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HomeMy WebLinkAboutWQ0038071_Application_20200610PO Box 146 Ronda, NC 28670 336-777-6909 www.usbiosolids.com Tuesday, June 9, 2020 North Carolina Department of Environmental Quality Division of Water Resources Water Quality Section Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Reference: Permit Renewal Permit No. WQ0038071 U.S. Biosolids, Inc. Class A Distribution Program U.S. Biosolids, Inc. is submitting this permit renewal package for the distribution of class A residuals. There are no changes or modifications in this renewal package since the last issuance of Permit WQ0038071. There are currently three residuals sources listed in permit WQ0038071: Town of Forest City Water Treatment Plant, Town of Denton Water Treatment Plant, and the City of Mount Holly Water Treatment Plant. These three residual sources are requested to be renewed with this permit. Your attention in the review of this permit renewal application is highly appreciated. Should any questions or concerns arise during the review of this permit renewal package, please do not hesitate to contact me at my direct line at 336-777-6909 or at zachkey@usbiosolids.com Sincerely, " Y�� Zach Key U.S. Blosolids, Inc. State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application_ and su ortin documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General —This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T . l 100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ❑ Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ The project name should be consistent on the plans, specifications, etc. ❑ The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0I06(b). ❑ if this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). ... Facility Classification New Permit Major Modification' Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 . .... ......... ......... ......... . Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage, adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (AII Application Packages) ❑ List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page I of D. Program Information (All Application Packages) ❑ Provide a narrative explaining the following: ❑ How the materials will be handled and transported from where the residuals were produced to where it will be treated. El How the residuals will be processed/treated (attach process flow diagram). ❑ How leachate collection will be handled. [] Where the residuals will be stored until processed. ❑ How the final product will be distributed (packaging, bulk, etc.) ❑ What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ❑ Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ❑ Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ❑ Name and address of the person who prepared the residual that is sold or given away. ❑ A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ❑ Information on all applicable setbacks in accordance with 15A NCAC 02T. l 108(b). ❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .l 104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T. I 108 a on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T. 1104(a)(2)(B}, including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN —NOT RELEASED FOR CONSTRUCTION, F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 104(a - C. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of H. Operation and Maintenance Plan (New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ❑ Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ❑ Safety measures; may include safety training program, manuals, signs, etc. ❑ Spill response plan. including control, containment, remediation, emergency contact information, etc. ❑ inspection plan including the following information; ❑ Names and titles of personnel responsible for conducting the inspections. ❑ Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ❑ Sampling and monitoring plan including the following information; ❑ Names and titles of personnel responsible for conducting the sampling and monitoring. ❑ Detailed description of monitoring procedures including parameters to be monitored. ❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 BV Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina Department of Environmental Quality Division of Water Resources DWR Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 1. APPLICANT INFORMATION: 1. Applicant's name: U.S Biosolids Inc. Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Zach Key Title: President Applicant's mailing address: 958 Hoots Road City: Roaring River State: NC Zip: 28669 Telephone number: (336) 777-6909 Email Address: zachkeyAusbiosolids.com 2. Consultant's name: License Number (for P.E.): Affiliation: ❑ On Staff ❑ Retained (Firm: ) Consultant's mailing address: City: State: Zip: - Telephone number: (_) _- Email Address: 3. Fee submitted: 0.00 (See Instruction B) 11. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, Z renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0038071 Date of most -recently issued permit: 12-9-2015 Date of most -recently certified Attachment A (if different than the permit): 1-17-2017 III. FACILITY INFORMATION: I . Name of residuals processing facility: Forest City Water Treatment Plant City: Forest City State: NC Zip: 28043 Coordinates: Latitude: 35' 20' 55.46" Longitude: 81' 51' 50.19" Datum: NAD83 Method of measurement: GPS Level of accuracy:.01 County where facility is located: Rutherford 2. Facility contact (person familiar with residuals preparation): Name: Jason Webb Title: Superintendent Mailing address: PO Box 728 City: Forest City State: NC Zip: 28043 Telephone number: (828) 248-5215 E-mail address: watrwebb2ctownofforestcit-y com FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 365+ days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: I . Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); other (explain); Given away to local farmers for soil amendment Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added ner 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 1500 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 1500 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): The residuals are stored in two 2 l 000 000- allon la oons l2rior to distribution. These lagoons are capable of storing the residuals for 365+ days. 6. Does the facility have a stormwater management plan? ❑ Yes; 0 No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: all runoff is held in the lagoon where the residuals are stored V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals .Source Cerlificatron and all associated documentation. RSC 06-16.doc FORM: DCAR 06-16 Page 2 of Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. 1 further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; 1, Zach Key President (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of th is program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. 1 will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: 6-8-2020 FORM: DCAR 06-16 Page 3 of 3 Program Information All of the residuals produced from the Town of Denton's Water Treatment plant are stored in the residuals holding pond. The first location during the treatment that the residuals are produced is from the sedimentation basins, from where the residuals are allowed to settle out. The return water left in the sedimentation basin is pumped to the sludge holding lagoons. The second place in the treatment process that produced residuals are from the filters. The filters are backwashed and the residuals from the backwash process are sent to the sludge holding pond. Also, residuals are sent to the pond when a filter is rewashed during plant start-up. Once the residuals reach the sludge holding pond, they are stored until the pond is full enough to need a distribution even. Once it is determined that a distribution event is needed, the residuals are pumped and loaded onto tanker trucks. The residuals are given to local landowner's for use as a soil amendment. All of the residual are stored in the sludge holding pond along with any leachate or run off the may be present. All land owners that receive the residuals are given an information sheet that will explain all of the requirements and regulations for the material. This information sheet will also highlight any nutrients that will be the limiting parameter for determining the residuals loading rate. In most cases, the limiting parameter for determining the loading rate will be nitrogen. Program Information All of the residuals produced from the City of Mount Holly's Water Treatment Plant are stored in two (2) 170' X 100' holding lagoons. The first location during the treatment that the residuals are produced is from the settling basins, from where the residuals are allowed to settle out. The return water left in the sedimentation basin is pumped to the sludge holding lagoons. The second place in the treatment process that produced residuals are from the filters. The filters are backwashed and the residuals from the backwash process are sent to the sludge holding lagoons. Also residuals are sent to the lagoons when a filter is rewashed during plant start-up. Once the residuals reach the sludge holding lagoons, they are stored until the lagoons are full enough to need a distribution even. Once it is determined that a distribution event is needed, the residuals are removed using pumps and tanker trucks. The residuals are given to local landowner's for use as a soil amendment. All of the residual are stored in the sludge holding lagoons along with any leachate or run off the may be present. All land owners that receive the residuals are given an information sheet that will explain all of the requirements and regulations for the material. This information sheet will also highlight any nutrients that will be the limiting parameter for determining the residuals loading rate. In most cases, the limiting parameter for determining the loading rate will be nitrogen. Program Information All of the residuals produced from the Town of Forest City's Water Treatment plant are stored in the two (2), one million (1,000,000) gallon sludge storage lagoons. The residuals are produced from the treatment of raw water from the Second Broad River. The residuals come from two places during the treatment process. The first location during the treatment that the residuals are produced is from the sedimentation basins, from where the residuals are allowed to settle out. The return water left in the sedimentation basin is pumped to the sludge holding lagoons. The second place in the treatment process that produced residuals are from the filters. The filters are backwashed and the residuals from the backwash process are sent to the sludge holding lagoons. Also residuals are sent to the lagoons when a filter is rewashed during plant start-up. Once the residuals reach the sludge holding lagoons, they are stored until the lagoons are full enough to need a distribution event. Once it is determined that a distribution event is needed, the residuals are allowed to dry and they are removed from the lagoon with front end loaders and dump trucks. The residuals are given to local landowner's for use as a soil amendment. All of the residual are stored in the sludge holding lagoons along with any leachate or run off the may be present. All land owners that receive the residuals are given an information sheet that will explain all of the requirements and regulations for the material. This information sheet will also highlight any nutrients that will be the limiting parameter for determining the residuals loading rate. In most cases, the limiting parameter for determining the loading rate will be nitrogen. Operation and Maintenance Plan City of Mount Holly, NC Water Treatment Plant In accordance to the requirements as issued by the North Carolina Department of Environmental Quality using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T .110, the City of Mount Holly and U.S. Biosolids, Inc. are implementing this Operation and Maintenance Plan. The Class A distribution program from the City of Mount Holly's Water Treatment Plant will be conducted from the Water Treatment facility, located at I I I Mountain Island Mount Holly, NC. Residuals will be removed and given away to local farmers to be used as a soil amendment. The residuals will be removed on as needed bases; as fluctuation in the output of the plant will vary with changing economic conditions. The day to day operation of the running of the Water Treatment will be conducted by City of Mount Holly. The operations of the distribution program will be conducted by Southern Soil Builders, Inc. A label shall be provided to every recipient of the residual material, in addition to this label, the ORC will make sure every recipient is educated in the proper use of the residuals. Prior to distributing these residuals to local farmers, the following sampling conditions must be met (as is outlined in greater detail in the sampling plan attached to this Operation and Maintenance Plan). Toxicity Characteristics Leaching Procedure (TCLP) will be conducted once per permit cycle. An analysis of the parameters will be conducted annually if a distribution event takes place. A fecal coliform test shall be conducted as required in 15A NCAC 027T .1106 chapters (a) and (b) to show that the density of the fecal coliform is less than 1,000 MPN per gram of total solids, each year a distribution event takes place These samples will be collected by the ORC or his/her designee and transported to an approved lab the same day the samples are taken, as in accordance to 15A NCAC 02B .0505. The samples must be taken in a matter to ensure a representative sample of the residuals has been taken. To prevent any spills and or safety issues from occurring the flowing will take place during a distribution event. In the unlikely event of a spill consult the spill control plan immediately. 1. Access to the facility will be controlled with a locked gate and signs to prevent any unauthorized entry into the complex; this gate will be lock at the end of each day. 2. All pumps and hose will be checked at the start of each day for leaks or loose fittings. 3. All tanker valves are closed prior to loading and lids are closed prior to transport. 4. All dump trailers or dump trucks gates are tightly fastened and do not leak prior to transport. 5. All on road equipment is check as per DOT regulations for any safety or mechanical hazards or issues. 6. All equipment is secured at the end of each working day to prevent any tampering or unauthorized use. The fields should be inspected daily by the ORC or the BORC for compliance with the conditions that is outline in then permit. The inspection should consist of (but not limited to): 2. 3. All required set -backs and buffers are in compliance All required record keeping of truck and fields sheets are maintained and properly filled out so accurate records of the volume and locate of residuals are keep. All public access points are controlled (signs posted, gates closed) Make sure all fields records are turned over to the ORC and the City of Mount Holly so records and be reviewed by NCDEQ and an annual report can be constructed. If any issues or violations are discovered, the ORC, Mount Holly WTP and Mooresville Regional Office should be contacted as soon as safely possible. SPILL CONTROL PLAN- U.S. Biosolids Inc. Permit WQ0038071 City of Mount Holly -Water Treatment Plant In the event of a spill, the following should be taken IMMEDITALY. Make sure all personal and bystanders are safe- if not contact emergency services 2. Halt the source of the spill- overturned truck, leaking valve, ruptured tank. 3. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill. 4. Cleanup. Employ vacuum trucks, dump trucks, and loaders to remove as much of the spilled material as possible. Use straw to soak -up the remaining material. Dispose of the same in a landfill. 5. Flush the roadways with water if needed. If the spill occurred on a tillable area, till the same into the soil and spread lime if necessary. If a spill occurs on private property, final clean-up should be to the satisfaction of the owner. 6. Notification. (This should be done as soon as safely possible.) A. U.S. Biosolids, Inc. Main Office (336)777-6909 B. City of Mount Holly, WTP (704) 822-2928 C. NCDEQ-Mooresville Regional Office (704) 663-1699 D. County Emergency Services (Sheriff, Fire Dept.) 911 7. Reporting: The Permittee shall report by telephone to the Mooresville Regional Office, telephone number (704) 663-1699, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: A. Surface disposal of residuals abnormal in quantity or characteristic. B. Any failure of the surface disposal program resulting in a release of material to surface waters. C. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. D. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment E. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside of normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300. Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. 8. Spill Prevention. The easiest way to clean a spill is to prevent one. A. Ensure loading personal watch the vehicle being loaded. B. Ensure all valves and lids are closed C. Inspect all seals and replace if necessary. U.S. Biosolids, Inc. Mount Holly, WTP Permit No. WQ0038071 SAMPLING PLAN Annually, if a land application event occurs, multiple individual grab samples are collected from the holding pond and sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by Southern Soil Builders, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical. All samples taken will be taken in the same condition as the residuals are to be land applied. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, % total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the holding ponds. Operation and Maintenance Plan City of Forest City Water Treatment Plant In accordance to the requirements as issued by the North Carolina Department of Environmental and Natural Resources using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T . 110, the City of Forest City and U.S Biosolids, Inc. are implementing this Operation and Maintenance Plan. The Class A distribution program from the City of Forest City Water Treatment Plant will be conducted from the Water Treatment facility, located at 581 Vance Street Forest City, NC. Residuals will be removed and given away to local farmers to be used as a soil amendment. The residuals will be removed on as needed bases; as fluctuation in the output of the plant will vary with changing economic conditions. The day to day operation of the running of the Water Treatment will be conducted by the City of Forest City. The operations of the distribution program will be conducted by Southern Soil Builders, Inc. A label shall be provided to every recipient of the residual material, in addition to this label, the ORC will make sure every recipient is educated in the proper use of the residuals. Prior to distributing these residuals to local farmers, the following sampling conditions must be met (as is outlined in greater detail in the sampling plan attached to this Operation and Maintenance Plan). Toxicity Characteristics Leaching Procedure (TCLP) will be conducted once per permit cycle. An analysis of the parameters will be conducted annually if a distribution event takes place. A fecal coliform test shall be conducted as required in 15A NCAC 027T .1106 chapters (a) and (b) to show that the density of the fecal coliform is less than 1,000 MPN per gram of total solids, each year a distribution event takes place These samples will be collected by the ORC or his/her designee and transported to an approved lab the same day the samples are taken, as in accordance to 15A NCAC 02B .0505. The samples must be taken in a matter to ensure a representative sample of the residuals has been taken. To prevent any spills and or safety issues from occurring the flowing will take place during a distribution event. In the unlikely event of a spill consult the spill control plan immediately. 1. Access to the facility will be controlled with a locked gate and signs to prevent any unauthorized entry into the complex; this gate will be lock at the end of each day. 2. All pumps and hose will be checked at the start of each day for leaks or loose fittings. 3. All tanker valves are closed prior to loading and lids are closed prior to transport. 4. All dump trailers or dump trucks gates are tightly fastened and do not leak prior to transport. 5. All on road equipment is check as per DOT regulations for any safety or mechanical hazards or issues. 6. All equipment is secured at the end of each working day to prevent any tampering or unauthorized use. The fields should be inspected daily by the ORC or the BORC for compliance with the conditions that is outline in then permit. The inspection should consist of (but not limited to): 1. 2. All required set -backs and buffers are in compliance All required record keeping of truck and fields sheets are maintained and properly filled out so accurate records of the volume and locate of residuals are keep. All public access points are controlled (signs posted, gates closed) Make sure all fields records are turned over to the ORC and the City of Forest City so records and be reviewed by NCDENR and an annual report can be If any issues or violations are discovered, the ORC, Forest City Water Treatment Plant and the Asheville Regional Office should be contacted as soon as safely possible. SPILL CONTROL PLAN- U.S. Biosolids, Inc. CITY OF FOREST CITY -WATER TREATMENT PLANT In the event of a spill, the following should be taken IMMEDITALY. Make sure all personal and bystanders are safe; if not, contact emergency services without delay. 2. Halt the source of the spill- overturned truck, leaking valve, ruptured tank. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill. 4. Cleanup. Employ vacuum trucks, dump trucks, and loaders to remove as much of the spilled material as possible. Use straw to soak -up the remaining material. Dispose of the same in a landfill. 5. Flush the roadways with water if needed. If the spill occurred on a tillable area, till the same into the soil and spread time if necessary. If a spill occurs on private property, final clean-up should be to the satisfaction of the owner. 6. Notification. (This should be done as soon as safely possible.) U.S. Biosolids, Inc. Main Office (336) 777-6909 City of Forest City Water Treatment Plant (828) 248-5215 NCDEQ, Asheville Regional Office (828) 296-4500 County/City Emergency Services (Sheriff, Fire Dept.) 911 7. Reporting. The project manager shall detail how the spill occurred and all action that was taken. A written report shall be given to the Asheville regional office as soon as possible, and within 24 hours of the spill, or next working day. 8. Spill Prevention. The easiest way to clean a spill is to prevent one. A. Ensure loading personal watch the vehicle being loaded. B. Ensure all valves and lids are closed. C. Inspect all seals and replace if necessary. U.S. Biosolids, Inc. Forest City, WTP Permit No. WQ0038071 SAMPLING PLAN Quarterly, if a land application event occurs, multiple individual grab samples are collected from the holding pond and sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by U.S. Siosolids, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical. Ail samples taken will be taken in the same condition as the residuals are to be land applied. Quarterly, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, %total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the holding ponds. This test will be done by a NC certified laboratory. Operation and Maintenance Plan U.S. Biosolids, Inc. Town of Denton Water Treatment Plant In accordance to the requirements as issued by the North Carolina Department of Environmental and Natural Resources using NCGS 143-215.1 and 143-215.3(a) based on 15A NCAC 02T .110, the Town of Denton and Southern Soil Builders, Inc. is implementing this Operation and Maintenance Plan. The Class A distribution program from the Town of Denton's Water Treatment Plant will be conducted from the Water Treatment facility, located at 3049 Bringle Ferry Road Denton, NC. Residuals will be removed and given away to local farmers to be used as a soil amendment. The residuals will be removed on as needed bases; as fluctuation in the output of the plant will vary with changing economic conditions. The day to day operation of the running of the Water Treatment will be conducted by the Town of Denton. The operations of the distribution program will be conducted by Southern Soil Builders, Inc. A label shall be provided to every recipient of the residual material, in addition to this label, the ORC will make sure every recipient is educated in the proper use of the residuals. Prior to distributing these residuals to local farmers, the following sampling conditions must be met (as is outlined in greater detail in the sampling plan attached to this Operation and Maintenance Plan). Toxicity Characteristics Leaching Procedure (TCLP) will be conducted once per permit cycle. An analysis of the parameters will be conducted annually if a distribution event takes place. A fecal coliform test shall be conducted as required in 15A NCAC 027T .1106 chapters (a) and (b) to show that the density of the fecal coliform is less than 1,000 MPN per gram of total solids, each year a distribution event takes place These samples will be collected by the ORC or his/her designee and transported to an approved lab the same day the samples are taken, as in accordance to 15A NCAC 02B .0505. The samples must be taken in a matter to ensure a representative sample of the residuals has been taken. To prevent any spills and or safety issues from occurring the flowing will take place during a distribution event. In the unlikely event of a spill consult the spill control plan immediately. Access to the facility will be controlled with a locked gate and signs to prevent any unauthorized entry into the complex; this gate will be lock at the end of each day. 2. All pumps and hose will be checked at the start of each day for leaks or loose fittings. 3. All tanker valves are closed prior to loading and lids are closed prior to transport. 4. All dump trailers or dump trucks gates are tightly fastened and do not leak prior to transport. 5. All on road equipment is check as per DOT regulations for any safety or mechanical hazards or issues. 6. All equipment is secured at the end of each working day to prevent any tampering or unauthorized use. The fields should be inspected daily by the ORC or the BORC for compliance with the conditions that is outline in then permit. The inspection should consist of (but not limited to): 1. All required set -backs and buffers are in compliance 2. All required record keeping of truck and fields sheets are maintained and properly filled out so accurate records of the volume and locate of residuals are keep. 3. All public access points are controlled (signs posted, gates closed) 4. Make sure all fields records are turned over to the ORC and the Town of Denton so records and be reviewed by NCDENR and an annual report can be constructed. If any issues or violations are discovered, the ORC, Denton Water Treatment Plant and the Winston Regional Office should be contacted as soon as safely possible. SPILL CONTROL PLAN- U.S. Biosolids Inc. TOWN OF DENTON-WATER TREATMENT PLANT In the event of a spill, the following should be taken IMMEDITALY. 1. Make sure all personal and bystanders are safe; if not, contact emergency services without delay. 2. Halt the source of the spill- overturned truck, leaking valve, ruptured tank. 3. Contain the spill. Use straw bales or earthen barrier to form a dike to contain the spill. 4. Cleanup. Employ vacuum trucks, dump trucks, and loaders to remove as much of the spilled material as possible. Use straw to soak -up the remaining material. Dispose of the same in a landfill. 5. Flush the roadways with water if needed. If the spill occurred on a tillable area, till the same into the soil and spread lime if necessary. If a spill occurs on private property, final clean-up should be to the satisfaction of the owner. 6. Notification. (This should be done as soon as safely possible.) U.S. Biosolids, Inc. Main Office (336) 777-6909 City of Forest City Water Treatment Plant (828) 248-5215 NCDEQ, Winston-Salem Regional Office (336) 776-9800 County/City Emergency Services (Sheriff, Fire Dept.) 911 7. Reporting. The project manager shall detail how the spill occurred and all action that was taken. A written report shall be given to the Asheville regional office as soon as possible, and within 24 hours of the spill, or next working day. 8. Spill Prevention. The easiest way to clean a spill is to prevent one. A. Ensure loading personal watch the vehicle being loaded. B. Ensure all valves and lids are closed. C. Inspect all seats and replace if necessary. U.S. Biosolids, Inc. Town of Denton WTP Permit No, WQ0038071 SAMPLING PLAN Annually, if a land application event occurs, grab samples are collected from the holding pond. Samples from the pond will be combined to form individual grab samples to be sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by Southern Soil Builders, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical. All samples taken will be taken in the same condition as the residuals are to be land applied. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, %total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the residuals holding pond State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two codes of the application and supportima documentation For more information, visit the Water Quality Perm itting.Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .l 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-115): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC I 1-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: ❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the"Map Guidance for Residuals Land_ Application Permits". ❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: U.S. Biosolids, Inc. Status Code° Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Town of Forest City Forest City WTP Rutherford NCO074306 1500 1500 R Town of Denton Denton WTP Davidson NCO082949 300 300 R City of Mount Holly Mt Holly WTP Gaston NCO 136020 300 300 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution. land application. or disposal (i.e. not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page l Town of Forest City Water Treatment Plant Residuals Source Certification (RSC) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Divislon of Water ReSOUMes RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Town of Forest City 2. Facility permit holder is: ❑ Federal, [] State, [D Local Government, or Ej Private. Facility permit issued by: 0 Div. of Water Resources, 0 Div. of Environmental Health, or Ej Other (explain ). 3. Facility contact person and title: Jason Webb Complete mailing address: PO Box 7285 City: Forest City State: NC Zip: 28043 Telephone number: (828) 248-5215 E-mail address: watrwebb rt townofforestcity com 4. Facility physical address: 581 Vance Street City: Forest City State: NC Zip: 28043 Coordinates: Latitude: 35' 20' 55.446" Longitude: 81 ° 5 V 50.19" Datum: NAD83 Level of accuracy:.01 Method of measurement: GPS 5. Purpose of the faci I ity: Etreatment of municipal wastewater, 0 treatment of 100% domestic wastewater, Z treatment of potable water, 0 treatment of 100% industrial wastewater, C1 treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) E] other (explain: ' ). 6. Does the facility have an approved pretreatment program: 0 Yes No 7. Facility permitted/design flow: 8 MGD and facility average daily flow: 2_4 MGD 8. Average amount of residuals being generated at this facility 783.43 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: two (2) one million -gallon lagoons Type and volume of residuals storage (i.e., outside of residuals treatment units): two (2) one million -gallon lagoons 11. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1 102(6) as: E] Biological [D Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page I of 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: El yes E no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: [] yes 2 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 08-21-2018 Passed corrosivity test: N yes E] no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: 0 yes Ej no. Flashpoint: 200 °F (> 140°F) Passed reactivity test: M yes E]no. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500) TCLP Parameter Limit (m9/0 Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 0.68 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pe ntach loro phenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-DichloroethyIene 0.7 ND 2,4,5-Trichloropheno1 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichloropheno1 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 6-29-2018 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 5 Cadmium 85 39 1 Copper 4,300 1,500 33.4 Lead 840 300 18.9 Mercury 57 17 0.4 Molybdenum 75 n/a 2.84 Nickel 420 420 17A Selenium 100 100 5 Zinc 7,500 2,800 116 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) Q > 0 but < 25 30 200 210 > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 Q > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 0 > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 39.27 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 6-29-2018 Parameter Result (mg4g) Aluminum 11500 Ammon ia-N itrogen 255 Calcium 1 160 Magnesium 2880 Nitrate -Nitrite Nitrogen 2.45 pH (Standard knit) 6.1 Phosphorus 1150 Potassium 1640 Sodium 250 Total Kjeidahl Nitrogen 3840 c. Using the results listed in Item 11, 5b. above, calculate the sodium adsorption ration (SAR): 0.558 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): 0 default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical Justification as to why the selected default value is appropriate to be applied to these residuals: Non -Processed Residuals e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 1563.95 1673.42 Injection/Incorporation 1691.45 1809.85 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Laud Application of Class A or Equivalent. Q A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or 0 A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): E] Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)] - Alkaline `treatment. Q Alternative 3 [15A NCAC 02T.1 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. [] Alternative 4 [15A NCAC 02T.1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helm inth Ova. Ej Alternative 5 [15A NCAC 0211106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: 0 composting, ED heat drying, E] heat treatment, El thermophilic aerobic digestion, El beta ray irradiation, C ] gamma ray irradiation, or ❑ pasteurization. b. For Laud Application of Class B: El Alternative I [15A NCAC 02T.1106(c)(I)]- Fecal Coliform Density Demonstration. E] Alternative 2 [15A NCAC 02T.1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: 0 aerobic digestion, [] air drying, Ej anaerobic digestion, 11 composting, or Q lime stabilization. c. For Surface Disposal: El Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. 0 Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above. El Exempt - if Daily Cover Alternative is chosen in Item 11.8. below [ 15A NCAC 02T. l 106(a)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: [] Alternative I [15A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). 7 Alternative 2 [15A NCAC 02T.1 107(a)(2)1 - 40-Day Bench Scale Test (Anaerobic Digestion). ED Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). D Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). 0 Alternative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.1 107(a)(6)] - Alkaline Stabilization. [] Alternative 7 [15A NCAC 02T.1 107(a)(7)] - Drying of Stabilized Residuals, Alternative 8 [15A NCAC 02T.1 107(a)(8)] - Drying of Unstabilized Residuals. Q Alternative 9 [ISA NCAC 02T.1 107(a)(9)] - Injection. El Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.1 107(b)(2)]. Z Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Ll Ll CF) ol Lill C) C) r- 0 4W LO c CO -I-- c CU 73 4) 06 ca 4W Co L) Z O U) U C M > O co 0 Ln L6 Process Flow Narrative The Town of Forest City receives its raw water from the Second Broad River, where the water is pumped to the Water Treatment Plant from the river. After the water reaches the Water Treatment Plant, it is feed Poly Aluminum Chloride and Sodium Hypochlorite in the flash mixer, where they are mixed with the raw water. After the water is mixed with the Aluminum Chloride and Sodium Hypochlorite, it goes from the flash mixer to a sedimentation basin, where the impurities in the water are allowed to settle out. The water in the return from the sedimentation basin is pumped to one of the two one million gallon sludge lagoons. After the water leaves the sedimentation basin, it is sent to the filters where any remaining residuals are captured and sent to the sludge lagoons when a filter is backwashed. Residuals are also sent to the sludge lagoons when a filter is rewashed during plant start-up. Once the residuals reach the sludge lagoons, it is stored until a distribution event is needed. When a distribution event is needed, the lagoon is allowed to dry out till the residuals are dry enough to be removed using front end loaders and dump trucks. Once it has been determined that the residuals have sufficiently dried enough, the residuals are sampled and distributed to local land owners for use as a soil amendment. Quantitative Justification of Residuals Production Rate The Town of Forest City produces an estimated 860 Dry Tons per year of residuals through the treatment of Potable Water. The currently requested 1500 Dry Tons should allow for any growth in the water system and for any unforeseen increases in the amount of residuals that the Water Treatment Plant in producing. U.S. Biosolids, Inc. Town of Forest City WTP Permit No. WQ0038071 SAMPLING PLAN Annually, if a land application event occurs, grab samples are collected from the holding pond. Samples from the pond will be combined to form individual grab samples to be sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by Southern Soil Builders, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical. All samples taken will be taken in the same condition as the residuals are to be land applied. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, %total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the residuals holding pond Report Number: 18-183-0201 • Account Number: 46381 �����' �� 7621 Whitepine Road, Richmond, VA-23237 Main 804-743-9401 O Fax SO4-271-6446 ANALYTICAL www.waypointanalytical.com Send To: Southern Soil Builders Project : Forest City Dennis Key 958 Hoots Road Roaring River, NC 28669 REPORT OFANALYSIS Date Sampled: 6/29/2018 14:00-00 Lab Number: 61472 Date Received: 07/02/2018 00:00 Sample Id : Forest City Date Reported: 07/12/2018 QUANT11TATIONLIMIT ANALYST * ! ► Total Solids' 39.27 392700 100.0 JM 07/02/2018 13:40 SM-2540G Moisture ' 60,72 100.0 JM 07/02/2018 13:40 SM-254OG Total Kjeldahl Nitrogen 0.38 3840 50.0 R D 07/03/2018 09:00 SM-4500-NH3C-TKN Phosphorus 0.12 1150 50.0 KKM 07/10/2018 00:27 60100 Potassium 0,16 1640 50.0 JTR 07/10/2018 00:27 6010D Sulfur 0.21 2050 50.0 KKM 07/10/2018 00:27 6010D Calcium 0.12 1160 50.0 KKM 07/10/2018 00:27 6010D Magnesium 0.29 2880 50.0 KKM 07/10/2018 00:27 6010D Sodium <0A3 <250 250 KKM 07/11/2018 00:45 6010D Iron 50700 50.0 KKM 07/10/2018 00:27 6010D Aluminum 115000 500 SKN 07/11/201811:25 6010D Manganese 987 5.00 KKM 07/10/2018 00,27 6010D Copper 33.4 2.50 KKM 07/10/2018 0027 6010D Zinc 116 5.00 KKM 07/10/2018 00:27 6010D Ammonia Nitrogen 0.03 255 50.0 R D 07/03/2018 09:00 SM-4500-NI3C Organic N 0.35 3585 50.0 07/03/2018 09:00 CALCULATION Nitrate+Nitrite-N <2.45 2.45 MMT 07/05/2018 09:50 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. �G PaW� GI E m � _, _. ... .. ., _ �, :� - . _._ -... , , - „ -.. _ .,< Pauric McGroary Agronomist Report Number: 18-183-0201 Account Number_ 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number'. 61472 Sample Id : Forest City Waypoint0 ANALYTICAL Cadmium <1.00 Chromium 45.2 Nickel 17.4 Lead 18.9 Arsenic <5.00 Mercury <0.400 Selenium <5.00 pH' 6.1 Molybdenum 2.84 Comments: NC CERT4257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. Project : Forest City REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Hate Sampled: 6/29/2018 14:00:00 Date Received: 07/02/2018 00:00 Date Reported: 07/12/2018 1.00 KKM 07/10/2018 00,27 6010D 2.50 KKM 07/10/2018 00:27 60100 2.50 KKM 07/10/2018 00:27 6010D 3.00 KKM 0711012018 00:27 6010D 5.00 KKM 07/11/2018 00:45 6010D 0.400 SMC 07/06/2018 13:52 SW-7471 B 5.00 KKM 07/10/2018 00-27 6010D 1.0 R D 07/03/2018 09:00 9045D 2.50 KKM 07110/2018 00:27 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. poJ{G Inc &Wr Pauric McGroary Agronomist PAN Mineralization Rate TKN::[ NH3 NO3 0.4 3840 255 2,45 PAN Surface —1563.951 mglkg 3.1279 lbs/dry ton 2450.491 Ibs total PAN 28.8293 !bs PAN/acre PAN In'ection 1691.45 mg/kg 3.3829 Ibsld ton 2650.265 lbs total PAN 31.17959 lbs PANlacre Dry Tons/1000 gal. 1.637659 1st year PAN Surface lbs. 2450.490697 1st year PAN Injected lbs. 2650.265347 lbs./acre Surface 28.82930232 lbs./acre Injected 31.17959232 as uecimal Total�r Acres NO2 % Solids tons/year Applied on 0 0.3927 783.43 85 MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg mglkg x .002 =Ibs/dry ton MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =Ibs/dry ton 1000 X 8.34 X %501ids X sp. q ravi "=dry tons/1000gal." 2000 SAR Sodium Absorption Ratio Na: Sodium (MgIL) Equivalent weight: 23 Ca: Calcium (MgIL) Equivalent weight: 20 Mg : Magnesium (MgIL) Equivalent weight: 12 Mil#i Equivalent = MgIL 1 Equivalent weight Na M /L Ca(Mg/L) M MIL 98.17 1 455.53 1 1130.97 Na (ME} Ca (ME) Mg (ME) 4268261 1 22.7765 1 94.2475 SAID= Na Mslli Equivalenil10.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power 5AR = 0.557993 (From MgIL entered above) TSAR= 0.(From ME entered below) Na (ME) Ca (ME) Mg (ME) 4.27 1 22.78 1 94.25 The amount of exchangeable sodium ions ver amount of exchangeable calcium & magnesiu Permitting guidance is if greater than 10 requi Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 08/21/2018 Reported: 09/10/2018 For: Forest City Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 180821-29-01 TCLP Forest City See Attached as Noted 0910612018 PACE Respectfully submitted, r0,3 Ut/a., J')'')) ,rL ,,I Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Paget of 29 Condition of Receipt Sam le Numbor 180821-29-D1 Temp on Arrival: 2.3 Parameter Schedule: TCLP Received on Ice PO Box 228 - Statesville, NC 28687 - 704/872/4697 Page 2 of 29 vllcl 11. Address: 004hern sort Q 1 Je. :.r%c Contact Person: PO t; Cuslorner Sample Ips !KO C. Lab -ID n LjLi'Q T— Sarr pled (Grab Only) - 4L1 l� .4Q tx sitioned by: Crete Date) TA9 LAParamcters rewested for ansiysis st.aa. ww_l$ x, 7�L STATES V11XE A NALYnCAL 122 Goat Stint • P.O. Box 228 SSatesvilte, NC 28b87 (704)872-407 Chain of Custody Record Relinquished by: Time I am, Date L !�ff V Sampled P by: NY Received by: Time �j t1 prr am Date �t 21i I � Transported by. Relinquished by: Time am, pm Date ��I Holding times met: Received by: Time am m Date ' p �lLo�Samnting #1: Compliance work: Time begin am, pm Date !_j_ Non-compliance work - Time end am, pm Date Lab Ctxrtments: ggwglite mp q �. Samples Transported on Ice: Time begin am, pm Date !� Time end am, pm Date "tials: h rn v \ N N O h 0 \ N a h �- • h 00 to 00 N V 2 aU � D ,` -, aceARa!ytrcal wewrlacelabscvm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 KinCeyAve- Suiie 100 Huntersville. NC 28078 (704)675.9092 Project: 180821-29.01 Pace Project No.: 92396772 Sample: 180821.29-01 Lab ID: 92396772001 Collected; 0812li18 11:00 Received: 08/22118 10:55 Matrix: Solid Results reported on a 'dry weight" bssls and are adjusted for percent moisture, sample site and any dilutions. Parameters Results Units Report Limit OF Prepared Analyzed -`------- _ p Y GAS No. Oual 8081 TCLP Pesticides RVE gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachlaro-m-xylene (S) 8082 GCS PCB PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1246 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlcrobipheryl (S) 8151A Cl Acid Herbicides TCLP 2.4-D 2,4,5-TP (Siivex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP Arsenic 8a6um Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury Date; 09/06/2018 04:43 PM Analytical Method: EPA 808113 Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 0813011a 16:22 Initial pH: 4.9; Final PH: 5 NO NO ug/L ug/L 0.50 3.0 1 09104/1815:33 09/05/1816:26 58-89.9 NO ug1L 0.50 1 09/0411815:33 09105/1816:26 57-74-9 1 NO u911, 0.50 09104/7815:33 09/0511816:26 72-20-8 1 09104/1815:33 09/05/1816:26 76,44.8 NO NO ug1L ug/L 0.50 1 09/0411815:33 0910511816:26 1024-57-3 NO ug1L 1000 1 0910411815:33 0910511816:26 72-43-5 3.0 1 09/0411815:33 09/05/1816:26 8001.35-2 53 % 10.138 44 % 10-110 0910411815:33 09/0511816:26 2051-24-3 09/04/1815:33 09105/1816:26 877-09-8 Analytical Method: EPA 8082A Preparation Method: EPA 3546 NO uglkg 50.5 1 NO u91k9 08/22/18 21:40 08/23/18 19:21 12674-11-2 50.5 1 NO uglkg 08/22118 21:40 08/23118 19:21 11104-28-2 50.5 1 NO ug/kg 08122/18 21:40 08/23118 19:21 11141.16.5 50.5 1 NO uglkg 50,5 1 08122/1821A0 08/2311819:21 53469.21.9 NO uglkg 50.5 1 08/22/18 21:40 06/23118 19:21 12672-29-6 NO uglkg 50.5 1 08122/18 21 A0 08/23/18 19:21 11097-69-1 0812208 21:40 08123/18 19:21 11096,82-5 53 % 21-132 1 08122/1821:40 08/23/1819:21 2051-24.3 Analytical Method; EPA 8151A Preparation Method: EPA 8151A Leachate MethodlDate: EPA 1311; 08127/18 15:45 Initial PH: 5.8; Final pH: 4.91 NO mg1L 0.0050 1 NO 08/29118 09:30 08/31/18 13:08 94-75.7 mg1L 0.010 1 08129118 09:30 08/31118 13:08 93-72-1 67 %. 10-155 1 08/29/18 09:30 08/31/18 13:08 19719-28-9 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Leachate Method/Data: EPA 1311; 08124/18 21:30 Initial pH: 6.91; Final pH; 4.5 NO mg1L 0.050 1 0.68 mg1L W2711819:21 08/28/1817:09 7440-38-2 0,25 1 NO mg1L 08127/1819:21 08/2811817:09 7440-39.3 0.0050 1 NO mglL 0.050 08/27/1819:21 08/28/1817;09 7440-43-9 1 ND mglL 08127/1819:21 08/28/1817:09 7440-47-3 0.025 1 NO mg1L 08127/1819:21 0812811817709 7439-92-1 0.10 1 NO mg1L 0-025 1 0812711819:21 08/28/1817:09 7782-49.2 08/27/1819:21 08/2811817:09 7440-22-4 Analytical Method; EPA 7470A Preparation Method: EPA 7470A Leachate Method/Date: EPA 1311; 08/24/18 21:30 Initial pH: 6,91; Final pH: 4.5 NO mg1L 0.00020 1 0812711820;16 00/30/1812:52 7439-97.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, wlthovt the writlan consent of Pace Anatylical Services, LLC, Page 4 of 26 PO BOX 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 29 - , ;ZeAnalXicalo !' 1NIM1Y,(laCBl8bd L9Ri ANALYTICAL RESULTS Project: 180821-29-01 Pace Project No.: 92396772 Pace Analytical Services, LLC 9800 Kincey Ave. Surke 100 Huntersvllle, NC 28078 (704)875-9092 Sample: 180821-29.01 Lab ID: 02396772001 Collected: 08121/18 11:00 Received: 08122/18 10:55 Results reported on a "dry weight' basis and are adjusted for Matrix: Solid percent moisture, sample sire and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Analyticaf Method: EPA 8270D Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311: 08/30/18 16:22 Initial pH: 4A: Final pH: 5 1,4-Dichforobenzene 2,4-binilrokotuene NO ug1L 50.0 1 09/04/18 13:20 09/06/18 08:31 106-4fi-7ND Hexachloro-1,3•butadiene NO ug1L 50.0 1 09/04/18 13:20 09106/18 08:31 121-14.2 Hexachlorobenzene NO uglL 50.0 1 09/04/18 13:20 09/06/18 08:31 87-68.3 Hexachloroethane NO ug/L 50.0 1 09/04/18 13:20 09/06/18 08:31 f18-74.1 2-Methylphenol(o-Cresol) NO ug1L 50.0 1 09/04/18 13:20 09/06/18 08:31 67-72-1 384-Methylphenol(m&pCresol) NO uglL 50.0 1 09/04/18 13:20 09/06/18 08:31 95-48.7 Nitrobenzene NO ug1L 50.0 1 09104/1813:20 09/06/18 08:31 15831-10-4 Pentachlorophenot NO ug1L 50.0 1 09/04/18 13:20 09106H8 08:31 98-95-3 Pyridine NO uglL 100 1 09104118 13:20 09/06/18 W31 87.86-5 2,4,5-Trichlorophenof NO 4/1- 50.0 1 09/04/18 13:20 09/06/18 08:31 110-86-1 orophenol ND ug/L 50.0 1 09/04/18 13:20 09/06/18 08:31 95-95 4 Surrogates Surrogate ug1L 50.0 1 09/04118 13:20 09106/18 08:31 88-06.2 Nitrobenzene-d5 (S) 2-Fluorobiphenyl(S) 76 % 12-102 1 0910411a 13:20 09/06/18 08:31 4165.60-0 Terphenyl-d14 (S) 72 88 % ,/o 13-107 1 09/04118 13:20 09/06118 08:31 321-60-8 Phenol-d6 (S) 45 21.132 1 09704118 13:20 09108/18 08:31 1718-51-0 2-Fluorophenol(S) 59 % "/a 10-110 1 09104/18 13:20 09/06/18 0&31 13127.88-3 2,4,6-Tribromophenol (S) 85 10.110 1 09104l18 13:24 09/06118 08:31 367-12-4 % 27.108 1 09/04118 13:20 09/00118 08:31 118-79-6 8260 MSV TCLP Analytical Method: EPA 82606 Leachate Method/Dade: EPA 1311: 08/23/18 15:52 Benzene 2-Butanone (MEK) NO NO ug1L 100 20 08127l18 10:41 71.43-2 Carbon tetrachloride ND u 1L 9 200 20 OB12T118 10:41 78-93-3 Carbonenzene NO uglL ug1L 100 20 08/2711810A1 56-23-5 Chloroform Chloroform NO uglL 100 20 0812711810:41 108.90-7 benzene NO ug/L 100 20 08/27118 10:41 67-66-3 1,2-Dichlorobenze NO ug/L 100 20 0812711810:41 106.46-7 1,1-Dichloroethene ND ug1L 100 20 08/2711810:41 107-06.2 Tetrachloroethena loroetne NO uglL 100 20 0812711810:41 75-35-4 Tetrac ND uglL 100 20 08/27/18 10:41 127-18-4 Vinyl chloride NO uglL 100 20 08/27/18 10:41 79-01-6 Surrogates 100 20 08127/1810:41 75-01-4 12-Dichloroethane-d4 (5) 97 % Toluene-d8 (B) 109 % 70-130 20 06/27/18 10:41 17060.07.0 4-Bromofluorobenzene (S) 100 % 67-135 20 08/27/1810:41 2037-26.5 70-130 20 08127! 18 10:41 4 fi0.40.4 Percent Mofsture Analytical Method: ASTM D2974.87 Percent Moisture 35,7 % 0.10 1 08124l18 17:19 1010 Flashpolnt,Closed Cup Analytical Method: EPA 1010A Rashpoint >200 deg F 70.0 1 09101118 02:04 Date: 09106/2018 04:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, whhout the written consent of Pace Analytical Services. LLC, Page 5 of 26 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 8 of 29 xuwDeoa7a6s.mm 1 , ANALYTICAL RESULTS Pace Analyticat Services, LLC 9800 KincoyAve, Suite 100 Huntersville, NC 28878 (704)875-9092 Project: 180821-29-01 Pace Project No,: 92396772 Sample: 180821-29.01 Lab l0: 9239677200i Collected: 08/21118 11:00 Received: 08/22118 10:55 Matrix: Solid Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 9045 pH Soil Analytical Method: EPA 9045D� pH at 25 Degrees C 5.4 Std. Units 0.10 1 08l25118 00:32 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-946 7.3.3.2 Cyanide, Reactive ND mg/kg 1.5 1 08/28118 18:38 08128/18 19:55 734S Raactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2 Sulfide, Reactive ND mglkg 15A 1 08/28/1818:38 08/28M818:41 Data: 091061201804:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the wrglan consent of Pace Analytical Services, LLC. Page 6 of 26 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 9 of 29 Town of Denton Water Treatment Plant Residuals Source Certification (RSC) Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction 13.): 1. Facility Name: Town of Denton Water Treatment Plant 2. Facility permit holder is: El Federal, Q State, 0 Local Government, or 0 Private. Facility permit issued by: [ Div. of Water Resources, EJ Div. of Environmental Health, or [ Other (explain: }. 3. Facility contact person and title: Heather Hicks, ORC Complete mailing address: PO Box 306 City: Denton State: NC Zip: 27239 'Telephone number: (336) 859-3139 E-mail address: dentonwaterplant@townofdenton.com 4. Facility physical address: 3049 Brin Ig e Ferry Road City: Denton State: NC Zip: 27239 Coordinates: Latitude: 35' 35' 53.54" Longitude: 80' 13' 25.17" Datum: NAD83 Level of accuracy:.01 Method of measurement: GPS 5. Purpose of the facility: treatment of municipal wastewater, El treatment of 100% domestic wastewater, treatment of potable water, 0 treatment of 100% industrial wastewater, 0 treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages:.I::'.;:::. % industrial and % domestic) [] other (explain::: ). 6. Does the facility have an approved pretreatment program: Yes JZ No 7. Facility permitted/design flow: 2.25 MGD and facility average daily flow: I MGD 8. Average amount of residuals being generated at this facility 200 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: One (1) 200'X150" holding pond and two (2) 40'x 120' drying beds Type and volume of residuals storage (i.e., outside of residuals treatment units): 11. RESIDUALS QUALITY INFORMATION (See Instruction C.): I. Specify if residuals are regulated under: Q 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: 0 Biological Z Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC06-16 Page 1 of 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: Q yes N no. If yes, list the number(s) b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: n yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 3-15-2016 Passed corrosivity test: yes [ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes 0 no. Flashpoint: 200 OF (> 140°F) Passed reactivity test: S yes Elno. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500) TCLP Parameter Limit (m9/1) Result (m9/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND ],I-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1 105. a. For Dislribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 8-25-2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 8.61 Cadmium 85 39 1 Copper 4,300 1,500 48.5 Lead 840 300 21.7 Mercury 57 17 0.0585 Molybdenum 75 n/a 2.5 Nickel 420 420 17.5 Selenium 100 100 5 Zinc 7,500 2,800 77.5 b. For SurfaceVjsXosal Unit (land: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratoryand Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mglkg) Chromium (mg/kg) Mickel (mg/kg) Q > 0 but < 25 30 200 210 > 25 but < 50 34 220 240 0 > 50 but < 75 39 260 270 Q > 75 but < 100 46 300 320 E] > 100 but < 125 53 360 390 Q > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 S. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 4.79 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 8-25-2019 Parameter Result (mg/kg) Aluminum 152000 Ammonia -Nitrogen 2920 Calcium 2810 Magnesium 1430 Nitrate -Nitrite Nitrogen 4.63 pH (Standard Unit) 6.5 Phosphorus 1840 Potassium 982 Sodium 297 Total Kjeldahl Nitrogen 9790 C. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0,248 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): EJ default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Non -Processed Residuals e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First Wf) Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 4212.63 4507,51 Injection/Incorporation 5672.63 6348.71 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: El A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or 0 A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): El Alternative l [I5A NCAC 02T.1 106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.1 106(b)(3)(13)] - Alkaline Treatment. n Alternative 3 [15A NCAC 02T.1 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. E3 Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, C] heat drying, heat treatment, thermophilic aerobic digestion,] beta ray irradiation, gamma ray irradiation, or pasteurization. b. For Land Application of Class 8: Alternative I [15A NCAC 02T.1 106(c)(1)] - Fecal Coliform Density Demonstration. 0 Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, ,] air drying, F� anaerobic digestion, composting, or lime stabilization. c. For Surface Di_,posal: 0 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. 0 Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item It. 7b. above. 0 Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: 0 Alternative I [ 15A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). 0 Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [ 15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Q Alternative 4 [15A NCAC 02T. l 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Q Alternative 5 [15A NCAC 02T. 1107(a)(5)] - 14-Day Aerobic Processes. 0 Alternative 6 [15A NCAC 02T.1 107(a)(6)] - Alkaline Stabilization. 0 Alternative 7 [15A NCAC 02T.1 107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. 0 Alternative 9 [15A NCAC 02T.1 107(a)(9)] - Injection. 0 Alternative 10 [15A NCAC 02T.1 107(a)(10)] - Incorporation. [] Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.1 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 t A Wi WTP Process Flow Narrative: The Town of Denton's Water Treatment Plant receives its water from the Tuckertown Reservoir which is in the Yadkin River basin. We have a conventional drinking water treatment plant. Depending on the quality of the incoming raw water, treatment facilities use a variety of processes to make the water safe to drink. At our plant workers first add alum, caustic, potassium permanganate, and when conditions call for it, carbon, to the incoming water. These chemicals coagulate suspended particles, algae, protozoa, viruses, bacteria, iron and manganese into larger particles that settle to the bottom of the settling basins. This process also reduces the turbidity as the water flows through the basins. Water then comes to the entrance of the filters, (if plant operations are optimized, the turbidity entering the filters is at 10% of the original raw water turbidity entering the plant). Facility workers then add chlorine into the water, on top of the filters, to kill bacteria, viruses, and protozoa. This chlorine then goes through the filters, keeping the filters free from bacteria. Next, they use activated carbon filters to remove organic compounds and any suspended particles still in the water. After filtration, chlorine is added again to satisfy any demand on chlorine by the water, (to keep within the regulations set forth by the State and E.F.A.) and kills any remaining bacteria that may have entered the water during the filtration process. The next step is the addition of phosphates to help to control the corrosion that happens in every distribution system (Water + metals = corrosion). The final step involves adjusting the water's pH level to limit corrosion in the public water system and, in some communities, adding fluoride to help fight tooth decay in the population. We do add Fluoride at an average of 1.0 ppm. During the whole treatment process, the plant operators constantly monitor the water moving through the treatment plant, and its various different processes. After the water has gone through the treatment process, there is a solids waste (Alum Sludge) that is produced and has to be removed and disposed of in accordance with our discharge permit. Quantitative Justification of Residuals Production Rate The Town of Denton's Water Treatment Plant produces an estimated 150 Dry Tons per year of residuals through the treatment of Potable Water. The currently requested 300 Dry Tons should allow for any growth in the water system and for any unforeseen increases in the amount of residuals that the Water Treatment Plant produces. U.S. Biosolids, Inc. Town of Denton WTP Permit No. WQ0038071 SAMPLING PLAN Annually, if a land application event occurs, grab samples are collected from the holding pond. Samples from the pond will be combined to form individual grab samples to be sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (Le. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by Southern Soil Builders, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical. All samples taken will be taken in the same condition as the residuals are to be land applied. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, % total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the residuals holding pond C Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 03/14/2016 Reported: 03/30/2016 For: Denton WTP Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 160314-14-01 Fecal Coliforms 1 <2,667 MPNIg SM92210E-2006 03/14/2016 WL 160314-14-01 Percent Solids 1 0.75 % SM25408-1997 03/14/2016 WL 160314-14-02 Fecal Coliforms 2 <8,696 MPNIg SM92210E-2006 03/14/2016 WL 160314-14-02 Percent Solids 2 0.23 % SM2540B-1997 03/14/2016 WL 160314-14-03 Fecal Coliforms 3 <6,060 MPNIg SM92210E-2006 03/14/2016 WL 160314-14-03 Percent Solids 3 0,33 % SM25408-1997 03/14/2016 WL 160314-14-04 Fecal Coliforms 4 <3,125 MPN/g SM92210E-2006 03/14/2016 WL 160314-14-04 Percent Solids 4 0.64 % SM25408-1997 03/14/2016 WL 160314-14-05 Fecal Coliforms 5 <2,247 MPN/g SM92210E-2006 03/14/2016 WL 160314-14-05 Percent Solids 5 0.89 % SM254OB-1997 03114/2016 WL 160314-14-06 Fecal Coliforms 6 <3,846 MPNIg SM92210E-2006 03/14/2016 WL 160314-14-06 Percent Solids 6 0.52 % SM254OB-1997 03/14/2016 WL 160314-14-08 Corrosivity Denton WTP See SW-846 03/14/2016 PACE Attached 160314-14-08 Ignitability Denton WTP See 1010M 03/14/2016 PACE Attached 160314-14-08 Reactivity Denton WTP See SW-846 03/14/2016 PACE Attached 160314-14-08 TCLP Denton WTP See as Noted 03/14/2016 PACE Attached Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 a 704/872/4697 Page 1 of t Pace Analytical Servic9s, Inc. /�alcemalXical* 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: 160314-14-08 Pace Project No.: 92290083 Sample: 160314-14-08 LabID: 92290083001 Collected: 03/14/16 07A5 Received: 03/15/16 10:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate MethodlDate: EPA 1311; 03126tl6 14:00 Hexachloro-1,3-butadiene ND uglL 50.0 1 03128/1611:25 03/28/1617:40 87-68-3 Hexachlorobenzene ND ug& 50.0 1 0312811611:25 03/28/1617:40 118-74-1 Hexachloroethane ND uglL 50.0 1 03/2811611:25 03/28/1617;40 67-72-1 2-Methylphenol(o-Cresot) NO ug/L 50.0 1 03128/1611:25 0312811617:40 95-48-7 384-Methylphenol(m&p Cresol) NO ug/L 50.0 1 03/28/16 11:26 03/28116 17:40 Nitrobenzene NO ug/L 50.0 1 03/2811611:25 03/28/1617A0 98-95-3 Pentachlorophenol ND ug/L 100 1 03/28/1611:25 03/28/1617:40 87-86-5 Pyridine ND ug/L 50.0 1 0312811611:25 0312811617:40 110-86-1 2,4,5-Trichlorophenol NO ug/L 50.0 1 0312811611:25 03/2811617:40 95-96-4 2,4,6-Trichiorophenol NO ug/L 50.0 1 0312811611:25 03128/1617:40 88-06-2 Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphanyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenoi (S) Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1, 2-Dichloroethane 1,1-Dichlaroethene Tetrachloroethene Trichloroelhene Vinyl Chloride Surrogates 1,2-Dichloroethene-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 1010 Flashpoint,Clnsed Cup Flashpoint 9045 pH Soil pH at 25 Degrees C 9095 Paint Filter Liquid Test Free Liquids Date: 03129/2016 04:40 PM 72 % 12-102 1 03/28116 11725 03/28/16 17,40 4165-60-0 74 % 13-107 1 03/28/16 11:25 03/28116 17 40 321-60-8 99 % 21.132 1 03/2811611:25 0312811617:40 1718-51-0 26 % 10-110 1 0312&1611:25 0312811617:40 13127-88-3 40 % 10-110 1 03/28/1611:25 03/2911617:40 367.12.4 63 % 27-108 1 03128/1611:25 03/28/1617:40 118-79-6 Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 03/16/16 10:42 NO ug/1- 100 20 03/22/16 00:31 71-43-2 NO ug/L 20C 20 03/22/16 0031 78-93-3 NO ug/L 10C 20 03/22/16 00:31 56-23-5 NO ug/L 100 20 03/22/16 00:31 108-90-7 NO ug/L 100 20 03/22/16 00:31 67-66-3 ND ug/L 100 20 03/22/16 00:31 106-46-7 NO ug/L 100 20 03/22/16 00:31 107-06-2 NO ug/L 100 20 03/22/16 00:31 75-35-4 ND ug/L 100 20 03/22/16 00:31 127-18-4 ND ug/L 100 20 03/22/16 00:31 79-01-6 ND u91L 100 20 03/22/16 00:31 75-01-4 107 % 70-130 20 03/22/16 00:31 17060-07-0 98 % 67-135 20 03/22/16 00:31 2037-26-5 99 % 70-130 20 03/22116 00:31 460-00-4 Analytical Method: EPA 1010 >200 deg F 70.0 1 03/27/16 12:15 Analytical Method: EPA9045 6.8 Std. Units 0.10 1 03/18/16 14:35 H6 Analytical Method: EPA 9095 FAIL 1.0 1 03117/16 14:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of PaceAnalytical Services, Inc.. Page 5 of 26 ® Pace Analyticai Services, Inc. /�4ceAnal/Xical 9800 Kincey Ave. Suite 100 wwwDaoMabamm Huntersville, NC 28078 (704)875-9W2 ANALYTICAL RESULTS Project: 160314-14-08 Pace Project No.: 92290083 Sample 160314-14-08 Lab ID: 92290083001 Collected: 03114/1607:45 Received: 0311511610:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311: 0312FW16 14:00 gamma-BHC (Lindane) ND ug/L 0.50 1 03/28/16 12:50 03/28/16 18:37 58-89-9 Chlordane (Technical) ND ug1L 3.0 1 03/28/16 12:50 03/28/16 18:37 57-74-9 Endrin NO ug/L 0.50 1 03/28/16 12:50 03128/1618:37 72-20-8 Heptachlor epoxide NO ug/L 0.50 1 03/28/16 12:50 03/28/16 18:37 1024-57-3 Methoxychlor NO ug/L 1000 1 03/2811612:50 03/2&1618:37 72-43-5 Toxaphene NO ug/L 3.0 1 0312811612:50 =28/1618:37 8001-35-2 Surrogates Decachlorobiphenyl(S) 50 % 10-138 1 03/28/16 12:50 03/2811618:37 20,1-24-3 Tetrachloro-m-xylene (S) 75 % 10-110 1 03/28/16 12:50 03/28/16 18:37 877-D9-8 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3510 PCB-1016 (Aroclor 1016) ND uglL 0.50 1 03118/16 09:07 03/18/16 20:26 12674-11-2 PCB-1221 (Arodor 1221) NO ug/L 0.50 1 03/18116 09:07 03/18/16 20:26 11104-28-2 PCB-1232 (Arodor 1232) ND ug/L 0.50 1 03/18/16 09:07 03/18/16 20:26 11141-16-5 PCB-1242 (Arodor 1242) NO uglL 0.50 1 0311a/1609:07 03/18/16 20:26 53469-21.9 PCB-1248 (Arodor 1248) ND ug1L 0.50 1 03/18/16 09:07 03/18/16 20:26 12672.29-6 PC8-1254 (Arodor 1254) NO ug/L 0.50 1 03/18/16 09:07 03/18/16 20:26 11097.W-1 PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 03118/18 09:07 03/18/16 20:26 11 D96-82-5 Surrogates Decachlorobiphenyl (3) 45 % 10-132 1 03/18/16 09:07 03/18/16 20:26 2051-24-3 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-0 NO mg/L D.010 1 03/24/16 12:55 03/26/16 02:58 94-75.7 2,4,5-TP (Silvex) NO mg1L 0.010 1 03/24A6 12:55 03/26/16 02:58 93-72-1 Surrogates 2,4-DCAA (S) 99 % 42-142 1 03/24/16 12:55 03/26/16 02:58 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Leachate Method/Date- EPA 1311; 03/22/16 0&00 Initial pH: 5: Final pH: 5 Arsenic ND mg1L 0,050 1 03/23/16 03:00 03/23/16 13:57 7440-38.2 Barium NO mg/L 0,25 1 03/23/16 03:00 03/23/16 13:57 7440-39-3 Cadmium NO mg1L 0.0050 1 03/23/16 03:00 03/23/16 13:57 7440-43-9 Chromium ND mglL 0.025 1 03/23/16 03:00 03/23/16 13:57 7440-47-3 Lead NO mg/L 0.025 1 03/23M6 03:00 03/23116 13-57 7439-92-1 Selenium NO mg/L 0.10 1 03/23/16 03:00 03/23/16 13:57 778249-2 Silver NO mg/L 0.025 1 03/23/16 03:00 03/23/16 13:57 7440-224 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate MethodlDate: EPA 1311: 03/22/16 03:00 Initial pH- 5: Final pH: 5 Mercury NO mg1L 0.00020 1 03/23/16 11 *00 03/211614:15 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate MethodlDate: EPA 1311; 03/26/16 14:00 1,4-Dichlombenzene NO ug/L 50.0 1 03/2811611:25 03128/1617:40 106-46-7 2,4-Dinitrototuene NO uglL 50.0 1 03/28/1611:25 03/28/1617:40 121-14-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/29/2016 04:40 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 25 Pace Analytical Services, Inc. aceAnalytical • 9800 Kincey Ave. Suite 100 lwwwpwakk co Hunteraville, NC 28078 i7041875.9092 ANALYTICAL RESULTS Project: 160314-14-08 Pace Project No.: 92290083 Sample: 160314-14-08 Lab lD: 92290083001 Collected: 03/14116 07:45 Received: 03/15/16 %00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/L 0.010 1 03121/16 21:40 734S Reactive Sulfide Analytical Method: SW-848 7.3.4.2 Sulfide, Reactive ND mg/L 1.0 1 03/21/16 18:20 I! REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/29/2016 04:40 PM vrilhout the written consent of Pace Analytical Services, Inc.. Page 6 of 25 4.79 95.20 0.98 0.18 0.10 0.33 0.28 0.14 0.03 0.29 0.69 O Waypoient ANALYTICAL 9790 1840 982 3260 2810 1430 297 36500 152000 2700 48.5 77.5 2920 6870 <4.63 Report Number: 19-240-0010 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number: 67986 Sample Id : Denton WTP Total Solids " Moisture " Total Kjeldahl Nitrogen Phosphorus Potassium Sulfur Calcium Magnesium Sodium Iron Aluminum Manganese Copper Zinc Ammonia Nitrogen Organic N Nitrate+Nitrite-N Project: Denton WTP REPORT OFANALYSIS 7621 Whitepine Road, Richmand, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www-waypointanalytical.com Date Sampled: 8/25/2019 11.52:00 Date Received: 08/28/2019 00:00 Date Reported: 09/06/2019 08/30/20 i 9 15:57 08/30/2019-15:57 09/04/2019 13:00 09/03/2019 19:53 09/03/2019 19:53 09/03/2019 19:53 09/03/2019 19:53 09/03/2019 19:53 09/03/2019 19-53 09/03/2019 19:53 09/04/2019 17:46 09/03/2019 19:53 09/03/2019 19:53 09/03/2019 19:53 09/05/2019 13:00 09/04/2019 13:00 09/0412019 15:2 1 Ail values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time 250 Wo 50.0 50.0 250 50.0 250 50.0 500 5.00 2.50 12.5 100 250 4.63 ADM ADM JPJ JTR JTR JTR JTR JTR JTR JTR JTR JTR JTR JTR JPJ ZBD SM-2540G SM-254OG SM-4500-NH3C-TKN 6010D 6010D 601 OD 6010D 6010D 601 OD 6010D 601 OD 601 OD 6010D 6010D S M-4500-N H 3C CALCULATION 4500NO3r-2011 PcWtic/` 6aire Pauric McGroary Agronomist Page 3 of 6 Report Number: 19-240-0010 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 0 (2) Waypoint, ANALYTICAL Project : Denton WTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010Fax SO4-271-6446 www_waypoi ntanal ytical.com Lab Number. 67986 REPORT OFANALYSIS Date Sampled: 8/25/2019 11:52:00 Sample Id : Denton WTP Date Received: 08/28/2019 00:00 Date Reported: 09/06/2019 Cadmium Chromium <1.00 1.00 JTR 09103/201919:53 Nickel 43.3 2.50 JTR 09/03120i919:53 Lead 17.5 2.50 JTR 09103/201919:53 Arsenic 21.7 3.00 JTR 09/03/201919:53 Mercury 8.61 5.00 JTR 09/03/201919:53 Selenium 0.0585 0.0141 TJS 09/03/201914:49 pH. <5.00 5.00 JTR 09/03/201919:53 Molybdenum 6.5 JSL 09/03/2019 05:31 Comments: <2.50 2.50 JTR 09/03/201919:53 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis_ B-Analyte detected in blank H - Beyond holding time 601DD 601OD 601OD 601OD 6010D SW-7471 B 6010D 9045D 601 OD po' LG ("C V *Awr Pauric McGroary Agronomist Page 4 of 6 PAN Mineralization 1. Rate TKN NH3 NO3 0.4 9 990 2920 4.63 PAN Surface 4212.63 1 mg/kg 8.42526 lbs/dry ton 0 i bs total PAN #DIVIO! Ilbs PAN/acre PAN Injection 5672.63 mg/kg 11.34526 Ibs/dry ton 0 Ibs total PAN #DIVIO! IIbs PANlacre Dry Tons11000 gal. 0.199743 1st year PAN Surface Ibs. 0 1st year PAN Injected lbs. 0 Ibs./acre Surface #DIV/0! lbs_/acre Injected #DfV/0' as decimal _Total dry Acres NO2 % Solids tons/year Applied on 0 0.0479 MR(TKN-NH3)} + .5(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =Ibs/dry ton MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mg/kg mg/kg x .002 7-Ibs/dry ton 1000 X 8.34 X %solids X sp graviiv "=dry tons/1000gal," 2000 SAR Sodium Absorption Ratio Na M IL I- M u M M /L Na: Sodium (Mg/L) Equivalent weight: 23 14.22 134,E 68.49 Ca: Calcium (Mg/L) Equivalent weight. 20 Mg : Magnesium (MgIL) Equivalent weight 12 Na ME Ca ME Milli Equivalent = MgIL / Equivalent weight 0.618261 6.73 5.7075 The amour SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power amount of i SAR = 0.247925 (From MgIL entered above) Permitting t SAR= 0.248597 (From ME entered below) NaLE� Ca ME Mg- MQ 0.62 6.73 5.71 Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: Reported: For: Comments Analytical Results 09/10/2019 09/12/2019 Denton WTP <435 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 190910-37-01 Fecal Coliforms 1 <490 MPN/g SM92210E-2006 09/11/2019 WC 190910-37-01 Percent Solids 1 4.08 % SMr25408-2011 09/11/2019 WC 190910-37-02 Fecal Coliforms 2 <34$ MPNIg SM92210E-2006 09/11/2019 WC 190910-37-02 Percent Solids 2 5.74 % SM25409.2011 09/11/2019 WC 190910-37-03 Fecal Coliforms 3 <442 MPNIg SM92210E-2006 09/11/2019 WC 190910-37-03 Percent Solids 3 4.52 % SM25408-2011 09/11/2019 WC 190910-37-04 Feca! Coliforms 4 <424 MPN/g SM92210E-2005 09/11/2019 WC 190910-37-04 Percent Solids 4 4,72 % SM254OB-2011 09/11/2019 WC 190910-37-05 Fecal Coliforms 5 <476 MPNIg SM92210E-2006 09/11/2019 WC 190910-37-05 Percent Solids 5 4.20 % SM25408-2011 09/11/2019 WC 190910-37-06 Fecal Coliforms 6 <435 MPNIg SM92210E-2000 09/11/2019 WC 190910-37-06 Percent Solids 6 4.60 % SM2540B-2011 09/11/2019 WC 190910-37-07 Fecal Coliforms 7 <443 MPNIg SM9221Ge-2006 09/11/2019 WC 190910-37-07 Percent Solids 7 4.51 % SM25406-2011 09/11/2019 WC Respectfully submitted, n�,l ' "i /'q, " ,'17 � , Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 City of Mount Holly Water Treatment Plant Residuals Source Certification (RSC) Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: City of Mount Holy WTP 2. Facility permit holder is: El Federal, 0 State, 0 Local Government, or 0 Private. Facility permit issued by: Div. of Water Resources, Div. of Environmental Health, or E] Other (explain: ). 3. Facility contact person and title: Gina Miller Complete mailing address: PO Box 406 City: Mount Holly State: NC Zip: 28120 Telephone number: (704) 822-2928 E-mail address: gina.miller rr mtholly.us 4. Facility physical address: I I I Mountain Island Road City: Mount Holly State: NC Zip: 28120 Coordinates: Latitude: 35' 20' 06" Longitude: 80' 59' 51" Datum: NAD83 Level of accuracy: 01" Method of measurement: MAP 5. Purpose of the facility: 0 treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, Q treatment of 100% industrial wastewater, [] treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: 0 Yes No 7. Facility permitted/design flow: 6_0 MGD and facility average daily flow: 3.001 MGD 8. Average amount of residuals being generated at this facility 200 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Two (2) 170' X 100' holding ponds Type and volume of residuals storage (i.e., outside of residuals treatment units): None II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: El 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(61 as: Biological S Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06- l6 Pagel of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ] yes no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes M. no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitabiiity, and reactivity: Laboratory: Pace Analytical and Date of analysis: 10-24-2016 Passed corrosivity test: 0 yes El no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: E yes 0 no. Flashpoint: 200 IF (> 140°F) Passed reactivity test: S yes Qno. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (m9/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.o ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachioroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND l,l-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 10-24-2016 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration limits (Class A Only) (mg/kg) Result (m9/k9) Arsenic 75 41 32.3 Cadmium 85 39 2 Copper 4,300 1,500 88.7 Lead 840 300 21.6 Mercury 57 17 0.4 Molybdenum 75 n/a 5 Nickel 420 420 10.8 Selenium 100 100 5 Zinc 7,500 2,800 57.1 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory:. and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) [] > 0 but < 25 30 200 210 Cj > 25 but < 50 34 220 240 Q > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 E] > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 0.38 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 10-24-2016 Parameter Result (mg/kg) Aluminum 170000 Ammonia -Nitrogen 5130 Calcium 6100 Magnesium 940 Nitrate -Nitrite Nitrogen 1.01 pH (Standard Unit) 8 Phosphorus 1270 Potassium 842 Sodium 449 Total Kjeldahl Nitrogen 43600 c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0.08 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g„ gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): 0 default value, or El actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Non processed residuals e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mg�kg� (mg/kg) Surface 17954.01 19210.78 Injection/Incorporation 20519.01 21955.34 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Patho en Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For DistrihutionlLand Application of Class A_ or Equivalent: El A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or El A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Q Alternative 1 [15A NCAC 02T.1 106(b)(3)(A)] - TimelTemperature Compliance. Q Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)] - Alkaline Treatment. 0 Alternative 3 [15A NCAC 02T.1 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. 0 Alternative 4 [15A NCAC 02T.1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: 0 composting, 0 heat drying, 0 heat treatment, 0 thermophilic aerobic digestion, EJ beta ray irradiation, 0 gamma ray irradiation, or 0 pasteurization. b. For Land ApBlicaflon of Class B: [] Alternative 1 [15A NCAC 02T.1 106(c)(1)] - Fecal Coliform Density Demonstration. [] Alternative 2 [15A NCAC 02T.] 106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: ] aerobic digestion, Q air drying, :Q anaerobic digestion, El composting, or 0 lime stabilization. c. For Surface Disposal: 0 Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. 0 Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above. 0 Exempt - If Daily Cover Alternative is chosen in Item 1I.8. below [ 15A NCAC 02T.1 106(a)(2)]. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution, 8. Vector Attraction Reduction (VAR}: Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: Q Alternative 1 [I5A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 (15A NCAC 02T.1 107(a)(2)1- 40-Day Bench Scale Test (Anaerobic Digestion). 0 Alternative 3 [15A NCAC 02T. 1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). E] Alternative 4 [15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). E] Alternative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. [] Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. Q Alternative 9 [15A NCAC 02T. i 107(a)(9)] - Injection. 0 Alternative 10 [15A NCAC 02T.1 107(a)(10)] - Incorporation. [] Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1 ]07(b)(2)1. 0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Vicinity Map City of Mount Holly Water Treatment Plant Process Flow Diagram A is ,a .�M C TO F INi5nEa ........... ........_. ... - ... .. ... ... .. -RUNFiNt15lAi.-DN $CUTM CORNER ... )+610 i �'/T.d ... riESTCORMEN 1a A80 1-11 0 RtlMFN 8111LOING _ - ENTRANCE DRWE iL .. 4•2i5.i CHEMd CAL FFE6 - i ENTRANc[ rt I' 7-25.Vl�. T - y EIIIURI VAOL.3- CENTiF .. 8.19.0 S { E . CLGARMPEIL CFNT�R .. ■+,500-._ LAGTR i©LI3 OOOXECNOSMrER IUN 10•Al.tl - ^_ 4r55.e - ..^ Y - - . - LAGOON NO, 3 CENTER3-ii ..• �Syy 1 �1 t L 1ICAON J<p 2CEN7ER 10+79.0 5.6A J r l 0 0. I y LAgl(ON ENTRANCE S „'[Att. ^ •. '^ { /''� (•� OR -YE IoyS % ! L105..1 IM0.TCNLIN, WITH RAW WATER €- ., ..... C[ r -»� -. -. ... 7RANSM155JtlN41NF ............. .......e.,.an •- � f =e r *' 1 :.a +d .4 L Quantitative Justification of Residuals Production Rate The City of Mount Holly's Water Treatment Plant produces an estimated 200 Dry Tons per year of residuals through the treatment of Potable Water. The currently requested 300 Dry Tons should allow for any growth in the water system and for any unforeseen increases in the amount of residuals that the Water Treatment Plant produces. U.S. Biosolids, Inc. Mount Holly, WTP Permit No. WQ0038071 SAMPLING PLAN Annually, if a land application event occurs, multiple individual grab samples are collected from the holding pond and sent to a laboratory for analysis. If a land application event is to occur in the early part of a calendar year (i.e. January or early February) these samples may have to be taken in December so results can be obtained before the land application event, as some results take 30+ days to receive. These individual grab samples are collected and tested for nutrient analysis, and a TCLP test. These tests will be taken by Southern Soil Builders, Inc. All samples with the exception of the composite residual sample will be taken to Statesville Analytical, All samples taken will be taken in the same condition as the residuals are to be land applied. Annually, if land application occurs, a composite residual sample will be analyzed, prior to a land application event for: Cadmium, Copper, Lead, Mercury, Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia Nitrogen, Calcium, Nitrate Nitrogen, Magnesium, % total Solids, pH, Phosphorus, Potassium, TKN, Sodium From this information, the Plant Available Nitrogen (PAN) and a Sodium Absorption Ratio (SAR) will be calculated. This sample will collected in a non -breakable container, at least one quart in size. This sample will be taken from the holding ponds. This test will be done by A&L Labs. Page: 1 of 2 Report Number: 16-301-0206 ' Account Number: 46381 Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: Southern Soil Builders Project: MT Holly WTP Dennis Key INC Cert #257 958 Hoots Road Roaring River, NC 28669 REPORT OF ANALYSIS Date Sampled: 10/24/2016 12:55:00 Lab Number: 60432 Date Received: 10/27/2016 00:00 Sample Ild : MT Holly WTP Date Reported: 11/02/2016 METHODPARAMETER RESULT RESULT QUANTITATION LIMIT ANALYSIS Total Solids " 0.38 3800 100.0 JM 10/27/2016 15:05 SM-2540G Moisture' 99.61 100.0 JM 10/27/201615:05 SM-254OG Total Kjeldahl Nitrogen 4.36 43600 10.0 JM 10/31/2016 09:35 SM-4500-NH3C-TKN Total Phosphorus 0.13 1270 100 JTR I IIM2016 07:49 6010C Total Potassium 0.08 842 100 JTR 11/02/2016 07:49 6010C Total Sulfur 0.53 5280 100 JTR 11/02/2016 07:49 6010C Total Calcium 0.61 6100 100 JTR 11/02/2016 07:49 6010C Total Magnesium 0.09 940 100 JTR 11/02/2016 OT49 6010C Total Sodium 0,04 449 100 JTR 11102/2016 OT49 6010C Total Iron 17300 100 JTR 11/02/2016 07:49 6010C Total Aluminum 170000 1000 JTR 11/02/2016 07:53 6010C Total Manganese 329 5.00 JTR 11/02/2016 07:49 6010C Total Copper 88.7 5.00 JTR 11/02/2016 07:49 6010C Total Zinc 57.1 5,00 JTR 11/02/2016 07:49 6010C Ammonia Nitrogen 0.51 5130 10.0 SJB 10/28/2016 09:00 SM-4500-NH3C Organic N 3.85 38470 10.0 10/28/2016 09:00 CALCULATION Nitrate+Nitrite-N <1.01 1.01 SJB 10/31/201613:50 450ONO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. A41W Our reports a00 gerltlr5 are for ;r;e eoa,�s,ve aou c,)ntdlIrIfai o5e of our cf;enis. and niay norLe reproduced rn whole or pan, -ormay any reference be made M�l to the work rho resuirs, or the company in any advenisrng, ne�ii release or olher public announcements withoul obta+n+ng our prior wntrere aufhonzafion Debbie Halt Laboratory Supervisor Page: 2 of 2 Report Number: 16-301-0206 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number: 60432 Sample Id : MT Holly WTP Waypoint(D ANALYTICAL Project: MT Holly WTP NC Cert #257 REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/24/2016 12:55:00 Date Received: 10/27/2016 00:00 Date Reported: 11/02/2016 Total Cadmium <2.00 2.00 JTR 11/02/2016 07:49 6010C Total Chromium 123 5.00 JTR 11/02/2016 07:49 6010C Total Nickel 10.8 5.00 JTR 11/02/2016 07:49 6010C Total Lead 21.6 5.00 JTR 11/02/2016 07:49 6010C Total Arsenic 32.3 3.00 JTR 11/02/2016 07:49 6010C Total Mercury <0.400 0.400 JM 11/01/2016 10.30 SW-7471B Total Selenium <5.00 5.00 JTR 11/02/2016 07 49 6010C pH (Standard Units) * 800 SJB 10/28/2016 09:00 SW-9045D Total Molybdenum <5.00 5A0 JTR 11/02/2016 07:49 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. / Debbie Holt Laboratory Supervisor Z Mineralization as decimal ITotal dry tonslyear Acres Apo[ied on Rate 0.4 TKN 43600 NH3 1 5130 NO3 1.01 NO2 0 % Solids 0.0038 1 300 PAN Surface 17964.01 1mg/ky 35.90802 Ibsld ton 10772.41 Ilbs total PAN #DIVIO! jibs PANlacre PAN Injection 20519.01 lmgfkg 41.03802 lbs/dry ton 12311.4f Ibs total PAN #DIVI01 jibs PAN/acre Dry Tons11000 gal. 0.015846 1st year PAN Surface lbs. f st year PAN Injected Ibs. 1231 1.406 Ibs.lacre Surface #DIV10� Ibs.lacre Injected #DIV/ MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mglkg mg/kg x .002 =lbsldry ton MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =lbsldry ton 1000 X 8.34 X %solids X sp. gravity " dry tons11000gal." 2000 SAR Sodium Absorption Ratio Na M IL Ca(Mq/L) M M /L Na: Sodium (Mg/L) Equivalent weight: 23 1.7 23.18 3.57 Ca: Calcium (MgIL) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Na (ME) Ca (ME) Mq (ME) 0.073913 1.159 0.2975 Milli Equivalent = MgIL I Equivalent weight The amour amount of SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power Permitting { SAR = 0.086613 (From Mg/L entered above) SAR= 0.083966 (From ME entered below) Na (ME) Ca (ME) Mg (ME) 0.07 1.16 0.23 Analytical Results Southern Soil Builders 958 Moots Road Roaring River, NC 28669 Receive Date: 10/24/2016 Reported: 11/14/2016 For: Mt Holly WTP Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 161024-13-01 Corrosivity Mt. Holly WTP See Attached sw-846 10/26/2016 Pace 161024-13-01 Ignitability Mt. Holly WTP See Attached 1010M 1012612016 Pace 161024-13-01 Reactivity Mt. Holly WTP See Attached Sw'646 10/26/2016 Pace 161024-13-01 TCLP Mt. Holly WTP See Attached as Noted 10/26/2016 Pace Respectfully submitted, �11� �vOGJ`Y- Dena Myers NC Cert #440, NCDW Cert #37755. EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 aceAnalytica! —pacelabs.com ANALYTICAL RESULTS Project: 161024-13 Pace Project No.: 92317194 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 161024-13 Lab Id: 92317194001 Collected: 10124/16 12:55 Received: 10/25/16 08:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311: 11/02/16 14:00 gamma-SHC (Lindane) ND ug1L 0.50 1 11/07/16 15:44 11/08/16 13:26 58-89-9 Chlordane (Technical) ND ug1L 3.0 1 11/07/16 15:44 11/08/16 13:26 57-74-9 Endrin ND uglL 0.50 1 11/07/16 15:44 11/0811613:26 72-20-8 Heptachlor ND uglL 0.50 1 11/07/16 15:44 11/08/1613:26 76-44-8 Heptachlor epoxide ND uglL 0.50 1 11/0711615:44 11/0811613:26 1024-57-3 Methoxychlor ND uglL 1000 1 11/0711615:44 11/0811613:26 72-43-5 Toxaphene ND uglL 3.0 1 11/07/16 15:44 11/0811613:26 8001-36-2 Surrogates Decachlorobiphenyl (S) 60 % 10-138 1 11/07/16 15:44 11/08/16 13:26 2051-24-3 Tetrachloro-m-xylene (S) 68 % 10-110 1 11/07/16 15:44 11/08/16 13:26 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-D ND mglL 0.010 1 11/08/1610:00 11/10/1603:39 94-75-7 2,4,5-TP(Silvex) ND mg/L 0,010 1 11/08/1610:00 11/10/1603:39 93-72-1 Surrogates 2,4-DCAA (8) 96 % 39-139 1 11/08/16 10:00 11/10/16 03:39 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA6010 Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311: 11/01/16 18:40 Initial pH: 5.6; Final pH: 5.6 Arsenic ND mglL 0.050 1 11/0211616:30 11/0411601:20 7440-38-2 Barium ND mglL 0.25 1 11/02/16 16:30 11/04/16 01:20 7440-39-3 Cadmium ND mglL 0.0050 1 11/02/16 16:30 11/04/16 01:20 7440-43-9 Chromium ND mglL 0.050 1 11/02/16 16:30 11/04/16 01:20 7440-47-3 Lead ND mglL 0,025 1 11/02/16 16:30 11/04/16 01:20 7439-92-1 Selenium ND mg1L 0A0 1 1110211616:30 11/041160120 7782-49-2 Silver ND mg1L 0.025 1 11/02/16 16:30 11/04/16 0110 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 11/01/16 18:40 Initial pH: 5.6; Final pH: 5.6 Mercury ND mg1L 0.00020 1 11/02/16 20:35 11/03/16 10:29 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 11/02/16 14:00 1,4-Dichlorobenzene ND uglL 50.0 1 11/0711614:30 1110811610:36 106-46-7 2,4-Dinitrotoluene ND uglL 50.0 1 11/0711614:30 1110811610:36 121-14-2 Hexachloro-1,3-butadiene ND uglL 50.0 1 1110711614:30 1110811610:36 87-68-3 Hexachiorobenzene ND uglL 50.0 1 11/0711614:30 1110811610:36 118-74-1 Hexachloroethane ND ug/L 50.0 1 11/0711614:30 1110811610:36 67-72-1 2-Methylphenol(o-Cresol) ND uglL 50.0 1 11/07/1614:30 1110811610:36 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/l_ 50.0 1 11/07/16 14:30 11/08/16 10:36 Nitrobenzene ND ug1L 50.0 1 11107/1614:30 11/0811610:36 98-95-3 Pentachlorophenol ND ug1L 100 1 11/0711614:30 11/0811610:36 87-86-5 Pyridine ND ug1L 50.0 1 11/0711614:30 11/0811610:36 110-86-1 2,4,5-Trichlorophenol ND uglL 50.0 1 11107/1614:30 1110811610:36 95-95-4 2,4,6-Trichlorophenol ND uglL 50.0 1 1110711614:30 11/0811610:36 88-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/10/2016 06:22 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 27 aceAnalytrcal e ..pacalab&com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Project: 161024-13 Pace Project No.: 92317194 Sample: 161024.13 Lab ID: 92317194001 Collected: 10/24/16 12:55 Received: 10/25/16 08:25 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-D ihlorobenzene 1,2-D ichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-6romotiuorobenzene (S) Percent Moisture Percent Moisture 1010 Flash point,Closed Cup Flashpoint 9045 pH Soil pH at 25 Degrees C 9095 Paint Filter Liquid Test Free Liquids 733C S Reactive Cyanide Cyanide, Reactive 736S Reactive Sulfide Sulfide, Reactive Date: 11/10/2016 05:22 PM Analytical Method: EPA8270 Preparation Method: EPA3510 Leachate MethodlDate: EPA 1311; 11/02/16 14:00 67 % 12-102 1 11107/1614:30 11/0811610:36 4165-60-0 60 % 13-107 1 11/0711614:30 11/0811610:36 321-60-8 94 % 21-132 1 11/0711614:30 111081161036 1718-51-0 32 % 10-110 1 11/07/1614:30 1110811610:36 13127-88-3 44 % 10-110 1 11/07/1614:30 11/0811610:36 367-12-4 71 % 27-108 1 11107/161430 11/08/1610:36 118-79-6 Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311: 11/01/16 15:18 NO ug/L 5.0 1 11/0411617:12 71-43-2 NO ug/L 10.0 1 11/0411617:12 78-93-3 NO ug1L 5.0 1 11/04/1617:12 56-23-5 NO ug1L 5.0 1 1110411617:12 108-90-7 NO uglL 5.0 1 1110411617:12 67-66-3 NO ug/L 5.0 1 1110411617:12 106-46-7 ND ug/L 5.0 1 111041161712 107-066-2 NO ug1L 5.0 1 11/0411617:12 75-35-4 ND ug1L 5.0 1 11/0411617:12 127-18-4 NO ug/L 5.0 1 11/04/1617:12 79-01-6 ND ug/L 5.0 1 11104/1617:12 75-01-4 96 % 70-130 1 11104/1617:12 17060-07-0 106 % 67-135 1 11/04/1617:12 2037-26-5 95 % 70-130 1 11104/1617:12 460-00-4 Analytical Method: ASTM D2974-87 99.7 % 0.10 1 10/26/16 07:44 Analytical Method: EPA 1010 >200 deg F 70.0 1 10/31/16 10:19 Analytical Method: EPA 9045 6.6 Std. Units 0A0 1 10/31/16 14:23 H1 Analytical Method: EPA 9095 FAIL 1.0 1 11/07/16 16:35 Analytical Method: SW-846 7.3.3.2 NO mg/kg 385 1 11/02/16 20:49 Analytical Method: SW 846 7.3.4.2 ND mg/kg 3850 1 11/0211616:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuh, without the written consent of Pace Analytical Services, LLC. Page 6 of 27