NC0088919_Toxicity Reduction Evaluation Progress Report_20140130

TEUest`. RECEIV
— N. C. D E®
t. epk op ENR
- ����� FEB .... -_
ENVIRONMENTAL CONSULTANTS, P.C. - �. 6 `o •'�01 r
A V"STON-SALEy REGIONAL OFFICE
january30, 2014
W: Corey Basinger - Regional Supervisor
Surface Water Protection Section - Winston-Salem Regional Office
Division of Water Quality
585 Waughtowri Street
Winston-Salem, NC 27107-2241
Re: Toxicity Reduction Evaluation,Progress Report
Former. Coliseum Shell — Quality -Oil Company, LLC'
NPDES Permit No..N00088919
NCDWM-UST Incident No.: 15260
Terraquest-Project No.: 01195
Dear.Mr: Basinger
On behalf of the permitee, Quality Oil Company, LLC, Ter.raquest.Environmental _Consultants, P.C..
hereby submits this Toxicity Reduction Evaluation Progress Report in accordance with the Special
Order. by Consent EMC SOC WQS-12=004.
Section 2 (a) 2) of the SOC states the following:
"scope. of the THE work . ,should ` consider but is not limited to: effluent
characterization/identification/confirmation: of suspected toxicants,, evaluation..of'pgint source
contributions to toxicity, pretreatment bench scale freatability studies,, toxicity source, reduction
Strategies"
As required, consideration to each of those items throughout the latest testing quarter that
ended in'December per Sectiori 2 (a) 3) of the SOC follows: ;
effluent characterization/identification/confirmation of suspected toxicants:
During the October, November, December. 2013 discharge` quarter, .weekly inspections of the, ;
subject treatment system were performed by either. the OR.0 or backup ORC for routine
maintenance -and oversight as required by the permit and also to. investigate the source or -
situation that .might;be causing. the- toxicity. to Ceriodaphnia, Dubia. "No finite .toxicant was
identified throughout the period. Routine maintenance activities included the replacement' of
polyethylene bag filters, replacement of carbon filtration media; and a. sludge/sediment removal
event via vacuum truck: Site visits were' made on.10/7, 10/14,
10/21 10/29 11/4,:11/11, 11/18,
11/25, 12/2, 12/9, 12/16, 12/26, and 12/30: Associated checklists are enclosed.
100 E. Ruffin Street - Mebane, -North Carolina'27302
Telephone [phone].- Facsimile [phone]
wWwAerraquestpp,com

Paget
C. Basinger'
1/30/14
Monthly system samples were -collected from the -treatment system influent; "after air stripper,
after,first carbon filter, and effluent port locations.: Those samples:were'.submitted to an NG-
:certified'laboratory for analysis of the, VOCs that are the subject of both the'site's remediation
and of the-TRE.` As shown on the attached Table' 1-Summary of Groundwater Sampling Results,.
no toxicants'_are apparent. The analytical results are., similar to hisfcirical,'resuIts. :Historical .
analytical datash,eets 'for influent; after air stripper, after first.carbon, and effluent ports _are
enclosed along with,the lab: reports -for October,'November,,an•d December. 2013 for. "reference:
evaluation of pointsource contributions;to toxicity:'
' Terraquest has. reviewed possible'contributorsof toxicants at;this site:; No new.information is'
available and'the'toxicant remains undefined. As',noted, recent analytical data'mimics historical
results:. .
;{pretreatment bench scale tre't6biliiy'siudies: '
Consideration was�provided'to bench sale treatability studies;, however, at this time there -are no
:,suspected toxicants nor have Terraquest,;Dwb or several"third parties been able ;to discern a
way to, discover the'toxi.cant: Study of the contaminants involved at the site will continue:.
toxicity, source. red&ction`strateWe5:
Consideration -to toxicity reductiori was' given,. however; the. toxicity ,source .has hot been
identified:'. Teriaquest recommends.continue'd remediatio'n 'of the subject contaminant -plume
while attention is. paid to possible sources of the toxicity:
To date; the toxicant to C. Dubia remains unclear..:.In compliance with the SOC' Terraquest' has
.considered the items set,forth in Section'2,(a) 2) of the; SOC,� however, those considerations have
not produced a solution -to the toxicity.at this'time.,,,The'.evaluation'of toxicity Will continue:

TERRA uest
IM
ENVIRONMENTAL CON VLTANTS. P.C.
Inspector �; P.C.
rs
Coliseum shell System Inspection Checklist
rya ity'' Oil
Date of Inspection
across sep elem.
on LRP
before filter -
after.filter
Vacuum pressure
vadose sparge
scfm
Totalizer Reading
(`
/ 77 -000
gallons
�(l6
LRP run hours
hours
AST blower run hours - C� ¢
I �/� 7
hours
Control Panel
OK `�
Comments:
Temp
/l deg. F
Liquid Ring Pump
OK
added coolant Change coolant
./U0
/
Comments:
OWS Condition
OK N
OWS transfer pump
OK T
Comments:
/
AST Blower Operation
OK C
Comments:
ASTtransferpump
OK
Comments:
Bag filters dirty? Lots
Some Mini None Didn't check
Changed bag
Yes/(5)
Changed sand
Yes / doo
# bags
/
Comments &Observations:
k
Iry 41 -

TERRA u_est
Wan,
ENVIRONMENTALCONSULT NTS.P.O.
GLK- G�-�+_iG-f
Inspector
Coliseum Shell System Inspection Checklist
uality tail
�
Date of InspectionZ�."Z/A
aacrr�/o�ss sep elem.
on LRP '�@
beforre filter." '
afteer.filter
Vacuum pressure
(/
vadose spa rge
scfm
�/ gallons
Totalizer Reading
�Z
iOV
% / hours
LRP run hours
AST blower run hours
I / S 3 hours
Control Panel
OK Comments:
Liquid Ring Pump
OK Temp
G� deg. F ��'�✓
,,ll et��
added coolant Change coolant
,v
Comments:
OWS Condition
OK
i
OWStransferpump
OK Comments:
✓ Comments:
AST Blower Operation
OK
Comments:
AST transfer pump
OK
Bag filters dirty? Lots
Some Minimal None idn'
Changed bag
Yes /y
Changed sand
Yes /(9
# bags
Comments & Observations:
W �i/' NG� dtv /Uty Z. 1%-1
C"(Gt �c� C? /�fi/'y�Y r>> ( 'r--/c�cy� !� �'�•uprn.�,Jrr. �
L�

TERRA uest
ENVIRONMENTAL CONSULTANTS. P.G.
Inspector
Coliseum Shell System Inspection Checklist
ality Oi-I
Date of Inspection —
across sep el�e+m�
on LRP
beforefilter
afterfilte.r
CS �- 6c"u/
-- Z_'
Z�
-
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changedsand
Comments & Observations:
scfm
f / gallons
73 /A _ ours
c / -7d hours
OK ✓ Comments:
OK Temp
added coolant
OK
OK��
OK �G
OK
Some Minimal None
Yes / 0
Yes / I0
Change coolant �,ce-6
id chcheck
Comments:
Comments:
Comments:
Comments:
! deg. F
# bags
C4a G e ( Cl
--� r� c `� Gw ,L �S .Sec �' � dw.l r �s %/i�✓�
q Tr
SLI'+q &c/CWr 17r-

TERRA uest
ENVIRONMENTAL CONSULTANTS, P.C.
Inspector"
r
Coliseum Shell System Inspection Checklist
uslity 0iL
Date of Inspection 6 9i /3
Vacuum pressure
across sep elem.:
(/%''Z e
on LRP
before filter
after.filter
vadosesparge
sdrn
Totalizer Reading
J J / �DUd gallons
LRP run hours
! LyI �J hours
AST blower run hours
/7
P t� ! hours
Control Panel
OK II Comments:
Liquid Ring Pump
OKA7 Temp deg. F
0,
added coolant Change coolant
OWS Condition
OKV, Comments:
OWS transfer pump
OK Comments:
AST Blower Operation
OK Comments:
ASTtransfer pump
OK_)�_ Comments:.
Bag filters dirty? Lots
Some Minimal one Didn't check
Changed bag
YesZV
Yes/� # bags
Changed sand
_
Comments & Observations:
/J4< Z—r5 Dl����°. ltict S®eyrL
U ' 6

TERRA P.G. uest
ENVIRONMENTAL CONSULTANTS.
��
Inspector 111'trtr�
Coliseum Shell System Inspection Checklist
uslity Oi l
Date of Inspection dq �rJ
across sep elem.
on LRP
before filter
after filter
Vacuum pressure
v ,—
2,0, jr-,
Z6
L�
vadosesparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
ASTtransfer pump
Bag filters dirty? Lots
Changed bag
Changedsand
Comments & Observations:
scfm
I P40®cl
gallons
yr �� hours
15 O� Z- hours
OK Comments:
OK Temp G(0 deg. F
added coolant �)'`"" t Change coolant .4jo
OK V/ Comments: r/ol ` r��z` s10/ w � � �O�Jro 111'r'
OK / Comments:
OK ✓ f Comments:
OK V 1 ��Comments:
Some Minimal None Didn't check
Yes / No
Yes / # bags
r'if ff
� I
5vC%G a,1 40113 V r� 4-A/K
S,w(lej 5ys4»,
77'6(

TERRAC Ues t
ENVIRONrArNTALLCCONSULTANTS, P.C.
Inspector )Lt OlLK' rar-dl j
Coliseum Shell System inspection Checklist
alit / 0i.1
Date of inspection
across sep elem.
on LRP
before filter
afterfilter,
G2Cev
- ��
—Z 2
,r
�
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag �.
Changedsand
Comments & Observations:
scfm
0" gallons
�! (3 hours
0 hours
OK ✓ Comments:
OK Temp
/(0 Y deg. F 6-;4- C&i1
added coolant i ei5 Change coolant A
OK >� Comments:
OK Comments:
OK Comments:
OK Comments:
Some Minimal None Didn't check %
es No fiU�fS�G� SCE f� jf l2dZ�.Sih �j S
Yes /9 # bags
l L iJ C�li/?7/l4 (� [ •rd �'`e O id CO: tAf �SSC3
C9a le SC/ r' f Ift T% %l d' o%4
de c motor �'j y ��. S � t i rc L`C(c
It J � I a
Qcoai����it) ( il ow
MTV ct. {! w 11 I _
,ac
Pr

TERRA ue��t
=-
ENVIRONM19ENTAL CCN¢ TANTS, P.C.
Inspector
Coliseum Shell System Inspection Checklist
taality Oil
Date of Inspection " / � e' " -
across sep elem.on LRP before filter afterfilter
Vacuum pressure
vadose spa rge
scfm
�oo
Totalizer Reading
/3Y,,
gallons
hours
LRP run hours
AST blower run hours
G�}
A; 067 ' /
hours
Control Panel
OK
Comments:
�
Liquid Ring Pump 66z✓
A CXOSS S Alf 4 (OK
Temp
added coolant i( (1j Change coolant ^ Vo
�
OWS Condition—' � �' �`
� OK
Comments:
OK C� d
Comments:
OWS transfer pump J��
f h„57.
/
AST Blower Operation
OK
Comments:
AST transfer pump
OK
Comments:
Bag filters dirty? Lots
Some Minimal None (El dn'tc
Changed bag
Yes/
Changedsand
Yes/0
Comments & Observations:
/,(/l/n
l S deg. F
# bags
cq L2,7 to ac
(P5cl (V �teIf
Je S
op yam© AA
Q�
r % % v

_nest
sm
ENVIRONMENTAL CONSULTANTS, RC.
_ Inspector AV
Coliseum Shell System Inspection Checklist
u sl I ity►I' Co i l
i 9
Date of Inspection11
across sep elem: on LRP before filter. afterfilter
Vacuum pressure an
vadosesparge
sdrn
I b�� 700
gallons
Totalizer Reading
J
hours
LRP run hours
�2�7/�/
3 b O
hours
AST blower run hours
Control Panel
OK %/
Comments:
OK-Y-101
Templ
—deg. F
Liquid Ring Pump
A
b
added coolant O Change coolant
I �
OWS Condition
OK�
Comments:
OWS transfer pump
OK,
Comments:
AST BI ower Operati on
OK
Comments:
AST transfer pump
OK _%/
Comments:
Bag filtersdirtV? Lots
Some Minimal None Didn't check
Changed bag
Yes No
Changed sand
Ye No
#bags
Comments & Observations:
D
t

TERRA ues
ENVIRONMENTAL CONSULTANTS, P.C.
Inspector /;,-, "-)
Coliseum Shell System Inspection Checklist
utility Oil
Date of Inspection
across sepelem.
onnLRP-
before filter
after filter
Vacuum pressure
v e ee4)
j�
, "z ! !
— -0 �' r
— Z / J
AST sf
vadosesparge
sdrn
�, 66Y/y/�
o
Totalizer Reading
gallons
-77(�
hours
LRP run hours
/
� ��
hours
AST blower run hours
( / /
Control Panel
OK
Comments:
Liquid Ring Pump 61
/ p %
(e/e l /�"
OK
Temp
added coolant
/i.0 Change coolant
f16
OWS Condition
OK_Z
Comments:
OWS transfer pump
OK
Comments:
AST Blower Operation
OK
Comments:
OK
Comments:
tran er pump
Bag filters dirty? Lots Some Minimal None
Changed bag Yes/ o
Changedsand Yes o
Comments & Observations:
idn't check
/I I,"7 deg. F
# bags

TERRA uest
ENVIRONMENTAL ONSVLTANTSP.G.
Inspector t�
Coliseum Shell System Inspection Checklist
uWity 01111
Date of Inspection ' Z' � A
across sepelem.
on LRP
beforefilter
afterfilter
V'l� ss-C—ev
'- L z.
" Z z'
I Z t
Vacuum pressure
Z elegy
vadose sparge
scfm
/� gallons
Totalizer Reading
ry 6
LRP run hours
i "' _ hours
6 3 hours
I/
AST blower run hours
L
Control Panel
OK " Comments:
Liquid Ring Pump
OK ✓ Temp
�6 Z deg. F
added coolant b Change coolant �6
/
Comments:
OWS Condition
OK
OWS transfer pump
OK Comments:
AST Blower Operation
— ZGt( as uA OK � Comments:
OK ✓ Comments:.
AST transfer pump
Bag filters dirty? Lots Some Minima jNQone Didn't check
Changed bag / / Y& / No
Changed sand Yes / J0 # bags
Comments & Observations:
._ Q r L !� GC �� �y(I yr O r'J 'Y` i ✓ �( 'S Q 1 ��`d r'�NA'�
•� C 40a;11
G.V. /i"r-
of J w� 8 ��f l , Z AL',?-(
I -Lon ft a VVAV otr.?I 4^Iart—L
t- .&MIJ &&� (to
< < pS -
0,l o
�r ra i (w ` ��
J
�r
III�U i'0 W c as �,c r � � • ` 4r,

Coliseum Shell System Inspection Checklist
TERRA uest
ENVIRONMENTAL CONSULTANTS, P.G.
Inspector All
+uality Oil
Date of Inspection 1Z/' 6 / 5
ac�osssepelem.,
'66LRP
beforefiltEf"""
aft6Ffilf4
Vacuum pressure
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
scfm a a
-7jogallons
-7.c7 r� - % hours
161 84-f . s' hours
OK Comments:
Liquid Ring Pump besi-'a;/ A C11) p 13Z9' 9 R--r ial-e'61 K
OWS Condition
OWS transfer pump
AST Blower Operation /
AST transfer pump `] ,I
Temp 166 deg. F
added coolant
Change coolant J�
OK
Comments:
OK /
Comments:
OK y
Comments:
OK
Comments:
Bag filters dirty? Lots Some Minimal None Did'nftcfi�ek
Changed bag Yes/ Flo
Changed sand Yes # bags
Comments&Observations: 4Af ku++tr&'- S S0 o/.
r�lllr� > • -14
jaxle,
S�lt r_ F- t) J (9 w �/uG�L C/, Gt I��✓ ff a2 0l� `G` f sLl�✓ (. �/� /�✓ Z)

TERRA uest
BSI
ENVIRONMENTAL CONSULTANTS, P.C.1
Inspector 4���1�f
Coliseum Shell System Inspection Checklist
uality° Oil
MMENe J
Date of Inspection / /--1- 641
accrross—sepeIi— `:'
ohLRP'.' '. `"
before filter
afterfilter,
Vacuum pressure
L`
10ad C �/'�� Cady' �c�.(�s.`• •� C+'/;4.v LaCur�/
vadose sparge �" scfm
Totalizer Reading // 76 7/ ?00 gallons
%� :
LRP run hours 'l�fS"G) 7� hours
Control Panel OK i/ Comments:
Liquid Ring Pump �C ZZ4"t` OK ✓ Temp
OWS Condition
OWS transfer pump
AST Blower Operation %v" Fit
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changedsand
rnmmantc P, nhgPn ntinnc
added coolant yg Change coolant ./t/v
OK Comments:
OK Comments:
OK Comments:
OK Comments:
Some OED None Didn't check
Yes /
Yes/0
# bags
1I6, L deg. F

TERRA nest
ENVIRONNENTAL.CONSULTANTS. P.G.
NJ
wtumly-,
Inspector
Coliseum Shell System Inspection Checklist
t, alitry► Oil
Date of Inspection / O I3
" ` " `across sep elem. `• ' "
' "' '' on LRP
'before filter' """ '"
:afterfilter " ` ' `
":`""'"` "''
Vacuum pressure
«`
vadose sparge
Totalizer Reading
LRP run hours
AST blower run hours
Control Panel
Liquid Ring Pump
OWS Condition
1
OWS transfer pump
AST Blower Operation
AST transfer pump
Bag filters dirty? Lots
Changed bag
Changedsand
Comments & Observations:
scfm
7 f Z _gallons
J A I l 23
hours
hours
OK%Z/
Comments:
OK V
Temp
h1
added coolant ► V /')
Change coolant
OK _\Z
Comments:
'%/
OK
Comments:
OK
Comments:
OK V
Comments:
Some 1 Minimal None Didn't check
Yes No
Yes6)
- 1-4-3 —deg. F
# bags

Table 1 SUMMARY OF GROUNDWATER SAMPLING RESULTS
Date: 1 30 14 Incident Name: Coliseum Shell Service Incident No.:15260 acilitv ID No: G-020021
o
m
• Analytical Method
$
c
c
e
a
v
t
w
a4
L
S
Z
€
o
o
E
E
a�
c
i
Contaminant of Concern
o
F-
5L
L°
�=
a
w
m
14
x
Sam Ie ID
Date Collected
INFLUENT
10/7113
21
94
<10
102
1,000
25
<500
-
-
<100
<50
-
<1D0
-
-
<50
<10
<10
-
32
<10
-
-
AFTER AST
10/7/13
<1
<5
<1
<3
<1
<1
<50
-
-
<10
<5
-
<10
-
-
<5
<1
<1
-
<1
<1
-
-
-
AFTER 15TGAC
10/7/13
<1
<5
<1
<3
2
<1
<50
-
-
<10
<5
-
<10
-
-
<5
<1
<1
-
<1
<1
-
-
-
EFFLUENT
1Qn113
<1
<5
<1
<3
<1
c1
<50
-
-
<10
<5
-
<10
-
-
<5
<i
<1
-
<1
<1
25
<2.5
<5
INFLUENT
11/4/13
45
194D
22.4
158.3
1,730D
49.8
111
0.230J
0.3201
107
<0.172
33.7
<0.253
0.880
0.3201
36.21D
3.75
3.56
0.2601
65.7
15
-
-
-
AFTERAST
11/4/13
<0.119
<0.0570
<0.0920
<0.298
3.06
<0.0920
<0.352
<0.0920
<0.0890
<0.378
<0.172
<0.352
c0.253
<0.0980
:0.0890
<0.0940
<0.0650
<0.0740
:0.0540
<0.103
<0.0870
-
-
-
AFTERLSTGAC
1114/13
0.2101
<0.0570
<0.0920
<0.298
0.770
<0.0920
<0.352
<0.0920
<0.0890
<0.378
0.860
<0.352
<0.253
<0.0980
<0.0890
<0.0940
<0.0650
<0.0740
<0.0540
<0.103
<0.0870
-
-
-
EFFLUENT
1 4 13
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0.352
c0.0920
<0.0890
<0.378
<0.172
<0.352
<0.253
<0.0980
<0.0890
<0.0940
<0.0650
c0.0740
<0.0540
<0.103
<0.0870
<.3 500
<3.30
INFLUENT
12/2/13
32.2
262 D
31.4
206.3
2,340 D
41.1
181
<0.0920
<0.0890
114
<0.172
29.5
<0.253
1.18
<0.0890
628 D
5.03
<0.0740
<0.0540
83.4
18.7
-
-
-
AFTERAST
12/2/13
<0.119
0.690
<0.0920
<0.296
6.46
c0.0920
<0.352
<0.0920
<0.0890
<0.378
<0.172
<0.352
<0.253
<0.0980
<0.0890
3.43
<0.0650
<0.0740
<0.0540
<0.103
<0.0870
-
-
-
AFTER-TGAC
12/2/13
<0.119
<0.0570
<0.0920
<0.298
2.23
<0.0920
<0.352
<0.0910
<0.0890
<0.378
0.800
<0.352
<0.253
<0.0980
<0.0890
<0.0940
<0.0650
<0.0740
<0.0540
<0.103
<0.0870
-
-
-
EFFLUENT
12/2/13
<0.119
<0.0570
<0.0920
<0.298
<0.169
c0.0920
<0.352
<0.0920
<0.0890
<0.378
<0.172
<0.352
10.253
<0.0980
<0.0890
c0.0940
<0.0650
<0.0740
<0.0540
<0.103
<0.0870
-
<3.50
13.30
15A NCAC 2L.0202(g
Standards
1
600
600
500
20
70
6,000
70
70
4,GDt1
70
40
NE
70
25
6
70
70
0.7
400
400
NE
NE
15
GCLViolation
5000
260000
84500
95500
20000
70000
6000000
8500
15000
00E00
70
411_1
NE
250E00
117E00
1001
30000
70N000
700
28500
25000
NE
NE
15000
N P DES Effluent Limitations month) ave.
5
690
NE
NE
NE
NE
N
NE
E
N
30
NE
E
N
E
39
NE
90
30000
25
Note:
L All resdis in parts per billion
2. Total Suspended Solids results are In mg/L.
3. <p Indicates resdt is less than method detection limit.
5. NE = Not established
6. RED indicates a permitviolation.
7. Bold denotes a detected compound. Shading denotes a GCL violation
8. "1"=The target analyte was positively Identified below the quantiation limit and above the detection limit.
9. "D-=Tte samples) were dluted due to targets detected over the highest pant of the calibration curve, or due to matrix Interference Dilution factors are included in the final results The result isfrom a diluted sample

GROUNDWATER ANALYTICAL HISTORY- INFLUENT
COLISEUM SHELL SERVICE
NCDW M-UST INCIDENT N0.: M06
TERRAQUEST PROJECT NO.: 01195
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7/25/2011
6200E
120
460
84
530
1,100
60
590
300
-
2.3 - -
3.2
-
-
150
30
11
-
-
-
120
36
8/29/2011
6200E
87
520
66
480
800
41
160
140
-
1.2 -
2.4
-
29
110
7.7
9.4
-
-
-
110
27
10/17/2011
6200E
84
650
100
680
1,000
32
<500
<100
-
<10 - -
<10
-
<100
130
14
<10
880
-
-
170
45
11/28/2011
6200B
75
400
93
530
1,100
33
240
130
-
<1 - -
3.8
-
25
1S0
14
14
-
-
-
160
41
12/5/2011
6200B
74
590
120
800
2,200
28
<250
92
-
<5 - -
<5
-
<50
150
17
18
1,600
-
-
220
55
6/8/2012
6200B
1.6
8.1
<1
27.6
130
2.4
66
27
-
<1 - -
<1
1.1
<10
16
<1
<1
710
-
-
10
13
7/9/2012
6200B
9.6
47
<5
50
220
<5
<250
100
-
<5 - -
<5
<5
<50
<25
<5
<5
450
-
-
11
6.1
8/6/2012
6200B
14
78
19
130
400
7.3
81
51
-
<1 - -
<1
<1
<10
54
3.2
3.9
1,400
-
-
46
12
9/10/2012
6200B
72
480
86
600
1,200
<50
<2,500
<500
-
<50 - -
<50
.50
<500
260
<50
<50
1,800
-
-
200
50
10/1/2012
6200B
21
150
46
370
440
20
<S00
100
-
<10 - -
<10
<10
<100
90
16
<10
970
-
-
160
52
11/5/2012
6200E
46
330
62
2,070
1,400
37
<500
100
-
<10 - -
<10
<10
<100
170
11
10
1,800
-
-
150
36
12/10/2012
6200B
45
310
55
410
1,100
36
<250
<So
-
<5 - -
<5
<5
<50
190
8.9
<5
1,100
-
-
140
35
1/7/2013
6200E
65
480
92
550
1,500
42
69
68
-
1.5 - -
3.8
<1
13
<250
14
19
1,400
-
-
170
58
2/4/2013
6200E
34
270
51
360
1,000
25
<1,000
<200
-
<20 - -
<20
<20
<200
150
<20
QO
810
-
-
140
33
3/8/2013
6200B
37
250
38
350
1,700
42
<500
<100
-
<10 - -
<10
<10
<100
140
<10
<30
-
-
-
230
36
4/1/2013
6200E
32
200
37
270
2,700
41
<500
100
-
<10 - -
<10
<10
<100
130
<10
<10
-
-
-
100
24
5/6/2013
6200B
27
170
27
209
1,400
28
<500
<100
-
QO - -
<10
<10
<100
78
<10
<10
-
-
-
77
18
6/3/2013
6200B
25
130
18
152
1,000
24
<500
<100
-
<10 - -
<10
<10
<100
61
<10
<10
-
-
-
54
13
7/1/2013
6200E
32
200
25
190
960
24
c500
<100
-
<10 - -
<10
<10
<100
58
<10
<10
-
-
-
55
14
8/5/2013
6200B
22
120
19
150
1,100
25
<250
72
-
<5 - -
<.5
<.50
<50
76
<5
c5
-
-
-
56
12
9/3/2013
6200B
5.77
30.8
5.73
59.3
343 D
10.2
179 D
130
17.7
<0.0600 - -
<0.0980
<0.0890
9.39
27.1
0.700J
1.32
<3
-
-
15.3
3.10
10/7/2013
6200B
21
94
<10
102
1,000
25
<500
<100
-
<10 - -
<10
<10
<100
<50
<10
<10
-
-
-
32
<10
11/4/2013
6200E
45
194 D
22.4
158.3
2,730 D
49.8
111
107
33.7
<0.0600 0.7,30 J 0.3201
0.880
03201
<0.253
36.2113
3.75
3.56
-
0.2601
-
65.7
15
12 2 2013
6200B
32.2
262 D
31.4
206.3
2,340 D
41.1
181
114
29.5
<0.0600 <0.0920 <0.0890
1.180
<0.0890
<0.253
628 D
5.03
<0.0740
-
<0.0540
-
83.4
18.7
2L Standard
1
600
600
500
20
70
6,000
4,000
40
70 70 70
70
25
NE
6
70
70
10
0.7
0.4
400
400
GCLI
5,000
260,000
84,500
85,500
200,000
70,000
6,000,000 4,000,000
40,000
6,900 8,500 15,000
25,000
11700
NE
6,000
30,000
70,000
10,000
700
400
28,500
25,000
Notes:
1. All results
In Ng/L
2. Bold denotes
a detected concentration.
3. Shading denotes a concentration in excess of the Gross Contamination
Levels GCLs .

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GROUNDWATER ANALYTICAL HISTORY - AFTER FIRST CARBON
COLISEUM SHELL
SERVICE
NCDWM-UST INCIDENT NO.: 15206
TERRAQUEST PROJECT NO.: 01195
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7/25/2011
6200B
<1
<5
<1
<3
<1
<1
380
-
32
7.4
5.6
<1
<1
8/29/2011
6200B
2.3
<5
<1
<3
<1
<1
77
-
<10
<5
<5
<1
<1
10/17/2011
6200B
<1
<5
<1
<3
<1
<1
<50
460
<10
<5
<5
<1
<1
11/28/2011
6200E
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<5
<1
<1
12/5/2011
6200B
<1
<5
<1
<3
<1
<1
<50
770
<10
<5
<5
<1
<1
6/8/2012
6200B
<1
<5
<1
<3
<1
<1
<50
270
<10
<5
<5
<1
<1
7/9/2012
6200B
<1
<5
<1
<3
<1
<1
<50
220
<10
<5
<5
<1
<1
8/6/2012
6200B
<1
<5
<1
<3
<1
<1
<50
280
<10
<5
<5
<1
<1
9/10/2012
6200B
<1
<5
<1
<3
1.5
<1
<50
420
<10
<5
<5
<1
<1
10/1/2012
6200B
<2
<10
2
<6
<2
<2
<100
300
<20
<10
<10
<2
<2
11/5/2012
6200B
<2
<10
2
<6
<2
<2
<100
460
<20
<10
<10
<2
<2
12/10/2012
6200B
<1
<5
<1
<3
<1
<1
<50
230
<10
<5
<5
<1
<1
1/7/2013
6200E
<1
<5
<1
<3
1.6
<1
<50
100
<10
<5
<5
<1
<1
2/4/2013
6200B
<2
<10
2
<6
<2
<2
<100
190
<20
<10
<10
<2
<2
3/8/2013
6200B
<1
<5
<1
<3
2.2
<1
<50
-
<10
<5
<5
<1
<1
4/1/2013
6200B
<1
<5
<1
<3
2
<1
<50
-
<10
<5
<5
<1
<1
5/6/2013
6200B
<1
<5
<1
<3
1.1
<1
<50
-
<10
<5
<5
<1
<1
6/3/2013
6200B
<1
<5
<1
<3
1.6
<1
<50
-
<10
<5
<5
<1
<1
7/1/2013
6200E
<1
<5
<1
<3
1
<1
<50
-
<10
<5
<5
<1
<1
8/5/2013
6200B
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<5
<1
<1
9/3/2013
6200B
0.210 J
<0.0570
<0.0920
<0.298
0.790
<0.0920
8.73
-
<0.378
0.990
<0.0940
<0.103
<0.0870
10/7/2013
6200B
<1
<5
<1
<3
<1
<1
<50
-
<10
<5
<5
<1
<1
11/4/2013
6200B
0.210 J
<0.0570
<0.0920
<0.298
0.770
<0.0920
<0.352
-
<0.378
0.860
<0.0940
<0.103
<0.0870
12/2/2013
6200B
<0.119
<0.0570
<0.0920
<0.298
2.23
<0.0920
<0.352
-
<0.378
0.800
<0.0940
<0.103
<0.0870
2L Standardl
1
600
600
500
20
70
6,000
NE
4,000
70
6
400
400
GCLI
5,000
260,000
84,500
85,500
200,000
70,000
6,000,000
NE
4,000,000
70,000
6,000
28,500
25,000
Notes:
1. All results in µg/L.
2. Bold denotes a detected concentration.
3. Shading denotes a concentration in excess of the
Gross Contamination Levels (GCLs).

GROUNDWATER ANALYTICAL HISTORY- EFFLUENT
COLISEUM SHELL SERVICE
NCDWM-UST INCIDENT NO.: 15206
TERRAQU EST PROJECT NO.: 01195
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7/25/2011
6200B
<1
<5
<1
<3
<1
<1
380
- <1 <1
-
-
-
-
-
140
-
-
-
-
8/29/2011
6200B
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
25.7
1,600
<5
-
-
-
-
10/17/2011
6200B
<1
<5
<1
<3
<1
<1
160
270 <1 <1
-
-
-
12.5
<1,000
<5
-
-
-
-
11/28/2011
6200B
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
-
<1
9.4
-
-
-
-
12/5/2011
6200E
<1
<5
<1
<3
<1
<1
<50
720 <1 <1
350
<100
<100
12.5
<1
<5
-
-
-
-
6/8/2012
6200E
<1
<5
<1
<3
<1
<1
<SO
440 <1 <1
-
-
-
-
1,300
25
-
-
-
-
7/9/2012
6200E
<1
<5
<1
<3
<1
<1
<50
190 <1 <1
-
-
-
-
-
<5
-
-
-
-
8/6/2012
6200B
<1
<5
<1
<3
<1
<1
<50
7.6 <1 <1
-
-
-
7/11/12<12.5
<1,000
<5
-
-
-
-
9/10/2012
6200B
<1
<5
<1
<3
<1
<1
<50
220 <1 <1
-
-
-
-
2.1
<5
-
-
-
-
10/1/2012
6200B
<1
<5
<1
<3
<1
<1
<SO
<5 <1 <1
-
-
-
25
-
-
-
-
-
-
11/5/2012
6200B
<1
<5
<1
<3
<1
<1
<50
660 <1 <1
-
-
-
-
-
-
-
-
-
12/10/2012
6200B
<1
<5
<1
<3
<1
<1
<50
230 <1 <1
-
-
-
-
2,200
11
230
11,000
<20
<10
1/7/2013
6200E
<1
<5
<1
<3
<1
<1
cso
590 <1 <1
-
-
-
25
<1,000
<5
-
-
-
-
2/4/2013
6200B
<10
<50
<10
<30
<10
<10
<500
250 <10 <10
-
-
-
-
<1,000
<5
-
-
-
-
3/8/2013
6200B
<1
<5
<1
<3
1.7
<1
<50
- <1 <1
-
-
-
-
1,000
<5
-
-
-
-
4/1/2013
6200B
<1
<5
<1
<3
2.2
<1
<SO
- <1 <1
-
-
4/8/13 <12.5
1,800
<5
-
-
-
-
5/6/2013
6200E
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
-
4,700
<5
-
-
-
-
6/3/2013
6200E
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
-
<2.5
<5
-
-
-
-
7/1/2012
6200E
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
7/8/13<12.5
<2.5
<5
-
-
-
-
8/5/2013
6200B
<1
<5
<1
<3
<1
<1
<50
- <1 <1
-
-
-
7/8/13<12.5
<2.5
<5
-
-
-
-
9/3/2013
6200E
<0.119
<0.0570
<3
<0.298
<0.169
<0.0920
<0352
- <0.103 <0.0870
-
-
-
-
<3.50
<3.30
-
-
-
-
10/7/2013
6200B
<1
<5
<1
<3
<1
<1
<SO
- <1 <1
-
-
-
25
<2.5
<5
-
-
-
-
11/4/2013
6200B
<0.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0352
- <0.103 <0.0870
-
-
-
-
<3,500
<330
-
-
-
-
12 2 2013
1
6200E
10.119
<0.0570
<0.0920
<0.298
<0.169
<0.0920
<0352
- <0.103 <0.0870
-
-
-
-
<3.50
<330
-
-
-
-
2LStandard
1
600
600
500
20
70
6000
NE 400 400
400
700
200
NE
NE
15
NE
50
100
NE
GCLI
5,000
260,000
84,500
85,500
200,000
70,000
6,000,000
NE 28,500 25 000
NE
NE
NE
NE
NE
15,000
NE
NE
NE
NE
Notes:
1. All results in Ng/L.
2. Bold denotes a detected
concentration.
3. Shading denotes a concentration in excess of the Grass Contamination Levels
GCLss).

L-A-B S•C-I-K-N•C•E•S
12065 Lebanon Rd.
Mt. Juliet, TIT 37122
(6151 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est, 1970
REPORT
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received October 08, 2013
Description Coliseum Shell
Sample ID INFLUENT
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:42
Parameter Result
OF ANALYSIS
Det. Limit
October 20,2013
ESC Sample $ L661803-01
Site ID 1 i•IINSTON-SALEM, NC
Project 01195
Units Method Date
Ail,
Volatile organics
Acetone
BDL
500
ug/1
620OB-1997
10/10/13
1(
Acrolein
BDL
500
ug/1
6200B--1997
10/10/13
1(
Acrylonitrile
BDL
100
ug/l
6200B-1997
10/10/13
1(
Benzene
21.
10.
ug/1
6200B-1997
10/10/13
1(
Bromobenzene
BDL
10.
ug/1
620OB-1997
10/10/13
1(
Bromodichloromethane
BDL
10.
ug/1
6200B-1997
10/10/13
1(
Bromoform
BDL
10.
ug/l
620OB-1997
10/10/13
1(
Bromomethane
BDL
50.
ug/1
6200B-1997
10/10/13
1(
n-Butylbenzene
BDL
10.
ug/1
6200B-1997
20/10/13
1(
sec-Butylbenzene
BDL
10.
ug/l
6200B-1997
10/10/13
1(
tent-Butylbenzene
BDL
10.
ug/1
6200B-1997
10/10/13
1(
Carbon tetrachloride
BDL
10.
ug/1
6200B-1997
10/10/13
1(
Chlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
1(
Chlorodibromomethane
BDL
10.
ug/1
6200B-1997
10/10/13
V
Chloroethane
BDL
50.
ug/1
6200B-1997
10/10/13
1(
Chloroform
BDL
50.
ug/1
6200B-1997
10/10/13
V
Chloromethane
BDL
25.
ug/l
6200B-1997
10/10/13
V
2-Chlorotoluene
BDL
10.
ug/l
620OB-1997
10/10/13
V
4-Chlorotoluene
BDL
10.
ug/1
6200B-1997
10/10/13
1(
1,2-Dibromo-3-Chloropropane
BDL
50.
ug/1
6200E-1997
10/10/13
11
1,2-Dibromoethane
BDL
10.
ug/l
6200B-1997
10/10/13
11
Dibromomethane
BDL
10.
ug/1
6200E-1997
20/10/13
11
1,2-Dichlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
11
1,3-Dichlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
11
1,4-Dichlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
11
Dichlorodifluoromethane
BDL
50.
ug/1
6200B-1997
10/10/13
11
1,1-Dichloroethane
BDL
10.
ug/l
6200B-1997
10/10/13
11
1,2-Dichloroethane
BDL
10.
ug/l
6200B-1997
10/10/13
11
1,1-Dichloroethene
BDL
10.
ug/1
6200B-1997
10/10/13
it
cis-1,2-Dichloroethene
BDL
10.
ug/1
620OB-1997
10/10/13
11
trans-1,2-Dichloroethene
BDL
10.
ug/1
6200B-1997
10/10/13
11
1,2-Dichloropropane
BDL
10.
ug/1
6200B--1997
10/10/13
li
1,1-Dichloropropene
BDL
10.
ug/l
6200B-1997
10/10/13
li
1,3-Dichloropropane
BDL
10.
ug/1
6200B-1997
10/10/13
li
2,2-Dichloropropane
BDL
10.
ug/1
620OB-1997
10/10/13
11
Di -isopropyl ether
25.
10.
ug/1
6200B-1997
10/10/13
li
Ethylbenzene
BDL
10.
ug/1
6200B-1997
10/10/13
11
Rexachloro-1,3-butadiene
BDL
10.
ug/1
6200B-1997
10/10/13
11
Isopropylbenzene
BDL
10.
ug/1
620OB-1997
10/10/13
1,
p-Isopropyltoluene
BDL
10.
ug/1
620OB-1997
10/10/13
1,
2-Butanone (MEK)
BDL
100
ug/1
6200B-1997
10/10/13
1
Methylene Chloride
BDL
50.
ug/1
6200B-1997
10/10/13
1
4-Methyl-2-pentanone (MIBK)
BDL
100
ug/1
6200B-1997
10/10/13
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 2 of 28

4W
L•A•B S•C-I•E'N•C•C's
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0614289
Est. 1970
October 20,2013
ESC Sample # : L661803-01
Date Received October 08, 2013
Description Coliseum Shell
Site
ID : FIZNSTON-SALEt4,
NC
Sample ID, INFLUENT
Project # 01195
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:42
Parameter
Result
Det. Limit
Units
Method
Date
Dill
Methyl tert-butyl ether
1000
10.
ug/1
6200B-1997
10/10/13
10
Naphthalene
BDL
50.
ug/1
6200B-1997
10/10/13
10
n-Propylbenzene
BDL
10.
ug/1
6200B-1997
10/10/13
10
Styrene
BDL
10.
ug/1
6200B-1997
10/10/13
10
1,1,1,2-Tetrachloroethane
BDL
10.
ug/1
6200B-1997
10/10/13
10
1,1,2,2-Tetrachloroethane
BDL
10.
ug/1
6200B-1997
10/10/13
10
Tetrachloroethene
BDL
10.
ug/1
6200B-1997
10/10/13
10
Toluene
94.
50.
ug/1
6200B-1997
10/10/13
10
1,2,3-Trichlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
10
1,2,4-Trichlorobenzene
BDL
10.
ug/1
6200B-1997
10/10/13
10
1,1,1-Trichloroethane
BDL
10.
ug/1
6200B-1997
10/10/13
10
1,1,2-Trichloroethane
BDL
10.
ug/1
6200B-1997
10/10/13
10
Trichloroethene
BDL
10.
ug/1
6200B-1997
10/10/13
10
Trichlorofluoromethane
BDL
50.
ug/1
6200B-1997
10/10/13
10
1,2,3-Trichloropropane
BDL
25.
ug/1
6200B-1997
10/10/13
10
1,2,4-Trimethylbenzene
32.
10.
ug/1
6200B-1997
10/10/13
10
1,3,5-Trimethylbenzene
BDL
10.
ug/1
6200B-1997
10/10/13
10
vinyl chloride
BDL
10.
ug/l
6200B-1997
10/10/13
10
o-Xylene
43.
10.
ug/l
6200E-1997
10/10/13
10
m&p-Xylenes
59.
20.
ug/1
6200B-1997
10/10/13
10
Surrogate Recovery
Toluene-d8
105.
% Rec.
6200B-1997
10/10/13
10
Dibromofluoromethane
98.6
% Rec.
620OB-1997
10/10/13
10
a,a,a-Trifluorotoluene
109.
F4 Rec.
6200E-1997
10/10/13
10
4-Bromofluorobenzene
99.8
J� Rec.
6200E-1997
10/10/13
10
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 3 of 28

OESC
1
12065 Lebanon Rd.
FJt. Juliet, T11 37122
1615) 758-5858
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received October 08, 2013
Description Coliseum Shell
Sample ID AFTER AST
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:45
Parameter Result
OF ANALYSIS
Det. Limit
October 20,2013
ESC Sample # L661803-02
Site ID 47INSTON-SALEI4, NC
Project @ 01195
Units Method Date
Dil.
Volatile Organics
ti
Acetone
BDL
50.
ug/1
6200B-1997
10/10/13
1
Acrolein
BDL
50.
ug/1
620OB-1997
10/10/13
1
Acrylonitrile
BDL
10.
ug/1
620OB-1997
10/10/13
1
Benzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Bromobenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Bromodichloromethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
-Bromoform
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Bromomethane
BDL
5.0
ug/1
620OB-1997
10/10/13
1
n-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
sec-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
text-Butylbenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Carbon tetrachloride
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Chlorobenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Chlorodibromomethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Chloroethane
BDL
5.0
ug/1
620OB-1997
10/10/13
1
Chloroform
BDL
5.0
ug/1
620OB-1997
10/10/13
1
Chloromethane
BDL
2.5
ug/1
620OB-1997
10/10/13
1
2-Chlorotoluene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
4-Chlorotoluene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
1,2-Dibromo-3-Chloropropane
BDL
5.0
ug/1
620OB-1997
10/10/13
1
1,2-Dibromoethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Dibromomethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,2-Dichlorobenzene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
1,3-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
10/10/13
1
1,4-Dichlorobenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Dichlorodifluoromethane
BDL
5.0
ug/1
620OB-1997
10/10/13
1
1,1-Dichloroethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,2-Dichloroethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,1-Dichloroethene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
cis-1,2-Dichloroethene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
trans-1,2-Dichloroethene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
1,2-Dichloropropane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,1-Dichloropropene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,3-Dichloropropane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
2,2-Dichloropropane
BDL
2.0
ug/1
620OB-1997
10/10/13
1
Di -isopropyl ether
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Ethylbenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Rexachloro-1,3-butadiene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Isopropylbenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
p-Isopropyltoluene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
2-Butanone (MEK)
BDL
10.
ug/l
620OB-1997
10/10/13
1
Methylene Chloride
BDL
5.0
ug/1
620OB-1997
10/10/13
1
4-Methyl-2-pentanone (MIRK)
BDL
10.
ug/1
6200B-1997
10/10/13
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 4 of 28

Y:O U R
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, T11 37122
[phone]
1-600-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 20,2013
ESC Sample f : L661803-02
Date Received October 08, 2013
Description Coliseum Shell
Site
ID Y7INST0N-SALEt4,
NC
Sample ID AFTER AST
Project 8 01195
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:45
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Methyl tert-butyl ether
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Naphthalene
BDL
5.0
ug/1
620OB-1997
10/10/13
1
n-Propylbenzene
BDL
1.0
ug/1
620013-1997
10/10/13
1
Styrene
BDL
1.0
ug/1
6200R-1997
10/10/13
1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Tetrachloroethene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Toluene
BDL
5.0
ug/1
6200B-1997
10/10/13
1
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
62005-1997
10/10/13
1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
62003-1997
10/10/13
1
1,1,1-Trichloroethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,1,2-Trichloroethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Trichloroethene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Trichlorofluoromethane
BDL
5.0
ug/1
6200B-1997
10/10/13
1
1,2,3-Trichloropropane
BDL
2.5
ug/1
620OB-1997
10/10/13
1
1,2,4-Trimethylbenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Vinyl chloride
BDL
1.0
ug/1
6200B-1997
10/10/13
1
o-Xylene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
m&p-Xylenes
BDL
2.0
ug/1
6200B-1997
10/10/13
1
Surrogate Recovery
Toluene-d8
108.
% Rec.
620OB-1997
10/10/13
1
Dibromofluoromethane
99.8
% Rec.
620OB-1997
10/10/13
1
a,a,a-Trifluorotoluene
Ill.
% Rec.
6200E-1997
10/10/13
1
4-Bromofluorobenzene
102.
% Rec.
620OB-1997
10/10/13
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 5 of 28

L-A-B s•C-I•E•N•C•M•s
12065 Lebanon Rd'.
Mt. Juliet, TII 37122
[phone]
1-800-767-5659
Fax [phone]
Tax I.D. 62-0014289
Est. 1970
REPORT
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received October 08, 2013
Description Coliseum Shell
Sample ID AFTER 1ST CARBON
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:48
Parameter Result
OF ANALYSIS
Det. Limit
October 20,2013
ESC Sample # L661803-03
Site ID : WINSTON-SALEM, NC
Project 9 01195
Units Method Date
Dil.
Volatile Organics
Acetone
BDL
50.
ug/1
6200B-1997
10/10/13
1
Acrolein
BDL
50.
ug/l
6200B-1997
10/10/13
1
Acrylonitrile
BDL
10.
ug/l
620OB-1997
10/10/13
1
Benzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Bromobenzene
BDL
1.0
ug/1
620OB-1997
10/20/13
1
Bromodichloromethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Bromoform
BDL
1.0
ug/l
620OB-1997
10/10/13
1
Bromomethane
BDL
5.0
ug/1
620OB-1997
10/10/13
1
n-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/20/13
1
sec-Butylbenzene
BDL
1.0
ug/1'
620OB-1997
10/10/13
1
tert-Butylbenzene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
Carbon tetrachloride
BDL
1.0
ug/l
620OB-1997
10/10/13
1
Chlorobenzene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
Chlorodibromomethane
BDL
1.0
ug/l
620OB-1997
10/10/13
1
Chloroethane
BDL
5.0
ug/l
62008-1997
10/10/13
1
Chloroform
BDL
5.0
ug/l
620OB-1997
10/10/13
1
Chloromethane
BDL
2.5
ug/1
620OB-1997
10/10/13
1
2-Chlorotoluene
BDL
1.0
ug/l
620OB-1997
10/10/13
1
4-Chlorotoluene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,2-Dibromo-3-Chloropropane
BDL
5.0
ug/l
620OB-1997
10/10/13
1
1,2-Dibromoethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Dibromomethane
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,2-Dichlorobenzene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
1,3-Dichlorobenzene
BDL
1.0
ug/l
6200B-1997
10/10/13
1
1,4-Dichlorobenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Dichlorodifluoromethane
BDL
5.0
ug/1
6200B-1997
10/10/13
1
1,1-Dichloroethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,2-Dichloroethane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,1-Dichloroethene
BDL
1.0
ug/l
6200B-1997
10/10/13
1
cis-1,2-Dichloroethene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
trans-1,2-Dichloroethene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,2-Dichloropropane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
1,1-Dichloropropene
BDL
1.0
ug/l
6200B-1997
10/10/13
1
1,3-Dichloropropane
BDL
1.0
ug/1
6200D-1997
10/10/13
1
2,2-Dichloropropane
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Di -isopropyl ether
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Ethylbenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Hexachloro-1,3-butadiene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Isopropylbenzene
BDL
1.0
ug/1
6200B-1997
10/10/13
1
p-Isopropyltoluene
BDL
1.0
ug/1
620OB-1997
10/10/13
1
2-Butanone (MEK)
BDL
10.
ug/l
6200B-1997
10/10/13
1
Methylene Chloride
BDL
5.0
ug/l
6200B-1997
10/10/13
1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
6200B-1997
10/10/13
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 6 of 28

:t
+YO U'R L-'AB-0 F: CH Oi'GE
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, Tli 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814269
Est. 1970
October 20,2013
ESC Sample 4 : L661803-03
Date Received October 08, 2013
Description Coliseum Shell
Site
ID WINSTON-SALEM,
NC
Sample ID AFTER 1ST CARBON
project $ 01195
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:48
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Methyl tert-butyl ether
2.0
1.0
5.0
u9/1
ug/1
620OB-1997
6200E-1997
10/10/13
10/10/13
1
1
Naphthalene
n-Propylbenzene
BDL
BDL
1.0
ug/1
6200B-1997
10/10/13
1
Styrene
BDL
1.0
1.0
ug/1
ug/1
620OB-1997
620OB-1997
10/10/13
10/10/13
1
1
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
BDL
BDL
1.0
ug/1
620OB-1997
10/10/13
1
Tetrachloroethene
BDL
1.0
5.0
ug/1
ug/l
6200B-1997
6200B-1997
10/10/13
10/10/13
1
1
Toluene
1,2,3-Trichlorobenzene
BDL
BDL
1.0
ug/1
620013-1997
10/10/13
10/10/13
1
1
1,2,4-Trichlorobenzene
BDL
1.0
1.0
ug/l
ug/l
6200B-1997
620OB-1997
10/10/13
1
1,1,1-Trichloroethane
1,1,2-Trichloroethane
BDL
BDL
1.0
ug/l
6200B-1997
10/10/13
1
Trichloroethene
BDL
1.0
5.0
ug/l
ug/1
6200B-1997
620OB-1997
10/10/13
10/10/13
1
1
Trichlorofluoromethane
BDL
BDL
2.5
ug/1
620OB-1997
10/10/13
1
1,213-Trichloropropane
1,219-Trimethylbenzene
BDL
1.0
ug/l
6200B-1997
10/10/13
1
1,3,5-Trimethylbenzene
BDL
1.0
1.0
ug/1
ug/1
6200B-1997
6200B-1997
10/10/13
10/10/13
1
1
Vinyl chloride
BDL
BDL
1.0
ug/1
6200B-1997
10/10/13
1
o-Xylene
m&p-Xylenes
BDL
2.0
ug/1
6200B-1997
10/10/13
1
Surrogate Recovery
108.
% Rec.
6200B-1997
10/10/13
1
Toluene-d8
Dibromofluoromethane
99.0
% Rec.
620OB-1997
10/10/13
1
1
a,a,a-Trifluorotoluene
115.
% Rec.
Rec.
6200E-1997
6200E-1997
10/10/13
1
4-Bromofluorobenzene
101.
6
.10/10/13
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 7 of 28

REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received October 08, 2013
Description Coliseum Shell
Sample ID EFFLUENT
Collected By Ryan'D. Kerins
Collection Date 10/07/13 10:35
12065 Lebanon Rd.
Mt. Juliet, TCI 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.A. 62-0814289
Est. 1970
October 20, 2013
ESC Sample 4 : L661803-04
Site ID WINSTON-SALEM, NC
Project 4 01195
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
NOEC - C.dubia
25.
%
1002.0
10/08/13
1
ALK
37900
20000
ug/l
2320 B-201
10/15/13
1
Hardness, Total (mg/L as CaCO3)
42900
30000
ug/l
130.1
10/15/13
1
Lead
BDL
5.0
ug/l
60105
10/19/13
1
Volatile Organics
Acetone
BDL
50.
ug/1
620OB-1997
10/11/13
1
Acrolein
BDL
50.
ug/1
620OB-1997
10/11/13
1
Acrylonitrile
BDL
10.
ug/l
620OB-1997
10/11/13
1
Benzene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Bromobenzene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Bromodichloromethane
BDL
1.0
ug/1
620OB-1997
10/11/13
1
Bromoform
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Bromomethane
BDL
5.0
ug/1
620OB-1997
10/11/13
1
n-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/11/13
1
sec-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/11/13
1
tent-Butylbenzene
BDL
1.0
ug/1
620OB-1997
10/11/13
1
Carbon tetrachloride
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Chlorobenzene
BDL
1.0
ug/1
620OB-1997
10/11/13
1
Chlorodibromomethane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Chloroethane
BDL
5.0
ug/1
620013-1997
10/11/13
1
Chloroform
BDL
5.0
ug/1
620OB-1997
10/11/13
1
Chloromethane
BDL
2.5
ug/1
620OB-1997
10/11/13
1
2-Chlorotoluene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
4-Chlorotoluene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,2-Dibromo-3-Chloropropane
BDL
5.0
ug/1
620OB-1997
10/11/13
1
1,2-Dibromoethane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Dibromomethane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,2-Dichlorobenzene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,3-Dichlorobenzene
BDL
1.0
ug/1
620OB-1997
10/11/13
1
1,4-Dichlorobenzene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
Dichlorodifluoromethane
BDL
5.0
ug/l
620OB-1997
10/11/13
1
1,1-Dichloroethane
BDL
1.0
ug/1
620OB-1997
10/11/13
1
1,2-Dichloroethane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,1-Dichloroethene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
cis-1,2-Dichloroethene
BDL
1.0
ug/l
62008-1997
10/11/13
1
trans-1,2-Dichloroethene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,2-Dichloropropane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,1-Dichloropropene
BDL
1.0
ug/l
620OB-1997
10/11/13
1
1,3-Dichloropropane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
2,2-Dichloropropane
BDL
1.0
ug/l
620OB-1997
10/11/13
1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
Page 8 of 28

` zx
xXO lJ R'°6:A.Ja':bf R. C 14O i'dE'
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
Date Received October 08, 2013
Description Coliseum Shell
Sample ID EFFLUENT
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:35
12065 Lebanon Rd.
Mt. Juliet, TH 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0614269
Est. 1970
October 20, 2013
ESC Sample 4 : L661803-04
Site ID WINSTON-SALEM, NC
Project # 01195
Parameter Result Dot. Limit Units Method Date_ Dil.
Di -isopropyl ether
BDL
1.0
ug/l
6200B-1997
10/11/13 1
Ethylbenzene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
Hexachloro-1,3-butadiene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
Isopropylbenzene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
p-Isopropyltoluene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
2-Butanone (MEK)
BDL
10.
ug/l
6200E-1997
10/11/13 1
Methylene Chloride
BDL
5.0
ug/1
620OB-1997
10/11/13 1
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/1
620OB-1997
10/11/13 1
Methyl tert-butyl ether
BDL
1.0
ug/l
620OB-1997
10/11/13 1
Naphthalene
BDL
5.0
ug/1
620OB-1997
10/11/13 1
n-Propylbenzene
BDL
1.0
ug/l
6200B-1997
10/11/13 1
Styrene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
620OB-1997
10/11/13 1
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
620013-1997
10/11/13 1
Tetrachloroethane
BDL
1.0
ug/1
620OB-1997
10/11/13 1
Toluene
BDL
5.0
ug/1
620OB-1997
10/11/13 1
1,2,3-Trichlorobenzene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
1,1,1-Trichloroethane
BDL
1.0
ug/1
620013-1997
10/11/13 1
1,1,2-Trichloroethane
BDL
1.0
ug/l
620DB-1997
10/11/13 1
Trichloroethene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
Trichloro£luoromethane
BDL
5.0
ug/l
620OB-1997
10/11/13 1
1,2,3-Trichloropropane
BDL
2.5
ug/l
6200B-1997
10/11/13 1
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
620OB-1997
10/11/13 1
1,315-Trimethylbenzene
BDL
1.0
ug/1
6200B-1997
10/11/13 1
Vinyl chloride
BDL
1.0
ug/1
620OB-1997
10/11/13 1
o-Xylene
BDL
1.0
ug/1
620OB-1997
10/11/13 1
m&p-Xylenes
BDL
2.0
ug/1
6200B-1997
10/11/13 1
Surrogate Recovery
Toluene-d8
102.
3 Rec.
6200B-1997
10/11/13 1
Dibromofluoromethane
105.
% Rec.
620OB-1997
10/11/13 1
a,a,a-Trifluorotoluene
99.9
% Rec.
620OB-1997
10/11/13 1
4-Bromofluorobenzene
95.4
% Rec.
620OB-2997
10/11/13 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 9 of 28

7
F.-&C4-{ O. eeE
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, TIT 37122
[phone]
1-800-767-5859
Fax [phone]
Tau I.D. 62-0814289
Est. 1970
October 20, 2013
ESC Sample F : L661803-05
Date Received October 08, 2013
Description Coliseum Shell
Site ID I 4)INSTON-SALEhf, NC
Sample ID EFFLUENT
Project 01195
Collected By Ryan D. Kerins
Collection Date 10/07/13 10:35
Parameter Result Det. Limit Units Method Date Dil.
Suspended Solids BDL 2.5 mg/l 2540 D-2011 10/11/13 1
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 10 of 28

OESC
1
REPORT OF ANALYSIS
Ryan Kerins
TerraQuest Environmental Consultant
100 East Ruffin Street
Mebane, NC 27302
12065 Lebanon Rd.
Mt. Juliet, 711 37122
[phone]
1-800-167-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 20, 2013
ESC Sample # : L661803-06
Date Received
October 10, 2013
Description
Coliseum Shell
Site ID NC0088919
Sample ID
SAMPLE 2
Project $
FORMER COLISEUM SHEL
Collected By
Brad Hayes
Collection Date
10/09/13 11:10
Parameter
Result
Det. Limit Units
Method
Date Dil.
ALK
29.2
20.0 mg/l
2320 B-2011
10/17/13 1
Hardness, Total
(mg/L as CaCO3) 41.
30. mg/1
130.1
10/15/13 1
BDL - Below Detection Limit
Dot. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/20/13 12:12 Printed: 10/20/13 12:12
Page 11 of 28

Certificate of Analytical Results 473415 rtw)
EQZQ U.
...W� ..a...
Florida Testing Services, LLC
Sample Id: Influent
Lab Sample Id: 473415-001
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Water
Date Collected: 11.04.13 11.10
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA Date Prep: 11.06.13 06.23
Seq Number: 926998
Date Received:11.05.13 11.00
Prep Method: SM6200B_PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
11.06.1317.03
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
11.06.13 17.03
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
11.06.1317.03
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
11.06.1317.03
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
11.06.1317.03
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
11.06.13 17.03
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
11.06.1317.03
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
11.06.1317.03
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
11.06.13 17.03
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
11.06.13 17.03
U
1
1,2,4-Trimethylbenzene
95-63-6
65.7
0.500
0.103
ug/L
11.06.13 17.03
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
11.06.13 17.03
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
11.06.1317.03
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
11.06.1317.03
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
11.06.13 17.03
U
1
1,3,5-Trimethylbenzene
108-67-8
15.0
0.500
0.0870
ug/L
11.06.1317.03
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
11.06.1317.03
U
I
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
11.06.13 17.03
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
11.06.13 17.03
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
11.06.13 17.03
U
1
2-Butanone (MEK)
78-93-3
107
20.0
0.378
ug/L
11.06.13 17.03
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
11.06.1317.03
U
I
2-Hexanone
591-78-6
33.7
0.400
0.352
ug/L
11.06.1317.03
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
11.06.1317.03
U
1
4-Isopropyltoluene
99-87-6
0.320
0.500
0.0890
ug/L
11.06.1317.03
J
1
4-Methyl-2-pentanone (M113K)
108-10-1
U
0.400
0.253
ug/L
11.06.13 17.03
U
1
Acetone
67-64-1
111
2.00
0.352
ug/L
11.06.1317.03
1
Benzene
71-43-2
45.0
0.500
0.119
ug/L
11.06.1317.03
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L,
11.06.1317.03
U
1
Bromocbloromethane
74-97-5
U
0.500
0.112
ug/L
11.06.1317.03
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
11.06.1317.03
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
11.06.1317.03
U
1
Bromomethane
74-93-9
U
1.00
0.0970
ug/L
11.06.1317.03
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
11.06.13 17.03
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
11.06.1317.03
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
11.06.1317.03
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
11.06.1317.03
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/1,
11.06.1317.03
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
11.06.1317.03
U
1
Page 9 of 31 Final 1.000

Certificate of Analytical Results 473415
t r�u
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Influent Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-001 Date Collected: 11.04.13 11.10
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 926998
Parameter Cas Number
Date Prep:
Result
11.06.13 06.23
RL MDL
Prep Method: SM6200B_PREP
% Moisture:
Units Analysis Date Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
11.06.1317.03
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
11.06.13 17.03
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
11.06.1317.03
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
11.06.13 17.03
U
1
Ethylbenzene
100-41-4
22.4
0.500
0.0920
ug/L
11.06.1317.03
1
Isopropyl ether
108-20-3
49.8
0.500
0.0920
ug/L
11.06.13 17.03
1
Isopropylbenzene
98-82-8
0.880
0.500
0.0980
ug/L
11.06.1317.03
1
Methyl tert-butyl ether (MTBE)
1634-04-4
1730
10.0
3.38
ug/L
11.07.13 14.57
D
20
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L,
11.06.13 17.03
U
1
Naphthalene
91-20-3
36.2
40.0
1.88
ug/L
11.07.1314.57
JD
20
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
11.06.13 17.03
U
1
n-Propylbenzene
103-65-1
3.75
1.00
0.0650
ug/L
11.06.1317.03
1
sec-Butylbenzene
135-98-8
0.230
0.500
0.0920
ug/L
11.06.13 17.03
J
1
Styrene
100-42-5
3.56
0.500
0.0740
ug/L
11.06.1317.03
1
tert-Butylbenzene
98-06-6
0.320
0.500
0.0890
ug/L
11.06.1317.03
J
1
Tetrachloroethene (PCE)
127-19-4
0.260
0.500
0.0540
ug/L
11.06.13 17.03
J
1
Toluene
108-88-3
194
10.0
1.14
ug/L
11.07.1314.57
D
20
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
11.06.13 17.03
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
11.06.13 17.03
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L.
11.06.1317.03
U
1
Trichlorofluoromethane
75-694
U
0.500
0.0540
ug/L
11.06.1317.03
U
I
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
11.06.13 17.03
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
11.06.13 17.03
U
1
m,p-Xylenes
179601-23-1
97.2
1.00
0.176
ug/L
11.06.1317.03
1
o-Xylene
95-47-6
61.1
0.500
0.122
ug/L
11.06.1317.03
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
98
%
53-159
11.06.1317.03
4-Bromofluorobenzene
460-00-4
93
%
30-186
11.06.13 17.03
Toluene-D8
2037-26-5
102
%
70-130
11.06.1317.03
Page 10 of 31 Final 1.000

Certificate of Analytical Results 473415 �a
s r�u
..QR ewwar,w
Florida Testing Services, LLC
Sample Id: After AST
Lab Sample Id: 473415-002
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Water Date Received:11.05.13 11.00
Date Collected: 11.04.13 11.15
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 927155
Parameter Cas Number
Date Prep:
Result
11.07.13 06.32
RL MDL
Units
Prep Method: SM6200B_PREP
% Moisture:
Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
11.07.1311.23
U
1
1, 1, 1 -Trichl oroethane
71-55-6
U
0.500
0.0760
ug/L
11.07.1311.23
U
1
1, 1,2,2-Tetrachloro ethane
79-34-5
U
0.500
0.0700
ug/L
11.07.1311.23
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
11.07.13 11.23
U
1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
11.07.13 11.23
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
11.07.13 11.23
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
11.07.1311.23
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
11.07.1311.23
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
11.07.13 11.23
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
11.07.13 11.23
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
11.07.1311.23
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
11.07.13 11.23
U
I
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
11.07.13 11.23
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
11.07.13 11.23
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/1-
11.07.13 11.23
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
11.07.1311.23
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
11.07.1311.23
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
11.07.1311.23
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
11.07.1311.23
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
11.07.13 11.23
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
11.07.13 11.23
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
11.07.13 11.23
U
I
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
11.07.1311.23
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
11.07.13 11.23
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
11.07.1311.23
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
11.07.13 11.23
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
11.07.1311.23
U
I
Benzene
71-43-2
U
0.500
0.119
ug/L
11.07.13 11.23
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
11.07.1311.23
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
11.07.1311.23
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
11.07.1311.23
U
I
Bromoform
75-25-2
U
2.00
0.159
ug/L
11.07.1311.23
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
11.07.1311.23
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
11.07.13 11.23
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
11.07.13 11.23
U
I
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
11.07.1311.23
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
11.07.1311.23
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
11.07.13 11.23
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
11.07.1311.23
U
I
Page 11 of 31 Final 1.000

Certificate of Analytical Results 473415
rau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-002 Date Collected: 11.04.13 11.15
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 927155
Parameter Cas Number
Date Prep:
Result
11.07.13 06.32
RL MDL
Prep Method: SM6200B_PREP
% Moisture:
Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
11.07.1311.23
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
11.07.13 11.23
U
I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
11.07.1311.23
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
11.07.1311.23
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
11.07.13 11.23
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
11.07.13 11.23
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
11.07.13 11.23
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
3.06
0.500
0.169
ug/L
11.07.13 11.23
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
11.07.13 11.23
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
11.07.1311.23
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
11.07.1311.23
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
11.07.13 11.23
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
11.07.13 11.23
U
I
Styrene
100-42-5
U
0.500
0.0740
ug/L
11.07.13 11.23
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
11.07.13 11.23
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
11.07.13 11.23
U
I
Toluene
108-88-3
U
0.500
0.0570
ug/L
11.07.13 11.23
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
11.07.13 11.23
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
11.07.1311.23
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
11.07.13 11.23
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
11.07.1311.23
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
11.07.13 11.23
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
11.07.13 11.23
U
I
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
11.07.1311.23
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
11.07.13 11.23
U
I
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
101
%
53-159
11.07.1311.23
4-Bromofluorobenzene
460-00-4
104
%
30-186
11.07.1311.23
Toluene-D8
2037-26-5
107
%
70-130
11.07.1311.23
Page 12 of 31 Final 1.000

/�/,pttRFO
Certificate of Analytical Results 473415�B
Florida Testing Services, LLC
Sample Id: After 1st GAC
Lab Sample Id: 473415-003
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Water
Date Collected: 11.04.13 11.20
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA Date Prep: 11.07.13 06.32
Seq Number: 927155
Date Received:11.05.13 11.00
Prep Method: SM6200B PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
11.07.1310.56
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
11.07.1310.56
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
11.07.1310.56
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
11.07.1310.56
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
11.07.1310.56
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
11.07.1310.56
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
11.07.1310.56
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
11.07.13 10.56
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
11.07.1310.56
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
11.07.1310.56
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
11.07.13 10.56
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
11.07.13 10.56
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
11.07.13 10.56
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
11.07.13 10.56
U
I
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
11.07.13 10.56
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
11.07.1310.56
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
11.07.13 10.56
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
11.07.1310.56
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
11.07.13 10.56
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
11.07.1310.56
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
11.07.13 10.56
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
11.07.13 10.56
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
11.07.1310.56
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
11.07.13 10.56
U
I
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
11.07.13 10.56
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
11.07.13 10.56
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
11.07.13 10.56
U
I
Benzene
71-43-2
0.210
0.500
0.119
ug/L
11.07.1310.56
J
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
11.07.1310.56
U
I
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
11.07.1310.56
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
11.07.1310.56
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
11.07.1310.56
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
11.07.1310.56
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
11.07.13 10.56
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
11.07.1310.56
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
11.07.1310.56
U
I
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
11.07.1310.56
U
1
Chloroform
67-66-3
0.860
0.500
0.172
ug/L
11.07.1310.56
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
11.07.1310.56
U
1
Page 13 of 31 Final 1.000

Certificate of Analytical Results 473415
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st GAC Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-003 Date Collected: 11.04.13 11.20
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 927155
Parameter Cas Number
Date Prep:
Result
11.07.13 06.32
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
11.07.1310.56
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
11.07.13 10.56
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
11.07.13 10.56
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
11.07.13 10.56
U
1
Etylbenzene
100-41-4
U
0.500
0.0920
ug/L
11.07.1310.56
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
11.07.13 10.56
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
11.07.13 10.56
U
1
Methyl tert-butyl ether (MTBE)
1634-044
0.770
0.500
0.169
ug/L,
11.07.13 10.56
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
11.07.13 10.56
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
11.07.13 10.56
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
11.07.13 10.56
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
11.07.13 10.56
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
11.07.13 10.56
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L,
11.07.13 10.56
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
11.07.13 10.56
U
1
Tetrachloroethene (PCE)
127-184
U
0.500
0.0540
ug/L
11.07.13 10.56
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
11.07.13 10.56
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
11.07.13 10.56
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
11.07.13 10.56
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
11.07.1310.56
U
1
Trichlorofluoromethane
75-694
U
0.500
0.0540
ug/L
11.07.13 10.56
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
11.07.13 10.56
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
11.07.13 10.56
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
11.07.1310.56
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
11.07.1310.56
U
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
102
%
53-159
11.07.1310.56
4-Bromofluorobenzene
460-00-4
122
%
30-186
11.07.13 10.56
Toluene-D8
2037-26-5
112
%
70-130
11.07.1310.56
Page 14 of 31 Final 1.000

�«qFp
Certificate of Analytical Results 4734154 PJ A
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-004 Date Collected: 11.04.13 11.00
Analytical Method: TSS by SM2540D
Tech: 4153
Analyst: NV4154
Seq Number: 927184
Parameter
Total Suspended Solids
Cas Number Result RL
U 4.00
% Moisture:
MDL Units Analysis Date Flag Dil
3.50 mg/L 11.07.1316.00 U 1
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR % Moisture:
Analyst: 4150 Date Prep: 11.06.13 13.30
Seq Number: 927017
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
Lead 7439-92-1 U 0.0100 0.00330 mR/L 11.07.1313.42 U 1
Page 15 of 31 Final 1.000

Certificate of Analytical Results 473415
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-004 Date Collected: 11.04.13 11.00
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 927155
Parameter Cas Number
Date Prep:
Result
11.07.13 06.32
RL NWL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
11.07.13 10.29
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
11.07.13 10.29
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
11.07.13 10.29
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
11.07.13 10.29
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
11.07.1310.29
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
11.07.13 10.29
U
1
1,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
11.07.13 10.29
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
11.07.1310.29
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
11.07.13 10.29
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
11.07.13 10.29
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
11.07.1310.29
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
11.07.13 10.29
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
11.07.1310.29
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
11.07.13 10.29
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
11.07.13 10.29
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L.
11.07.1310.29
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
11.07.1310.29
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
11.07.1310.29
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
11.07.13 10.29
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
11.07.1310.29
U
I
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
11.07.13 10.29
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
11.07.13 10.29
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
11.07.1310.29
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
11.07.13 10.29
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L.
11.07.1310.29
U
1
4-Methyl-2-pentanone (MIRK)
108-10-1
U
0.400
0.253
ug/L
11.07.13 10.29
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L.
11.07.1310.29
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
11.07.13 10.29
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
11.07.1310.29
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
11.07.1310.29
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
11.07.1310.29
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
11.07.1310.29
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
11.07.1310.29
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
11.07.13 10.29
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
11.07.1310.29
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
11.07.1310.29
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
11.07.1310.29
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
11.07.1310.29
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
11.07.1310.29
U
1
Page 16 of 31 Final 1.000

�PCCq�,
/r tt�j1'6
Certificate of Analytical Results 473415
rau
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Water Date Received:11.05.13 11.00
Lab Sample Id: 473415-004 Date Collected: 11.04.13 11.00
Analytical Method: VOCs by GC/MS by SM6200B
Tech: MWE
Analyst: MLA
Seq Number: 927155
Parameter
Cas Numbe.
cis-1,2-Dichloroethene
156-59-2
cis-1,3-Dichloropropene
10061-01-5
Dichlorodifluoromethane
75-71-8
Ethanol
64-17-5
Ethylbenzene
100-41-4
Isopropyl ether
108-20-3
Isopropylbenzene
98-82-8
Methyl tert-butyl ether (MTBE)
1634-044
Methylene Chloride
75-09-2
Naphthalene
91-20-3
n-Butylbenzene
104-51-8
n-Propylbenzene
103-65-1
sec-Butylbenzene
135-98-8
Styrene
100-42-5
tert-Butylbenzene
98-06-6
Tetrachloroethene (PCE)
127-18-4
Toluene
108-88-3
trans-1,2-Dichloroethene
156-60-5
trans-1,3-Dichloropropene
10061-02-6
Trichloroethene
79-01-6
Trichlorofluoromethane
75-69-4
Vinyl Acetate
108-05-4
Vinyl Chloride
75-01-4
m,p-Xylenes
179601-23-1
o-Xylene
95-47-6
Surrogate
1,2-Dichloroethane-D4
4-Bromofluorobenzene
Toluene-D8
Prep Method: SM6200B PREP
% Moisture:
Date Prep: 11.07.13 06.32
Result
RL
MDL
Units
Analysis Date
Flag
Dil
U
0.500
0.114
ug/L
11.07.1310.29
U
1
U
1.00
0.100
ug/L
11.07.1310.29
U
1
U
1.00
0.0670
ug/L
11.07.1310.29
U
1
U
50.0
3.00
ug/L
11.07.1310.29
U
1
U
0.500
0.0920
ug/L
11.07.1310.29
U
1
U
0.500
0.0920
ug/L.
11.07.1310.29
U
I
U
0.500
0.0980
ug/L
11.07.1310.29
U
1
U
0.500
0.169
ug/L
11.07.1310.29
U
1
U
0.500
0.190
ug/L
11.07.1310.29
U
1
U
2.00
0.0940
ug/L
11.07.1310.29
U
1
U
2.00
0.0600
ug/L
11.07.1310.29
U
1
U
1.00
0.0650
ug/L
11.07.13 10.29
U
1
U
0.500
0.0920
ug/L
11.07.1310.29
U
1
U
0.500
0.0740
ug/L
11.07.1310.29
U
1
U
0.500
0.0890
ug/L
11.07.1310.29
U
1
U
0.500
0.0540
ug/L
11.07.1310.29
U
1
U
0.500
0.0570
ug/L
11.07.1310.29
U
I
U
0.500
0.188
ug/L
11.07.1310.29
U
1
U
1.00
0.110
ug/L
11.07.1310.29
U
1
U
0.500
0.139
ug/L
11.07.1310.29
U
1
U
0.500
0.0540
ug/L
11.07.1310.29
U
I
U
1.00
0.720
ug/L
11.07.13 10.29
U
1
U
0.500
0.0810
ug/L
11.07.1310.29
U
1
U
1.00
0.176
ug/L
11.07.1310.29
U
1
U
0.500
0.122
ug/L
11.07.1310.29
U
1
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
17060-07-0
103
%
53-159
11.07.1310.29
460-00-4
136
%
30-186
11.07.1310.29
2037-26-5
114
%
70-130
11.07.1310.29
Page 17 of 31 Final 1.000

PURpO�
Certificate of Analytical Results 475240 4f.
Florida Testing Services. LLC
Sample Id: Influent
Lab Sample Id: 475240-001
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Matrix: Ground Water
Date Collected: 12.02.13 13.35
Analytical Method: VOCs by GUMS by SM6200B
Tech: JOL
Analyst: JOL Date Prep: 12.05.13 12.12
Seq Number: 929171
Date Received:12.04.13 10.30
Prep Method: SM6200B PREP
% Moisture:
Parameter
Cas Number
Result
RL
MDL
Units
Analysis Date
Flag
Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
12.05.1320.29
U
I
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
12.05.13 20.29
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
12.05.13 20.29
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L.
12.05.13 20.29
U
1
1, 1 -Dichloroethane
75-34-3
U
0.500
0.121
ug/L
12.05.13 20.29
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
12.05.13 20.29
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
12.05.13 20.29
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
12.05.13 20.29
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
12.05.13 20.29
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
12.05.13 20.29
U
1
1,2,4-Trimethylbenzene
95-63-6
83.4
0.500
0.103
ug/L
12.05.13 20.29
1
1,2-Dibromoethane(EDB)
106-93-4
U
1.00
0.180
ug/L
12.05.13 20.29
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
12.05.13 20.29
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
12.05.13 20.29
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
12.05.13 20.29
U
1
1,3,5-Trimethylbenzene
108-67-8
18.7
0.500
0.0870
ug/L
12.05.13 20.29
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
12.05.13 20.29
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
12.05.13 20.29
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
12.05.13 20.29
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
12.05.13 20.29
U
I
2-Butanone (MEK)
78-93-3
114
20.0
0.378
ug/L
12.05.13 20.29
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
12.05.13 20.29
U
1
2-Hexanone
591-78-6
29.5
0.400
0.352
ug/L
12.05.13 20.29
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
12.05.13 20.29
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
12.05.13 20.29
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
12.05.13 20.29
U
1
Acetone
67-64-1
181
2.00
0.352
ug/L
12.05.13 20.29
1
Benzene
71-43-2
32.2
0.500
0.119
ug/L
12.05.13 20.29
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
12.05.13 20.29
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
12.05.13 20.29
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
12.05.13 20.29
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
12.05.13 20.29
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
12.05.13 20.29
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
12.05.13 20.29
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
12.05.13 20.29
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
12.05.13 20.29
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
12.05.13 20.29
U
1
Chlorofonn
67-66-3
U
0.500
0.172
ug/L
12.05.13 20.29
U
I
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
12.05.13 20.29
U
1
Page 9 of 26 Final 1.000

Certificate of Analytical Results 475240 ,
��e,U
&:;m;;w
..ORat? - o.. a...,.,,.
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Influent Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-001 Date Collected: 12.02.13 13.35
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
Parameter Cas Number
Date Prep:
Result
12.05.13 12.12
RL MDL
Prep Method: SM620OB_PREP
% Moisture:
Units Analysis Date Flag
Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
12.05.13 20.29
U
1
cis- 1,3 -Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
12.05.13 20.29
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
12.05.13 20.29
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
12.05.13 20.29
U
1
Ethylbenzene
100-41-4
31.4
0.500
0.0920
ug/L
12.05.13 20.29
1
Isopropyl ether
108-20-3
41.1
0.500
0.0920
ug/L
12.05.13 20.29
1
Isopropylbenzene
98-82-8
1.18
0.500
0.0980
ug/L
12.05.13 20.29
1
Methyl tert-butyl ether (MTBE)
1634-04-4
2340
50.0
16.9
ug/L
12.05.13 21.03
D
100
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
12.05.13 20.29
U
1
Naphthalene
91-20-3
628
200
9.40
ug/L
12.05.13 21.03
D
100
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
12.05.13 20.29
U
1
n-Propylbenzene
103-65-1
5.03
1.00
0.0650
ug/L
12.05.13 20.29
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
12.05.13 20.29
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
12.05.13 20.29
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
12.05.13 20.29
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L,
12.05.13 20.29
U
1
Toluene
108-88-3
262
50.0
5.70
ug/L
12.05.13 21.03
D
100
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
12.05.13 20.29
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
12.05.13 20.29
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
12.05.13 20.29
U
1
Trichlorofluorometbane
75-69-4
U
0.500
0.0540
ug/L
12.05.13 20.29
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
12.05.13 20.29
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
12.05.13 20.29
U
1
m,p-Xylenes
179601-23-1
129
1.00
0.176
ug/L
12.05.13 20.29
1
o-Xylene
95-47-6
77.3
0.500
0.122
ug/L
12.05.13 20.29
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
104
%
53-159
12.05.13 20.29
4-Bromofluorobenzene
460-00-4
90
%
30-186
12.05.13 20.29
Toluene-D8
2037-26-5
96
%
70-130
12.05.13 20.29
Page 10 of 26 Final 1.000

PUR
Certificate of Analytical Results 475240 \4a
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-002 Date Collected: 12.02.13 13.40
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
Parameter Cas Number
Date Prep:
Result
12.05.13 12.12
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
12.05.1318.21
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
12.05.13 18.21
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
12.05.1318.21
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
12.05.13 18.21
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
12.05.1318.21
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
12.05.13 18.21
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
12.05.13 18.21
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
12.05.13 18.21
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
12.05.1318.21
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
12.05.13 18.21
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
12.05.13 18.21
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
12.05.13 18.21
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
12.05.13 18.21
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
12.05.1318.21
U
1
1,2-Dichloropropane
78-97-5
U
0.500
0.122
ug/L
12.05.13 18.21
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
12.05.1318.21
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
12.05.1318.21
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
12.05.13 18.21
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
12.05.13 18.21
U
I
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L.
12.05.13 18.21
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
12.05.13 18.21
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
12.05.13 18.21
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
12.05.13 18.21
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
12.05.13 18.21
U
I
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
12.05.13 18.21
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
12.05.13 18.21
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
12.05.13 18.21
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
12.05.13 18.21
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
12.05.1318.21
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
12.05.1318.21
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
12.05.1318.21
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
12.05.1318.21
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
12.05.1318.21
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
12.05.13 18.21
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
12.05.1318.21
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
12.05.1318.21
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
12.05.1318.21
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L
12.05.13 18.21
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
12.05.1318.21
U
1
Page 11 of 26 Final 1.000

pC�O
hil Certificate of Analytical Results 475240 LL t
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After AST Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-002 Date Collected: 12.02.13 13.40
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
Parameter Cas Number
Date Prep:
Result
12.05.13 12.12
RL MDL
Units
Prep Method: SM6200B PREP
% Moisture:
Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
12.05.1318.21
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
12.05.13 18.21
U
1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
12.05.13 18.21
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
12.05.1318.21
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
12.05.13 18.21
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
12.05.13 18.21
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
12.05.13 18.21
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
6.46
0.500
0.169
ug/L
12.05.13 18.21
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
12.05.13 18.21
U
1
Naphthalene
91-20-3
3.43
2.00
0.0940
ug/L
12.05.1318.21
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
12.05.13 18.21
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
12.05.13 18.21
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
12.05.13 18.21
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
12.05.13 18.21
U
I
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
12.05.1318.21
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
12.05.13 18.21
U
1
Toluene
108-88-3
0.690
0.500
0.0570
ug/L
12.05.1318.21
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L.
12.05.1318.21
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
12.05.1318.21
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
12.05.1318.21
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
12.05.1318.21
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
12.05.13 18.21
U
1
Vinyl Chloride
75-014
U
0.500
0.0810
ug/L
12.05.13 18.21
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
12.05.13 18.21
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
12.05.13 18.21
U
1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
98
%
53-159
12.05.1318.21
4-Bromofluorobenzene
460-00-4
102
%
30-186
12.05.1318.21
Toluene-D8
2037-26-5
104
%
70-130
12.05.1318.21
Page 12 of 26 Final 1.000

Certificate of analytical Results 475240
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st GAC
Lab Sample Id: 475240-003
Analytical Method: VOCs by GUMS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
P_QRfO
r�u
Matrix: Ground Water Date Received:12.04.13 10.30
Date Collected: 12.02.13 13.45
Date Prep: 12.05.13 12.12
Prep Method: SM6200B PREP
% Moisture:
Parameter
Cas Number
Result
RL
NIDL
Units
Analysis Date
Flag
Dil
1, 1, 1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
12.05.1317.03
U
1
1, 1, 1 -Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
12.05.13 17.03
U
1
1,1,2,2-Tetracbloroethane
79-34-5
U
0.500
0.0700
ug/L
12.05.1317.03
U
I
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
12.05.13 17.03
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
12.05.1317.03
U
1
1, 1 -Dichloroethene
75-35-4
U
0.500
0.104
ug/L
12.05.13 17.03
U
1
1, 1 -Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
12.05.13 17.03
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
12.05.13 17.03
U
1
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
12.05.1317.03
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
12.05.13 17.03
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
12.05.1317.03
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
12.05.13 17.03
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
12.05.1317.03
U
I
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
12.05.1317.03
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
12.05.13 17.03
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
12.05.13 17.03
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
12.05.1317.03
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
12.05.13 17.03
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
12.05.13 17.03
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
12.05.13 17.03
U
1
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
12.05.13 17.03
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
12.05.13 17.03
U
1
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
12.05.1317.03
U
1
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
12.05.13 17.03
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
12.05.13 17.03
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
12.05.13 17.03
U
I
Acetone
67-64-1
U
2.00
0.352
ug/L
12.05.1317.03
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
12.05.1317.03
U
I
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
12.05.13 17.03
U
1
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
12.05.1317.03
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
12.05.1317.03
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
12.05.1317.03
U
I
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
12.05.1317.03
U
I
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
12.05.13 17.03
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
12.05.13 17.03
U
1
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
12.05.1317.03
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
12.05.1317.03
U
1
Chloroform
67-66-3
0.800
0.500
0.172 .
ug/L
12.05.13 17.03
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
12.05.1317.03
U
1
Page 13 of 26 Final 1.000

I " 1
1 ��
Certificate of Analytical Results 475240
eaR!P ....Wm...,.,..
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: After 1st GAC Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-003 Date Collected: 12.02.13 13.45
Analytical Method: VOCs by GC/MS by SM6200B Prep Method: SM620OB_PREP
Tech: JOL % Moisture:
Analyst: JOL Date Prep: 12.05.13 12.12
Seq Number: 929171
Parameter Cas Number Result RL MDL Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
12.05.13 17.03
U
1
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
12.05.13 17.03
U
I
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
12.05.1317.03
U
1
Ethanol
64-17-5
U
50.0
3.00
ug/L
12.05.13 17.03
U
1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
12.05.13 17.03
U
1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
12.05.13 17.03
U
1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
12.05.13 17.03
U
1
Methyl tert-butyl ether (MTBE)
1634-04-4
2.23
0.500
0.169
ug/L
12.05.13 17.03
1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
12.05.13 17.03
U
1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
12.05.13 17.03
U
1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
12.05.13 17.03
U
1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
12.05.13 17.03
U
1
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
12.05.13 17.03
U
1
Styrene
100-42-5
U
0.500
0.0740
ug/L
12.05.13 17.03
U
1
tert-Butylbenzene
98-06-6
U
0.500
0.0990
ug/L
12.05.1317.03
U
1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
12.05.13 17.03
U
1
Toluene
108-88-3
U
0.500
0.0570
ug/L
12.05.13 17.03
U
1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
12.05.13 17.03
U
1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
12.05.13 17.03
U
1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
12.05.13 17.03
U
1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
12.05.13 17.03
U
1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
12.05.13 17.03
U
1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
12.05.13 17.03
U
1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L.
12.05.13 17.03
U
1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
12.05.1317.03
U
1
Surrogate
Cas Number
Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
100
%
53-159
12.05.13 17.03
4-Bromofluorobenzene
460-00-4
118
%
30-186
12.05.1317.03
Toluene-D8
2037-26-5
106
%
70-130
12.05.1317.03
Page 14 of 26 Final 1.000

0
Florida Testing Services, LLC
Certificate of Analytical Results 475240 4 PJIA
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-004 Date Collected: 12.02.13 13.50
Analytical Method: TSS by SM2540D
Tech: BLF
Analyst: NIV
Seq Number: 929357
Parameter
Total Suspended Solids
% Moisture:
Cas Number Result RL MDL Units Analysis Date Flag Dil
U 4.00 3.50 mg/L 12.05.1311.50 U I
Analytical Method: Lead by SW-846 6010C Prep Method: SW3010A
Tech: JDR % Moisture:
Analyst: 4150 Date Prep: 12.06.13 11.45
Seq Number: 929352
Parameter Cas Number Result RL NIDL Units Analysis Date Flag Dil
Lead 7439-92-1 U 0.0100 0.00330 mg/L 12.09.1315.56 U 1
Page 15 of 26 Final 1.000

P«p'
Certificate of Analytical Results 475240 r�u
�'
t
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-004 Date Collected: 12.02.13 13.50
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
Parameter Cas Number
Date Prep:
Result
12.05.13 12.12
RL MDL
Units
Prep Method: SM620OB_PREP
% Moisture:
Analysis Date Flag Dil
1,1,1,2-Tetrachloroethane
630-20-6
U
1.00
0.180
ug/L
12.05.1316.00
U
1
1,1,1-Trichloroethane
71-55-6
U
0.500
0.0760
ug/L
12.05.13 16.00
U
1
1,1,2,2-Tetrachloroethane
79-34-5
U
0.500
0.0700
ug/L
12.05.13 16.00
U
1
1,1,2-Trichloroethane
79-00-5
U
0.500
0.113
ug/L
12.05.13 16.00
U
1
1,1-Dichloroethane
75-34-3
U
0.500
0.121
ug/L
12.05.13 16.00
U
1
1,1-Dichloroethene
75-35-4
U
0.500
0.104
ug/L
12.05.13 16.00
U
1
I,1-Dichloropropene
563-58-6
U
0.500
0.0600
ug/L
12.05.13 16.00
U
1
1,2,3-Trichlorobenzene
87-61-6
U
2.00
0.118
ug/L
12.05.1316.00
U
I
1,2,3-Trichloropropane
96-18-4
U
1.00
0.138
ug/L
12.05.13 16.00
U
1
1,2,4-Trichlorobenzene
120-82-1
U
1.00
0.0690
ug/L
12.05.13 16.00
U
1
1,2,4-Trimethylbenzene
95-63-6
U
0.500
0.103
ug/L
12.05.13 16.00
U
1
1,2-Dibromoethane (EDB)
106-93-4
U
1.00
0.180
ug/L
12.05.13 16.00
U
1
1,2-Dichlorobenzene
95-50-1
U
0.500
0.0940
ug/L
12.05.1316.00
U
1
1,2-Dichloroethane
107-06-2
U
0.500
0.0900
ug/L
12.05.1316.00
U
1
1,2-Dichloropropane
78-87-5
U
0.500
0.122
ug/L
12.05.13 16.00
U
1
1,3,5-Trimethylbenzene
108-67-8
U
0.500
0.0870
ug/L
12.05.13 16.00
U
1
1,3-Dichlorobenzene
541-73-1
U
0.500
0.0980
ug/L
12.05.13 16.00
U
1
1,3-Dichloropropane
142-28-9
U
0.500
0.133
ug/L
12.05.13 16.00
U
1
1,4-Dichlorobenzene
106-46-7
U
0.500
0.0670
ug/L
12.05.1316.00
U
1
2,2-Dichloropropane
594-20-7
U
0.200
0.0970
ug/L
12.05.13 16.00
U
I
2-Butanone (MEK)
78-93-3
U
20.0
0.378
ug/L
12.05.13 16.00
U
1
2-Chlorotoluene
95-49-8
U
0.200
0.0880
ug/L
12.05.13 16.00
U
I
2-Hexanone
591-78-6
U
0.400
0.352
ug/L
12.05.13 16.00
U
I
4-Chlorotoluene
106-43-4
U
0.500
0.0900
ug/L
12.05.13 16.00
U
1
4-Isopropyltoluene
99-87-6
U
0.500
0.0890
ug/L
12.05.13 16.00
U
1
4-Methyl-2-pentanone (MIBK)
108-10-1
U
0.400
0.253
ug/L
12.05.13 16.00
U
1
Acetone
67-64-1
U
2.00
0.352
ug/L
12.05.13 16.00
U
1
Benzene
71-43-2
U
0.500
0.119
ug/L
12.05.13 16.00
U
1
Bromobenzene
108-86-1
U
0.500
0.132
ug/L
12.05.1316.00
U
I
Bromochloromethane
74-97-5
U
0.500
0.112
ug/L
12.05.1316.00
U
1
Bromodichloromethane
75-27-4
U
0.500
0.124
ug/L
12.05.1316.00
U
1
Bromoform
75-25-2
U
2.00
0.159
ug/L
12.05.1316.00
U
1
Bromomethane
74-83-9
U
1.00
0.0970
ug/L
12.05.1316.00
U
1
Carbon tetrachloride
56-23-5
U
0.500
0.0990
ug/L
12.05.13 16.00
U
1
Chlorobenzene
108-90-7
U
0.500
0.105
ug/L
12.05.13 16.00
U
I
Chlorodibromomethane
124-48-1
U
0.500
0.177
ug/L
12.05.1316.00
U
1
Chloroethane
75-00-3
U
0.500
0.0420
ug/L
12.05.13 16.00
U
1
Chloroform
67-66-3
U
0.500
0.172
ug/L,
12.05.13 16.00
U
1
Chloromethane
74-87-3
U
0.500
0.0850
ug/L
12.05.1316.00
U
1
Page 16 of 26 Final 1.000

Certificate of Analytical Results 475240 f`
t9BQRBT9�.
Florida Testing Services, LLC
Terraquest Environmental Consultants, P.C., Mebane, NC
Coliseum Shell
Sample Id: Effluent Matrix: Ground Water Date Received:12.04.13 10.30
Lab Sample Id: 475240-004 Date Collected: 12.02.13 13.50
Analytical Method: VOCs by GC/MS by SM6200B
Tech: JOL
Analyst: JOL
Seq Number: 929171
Parameter Cas Number
Date Prep:
Result
12.05.13 12.12
RL MDL
Prep Method: SM6200B PREP
% Moisture:
Units Analysis Date Flag Dil
cis-1,2-Dichloroethene
156-59-2
U
0.500
0.114
ug/L
12.05.13 16.00
U I
cis-1,3-Dichloropropene
10061-01-5
U
1.00
0.100
ug/L
12.05.13 16.00
U 1
Dichlorodifluoromethane
75-71-8
U
1.00
0.0670
ug/L
12.05.13 16.00
U 1
Ethanol
64-17-5
U
50.0
3.00
ug/L
12.05.13 16.00
U 1
Ethylbenzene
100-41-4
U
0.500
0.0920
ug/L
12.05.13 16.00
U 1
Isopropyl ether
108-20-3
U
0.500
0.0920
ug/L
12.05.13 16.00
U 1
Isopropylbenzene
98-82-8
U
0.500
0.0980
ug/L
12.05.1316.00
U I
Methyl tert-butyl ether (MTBE)
1634-04-4
U
0.500
0.169
ug/L
12.05.13 16.00
U 1
Methylene Chloride
75-09-2
U
0.500
0.190
ug/L
12.05.13 16.00
U 1
Naphthalene
91-20-3
U
2.00
0.0940
ug/L
12.05.1316.00
U 1
n-Butylbenzene
104-51-8
U
2.00
0.0600
ug/L
12.05.13 16.00
U 1
n-Propylbenzene
103-65-1
U
1.00
0.0650
ug/L
12.05.13 16.00
U I
sec-Butylbenzene
135-98-8
U
0.500
0.0920
ug/L
12.05.13 16.00
U 1
Styrene
100-42-5
U
0.500
0.0740
ug/L
12.05.1316.00
U 1
tert-Butylbenzene
98-06-6
U
0.500
0.0890
ug/L
12.05.13 16.00
U 1
Tetrachloroethene (PCE)
127-18-4
U
0.500
0.0540
ug/L
12.05.13 16.00
U 1
Toluene
108-88-3
U
0.500
0.0570
ug/L
12.05.1316.00
U 1
trans-1,2-Dichloroethene
156-60-5
U
0.500
0.188
ug/L
12.05.13 16.00
U 1
trans-1,3-Dichloropropene
10061-02-6
U
1.00
0.110
ug/L
12.05.13 16.00
U 1
Trichloroethene
79-01-6
U
0.500
0.139
ug/L
12.05.13 16.00
U 1
Trichlorofluoromethane
75-69-4
U
0.500
0.0540
ug/L
12.05.1316.00
U 1
Vinyl Acetate
108-05-4
U
1.00
0.720
ug/L
12.05.13 16.00
U 1
Vinyl Chloride
75-01-4
U
0.500
0.0810
ug/L
12.05.13 16.00
U 1
m,p-Xylenes
179601-23-1
U
1.00
0.176
ug/L
12.05.13 16.00
U 1
o-Xylene
95-47-6
U
0.500
0.122
ug/L
12.05.1316.00
U 1
Surrogate
Cas Number Recovery
Units
Limits
Analysis Date
Flag
1,2-Dichloroethane-D4
17060-07-0
99
%
53-159
12.05.13 16.00
4-Bromofluorobenzene
460-00-4
129
%
30-186
12.05.1316.00
Toluene-D8
2037-26-5
108
%
70-130
12.05.1316.00
Page 17 of 26 Final 1.000