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Home My WebLink AboutNCS000115_MONITORING INFO_20190708STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. 1 DOC TYPE ❑FINAL PERMIT b4 MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE z)U I b ❑ I YYYYMMDD STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS.0001 15 EECEIVED JUL D S 2919 FACILITY NAME Novozyrnes,_NA Inc. i i um_ FILES PERSON COLLECTING SAMPLE(S) Joe Ladd �Y iy St, i juN CERTIFIED LABORATORY(S) Enco Labs Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Franklin PHONE NO. 9(119-_) 494-3000 aREO ATURE OF PERMITTEE OR DESIGNEE UIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall pH BOD COD TSS mo/dd/ r MG inches 1 6/20/2019 1.0" 7.8 T8 44 86 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Dyes @no (if yes, complete Pan B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&GITPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/ddl r MG inches m m unit gaumo Form SWU-247, last revised 611212015 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 6120/19 Total Event Precipitation (inches): 1.0 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable— see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7/1 /2019 ' (Signature of Permee) (Date) Form SWU-247, last revised 611212015 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000115 FACILITY NAME Novozymes, NA Inc. _ PERSON COLLECTING SAMPLE(S) Joe Ladd CERTIFIED LABORATORY(S) Enco Labs Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Franklin PHONE NO. 9( 19 ) 494-3000 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall pH BOD COD TSS moldd/ r MG inches 2 6/20/2019 1.0" 7.2 28 69 54 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Oyes ono (if yes, complete Part B) Part B: Vehicle Maintenance Acti ity MonitoringRe uirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage moldd/ r MG inches mg/1 m unit al/mo Form SWU-247, Iasi revised 611212015 Page I oft STORM EVENT CHARACTERISTICS: Date 6/20/19 Total Event Precipitation (inches): 1.0 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7/ 1 /2019 (Signature of Permittee) (Date) Form SWU-247, last revised 611212015 Page 2 of 2 ENCO Laboraton'es Accurate. Timely. Responsive. Innovative. 102-A woodwinds industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, July 1, 2019 Novozymes North America (NO008) Attn: Joe Ladd 77 Perry Chapel Church Road Franklinton, NC 27525 RE: Laboratory Results for Project Number: [none), Project Name/Desi 5tormwater Testing ENCO Workorder(s): CC00484 Dear Joe Ladd, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, June 21, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OWLC---�0 Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outtall 1 Lab ID: CC00484-01 Sampled: 06/20/19 16:15 Received: 06/21/19 08:48 Paramete Preparation Hold Date/Time(sl Prep DatelTime(s) Analysis DatelT1mefsl SM 254OD-2011 NO PREP 06/27/19 06/25/19 12:51 06/25/19 12:51 SM 5210 8-2011 NO PREP 06/22/19 16:15 06/21/19 12:05 06/21/19 12:05 SM 5220D-2011 Same 07/18/19 06/25/19 11:19 06/25/19 18A2 Client ID: Outtall 2 Lab ID: CC00484-02 Sampled: 06/20/19 16:30 Received: 05/21/19 08:48 Parameter Preparation Hold Da /Time(sl Preo DatelTime(slAnalysis Dall/rime(sl SM 254OD-2011 NO PREP 06/27/19 06/24/19 12:16 06/24/19 12:16 SM 5210 8-2011 NO PREP 06/22/19 16:30 06/21/19 12:05 06/21/19 12:05 SM 5220D-2011 Same 07/18/19 06/25/19 11:19 06/25/19 18:12 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 www.encolabs.com SAMPLE DETECTION SUMMARY I Client ID. Outfall 1 Lab ID: CCDO484-01 AaalYSS Results fwa MU EQL units Method Notes Biochemical Oxygen Demand 7.8 2.0 2.0 mg/L SM 5210 8-2011 Chemical Oxygen Demand 44 10 10 mg/L SM 5220D-2011 Total Suspended Solids 86 12 12 mg/L SM 254OD-2011 Client ID: Outfall 2 Lab ID: CCO0484-02 AaalYtB Results tin Hu P4L Units Method Notes Biochemical Oxygen Demand 28 2.0 2.0 mg/L SM 5210 B-2011 Chemical Oxygen Demand 69 10 10 mg/L SM S220D-2011 Total Suspended Solids 54 12 12 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 www.encolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID:CC00484-01 Received: 06/21/19 08:48 Matrix: Surface Water Sampled:06/20/19 16:15 Work Order: CC00484 Project: StormwaterTesting Sampled By:)oe Ladd Classical Chemistry Parameters ^ - EACO 6ry certified analyte (NC 5911 Analyte_FCAS Numbed Results Fig uniu PE HDL PDL Batch Method Analyzed gy Notes Biochemical Oxygen Demand^ 7.8 mg/L 1 2,0 2X 9F21001 SM 5210 8-2011 06/21/19 12:05 30C Chemical Oxygen Demand, 44 mg/L 1 10 10 9F25010 SM 5220D-2011 06/25/19 18:12 30C Total Suspended Solids^ 86 mg/L 5 12 12 9F25029 SM 2WD-2011 06/25/19 12:51 LG Description: Outfall 2 Lab Sample ID:CCOD484-02 Received: 06/21/19 08:48 Matrix: Surface Water Sampled:06/20/19 16:30 Work Order: CC00484 Project: Stormwater Testing Sampled By: Joe Ladd Classical Chemistry Parameters ^ - Emco Cary cerwyed ana4 to [AC 591] Analyte KAS Numberl Results Eag Units PF MDL PPOL_ Batch Method Analyzed By Notes Biochemical Oxygen Demand' 28 mg/L 1 2.0 2.0 91`21001 SM 5210 B-2011 06/21/19 12:05 30C Chemical Oxygen Demand^ 69 mg/L 1 10 10 9F25010 SM 5220D-2011 06/25/19 18:12 30C Total Suspended Solids^ S4 mg/L 5 12 12 91`24033 SM 2540D-2011 06/24/19 12:16 LG FINAL This report relates onty to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 (� �60 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9F21001 - NO PREP Blank (9F21001-BLKl) Prepared & Analyzed: 06/21/2019 12:05 Spike Source o/aREC RPD Analyte Result Flag ROL Units Level Result %REC Limits RPD Limit Notes Biochemical Oxygen Demand 2.0 U 2.0 mg/L LCS (9F21001-BS1) Prepared & Analyzed: 06/21/2019 12:05 Spike Source %REC RPD .Analvte Result Flag ROL Units Level Result c/aREC Limits RPD Limit Notes Biochemical Oxygen Demand 170 2.0 mg/L 198 87 85-115 Duplicate (9F21001-DUPi) Prepared & Analyzed: 06/21/2019 12:05 Source: CCO0484-01 Spike Source %REC RPD .Analtfte Result Flap ROL Units Level Result %REC Limits RPD Limit Notes Biochemical Oxygen Demand 7,8 2.0 mg/L 7.8 0.4 30 Batch 9F24033 - NO PREP Blank (9F24033-BLKi) Prepared & Analyzed: 06/24/2019 12:16 Spike Source %REC RPD .Anahrte Result Flag ROL Units Level Result o/aREC UMIJA RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9F24033-BS1) Prepared & Analyzed: 06/24/2019 12:16 Spike Source %REC RPD _AnaMe Rsssul flag NX Units Level Result %REC LllIM RPD Limit Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 Duplicate (9F24033-DUP1) Prepared & Analyzed: 06/24/2019 12:16 Source: CC10083-01 Spike Source %REC RPD AnalYte Result Flag ROL Units Level Result %REC Limll+4 RPD Lhnit Notes Total Suspended Solids 36 8.3 mg/L 40 11 20 Batch 9F25010 - Same Blank (9F25010-BLK1) Prepared: 06/25/2019 11:19 Analyzed: 06/25/2019 18:12 Spike Source p/oREC RPD Anal Result flag ROL Units Level Rig %REC Limits RPD Lit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (9f2S010-BS1) Prepared: 06/25/2019 11:19 Analyzed: 06/25/2019 18:12 Spike Source %REC RPD .Analyte Result Flag ROL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 480 10 mg/L Soo 96 90-110 Matrix Spike (91`25010-MS1) Prepared: 06/25/2019 11:19 Analyzed: 06/25/2019 18:12 Source: CCO2330-01 Spike Source %REC RPD Analve Result Flag ROL Units Level Result %REC Limits RPD L.Mi! Notes Chemical Oxygen Demand 520 10 mg/L 526 19 95 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9F25010 - Same - Continued Matrix Spike Dup (9F25010-MSDI) Prepared: 06/25/2019 11:19 Analyzed; 06/25/2019 18:12 Source: CCO2330-01 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result °/nREC Limits RPD Limh Notes Chemical Oxygen Demand 520 10 mg/L 526 19 95 90-110 0.4 10 Batch 9F25029 - NO PREP Blank (9F25029-BLKI) Prepared & Analyzed: 06/25/2019 12:51 Spike Source %REC RPD Anal vte Ruult Elag P- L Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9F25029-BSI) Prepared & Analyzed: 06/25/2019 12:51 Spike Source %REC RPD _Anahfte Result Flag POI Units Level Result °&REC Limits RPD limit Notes Total Suspended Solids 93 2.5 mg/L 100 93 BO-120 Duplicate (9F25029-DUPI) Prepared & Analyzed: 06/25/2019 12:51 Source: CC09691-01 Spike Source %REC RPD .Analvte Result Flag POL Units Level Result %REC Llrnits RPD limjj Notes Total Suspended Solids 220 50 mglL 230 6 20 Duplicate (9F25029-DUP2) Prepared & Analyzed: 06/25/2019 12:51 Source: CC10767-01 Spike Source %REC RPD _ADalvtc Result Elao POL units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 12 12 mg/L 12 20 LP-04 FINIAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 6 of 8 .ql �Cmo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit, The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. LP-04 Filtration time exceeded the method limit. Sample volume was reduced according to method requirements. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 7 of 8 ENVIRONMENTAL_ CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com come= C® 10775 Central Port Dr. Executive Park ice 111 Woodwinds indus[rel Ct. Orlando. FL a2Ja*sgh��F22i&$m9 Cary, NC 27511 (407) 526.5314 Fax (407) a5"945 (904) 296-3D07 Fax (904) 296.6210 (919) 467-3090 Fax (919) 467-3515 Page -I— Of Client Name Project Number Requested Anatytsea Requested Turnaround Novozymes North America (NO008) [none] ernes Addres Prgad NamerDesc Now : Rush requests sub*l to 77 Perry Chapel Church Road Stormwater Testing acceptance by thefarJOty CiiyISTJLp PO x 7 BIlliq Inlo Franklinton, NC 27525 38364801 M 0pStandard Tel Fax Reporting Contact O 04 o 454-3370 Joe Ladd CO 1.0 N _ Expedited Sampler(s) Name. Attaiaiion (Print) B'er Contact C C N Accounts Payable Cn Due _I____I Sa rls) Signaar Site Location r Time zone O 0 Lab WOrkOrder b�U°a U CCO0484 Preseriattan (See Codes) (ComDtne as necessary) Cdlction Matrix Tau# n of Item s Sample ID (Field Identification) Collection Date T,0,21 Comp I Grab (See codes) Conlame(s Sample Comments Outfall1 �• 1(p1S Sw, 3 X. X, X -See rib Outfall 2 )_O -,2U9 16P__Sw 3 X X X c? low < Total # of Containers Sample Kit Prepared BY Dateirune Relinquished By Datefrwne e-x,l i� By Datelilme I✓t,% 1- I a. 7SX Lo I Z D l �I �� CommentslSSpejckall Reporting Requirement V Ira i tt N F I- P Relinquished By Dab A ByU Daternme Relinquished By Dater re" Received By Data/rime .� Cooler e's d Temps on Receipt Condition Upon ReceMC O ( Acceptable Unacceptable Matrix : GW�Groundwatar SO -Sod DW-Drin" Water SE-Sedimem StN-Surface Water W W Wastewater A•A r 0-0Ih>er (detail in comments) Preservation: Hce H-HCI N+1x03 9-FL804 No•NaOF[ O-Other (detad in canunentsl time: All samptes submitted to ENCO Labs are in accordance with the terms and avnditlons listed an the reverse of this form. unim prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CCO0484 Client: Novozymes North America (NO008) Project: Stormwater Testing Project * [none] Preservation Check Performed B : Logged By: Rachel An L ed In: 1-Jun-19 08:48 }n Yvnis r! Y _ - �V -- DateMme: 1 p� 1, "1 9 l7i�_) CCO0484-01 a Gant , u 4, ' Type ,, ,; - , s Pres (pH),. pH he /, Requircement,. ;In:Conuol ateMme pH Adjusted s T Adjusted ,, . I �,�c ,I Reagent t7sai11Corr►ments }: �_ . :f y t _ C 250mLP+H2SO4 <2 Y N/ NA Y N NA CCO0484-02 ;C41 orit '� x Type "Press P .ly P. H,Checke -1 pH Adjusted .. ate�me .�; ReagenkUsed/Gorrimenfs .€ t: Requirerttent In, ontrol , : _ Adjusted ,+ , 5 , w •, C 250mLP+H2SO4 <2 N/ NA Y N NA Reagent Name ID 1 2 pH Strip ID: Reagent Name ID 3 4 Reagent Name ID 5 6 PH Strips C8J0741 C:lelmntlPrir,,,rer%v_r,eaaIvdL[UnL.necK.rpt Page 1 of 1