Loading...
HomeMy WebLinkAboutWQ0000430_More Information (Received)_20200415o�0F w a rF,�QG State of North Carolina Department of Environment and Natural Resources Division of Water Quality ft 'C LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 08-11 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information or for an electronic version of this form, visit the Land Application Unit (LAU) web site at. http: //portal. ncdenr. org/webhvg/aps/lau General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 08-11 or FORM: SDR 08-11). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 08-11): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: LASC 08-11) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ® For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: ® The status of the land application site with respect to this residuals land application program must be provided in table L The status categories and their corresponding codes are as follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ® Attach the following in accordance with each status code: Status Code Required Item N R T M County Manager Notification W y Land Owner Agreement (If applicable) Setback Waiver Agreement An updated vicinity/setback map in accordance with the "Map Guidance for Residuals Land Application Permits" ✓ ✓ ✓ A soils and agronomic evaluation in accordance with the "Soil Scientist ✓ Evaluation Policy" An updated accounting of the land application site's cumulative ✓ ✓ pollutant loading rates (CPLRs) INSTRUCTIONS FOR FORM: LASC 08-11 Page 1 of 3 Required Item Status Code N R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly ✓ ✓ ✓ indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Permittee relinquishing field ✓ Acknowledgement of field transfer from Land Owner (Fields may not ✓ be permitted to multiple Permittees over the same time period) * This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ® Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ® For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. ® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Digital or Raw Photo Extraction (EXT) • Aerial Photography with Ground Control (AER) • Geodetic Quality GPS Survey (GEO) • Cadastral Survey (SUR) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS (GPS) • Conversion from Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Mere (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) ® Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ® Surface water body classifications information may be found at: http://portal.ncdenr.ora/web/wq/�s/csu ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: http://portal.ncdenr.ora/web/wg/home/ro ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link hU://h2o.enr.state.nc.us/bims/reports/reportsWB.htrnl. If this link does not work, open http://portal.ncdenr.org/web/wg//s/csu/classifications and download weekly -updated classification lists for named waterbodies. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Error! Objects cannot be created from editing field codes. Basin sorted Error! Objects cannot be created from editing field codes. report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 08-11 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in Error! Objects cannot be created from editing field codes. county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B .030l(i). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified 'B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "SC." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 08-11 Page 3 of 3 Applicant's name: City of CheMnAlle Land application sites currently certified: 78.3 net acres and Total to be certified: 116.6 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Predominant Soil Status Codes Site/Field ID Landowners O Lessees or Operator(s) O Net Acres Count y Crop(s) s pO Series Name Mapping Unit or Rep. Slope° R NC-LT-120-02 Wayne Gilbert 27.6 Lincoln Fescue (hay) Cecil CeB2 R NC-LT-120-03 Wayne Gilbert 11.0 Lincoln Row Crops Cecil CeB2 D NC-LT-124-01 Keith Beam Keith Beam 30.0 Lincoln Fescue (pasture) Cecil CeB2 D NC-LT-124-02 Keith Beam Keith Beam 10.1 Lincoln Fescue (pasture) Pacolet PeC2 R NC-LT-107-01 Jason Huitt 10.7 Lincoln Fescue (pasture) Cecil CeB2 R NC-LT-107-02 Jason Huitt 12.0 Lincoln Fescue (pasture) Cecil CeB2 R NC-LT-107-03 Calvin Wehunt 17.0 Lincoln Corn(silage), Sorghum, Cecil CeB2 Sudex N NC-LT-107-04 Calvin Wehunt 10.9 Lincoln escue (pasture) Corn(silage), Rion Somhum, Sudex N NC-LT-107-05 Calvin Wehunt 17.8 Lincoln Fescue (pasture) Corn(silage), Cecil CeB2 Sorghum, Sudex N NC-LT-107-06 Calvin Wehunt 9.5 Lincoln Fescue (pasture) Corn(silage), Cecil CeB2 Somhum, Sudex a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) C. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed Class NC-LT-107-04 35.4737 -81.4674 NAD 83 MAP Second Little Buffalo Creek WS-111 WS-111 NC-LT-107-05 35.4717 -81.4664 NAD 83 MAP Second Little Buffalo Creek WS-111 WS-111 NC-LT-107-06 35.4701 -81.4633 NAD 83 MAP Second Little Buffalo Creek WS-111 WS-111 o�0F w a rF,�QG State of North Carolina Department of Environment and Natural Resources Division of Water Quality ft 'C RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 08-11 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more information or for an electronic version of this form, visit the Land Application Unit (LAU) web site at: http: //portal. ncdenr. org/webhvq/aps/lau General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 08-11, FORM: DCAR 08-11, or FORM: SDR 08-11). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 08-11): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 08-11) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 08-11 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: City of Cherryville Status Code ° Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current n Proposed R City of Cherryville City of Cherryville WWTP Gaston NCO044440 273 273 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 08-11 Page 1 o�0F w a rF,�QG State of North Carolina Department of Environment and Natural Resources Division of Water Quality ft 'C RESIDUALS SOURCE CERTIFICATION FORM: RSC 08-11 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: City of Cherrvville WWTP 2. Facility permit holder is: ❑ Federal, 0 State, Local Government, or 11 Private. Facility permit issued by: U Div. of Water Quality, Div. of Environmental Health, or W Other (explain: �). 3. Facility contact person and title: Larry Wright, Plant Supervisor, ORC Complete mailing address: 116 South Mountain Street City: Cherryville State: NC Zip: 28021 Telephone number: (704) 214-1162 E-mail address: lwrightkcityofcherryville.com 4. Facility physical address: 736 Tot Dellinger Road City: Cherryville State: NC Zip: 28021 Coordinates: Latitude: 35' 24' 51" Longitude: 81' 22' 08" Datum: NAD83 Level of accuracy: Second Method of measurement: MAP 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: 2.0 MGD and facility average daily flow: 350,000 MGD 8. Average amount of residuals being generated at this facility 108.0 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: sludge holding tank: 248,000 gallons Type and volume of residuals storage (i.e., outside of residuals treatment units): sludge lagoon: 250,000 gallons II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological FORM: RSC 08-11 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: " yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental Technologies, Inc. and Date(s) of analysis: 06/05/2019 Passed corrosivity test: 0 yes ❑ no. pH: 7_1 s.u. (2 < pH < 12.5) Passed ignitability test: 0 yes Ld no. Flashpoint: >140 OF (> 140°F) Passed reactivity test: W yes ❑Ino. HCN: nd mg/kg (<250) & H2S: nd mg/kg (<500) TCLP Parameter Limit (m917) Result (m917) TCLP Parameter Limit (m917) Result (m917) Arsenic 5.0 nd Hexachlorobenzene 0.13 nd Barium 100.0 nd Hexachloro-1,3-Butadiene 0.5 nd Benzene 0.5 nd Hexachloroethane 3.0 nd Cadmium 1.0 nd Lead 5.0 nd Carbon Tetrachloride 0.5 nd Lindane 0.4 nd Chlordane 0.03 nd Mercury 0.2 nd Chlorobenzene 100.0 nd Methoxychlor 10.0 nd Chloroform 6.0 nd Methyl Ethyl Ketone 200.0 nd Chromium 5.0 nd Nitrobenzene 2.0 nd m-Cresol 200.0 nd Pentachlorophenol 100.0 nd o-Cresol 200.0 nd Pyridine 5.0 nd p-Cresol 200.0 nd Selenium 1.0 nd Cresol 200.0 nd Silver 5.0 nd 2,4-D 10.0 nd Tetrachloroethylene 0.7 nd 1,4-Dichlorobenzene 7.5 nd Toxaphene 0.5 nd 1,2-Dichloroethane 0.5 nd Trichloroethylene 0.5 nd 1, 1 -Dichloroethylene 0.7 nd 2,4,5-Trichlorophenol 400.0 nd 2,4-Dinitrotoluene 0.13 nd 2,4,6-Trichlorophenol 2.0 nd Endrin 0.02 nd 2,4,5-TP (Silvex) 1.0 nd Heptachlor and its Hydroxide 0.008 nd Vinyl Chloride 0.2 nd FORM: RSC 08-11 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: WayPoint Analytical and Date of analysis: 05/24/2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 <5.0 Cadmium 85 39 2.57 Copper 4,300 1,500 996 Lead 840 300 34.7 Mercury 57 17 2.15 Molybdenum 75 n/a 8.44 Nickel 420 420 70.8 Selenium 100 100 <5.0 Zinc 7,500 2,800 897 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) N > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 08-11 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 4.51 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 05/24/2019 Parameter Result (mglkg) Aluminum 16,500 Ammonia -Nitrogen 4,220 Calcium 7,590 Magnesium 2,230 Nitrate -Nitrite Nitrogen 195 pH (Standard Unit) 6.7 Phosphorus 12,900 Potassium 1,700 Sodium 833 Total Kjeldahl Nitrogen 31,800 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.56 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): JJ default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: This is a default value for water treatment plant alum residuals. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (15) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 10,579 15,960 Inj ection/Incorporation 12,689 18,070 Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: No FORM: RSC 08-11 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): q Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. q Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. q Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, 0 heat drying, heat treatment, ❑ thermophilic aerobic digestion, beta ray irradiation, ❑ gamma ray irradiation, or pasteurization. b. For Land Application of Class B. Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ® aerobic digestion, I air drying, EI anaerobic digestion, LJ composting, or lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. E] Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). E] Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. E] Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. E] Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. E] Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. E] Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. q Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. n Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 08-11 Page 5 of 5 SPILL RESPONSE PLAN PROJECT: City of Cherryville Permit W00000430 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the City of Cherryville or the NC Department of Transportation, and other private contractors as necessary. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation, i.e., local farmers, farm supply centers, nurseries, etc. 4. CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION: As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central office, and they will then be responsible for notifying other key Synagro personnel. 7. REPORTING: Synagro Central personnel will notify the Mooresville Regional office for The City of Cherryville WWTP as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Operations Manager shall provide a written report within 48 hours of the spill to the Technical Services Manager. The report shall list all relative information and actions taken. Synagro Central personnel will file a written report to the Mooresville Regional office of the NCDENR within 5 days of the occurrence. For after hours reporting the Division's emergency number shall be called to report all incidences (800-662-7956 or 800-858-0368 or 919-733-3300) Contact Numbers: Mocksville Regional Office- 336-790-1610 Waypointo ANALYTICAL 4/14/2020 Synagro Central LLC/ Cherryville Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 20-099-0001 Project Description: Calvin Wehunt Cherryville WWTP LT-107 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 4/8/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pam« mar,-- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 • 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-099-0001 Client Project Description: Calvin Wehunt Cherryville WWTP LT-107 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 70986 4 Solids 04/08/2020 SW-7471B WP MTN 70987 5 Solids 04/08/2020 SW-7471B WP MTN 70988 6 Solids 04/08/2020 SW-7471B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 7 WayPANALYTICAL 46442 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Cherryville Alex Fox Mary Brewer Project Calvin Wehunt Report Date : 04/14/2020 284 Boger Road Information : Cherryville WWTP Received : 04/08/2020 Mocksville , NC 27028 LT- 107 mL 60wr Submitted By : Alex Fox Pauric McGroary Report Number : 20-099-0001 REPORT OFANALYSIS Agronomist Lab No : 70986 Matrix: Solids Sample ID : 4 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0256 mg/Kg 0.0148 1 04/13/2011:19 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 7 WayPANALYTICAL 46442 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Cherryville Alex Fox Mary Brewer Project Calvin Wehunt Report Date : 04/14/2020 284 Boger Road Information : Cherryville WWTP Received : 04/08/2020 Mocksville , NC 27028 LT- 107 mL 60wr Submitted By : Alex Fox Pauric McGroary Report Number : 20-099-0001 REPORT OFANALYSIS Agronomist Lab No : 70987 Matrix: Solids Sample ID : 5 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0225 mg/Kg 0.0152 1 04/13/2011:20 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 WayPANALYTICAL 46442 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Cherryville Alex Fox Mary Brewer Project Calvin Wehunt Report Date : 04/14/2020 284 Boger Road Information : Cherryville WWTP Received : 04/08/2020 Mocksville , NC 27028 LT- 107 mL 60wr Submitted By : Alex Fox Pauric McGroary Report Number : 20-099-0001 REPORT OFANALYSIS Agronomist Lab No : 70988 Matrix: Solids Sample ID : 6 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0540 mg/Kg 0.0146 1 04/13/2011:22 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 5 of 7 WayPAoInt.. NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46442 Customer Name: Synagro Central LLC/ Cherryville Report Number: 20-099-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab ® UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No ! Not Present Custody seals intact on sample bottles? 0 Yes 0 No ® Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes ® No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes ® No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes ® No Comments: Signature: lBrandi Watson Date & Time: 04/08/2020 09:59:41 Page 6 of 7 Waypoint.0 ANALYTICAL 5 III ir���� 1111111111111111111 IN ti1i 46"2 ��, Svnawa Central LLC. w Cherrille fl4-08-2026 calvm 1Nehunl 09 58.07 Account # Grower/Project Information _ nformation t14k_11__ Submitted By Charge To L',/ V Farm ID Field ID Credit Card # CSV Exp. Date. Phone # 76 E-mail address S Crop Info For Recommendations Sample ID Lab Number (Lab Use Only) SIM S2M - Specify additional Tests S3M Soluble Sall's Texture NOa-N Additional Tests Intended Crop Yield Goal Alternative Crop Yield Goal previous Crop B Cu Fe Mn Na 5 Zn s u Mehlich III Test Mackages Special Instructions or Additional Tests S1M - Organic matter, Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH Cation Exchange Capacity, and % Base Saturation. S2l'JI - Test S1 M plus any two of the following: Sodium, Sulfur, Boron, Zinc, Manganese, Iron, Copper. Each additional test (above two) cost 100. PM - Test S 1 M pi us Sodium, Sulfur, Boron, Zinc, Manganese, Capper, and iron. J4 fC u P � %VS R (older, more conservative method) %VS in 0.5483 Enter in %VS Out F 0.4953 decimal form %VSR= (%VS in - %VS out) ((%VS in - (%VS in x %VS out)) %VSR= 19.15 (method from p.132 of WH manual) %VSR= (%VS in - %VS out) %VS in %VSR= 9,67 Results must be either greater than 38%; less than 17% for a 40-day bench - scale test; or less than 15% for a 30-clay bench -scale test. Analytical Results Synagro 284 Boger Rd. Mocksville, NC 27028 Receive Date: 01/20/2020 Reported: 02/28/2020 For: Cherryville WWTP Comments: Geometric Mean: 1265 MPN/g STATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 200120-20-01 Fecal Coliforms 1 3553 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-01 Percent Solids 1 3.94 % SM254OB-2011 01/20/2020 MD 200120-20-02 Fecal Coliforms 2 875 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-02 Percent Solids 2 4.57 % SM254OB-2011 01/20/2020 MD 200120-20-03 Fecal Coliforms 3 897 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-03 Percent Solids 3 4.46 % SM25408-2011 01/20/2020 MD 200120-20-04 Fecal Coliforms 4 2477 A1fPNlg SM9221CF-2000 01/20/2020 MD 200120-20-04 Percent Solids 4 4.44 % SM254OB-2011 01/20/2020 MD 200120-20-05 Fecal Coliforms 5 406 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-05 Percent Solids 5 4.93 % SM2546B-2011 01/20/2020 MD 200120-20-06 Fecal Coliforms 6 412 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-06 Percent Solids 6 4.86 % SM25408-2011 01/20/2020 MD 200120-20-07 Fecal Coliforms 7 4474 MPNIg SM92210E-2006 01/20/2020 MD 200120-20-07 Percent Solids 7 3.8 % SM25408-2011 01/20/2020 MD 200120-20-08 30 Day Benchscale Cherryville 19.2 % EPA625-R-9210 01/20/2020 WC WWTP Respectfully submitted, & _w1n, jll�lt ') Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NCO0909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page t of 9 Condition of Receipt Sample Number 200120-20-01 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-02 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-03 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-04 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-05 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 9 Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-06 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Sample Number 200120-20-07 Temp on Arrival: 3.5 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200120-20-08 Temp on Arrival: 3.5 Parameter Schedule: Chemicals in containers, lab Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 9 Criern: d �TATESVILLE ANALYTICAL L Address: P A 2-v / JC /� 122 Court Street t - ] :[). Eiez L''S SLWC�vllle. NC 214687 _ 170,11 97'---iA97 Ch:lil! Of Custody Record Contact Person_ Phone #It Ees. FAXJt PO # Requisitioned by: X (l me aI I ��� rp / rQ Customer Sample IDA Lab-1D a Time 5arnpted (Grate Only) Dole Sampled (Grab Only) Matra ww I':muncicn requested fnra�mlvgia Z 0 0 Co � Q 30 D, OS Relinquished by: Time arn. p !Z� Z-0 Sampled by: Received by: Time P 469 ame Date 144724 Transported by: S Relinquished by: Time am, pm Date �1-1— Holding times met: Received by: Time am, pm Date �1�/ Compliance work: X Composite Sa�kln _C Time begin am. pm Date 11 Non-compliance work: Time end am, pm Date �1 !�. Lab Comments: Samples Transported On lta: Composite Sampling#2: Time begin am, pm Date __I__I_. Time end pm Date. I�l__ --am. Initials: n 00 t,p 00 N U Z 0i t11 V) 00 (V N X O m 0 t1 Sample #: 200120-20-08 Client: Synagro 0yn�0 30 Day Bench Test- Aerobic Sample Name: Cherryville WWTP; Collect Dt: Jar: 20 2020 11:15AM Elm EPA625-R-9210 SM 5Q0 ,2111 Tests: 30 Day !late began: 'l} `, i Digester Dimensions: Analyst: Volume of sample in digester: mis rinse Started: Initial DO reading of sample: 'j � (>2) initial Dav DO: 3J (>2) Tens ; 6i C Day DO- J-µ14 (>2) Temp:X, C Date: Time: �Date: 1 17 , ime f l nl, % Total Solids % Total Solids Dish #: 10 _ Dish #: 10 Dry Wt.-' Dish Wt.: Dry Wt. + Dish Wt,: — �. � q— Dish Wt,: Dish Wt,-, _ 1� S a m p I c Wt.: 1 u Sample Wt.: _- %Total Solids: %Total Solids: Ye Volatile Solids % Volatile Solids Dry Wt,& Dish Wt,: 4-3 3 ! Dry WU Dish Wt.: �f 2S j Ash Wt.: A�f Ash Wu tt Sample Wt.: % T Sample Wt.: % Vol. Solids: y % Vol. Solids: Yo Total Solids % Total Solids Dish tk Ui Dish #: ,{ Dry Wt. + Dish Wt.: tl / 7 ,.�_ Dry Wt. +Dish Wt.: _4 Dish Wt.. Dish Wt.: -- Sample Wt.: �"? _ Sample Wt.: _ % Total Solids: % Total Solids: Yo Volatile Solids % Volatile Solids Dry Wt.& Dish Wt.. 1 Dry Wt,& Dish Wt.: 41)0��� Ash Wt.: lQ Ash Wt.: - Sample Wt.: Sample Wt,: % Vol. Solids: ........ Z % Vol. Solids: r Yo Total Solids( % Total Solids Dish 9:y Dish ft: Dry Wt. + Dish Wt.: 1. Dry Wt. i- Dish Wt.: �} Dish Wt.: Dish Wt.: Sample Wt.:_ _ Sample Wt.: % Total Solids: % Total Solids: Yo Volatile Solids % Volatile Solids ' Try Wt,& Dish Wt,: CD _ _ Dry Wt.& Nish Wt.: Ash Wt.: 5 Ash Wt,: k ' Sample Wt.: - Sample Wt,: _ °/u Vol. Solids: �. y I % Vol. Solids: --- [Type here] PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 9 Sample 1D# Dar 12 DO: •7 5 (>2) m T �p :`�.61 C Date: 2 � Time: OU Day, 18 DO: 3.�fi (>2) Temp: q C 9- hne: Date: Yo Total Solids 1 % Total Solids Dish #: 1 Dish #: Dry Wt. + Dish Wt.: Dry Wt. + Dish Wt.: , �Q Dish Wt.: Dish Wt.: Sample Wt.: Sample Wt.: %'Total Solids: _ O. !� 4 % Total Solids: Ye Volatile Solids 1 ,, % Volatile Solids Dry Wt.& Dish Wt.: Dry Wt.& Dish Wt.: q4. 1el3 Ash Wt,: Ash Wt.. Q, Sample Wt.: Sample WL: % Vol. Solids: 0. r' % Vol. Solids: Yo Total Solids Dish #: % Total Solids / Dish #: "! Dry Wt. + Dish Wt,: Dry Wt. + Dish Wu !7 Dish Wt.: Dish Wt.: Sample Wt.: Sample Wt.: % Total Solids: d. '�/ _ % Total Solids: Yo Volatile Solids % Volatile Solids lx Dry Wt.& Dish Wt.: 4cl. iMq Dry Wt.& Dish Wt Ash Wt.: Ash Wt.. D? Sample Wt.: �� �/� Sample Wt.: % Vol. Solids: �, 3 r % Vol. Solids: Yo Total Solids , j , Dish #: �-1` % Total Solids Dish #: Dry Wt, + Dish Wt.: Dry Wt. + Dish Wt.: !i 9 Dish Wt.: Dish Wt: Sample Wt.: Sample Wt.: % Total Solids: % Total Solids: .......Y..SC A Volatile Solids nn Dry WU Dish A-Vi 53LOC % Volatile Solids Wt.: . Dry Wt.& Dish Wt.: Ash Wt.: Ash Wt.: ! •� Sample Wt.: Sample Wt,: % Vol. Solids: % Vol. Solids: 0, qj [Type here] PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 9 Sample ]DO ._ 41611261_ 9g a Dav24 DO: (>2) Temp: .�% C Day 30 DO '7, ��' (>2} Temp: Date 2 m Time• 62Q1j Date: 2 Time: dQ . Total Solids % Total Solids Dish #: /Z Dish#: Dry Wt. + Dish Wt.: S�. ;A // _...._ . Dry Wt. + Dish Wt: DishWt.:... jy /.4 Dish Wt: L 19 Sample Wt.-. 5 Sample Wt: , % Total Solids: n, ^tZ % Total Solids. Yo Volatile Solids % Volatile Solids Dry Wt. & Dish Wt.: 5a, ull Dry Wt. & Dish Wt: i _ 96 f3 Ash Wt.: ___.. fo,..,Zj/,3 Ash Wt: _ 7146 Sample Wt.: Sample Wt: 15 % Vol. Solids: — Q_ �/s % Vol Solids: Yo Total Solids % Total Solids Dish #: _ ,� Dish#: i Dry Wt. + Dish Wt.: Vtf, 316,94 Dry Wt. + Dish Wt:.., tf k, 7452 Dish Wt.: VV Z 02-4 . Dish Wt: Qftf. Sample Wt.; '15-41146�_ Sample Wt: r` %Total Solids: Q, 7/cr %Total Solids: Yo Volatile Solids % Volatile Solids Dry Wt. & Dish W€.: q, Jgg.f Dry Wt. & Dish Wt: x Ash Wt.- �! _ z993 Ash Wt: Sample Wt.: Sample Wt: Zr % Vol. Solids: d(e % Vol Solids: Yo Total Solids % Total Solids Dish #: p Dish#: Dry Wt. -* Dish Wt.: -T/. 04 Dry Wt. + Dish Wt: Dish Wt.: 51. j / 56 Dish Wt: Sample Wt.: Z6 Sample Wt: 2 ,- % Total Solids: !1 `l2 % Total Solids: Yo Volatile Solids % Volatile Solids Dry Wt. & Dish Wt.: „�!- itQ 73 Dry Wt. & Dish Wt: Ash Wt.: Yl2YZ _ Ash Wt: V6. 524'z Sample Wt.: Sample Wt: 7 5 % Vol. Solids: Q., .i (e % Vol Solids: [Type here] PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 9 VOTE: oil/particle free air was supplied to the bottom of the Digester via a porous stone at a rate sufficient to mix the ;ample 10 day bench checklist —COMPLETE DAILY Sample v( I�X,ob **DO METER CALIBRATION" Da Water level Sample Temp 2OX Scrape Sollds/Mi DO Meter % DO Meter 'I'em °C DO Meter Calm 1. Comments 1 i 2I• � 2 A qX.2 22 . -7 0 Z 22.3G 1 t5- E;-1 4 3 _ �5•2 21. -71 6 l 2 7 b 2 . LP . 5 8 U 5 2 3 � 0 22.57 37 10 1l2 G10 21• 54 12 . l j -- 13 2.q . 14 2-2 , 00' ?. 20 . 15 qT 1 23.1 3 160 17 i ,�` q -7 . 9 7 , z 23 . I 21,07 .30 - b. U LP 18 12 C)-1.2 2.2.24 l9 5 2 •' 1 20 21 f 22.1 22 1 23 Ib. D 24 p 1 25 26 _..... 2 Z. 27 5 �_._._...._. 26 1P ✓ 29 30 ✓ , DI 7 !_ tt— [Type here] PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 8 of 9 30 Day Bench Worksheet Sample 11) #1001110. MA WEEK 1 Samples I Total Solids Volatile Solids % Volatile Fraction 1 1. 7 -7U 2 rj2 .1530 3 1j414 Average: 0 . C) {p 0. 53 0 • 4'9 WEEK 2 Sam les Total Solids Volatile Solids % Volatile Fraction 1 �3 z 0 `t - 5057 3 1 1 2 ,T -46i 3 Average: 1 I -0-4 0.52..O. 50-3 WEEK 3 —Samples Total Solids Volatile Solids % Volatile Fraction 1 0-35 D,5 72. 2 `71 3 3 0_ 3CI 0. Average: d. 7 50-a 0.4s,62 WEEK 4 Samples I Total Solids Volatile Solids % Volatile Fraction I -'7 d.3 7 2 0. CIO 0.43 0 1 `l I O. ..Average; $ j p . 393 q WEEK 5 Samples Total Solids Volatile Solids % Volatile Fraction 1 " U0 2 rl '1 l7 3 Average. 0. 7 9` Q . (p 01 5000 WEEK 6 Samples I Total Solids Volatile Solids % Volatile Fraction 0 0 3 5 0 2 0.71 0.35 0. 3 3 O. Q, 2 Avera e• . 10 0-4PS5 0.5g83-0.140153 �Ioo G•543-M5Ur�=3X O.u0153) Van Kleeck Reduction: Initial % Vol. Frac. - °/a Finat Vol. Frac. X 100 = % 01 514 ?3- 0. 12-1 U Initial % Vol. Frac. — ( Initial % Vol. Frac. X Final % Vol. Frac) 1 p, 53 x !aa FINAL. RESULT % OCl— q__ — � 0/ 0) PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 9 of 9