NC0088919_Toxicity Reduction Evaluation Progress Report_20141001

TERRAc uest
ENVIRONMENTAL CONSULTANTS, P.C.
October 1, 2014
W. Corey Basinger - Regional Supervisor
Surface Water Protection Section - Winston-Salem Regional Office
Division of Water Quality
585 Waughtown Street
Winston-Salem, NC 27107-2241
Re: Toxicity Reduction Evaluation Progress Report
Former Coliseum Shell — Quality Oil Company, LLC
NPDES Permit No. NCO088919
NCDWM-UST Incident No.: 15260
Terraquest Project No.: 01195
Dear Mr. Basinger: .
- Ktl,Clvcv
-.• N.O.Dept. of ENR
OCT 0 3 20%
Winston-Saic;ill
Regional Office
On behalf of the permitee, Quality Oil Company, LLC, Terraquest Environmental Consultants, P.C.
hereby submits this Toxicity Reduction Evaluation Progress Report in accordance with.the Special
Order by Consent EMC SOC WQ S-12-004.
Section 2 (a) 2) of the SOC states the following:
"scope of the THE work should consider but is not limited to: effluent
characterization/identification/confi'rmation ,of suspected toxicants, evaluation of point source
contributions to toxicity, pretreatment bench scale treatability studies, toxicity source reduction,
strategies"
As ,required, consideration to each of those items throughout the latest testing quarter that
1 ended in September 2014 per Section 2 a 3 of the SOC follows:.
effluent characterization/identification/confirmation of suspected toxicants:
r1 During the July, August, September 2014 discharge quarter, weekly inspections of the subject
treatment system were performed by either the ORC or backup ORC for routine maintenance
and oversight as required by the permit and also to investigate the source or situation that might
be causing the toxicity to Ceriodaphnia Dubia. No finite toxicant was identified throughout the
period. Routine maintenance activities including general cleaning and the replacement of
polyethylene bag filters was conducted with site visits made on 7/8/14, 7/14/14, 7/15/14,
7/21/14, 7/22/14, 7/28/14, 8/4/14, 8/11/14, 8/18/14, 8/25/14, 9/2/14, 9/5/14, 9/24/14, and
9/29/14. Associated checklists are enclosed.
100 E. Ruffin Street • Mebane, North Carolina 27302
Telephone [phone] • Facsimile [phone]
www.terraquestpc.com

Page'2
C. Basinger
10/1/14
Monthly system samples,were collected from the treatment system's influent; after air stri'pper,.
after first. carbon filter, and effluent; port locations. Those samples were submitted to an. NC'
certified .laboratory for analysis of the VOCs that -are the subject of both the site's-remediation
and of the TRE. No toxicants are apparent. The analytical results are similar:to.historical results.:
Lab reports for July, August, and September 2014 are included for reference'.
evaluation of point source 'contributions to toxicity: '
Terraquest, has reviewed possible contributors of toxicants at this site. No new information'is
available and the toxicant remains undefined. As noted, recent analytical data mimics historical,
results.
pretreatment bench scale treatability studies:
Consideration vvas provided to::bench sale treatability studies;. however, at this time.there are no.
suspected toxicants nor •have Terraquest, DWQ,:or several third parties'been' able to discern.a.
way to discover the -toxicant. Study of the.contaminants involved at the. site will continue.
toxicity source. reduction strategies: ` ; -
Consid&ation -to .toxicity, reduction was given, however, the'toxicity. source has 'not been
identified: Terraquest•recommends continued remediation of the subject contaminant plume.
-while attention is paid to possible sources of the toxicity.
To date; the toxicant to C. Dubia. remains unclear.. In compliance With the SOC, Terraquest has .
considered the items set forth in -Section 2 (a) 2) of the SOC, however, those considerations have '.
not produceda solution to the toxicity at this time. The evaluation Of 'toxicity wiII continue.`; .
Please contact me with any questions or. concerns :you ma.y have.. Thank you..
Sincerely,.
TERRAQUEST ENV[ RONMENTAL'CONSULTANTS, P.C.
Ryan D:_ Kerins,
Project Manager
Enclosed: System checklists, Analytical Reports :.

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le
'1'EiiRA nest
a.
ENVIRONMENTAL C.S.I. P.C.
P \
Inspector
�L j c� Ca ri C-v--e
u °
Coliseum Shell System Inspection Checklist
uality oil
Date of Inspection
across sep elem.
on LRP
before filter
after filter
Vacuum pressure
D c-
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
added coolant
scfm
�zZZJ `t p
gallons
(� +�
hours
hours
OK
Comments:
OK
Temp
Change coolant
OWS Condition
OK
Comments:
OWS transfer pump
OK
Comments:
AST Blower Operation
OK
Comments:
AST transfer pump
OK
Comments:
Bag filters dirty? Lots
Some Minimal
None idn't c
Changed bag
Yes/ JV
Changed sand
Yes & fr
OI
# bags
Comments &Observations:
rSu "CO o"`
r- Se-�
II
�e 1-e`�I?
re
Ms
r � t'f Zh
r
AAA3 w�Y� Lo
i
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EIIVIROil1.4E11TJ.L COV$VLT:.IIT�� ItC.
Inspector
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
Coliseum Shell System Inspection Checldist
wualfty 011
Date of Inspection � ` F
across sep elem.
On LRP beforefilt& alter noel
scfm �% �q iJ
vC 2 2 / gallons
hours
1 7 hours
OK Comments: {
OK f Z- Temp I deg. F
c
added coolant
OWS Condition
OK
OK l�
OWStransfer pump
AST Blower Operation
OK C/
OK
AST transfer pump
Bag filters dirty? Lots
Some Minimal None
Changed bag
Yes N
Changed sand
Yes No ,
t & Observations:
Commen s
off)
r7 ,sz..� ram•' ��'� l!� � � ,v�. � r
Change coolant L 1 1fyt-�j� fO
Comments:
Comments:
Comments:
Comments:
Didn't chec
C'-- -/
# bags

TERi, uest
_�-
EN V IRONIAENiAt CONjULTANT., P.C.
p
Inspector J C^—
Coliseum Shelf System Inspection Checklist
uality Oil
e
Date of InspectionAx
acrosssep m,
on LRP
before filter
after filter
Vacuum pressure
vadose sparge
scfm
Totalizer Reading
gallons
LRP run hours
hours
AST blower run hours
hours
Control Panel
OK _
Comments:
Liquid Ring Pump
OK _
Temp
deg. F
added coolant
Change coolant
OWS Condition
OK _
Comments:
OWS transfer pump
OK_
Comments:
AST Blower Operation
OK _
Comments:
AST transfer pump
OK _
Comments:
Bag filters dirty? Lots
Some Minimal
None
Didn't check
Changed bag
Yes / No
Changed sand
Yes / No
q bags
Comments & Observations:
I
O-rL4_t
— o Gecl
q S 6e
✓t 0
Prbtt
rcP�:i'
Sc l�

Mest
ENVIRONMENTAL CONSULTANTS, P.C.
Inspector _/1j
Coliseum Shell System Inspection Checklist
mM4KOl,'jiVbITV��
//%Vl/
Date of Inspection �`
across sep elem.
on LRP
before filtei
after filter
U 'ecW
fit6K(2
�( (T"�
` -(� ( /
— T_ r
Vacuum pressure
vadose sparge ©h r scfm
Totalizer Reading �1 �I �w gallons
LRP run hours Za/ 'T hours
AST blower run hours 7/Z hours
Control Panel OK v Comments:
Liquid Ring Pump OK Temp c Z deg. F
added coolant � Change coolant AA
OWS Condition OK ✓ Comments:
OWS transfer pump OK ✓ Comments:
AST Blower Operation OK Comments:
v/
AST transfer pump OK Comments:
Bag filters dirty? Lots Some Minimal None n t cti ck
Changed bag Yes/ a
Changed sand Yes N / # bags
Comments & Observations:

Coliseum Shell System Inspection Checklist
TE uest ud 1"t�' ®1
IR ENVONtAENTAL1CONSULTANTS. P.C.
Inspector A W Date of Inspection 249j-- q
across sep elem.
onIRPP
before filter
after filter
r
/ `J'�17
I -7-
Vacuum pressure
vadose sparge
scfm
Totalizer Reading'
6 V r) gallons
LRP run hours
hours
1
AST blower run hours
hours
Control Panel
OK %Z
Comments:
Liquid Ring Pump
OK
Temp 7 (� deg. F
added coolant
Change coolant
OWS Condition
OK V
Comments:
OWS transfer pump
OK V
Comments:
AST Blower Operation
OK V
Comments:
AST transfer pump
OK —\/—
Comments:
Bag filters dirty? Lots
Some Minimal None
Didn't check
Changed bag
Ye(/ Noy
Changed sand
Yes No
# bags
Comments &Observations:
C"'J
-,' C—GiC�
�`/N C�9+'�rD,�p�sny
LP

TERRA ue
ENVIRONMENTALP.C.
Inspec
tor
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection
across sep elem.
on LRP
before filter
after filter
C y✓
z 73� z
j�
— f
Vacuum pressure
vadose sparge / scfm
x r z 10 g690
Totalizer Reading ��� S / gallons
(� y�
LRP run hours 0 -eD / (V � hours
AST blower run hours hours
Control Panel OK / Comments: /
Liquid Ring Pump
OK V Temp i �a deg. F
added coolant Change coolant /VO
OWS Condition OK Comments:
OWS transfer pump OK Comments:
AST Blower Operation OK - Comments:
AST transfer pump OK Comments:: S �7
Som Minimal None Didn't check
Bag filters dirty? Lots �C�l r �L SI/
Changed bag x/ ay-,/ No /
Changed sand Yes /6 # bags
Comments &Observations: � /
m

Coliseum Shell System Inspection Checklist
TERRA Uest Uality Oil
ENVIRONMENT7CULT,I.,,NTs�PC.Inspector / l Date of Inspection
across sep elem.
on LRP
before filter
after filter
Cr eee,,
— 2(
— P 6
-- � s
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours f 6 rV1,1 on
Control Panel
Liquid Ring Pump
scfm
gallons
Q S� hours
hours
OK Comments:
OK Temp / deg. F
added coolant A-0 Change coolant A.-V
OWS Condition OK /f Comments:
OWS transfer pump OK V" Comments:
AST Blower Operati OK" Comments:
AST transfer pump OK Comments:
Bag filters dirty? Lots Some Minimal None Didn't check
Changed bag Yes / No
Changed sand Yes / N bags
Comments & Observations:
U`L C Pin_AWL[ Pam( a �P�1� ✓Li�

TERRA Uest
ENVIRONMENTAL OONSULTANTS, P.C.
Inspector 4 a L.41'hf
Coliseum Shell System Inspection Checklist
uali ty Oil
Date of Inspection
across sep eleem..—�
on LRP
before filfir
after filter
Vacuum pressure
vadose sparge � scfm
Totalizer Reading c�,c((,� Ok f ,(—. e c(e'—f— gallons J
f
LRP run hours
�0
-7
J ) � r
hours
AST blower run hours
� I � , � W1 4-r6 4s pl t -n 01
I 9
Z� !
� 1
hours.
Control Panel
OK tr/
Comments:
Liquid Ring Pump
OK ✓
Temp
added coolant /(/(f
Change coolant
A10
OWS Condition
OK Vl'
Comments:
OWS transfer pump
OK y
Comments:
AST Blower Operation
OK "
Comments:
/
AST transfer pump
OK v
Comments:
Bag filters dirty?
Lots Some Minimal
None
Didn't check
Changed bag
Oe/ No
a Changed sand
Yes 11
# bags
deg. F
Comments & Observations: r
64 i- l c u. 6� �(Vt—e'(
' a 5Al 15 Q r� u`� µw I'vC fn C o
r f
M�f 3 (aki) 15 n
�Vlq )64 W Qwll r MY 5", � p'� �,�s Trial

. �- �i ��Q �2�� 7�•�Y� .�l f �Y l�(S Q-1 J t/�i' ! r. e'� w / inC • of �� J/� / � (C/ E'�
Inspector
6 ` 3 , 9e, %b
G� a �� c�u l�� �✓� a�� _rep- i
Coliseum Shell System Inspection Checklist
Uest ality Oil u�Kel III I V,.1 FORM - - - -
S P`I
Date of Inspection Zt5 ( /
across sep elem. on�L7RP before filter after filter
Vacuum pressureN G (✓ r ZO — 2
vadose sparge I scfm
Totalizer Reading ZJ ( �/ [ D gallons
LRP run hours IXGI�{ Crro�aKCIeaK (� /��` hours
AST blower run hours G �/ J hours
Control Panel OK '`` Comments:
Liquid Ring Pump OK " Temp
added coolant rcS
OWS Condition
OWS transfer pump //'
AST Blower Operation �Z �1
AST transfer pump
Change coolant /W
OK 4?0tt Comments:
OK r / Comments:
OK Comments:
OK Comments:
4-, CGU(tir
70 /0'deg. F
Bag filters dirtyl''- Lots Some Min a`
None
Didn't check Ve 21,
���� Cya�e
Changed bag
7i es No
Changed sand
Yes/9
# bags
Comments & Observations:
ff jf
OLL = c.GiGC�b� 0, `
c4dC aj U
'CAyiw (v( ok� oC� p J �
RL/L�
�ILiGti�( dl GFH-tx �G�-r`t7' ��Z
H

TERRA nest
ENVIRONMENTAL CONSULTANTS, P.C.
Inspector L {—c"( l — �S
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection 2�1 �q
across sep elem: ' ',
on LRP
before filter,
after filter `
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changed sand
Comments & Observations:
scfm
gallons
hours
hours
OK Comments:
OK Temp deg.F
added coolant Change coolant
Some
OK Comments:
OK Comments:
OK Comments:
OK Comments:
Minimal None Didn't check
Yes / No
Yes / No # bags

FC4 K <�q
TERRA nest
ENVIRONMENTAL CONSULTANTS. P.C.
P
Ins ector ar4�f
Coliseum Shell System Inspection Checklist
uality Oil
Date of Inspection 2 //91
across sep elem.
on LRP
before filtei
after filter
41ppt6 67k6e l
'Z6-<
- /9
°- /9
Vacuum pressure
Lk
vadose sparge
Totalizer Reading
LRP run hours
u
AST blower run hours
dti s
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed ball—.
Changed sand
Comments & Observations:
added coolant ^/0
1
scfm
2l ZZl qot,
gallons
ZG+
S
d°-77 '
hours
hours
OK
Comments:
/
OK
V
Temp
Change coolant
ND
/
OK
Comments:
OK
J
Comments:
OK-v.
Comments:
OK
'✓
Comments:
Some
Minimal None Didn't check
�Z
/Yes' on\X No
Yes 1109
/ W deg. F
# bags
�0�& Coo- ( C:, 1, )
I

nest
ENVIRONMENTAL CONS VLTANTS, P.C.
Inspector AV16
Coliseum Shell System Inspection Checklist
uality Oil
•
Date of InspectionVlq—wllq
across sep elem.
onLRP
before filtef
after filter
Vacuum pressure
--a0
-... l a
l
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
scfm
,^ 0 gallons
�6 1 hours
hours
OK Comments:
OK Temp
1:7=3 —deg. F
Change coolant O
added coolant
OWS Condition
OK_
Comments: LdeaJ
OWS transfer pump
OK NZ
Comments:
AST Blower Operation
OK V
Comments:
AST transfer pump
OK 1Z
Comments:
Bag filters dirty? Lots
Some Minimal None
Didn't check
Changed bag
Yes No
Changed sand
Yes / No`�,r
# bags
7/ I (A A 4 117"t
Comments & Observations:
"N
A
C1jAS14c,_
e . •
c1�"j 0. � C-OCIL-ro

nest
ENVIRONMENTAL CONSULTANTS., P.C.
(4
Inspector AC.— Lt-�O�)
Coliseum Shell System Inspection Checklist
2ality Oil
Date of Inspection
:
do LRP ```' `
before filter"":
afterfilter'''',°
�ecro(sjs`sep'elem
v '_
l
Vacuum pressure
vadosesparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changed sand
Comments & Observations:
scfm
OK
OK
added coolant
OK
OK ✓
OK
OK ✓
Some Minimal None
Yes /
Yes o
gallons
hours
hours
Comments:
Temp
Change coolant /4-10
Comments:
Comments:
Comments:
Comments:
Didn't check
# bags
deg. F

Coliseum Shell System Inspection Checklist
TERRA uest uality Oil
ENVIRONMENTAL CONSULTANTS, P.C. Q
Inspector Date of Inspection-V
across sep elem. on LRP before filter after filter
vadosesparge
Totalizer Reading
LRP run hours
AST blower run'hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changedsand
Comments & Observations:
added coolant 10
Some
scfm
�5 vv gallons
hours
hours
OK " Comments:
OK V Temp I �y deg. F
Change coolant _A/V
�W:,e f/ n.)
OK
Comments.
/
OK I//
Comments:
OK
Comments:
OK
Comments:
Minimal None
Didn't check
Yes / No
Yes No # bags

GROUNDWATER ANALYTICAL HISTORY- INFLUENT
COLISEUM SHELL SERVICE
NCDWM-UST INQDENT
NO, 15206
TERRAQU EST PROJECT
NO, 01195
1
°
g
;
e
a
P.
w
Date
Analysis
°
°
i
°
2
C
li
110
36
7/LS/2011
62008
120
460
94
530
1.200
60
59D
-
300
-
_
23
2A
_
_
150.
11
_
_
_
e/29/2011
6200E
87
520
66
490
am
41
ISO
140
-
-
L2
-
-
2A
-
29
110
.
77
9A
-
-
-
I10
27
10/17/2011
620DO
84
650
100
690
1.000
32
600
-
<100
-
-
<10
-
-
<10
-
<100
230
14
<10
880
-
-
270
45
11/28MIl
62008
75
400
93
530
I,200
33
240
-
130
-
_
cl
-
_
3.8
-
25
250
14
14
360
41
12/5/2012
62D0S
74
590
120
B00
1.200
28
<250
-
92
-
-
6
-
-
6
-
<50
250
27
18
1,6DO
-
-
221
55
6/8/2012
6200E
L6
82
<1
27.6
130
2.4
66
-
27
-
-
<1
-
-
<1
1.1
<10
16
<1
<1
710
-
-
10
33
7/9/2012
6200E
9.6
47
<5
SO
121
6
Q50
-
100
-
-
<5
-
-
<5
<5
60
Q5
<5
<5
450
-
-
11
6.1
8/6/2012
62008
14
78
19
230
400
73
81
-
51
-
-
<1
-
-
<1
Q
<0
54
32
3.9
IA00
-
-
46
12
9/10/2012
6200E
72
480
86
600
2,200
<50
Q,500
-
<500
_
_
.50
_
_
<50
<50
<500
260
-50
<50
1,800
-
_
2D0
50
10/1/2012
62008
21
ISO
46
370
440
20
<500
-
100
-
-
<10
-
-
<10
40
<200
90
16
<30
970
-
-
160
52
11/5/2012
62ODS
46
330
62
2A70
2,400
37
<lm
_
100
-
-
<10
-
-
<10
<10
<100
270
1120
1,800
-
-
250
36
22/10/2012
62008
45
310
55
410
2,100
36
Q50
-
60
-
-
6
-
-
<5
<5
<50
190
&9
<5
1,200
-
-
140
35
I/7/2013
62008
65
490
92
SSO,
I,500
42
69
-
68
-
-
1.5
-
-
39
<1
13
<250
14
19
1,400
-
-
270
58
2/4/2013
6200E
34
In
51
360
21000
25
<1,000
-
<200
-
-
QO
-
-
QO
Q0
<200
190
QO
QO
RIC
-
-
140
33
3/8/2013
62008
37
ISO
38
3SO
1,700
42
60O
-
<100
-
-
<10
-
-
<30
<10
<100
140
<30
<10
-
-
-
230
36
4/1/2013
6200E
32
200
37
270
1,700
41
<500
-
100
-
-
<10
-
-
<30
<30
<100
130
'<10
<10
-
-
-
100
24
5/6/2013
62008
27
170
27
2D9
IAOD
28
I M
-
<100
-
<10
-
-
<10
<10
<100
78
<30
<20
-
-
-
77
18
6%3/2013
6200E
25
130
I8
152
I.DDO
24
600
-
<100
-
-
<10
-
-
<10
QO
<100
fit
<10
<10
-
-
-
54
13
7AM13
6100E
32
200
25
190
960
24
<500
-
<100
-
-
<10
-
-
<10
<10
<100
58
<10
<10
-
-
-
55
14
8/5/2013
62008
22
120
19
ISO
3,100
25
Q50
-
72
-
-
<5
-
-
<5
<50
60
.1
<5
<5
-
-
-
56
12
9/3/2013
620M
5.77
30.8
5.73
593
343 D
102
179 D
110
-
27.7
<0.0600
-
-
<0.0980
10.0890
9.39
77.1
0.700 J
L32
c3
-
-
25.3
3.20
10/7/2013
62008
21
94
<10
202
1,000
25
-0500
-
<100
-
-
Q0
-
-
<0
<10
<100
<50
<10
<10
-
-
-
32
Q0
11/4/2013
62DOB
45
194 D
22A
25&3
1,730 D
49.8
Ill
-
107
-
33.7
<0.0600
23
001
03201
Dim
0.3201
.0.253
36.2ID
3.75
356
-
0.260 J
-
65.7
35
32/2/2013
62008
322
262D
314
206.3
2,340D
4L3
291
-
114
-
295
<0.06DO
<0.0920
<0.0890
1.190
<0.0890
4.253
6280
5.03
<0.0740
-
.0.0540
-
83.4
19.7
1/6/2014
6200E
34
190
30
212
Z300
62
100
-
120
-
-
Q
<1
Q
L3
LI
11
140
45
43
-
12
1
75
17
2/17/2014
62008
25.6
122 D
249
285.1
1,960 D
SL7
390 D
-
<0.378
-
33.1
10.0600
<0.0920
<0.0890
54.7
<0.0890
<0.253
214 D
3.19
393
-
<0.0540
<0.139
639
119
3/3/2014
62008
25A
139 D
29A
232.3
L510 D
39.2
10.352
16
95.9
9.2
24.8
SA6
<0.0920
N.0890
<0.0980
<0.0890
35.5
88.5
4.49
5.03.
-
4.0540
N.139
87.5
19
6200E
24
<100
QO
108
1,700
37
<3,000
QO
QOO
QO
-
QO
QO
QO
QO
Q0
Q00
<100
QO
Q0
-
QO
QO
44
QO
4/7/2014
19.9
1"
20
I30.1
915
285
113
<0.132
201
<0.088
24.5
<0.D6
<0.092
0.62
0.79
<0.089
<0.253
55.7
339
<0.074
-
<0.054
<0.09
50
IL6
5/5/2014
6200E
20.8
67.5
12.4
869
1,580
31.3
161
<0.132
939
<0.088
23
<0.06
4.092
�0.089
OA6
0.26
c0.253
35.6
L68
<O.074
-
<0.054
<0.09
23
639
5/4/2014
62005
52.1
498
422
1.350 D
3LI
119 HF
<0.132
<0.378
<0.880
19A HF
4.M
<0.0920
<O.0890
<0.098D
4.0990
6.62
259
<0.0650
0.62
-
<0.0540
.0.0900
10A
338
7/Bn014
8/11/2014
62006
62008
19A
36S
II2 D
2E5
192A
1,740 0
37.6
III
<0.132
<0378
<O.Offi0
<0352
<0.0600
02301
<0.0890
LIO
O.2.1
<0.253
635
4A9
<0.0.0
-
c0.0540
<0.0900
59.7
ISS
9 14
6I008
14.5
05.1
358
48.2
1250 D
3&1
1.
<0.132
29.1
<0 .
<0352
<0.0600
�.0920
<0.0890
<0.0930
<0.0890
10.253
14.1
<0.0650
0.69
-
<0.0540
<0.0900
7.99
3.28
2L Standard
1
600
600
500
20
70
6000
NE
4000
100
40
70
-70
70
70
25
NE
6
70
70
10
0.7
0.4
400
400
GCL
5 000
260 000
84
85 500
20 000
70 ODD
000.
NE
4 000 000
NE
40 000
900
8
15 000
15 000
1700
NE
6.000
30.000
70 000
10 000
700
400
28500
25.000
Notes:
1. A8 -Im In y8/1..
2. Bold de" a detected wncentratl_on.
3. Sh dIN denotes a
corce Mtlon In ei¢ess of the Gross COntaminatl°n Levels GCL .

GROUNDWATER ANALYTICAL HISTORY - AFTER AST
COLISEUM
SHELL SERVICE
NCDWM-UST INCIDENT
NO.: 15206
TERRAQUEST PROJECT NO.: 01195
O
W
v
C
N
a
m
C
(V
Cl
L
C
a)n
C
w
U°
N
N
C
N
N
N
cai
o
E
E
C
N
C
X
w
O
m
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L
F7
V
F7
L
7
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(0
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m
�
U
L'
°J
m
a
z
N
r
Date
Analysis
m
°
w
a
N
Ir
.-i
7/25/2011
6200B
<1
<5
<1
<3
<1
<1
86
20
5.6
<1
<1
8/29/2011
6200B
<1
<5
<1
<3
<1
<1
<50
-
15
<5
<1
<1
10/17/2011
6200B
<1
<5
<1
<3
<1
<1
<50
460
<10
<5
<1
<1
11/28/2011
6200B
<1
<5
<1
<3
<1
<1
<50
-
10
<5
<1
<1
12/5/2011
6200B
<1
<5
<1
<3
<1
<1
<50
750
11
<5
<1
<1
6/8/2012
6200E
<1
<5
<1
<3
<1
<1
<50
110
<10
<5
<1
<1
7/9/2012
6200B
<1
<5
<1
<3
<1
<1
<50
110
<10
<5
<1
<1
8/6/2012
6200B
<1
<5
<1
<3
1.6
<1
<50
130
<10
<5
<1
<1
9/10/2012
6200B
<1
<5
<1
<3
1.2
<1
<50
590
<10
<5
<1
<1
10/1/2012
6200E
<1
<5
<1
<3
<1
<1
61
97
<10
<5
<1
<1
11/5/2012
6200B
<1
<5
<1
<3
<1
<1
<50
540
12
<5
<1
<1
12/10/2012
6200B
<1
<5
<1
<3
<1
<1
<50
260
<10
<5
<1
<1
1/7/2013
6200B
<1
<5
<1
<3
<1
<1
<50
880
<10
<5
<1
<1
2/4/2013
6200B
<5
<25
<5
<15
<5
<5
<250
350
<50
<25
<5
<5
3/8/2013
6200E
<1
<5
<1
<3
2
<1
<50
-
<10
<5
<1
<1
4/1/2013
6200B
<1
<5
<1
<3
3.7
<1
<50
-
<10
<5
<1
<1
5/6/2013
6200B
<5
<25
<5
<15
<5
<5
<250
-
<10
<5
<1
<1
6/3/2013
6200E
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<1
<1
7/1/2013
6200B
<1
<5
<1
<3
1.4
<1
<50
-
<10
<5
<1
<1
8/5/2013
6200E
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<1
<1
9/3/2013
6200B
<0.119
0.310 J
<0.0920
<0.298
2.23
<0.0920
191
<3
15.5 J
<0.0940
<0.103
<0.0870
10/7/2013
6200B
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<1
<1
11/2/2013
6200B
<0.119
<0.0570
<0.0920
<0.298
3.06
<0.0920
<0352
<3
<0.378
<0.0940
<0.103
<0.0870
12/2/2013
6200B
<0.119
0.690
<0.0920
<0.298
6.46
<0.0920
<0352
<3
<0378
3.43
<0.103
<0.0870
1/6/2014
6200B
<1
<5
<1
<3
10
<1
<50
-
28
<5
<1
<1
2/17/2014
6200B
<0.119
<0.0570
<0.0920
1.636
5.79
<0.0920
63.9
-
14.5 J
2.6
<0.103
<0.0870
3/3/2014
6200E
<0.119
<0.0570
<0.0920
<0.298
3.11
<0.0920
43.4
-
11.9 J
<0.0940
<0.103
<0.0870
4/7/2014
6200B
<1
<5
<1
<3
1.6
<1
<50
-
<10
<5
<1
<1
5/5/2014
6200B
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
31.8
-
7.49
<0.0940
<0.103
<0.0870
6/4/2014
6200E
0.14
0.46
<0.092
0.68
8.16
<0.092
28.7
-
<0378
0.45
0.28
<0.0870
7/8/2014
6200B
<0.119
<0.0570
<0.0920
<0.298
3.01
<0.0920
25.3 HF
-
<0378
<0.0940
<0.103
<0.0870
8/11/2014
6200B
<0.119
0.34
<0.0920
0.42
1.67
<0.0920
24.1
-
<0378
1.39
0.22
<0.0870
9/2/2014
6200B
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
5.33
-
<0378
<0.0940
<0.303
<0.0870
2LStandard
1
600
600
500
20
70
6,000
NE
4,000
6
400
400
GCLI
5,000
260,000
84,500
85,500
200,000
70,000
6,000,000
NE
4,000,000
6,000
28,500
25,000
Notes:
1. All results in µg/L.
2. Bold denotes a detected concentration.
3. Shading denotes a concentration in excess of the
Gross Contamination Levels (GCLs).

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8/29/2011
10/17/2011
11/28/2011
12/5/2011
6/8/2012
7/9/2012
8/6/2012
9/10/2012
10/1/2012
11/5/2012
12/10/2012
1/7/2013
2/4/2013
3/8/2013
4/1/2013
5/6/2013
6/3/2013
7/1/2012
8/5/2013
9/3/2013
10/7/2013
11/4/2013
12/2/2013
1/6/2014
1/13/2014
2/17/2014
3/3/2014
4/7/2014
5/5/2014
6/4/2014
7/8/2014
7/16/2014
8/11/2014
1. All results in µg/L
2. Bold denotes a de
3. Shading denotes z
62003
6200B
6200B
6200B
6200B
6200B
6200B
6200E
6200E
6200B
6200B
6200B
6200B
6200B
6200B
6200B
6200B
6200E
6200B
6200E
6200B
6200E
6200E
6200B
6200B
6200B
6200B
6200E
6200B
6200E
6200E
6200B
6200B
GROUNDWATER ANALYTICAL HISTORY - EF
COLISEUM SHELLSERVICE
NCDW M-UST INCIDENT NO.: 15206
TERRAQUEST PROJECT NO.: 01195
a
r S S `o
r 8 § 5 {
<1
<5
<1
<3
<1
<1
380
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
160
270
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
720
<1,
<1
-
<1
<5
<1
<3
<1
<1
<50
440
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
190
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
7.6
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
220
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
<5
<1
<1
-
<1
<5
<1
<3
<1
<1.
<50
660
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
230
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
590
<1
<1
-
<10
<50
<10
<30
<10
<10
<500
250
<10
<10
-
<1
<5
<1
<3
1.7
<1
<50
-
<1
<1
-
<1
<5
<1
<3
2.2
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<0.119
<0.0570
<3
<0.298
,<0.169
<0.0920
<0.352
-
<0.103
<0.0870
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
-
<0.103
<0.0870
-
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
-
<0.103
<0.0870
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
-
<0.103
<0.0870
-
<0.119
<0.0570
<0.0920
<0.298
1.9
<0.0920
<0.352
-
<0.103
<0.0870
-
<1
<5
<1
<3
<1
<1
<50
-
<1
<1
-
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
1.34
-
<0.103
<0.0870
-
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
9.11
-
<0.103
<0.0870
0.47
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
-
<0.103
<0.0870
0.77
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
-
<0.103
<0.0870
<0.190
- ".
.n -
- n-
- 1oa
- -
en n47n
<n 357
-
<0.1OR
<0.OR70
<0.190
E
- - - -
-
140 - - - -
- - - 26.7
1,600
<5 - - - -
- - - 12.5
<1,000
<5-
- - - -
<1
9.4- - -
350 <100 <100 12.5
<1
<5 - - - -
- - - -
1,300
25 - - - -
_ _
_
<5
- - - 7/11/12 <12.5
<1,000
<5 - - - -
- - - -
2.1
<5 - - - -
_ 25
_
_
- - - -
2,200
11 230 11,000 <20 <10
- - - 25
<1,000
<5 - 7 - -
- - - -
<1,000
<5 - - -
- - - -
1,000
<5 - - - -
- - - 4/8/13 <12.5
1,800
<5 - - - -
- - - -
4,700
<5 - - - -
- - - -
<2.5
<5 - - - -
- - - 7/8/13<12.5
<2.5
<5 - - - -
- - - 7/8/13<12.5
<2.5
<5 - - - -
- - - -
<3.50
<3.30 - - - -
- - - 25
<2.5
<5-
- - - -
<3,500
<3.30 - - - -
- - - -
<3.50
<3.30 - - - -
- - - -
<2.5
<5 - - - -
_ 12.5
_
_
- - - -
<3.50
<3.30 - - - -
- - - -
<3,500
3.51 - - - -
- - - 12.5
<2.5
<5 - - - -
- - - -
<3.5
<3.3 - - - -
- - - -
4
<0.0033 - - - -
- - - -
7
<0.0033 - - - -
- - - 61.24
-
- - - - -
- - - -
<3.5
<3.30 - - -
8,000
<3.30
400 700 200 NE
NE
IS NE 50 100 NE
NE NE NE NE
NE
15.000 NE NE NE NE

Analytical Report .492563 -
for
Terraquest Environmental Consultants, P.C.
Project Manager:: Ryan Kerins
Colliseum
'01195
09-SEP-14
Collected By: Client
MENCO
Laboratories
Florida Testing Services, LLC
*,T,1*0--�0`61
vau
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab. code: TX00122):
Texas (T104704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T 1 04704400-TX) -
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104.704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)

Table of Contents
Cover Fage _
1`
Cover Letter
3
Sample ID Cross Reference
4t
Explanation of Qualifiers (Flags)
5.
Hits Summary
6
Certificate of Analysis (Detailed. Report)
10
Summary of Quality control
Blank Summary
19,
24
Chain of Custody
28
Sample Receipt Conformance Report
30
Page 2 of 30 Final 1.000

' •
Florida Testing Services, LLC
09-SEP-14
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 492563
Colliseum
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 492563. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 492563 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectftilly,
Mike Kimmel
Client Services Manager
Recipient of the Prestigious Small Business Administration: Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 3 of 30 Final 1.000

r/ to
• Sample Cross Reference 492563 E
I eau
..pjtRL�'W
Florida Testing Services, LLC Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id
Matrix
Date Collected Sample Depth
Lab Sample Id
Influent
W
09-02-1411:30
492563-001
After AST
W
09-02-14 11:25
492563-002
After 1st Carbon
W
09-02-14 11:05
492563-003
Effluent
W
09-02-14 11:00
492563-004
Page 4 of 30 Final 1.000

1
Flagging Criteria eORP
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Recipient of the Prestigious Sn:all Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd, Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone
Fax
(281) 2404200
[phone]
[phone]
[phone]
[phone]
[phone]
(8i3) 620-2000
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Page 5 of 30 Final 1.000

Hits Summary 492563 E`
Pau
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliscum
Sample Id: Influent
Matrix:
Ground Water
% Moisture:
Lab Sample Id: 492563-001
Date Collected:
09.02.14 11.30
Date Received: 09.03.14 10.50
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method:
SM620OB_PREP
Seq Number 950062
Date Prep:
09.07.14 22.12
Parameter
Cas Number
Result
Units
Analysis Date
Flag Dil
1,2,4-Trimethylbenzene
95-63-6
7.89
ug/L
09.08.14 03.29
1
1,3,5-Trimethylbenzene
108-67-8
3.28
ug/L
09.08.14 03.29
1
2-Butanone (MEK)
78-93-3
29.1
ug/L
09.08.14 03.29
1
Acetone
67-64-1
184
ug/L
09.08.14 03.29
1
Benzene
71-43-2
14.5
ug/L
09.08.14 03.29
1
Ethylbenzene
100-41-4
3.58
ug/L
09.08.14 03.29
1
Isopropyl ether
108-20-3
30.1
ug/L
09.08.14 03.29
1
Methyl tert-butyl ether (MTBE)
1634-04-4
1250
ug/L
09.08.14 04.00
D 50
Naphthalene
91-20-3
14.1
ug/L
09.08.14 03.29
1
Styrene
100-42-5
0.690
ug/L
09.08.14 03.29
1
Toluene
108-88-3
45.1
ug/L
09.08.14 03.29
1
m,p-Xylenes
179601-23-1
22.9
ug/L
09.08.14 03.29
1
o-Xylene
95-47-6
25.3
ug/L
09.08.14 03.29
1
Page 6 of 30 Final 1.000

Hits Summary 492563 �'
yy[w",
r�u
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: After AST Matrix: Ground Water % Moisture
Lab Sample Id: 492563-002 Date Collected: 09.02.14 11.25
Date Received: 09.03.14 10.50
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM620OB_PREP
Seq Number 950062 Date Prep: 09.07.14 22.12
Parameter Cas Number Result Units Analysis Date Flag Dil
Acetone 67-64-1 5.33 ug/L 09.08.14 03.01 1
Page 7 of 30 Final 1.000

f r % 75*
Hits Summary 492563 N
rau
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: After 1st Carbon Matrix : Ground Water % Moisture:
Lab Sample Id: 492563-003 Date Collected: 09.02.14 11.05
Date Received: 09.03.14 10.50
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B PREP
Seq Number 950062 Date Prep: 09.07.14 22.12
Parameter Cas Number Result Units Analysis Date Flag Dil
Acetone 67-64-1 13.8 ug/L 09.08.14 02.32 1
Chloroform 67-66-3 1.60 ug/L 09.08.14 02.32 1
Methyl tert-butyl ether (MTBE) 1634-04-4 2.68 ug/L 09.08.14 02.32 1
Page 8 of 30 Final 1.000

• Hits Summary 492563 MY
Florida Testing Services, LLC
Sample Id: Effluent
Lab Sample Id: 492563-004
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Matrix : Ground Water % Moisture
Date Collected: 09.02.14 11.00
Date Received: 09.03.14 10.50
Analytical Method: TSS by SM2540D
Seq Number 949829
Parameter
Total Suspended Solids
Cas Number Result Units Analysis Date Flag Dil
8.00 mg/L 09.03.1416.00 1
Page 9 of 30 Final 1.000

AV,
hij Certificate of Analytical Results 492563 tqe n
rau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: Influent
Lab Sample Id: 492563-001
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 950062
Parameter Cas Number
Matrix: Ground Water
Date Collected: 09.02.14 11.30
Date Prep: 09.07.14 22.12
Result RL MDL
Units
Date Received:09.03.14 10.50
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
09.08.1403.29
U 1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
09.08.14 03.29
U 1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
09.08.1403.29
U I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
09.08.14 03.29
U 1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
09.08.14 03.29
U 1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
09.08.14 03.29
U 1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
09.08.1403.29
U 1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
09.08.14 03.29
U 1
1,2,3-Tichloropropane
96-18-4
U
1.00
0.138
ug/L
09.08.14 03.29
U 1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
09.08.14 03.29
U 1
1,2,4-Trimethylbenzene
95-63-6
7.89
0.500
0.103
ug/L
09.08.14 03.29
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
09.08.14 03.29
U I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
09.08.14 03.29
U 1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
09.08.14 03.29
U 1
1,2-Dichloropropanc
78-87-5
U
0.500
0.122
ug/L
09.08.14 03.29
U 1
1,3,5-Trimethylbenzene
108-67-8
3.28
0.500
0.0870
ug/L
09.08.14 03.29
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
09.08.14 03.29
U 1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
09.08.14 03.29
U 1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
09.08.14 03.29
U 1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
09.08.14 03.29
U 1
2-Butanone (MEK)
78-93-3
29.1
20.0
0.378
ug/L
09.08.14 03.29
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
09.08.14 03.29
U 1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
09.08.14 03.29
U 1
4-Chlorotoluene
10643-4
U
0.500
0.0900
ug/L
09.08.14 03.29
U I
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
09.08.14 03.29
U 1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
09.08.14 03.29
U 1
Acetone
67-64-1
184
2.00
0.352
ug/L
09.08.14 03.29
1
Benzene
71-43-2
14.5
0.500
0.119
ug/L
09.08.14 03.29
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
09.08.14 03.29
U 1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
09.08.14 03.29
U I
Bromodichloromethane
75-274
U
0.500
0.124
ug/L
09.08.14 03.29
U 1
Bromoform
75-25-2
U
2.00
0.159
ug/L
09.08.14 03.29
U 1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
09.08.14 03.29
U 1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
09.08.14 03.29
U 1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
09.08.14 03.29
U 1
Chlorodibromomethane
12448-1
U
0.500
0.177
ug/L
09.08.14 03.29
U 1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
09.08.14 03.29
U 1
Chloroform
67-66-3
U
0.500
0.172
ug/L
09.08.14 03.29
U 1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
09.08.14 03.29
U 1
Page 10 of 30 Final 1.000

Certificate of Analytical Results 492563
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliscum
Sample Id: Influent
Lab Sample Id: 492563-001
Analytical Method: VOCs by GUMS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 950062
Parameter
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene (PCE)
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl Acetate
Vinyl Chloride
m,p-Xylenes
o-Xylene
Surrogate
1,2-D ichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Matrix: Ground Water Date Received:09.03.14 10.50
Date Collected: 09.02.14 11.30
Date Prep: 09.07.14 22.12
Cas Number
Result
RL
156-59-2
U
0.500
10061-01-5
U
1.00
75-71-8
U
1.00
64-17-5
U
50.0
100-41-4
3.58
0.500
108-20-3
30.1
0.500
98-82-8
U
0.500
1634-044
1250
25.0
75-09-2
U
0.500
91-20-3
14.1
2.00
104-51-8
U
2.00
103-65-1
U
1.00
135-98-8
U
0.500
100-42-5
0.690
0.500
98-06-6
U
0.500
127-18-4
U
0.500
108-88-3
45.1
0.500
156-60-5
U
0.500
10061-02-6
U
1.00
79-01-6
U
0.500
75-69-4
U
0.500
108-05-4
U
1.00
75-01-4
U
0.500
179601-23-1
22.9
1.00
95-47-6
25.3
0.500
Cas Number
Recovery
17060-07-0
98
460-00-4
98
2037-26-5
98
Prep Method: SM6200B_PREP
% Moisture:
MDL
Units
Analysis Date
0.114
ug/L
09.08.14 03.29
0.100
ug/L
09.08.14 03.29
0.0670
ug/L
09.08.14 03.29
3.00
ug/L
09.08.14 03.29
0.0920
ug/L
09.08.14 03.29
0.0920
ug/L
09.08.14 03.29
0.0980
ug/L
09.08.14 03.29
8.45
ug/L
09.08.14 04.00
0.190
ug/L
09.08.14 03.29
0.0940
ug/L
09.08.14 03.29
0.0600
ug/L
09.08.14 03.29
0.0650
ug/L
09.08.14 03.29
0.0920
ug/L
09.08.14 03.29
0.0740
ug/L
09.08.14 03.29
0.0890
ug/L
09.08.14 03.29
0.0540
ug/L
09.08.14 03.29
0.0570
ug/L
09.08.14 03.29
0.188
ug/L
09.08.14 03.29
0.110
ug/L
09.08.14 03.29
0.139
ug/L
09.08.14 03.29
0.0540
ug/L
09.08.14 03.29
0.720
ug/L
09.08.14 03.29
0.0810
ug/L
09.08.14 03.29
0.176
ug/L
09.08.14 03.29
0.122
ug/L
09.08.14 03.29
Units
Limits
Analysis Date
%
65-126
09.08.14 03.29
%
86-111
09.08.14 03.29
%
83-116
09.08.14 03.29
Flag
U
U
U
U
U
D
U
U
U
U
U
U
U
U
U
U
U
U
Flag.
Dil
1
1
1
1
1
1
1
50
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Page 11 of 30
Final 1.000

Certificate of Analytical Results 492563 �° t
f' 0� eau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: After AST Matrix: Ground Water Date Received:09.03.14 10.50
Lab Sample Id: 492563-002 Date Collected: 09.02.14 11.25
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 950062
Parameter Cas Number
Date Prep:
Result
09.07.14 22.12
RL MDL
Units
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
09.08.14 03.01
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
09.08.14 03.01
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
09.08.14 03.01
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
09.08.14 03.01
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
09.08.14 03.01
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
09.08.14 03.01
U
1
I,l-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
09.08.14 03.01
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
09.08.14 03.01
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
09.08.14 03.01
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
09.08.14 03.01
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
09.08.14 03.01
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
09.08.14 03.01
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
09.08.14 03.01
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
09.08.14 03.01
U
I
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
09.08.14 03.01
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
09.08.14 03.01
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
09.08.14 03.01
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
09.08.14 03.01
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
09.08.14 03.01
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
09.08.14 03.01
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
09.08.14 03.01
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0980
ug/L
09.08.14 03.01
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
09.08.14 03.01
U
1
4-Chlorotoluene
106-434
U
0.500
0.0900
ug/L
09.08.14 03.01
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
09.08.14 03.01
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
09.08.14 03.01
U
I
Acetone
67-64-1
5.33
2.00
0.352
ug/L,
09.09.14 03.01
1
Benzene
71-43-2
U
0.500
0.119
ug/L
09.08.14 03.01
U
I
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
09.08.14 03.01
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
09.08.14 03.01
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
09.08.14 03.01
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
09.08.14 03.01
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
09.08.14 03.01
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
09.08.14 03.01
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
09.08.14 03.01
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
09.08.14 03.01
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
09.08.14 03.01
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
09.08.14 03.01
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
09.08.14 03.01
U
1
Page 12 of 30 Final 1.000

• -��TO
Certificate of Analytical Results 492563
Terraquest Environmental Consultants, P.C., Mebane, NC
Collisetim
Sample Id: After AST Matrix: Ground Water Date Received:09.03.14 10.50
Lab Sample Id: 492563-002 Date Collected: 09.02.14 11.25
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 950062
Parameter Cas Number
Prep Method: SM620OB_PREP
% Moisture:
Date Prep: 09.07.14 22.12
Result RL MDL Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
09.08.14 03.01
U
I
cis- 1,3 -Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
09.08.14 03.01
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
09.08.14 03.01
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
09.08.14 03.01
U
1
Ethylbenzene
100-414
U
0.500
0.0920
ug/L
09.08.14 03.01
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
09.08.14 03.01
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
09.08.14 03.01
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
09.08.14 03.01
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
09.08.14 03.01
U
I
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
09.08.14 03.01
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
09.08.14 03.01
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
09.08.14 03.01
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
09.08.14 03.01
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
09.08.14 03.01
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
09.08.14 03.01
U
1
Tetrachloroethene(PCE)
127-184
U
0.500
0.0540
ug/L
09.08.14 03.01
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
09.08.14 03.01
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
09.08.14 03.01
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
09.08.14 03.01
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
09.08.14 03.01
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
09.08.14 03.01
U
1
Vinyl Acetate
108-054
U
1.00
0.720
ug/L
09.08.14 03.01
U
1
Vinyl Chloride
75-014
U
0.500
0.0810
ug/L
09.08.14 03.01
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
09.08.14 03.01
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
09.08.14 03.01
U
1
surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
94
%
65-126
09.08.14 03.01
4-Bromofluorobenzene
460-00-4
102
%
86-111
09.08.14 03.01
Toluene-D8
2037-26-5
98
%
83-116
09.08.14 03.01
Page 13 of 30 Final 1.000

f� LCertificate of Analytical Results 492563 �4elhtiiim ' i PJu
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: After 1st Carbon Matrix: Ground Water Date Received:09.03.14 10.50
Lab Sample Id: 492563-003 Date Collected: 09.02.14 11.05
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 950062
Parameter Cas Number
Date Prep:
Result
09.07.14 22.12
RL MDL
Units
Prep Method: SM620OB_PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
09.08.14 02.32
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
09.08.14 02.32
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
09.08.14 02.32
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
09.08.14 02.32
U
I
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
09.08.14 02.32
U
1
1,1-Dichloroethene
75-354
U
0.500
0.104
ug/L
09.08.14 02.32
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
09.08.14 02.32
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
09.08.14 02.32
U
1
1,2,3-Trichloropropane
96-184
U
1.00
0.138
ug/L
09.08.14 02.32
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
09.08.14 02.32
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
09.08.14 02.32
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
09.08.14 02.32
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
09.08.14 02.32
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
09.08.14 02.32
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
09.08.14 02.32
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
09.08.14 02.32
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
09.08.14 02.32
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
09.08.14 02.32
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
09.08.14 02.32
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
09.08.14 02.32
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
09.08.14 02.32
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
09.08.14 02.32
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
09.08.14 02.32
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
09.08.14 02.32
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
09.08.14 02.32
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
09.08.14 02.32
U
1
Acetone
67-64-1
13.8
2.00
0.352
ug/L
09.08.14 02.32
1
Benzene
71-43-2
U
0.500
0.119
ug/L
09.08.14 02.32
U
I
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
09.08.14 02.32
U
I
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
09.08.14 02.32
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
09.08.14 02.32
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
09.08.14 02.32
U
I
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
09.08.14 02.32
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
09.08.14 02.32
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
09.08.14 02.32
U
I
Chlorodibromomethane
12448-1
U
0.500
0.177
ug/L
09.08.14 02.32
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
09.08.14 02.32
U
1
Chloroform
67-66-3
1.60
0.500
0.172
ug/L
09.08.14 02.32
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
09.08.14 02.32
U
1
Page 14 of 30 Final 1.000

&
k lie
Certificate of Analytical
Results
492563
T
PJIA
Florida Testing Services, LLC
Terraquest Environmental
Consultants,
P.C.,
Mebane, NC
Colliseum
Sample Id: After 1st Carbon
Matrix:
Ground Water
Date Received:09.03.14 10.50
Lab Sample Id: 492563-003
Date Collected: 09.02.14
11.05
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
% Moisture:
Analyst: JOL
Date Prep:
09.07.14
22.12
Seq Number: 950062
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
09.08.14 02.32
U
1
cis- 1,3 -Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
09.08.14 02.32
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
09.08.14 02.32
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
09.08.14 02.32
U
1
Ethylbenzene
100-414
U
0.500
0.0920
ug/L
09.08.14 02.32
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
09.08.14 02.32
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
09.08.14 02.32
U
I
Methyl tert-butyl ether (MTBE)
1634-04-4
2.68
0.500
0.169
ug/L
09.08.14 02.32
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
09.08.14 02.32
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
09.08.14 02.32
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
09.08.14 02.32
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
09.08.14 02.32
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
09.08.14 02.32
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
09.08.14 02.32
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
09.08.14 02.32
U
1
Tetrachloroethene (PCE)
127-184
U
0.500
0.0540
ug/L
09.08.14 02.32
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
09.08.14 02.32
. U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
09.08.14 02.32
U
1
trans-1,3-Dichloropropene
10061-02-6.
U
1.00
0.110
ug/L
09.08.14 02.32
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
09.08.14 02.32
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
09.08.14 02.32
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
09.08.14 02.32
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
09.08.14 02.32
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
09.08.14 02.32
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
09.08.14 02.32
U
1
Surrogate
Cas Number Recovery
Units
Limits Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
95
%
65-126
09.08.14 02.32
4-Bromofluorobenzene
460-00-4
102
%
86-111
09.08.14 02.32
Toluene-D8
2037-26-5
100
%
83-116
09.08.14 02.32
Page 15 of 30 Final 1.000

Certificate of Analytical Results 492563 f'
Florida Testing services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: Effluent Matrix: Ground Water Date Received:09.03.14 10.50
Lab Sample Id: 492563-004 Date Collected: 09.02.14 11.00
Analytical Method: TSS by SM2540D
Tech: NSI
Analyst: NSI
Seq Number: 949829
Parameter
Total Suspended Solids
% Moisture:
Cas Number Result RL MDL Units Analysis Date Flag
8.00 4.00 3.50 mg/L 09.03.1416.00
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR % Moisture:
Analyst: 4150 Date Prep: 09.03.14 13.26
Seq Number: 949838
Parameter Cas Number Result RL MDL Units Analysis Date Flag
Lead 7439-92-1 U 0.0100 0.00330 mg/L 09.04.1413.31 U
Page 16 of 30 Final 1.000

Certificate Analytical Results 492563
of
Florida Testing Services, LLC
Terraquest Environmental
Consultants,
P.C.,
Mebane, NC
Colliseum
Sample Id: Effluent
Matrix:
Ground Water
Date Received:09.03.14 10.50
Lab Sample Id: 492563-004
Date Collected: 09.02.14 11.00
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM6200B PREP
Tech: JOL
% Moisture:
Analyst: JOL
Date Prep:
09.07.14 22.12
Seq Number: 950062
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
09.08.14 02.03
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
09.08.14 02.03
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
09.08.14 02.03
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
09.08.14 02.03
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
09.08.14 02.03
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
09.08.14 02.03
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
09.08.14 02.03
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
09.08.14 02.03
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
09.08.14 02.03
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
09.08.14 02.03
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
09.08.14 02.03
U
1
1,2-Dibromoethane(EDB)
106-93-4
U
1.00
0.180
ug/L
09.08.14 02.03
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
09.08.14 02.03
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
09.08.14 02.03
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
09.08.14 02.03
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
09.08.14 02.03
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
09.08.14 02.03
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
09.08.14 02.03
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
09.08.14 02.03
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
09.08.14 02.03
U
1
2-Butanone(MEK)
78-93-3
U
20.0
0.378
ug/L
09.08.14 02.03
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
09.08.14 02.03
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
09.08.14 02.03
U
1
4-Chlorotoluene
106-434
U
0.500
0.0900
ug/L
09.08.14 02.03
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
09.08.14 02.03
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
09.08.14 02.03
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
09.08.14 02.03
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
09.08.14 02.03
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
09.08.14 02.03
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
09.08.14 02.03
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
09.08.14 02.03
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
09.08.14 02.03
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
09.08.14 02.03
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
09.08.14 02.03
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
09.08.14 02.03
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
09.08.14 02.03
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
09.08.14 02.03
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
09.08.14 02.03
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
09.08.14 02.03
U
1
Page 17 of 30 Final 1.000

\'a LCertificate of Analytical Results 492563 �B
v�u
Terraquest Environmental Consultants, P.C.,
Colliseum
Sample Id: Effluent Matrix: Ground Water
Lab Sample Id: 492563-004 Date Collected: 09.02.14 11.00
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL Date Prep: 09.07.14 22.12
Seq Number: 950062
Parameter Cas Number Result RL MDL Units
Mebane, NC
Date Received:09.03.14 10.50
Prep Method: SM620OB_PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
09.08.14 02.03
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
09.08.14 02.03
U
I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
09.08.14 02.03
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
09.08.14 02.03
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
09.08.14 02.03
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
09.08.14 02.03
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
09.08.14 02.03
U
1
Methyl tert-butyl ether (MTBE)
1634-044
U
0.500
0.169
ug/L
09.08.14 02.03
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
09.08.14 02.03
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
09.08.14 02.03
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
09.08.14 02.03
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
09.08.14 02.03
U
I
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
09.08.14 02.03
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
09.08.14 02.03
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
09.08.14 02.03
U
1
Tetrachloroethene(PCE)
127-18-4
U
0.500
0.0540
ug/L
09.08.14 02.03
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
09.08.14 02.03
U
I
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
09.08.14 02.03
U
1
trans- l,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
09.08.14 02.03
U
I
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
09.08.14 02.03
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
09.08.14 02.03
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
09.08.14 02.03
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
09.08.14 02.03
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
09.08.14 02.03
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
09.08.14 02.03
U
I
Surrogate
Cas Number Recovery
Units
Limits Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
96
%
65-126
09.08.14 02.03
4-Bromofluorobenzene
460-00-4
102
%
86-111
09.08.14 02.03
Toluene-D8
2037-26-5
100
%
83-116
09.08.14 02.03
Page 18 of 30 Final 1.000

�[C Q
� QC Summary 492563
Qi Pau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Colliseum
Analytical Method: TSS by SM2540D
Seq Number: 949829
Matrix:
Water
MB Sample Id: 949829-1-BLK
LCS Sample Id:
949829-1-BKS
LCSD Sample Id: 949829-1-BSD
MB Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Parameter Result Amount
Result %Rec
Result %Rec
Limit Date
Total Suspended Solids <3.50 100
97.0 97
94.0 94
80-120 3 10 mg/L 09.03.14 16:00
Analytical Method: TSS by SM2540D
Seq Number:
949829
Matrix:
Water
Parent Sample Id:
492533-009
MD Sample Id:
492533-009 D
Parent
MD
%RPD RPD Units Analysis Flag
Parameter
Result
Result
Limit Date
Total Suspended Solids
15.0
15.0
0 10 mg/L 09.03.14 16:00
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
949838
Matrix:
Water
Date Prep: 09.03.14
MB Sample Id:
660977-1-BLK
LCS Sample Id:
660977-1-BKS
LCSD Sample Id: 660977-1-BSD
MB Spike
LCS LCS
LCSD LCSD Limits
%RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
0.981 98
0.988 99 80-120
1 20 mg/L 09.04.1412:58
Analytical Method: Lead by SW-846 6010C
Seq Number: 949838 Matrix: Water
Parent Sample Id: 492533-003 MD Sample Id: 492533-003 D
Parent MD
Parameter
Result Result
Lead 0.00410 0.0129
Prep Method: SW3010A
Date Prep: 09.03.14
%RPD RPD Units Analysis Flag
Limit Date
104 20 mg/L 09.04.1413:03 F
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
949838
Matrix:
Water
Date Prep: 09.03.14
Parent Sample Id:
492533-003
MS Sample Id:
492533-003 S
MSD Sample Id: 492533-003 SD
Parent Spike
MS MS
MSD MSD Limits
%RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
0.00410 1.00
1.05 105
1.14 114 80-120
8 20 mg/L 09.04.1413:05
Page 19 of 30 Final 1.000

•
Florida Testing Services, LLC
Analytical Method:
Seq Number:
MB Sample Id:
Parameter
QC Summary 492563
Terraquest Environmental Consultants, P.C.
Colliseum
VOCs by GUMS by SM6200B
950062 Matrix: Water
661189-1-BLK LCS Sample Id: 661189-1-BKS
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1, 1 -Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloroprop ane
1,2,4-Trichlorobenzene
1,2,4-Trimethylb enzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
MB
Spike
LCS
LCS
LCSD
LCSD
Result
Amount
Result
%Rec
Result
%Rec
<0.180
25.0
26.8
107
28.1
112
<0.0760
25.0
26.1
104
26.9
108
<0.0700
25.0
27.5
110
27.2
109
<0.113
25.0
28.1
112
29.9
120
<0.121
25.0
26.9
108
27.3
109
<0.104
25.0
28.4
114
26.9
108
<0.0600
25.0
27.1
108
27.4
110
<0.118
25.0
25.9
104
25.6
102
<0.138
25.0
26.9
108
27.8
ill
<0.0690
25.0
29.1
116
29.8
119
<0.103
25.0
26.4
106
27.3
109
<0.180
25.0
27.3
109
27.6
110
<0.0940
25.0
27.1
108
27.6
110
<0.0900
25.0
26.7
107
26.0
104
<0.122
25.0
26.6
106
27.4
110
<0.0870
25.0
26.4
106
27.2
109
<0.0980
25.0
26.4
106
26.8
107
<0.133
25.0
28.2
113
28.3
113
<0.0670
25.0
26.2
105
26.9
108
<0.0970
25.0
28.4
114
28.8
115
<0.378
50.0
57.1
114
56.0
112
<0.0880
25.0
25.1
100
25.6
102
<0.352
50.0
58.6
117
59.4
119
<0.0900
25.0
26.3
105
26.9
108
<0.0890
25.0
26.5
106
27.2
109
<0.253
50.0
54.2
108
53.0
106
<0.352
50.0
51.2
102
55.2
110
<0.119
25.0
26.9
108
27.3
109
<0.132
25.0
25.5
102
25.3
101
<0.112
25.0
29.3
117
28.8
115
<0.124
25.0
27.7
ill
27.7
ill
<0.159
25.0
29.0
116
28.9
116
<0.0970
25.0
26.8
107
27.2
109
<0.0990
25.0
26.8
107
27.2
109
<0.105
25.0
26.5
106
26.8
107
<0.177
25.0
27.7
ill
28.2
113
<0.0420
25.0
26.0
104
26.1
104
<0.172
25.0
27.1
108
27.4
110
<0.0850
25.0
24.5
98
25.4
102
<0.114
25.0
27.0
108
28.3
113
<0.100
25.0
28.8
115
29.1
116
<0.0670
25.0
27.7
ill
26.9
108
<3.00
1000
1130
113
1120
112
<0.0920
25.0
27.3
109
27.8
ill
<0.0920
25.0
27.1
108
27.1
108
<0.0980
25.0
26.1
104
26.9
108
<0.169
50.0
57.6
115
57.9
116
<0.190
25.0
26.0
104
25.9
104
<0.0940
25.0
25.9
104
26.0
104
<0.0600
25.0
27.4
110
28.1
112
<0.0650
25.0
26.0
104
26.7
107
<0.0920
25.0
25.8
103
26.9
108
Prep Method:
SM620OB_PREP
Date Prep:
09.07.14
LCSD Sample Id: 661189-1-BSD
Limits
%RPD
RPD
Units
Analysis Flag
Limit
Date
75-127
5
20
ug/L
09.07.14 23:40
62-128
3
20
ug(L
09.07.14 23:40
77-129
1
20
ug/L
09.07.14 23:40
86-120
6
20
ug/L
09.07.14 23:40
82-114
1
20
ug(L
09.07.14 23:40
73-123
5
22
ug/L
09.07.14 23:40
83-125
1
20
ug/L
09.07.14 23:40
57-127
1
20
ug/L
09.07.14 23:40
79-118
3
20
ug/L
09.07.14 23:40
59-125
2
20
ug/L
09.07.14 23:40
84-118
3
20
ug/L
09,07.14 23:40
83-126
1
20
ug/L
09.07.14 23:40
89-126
2
20
ug/L
09.07.14 23:40
56-133
3
20
ug/L
09.07.14 23:40
79-127
3
20
ug/L
09.07.14 23:40
86-118
3
20
ug/L
09.07.14 23:40
90-126
2
20
ug/L
09.07.14 23:40
85-121
0
20
ug(L
09.07.14 23:40
88-121
3
20
ug(L
09.07.14 23:40
76-126
1
20
ug/L
09.07.14 23:40
66-133
2
20
ug/L
09.07.14 23:40
80-128
2
20
ug/L
09.07.14 23:40
70-130
1
20
ug(L
09.07.14 23:40
82-130
2
20
ug/L
09.07.14 23:40
80-128
3
20
ug/L
09.07.14 23:40
74-129
2
20
ug/L
09.07.14 23:40
51-143
8
21
ug/L
09.07.14 23:40
81-123
1
20
ug/L
09.07.14 23:40
84-114
1
20
ug/L
09.07.14 23:40
89-127
2
20
ug/L
09.07.14 23:40
70-129
0
20
ug/L
09.07.14 23:40
73-140
0
20
ug/L
09.07.14 23:40
53-143
1
20
ug/L
09.07.14 23:40
66-136
1
20
ug/L
09.07.14 23:40
88-118
1
20
ug/L
09.07.14 23:40
73-139
2
20
ug/L
09.07.14 23:40
70-123
0
20
ug/L
09.07.14 23:40
72-118
1
20
ug/L
09.07.14 23:40
65-125
4
20
ug/L
09.07.14 23:40
85-125
5
20
ug/L
09.07.14 23:40
92-126
1
20
ug/L
09.07.14 23:40
48-143
3
20
ug/L
09.07.14 23:40
61-133
1
20
ug(L
09.07.14 23:40
87-123
2
20
ug(L
09.07.14 23:40
77-125
0
20
ug/L
09.07.14 23:40
82-115
3
20
ug/L
09.07.14 23:40
53-149
1
20
ug/L
09.07.14 23:40
75-119
0
20
ug/L
09.07.14 23:40
52-116
0
20
ug(L
09.07.14 23:40
83-130
3
20
ug/L
09.07.14 23:40
84-122
3
20
ug/L
09.07.14 23:40
86-120
4
20
ug/L
09.07.14 23:40
Page 20 of 30 Final 1.000

•
1
Florida Testing Services, LLC
QC Summary 492563
Terraquest Environmental Consultants, P.C.
Colliseum
Analytical Method:
VOCs by GCIMS by SM6200B
Prep Method: SM620OB_PREP
Seq Number:
950062
Matrix:
Water
Date Prep: 09.07.14
MB Sample Id:
661189-1-BLK
LCS Sample Id:
661189-1-BKS
LCSD Sample Id: 661189-1-BSD
MB
Spike
LCS
LCS
LCSD
LCSD
Limits %RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
27.8
111
28.3
113
85-123
2 20
ug/L
09.07.14 23:40
tert-Butylbenzene
<0.0890
25.0
25.8
103
26.8
107
79-126
4 20
ug/L
09.07.14 23:40
Tetrachloroethene (PCE)
<0.0540
25.0
26.9
108
27.7
111
64-131
3 20
ug/L
09.07.14 23:40
Toluene
<0.0570
25.0
26.5
106
26.8
107
89-116
1 20
ug/L
09.07.14 23:40
trans-1,2-Dichloroethene
<0.188
25.0
27.0
108
27.1
108
78-118
0 20
ug/L
09.07.14 23:40
trans-1,3-Dichloropropene <0.110
25.0
30.5
122
30.2
121
86-127
1 20
ug/L
09.07.14 23:40
Trichloroethene
<0.139
25.0
26.9
108
27.5
110
82-119
2 20
ug/L
09.07.14 23:40
Trichlorofluoromethane
<0.0540
25.0
28.3
113
27.7
111
46-144
2 20
ug/L
09.07.14 23:40
Vinyl Acetate
<0.720
25.0
28.3
113
28.5
114
58-141
1 20
ug/L
09.07.14 23:40
Vinyl Chloride
<0.0810
25.0
28.1
112
27.1
108
76-122
4 20
ug/L
09.07.14 23:40
m,p-Xylenes
<0.176
50.0
53.4
107
55.2
110
90-125
3 20
ug/L
09.07.14 23:40
o-Xylene
<0.122
25.0
27.3
109
27.6
110
86-119
1 20
ug/L
09.07.14 23:40
MB
MB
LCS
LCS
LCSD
LCSD
Limits
Units
Analvsis
Surrogate
%Rec
Flag
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
99
100
99
65-126
%
09.07.14 23:40
4-Bromofluorobenzene
104
99
99
70-130
%
09.07.14 23:40
Toluene-D8
100
100
100
83-116
%
09.07.14 23:40
Page 21 of 30 Final 1.000

t
Florida Testing Services, LLC
Analytical Method:
Seq Number:
Parent Sample Id:
Parameter
QC Summary 492563
Terraquest Environmental Consultants, P.C.
Colliseum
VOCs by GC/MS by SM6200B Prep Method:
950062 Matrix: Ground Water Date Prep:
492563-004 MS Sample Id: 492563-004 S MSD Sample Id:
1, 1, 1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1, 1 -Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimetliylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyltoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodi fluoromethane
Ethanol
Etylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
PU BE0
/ rau
SM620OB_PREP
09.07.14
492563-004 SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD
RPD
Units
Analysis Flag
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
<0.180
25.0
28.0
112
26.7
107
76-126
5
20
ug/L
09.08.14 04:33
<0.0760
25.0
26.6
106
25.0
100
63-128
6
20
ug/L
09.08.14 04:33
<0.0700
25.0
26.8
107
27.2
109
79-133
1
20
ug/L
09.03.14 04:33
<0.113
25.0
28.5
114
28.8
115
82-126
1
20
ug/L
09.08.14 04:33
<0.121
25.0
26.9
108
25.3
101
77-120
6
20
ug/L
09.08.14 04:33
<0.104
25.0
26.2
105
25.4
102
67-123
3
22
ug/L
09.08.14 04:33
<0.0600
25.0
26.8
107
25.4
102
76-126
5
20
ug1L
09.08.14 04:33
<0.118
25.0
25.2
101
24.3
97
41-136
4
20
ug/L
09.08.14 04:33
<0.138
25.0
24.6
98
26.7
107
77-125
8
20
ug/L
09.08.14 04:33
<0.0690
25.0
28.7
115
26.4
106
41-132
8
20
ug/L
09.08.14 04:33
<0.103
25.0
26.6
106
25.0
100
53-141
6
20
ug/L
09.08.14 04:33
<0.180
25.0
27.1
108
27.3
109
82-130
1
20
ug/L
09.08.14 04:33
<0.0940
25.0
27.3
109
25.8
103
83-128
6
20
ug/L
09.08.14 04:33
<0.0900
25.0
26.4
106
26.2
105
59-134
1
20
ug/L
09.08.14 04:33
<0.122
25.0
26.5
106
25.8
103
79-125
3
20
ug/L
09.08.14 04:33
<0.0870
25.0
26.5
106
24.6
98
69-125
7
20
ug/L
09.08.14 04:33
<0.0980
25.0
25.6
102
24.5
98
83-126
4
20
ug/L
09.08.14 04:33
<0.133
25.0
28.1
112
27.3
109
85-124
3
20
ug(L
09.08.14 04:33
<0.0670
25.0
26.2
105
24.7
99
82-121
6
20
ug/L
09.08.14 04:33
<0.0970
25.0
23.0
92
22.4
90
56-122
3
20
ug/L
09.08.14 04:33
<0.378
50.0
52.0
104
58.7
117
66-136
12
20
ug/L
09.08.14 04:33
<0.0880
25.0
25.6
102
24.2
97
73-129
6
20
ug/L
09.08.14 04:33
<0.352
50.0
58.0
116
61.3
123
63-140
6
20
ug/L
09.08.14 04:33
<0.0900
25.0
26.0
104
24.7
99
76-129
5
20
ug/L
09.08.14 04:33
<0.0890
25.0
26.3
105
24.5
98
73-126
7
20
ug/L
09.08.14 04:33
<0.253
50.0
53.6
107
55.7
Ill
71-140
4
20
ug/L
09.08.14 04:33
<0.352
50.0
49.5
99
57.8
116
47-138
15
21
ug/L
09.08.14 04:33
<0.119
25.0
27.1
108
25.4
102
70-135
6
20
ug/L
09.08.14 04:33
<0.132
25.0
25.8
103
24.8
99
76-120
4
20
ug/L
09.08.14 04:33
<0.112
25.0
29.0
116
29.0
116
83-132
0
20
ug/L
09.08.14 04:33
<0.124
25.0
26.8
107
27.1
108
66-132
1
20
ug/L
09.08.14 04:33
<0.159
25.0
28.1
112
28.9
116
63-143
3
20
ug/L
09.08.14 04:33
<0.0970
25.0
26.2
105
24.1
96
60-134
8
20
ug/L
09.08.14 04:33
<0.0990
25.0
26.9
108
25.2
101
59-139
7
20
ug/L
09.08.14 04:33
<0.105
25.0
26.5
106
24.8
99
83-120
7
20
ug/L
09.08.14 04:33
<0.177
25.0
28.3
113
27.9
112
68-140
1
20
ug/L
09.08.14 04:33
<0.0420
25.0
25.7
103
22.3
89
67-125
14
20
ug(L
09.08.14 04:33
<0.172
25.0
26.9
108
26.0
104
72-120
3
20
ug/L
09.08.14 04:33
<0.0850
25.0
23.8
95
22.7
91
59-128
5
20
ug/L
09.08.14 04:33
<0.114
25.0
27.3
109
26.4
106
80-125
3
20
ug/L
09.08.14 04:33
<0.100
25.0
27.0
108
26.8
107
74-122
1
20
ug/L
09.08.14 04:33
<0.0670
25.0
26.9
108
24.8
99
48-138
8
20
ug/L
09.08.14 04:33
<3.00
1000
968
97
1080
108
55-140
11
20
ug/L
09.08.14 04:33
<0.0920
25.0
27.3
109
26.0
104
70-140
5
20
ug/L
09.08.14 04:33
<0.0920
25.0
27.0
108
26.6
106
70-132
1
20
ug/L
09.08.14 04:33
<0.0980
25.0
26.0
104
24.8
99
75-117
5
20
ug/L
09.08.14 04:33
<0.169
50.0
55.0
110
57.1
114
51-155
4
20
ug/L
09.08.14 04:33
<0.190
25.0
20.6
82
21.0
84
71-126
2
20
ug/L
09.08.14 04:33
<0.0940
25.0
25.1
100
24.7
99
34-135
2
20
ug/L
09.08.14 04:33
<0.0600
25.0
27.1
108
24.5
98
73-128
10
20
ug(L
09.08.14 04:33
<0.0650
25.0
26.0
104
24.6
98
75-125
6
20
ug/L
09.08.14 04:33
<0.0920
25.0
25.8
103
24.2
97
77-122
6
20
ug/L
09.08.14 04:33
Page 22 of 30 Final 1.000

QC Summary 492563
• 9 �JIA
L NIF rw
Flodda Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Colliseum
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM620OB_PREP
Seq Number: 950062
Matrix:
Ground Water
Date Prep: 09.07.14
Parent Sample Id: 492563-004
MS Sample Id:
492563-004 S
MSD Sample Id: 492563-004 SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
28.6
114
26.9
108
54-137
6
20
ug/L
09.08.14 04:33
tert-Butylbenzene
<0.0890
25.0
25.9
104
24.3
97
74-124
6
20
ug/L
09.08.14 04:33
Tetrachloroethene (PCE)
<0.0540
25.0
26.7
107
25.6
102
57-130
4
20
ug/L
09.08.14 04:33
Toluene
<0.0570
25.0
26.7
107
25.3
101
81-125
5
20
ug/L
09.08.14 04:33
trans-1,2-Dichloroethene
<0.188
25.0
27.6
110
25.9
104
69-122
6
20
ug/L
09.08.14 04:33
trans-1,3-Dichloropropene
<0.110
25.0
29.3
117
28.6
114
73-129
2
20
ug/L
09.08.14 04:33
Trichloroethene
<0.139
25.0
27.5
110
25.0
100
73-124
10
20
ug/L
09.08.14 04:33
Trichlorofluoromethane
<0.0540
25.0
26.9
108
25.1
100
49-139
7
20
ug/L
09.08.14 04:33
Vinyl Acetate
<0.720
25.0
27.1
108
26.3
105
57-134
3
20
ug/L
09.08.14 04:33
Vinyl Chloride
<0.0810
25.0
26.3
105
24.8
99
70-121
6
20
ug/L
09.08.14 04:33
m,p-Xylenes
<0.176
50.0
54.3
109
51.1
102
65-151
6
20
ug/L
09.08.14 04:33
o-Xylene
<0.122
25.0
27.5
110
26.2
105
58-148
5
20
ug/L
09.08.14 04:33
MS
MS
MSD
MSD
Limits
Units
Analysis
Surrogate
g
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
99
100
65-126
%
09.08.14 04:33
4-Bromofluorobenzene
99
98
86-111
%
09.08.14 04:33
Toluene-D8
99
98
83-116
%
09.08.14 04:33
Page 23 of 30 Final 1.000

• Blank Summary 492563
.,.—
t ... o'..Ju
B9RASo• ' �
Florida Testing Services, LLC
Sample Id: 660977-1-BLK
Lab Sample Id: 660977-1-BLK
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Matrix: WATER
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR
Analyst: 4150 Date Prep: 09.03.14 13:26
Seq Number: 949838
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Lead 7439-92-1 U 0.0100 0.00330 mg/L 09.04.1412:51 U I
Page 24 of 30 Final 1.000

• Blank Summary 492563
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: 661189-1-BLK Matrix: WATER
Lab Sample Id: 661189-1-BLK
Analytical Method: VOCs by GUMS by SM6200B Prep Method: SM620OB_PREP
Tech: JOL
Analyst: JOL Date Prep: 09.07.14 22:12
Seq Number: 950062
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
1, 1, 1,2-Tetrachloroethane 630-20-6 U 1.00 0.180 ug/L 09.08.14 01:35 U I
1, 1, 1 -Trichloro ethane 71-55-6 U 0.500 0.0760 ug/L 09.08.14 01:35 U 1
1,1,2,2-Tetrachloroethane 79-34-5 U 0.500 0.0700 ug/L 09.08.14 01:35 U 1
1,1,2-Trichloroethane 79-00-5 U 0.500 0.113 ug/L 09.08.14 01:35 U 1
1, 1 -Dichloroethane 75-34-3 U 0.500 0.121 ug/L 09.08.14 01:35 U 1
1,1-Dichloroethene 75-35-4 U 0.500 0.104 ug/L 09.08.14 01:35 U 1
1,1-Dichloropropene 563-58-6 U 0.500 0.0600 ug/L 09.08.14 01:35 U 1
1,2,3-Trichlorobenzene 87-61-6 U 2.00 0.118 ug/L 09.08.14 01:35 U 1
1,2,3-Trichloropropane 96-18-4 U 1.00 0.138 ug/L 09.08.14 01:35 U I
1,2,4-Trichlorobenzene 120-82-1 U 1.00 0.0690 ug/L 09.08.14 01:35 U 1
1,2,4-Trimethylbenzene 95-63-6 U 0.500 0.103 ug/L 09.08.14 01:35 U 1
1,2-Dibromoethane (EDB) 106-93-4 U 1.00 0.180 ug/L 09.08.14 01:35 U 1
1,2-Dichlorobenzene 95-50-1 U 0.500 0.0940 ug/L 09.08.14 01:35 U 1
1,2-Dichloroethane 107-06-2 U 0.500 0.0900 ug/L 09.08.14 01:35 U 1
1,2-Dichloropropane 78-87-5 U 0.500 0.122 ug/L 09.08.14 01:35 U 1
1,3,5-Trimethylbenzene 108-67-8 U 0.500 0.0870 ug/L 09.08.14 01:35- U I
1,3-Dichlorobenzene 541-73-1 U 0.500 0.0980 ug/L 09.08.14 01:35 U I
1,3-Dichloropropane 142-28-9 U 0.500 0.133 ug/L 09.08.14 01:35 U I
1,4-Dichlorobenzene 106-46-7 U 0.500 0.0670 ug/L 09.08.14 01:35 U 1
2,2-Dichloropropane 594-20-7 U 0.200 0.0970 ug/L 09.08.14 01:35 U 1
2-Butanone (MEK) 78-93-3 U 20.0 0.378 ug/L 09.08.14 01:35 U 1
2-Chlorotoluene 95.49-8 U 0.200 0.0880 ug/L 09.08.14 01:35 U 1
2-Hexanone 591-78-6 U 0.400 0.352 ug/L 09.08.14 01:35 U I
4-Chlorotoluene 106-43-4 U 0.500 0.0900 ug/L 09.08.14 01:35 U 1
4-Isopropyltoluene 99-87-6 U 0.500 0.0890 ug/t 09.08.14 01:35 U 1
4-Methyl-2-pentanone (MIBK) 108-10-1 U 0.400 0.253 ug/L 09.08.14 01:35 U 1
Acetone 67-64-1 U 2.00 0.352 ug/L 09.08.14 01:35 U 1
Benzene 71-43-2 U 0.500 0.119 ug/L 09.08.14 01:35 U 1
Bromobenzene 108-86-1 U 0.500 0.132 ug/L 09.08.14 01:35 U 1
Bromochloromethane 74-97-5 U 0.500 0.112 ug/L 09.08.14 01:35 U 1
Bromodichloromethane 75-27-4 U 0.500 0.124 ug/L 09.08.14 01:35 U 1
Bromoform 75-25-2 U 2.00 0.159 ug/L 09.08.14 01:35 U 1
Bromomethane 74-83-9 U 1.00 0.0970 ug/L 09.08.14 01:35 U 1
Carbon tetrachloride 56-23-5 U 0.500 0.0990 ug/L 09.08.14 01:35 U I
Chlorobenzene 108-90-7 U 0.500 0.105 ug/L 09.08.14 01:35 U 1
Chlorodibromomethane 124-48-1 U 0.500 0.177 ug/L 09.08.14 01:35 U 1
Chloroethane 75-00-3 U 0.500 0.0420 ug/L 09.08.14 01:35 U 1
Chloroform 67-66-3 U 0.500 0.172 ug/L 09.08.14 01:35 U 1
Chloromethane 74-87-3 U 0.500 0.0850 ug/L 09.08.14 01:35 U 1
cis-1,2-Dichloroethene 156-59-2 U 0.500 0.114 ug/L 09.08.14 01:35 U 1
Page 25 of 30 Final 1.000

• Blank Summary 492563
l eau
Florida Testing Services, LLC
Sample Id: 661189-1-BLK
Lab Sample Id: 661189-1-BLK
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Matrix: WATER
Analytical Method: VOCs by GOMS by SM6200B
Prep Method: SM620OB_PREP
Tech: JOL
Analyst: JOL
Date Prep: 09.07.14 22:12
Seq Number: 950062
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
09.08.14 01:35
U
I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
09.08.14 01:35
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
09.08.14 01:35
U
1
Ethylbenzene
100-414
U
0.500
0.0920
ug/L
09.08.14 01:35
U
I
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
09.08.14 01:35
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
09.08.14 01:35
U
I
Methyl tert-butyl ether (MTBE)
1634-044
U
0.500
0.169
ug/L
09.08.14 01:35
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
09.08.14 01:35
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
09.08.14 01:35
U
I
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
09.08.14 01:35
U
I
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
09.08.14 01:35
U
I
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
09.08.14 01:35
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
09.08.14 01:35
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
09.08.14 01:35
U
1
Tetrachloroethene (PCE)
127-184
U
0.500
0.0540
ug/L
09.08.14 01:35
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
09.08.14 01:35
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
09.08.14 01:35
U
I
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
09.08.14 01:35
U
I
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
09.08.14 01:35
U
I
Trichlorofluoromethane
75-694
U
0.500
0.0540
ug/L
09.08.14 01:35
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
09.08.14 01:35
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
09.08.14 01:35
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
09.08.14 01:35
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
09.08.14 01:35
U
1
Page 26 of 30 Final 1.000

l?O\
Blank Summary 492563
V
(y PJu
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum
Sample Id: 949829-1-BLK Matrix: WATER
Lab Sample'Id: 949829-1-BLK
Analytical Method: TSS by SM2540D Prep Method:
Tech: NSI
Analyst: NSI Date Prep:
Seq Number: 949829
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Total Suspended Solids U 4.00 3.50 mg/L 09.03.14 16:00 U 1
Page 27 of 30 Final 1.000

"011 CHAIN OF CUSTODY Page l ofL
X.AVORATOPPES,
' �y'
FED -EX/ UPS: Tracking #
Bottle Order Control #
6017 Financial Drive, Norcross, GA 30071 (770.449-8800)
Xenco Quote #
Xenco Work order#
4143 Greenbriar Dr., Stafford, TX 77477 (281-240-4200)
9701 Harry Hines Blvd, Dallas, TX 75220 (214-902-0300)
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Project Number(ID): 11 -1�
GW =Ground Water
Terra nest Environmental Consultants, P.C.
a • •
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DW =-Drinking Water
SW zi Surface water
Project contact E-mail 11
Project Name: (streeUoross road, location)
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PLoProduct Liquid
Address
WW IN waste water
100-E. Ruffin Street
S-soil/sed /solid
Purchase Order I (it required)
city. Mebane, NO 27302
SL=sludge
O =oil
phone:[phone] Fax[phone]
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XENCO. Laboratories
Prelogin/Nonconformarice. Report- Sample Log -In
Florida Testing Services, LLC
Client: Terraquest Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC
Date/ Time Received: 09/03/2014 10:50:00 AM Air and Metal samples Acceptable Range: Ambient
Work Order #: 492563 Temperature Measuring device used : #61
Sample Receipt Checklist Comments
#1 *Temperature of cooler(s)?
1.5
#2 *Shipping container in good condition?
Yes
#3 *Samples received on ice?
Yes
#4 *Custody Seals intact on shipping container/ cooler?
N/A
#5 Custody Seals intact on sample bottles?
N/A
#6 *Custody Seals Signed and dated?
N/A
#7 *Chain of Custody present?
Yes
#8 Sample instructions complete on Chain of Custody?
Yes
#9 Any missing/extra samples?
No
#10 Chain of Custody signed when relinquished/ received?
Yes
#11 Chain of Custody agrees with sample label(s)?
Yes
#12 Container label(s) legible and intact?
Yes
#13 Sample matrix/ properties agree with Chain of Custody?
Yes
#14 Samples in proper container/ bottle?
Yes
#15 Samples properly preserved?
Yes
#16 Sample container(s) intact?
Yes
#17 Sufficient sample amount for indicated test(s)?
Yes
#18 All samples received within hold time?
Yes
#19 Subcontract of sample(s)?
No
#20 VOC samples have 'zero headspace (less than 1/4 inch bubble)?
Yes
#21 <2 for all samples preserved with HNO3,HCL, H2SO4?
Yes
#22 >10 for all samples preserved with NaAs02+NaOH, ZnAc+NaOH?
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: DL PH Device/Lot#: 1016662-2
Checklist completed by: Z901
Dario Lagunas
Checklist reviewed by:�
Mike Kimmel
Date: 09/03/2014 .
Date: 09/04/2014
Page 30 of 30 Final 1.000

Analytical Report 491299
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Colliseum Shell
01195
19-AUG-14
Collected By: Client
XIENCO
Laboratories
Florida Testing Services, LLC
PCC���
a ��A'
•�--= .. ..der
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (Tl04704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Texas (T104704477), Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (Tl04704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (T104704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Page 1 of 29 Final 1.000

Table of Contents
Cover Letter
—
3
�4
Sample ID Cross Reference _ _
Explanation of Qualifiers (Flags)
_ _ _ 4
5
Hits Summary �^
Certificate of Analysis (Detailed Report)
9
�—
Summary of Quality contrgl_ �
_ 181
Blank Summary
23
Chain of Custody y
_ 27
Sample Receipt Conformance Report
29
Page 2 of 29 Final 1.000

p[Cgp�
,9 i PJIA
19-AUG-14
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 491299
Colliseum Shell
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 491299. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this reportwill remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by-XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 491299 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we,
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Mike Kimmel
Client Services Manager
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 3 of 29 Final 1.000

WNI
Sample Cross Reference 491299BQRA39
Florida Testing Services,LLc Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id
Matrix
Date Collected Sample Depth
Lab Sample Id
Influent
W
08-11-1411:50
491299-001
After AST
W
08-11-14 11:45
491299-002
After 1st Carbon
W
08-11-14 11:47
491299-003
Effluent
W
08-11-1411:35
491299-004
Page 4 of 29 Final 1.000

LU
•
in US
Flagging Criteria aea�'
Florida Testing Services, LLC
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
Phone Fax
4143 Greenbriar Dr, Stafford, TX 77477 [phone] (281) 2404280
9701 Harry Hines Blvd, Dallas, TX 75220 [phone] [phone]
5332 Blackberry Drive, San Antonio TX 78238 [phone] [phone]
2505 North Falkenburg Rd, Tampa, FL 33619 [phone] [phone]
12600 West I-20 East, Odessa, TX 79765 [phone] [phone]
6017 Financial Drive, Norcross, GA 30071 [phone] [phone]
3725 E. Atlanta Ave, Phoenix, AZ 85040 [phone]
Page 5 of 29 Final 1.000

Hits Summary 491299
rcc�,a
Sample Id: Influent
Lab Sample Id: 491299-001
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Matrix : Ground Water
Date Collected: 08.11.14 11.50
Date Received: 08.12.14 14.20
Analytical Method: VOCs by GUMS by SM6200B
Seq Number 948247
Parameter
Cas Number
1,2,4-Trimethylbenzene
95-63-6
1,3,5-Trimethylbenzene
108-67-8
4-Isopropyltoluene
99-87-6
Acetone
67-64-1
Benzene
71-43-2
Ethylbenzene
100-41-4
Isopropyl ether
108-20-3
Isopropylbenzene
98-82-8
Methyl tert-butyl ether (MTBE)
1634-04-4
Naphthalene
91-20-3
n-Propylbenzene
103-65-1
sec-Butylbenzene
135-98-8
Toluene
108-88-3
m,p-Xylenes
179601-23-1
o-Xylene
95-47-6
Result
59.7
15.5
0.200
100
36.5
28.5
37.6
1.10
1740
63.5
4.49
0.230
122
115
77.4
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
% Moisture:
Prep Method: SM620OB_PREP
Date Prep: 08.14.14 06.34
Analysis Date Flag Dil
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 15.01
1
1
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 16.56
D
10
08.14.14 15.01
1
08.14.14 15.01
1
08.14.14 15.01
1
1
08.14.14 16.56
D
10
08.14.14 15.01
1
08.14.14 15.01
1
Page 6 of 29
Final 1.000

• Hits Summary 491299 (((
Florida Testing Services, LLC
- -
Terraquest Environmental Consultants, P.C., Mebane,
NC
Colliseum Shell
Sample Id: After AST
Matrix : Ground Water
% Moisture:
Lab Sample Id: 491299-002
Date Collected: 08.11.14 11.45
Date Received: 08.12.14 14.20
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method:
SM6200B_PREP
Seq Number 948247
Date Prep:
08.14.14 06.34
Parameter
Cas Number Result Units
Analysis Date
Flag
Dil
1,2,4-Trimethylbenzene
95-63-6 0.220 ug/L
08.14.1415.29
1
1
Acetone
67-64-1 24.1 ug/L
08.14.1415.29
1
Methyl tert-butyl ether (MTBE).
1634-04-4 1.67 ug/L
08.14.14 15.29
1
Naphthalene
91-20-3 1.39 ug/L
08.14.1415.29
J
1
Toluene
108-88-3 0.340 ug/L
08.14.1415.29
7
1
m,p-Xylenes
179601-23-1 0.270 ug/L
08.14.1415.29
1
1
o-Xylene
95-47-6 0.150 ug/L
08.14.1415.29
J
1
Page 7 of 29 Final 1.000

�W"F%%
2 "�i%y EO
• Hits Summary 491299:
e�eu
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st Carbon Matrix : Ground Water % Moisture:
Lab Sample Id : 491299-003 Date Collected: 08.11.14 11.47
Date Received: 08.12.14 14.20
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
Seq Number 948247 Date Prep: 08.14.14 06.34.
Parameter Cas Number Result Units Analysis Date Flag Dil
Chloroform 67-66-3 1.73 ug/L 08.14.1415.57 1
Methyl tert-butyl ether (MTBE) 1634-04-4 2.91 ug/L 08.14.14 15.57 1
Page 8 of 29 Final 1.000

Certificate of Analytical Results 491299 t
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Influent Matrix: Ground.Water Date Received: 08.12.14 14.20
Lab Sample Id: 491299-001 Date Collected: 08.11.14 11.50
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Parameter Cas Number
Date Prep:
Result
- 08.14.14 06.34
RL NWL
Units
Prep Method: SM620OB_PREP
% Moisture:
Analysis Date . Flag DR
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
08.14.1415.01
U
1 .
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
08.14.1415.01
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
08.14.1415.01
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
08.14.1415.01
U
1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
08.14.1415.01
U
1
1,I'Dichloroethene
75-35-4
U
0.500
0.104
ug/L
08.14.1415.01
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
08.14.14 15.01
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
08.14.1415.01
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
08.14.14 15.01
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
08.14.1415.01
U
1
1,2,4-Trimethylbenzene
95-63-6
59.7
0.500
0.103
ug/L
08.14.1415.01
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
08.14.14 15.01
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
08.14.1415.01
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
08.14.1415.01
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
08.14.1415.01
U
1
1,3,5-Trimethylbenzene
108-67-8
15.5
0.500
0.0870
ug/L
08.14.1415.01
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
08.14.1415.01
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
08.14.14 15.01
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
08.14.1415.01
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
08.14.1415.01
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
08.14.14 15.01
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
08.14.14 15.01
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
08.14.1415.01
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
08.14.1415.01
U
1
4-Isopropyltoluene
99-87-6
0.200
0.500
0.0890
ug/L
08.14.1415.01
J
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
08.14.14 15.01
U
1
Acetone
67-64-1
100
2.00
0.352
ug/L
08.14.1415.01
1
Benzene
71-43-2
36.5
0.500
0.119
ug/L
08.14.1415.01
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
08.14.1415.01
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
08.14.1415.01
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
08.14.1415.01
U
I
Bromoform
75-25-2
U
2.00
0.159
ug/L
08.14.1415.01
U
1
Broniomethane
74-83-9
U
1.00
0.0970
ug/L
08.14.1415.01
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
08.14.1415.01
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
08.14.1415.01
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
08.14.1415.01
U
I
Chloioethane
75-00-3
U.
0.500
0.0420
ug/L
08.14.1415:01
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
08.14.1415.01
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
08.14.1415.01
U
1
Page 9 of 29 Final 1.000

PCCHp°�
Certificate of Analytical Results 491299 ��
PJIA
� �@� oao.W nii.wa,
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Influent Matrix: Ground Water Date Received:08.12.14 14.20
Lab Sample Id: 491299-001 Date Collected: 08.11.14 11.50
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Parameter Cas Number
Date Prep:
Result
08.14.14 06.34
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
08.14.1415.01
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
08.14.14 15.01.
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
08.14.1415.01
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
08.14.1415.01
U
1
Ethylbenzene
100-41-4
28.5
0.500
0.0920
ug/L
08.14.1415.01
1
Isopropyl ether
108-20-3
37.6
0.500
0.0920
ug/L
08.14.14 15.01
1
Isopropylbenzene
98-82-8
1.10
0.500
0.0980
ug/L
08.14.1415.01
1
Methyl tert-butyl ether (MTBE)
1634-04-4
1740
5.00
1.69
ug/L
08.14.14 16.56
D
10
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
08.14.14 15.01
U
1
Naphthalene
91-20-3
63.5
2.00
0.0940
ug/L
08.14.1415.01
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
08.14.14 15.01
U
1
n-Propylbenzene
103-65-1
4.49
1.00
0.0650
ug/L
08.14.1415.01
1
sec-Butylbenzene
135-98-8
0.230
0.500
0.0920
ug/L
08.14.14 15.01
1
1
Styrene
100-42-5
U
0.500
0.0740
ug/L,
08.14.1415.01
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
08.14.1415.01
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
08.14.14 15.01
U
1
Toluene
108-88-3
122
5.00
0.570
ug/L
08.14.1416.56
D
10
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
08.14.14 15.01
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
08.14.14 15.01
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
08.14.1415.01
U
I
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
08.14.14 15.01
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
08.14.14 15.01
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
08.14.14 15.01
U
1
m,p-Xylenes
179601-23-1
115
1.00
0.176
ug/L
08.14.1415.01
1
o-Xylene
95-47-6
77.4
0.500
0.122
ug/L
08.14.1415.01
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
94
%
65-134
08.14.14 15.01
4-Bromofluorobenzene
460-00-4
102
%
60-148
08.14.1415.01
Toluene-D8
2037-26-5
90
%
87-114
08.14.1415.01
Page 10 of 29 Final 1.000

P�_CRFD roro �^
' PJIA
Certificate of Analytical Results 491299
Terraquest Environmental Consultants, P.C.; Mebane, NC
Colliseum Shell
Sample Id: After AST
Lab Sample Id: 491299-002
Analytical Method: VOCs by GUMS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Matrix: Ground Water Date Received:08.12.14 14.20
Date Collected: 08.11.14 11.45
Date Prep: 08.14.14 06.34
Prep Method: SM6200B PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
08.14.1415.29
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
08.14.14 15.29
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
08.14.1415.29
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
08.14.1415.29
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
08.14.1415.29
U
1
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
08.14.14 15.29
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
08.14.14 15.29
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
08.14.1415.29
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
08.14.14 15.29
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
08.14.1415.29
U
1
1,2,4-Trimethylbenzene
95-63-6
0.220
0.500
0.103
ug/L
08.14.1415.29
1
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
08.14.14 15.29
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
08.14.14 15.29
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L.
08.14.1415.29
U
.1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
08.14.1415.29
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
08.14.1415.29
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
08.14.1415.29
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
08.14.1415.29
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
08.14.1415.29
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
08.14.14 15.29
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
08.14.14 15.29
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
08.14.14 15.29
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
08.14.1415.29
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
08.14.14 15.29
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
08.14.1415.29
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
08.14.14 15.29
U
1
Acetone
67-64-1
24.1
2.00
0.352
ug/L
08.14.1415.29
1
Benzene
71-43-2
U
0.500
0.119
ug/L
08.14.1415.29
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
08.14.1415.29
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
08.14.1415.29
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
08.14.1415.29
U
1
Bromofonn
75-25-2
U
2.00
0.159
ug/L
08.14.1415.29
U
1 -
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
08.14.1415.29
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
08.14.14 15.29
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L.
08.14.1415.29
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
08.14.1415.29
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
08.14.1415.29
U
1
Chloroform
.67-66-3
U
0.500
0.172
ug/L
08.14.14 15.29
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L.
08.14.1415.29
U
1
Page 11 of 29 Final 1.000

r p�\
Certificate of Analytical Results 491299 ,ut �►
PJIA
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After AST Matrix: Ground Water Date Received:08.12.14 14.20
Lab Sample Id: 491299-002 Date Collected: 08.11.14 11.45
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
Tech: LIH % Moisture:
Analyst: MLA Date Prep: 08.14.14 06.34
Seq Number: 948247
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
08.14.1415.29
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
08.14.1415.29
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
08.14.1415.29
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
08.14.1415.29
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
08.14.1415.29
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
08.14.14 15.29
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
08.14.14 15.29
U
1
Methyl tert-butyl ether (NITBE)
1634-04-4
1.67
0.500
0.169
ug/L
08.14.14 15.29
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
08.14.14 15.29
U
1
Naphthalene
91-20-3
1.39
2.00
0.0940
ug/L
08.14.1415.29
1
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L,
08.14.1415.29
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
08.14.14 15.29
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
08.14.14 15.29
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
08.14.14 15.29
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
08.14.14 15.29
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
08.14.14 15.29
U
1
Toluene
108-88-3
0.340
0.500
0.0570
ug/L
08.14.1415.29
J
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
08.14.1415.29
U
1
trans-1,3-Dichloropropene
10061-02-6
U -
1.00
0.110
ug/L
08.14.14 15.29
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
08.14.14 15.29
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
08.14.1415.29
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
08.14.14 15.29
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
08.14.14 15.29
U
1
m,p-Xylenes
179601-23-1
0.270
1.00
0.176
ug/L
08.14.1415.29
J
1
o-Xylene
95-47-6
0.150
0.500
0.122
ug/L
08.14.14 15.29
J
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
94
%
65-134
08.14.14 15.29
4-Bromofluorobenzene
460-00-4
94
%
60-148
08.14.1415.29
Toluene-138
2037-26-5
138
%
87-114
08.14.1415.29
**
Page 12 of 29 Final 1.000

• Certificate of Analytical Results 4912994e
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st Carbon Matrix: Ground Water Date Received: 08.12.14.14.20
Lab Sample Id: 491299-003 Date Collected: 08.11.14 11.47
Analytical Method: VOCs by GUMS by SM6200B Prep Method: SM6200B PREP
Tech: LIH % Moisture:
Analyst: MLA - Date Prep: 08.14.14 06.54
Seq Number: 948247
Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
08.14.14 15.57
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
08.14.1415.57
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700.
ug/L
08.14.1415.57
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
08.14.1415.57
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
08.14.1415.57
U
1
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
08.14.1415.57
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
08.14.1415.57
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
08.14.1415.57
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L,
08.14.1415.57
U
1
1,2,4-Trichlorobenzene
120-82-1
U.
1.00
0.0690
ug/L
08.14.1415.57
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
08.14.1415.57
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
08.14.14 15.57
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
08.14.1415.57
U
1
1,2-Dichloroethane
107-06-2
U:
0.500
0.0900
ug/L
08.14.1415.57
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
08.14.14 15.57
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
08.14.1415.57
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
08.14.1415.57
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
08.14.1415.57
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
08.14.1415.57
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
08.14.14 15.57
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
08.14.14 15.57
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
08.14.1415.57
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
08.14.1415.57
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
08.14.1415.57
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
08.14.1415.57
U
1
4-Methyl-2-pentanone (MIBK)
168-10-1
U
0.400
0.253
ug/L
09.14.14 15.57
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L,
08.14.1415.57
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
08.14.1415.57
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
08.14.14 15.57
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L,
08.14.1415.57
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
08.14.1415.57
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
08.14.1415.57
U
1
Bromomethane
74-83-9
U.
1.00
0.0970
ug/L
08.14.1415.57
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
08.14.14 15.57
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
08.14.1415.57
U
1
Chlorodibromomethanc
124-48-1
U
0.500
0.177
ug/L
08.14.1415.57
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
08.14.1415.57
U
.1
Chloroform
67-66-3
1.73
0.500
0.172
ug/L,
08.14.1415.57
.1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
08.14.1415.57
U
1
Page 13 of 29 Final 1.000

T F°
'F .'
Certificate of Analytical Results 4912994e9
wu
Flodda Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st Carbon Matrix: Ground Water Date Received:08.12.14 14.20
Lab Sample Id: 491299-003 Date Collected: 08.11.14 11.47
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Parameter
Cas Numbei
cis-1,2-Dichloroethene
156-59-2
cis-1,3-Dichloropropene
10061-01-5
Dichlorodifluoromethane
75-71-8
Ethanol
64-17-5
Ethylbenzene
100-41-4
Isopropyl ether
108-20-3
Isopropylbenzene
98-82-8
Methyl tert-butyl ether (MTBE)
1634-04-4
Methylene Chloride
75-09-2
Naphthalene
91-20-3
n-Butylbenzene
104-51-8
n-Propylbenzene
103-65-1
sec-Butylbenzene
135-98-8
Styrene
100-42-5
tert-Butylbenzene
98-06-6
Tetrachloroethene (PCE)
127-18-4
Toluene
108-88-3
trans-1,2-Dichloroethene
156-60-5
trans-1,3-Dichloropropene
10061-02-6
Trichloroethene
79-01-6
Trichlorofluoromethane
75-69-4
Vinyl Acetate
108-05-4
Vinyl Chloride
75-01-4
m,p-Xylenes
179601-23-1
o-Xylene
95-47-6
Surrogate
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Prep Method: SM6200B_PREP
% Moisture:
Date Prep: 08.14.14 06.34
Result
RL
MDL
Units
Analysis Date
Flag
Dil
U
0.500
0.114
ug/L
08.14.1415.57
U
1
U
1.00
0.100
ug/L
08.14.1415.57
U
1
U
1.00
0.0670
ug/L
08.14.1415.57
U
1
U
50.0
3.00
ug/L
08.14.1415.57
U
1
U
0.500
0.0920
ug/L
08.14.1415.57
U
1
U
0.500
0.0920
ug/L
08.14.1415.57
U
1
U
0.500
0.0980
ug/L
08.14.1415.57
U
1
2.91
0.500
0.169
ug/L
08.14.1415.57
1
U
0.500
0.190
ug/L,
08.14.1415.57
U
1
U
2.00
0.0940
ug/L
08.14.1415.57
U
1
U
2.00
0.0600
ug/L
08.14.1415.57
U
1
U
1.00
0.0650
ug/L
08.14.1415.57
U
1
U
0.500
0.0920
ug/L
08.14.1415.57
U
1
U
0.500
0.0740
ug/L,
08.14.1415.57
U
1
U
0.500
0.0890
ug/L,
08.14.1415.57
U
1
U
0.500
0.0540
ug/L
08.14.1415.57
U
I
U
0.500
0.0570
ug/L
08.14.1415.57
U
1
U
0.500
0.188
ug/L
08.14.1415.57
U
1
U
1.00
0.110
ug/L.
08.14.1415.57
U
1
U
0.500
0.139
ug/L
08.14.1415.57
U
1
U
0.500
0.0540
ug/L
08.14.1415.57
U
1
U
1.00
0.720
ug/L
08.14.1415.57
U
1
U
0.500
0.0810
ug/L
08.14.1415.57
U
1
U
1.00
0.176
ug/L
08.14.1415.57
U
1
U
0.500
0.122
ug/L
08.14.14 15.57
U
1
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
17060-07-0
88
%
65-134
08.14.1415.57
460-00-4
104
%
60-148
08.14.1415.57
2037-26-5
94
%
87-114
08.14.1415.57
Page 14 of 29 Final 1.000

Certificate of Analytical Results 491299
13
r�u
e48919- .�.....>.
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received: 08.12.14 14.20
Lab Sample Id: 491299-004 Date Collected: 08.11.14 11.35
Analytical Method: TSS by SM2540D
Tech: NSI
Analyst: NSI
Seq Number: 948130
Parameter
Total Suspended Solids
% Moisture:
Cas Number Result RL MDL Units Analysis Date Flag
U 4.00 3.50 mg/L 08.12.1415.00 U
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR % Moisture:
Analyst: ABA Date Prep: 08.14.14 10.14
Seq Number: 948303
Parameter Cas Number Result RL MDL _ Units Analysis Date Flag
Lead 7439-92-1 U 0.0100 0.00330 mg/L 08.15.14 13.44 U
Dil
1
Page 15 of 29 Final 1.000

C�
Certificate of Analytical Results 491299
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent
Lab Sample Id: 491299-004
Analytical Method: VOCs by GUMS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Parameter Cas Number
Matrix: Ground Water
Date Collected: 08.11.14 11.35
Date Prep: 08.14.14 06.34
Result RL MDL
Units
Date Received:08.12.14 14.20
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
08.14.14 16.26
U
1
I,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
08.14.14 16.26
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
08.14.14 16.26
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
08.14.14 16.26
U
I
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
08.14.1416.26
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
08.14.14 16.26
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
08.14.1416.26
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
08.14.14 16.26
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
08.14.14 16.26
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
08.14.14 16.26
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
08.14.1416.26
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
08.14.14 16.26
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
08.14.14 16.26
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
08.14.14 16.26
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
08.14.14 16.26
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L.
08.14.1416.26
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
08.14.1416.26
U
I
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
08.14.1416.26
U
I
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
08.14.1416.26
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
08.14.1416.26
U
I
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
08.14.14 16.26
U
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
08.14.14 16.26
U
I
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
08.14.1416.26
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
08.14.14 16.26
U
I
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
08.14.14 16.26
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
08.14.14 16.26
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
08.14.1416.26
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
08.14.1416.26
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
08.14.1416.26
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
08.14.14 16.26
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
08.14.1416.26
U
1
Bromofonn
75-25-2
U
2.00
0.159
ug/L
08.14.1416.26
U
I
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
08.14.1416.26
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
08.14.14 16.26
U
I
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
08.14.1416.26
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
08.14.1416.26
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
08,14.1416.26
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
08.14.14 16.26
U
I
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
08.14.14 16.26
U
1
Page 16 of 29 Final 1.000

Certificate of Analytical Results 491299
PJV1
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent
Lab Sample Id: 491299-004
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 948247
Matrix: Ground Water Date Received:08.12.14 14.20
Date Collected: 08.11.14 11.35
Date Prep: 08.14.14 06.34
Prep Method: SM6200B_PREP
% Moisture:
Parameter
Cas Number
Result
RL
NJDL
Units
Analysis Date
Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
08.14.1416.26
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
08.14.14 16.26
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
08.14.1416.26
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
08.14.14 16.26
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
08.14.14 16.26
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
08.14.14 16.26
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
08.14.14 16.26
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
08.14.14 16.26
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
08.14.14 16.26
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
08.14.14 16.26
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
08.14.1416.26
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
08.14.14 16.26
U
I
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
08.14.1416.26
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
08.14.1416.26
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
08.14.1416.26
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
08.14.14 16.26
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
08.14.1416.26
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
08.14.14 16.26
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
08.14.14 16.26
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
08.14.1416.26
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
08.14.1416.26
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
08.14.14 16.26
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
08.14.14 16.26
U
I
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
08.14.1416.26
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
08.14.1416.26
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
96
%
65-134
08.14.1416.26
4-Bromofluorobenzene
460-00-4
97
%
60-148
08.14.14 16.26
Toluene-D8
2037-26-5
139
%
87-114
08.14.1416.26
**
Page 17 of 29 Final 1.000

QC Summary 491299
Terraquest Environmental Consultants, P.C.
Colliseum Shell
Analytical Method: TSS by SM2540D
Seq Number: 948130
Matrix:
Water
MB Sample Id: 948130-1-BLK
LCS Sample Id:
948130-1-BKS
LCSD Sample Id: 948130-1-BSD
MB Spike
Parameter
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Result Amount
Result %Rec
Result %Rec
Limit Date
Total Suspended Solids <3.50 100
89.0 89
94.0 94
80-120 5 10 mg/L 08.12.14 15:00
Analytical Method: TSS by SM2540D
Seq Number: 948130
Parent Sample Id: 491299-004
Parameter Parent
Result
Total Suspended Solids <3.50
Matrix: Ground Water
MD Sample Id: 491299-004 D
MD
Result
<3.50
%RPD RPD Units Analysis Flag
Limit Date
0 10 mg/L 08.12.1415:00 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
948303
Matrix:
Water
Date Prep: 08.14.14
MB Sample Id:
659992-1-BLK
LCS Sample Id:
659992-1-BKS
LCSD Sample Id: 659992-1-BSD
Parameter
MB Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
0.951 95
0.949 95
80-120 0 20 mg/L 08.15.1413:40
Analytical Method: Lead by SW-846 6010C
Seq Number: 948303 Matrix: Ground Water
Parent Sample Id: 491299-004 MD Sample Id: 491299-004 D
Parent MD
Parameter
Result Result
Lead <0.00330 <0.00330
Prep Method: SW3010A
Date Prep: 08.14.14
%RPD RPD Units Analysis Flag
Limit Date
0 20 mg/L 08.15.1413:46 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
948303
Matrix:
Ground Water
Date Prep: 08.14.14
Parent Sample Id:
491299-004
MS Sample Id:
491299-004 S
MSD Sample Id: 491299-004 SD
Parent Spike
MS MS
MSD MSD
Limits %RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
0.958 96
0.950 95
80-120 1 20 mg/L 08.15.1413:48
Page 18 of 29 Final 1.000

e
RELIggam
Florida Testing Services, LLC
Analytical Method:
Seq Number:
MB Sample Id:
Parameter
QC Summary 491299
Terraquest Environmental Consultants, P.C.
Colliseum Shell
VOCs by GC/MS by SM6200B
948247 Matrix: Water
660051-1-BLK LCS Sample Id: 660051-1-BKS
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Isopropyholuene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorodifluoromethane
Ethanol
Ethylbenzene
Isopropyl ether
Isopropylbenzene
Methyl tert-butyl ether (MTBE)
Methylene Chloride
Naphthalene
n-Butylbenzene
n-Propylbenzene
sec-Butylbenzene
MB
Spike
LCS
LCS
LCSD
LCSD
Result
Amount
Result
%Rec
Result
%Rec
<0.180
25.0
25.7
103
26.2
105
<0.0760
25.0
23.8
95
24.7
99
<0.0700
25.0
27.8
111
26.3
105
<0.113
25.0
24.6
98
29.8
119
<0.121
25.0
26.0
104
21.6
86
<0.104
25.0
26.0
104
21.0
84
<0.0600
25.0
25.3
101
27.2
109
<0.118
25.0
22.3
89
23.9
96
<0.138
25.0
28.6
114
26.4
106
<0.0690
25.0
22.3
89
23.4
94
<0.103
25.0
26.3
105
24.9
100
<0.180
25.0
25.2
101
28.0
112
<0.0940
25.0
25.3
101
25.8
103
<0.0900
25.0
23.3
93
25.5
102
<0.122
25.0
25.9
104
29.2
117
<0.0870
25.0
26.9
108
25.4
102
<0.0980
25.0
26.5
106
26.3
105
<0.133
25.0
24.8
99
29.2
117
<0.0670
25.0
25.6
102
25.7
103
<0.0970
25.0
26.4
106
22.7
91
<0.378
50.0
50.9
102
56.2
112
<0.0880
25.0
27.6
110
25.4
102
<0.352
50.0
47.9
96
62.3
125
<0.0900
25.0
27.9
112
25.8
103
<0.0890
25.0
27.1
108
26.7
107
<0.253
50.0
48.7
97
60.4
121
<0.352
50.0
43.5
87
41.9
84
<0.119
25.0
25.2
101
27.3
109
<0.132
25.0
28.3
113
25.9
104
<0.112
25.0
26.5
106
27.0
108
<0.124
25.0
25.3
101
26.5
106
<0.159
25.0
25.3
101
32.9
132
<0.0970
25.0
24.8
99
21.5
86
<0.0990
25.0
24.1
96
24.9
100
<0.105
25.0
26.0
104
26.2
105
<0.177
25.0
24.4
98
26.9
108
<0.0420
25.0
26.4
106
24.1
96
<0.172
25.0
24.1
96
27.0
108
<0.0850
25.0
25.5
102
24.5
98
<0.114
25.0
27.9
112
24.3
97
<0.100
25.0
27.5
110
29.1
116
<0.0670
25.0
23.7
95
21.3
85
<3.00
1000
976
98
757
76
<0.0920
25.0
26.0
104
27.3
109
<0.0920
25.0
26.0
104
22.8
91
<0.0980
25.0
26.5
106
33.0
132
<0.169
50.0
48.9
98
40.7
81
<0.190
25.0
28.1
112
20.2
81
<0.0940
25.0
21.4
86
22.7
91
<0.0600
25.0
29.7
119
27.6
110
<0.0650
25.0
28.5
114
26.3
105
<0.0920
25.0
27.3
109
25.5
102
(k
0ii
4eea.,. � � ....
Prep Method:
SM620OB_PREP
Date Prep:
08.14.14
LCSD Sample Id: 660051-1-BSD
Limits
%RPD
RPD
Units
Analysis
Limit
Date
75-127
2
20
ug/L
08.14.14 07:26
62-128
4
20
ug/L
08.14.14 07:26
77-129
6
20
ug/L
08.14.14 07:26
86-120
19
20
ug/L
08.14.14 07:26
82-114
18
20
ug/L
08.14.14 07:26
73-123
21
22
ug/L
08.14.14 07:26
83-125
7
20
ug/L
08.14.14 07:26
57-127
7
20
ug/L
08.14.14 07:26
79-118
8
20
ug/L
08.14.14 07:26
59-125
5
20
ug/L
08.14.14 07:26
84-118
5
20
ug/L
08.14.14 07:26
83-126
11
20
ug/L
08.14.14 07:26
89-126
2
20
ug/L.
08.14.14 07:26
56-133
9
20
ug/L
08.14.14 07:26
79-127
12
20
ug/L
08.14.14 07:26
86-118
6
20
ug/L
08.14.14 07:26
90-126
1
20
ug/L
08.14.14 07:26
85-121
16
20
ug/L
08.14.14 07:26
88-121
0
20
ug/L
08.14.14 07:26
76-126
15
20
ug/L
08.14.14 07:26
66-133
10
20
ug/L
08.14.14 07:26
80-128
8
20
ug/L
08.14.14 07:26
70-130
26
20
ug/L
08.14.14 07:26
82-130
8
20
ug/L
08.14.14 07:26
80-128
1
20
ug/L
08.14.14 07:26
74-129
21
20
ug/L
08.14.14 07:26
51-143
4
21
ug/L
08,14.14 07:26
81-123
8
20
ug/L
08.14.14 07:26
84-114
9
20
ug/L
08.14.14 07:26
89-127
2
20
ug/L
09.14.14 07:26
70-129
5
20
ug/L
08.14.14 07:26
73-140
26
20
ug/L
08.14.14 07:26
53-143
14
20
ug/L
08.14.14 07:26
66-136
3
20
ug/L
08.14.14 07:26
88-118
1
20
ug/L
08.14.14 07:26
73-139
10
20
ug/L
08.14.14 07:26
70-123
9
20
ug/L
08.14.14 07:26
72-118
11
20
ug/L
08.14.14 07:26
65-125
4
20
ug/L
08.14.14 07:26
85-125
14
20
ug/L
08.14.14 07:26
92-126
6
20
ug/L
08.14.14 07:26
48-143
11
20
ug/L
08.14.14 07:26
61-133
25
20
ug/L
08.14.14 07:26
87-123
5
20
ug/L
08.14.14 07:26
77-125
13
20
ug/L
08.14.14 07:26
82-115
22
20
ug/L
08.14.14 07:26
53-149
18
20
ug/L
08.14.14 07:26
75-119
33
20
ug/L
08.14.14 07:26
52-116
6
20
ug/L
08.14.14 07:26
83-130
7
20
ug/L
08.14.14 07:26
84-122
8
20
ug/L
08.14.14 07:26
86-120
7
20
ug/L :
09.14.14 07:26
Flag
F
F
F
F
HF
F
Page 19 of 29 Final 1.000

•
t t
Florida Testing Services, LLC
QC Summary 491299
Terraquest Environmental Consultants, P.C.
Colliseum Shell
P�fRfp A_
`401.I'll
Analytical Method:
VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Seq Number:
948247
Matrix:
Water
Date Prep: 08.14.14
MB Sample Id:
660051-1-BLK
LCS Sample
Id:
660051-1-BKS
LCSD Sample Id: 660051-1-BSD
Parameter
MB
Spike
LCS
LCS
LCSD
LCSD
Limits %RPD RPD
Units
Analysis
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
27.7
111
27.5
110
85-123
1
20
ug/L
08.14.14 07:26
tert-Butylbenzene
<0.0890
25.0
26.3
105
25.4
102
79-126
3
20
ug/L
08.14.14 07:26
Tetrachloroethene (PCE)
<0.0540
25.0
23.8
95
25.0
100
64-131
5
20
ug/L
08.14.14 07:26
Toluene
<0.0570
25.0
24.7
99
28.1
112
89-116
13
20
ug/L
08.14.14 07:26
trans-1,2-Dichloroethene
<0.188
25.0
26.5
106
21.5
86
78-118
21
20
ug/L
08.14.14 07:26
trans-1,3-Dichloropropene
<0.110
25.0
25.6
102
30.1
120
86-127
16
20
ug/L
08.14.14 07:26
Trichloroethene
<0.139
25.0
25.8
103
26.7
107
82-119
3
20
ug/L
08.14.14 07:26
Trichlorofluorometbane
<0.0540
25.0
26.7
107
25.3
101
46-144
5
20
ug/L
08.14.14 07:26
Vinyl Acetate
<0.720
25.0
26.5
106
24.4
98
58-141
8
20
ug/L
08.14.14 07:26
Vinyl Chloride
<0.0810
25.0
25.7
103
24.9
100
76-122
3
20
ug/L
08.14.14 07:26
m,p-Xylenes
<0.176
50.0
51.7
103
52.7
105
90-125
2
20
ug/L
08.14.14 07:26
o-Xylene
<0.122
25.0
27.0
108
26.8
107
86-119
1
20
ug/L
08.14.14 07:26
Surrogate
MB
MB
LCS
LCS
LCSD
LCSD
Limits
Units
Analysis
%Rec
Flag
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
92
89
95
65-134
%
08.14.14 07:26
4-Bromofluorobenzene
104
104
108
70-130
%
08.14.14 07:26
Toluene-138
112
95
107
87-114
%
08.14.14 07:26
Flag
F
Page 20 of 29 Final 1.000

QC Summary 491299�
i"
NI r��u
Florida Testing Services, LICE
Terraquest Elivironmental Consultants, P.C.
Colliseum Shell
Analytical Method: VOCs by GUMS by SM620013
Prep Method:
SM6200B_PREP
Seq Number: 948247
Matrix:
Ground Water
Date Prep:
08.14.14
Parent Sample Id: 491155-006
MS Sample Id:
491155-006 S
MSD Sample Id: 491155-006
SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD
RPD
Units
Analysis
Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
1, 1, 1,2-Tetrachloroethane
<0.180
25.0
25.2
101
24.8
99
76-126
2
20
ug/L
08.14.14 17:29
1, 1, 1 -Trichloroethane
<0.0760
25.0
23.9
96
22.7
91
63-128
5
20
ug/L
06.14.14 17:29
1,1,2,2-Tetrachloroethane
<0.0700
25.0
29.4
118
25.9
104
79-133
13
20
ug/L
08.14.14 17:29
1,1,2-Trichloroethane
<0.113
25.0
29.0
116'
28.7
115
82-126
1
20
ug/L
08.14.14 17:29
1,1-Dichloroethane
<0.121
25.0
21.1
84
21.4
86
77-120
1
20
ug/L
08.14.14 17:29
1,1-Dichloroethene
<0.104
25.0
20.8
83
23.2
93
67-123
11
22
ug/L
08.14.14 17:29
1,1-Dichloropropene
<0.0600
25.0
26.5
106
26.1
104
76-126
2
20
ug/L
08.14.14 17:29
1,2,3-Trichlorobenzene
<0.118
25.0
24.0
96
24.6
98
41-136
2
20
ug/L
08.14.14 17:29
1,2,3-Trichloropropane
<0.138
25.0
28.9
116
25.5
102
77-125
13
20
ug/L
08.14.14 17:29
1,2,4-Trichlorobenzene
<0.0690
25.0
22.8
91
23.2
93
41-132
2
20
ug/L
08.14.14 17:29
1,2,4-Trimethylbenzene
<0.103
25.0
24.2
97
23.5
94
53-141
3
20
ug/L
08.14.14 17:29
1,2-Dibromoethane (EDB)
<0.180
25.0
27.6
110
26.7
107
82-130
3
20
ug/L
08.14.14 17:29
1,2-Dichlorobenzene
<0.0940
25.0
25.8
103
25.1
100
83-128
3
20
ug/L
08.14.14 17:29
1,2-Dichloroethane
<0.0900
25.0
24.4
98
24.5
98
59-134
0
20
ug/L
08.14.14 17:29
1,2-Dichloropropane
<0.122
25.0
29.0
116
28.1
112
79-125
3
20
ug/L
08.14.14 17:29
1,3,5-Trimethylbenzene
<0.0870
25.0
26.1
104
23.9
96
69-125
9
20
ug/L
08.14.14 17:29
1,3-Dichlorobenzene
<0.0980
25.0
25.9
104
25.0
100
83-126
4
20
ug/L
08.14.14 17:29
1,3-Dichloropropane
<0.133
25.0
28.3
113
28.0
112
85-124
1
20
ug/L
08.14.14 17:29
1,4-Dichlorobenzene
<0.0670
25.0
25.1
100
24.1
96
82-121
4
20
ug/L
08.14.14 17:29
2,2-Dichloropropane
<0.0970
25.0
23.7
95
23.8
95
56-122
0
20
ug/L
08.14.14 17:29
2-Butanone (MEK)
<0.378
50.0
60.7
121
57.5
115
66-136
5
20
ug/L
08.14.14 17:29
2-Chlorotoluene
<0.0880
25.0
26.8
107
23.9
96
73-129
11
20
ug/L
08.14.14 17:29
2-Hexanone
<0.352
50.0
65.0
130
64.9
130
63-140
0
20
ug/L
08.14.14 17:29
4-Chlorotoluene
<0.0900
25.0
27.4
110
24.5
98
76-129
11
20
ug/L
08.14.14 17:29
4-Isopropyholuene
<0.0890
25.0
26.9
108
25.0
100
73-126
7
20
ug/L
08.14.14 17:29
4-Methyl-2-pentanone (MIBK)
<0.253
50.0
61.5
123
61.9
124
71-140
1
20
ug/L
08.14.14 17:29
Acetone
<0.352
50.0
39.0
78
31.1
62
47-138
23
21
ug/L
08.14.14 17:29
F
Benzene
<0.119
25.0
26.7
107
26.2
105
70-135
2
20
ug/L
08.14.14 17:29
Bromobenzene
<0.132
25.0
28.0
112
24.4
98
76-120
14
20
ug/L
08.14.14 17:29
Bromochloromethane
<0.112
25.0
26.2
105
25.5
102
83-132
3
20
ug/L
08.14.14 17:29
Bromodichloromethane
<0.124
25.0
25.4
102
25.4
102
66-132
0
20
ug/L
08.14.14 17:29
Bromoform
<0.159
25.0
26.4
106
25.4
102
63-143
4
20
ug/L
08.14.14 17:29
Bromomethane
<0.0970
25.0
22.5
90
15.4
62
60-134
37
20
ug/L
08.14.14 17:29
F
Carbon tetrachloride
<0.0990
25.0
23.9
96
23.7
95
59-139
1
20
ug/L
08.14.14 17:29
Chlorobenzene
<0.105
25.0
25.5
102
24.7
99
83-120
3
20
ug/L
08.14.14 17:29
Chlorodibromomethane
<0.177
25.0
25.8
103
25.4
102
68-140
2
20
ug/L
08.14.14 17:29
Chloroethane
<0.0420
25.0
25.4
102
19.6
78
67-125
26
20
ug/L
08.14.14 17:29
F
Chloroform
<0.172
25.0
26.2
105
24.6
98
72-120
6
20
ug/L
08.14.14 17:29
Chloromethane
<0.0850
25.0
27.7
ill
26.4
106
59-128
5
20
ug/L
08.14.14 17:29
cis-1,2-Dichloroethene
<0.114
25.0
28.3
113
27.8
Ill
80-125
2
20
ug/L
08.14.14 17:29
cis-1,3-Dichloropropene
<0.100
25.0
27.5
110
27.4
110
74-122
0
20
ug/L
08.14.14 17:29
Dichlorodifluoromethane
.<0.0670
25.0
22.1
88
21.4
86
48-138
3
20
ug/L
08.14.14 17:29
Ethanol
<3.00
1000
820
82
857
86
55-140
4
20
ug/L
08.14.14 17:29
Ethylbenzene
<0.0920
25.0
26.2
105
25.5
102
70-140
3
20
ug/L
08.14.14 17:29
Isopropyl ether
<0.0920
25.0
22.1
88
23.1
92
70-132
4
20
ug/L
08.14.14 17:29
Isopropylbenzene
<0.0980
25.0
26.2
105
24.0
96
75-117
9
20
ug/L
08.14.14 17:29
Methyl tert-butyl ether (MTBE)
<0.169
50.0
40.4
81
40.2
80
51-155
0
20
ug/L
08.14.14 17:29
Methylene Chloride
0.350
25.0
19.6
77
19.7
77
71-126
1
20
ug/L
08.14.14 17:29
Naphthalene
<0.0940
25.0
22.6
90
22.4
90
34-135
1
20
ug/L
08.14.14 17:29
n-Butylbenzene
<0.0600
25.0
28.6
114
25.6
102
73-128
11
20
ug/L
08.14.14 17:29
n-Propylbenzene
<0.0650
25.0
27.7
ill
24.8
99
75-125
11
20
ug/L
08.14.14 17:29
sec-Butylbenzene
<0.0920
25.0
23.9
96
24.0
96
77-122
0
20
ug/L
08.14.1417:29
Page 21
of 29
Final
1.000

QC Summary 491299
Terraquest Environmental Consultants, P.C.
Colliseum Shell
PURf�p(
kit
` �B
Analytical Method:
VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Seq Number:
948247
Matrix:
Ground Water
Date Prep: 08.14.14
Parent Sample Id:
491155-006
MS Sample Id:
491155-006 S
MSD Sample Id: 491155-006
SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD RPD
Units
Analysis
Parameter
Result
Amount
Result %Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
26.7
107
20.1
80
54-137
28
20
ug/L
08.14.14 17:29
tert-Butylbenzene
<0.0890
25.0
26.0
104
23.8
95
74-124
9
20
ug/L
08.14.14 17:29
Tetrachloroethene (PCE)
<0.0540
25.0
23.6
94
22.7
91
57-130
4
20
ug/L
08.14.14 17:29
Toluene
<0.0570
25.0
27.4
110
26.3
105
81-125
4
20
ug/L
08.14.14 17:29
trans-1,2-Dichloroethene
<0.188
25.0
21.1
84
21.1
84
69-122
0
20
ug/L
08.14.14 17:29
trans-1,3-Dichloropropene
<0.110
25.0
28.6
114
27.9
112
73-129
2
20
ug/L
08.14.14 17:29
Trichloroethene
<0.139
25.0
26.0
104
25.5
102
73-124
2
20
ug/L
08.14.14 17:29
Trichlorofluoromethane
<0.0540
25.0
20.4
82
23.1
92
49-139
12
20
ug/L
08.14.14 17:29
Vinyl Acetate
<0.720
25.0
22.0
88
22.4
90
57-134
2
20
ug/L
08.14.14 17:29
Vinyl Chloride
<0.0810
25.0
27.3
109
24.6
98
70-121
10
20
ug/L
08.14.14 17:29
m,p-Xylenes
<0.176
50.0
50.7
101
48.9
98
65-151
4
20
ug/L
08.14.14 17:29
o-Xylene
<0.122
25.0
26.2
105
22.7
91
58-148
14
20
ug/L
08.14.14 17:29
MS
MS
MSD
MSD
Limits
Units
Analysis
Surrogate
%Rec
Flag
%Rec
Flag
Date
1,2-Dichloroethane-D4
93
93
65-134
%
08.14.14 17:29
4-Bromofluorobenzene
103
96
60-148
%
08.14.14 17:29
Toluene-D8
106
107
87-114
%
08.14.14 17:29
Flag
F
Page 22 of 29 Final 1.000

X 7
Blank Summary 491299A &
Sample Id: 659992-1-BLK
Lab Sample Id: 659992-1-BLK
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Matrix: WATER
Analytical Method: Lead by SW-846 6010C
Tech: JDR
Analyst: ABA
Seq Number: 948303
Date Prep: 08.14.14 10:14
Prep Method: SW3010A
Parameter Cas Number Result RL p4DL Units Analysis Flag Dil
Date
Lead 7439-92-1 U 0.0100 0.00330 mg/L 08.15.1413:34 U 1
Page 23 of 29 Final 1.000

•
Blank Summary
491299
t
y
rju
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.,
Mebane,
NC
Colliseum Shell
Sample Id: 660051-1-BLK
Matrix: WATER
Lab Sample Id: 660051-1-BLK
Analytical Method: VOCs by GCIMS by SM6200B
Prep Method: SM6200B_PREP
Tech: LIH
Analyst: MLA
Date
Prep: 08.14.14 06:34
Seq Number: 948247
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
08.14.14 09:20
U
I
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
08.14.14 09:20
U
I
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
08.14.14 09:20
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
08.14.14 09:20
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
08.14.14 09:20
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
08.14.14 09:20
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
08.14.14 09:20
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
08.14.14 09:20
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
08.14.14 09:20
U
I
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
08.14.14 09:20
U
I
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
08.14.14 09:20
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
I.00
0.180
ug/L
08.14.14 09:20
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
08.14.14 09:20
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
08.14.14 09:20
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
08.14.14 09:20
U
I
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
08.14.14 09:20
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
08.14.14 09:20
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
08.14.14 09:20
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
08.14.14 09:20
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
08.14.14 09:20
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
08.14.14 09:20
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
09.14.14 09:20
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
08.14.14 09:20
U
I
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
08.14.14 09:20
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
08.14.14 09:20
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
08.14.14 09:20
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
08.14.14 09:20
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
08.14.14 09:20
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
08.14.14 09:20
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
08.14.14 09:20
U
I
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
08.14.14 09:20
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
08.14.14 09:20
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
08.14.14 09:20
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
08.14.14 09:20
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
08.14.14 09:20
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
08.14.14 09:20
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
08.14.14 09:20
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
08.14.14 09:20
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
08.14.14 09:20
U
1
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
08.14.14 09:20
U
1
Page 24 of 29 Final 1.000

•
t
Florida Testing Services, LLC
0un-
Blank Summary 491299A*
�
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: 660051-1-BLK Matrix: WATER
Lab Sample Id: 660051-1-BLK
Analytical Method: VOCs by GUMS by SM6200B Prep Method: SM6200B_PREP
Tech: LIH
Analyst: MLA Date Prep: 08.14.14 06:34
Seq Number: 948247
Parameter
Cas Number
Result
RL
MDL
Units
Analysis
Flag
Dil
Date
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
08.14.14 09:20
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
08.14.14 09:20
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
08.14.14 09:20
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
09.14.14 09:20
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
08.14.14 09:20
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L.
08.14.14 09:20
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
08.14.14 09:20
U
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
08.14.14 09:20
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
08.14.14 09:20
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
08.14.14 09:20
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
08.14.14 09:20
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
08.14.14 09:20
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
08.14.14 09:20
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
08.14.14 09:20
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
08.14.14 09:20
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
08.14.14 09:20
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
09.14.14 09:20
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
08.14.14 09:20
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
08.14.14 09:20
U
I
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
08.14.14 09:20
U
I
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
08.14.14 09:20
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
08.14.14 09:20
U
1
m,p-Xylenes
179601-23-1 .
U
1.00
0.176
ug/L
08.14.14 09:20
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
08.14.14 09:20
U
1
Page 25 of 29 Final 1.000

Blank Summary 491299
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: 948130-1-BLK Matrix: WATER
Lab Sample Id: 948130-1-BLK
Analytical Method: TSS by SM2540D Prep Method:
Tech: NSI
Analyst: NSI Date Prep:
Seq Number: 948130
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Total Suspended Solids U 4.00 3.50 mg/L 08.12.14 15:00 U 1
Page 26 of 29 Final 1.000

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HIID S.b�
y
g No, Yes, M - I
0
tw' M-a-
Address
r
E 4.
CargoAlrersi rhy DO,
HOLD
2
7 Payment Hana,
State
ZIP 3110i�.. 5
Obtain eco.
rm
d&ACMNaCtC,,,[nCard N&b*jmv. AM No. L-I
ROCIP
lent❑Third Party CreditCard El CadVCheek
Total Packages TotalWeWl O.LACWA�
16051
8748 2M 0468
SRS

XENCO Laboratories
.
Prelogin/Nonconformance Report= Sample Log -In
Florida Testing Services, LLC
Client 3er-aquest ,Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC
Date/Time Received: 08/12/2014 02:2000 PM Air: and Metal samples Acceptable Range: Ambient
Work Order #: 491299 Temperature Measuring device used : #61
Sample Receipt Checklist
Comments
#1 *Temperature of cooler(s)?
1.4
42 *Shipping container in good condition?
Yes
#3 *Samples received on ice?
Yes
#4 *Custody Seals intact on shipping container/ cooler?
N/A
#5 Custody Seals -intact on sample bottles?
N/A
#6 *Custody Seals Signed and dated?
N/A
#7 *Chain of Custody present?
Yes
#8 Sample instructions complete on Chain of Custody?
Yes
#9 Any missing/extra samples?
No
#10 Chain of Custody signed when relinquished/ received?
Yes
#11 Chain of Custody agrees with sample label(s)?
Yes
#12 Container label(s) legible and intact?
Yes
#13 Sample matrix/ properties agree with Chain of Custody?
Yes
#14 Samples in proper container/ bottle?
Yes
#15 Samples properly preserved?
Yes
#16 Sample.container(s) intact?
Yes
#17 Sufficient sample amount for indicated test(s)?
Yes
#18 All samples received within hold time?
Yes
#19 Subcontract of sample(s)?
No
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
Yes
#21 <2 for all samples preserved with HNO3,HCL, H2SO4?
Yes
#22 >10 for all samples preserved with NaAs02+NaOH, ZnAc+NaOH?
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: DL PH Device/Lot#: 1016662-2
Checklist completed b
P y
Date:08/12/2014
Dario Lagunas
Checklist reviewed by:�� �(
l
Date: 08/12/2014
Mike Kimmel
Page 29 of 29
Final 1.000

Kw im wA e. Nardi Cadre 27284
TerraQuest Environmental Consultants, P.C.
100 E Ruffin Street
Mebane, NC 27302
Attention: Ryan Kerins
Past Off= Banc 473
A]
C
Md
4
NyprB N0. 11617M
28 July 2.Q14
TERMS: NET 30
"PAST DUE INVOICES ACCRUE
INTEREST AT 1 Ya % INTEREST PER
MONTH UNTIL PAID
SHOULD COLLECTION BE REQUIRED,
CUSTOMER AGREES'TO PAY
ALL EXPENSES INCURRED INCLUDING
ATTORNEY'S FEES"
RE:
Phone [phone]

n
RESEARCh & ANALYTICAL
LA ORATORIES INC.
L� Analyflcol/Process Consultaflons
July 28, 2014
TerraQuest Environmental Consultants, P.C.
100 E Ruffin Street
Mebane, NC 27302
Attention: Ryan Kerins
L Miscellaneous Effluent
Coliseum Shell
Parameters Unit Results
Cadmium, Soluble
mg/L
<0.002
Chromium, Soluble
mg/L
<0.005
Copper, Soluble
mg/L
<0.005
Nickel, Soluble
mg/L
<0.005
Lead, Soluble
mg/L
<0.005
Zinc, Soluble
mg/L
0.014
Aluminum, Soluble
mg/L
0.517
Cobalt, Soluble
mg/L
<0.005
Iron, Soluble
mg/L
0.208
Manganese, Soluble
mg/L
0.026
Arsenic, Soluble
mg/L
0.011
Mercury, Soluble
mg/L
<0.0002
Calcium, Soluble
mg/L
15.1
Magnesium, Soluble
mg/L
4.42
Potasium, Soluble
mg/L
2.59
RAL Sample Number: 790270
Date Collected: 07/16/14
Time Collected: 0938
mg/L - milligrams per Liter = parts per million (ppm) < = Less than or below detection limit

Effluent Aquatic Toxicity Report/Phase II Chronic Ceriodaphnia
07/23/14
Facility ' Coliseum Shell NPDES#NC 0088919 Pipe# 001 - County Forsyth .
Laboratory Performing Test - Research & nalyti al Labs, Inc. Comments: Final Effluent
X X .. A Terraquest Env. Project
Signature of O.R.C. S• atur of.Lab S ervlsor.. RAL 9790270/790509
Sample Information
Collection Start Date
Grab
Composite
(Duration)
Hardness (mg/1)
Spec.Cond. (-mhos/cm)
Chlorine (mg/L)
Sample temp: at receipt
Sample 1
Sample 2
Control
07/16/14
07/18/14
X
X
-
. _... ... .
I r u
48
179
142
192
0.03
0.02
3.30
.3.10
imil
Infomation•
Treatment
pH Initial
pH Final
D.O. Initial
D.O. Final
Temp. initial
Temp. Final
Start Date
07/16/14
End Date
07123/14
Start Tune
14,47 PM
End Time
11:16 AM
Start
Renew I
Renew 2
Start
Renew I
Renew 2
90%
9D°/a
90%
Control
Control,
Control
8.65 .
7.24
7.24
6.9.4
6.97
6.98..
8.53
7.32
7.33
7.03
: , 7.03
7.07
8.5
8.6
8.6
8.5
8.6
8.6
8.2
81
8.4
8.3
8.3
8A
24.7
24.9
24.6
24A
24A
24.2
24A
24.9
.24.6
24A
24.9
24.6
Chronic Test Results'
Or and ism#
Final Contml mm'Wity %
0
1
2.
3
4
5. 6 7
8
9
10 11'
12 Mean
%Control 3rd Brood
100
Control
Control Repro CV
6.47
1
2
3
4
5 6 7
8
9
10 n,
12 Mean
Control IWC
Effluent %
q Young
24
21
23
T2
24
25
21
23
21
24
22.8
Adult
•
(L)i4e(D)ead
L
L
L
L.
L
L
L
L
L
L,.
_
M Young
23
21
25
21
23
22
25
22
23
24
229
Adult
(L)ive (D)e9d
L
L
L
L
L
L
L
L
L
L
°/. Red t
-0.42%
0 of 10 0 of 10
sigoi6wn9 Y Lt
Fiinal Mortality Significant Q
1 2 3 4 5 6 7 8 9 10 Mean 2 or No Cona
Effluent
Reproduction
Y.
fl Young
22
24
21
20
22
20
.24.
23
21
21
218
Adult
%Red t
14.39
2$
(Lrve(D)md
L
I.
L
L
L
L
L
L
L
L
Repro. LOEC = 50% NOEC = 25%
Method: Steel's Many One Test ,
1 2 3 4 ..5 6 1 8 9 to NormalDistrib? No Method: 'Kolmogorov
Etiltumt+h
q Young .'
19
19.
20
19
22
19.
19
21
19
21
19.8
Adult°b
Red t
50
(Love (D)ead
L
L
L
L
L
L
L
L
L
L
13.2
Statistic: 1.07 Critical: 1.035
Etlrml Variances? yes Method: Bartletts
Statistic: 7.32 Critical: 15.08
1 2 3. 4 .5 :. 6 7 ' 8 9 l0 Mean Non -Parametric Analysis fifanplicable):
Enluem %
75
tl Young
16
IS
21
19
19
17
20
19
18
17
18.1
Adult
(Dive (Dkad
L
L
L
L
L
L
L
L
L
L
°/+Red t
20.6
Method: Steel's Many One Test
uent°/
Rank Sum Critical Sum
12.5
106.3 75
25
86.5 75
' S0 61.5 75
75 56.5 75
1 2 3 4 5 6 7 8 9 10 Mean 90 55 75
Enlucnt %
1:1
erall nal U=
Result = PASSIFAIL or
Tat LOEC � 75 %: NOEC= 50016
Chronic Value= 61.24
ATT: Environmental Sciences Branch • Should use highest test concentration or
Div _ Of Water Quality highest concentration with D.O. >5.0 mg/I
MAIL N.C. DENR
To.. 1621 Mail SerPiee Center 1% Reduction from Control Reproduction Mean
Raleigh, NC 27699-1621
Copy DWQ form AT-3 (8191) Rev. 11/9S
tYYoung
14
10
16
18.
16
IS
19
13.
18
17
15.8
Adult
(L)ive (Dkad
L
L
L
L
L_
L
L
L
L
L
1+R� t
30.7

RESEARCh & AWYACA[
LkOR IJORIES Bo o
Analytical/Process Consultations
BIOASSAY CHAIN OF CUSTODY RECORD
Client: l��rvr._oc+ SI L-rViYet1 �n-f-ct f County: Pipe (#:001 NPDES #:_�ffq 9
L
Collector (Print) : AvJ,,( W✓e�neti ::onrict Person.
Collector (Signature: C_ -- Address: �d0 �. Qw-i-+`r. h G'9-
Phone Number:::[
Lab f#
WAL only)
Sample
Description
(see note•)
Sample Collection
Sample Type
No. of
containers
sent
Temp
Upon
Arrival
(°C)
Analysis
Required
(acute, chronic
bioassay)
7atteDate/
Time
Ended
Temp
(°C)
End
Comp.
Grab
p
�.
2 '
c , pel" C-
13
for Sample Description please use Effluent, Influent, Upstream, Post Cl2, Etc.
Relinquished by: (Signature)
Received by: (Signature)
Date/Time
�llla/i�C lv�.�,�
Relinq hed by: (Signature)
Received by: (Signs re)
Date/Time
Method of Shipment:
Logged in by: Moved to bioassay dept. by:
Initials Initials= ,1-7 Date_%�/`' /-/Time
i
Note: Original sent. with shipment
Copy retained by.collector
P.O. Box 473 0 106 Short Street- Kernersville, North Carolina 27284 0 336-996-2841 Fax [phone]
www.randalabs.com

Analytical/Process Consultations
BIOASSAY CHAIN OF CUSTODY RECORD
Client: �� �u eS' virbvi e,..�( Count 1.0 0C ( a$ 71 l9
n I t , y: Pipe #: NPDES' #:
Collector (Print): 7 rj,.! Wt`�XA Goneact Person.
S �vTe4r.�e me
a
: fee C ea:.,Collector (Signature:. ' ~ Address:
Phone Number: (� S� 3 Oct l
Lab #
only)
(RAIL only)
Sample
Description
(see note*)-
Sample..Collection
•
Sample TV .
No. of
containers
sent
Temp Upon
Arrival '
(°C)
Analysis
Required
(acute, chronic
bioassay)
Date/
Time
Started
Date/
Time
Ended
Temp
(°C)
End
Grab
1VT-10
C Wt�eA �
.3
G �,,,caP, "-%
3.
L
(Z•S rr, So,�rrgy
.u�ls
/ Cr /%DNA, Pj,
e . r
° for Sample Description please use Effluent, Influent, Upstream, Post Clz, Etc.
IYJ
Relinquished by: (Signature)
Receiveeeddf by: (Signature)
Date/time
Relin fished by: (Signature)
Received by: (S' ` ature)
Date/Time
Method of Shipment:
Logged in by:
Moved to bioassay dept. by:
Initials KnA
1 ' 1 /
Initials Date Time
Note: Original sent with shipment
Copy retained by collector
P.O. Box 473 0 106 Short Street ^ Kernersville, North Carolina 27284 0 386-996-2841 Fax [phone]
www.randalabs.com

Analytical Report 488977
for
Terraquest Environmental Consultants, P.C.
Project Manager: Ryan Kerins
Colliseum Shell
01195
14-JUL-14
Collected By: Client
XGHC0
Laboratories
Florida Testing Services, LLC
�CCRF
!W""V
qeun a�..nc�ui.o-a
6017 Financial Dr., Norcross, GA 30071
Ph:[phone] Fax:[phone]
Xenco-Houston (EPA Lab code: TX00122):
Texas (Tl04704215-14-16-TX), Arizona (AZ0765), Florida (E871002), Louisiana (03054)
New Jersey (TX007), North Carolina(681), Oklahoma (9218), Pennsylvania (68-03610)
Xenco-Atlanta (EPA Lab Code: GA00046):
Florida (E87429), North Carolina (483), South Carolina (98015), Kentucky (85), DoD ( L10-135)
Louisiana (04176), USDA (P330-07-00105)
Xenco-Lakeland: Florida (E84098)
Xenco-Odessa (EPA Lab code: TX00158): Texas (T104704400-TX)
Xenco-Dallas (EPA Lab code: TX01468): Texas (Tl04704295-TX)
Xenco Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)
Xenco-Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)
Xenco Tucson (EPA Lab code:AZ000989): Arizona (AZ0758)
Page 1 of 31 Final 1.000

Table of Contents
Cover Page
Cover Letter 3
Sarnpie 1[5 Cross Reference 4
Case Narrative 5
Explanation of Qualifiers (Flags) 61
Hits Summary 7
—certificate of Analysis (Detailed Report)
Summary of Quality control 20
LBIank Summary ' 25 j
Chain of Custody 29
Sample Receipt Conformance Report 31.1
Page 2 of 31 Final 1.000

40
a.4RAtd aWm.aw.n
14-JUL-14
Project Manager: Ryan Kerins
Terraquest Environmental Consultants, P.C.
100 E. Ruffin Street
Mebane, NC 27302
Reference: XENCO Report No(s): 488977
Colliseum Shell
Project Address: NC
Ryan Kerins:
We are reporting to you the results of the analyses performed on the samples received under the project name
referenced above and identified with the XENCO Report Number(s) 488977. All results being reported under
this Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.
Subcontracted analyses are identified in this report with either the NELAC certification number of the
subcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.
Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance with
NELAC standards. The uncertainty of measurement associated with the results of analysis reported is
available upon request. Should insufficient sample be provided to the laboratory to meet the method and
NELAC Matrix Duplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and
reported using all other available quality control measures.
The validity and integrity of this report will remain intact as long as it is accompanied by this letter and
reproduced in full, unless written approval is granted by XENCO Laboratories. This report will be filed for at
least 5 years in our archives after which time it will be destroyed without further notice, unless otherwise
arranged with you. The samples received, and described as recorded in Report No. 488977 will be filed for
60 days, and after that time they will be properly disposed without further notice, unless otherwise arranged
with you. We reserve the right to return to you any unused samples, extracts or solutions related to them if we
consider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standard
practices, controlled substances under regulated protocols, etc).
We thank you for selecting XENCO Laboratories to serve your analytical needs. If you have any questions
concerning this report, please feel free to contact us at any time.
Respectfully,
Eben Buchanan
Project Manager
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America
Page 3 of 31 Final 1.000

s
Sample Cross Reference 488977
r�u
lodda Testing Services, u.c
Terraquest Environmental Consultants, P.C., Mebane,
NC
Colliseum Shell
Sample Id
Matrix Date Collected Sample Depth
Lab Sample Id
Influent
W 07-08-14 12:20
488977-001
After Ast
W 07-08-14 12:30
488977-002
After 1st GAC
W 07-08-14 12:06
488977-003
Effluent
W 07-08-14 12:08
488977-004
Page 4 of 31 Final 1.000

CASE NARRATIVEA W6.
rau
lcrida Testing Services, «c Client Name: Terraquest Environmental Consultants, P. C.
Project Name: Colliseum Shell
Project ID: 01195 Report Date: 14-JUL-14
Work Order Number(s): 488977 Date Received: 0710912014
Sample receipt non conformances and comments:
Sample receipt non conformances and comments per sample:
None
Analytical non conformances and comments:
Batch: LBA-945325 VOCs by GUMS by SM6200B
2-Hexanone, Acetone recovered above QC limits in the laboratory control sample indicating a potential
high bias. Both analytes were acceptable in the associated MS/MSD sample and therefore the data was
accepted.
2-Butanone (MEK), 2-Hexanone, Acetone RPD between the BKS & BSD was outside laboratory control
limits.
Samples affected are: 488977-001, -004, -003, -002
Page 5 of 31 Final 1.000

A«R�
Flagging Criteria ??%WK
Florida Testing Services, LLC
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be
outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough
to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or
laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference.
Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and
QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the
Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated
numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non -Calculable
+ NELAC certification not offered for this compound.
* (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.
Certified and approved by numerous States and Agencies.
A Small Business and Minority Status Company that delivers SERVICE and QUALITY
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 77477
9701 Harry Hines Blvd, Dallas, TX 75220
5332 Blackberry Drive, San Antonio TX 78238
2505 North Falkenburg Rd, Tampa, FL 33619
12600 West I-20 East, Odessa, TX 79765
6017 Financial Drive, Norcross, GA 30071
3725 E. Atlanta Ave, Phoenix, AZ 85040
Phone
Fax
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
[phone]
Page 6 of 31 Final 1.000

Hits Summary 488977
Florida TWng Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Influent Matrix: Ground Water % Moisture
Lab Sample Id : 488977-001 Date Collected: 07.08.14 12.20
Date Received: 07.09.14 11.05
Analytical Method: VOCs by GC/MS by SM6200B
Seq Number 945325
Parameter Cas Number
Result
Units
Prep Method:
Date Prep:
Analysis Date
SM620OB_PREP
07.10.14 06.45
Flag Dil
1,2,4-Trimethylbenzene
95-63-6
10.4
ug/L
07.10.1411.57
1
1,3,5-Trimethylbenzene
108-67-8
3.38
ug/L
07.10.1411.57
1
2-Hexanone
591-78-6
19.4
ug/L
07.10.1411.57
BF 1
4-Methyl-2-pentanone (MIBK)
108-10-1
6.62
ug/L
07.10.14 11.57
1
Acetone
67-64-1
119
ug/L
07.10.1411.57
HF 1
Benzene
71-43-2
19.4
ug/L
07.10.1411.57
1
Ethylbenzene
100-41-4
4.88
ug/L
07.10.1411.57
1
Isopropyl ether
108-20-3
33.1
ug/L
07.10.14 11.57
1
Methyl tert-butyl ether (MTBE)
1634-04-4
1350
ug/L
07.10.14 12.28
D 50
Naphthalene
91-20-3
25.9
ug/L
07.10.1411.57
1
Styrene
100-42-5
0.620
ug/L
07.10.1411.57
1
Toluene
108-88-3
52.1
ug/L
07.10.1411.57
1
m,p-Xylenes
179601-23-1
22.7
ug/L
07.10.1411.57
1
o-Xylene
95-47-6
19.5
ug/L
07.10.1411.57
1
Page 7 of 31 Final 1.000

• Hits Summary 488977
I rau
Flodda Testlng Services, LLC
Terraquest Environmental Consultants, P.C., Mebane,
NC
Colliseum Shell
Sample Id: After Ast
Matrix: Ground Water
% Moisture:
Lab Sample Id: 488977-002
Date Collected: 07.08.14 12.30
Date Received: 07.09.14 11.05
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method:
SM6200B_PREP
Seq Number 945325
Date Prep:
07.10.14 06.45
Parameter
Cas Number Result Units
Analysis Date
Flag Dil
Acetone
67-64-1 25.3 ug/L
07.10.1411.29
l3F 1
Methyl tert-butyl ether (MTBE)
1634-04-4 3.01 ug/L
07.10.14 11.29
1
Page 8 of 31 Final 1.000

/ACC
Hits Summary 488977
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water % Moisture:
Lab Sample Id : 488977-003 Date Collected : 07.08.14 12.06
Date Received: 07.09.14 11.05
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM6200B_PREP
Seq Number 945325 Date Prep: 07.10.14 06.45
Parameter Cas Number Result Units Analysis Date Flag Dil
Acetone 67-64-1 11.6 ug/L 07.10.1411.00 HF 1
Chloroform 67-66-3 3.15 ug/L 07.10.1411.00 1
Methyl tert-butyl ether (MTBE) 1634-04-4 2.49 ug/L 07.10.14 11.00 1
Page 9 of 31 Final 1.000

• Hits Summary 488977TRt-
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent Matrix : Ground Water % Moisture:
Lab Sample Id: 488977-004 Date Collected: 07.08.14 12.08
Date Received: 07.09.14 11.05
Analytical Method: TSS by SM2540D
Seq Number 945410
Parameter
Cas Number Result Units Analysis Date Flag Dil
Total Suspended Solids 7.00 mg/L 07.10.14 11.00 1
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM620OB_PREP
Seq Number 945325 Date Prep: 07.10.14 06.45
Parameter Cas Number Result Units Analysis Date Flag Dil
Methylene Chloride 75-09-2 0.770 ug/L 07.10.14 10.31 1
Page 10 of 31 Final 1.000

Certificate of Analytical Results 488977
r�au
�BQR9L9� ... o..n......,.
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Influent
Lab Sample Id: 488977-001
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Matrix: Ground Water
Date Collected: 07.08.14 12.20
Date Prep: 07.10.14 06.45
Result RL MDL
Units
Date Received:07.09.14 11.05
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
07.10.1411.57
U
I
I,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
07.10.1411.57
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
07.10.1411.57
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
07.10.1411.57
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
07.10.1411.57
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
07.10.14 11.57
U
I
I,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
07.10.14 11.57
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
07.10.1411.57
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
07.10.1411.57
U
I
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
07.10.14 11.57
U
1
1,2,4-Trimethylbenzene
95-63-6
10.4
0.500
0.103
ug/L
07.10.14 11.57
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
07.10.14 11.57
U
I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
07.10.1411.57
U
I
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
07.10.1411.57
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
07.10.14 11.57
U
1
1,3,5-Trimethylbenzene
108-67-8
3.38
0.500
0.0870
ug/L
07.10.1411.57
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
07.10.14 11.57
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
07.10.1411.57
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
07.10.1411.57
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
07.10.14 11.57
U
I
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
07.10.1411.57
OF
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
07.10.1411.57
U
I
2-Hexanone
591-78-6
19.4
0.400
0.352
ug/L
07.10.1411.57
HF
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
07.10.1411.57
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
07.10.1411.57
U
I
4-Methyl-2-pentanone (MIBK)
108-10-1
6.62
0.400
0.253
ug/L
07.10.14 11.57
1
Acetone
67-64-1
119
2.00
0.352
ug/L
07.10.1411.57
HF
1
Benzene
71-43-2
19.4
0.500
0.119
ug/L
07.10.1411.57
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
07.10.1411.57
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
07.10.1411.57
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
07.10.1411.57
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
07.10.1411.57
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
07.10.1411.57
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
07.10.14 11.57
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
07.10.14 11.57
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
07.10.1411.57
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
07.10.1411.57
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
07.10.14 11.57
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
07.10.1411.57
U
1
Page 11 of 31 Final 1.000

Lil, Lie Certificate of Analytical Results 488977 f �B
r�u
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Influent Matrix: Ground Water Date Received:07.09.14 11.05
Lab Sample Id: 488977-001 Date Collected: 07.08.14 12.20
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LTH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Date Prep:
Result
07.10.14 06.45
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
07.10.1411.57
U 1
cis- 1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
07.10.14 11.57
U 1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
07.10.1411.57
U 1
Ethanol
64-17-5
U
50.0
3.00
ug/L
07.10.1411.57
U 1
Ethylbenzene
100-41-4
4.88
0.500
0.0920
ug/L
07.10.1411.57
1
Isopropyl ether
108-20-3
33.1
0.500
0.0920
ug/L
07.10.14 11.57
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
07.10.14 11.57
U 1
Methyl tert-butyl ether (MTBE)
1634-04-4
1350
25.0
8.45
ug/L
07.10.14 12.28
D 50
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
07.10.14 11.57
U I
Naphthalene
91-20-3
25.9
2.00
0.0940
ug/L
07.10.1411.57
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
07.10.14 11.57
U 1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
07.10.1411.57
U I
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
07.10.1411.57
U 1
Styrene
100-42-5
0.620
0.500
0.0740
ug/L
07.10.1411.57
I
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
07.10.14 11.57
U I
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
07.10.14 11.57
U I
Toluene
108-88-3
52.1
0.500
0.0570
ug/L
07.10.1411.57
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
07.10.1411.57
U 1
trans- l,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
07.10.14 11.57
U 1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
07.10.1411.57
U 1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L,
07.10.1411.57
U 1
Vinyl Acetate
108-05-4
U
I.00
0.720
ug/L
07.10.14 11.57
U 1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
07.10.14 11.57
U 1
m,p-Xylenes
179601-23-1
22.7
1.00
0.176
ug/L
07.10.1411.57
1
o-Xylene
95-47-6
19.5
0.500
0.122
ug/L
07.10.1411.57
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
109
%
65-134
07.10.1411.57
4-Bromofluorobenzene
460-00-4
100
%
60-148
07.10.1411.57
Toluene-D8
2037-26-5
104
%
87-114
07.10.1411.57
Page 12 of 31 Final 1.000

Certificate of Analytical Results 488977
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After Ast
Lab Sample Id: 488977-002
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Matrix: Ground Water
Date Collected: 07.08.14 12.30
Date Prep: 07.10.14 06.45
P«Ap0
NI
r�u
Date Received:07.09.14 11.05
Prep Method: SM6200B PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
07.10.1411.29
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
07.10.1411.29
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L.
07.10.1411.29
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
07.10.1411.29
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
07.10.1411.29
U
1
1,1-Dichloroethene
75-354
U
0.500
0.104
ug/L
07.10.14 11.29
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
07.10.1411.29
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
07.10.1411.29
U
I
1,2,3-Trichloropropane
96-I8-4
U
1.00
0.138
ug/L
07.10.1411.29
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
07.10.1411.29
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
07.10.1411.29
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
07.10.14 11.29
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
07.10.1411.29
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
07.10.1411.29
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
07.10.1411.29
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
07.10.1411.29
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
07.10.1411.29
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L.
07.10.1411.29
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
07.10.1411.29
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
07.10.1411.29
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
07.10.14 11.29
OF
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L.
07.10.1411.29
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
07.10.1411.29
UHF
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
07.10.14 11.29
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
07.10.14 11.29
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
07.10.14 11.29
U
1
Acetone
67-64-1
25.3
2.00
0.352
ug/L
07.10.1411.29
HF
1
Benzene
71-43-2
U
0.500
0.119
ug/L
07.10.1411.29
U
1
Bromobenzene
109-86-1
U
0.500
0.132
ug/L
07.10.1411.29
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
07.10.1411.29
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
07.10.1411.29
U
I
Bromoform
75-25-2
U
2.00
0.159
ug/L
07.10.1411.29
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
07.10.1411.29
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
07.10.14 11.29
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
07.10.1411.29
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
07.10.1411.29
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
07.10.14 11.29
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L.
07.10.1411.29
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
07.10.1411.29
U
1
Page 13 of 31 Final 1.000

Certificate of Analytical Results 488977
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After Ast Matrix: Ground Water Date Received:07.09.14 11.05
Lab Sample Id: 488977-002 Date Collected: 07.08.14 12.30
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Date Prep:
Result
07.10.14 06.45
RL MDL
Prep Method: SM6200B PREP
% Moisture:
Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
07.10.14 11.29
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
07.10.1411.29
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
07.10.14 11.29
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
07.10.1411.29
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
07.10.14 11.29
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
07.10.14 11.29
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
07.10.14 11.29
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
3.01
0.500
0.169
ug/L
07.10.14 11.29
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L.
07.10.14 11.29
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
07.10.14 11.29
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
07.10.1411.29
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
07.10.14 11.29
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
07.10.14 11.29
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
07.10.14 11.29
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
07.10.14 11.29
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
07.10.14 11.29
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L,
07.10.1411.29
U
I
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
07.10.14 11.29
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
07.10.14 11.29
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
07.10.1411.29
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L,
07.10.1411.29
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
07.10.14 11.29
U
I
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
07.10.14 11.29
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
07.10.1411.29
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
07.10.1411.29
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
104
%
65-134
07.10.1411.29
4-Bromofluorobenzene
460-00-4
102
%
60-148
07.10.14 11.29
Toluene-D8
2037-26-5
106
%
87-114
07.10.1411.29
Page 14 of 31 Final 1.000

Certificate of Analytical Results 488977
�1/ eau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water Date Received:07.09.14 11.05
Lab Sample Id: 488977-003 Date Collected: 07.08.14 12.06
Analytical Method: VOCs by GUMS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Prep Method: SM6200B_PREP
% Moisture:
Date Prep: 07.10.14 06.45
Result RL MDL Units Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
07.10.1411.00
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
07.10.1411.00
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
07.10.1411.00
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
07.10.1411.00
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
07.10.1411.00
U
1
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
07.10.14 11.00
U
I
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
07.10.14 I1.00
U
I
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
07.10.1411.00
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
07.10.14 11.00
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
07.10.14 11.00
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
07.10.14 11.00
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
07.10.14 11.00
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
07.10.1411.00
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
07.10.1411.00
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
07.10.14 11.00
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
07.10.14 11.00
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
07.10.1411.00
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
07.10.1411.00
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
07.10.14 11.00
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
07.10.14 11.00
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
07.10.14 11.00
OF
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
07.10.14 11.00
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
07.10.14 11.00
UHF
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
07.10.14 11.00
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
07.10.14 11.00
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
07.10.1411.00
U
1
Acetone
67-64-1
11.6
2.00
0.352
ug/L
07.10.1411.00
BF
1
Benzene
71-43-2
U
0.500
0.119
ug/L
07.10.1411.00
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
07.10.1411.00
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
07.10.14 11.00
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
07.10.1411.00
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
07.10.1411.00
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
07.10.1411.00
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
07.10.14 11.00
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
07.10.1411.00
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
07.10.1411.00
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
07.10.14 11.00
U
1
Chloroform
67-66-3
3.15
0.500
0.172
ug/L
07.10.14 11.00
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
07.10.1411.00
U
1
Page 15 of 31 Final 1.000

Certificate of Analytical Results 488977 OWN
rau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water Date Received:07.09.14 11.05
Lab Sample Id: 488977-003 Date Collected: 07.08.14 12.06
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Date Prep:
Result
07.10.14 06.45
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
07.10.1411.00
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
07.10.14 11.00
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
07.10.14 11.00
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
07.10.14 11.00
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
07.10.1411.00
U
I
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
07.10.14 11.00
U
I
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
07.10.14 11.00
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
2.49
0.500
0.169
ug/L
07.10.14 11.00
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
07.10.14 11.00
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
07.10.1411.00
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
07.10.14 I1.00
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
07.10.14 11.00
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
07.10.14 11.00
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
07.10.1411.00
U
I
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
07.10.1411.00
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
07.10.14 11.00
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
07.10.1411.00
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
07.10.14 11.00
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
07.10.14 11.00
U
1
Trichloroetbene
79-01-6
U
0.500
0.139
ug/L
07.10.1411.00
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
07.10.14 11.00
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
07.10.14 11.00
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
07.10.14 11.00
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
07.10.14 11.00
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L,
07.10.1411.00
U
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
101
%
65-134
07.10.1411.00
4-Bromofluorobenzene
460-004
103
%
60-148
07.10.14 11.00
Toluene-D8
2037-26-5
107
%
87-114
07.10.1411.00
Page 16 of 31 Final 1.000

Certificate of Analytical Results 488977
ru
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent
Lab Sample Id: 488977-004
Analytical Method: TSS by SM2540D
Tech: NSI
Analyst: NSI
Seq Number: 945410
Parameter
Total Suspended Solids
Matrix: Ground Water Date Received:07.09.14 11.05
Date Collected: 07.08.14 12.08
% Moisture:
Cas Number Result RL NIDL Units Analysis Date Flag Dil
Analytical Method: Lead by SW-846 6010C
Tech: JDR
Analyst: 4150
Seq Number: 945515
7.00 4.00 3.50 mg/L 07.10.1411.00 1
Date Prep: 07.12.14 13.01
Prep Method: SW3010A
% Moisture:
Parameter Cas Number Result RL NIDL Units Analysis Date Flag DR
Lead 7439-92-1 U 0.0100 0.00330 mg/L 07.14.1414.10 U 1
Page 17 of 31 Final 1.000

ACcgFp\
Certificate of Analytical Results 488977
rLu
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:07.09.14 11.05
Lab Sample Id: 488977-004 Date Collected: 07.08.14 12.08
Analytical Method: VOCs by GC/MS by SM6200B
Tech: LIH
Analyst: MLA
Seq Number: 945325
Parameter Cas Number
Prep Method: SM6200B PREP
% Moisture:
Date Prep: 07.10.14 06.45
Result RL MDL Units Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
07.10.1410.31
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
07.10.14 10.31
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
07.10.1410.31
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
07.10.14 10.31
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
07.10.14 10.31
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
07.10.14 10.31
U
I
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
07.10.14 10.31
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
07.10.14 10.31
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
07.10.14 10.31
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
07.10.1410.31
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
07.10.14 10.31
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
07.10.14 10.31
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
07.10.1410.31
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
07.10.1410.31
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
07.10.14 10.31
U
I
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
07.10.14 10.31
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
07.10.14 10.31
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
07.10.14 10.31
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
07.10.1410.31
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
07.10.14 10.31
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
07.10.14 10.31
OF
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
07.10.14 10.31
U
I
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
07.10.1410.31
UHF
I
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
07.10.14 10.31
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
07.10.14 10.31
U
1
4-Methyl-2-pentanone (MLBK)
109-10-1
U
0.400
0.253
ug/L
07.10.14 10.31
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
07.10.1410.31
UHF
1
Benzene
71-43-2
U
0.500
0.119
ug/L,
07.10.1410.31
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L,
07.10.1410.31
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
07.10.1410.31
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
07.10.1410.31
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L,
07.10.1410.31
U
1
Bromoinethane
74-83-9
U
1.00
0.0970
ug/L
07.10.1410.31
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
07.10.14 10.31
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
07.10.1410.31
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
07.10.1410.31
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
07.10.1410.31
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
07.10.14 10.31
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
07.10.14 10.31
U
1
Page 18 of 31 Final 1.000

Certificate of Analytical Results 488977 �e t
rau
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: Effluent
Matrix:
Ground Water
Date Received:07.09.14 11.05
Lab Sample Id: 488977-004
Date Collected: 07.08.14
12.08
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM6200B PREP
Tech: LIH
% Moisture:
Analyst: MLA
Date Prep:
07.10.14 06.45
Seq Number: 945325
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
07.10.1410.31
U 1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
07.10.14 10.31
U 1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
07.10.1410.31
U 1
Ethanol
64-17-5
U
50.0
3.00
ug/L
07.10.14 10.31
U 1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
07.10.1410.31
U I
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
07.10.14 10.31
U 1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
07.10.14 10.31
U 1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
07.10.14 10.31
U 1
Methylene Chloride
75-09-2
0.770
0.500
0.190
ug/L
07.10.14 10.31
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
07.10.14 10.31
U 1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
07.10.1410.31
U 1
n-Propylbenzene
103-65-1
U
I.00
0.0650
ug/L
07.10.14 10.31
U 1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L,
07.10.1410.31
U 1
Styrene
100-42-5
U
0.500
0.0740
ug/L.
07.10.1410.31
U 1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
07.10.1410.31
U 1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
07.10.14 10.31
U 1
Toluene
108-88-3
U
0.500
6.0570
ug/L
07.10.1410.31
U I
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
07.10.1410.31
U 1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
07.10.14 10.31
U 1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
07.10.1410.31
U 1
Trichlorofluorometbane
75-69-4
U
0.500
0.0540
ug/L.
07.10.1410.31
U I
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
07.10.14 10.31
U I
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
07.10.1410.31
U 1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
07.10.1410.31
U 1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
07.10.1410.31
U 1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
106
%
65-134
07.10.1410.31
4-Bromofluorobenzene
460-00-4
105
%
60-148
07.10.14 10.31
Toluene-D8
2037-26-5
106
%
87-114
07.10.1410.31
Page 19 of 31 Final 1.000

QC Summary 488977 ~' n
• t eeu
Florida Testing Services. LLC
Terraquest Environmental Consultants, P.C.
Colliseum Shell
Analytical Method: TSS by SM2540D
Seq Number: 945410
Matrix:
Water
MB Sample Id: 945410-1-BLK
LCS Sample Id:
945410-1-BKS
LCSD Sample Id: 945410-1-BSD
MB Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Parameter Result Amount
Result %Rec
Result %Rec
Limit Date
Total Suspended Solids <3.50 100
95.0 95
96.0 96
80-120 1 10 mg/L 07.10.14 11:00
Analytical Method: TSS by SM2540D
Seq Number:
945410
Matrix:
Ground Water
Parent Sample Id:
488977-004
MD Sample Id:
488977-004 D
Parameter
Parent
MD
%RPD RPD Units Analysis Flag
Result
Result
Limit Date
Total Suspended Solids
7.00
7.00
0 10 mg/L 07.10.14 11:00
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
945515
Matrix:
Water
Date Prep: 07.12.14
MB Sample Id:
658251-1-BLK
LCS Sample Id:
658251-1-BKS
LCSD Sample Id: 658251-1-BSD
MB Spike
LCS LCS
LCSD LCSD
Limits %RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
1.02 102
1.02 102
80-120 0 20 mg/L 07.14.1413:31
Analytical Method: Lead by SW-846 6010C
Seq Number: 945515 Matrix: Water
Parent Sample Id: 488271-002 MD Sample Id: 488271-002 D
PParent MD
arameter
Result Result
Lead <0.00330 <0.00330
Prep Method: SW3010A
Date Prep: 07.12.14
%RPD RPD Units Analysis Flag
Limit Date
0 20 mg/L 07.14.1413:42 U
Analytical Method:
Lead by SW-846 6010C
Prep Method: SW3010A
Seq Number:
945515
Matrix:
Water
Date Prep: 07.12.14
Parent Sample Id:
488271-002
MS Sample Id:
488271-002 S
MSD Sample Id: 488271-002 SD
Parent Spike
MS MS
MSD MSD
Limits %RPD RPD Units Analysis Flag
Parameter
Result Amount
Result %Rec
Result %Rec
Limit Date
Lead
<0.00330 1.00
1.02 102
1.02 102
80-120 0 20 mg/L 07.14.1413:44
Page 20 of 31 Final 1.000

QC Summary 488977
Terraquest Environmental Consultants, P.C.
Colliseum
Shell
Analytical Method: VOCs by
GUMS by SM6200B
Prep Method:
SM620OB_PREP
Seq Number: 945325
Matrix:
Water
Date Prep:
07.10.14
MB Sample Id: 658162-1-BLK
LCS Sample Id:
658162-1-BKS
LCSD Sample Id: 658162-1-BSD
MB
Spike
LCS
LCS
LCSD
LCSD
Limits
%RPD
RPD
Units
Analysis
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
1,1,1,2-Tetrachloroethane
<0.180
25.0
27.4
110
26.4
106
75-127
4
20
ug/L
07.10.14 08:10
1,1,1-Trichloroethane
<0.0760
25.0
25.8
103
25.5
102
62-128
1
20
ug/L
07.10.14 08:10
1,1,2,2-Tetrachloroethane
<0.0700
25.0
27.1
108
26.7
107
77-129
1
20
ug/L
07.10.14 08:10
1,1,2-Trichloroethane
<0.113
25.0
26.9
108
25.9
104
86-120
4
20
ug/L
07.10.14 08:10
1,1-Dichloroethane
<0.121
25.0
25.4
102
25.0
100
82-114
2
20
ug/L
07.10.14 08:10
1,1-Dichloroethene
<0.104
25.0
26.7
107
25.7
103
73-123
4
22
ug/L
07.10.14 08:10
1, 1 -Dichloropropene
<0.0600
25.0
25.8
103
25.3
101
83-125
2
20
ug/L
07.10.14 08:10
1,2,3-Trichlorobenzene
<0.118
25.0
29.2
117
27.5
110
57-127
6
20
ug/L
07.10.14 08:10
1,2,3-Tiichloropropane
<0.138
25.0
26.7
107
29.0
116
79-118
8
20
ug/L
07.10.14 08:10
1,2,4-Trichlorobenzene
<0.0690
25.0
28.5
114
27.3
109
59-125
4
20
ug/L
07.10.14 08:10
1,2,4-Trimethylbenzene
<0.103
25.0
27.9
112
27.6
110
84-118
1
20
ug/L
07.10.14 08:10
1,2-Dibromoethane (EDB)
<0.180
25.0
27.1
108
26.4
106
83-126
3
20
ug/L
07.10.14 08:10
1,2-Dichlorobenzene
<0.0940
25.0
27.6
110
27.1
108
89-126
2
20
ug/L
07.10.14 08:10
1,2-Dichloroethane
<0.0900
25.0
25.7
103
25.0
100
56-133
3
20
ug/L
07.10.14 08:10
1,2-Dichloropropane
<0.122
25.0
25.3
101
24.5
98
79-127
3
20
ug/L
07.10.14 08:10
1,3,5-Trimethylbenzene
<0.0870
25.0
28.3
113
27.5
110
86-118
3
20
ug/L
07.10.14 08:10
1,3-Dichlorobenzene
<0.0980
25.0
27.6
110
27.5
110
90-126
0
20
ug/L
07.10.14 08:10
1,3-Dichloropropane
<0.133
25.0
26.4
106
25.5
102
85-121
3
20
ug/L
07.10.14 08:10
1,4-Dichlorobenzene
<0.0670
25.0
27.8
111
27.2
109
88-121
2
20
ug/L
07.10.14 08:10
2,2-Dichloropropane
<0.0970
25.0
27.4
110
28.2
113
76-126
3
20
ug/L
07.10.14 08:10
2-Butanone (MEK)
<0.378
50.0
63.7
127
50.8
102
66-133
23
20
ug/L
07.10.14 08:10
2-Chlorotoluene
<0.0880
25.0
27.8
111
27.2
109
80-128
2
20
ug/L
OTI0.1408:10
2-Hexanone
<0.352
50.0
67.5
135
53.9
108
70-130
22
20
ug/L
07.10.14 08:10
4-Chlorotoluene
<0.0900
25.0
27.6
110
27.3
109
82-130
1
20
ug/L
07.10.14 08:10
4-Isopropyltoluene
<0.0890
25.0
28.8
115
28.2
113
80-128
2
20
ug/L
07.10.14 08:10
4-Methyl-2-pentanone (MIBK)
<0.253
50.0
48.4
97
45.0
90
74-129
7
20
ug/L
07.10.14 08:10
Acetone
<0.352
50.0
84.8
170
60.6
121
51-143
33
21
ug/L
07.10.14 08:10
Benzene
<0.119
25.0
24.9
100
24.5
98
81-123
2
20
ug/L
07.10.14 08:10
Bromobenzene
<0.132
25.0
27.4
110
26.8
107
84-114
2
20
ug/L
07.10.14 08:10
Bromochloromethane
<0.112
25.0
26.1
104
25.4
102
89-127
3
20
ug/L
07.10.14 08:10
Br6modichloromethane
<0.124
25.0
25.7
103
25.3
101
70-129
2
20
ug/L
07.10.14 08:10
Bromoform
<0.159
25.0
28.8
115
28.1
112
73-140
2
20
ug/L
07.10.14 08:10
Bromomethane
<0.0970
25.0
28.3
113
27.8
111
53-143
2
20
ug/L
07.10.14 08:10.
Carbon tetrachloride
<0.0990
25.0
26.1
104
25.5
102
66-136
2
20
ug/L
07.10.14 08:10
Chlorobenzene
<0.105
25.0
26.6
106
26.1
104
88-118
2
20
ug/L
07.10.14 08:10
Chlorodibromomethane
<0.177
25.0
27.8
Ill
26.9
108
73-139
3
20
ug/L
07.10.14 08:10
Chloroethane
<0.0420
25.0
26.2
105
25.5
102
70-123
3
20
ug/L
07.10.14 08:10
Chloroform
<0.172
25.0
25.5
102
25.2
101
72-118
1
20
ug/L
07.10.14 08:10
Chloromethane
<0.0850
25.0
25.5
102
24.4
98
65-125
4
20
ug/L
07.10.14 08:10
cis-1,2-Dichloroethene
<0.114
25.0
25.7
103
24.7
99
85-125
4
20
ug/L
07.10.14 08:10
cis-1,3-Dichloropropene
<0.100
25.0
26.2
105
25.0
100
92-126
5
20
ug/L
07.10.14 08:10
Dichlorodifluoromethane
<0.0670
25.0
30.4
122
29.5
118
48-143
3
20
ug/L
07.10.14 08:10
Ethanol
<3.00
1000
1020
102
969
97
61-133
5
20
ug/L
07.10.14 08:10
Ethylbenzene
<0.0920
25.0
26.9
108
26.2
105
87-123
3
20
ug/L
07.10.14 08:10
Isopropyl ether
<0.0920
25.0
25.6
102
25.1
100
77-125
2
20
ug/L
07.10.14 08:10
Isopropylbenzene
<0.0980
25.0
27.7
ill
26.8
107
82-115
3
20
ug/L
07.10.14 08:10
Methyl tert-butyl ether (MTBE)
<0.169
50.0
51.3
103
49.7
99
53-149
3
20
ug/L
07.10.14 08:10
Methylene Chloride
<0.190
25.0
24.1
96
24.8
99
75-119
3
20
ug/L
07.10.14 08:10
Naphthalene
<0.0940
25.0
28.9
116
27.6
110
52-116
5
20
ug/L
07.10.14 08:10
n-Butylbenzene
<0.0600
25.0
29.9
120
29.2
117
83-130
2
20
ug/L
07.10.14 08:10
n-Propylbenzene
<0.0650
25.0
28.1
112
27.4
110
84-122
3
20
ug/L
07.10.14 08:10
sec-Butylbenzene
<0.0920
25.0
28.3
113
27.6
110
86-120
3
20
ug/L
07.10.14 08:10
Flag
F
HF
HF
Page 21 of 31 Final 1.000

s
LZMEMO
Florida Testing Services, LLC
QC Summary 488977
Terraquest Environmental Consultants, P.C.
Colliseum Shell
wA«
i 6; 1%
Analytical Method:
VOCs by GUMS by SM6200B
Prep Method:
SM620OB_PREP
Seq Number:
945325
Matrix:
Water
Date Prep:
07.10.14
MB Sample Id:
658162-1-BLK
LCS Sample
Id:
658162-1-BKS
LCSD Sample Id: 658162-1-BSD
MB
Spike
LCS
LCS
LCSD
LCSD
Limits %RPD RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Rec
Result
%Rec
Limit
Date
Styrene
<0.0740
25.0
27.5
110
26.9
108
85-123
2
20
ug/L
07.10.14 08:10
tert-Butylbenzene
<0.0890
25.0
27.9
112
27.1
108
79-126
3
20
ug/L
07.10.14 08:10
Tetrachloroethene (PCE)
<0.0540
25.0
27.5
110
27.0
108
64-131
2
20
ug/L
07.10.14 08:10
Toluene
<0.0570
25.0
26.8
107
26.2
105
89-116
2
20
ug/L
07.10.14 08:10
trans-1,2-Dichloroethene
<0.188
25.0
25.7
103
25.3
101
78-118
2
20
ug/L
07.10.14 08:10
trans-1,3-Dichloropropene
<0.110
25.0
28.2
113
27.4
110
86-127
3
20
ug/L
07.10.14 08:10
Trichloroethene
<0.139
25.0
25.4
102
25.5
102
82-119
0
20
ug/L
07.10.14 08:10
Trichlorofluoromethane
<0.0540
25.0
27.8
ill
27.8
111
46-144
0
20
ug/L
07.10.14 08:10
Vinyl Acetate
<0.720
25.0
25.8
103
24.9
100
58-141
4
20
ug/L
07.10.14 08:10
Vinyl Chloride
<0.0810
25.0
26.1
104
24.9
100
76-122
5
20
ug/L
07.10.14 08:10
m,p-Xylenes
<0.176
50.0
54.0
108
52.3
105
90-125
3
20
ug/L
07.10.14 08:10
o-Xylene
<0.122
25.0
26.8
107
26.6
106
86-119
1
20
ug/L
07.10.14 08:10
MB
MB
LCS
LCS
LCSD
LCSD
Limits Units
Analysis
Surrogate
%Rec
Flag
%Rec
Flag
%Rec Rec
Flag
Date
1,2-Dichloroethane-D4
102
103
102
65-134
%
07.10.14 08:10
4-Bromofluorobenzene
103
100
100
70-130
%
07.10.14 08:10
Toluene-D8
107
105
104
87-114
%
07.10.14 08:10
Page 22 of 31 Final 1.000

QC Summary
488977
Pli,
Vrje
rau
BQx.RSg .m....a...,.,,.
Florida Testing Services, LLC
Terraquest
Environmental Consultants, P.C.
Colliseum
Shell
Analytical Method: VOCs by GUMS by SM6200B
Prep Method:
SM6200B_PREP
Seq Number: 945325
Matrix:
Ground Water
Date Prep:
07.10.14
Parent Sample Id: 488977-004
MS Sample Id:
488977-004 S
MSD Sample Id: 488977-004 SD
Parent
Spike
MS
MS
MSD
MSD
Limits
%RPD
RPD
Units
Analysis Flag
Parameter
Result
Amount
Result
%Ree
Result
%Ree
Limit
Date
1, 1, 1,2-Tetrachloroethane
<0.180
25.0
26.4
106
25.5
102
76-126
3
20
ug/L
07.10.14 13:35
1, 1, 1 -Trichloroethane
<0.0760
25.0
25.1
100
23.8
95
63-128
5
20
ug/L
07.10.14 13:35
1,1,2,2-Tetrachloroethane
<0.0700
25.0
26.5
106
27.1
108
79-133
2
20
ug/L
07.10.1413:35
1,1,2-Trichloroethane
<0.113
25.0
26.8
107
26.3
105
82-126
2
20
ug/L
07.10.14 13:35
1,1-Dichloroethane
<0.121
25.0
24.9
100
23.9
96
77-120
4
20
ug/L
07.10.14 13:35
1,1-Dichloroethene
<0.104
25.0
25.8
103
24.0
96
67-123
7
22
ug/L
07.10.14 13:35
1,1-Dichloropropene
<0.0600
25.0
25.2
101
23.9
96
76-126
5
20
ug/L
07.10.14 13:35
1,2,3-Trichlorobenzene
<0.118
25.0
28.3
113
27.3
109
41-136
4
20
ug/L
07.10.14 13:35
1,2,3-Trichloropropane
<0.138
25.0
28.2
113
26.6
106
77-125
6
20
ug/L
07.10.14 13:35
1,2,4-Trichlorobenzene
<0.0690
25.0
27.5
110
26.2
105 .
41-132
5
20
ug/L
07.10.14 13:35
1,2,4-Trimethylbenzene
<0.103
25.0
26.6
106
25.6
102
53-141
4
20
ug/L
07.10.14 13:35
1,2-Dibromoethane (EDB)
<0.180
25.0
26.9
108
26.5
106
82-130
1
20
ug/L
07.10.14 13:35
1,2-Dichlorobenzene
<0.0940
25.0
27.1
108
26.0
104
83-128
4
20
ug/L
07.10.1413:35
1,2-Dichloroethane
<0.0900
25.0
25.2
101
24.8
99
59-134
2
20
ug/L
07.10.14 13:35
1,2-Dichloropropane
<0.122
25.0
25.1
100
24.2
97
79-125
4
20
ug/L
07.10.14 13:35
1,3,5-Trimethylbenzene
<0.0870
25.0
26.8
107
25.5
102
69-125
5
20
ug/L
07.10.14 13:35
1,3-Dichlorobenzene
<0.0980
25.0
26.6
106
25.6
102
83-126
4
20
ug/L
07.10.14 13:35
1,3-Dichloropropane
<0.133
25.0
26.0
104
26.0
104
85-124
0
20
ug/L
07.10.14 13:35
1,4-Dichlorobenzene
<0.0670
25.0
26.7
107
25.5
102
82-121
5
20
ug/L
07.10.14 13:35
2,2-Dichloropropane
<0.0970
25.0
26.3
105
23.5
94
56-122
11
20
ug/L
07.10.14 13:35
2-Butanone (MEK)
<0.378
50.0
49.7
99
51.4
103
66-136
3
20
ug/L
07.10.14 13:35
2-Chlorotoluene
<0.0880
25.0
26.1
104
24.8
99
73-129
5
20
ug/L
07.10.14 13:35
2-Hexanone
<0.352
50.0
53.6
107
54.3
109
63-140
1
20
ug/L
07.10.14 13:35
4-Chlorotoluene
<0.0900
25.0
26.3
105
25.1
100
76-129
5
20
ug/L
07.10.14 13:35
4-Isopropyltoluene
<0.0890
25.0
27.2
109
25.9
104
73-126
5
20
ug/L
07.10.14 13:35
4-Methyl-2-pentanone (MIBK)
<0.253
50.0
47.6
95
49.2
98
71-140
3
20
ug/L
07.10.14 13:35
Acetone
<0.352
50.0
50.1
100
50.2
100
47-138
0
21
ug/L
07.10.14 13:35
Benzene
<0.119
25.0
24.7
99
23.5
94
70-135
5
20
ug/1-
07.10.14 13:35
Bromobenzene
<0.132
25.0
25.9
104
25.1
100
76-120
3
20
ug/1-
07.10.14 13:35
Bromochloromethane
<0.112
25.0
25.9
104
25.2
101
83-132
3
20
ug/L
07.10.14 13:35
Bromodichloromethane
<0.124
25.0
25.4
102
24.7
99
66-132
3
20
ug/L
07.10.14 13:35
Bromoform
<0.159
25.0
27.7
111
27.5
110
63-143
1
20
ug/L
07.10.14 13:35
Bromomethane
<0.0970
25.0
27.6
110
26.8
107
60-134
3
20
ug/L
07.10.14 13:35
Carbon tetrachloride
<0.0990
25.0
24.9
100
23.7
95
59-139
5
20
ug/L
07.10.14 13:35
Chlorobenzene
<0.105
25.0
25.9
104
24.9
100
83-120
4
20
ug/L
07.10.14 13:35
Chlorodibromomethane
<0.177
25.0
27.3
109
26.5
106
68-140
3
20
ug/L
07.10.14 13:35
Chloroethane
<0.0420
25.0
25.9
104
24.9
100
67-125
4
20
ug/L
07.10.14 13:35
Chloroform
<0.172
25.0
25.0
100
22.6
90
72-120
10
20
ug/L
07.10.1413:35
Chloromethane
<0.0850
25.0
28.3
113
26.2
105
59-128
8
20
ug/L
07.10.14 13:35
cis-1,2-Dichloroethene
<0.114
25.0
24.7
99
24.3
97
80-125
2
20
ug/L
07.10.14 13:35
cis-1,3-Dichloropropene
<0.100
25.0
25.7
103
24.9
100
74-122
3
20
ug/L
07.10.14 13:35
Dichlorodifluoromethane
<0.0670
25.0
32.3
129
29.9
120
48-138
8
20
ug/L
07.10.14 13:35
Ethanol
<3.00
1000
896
90
902
90
55-140
1
20
ug/L
07.10.14 13:35
Ethylbenzene
<0.0920
25.0
26.1
104
24.7
99
70-140
6
20
ug/L
07.10.14 13:35
Isopropyl ether
<0.0920
25.0
25.5
102
25.1
100
70-132
2
20
ug/L
07.10.14 13:35
Isopropylbenzene
<0.0980
25.0
26.5
106
25.1
100
75-117
5
20
ug/L
07.10.14 13:35
Methyl tert-butyl ether (MTBE)
<0.169
50.0
49.4
99
50.3
101
51-155
2
20
ug/L
07.10.14 13:35
Methylene Chloride
0.770
25.0
24.4
95
23.6
91
71-126
3
20
ug/L
07.10.14 13:35
Naphthalene
<0.0940
25.0
28.8
115
28.2
113
34-135
2
20
ug/L
07.10.14 13:35
n-Butylbenzene
<0.0600
25.0
28.6
114
26.5
106
73-128
8
20
ug/L
07.10.14 13:35
n-Propylbenzene
<0.0650
25.0
26.5
106
25.0
100
75-125
6
20
ug/L
07.10.14 13:35
sec-Butylbenzene
<0.0920
25.0
27.1
108
25.3
101
77-122
7
20
ug/L
07.10.14 13:35
Page 23 of 31 Final 1.000

QC Summary 488977
1�s
LU, Lie
r�u
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C.
Colliseum Shell
Analytical Method: VOCs by GUMS by SM6200B Prep Method: SM6200B_PREP
Seq Number: 945325 Matrix: Ground Water Date Prep: 07.10.14
Parent Sample Id: 488977-004 MS Sample Id: 488977-004 S MSD Sample Id: 488977-004 SD
Parent Spike MS MS MSD MSD Limits %RPD RPD Units Analysis Flag
Parameter Result Amount Result %Rec Result %Rec Limit Date
Styrene <0.0740 25.0 26.4 106 25.2 101 54-137 5 20 ug/L 07.10.14 13:35
tert-Butylbenzene <0.0890 25.0 26.6 106 25.0 100 74-124 6 20 ug/L 07.10,1413:35
Tetrachloroethene (PCE) <0.0540 25.0 26.6 106 25.1 100 57-130 6 20 ug/L 07.10.14 13:35
Toluene <0.0570 25.0 26.3 105 24.9 100 81-125 5 20 ug/L 07.10.14 13:35
trans-1,2-Dichloroethene <0.188 25.0 25.3 101 23.8 95 69-122 6 20 ug/L 07.10.14 13:35
trans-1,3-Dichloropropene <0.110 25.0 27.6 110 26.9 108 73-129 3 20 ug/L 07.10.14 13:35
Trichloroethene <0.139 25.0 24.9 100 23.4 94 73-124 6 20 ug/L 07.10.14 13:35
Trichlorofluoromethane <0.0540 25.0 27.5 110 25.9 104 49-139 6 20 ug/L 07.10.14 13:35
Vinyl Acetate <0.720 25.0 25.4 102 24.9 100 57-134 2 20 ug/L 07.10.14 13:35
Vinyl Chloride <0.0810 25.0 27.4 110 25.1 100 70-121 9 20 ug/1- 07.10.14 13:35
m,p-Xylenes <0.176 50.0 52.4 105 49.7 99 65-151 5 20 ug/L 07.10.14 13:35
o-Xylene <0.122 25.0 26.3 105 25.0 100 58-148 5 20 ug/L 07.10.14 13:35
g MS MS MSD MSD Limits Units Analysis
Surrogate %Rec Flag %Rec Flag Date
1,2-Dichloroethane-D4 103 103 65-134 % 07.10.14 13:35
4-Bromofluorobenzene 98 98 60-148 % 07.10.14 13:35
Toluene-D8 104 107 87-114 % 07.10.14 13:35
Page 24 of 31 Final 1.000

Blank Summary
488977
�' t
�BQRaP'
off..
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: 658162-1-BLK
Matrix: WATER
Lab Sample Id: 658162-1-BLK
Analytical Method: VOCs by GUMS by SM6200B
Prep Method: SM620OB_PREP
Tech: LIH
Analyst: MLA
Date
Prep: 07.10.14 06:45
Seq Number: 945325
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
07.10.14 13:02
U
I
1, 1, 1 -Trichloro ethane
71-55-6
U
0.500
0.0760
ug/L
07.10.14 13:02
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
07.10.14 13:02
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
07.10.14 13:02
U
I
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
07.10.14 13:02
U
I
I,I-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
07.10.14 13:02
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
07.10.14 13:02
U
I
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
07.10.14 13:02
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
07.10.14 13:02
U
I
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
07.10.14 13:02
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
07.10.14 13:02
U
I
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
07.10.14 13:02
U
I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
07.10.14 13:02
U
I
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
07.10.14 13:02
U
I
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
07.10.14 13:02
U
I
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
07.10.14 13:02
U
I
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
07.10.14 13:02
U
I
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
07.10.14 13:02
U
I
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
07.10.14 13:02
. U
I
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
07.10.14 13:02
U
I
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
07.10.14 13:02
U
I
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
07.10.14 13:02
U
I
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
07.10.14 13:02
U
I
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
07.10.14 13:02
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
07.10.14 13:02
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
07.10.14 13:02
U
I
Acetone
67-64-1
U
2.00
0.352
ug/L
07.10.14 13:02
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
07.10.14 13:02
U
I
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
07.10.14 13:02
U
I
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
07.10.14 13:02
U
I
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
07.10.14 13:02
U
I
Bromoform
75-25-2
U
2.00
0.159
ug/L
07.10.14 13:02
U
I
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
07.10.14 13:02
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
07.10.14 13:02
U
I
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
07.10.14 13:02
U
1
Chlorodibromomethane
124-48-I
U
0.500
0.177
ug/L
07.10.14 13:02
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
07.10.14 13:02
U
I
Chloroform
67-66-3
U
0.500
0.172
ug/L
07.10.14 13:02
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
07.10.14 13:02
U
1
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
07.10.14 13:02
U
1
Page 25 of 31 Final 1.000

Or/'PUMPO
FCC
Blank Summary 488977
rarw
Florida Testing Services, LLC
Sample Id: 658162-1-BLK
Lab Sample Id: 658162-1-BLK
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Matrix: WATER
Analytical Method: VOCs by GC/MS by SM6200B
Prep Method: SM6200B_PREP
Tech: LIH
Analyst: MLA
Date Prep: 07.10.14 06:45
Seq Number: 945325
Parameter
Cas Number
Result
RL MDL
Units
Analysis
Flag
Dil
Date
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
07.10.14 13:02
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
07.10.14 13:02
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
07.10.14 13:02
U
1
Ethylbenzene
100414
U
0.500
0.0920
ug/L
07.10.14 13:02
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
07.10.14 13:02
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
07.10.14 13:02
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
07.10.14 13:02
U
I
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
07.10.14 13:02
U
I
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
07.10.14 13:02
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
07.10.14 13:02
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
07.10.14 13:02
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
07.10.14 13:02
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
07.10.14 13:02
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
07.10.14 13:02
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L,
07.10.14 13:02
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
07.10.14 13:02
U
I
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
07.10.14 13:02
U
I
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
07.10.14 13:02
U
I
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
07.10.14 13:02
U
I
Trichlorofluoromethane
75-69-4
U
0.500
0,0540
ug/L
07.10.14 13:02
U
1
Vinyl Acetate
108-054
U
I.00
0.720
ug/L
07.10.14 13:02
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
07.10.14 13:02
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
07.10.14 13:02
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
07.10.14 13:02
U
1
Page 26 of 31 Final 1.000

XGNC
Sample Id: 658251-1-BLK
Lab Sample Id: 658251-1-BLK
Blank Summary 488977
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Matrix: WATER
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR
Analyst: 4150 Date Prep: 07.12.14 13:01
Seq Number: 945515
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Lead 7439-92-1 U 0.0100 0.00330 mg/L 07.14.1413:29 U 1
Page 27 of 31 Final 1.000

• Blank Summary 488977 L*'
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Colliseum Shell
Sample Id: 945410-1-BLK Matrix: WATER
Lab Sample Id: 945410-1-BLK
Analytical Method: TSS by SM2540D Prep Method:
Tech: NSI
Analyst: NSI Date Prep:
Seq Number: 945410
Parameter Cas Number Result RL MDL Units Analysis Flag Dil
Date
Total Suspended Solids U 4.00 3.50 mg/L 07.10.14 11:00 U 1
Page 28 of 31 Final 1.000

O
W
?XEMCO CHAIN OF CUSTODY
ARATnRIES
Page _ of _
FED -EX / UPS: Tracking #
Bottle Order Control #
6017 Financial Drive, Norcross, GA 30071 (770449-8800)
Xenco Quote #
Xenco Work Order#
.
4143 Greenbriar Dr., Stafford, TX 77477 (281-240-4200)
�
9701 Harry Hines Blvd, Dallas, TX 75220 (214-902-0300)
3
12600 West i ZO East, Odessa, TX 79765 432-563-1800
Information n1A .f s' �' ! •R s Invoice Information
!1nf "l i;:rt lPL4ii. rf�Nl '!it
i. , ilk =11
IHiIgrli.e`
Requested
Analyses
00
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a es
GW Ground er
nkingW to
DW =Drinking Water
Oent! Re rtin
Company Name ProjectNumber(101.
Terraquest Environmental Consultants, P.C.6105
SW = Surface water
OW=Oceanlsea Water
Project Contact E-Mall
Project Name: (stro0cross road, location)
PL - Product Liquid
WIN - waste water
Address
W =Wipe
100 E. Ruffin Street
S = solUsed (solid
SL=sludge
Purchase Order# (if required)
(%% 50
city: Mebane, NC 27302
(Q
0 = 011
Phone: [phone] Fax: [phone]
Report & Invoice to: Megan Webster / mwebster@terraquestpc-corn
Sampiews Name / j, Samplors's Signature
j
Collection
Number of oreserved betties
Line # Field ID ! Point of Collection
# of
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Contract TATNeed Results: Date Mine � Level
Fl UST(state?)
10 Day TAT
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ED SC DEHEC
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3 Day EMERGENCY
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HOLD TRIP BLANKS PENDING HITS
1 Day EMERGENCY
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Project I Client specific MS I MSD selected
Same Day TAT
Level Results & Standard QC
Special Detection limits needed to achieve
TAT Starts on day recieved at Lab if received by Noon
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send Confirmation chain aka tog an
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SAMPLE CUSTODY MUST BE DOCUMENTED BELO IM AMPLE CHANGE POSSESSION. INCLUDING COURIER DELIVERY �tgi ;t!;r x;?i'j>q!` ' • 4i ;}I'r.i! irTj"" '7':'i'5:aDfit7Sij[iii
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XENCO Laboratories
• Prelogin/Nonconformance Report- Sample Log -In
Florida Testing Services, LLC
Client: Terraquest Environmental Consultants, F Acceptable Temperature Range: 0 - 6 degC
Date/ Time Received: 07/09/2014 11:05:00 AM Air and Metal samples Acceptable Range: Ambient
Work Order #: 488977 Temperature Measuring device used :
Sample Receipt Checklist Comments
#1 *Temperature of cooler(s)?
2.6
#2 *Shipping container in good condition?
Yes
#3 *Samples received on ice?
Yes
#4 *Custody Seals intact on shipping container/ cooler?
N/A
#5 Custody Seals intact on sample bottles?
N/A
#6 *Custody Seals Signed and dated?
N/A
#7 *Chain of Custody present?
Yes
#8 Sample instructions complete on Chain of Custody?
Yes
#9 Any missing/extra samples?
No
#10 Chain of Custody signed when relinquished/ received?
Yes
#11 Chain of Custody agrees with sample label(s)?
Yes
#12 Container label(s) legible and intact?
Yes
#13 Sample matrix/ properties agree with Chain of Custody?
Yes
#14 Samples in proper container/ bottle?
Yes
#15 Samples properly preserved?
Yes
#16 Sample container(s) intact?
Yes
#17 Sufficient sample amount for indicated test(s)?
Yes
#18 All samples received within hold time?
Yes
#19 Subcontract of sample(s)?
No
#20 VOC samples have zero headspace (less than 1/4 inch bubble)?
Yes
#21 <2 for all samples preserved with HNO3,HCL, H2SO4?
Yes
#22 >10 for all samples preserved with NaAs02+NaOH, ZnAc+NaOH?
N/A
* Must be completed for after-hours delivery of samples prior to placing in the refrigerator
Analyst: JDR PH Device/Lot#: 016662-2
Checklist completed by: I& '" dy
J. Derek Rounsley
Checklist reviewed by: th'a)aj—J
Eben Buchanan
Date: 07/09/2014
Date: 07109/2014
r�u
Page 31 of 31 Final 1.000