by GUMS by SM6200B Prep Method: SM6200B_PREP
Seq Number: 940303 Matrix: Ground Water Date Prep: 05.07.14
Parent Sample Id: 484686-004 MS Sample Id: 484686-004 S MSD Sample Id: 484686-004 SD
Parent Spike MS MS MSD MSD Limits %RPD RPD Units Analysis Fla
Parameter Result Amount Result %Rec Result %Rec Limit Date g
1,1,1,2-Tetrachloroethane <0.180 25.0 22.4 90 23.0 92 76-126 3 20 ug/L 05.07.14 12:16
1, 1, 1 -Trichloroethane <0.0760 25.0 22.1 88 22.2 89 63-128 0 20 ug/L 05.07.14 12:16
1,1,2,2-Tetrachloroethane <0.0700 25.0 26.8 107 27.8 Ill 79-133 4 20 ug/L 05.07.1412:16
1,1,2-Trichloroethane <0.113 25.0 26.4 106 26.5 106 82-126 0 20 ug/L 05.07.14 12:16
1,1-Dichloroethane <0.121 25.0 23.9 96 24.2 97 77-120 1 20 ug/L 05.07.14 12:16
1,1-Dichloroethene <0.104 25.0 21.3 85 20.7 83 67-123 3 22 ug/L 05.07.14 12:16
I,1-Dichloropropene <0.0600 25.0 23.7 95 24.3 97 76-126 3 20 ug/L 05.07.14 12:16
1,2,3-Trichlorobenzene <0.118 25.0 21.5 86 24.1 96 41-136 11 20 ug/L 05.07.14 12:16
1,2,3-Trichloropropane <0.138 25.0 23.8 95 25.0 100 77-125 5 20 ug/L 05.07.14 12:16
1,2,4-Trichlorobenzene <0.0690 25.0 21.3 85 23.2 93 41-132 9 20 ug/L 05.07.14 12:16
1,2,4-Trimethylbenzene <0.103 25.0 25.3 101 26.8 107 53-141 6 20 ug/L 05.07.14 12:16
1,2-Dibromoethane (EDB) <0.180 25.0 23.9 96 24.5 98 82-130 2 20 ug/L 05.07.14 12:16
1,2-Dichlorobenzene <0.0940 25.0 23.3 93 24.6 98 83-128 5 20 ug/L 05.07.14 12:16
1,2-Dichloroethane <0.0900 25.0 22.7 91 23.5 94 59-134 3 20 ug/L 05.07.14 12:16
1,2-Dichloropropane <0.122 25.0 26.0 104 26.6 106 79-125 2 20 ug/L 05.07.14 12:16
1,3,5-Trimethylbenzene <0.0870 25.0 24.6 98 26.0 104 69-125 6 20 ug/L 05.07.14 12:16
1,3-Dichlorobenzene <0.0980 25.0 23.5 94 24.7 99 83-126 5 20 ug/L 05.07.14 12:16
1,3-Dichloropropane <0.133 25.0 25.0 100 25.6 102 85-124 2 20 ug/L 05.07.14 12:16
1,4-Dichlorobenzene <0.0670 25.0 22.9 92 23.9 96 82-121 4 20 ug/L 05.07.14 12:16
2,2-Dichloropropane <0.0970 25.0 24.1 96 23.6 94 56-122 2 20 ug/L 05.07.14 12:16
2-Butanone (MEK) <0.378 50.0 51.3 103 53.7 107 66-136 5 20 ug/L 05.07.14 12:16
2-Chlorotoluene <0.0880 25.0 25.2 101 26.3 105 73-129 4 20 ug/L 05.07.14 12:16
2-Hexanone <0.352 50.0 58.4 117 60.1 120 63-140 3 20 ug/L 05.07.14 12:16
4-Chlorotoluene <0.0900 25.0 26.4 106 27.7 Ill 76-129 5 20 ug/L 05.07.14 12:16
4-Isopropyholuene <0.0890 25.0 24.0 96 25.6 102 73-126 6 20 ug/L 05.07.14 12:16
4-Methyl-2-pentanone (MIBK) <0.253 50.0 51.1 102 53.1 106 71-140 4 20 ug/L 05.07.14 12:16
Acetone 1.34 50.0 40.9 79 41.1 80 47-138 0 21 ug/L 05.07.14 12:16
Benzene <0.119 25.0 24.1 96 24.5 98 70-135 2 20 ug/L 05.07.14 12:16
Bromobenzene <0.132 25.0 26.4 106 27.4 110 76-120 4 20 ug/L 05.07.14 12:16
Bromochloromethane <0.112 25.0 22.0 88 22.6 90 83-132 3 20 ug/L 05.07.14 12:16
Bromodichloromethane <0.124 25.0 23.4 94 24.3 97 66-132 4 20 ug/L 05.07.14 12:16
Bromoform <0.159 25.0 22.8 91 23.3 93 63-143 2 20 ug/L 05.07.14 12:16
Bromomethane <0.0970 25.0 18.9 76 19.1 76 60-134 1 20 ug/L 05.07.14 12:16
Carbon tetrachloride <0.0990 25.0 21.2 85 21.4 86 59-139 1 20 ug/L 05.07.14 12:16
Chlorobenzene <0.105 25.0 22.9 92 23.6 94 83-120 3 20 ug/L 05.07.14 12:16
Chlorodibromomethane <0.177 25.0 22.7 91 23.1 92 68-140 2 20 ug/L 05.07.14 12:16
Chloroethane <0.0420 25.0 19.3 77 19.8 79 67-125 3 20 ug/L 05.07.14 12:16
Chloroform <0.172 25.0 22.9 92 23.8 95 72-120 4 20 ug/L 05.07.14 12:16
Chloromethane <0.0850 25.0 20.1 80 19.6 78 59-128 3 20 ug/L 05.07.14 12:16
cis-1,2-Dichloroethene <0.114 25.0 23.3 93 23.9 96 80-125 3 20 ug/L 05.07.14 12:16
cis-1,3-Dichloropropene <0.100 25.0 23.3 93 23.6 94 74-122 1 20 ug/L 05.07.14 12:16
Dichlorodifluoromethane <0.0670 25.0 22.7 91 22.7 91 48-138 0 20 ug/L 05.07.14 12:16
Ethanol <3.00 1000 733 73 654 65 55-140 11 20 ug/L 05.07.14 12:16
Etylbenzene <0.0920 25.0 24.2 97 24.8 99 70-140 2 20 ug/L 05.07.14 12:16
Isopropyl ether <0.0920 25.0 26.8 107 27.2 109 70-132 1 20 ug/L 05.07.14 12:16
Isopropylbenzene <0.0980 25.0 24.4 98 25.7 103 75-117 5 20 ug/L 05.07.14 12:16
Methyl tert-butyl ether (MTBE) <0.169 50.0 43.1 86 42.3 85 51-155 2 20 ug/L, 05.07.14 12:16
Methylene Chloride <0.190 25.0 25.4 102 25.1 100 71-126 1 20 ug/L 05.07.14 12:16
Naphthalene <0.0940 25.0 20.9 84 22.6 90 34-135 8 20 ug/L 05.07.14 12:16
n-Butylbenzene <0.0600 25.0 27.0 108 28.9 116 73-128 7 20 ug/L 05.07.14 12:16
n-Propylbenzene <0.0650 25.0 26.1 104 27.7 111 75-125 6 20 ug/L 05.07.14 12:16
sec-Butylbenzene <0.0920 25.0 24.5 98 26.0 104 77-122 6 20 ug/L 05.07.14 12:16
Page 17 of 24 Final 1.000

, •
Florida Testing Services, LLC
QC Summary 484686
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method:
VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Seq Number:
940303
Matrix:
Ground Water
Date Prep: 05.07.14
Parent Sample Id:
484686-004
MS Sample Id:
484686-004 S
MSD Sample Id: 484686-004 SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
23.5
94
24.2
97
54-137
3
20
ug/L
05.07.14 12:16
tert-Butylbenzene
<0.0890
25.0
23.7
95
25.0
100
74-124
5
20
ug/L
05.07.14 12:16
Tetrachloroethene (PCE)
<0.0540
25.0
22.3
89
22.8
91
57-130
2
20
ug/L
05.07.14 12:16
Toluene
<0.0570
25.0
24.2
97
24.3
97
81-125
0
20
ug/L
05.07.14 12:16
trans-1,2-Dichloroethene
<0.188
25.0
21.2
85
21.3
85
69-122
0
20
ug/L
05.07.14 12:16
trans-1,3-Dichloropropene
<0.110
25.0
26.1
104
26.6
106
73-129
2
20
ug/L
05.07.14 12:16
Trichloroethene
<0.139
25.0
23.1
92
23.6
94
73-124
2
20
ug/L
05.07.14 12:16
Trichlorofluoromethane
<0.0540
25.0
18.1
72
17.2
69
49-139
5
20
ug/L
05.07.14 12:16
Vinyl Acetate
<0.720
25.0
24.7
99
24.8
99
57-134
0
20
ug/L
05.07.14 12:16
Vinyl Chloride
<0.0810
25.0
22.1
88
22.1
88
70-121
0
20
ug/L
05.07.14 12:16
m,p-Xylenes
<0.176
50.0
46.5
93
48.0
96
65-151
3
20
ug/L
05.07.14 12:16
o-Xylene
<0.122
25.0
23.5
94
24.2
97
58-148
3
20
ug/L
05.07.14 12:16
MS
MS
MSD
MSD
Limits
Units
Analysis
Surrogate
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
99
100
65-134
%
05.07.14 12:16
4-Bromofluorobenzene
110
111
60-148
%
05.07.14 12:16
Toluene-D8
110
109
87-114
%
05.07.14 12:16
Page 18 of 24 Final 1.000

•
Blank Summary
484686
_y'
4a�_.
eeu
eum .um
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.,
Mebane, NC
Coliseum Shell
Sample Id: 655073-1-BLK
Matrix: WATER
Lab Sample Id: 655073-1-BLK
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
Analyst: MLA
Date Prep: 05.07.14 06:35
Seq Number: 940303
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
05.07.14 09:20
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
05.07.14 09:20
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
05.07.14 09:20
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
05.07.14 09:20
U
1
I,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
05.07.14 09:20
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
05.07.14 09:20
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
05.07.14 09:20
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
05.07.14 09:20
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
05.07.14 09:20
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
05.07.14 09:20
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
05.07.14 09:20
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
05.07.14 09:20
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
05.07.14 09:20
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
05.07.14 09:20
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
05.07.14 09:20
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
05.07.14 09:20
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
05.07.14 09:20
U
I
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
05.07.14 09:20
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
05.07.14 09:20
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
05.07.14 09:20
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
05.07.14 09:20
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
05.07.14 09:20
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
05.07.14 09:20
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
05.07.14 09:20
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
05.07.14 09:20
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
05.07.14 09:20
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
05.07.14 09:20
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
05.07.14 09:20
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L,
05.07.14 09:20
U
I
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
05.07.14 09:20
U
1
Bromodichloromethane
75-274
U
0.500
0.124
ug/L
05.07.14 09:20
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
05.07.14 09:20
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
05.07.14 09:20
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
05.07.14 09:20
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
05.07.14 09:20
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
05.07.14 09:20
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
05.07.14 09:20
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L,
05.07.14 09:20
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
05.07.14 09:20
U
1
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
05.07.14 09:20
U
1
Page 19 of 24 Final 1.000

•
Florida Testing Services, LLC
Sample Id: 655073-1-BLK
Lab Sample Id: 655073-1-BLK
Blank Summary 484686
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: WATER
t,
r�au
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
Analyst: MLA
Date
Prep: 05.07.14 06:35
Seq Number: 940303
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
cis-I,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
05.07.14 09:20
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
05.07.14 09:20
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
05.07.14 09:20
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
05.07.14 09:20
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
05.07.14 09:20
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
05.07.14 09:20
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
05.07.14 09:20
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
05.07.14 09:20
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
05.07.14 09:20
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
05.07.14 09:20
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
05.07.14 09:20
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
05.07.14 09:20
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
05.07.14 09:20
U
I
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
05.07.14 09:20
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
05.07.14 09:20
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L,
05.07.14 09:20
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
05.07.14 09:20
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
05.07.14 09:20
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
05.07.14 09:20
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
05.07.14 09:20
U
1
Vinyl Acetate
108-054
U
1.00
0.720
ug/L
05.07.14 09:20
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
05.07.14 09:20
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
05.07.14 09:20
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
05.07.14 09:20
U
1
Page 20 of 24 Final 1.000

• Blank Summary 484686�
PJIA
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: 655237-1-BLK Matrix: WATER
Lab Sample Id: 655237-1-BLK
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR
Analyst: 4150 Date Prep: 05.12.14 11:14
Seq Number: 940652
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Lead 7439-92-1 U 0.0100 0.00330 mg/L 05.12.1414:41 U 1
Page 21 of 24 Final 1.000

� k5n
Blank Summary 484686 a'
Sample Id: 940584-1-BLK
Lab Sample Id: 940584-1-BLK
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: WATER
Analytical Method: TSS by SM2540D Prep Method:
Tech: ANS
Analyst: ANS Date Prep:
Seq Number: 940584 SUB: E871002
Parameter Cas Number Result RL
Total Suspended Solids U 4.00
MDL Units Analysis Flag Dil
Date
3.50 mg/L 05.12.14 09:41 U 1
Page 22 of 24 Final 1.000

'
XENCO CHAIN OF CUSTODY
j: t
! page of
LABORATORIES..
.
FED=EX I UPS: Tracking # Baffle Order Control
6017 F'mancilil Drive, Norcrm,.GA 30071 (770449-8800)
4143 Greenbrier Dr., Stafford, TX 77477 = (281-240-4200)
Xenco Quote # Xenco Work Order#
l�(/I
9701 Harry Hines Blvd, Dallas'TX 75220 (21d-902-0300)
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12600 West 1-20 East, Odessa TX 79765 432-563-1800)
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DIN o Drinking Water
i 'RSi9h� . ' . fent / Re ort n Information !9i h' -i!
Company Name Project Number (ID): C G L
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Terractuest Environmental Consultants, P.C.
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City: Mebane, NC 27302
bster 1
[e-mail]
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Phono: 919-563.90p91 rax: 019-t5/63-9095 Report & invoice to: Megan YVc
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Analytical Report 486773
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Coliseum Shell
01195
13-JUN-14
Collected By: Client
XENCO'
Laboratories
Florida Testing Services, LLC
\@ PrMom
QR914 ,,,
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (Tl04704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610)
Xenco-Atlanta (EPA Lab Code: GA00046):
-Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (Tl04704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (Tl04704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Page 1 of 25 Final 1.000

13-JUN-14
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 486773
Coliseum Shell
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 486773. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 486773 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Eben Buchanan
Project Manager
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 2 of 25 Final 1.000

• Sample Cross Reference 486773 �+
`(4Wr�u
Florida Testing ServicesTerraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id
Matrix
Date Collected Sample Depth
Lab Sample Id
Influent
W
06-04-1410:24
486773-001
After AST
W
06-04-14 10:13
486773-002
After 1st Carbon
W
06-04-14 10:19
486773-003
Effluent
W
06-04-1410:31
486773-004
vasioR: 1. i
Page 3 of 25 Final 1.000

Flagging Criteria��e�'�
Florida Testing Services, LLC
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Lin -lit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix
- Latin America
Phone
Fax
4143 Greenbriar Dr, Stafford, TX 77477 (281) 2404200
[phone]
9701 Harry Hines Blvd, Dallas, TX 75220 [phone]
[phone]
5332 Blackberry Drive, San Antonio TX 78238 [phone]
[phone]
2505 North Falkenburg Rd, Tampa, FL 33619 [phone]
[phone]
12600 West I-20 East, Odessa, TX 79765 [phone]
[phone]
6017 Financial Drive, Norcross, GA 30071 [phone]
[phone]
3725 E. Atlanta Ave, Phoenix, AZ 85040 [phone]
Page 4 of 25 Final 1.000

Certificate of Analytical Results 486773 P�
BQRRL wewm am..,
Florida Testing Services, LLC
Sample Id: Influent
Lab Sample Id: 486773-001
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Ground Water Date Received:06.05.14 10.20
Date Collected: 06.04.14 10.24
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter Cas Number
Date Prep:
Result
06.09.14 06.33
RL MDL
Units
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
06.09.1413.05
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
06.09.1413.05
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
06.09.1413.05
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
06.09.1413.05
U
I
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
06.09.1413.05
U
I
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
06.09.1413.05
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
06.09.1413.05
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
06.09.14 13.05
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
06.09.14 13.05
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
06.09.14 13.05
U
1
1,2,4-Trimethylbenzene
95-63-6
23.0
0.500
0.103
ug/L
06.09.14 13.05
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
06.09.14 13.05
U
I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
06.09.14 13.05
U
I
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
06.09.1413.05
U
I
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
06.09.14 13.05
U
I
1,3,5-Trimethylbenzene
108-67-8
6.39
0.500
0.0870
ug/L
06.09.1413.05
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
06.09.1413.05
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
06.09.1413.05
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
06.09.14 13.05
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
06.09.1413.05
U
1
2-Butanone (MEI)
78-93-3
93.8
20.0
0.378
ug/L
06.09.14 13.05
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
06.09.1413.05
U
I
2-Hexanone
591-78-6
23.0
0.400
0.352
ug/L
06.09.1413.05
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
06.09.14 13.05
U
1
4-Isopropyltoluene
99-87-6
0.260
0.500
0.0890
ug/L
06.09.14 13.05
J
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
06.09.14 13.05
U
1
Acetone
67-64-1
161
2.00
0.352
ug/L
06.09.1413.05
1
Benzene
71-43-2
20.8
0.500
0.119
ug/L
06.09.1413.05
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
06.09.1413.05
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
06.09.1413.05
U
1
Brornodichloromethane
75-27-4
U
0.500
0.124
ug/L
06.09.1413.05
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
06.09.1413.05
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
06.09.1413.05
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
06.09.14 13.05
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
06.09.14 13.05
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
06.09.1413.05
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
06.09.1413.05
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
06.09.1413.05
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
06.09.1413.05
U
1
Page 5 of 25 Final 1.000

P«_REp
Certificate of Analytical Results 486773 t
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Influent Matrix: Ground Water Date Received:06.05.14 10.20
Lab Sample Id: 486773-001 Date Collected: 06.04.14 10.24
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter
Cas Numbe
cis-1,2-Dichloroethene
156-59-2
cis- 1,3 -Dichloropropene
10061-01-5
Dichlorodifluoromethane
75-71-8
Ethanol
64-17-5
Ethylbenzene
100-41-4
Isopropyl ether
108-20-3
Isopropylbenzene
98-82-8
Methyl tert-butyl ether (MTBE)
1634-04-4
Methylene Chloride
75-09-2
Naphthalene
91-20-3
n-Butylbenzene
104-51-8
u-Propylbenzene
103-65-1
sec-Butylbenzene
135-98-8
Styrene
100-42-5
tert-Butylbenzene
98-06-6
Tetrachloroethene (PCE)
127-18-4
Toluene
108-88-3
trans-1,2-Dichloroethene
156-60-5
trans-1,3-Dichloropropene
10061-02-6
Trichloroethene
79-01-6
Trichlorofluoromethane
75-69-4
Vinyl Acetate
108-05-4
Vinyl Chloride
75-01-4
m,p-Xylenes
179601-23-1
o-Xylene
95-47-6
Surrogate
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Prep Method: SM6200B PREP
% Moisture:
Date Prep: 06.09.14 06.33
Result
RL
MDL
Units
Analysis Date
Flag
Dil
U
0.500
0.114
ug/L
06.09.1413.05
U
I
U
1.00
0.100
ug/L
06.09.1413.05
U
1
U
1.00
0.0670
ug/L
06.09.1413.05
U
1
U
50.0
3.00
ug/L
06.09.1413.05
U
1
12.4
0.500
0.0920
ug/L
06.09.1413.05
1
31.3
0.500
0.0920
ug/L
06.09.1413.05
1
0.460
0.500
0.0980
ug/L
06.09.1413.05
J
1
1580
25.0
8.45
ug/L
06.09.1414.39
D
50
U
0.500
0.190
ug/L
06.09.1413.05
U
1
35.6
2.00
0.0940
ug/1-
06.09.1413.05
1
U
2.00
0.0600
ug/L,
06.09.1413.05
U
1
1.68
1.00
0.0650
ug/L
06.09.1413.05
1
U
0.500
0.0920
ug/L
06.09.1413.05
U
1
U
0.500
0.0740
ug/L
06.09.1413.05
U
1
U
0.500
0.0890
ug/1-
06.09.1413.05
U
1
U
0.500
0.0540
ug/L
06.09.1413.05
U
1
67.5
0.500
0.0570
ug/L
06.09.1413.05
1
U
0.500
0.188
ug/L
06.09.1413.05
U
I
U
1.00
0.110
ug/L
06.09.1413.05
U
1
U
0.500
0.139
ug/L
06.09.1413.05
U
1
U
0.500
0.0540
ug/L
06.09.1413.05
U
1
U
1.00
0.720
ug/L
06.09.1413.05
U
I
U
0.500
0.0810
ug/L
06.09.1413.05
U
1
51.3
1.00
0.176
ug/L
06.09.1413.05
1
35.3
0.500
0.122
ug/L
06.09.1413.05
1
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
17060-07-0
95
%
65-134
06.09.1413.05
460-00-4
98
%
60-148
06.09.1413.05
2037-26-5
97
%
87-114
06.09.1413.05
Page 6 of 25 Final 1.000

Certificate of Analytical Results 486773
/ PJU
Q� eaewunvs.v
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST Matrix: Ground Water Date Received: 06.05.14 10.20
Lab Sample Id: 486773-002 Date Collected: 06.04.14 10.13
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter Cas Number
Prep Method: SM620OB_PREP
% Moisture:
Date Prep: 06.09.14 06.33
Result RL MDL Units Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
06.09.1410.44
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L,
06.09.14 10.44
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
06.09.1410.44
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
06.09.14 10.44
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
06.09.1410.44
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
06.09.14 10.44
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
06.09.14 10.44
U
I
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
06.09.14 10.44
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
06.09.14 10.44
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
06.09.14 10.44
U
1
1,2,4-Trimethylbenzene
95-63-6
0.280
0.500
0.103
ug/L
06.09.1410.44
J
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
06.09.14 10.44
U
I
1,2-Dichloroben2ene
95-50-1
U
0.500
0.0940
ug/L
06.09.14 10.44
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
06.09.1410.44
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
06.09.14 10.44
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
06.09.14 10.44
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
06.09.14 10.44
U
I
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
06.09.14 10.44
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
06.09.1410.44
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
06.09.14 10.44
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L,
06.09.14 10.44
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
06.09.1410.44
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
06.09.1410.44
U
I
4-Chlorotoluene
106-434
U
0.500
0.0900
ug/L,
06.09.14 10.44
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
06.09.14 10.44
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
06.09.14 10.44
U
1
Acetone
67-64-1
28.7
2.00
0.352
ug/L
06.09.1410.44
1
Benzene
71-43-2
0.140
0.500
0.119
ug/L
06.09.1410.44
J
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
06.09.1410.44
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
06.09.1410.44
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
06.09.1410.44
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
06.09.1410.44
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
06.09.1410.44
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
06.09.14 10.44
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L.
06.09.1410.44
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
06.09.1410.44
U
1
Chloroetbane
75-00-3
U
0.500
0.0420
ug/L
06.09.1410.44
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
06.09.1410.44
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
06.09.1410.44
U
1
Page 7 of 25 Final 1.000

Certificate of Analytical Results 486773 �4e
Terraquest Environmental Consultants, P.C.,
Coliseum Shell
Sample Id: After AST Matrix: Ground Water
Lab Sample Id: 486773-002 Date Collected: 06.04.14 10.13
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA Date Prep: 06.09.14 06.33
Seq Number: 942952
Parameter Cas Number Result RL MDL Units
Mebane, NC
Date Received:06.05.14 10.20
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
06.09.1410.44
U
I
cis- 1, 3-Dichloropropene
10061-01-5
U
I.00
0.100
ug/L
06.09.1410.44
U
I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
06.09.1410.44
U
I
Ethanol
64-17-5
U
50.0
3.00
ug/L
06.09.1410.44
U
I
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
06.09.1410.44
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
06.09.14 10.44
U
I
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L,
06.09.1410.44
U
I
Methyl tert-butyl ether (INITBE)
1634-04-4
8.16
0.500
0.169
ug/L
06.09.14 10.44
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
06.09.14 10.44
U
1
Naphthalene
91-20-3
0.450
2.00
0.0940
ug/L
06.09.1410.44
J
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
06.09.1410.44
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
06.09.1410.44
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
06.09.1410.44
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
06.09.1410.44
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L.
06.09.1410.44
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
06.09.14 10.44
U
1
Toluene
108-88-3
0.460
0.500
0.0570
ug/L
06.09.1410.44
J
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
06.09.1410.44
U
I
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
06.09.14 10.44
U
I
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
06.09.1410.44
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
06.09.1410.44
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
06.09.14 10.44
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
06.09.14 10.44
U
1
m,p-Xylenes
179601-23-1
0.400
1.00
0.176
ug/L
06.09.1410.44
J
1
o-Xylene
95-47-6
0.280
0.500
0.122
ug/L
06.09.1410.44
J
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
97
%
65-134
06.09.1410.44
4-Bromofluorobenzene
460-00-4
99
%
60-148
06.09.1410.44
Toluene-D8
2037-26-5
99
%
87-114
06.09.1410.44
Page 8 of 25 Final 1.000

Certificate of Analytical Results 486773 „u
8977-
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st Carbon Matrix: Ground Water Date Received:06.05.14 10.20
Lab Sample Id: 486773-003 Date Collected: 06.04.14 10.19
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter Cas Number
Prep Method: SM6200B_PREP
% Moisture:
Date Prep: 06.09.14 06.33
Result RL MDL Units Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
06.09.1410.16
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
06.09.14 10.16
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
06.09.1410.16
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
06.09.14 10.16
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
06.09.14 10.16
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
06.09.14 10.16
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
06.09.1410.16
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
06.09.1410.16
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
06.09.14 10.16
U
1
1,2,4-Tichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
06.09.1410.16
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L.
06.09.1410.16
U
1
1,2-Dibromoethane (EDB)
106-934
U
1.00
0.180
ug/L
06.09.14 10.16
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
06.09.14 10.16
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
06.09.1410.16
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
06.09.14 10.16
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
06.09.1410.16
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
06.09.1410.16
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
06.09.14 10.16
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
06.09.14 10.16
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
06.09.1410.16
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
06.09.14 10.16
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
06.09.14 10.16
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L,
06.09.1410.16
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
06.09.1410.16
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L,
06.09.1410.16
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
06.09.14 10.16
U
1
Acetone
67-64-1
13.6
2.00
0.352
ug/L
06.09.1410.16
1
Benzene
71-43-2
U
0.500
0.119
ug/L
06.09.14 10.16
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
06.09.1410.16
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
06.09.1410.16
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
06.09.1410.16
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
06.09.1410.16
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
06.09.1410.16
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
06.09.14 10.16
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
06.09.14 10.16
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
06.09.1410.16
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
06.09.1410.16
U
1
Chloroform
67-66-3
2.02
0.500
0.172
ug/L
06.09.1410.16
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
06.09.1410.16
U
1
Page 9 of 25 Final 1.000

r
Certificate of Analytical Results 486773 4B
r�u
-RRrct4-'
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st Carbon Matrix: Ground Water Date Received:06.05.14 10.20
Lab Sample Id: 486773-003 Date Collected: 06.04.14 10.19
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter Cas Number
Date Prep:
Result
06.09.14 06.33
RL MDL
Prep Method: SM620OB_PREP
% Moisture:
Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
06.09.1410.16
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
06.09.14 10.16
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
06.09.1410.16
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
06.09.1410.16
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
06.09.14 10.16
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
06.09.14 10.16
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
06.09.14 10.16
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
4.01
0.500
0.169
ug/L
06.09.14 10.16
1
Methylene Chloride
75-09-2
0.270
0.500
0.190
ug/L
06.09.14 10.16
J
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L.
06.09.1410.16
U
I
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
06.09.14 10.16
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
06.09.14 10.16
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
06.09.1410.16
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L.
06.09.1410.16
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
06.09.1410.16
U
I
Tetrachloroethene(PCE)
127-18-4
U
0.500
0.0540
ug/L
06.09.14 10.16
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
06.09.1410.16
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
06.09.14 10.16
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
06.09.14 10.16
U
I
Tichloroethene
79-01-6
U
0.500
0.139
ug/L
06.09.1410.16
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
06.09.1410.16
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
06.09.14 10.16
U
I
Vinyl Chloride
75-014
U
0.500
0.0810
ug/L
06.09.1410.16
U
1
m,p-Xylenes
179601-23-I
U
1.00
0.176
ug/L
06.09.1410.16
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
06.09.1410.16
U
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
97
%
65-134
06.09.1410.16
4-Bromofluorobenzene
460-00-4
101
%
60-148
06.09.14 10.16
Toluene-D8
2037-26-5
98
%
87-114
06.09.1410.16
Page 10 of 25 Final 1.000

Certificate of Analytical Results 486773 P,u
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:06.05.14 10.20
Lab Sample Id: 486773-004 Date Collected: 06.04.14 10.31
Analytical Method: TSS by SM2540D
Tech: ANS
Analyst: ANS
Seq Number: 943160
Parameter
% Moisture:
SUB: E871002
Cas Number Result RL MDL Units Analysis Date Flag Dil
Total Suspended Solids
4.00 4.00 3.50
mg/L 06.11.14 17.09 J 1
Analytical Method: Lead by SW-846 6010C
Prep Method: SW3010A
Tech: JDR
% Moisture:
Analyst: 4150
Date Prep: 06.10.14 12.42
Seq Number: 943100
Parameter Cas Number
Result RL NIDL
Units Analysis Date Flag Dil
Lead 7439-92-1
U 0.0100 0.00330
mg/L 06.11.1411.43 U 1
Page 11 of 25 Final 1.000

Certificate of Analytical Results 486773 �e �
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:06.05.14 10.20
Lab Sample Id: 486773-004 Date Collected: 06.04.14 10.31
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA
Seq Number: 942952
Parameter Cas Number
Date Prep:
Result
06.09.14 06.33
RL MDL
Units
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
06.09.14 09.47
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
06.09.1409.47
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
06.09.14 09.47
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L,
06.09.14 09.47
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
06.09.14 09.47
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
06.09.1409.47
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
06.09.1409.47
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
06.09.14 09.47
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
06.09.14 09.47
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
06.09.14 09.47
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
06.09.14 09.47
U
1
1,2-Dibromoethane (EDB)
106-934
U
1.00
0.180
ug/L
06.09.14 09.47
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
06.09.14 09.47
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
06.09.14 09.47
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
06.09.14 09.47
U
I
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
06.09.14 09.47
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
06.09.14 09.47
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
06.09.14 09.47
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
06.09.14 09.47
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
06.09.14 09.47
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
06.09.14 09.47
U
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
06.09.14 09.47
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
06.09.14 09.47
U
1
4-Chlorotoluene
106-434
U
0.500
0.0900
ug/L
06.09.14 09.47
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
06.09.14 09.47
U
I
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
06.09.14 09.47
U
1
Acetone
67-64-1
9.11
2.00
0.352
ug/L
06.09.14 09.47
1
Benzene
71-43-2
U
0.500
0.119
ug/L
06.09.14 09.47
U
I
Bromobenzene
108-86-I
U
0.500
0.132
ug/L
06.09.14 09.47
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
06.09.14 09.47
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
06.09.14 09.47
U
1
Bromofonn
75-25-2
U
2.00
0.159
ug/L
06.09.14 09.47
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
06.09.14 09.47
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
06.09.14 09.47
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
06.09.14 09.47
U
I
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
06.09.14 09.47
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
06.09.14 09.47
U
1
Chlorofonn
67-66-3
U
0.500
0.172
ug/L
06.09.14 09.47
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
06.09.14 09.47
U
1
Page 12 of 25 Final 1.000

Certificate of Analytical Results 486773 �eW-P
Florida Testing Services, LLC
Sample Id: Effluent
Lab Sample Id: 486773-004
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Ground Water
Date Collected: 06.04.14 10.31
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: MLA Date Prep: 06.09.14 06.33
Seq Number: 942952
Date Received:06.05.14 10.20
Prep Method: SM6200B_PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
06.09.14 09.47
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
06.09.14 09.47
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
06.09.14 09.47
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
06.09.14 09.47
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
06.09.14 09.47
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
06.09.14 09.47
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
06.09.14 09.47
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
06.09.14 09.47
U
1
Methylene Chloride
75-09-2
0.470
0.500
0.190
ug/L
06.09.14 09.47
J
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
06.09.14 09.47
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
06.09.14 09.47
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
06.09.14 09.47
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
06.09.14 09.47
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
06.09.14 09.47
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
06.09.14 09.47
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
06.09.14 09.47
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
06.09.14 09.47
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
06.09.14 09.47
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
06.09.14 09.47
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
06.09.14 09.47
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
06.09.14 09.47
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
06.09.14 09.47
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
06.09.14 09.47
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
06.09.14 09.47
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
06.09.14 09.47
U
I
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dicbloroethane-D4
17060-07-0
97
%
65-134
06.09.14 09.47
4-Bromofluorobenzene
460-004
102
%
60-148
06.09.14 09.47
Toluene-D8
2037-26-5
100
%
87-114
06.09.14 09.47
Page 13 of 25 Final 1.000

QC Summary 486773
r�u
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method: TSS by SM2540D
Seq Number: 943160
Matrix:
Water
MB Sample Id: 943160-1-BLK
LCS Sample Id:
943160-1-BKS
LCSD Sample Id: 943160-1-BSD
MB Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Parameter Result Amount
Result %Rec
Result %Rec
Limit Date
Total Suspended Solids <3.50 100
84.0 84
88.0 88
80-120 5 10 mg/L 06.11.14 17:09
Analytical Method: TSS by SM2540D
Seq Number: 943160
Parent Sample Id: 486730-001
Parent
Parameter
Result
Total Suspended Solids <3.50
Analytical Method: TSS by SM2540D
Seq Number: 943160
Parent Sample Id: 486811-003
Parent
Parameter
Result
Total Suspended Solids 410
Matrix: Water
MD Sample Id: 486730-001 D
MD
Result
<3.50
Matrix: Water
MD Sample Id: 486811-003 D
MD
Result
409
%RPD RPD Units Analysis Flag
Limit Date
0 10 mg/L 06.11.1417:09 U
%RPD RPD Units Analysis Flag
Limit Date
0 10 mg/L 06.11.1417:09
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
943100
Matrix:
Water
Date Prep: 06.10.14
MB Sample Id:
656764-1-BLK
LCS Sample Id:
656764-1-BKS
LCSD Sample Id: 656764-1-BSD
M B Spike
LCS LCS
LCSD LCSD Limits
%RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
1.01 101
1.01 101 80-120
0 20 mg/L 06.11.14 11:39
Analytical Method: Lead by SW-846 6010C
Seq Number: 943100 Matrix: Ground Water
Parent Sample Id: 486773-004 MD Sample Id: 486773-004 D
Parent MD
Parameter
Result Result
Lead <0.00330 <0.00330
Prep Method: SW3010A
Date Prep: 06.10.14
%RPD RPD Units Analysis Flag
Limit Date
0 20 mg/L 06.11.1411:45 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
943100
Matrix:
Ground Water
Date Prep: 06.10.14
Parent Sample Id:
486773-004
MS Sample Id:
486773-004 S
MSD Sample Id: 486773-004 SD
Parent Spike
MS MS
MSD MSD Limits
%RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
1.01 101
1.02 102 80-120
1 20 mg/L, 06.11.1411:47
Page 14 of 25 Final 1.000

t t •
Florida Testing Services, LLC
QC Summary 486773
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method: VOCs by GUMS by SM6200B
Seq Number: 942952
MB Sample Id: 656737-1-BLK
Parameter
MB
Spike
Result
Amount
1, 1, 1,2-Tetrachloroethane
<0.180
25.0
1, 1, 1 -Trichloroethane
<0.0760
25.0
1,1,2,2-Tetrachloroethane
<0.0700
25.0
1,1,2-Trichloroethane
<0.113
25.0
1,1-Dichloroethane
<0.121
25.0
1,1-Dichloroethene
<0.104
25.0
1,1-Dichloropropene
<0.0600
25.0
1,2,3-Trichlorobenzene
<0.118
25.0
1,2,3-Trichloropropane
<0.138
25.0
1,2,4-Trichlorobenzene
<0.0690
25.0
1,2,4-Trimethylbenzene
<0.103
25.0
1,2-Dibromoethane (EDB)
<0.180
25.0
1,2-Dichlorobenzene
<0.0940
25.0
1,2-Dichloroethane
<0.0900
25.0
1,2-Dichloropropane
<0.122
25.0
1,3,5-Trimethylbenzene
<0.0870
25.0
1,3-Dichlorobenzene
<0.0980
25.0
1,3-Dichloropropane
<0.133
25.0
1,4-Dichlorobenzene
<0.0670
25.0
2,2-Dichloropropane
<0.0970
25.0
2-Butanone (MEK)
<0.378
50.0
2-Chlorotoluene
<0.0880
25.0
2-Hexanone
<0.352
50.0
4-Chlorotoluene
<0.0900
25.0
4-Isopropyltoluene
<0.0890
25.0
4-Methyl-2-pentanone (MIBK)
<0.253
50.0
Acetone
<0.352
50.0
Benzene
<0.119
25.0
Bromobenzene
<0.132
25.0
Bromochloromethane
<0.112
25.0
Bromodichloromethane
<0.124
25.0
Bromoform
<0.159
25.0
Bromomethane
<0.0970
25.0
Carbon tetrachloride
<0.0990
25.0
Chlorobenzene
<0.105
25.0
Chlorodibromomethane
<0.177
25.0
Chloroethane
<0.0420
25.0
Chloroform
<0.172
25.0
Chloromethane
<0.0850
25.0
cis-1,2-Dichloroethene
<0.114
25.0
cis-1,3-Dichloropropene
<0.100
25.0
Dichlorodifluoromethane
<0.0670
25.0
Ethanol
<3.00
1000
Ethylbenzene
<0.0920
25.0
Isopropyl ether
<0.0920
25.0
Isopropylbenzene
<0.0980
25.0
Methyl tert-butyl ether (MTBE)
<0.169
50.0
Methylene Chloride
<0.190
25.0
Naphthalene
<0.0940
25.0
n-Butylbenzene
<0.0600
25.0
n-Propylbenzene
<0.0650
25.0
sec-Butylbenzene
<0.0920
25.0
Prep Method:
SM6200B_PREP
Matrix:
Water
Date Prep:
06.09.14
LCS Sample Id:
656737-1-BKS
LCSD Sample Id: 656737-1-BSD
LCS
LCS
LCSD
LCSD
Limits
%RPD
RPD
Units
Analysis Flag
Result
%Ree
Result
%Rec
Limit
Date
27.8
111
27.5
110
75-127
1
20
ug/L
06.09.14 07:25
26.9
108
27.2
109
62-128
1
20
ug/L
06.09.14 07:25
28.4
114
28.2
113
77-129
1
20
ug/L
06.09.14 07:25
25.9
104
25.6
102
86-120
1
20
ug/L
06.09.14 07:25
27.8
111
27.0
108
82-114
3
20
ug/L
06.09.14 07:25
28.5
114
29.8
119
73-123
4
22
ug/L
06.09.14 07:25
27.5
110
27.3
109
83-125
1
20
ug/L
06.09.14 07:25
27.4
110
27.8
111
57-127
1
20
ug/L
06.09.14 07:25
22.3
89
24.8
99
79-118
11
20
ug/L
06.09.14 07:25
28.9
116
29.0
116
59-125
0
20
ug/L
06.09.14 07:25
27.9
112
27.9
112
84-118
0
20
ug/L
06.09.14 07:25
26.6
106
26.5
106
83-126
0
20
ug/L
06.09.14 07:25
26.9
108
27.1
108
89-126
1
20
ug/L
06.09.14 07:25
25.4
102
25.0
100
56-133
2
20
ug/L
06.09.14 07:25
26.8
107
26.6
106
79-127
1
20
ug/L
06.09.14 07:25
28.1
112
28.0
112
86-118
0
20
ug/L
06.09.14 07:25
27.8
111
27.8
111
90-126
0
20
ug/L
06.09.14 07:25
25.8
103
25.0
100
85-121
3
20
ug/1-
06.09.14 07:25
27.2
109
27.3
109
88-121
0
20
ug/L
06.09.14 07:25
29.4
118
29.8
119
76-126
1
20
ug/L
06.09.14 07:25
46.1
92
47.7
95
66-133
3
20
ug/L
06.09.14 07:25
27.0
108
27.5
110
80-128
2
20
ug/L
06.09.14 07:25
49.8
100
48.9
98
70-130
2
20
ug/L
06.09.14 07:25
28.8
115
28.8
115
82-130
0
20
ug/L
06.09.14 07:25
29.0
116
29.1
116
80-128
0
20
ug/L
06.09.14 07:25
45.6
91
45.6
91
74-129
0
20
ug/L
06.09.14 07:25
46.5
93
48.6
97
51-143
4
21
ug/L
06.09.14 07:25
27.2
109
26.6
106
81-123
2
20
ug/L
06.09.14 07:25
26.8
107
26.9
108
84-114
0
20
ug/L
06.09.14 07:25
28.2
113
27.7
Ill
89-127
2
20
ug/L
06.09.14 07:25
27.4
110
27.4
110
70-129
0
20
ug/1-
06.09.14 07:25
22.7
91
22.9
92
73-140
1
20
ug/L
06.09.14 07:25
23.9
96
22.5
90
53-143
6
20
ug/L
06.09.14 07:25
28.1
112
28.0
112
66-136
0
20
ug/L
06.09.14 07:25
27.6
110
27.1
108
88-118
2
20
ug/L
06.09.14 07:25
28.2
113
27.6
110
73-139
2
20
ug/L
06.09.14 07:25
22.6
90
20.5
82
70-123
10
20
ug/L
06.09.14 07:25
27.0
108
26.5
106
72-118
2
20
ug/L
06.09.14 07:25
25.8
103
25.7
103
65-125
0
20
ug/1-
06.09.14 07:25
27.8
ill
28.1
112
85-125
1
20
ug/L
06.09.14 07:25
28.5
114
28.2
113
92-126
1
20
ug/1-
06.09.14 07:25
28.9
116
29.3
117
48-143
1
20
ug/L
06.09.14 07:25
1050
105
997
100
61-133
5
20
ug/L
06.09.14 07:25
27.7
ill
27.2
109
87-123
2
20
ug/1-
06.09.14 07:25
26.7
107
26.5
106
77-125
1
20
ug/L
06.09.14 07:25
27.7
Ill
27.8
Ill
82-115
0
20
ug/L
06.09.14 07:25
48.6
97
48.9
98
53-149
1
20
ug/L
06.09.14 07:25
27.3
109
28.1
112
75-119
3
20
ug/L
06.09.14 07:25
26.8
107
26.9
108
52-116
0
20
ug/L
06.09.14 07:25
29.1
116
29.5
118
83-130
1 .
20
ug/L
06.09.14 07:25
28.7
115
28.5
114
84-122
1
20
ug/L
06.09.14 07:25
28.4
114
28.8
115
86-120
1
20
ug/L
06.09.14 07:25
Page 15 of 25 Final 1.000

►caEo
FSE QC Summary 486773
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Coliseum Shell
Analytical Method:
VOCs by CC/MS by SM6200B
Prep Method: SM620OB_PREP
Seq Number:
942952
Matrix:
Water
Date Prep: 06.09.14
MB Sample Id:
656737-1-BLK
LCS Sample
Id:
656737-1-BKS
LCSD Sample Id: 656737-1-BSD
MB
Spike
LCS
LCS
LCSD
LCSD
Limits %RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Ree
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
28.1
112
27.4
110
85-123
3 20
ug/L
06.09.14 07:25
tert-Butylbenzene
<0.0890
25.0
27.9
112
28.3
113
79-126
1 20
ug/L
06.09.14 07:25
Tetrachloroethene (PCE)
<0.0540
25.0
23.7
95
23.7
95
64-131
0 20
ug/L
06.09.14 07:25
Toluene
<0.0570
25.0
27.5
110
26.8
107
89-116
3 20
ug/L
06.09.14 07:25
trans-1,2-Dichloroethene
<0.188
25.0
28.8
115
29.0
116
78-118
1 20
ug/L
06.09.14 07:25
trans-1,3-Dichloropropene
<0.110
25.0
28.2
113
27.7
111
86-127
2 20
ug/L
06.09.14 07:25
Trichloroethene
<0.139
25.0
25.9
104
25.3
101
82-119
2 20
ug/L
06.09.14 07:25
Trichlorofluoromethane
<0.0540
25.0
27.8
ill
27.9
112
46-144
0 20
ug/L
06.09.14 07:25
Vinyl Acetate
<0.720
25.0
26.8
107
25.6
102
58-141
5 20
ug/L
06.09.14 07:25
Vinyl Chloride
<0.0810
25.0
25.4
102
27.6
110
76-122
8 20
ug/L
06.09.14 07:25
m,p-Xylenes
<0.176
50.0
55.4
ill
54.9
110
90-125
1 20
ug/L
06.09.14 07:25
o-Xylene
<0.122
25.0
28.1
112
27.5
110
86-119
2 20
ug/L
06.09.14 07:25
MB
MB
LCS
LCS
LCSD
LCSD
Limits
Units
Analysis
Surrogate
%Rec
Flag
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
96
92
93
65-134
%
06.09.14 07:25
4-Bromofluorobenzene
99
98
100
70-130
%
06.09.14 07:25
Toluene-D8
100
96
98
87-114
%
06.09.14 07:25
Page 16 of 25 Final 1.000

•
QC Summary
486773
��)�f.4
vi
&Q11CLma
WSW
Florida Testing Services, LLC
Terraquest Environmental
Consultants, P.C.
Coliseum Shell
Analytical Method: VOCs by
GUMS by SM6200B
Prep Method:
SM6200B_PREP
Seq Number: 942952
Matrix:
Ground Water
Date Prep:
06.09.14
Parent Sample Id: 486781-004
MS Sample Id:
486781-004 S
MSD Sample Id:
486781-004 SD
Parameter
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD
RPD
Units
Analysis Fla g
Result
Amount
Result
%Rce
Result
%Rec
Limit
Date
1, 1, 1,2-Tetrachloroethane
<0.180
25.0
28.3
113
27.1
108
76-126
4
20
ug/L
06.09.14 17:28
1, 1, 1 -Trichloroethane
<0.0760
25.0
27.6
110
26.3
105
63-128
5
20
ug/L
06.09.14 17:28
1,1,2,2-Tetrachloroethane
<0.0700
25.0
31.4
126
30.9
124
79-133
2
20
ug/L
06.09.14 17:28
1,1,2-Trichloroethane
<0.113
25.0
26.8
107
26.2
105
82-126
2
20
ug/L
06.09.14 17:28
1, 1 -Dichloroethane
<0.121
25.0
27.7
111
26.6
106
77-120
4
20
ug/L
06.09.14 17:28
1,1-Dichloroethene
<0.104
25.0
28.2
113
26.3
105
67-123
7
22
ug/L
06.09.14 17:28
1, 1 -Dichloropropene
<0.0600
25.0
28.0
112
26.6
106
76-126
5
20
ug/L
06.09.14 17:28
1,2,3-Trichoorobenzene
<0.118
25.0
25.3
101
25.9
104
41-136
2
20
ug/L
06.09.14 17:28
1,2,3-Trichloropropane
<0.138
25.0
28.1
112
26.4
106
77-125
6
20
ug/L
06.09.14 17:28
1,2,4-Trichlorobenzene
<0.0690
25.0
27.1
108
27.0
108
41-132
0
20
ug/L
06.09.14 17:28
1,2,4-Trimethylbenzene
<0.103
25.0
27.7
ill
26.7
107
53-141
4
20
ug/L
06.09.14 17:28
1,2-Dibromoethane (EDB)
<0.180
25.0
27.6
110
26.7
107
82-130
3
20
ug/L
06.09.14 17:28
1,2-Dichlorobenzene
<0.0940
25.0
27.7
111
26.7
107
83-128
4
20
ug/L
06.09.14 17:28
1,2-Dichloroethane
<0.0900
25.0
27.0
108
26.6
106
59-134
1
20
ug/L
06.09.14 17:28
1,2-Dichloropropane
<0.122
25.0
26.9
108
26.5
106
79-125
1
20
ug/L
06.09.14 17:28
1,3,5-Trimethylbenzene
<0.0870
25.0
27.7
ill
26.5
106
69-125
4
20
ug/L
06.09.14 17:28
1,3-Dichlorobenzene
<0.0980
25.0
28.1
112
26.7
107
83-126
5
20
ug/L
06.09.14 17:28
1,3-Dichloropropane
<0.133
25.0
26.9
108
25.9
104
85-124
4
20
ug/L
06.09.14 17:28
1,4-Dichlorobenzene
<0.0670
25.0
27.2
109
26.4
106
82-121
3
20
ug/L
06.09.14 17:28
2,2-Dichloropropane
<0.0970
25.0
29.2
117
26.5
106
56-122
10
20
ug/L
06.09.14 17:28
2-Butanone (MEK)
<0.378
50.0
53.0
106
53.8
108
66-136
1
20
ug/L
06.09.14 17:28
2-Chlorotoluene
<0.0880
25.0
28.2
113
26.6
106
73-129
6
20
ug/L
06.09.14 17:28
2-Hexanone
<0.352
50.0
52.8
106
52.7
105
63-140
0
20
ug/L
06.09.14 17:28
4-Chlorotoluene
<0.0900
25.0
28.8
115
27.3
109
76-129
5
20
ug/L
06.09.14 17:28
4-Isopropyltoluene
<0.0890
25.0
27.7
ill
26.8
107
73-126
3
20
ug/L
06.09.14 17:28
4-Methyl-2-pentanone (MIBK)
<0.253
50.0
49.9
100
50.1
100
71-140
0
20
ug/L
06.09.14 17:28
Acetone
<0.352
50.0
50.6
101
53.0
106
47-138
5
21
ug/L
06.09.14 17:28
Benzene
<0.119
25.0
27.3
109
26.4
106
70-135
3
20
ug/L
06.09.14 17:28
Bromobenzene
<0.132
25.0
27.7
ill
26.4
106
76-120
5
20
ug/L
06.09.14 17:28
Bromochloromethane
<0.112
25.0
29.0
116
28.1
112
83-132
3
20
ug/L
06.09.14 17:28
Bromodichloromethane
<0.124
25.0
28.5
114
27.7
111
66-132
3
20
ug/L
06.09.14 17:28
Bromoform
<0.159
25.0
24.6
98
23.8
95
63-143
3
20
ug/L
06.09.14 17:28
Bromomethane
<0.0970
25.0
22.0
88
21.7
87
60-134
1
20
ug/L
06.09.14 17:28
Carbon tetrachloride
<0.0990
25.0
28.5
114
26.8
107
59-139
6
20
ug/L
06.09.14 17:28
Chlorobenzene
<0.105
25.0
27.6
110
26.3
105
83-120
5
20
ug/1-
06.09.14 17:28
Chlorodibromomethane
<0.177
25.0
28.8
115
27.9
112
68-140
3
20
ug/L
06.09.14 17:28
Chloroethane
<0.0420
25.0
21.7
87
22.4
90
67-125
3
20
ug/L
06.09.14 17:28
Chloroform
<0.172
25.0
27.6
110
26.6
106
72-120
4
20
ug/L
06.09.14 17:28
Chloromethane
<0.0850
25.0
26.4
106
23.6
94
59-128
11
20
ug/L
06.09.14 17:28
cis-1,2-Dichloroethene
<0.114
25.0
28.0
112
26.8
107
80-125
4
20
ug/L
06.09.14 17:28
cis-1,3-Dichloropropene
<0.100
25.0
28.8
115
28.4
114
74-122
1
20
ug/L
06.09.14 17:28
Dichlorodifluoromethane
<0.0670
25.0
28.8
115
25.6
102
48-138
12
20
ug/L
06.09.14 17:28
Ethanol
<3.00
1000
1160
116
1060
106
55-140
9
20
ug/L,
06.09.14 17:28
Ethylbenzene
<0.0920
25.0
27.7
ill
26.2
105
70-140
6
20
ug/L,
06.09.14 17:28
Isopropyl ether
<0.0920
25.0
27.7
ill
27.0
108
70-132
3
20
ug/L
06.09.14 17:28
Isopropylbenzene
<0.0980
25.0
28.2
113
26.7
107
75-117
5
20
ug/L
06.09.14 17:28
Methyl tert-butyl ether (MTBE)
<0.169
50.0
53.8
108
53.0
106
51-155
1
20
ug/L
06.09.14 17:28
Methylene Chloride
0.310
25.0
26.8
106
25.9
102
71-126
3
20
ug/L
06.09.14 17:28
Naphthalene
<0.0940
25.0
26.7
107
27.0
108
34-135
1
20
ug/L
06.09.14 17:28
n-Butylbenzene
<0.0600
25.0
27.2
109
26.9
108
73-128
1
20
ug/L
06.09.14 17:28
n-Propylbenzene
<0.0650
25.0
28.4
114
26.7
107
75-125
6
20
ug/L
06.09.14 17:28
sec-Butylbenzene
<0.0920
25.0
27.1
108
26.2
105
77-122
3
20
ug/L
06.09.14 17:28
Page 17 of 25 Final 1.000

41 QC Summary 486773
t
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Coliseum Shell
PC[gp�
/ eru
Analytical Method:
VOCs by COMS by SM6200B
Prep Method:
SM620OB_PREP
Seq Number:
942952
Matrix:
Ground Water
Date Prep:
06.09.14
Parent Sample Id:
486781-004
MS Sample
Id:
486781-004 S
MSD Sample Id: 486781-004 SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD
RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
28.0
112
26.3
105
54-137
6
20
ug/L
06.09.14 17:28
tert-Butylbenzene
<0.0890
25.0
27.1
108
26.2
105
74-124
3
20
ug/L
06.09.14 17:28
Tetrachloroethene(PCE)
<0.0540
25.0
22.3
89
21.0
84
57-130
6
20
ug/L
06.09.14 17:28
Toluene
<0.0570
25.0
27.7
111
26.0
104
81-125
6
20
ug/L
06.09.14 17:28
trans-1,2-Dichloroethene
<0.188
25.0
28.9
116
27.0
108
69-122
7
20
ug/L
06.09.14 17:28
trans-1,3-Dichloropropene <0.110
25.0
29.2
117
28.0
112
73-129
4
20
ug/L
06.09.14 17:28
Trichloroethene
<0.139
25.0
25.4
102
24.6
98
73-124
3
20
ug/L
06.09.14 17:28
Trichlorofluoromethane
<0.0540
25.0
28.8
115
27.6
110
49-139
4
20
ug/L
06.09.14 17:28
Vinyl Acetate
<0.720
25.0
27.4
110
27.2
109
57-134
1
20
ug/L
06.09.14 17:28
Vinyl Chloride
<0.0810
25.0
26.5
106
23.1
92
70-121
14
20
ug/L
06.09.14 17:28
m,p-Xylenes
<0.176
50.0
56.2
112
52.9
106
65-151
6
20
ug/L
06.09.14 17:28
o-Xylene
<0.122
25.0
28.3
113
26.9
108
58-148
5
20
ug/L
06.09.14 17:28
MS
MS
MSD
MSD
Limits Units
Analysis
Surrogate
g
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
96
97
65-134
%
06.09.14 17:28
4-Brornofluorobenzene
102
99
60-148
%
06.09.14 17:28
Toluene-D8
98
98
87-114
%
06.09.14 17:28
Page 18 of 25 Final 1.000

•
Blank Summary
486773
t '• t
B2a9tQ
eeeo..e'w...,.,,.
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.,
Mebane, NC
Coliseum Shell
Sample Id: 656737-1-BLK
Matrix: WATER
Lab Sample Id: 656737-1-BLK
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
Analyst: MLA
Date Prep: 06.09.14 06:33
Seq Number: 942952
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
06.09.14 09:19
U
1
I,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
06.09.14 09:19
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
06.09.14 09:19
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
06.09.14 09:19
U
I
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
06.09.14 09:19
U
1
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
06.09.14 09:19
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
06.09.14 09:19
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
06.09.14 09:19
U
1
1,2,3-Trichloropropane
96-184
U
1.00
0.138
ug/L
06.09.14 09:19
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
06.09.14 09:19
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
06.09.14 09:19
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
06.09.14 09:19
U
I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
06.09.14 09:19
U
I
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
06.09.14 09:19
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
06.09.14 09:19
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
06.09.14 09:19
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
06.09.14 09:19
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
06.09.14 09:19
U
1
1,4-Dichlorobenzene
10646-7
U
0.500
0.0670
ug/L
06.09.14 09:19
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
06.09.14 09:19
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
06.09.14 09:19
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
06.09.14 09:19
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
06.09.14 09:19
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
06.09.14 09:19
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
06.09.14 09:19
U
1
4-Methyl-2-pentanone (MLBK)
108-10-1
U
0.400
0.253
ug/L
06.09.14 09:19
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
06.09.14 09:19
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
06.09.14 09:19
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
06.09.14 09:19
U
1
Bromochlorornethane
74-97-5
U
0.500
0.112
ug/L
06.09.14 09:19
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
06.09.14 09:19
U
1
Bromofonn
75-25-2
U
2.00
0.159
ug/L
06.09.14 09:19
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
06.09.14 09:19
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
06.09.14 09:19
U -
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
06.09.14 09:19
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
06.09.14 09:19
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L.
06.09.14 09:19
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
06.09.14 09:19
U
I
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
06.09.14 09:19
U
1
cis-1,2-Dichloroetbene
156-59-2
U
0.500
0.114
ug/L
06.09.14 09:19
U
1
Page 19 of 25 Final 1.000

LIJ Lie
Florida Testing Services, LLC
Sample Id: 656737-1-BLK
Lab Sample Id: 656737-1-BLK
Blank Summary 486773
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: WATER
�PUR�
ARR2tKV
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
Analyst: MLA
Date
Prep: 06.09.14 06:33
Seq Number: 942952
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag Dil
Date
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
06.09.14 09:19
U I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
06.09.14 09:19
U 1
Ethanol
64-17-5
U
50.0
3.00
ug/L
06.09.14 09:19
U 1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
06.09.14 09:19
U 1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
06.09.14 09:19
U 1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
06.09.14 09:19
U 1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
06.09.14 09:19
U 1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
06.09.14 09:19
U I
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
06.09.14 09:19
U 1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
06.09.14 09:19
U 1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
06.09.14 09:19
U 1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L.
06.09.14 09:19
U 1
Styrene
100-42-5
U
0.500
0.0740
ug/L,
06.09.14 09:19
U I
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L.
06.09.14 09:19
U 1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
06.09.14 09:19
U 1
Toluene
108-88-3
U
0.500
0.0570
ug/L
06.09.14 09:19
U 1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
06.09.14 09:19
U 1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
06.09.14 09:19
U 1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
06.09.14 09:19
U 1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
06.09.14 09:19
U 1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
06.09.14 09:19
U 1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
06.09.14 09:19'
U 1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
06.09.14 09:19
U 1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
06.09.14 09:19
U 1
Page 20 of 25 Final 1.000

Blank Summary 486773
Mlt
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: 656764-1-BLK Matrix: WATER
Lab Sample Id: 656764-1-BLK
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR
Analyst: 4150 Date Prep: 06.10.14 12:42
Seq Number: 943100
Parameter Cas Number Result RL MDL Units Analysis Flag
Date
Lead 7439-92-1 U 0.0100 0.00330 mg/L 06.11.1411:33 U
Page 21 of 25 Final 1.000

Blank Summary
486773
�! ccrtro�
eQAAtQ; ""�
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: 943160-1-BLK
Matrix: WATER
Lab Sample Id: 943160-1-BLK
Analytical Method: TSS by SM2540D
Prep Method:
Tech: ANS
Analyst: ANS
Date Prep:
Seq Number: 943160
SUB: E871002
Parameter Cas Number Result RL MDL
Units Analysis
Flag Dil
Date
Total Suspended Solids
U 4.00 3.50
mg/L. 06.11.14 17:09
U 1
Page 22 of 25 Final 1.000

X co CHAIN OF CUSTODY Page � Of
LABORATORIES
WNW
FED -EX I UPS: Tracking If
Bottle Order Control #
6017 Financial Drive, Norcross, GA 30071 (770-449-S800)
Xenco Quote At
Xenco Work Orden; ']�
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4143 Greenbriar Dr., Stafford, TX 77477 . (281-240-4200)
9701 Harry. Hines Blvd, Dallas, TX 75220 (214 9074300)
12600 West I-20 East -Odes TX 79765 432-563-1800
1 lent a ortin In ormat on I S' . j Iti 9' ' a?t 1 Invoice Information
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Analyses
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Company Name
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Terracluest Environmental Consultants, P.C.
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city. Mebane, NC, 27302
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Phone: [phone] Fax: [phone]
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3 Day EMERGENCY ED EDD? NC DENR LAB FILTER METALS (unpreserved)
2 Day EMERGENCY 0 LA RECAP HOLD TRIP BLANKS PENDING HITS
'I Day EMERGENCY O O Omer Project [Client specific MS I MSD selected
Sartre Day TAT - Level 2 Results &sumdard OC Special Detection limits needed to achieve
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XENCO Laboratories
Prelogin/Nonconformance Report- Sample Log -In
Florida Testing Services, LLC
Client: Terraquest Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC
Date/ Time Received: 06/05/2014 10:20:00 AM Air and Metal samples Acceptable Range: Ambient
Work Order #: 486773 Temperature Measuring device used : #61
Sample Receipt Checklist Comments
#1 'Temperature of cooler(s)?
1.4
#2 *Shipping container in good condition?
Yes
#3 *Samples received on ice?
Yes
#4 *Custody Seals intact on shipping container/ cooler?
N/A
#5 Custody Seals intact on sample bottles?
N/A
#6 *Custody Seals Signed and dated?
N/A
#7 *Chain of Custody present?
Yes
#8 Sample instructions complete on Chain of Custody?
Yes
#9 Any missing/extra samples?
No
#10 Chain of Custody signed when relinquished/ received?
Yes
#11 Chain of Custody agrees with sample label(s)?
Yes
#12 Container label(s) legible and intact?
Yes
#13 Sample matrix/ properties agree with Chain of Custody?
Yes
#14 Samples in proper container/ bottle?
Yes
#15 Samples properly preserved?
Yes
#16 Sample container(s) intact?
Yes
#17 Sufficient sample amount for indicated test(s)?
Yes
#18 All samples received within hold time?
Yes
#19 Subcontract of sample(s)?
No
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
Yes
#21 <2 for all samples preserved with HNO3,HCL, H2SO4?
Yes
#22 >10 for all samples preserved with NaAs02+NaOH, ZnAc+NaOH?
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: DL I PH Device/Lot#: 1016662-2
Checklist completed by:
Dario Lagunas
Checklist reviewed by:��
Eben Buchanan
Date: 06/05/2014
Date: 06/05/2014
PCCR—��1/'aj
2
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Page 25 of 25 Final 1.000