NC0021954_Method 625 Scan_20200219

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Subrrit by Anonymous User 2/19/2020 10:42:14 AM (Supplemental Submittal)
Submit by Thedford, Wren 5/12/2020 9:22:15 AM (Supplemental Info Submittal)
• Thedford, Wren assigned the task to Thedford, Wren 5/12/2020 9:21 AM
• The task was assigned to Thedford, Wren, Bennett, Bradley 2/19/2020 10:42 AM

Initial Review Information
Updated ID#:* IWORTANf:FEVIBAERSHOLLDVERFYand revise here ifnecessary.
NC0021954
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Information Submitted on 2/19/2020
Submitter Information
Name: Willard Hardison
Vft is subrritting the information?
Email Address:* [e-mail]
Submittal Information
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Project Information:
Rease SUDDly the Dernit nun ber for this
Existing ID#* PerrritNurrber
NC0021954
Exarrples: NOKxxxxxx or NO&xxxxx
Facility Name:* CITGO Petroleum Corp.
County: Wayne
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625.pdf 1.07MB
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625 scan compound the scanned submittal.
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• I agree to conduct this transaction by electronic means pursuant to Chapter 66, Article 40 of the NC General Statutes
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Full Name: Willard Hardison
Signature:
Date Submitted: 02/19/2020

ANALYTICAL REPORT
January 30, 2020
CITGO-Selma, NC
Sample Delivery Group:
Samples Received:
Project Number:
Description:
Site:
Report To:
L1181559
01/22/2020
Semiann Outfalls
Outfalls-Semiann Monitoring
SELMA (3442)
H. Wayne Whiting
4095 Buffalo Road
Selma, NC 27576
Entire Report Reviewed By
��MJarda ,' P�ti
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
aceAnalytical
National Center for Testing & Innovation
AW
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:03 1 of 19

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
OUTFALL 001 L1181559-01
5
Fn
Qc: Quality Control Summary
Gravimetric Analysis by Method 2540 D-2011
7
Fr
Wet Chemistry by Method 1664B
8
Wet Chemistry by Method 2130 B-2011
9
FC
Wet Chemistry by Method 420.4
10
F
Volatile Organic Compounds (GC/MS) by Method 624.1
11
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
12
[Al
GI: Glossary of Terms
17
Al: Accreditations & Locations
18
RC
Sc: Sample Chain of Custody
19
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559
01/30/20 12:03
2 of 19

OUTFALL 001 L1181559-01 WW
SAMPLE
SUMMARY
Collected by
Brentrhornton
Collected date/time
01/21/20 08:00
ONE LAB. NATIONWIDE.
Received date/time
01/22/20 08:45
FP
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
F
Gravimetric Analysis by Method 2540 D-2011
WG1415710
1 01/23/20 06:43
01/23/20 08:00
TH
Mt. Juliet, TN
Wet Chemistry by Method 1664B
WG1415700
1 01/23/20 07:07
01/23/2013:36
AMG
Mt. Juliet, TN
Wet Chemistry by Method 2130 B-2011
WG1415601
1 01/22/20 2120
01/22/20 2120
MSP
Mt. Juliet, TN
Wet Chemistry by Method 420.4
WG1415420
1 01/22/2015:16
01/23/2014:07
JER
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 624.1
WG1415157
1 01/22/2016:29
01/22/2016:29
ACG
Mt. Juliet, TN
Fn
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG1415666
1 01/23/2010:31
01/24/20 05:14
JNJ
Mt. Juliet, TN
Fr
FC
�GI
SAI
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
CITGO-Selma, NC
Semiann Outfalls
L1131559
01/30/20 12:08
3 of 19

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Cassandra Foster
Project Manager
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:03 4 of 19

OUTFALL 001 SAMPLE RESULTS - 01
Collected date/time: 01/21/20 08:00 L1181559
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier
MDL
Analyte mg/I
mg/I
Suspended Solids 1.30 J
0.350
Wet Chemistry by Method 1664B
Result Qualifier
MDL
Analyte mg/I
mg/I
Oil & Grease (Hexane Extr) U
1.29
Wet Chemistry by Method 2130 B-2011
RDL Dilution Analysis Batch
mg/I date / time
2.50 1 01/23/2020 08:00 WG1415710
RDL Dilution Analysis Batch
mg/I date / time
5.56 1 01/23/202013:36 WG1415700
Result Qualifier MDL RDL
Analyte NTU NTU NTU
Turbidity 1.24 0.0310 0.300
Wet Chemistry by Method 420.4
Result Qualifier MDL RDL
Analyte mg/I mg/I mg/I
Total Phenol by4AAP U J6 0.00830 0.0400
Volatile Organic Compounds (GC/MS) by Method 624.1
Dilution Analysis
date / time
1 01/22/2020 21:20
Batch
WG1415601
Dilution Analysis Batch
date / time
1 01/23/202014:07 WG1415420
Result Qualifier MDL
RDL Dilution
Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
U
0.000331
0.00100 1
01/22/202016:29
WG1415157
Ethylbenzene
U
0.000384
0.00100 1
01/22/202016:29
WG1415157
Toluene
U
0.000412
0.00100 1
01/22/202016:29
WG1415157
Xylenes, Total
U
0.00106
0.00300 1
01/22/202016:29
WG1415157
Methyl tert-butyl ether
U
0.000367
0.00500 1
01/22/202016:29
WG1415157
(S) Toluene-dH
105
80.0-120
0112212020 16.29
WG1415157
(S) 4-Bromofluorobenzene
96.9
80.0-120
0112212020 16.29
WG1415157
(S) 1,2-Dichloroethone-d4
99.2
70.0-130
011221202016.29
WG1415157
Semi Volatile Organic
Compounds
(GC/MS) by Method 625.1
Result
Analyte
mg/I
Acenaphthene
U
Acenaphthylene
U
Anthracene
U
Benzidine
U
Benzo(a)anthracene
U
Benzo(b)fluoranthene
U
Benzo(k)fluoranthene
U
Benzo(g,h,i)perylene
U
Benzo(a)pyrene
U
Bis(2-chlorethoxy)methane
U
Bis(2-chloroethyl)ether
U
2,2-Oxybis(1-Chloropropane)
U
4-Bromophenyl-phenylether
U
2-Chloronaphthalene
U
4-Chlorophenyl-phenylether
U
Chrysene
U
Dibenz(a,h)anthracene
U
3,3-Dichlorobenzidine
U
2,4-Dinitrotoluene
U
2,6-Dinitrotoluene
U
1,2-Diphenylhydrazine
U
ACCOUNT:
CITGO-Selma, NC
Qualifier MDL
m g/I
RDL
mg/I
0.000316
0.00100
0.000309
0.00100
0.000291
0.00100
0.00432
0.0100
0.0000975
0.00100
0.0000896
0.00100
0.000355
0.00100
0.000161
0.00100
0.000340
0.00100
0.000329
0.0100
0.00162
0.0100
0.000445
0.0100
0.000335
0.0100
0.000330
0.00100
0.000303
0.0100
0.000332
0.00100
0.000279
0.00100
0.00202
0.0100
0.00165
0.0100
0.000279
0.0100
0.000318
0.0100
Dilution Analysis
date / time
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
1 01/24/2020 05:14
PROJECT: SDG:
Semiann Outfalls L1131559
ONE LAB. NATIONWIDE. *
Fp
_ Fc
FS
Fn
Fc
F,
SAI
Rc
Batch
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
WG1415666
DATE/TIME:
01/30/20 12:08
PAGE:
5of19

ONE LAB. NATIONWIDE. *
OUTFALL 001 SAMPLE RESULTS - 01
Collected date/time: 01/21/20 08:00 L1181559
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Analyte
mg/I
Fluoranthene
U
Fluorene
U
Hexachlorobenzene
U
HexachIoro-1,3-butadiene
U
HexachIorocyclopentadiene
U
Hexachloroethane
U
Ind eno(1,2,3-cd)pyrene
U
Isophorone
U
Naphthalene
U
Nitrobenzene
U
n-Nitrosodimethyl amine
U
n-Nitrosodiphenylamine
U
n-Nitrosodi-n-propylamine
U
Phenanthrene
U
Benzylbutyl phthalate
U
B is(2-ethyl hexyl)phthal ate
U
Di-n-butyl phthalate
U
Diethyl phthalate
U
Dimethyl phthalate
U
Di-n-octyl phthalate
U
Pyrene
U
1,2,4-Trichlorobenzene
U
4-Chloro-3-methyl phenol
U
2-Chorophenol
U
2,4-Dichlorophenol
U
2,4-Dimethylphenol
U
4,6-Dinitro-2-methylphenol
U
2,4-Dinitrophenol
U
2-Nitrophenol
U
4-Nitrophenol
U
Pentachlorophenol
U
Phenol
0.000488
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
59.4
(S) 2-Fluorobiphenyl
75.8
(S) p-Terphenyl-d14
83.1
(S) Phenol-d5
23.4
(S) 2-Fluorophenol
37.E
(S)Z4,6-Tribromophenol
89.4
Qualifier MDL RDL Dilution Analysis Batch
mg/I mg/I date/time
J
0.000310
0.00100 1
01/24/2020 05:14
WG1415666
0.000323
0.00100 1
01/24/2020 05:14
WG1415666
0.000341
0.00100 1
01/24/2020 05:14
WG1415666
0.000329
0.0100 1
01/24/2020 05:14
WG1415666
0.00233
0.0100 1
01/24/2020 05:14
WG1415666
0.000365
0.0100 1
01/24/2020 05:14
WG1415666
0.000279
0.00100 1
01/24/2020 05:14
WG1415666
0.000272
0.0100 1
01/24/2020 05:14
WG1415666
0.000372
0.00100 1
01/24/2020 05:14
WG1415666
0.000367
0.0100 1
01/24/2020 05:14
WG1415666
0.00126
0.0100 1
01/24/2020 05:14
WG1415666
0.00119
0.0100 1
01/24/2020 05:14
WG1415666
0.000403
0.0100 1
01/24/2020 05:14
WG1415666
0.000366
0.00100 1
01/24/2020 05:14
WG1415666
0.000275
0.00300 1
01/24/2020 05:14
WG1415666
0.000709
0.00300 1
01/24/2020 05:14
WG1415666
0.000266
0.00300 1
01/24/2020 05:14
WG1415666
0.000282
0.00300 1
01/24/2020 05:14
WG1415666
0.000283
0.00300 1
01/24/2020 05:14
WG1415666
0.000278
0.00300 1
01/24/2020 05:14
WG1415666
0.000330
0.00100 1
01/24/2020 05:14
WG1415666
0.000355
0.0100 1
01/24/2020 05:14
WG1415666
0.000263
0.0100 1
01/24/2020 05:14
WG1415666
0.000283
0.0100 1
01/24/2020 05:14
WG1415666
0.000284
0.0100 1
01/24/2020 05:14
WG1415666
0.000624
0.0100 1
01/24/2020 05:14
WG1415666
0.00262
0.0100 1
01/24/2020 05:14
WG1415666
0.00325
0.0100 1
01/24/2020 05:14
WG1415666
0.000320
0.0100 1
01/24/2020 05:14
WG1415666
0.00201
0.0100 1
01/24/2020 05:14
WG1415666
0.000313
0.0100 1
01/24/2020 05:14
WG1415666
0.000334
0.0100 1
01/24/2020 05:14
WG1415666
0.000297
0.0100 1
01/24/2020 05:14
WG1415666
15.0-314
0112412020 05.14
WG1415666
22.0-127
0112412020 05.14
WG1415666
29.0-141
0112412020 05.14
WG1415666
8.00-424
0112412020 05.14
WG1415666
10.0-120
0112412020 05.14
WG1415666
10.0-153
0112412020 05.14
WG1415666
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 6 of 19

WG1415710
Gravimetric Analysis by Method 2540 D-2011
Method Blank (MB)
(MB) R3494666-1 01/23/20 03 00
MB Result
Analyte mg/I
Suspended Solids U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.350 2.50
L1181597-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1181559-01
(OS) L1131597-01 01/23/20 03:00 • (DUP) R3494666-3 01/23/20 03 00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Suspended Solids 84.0 80.0 1 4.88 5
L1181659-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1131659-01 01/23/20 03:00 • (DUP) R3494666-4 01/23/20 03 00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Suspended Solids 134 122 1 9.38 P1 5
Laboratory Control Sample (LCS)
(LCS) R3494666-2 01/23/20 03 00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Suspended Solids 773 828 107 85.0-115
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 7 of 19

WG1415700
Wet Chemistry by Method 1664B
Method Blank (MB)
(MB) R3493456-1 01/23/201150
MB Result
Analyte mg/I
Oil & Grease (Hexane Extr) U
MB Qualifier MB MDL MB RDL
mg/I mg/I
1.16 5.00
QUALITY CONTROL SUMMARY
L1181559-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493456-2 01/23/2011:50 • (LCSD) R3493456-3 01/23/201150
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD
Analyte mg/I mg/I mg/I
Oil & Grease (Hexane Extr) 40.0 38.0 32.5 95.0 81.3 78.0-114 15.6
RPD Limits
20
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 3 of 19

WG1415601
Wet Chemistry by Method 2130 B-2011
Method Blank (MB)
(MB) R3493193-1 01/22/20 2120
MB Result
Analyte NTU
Turbidity 0.0680
MB Qualifier MB MDL MB RDL
NTU NTU
J 0.0310 0.300
L1181559-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1181559-01
(OS) L1131559-01 01/22/20 2120 • (DUP) R3493193-3 01/22/20 2120
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte NTU NTU
Turbidity 1.24 1.20 1 3.28 20
Laboratory Control Sample (LCS)
(LCS) R3493193-2 01/22/20 2120
Spike Amount LCS Result
Analyte NTU NTU
Turbidity 40.0 36.6
LCS Rec. Rec. Limits LCS Qualifier
91.5 90.0-110
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 9 of 19

WG1415420 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 420.4 L1181559-01
Method Blank (MB)
(MB) R3493610-1 01/23/2013:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Total Phenol by4AAP 0.0117 J 0.00830 0.0400
L1177617-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1177617-02 01/23/20 13:54 • (DUP) R3493610-3 01/23/20 13:55
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I %_
Total Phenol by4AAP ND 0.000 1 0.000 20
L1181164-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1131164-02 01/23/2014:25 • (DUP) R3493610-5 01/23/2014:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I
Total Phenol by4AAP 0.0497 0.0337 1 38.4 P1 20
Laboratory Control Sample (LCS)
(LCS) R3493610-2 01/23/20 13:54
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
Total Phenol by4AAP 0.500 0.550 110 90.0-110
L1181559-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1131559-01 01/23/20 14:07 • (MS) R3493610-4 01/23/20 14:03
Spike Amount Original Result MS Result MS Rec.
Analyte mg/I mg/I mg/I
Total Phenol by4AAP 1.00 U 0.0318 3.18
Dilution Rec. Limits MS Qualifier
1 90.0-110 J6
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 10 of 19

WG1415157
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS)
by Method
624.1
L1181559-01
Method Blank (MB)
C p
(MB) R3493274-2 01/22/201013
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
TC
I
Benzene U
0.000331
0.00100
Ethylbenzene U
0.000384
0.00100
FS
Methyl tert-butyl ether U
0.000367
0.00500
Toluene U
0.000412
0.00100
Xylenes, Total U
0.00106
0.00300
[Cn]
(S) Toluene-dH 102
80.0-120
(S) 4-Bromofluorobenzene 84.2
80.0-120
5
Sr
(S) 1,2-Dichloroethane-d4 98.3
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3493274-1 01/22/20 09:33
G1
I
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
FAI
Benzene 0.00500
0.00454
90.8
65.0-135
Ethylbenzene 0.00500
0.00422
84.4
60.0-140
Methyl tert-butyl ether 0.00500
0.00457
91.4
64.0-123
SC
F
Toluene 0.00500
0.00406
81.2
70.0-130
Xylenes, Total 0.0150
0.0124
82.7
77.0-120
(S) Toluene-dH
98.4
80.0-120
(S) 4-Bromofluorobenzene
82.1
80.0-120
(S) 1,2-Dichloroethane-d4
106
70.0-130
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
CITGO-Selma, NC
Semiann Outfalls L1131559
01/30/20 12:08 11 of 19

1
WG1415666
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by Method 625.1
L1181559-01
Method Blank (MB)
C p
(MB) R3493691-2 01/23/20 2320
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
TC
I
Acenaphthene U
0.000316
0.00100
Acenaphthylene U
0.000309
0.00100
FSS
Anthracene U
0.000291
0.00100
Benzidine U
0.00432
0.0100
Benzo(a)anthracene U
0.0000975
0.00100
[Cn]
Benzo(b)fluoranthene U
0.0000896
0.00100
Benzo(k)fluoranthene U
0.000355
0.00100
FSr
Benzo(g,h,i)perylene U
0.000161
0.00100
Benzo(a)pyrene U
0.000340
0.00100
Bis(2-chlorethoxy)methane U
0.000329
0.0100
Bis(2-chloroethyl)ether U
0.00162
0.0100
2,2-oxybis(1-chloropropane) U
0.000445
0.0100
7GI
4-Bromophenyl-phenylether U
0.000335
0.0100
2-Chloronaphthalene U
0.000330
0.00100
4-Chlorophenyl-phenylether U
0.000303
0.0100
FAI
Chrysene U
0.000332
0.00100
Dibenz(a,h)anthracene U
0.000279
0.00100
FSC
3,3-Dichlorobenzidine U
0.00202
0.0100
2,4-Dinitrotoluene U
0.00165
0.0100
2,6-Dinitrotoluene U
0.000279
0.0100
Fluoranthene U
0.000310
0.00100
Fluorene U
0.000323
0.00100
Hexachlorobenzene U
0.000341
0.00100
Hexachloro-1,3-butadiene U
0.000329
0.0100
Hexachlorocyclopentadiene U
0.00233
0.0100
Hexachloroethane U
0.000365
0.0100
Indeno(1,2,3-cd)pyrene U
0.000279
0.00100
Isophorone U
0.000272
0.0100
Naphthalene 0.00215
0.000372
0.00100
Nitrobenzene U
0.000367
0.0100
n-Nitrosodimethylamine U
0.00126
0.0100
n-Nitrosodiphenylamine U
0.00119
0.0100
n-Nitrosodi-n-propylamine U
0.000403
0.0100
Phenanthrene U
0.000366
0.00100
Benzylbutyl phthalate U
0.000275
0.00300
B is(2-ethyl hexyl)phthal ate U
0.000709
0.00300
Di-n-butyl phthalate U
0.000266
0.00300
Diethyl phthalate U
0.000282
0.00300
Dimethyl phthalate U
0.000283
0.00300
Di-n-octyl phthalate U
0.000278
0.00300
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
CITGO-Selma, NC
Semiann Outfalls
L1131559
01/30/2012:03 12 of19

1
WG1415666
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by Method 625.1
L1181559-01
Method Blank (MB)
C p
(MB) R3493691-2 01/23/20 2320
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
z
TC
Pyrene U
0.000330
0.00100
1,2,4-Trichlorobenzene U
0.000355
0.0100
FS
1,2-Diphenylhydrazine U
0.000318
0.0100
4-Chl oro-3-m ethyl phenol U
0.000263
0.0100
2-Chorophenol U
0.000283
0.0100
[Cn]
2-Nitrophenol U
0.000320
0.0100
4-Nitrophenol U
0.00201
0.0100
5
Sr
Pentachlorophenol U
0.000313
0.0100
Phenol U
0.000334
0.0100
2,4,6-Trichlorophenol U
0.000297
0.0100
2,4-Dichlorophenol U
0.000284
0.0100
2,4-Dimethylphenol U
0.000624
0.0100
7GI
4,6-Dinitro-2-methylphenol U
0.00262
0.0100
2,4-Dinitrophenol U
0.00325
0.0100
(S) Nitrobenzene-d5 61.6
15.0-314
FAI
(S) 2-Fluorobiphenyl 77.7
22.0-127
(S) p-Terphenyl-d14 79.3
29.0-141
FS
(S) Phenol-d5 24.2
8.00-424
(S) 2-Fluorophenol 38.6
10.0-120
(S) 2,4, 6-Tribromophenol 84.5
10. 0-153
Laboratory Control Sample (LCS)
(LCS) R3493691-1 01/23/20 22:59
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Acenaphthene
0.0500
0.0359
71.8
47.0-145
Acenaphthylene
0.0500
0.0386
77.2
33.0-145
Anthracene
0.0500
0.0392
78.4
27.0-133
Benzidine
0.100
0.0273
27.3
1.00-120
Benzo(a)anthracene
0.0500
0.0391
78.2
33.0-143
Benzo(b)fluoranthene
0.0500
0.0419
83.8
24.0-159
Benzo(k)fluoranthene
0.0500
0.0396
79.2
11.0-162
Benzo(g,h,i)perylene
0.0500
0.0448
89.6
1.00-219
Benzo(a)pyrene
0.0500
0.0436
87.2
17.0-163
Bis(2-chlorethoxy)methane
0.0500
0.0319
63.8
1.00-219
Bis(2-chloroethyl)ether
0.0500
0.0334
66.8
33.0-185
2,2-oxybis(1-chloropropane)
0.0500
0.0332
66.4
36.0-166
4-Bromophenyl-phenylether
0.0500
0.0429
85.8
53.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma,
NC
Semiann Outfalls L1131559 01/30/2012:03 13 of19

WG1415666
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by
Method 625.1
L1181559-01
Laboratory Control Sample (LCS)
C
Fp
(LCS) R3493691-1 01/23/20 22:59
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
E
2-Chloronaphthalene 0.0500
0.0361
72.2
60.0-120
4-Chlorophenyl-phenylether 0.0500
0.0399
79.8
25.0-158
FS
Chrysene 0.0500
0.0399
79.8
17.0-168
Dibenz(a,h)anthracene 0.0500
0.0387
77.4
1.00-227
3,3-Dichlorobenzidine 0.100
0.0851
85.1
1.00-262
FC n
2,4-Dinitrotoluene 0.0500
0.0412
82.4
39.0-139
2,6-Dinitrotoluene 0.0500
0.0411
82.2
50.0-158
E
Fluoranthene 0.0500
0.0415
83.0
26.0-137
Fluorene 0.0500
0.0382
76.4
59.0-121
Hexachlorobenzene 0.0500
0.0425
85.0
1.00-152
Hexachloro-1,3-butadiene 0.0500
0.0338
67.6
24.0-120
Hexachlorocyclopentadiene 0.0500
0.0317
63.4
10.0-120
FGI
Hexachloroethane 0.0500
0.0352
70.4
40.0-120
Indeno(1,2,3-cd)pyrene 0.0500
0.0399
79.8
1.00-171
Isophorone 0.0500
0.0315
63.0
21.0-196
FAI
Naphthalene 0.0500
0.0339
67.8
21.0-133
Nitrobenzene 0.0500
0.0305
61.0
35.0-180
E
n-Nitrosodimethylamine 0.0500
0.0180
36.0
10.0-120
n-Nitrosodiphenylamine 0.0500
0.0401
80.2
44.0-120
n-Nitrosodi-n-propylamine 0.0500
0.0333
66.6
1.00-230
Phenanthrene 0.0500
0.0386
77.2
54.0-120
Benzylbutyl phthalate 0.0500
0.0366
73.2
1.00-152
B is(2-ethyl hexyl)phthal ate 0.0500
0.0352
70.4
8.00-158
Di-n-butyl phthalate 0.0500
0.0423
84.6
1.00-120
Diethyl phthalate 0.0500
0.0396
79.2
1.00-120
Dimethyl phthalate 0.0500
0.0390
78.0
1.00-120
Di-n-octyl phthalate 0.0500
0.0370
74.0
4.00-146
Pyrene 0.0500
0.0386
77.2
52.0-120
1,2,4-Trichlorobenzene 0.0500
0.0328
65.6
44.0-142
1,2-Diphenylhydrazine 0.0500
0.0357
71.4
37.0-125
4-Chl oro-3-m ethyl phenol 0.0500
0.0335
67.0
22.0-147
2-Chlorophenol 0.0500
0.0326
65.2
23.0-134
2,4-Dichlorophenol 0.0500
0.0340
68.0
39.0-135
2,4-Dimethylphenol 0.0500
0.0300
60.0
32.0-120
4,6-Dinitro-2-methylphenol 0.0500
0.0444
88.8
1.00-181
2,4-Dinitrophenol 0.0500
0.0430
86.0
1.00-191
2-Nitrophenol 0.0500
0.0342
68.4
29.0-182
4-Nitrophenol 0.0500
0.0171
34.2
1.00-132
Pentachlorophenol 0.0500
0.0419
83.8
14.0-176
Phenol 0.0500
0.0158
31.6
5.00-120
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
CITGO-Selma, NC
Semiann Outfalls
L1131559
01/30/20 12:08 14 of 19

WG1415666 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1181559-01
Laboratory Control Sample (LCS)
(LCS) R3493691-1 01/23/20 22:59
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I mg/I
2,4,6-Trichlorophenol 0.0500 0.0384
76.8
37.0-144
(S) Nitrobenzene-d5
54.2
15.0-314
(S) 2-Fluorobiphenyl
76.8
22.0-127
(S) p-Terphenyl-d14
77.7
29.0-141
(S) Phenol-d5
25.8
8.00-424
(S) 2-Fluorophenol
40.8
10.0-120
(S) 2,4, 6-Tribromophenol
92.0
10. 0-153
L1181880-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1131330-01 01/24/20 0105 • (MS) R3493691-3 01/24/20 0126 • (MSD) R3493691-4 01/24/20 0146
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Acenaphthene
0.0500
ND
0.0359
0.0364
71.8
72.8
1 47.0-145
Acenaphthylene
0.0500
ND
0.0383
0.0390
76.6
78.0
1 33.0-145
Anthracene
0.0500
ND
0.0378
0.0397
75.6
79.4
1 27.0-133
Benzidine
0.100
ND
ND
ND
0.000
0.000
1 1.00-120
Benzo(a)anthracene
0.0500
ND
0.0391
0.0403
78.2
80.6
1 33.0-143
Benzo(b)fluoranthene
0.0500
ND
0.0422
0.0431
84.4
86.2
1 24.0-159
Benzo(k)fluoranthene
0.0500
ND
0.0394
0.0409
78.8
81.8
1 11.0-162
Benzo(g,h,i)perylene
0.0500
ND
0.0422
0.0435
84.4
87.0
1 1.00-219
Benzo(a)pyrene
0.0500
ND
0.0435
0.0451
87.0
90.2
1 17.0-163
Bis(2-chlorethoxy)methane
0.0500
ND
0.0322
0.0337
64.4
67.4
1 33.0-184
Bis(2-chloroethyl)ether
0.0500
ND
0.0328
0.0331
65.6
66.2
1 12.0-158
2,2-oxybis(1-chloropropane)
0.0500
ND
0.0319
0.0324
63.8
64.8
1 36.0-166
4-Bromophenyl-phenylether
0.0500
ND
0.0427
0.0450
85.4
90.0
1 53.0-127
2-Chloronaphthalene
0.0500
ND
0.0362
0.0375
72.4
75.0
1 60.0-120
4-Chlorophenyl-phenylether
0.0500
ND
0.0394
0.0406
78.8
81.2
1 25.0-158
Chrysene
0.0500
ND
0.0383
0.0400
76.6
80.0
1 17.0-168
Dibenz(a,h)anthracene
0.0500
ND
0.0370
0.0384
74.0
76.8
1 1.00-227
3,3-Dichlorobenzidine
0.100
ND
0.0576
0.0559
57.6
55.9
1 1.00-262
2,4-Dinitrotoluene
0.0500
ND
0.0402
0.0417
80.4
83.4
1 39.0-139
2,6-Dinitrotoluene
0.0500
ND
0.0408
0.0415
81.6
83.0
1 50.0-158
Fluoranthene
0.0500
ND
0.0410
0.0423
82.0
84.6
1 26.0-137
Fluorene
0.0500
ND
0.0381
0.0389
76.2
77.8
1 59.0-121
Hexachlorobenzene
0.0500
ND
0.0437
0.0455
87.4
91.0
1 1.00-152
Hexachloro-1,3-butadiene
0.0500
ND
0.0364
0.0366
72.8
73.2
1 24.0-120
Hexachlorocyclopentadiene
0.0500
ND
0.0323
0.0343
64.6
68.6
1 10.0-146
Hexachloroethane
0.0500
ND
0.0309
0.0315
61.8
63.0
1 40.0-120
MS Qualifier MSD Qualifier RPD RPD Limits
J6 J6
1.38
1.81
4.90
0.000
3.02
2.11
3.74
3.03
3.61
4.55
0.910
1.56
5.25
3.53
3.00
4.34
3.71
3.00
3.66
1.70
3.12
2.08
4.04
0.548
6.01
1.92
48
74
66
40
53
71
63
97
72
54
108
76
43
24
61
87
126
108
42
48
66
38
55
62
34
52
ACCOUNT: PROJECT: SDG:
CITGO-Selma, NC Semiann Outfalls L1131559
DATE/TIME:
01/30/20 12:08
PAGE:
15 of 19

WG1415666 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1181559-01
ONE LAB. NATIONWIDE. *
L1181880-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1131330-01 01/24/20 0105 • (MS) R3493691-3 01/24/20 0126 • (MSD) R3493691-4 01/24/20 0146
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Indeno(1,2,3-cd)pyrene
0.0500
ND
0.0388
0.0401
77.6
80.2
Isophorone
0.0500
ND
0.0329
0.0343
65.8
68.6
Naphthalene
0.0500
ND
0.0319
0.0318
63.8
63.6
Nitrobenzene
0.0500
ND
0.0320
0.0329
64.0
65.8
n-Nitrosodimethylamine
0.0500
ND
0.0169
0.0182
33.8
36.4
n-Nitrosodiphenylamine
0.0500
ND
0.0403
0.0414
80.6
82.8
n-Nitrosodi-n-propylamine
0.0500
ND
0.0321
0.0329
64.2
65.8
Phenanthrene
0.0500
ND
0.0380
0.0390
76.0
78.0
Benzylbutyl phthalate
0.0500
ND
0.0376
0.0394
75.2
78.8
B is(2-ethyl hexyl)phthal ate
0.0500
ND
0.0359
0.0380
71.8
76.0
Di-n-butyl phthalate
0.0500
ND
0.0426
0.0437
85.2
87.4
Diethyl phthalate
0.0500
ND
0.0397
0.0395
79.4
79.0
Dimethyl phthalate
0.0500
ND
0.0398
0.0404
79.6
80.8
Di-n-octyl phthalate
0.0500
ND
0.0387
0.0403
77.4
80.6
Pyrene
0.0500
ND
0.0389
0.0404
77.8
80.8
1,2,4-Trichlorobenzene
0.0500
ND
0.0345
0.0350
69.0
70.0
1,2-Diphenylhydrazine
0.0500
ND
0.0380
0.0393
76.0
78.6
4-Chl oro-3-m ethyl phenol
0.0500
ND
0.0336
0.0353
67.2
70.6
2-Chorophenol
0.0500
ND
0.0294
0.0317
58.8
63.4
2,4-Dichlorophenol
0.0500
ND
0.0346
0.0358
69.2
71.6
2,4-Dimethylphenol
0.0500
ND
0.0306
0.0326
61.2
65.2
4,6-Dinitro-2-methylphenol
0.0500
ND
0.0445
0.0452
89.0
90.4
2,4-Dinitrophenol
0.0500
ND
0.0440
0.0447
88.0
89.4
2-Nitrophenol
0.0500
ND
0.0356
0.0370
71.2
74.0
4-Nitrophenol
0.0500
ND
0.0929
0.0943
186
189
Pentachlorophenol
0.0500
ND
0.0414
0.0429
82.8
85.8
Phenol
0.0500
ND
0.0126
0.0141
25.2
28.2
2,4,6-Trichlorophenol
0.0500
ND
0.0379
0.0390
75.8
78.0
(S) Nitrobenzene-d5
54.3
57.6
(S) 2-Fluorobiphenyl
75.7
79.7
(S) p-Terphenyl-d14
79.8
84.5
(S) Phenol-d5
23.0
26.3
(S) 2-Fluorophenol
36.7
42.4
(S)Z4,6-Tribromophenol
95.5
96.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 1.00-171
3.30
99
1 21.0-196
4.17
93
1 21.0-133
0.314
65
1 35.0-180
2.77
62
1 10.0-120
7.41
40
1 16.0-160
2.69
28
1 1.00-230
2.46
87
1 54.0-120
2.60
39
1 1.00-152
4.68
60
1 8.00-158
5.68
82
1 1.00-120
2.55
47
1 1.00-120
0.505
100
1 1.00-120
1.50
183
1 4.00-146
4.05
69
1 52.0-120
3.78
49
1 44.0-142
1.44
50
1 18.0-156
3.36
34
1 22.0-147
4.93
73
1 23.0-134
7.53
61
1 39.0-135
3.41
50
1 32.0-120
6.33
58
1 1.00-181
1.56
203
1 1.00-191
1.58
132
1 29.0-182
3.86
55
1 1.00-132
J5 J5 1.50
131
1 14.0-176
3.56
86
1 5.00-120
11.2
64
1 37.0-144
2.86
58
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:08 16 of 19

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
Fp
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FS
Fn
Fr
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SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
CITGO-Selma, NC Semiann Outfalls L1131559 01/30/20 12:03 17 of 19

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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SDG: DATE/TIME: PAGE:
L1131559 01/30/20 12:03 13 of 19

Billing Information:
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Chain of Custody Page _ of
CITGO-Selma, NC
H. Wayne Whiting [re
4095 Buffalo Road
aceAnal ical'
4095 Buffalo Road
Selma, NC 27576
Henxe+Ce�rer !c. rarv.�S'�'mtAnn.,
Selma, NC 27576
12065 Lebanon Rd
Report to:
Email To [e-mail];
H. Wayne Whiting
[e-mail],[e-mail]
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Phount ne 615-7TN �712
58 58587
Phone-800-767-5859
Fax: [phone]
Project
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Outfalls-Semiann Monitoring
Collected:
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_ Next Day _ 5 Day (Rad Only) Date Results Needed
Two Day 10 pay (Rad Only)
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' Matrix: emarks:Please call Keith Oravits at the ESC Raleigh office, for sample pickup. Sample Receipt C kl.: F
SS - Soil AIR - Air F- Filter 19-210-5148 We would appreciate 24 hourdtiPH Temp COC seal present/Intact: P _Y _N
pp advance notice COC Signed/Accurate: /Y N
GW -Groundwater S- Bioassay hank you-ESC FlowBottles arrive intact: _ �Y N
Other
WW - Waste Water Correct bottles used: �Y
_N
DW- Drinking Water Sufficient volume sent: _7Y _N
Samples returned via: Tracking # �l f
T - Other
_UPS _ FedEx —Courier VOA Zero Headspace: 4eY N
Relinquished by: (Signature} Date; Time: Received by: nat - Tr' nk Received: Y No Preservation Correct/Checked: N
RAD Screen <0.5 mR/hr:l —N
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Relinquished by (Sig na j
Date:
Time:
eore}
Temp: °[ Battles Received:
If preservation required by Login: Date/Time
Relinquished t7y- {Sat
Date:
Time:
Received for lab by: signature}
Date: Time:
Hold:
Condition:
NCF /
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