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HomeMy WebLinkAboutNCS000003_MONITORING INFO_20190212STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. /V(SV00V U 2D DOC TYPE ❑FINAL PERMIT MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ a 0 I � 0,,� I YYYYMMDD CHROMIUM CERTIFIED MAIL 91 7108 2133 3939 7137 1006 RETURN RECEIPT REQUESTED February 7, 2019 RECEIVED FEB 12 20 NC DENR-Division of Water Quality FILESWater Quality Section CENTRAL ATTN: Central Files D1NR SECTION 1617 Mail Service Center Raleigh, NC 27699-1617 RE. Storm Water Discharge Monitoring Report (DMR) Submittal, 2nd Half 2018 NPDES Permit No. NCS000003 Elementis Chromium, Castle Hayne Plant, New Hanover County Dear Sirs: Enclosed, please find the originals and one copy of each of the stone water discharge monitoring reports for the 2"d half of 2018 as required by Part 11, Section E.2 of our current NPDES Permit No. NC000003. A representative sample was collected on December 20, 2018 and the tab report was received by the facility on January 11, 2018. If you have any questions concerning these reports, please contact Sean Coury at (910) 685-3662. Sincerely, Calvin Overcash Vice President — Regulatory Manager Enclosures Elementis Chromium 5408 I lolly Shelter Road Castle Ilayne, NC 28429 Telephone; (910) 675-7200 Facsimile: (910) 675-7201 STOR,MWATER DISCHARGE OUTFALL (SDO) ,MONITORING REPORT Permit Number NCS000003 SAMPLES COLLECTED DURING CALENDAR YEAR: 0 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Elementis Chromium PERSON COLLECTING SA,-*IPLE(S) Dean Riggs CERTIFIED LABORATORt'(S) Environmental Chemists Lab #! Part A: Specific Monitoring Requirements Lab #_094 COUNTY New Hanover PHONE NO. (_910__) 675-7229 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow (if app.) Total Rainfall pH Chromium Nitrate plus Nitrite Nitrogen mo/dd/yr MG inches Std Units m I 1�1 11 001 12/20/18 n/a 0.60 7.03 0.331 0.62 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _x_no (if yes. complete Part B) Form SWU-247, last revised 21212012 Page 1 of 2 Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&GITPH (Method 1664 SGT-HEAT), if appl. Total Suspended Solids pH New Motor Oil Usage mo/ddl r MG inches m Il m /l unit allmo STORM EVENT CHARACTERISTICS: Date _n/a Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one cope to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including jbf possibility of fi5a<A_#d imprysapment for knowing violations." (Signature of Permi (Date) Form SWU-247, last revised 21212012 Page 2 of 2 e Storm Water Prevention Plan Fortress Wood Products, Inc. Elizabeth City, NC STORM WATER DISCHARGE OUTFALL (SDO)- SUMMARY DATA MONITORING REPORT (DMR) JAN 2 8 Z019 Calendar Year 2018 CENTRAL FILES UVIR Individual NPDES Permit No. NCS000008 or Certificate of Coverage (COC) No. NCG This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 1st of the following year. Facility Name: Fortress Wood Products, Inc., 899 Foreman Bundy Road, Elizabeth City, NC 27909 County: Pasquotank Phone Number: (252) 264-2466 Total number of SDOs monitored: 5 Outfall No. 1 Is this outfall currently in Tier II (monitored monthly)? Yes [XI No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [XI No a If this outfall was in Tier 11 for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency p Received approval from DWQ to reduce monitoring frequency 0 Other Was this S©O monitored because of vehicle maintenance activities? Yes a No [X] Page 1 of 4 Storm Water Prevention Plan Fortress Wood Products, Inc. t:gzabetn cart , Nu Outfall No. 2 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No 0 Was this outfall ever in Tier 11 (monitored monthly) in the past year? Yes [X] No 0 If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency 0 Received approval from DWQ to reduce monitoring frequency 0 Other 0 Was this SDO monitored because of vehicle maintenance activities? Yes 0 No [X] ;Paramete.r,,(unfts) ;:.; Ammonia Copper Total ' Tier ll MonthlyRainfall,,,,Tot, BODSal a CO❑ x ' TSS.. pH:. Inches �' ,;.._... "(5-day)" Nitrogen recoverable Non -Trout Benchmark NIA 30 120 7.2 0.007 100 6-9 Date Sample Collected, 12/31/2018 Tier II NO FLOW Outfall No. 3 Is this outfall currently in Tier 11 (monitored monthly)? Yes [X] No 0 Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No 0 If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency 0 Received approval from DWQ to reduce monitoring frequency 0 Other 0 Was this SDO monitored because of vehicle maintenance activities? Yes 0 No [X] Parameter, (units)- Ammonia..Copper Total, Tier II Monthly Rainfall,, BODS <. COD.,'total� Total TSS:; lnches' (6 day) Nitrogen. recoverable Nan -Trout Benchmark N/A 30 120 7.2 0.007 100 6-9 Date Sample Collected, 1213112018 Tier II NO FLOW Page 2 of 4 Storm Water Prevention Plan Fortress Wood Products, Inc. Elizabeth City, NC Outfall No. 4 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency a Received approval from DWQ to reduce monitoring frequency Other [] Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] :,.POr' fh er,,(u'nits), ' Total Copper '��� bier Il Monthly Rainfall BODS "� CODS Natal, i�'rh �� s F,wb, � � •� , u fatal TSS -v,°+Indies". (5 day) Nitrogen" , r pR " 'recover'able; Non -Trout Benchmark NIA 30 120 7.2 0.007 700 6-9 Date Sample : Collected, 12/31 /201 i3 Tier II NO FLOW Outfall No. 5 Is this outfall currently. in Tier 11(monitored monthly)? Yes [X] No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier.11 for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency [j Received approval from DWQ to reduce monitoring frequency Other [j Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] P.,arameter (units),:;.. K Tier 11 Month(y Total' Rainfalii,;�° inches ;....(5 Ammonia 8OD5 `.CoD tal":� clay) ..:: Nitrogen Ate,. w Norti-Trout ' recoverable pR Benchmark NIA 30 120 7.2 0.007 100 6-9. Date Sample: 'Collected;: 12/3/12018 ' Tier II NO FLOW Page 3 of 4 I certify under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or. persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Responsible Official Signature: -- Printed Name: Ken McBride Title: Director of Manufacturing Date: 12/31/2018 Page 4 of 4 Q RECEIVE JAIL 0 2 2019 Storm Water Prevention Plan Fortress Wood Products, Inc. CENTRAL FILES Elizabeth City, NC DVVR SECTION STORM WATER DISCHARGE OUTFALL (SDO) SUMMARY DATA MONITORING REPORT (DMR) Calendar Year 2018 Individual NPDES Permit No. NCS000008� or Certificate of Coverage (COC) No. NCG This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March 95t of the following year. Facility Name: Fortress Wood Products, Inc., 899 Foreman Bundy Road, Elizabeth City, NC 27909 County: Pasquotank Phone Number: (252) 264-2466 Total number of SDOs monitored: 5 Outfall No. 1 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No [[ Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No 1] If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency Q Received approval from DWQ to reduce monitoring frequency Other Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] Parameter, (units)' Ammonia Total Semi Annual Rainfall, BOD5 Total Copper Inches (5 day) COD Nitrogen total TSS pH Non -Trout recoverable Benchmark NIA 30 120 7.2 0.007 100 6-9 Date Sample S Collected, 111151201$ 3.0 <2 34 <0.1 .074 144 6.69 Page 1 of 4 m Storm Water Prevention Plan Fortress Wood Products, Inc. Elizabeth City, NC Outfall No. 2 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No a Was this outfall ever in Tier 11(monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency Q Received approval from DWQ to reduce monitoring frequency Other Was this SDO monitored because of vehicle maintenance activities? Yes [] No [X] Parameter, (units) Ammonia Copper Total Semi Annual Rainfall, BADS Total Inches (5 day) COD. —Nitrogen total TSS pH Non -Trout recoverable Benchmark NIA 30 120 7.2 0.007 100 6-9 Date Sample Collected, 11/15/2018 3.00 2.33 28 <0.1 .099 266 7.87 Outfall No. 3 Is this outfall currently in Tier Il (monitored monthly)? Yes [X] No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier 11 for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency a Received approval from DWQ to reduce monitoring frequency [] Other p Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] Semi Annual Total Rainfall, Inches Parameter, (units) BODE (5 day) COD Ammonia Total Nitrogen (Non-Trout)recoverable Copper total. TSS pH Benchmark NIA 30 120 7.2 0.007 100 6-9 Date, Sample Collected, 11M 512018 , 3.00 7.02 78 <0.01 1.14 1030 7.74 Page 2 of 4 Storm Water Prevention Plan Fortress Wood Products, Inc. Elizabeth Ci , NC Outfall No. 4 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency a Received approval from DWQ to reduce monitoring frequency a Other a Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] Semi Annual Total Rainfall, Inches Parameter, (units) BODS (5 day) COD Ammonia Total Nitrogen Non -Trout Copper total recoverable TSS pH Benchmark NIA 30 120 7.2 0.007 100 6-9 Date Sample Collected, 11115120113 3.0 3.74 82 .332 1.62 488 6.69 Outfall No. 5 Is this outfall currently in Tier II (monitored monthly)? Yes [X] No a Was this outfall ever in Tier II (monitored monthly) in the past year? Yes [X] No a If this outfall was in Tier II for the last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency a Received approval from DWQ to reduce monitoring frequency a Other a Was this SDO monitored because of vehicle maintenance activities? Yes a No [X] Parameter, (units) Total Ammonia Semi Annual Rainfall, BODS Total Copper Inches (6 day) COD Nitrogen total TSS pH Non -Trout recoverable Benchmark NIA 30 120 7.2 0.007 100 6-9 Date Sample Collected, 11/1512018 3.0 2,69 51 <0.1 .086 23.2 6.95 Page 3 of 4 "I certify under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Responsible Official Signature: Printed Name: Ken McBride Title: Director of Manufacturing Date: _ November 15, 2018 Page 4 of 4 Agpb##N STEELS Since 1989 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Stormwater Enforcement Group: January 9, 2019 REGFIVED FEB 18 2019 CrENTrtML TILES MIR SECTION Please find enclosed the Stormwater Discharge Outfall Monitoring Report for permit numbers NCG030255 and NCS000018 for the J. C. Steele & Sons, Inc., facility in Statesville. For permit NCG030255 the Zinc levels in outfall 3 are above the benchmarks however; a letter of relief for Copper and Zinc was sent to us by Zahid S. Khan on January 7, 2015. The Non — Polar 0 & G at outfall # 1 results were 20 mg/I compared to a benchmark of 15 mg/l. We will start Tier One compliance for Outfall #1 for permit NCG030255. If you have any questions please feel free to contact Curtis Daniels of J. C. Steele & Sons, Inc. at (704) 768-3230 or (704) 872-3681 Ext. 151. Sincerely, LLIV'4a David Steele President J. C. Steele & Sons, Inc. J.C. STEELE & SONS, INC • 710 S. Mulberry Street • Statesville, NC 28677 • P.O. Box 1834 (28687) +1.704.872.3681 • 800,278,3353 • www.jcsteele.com STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 00001 S FACILITY NAPl1E J. C. Steele & Sons, Inc. PERSON COLLECTING SAMPLE(S) Cody Brown CERTIFIED LABORATORY(S) Statesville Analytical_: Statesville Analytical Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR. 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Iredell PHONE NO. (704) 872-3681 Lab NC # 440 Lab #NC DW37755 (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Outfall Date 50050 No. Sample Collected Total Flow (if app.) Total Rainfall Total Suspended Solids m 1L COD m L Iron m /L Chromium Total Recoverable m IL pH unit - molddlvr MG inches 100 120 2 1 6.0 — 9.0 #4 As of February 2013 this outfall has been diverted to Outfall No. 6 per our letter dated Feb. 8, 20I3 #5 No Flow — due to improvements at this outfall. #6 12/20/2018 2.22" 1 14 1 QS 1 .6 1 .0029 7.2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes X no (if yes, complete Part 13) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil and Grease Non -polar O&GITPH (Method 1664 SGT—HEM), if appl. Total Suspended Solids pH New Motor Oil Usage moldd/vr \IG inches m /L m /L unit allmo Form SWU-247-062310 Page I of 2 STORM EVENT CHARACTERISTICS: Date 1 2/20/2018 Total Event Precipitation (inches):2.22" Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit) ,Mail Original and one coAy to: Division of Water Quality Attn! Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violati ns." (Signature of Permittee) (Date) Dorm SWU-247-062310 Page 2 of 2 DUKE ENERGY January 8, 2019 NCDEQ - Division of Water Resources Attention: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Duke Energy McGuire Nuclear SWIM] 12700 Hagers Ferry Road HUnICI-SVllle, NC 28078 Subject: Stormwater Monitoring Report McGuire Nuclear Station — Mecklenburg County Permit #: NCS000020 Certified Mail: 7016 0910 0001 0230 4653 Attention: Central Files 110 Fb CENT, ES /R SECTION V;,oeCIE Gf) �Eg182019 CEh� �TIO•1 D\nt ' s E Attached is the second Semi -Annual Stormwater Monitoring Report for McGuire Nuclear Station for 2018, This report is required by Stormwater Permit No. NCS000020. The Stormwater samples were collected on 1 1/23/18. Lab results were received by the station on 12/1 1/18. All samples were in compliance with benchmark values for this sampling event. Should you have any questions concerning this report, you may contact John Ballard, McGuire Environmental Coordinator by phone: 980-875-5227 or e-mail: John. Ballard@Duke-Energy.com. Sincerely, Steven M. Snider Plant Manager McGuire Nuclear Station RECEIVED FEB 18 2019 CENTRAL FILE;; [) JP/R SECTION STORMWATER DISCHARGE OUTFALL (SDO) ,NIONITORING REPORT PERNIIT NO.: NCS000020 Facility Name: McGuire Nuclear Station 2018 PERSON COLLECTING SMVIPLE(S): Janna Clark/Jeff Cagc (This monitoring report shall be received by the CERTIFIED LABORATORY(S): Duke Enemy Lab #: 248 Division no later than 30 days from the date the facility' receives the sampling results front the laboratory). COUNTY: Mecklenburg PHONE NO. 9�) 875-5227 (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected 50050 z Total Flow 00530 TSS 39516 PCB 50061 TPH' 00400. PH mo/dd/yr \IG mg/I ng/1 mg/L s.u. SWO04 11/23/2018 0.030 18.00 ND ND 7.26 SWO06 11/23/2018 0.112 <5 ND ND 7.67 Footnote: ! Lab reporting limit is 500 ngll. Flows calculated using total precipitation. drainage area, storm duration. and runoff coeff icient I Lab reporting limit is 5 mg/L McGuire NCS000020 Page I of 2 Form MRNCS Part B: Vehicle Maintenance Activitv Nionitorine Requirements OutfaIl No. Date Sample Collected 50050 Total Flow 00530 TSS 50061 ; TPH' 00400 pH New Motor Oil Usage- mo/dd/yr IN4G mg/l mg/L unit gal/mo SW008 1 11/23/2018 1 0,042 1 19.0 1 ND 1 7.45 1 75.02 Footnotes: °Applies only for facilities at which fuclinI occurs. Monthly average for 2018 Lab reporting limit is 5 nic/L STORM EVENT CHARACTERISTICS: Date: I_ 11/23/2018 Total Event Precipitation (inches) 0.55 Event Duration (hours): 10:00 (if more than one storm event was sampled) Date: Total Event Precipitation (inches): Event Duration (hours): Mail original and one copy to: NCDEQ Attention: Central Files Division of Water Resources 1617 Mail Service Center Raleigh. NC 27699-1617 "l certify, under penalty of law. that this document and all attachments were prepared under my direction or Supervision in accordance with it system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information. the information submitted is, to the hest of my knowledge and belief, true, accurate. and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) McGuire NCS0{10020 Pace 2 of 2 Form MRNCS r Certified Mail 7017 2620 0000 9425 9323 Return to Renee Culler December 13, 2018 NCDEQ Division of Water Quality Surface Water Protection Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ATTN: Central Files Celanese The chemistry inside innovation" R E C E 1VE ti,,." CE WRAL FILES DWR SECTION Celanese Corporation 2525 Blacksburg Road Grover, NC 28073-9641 www.celanese.com Reference: Semi -Annual Monitoring Results — CNA Holdings LLC- Shelby Plant - Stormwater Permit No. NCS 000064 To Whom It May Concern: In accordance with the facility's Stormwater NPDES Permit, semi-annual monitoring must be conducted in accordance with permit no. NCS000064. The following represent the semi-annual monitoring results from the sampling period of September 1— November 30, 2018. Duplicate copies of the signed DMR report are attached. The monitoring results have been compared to the benchmark values of Table 3, which are not permit limits but are guidelines for us to use in evaluating the sources of any benchmark exceedance and for the evaluation of the effectiveness of our BMPs. Outfall TSS : 100 mg/I GODS: 30 mg/I COD: 120 mg/I pH: 6-9 North Outfall 9.2 5.2 120 7.4 South Outfall 7.9 BRL BRL 6.7 East Outfall 6.5 BRL BRL 7.3 CNA Holding LLC — Shelby Plant is committed to ensuring compliance with all County, State, and Federal regulations. Should there be a need for further discussion pertaining to the information above, feel free to call me at 704/480-5726 or via email at renee.cullerPcelanese.com. Sincerely, 1 U e ,Cueelei EHS Manager Attachments: Stormwater Discharge Outfall (SDO) Monitoring Report (2 copies) STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000064 FACILITY NAME _CNA Holdings LLC — Shelby Plant PERSON COLLECTING SAMPLE(S)_Mike Sparks & Randall Turner CERTIFIED LABORATORY(S) Prism Laboratory_Lab #_402 _ CNA Holdings LLC - ShelbyLab 4_221_ Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Cleveland PHONE NO. (_704_) 480-5793. SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PACE 2. Outfall No. Date Sample Collected 50050 00530 00310 00340 00400 Total Flow (if app.) Total Rainfall Total Suspended Solid BOD5 COD pH mo/ddl r MG inches MgA M /l M /l standard North 11/12/18 n/a 3.0 9.2 5.2 120 7.4 South t 1/12/18 n/a 3.0 79 BRL BRL 6.7 East 11/12/18 n/a 3.0 6.5 BRL BRL 7.3 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitorinjj Requirements Outfall Date 50050 00556 00530 00400 Total Flow Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if appi. mo/dd/ r MG inches mg/1 m /I unit al/mo Form SWU-247, last revised 21212012 Page I of 2 STORM EVENT CHARACTERISTICS: Date 11/12/18 Total Event Precipitation (inches): 3.0 Event Duration (hours): 24 (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, incl,gding the possibility of tines and imprisonment for knowing violations." of December 13, 2018 (Date) Form SWU-247, last revised 21212012 Page 2 of 2 A STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000064 FACILITY NAME _CNA Holdings LLC — Shelby Plant PERSON COLLECTING SAMPLE(S) _Mike Sparks & Randall Turner CERTIFIED LABORATORY(S) Prism Laboratory_Lab #4402 _ CNA Holdings LLC - ShelbyLab #-221_ Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Cleveland PHONE NO, (_704_) 480-5793 SIGNATURE OF PERM ITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 00530 00310 00340 00400 Total Flow (if app.) Total Rainfall Total Suspended Solid BOD5 COD pH mo/dd/ r MG inches M /I Mg/1 Mg/1 standard North 11/12/18 n/a 3.0 9.2 5.2 120 7.4 South 11/12/18 n/a 3.0 7.9 BRL BRL 6.7 East 11/12/18 n/a 3.0 6.5 BRL BRL 7.3 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no (if yes, complete Pan B) Part B. Vehicle Maintenance Activity Monitoring Requirements OutfaIl Date 50050 00556 i 00530 00400 Total Flow Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if a221. mo/dd/ r MG inches m /I m /l unit al/mo Form SWU-247, last revised 21212012 Pagel of 2 STORM EVENT CHARACTERISTICS: Date 11/12/18 Total Event Precipitation (inches): _3.0 _ Event Duration (hours): 24 (only if applicable —see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information; the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, inpl,qding the possibility of fines and imprisonment for knowing violations." December 13 2018 Pe ittec) (Date) Form SWU-247, last revised 21212012 Page 2 of 2 (1� �TTN(� - Coming Incorporated t 910-784-7200 r._ v VR \ 1 V 310 North College Road www.commg,com Wilmington, NC 28405 December 7, 2018 Division of Water Quality ATTN: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Permit NCS000076 RECEIVED FEB 18 2018 CCN7'�,gL �1 Enclosed please find the attached complete report for the Corning Incorporated, Wilmington facility, for the stormwater discharge sampling taken on 11/19/2018. This represents the semi-annual monitoring period of (July 1, 2018 -- December 31, 2018). During these measureable storm events, Outfalls 001, 002, 003, 004, and 005 were discharging. Outfall 008 has representative outfall status granted, so analytical monitoring was not completed for that specific outfall. All data was collected using•DWQ approved methods. If you have any questions concerning this information, please call me at (910) 784-7476, Sincerely, 4� Carol B. Y tes Environmental Control Supervisor STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000076 FACILITY NAME _Corning Inc. Wilmington Facility PERSON COLLECTING SAMPLE(S) _Rusty Hickman CERTIFIED LABORATORY(S) _Environmental Chemists _Lab #_94_ _Corning Inc. Wilmington —Lab #_5503 Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY New Hanover PHONE NO. (_910_) 784-7476 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 00400 00530 Total Flow (if app.) Total Rainfall pH Non -polar O&G1TPH (Method 1664 SGT-HEM Total Suspended Solids moldd/ r MG inches units m IL m IL Outfall 001 11/19/2018 1.50 7.20 < 5 4.1 Outfall 002 11/19/2018 1.50 7.14 < 5 36.5 Outfall 003 11/19/2018 1.50 8.41 < 5 < 2.6 Outfall004 11/19/2018 1.50 7.75 <5 6.9 Outfall005 11/19/2018 1.50 7.16 <5 4.0 Outfall008 *** Representative Outfall Status at Outfall 003 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X_no (if yes; complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample 50050 00556 00530 00400 Total Flow Total Oil & Grease Non -polar Total pH New Motor Collected (if applicable) Rainfall (if appl.) O&G/TPH Suspended Oil Usage (Method 1664 Solids SGT-HEM), if appl. Form SWU-247, last revised 21212012 Page 1 of 2 mo/dd/ r MG. inches% m /l` I m unit I gal/Mo. STORM EVENT CHARACTERISTICS: Date _11/19/2018 Total Event Precipitation (inches): _1.50 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of 121� �S (Date) Form SWU-247, last revised 2/2/26 Page 2 of 'I Environmental Chemists, Inc. 41 NOP'i 6602 Windmill Way, Wilmington, NC 28405 • 910,392,022-3 I_ab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 279954 • 252.473.5702 Lab/Fax ' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info a environmentalchemists.com Corning, Inc. Date of Report: Dec 06, 2018 310 North College Road Customer PO #: Wilmington NC 28405 Customer ID: 08100038 Attention: Rusty Hickman Report #: 2018-19094 Project ID: Stormwater Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-48355 Site: Outfall # 001 11/19/2018 7:55 AM Water Rusty Hickman Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 11/30/2018 Residue Suspended (TSS) SM 2540 D 4.1 mg/L 11/20/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 1 BA8356 Site: Outfall # 002 11/19/2018 7:50 AM Water Rusty Hickman Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 11/30/2018 Residue Suspended (TSS) SM 2540 D 36.5 mg/L 11/20/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-48357 Site: Outfall # 003 11/19/2018 7:40 AM Water Rusty Hickman Test Method Results Date Analyzed Oil & Grease (O&G) EPA 16a4 <5 mg/L 11130/2018 Residue Suspended (TSS) SM 2540 D <2.6 mg/L 11120/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-48358 Site: Outfall # 004 11/19/2018 7:45 AM Water Rusty Hickman Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 11130/2018 Residue Suspended (TSS) SM 2640 D 6.9 mg/L 11120/2018 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 1848359 Site: Outfall # 005 11/19/2018 7:47 AM Water Rusty Hickman Test Method Results Date Analyzed Oil & Grease (O&G) EPA 1664 <5 mg/L 11/30/2018 Residue Suspended (TSS) SM 2540 D 4.0 mg/L 11/20/2018 Report M: 2018-19094 Pace 1 of 2 Corning, Inc. 310 North College Road Wilmington NC Attention: Rusty Hickman Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax iiiIZ3@environment,tichemists.com environmentaichemists.com Date of Report: Dec 06, 2018 Customer PO M 28405 Customer ID: 08100038 Report M. 2018-19094 Project ID: Stormwater Comment: Reviewed by Reporl k: 2M.19o94 Page 2 of 2 4UPENVIRONMENTAL CHEMISTS, INC' sao2,uina�lll"wilminoon, NC nW Anal b" & ConwAft Che hft NCDB RFATIDN DM CE# % MCMM: MS CMnMAnM # 311 OFFIM 91"24)M FAX 910-M-442# COLLECTI(AI AND CHA#N OF CUSTODY CLlBVT: PROJECT REPORT NO: An&ww: b CAL CONTACT NAME: S `AMW PO NO: q(Q `2! 44i- 7-7C3 ` I �►fj i N C- 2 g S REPORT TO' �C r i t o PHONPIFIX:_ COPY TO: E-MAIL:_ Sampled ft Vl�gn - - SAMPLE TYPE: I - In4uent. E a Effluent, W s Well. ST Q Strewn, SO a $oil, SL = Sludge. Ouwer -� MM IBM memo N. I ILL-7 MEN T when m Domes tic Mail Only r` RAL H"APIU I A L CeMfled &W Fee $3.45 Iti $ c BBS ftYm& b" add rea p ❑ Foam R 010 SwAooW f o ❑ Foam Rewq (doI f Sid . 00 d ❑ 0.1 ma Rmm w baNary $_ — 17-3 ❑— s,a,aane mq— S _ 0 ❑ Ackn S onw.+m Rawlctw De9wy f r` Postage C3 s$y1�.4t2 rl Di `p T F#2 Te 8 Division o r Quality s Attn: Central Files m 1617 Mail Service Center s Raleigh, NC 27699-1617 11 U I E f1400 20 PosUnark Here 12/07/2018 Dow Silicones Corporation 2914 Patterson Street Greensboro, NC 27407 January 23, 2019 RECEIVED Division of Energy Mineral and Land Resources Attn: Central Files JAN 2 5 2019 1617 Mail Service Center CENTRAL FILES Raleigh, North Carolina 27699-1617 DWR SECTION Re: Transmittal 2018 Semi -Annual Stormwater Discharge Outfall Monitoring Report (H2-2018) NPDES Permit No. NCS000077 Enclosed please find an original and one copy of the Semi -Annual Stormwater Discharge Monitoring Report (DMR) for Permit No. NCS000077. The stormwater event in which the samples were collected occurred on December 20, 2018. All reported results were all within the permit limits. The pH values for each of the stormwater outfalls were tested on site on the day of collection and within the 15 minute time frame specified. The results met the desired benchmark value range and can be found in the attached stormwater discharge outfall (SDO) monitoring report. If you have questions or comments regarding this submittal, please contact Richard Kelley at 336-547-7273. Sincerely, Darren Cammin Site Manager STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000077 FACILITY NAME DDP Specialty Electronic Mateials US9, LLC PERSON COLLECTING SAi%IPLE(S) Richard Kelley CERTIFIED LABORATORY(S) Pace Analytical Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Guilford PHIPUNE NO. 336 } 7-7273 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow (if a Total Rainfall TSS - mglL pH Nitrogen-mglL Phos - mglL moldd/vr ,SIG inches 001 12/20/18 1.2 12.5 7.0 ND 0.099 002 12/20/18 1.2 ND 7.0 ND NO 003 12/20/18 1.2 5.6 7.0 ND 0.062 004 12/20/18 1.2 10.8 7.0 ND 0.051 005 12/20/18 1.2 36.8 7.0 ND 0.068 006 12/20/18 1.2 7.9 7.0 ND ND Iaoes this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month'? Dyes Ono (if yes. complete fart 13) Part B: Vehicle Maintenance Activity MonitoringRe uirements Outfall No. Date Sample Collected 50050 00556 100530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/vr MG inches m /I m /I unit al/mo Form SWU-247. last revised 611212015 Page I of 2 STORM EVENT CHARACTERISTICS: Date 12/20/18 Total Event Precipitation (inches): 1.2 Event Duration (hours): 6 (only, if applicabie —see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only it'applicable — see permit.) Mail Original and one cope to: Division o1'Energv,Vfineral and Land Resources Attn: Central Files 1617 Mail Sen,ice Center Ralcigh. North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 11�3ja019 (Signature of Permittee) (Date) Form SWU-247. last revised 611212015 Page 2 of 2 a aceAnalytical wwwpatelaba.com January 22, 2019 Richard Kelley Dow Corning 2914 Patterson St Building 2 Greensboro, NC 27407 RE: Project: Stormwater Pace Project No.: 92411951 Dear Richard Kelley: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704) B75-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Allen Hetzer, Dow Corning REPORT OF LABORATORY ANALYSIS TNs report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 28 aceAnalytrcal wwwpacafaftmn Project: Stormwater Pace Project No.: 92441951 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 t704)B75.9092 Page 2 of 28 aceAnalytical. wwwpacelabs.mn l WIM1111161�1FAMA Project: Stormwater Pace Project No.: 92411951 Lab ID Sample ID Matrix Date Collected Date Received 92411951001 1-8 Water 12120/1812:18 12/2111814:50 92411961002 2-13 Water 12/20/1812:18 12/2111814:50 924111951003 3-B Water 12/201181218 12/21/1814:50 92411951004 4-13 Water 12/2011812:18 12/2111814:50 92411951005 5-13 Water 12/20/1812:18 12/21/1814:50 92411951006 6-13 Water 1212011812:18 12/21/1814:50 92411951007 t-A Water 1212011812:18 12/2111814:50 92411951008 2-A Water 12/20/1812:18 12/21/1814:50 92411951009 3-A Water 12120/1812:18 12121/1814:50 92411951010 4-A Water 12120/1812:18 12/21/1814:50 92411951011 5-A Water 12/20/1812:18 12/21/1814:50 92411951012 5-A Water 12120/1812:18 12/21/1814;50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 Page 3 of 28 aceAnalytrcal gwwpawlabs.wm SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Project: Pace Project No.: Stormwater 92411951 Analyles Lab ID Sample ID Mothod Analysts Reported Laboratory 92411951001 1-8 TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 CJH1 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A 92411951002 2-B TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 CJH1 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASM 92411951003 3-13 TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2,0 1993 MDW 1 PASI-A 92411951004 4-B TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A 92411951005 5-13 TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A 92411961006 6-13 TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A 92411951007 1-A SM 2540D-2011 CEH 1 PASI-A 92411951008 2-A SM 2540D-2011 CEH 1 PASI-A 92411951009 3-A SM 2540D-2011 CEH 1 PASI-A 92411951010 4-A SM 2540D-2011 CRV 1 PASI-A 92411951011 5-A SM 254OD-2011 CRV 1 PASI-A 92411951012 6-A SM 25401)-2011 CRV 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 28 acmnalXical www.pecolabs.com ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: 1-13 Parameters Lab ID: 92411951001 Collected: 12/20/18 12:18 Results Units Report Limit DF Received: 12121/18 14:50 Matrix: Water Prepared Analyzed CAS No. Qual Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen ND mg1L 0.52 1 01/22/19 09:44 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mglL 0.50 1 12/23/18 15:00 12124/18 14:58 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.051 mglL 0.020 1 12124M8 13:20 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1903 Phosphorus 0.099 mg1L 0,050 1 12/24/18 15:35 12/24/18 21:25 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 28 o aceAnalytical wwwpecalaus-com ANALYTICAL RESULTS Pace Analytical Sarvicas, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 132411951 Samplo: 2-13 Lab ID: 92411951002 Collected: 12/20/18 12:18 Received: 12/21118 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen ND mg/L 0.52 1 01/22/19 09:44 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mg/L 0.50 1 12/23/18 15:00 12/24118 14:58 7727-37-9 363.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.064 mg1L 0.020 1 12/24/18 13:24 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2,0 1993 Phosphorus ND mg1L 0.050 1 12124/18 15:35 12/24/18 21:26 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01122/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 28 aoAnalyfical www.pacelefte m ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Hvntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92411951 Sample: 3-B Lab ID: 92411961003 Collected: 12120/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen NO mgfL 0,52 1 01/22/1909:44 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total NO mglL 0.50 1 12/28/18 00:38 12/29/18 02:17 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.055 mg1L 0.020 1 12/24/18 13:32 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.062 mg1L 0.050 1 12/24/18 15:35 12/24/18 21:28 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 28 aceAnalXical ffm pacelabs, coin ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinceyAve. Suite too Hunlersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92411951 Sample: 4-13 Lab ID: 92411951004 Collected: 12/20/18 12:18 Received: 12121/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen ND mg1L 0.52 1 01/22/19 09:44 351.2 Total Kjoldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kieldahl, Total ND mglL 0.50 1 12/28/18 00:38 12129/18 02:18 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.021 mg/L 0.020 1 12/24/18 13:37 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.051 mg/L 0.050 1 12/24/18 15:35 12/24118 21:30 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/2212019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 28 aceAnalytical www.paceigbs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92411951 Sample: 5-13 Lab ID: 92411951005 Collected: 12120/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen ND mg1L 0.52 1 01/22/19 09:44 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mglL 0.50 1 12/28/18 00:38 12/29118 02:21 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.032 mglL 0.020 1 12/24/18 13:41 366.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.068 mg1L 0.050 1 12/24/18 15:35 12/24/18 21:31 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 213 e aceARalytical www.pacelabs.com ANALYTICAL RESULTS Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92411951 Sample: 6•13 Lab ID: 92411951006 Collected: 12/20/18 12:18 Received: 12121118 14:50 Matrix: Water Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Qual Total Nitrogen Calculation Analytical Method: TKN+NQ3+NO2 Calculation Total Nitrogen ND mg1L 0.52 1 01/22/19 09:44 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total ND mg1L 0,50 1 12/28/18 00:38 12/29/18 02:22 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg1L 0.020 1 12/24/18 13:42 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus ND mg1L 0.050 1 12/24/18 15:35 12/24/18 21:32 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not 5e reproduced, except in full, Date: 01/2212019 09:54 AM without the written consent of Pace Analytical Services, LLC, Page 10 of 28 aceAnalytica! www.pfelabs.com ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Paco Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: 1-A Lab ID: 92411951007 Collected: 12120/18 12:18 Received: 12/21118 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 2640D Total Suspended Solids Analytical Method: SM 25400-2011 Total Suspended Solids 12.5 mg/L 3.8 1 12/21/18 22:56 Date: 01122/2019 09:54 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 28 aceAnalytrcal ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Pace Analytical Services, LLC 9B00 KinceyAve. Suite 100 Hunlersville, NC 28078 (704)875-9092 Sample: 2-A Lab ID: 92411961008 Collected: 12/20/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids Date: 01/2212019 09:54 AM Analytical Method: SM 2540D-2011 ND mg/L 2.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 12/21118 22:56 Page 12 of 28 0 aoAnalytical wwwpscelaftwn ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Pace AnalytiCal Services, LLC 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 Sample: 9-A Lab ID: 92411951009 Collected: 12/20/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 5.6 mglL 2.6 1 12/21/18 22:56 Date: 01/22/2019 09:54 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 13 of 28 acMnalyticale www.pacelabs.nn ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Paco Analytical Services, LLC 9800 Kinney Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Samplo: 4-A Lab ID: 92411951010 Collected: 12/20/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids Date: 01 /22/2019 09:54 AM Analytical Method: SM 2540D-2011 10.8 mg1L 2.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 1212411814:15 Page 14 of 28 aceAnalXica! www.pacelabs.corn ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Paco Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 5-A Lab ID: 92411951011 Collected: 12/20/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 36.8 mglL 5.0 1 12/24/18 14:15 Date: 01/22/2019 09:54 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 28 aceAnalXica! wwwpecelabscnm ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92411951 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9D92 Sample: 6-A Lab ID: 92411951012 Collected: 12/20/18 12:18 Received: 12/21/18 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 7.9 mg/L 2.8 1 12/24/18 14:15 Date: 01/22/2019 09:54 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 28 aceAnalXical ` www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 {704)875-9092 Project: Stormwater Pace Project No.: 92411951 QC Batch: 449270 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92411951007, 92411951008, 92411951009 METHOD BLANK: 2460381 Matrix: Water Associated Lab Samples: 92411951007, 92411951008, 92411951009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 12/21/18 22:51 LABORATORY CONTROL SAMPLE: 2460382 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 251 254 101 90-110 SAMPLE DUPLICATE: 2460383 92411950001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL 22.0 21.7 2 5 SAMPLE DUPLICATE: 2460384 92411948002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL 18.6 17.8 4 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01122/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 28 to aceAnalytical IIW1Y.pacefabs.core QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92411951 Pace Analytical Services, LLC 9800KinceyAve. Suite100 Huntersville, NC 28078 (704)875-9092 QC Batch: 449436 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92411951010, 92411951011, 92411951012 METHOD BLANK: 2461024 Matrix: Water Associated Lab Samples: 92411951010, 92411951011, 92411951012 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/24118 14:12 LABORATORY CONTROL SAMPLE: 2461025 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 254 101 90-110 SAMPLE DUPLICATE: 2461026 92411994001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 4180 5180 21 5 D6 SAMPLE DUPLICATE: 2461027 92411955001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg1L 260 288 10 5 D6 Results presented on this pago am in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 28 aceAnalytical WW..pacefaba.00m QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92411951 QC Batch: 449350 Analysis Method: EPA 351,2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 Ti Associated Lab Samples: 92411951001, 92411951002 METHOD BLANK: 2460660 Matrix: Water Associated Lab Samples: 92411951001, 92411951002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 12/24/18 14:46 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2460661 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460662 2460663 MS MSD 92411991005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, Kjeldahl, Total mg/t_ 0.85 10 10 8.4 9.8 75 89 90.110 15 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 28 aceAnalytical wrrw.pat Blab$ =" QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92411951 QC Batch: 449892 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92411951003, 92411951004, 92411951005, 92411951006 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2462482 Matrix: Water Associated Lab Samples: 92411951003, 92411951004, 92411951005, 92411951006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg1L ND • 0.50 12129/18 02:16 LABORATORY CONTROL SAMPLE: 2462483 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg1L 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2462484 2462485 MS MSD 92411972001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, Kjeldahl, Total mg1L ND 10 10 8.8 8.9 87 88 90-110 2 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2462560 2462561 MS MSD 92411639001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, Kjeldahl, Total mg/L 41.5 10 10 55.2 59.8 137 183 90-110 8 10 M1 Results presented on this page arc In the units Indicated by the "Units" column except where an alternate unit Is prosentad to the right of the result. REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, Date: 01 /22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 28 aceAnalytica! www pacelabs corn QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92411951 QC Batch: 449368 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2,0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92411951001, 92411951002 METHOD BLANK:' 2460712 Matrix: Water Associated Lab Samples: 92411951001, 92411951002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mglL ND 0.020 12/24/18 12:49 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704) 875-9092 LABORATORY CONTROL SAMPLE: 2460713 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460714 2460715 MS MSD 92411746001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, NO2 plus NO3 mglL 0.033 2.5 2.5 2.6 2.5 103 98 75-125 4 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460716 2460717 MS MSD 92411170001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, NO2 plus NO3 mg/L 107 2.5 2.5 112 110 224 134 75-125 2 10 M6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01122/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 28 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92411951 QC Batch: 449369 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92411951003, 92411951004, 92411951005, 92411951006 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 10D Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2460718 Matrix: Water Associated Lab Samples: 92411951003, 92411951004, 92411951005, 92411951006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.020 12/24/18 13:30 LABORATORY CONTROL SAMPLE: 2460719 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2,5 2.6 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460720 2460721 MS MSD 92411951003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.055 2.5 2.5 2.5 2.5 98 99 75-125 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460722 2460723 MS MSD 92411951004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Cone. Result Result % Rec % Roc Limits RPD RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.021 2.5 2.5 2.7 2.7 108 108 75-125 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01I2212019 09:54 AM without the written consent of Pace Analytical Services, LLC, Page 22 of 28 aceAnalyticale wwwpacelabs.cam QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92411951 QC Batch: 449425 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92411951001, 92411951002, 92411951003, 92411951004, 92411951005, 92411951006 METHOD BLANK: 2460974 Matrix: Water Associated Lab Samples: 92411951001, 92411951002, 92411951003, 92411951004, 92411951005, 92411951006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 12/24118 21:15 LABORATORY CONTROL SAMPLE: 2460975 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mg1L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460976 2460977 MS MSD 92411747001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Cone. Conc. Result Result % Rae % Rec Limits RPD RPD Qual Phosphorus mg1L 1.1 2.5 2.5 3.7 3.7 103 104 90-110 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460978 2460979 MS MSD 92411951003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Phosphorus mg1L 0.062 2.5 2.5 2.6 2.6 103 103 90.110 0 10 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /22/2019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 28 aceAnalytical o www.pacalabs. w Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Stormwater Pace Project No.: 92411951 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantilation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroothylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace AnalyticaiServices- Asheville ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0112212019 09:54 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 28 aceAnalytrcal wwwpacefabs,com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, PLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)675-9092 Project: Pace Project No.: Stormwater 92411951 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92411951007 1-A SM 254OD-2011 449270 92411951008 2-A SM 254OD-2011 449270 92411951009 3-A SM 254OD-2011 449270 92411951010 4-A SM 2540D-2011 449436 92411951011 5-A SM 254OD-2011 449436 92411951012 6-A SM 2540D-2011 449436 92411951001 1-B TKN+NO3+NQ2 453649 Calculation 92411951002 2-B TKN+NO3+NO2 453649 Calculation 92411951003 3-B TKN+NO3+NO2 453649 Calculation 92411951004 4-B TKN+NO3+NO2 453649 Calculation 92411951006 5-B TKN+NO3+NO2 453649 Calculation 92411951006 6-B TKN+NO3+NO2 453649 Calculation 92411951001 1-B EPA 351.2 Rev 2.0 1993 449350 EPA 351.2 Rev 2.0 1993 449417 92411951002 2-B EPA 351.2 Rev 2.0 1993 449350 EPA 351.2 Rev 2.0 1993 449417 92411951003 3-B EPA 351.2 Rev 2.0 1993 449892 EPA 351.2 Rev 2.0 1993 450118 92411951004 4-B EPA 351.2 Rev 2.0 1993 449892 EPA 351.2 Rev 2.0 1993 450118 92411951005 5-B EPA 351.2 Rev 2.0 1993 449892 EPA 351,2 Rev 2.0 1993 450118 92411951006 6-B EPA 351.2 Rev 2.0 1993 449892 EPA 351.2 Rev 2.0 1993 450118 92411951001 1-B EPA 353.2 Rev 2.0 1993 449368 92411951002 2-B EPA 353.2 Rev 2.0 1993 449368 92411951003 3-B EPA 353.2 Rev 2.0 1993 449369 92411951004 4-B EPA 353.2 Rev 2.0 1993 449369 92411951005 5-B EPA 353.2 Rev 2.0 1993 449369 92411961006 6-B EPA 353.2 Rev 2.0 1993 449369 92411951001 1-B EPA 365.1 Rev 2.0 1993 449425 EPA 365.1 Rev 2.0 1993 449456 92411951002 2-B EPA 365A Rev 2.0 1993 449425 EPA 365.1 Rev 2.0 1993 449456 92411951003 3-B EPA 365A Rev 2.0 1993 449425 EPA 365.1 Rev 2.0 1993 449456 92411951004 4-B EPA 365A Rev 2.0 1993 449425 EPA 365.1 Rev 2.0 1993 449456 92411951005 5-B EPA 365.1 Rev 2.0 1993 449425 EPA 365.1 Rev 2.0 1993 449456 92411961006 6-B EPA 365.1 Rev 2.0 1993 449425 EPA 365A Rev 2.0 1993 449456 Date: 01/2212019 09:54 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. LLC, Page 25 of 28 uocument Name: ••• - • Sample Condition Upon Recei t(SCUR Page 1 of 2 i3G8f�!?d1yE?=Cd( DocumentNo.: - issuing Authority: F•CAR-CS-033•Rev.06 -Pace Carolinas Qual office Laboratory recelving samples. Asheville Eden❑ Greenwood ❑ Huntersville �� . Raleigh[] Mechanicsville[] Client Name: WV# : 92411951 ', � ,nArce'pli� .r Projectp Courier: Fed ix ❑i,p5 ❑U5P5 0 ,lent III III I I IN ICI 1111111 ❑ Commerdal ❑Pace ❑Other:92411951 Custody Seal Frtstnt? ❑Yes QNo Seals Intact? []Yes Q o Packing Matelal: ❑Bubble Wrap ❑Bubble Bags HNone ❑ Other Thermometer. ❑ a Cus rD:. 92T"0 46 Type of ice: ❑� ❑Blue Cooler Temp {lq; Correction Factor: Add/Subtract ('CI Cooler Temp Corrected ('Cl: 2 C� USDA Regulated Soil (❑N N/A, water sample) Did samples 000e n a quarantine zone within the United States: CA, NY, orSC (check maps)? Yes f� s Date/lnitlals Person Examining Contents: Vv 1 41— Biological Tissue Frozen?. ❑Yes ❑No ❑N/A ❑Ntts Tempshauld be above freezing to 6'C ❑sanpLs out of temp criteria. Samples on Ice, cooling process has5e;ua Dld sirspLes originate from a foreign source {internationally, Inciud}g Hawaii and Puerto Ricol? []Yes Me-- Comments/Discrepancy: tu!tcd,, Present? es No NJA 1. krrved;vithin Hold Time? Oes No ❑NJA 2. il TlmeAialysis <72 hr.j? []Yes ONo " NIA 3. NTurs sAroundTlmeRequested? ❑Ye/s QNo NIA 4. Vaune7 Y; No NIA 5. nianersUsed?©Yes/ ortainers Used? ©des ❑No ❑No ❑NIA ❑NJA 6. hYict? yes ❑No El N/A. 7. Dissolved ra ! sts: s amples Field Filtered? ❑Yes ❑Na .N A S. sample LabdsMauh CDC? -Includs Dater l"epO/Analysis Matrix: r Headspaa Ll VGA Vials(>5-6mm)? ( ycls � f l l � ❑Yes ❑No � [5. ❑No N/A ❑NIA, 9. 10. Trip BlankPreent7 Trl BlankCistod Seals Present? []Yes ❑Yes ❑Ito ❑No QN/%A NIA 11 COMMENTSAAWLE DISCREPANCY Lot ID of , lit containers: CLIENT NDTIFI{Ap�ry/gE50LUTI0N Person contacted: Date/Time: Field Data Required? []Yes ❑No Project MiriagerSCURF Review: Date: Project ManagerSRF Review: 1 Date: r� r Page 26 of 28 Sample Condition Upan Receipt SCURj Page 1 of 2 !KcekaOaDocumenttVa.: IssuingAuthority. °_retr_�e_naa_ne„ na Pace Carolinas Quallty Office 'Check mark top half of box if pH and/or dechiorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Caliform, TOC, Oil and Grease, DRO/SW (water) DOC, LLHS "Bottom half of box is to list number of bottle . Projec Wp# : 9241195_1 PM: TIH Due Date: 01/03/19 CLIENT: 92-DOW CORN U T7 2 cu N ar 4 E K ] 6 Yl 2 O '- ? d E c N ] S 44 2 V N o o a E g ul J 6 .Z. Q' u- ? d- m N r v ^� u yry� VI d m N Y d m Z a E o u� 6 m Ri ,v W �i Z u a E 0. V 'i A a Y a E N 0. CL N m E u y ? 3 Q Y v ° N d c lu `m •-1 V' a N V Y lu a d `m a •-1 �1' a y 2 vNN ` a J E C7 a N V .=a. vn N yHy1� l7 a y Z O. S T a E n Ln Ny lh a z U R s 2 a a E l7 a z x > c q l7 s _ < <X > -� E O �) > Z 6 0 J o 4 Q ? Z Vp z o S 3 E oa i �: Y 1n m x a _ 9 Y. z f,' Y H t7 \ s > Y a f m s > I 6 =' V N n v H � E N .a i \ V N a E i a,m N N Z d E a b W N 61 a 3 E a 1 E - •� a Z n > C ; c is V L N > �. R 3 E j E a O 1 z 3 a i - 7 I N\ a •�/ 9 10 it { li 1 1Z I[---N N pH Adjustment Log for Preserved Sanples Sample ID Type of Preservative pH upon receipt Dote preservation adjusted Time preuMWfl Amount of Preservative Lot p adjurad added Note: Whenever there is a discrepancy affecting North Carollna compliance samples, a copy of this form will'te sent to the North Carolina DEHNR CeniffCattan Office {i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers. Page 27 of 28 CHAIN -OF -CUSTODY / Analytical Request Document The Chain of -Custody is a LEGAL DOCUMENT. All relevant Gelds must be completed accurately. Section A Section 9 Section C r Required Client Information: Required Project Information: Invoice Information: Pa..: 7 Of t Company= Dow coming Report To: _ Ltd r Auentmn: Address: 29ta Patterson St. Copy To: Company Name: Greensboro. NC 27407 Address: R - - -- Email: f L v(liC.i.'1rd'•'1 a @Tb' Pace Quote: / �� Phone: , --j j Fax Project Name: Stormwater Pace Project Manager, tyriek,000k tass.cem. .3.: .• Scab 1 Lo�tld� . _ - ' Requested Due Date: Project C: Pace Profile 9: 4169-1 NC Requested Fllbnd ' - - i< = - -' .l^ w,mix cone 2 ` o V COLLECTED y Preservatives 1 p.rnasy wrn Ow wT ` 3 v O wra wave wwK wry s H _ a. z SAMPLE ID sowsow a t7 — START END 0 a One Character per box. wow WP wr: w w z 'o e ` r o # (A-Z- 0.9 1, -t Sample kola must be unique iuiur TS O u a o c m = K p N b 44//////�� ((`�7f[[ ~ v`, DATE TIME DATE TIME K _ _ = z z o ; r i 007 -: r2A l [ CI l r 44P C x of v 2N �D Z'-is: 6 _ Cr z�zv I 1-0 lzr-;r '_Ty�'•t+{w•'".�ApOrMNA� ti. - LC01tlrENTSi '` "`= Y'l�Y! Y_ .'r"^:: ^^1.:..-:.�'f w'"e•,3ki+h d.-?��"RFil1+IC1115F�ED BYIAFFlLJATION :wr` - - ��7�7 F�O117'E`+. } _f �'�YAMt' '.ems "� �'��y'ACCEPTEn 61'IAFflIIATtt7N. 1;"i!r,• L.x 'V-Z'-r' ti 'rMTE 1' TIrE� _ _3A1�Pl.E r�t�IT10NS_V. Z2 T i J SiMPLE_R i"eAt&Si&ATURE - • ° y _ ,{.' - _S.*. - . -_ - - PRINT Name of SAMPLER: �G^CL t m N , o r rr a m$ V m Y to c SIGNATURE or SAMPLER: E apdi Co G� — y STORMWATER D_!XHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCSSAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAMEti^��LS�'r��� . ZnQ PERSON COLLECTING SAMPLE(S) r vl" CAI CERTIFIED LABORATORY(S) _��+� _ +�Qlvtci� Lab # E 4 20 r9 FE� Part A: Specific Monitoring Requirements C FE , . � i:n COUNTY t4e_V3 t4�oac',� PHONE NO. (°+1Q (SIGNATURE OF PERNKTTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Outfall No. Date Sample Collected 50050 —, `� C I Total Flow (if app.) Total Rainfall L6 B mo/ddl r . MG inches. aoa iZ'Z6 110 ,.b 3•, ,o Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes no (if yes, complete Part 13) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 . SGT-HEPi? ), if appl.' Total Suspended Solids pH New Motor Oil Usage mo/d!y r MG, inches mgA m unit allmo Form S WU-247-062310 D_ 1 -f- I STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit:) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable —see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified: personnel properlygather and evaluate the information submitted. 'Based on my inquiry -of the person or persons who manage the system, or those persons directly -responsible for•gathering.the.information,.the information submitted is, to the best of -my knowledge and -belief, true, accurate, and complete. I am aware that there are significant.penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Form S WU-247-0623 10 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000088 SAMPLES COLLECTED DURING CALENDAR YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from ` the date the facility receives the sampling results from the laboratory.) FACILITY NAME Hexion, INC E�. , F—: 1V97COUNTY Cumberland PERSON COLLECTING SAMPLE(S) Jonathan Shaw I Caleb Stoker PHONE NO. 9( 10 ) 483-1311 CERTIFIED LABORATORY(S) Microbac Lab 4 11 JAN 2 5 2019 -- — -- �-- Envirochem Lab # 94 CENTRAL FILE - SIGNATURE OF PERMITTEE OR DESIGNEE DV` R SEuTI - REQUIRED ON PAGE 2. Part A: Specific Monitoring Requirements - !1-�o,ONra.N:uon'' ':�t..��f.,fah�x1l.Ffl•: __7F`^x,±',;:���.t_d- r�r�.'..:.k k'7cF� 4 :`��SG�':ao7,Lm'li'lC,e.p'kc':t-. .e'mady�>v'��^.��-- _'e � �5E0lo0_ w5.0 .!. t:f'Dt�� rTotal oa.:tm ,.�}'.�UcR,!�•�.,. .% .�3aC'Qti•.D+i�f";'as.," ;-,t C ,ti,`.,.:;:,:cr .r� r•-�-.•...., CQ �D 4,1s:Methanolh Ft:�'. ,^«A"n.x•:.h.�.t'-a{•�•c,-�qa_ 'y � t�, e � �Jt-TKN i?��f. F,�.det. �a•:l,.kff.:a .:.;t-r.or'��._; gS_v.3e�1�ni E �,rAm'...s-;:'_1�'.,.! .�.:.or.t '�.,,tit m. >mo/d'd/'r�;.N 002 08/13/2018 Nla 0.81 5.80 20.2 <1.00 1.06 1.54 <0.500 001 10/11/2018 Nia 0.51 11.0 27.0 <5.00 1.9 1.9 0.5 003 10/11/2018 N/a 0.51 TO 74.0 <5.00 2.6 4.9 0.4 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? oyes &no (if yes, complete Part B) Part B: Vehicle Maintenance Activity MonitoringRe uirements Outfall"€��xy !Date_i µ°� s<50050h k �u�.r a'04556� t: 1 ,. r >f OQ40Q w, x h x r� f ' �OQS30k� iNo , �,, r$am le � (f�C^yoIIected'/ifian To"talMFlow' Totals a h ' rOillt&iGrease"� N_oui`"olar Total„ ° ' i +`HG" are 1: ' �Nii v Motors M" 1. hcaiile-< -Rainfalls " �f,a t �� PP) tq O&G/I1'H z 7 =Sus ended P - OUsa es g - S F 4r�` t y, ..� ..K ,pk a s►- �C s 1 l'P .) 3#' - r n "+ _r, -A �., 9 � r � {[ � , _ �}""^.7. ' .s<i-.. 166,V } =r fi+.y + �' �� a- �.+ � .. ✓ - � y � (Methi ".', ,SoUds� s 9 f � yai x /�54GT`HEM), if=:J+ F1 �� T -. �" � '�• J Y-- M [ i 1:�` R; -.._� � µ � - - m 'F'T -A c. _^. - ... elF G: .,.,.c rS.t^, ,�. . :.L.: .. � ,a�+r�eJ _tS .r,. .,» ..tat? .a R.;3:� � nsi f �!�,". tar" r•. � } .-F • Y' 'Y: `�- 'C` .�-�' - '�.�+ yfiKi i:' Fr �.6� „�...:imcfies [ M1. L2' ' Y„ s. i +.✓ 3. l --nt e Y r s•�-.- r ' ' [r r ; eIVIG Form SWU-247, last revised 6/1212015 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 08/13/18 Total Event Precipitation (inches): 0.81 Event Duration (hours): N/a (only if applicable — see permit.) (if more than one storm event was sampled) Date 10/11/18 Total Event Precipitation (inches): 0.51 Event Duration (hours): N/a (only if applicable — see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and be ie.,true, accurate, and complete. I am aware that there are significant penalties for submitting false information, includtug t_I oe�ss �y of fines Ad imprisonment for knowing violations." (Date) Form SWU-247, last revised 611212015 Page 2 of 2 &�MICROBAC& Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8H0199 Hexion Project Name: Stormwater samples Mr. Jonathan Shaw Project 1 PO Number: NIA 1411 Industrial Drive Received: 08/14/2018 Fayetteville, NC 28301 Reported: 0813012018 Case Narrative Total Nitrogen Calculation: 2.60 Analytical Testing Parameters Client Sample ID: Outfall 002, grab Sample Matrix: Aqueous Collected By: Client Lab Sample 11): K81-t0199-01 Collection Date: 08/13/2018 9:20 Wet Chem -is" Result RL Units Note Prepared Analyzed Analyst Method: Calculation Total Nitrogen 1.54 0.0300 mg/L 08114/18 0946 08/15/18 1618 DSK Method: EPA 300.0, Rev. 2A (1993) Nitrate as N 1.07 0,0300 mg1L 08/14/18 0946 0811511E 1618 DSK Nitrite as N 0.470 0.0500 mg1L 08/14/18 0946 08/15/18 1618 DSK Method: SM 4500 NH3 C-2011 Ammonia as N <0.500 0.500 mg1L 081151M 0945 MT Method: SM 5210 B-2011 BOD 5.80 2.00 mg/L G1 08/15/18 0919 ❑C Method: SM 5220 D-2011 COD, Totai 20.2 10.0 m91L 08/23/18 0834 DC Subcontracted Analyses Result RL Units Note Prepared Analyzed Analyst Method: EPA 1671 Methanol <1.00 1.00 mglL Y 08/20118 1303 JAW Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Result RL Units Note Prepared Analyzed Analyst Method: EPA351.2 Nitrogen, Total Kjeldahl 1.06 0,200 mg/L 08/25/18 1211 TMM Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com page 1 of 3 �VMICR®BACs Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8H0199 Definitions Gi: The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0,20 mg/L. MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted.[/l�iLdZ P—e The data and information on this, and other accompanying documents, represents Jeanne Overstreet only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. ClEent Relationship Specialist, Environmental Reported: 0813012018 13:18 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Pogo 2 of 3 Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (91 D) 864-1920 �d � � 1� Q B � C �' *K8H0199* CHAIN OF CUSTODY RECORD CLIENT NAME&ADDRESS: Hexion 1411 Industrial Drive Fayetteville, NC 28301 PO9 I PROJECT] LOCATION: Stormwater - Semiannual #OF s O T T L E s TYPE OF ANALYSIS PRESERVATION CODE O M ¢ Z 0 Q Z Y O 0 -. O z = LV 2i co Z N O Z CODE: A = <4°C ONLY B = HNO3 (pH<2) + <4°C C = H2SO4 (pH<2):+ <4"C D = NaOH + <4'C .;_ E= ZN Acetate <4°C F = Sodium Thio. CONTACT PERSON:- PHONE: 910-987-5928 SAMPLER: DATE IMETHOD OF SHIPMENT: LAB 1D # SAMPLE TYPE DATE TIME COMP GRAB PH FtD S.u. D.O. TEMP'C RES. CHLORINE V� v Outfall 00�2' �. (�� �1,' ZD X 4 A A A I I 1 C Relin 'she b Signature) 110 Date Time Re c ' ed • (Signature). L z Date Time Relinquished by; (Si aura) Date Time Received by: [Signature[. Date Time 3 4 Relinquished by., (Signature) Date une Received by: (Signature) Date Time 5 1 1 6 Comments or Special Hazards: Page 3 of 3 Environnmental Chemists, Inc. 6602 Windmill Way, Wilnington, NC 28405 • 910,392,02.23 Lab • 910.392.4424 Fax 710 Bowsertowa Road, Ivlanteo, NC 27954 ■ 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmetitalchemists.com Hexion-Fayetteville, NC Date of Report: Nov 11, 2018 1411 Industrial Drive Customer PO #: Fayetteville NC 28301 Customer 1D, 18080043 Attention: Caleb Stoker Report #: 2018-16830 Project ID: Semi -Annual Storm Water Samples Lab lD Sample ID: Collect Date/Time Matrix Sampled by 18-42500 Site: outfall 001 10/11/2018 2:02 PM Water client Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1 0.5 mg/L 10/28/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 1.9 mg1L 10/2912018 SOD SM 5210 s 11 mg1L 10/12/2018 COD SM 5220D 27 mg/L 10/18/2018 Methanol SW 846 method B015 <5 mg/L 11/08/2018 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.03mg/L 10/12/2018 Nitrate Nitrogen Subtraction Method <0.02mg/L 10/28/2018 Total Nitrogen (Calc) Nitrate+Nitrite-Nitrogen EPA353.2 0.04 mg/L 10/24/2018 Total Nitrogen Total Nitrogen 1.9 mg/L 11/08/2018 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 18-42501 Site: outfall 003 10/11/2018 2:09 PM Water client Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1 0.4 mg/L 10/28/2018 Total Kjeldahl Nitrogen (TKN) EPA 351.2 2.6'mg/L 10/29/2018 BOD SM 5210 8 7 mg/L 10/12/2018 COD SM 5220D 74 mg/L 10/18/2018 Methanol SW 846 method 8015 <5 mg1L 111C812D18 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.12 mg/L 10/12/2018 Nitrate Nitrogen Subtraction Method 2.21 mg/L 11/08/2018 Total Nitrogen (Calc) Nitrate+ N itrite-N itrogen EPA353.2 2.33mg1L 11/07/2018 Total Nitrogen Total Nitrogen 4.9 mg/L 11/08/2018 Report #:: 201 B-1fi830 Page 1 of 2 Environmental Chemists, Inc. e_ nviir em- ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highwa`; Jacksonville, NC 28540 a 910,347.5843 Lab/Fax info@environmentalchemists.com Hexion-Fayetteville, NC Date of Report: Nov 11, 2018 1411 Industrial Drive Customer PO #: Fayetteville NC 28301 Customer ID: 18080043 Attention: Caleb Stoker Report #: 2018-16830 Project ID: Semi -Annual Storm Water Samples Comment: S Reviewed Report #:: 2018-16830 Page 2 of 2 6602 Windmill Way onNC min ENVIRONMENTAL CHEMISTS, I N C OFFICE: 910-392-223iIFAX 910 -392-4424 5 Analyticai & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client. Hexion-Fa etteville, NC PROJECT NAME: Semi -Annual Storm Water Samples REPORT NO: ADDRESS: 1411 Industrial Drive CONTACT NAME: Caleb Stoker PO NO: Fayetteville, NC 28301 REPORT TO: Sonya M ers PHONEIFAX: COPY TO: Caleb Stoker email: calcb.stoker@hexion.com Samoled Bv: SAMPI F TYPE: I = Influent. E = EffluPnt. W = WPII. ST = Stream. SO = Soil.-SL = Sludae. Other: Sample Identification Collection R A E `o tC? c U ;a �c� `o U � _� r E U � 2 m� Z PRESERVATION ANALYSIS REQUESTED Date Time Temp z i U x N ij o z o ~ z O Outfall 001 - Aqueous (grab) G 1 o-t 4� C P 1� COD, BOD, McOH, TKN, NH3 as N,- Total N, Nitrate as N, Nitrite as N G GZ'� C P G G Outfall 003 - Aqueous (grab„G, c� l t b I ` E C P �ib COD, BOD, McOH, TKN, NH3 as N. Total N. Nitrate as N, Nitrite as N G C P G G C P G G C P G G C P G G C P G G C P G G Metals: Transfer Relinquished By: Date/Time Received By: DateMme 2. Temperature when Received--__ '7 Accepted: ✓ Delivered By: Received By: Comments: ample Requested: )ate: ime: ot• ' TURNAROUND: �.S January 2, 2019 Division of Water Quality ATTENTION: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: SDO Monitoring Report Sample 41 Year 1 Period 2 BRP US Inc, Spruce Pine, Mitchell County Permit No. NCS000093 To Whom It May Concern: BRP US Inc. 1211 Greenwood Road Spruce Pine, North Carolina USA 28777 T 828.766.1100 F 828.765.2391 www.brp.com RECEIF D JAN 15 ZU19 DWR SECTION Enclosed are the original and one copy of the completed Stormwater Discharge Outfall (SDO) Monitoring Report for the BRP US Inc. facility located in Spruce Pine for samples collected December 14, 2018. This is Sample Number 1, Year 1 - Period 2 of the Monitoring Schedule. I trust this satisfies the reporting requirements pursuant to Permit Number NCS000093 Part III Section E 1 & 2. Should you have any questions regarding this information, please contact me at (828) 766-1185. Respectfully, Bernice Wilson EHS Coordinator cc: Curtis Taylor Ski -Doe Lynx Sea-Doo Evinrude Johnson Rotax Bombardier ATV ORIGINAL Permit Number NCS000093 STORMWATER DISCHARGE OUTFALL (SDO MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: 61 FACILITY NAME BULB INC. PERSON COLLECTING SAMPLE'S)Di() C1�jl 7b.11 CERTIFIED LABORATORY(S) A PJA0! t6 61 L, Lab # Lab # Part A: Specific Monitoring Requirements (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) Outf all No. Date Sample Collected Total Rainfall TSS Aluminum pH mod inches MWI m -f ] f� O.C. �� 3-//p %� 0,1 COUNTY �� I ��7( N C L PHONENO.(U4"'r�) -noo SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Xno (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date Total Flow Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if Rainfall (if appl.) O&G/TPH Suspended Oil Usage applicable) (Method 1664 Solids S GT-HEM), if appl. mod MG inches mo m unit a mo N/A FORM SWU-247, LAST REVISED 2/2/2012 PAGE 1 OF 2 JAM020 STORM EVENT CHARACTERISTICS: Date 12-1 ') Total Event Precipitation (inches): � Event Duration (hours): (only if applicable - see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable - see permit_) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-16T7 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Az (Date) FORM SWU-247, LAST REVISED 2/2/2012 PAGE 2 OF 2 e Permit Number NCS000093 STORMWATER DISCHARGE OUTFALL(SDO) MONITORING REPORT SAMPLES COLLECTED DURING CALENDAR YEAR: 0 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME PERSON COLLECTING SAMPLE(S) CERTIFIED LABORATORY(S) f h" APJA U1 �t 14L_ Lab # � -- Lab # Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected Total Rainfall TSS Aluminum pH mo dd/ r inches m mgA- VJ1 A 0,Z& 3- - 0►iOl 7- COUNTY A& T (, N ECC PHONE NO. ( Z } j 4.1 & — I i 00 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Does this facility perform Vehicle &Iamtenance Activities using more thail 55 gallons of new motor oil per month? _ yes X 110 (if yes, complete Part B) Part B: Vehicle Maintenance Ac ivity Monitoring Requirements OutfaII Date Total Flaw Total Oil & Grease Non -polar Total pH New Motor No. Sample Collected (if Rainfall (if appl.) O&G/TPH Suspended Oil Usage applicable) (Method 1664 Solids SGT-HEM), if appI. rno d r MG inches mWl m unit al rao N/A FORM SWU-247, LAST REVISED 2/2/2012 PAGE 1 OF 2 STORM EVENT CHARACTERISTICS: Date Total Event Precipitation (inches): Event Duration (flours): (only if applicable - see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): . - (only if applicable - see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of Iaw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r ttee) j (Date FORM SWU-247, LAST REVISED 2/2/2012 PAGE 2OF2 AALBEMARLE0 Kings Mountain Facility 348 Holiday inn Drive Kings Mountain NC 28086 January 31, 2019 Central Files - Stormwater 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Semiannual Stormwater Discharge Summary Report t-r Albemarle — Permit NCS000096 'ES 0 Kings Mountain, Cleveland County, NC 20iy Certified Mail 7014 2120 0004 3694 0931 CENTF,)A _ r--jLFc. l iNR C'�CTlpN Dear Sir or Madam: Please find attached a Semi -Annual Stormwater Discharge Outfall (SDO) Monitoring Report for the Albemarle facility located in Kings Mountain, North Carolina. This report was prepared in accordance with the site's General Stormwater Permit effective on November 1, 2009 and covers the Monitoring Period of November 2018 — April 2019. Based on the sampling results summarized herein, it appears that the site has met its benchmark goals during the reporting period and will continue to implement appropriate best management practices to maintain these goals. Should you have any questions or need additional information related to this data, please contact John Kuhn at 704-734-2708. Jon K n HSE Manager STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS000096 FACILITY NAME 6 \1 a n- d o— V— -- PERSON COLLECTING SAMPLE(S)-- CERTIFIED LABORATORY(S) 11 ct �1m c. Lab # tf0 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 0-019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Gle �-A a —J PHONE NO. ( 2- , 39 .1.5D 1 SIGNATURE OF PERMITTEE OR DESIGNEE REOUIRED.ON PAGE 2 • , DateI1 Sample . Collected 1 11 1 11 1I r . Total Susp�ndtd Solids Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes' no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall Date 50050 00556 00530 100400 No. Sample Total Flow Total Oil"& Grease Non -polar Total pH New Motor Collected (if Rainfall (if appl.) O&G/TPH Suspended Oil Usage applicable) (Method 1664 Solids SGT-HEM), if app1. j m dd/ _ MG . inches m me unit I gaJ6mo N/A I - PERMIT DATE: 11/1/2012-10/31/2017 7 SWU-245, LAST REVISED 10/25/2012 PAGE 1 OF 6 STORM EVENT CHARACTERISTICS: Date 412-41 let Total Event Precipitation (inches): D• (.3 Event Duration (hours): Co (only if applicable - see permit.) (if more tha-t-ope storm event was sampled) Date Total Event Precipitation (inch Event Duration (hours): (only ' icable - see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 3P lq (Signature of Perry t e) ( ate) PERMfi DATE: 11/1/2012-10/31/2017 SWU-245, LAST REVISED 10/25/2012 PAGE 2OF6 WestRock January 16, 2019 Division of Water Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 100 Gaston Road Roanoke Rapids, NC 27870 office: 262.533.6295 neal.davis rr westrock.com RECEIVED ,BAN 17 2019 CENTRAL FILES DWR SECTION Re: Stormwater Discharge Outfall Monitoring Report December 2018, KapStone Kraft Paper Corporation, Roanoke Rapids NC, NCS000106. To Whom It May Concern; As required by the Division of Water Quality, enclosed are three copies of the KapStone Kraft Paper Corporation, Roanoke Rapids, NC, Stormwater Discharge Outfall Monitoring Report for December 2018, The permit number is NCS000106. Results are for the monitoring period August 1, 2018 through January 31, 2019. December 12, 2013 we applied for our Stormwater permit renewal and at this time we have not received a renewal. On Friday November 2, 2018, KapStone Paper and Packaging Corporation became a wholly owned subsidiary of WestRock Company. This transaction will not result in a change in the legal entity holding the above referenced permit. As such, the Roanoke Rapids Mill is still owned by KapStone Paper and it is proper to file applications and maintain permits as KapStone Paper until further notice If you have any questions or concerns please feel free to contact me at 252-533-6295 or e-mail me at neal.davisgwestrock.com Sincerely, N I R. Davis Environmental Engineer / ORC Westrock Roanoke Rapids Mill 100 Gaston Road Roanoke Rapids, NC. 27870 STORMWA`I'ER DISCHARGE OUTFALL (SDO) Permit Number: NC NCS 000106 Certificate of Coverage Number: NCG MONITORING REPORT SANIPLES COLLECTED DURING CALENDER YEAR: 2018 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME KAPSTONE KRAFT PAPER CORP., ROANOKE RAPIDS, NC. COUNTY HALIFAX PERSON COLLECTING.SAMPLE(S) Neal Davis PHO1 O. d252 53 295 CERTIFIED LABORATORY (S) MERITECH, INC. ENVIRONMENTAL LAB AV LABORATORY CERTIFICATION No. 165 (SIG TURE OF PERMITTEE OR DESIGNEE) By t1fis signiture, 1 certify that this report is accurate complete to the best of my knowledge. Part A: Specific Monitoring Requirements Outfall No. Date Sample Collected 50056 EPA 410.4 SM 2540 D EPA 200.7 EPA 200.7 SM 4500 H B EPA 1664A Total Flow COD TSS Total Phosphorus Total Rec. LEAD Ph OIL & GREASE mo/dd/yr MG mg/L m mg/L mg/L standard m 'PENT 12/28/2018 0.271 MG < 15 5 0.034 0.056 6.8 < 5 Does this facility perform Vehicle Maintenance Activities using more then 55 gallons of new motor oil per month? _X_yes ,no (if yes, complete part B) *** ALL SUCH MAINTENANCE AREAS ARE INSIDE BUILDINGS WITH DRAINS TO MILL WASTEWATER FACILITIES Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow Oil and Grease Total Suspended Solids pH New Motor Oil Usage mo/dd/yr MG mg/I mg/l unit gal/mo Form SWU-246-051100 Page I of 2 STORM EVENT CHARACTERISTICS: Total Event Precipitation (inch/es): mid Event Duration (hours): Ap (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) iMail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh. North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting; false information, including the possibility of fines and imprisonment for knowing violations." /24",/Q4,W- 1,116119 (Signat re of ermittee) (Date) Form S W U-246-1 12609 Page 2 of 2 Perdue Foods Perdue Foods LLC Environmental Services 416 South Long Drive Rockingham, NC 28379 www.perd ue.com Central -Files Division of Water Resources 1617 Mail Center Raleigh, NC 27699-1617 Subject: Storm Water Monthly Monitoring Report Permit no. NCS000130 Perdue Farms, Rockingham, NC To Whom It May Concern: January 2, 2019 RECEIVED `t'1r -SECTION As specified under the Tier Two Storm Water permit requirements, please find attached two copies of the May 2018 monthly storm water monitoring report for the Perdue'Foods, LLC, facility located at Rockingham, North Carolina. This monitoring report meets the requirement under Part II; Section B; Analytical Monitoring Requirements for the facility's Storm Water Permit. For the month of December 2018, there was not a qualifying rain event where a storm water sample could be collected. This is required in statement 3 of the Tier Two requirements, please find attached the monthly monitoring report indicating "No Flow" If you should need any additional information, please contact me at 910-997-8593. Since ely, —� Dennis G. Parker Environmental Manager Cc: Fayetteville Regional Office Division of Water Resources 225 Green Street, Suite 714 Fayetteville, NC 28301 Perdue Foods. A Heritage of Innovation. STORMWATER DISCHARGE OUT(aALL (SDO) MONITORING REPORT Permit Number NCS /yn 4 FACILITY NAME PERSON COLLECTING SAMPLE(S) CERTIFIED LABORATORY(S) Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR:� / (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the s"pling results fronkte laboratory.) f COUNTY PHONE NO. SIGNATURE OF PERMITTEE OR DESIGNEE a REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall mo/dd/ r MG inches :a• j� Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall ' - `: No. Date : -` _ Sample � Collected :50050- 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) _ Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage rno/ d/ r -,,-MG inches mg/1 m /I unit aUmo Form SWU-247, last revised 21212012 Page 1 of 2 STORM .EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date D� Attn: Central Files Total Event Precipitation (inches). VV w 1617 Mail Service Center Event Duration (hours): (only if applicable —see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches); Event Duration (hours); (only if applicable —see permit.) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm ttee) (Date) Form S WU-247, last revised 21212012 Page 2 of 2