WQ0000020_Monitoring (Report)_20200225

DEPARTMENT OF ENVIRONMENTAL QUALITY
FACILITY INFORMATION
Facility Name:08/31/2020
Permit Name (if different):
Facility Address:
TYPE OF PERMITTED OPERATION BEING MONITORED
NC 28732 County
(State) (Zip)
Contact Person: Telephone#
Well Location/Site Name:8
(from Permit)
Units SW-2-A1 SW-3-A1 SW-4B-A1 SW-4C-A1 SW-5-A1 SW-6-A1 SW-8-A1 SW-9-A1
Well Depth [ft below land surface] ft N/A N/A N/A N/A N/A N/A N/A N/A
Measuring Point (toc) [ft above land surface] ft N/A N/A N/A N/A N/A N/A N/A N/A
Well Diameter in N/A N/A N/A N/A N/A N/A N/A N/A
Screen Top [ft below land surface] ft N/A N/A N/A N/A N/A N/A N/A N/A
Screen Bottom [ft below land surface] ft N/A N/A N/A N/A N/A N/A N/A N/A
Relative Measuring Point Elevation ft N/A N/A N/A N/A N/A N/A N/A N/A
15A-2B**Units SW-2-A1 SW-3-A1 SW-4B-A1 SW-4C-A1 SW-5-A1 SW-6-A1 SW-8-A1 SW-9-A1
Sample Date 01/13/2020 01/13/2020 01/13/2020 01/13/2020 01/13/2020 01/13/2020 01/13/2020 01/13/2020
Volume of Water pumped/bailed gal N/A N/A N/A N/A N/A N/A N/A N/A Appearance
Temperature (00010) deg. C 12.0 13.0 12.0 12.0 13.0 13.0 11.0 13.0 SW-4B-A1 Clear, Film on Surface, Sheen
Odor (00085)None None None None None None None None SW-5-A1 Clear, Red/Iron, Fines
Appearance Clear Clear / Fines See To Right Clear / Fines See To Right See To Right See To Right See To Right SW-6-A1 Red/Iron, Sheen, Fines
Turbidity (82078) NTU 4.1 11.5 1.6 18.6 27.1 12.1 56.8 31.3 SW-8-A1 Turbid, Red/Iron, Film on Surface, Sheen, Floc
Dissolved Oxygen (00300) ≥ 5.0 mg/L 8.79 8.97 5.79 8.56 7.02 7.12 5.43 8.92 SW-9-A1 Turbid, Film on Surface, Sheen
Oxidation Reduction Potential (00090) mV 361 251 337 183 295 313 131 248
Specific Cond - field (00094) umhos/cm 110 124 88 222 155 96 858 138
Water Level [ft below measuring pt.] (82546) ft N/A N/A N/A N/A N/A N/A N/A N/A
pH - field (00400)6 - 9 SU 6.2 6.2 5.8 6.7 6.0 6.2 6.8 5.7
Laboratory Name Yes No
Sample Analysis Date Yes No
15A-2B**Units SW-2-A1 SW-3-A1 SW-4B-A1 SW-4C-A1 SW-5-A1 SW-6-A1 SW-8-A1 SW-9-A1
TDS - Total Diss. Solids (70300) NE mg/l 63 68 35 105 96 50 479 75 0 0 0 0 0 0 0 0 0
Cl - Chloride (00940) R 230 mg/l 14.5 11.5 2.8 11.6 5.6 5.2 3.7 13.1 0 0 0 0 0 0 0 0 0
As - Arsenic (01002) 10 ug/l 0.12 0.33 0.12 0.39 2.5 0.32 290 0.39 0 0 0 0 0 0 0 0 0
SO4 - Sulfate (00945) NE mg/l 2.5 3.5 9.3 7.6 4.5 5.1 28.9 4.3 0 0 0 0 0 0 0 0 0
Cd - Cadmium (01025) 1 0.15 ug/l <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 <0.08 0 0 0 0 0 0 0 0 0
Cr - Chromium, tot (01034) NE ug/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Cr - Chromium, diss (01030) 1 NE ug/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Cu - Copper (01040) R,1 2.7 ug/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Fe - Iron (01045) NE ug/l 198 2,480 924 15,500 14,800 2,790 20,600 5,970 0 0 0 0 0 0 0 0 0
Hg - Mercury (71900) 0.012 ug/l <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 0 0 0 0 0 0 0 0 0
Mn - Manganese (01055) NE ug/l 102 479 187 1930 2070 550 6230 739 0 0 0 0 0 0 0 0 0
Ni - Nickel (01065) 1 16 ug/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Pb - Lead (01049) 1 0.54 ug/l <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0 0 0 0 0 0 0 0 0
Zn - Zinc (01090) R,1 0.036 mg/L 0.013 <0.01 <0.01 <0.01 0.011 <0.01 <0.01 <0.01 0 0 0 0 0 0 0 0 0
Ba - Barium (01007) T 21,000 ug/l 47.4 41.6 21.6 48.8 79.2 19 228 53 0 0 0 0 0 0 0 0 0
B - Boron (01022) NE ug/l <50 <50 111 108 127 <50 1100 <50 0 0 0 0 0 0 0 0 0
Tl - Thallium (01059) 2 ug/l <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0 0 0 0 0 0 0 0 0
Sb - Antimony (01097) T 5300 ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0 0 0 0 0 0 0 0 0
Se - Selenium (01147) 5 ug/l <0.5 <0.5 2.3 <0.5 0.61 <0.5 <0.5 <0.5 0 0 0 0 0 0 0 0 0
Alkalinity - (00410) NE mg/l 14.6 30.8 23.5 59 69 34.2 438 30.8 0 0 0 0 0 0 0 0 0
Al - Aluminum (01105) 2 160 ug/l <100 353 <100 598 1,590 <100 4,740 1,040 0 0 0 0 0 0 0 0 0
Be - Beryllium (01010) 1 6.5 ug/l <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0 0 0 0 0 0 0 0 0
HCO3 - Bicarbonate (00440) NE mg/l 14.6 30.8 23.5 59 69 34.2 438 30.8 0 0 0 0 0 0 0 0 0
Ca - Calcium (00916) NE mg/l 6.8 9.5 6.3 14.8 18.7 8.8 131 9.9 0 0 0 0 0 0 0 0 0
CO3 - Carbonate (00445) NE mg/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Co - Cobalt (01037) T 1.6 ug/l 0.3 1.9 0.56 8.7 4.3 1.5 13.4 3.6 0 0 0 0 0 0 0 0 0
Mg - Magnesium (00927) NE mg/l 2.7 3.6 3.4 6.8 5.1 3.4 27.2 4 0 0 0 0 0 0 0 0 0
Mo - Molybdenum (01062) T 2,000 ug/l <0.5 <0.5 <0.5 <0.5 6.7 <0.5 79.3 <0.5 0 0 0 0 0 0 0 0 0
K - Potassium (00937) NE mg/l <5 <5 <5 <5 <5 <5 <5 <5 0 0 0 0 0 0 0 0 0
Na - Sodium (82035) NE mg/l 6.3 5.2 <5 <5 <5 <5 5.9 5.8 0 0 0 0 0 0 0 0 0
TSS - Total Susp. Solids (70031) NE mg/l <2.9 9.6 <2.6 45.8 20.3 <8.3 221 30.3 0 0 0 0 0 0 0 0 0
V - Vanadium (01087) NE ug/l 0.37 0.71 <0.3 0.70 1.9 <0.3 3.0 1.6 0 0 0 0 0 0 0 0 0
Sr - Strontium (01082) T 40 mg/l 0.051 0.085 0.059 0.15 0.257 0.041 2.02 0.077 0 0 0 0 0 0 0 0 0
NE = Not Established
BOLD values equal or exceed the corresponding 2B standard R = Regular Criteria T= In-Stream Target Value Notes:
GW-59CCR 09/2015 - Voluntary **November 1, 2019 2B values are for Chronic Class B waters (April 2018 for Thallium)
1 - Listed standard is dissolved fraction, chronic value at 25 mg/L hardness
2 - Dec. 2018 revised EPA criteria
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) Date
Turbidity is field analyzed for information use only.

Laboratory Information
Pace Analytical Services Certification #NC DENR # 40 Samples for metals were collected unfiltered:
January 14 - 17, 2020 and field acidified:
CHECK IF DRY WELL AT TIME OF SAMPLING
(City)
John Toepfer 919-546-7863
Structural Fill Area I No. of SW to be sampled:
Monitoring Well Construction Information
Well ID Number (From Permit)
Sampling Information and Field Analysis
61 Terminal Drive
(Street) Coal Ash Structural Fill
Fletcher Buncombe
Asheville Regional Airport Permit Type:CCP Structural Fill Projects Expiration Date:
Duke Energy Progress, Inc.PERMIT Number:WQ0000020
Please Print Clearly or Type
Mail original
and 1 copy to:
GROUNDWATER QUALITY MONITORING
COMPLIANCE REPORT FORM DIVISION OF WATER QUALITY - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRYDRYDRYDRY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Vendor QC Data Review
Summary Report
Analytical Laboratory
Order Number:J20010314
Project Name:ASHEVILLE - AIRPORT FILL AREA I - SW - VENDOR
Lab Contact:Peggy Kendall
Customer Name(s):B Allison, B Moeller, T Hunsucker,H Seaton
Phone:[phone]
Report Authorized By:
(Signature)
Program Comments:
The samples were taken directly to the vendor laboratory after sample collection.
Please review all vendor data for case narratives with explanations of quality control failures and data qualifiers.
Any analytical tests or individual analytes within a test flagged with a qualifier indicate a deviation from the method quality
system or quality control requirement. Certified vendor results and QC qualifiers can be found in the vendor lab final report.
This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory.
Vendor Data Review Criteria:
This vendor data package has been reviewed at the Duke Analytical Laboratory for the following applicable criteria:
Required QC samples collected and analyzed
Required tests performed for all samples
Vendor Laboratory utilized required test methods for all analyses
Vendor Laboratory met all requested Reporting Limits (RL)
QC Results reviewed for outlying recovery values
Case Narrative:
1-27-2020
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#=CL#
January 24, 2020
LIMS USE: FR - PROGRAM MANAGER
LIMS OBJECT ID: 92460474
92460474
Project:
Pace Project No.:
RE:
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg. 7405 MG30A2
Huntersville, NC 28078
ASHEVILLE AIRPORT J20010314
Dear Program Manager:
Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney for
[e-mail]
HORIZON Database Administrator
Kevin Herring
1(704)875-9092
Enclosures
cc:Program Manager, Duke Energy
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 70
1-27-2020
Page 2 of 71
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 70
1-27-2020
Page 3 of 71
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID Matrix Date Collected Date Received
92460474001 ASA_SW-2-A1 Water 01/13/20 15:00 01/13/20 16:24
92460474002 ASA_SW-3-A1 Water 01/13/20 12:37 01/13/20 16:24
92460474003 ASA_SW-4B-A1 Water 01/13/20 11:15 01/13/20 16:24
92460474004 ASA_SW-5-A1 Water 01/13/20 12:17 01/13/20 16:24
92460474005 ASA_SW-6-A1 Water 01/13/20 13:15 01/13/20 16:24
92460474006 ASA_SW-8-A1 Water 01/13/20 10:36 01/13/20 16:24
92460474007 ASA_SW-9-A1 Water 01/13/20 11:25 01/13/20 16:24
92460474008 ASA_SW-4C-A1 Water 01/13/20 11:02 01/13/20 16:24
92460474009 ASA_FTB-20200113-1455 Water 01/13/20 14:55 01/13/20 16:24
92460474010 ASA_EB-20200113-1449 Water 01/13/20 14:49 01/13/20 16:24
92460474011 ASA_FB-20200113-1445 Water 01/13/20 14:45 01/13/20 16:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 70
1-27-2020
Page 4 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92460474001 ASA_SW-2-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474002 ASA_SW-3-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474003 ASA_SW-4B-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474004 ASA_SW-5-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 70
1-27-2020
Page 5 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474005 ASA_SW-6-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474006 ASA_SW-8-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS, SH1
EPA 200.7 Rev 4.4 1994 14 PASI-ADS, SH1
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474007 ASA_SW-9-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 70
1-27-2020
Page 6 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474008 ASA_SW-4C-A1 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
SM 2540C-2011 1 PASI-ACJL
SM 2540D-2011 1 PASI-AMJP
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474009 ASA_FTB-20200113-1455 EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
92460474010 ASA_EB-20200113-1449 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
92460474011 ASA_FB-20200113-1445 EPA 200.7 Rev 4.4 1994 15 PASI-ADS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 70
1-27-2020
Page 7 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 200.7 Rev 4.4 1994 14 PASI-ADS
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 200.8 Rev 5.4 10 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 6020B 1 PASI-AJOR
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
EPA 245.1 Rev 3.0 1994 1 PASI-ASOO
SM 2320B-2011 3 PASI-AECH
EPA 300.0 Rev 2.1 1993 3 PASI-ACDC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 70
1-27-2020
Page 8 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474001 ASA_SW-2-A1
Barium 47.4 ug/L 01/15/20 12:235.0EPA 200.7 Rev 4.4 1994
Calcium 6770 ug/L 01/15/20 12:23100EPA 200.7 Rev 4.4 1994
Iron 198 ug/L 01/15/20 12:2350.0EPA 200.7 Rev 4.4 1994
Magnesium 2720 ug/L 01/15/20 12:23100EPA 200.7 Rev 4.4 1994
Manganese 102 ug/L 01/15/20 12:235.0EPA 200.7 Rev 4.4 1994
Sodium 6300 ug/L 01/15/20 12:235000EPA 200.7 Rev 4.4 1994
Strontium 51.2 ug/L 01/15/20 12:235.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)28100 ug/L 01/15/20 12:23662EPA 200.7 Rev 4.4 1994
Zinc 12.3 ug/L 01/15/20 12:2310.0EPA 200.7 Rev 4.4 1994
Barium, Dissolved 41.7 ug/L 01/15/20 18:595.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 7320 ug/L 01/15/20 18:59100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 150 ug/L 01/15/20 18:5950.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 2700 ug/L 01/15/20 18:59100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 124 ug/L 01/15/20 18:595.0EPA 200.7 Rev 4.4 1994
Sodium, Dissolved 6360 ug/L 01/15/20 18:595000EPA 200.7 Rev 4.4 1994
Zinc, Dissolved 12.5 ug/L 01/15/20 18:5910.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 48.4 ug/L 01/15/20 18:595.0EPA 200.7 Rev 4.4 1994
Arsenic 0.12 ug/L 01/15/20 14:330.10EPA 200.8 Rev 5.4
Cobalt 0.30 ug/L 01/15/20 14:330.10EPA 200.8 Rev 5.4
Lead 0.26 ug/L 01/15/20 14:330.10EPA 200.8 Rev 5.4
Vanadium 0.37 ug/L 01/15/20 14:330.30EPA 200.8 Rev 5.4
Cobalt, Dissolved 0.36 ug/L 01/17/20 11:230.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)14.6 mg/L 01/15/20 16:465.0SM 2320B-2011
Alkalinity, Total as CaCO3 14.6 mg/L 01/15/20 16:465.0SM 2320B-2011
Total Dissolved Solids 63.0 mg/L 01/15/20 16:3925.0SM 2540C-2011
Chloride 14.5 mg/L 01/14/20 16:521.0EPA 300.0 Rev 2.1 1993
Sulfate 2.5 mg/L 01/14/20 16:521.0EPA 300.0 Rev 2.1 1993
92460474002 ASA_SW-3-A1
Aluminum 353 ug/L 01/15/20 12:32100EPA 200.7 Rev 4.4 1994
Barium 41.6 ug/L 01/15/20 12:325.0EPA 200.7 Rev 4.4 1994
Calcium 9480 ug/L 01/15/20 12:32100EPA 200.7 Rev 4.4 1994
Iron 2480 ug/L 01/15/20 12:3250.0EPA 200.7 Rev 4.4 1994
Magnesium 3560 ug/L 01/15/20 12:32100EPA 200.7 Rev 4.4 1994
Manganese 479 ug/L 01/15/20 12:325.0EPA 200.7 Rev 4.4 1994
Sodium 5230 ug/L 01/15/20 12:325000EPA 200.7 Rev 4.4 1994
Strontium 85.2 ug/L 01/15/20 12:325.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)38400 ug/L 01/15/20 12:32662EPA 200.7 Rev 4.4 1994
Zinc 10.3 ug/L 01/15/20 12:3210.0EPA 200.7 Rev 4.4 1994
Barium, Dissolved 35.1 ug/L 01/15/20 19:095.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 8540 ug/L 01/15/20 19:09100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 1470 ug/L 01/15/20 19:0950.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 3280 ug/L 01/15/20 19:09100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 413 ug/L 01/15/20 19:095.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 77.3 ug/L 01/15/20 19:095.0EPA 200.7 Rev 4.4 1994
Arsenic 0.33 ug/L 01/15/20 14:410.10EPA 200.8 Rev 5.4
Cobalt 1.9 ug/L 01/15/20 14:410.10EPA 200.8 Rev 5.4
Lead 0.30 ug/L 01/15/20 14:410.10EPA 200.8 Rev 5.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 70
1-27-2020
Page 9 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474002 ASA_SW-3-A1
Vanadium 0.71 ug/L 01/15/20 14:410.30EPA 200.8 Rev 5.4
Cobalt, Dissolved 1.6 ug/L 01/16/20 15:330.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)30.8 mg/L 01/15/20 17:055.0SM 2320B-2011
Alkalinity, Total as CaCO3 30.8 mg/L 01/15/20 17:055.0SM 2320B-2011
Total Dissolved Solids 68.0 mg/L 01/15/20 16:3925.0SM 2540C-2011
Total Suspended Solids 9.6 mg/L 01/16/20 12:322.5SM 2540D-2011
Chloride 11.5 mg/L 01/14/20 17:061.0EPA 300.0 Rev 2.1 1993
Sulfate 3.5 mg/L 01/14/20 17:061.0EPA 300.0 Rev 2.1 1993
92460474003 ASA_SW-4B-A1
Barium 21.6 ug/L 01/15/20 12:365.0EPA 200.7 Rev 4.4 1994
Boron 111 ug/L 01/15/20 12:3650.0EPA 200.7 Rev 4.4 1994
Calcium 6280 ug/L 01/15/20 12:36100EPA 200.7 Rev 4.4 1994
Iron 924 ug/L 01/15/20 12:3650.0EPA 200.7 Rev 4.4 1994
Magnesium 3420 ug/L 01/15/20 12:36100EPA 200.7 Rev 4.4 1994
Manganese 187 ug/L 01/15/20 12:365.0EPA 200.7 Rev 4.4 1994
Strontium 58.8 ug/L 01/15/20 12:365.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)29800 ug/L 01/15/20 12:36662EPA 200.7 Rev 4.4 1994
Barium, Dissolved 19.0 ug/L 01/15/20 19:185.0EPA 200.7 Rev 4.4 1994
Boron, Dissolved 103 ug/L 01/15/20 19:1850.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 5560 ug/L 01/15/20 19:18100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 634 ug/L 01/15/20 19:1850.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 3120 ug/L 01/15/20 19:18100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 166 ug/L 01/15/20 19:185.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 52.6 ug/L 01/15/20 19:185.0EPA 200.7 Rev 4.4 1994
Arsenic 0.12 ug/L 01/15/20 15:080.10EPA 200.8 Rev 5.4
Cobalt 0.56 ug/L 01/15/20 15:080.10EPA 200.8 Rev 5.4
Selenium 2.3 ug/L 01/15/20 15:080.50EPA 200.8 Rev 5.4
Selenium, Dissolved 2.2 ug/L 01/16/20 15:370.50EPA 200.8 Rev 5.4
Cobalt, Dissolved 0.50 ug/L 01/16/20 15:370.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)23.5 mg/L 01/15/20 17:115.0SM 2320B-2011
Alkalinity, Total as CaCO3 23.5 mg/L 01/15/20 17:115.0SM 2320B-2011
Total Dissolved Solids 35.0 mg/L 01/15/20 16:3925.0SM 2540C-2011
Chloride 2.8 mg/L 01/14/20 17:201.0EPA 300.0 Rev 2.1 1993
Sulfate 9.3 mg/L 01/14/20 17:201.0EPA 300.0 Rev 2.1 1993
92460474004 ASA_SW-5-A1
Aluminum 1590 ug/L 01/15/20 12:39100EPA 200.7 Rev 4.4 1994
Barium 79.2 ug/L 01/15/20 12:395.0EPA 200.7 Rev 4.4 1994
Boron 127 ug/L 01/15/20 12:3950.0EPA 200.7 Rev 4.4 1994
Calcium 18700 ug/L 01/15/20 12:39100EPA 200.7 Rev 4.4 1994
Iron 14800 ug/L 01/15/20 12:3950.0EPA 200.7 Rev 4.4 1994
Magnesium 5060 ug/L 01/15/20 12:39100EPA 200.7 Rev 4.4 1994
Manganese 2070 ug/L 01/15/20 12:395.0EPA 200.7 Rev 4.4 1994
Strontium 257 ug/L 01/15/20 12:395.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)67400 ug/L 01/15/20 12:39662EPA 200.7 Rev 4.4 1994
Zinc 31.6 ug/L 01/15/20 12:3910.0EPA 200.7 Rev 4.4 1994
Barium, Dissolved 30.6 ug/L 01/15/20 19:215.0EPA 200.7 Rev 4.4 1994
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 70
1-27-2020
Page 10 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474004 ASA_SW-5-A1
Boron, Dissolved 117 ug/L 01/15/20 19:2150.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 16700 ug/L 01/15/20 19:21100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 341 ug/L 01/15/20 19:2150.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 4640 ug/L 01/15/20 19:21100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 498 ug/L 01/15/20 19:215.0EPA 200.7 Rev 4.4 1994
Zinc, Dissolved 10.6 ug/L 01/15/20 19:2110.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 228 ug/L 01/15/20 19:215.0EPA 200.7 Rev 4.4 1994
Arsenic 2.5 ug/L 01/16/20 14:510.10EPA 200.8 Rev 5.4
Cobalt 4.3 ug/L 01/16/20 14:510.10EPA 200.8 Rev 5.4
Lead 1.0 ug/L 01/16/20 14:510.10EPA 200.8 Rev 5.4
Molybdenum 6.7 ug/L 01/16/20 14:510.50EPA 200.8 Rev 5.4
Selenium 0.61 ug/L 01/16/20 14:510.50EPA 200.8 Rev 5.4
Vanadium 1.9 ug/L 01/15/20 17:220.30EPA 200.8 Rev 5.4
Arsenic, Dissolved 0.27 ug/L 01/16/20 15:410.10EPA 200.8 Rev 5.4
Molybdenum, Dissolved 2.6 ug/L 01/16/20 15:410.50EPA 200.8 Rev 5.4
Cobalt, Dissolved 0.82 ug/L 01/16/20 15:410.10EPA 200.8 Rev 5.4
Lithium 2.9 ug/L 01/16/20 14:512.5EPA 6020B
Alkalinity,Bicarbonate (CaCO3)69.0 mg/L 01/15/20 17:185.0SM 2320B-2011
Alkalinity, Total as CaCO3 69.0 mg/L 01/15/20 17:185.0SM 2320B-2011
Total Dissolved Solids 96.0 mg/L 01/15/20 16:4025.0SM 2540C-2011
Total Suspended Solids 20.3 mg/L 01/16/20 12:324.2SM 2540D-2011
Chloride 5.6 mg/L 01/14/20 17:341.0EPA 300.0 Rev 2.1 1993
Sulfate 4.5 mg/L 01/14/20 17:341.0EPA 300.0 Rev 2.1 1993
92460474005 ASA_SW-6-A1
Barium 19.0 ug/L 01/15/20 12:425.0EPA 200.7 Rev 4.4 1994
Calcium 8780 ug/L 01/15/20 12:42100EPA 200.7 Rev 4.4 1994
Iron 2790 ug/L 01/15/20 12:4250.0EPA 200.7 Rev 4.4 1994
Magnesium 3420 ug/L 01/15/20 12:42100EPA 200.7 Rev 4.4 1994
Manganese 550 ug/L 01/15/20 12:425.0EPA 200.7 Rev 4.4 1994
Strontium 41.2 ug/L 01/15/20 12:425.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)36000 ug/L 01/15/20 12:42662EPA 200.7 Rev 4.4 1994
Barium, Dissolved 16.8 ug/L 01/15/20 19:255.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 7910 ug/L 01/15/20 19:25100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 288 ug/L 01/15/20 19:2550.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 3170 ug/L 01/15/20 19:25100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 495 ug/L 01/15/20 19:255.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 37.2 ug/L 01/15/20 19:255.0EPA 200.7 Rev 4.4 1994
Arsenic 0.32 ug/L 01/17/20 12:250.10EPA 200.8 Rev 5.4
Cobalt 1.5 ug/L 01/17/20 12:250.10EPA 200.8 Rev 5.4
Arsenic, Dissolved 0.16 ug/L 01/16/20 15:450.10EPA 200.8 Rev 5.4
Cobalt, Dissolved 1.4 ug/L 01/16/20 15:450.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)34.2 mg/L 01/15/20 17:275.0SM 2320B-2011
Alkalinity, Total as CaCO3 34.2 mg/L 01/15/20 17:275.0SM 2320B-2011
Total Dissolved Solids 50.0 mg/L 01/15/20 16:4025.0SM 2540C-2011
Chloride 5.2 mg/L 01/14/20 17:481.0EPA 300.0 Rev 2.1 1993
Sulfate 5.1 mg/L 01/14/20 17:481.0EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 70
1-27-2020
Page 11 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474006 ASA_SW-8-A1
Aluminum 4740 ug/L 01/15/20 12:45100EPA 200.7 Rev 4.4 1994
Barium 228 ug/L 01/15/20 12:455.0EPA 200.7 Rev 4.4 1994
Boron 1100 ug/L 01/15/20 12:4550.0EPA 200.7 Rev 4.4 1994
Calcium 131000 ug/L 01/16/20 19:04500EPA 200.7 Rev 4.4 1994
Iron 20600 ug/L 01/15/20 12:4550.0EPA 200.7 Rev 4.4 1994
Magnesium 27200 ug/L 01/15/20 12:45100EPA 200.7 Rev 4.4 1994
Manganese 6230 ug/L 01/15/20 12:455.0EPA 200.7 Rev 4.4 1994
Sodium 5940 ug/L 01/15/20 12:455000EPA 200.7 Rev 4.4 1994
Strontium 2020 ug/L 01/15/20 12:455.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)439000 ug/L 01/16/20 19:043310EPA 200.7 Rev 4.4 1994
Zinc 10.7 ug/L 01/15/20 12:4510.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 118000 ug/L 01/16/20 18:42500EPA 200.7 Rev 4.4 1994
Barium, Dissolved 146 ug/L 01/15/20 19:285.0EPA 200.7 Rev 4.4 1994
Boron, Dissolved 992 ug/L 01/15/20 19:2850.0EPA 200.7 Rev 4.4 1994
Iron, Dissolved 9770 ug/L 01/15/20 19:2850.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 25100 ug/L 01/15/20 19:28100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 6100 ug/L 01/15/20 19:285.0EPA 200.7 Rev 4.4 1994
Sodium, Dissolved 5570 ug/L 01/15/20 19:285000EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 1890 ug/L 01/15/20 19:285.0EPA 200.7 Rev 4.4 1994
Arsenic 290 ug/L 01/14/20 18:300.10EPA 200.8 Rev 5.4
Cobalt 13.4 ug/L 01/17/20 12:290.50EPA 200.8 Rev 5.4
Lead 2.0 ug/L 01/14/20 18:300.10EPA 200.8 Rev 5.4
Molybdenum 79.3 ug/L 01/14/20 18:300.50EPA 200.8 Rev 5.4
Vanadium 3.0 ug/L 01/17/20 12:291.5EPA 200.8 Rev 5.4
Molybdenum, Dissolved 73.7 ug/L 01/16/20 15:495.0EPA 200.8 Rev 5.4
Cobalt, Dissolved 10.6 ug/L 01/16/20 15:491.0EPA 200.8 Rev 5.4
Arsenic, Dissolved 229 ug/L 01/15/20 19:310.10EPA 200.8 Rev 5.4
Lithium 38.1 ug/L 01/15/20 17:3812.5EPA 6020B
Lithium, Dissolved 33.9 ug/L 01/16/20 15:4925.0EPA 6020B
Alkalinity,Bicarbonate (CaCO3)438 mg/L 01/15/20 17:345.0SM 2320B-2011
Alkalinity, Total as CaCO3 438 mg/L 01/15/20 17:345.0SM 2320B-2011
Total Dissolved Solids 479 mg/L 01/15/20 16:4025.0SM 2540C-2011
Total Suspended Solids 221 mg/L 01/16/20 12:3216.7SM 2540D-2011
Chloride 3.7 mg/L 01/14/20 18:021.0EPA 300.0 Rev 2.1 1993
Fluoride 0.50 mg/L 01/14/20 18:020.10EPA 300.0 Rev 2.1 1993
Sulfate 28.9 mg/L 01/14/20 18:021.0EPA 300.0 Rev 2.1 1993
92460474007 ASA_SW-9-A1
Aluminum 1040 ug/L 01/15/20 12:48100EPA 200.7 Rev 4.4 1994
Barium 53.0 ug/L 01/15/20 12:485.0EPA 200.7 Rev 4.4 1994
Calcium 9920 ug/L 01/15/20 12:48100EPA 200.7 Rev 4.4 1994
Iron 5970 ug/L 01/15/20 12:4850.0EPA 200.7 Rev 4.4 1994
Magnesium 4000 ug/L 01/15/20 12:48100EPA 200.7 Rev 4.4 1994
Manganese 739 ug/L 01/15/20 12:485.0EPA 200.7 Rev 4.4 1994
Sodium 5790 ug/L 01/15/20 12:485000EPA 200.7 Rev 4.4 1994
Strontium 77.4 ug/L 01/15/20 12:485.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)41300 ug/L 01/15/20 12:48662EPA 200.7 Rev 4.4 1994
Zinc 15.7 ug/L 01/15/20 12:4810.0EPA 200.7 Rev 4.4 1994
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 70
1-27-2020
Page 12 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474007 ASA_SW-9-A1
Barium, Dissolved 40.8 ug/L 01/15/20 19:315.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 8740 ug/L 01/15/20 19:31100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 3740 ug/L 01/15/20 19:3150.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 3550 ug/L 01/15/20 19:31100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 581 ug/L 01/15/20 19:315.0EPA 200.7 Rev 4.4 1994
Sodium, Dissolved 5480 ug/L 01/15/20 19:315000EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 70.4 ug/L 01/15/20 19:315.0EPA 200.7 Rev 4.4 1994
Arsenic 0.39 ug/L 01/17/20 12:330.10EPA 200.8 Rev 5.4
Cobalt 3.6 ug/L 01/17/20 12:330.10EPA 200.8 Rev 5.4
Lead 0.85 ug/L 01/17/20 12:330.10EPA 200.8 Rev 5.4
Vanadium 1.6 ug/L 01/17/20 12:330.30EPA 200.8 Rev 5.4
Arsenic, Dissolved 0.10 ug/L 01/17/20 11:270.10EPA 200.8 Rev 5.4
Cobalt, Dissolved 2.5 ug/L 01/17/20 11:270.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)30.8 mg/L 01/15/20 18:075.0SM 2320B-2011
Alkalinity, Total as CaCO3 30.8 mg/L 01/15/20 18:075.0SM 2320B-2011
Total Dissolved Solids 75.0 mg/L 01/15/20 16:4025.0SM 2540C-2011
Total Suspended Solids 30.3 mg/L 01/16/20 12:324.2SM 2540D-2011
Chloride 13.1 mg/L 01/14/20 18:161.0EPA 300.0 Rev 2.1 1993
Sulfate 4.3 mg/L 01/14/20 18:161.0EPA 300.0 Rev 2.1 1993
92460474008 ASA_SW-4C-A1
Aluminum 598 ug/L 01/15/20 12:51100EPA 200.7 Rev 4.4 1994
Barium 48.8 ug/L 01/15/20 12:515.0EPA 200.7 Rev 4.4 1994
Boron 108 ug/L 01/15/20 12:5150.0EPA 200.7 Rev 4.4 1994
Calcium 14800 ug/L 01/15/20 12:51100EPA 200.7 Rev 4.4 1994
Iron 15500 ug/L 01/15/20 12:5150.0EPA 200.7 Rev 4.4 1994
Magnesium 6830 ug/L 01/15/20 12:51100EPA 200.7 Rev 4.4 1994
Manganese 1930 ug/L 01/15/20 12:515.0EPA 200.7 Rev 4.4 1994
Strontium 150 ug/L 01/15/20 12:515.0EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 2340B)65000 ug/L 01/15/20 12:51662EPA 200.7 Rev 4.4 1994
Barium, Dissolved 40.0 ug/L 01/15/20 19:345.0EPA 200.7 Rev 4.4 1994
Boron, Dissolved 97.6 ug/L 01/15/20 19:3450.0EPA 200.7 Rev 4.4 1994
Calcium, Dissolved 13100 ug/L 01/15/20 19:34100EPA 200.7 Rev 4.4 1994
Iron, Dissolved 13300 ug/L 01/15/20 19:3450.0EPA 200.7 Rev 4.4 1994
Magnesium, Dissolved 6170 ug/L 01/15/20 19:34100EPA 200.7 Rev 4.4 1994
Manganese, Dissolved 1740 ug/L 01/15/20 19:345.0EPA 200.7 Rev 4.4 1994
Strontium, Dissolved 135 ug/L 01/15/20 19:345.0EPA 200.7 Rev 4.4 1994
Arsenic 0.39 ug/L 01/16/20 14:540.10EPA 200.8 Rev 5.4
Cobalt 8.7 ug/L 01/16/20 14:540.10EPA 200.8 Rev 5.4
Lead 0.35 ug/L 01/16/20 14:540.10EPA 200.8 Rev 5.4
Vanadium 0.70 ug/L 01/15/20 17:530.30EPA 200.8 Rev 5.4
Arsenic, Dissolved 0.22 ug/L 01/17/20 11:310.10EPA 200.8 Rev 5.4
Cobalt, Dissolved 8.3 ug/L 01/17/20 11:310.10EPA 200.8 Rev 5.4
Alkalinity,Bicarbonate (CaCO3)59.0 mg/L 01/15/20 18:145.0SM 2320B-2011
Alkalinity, Total as CaCO3 59.0 mg/L 01/15/20 18:145.0SM 2320B-2011
Total Dissolved Solids 105 mg/L 01/15/20 16:4025.0SM 2540C-2011
Total Suspended Solids 45.8 mg/L 01/16/20 12:336.2SM 2540D-2011
Chloride 11.6 mg/L 01/14/20 18:581.0EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 70
1-27-2020
Page 13 of 71
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92460474008 ASA_SW-4C-A1
Sulfate 7.6 mg/L 01/14/20 18:581.0EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 70
1-27-2020
Page 14 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 200.7 Rev 4.4 1994
Date:January 24, 2020
Description:200.7 MET ICP
General Information:
10 samples were analyzed for EPA 200.7 Rev 4.4 1994. All samples were received in acceptable condition with any exceptions noted
below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 Rev 4.4 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 70
1-27-2020
Page 15 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 200.7 Rev 4.4 1994
Date:January 24, 2020
Description:200.7 MET ICP, Dissolved
General Information:
11 samples were analyzed for EPA 200.7 Rev 4.4 1994. All samples were received in acceptable condition with any exceptions noted
below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.7 Rev 4.4 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 70
1-27-2020
Page 16 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 200.8 Rev 5.4
Date:January 24, 2020
Description:200.8 MET ICPMS
General Information:
10 samples were analyzed for EPA 200.8 Rev 5.4. All samples were received in acceptable condition with any exceptions noted below
or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.8 Rev 5.4 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 519123
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• ASA_SW-8-A1 (Lab ID: 92460474006)
• Beryllium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 70
1-27-2020
Page 17 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 200.8 Rev 5.4
Date:January 24, 2020
Description:200.8 MET ICPMS, Dissolved
General Information:
11 samples were analyzed for EPA 200.8 Rev 5.4. All samples were received in acceptable condition with any exceptions noted below
or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.8 Rev 5.4 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 70
1-27-2020
Page 18 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 6020B
Date:January 24, 2020
Description:6020 MET ICPMS
General Information:
10 samples were analyzed for EPA 6020B. All samples were received in acceptable condition with any exceptions noted below or on
the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 70
1-27-2020
Page 19 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 6020B
Date:January 24, 2020
Description:6020 MET ICPMS, Dissolved
General Information:
11 samples were analyzed for EPA 6020B. All samples were received in acceptable condition with any exceptions noted below or on
the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 70
1-27-2020
Page 20 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 245.1 Rev 3.0 1994
Date:January 24, 2020
Description:245.1 Mercury
General Information:
10 samples were analyzed for EPA 245.1 Rev 3.0 1994. All samples were received in acceptable condition with any exceptions noted
below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 245.1 Rev 3.0 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 519180
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92459633005,92460064001
R1: RPD value was outside control limits.
• MSD (Lab ID: 2778905)
• Mercury
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 70
1-27-2020
Page 21 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 245.1 Rev 3.0 1994
Date:January 24, 2020
Description:245.1 Mercury, Dissolved
General Information:
11 samples were analyzed for EPA 245.1 Rev 3.0 1994. All samples were received in acceptable condition with any exceptions noted
below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 245.1 Rev 3.0 1994 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 70
1-27-2020
Page 22 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
SM 2320B-2011
Date:January 24, 2020
Description:2320B Alkalinity
General Information:
10 samples were analyzed for SM 2320B-2011. All samples were received in acceptable condition with any exceptions noted below or
on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 70
1-27-2020
Page 23 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
SM 2540C-2011
Date:January 24, 2020
Description:2540C Total Dissolved Solids
General Information:
8 samples were analyzed for SM 2540C-2011. All samples were received in acceptable condition with any exceptions noted below or
on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 70
1-27-2020
Page 24 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
SM 2540D-2011
Date:January 24, 2020
Description:2540D Total Suspended Solids
General Information:
8 samples were analyzed for SM 2540D-2011. All samples were received in acceptable condition with any exceptions noted below or
on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 70
1-27-2020
Page 25 of 71
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Method:
Client:Duke Energy
EPA 300.0 Rev 2.1 1993
Date:January 24, 2020
Description:300.0 IC Anions 28 Days
General Information:
10 samples were analyzed for EPA 300.0 Rev 2.1 1993. All samples were received in acceptable condition with any exceptions noted
below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 519174
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 2627482001,92460474008
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2778880)
• Sulfate
• MSD (Lab ID: 2778881)
• Sulfate
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 70
1-27-2020
Page 26 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-2-A1 Lab ID:92460474001 Collected:01/13/20 15:00 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum ND ug/L 01/15/20 12:23 7429-90-501/14/20 01:461001
Barium 47.4 ug/L 01/15/20 12:23 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 12:23 7440-42-801/14/20 01:4650.0 1
Calcium 6770 ug/L 01/15/20 12:23 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:23 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:23 7440-50-801/14/20 01:465.0 1
Iron 198 ug/L 01/15/20 12:23 7439-89-601/14/20 01:4650.0 1
Magnesium 2720 ug/L 01/15/20 12:23 7439-95-401/14/20 01:461001
Manganese 102 ug/L 01/15/20 12:23 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:23 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:23 7440-09-701/14/20 01:4650001
Sodium 6300 ug/L 01/15/20 12:23 7440-23-501/14/20 01:4650001
Strontium 51.2 ug/L 01/15/20 12:23 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)28100 ug/L 01/15/20 12:2301/14/20 01:466621
Zinc 12.3 ug/L 01/15/20 12:23 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 18:59 7429-90-501/14/20 15:331001
Barium, Dissolved 41.7 ug/L 01/15/20 18:59 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 18:59 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 7320 ug/L 01/15/20 18:59 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 18:59 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 18:59 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 150 ug/L 01/15/20 18:59 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 2700 ug/L 01/15/20 18:59 7439-95-401/14/20 15:331001
Manganese, Dissolved 124 ug/L 01/15/20 18:59 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 18:59 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 18:59 7440-09-701/14/20 15:3350001
Sodium, Dissolved 6360 ug/L 01/15/20 18:59 7440-23-501/14/20 15:3350001
Zinc, Dissolved 12.5 ug/L 01/15/20 18:59 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 48.4 ug/L 01/15/20 18:59 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/15/20 14:33 7440-36-001/14/20 01:580.50 1
Arsenic 0.12 ug/L 01/15/20 14:33 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/15/20 14:33 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/15/20 14:33 7440-43-901/14/20 01:580.080 1
Cobalt 0.30 ug/L 01/15/20 14:33 7440-48-401/14/20 01:580.10 1
Lead 0.26 ug/L 01/15/20 14:33 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/15/20 14:33 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/15/20 14:33 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/15/20 14:33 7440-28-001/14/20 01:580.10 1
Vanadium 0.37 ug/L 01/15/20 14:33 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/17/20 11:23 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 70
1-27-2020
Page 27 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-2-A1 Lab ID:92460474001 Collected:01/13/20 15:00 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/17/20 11:23 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/17/20 11:23 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/17/20 11:23 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/17/20 11:23 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/17/20 11:23 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/17/20 11:23 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/17/20 11:23 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/17/20 11:23 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved 0.36 ug/L 01/17/20 11:23 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 14:33 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/17/20 11:23 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/17/20 11:25 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:12 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)14.6 mg/L 01/15/20 16:465.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 16:465.0 1
Alkalinity, Total as CaCO3 14.6 mg/L 01/15/20 16:465.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 63.0 mg/L 01/15/20 16:3925.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids ND mg/L 01/16/20 12:312.9 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 14.5 mg/L 01/14/20 16:52 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 16:52 16984-48-80.10 1
Sulfate 2.5 mg/L 01/14/20 16:52 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 70
1-27-2020
Page 28 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-3-A1 Lab ID:92460474002 Collected:01/13/20 12:37 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum 353 ug/L 01/15/20 12:32 7429-90-501/14/20 01:461001
Barium 41.6 ug/L 01/15/20 12:32 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 12:32 7440-42-801/14/20 01:4650.0 1
Calcium 9480 ug/L 01/15/20 12:32 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:32 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:32 7440-50-801/14/20 01:465.0 1
Iron 2480 ug/L 01/15/20 12:32 7439-89-601/14/20 01:4650.0 1
Magnesium 3560 ug/L 01/15/20 12:32 7439-95-401/14/20 01:461001
Manganese 479 ug/L 01/15/20 12:32 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:32 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:32 7440-09-701/14/20 01:4650001
Sodium 5230 ug/L 01/15/20 12:32 7440-23-501/14/20 01:4650001
Strontium 85.2 ug/L 01/15/20 12:32 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)38400 ug/L 01/15/20 12:3201/14/20 01:466621
Zinc 10.3 ug/L 01/15/20 12:32 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:09 7429-90-501/14/20 15:331001
Barium, Dissolved 35.1 ug/L 01/15/20 19:09 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:09 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 8540 ug/L 01/15/20 19:09 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:09 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:09 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 1470 ug/L 01/15/20 19:09 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 3280 ug/L 01/15/20 19:09 7439-95-401/14/20 15:331001
Manganese, Dissolved 413 ug/L 01/15/20 19:09 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:09 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:09 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:09 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:09 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 77.3 ug/L 01/15/20 19:09 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/15/20 14:41 7440-36-001/14/20 01:580.50 1
Arsenic 0.33 ug/L 01/15/20 14:41 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/15/20 14:41 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/15/20 14:41 7440-43-901/14/20 01:580.080 1
Cobalt 1.9 ug/L 01/15/20 14:41 7440-48-401/14/20 01:580.10 1
Lead 0.30 ug/L 01/15/20 14:41 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/15/20 14:41 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/15/20 14:41 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/15/20 14:41 7440-28-001/14/20 01:580.10 1
Vanadium 0.71 ug/L 01/15/20 14:41 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/16/20 15:33 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-3-A1 Lab ID:92460474002 Collected:01/13/20 12:37 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/16/20 15:33 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/16/20 15:33 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/16/20 15:33 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/16/20 15:33 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/16/20 15:33 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/16/20 15:33 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/16/20 15:33 7440-28-001/14/20 15:330.10 1
Cobalt, Dissolved 1.6 ug/L 01/16/20 15:33 7440-48-401/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 18:25 7440-62-201/14/20 15:330.30 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 14:41 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/16/20 15:33 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/17/20 11:28 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:19 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)30.8 mg/L 01/15/20 17:055.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 17:055.0 1
Alkalinity, Total as CaCO3 30.8 mg/L 01/15/20 17:055.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 68.0 mg/L 01/15/20 16:3925.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 9.6 mg/L 01/16/20 12:322.5 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 11.5 mg/L 01/14/20 17:06 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 17:06 16984-48-80.10 1
Sulfate 3.5 mg/L 01/14/20 17:06 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 70
1-27-2020
Page 30 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-4B-A1 Lab ID:92460474003 Collected:01/13/20 11:15 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum ND ug/L 01/15/20 12:36 7429-90-501/14/20 01:461001
Barium 21.6 ug/L 01/15/20 12:36 7440-39-301/14/20 01:465.0 1
Boron 111 ug/L 01/15/20 12:36 7440-42-801/14/20 01:4650.0 1
Calcium 6280 ug/L 01/15/20 12:36 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:36 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:36 7440-50-801/14/20 01:465.0 1
Iron 924 ug/L 01/15/20 12:36 7439-89-601/14/20 01:4650.0 1
Magnesium 3420 ug/L 01/15/20 12:36 7439-95-401/14/20 01:461001
Manganese 187 ug/L 01/15/20 12:36 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:36 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:36 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 12:36 7440-23-501/14/20 01:4650001
Strontium 58.8 ug/L 01/15/20 12:36 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)29800 ug/L 01/15/20 12:3601/14/20 01:466621
Zinc ND ug/L 01/15/20 12:36 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:18 7429-90-501/14/20 15:331001
Barium, Dissolved 19.0 ug/L 01/15/20 19:18 7440-39-301/14/20 15:335.0 1
Boron, Dissolved 103 ug/L 01/15/20 19:18 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 5560 ug/L 01/15/20 19:18 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:18 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:18 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 634 ug/L 01/15/20 19:18 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 3120 ug/L 01/15/20 19:18 7439-95-401/14/20 15:331001
Manganese, Dissolved 166 ug/L 01/15/20 19:18 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:18 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:18 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:18 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:18 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 52.6 ug/L 01/15/20 19:18 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/15/20 15:08 7440-36-001/14/20 01:580.50 1
Arsenic 0.12 ug/L 01/15/20 15:08 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/15/20 15:08 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/15/20 15:08 7440-43-901/14/20 01:580.080 1
Cobalt 0.56 ug/L 01/15/20 15:08 7440-48-401/14/20 01:580.10 1
Lead ND ug/L 01/15/20 15:08 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/15/20 15:08 7439-98-701/14/20 01:580.50 1
Selenium 2.3 ug/L 01/15/20 15:08 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/15/20 15:08 7440-28-001/14/20 01:580.10 1
Vanadium ND ug/L 01/15/20 15:08 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/16/20 15:37 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 70
1-27-2020
Page 31 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-4B-A1 Lab ID:92460474003 Collected:01/13/20 11:15 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/16/20 15:37 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/16/20 15:37 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/16/20 15:37 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/16/20 15:37 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/16/20 15:37 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved 2.2 ug/L 01/16/20 15:37 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/16/20 15:37 7440-28-001/14/20 15:330.10 1
Cobalt, Dissolved 0.50 ug/L 01/16/20 15:37 7440-48-401/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 18:48 7440-62-201/14/20 15:330.30 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 15:08 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/16/20 15:37 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/17/20 11:30 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:21 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)23.5 mg/L 01/15/20 17:115.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 17:115.0 1
Alkalinity, Total as CaCO3 23.5 mg/L 01/15/20 17:115.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 35.0 mg/L 01/15/20 16:3925.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids ND mg/L 01/16/20 12:322.6 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 2.8 mg/L 01/14/20 17:20 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 17:20 16984-48-80.10 1
Sulfate 9.3 mg/L 01/14/20 17:20 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 70
1-27-2020
Page 32 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-5-A1 Lab ID:92460474004 Collected:01/13/20 12:17 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum 1590 ug/L 01/15/20 12:39 7429-90-501/14/20 01:461001
Barium 79.2 ug/L 01/15/20 12:39 7440-39-301/14/20 01:465.0 1
Boron 127 ug/L 01/15/20 12:39 7440-42-801/14/20 01:4650.0 1
Calcium 18700 ug/L 01/15/20 12:39 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:39 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:39 7440-50-801/14/20 01:465.0 1
Iron 14800 ug/L 01/15/20 12:39 7439-89-601/14/20 01:4650.0 1
Magnesium 5060 ug/L 01/15/20 12:39 7439-95-401/14/20 01:461001
Manganese 2070 ug/L 01/15/20 12:39 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:39 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:39 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 12:39 7440-23-501/14/20 01:4650001
Strontium 257 ug/L 01/15/20 12:39 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)67400 ug/L 01/15/20 12:3901/14/20 01:466621
Zinc 31.6 ug/L 01/15/20 12:39 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:21 7429-90-501/14/20 15:331001
Barium, Dissolved 30.6 ug/L 01/15/20 19:21 7440-39-301/14/20 15:335.0 1
Boron, Dissolved 117 ug/L 01/15/20 19:21 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 16700 ug/L 01/15/20 19:21 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:21 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:21 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 341 ug/L 01/15/20 19:21 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 4640 ug/L 01/15/20 19:21 7439-95-401/14/20 15:331001
Manganese, Dissolved 498 ug/L 01/15/20 19:21 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:21 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:21 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:21 7440-23-501/14/20 15:3350001
Zinc, Dissolved 10.6 ug/L 01/15/20 19:21 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 228 ug/L 01/15/20 19:21 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/16/20 14:51 7440-36-001/14/20 01:580.50 1
Arsenic 2.5 ug/L 01/16/20 14:51 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/16/20 14:51 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/16/20 14:51 7440-43-901/14/20 01:580.080 1
Cobalt 4.3 ug/L 01/16/20 14:51 7440-48-401/14/20 01:580.10 1
Lead 1.0 ug/L 01/16/20 14:51 7439-92-101/14/20 01:580.10 1
Molybdenum 6.7 ug/L 01/16/20 14:51 7439-98-701/14/20 01:580.50 1
Selenium 0.61 ug/L 01/16/20 14:51 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/16/20 14:51 7440-28-001/14/20 01:580.10 1
Vanadium 1.9 ug/L 01/15/20 17:22 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved 0.27 ug/L 01/16/20 15:41 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 70
1-27-2020
Page 33 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-5-A1 Lab ID:92460474004 Collected:01/13/20 12:17 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/16/20 15:41 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/16/20 15:41 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved 2.6 ug/L 01/16/20 15:41 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/16/20 15:41 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/16/20 15:41 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/16/20 15:41 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/16/20 15:41 7440-28-001/14/20 15:330.10 1
Cobalt, Dissolved 0.82 ug/L 01/16/20 15:41 7440-48-401/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 19:07 7440-62-201/14/20 15:330.30 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium 2.9 ug/L 01/16/20 14:51 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/16/20 15:41 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:29 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:24 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)69.0 mg/L 01/15/20 17:185.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 17:185.0 1
Alkalinity, Total as CaCO3 69.0 mg/L 01/15/20 17:185.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 96.0 mg/L 01/15/20 16:4025.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 20.3 mg/L 01/16/20 12:324.2 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 5.6 mg/L 01/14/20 17:34 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 17:34 16984-48-80.10 1
Sulfate 4.5 mg/L 01/14/20 17:34 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 70
1-27-2020
Page 34 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-6-A1 Lab ID:92460474005 Collected:01/13/20 13:15 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum ND ug/L 01/15/20 12:42 7429-90-501/14/20 01:461001
Barium 19.0 ug/L 01/15/20 12:42 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 12:42 7440-42-801/14/20 01:4650.0 1
Calcium 8780 ug/L 01/15/20 12:42 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:42 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:42 7440-50-801/14/20 01:465.0 1
Iron 2790 ug/L 01/15/20 12:42 7439-89-601/14/20 01:4650.0 1
Magnesium 3420 ug/L 01/15/20 12:42 7439-95-401/14/20 01:461001
Manganese 550 ug/L 01/15/20 12:42 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:42 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:42 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 12:42 7440-23-501/14/20 01:4650001
Strontium 41.2 ug/L 01/15/20 12:42 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)36000 ug/L 01/15/20 12:4201/14/20 01:466621
Zinc ND ug/L 01/15/20 12:42 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:25 7429-90-501/14/20 15:331001
Barium, Dissolved 16.8 ug/L 01/15/20 19:25 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:25 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 7910 ug/L 01/15/20 19:25 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:25 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:25 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 288 ug/L 01/15/20 19:25 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 3170 ug/L 01/15/20 19:25 7439-95-401/14/20 15:331001
Manganese, Dissolved 495 ug/L 01/15/20 19:25 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:25 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:25 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:25 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:25 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 37.2 ug/L 01/15/20 19:25 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/17/20 12:25 7440-36-001/14/20 01:580.50 1
Arsenic 0.32 ug/L 01/17/20 12:25 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/17/20 12:25 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/17/20 12:25 7440-43-901/14/20 01:580.080 1
Cobalt 1.5 ug/L 01/17/20 12:25 7440-48-401/14/20 01:580.10 1
Lead ND ug/L 01/17/20 12:25 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/17/20 12:25 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/17/20 12:25 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/17/20 12:25 7440-28-001/14/20 01:580.10 1
Vanadium ND ug/L 01/17/20 12:25 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Vanadium, Dissolved ND ug/L 01/15/20 19:19 7440-62-201/14/20 15:330.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 70
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Page 35 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-6-A1 Lab ID:92460474005 Collected:01/13/20 13:15 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved 0.16 ug/L 01/16/20 15:45 7440-38-201/14/20 15:330.10 1
Beryllium, Dissolved ND ug/L 01/16/20 15:45 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/16/20 15:45 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/16/20 15:45 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/16/20 15:45 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/16/20 15:45 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/16/20 15:45 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/16/20 15:45 7440-28-001/14/20 15:330.10 1
Cobalt, Dissolved 1.4 ug/L 01/16/20 15:45 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/16/20 16:32 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/16/20 15:45 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:32 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:26 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)34.2 mg/L 01/15/20 17:275.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 17:275.0 1
Alkalinity, Total as CaCO3 34.2 mg/L 01/15/20 17:275.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 50.0 mg/L 01/15/20 16:4025.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids ND mg/L 01/16/20 12:328.3 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 5.2 mg/L 01/14/20 17:48 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 17:48 16984-48-80.10 1
Sulfate 5.1 mg/L 01/14/20 17:48 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 70
1-27-2020
Page 36 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-8-A1 Lab ID:92460474006 Collected:01/13/20 10:36 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum 4740 ug/L 01/15/20 12:45 7429-90-501/14/20 01:461001
Barium 228 ug/L 01/15/20 12:45 7440-39-301/14/20 01:465.0 1
Boron 1100 ug/L 01/15/20 12:45 7440-42-801/14/20 01:4650.0 1
Calcium 131000 ug/L 01/16/20 19:04 7440-70-201/14/20 01:465005
Chromium ND ug/L 01/15/20 12:45 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:45 7440-50-801/14/20 01:465.0 1
Iron 20600 ug/L 01/15/20 12:45 7439-89-601/14/20 01:4650.0 1
Magnesium 27200 ug/L 01/15/20 12:45 7439-95-401/14/20 01:461001
Manganese 6230 ug/L 01/15/20 12:45 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:45 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:45 7440-09-701/14/20 01:4650001
Sodium 5940 ug/L 01/15/20 12:45 7440-23-501/14/20 01:4650001
Strontium 2020 ug/L 01/15/20 12:45 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)439000 ug/L 01/16/20 19:0401/14/20 01:4633105
Zinc 10.7 ug/L 01/15/20 12:45 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Calcium, Dissolved 118000 ug/L 01/16/20 18:42 7440-70-201/14/20 15:335005
Aluminum, Dissolved ND ug/L 01/15/20 19:28 7429-90-501/14/20 15:331001
Barium, Dissolved 146 ug/L 01/15/20 19:28 7440-39-301/14/20 15:335.0 1
Boron, Dissolved 992 ug/L 01/15/20 19:28 7440-42-801/14/20 15:3350.0 1
Chromium, Dissolved ND ug/L 01/15/20 19:28 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:28 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 9770 ug/L 01/15/20 19:28 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 25100 ug/L 01/15/20 19:28 7439-95-401/14/20 15:331001
Manganese, Dissolved 6100 ug/L 01/15/20 19:28 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:28 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:28 7440-09-701/14/20 15:3350001
Sodium, Dissolved 5570 ug/L 01/15/20 19:28 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:28 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 1890 ug/L 01/15/20 19:28 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/14/20 18:30 7440-36-001/14/20 01:580.50 1
Arsenic 290 ug/L 01/14/20 18:30 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/17/20 12:29 7440-41-7 D301/14/20 01:580.50 5
Cadmium ND ug/L 01/14/20 18:30 7440-43-901/14/20 01:580.080 1
Cobalt 13.4 ug/L 01/17/20 12:29 7440-48-401/14/20 01:580.50 5
Lead 2.0 ug/L 01/14/20 18:30 7439-92-101/14/20 01:580.10 1
Molybdenum 79.3 ug/L 01/14/20 18:30 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/14/20 18:30 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/14/20 18:30 7440-28-001/14/20 01:580.10 1
Vanadium 3.0 ug/L 01/17/20 12:29 7440-62-201/14/20 01:581.5 5
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Molybdenum, Dissolved 73.7 ug/L 01/16/20 15:49 7439-98-701/14/20 15:335.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 70
1-27-2020
Page 37 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-8-A1 Lab ID:92460474006 Collected:01/13/20 10:36 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Cobalt, Dissolved 10.6 ug/L 01/16/20 15:49 7440-48-401/14/20 15:331.0 10
Arsenic, Dissolved 229 ug/L 01/15/20 19:31 7440-38-201/14/20 15:330.10 1
Beryllium, Dissolved ND ug/L 01/15/20 19:31 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/15/20 19:31 7440-43-901/14/20 15:330.080 1
Lead, Dissolved ND ug/L 01/15/20 19:31 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/15/20 19:31 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/15/20 19:31 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/15/20 19:31 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 19:31 7440-62-201/14/20 15:330.30 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium 38.1 ug/L 01/15/20 17:38 7439-93-201/14/20 01:5812.5 5
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved 33.9 ug/L 01/16/20 15:49 7439-93-201/14/20 15:3325.0 10
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:34 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:28 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)438 mg/L 01/15/20 17:345.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 17:345.0 1
Alkalinity, Total as CaCO3 438 mg/L 01/15/20 17:345.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 479 mg/L 01/15/20 16:4025.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 221 mg/L 01/16/20 12:3216.7 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 3.7 mg/L 01/14/20 18:02 16887-00-61.0 1
Fluoride 0.50 mg/L 01/14/20 18:02 16984-48-80.10 1
Sulfate 28.9 mg/L 01/14/20 18:02 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 70
1-27-2020
Page 38 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-9-A1 Lab ID:92460474007 Collected:01/13/20 11:25 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum 1040 ug/L 01/15/20 12:48 7429-90-501/14/20 01:461001
Barium 53.0 ug/L 01/15/20 12:48 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 12:48 7440-42-801/14/20 01:4650.0 1
Calcium 9920 ug/L 01/15/20 12:48 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:48 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:48 7440-50-801/14/20 01:465.0 1
Iron 5970 ug/L 01/15/20 12:48 7439-89-601/14/20 01:4650.0 1
Magnesium 4000 ug/L 01/15/20 12:48 7439-95-401/14/20 01:461001
Manganese 739 ug/L 01/15/20 12:48 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:48 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:48 7440-09-701/14/20 01:4650001
Sodium 5790 ug/L 01/15/20 12:48 7440-23-501/14/20 01:4650001
Strontium 77.4 ug/L 01/15/20 12:48 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)41300 ug/L 01/15/20 12:4801/14/20 01:466621
Zinc 15.7 ug/L 01/15/20 12:48 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:31 7429-90-501/14/20 15:331001
Barium, Dissolved 40.8 ug/L 01/15/20 19:31 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:31 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 8740 ug/L 01/15/20 19:31 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:31 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:31 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 3740 ug/L 01/15/20 19:31 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 3550 ug/L 01/15/20 19:31 7439-95-401/14/20 15:331001
Manganese, Dissolved 581 ug/L 01/15/20 19:31 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:31 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:31 7440-09-701/14/20 15:3350001
Sodium, Dissolved 5480 ug/L 01/15/20 19:31 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:31 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 70.4 ug/L 01/15/20 19:31 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/17/20 12:33 7440-36-001/14/20 01:580.50 1
Arsenic 0.39 ug/L 01/17/20 12:33 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/17/20 12:33 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/17/20 12:33 7440-43-901/14/20 01:580.080 1
Cobalt 3.6 ug/L 01/17/20 12:33 7440-48-401/14/20 01:580.10 1
Lead 0.85 ug/L 01/17/20 12:33 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/17/20 12:33 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/17/20 12:33 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/17/20 12:33 7440-28-001/14/20 01:580.10 1
Vanadium 1.6 ug/L 01/17/20 12:33 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved 0.10 ug/L 01/17/20 11:27 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 70
1-27-2020
Page 39 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-9-A1 Lab ID:92460474007 Collected:01/13/20 11:25 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/17/20 11:27 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/17/20 11:27 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/17/20 11:27 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/17/20 11:27 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/17/20 11:27 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/17/20 11:27 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/17/20 11:27 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/17/20 11:27 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved 2.5 ug/L 01/17/20 11:27 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 17:46 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/17/20 11:27 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:36 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:36 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)30.8 mg/L 01/15/20 18:075.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 18:075.0 1
Alkalinity, Total as CaCO3 30.8 mg/L 01/15/20 18:075.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 75.0 mg/L 01/15/20 16:4025.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 30.3 mg/L 01/16/20 12:324.2 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 13.1 mg/L 01/14/20 18:16 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 18:16 16984-48-80.10 1
Sulfate 4.3 mg/L 01/14/20 18:16 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 70
1-27-2020
Page 40 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-4C-A1 Lab ID:92460474008 Collected:01/13/20 11:02 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum 598 ug/L 01/15/20 12:51 7429-90-501/14/20 01:461001
Barium 48.8 ug/L 01/15/20 12:51 7440-39-301/14/20 01:465.0 1
Boron 108 ug/L 01/15/20 12:51 7440-42-801/14/20 01:4650.0 1
Calcium 14800 ug/L 01/15/20 12:51 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 12:51 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 12:51 7440-50-801/14/20 01:465.0 1
Iron 15500 ug/L 01/15/20 12:51 7439-89-601/14/20 01:4650.0 1
Magnesium 6830 ug/L 01/15/20 12:51 7439-95-401/14/20 01:461001
Manganese 1930 ug/L 01/15/20 12:51 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 12:51 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 12:51 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 12:51 7440-23-501/14/20 01:4650001
Strontium 150 ug/L 01/15/20 12:51 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)65000 ug/L 01/15/20 12:5101/14/20 01:466621
Zinc ND ug/L 01/15/20 12:51 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:34 7429-90-501/14/20 15:331001
Barium, Dissolved 40.0 ug/L 01/15/20 19:34 7440-39-301/14/20 15:335.0 1
Boron, Dissolved 97.6 ug/L 01/15/20 19:34 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved 13100 ug/L 01/15/20 19:34 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:34 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:34 7440-50-801/14/20 15:335.0 1
Iron, Dissolved 13300 ug/L 01/15/20 19:34 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved 6170 ug/L 01/15/20 19:34 7439-95-401/14/20 15:331001
Manganese, Dissolved 1740 ug/L 01/15/20 19:34 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:34 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:34 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:34 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:34 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved 135 ug/L 01/15/20 19:34 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/16/20 14:54 7440-36-001/14/20 01:580.50 1
Arsenic 0.39 ug/L 01/16/20 14:54 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/16/20 14:54 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/16/20 14:54 7440-43-901/14/20 01:580.080 1
Cobalt 8.7 ug/L 01/16/20 14:54 7440-48-401/14/20 01:580.10 1
Lead 0.35 ug/L 01/16/20 14:54 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/16/20 14:54 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/16/20 14:54 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/16/20 14:54 7440-28-001/14/20 01:580.10 1
Vanadium 0.70 ug/L 01/15/20 17:53 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved 0.22 ug/L 01/17/20 11:31 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 70
1-27-2020
Page 41 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_SW-4C-A1 Lab ID:92460474008 Collected:01/13/20 11:02 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/17/20 11:31 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/17/20 11:31 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/17/20 11:31 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/17/20 11:31 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/17/20 11:31 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/17/20 11:31 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/17/20 11:31 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/17/20 11:31 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved 8.3 ug/L 01/17/20 11:31 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/16/20 14:54 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/17/20 11:31 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:39 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:38 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)59.0 mg/L 01/15/20 18:145.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 18:145.0 1
Alkalinity, Total as CaCO3 59.0 mg/L 01/15/20 18:145.0 1
Analytical Method: SM 2540C-20112540C Total Dissolved Solids
Total Dissolved Solids 105 mg/L 01/15/20 16:4025.0 1
Analytical Method: SM 2540D-20112540D Total Suspended Solids
Total Suspended Solids 45.8 mg/L 01/16/20 12:336.2 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 11.6 mg/L 01/14/20 18:58 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 18:58 16984-48-80.10 1
Sulfate 7.6 mg/L 01/14/20 18:58 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 70
1-27-2020
Page 42 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_FTB-20200113-1455 Lab ID:92460474009 Collected:01/13/20 14:55 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:37 7429-90-501/14/20 15:331001
Barium, Dissolved ND ug/L 01/15/20 19:37 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:37 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved ND ug/L 01/15/20 19:37 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:37 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:37 7440-50-801/14/20 15:335.0 1
Iron, Dissolved ND ug/L 01/15/20 19:37 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved ND ug/L 01/15/20 19:37 7439-95-401/14/20 15:331001
Manganese, Dissolved ND ug/L 01/15/20 19:37 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:37 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:37 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:37 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:37 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved ND ug/L 01/15/20 19:37 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/15/20 12:38 7440-38-201/14/20 15:330.10 1
Beryllium, Dissolved ND ug/L 01/15/20 12:38 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/15/20 12:38 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/15/20 12:38 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/15/20 12:38 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/15/20 12:38 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/15/20 12:38 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/15/20 12:38 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 12:38 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved ND ug/L 01/15/20 12:38 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/15/20 12:38 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:40 7439-97-601/14/20 11:550.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 70
1-27-2020
Page 43 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_EB-20200113-1449 Lab ID:92460474010 Collected:01/13/20 14:49 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum ND ug/L 01/15/20 13:07 7429-90-501/14/20 01:461001
Barium ND ug/L 01/15/20 13:07 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 13:07 7440-42-801/14/20 01:4650.0 1
Calcium ND ug/L 01/15/20 13:07 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 13:07 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 13:07 7440-50-801/14/20 01:465.0 1
Iron ND ug/L 01/15/20 13:07 7439-89-601/14/20 01:4650.0 1
Magnesium ND ug/L 01/15/20 13:07 7439-95-401/14/20 01:461001
Manganese ND ug/L 01/15/20 13:07 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 13:07 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 13:07 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 13:07 7440-23-501/14/20 01:4650001
Strontium ND ug/L 01/15/20 13:07 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)ND ug/L 01/15/20 13:0701/14/20 01:466621
Zinc ND ug/L 01/15/20 13:07 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:40 7429-90-501/14/20 15:331001
Barium, Dissolved ND ug/L 01/15/20 19:40 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:40 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved ND ug/L 01/15/20 19:40 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:40 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:40 7440-50-801/14/20 15:335.0 1
Iron, Dissolved ND ug/L 01/15/20 19:40 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved ND ug/L 01/15/20 19:40 7439-95-401/14/20 15:331001
Manganese, Dissolved ND ug/L 01/15/20 19:40 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:40 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:40 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:40 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:40 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved ND ug/L 01/15/20 19:40 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/15/20 12:18 7440-36-001/14/20 01:580.50 1
Arsenic ND ug/L 01/15/20 12:18 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/15/20 12:18 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/15/20 12:18 7440-43-901/14/20 01:580.080 1
Cobalt ND ug/L 01/15/20 12:18 7440-48-401/14/20 01:580.10 1
Lead ND ug/L 01/15/20 12:18 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/15/20 12:18 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/15/20 12:18 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/15/20 12:18 7440-28-001/14/20 01:580.10 1
Vanadium ND ug/L 01/15/20 12:18 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/15/20 12:41 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 70
1-27-2020
Page 44 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_EB-20200113-1449 Lab ID:92460474010 Collected:01/13/20 14:49 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/15/20 12:41 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/15/20 12:41 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/15/20 12:41 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/15/20 12:41 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/15/20 12:41 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/15/20 12:41 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/15/20 12:41 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 12:41 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved ND ug/L 01/15/20 12:41 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 12:18 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/15/20 12:41 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 13:41 7439-97-601/14/20 11:550.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:43 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)ND mg/L 01/15/20 18:235.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 18:235.0 1
Alkalinity, Total as CaCO3 ND mg/L 01/15/20 18:235.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride ND mg/L 01/14/20 19:40 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 19:40 16984-48-80.10 1
Sulfate ND mg/L 01/14/20 19:40 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 70
1-27-2020
Page 45 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_FB-20200113-1445 Lab ID:92460474011 Collected:01/13/20 14:45 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP
Aluminum ND ug/L 01/15/20 13:10 7429-90-501/14/20 01:461001
Barium ND ug/L 01/15/20 13:10 7440-39-301/14/20 01:465.0 1
Boron ND ug/L 01/15/20 13:10 7440-42-801/14/20 01:4650.0 1
Calcium ND ug/L 01/15/20 13:10 7440-70-201/14/20 01:461001
Chromium ND ug/L 01/15/20 13:10 7440-47-301/14/20 01:465.0 1
Copper ND ug/L 01/15/20 13:10 7440-50-801/14/20 01:465.0 1
Iron ND ug/L 01/15/20 13:10 7439-89-601/14/20 01:4650.0 1
Magnesium ND ug/L 01/15/20 13:10 7439-95-401/14/20 01:461001
Manganese ND ug/L 01/15/20 13:10 7439-96-501/14/20 01:465.0 1
Nickel ND ug/L 01/15/20 13:10 7440-02-001/14/20 01:465.0 1
Potassium ND ug/L 01/15/20 13:10 7440-09-701/14/20 01:4650001
Sodium ND ug/L 01/15/20 13:10 7440-23-501/14/20 01:4650001
Strontium ND ug/L 01/15/20 13:10 7440-24-601/14/20 01:465.0 1
Hardness, Total(SM 2340B)ND ug/L 01/15/20 13:1001/14/20 01:466621
Zinc ND ug/L 01/15/20 13:10 7440-66-601/14/20 01:4610.0 1
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994200.7 MET ICP, Dissolved
Aluminum, Dissolved ND ug/L 01/15/20 19:43 7429-90-501/14/20 15:331001
Barium, Dissolved ND ug/L 01/15/20 19:43 7440-39-301/14/20 15:335.0 1
Boron, Dissolved ND ug/L 01/15/20 19:43 7440-42-801/14/20 15:3350.0 1
Calcium, Dissolved ND ug/L 01/15/20 19:43 7440-70-201/14/20 15:331001
Chromium, Dissolved ND ug/L 01/15/20 19:43 7440-47-301/14/20 15:335.0 1
Copper, Dissolved ND ug/L 01/15/20 19:43 7440-50-801/14/20 15:335.0 1
Iron, Dissolved ND ug/L 01/15/20 19:43 7439-89-601/14/20 15:3350.0 1
Magnesium, Dissolved ND ug/L 01/15/20 19:43 7439-95-401/14/20 15:331001
Manganese, Dissolved ND ug/L 01/15/20 19:43 7439-96-501/14/20 15:335.0 1
Nickel, Dissolved ND ug/L 01/15/20 19:43 7440-02-001/14/20 15:335.0 1
Potassium, Dissolved ND ug/L 01/15/20 19:43 7440-09-701/14/20 15:3350001
Sodium, Dissolved ND ug/L 01/15/20 19:43 7440-23-501/14/20 15:3350001
Zinc, Dissolved ND ug/L 01/15/20 19:43 7440-66-601/14/20 15:3310.0 1
Strontium, Dissolved ND ug/L 01/15/20 19:43 7440-24-601/14/20 15:335.0 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS
Antimony ND ug/L 01/15/20 12:22 7440-36-001/14/20 01:580.50 1
Arsenic ND ug/L 01/15/20 12:22 7440-38-201/14/20 01:580.10 1
Beryllium ND ug/L 01/15/20 12:22 7440-41-701/14/20 01:580.10 1
Cadmium ND ug/L 01/15/20 12:22 7440-43-901/14/20 01:580.080 1
Cobalt ND ug/L 01/15/20 12:22 7440-48-401/14/20 01:580.10 1
Lead ND ug/L 01/15/20 12:22 7439-92-101/14/20 01:580.10 1
Molybdenum ND ug/L 01/15/20 12:22 7439-98-701/14/20 01:580.50 1
Selenium ND ug/L 01/15/20 12:22 7782-49-201/14/20 01:580.50 1
Thallium ND ug/L 01/15/20 12:22 7440-28-001/14/20 01:580.10 1
Vanadium ND ug/L 01/15/20 12:22 7440-62-201/14/20 01:580.30 1
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Arsenic, Dissolved ND ug/L 01/15/20 13:01 7440-38-201/14/20 15:330.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 70
1-27-2020
Page 46 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Sample:ASA_FB-20200113-1445 Lab ID:92460474011 Collected:01/13/20 14:45 Received:01/13/20 16:24 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4200.8 MET ICPMS, Dissolved
Beryllium, Dissolved ND ug/L 01/15/20 13:01 7440-41-701/14/20 15:330.10 1
Cadmium, Dissolved ND ug/L 01/15/20 13:01 7440-43-901/14/20 15:330.080 1
Molybdenum, Dissolved ND ug/L 01/15/20 13:01 7439-98-701/14/20 15:330.50 1
Lead, Dissolved ND ug/L 01/15/20 13:01 7439-92-101/14/20 15:330.10 1
Antimony, Dissolved ND ug/L 01/15/20 13:01 7440-36-001/14/20 15:330.50 1
Selenium, Dissolved ND ug/L 01/15/20 13:01 7782-49-201/14/20 15:330.50 1
Thallium, Dissolved ND ug/L 01/15/20 13:01 7440-28-001/14/20 15:330.10 1
Vanadium, Dissolved ND ug/L 01/15/20 13:01 7440-62-201/14/20 15:330.30 1
Cobalt, Dissolved ND ug/L 01/15/20 13:01 7440-48-401/14/20 15:330.10 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS
Lithium ND ug/L 01/15/20 12:22 7439-93-201/14/20 01:582.5 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A6020 MET ICPMS, Dissolved
Lithium, Dissolved ND ug/L 01/15/20 13:01 7439-93-201/14/20 15:332.5 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury
Mercury ND ug/L 01/15/20 15:04 7439-97-601/14/20 12:050.20 1
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994245.1 Mercury, Dissolved
Mercury, Dissolved ND ug/L 01/15/20 14:45 7439-97-601/14/20 11:550.20 1
Analytical Method: SM 2320B-20112320B Alkalinity
Alkalinity,Bicarbonate (CaCO3)ND mg/L 01/15/20 18:285.0 1
Alkalinity,Carbonate (CaCO3)ND mg/L 01/15/20 18:285.0 1
Alkalinity, Total as CaCO3 ND mg/L 01/15/20 18:285.0 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride ND mg/L 01/14/20 19:54 16887-00-61.0 1
Fluoride ND mg/L 01/14/20 19:54 16984-48-80.10 1
Sulfate ND mg/L 01/14/20 19:54 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 70
1-27-2020
Page 47 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519180
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
245.1 Mercury
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778900
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 01/15/20 11:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778901LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 108 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778902MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460064001
2778903
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 107 70-130103 3 202.5ND 2.7 2.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92459633005
2778905
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L R12.5 85 70-130107 23 202.5ND 2.1 2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 70
1-27-2020
Page 48 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519181
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
245.1 Mercury
Associated Lab Samples:92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778906
Associated Lab Samples:92460474011
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 01/15/20 14:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778907LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778908MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474011
2778909
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 95 70-130104 8 202.5ND 2.4 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 70
1-27-2020
Page 49 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519179
EPA 245.1 Rev 3.0 1994
EPA 245.1 Rev 3.0 1994
245.1 Mercury - Dissolved
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778894
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Matrix:Water
Analyzed
Mercury, Dissolved ug/L ND 0.20 01/15/20 14:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778895LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury, Dissolved ug/L 2.72.5 106 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778896MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474001
2778897
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 102 70-130104 2 252.5ND 2.5 2.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778898MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2778899
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury, Dissolved ug/L 2.5 103 70-130106 2 252.5ND 2.6 2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 70
1-27-2020
Page 50 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519119
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778730
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Matrix:Water
Analyzed
Aluminum ug/L ND 100 01/15/20 12:10
Barium ug/L ND 5.0 01/15/20 12:10
Boron ug/L ND 50.0 01/15/20 12:10
Calcium ug/L ND 100 01/15/20 12:10
Chromium ug/L ND 5.0 01/15/20 12:10
Copper ug/L ND 5.0 01/15/20 12:10
Hardness, Total(SM 2340B)ug/L ND 662 01/15/20 12:10
Iron ug/L ND 50.0 01/15/20 12:10
Magnesium ug/L ND 100 01/15/20 12:10
Manganese ug/L ND 5.0 01/15/20 12:10
Nickel ug/L ND 5.0 01/15/20 12:10
Potassium ug/L ND 5000 01/15/20 12:10
Sodium ug/L ND 5000 01/15/20 12:10
Strontium ug/L ND 5.0 01/15/20 12:10
Zinc ug/L ND 10.0 01/15/20 12:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778731LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 46705000 93 85-115
Barium ug/L 478500 96 85-115
Boron ug/L 467500 93 85-115
Calcium ug/L 47005000 94 85-115
Chromium ug/L 470500 94 85-115
Copper ug/L 475500 95 85-115
Hardness, Total(SM 2340B)ug/L 3130033100 95 85-115
Iron ug/L 46805000 94 85-115
Magnesium ug/L 47505000 95 85-115
Manganese ug/L 475500 95 85-115
Nickel ug/L 477500 95 85-115
Potassium ug/L 4930J5000 99 85-115
Sodium ug/L 4870J5000 97 85-115
Strontium ug/L 470500 94 85-115
Zinc ug/L 464500 93 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 70
1-27-2020
Page 51 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778732MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474001
2778733
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 5000 99 70-130100 0 205000ND50205040
Barium ug/L 500 100 70-130100 0 2050047.4 546 548
Boron ug/L 500 102 70-130102 0 20500ND511512
Calcium ug/L 5000 106 70-130107 0 20500067701210012100
Chromium ug/L 500 100 70-130101 1 20500ND500507
Copper ug/L 500 100 70-130100 0 20500ND500502
Hardness, Total(SM 2340B)ug/L 33100 104 70-130103 0 2033100281006250062300
Iron ug/L 5000 99 70-13098 1 20500019851305100
Magnesium ug/L 5000 102 70-130101 1 205000272078407790
Manganese ug/L 500 100 70-13099 0 20500102599599
Nickel ug/L 500 100 70-130101 0 20500ND502504
Potassium ug/L 5000 102 70-130101 1 205000ND66006560
Sodium ug/L 5000 105 70-130104 0 20500063001160011500
Strontium ug/L 500 100 70-130100 0 2050051.2 549 551
Zinc ug/L 500 100 70-130101 1 2050012.3 512 516
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 70
1-27-2020
Page 52 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519284
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET Dissolved
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2779365
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Matrix:Water
Analyzed
Aluminum, Dissolved ug/L ND 100 01/15/20 18:53
Barium, Dissolved ug/L ND 5.0 01/15/20 18:53
Boron, Dissolved ug/L ND 50.0 01/15/20 18:53
Calcium, Dissolved ug/L ND 100 01/15/20 18:53
Chromium, Dissolved ug/L ND 5.0 01/15/20 18:53
Copper, Dissolved ug/L ND 5.0 01/15/20 18:53
Iron, Dissolved ug/L ND 50.0 01/15/20 18:53
Magnesium, Dissolved ug/L ND 100 01/15/20 18:53
Manganese, Dissolved ug/L ND 5.0 01/15/20 18:53
Nickel, Dissolved ug/L ND 5.0 01/15/20 18:53
Potassium, Dissolved ug/L ND 5000 01/15/20 18:53
Sodium, Dissolved ug/L ND 5000 01/15/20 18:53
Strontium, Dissolved ug/L ND 5.0 01/15/20 18:53
Zinc, Dissolved ug/L ND 10.0 01/15/20 18:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2779366LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum, Dissolved ug/L 46105000 92 85-115
Barium, Dissolved ug/L 464500 93 85-115
Boron, Dissolved ug/L 481500 96 85-115
Calcium, Dissolved ug/L 46705000 93 85-115
Chromium, Dissolved ug/L 477500 95 85-115
Copper, Dissolved ug/L 472500 94 85-115
Iron, Dissolved ug/L 45905000 92 85-115
Magnesium, Dissolved ug/L 47805000 96 85-115
Manganese, Dissolved ug/L 475500 95 85-115
Nickel, Dissolved ug/L 479500 96 85-115
Potassium, Dissolved ug/L 4740J5000 95 85-115
Sodium, Dissolved ug/L 4780J5000 96 85-115
Strontium, Dissolved ug/L 467500 93 85-115
Zinc, Dissolved ug/L 479500 96 85-115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 70
1-27-2020
Page 53 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2779367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474001
2779368
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 5000 85 70-13086 1 205000ND42704300
Barium, Dissolved ug/L 500 86 70-13086 0 2050041.7 470 471
Boron, Dissolved ug/L 500 88 70-13089 1 20500ND444450
Calcium, Dissolved ug/L 5000 81 70-13083 1 20500073201140011400
Chromium, Dissolved ug/L 500 87 70-13087 0 20500ND435437
Copper, Dissolved ug/L 500 86 70-13087 1 20500ND434436
Iron, Dissolved ug/L 5000 85 70-13085 1 20500015043904420
Magnesium, Dissolved ug/L 5000 85 70-13087 1 205000270069707050
Manganese, Dissolved ug/L 500 85 70-13087 1 20500124551557
Nickel, Dissolved ug/L 500 88 70-13088 1 20500ND438442
Potassium, Dissolved ug/L 5000 87 70-13087 0 205000ND58605850
Sodium, Dissolved ug/L 5000 82 70-13084 1 20500063601040010600
Strontium, Dissolved ug/L 500 86 70-13086 0 2050048.4 479 480
Zinc, Dissolved ug/L 500 87 70-13088 1 2050012.5 448 451
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2779369MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474011
2779370
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum, Dissolved ug/L 5000 86 70-13087 1 205000ND43204350
Barium, Dissolved ug/L 500 87 70-13088 0 20500ND436438
Boron, Dissolved ug/L 500 90 70-13089 1 20500ND448444
Calcium, Dissolved ug/L 5000 87 70-13087 0 205000ND43604380
Chromium, Dissolved ug/L 500 89 70-13088 2 20500ND447440
Copper, Dissolved ug/L 500 88 70-13087 2 20500ND442433
Iron, Dissolved ug/L 5000 86 70-13087 0 205000ND43104330
Magnesium, Dissolved ug/L 5000 90 70-13088 2 205000ND44804420
Manganese, Dissolved ug/L 500 89 70-13088 2 20500ND446439
Nickel, Dissolved ug/L 500 89 70-13090 0 20500ND447448
Potassium, Dissolved ug/L 5000 89 70-13088 205000ND4430J4400J
Sodium, Dissolved ug/L 5000 89 70-13089 205000ND4450J4470J
Strontium, Dissolved ug/L 500 87 70-13087 0 20500ND437436
Zinc, Dissolved ug/L 500 89 70-13091 2 20500ND446454
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 70
1-27-2020
Page 54 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519123
EPA 200.8 Rev 5.4
EPA 200.8 Rev 5.4
200.8 MET
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778752
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Matrix:Water
Analyzed
Antimony ug/L ND 0.50 01/15/20 11:23
Arsenic ug/L ND 0.10 01/15/20 11:23
Beryllium ug/L ND 0.10 01/15/20 11:23
Cadmium ug/L ND 0.080 01/15/20 11:23
Cobalt ug/L ND 0.10 01/15/20 11:23
Lead ug/L ND 0.10 01/15/20 11:23
Molybdenum ug/L ND 0.50 01/15/20 11:23
Selenium ug/L ND 0.50 01/15/20 11:23
Thallium ug/L ND 0.10 01/15/20 11:23
Vanadium ug/L ND 0.30 01/15/20 11:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778753LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony ug/L 52.550 105 85-115
Arsenic ug/L 9.710 97 85-115
Beryllium ug/L 9.610 96 85-115
Cadmium ug/L 10.210 102 85-115
Cobalt ug/L 10.010 100 85-115
Lead ug/L 51.050 102 85-115
Molybdenum ug/L 50.350 101 85-115
Selenium ug/L 48.650 97 85-115
Thallium ug/L 10.210 102 85-115
Vanadium ug/L 50.650 101 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2778755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 50 103 70-130103 0 2050ND51.6 51.6
Arsenic ug/L 10 96 70-13094 2 20100.33 10 9.7
Beryllium ug/L 10 88 70-13088 0 2010ND8.8 8.9
Cadmium ug/L 10 99 70-130100 1 2010ND1010.0
Cobalt ug/L 10 98 70-13098 0 20101.9 11.7 11.7
Lead ug/L 50 103 70-130103 0 20500.30 51.8 52.0
Molybdenum ug/L 50 100 70-13099 2 2050ND50.5 49.7
Selenium ug/L 50 95 70-13093 1 2050ND47.7 47.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 70
1-27-2020
Page 55 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2778755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium ug/L 10 105 70-130105 0 2010ND10.5 10.5
Vanadium ug/L 50 99 70-130100 1 20500.71 50.3 50.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 70
1-27-2020
Page 56 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519287
EPA 200.8 Rev 5.4
EPA 200.8 Rev 5.4
200.8 MET Dissolved
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2779391
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Matrix:Water
Analyzed
Antimony, Dissolved ug/L ND 0.50 01/15/20 12:30
Arsenic, Dissolved ug/L ND 0.10 01/15/20 12:30
Beryllium, Dissolved ug/L ND 0.10 01/15/20 12:30
Cadmium, Dissolved ug/L ND 0.080 01/15/20 12:30
Cobalt, Dissolved ug/L ND 0.10 01/15/20 12:30
Lead, Dissolved ug/L ND 0.10 01/15/20 12:30
Molybdenum, Dissolved ug/L ND 0.50 01/15/20 12:30
Selenium, Dissolved ug/L ND 0.50 01/15/20 12:30
Thallium, Dissolved ug/L ND 0.10 01/15/20 12:30
Vanadium, Dissolved ug/L ND 0.30 01/15/20 12:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2779392LABORATORY CONTROL SAMPLE:
LCSSpike
Antimony, Dissolved ug/L 50.450 101 85-115
Arsenic, Dissolved ug/L 9.610 96 85-115
Beryllium, Dissolved ug/L 9.610 96 85-115
Cadmium, Dissolved ug/L 10.010 100 85-115
Cobalt, Dissolved ug/L 9.910 99 85-115
Lead, Dissolved ug/L 49.750 99 85-115
Molybdenum, Dissolved ug/L 49.350 99 85-115
Selenium, Dissolved ug/L 49.050 98 85-115
Thallium, Dissolved ug/L 9.910 99 85-115
Vanadium, Dissolved ug/L 49.850 100 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2779393MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2779394
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 50 102 70-130101 1 2050ND51.3 50.8
Arsenic, Dissolved ug/L 10 97 70-13096 1 2010ND9.8 9.7
Beryllium, Dissolved ug/L 10 92 70-13094 2 2010ND9.2 9.4
Cadmium, Dissolved ug/L 10 99 70-13098 1 2010ND9.9 9.8
Cobalt, Dissolved ug/L 10 96 70-13097 0 20101.6 11.2 11.3
Lead, Dissolved ug/L 50 99 70-13099 0 2050ND49.7 49.5
Molybdenum, Dissolved ug/L 50 100 70-13099 1 2050ND50.3 49.7
Selenium, Dissolved ug/L 50 94 70-13096 1 2050ND47.4 48.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2779393MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2779394
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Thallium, Dissolved ug/L 10 96 70-13098 1 2010ND9.7 9.8
Vanadium, Dissolved ug/L 50 98 70-13098 0 2050ND48.9 49.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2779395MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474010
2779396
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony, Dissolved ug/L 50 93 70-13090 4 2050ND46.8 44.9
Arsenic, Dissolved ug/L 10 90 70-13087 4 2010ND9.0 8.7
Beryllium, Dissolved ug/L 10 89 70-13085 4 2010ND8.9 8.5
Cadmium, Dissolved ug/L 10 93 70-13090 4 2010ND9.3 9.0
Cobalt, Dissolved ug/L 10 92 70-13089 4 2010ND9.2 8.9
Lead, Dissolved ug/L 50 93 70-13090 3 2050ND46.6 45.1
Molybdenum, Dissolved ug/L 50 92 70-13087 5 2050ND46.0 43.6
Selenium, Dissolved ug/L 50 90 70-13089 2 2050ND45.2 44.4
Thallium, Dissolved ug/L 10 94 70-13091 3 2010ND9.4 9.1
Vanadium, Dissolved ug/L 50 92 70-13089 4 2050ND46.2 44.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 70
1-27-2020
Page 58 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
521295
EPA 3010A
EPA 6020B
6020 MET
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2788986
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Matrix:Water
Analyzed
Lithium ug/L ND 2.5 01/15/20 11:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2788987LABORATORY CONTROL SAMPLE:
LCSSpike
Lithium ug/L 48.450 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2788988MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2788989
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lithium ug/L 50 89 75-12591 1 2050ND45.5 46.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 70
1-27-2020
Page 59 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
521307
EPA 3010A
EPA 6020B
6020 MET Dissolved
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2789019
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474009, 92460474010, 92460474011
Matrix:Water
Analyzed
Lithium, Dissolved ug/L ND 2.5 01/15/20 12:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2789020LABORATORY CONTROL SAMPLE:
LCSSpike
Lithium, Dissolved ug/L 47.850 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2789021MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474002
2789022
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lithium, Dissolved ug/L 50 95 75-12596 2 2050ND47.9 48.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 70
1-27-2020
Page 60 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519470
SM 2320B-2011
SM 2320B-2011
2320B Alkalinity
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2780041
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Matrix:Water
Analyzed
Alkalinity, Total as CaCO3 mg/L ND 5.0 01/15/20 16:34
Alkalinity,Bicarbonate (CaCO3)mg/L ND 5.0 01/15/20 16:34
Alkalinity,Carbonate (CaCO3)mg/L ND 5.0 01/15/20 16:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2780042LABORATORY CONTROL SAMPLE:
LCSSpike
Alkalinity, Total as CaCO3 mg/L 51.150 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2780043MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474001
2780044
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 80-120100 0 255014.6 64.8 64.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2780045MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460656001
2780046
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Alkalinity, Total as CaCO3 mg/L 50 100 80-12099 1 255018.2 68.2 67.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 70
1-27-2020
Page 61 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519569
SM 2540C-2011
SM 2540C-2011
2540C Total Dissolved Solids
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2780622
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 01/15/20 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2780623LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 248250 99 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92460474001
2780624SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 55.0 14 2563.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92460659001
2780625SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 86.0 14 2575.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 70
1-27-2020
Page 62 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519743
SM 2540D-2011
SM 2540D-2011
2540D Total Suspended Solids
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2781515
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008
Matrix:Water
Analyzed
Total Suspended Solids mg/L ND 2.5 01/16/20 12:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2781516LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 240250 96 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92460764002
2781517SAMPLE DUPLICATE:
Total Suspended Solids mg/L 1210 6 251140
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92460751001
2781518SAMPLE DUPLICATE:
Total Suspended Solids mg/L 154 4 25148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 70
1-27-2020
Page 63 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519174
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2778878
Associated Lab Samples:92460474001, 92460474002, 92460474003, 92460474004, 92460474005, 92460474006, 92460474007,
92460474008, 92460474010, 92460474011
Matrix:Water
Analyzed
Chloride mg/L ND 1.0 01/14/20 12:49
Fluoride mg/L ND 0.10 01/14/20 12:49
Sulfate mg/L ND 1.0 01/14/20 12:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2778879LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 48.450 97 90-110
Fluoride mg/L 2.52.5 102 90-110
Sulfate mg/L 49.050 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778880MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
2627482001
2778881
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 99 90-110102 3 10502.4 51.9 53.4
Fluoride mg/L 2.5 103 90-110106 3 102.50.36 2.9 3.0
Sulfate mg/L M15013690-110138 0 1050210278279
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2778882MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92460474008
2778883
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloride mg/L 50 101 90-110103 1 105011.6 62.3 63.2
Fluoride mg/L 2.5 90 90-11092 2 102.5ND 2.3 2.3
Sulfate mg/L 50 102 90-110104 1 10507.6 58.7 59.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 70
1-27-2020
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92460474001 519119 519135ASA_SW-2-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474002 519119 519135ASA_SW-3-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474003 519119 519135ASA_SW-4B-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474004 519119 519135ASA_SW-5-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474005 519119 519135ASA_SW-6-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474006 519119 519135ASA_SW-8-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474007 519119 519135ASA_SW-9-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474008 519119 519135ASA_SW-4C-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474010 519119 519135ASA_EB-20200113-1449 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474011 519119 519135ASA_FB-20200113-1445 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474001 519284 519341ASA_SW-2-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474002 519284 519341ASA_SW-3-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474003 519284 519341ASA_SW-4B-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474004 519284 519341ASA_SW-5-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474005 519284 519341ASA_SW-6-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474006 519284 519341ASA_SW-8-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474007 519284 519341ASA_SW-9-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474008 519284 519341ASA_SW-4C-A1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474009 519284 519341ASA_FTB-20200113-1455 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474010 519284 519341ASA_EB-20200113-1449 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474011 519284 519341ASA_FB-20200113-1445 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92460474001 519123 519141ASA_SW-2-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474002 519123 519141ASA_SW-3-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474003 519123 519141ASA_SW-4B-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474004 519123 519141ASA_SW-5-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474005 519123 519141ASA_SW-6-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474006 519123 519141ASA_SW-8-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474007 519123 519141ASA_SW-9-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474008 519123 519141ASA_SW-4C-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474010 519123 519141ASA_EB-20200113-1449 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474011 519123 519141ASA_FB-20200113-1445 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474001 519287 519343ASA_SW-2-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474002 519287 519343ASA_SW-3-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474003 519287 519343ASA_SW-4B-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474004 519287 519343ASA_SW-5-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474005 519287 519343ASA_SW-6-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474006 519287 519343ASA_SW-8-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474007 519287 519343ASA_SW-9-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474008 519287 519343ASA_SW-4C-A1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474009 519287 519343ASA_FTB-20200113-1455 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474010 519287 519343ASA_EB-20200113-1449 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474011 519287 519343ASA_FB-20200113-1445 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4
92460474001 521295 521305ASA_SW-2-A1 EPA 3010A EPA 6020B
92460474002 521295 521305ASA_SW-3-A1 EPA 3010A EPA 6020B
92460474003 521295 521305ASA_SW-4B-A1 EPA 3010A EPA 6020B
92460474004 521295 521305ASA_SW-5-A1 EPA 3010A EPA 6020B
92460474005 521295 521305ASA_SW-6-A1 EPA 3010A EPA 6020B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 70
1-27-2020
Page 66 of 71
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92460474006 521295 521305ASA_SW-8-A1 EPA 3010A EPA 6020B
92460474007 521295 521305ASA_SW-9-A1 EPA 3010A EPA 6020B
92460474008 521295 521305ASA_SW-4C-A1 EPA 3010A EPA 6020B
92460474010 521295 521305ASA_EB-20200113-1449 EPA 3010A EPA 6020B
92460474011 521295 521305ASA_FB-20200113-1445 EPA 3010A EPA 6020B
92460474001 521307 521308ASA_SW-2-A1 EPA 3010A EPA 6020B
92460474002 521307 521308ASA_SW-3-A1 EPA 3010A EPA 6020B
92460474003 521307 521308ASA_SW-4B-A1 EPA 3010A EPA 6020B
92460474004 521307 521308ASA_SW-5-A1 EPA 3010A EPA 6020B
92460474005 521307 521308ASA_SW-6-A1 EPA 3010A EPA 6020B
92460474006 521307 521308ASA_SW-8-A1 EPA 3010A EPA 6020B
92460474007 521307 521308ASA_SW-9-A1 EPA 3010A EPA 6020B
92460474008 521307 521308ASA_SW-4C-A1 EPA 3010A EPA 6020B
92460474009 521307 521308ASA_FTB-20200113-1455 EPA 3010A EPA 6020B
92460474010 521307 521308ASA_EB-20200113-1449 EPA 3010A EPA 6020B
92460474011 521307 521308ASA_FB-20200113-1445 EPA 3010A EPA 6020B
92460474001 519180 519264ASA_SW-2-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474002 519180 519264ASA_SW-3-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474003 519180 519264ASA_SW-4B-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474004 519180 519264ASA_SW-5-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474005 519180 519264ASA_SW-6-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474006 519180 519264ASA_SW-8-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474007 519180 519264ASA_SW-9-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474008 519180 519264ASA_SW-4C-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474010 519180 519264ASA_EB-20200113-1449 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474011 519181 519259ASA_FB-20200113-1445 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474001 519179 519263ASA_SW-2-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474002 519179 519263ASA_SW-3-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474003 519179 519263ASA_SW-4B-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474004 519179 519263ASA_SW-5-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474005 519179 519263ASA_SW-6-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474006 519179 519263ASA_SW-8-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474007 519179 519263ASA_SW-9-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474008 519179 519263ASA_SW-4C-A1 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474009 519179 519263ASA_FTB-20200113-1455 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474010 519179 519263ASA_EB-20200113-1449 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474011 519179 519263ASA_FB-20200113-1445 EPA 245.1 Rev 3.0 1994 EPA 245.1 Rev 3.0 1994
92460474001 519470ASA_SW-2-A1 SM 2320B-2011
92460474002 519470ASA_SW-3-A1 SM 2320B-2011
92460474003 519470ASA_SW-4B-A1 SM 2320B-2011
92460474004 519470ASA_SW-5-A1 SM 2320B-2011
92460474005 519470ASA_SW-6-A1 SM 2320B-2011
92460474006 519470ASA_SW-8-A1 SM 2320B-2011
92460474007 519470ASA_SW-9-A1 SM 2320B-2011
92460474008 519470ASA_SW-4C-A1 SM 2320B-2011
92460474010 519470ASA_EB-20200113-1449 SM 2320B-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 70
1-27-2020
Page 67 of 71
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92460474
ASHEVILLE AIRPORT J20010314
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92460474011 519470ASA_FB-20200113-1445 SM 2320B-2011
92460474001 519569ASA_SW-2-A1 SM 2540C-2011
92460474002 519569ASA_SW-3-A1 SM 2540C-2011
92460474003 519569ASA_SW-4B-A1 SM 2540C-2011
92460474004 519569ASA_SW-5-A1 SM 2540C-2011
92460474005 519569ASA_SW-6-A1 SM 2540C-2011
92460474006 519569ASA_SW-8-A1 SM 2540C-2011
92460474007 519569ASA_SW-9-A1 SM 2540C-2011
92460474008 519569ASA_SW-4C-A1 SM 2540C-2011
92460474001 519743ASA_SW-2-A1 SM 2540D-2011
92460474002 519743ASA_SW-3-A1 SM 2540D-2011
92460474003 519743ASA_SW-4B-A1 SM 2540D-2011
92460474004 519743ASA_SW-5-A1 SM 2540D-2011
92460474005 519743ASA_SW-6-A1 SM 2540D-2011
92460474006 519743ASA_SW-8-A1 SM 2540D-2011
92460474007 519743ASA_SW-9-A1 SM 2540D-2011
92460474008 519743ASA_SW-4C-A1 SM 2540D-2011
92460474001 519174ASA_SW-2-A1 EPA 300.0 Rev 2.1 1993
92460474002 519174ASA_SW-3-A1 EPA 300.0 Rev 2.1 1993
92460474003 519174ASA_SW-4B-A1 EPA 300.0 Rev 2.1 1993
92460474004 519174ASA_SW-5-A1 EPA 300.0 Rev 2.1 1993
92460474005 519174ASA_SW-6-A1 EPA 300.0 Rev 2.1 1993
92460474006 519174ASA_SW-8-A1 EPA 300.0 Rev 2.1 1993
92460474007 519174ASA_SW-9-A1 EPA 300.0 Rev 2.1 1993
92460474008 519174ASA_SW-4C-A1 EPA 300.0 Rev 2.1 1993
92460474010 519174ASA_EB-20200113-1449 EPA 300.0 Rev 2.1 1993
92460474011 519174ASA_FB-20200113-1445 EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/24/2020 03:56 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 70
1-27-2020
Page 68 of 71
Page 68 of 70
1-27-2020
Page 69 of 71
Page 69 of 70
1-27-2020
Page 70 of 71
Page 70 of 70 1-27-2020 Page 71 of 71