WQ0041666_Application_20200505

-�Resources, Inc.
Permit Application
For
RECEIVED/NCDEQ/DWR
MAY 0 1 2020
Non -Discharge
Permitting Unit
EMA Resources, inc.
uilford Performance T'extiles WWT P'
Distribution of Class A Residuals
(5031',xempt)
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
April 30, 2020
Phone 336*751*1441 — Fax 336*75191442
755 Yadkinville Road — Mocksville, NC 27028

'M
--Resources, Inc.
April 30, 2020
NC Department of Environmental Quality
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
RE: Permit Application for Distribution of Class A Residuals
EMA Resources, Inc — Guilford Performance Textiles
Mr. Nathanial Thornburg, Unit Supervisor
RECEIVEWDEUDW
MAY 0 1 2020
Non -Discharge
Permitting Unit
EMA Resources, Inc in co-operation with Guilford Performance Textiles is submitting
this DCAR application for approval. You will find included in this permit application the
following: Cover Letter, Distribution of Class A Residuals Form, Program Information,
Residuals Analytical Data, Residuals Information Sheet, Operations & Maintenance Plan,
Residuals Source Certification Form (Guilford Performance Textiles), Vicinity
Map/Aerial Map, Site Plan/Process Flow Diagram and Quantitative Justification. Please
note that each form is supplemented with it accompanying attachments and are clearly
identified in the table of contents.
If you have any questions concerning this application, please contact Roy Whitaker at the
office number listed below or on mobile: [phone].
Respectfully,
EMA Resources, Inc.
Roy L. Whitaker
Director of Business Development/Operations
Phone 336*751*1441 —Fax 336*751*1442
755 Yadkinville Road — Mocksville, NC 27028

FORM DCAR
PROGRAM INFORMATION
RESIDUALS ANALYTICAL DATA
RESIDUALS INFORMATION
SHEET
OPERATIONS &MAINTENANCE
5 PLAN
FORM RSC
s
VICINITY MAP/AERIAL MAP
SITE PLAN/PROCESS FLOW
DIAGRAM
9 QUANTITATIVE JUSTIFICATION
10

State of Nortb Carolina
DWR Department of Environmen'tal Quality
Division of Water Resources
DWIslon of Water Resources 15A NCAC 02T .1100 - DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMIENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instralctions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
perm it application. Unless otherwise noted the Applicant shall submit one original and two copies of the ap lication and
sup)rting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website
General - This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residrials under I5A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. ❑istribution of Class A Residuals (FORM: DCAR 06-16):
❑ Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
❑ The project name should be consistent on the plans, specifications, etc.
rl The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(h .
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit Major Modification'
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245
' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3

D. Grogram Information (All Application Packages)
Provide a narrative explaining the following:
❑ How the materials will be handled and transported from where the residuals were produced to where it will be treated.
0 How the residuals will be processed/treated (attach process flow diagram).
❑ How leachate collection will be handled.
[] Where the residuals will be stored until processed.
❑ How the final product will be distributed (packaging, bulk, etc.)
❑ What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
❑ Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
Name and address of the person who prepared the residual that is sold or given away.
❑ A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
❑ A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
❑ Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a. Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .11081 a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T .I 104(a)(2)(B), including leakage and pressure testing as appropriate.
❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN -- NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104 a .
G. Environmental Assessments (Maybe Required —See 15A NCAC 1C .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. operation and Maintenance Plan (New and Renewal Application Packages)
For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
G] Submit the O&M Plan in accordance with 15A NCAC 02T .I 110 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
(r] Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
0 Safety measures; may include safety training program, manuals, signs, etc.
Spill response plan; including control, containment, remediation, emergency contact information, etc.
Q Inspection plan including the following information;
Names and titles of personnel responsible for conducting the inspections.
Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
[] Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
[] Sampling and monitoring plan including the following information;
Q Names and titles of personnel responsible for conducting the sampling and monitoring.
[] Detailed description of monitoring procedures including parameters to be monitored.
[ l Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3

DWR ...
State of Nortb Carolina
Department of Environmental Quality
Division of Water Resources
d pirfslon of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
1. &PPLICANT INFORMATION:
I . Applicant's name: EMA Resources Inc.
Applicant type: ❑ Individual Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Erik Blankenship. Title: President
Applicant's mailing address: 755 Yadkinville Road
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] Email Address: erik.blankenshi uaemaresourcesinc.com
2- Consultant's name: NA License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State: Zip:
Telephone number: (_) = Email Address:
3. Fee submitted: $810.00 (See Instruction B)
11. PERMIT INFORMATION:
1. Application is for (check all that apply): ® new, ❑ modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: NA
Date of most -recently issued permit: NA
Date of most -recently certified Attachment A (if different than the permit): NA
III. FACILITY INFORMATION:
1. Name of residuals processing facility: EMA Resources, Inc. (Guilford Performance Textiles Residuals)
City: Kenansville State: NC Zip: 28349-
Coordinates: Latitude: 35' 01' 04" Longitude: 77' 51' 32"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
County where facility is located: Duplin
2. Facility contact (person familiar with residuals preparation):
Name: Rov Whitaker Title: Director Business DevelopmenVOperari
Mailing address: 755 Yadkinville Road
City: Mocksville State: NC Zip: 27028-
Telephone number: [phone] E-mail address: [e-mail]
FORM: DCAR 06-16 Page 1 of 3

3 . Is the residual process facility also the generator? 0 Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
¢ _ Length of residuals storage at facility: 90 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1 _ Specify how these residuals will be distributed:
[-1 sold or given away in bags or other containers; E] lawn (bulk); E] home garden (bulk);
Z other (explain); Land application of Bulk Liquid
2.
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
Complete the following if residuals are to be mixed with other materials:
3. Approximate amounts of the residuals received and processed at the facility: 318 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 318 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): 90
6. Does the facility have a stormwater management plan?E] Yes; 0 No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: No runo&
contained in 500-000 allon liquid storage tank
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
IR
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3

ProfCssional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has be -en reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of roy knowledge
the pr-oposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may liave been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
ED Yes 0 No, Explain;
I, Erik Blankenship, President
(Signature Authority's Name PLEASE PRINT) (Title)
attest that this application for EMA Resources, Inc. (Guilford Performance Textiles Residuals)
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: 7, x--/, Aztj _ _ Date: V36l
FORM: DCAR 06-16 Page 3 of 3

Program Information
1. Provide a narrative explaining the following:
a. How will the materials be handled and transported from where the residuals were produced
to where it will be treated?
The residuals are organic solids from the manufacturing process and dyeing operations
of textile cloth. The WWTP treats the process water which accounts for 99+ percent of
the flow and the plant restrooms which is less than 1 % of the flow. The aerobically
digested solids are thickened via a rotary drum thickener and stored in a 500Kgallon
sludge storage basin. All residuals are handled by pumps and pipe lines onsite.
b. How will the residuals be processed/treated (attach process flow diagram).
The residuals are treated via aerobic digestion. See attached flow diagram
c. How will leachate collection be handled? Not Applicable.
d. Where will the residuals be stored until processed?
The residuals will be stored in the 500,000-gallon basin.
e. How will the final product be distributed (packaging)?
The residuals will be delivered to local farmers via 6500-gallon tanker loads. Each load
will be off-loaded to a high flotation applicator for application on a receiver site
(grassland or row crop).
2. Attach a marketability statement detailing destinations and approximate amounts of the final
product to be distributed.
The residuals have major (N, P, K) nutrient value, they have additional micro nutrients that
can be utilized by crops for optimum plant growth. The program will recruit local farmers to
participate in the bulk land application program They will be advised as to the nutrient
value of the residuals, and they will be offered up to one ton of agricultural lime for soil pH
adjustment where soil analysis indicates a need
3. Provide either a label that shall be affixed to the bagged processed residual or an information
sheet that shall be provided to the person who receives the processed residual. The label or
information sheet shall contain, at a minimum, the following information:
Note. Residuals will be distributed through bulk land application of liquid managed by a
contracted land application firm
See Attached Residuals Information Sheet.

a
ceAnalyticaJ
/"'W Cerrterlor Tasting 8 Inrmatbr
ANALYTICAL REPORT
January 21, 2020
EMiA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
L 1178358
01/10/2020
GUILFORD MILLS
Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: /�— a'41�'
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in. f •ll, without writen approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical Nabona: is performed per guidance provided In laborat" standard operating procedures ENV-SOP-MTJL-0G67 and
ENV-SOP-MT.1-0068. Where sampling conducted by the customer, .,esults relate to the accuracy of the informat;on provided.
and as the samples are received.
r3
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
EMA Resources GUILFORD MILLS L1178358 01/21/20 15:50 1 of 22

TABLE OF CONTENTS ONE LAB. NATIONWIDE,
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
F
GUILFORD MILLS L1178358-01
5
Qc: Quality Control Summary
7
En]
Wet Chemistry by Method 9012 B
7
Er
Wet Chemistry by Method 9034-9030B
g
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
Mercury by Method 7470A
11
F11
Metals (ICP) by Method 6010D
12
flAl
Volatile Organic Compounds (GC/MS) by Method 8260D
14
Chlorinated Acid Herbicides (GC) by Method 8151A
16
El
Pesticides (GC) by Method 808113
17
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
18
GI: Glossary of Terms
20
Al: Accreditations & Locations
21
Sr: Sample Chain of Custody
22
ACCOUNT: PROJECT: SDG: DATEfTIME: PAGE:
EMA Resources GUILFORD MILLS L1178358 01/21/20 15:50 2 of 22

SAMPLE SUMMARY
ONE LAB. NA.TION'NIDE. '
GUILFc7RG MILLS L1178358-01 Waste
"4ethod
Preparatloln by Method 1311
PreparaBoEi by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 90349030E
WetChemij" by Method 9045D
Wet Chem1:sty by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GUMS) by Method 8260D
Chlorinatec# Acid Herbicides (GC) by Method 8151A
Pesticides (4GC) by Method 8081E
Semi Volatite Organic Compounds (GC.RNS) by Method 8270E
Collected by
Roy Whittaker
Batch
Dilution Preparation.
date/time
WG141CO79
1 01/13/20 09:07
WG 1410099
1 O1/13120 08:47
WG i411287
1 01/15/20 09:07
WG1411620
1 01/16/20 21:06
WG1412940
1 01/17/2011:00
W G i 413920
1 01/2112012:25
WG1410658
1 01/14/2010:46
WG1410815
1 01/15/20 07:28
WG1410537
1 01114/2018:10
WG1412927
1 01/17/20 08:30
WG1410888
1 01l15/20 06:59
WG14121,88
1 01/16/2010:44
Collected date/time Received date/time
01/09/20 08:00 01/10/20 09:00
Analysis
Analyst
Location
date/time
OIJ13120 09:07
IDW
Mt- Juliet, TN
01/13/20 08:47
BAA
Mt. Juliet, TN
G1J1512013:41
JER
Mt. Juliet, TN
01/16/20 21:06
MJA
Mt. Juliet, TN
0111712012:00
MSP
Mt Juliet, TN
01/21/2012:25
MJA
Mt. Juliet, TN
01/14/20 20:49
TCT
Mt. Juliet, TN
01/15/201C:05
CCE
Mt Juliet, TN
01/1412918:10
BMB
Mt. Juliet, TN
01/17/2019:54
Mr
Mt. Juliet, TN
01/15/2018:06
HMH
Mt. Juliet, TN
01P6/20 20:59
JNJ
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
EMA RescurCe5 GUILFORD MILLS L1178358 01/2V2015:50 3 of 22

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples E
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my E
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. ■
F
Fc
E
Justin Carr a
Project Manager I Al
Project Narrative E
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sufde results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1178358 01/2112015:50 4 of 22

GUILfORD MILLS SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 01/09/20 08:00 L1178358
Prepar-ation by Method 1311
Result Qualifier Prep Batch
31yte
.:LP Extra for
TCLP ZHE Extraction
Fluid 1
Initial pH 7.12
Final pH 5.00
Wet Chemistry by Method 9012 B
date /time
s
A312020 9:07:16 AM
WG1410079
1/13/2020 8:47:14 AM
WG1410099
1/13/2020 9:07:16 AM
WG1410079
1/13/2020 9:07:16 AM
WG1410079
1/13/2020 9:07:16 AM
WG1410079
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 0.250 1 01/15/202013:41 WG1411287
Wet Chemistry by Method 9034-9030B
Result
Analyte mg/kg
Reactive Sulfide ND
Wet Chemistry by Method 9045D
Result Qualifier Dilution Analysis
Analyte su date / time
orrosivity by pH 7.13 TS 0111,712020 12:00
Sample Narrative:
L1178358-01 WG1412940: 7.13 at 22.6C
at Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis
Analyte Deg. I -'date / time
Ignitabiiity DNi at 170 1 01/21!2020122E
Mercury by Method 7470A
Qualifier RDL
mgJkg
25.0
Dilution Analysis
date / time
1 01/16/2020 21:06
Batch
WG1412940
Batch
WG1413920
Batch
WG1411620
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mgA mg/I dare / time
Mercory ND 0.0100 0.20 01/1412,320 20.49 WG1410658
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg!I mg/i mgil date/time
Arsenic NO 0.100 5 1 01/15/202010:05 WG1410815
Barium ND 0.100 100 1 01/15/202010:05 WG1410815
Cadmium ND 0.100 1 1 0 15i202010:05 WG1410815
Chromium ND C.100 5 01115/202O10:05 WG1410815
Lead ND -100 5 1 01;i5i2020'0:05 WG1410815
Selenium ND 0.100 11 01/15/202010:05 WG1410815
Sliver ND C'00 5 1 01/15!2C2C':0:05 WG1410815
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mgil mg/I date / time
7ene ND 0.0500 0.50 01114/202018:10 WG1410537
dcn tetrachicride ND 0.0500 0.50 1 011141202018:10 WG1410537
Chlcrobenzene ND 0.0500 100 1 01114/2020 18:10 WG1410537
Chloroform ND 0.250 6 1 01/14/202018:10 WG1410537
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS 1-1178358 C1,21i20 15:50 5 of 22
Qualifier RDL
mgJkg
25.0
Dilution Analysis
date / time
1 01/16/2020 21:06
Batch
WG1412940
Batch
WG1413920
Batch
WG1411620
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mgA mg/I dare / time
Mercory ND 0.0100 0.20 01/1412,320 20.49 WG1410658
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg!I mg/i mgil date/time
Arsenic NO 0.100 5 1 01/15/202010:05 WG1410815
Barium ND 0.100 100 1 01/15/202010:05 WG1410815
Cadmium ND 0.100 1 1 0 15i202010:05 WG1410815
Chromium ND C.100 5 01115/202O10:05 WG1410815
Lead ND -100 5 1 01;i5i2020'0:05 WG1410815
Selenium ND 0.100 11 01/15/202010:05 WG1410815
Sliver ND C'00 5 1 01/15!2C2C':0:05 WG1410815
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mgil mg/I date / time
7ene ND 0.0500 0.50 01114/202018:10 WG1410537
dcn tetrachicride ND 0.0500 0.50 1 011141202018:10 WG1410537
Chlcrobenzene ND 0.0500 100 1 01114/2020 18:10 WG1410537
Chloroform ND 0.250 6 1 01/14/202018:10 WG1410537
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS 1-1178358 C1,21i20 15:50 5 of 22
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS 1-1178358 C1,21i20 15:50 5 of 22

GUILFORD MILLS SAMPLE RESULTS - 01 ONE LAB.Ne4nONWIDE.
Collected dateitime: 01/09/20 08:00 L1178358
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
^natyte
mg/I
mg/I
mg/1
date / time
-Dichioroethane
ND
0.0500
0.50
1 0104/202016:10
1,1-Dichlor®ethere
ND
0.0500
0.70
1 01114/202018:10
2-Butanorw (MEK)
ND
J3 J4 0.500
200
i 01,1412020 18:10
Tetrachlorcethene
ND
0.0500
0.70
1 01/141202018:10
Trichloroett iene
ND
0.0500
0.50
1 01/14/202018:10
Virryl chlorf&
ND
0.0500
0.20
1 01/14/202018.10
(S) T01uCne-d8
104
80.0-120
01/141202018:10
(S) 4-@rvinoNuorcbenzene
93.8
77.0-126
OV14/202018.10
(S)1,2DfchloToethane{/4
107
70.0-130
OY141202018:10
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL Limit
Dilution Analysis
Analyte
mg/I
mg/I mg?l
da'.e/time
2,4,5-TP (Siivex)
ND
0.00200 1
01:17/202019:54
2,4-D
ND
MUM 10
0117i202019:54
(S)2,4-oichlorophery/Acetic Acid
56.8
14.0-158
011171202019:54
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Analyte
mg/1
mg/I
mg/I
date / time
Crlordane
ND
0.00500
0.03
1 01115/202018:06
Endrin
ND
0.00500
0.02
1 01/15/202018:06
Heptachior
ND
0.00500
0.0080
1 01?15/2C2018:06
Undane
ND
0.00500
0.40
1 CIJ151202018:06
Methoxychlor
ND
0.00500
10
1 0 dl5;202018:06
3phene
ND
0.0100
0.50
1 01115/202018:06
(S) Decochlorobiphenyl
74.6
10.0-128
011151202018:06
(S) Tetrochforo-m-xylene
67.3
10.0-127
OV151202018:06
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Analyte
mgf
mg/I
mg;l
i 4-Dichiorobenzene
ND
0.100
7.50
2,4-Dinitrotoluene
ND
0.100
6.13
Hexachlorobenzve
ND
C.100
0.13
Hexachloro-11,3-hutadive
ND
0.100
0.50
Hexachlaroethane
ND
0.100
3
Nitrobenzene
ND
0.100
2
Pyridine
ND
0.100
5
W-Methyl Phenol
ND
0.100
400
2-Methylphenoi
ND
0.100
201,
Pentachlorophenol
ND
0.100
100
2,4,5-1richlorophenol
ND
0100
400
2,4,61richlorophenol
ND
0?00
2
/S) 2-Fluorophencl
31.6
10.0-120
!S) Phenol-d5
19.0
10.0-120
lS) Nitrobenzene-15
51.0
10.0-127
(5) 2-Fluorobipheryl
67.2
10.0-130
rS) 2,4,6-Whromooherol
65.5
10.0-155
(S) p-Terphenyl-di4
69.5
10.0-128
Dilution
1
1
1
1
1
1
1
1
1
i
Analysis
date; time
01i16/2020 20:59
01i1612020 20:59
31/16/2020 20:59
01/16/2020 20:59
01/1612020 20:59
01/16/2020 20:59
01'16/2020 20:59
01116/2020 20:59
01/16/2020 20:59
01/16/2020 20:59
01t'6/2020 20:59
OV1612020 20:59
0111612020 20.59
014612020 20.59
01116.72020 20:59
OV1612020 20:59
0111612020 20:59
0111612020 20:59
Batch
WG1410537
WG1410537
WG1410537
WG1410537
WG1410537
WG1410537
WG1410537
WG1410537
WG1410537
Batch
WG1412927
WG1412927
WG1412927
Batch
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
Batch
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
WG1412188
r___
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources GUILFORD MILLS L1178358 0V21/2015:50
PAGE:
6 of 22

WG1411287 QUALITY CONTROL SUMMARY
Wet ChemiS try by Method 9012 B 0178358-0
Method Blank (MB)
(MB) R3490903-1 01115f201324
MB Result
Analyte Mg/kg
Reactive Cyanide U
M80ualifier MB MDL
MB RDL
mglkg
mg/kg
0.0390
0.250
L1178358-01 Original Sample (OS) • Duplicate (DUP)
(OS) 1-1178350-01 01115.2013:41 - (DUP) R3490983-4 01.1512013:42
Original Result DUP Result Dilution DUPRPD DUPOualifer DUP RPD
Limits
Analyte mglkg mgikg % %
P.eact've Cyanic a ND 0.0962 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3490983-5 0111512013:43
Spike Amount LCS Result LCS Rec. Rec Limits LCS Qualifier
Analyte mgikg mg/kg % %
Reactive Cyanide 2.50 2.80 112 50.0-150
7905-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1177905-01 0111512013:38 - (MS) R3490983-2 01.15/2013:39 • (MSD) R3490983-3 OV75'2013:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg rngikg mg/kg mgk9 % % % % %
Reactive Cyanide 1.67 ND 1.08 1.16 65.0 69.8 1 75.0-125 7.12 20
ACCOUNT: PRO. EM` SDG:
EMA Res,.,: ces GULFORD %LLS -1178358
DATErrIME
01121,2C 15:S0
PAGE
7,f22
F
E
Fn
Fr
■
7GI
E
E

WG1411620 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE
Wet Chemistry by Method 9034-90309 11178358-01
Method clank (MB)
(MB) R349t6r;14 01/16/20 21:06
MB Result MB Qualifw.. MB MDL NIB RDL
Analyte mgAg mgtk9 mg/kg
Reactive Sufride. U 7.63 25.0
E
L1178358-01 Original Sample (OS) • Duplicate (DUP)
0
'.
(OS) L117835F ^Ot?6;20 21:G6 • (DUP) R349.55 -3 Ot.�6/2C 2::05
Cn
OriglralResult DUPResult Dilution DUPRPD OUP Qualifier
?UPRPO
Limits
f
Analyte mg/kg mgkg %
%
Sf
ReameSaifde NO NO 1 O.000
20
a
L1178942-01 Original Sample (OS) • Duplicate (DUP)
7GI
(OS) L1178942-01 01/16/20 21:06 • (DUP) R3491651-4 01,116/20 21:06
Original Result DUP Result Dilution DUP RPD DUP Qualifier
DUP RPD
Limits
El,
Anatyte mgikg mgkg %
%
ReacSve SulRde NO NO i 0.000
20
;`c
Laooratory Control Sample (LCS)
(LCS; R3491657 2 01/16/20 21:06
Spike Amount LCS Result LCS Rec. Rec Limits LCS Qualifier
Aralyte mg/kg mg"(g % %
Reactive SutFde QO 95.6 95.6 70 0-!30
ACCOUNT: PROJECT:
SDG:
OATEMME: PAGE:
EMA Resources GUILFilRJ MILLS
; Y73-15S
0111i2a is SO 8 af'<2

WG1412940 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE
Wet Chemisl:fy by Method 9045D L1178358-01
L1178942-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1178942—Cl OV17/2012:00 • (DUP) R3491754-2 0111712012:00
Original Result DIP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su % %
Corrosivay by P" 8.50 8.55 1 0.587 1
Sample Narrative:
05 B.5 at 22C
DUP: 8.55 at 2'18C
Laboratory Control Sample (LCS)
(LCS) R3491754' 01;17✓2012:00
Spike Amount LCS Result LCS Re[. Rec Limits LCS Qualifier
Analyte su su % %
Ccrrosmty by pH 10.0 9.95 99.5 99.0-101
Sample Narrative:
LCS: 9.95 at IS-6C
ACCOUNT: PROJECT:
DAA Resot.rces G:A!FORC MILLS
SOG:
'1.78358
DATEMME:
OV21020 15:50
PAGE:
of 22

WG1413920 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE
Wet Chemis'atry Sy Method D9311010A L1178358.01
1-1178253-02 Original Sample (OS) • Duplicate (DUP)
(OS) LlTIS253-02 01/21/2012:25 • (DUP; R3492610-2 01/21;2012:25
Original Result DUP Resuft Dilution DUPRPD DUPOualirier DUPRPD
Limits
Anatyte Deg. F Deg. F % %
Ignitability 110 107 1 277 1.0
L1179547-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1179547-01 011212012:25 • (DUP) R3492610-3 0121/2012:25
Original Result DUP Result Dilution DUPRPD DUP Oualifier DUP RPD
Limits
Ana" Deg. F Deg. F % o
Ignmbilty DNI at 170 DNI at 170 i 0.000 10
Laboratory Control Sample (LCS)
(LCS)R3492610-1 CV21/2012:25
Spike Amount LCS Result LCS Rec. Rec, Limits LCS OualiFler
Anatyte Deg. F Deg. F % %
IgriRab3dy 82.0 81.8 99.7 97.0-103
ACCOUNT: PROJECT: SDG: DATEMME:
FMA Resources G�ALFORD MILLS L1178358 OV21,20!5:5C
PAGE:
1Go 22
SS
Cn
Fr
N
F
F-I
E

WG14140658 QUALITY CONTROL SUMMARY ONEU+B NATIONWIDE. .�
Mercury by Method 7470A L1178358.01
Method Blank (MB)
(MB) R34907-78-1 01/14/20 20:00
M3 Result MB Qualifier MB MDL MB RDL
Analyte mg/f mgA mg/1
Mercury U 0.00330 0-0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
{LCS) R3490778-2 C111420 20:02 • (LCSD; R3490778-3 01/14/20 20:04
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analte mgA mgA mgA % % % % %
Mercury 0.0300 0.0292 0.0294 9Z2 98.1 BC.0-120 0.919 20
L1178219-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(05; L1178219—U2 01/14/20 20:C6 - (MS) R3490778-4 01,14120 20:08 - (MSD) R3490778-5 0114120 20:10
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits
Analyte mgA mgil mgA mgA % % %
Mercury 0.0300 ND 0.0286 0.0287 95.2 95.8 1 75.0-125
'8302-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD
L1178302-02 DlP.A20 20:12 • (MS) R3490778-6 01/14/20 20:14 • (MSD) R3490778-7 01114i20 2022
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mgA mg:l mgA mg,1 % %
Mercury C.C300 ND 0.0293 0.0296 9-5 98.8
MS Qualifier MSD Qualifier RPD
0 614
Dilution Rec, Limits MS Qualifier MSD Qualifier RPD
i 75.0-125 1.28
ACCOUNT: PROJECT: SDG:
EMA Resources GNLFORD MILS !.1178258
DATEITIME:
C J252015:50
RPD Limits
%
20
RPD Limits
20
PAGE
11 or 22

WG14140815 QUALITY CONTROL SUMMARY ONE LABNATIONMVIDE.
Metals (ICP-) by Method 60101) L1178358-0
Method g lank (MB)
(o-rB; R34909©O-1 01/1520 09:31
MB Result
MB Oualifer MB MDL
MB RDL
Analyte mgA
mgA
mg,1
Arsenic J
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
C.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490900-2 0 ii15/20 09:33 • (LCSO) R3490930-3 01/15/20 09:36
Sp!ke Amount LCS Resuft
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Arayte
mg/1 mg/I
mg,1
%
%
%
Arsenic
10.0 9.85
9.91
98.5
99.1
801M.20
Barium
10.0 10.1
10.2
101
102
80.0-120
Cadmium
10.0 9.77
9.86
97.7
93.6
80.0-120
chraTWRi
10.0 936
9.75
97.6
97.5
80.0-120
10.0 9.82
9.92
98.2
99.2
80.0-12C
rum
10.0 10.1
102
101
102
80.0-120
Sliver
2.00 1.85
1.83
92.3
91.5
80.3-120
LCS Oualfier LCSD Qualifier RPD
RPD Limits
0.643
20
0.B34
20
0.928
20
0.113
20
1.03
20
0.691
20
0.785
20
L1178499-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1178499-04 01/15120 09:39 -!MS) R3490900-5 31/15/20 09 44 - (MSD) R3490900-6 01/15/20 C9:46
Spike Amount
Original Result MS Result
MSD Resu@
MS Rec.
MSD Rec.
Dilution Rec Limits
Analyte
mgA
mgA. mgA
mg.1
%
%
%
Arser:c
10.0
U 9.57
9.54
95.7
95.4
1 75 0.125
Baeum
10.0
U 10.3
102
102
101
F 75.0-125
Cadmium
10.0
U 9.69
9.65
96.9
96.5
75.0-125
Chromium
10.0
U 9.72
9.70
97.2
97.0
1 750-125
Lead
10.0
U 9.76
9.66
97.6
96.6
1 75.0-125
Selenium
10.0
U 9.74
9.64
97.4
96.4
1 75.0-125
Sdver
2.00
U 1.82
1.82
9M
91.0
i 75.0-125
ACCOUNT: PROJECT: SDG:
EMA Resources GUILFORD MILLS -1178358
MS Qualifier IASD Ouallw RPD
RPD Limits
0.237
20
0.845
20
OR54
20
0.148
20
1.09
20
1.04
20
0.0881
20
DATEMME:
01/242015:5C
PAGE:
'7 of 22

WG14140815
QUALITY CONTROL SUMMARY
ONE LAS NATIONWIDE.
Metals (ICP) by Method 60100
L1178350-01
L1178878-01 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD)
(OS) L1178973-01 01/15/20 09:49 - (MS) R3490900-7 01/15/20 09:51
• (MSD) R349MCO-8 OIA5120 09:54
Spike Amount
Original Result MS Result
MSD Result MS Rec. MSD Rec. Dilution
Rec. Limits PALS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte m0,1
rrg/I mgn
mgA % %
%
%
%
I j r
Arsenic. 10.0
ND 9.97
9.95 99.7 99.5 1
75.0-125
0.200
20
LL
Barmm 10.0
0.388 10.4
10.5 100 101 1
75.0-125
0.544
Z0
,$S
Cadmium 13.0
ND 9.88
9.93 98.8 99.3 1
75.0-:25
0-525
20
Chromium 10.0
ND 9.73
9.70 97.3 97.0 1
r-1.0.125
0.329
20
Lead 10.0
ND 9.84
9.91 98.4 99.1 1
75.0-125
0.701
20
a
Cn
Selentum 1G.0
ND 10.2
10.2 101 102 1
75.0-125
0.498
20
Sthrer 2.00
ND 1.86
1.86 93.2 93.1 1
75V,25
0.0688
20
s
Sr
ACCOUNT: PROJECT: SDG: DATFJrIM F' PAGE:
EMA Res-.:c 3Uf_FORD MILS L117B358 0112' , 0 15:50 13 of 22

WG141-0537 DUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Or¢anic Compounds (GCIM51 by Method 8260D L1178358-01
Method Blank (MB)
(MB) R3490638-8 01.114/2013:26
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/1
mgA
m9i1
Benzene
U
0.0167
0-0500
Carbontetrachlcirde
U
0,0167
0.0500
Chlarobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroelhene
U
0.0167
0.0500
2-Butanone (MEliq
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trchloreethene
U
0-0167
0.0500
Viq chloride
U
0.0167
0.0500
R) roluer!"s
103
80..412G
R)4-5remoiiUCMbenZP.ne
94.8
77.0-726
R)1,2-Dlchbroeftne- 4
104
70.0430
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
"S`, R3490638-1 01/14i20 09:04 • (LCSD) P3490638-3 01/14/20 11:2C
Spike Amount LCS Result
LCSD Result
LCS Rec-
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier, RPD
RPD Limits
a
mgA
mgA
mgA
%
%
%
%
%
Benzene
0.250
0.277
0.287
ill
115
70.0-1123
3.55
20
Carbon tetrdchbrlde
0.250
0.254
0.266
102
106
68.0-126
4.62
20
Chlorobenzene
0.250
0.244
0.267
97.6
107
80.0-121
9.00
20
Chloroform
0.250
0.276
0.2.88
TO
115
73.0-120
4.26
20
1,2-Dichloroethane
0.250
0.267
0.288
107
115
70.0-128
7.57
20
1,1,7ichloroethene
0.250
0.278
0.279
Ili
112
71.0-124
0.359
23
2-Butanone (MEIq
1.25
1.65
218
1.32
174
44-0-160
J3 J4 27,7
20
Tetrachloroethene
0.25C
0.239
0.253
95.6
1C1
72.0-1.32
5.69
20
Tnchloroethene
0.250
0.248
0.253
99.2
101
78.0.124
2.00
20
Vinyl chloride
0.250
0.259
0.291
104
116
67.0-131
11.6
20
R) roluene-a
102
103
80.4120
IS)4-8romoAuorcterzere
95.5
96.6
77.0-126
R)1,2-Dichioroedyane-d4
104
103
70.0-130
ACCOUNT: PROJECT: SDG: DATEITIME PAGE:
EMA Resourres GUILFORD MILS L:78358 Ot 2V2G 15:50 14 e 22

WG1410537 QUALITY CONTROL SUMMARY ONE LA13-NATIONWIDE
Volatile Organic Compounds (GC/MS) by Method 82600 L1178358-01
1-1178220-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS; L1178220--02 01714/2014,08 • (MS) R3490638.4 OI/l4/2011:45 • (MSD) R3490638-5 01Y4/2012:06
511ke Gmloum
Qrymal Resuft M5 Resu1:
M50 Sow)t
MS Rec
MSD Rec
OdUban
ROL Ln:d_
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyse
mg/l
my4
mgA
mgA
%
%
%
%
%
Benzene
0.250
N0
0.320
0.328
128
131
i
17.0-158
2.47
27
Carbontetrathlozide
0.250
:FO
0.300
0.315
120
126
1
23.0-159
4.88
28
Chlorobenzene
0.250
0.278
0.290
111
116
1
33.0-152
4.23
27
Chloroform
0.250
I.L
0311
0.320
124
1.28
1
29.0-154
2.85
28
1,2-Diolloroetharte
0.250
lir
0,297
0.305
119
122
1
29.0-151
2.66
27
1,1-DicNoroethene
0.250
%:10
0.318
0.330
127
132
1
11.0.160
3.70
29
2-Butanone(WEK)
125
uf�
1.95
2.02
156
162
1
10.0-160
J5 3.53
32
Tetrathloroethene
0.250
NL
0.279
0.283
11.2
113
1
10.0-160
1.42
27
Trlchlaroethene
0.250
N;
0.280
0.286
L'2
114
1
10.0-160
2.12
25
Vir6rl chloride
0.250
NO
0320
0324
128
130
1
10.0-160
1.24
27
5) 7oluene-dB
103
103
80.C-120
04-BromoNuorobeazene
95.4
977
77.0-126
(S%1,2-Dich/ovetham-64
104
F04
70.0-13G
L1178556-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1178556-04 01114/2014:27 • (MS) R3490633-6 0./14/2012:26
Spike Amount
Original Result MS Result
MS Rec.
Dilution Rec. Limits MS Qualifier
-
mgA
mgA
.gA
%
%
Benzene
0.250
NO
E.311
124
1 17.0-158
Carbon tetrachloride
0,250
NO
0.299
120
1 23.0.159
Chlombenzene
0.250
NO
0.280
112
1 33.0-152
Chloroform
0.250
NO
0217
127
1 29.0.34
1,2-Dich1oroethane
0250
NO
0.295
118
1 29.0-151
1,1-DiWoroethene
0.250
NO
0.315
126
1 11.0-160
2-Butanone(MElQ
1.25
Nn
1.81
145
1 10.0-160
Tetrachloroethene
0.250
NO
0.280
t12
1 1G.G160
Trichloroethene
0.250
NO
0.275
G
1 10.0-160
VinA dronde
C.250
NO
0.314
126
1 10.0-160
(.5) ruluene-d8
703
80.0-120
1S) 4-Bromoruombenzene
95.8
717.0-126
(S,' 1.2-Oich/oroethane-04
f04
70 0-130
ACCOUNT: PROJECT: SDG:
EMA Re-rc- GUILFORD MILLS L'178358
DATEI T IME:
OV2520 15:50
PAGE:
15 of 22

WG1412927
Mir
Chlorinated Acid Herbicides (GC)
by Method 8151A
Method Blionk (MB)
(MS) R3491837-1 0111712015:07
MB Result
MB Oualifter ME MDL
Analyte mgA
mgA
2,4-D u
0.000667
2,4,5-TP (Silvex) ::
0.000667
15) 2,4-D chlorOphanyl Acetc 686
Acid
Laboratory Control Sample (LCS)
(LCS) R3491837-2 0111712015:20
Spike Amount
LCS Result
LCS Rec.
Analyte
mgll
mtyl
%
2,45-TP(Silvex)
0.0500
0.0320
54.0
2,4-D
0.0500
O.G323
64.6
!S) 2,4-Dichlorophanyi Acetic
60.6
Acid
QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE
L1178358-01
ME RDL
mg/l
0.00200
0.00200
14.0-158
Rec. Limits LCS Qualifier
50.0-125
50.0-120
14, 0-158
L1178359-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
V78359-01 01t17120 20:G8 - (MS) R3491837-3 01,17/20 2022 - (MSD) R3491837-4 0107120 20:35
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualtfie, RPD
RPD Limits
H.wr7!e
mgA
mgil mg.4
rrgil
%
%
%
%
%
2,4,5-TP(Silv(,4
0.0500
ND C.0323
0.0331
64.6
66.2
1 50.0-125
2.45
20
2.4-D
U50G
ND 3.0316
0.0339
63.2
67.8
1 50.0-120
702
20
(5)1,4-Dlchlorophenyl Acetic
Aced
548
5E.6
14.0-158
ACCOUNT. PROJECT: SDG:
EMA Re— GJILPORD Mi- -S _ii75358
DA?ErnME:
PAGE:
lb of 22

WG14140888
QUALITY CONTROL SUMMARY
Pesticides ;(GC) by Method 8081E
Lf176356-01
Method gjank(MB)
(MB) R349122'7-1 075/2015:24
-
MB Result
MB Qualifier MB MDL
MS ROL
Analyte mg11
mg,:
mgP.
Gamma BHC U
000167
0.00500
Endr;n U
O.00tE7
0.005DO
Heptachkx U
0.00167
0.00500
Methoxychlor U
0.001,67
0.00500
Chlordane U
O.CO167
0.00500
Toxaphene U
0.00333
0.0100
(S) Decoolorobphenyl 858
10.0-128
(S)Tevochlorv-m-llene 74.2
10.0.127
Laboratory Control Sample (LCS)
(LCS) R3491,227-2 O';15/<O 15:36
Spike Amount
LCS Result
LCS Rec
Rec Limits LCS Qualifier
Analyte
mg11
mcyl
%
%
Gamma BHC
0.0100
0.00876
87.6
55.0-129
Ennis
0.0100
0.00926
92-6
57.0-134
Heptachlor
0.0100
0.00951,
95.1
27.0-132
lxychlor
0.0100
0."1
ill
54.0-1.55
ecochlorrxb phenyr
78.5
10.0-128
Telrochloro-m,rylene
68.4
10.0-127
L1177678-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
JU jq Ulf]W2U 1b:14 - IM.t>j tf3451227-3 01715201626 • (MSD; R3491227-4 011'5i2016:39
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg,9
mgA
mgA
17,94
%
%
Gamma BHC
0.0100
ND
0.00873
0.00890
87.3
89.0
Endnn
0.0100
ND
0.00907
0.00929
90.7
92.9
Heptachlor
0.WOO
ND
0.00946
0.00961
94.6
96.1
Methoxychlor
0.0100
ND
0.0132
0.0103
'02
103
(S) Decochiorobipheny'
7.9
75,0
57 retrachloro-m xylene
67.1
68.4
ONE LAB. NATIONWIDE
Dilution
Rec. Units
MS Qualifier MSD Qualifier RPD
RPD Limits
1
:4.D-141
1.93
40
1
iO.C-160
2.40
39
1
16.0.25
1.57
40
1
10.0-160
0.976
34
:06128
10. 0427
ACCOUNT: PROJECT: SDG:
EMA Res .rces GULFORD MILLS :178I58
DATE7TIME:
01d21, 20 15:50
PAGE:
17 of 22

WG1412188 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE
Semi Volatl#e Organic Compounds (GC/MSJ by Method 827CE L1173358-0
Method glank (MB)
(MB) R34916243-2 01A612017:52
MB Result
Analyte
mg/l
IA-MchlorohenZene
u
2.4-DinarotoluerrlE
u
Hexachlorobermcne
u
Hexathbro-1.343utadiene
u
Hexachlaroethafire
u
N robenzene
u
2-Methylphenol
u
3&4-Methyl Phenol
u
Pentachlorophend
u
2,4,54richloroptlenol
u
2,4,6-Trichloroplsenol
u
Pyrktne
u
WSJ 2-Ruoroph�-nol
35.1
Q Phemg-6
20.5
(S)Nftbenzene-d.5
591
1Sj 2-Rtwabiphen}d
72.4
(5 24.6-Tiibronrophenol
70.0
�Terpheny"14
72.5
MB Qualifier MS MDL
MB RDL
mgh
mg.4
0.0333
0.100
0.0333
0.100
0.0333
0.700
E
0.0333
0.100
0.0333
0.100
Cn
0-0333
0.100
0.0333
0.100
�Sr
0.0333
0.100
0.0333
0.0333
0,100
0.100
■
0.0333
0.100
0.0333
0.100
�GI
10.0-120
10.0-12o
10 0-127
nAl
10.0-130
;0. -755
10.0128
�C
Laboratory Control Sample (LCS)
(LC5; R3491629-1 U16120 17:31
Spike Amount
LCS Resuh
LCS Rec.
Rec. Limits
Analyte
mg/l
mg,1
%
%
1,4-0.,ct•.1omberzene
0.500
0336
67.2
1&0-120
2,4-DnihatoWene
0,530
0A03
80.6
49.0-124
Hexachlumbenzene
0.500
0AG,
80.2
41.u-120
Hexac1bro-1,3butadiene
0,500
0.327
65.4
19.0-120
Hexachioroethane
0.500
0.321
64.2
15.0-120
tlihZeozene
0.500
0,304
60.8
27.0-120
2-Methyiphenol
0.500
0.277
55.4
28.0-120
3&4-Whyl Phenol
0.500
0.275
55-0
31.0.120
Pertachloroohenol
C.500
0-367
73A
23.0-T20
2,4,5 Trichlorophenol
0.500
0.427
85.4
44.0420
2,4,6Trchlorophenol
0.500
C370
74.0
42.0-120
Pyridine
0.500
0.182
36A
10.0.120
,5) 2-F.r-ph-0l
35.2
I0.0-;20
I51 Phen01-d5
21.8
10.0-120
IS/ Ntlrobenzene-05
499
10.0-117
LCS Qualifier
ACCOUNT: PROJECT: SDG:
EMA Resajrces GIILFORD MFLS L;17S358
DATErrlME:
082b201 .:50
PAGE:
l8 ar 22

WG1412188 QUALITY CONTROL SUMMARY
Semi VoIaiiCe Organic Compounds (GC/MS) by Method 8270E L1178358-01
Laboratory Control Sample (LCS)
C-CS) R34916Z94 01/16/2017:31.
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyle mgA M91
%
%
¢J2-F,rwMpbenyl
77.2
1D.0 130
,q 2,4, 6-Tiibro-phenol
86.5
10.0-155
(4,q-Terphe 1--74
77.3
10.0-128
L1178358-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(0S; L717835"1 01/16/20 20:59 • (MS) R3491629-3 01/16120 21:20 • (MSD) R3491629-4 OV16/20 21:41.
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mgA
mgA
mgA
mgA
%
%
%
1.4-D'Ichlorobenzene
0.500
ND
0.247
0.228
49.4
45.6
1 17.0-120
24-Dinitrotoluene
0.500
NO
0.359
0.33E
71.8
67.6
i 39-0-725
Hexachkuobenzene
0500
NO
0.356
0.333
71.2
66.6
1 35.0-122
Hexaddoro-t3-butadrene
0.500
ND
0.239
0.233
47.8
46.6
1 12-0-120
Hexachlaroethane
0.500
ND
0.217
0.206
434
41.2
1 10.0-120
N1L•abenzene
0.500
NO
0268
0.245
53.6
49.0
1 12.0-120
2-Me,Wphenoi
0.500
ND
0,243
0-220
48.6
44.0
1 10.0-120
384Methyl Phenol
0.500
ND
0245
0.222
49.0
44.4
1 10.0-12G
hlorophenol
0.500
NO
0.319
0.282
63.8
56.4
1 10.0-128
. nchkrephenol
0.500
NO
0.379
0.332
75.8
66.4
i 33.0-120
2,4.6-Trchl rophenol
0.500
NO
0.325
6.284
65.0
56.E
1 2EO-120
Pyridine
0.500
ND
0.165
GA65
33.0
33.0
1 10-0-120
(5)2-Flo'orophenal
37.6
274
10.C,12C
.Q Pherto%d5
G.1
168
10.0-170
(Sj Nibobenzeae-6
45.3
40.8
10.0427
(5)2-Flnorolbph-)d
70.2
620
10.0-130
!S)Z.4,6-T.nhromophero.'
74.0
67..5
100-155
Q p-Terph-y1-d14
68.8
64.9
10.0-128
tdS Qualifier MSD Qualifier
ONE LAB NATIONWIDE.
RPD RPD Limits
8,00 40
6.03 25
6,68 24
2.54 34
5.20 40
8.97 30
9.94 30
9.85 36
12.3 37
13.2 31
13.5 31
0.000 37
ACCOUNT: PROJECT_ SDG: DATEfTIME
EMA P-., Es GUILFORD MILLS _n78358 :,172 u2015:50
PAGE
19&22

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
:ended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits. Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
14DL
Method Detection Limit
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Lirotts
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDU
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Qualit`j Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value ;s high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources GUILFORD MILLS L1178358 01/21r20 15:50 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
pale National is the only environmental laboratory aaredltedlcertlfiad to support your work nationwide from one location. One phone call, one point of contact, one laboretory. No other lab is as
accessible ororepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective totals of the network
atorias':i our industry. The most significant benefit to our one bcadon design Is the design of our labor
at. ry campus. The model is conducive to accelerated productivity, decreasing
turn r-arourd t: ae. and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
•Not all certifiations held by the laboratory are applicable to the are reported in the attached report
• pGcreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
E
State Hccreditation-
Alat3ama 40660
Nebraska
NEOS-15-05
E
Alaska 17-026
Nevada
TN-03-2002-34
ArlZena AZO612
Arkansas 88-0469
New Hampshire
NewJerse -NELAP
Y
2975
TNO02
E
California 2932
New Mexico'
Na
Colorado TN00003
Connecticut PH-0197
New York
North Carolina
11742
Env375
rsrl
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina'
41
Georgia' 923
North Dakota
R-140
Fc
Ida ha TNG0003
Ohio-VAP
CLOO69
Illinois 200008
Indfa na C-TN-01
Oklahoma
Oregon
9915
TN 200002
G
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
a
Rhode Island
LA000356
Kentucky 90010
South Carolina
84004
Kentucky' 16
South Dakota
n/a
Louisiana A130792
Tennessee "
2006
Louisiana' LA180010
Texas
T104704245-18-15
L` C
Maine TNG002
Texas s
LA80152
Maryland 324
Utah
TNO0003
Massachusetts M-TN003
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Wginla
233
Missouri 340
Wisconsin
99809399/.0
Montana CERT0086
Wyoming
A2LA
Third Party Federal Accreditatior,
A2LA - ISO 17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2LA-ISO7025 a 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TNG0003
' Drinking Wate, 'Underground Storage Tanks 3 Aquatic Toxicity ' Chemical/M:crobiologtal 'Mold 6 Wastewater n/a Accreditation not applicable
7ur Location
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our rna;a office. Pace National performs all testing at our central laboratory.
e33
r Na
� rLf
WY
pp NV_l_._..,.. NE
—
"A t p
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TX
AK
HI
r.I E
of
ACCOUNT: PROJECT:
EMA Resources GUILFORD MILLS
SDG: DATEMME: PAGE:
L1178358 01/21/20 15:50 21 of 22

tzlForma4drc--
EMAVResources
_
Mr. Brent Collins Pres
75S Yadkinville Road tick
755 Yaii iAville Road
Mocksvllle, NC 17028
Mocksvale, NC 27026
+
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Reporttos:.
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Mr. Brerat Collins
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F—&-
Project C ty/State
...Please ck
Dczcrfatipn_ Sludge Cofteetted: �l✓Ci'- {�
Pr iur Cr-�Yv'
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Lab -..Project #
setiti�-•� �,
Fax: [phone]
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Retie :�i3+hdS:by;jii;natwe) D r Tlme; Received by:{Stt-t—) a••r •. •., t "`
"trap;,. :L�' �, f pl'R1M a' :' �..r• `y i� � ;la's' T�I
Relinquished by-(Si`nattue)
Date. Time:
L t fug,t,•Vj
Kmd,
_ 7 L
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RESIDUALS ANALYSIS REPORT 71
PROJECT:
Guilford Performance Textile
Sample Date: 1/22/2020
% Solids
2.64
pH: 6.80
CONVERSION TABLE
PARAMETER
%
X 10000
= ppm dry wt.
X 0.002
= Ibs/dt
Nitrogen TKN
3.06
30600
61.2
Phosphorus
1.33
13300
26.6
Potassium
0.201
2010
4.02
Sulfur
1.44
14400
28.8
Calcium
0.715
7150
14.3
Magnesium
0.154
1540
3.08
Sodium
0.207
2070
4.14
Ammonia N
0.535
5350
10.7
Nitrate N
0.0192
192.00
0.384
Iron
0.0361
i Ceiling
361.00
0.722
Concent.
Aluminum
9.85
98500.00
197
Chromium
0.000731
ppm
7.31
0.01462
Manganese
0.00369
36.90
0.0738
Copper
0.00481
4300.00
48.10
0.0962
Zinc
0.00415
7500.00
41.50
0.083
Cadmium
0.00019
85.00
1.90
0.0038
Nickel
0.000635
420.00
6.35
0.0127
Lead
0.000573
840.00
5.73
0.01146
Arsenic
0.00161
75.00
16.10
0.0322
57.00
Mercury
0.0000125
.00
10000.00
0.13
0.00025
Selenium
0.00188
75
18.80
0.0376
Molybdenum
0.00127
12.70
0.0254
PLANT AVAILABLE NITROGEN CALCULATION (PAN)
MR
(TKN - AmN)
+ .5(AmN)
+ NO3N
X .002 = lbs. PAN/dt
Surface
7575
2675
192
20.884
MR
(TKN - AmN)
+ AmN
+ NO3N
X .002 = lbs. PAN/dt
Injection
7575
5350
192
26.234

Guilford Performance Textiles
TKN
30600
mg/kg
2nd yr min. rate
NH3
5350
mg/kg
3rd yr min. rate
Organic N
25250
mg/kg
4th yr min. rate
NO2NO3
192
mg/kg
5th yr min. rate
1st yr min. rate
0.3
I st year PAN Calculation (Surface)
L-bs/DT PAN = [min. rate x (TKN - NH3) + (.5NH3) + NO2NO31 x .002
Lbs/DT = 0.3 25250 2675 192 x .002
Lbs/DT =1 20.884
Znd year Residual PAN Calculation
LIbs/DT PAN = [min. rate yr 2 x (lst yr organic N - 2nd yr mineralized organic N)] x .002
Lbs/DT = 0.16 25250 7575 x .002
Lbs/DT = 5.30
3wd year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 3 x (2nd yr organic N - 3rd yr mineralized organic N)] x .002
Lbs/DT = 0.075 17675 2651.25 1 x .002
Lbs/DT = 2.25
4th year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 4 x 3rd yr organic N - 4th yr mineralized organic N)] x .002
Lbs/DT =1 0.0375 15023.75 1127 1 x .002
Lbs/DT = 1.04
5th year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 5 x 4th yr organic N - 5th yr mineralized or anic N)] x .002
Lbs/DT =1 0.01875 13897 521 x .002
Lbs/DT = 0.50
Five Year Maximum Adjusted PAN = { 2 99{ 8 1Lbs/DT
Five Year Maximum Adjusted PAN = 14992 mg/kg
0.15
0.075
0.0375
0.01875

iGuilford Performance Textiles
TKN
30600
mglkg
2nd yr min. rate
NH3
5350
mg/kg
3rd yr min. rate
Organic N
25250
mg/kg
4th yr min. rate
NO2NO3
192
mg/kg
5th yr min. rate
1st yr min. rate
0.3
%
I st year PAN Calculation (injection)
I_bs/DT PAN = [min. rate x (TKN - NH3) + NH3 + NO2NO31 x .002
Lbs/DT = 0.3 25250 5350 192 x .002
Lbs/DT = 26.23
2nd year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 2 x (1st yr organic N - 2nd yr mineralized organic N)] x .002
Lbs/DT = 1 0.15 26260 7575 x .002
Lbs/DT = 1 5.30
3rd year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 3 x (2nd yr organic N - 3rd yr mineralized or anic N ] x .002
Lbs/DT = 0.075 17676 2651.25 x .002
Lbs/DT = 2.25
4th year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 4 x (3rd yr organic N - 4th yr mineralized organic N)] x .002
Lbs/DT = 0.0375 15023.75 1127 x .002
Lbs/DT = 1.04
51th year Residual PAN Calculation
Lbs/DT PAN = [min. rate yr 5 x (4th yr organic N - 5th yr mineralized organic N) x .002
Lbs/DT = 0.01875 13897 521 x .002
Lbs/DT = 0.50
Five Year Maximum Adjusted PAN = 35.33 Lbs/DT
F;ve Year Maximum Adjusted PAN = 17667 mg/kg
0.15
0.075
0.0375
0.01875

waypoint
ANALYTICAL
1/22/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-010-0059
Client Project Description: Guilfield Wills
Kenansville, NC
2790 Whitten Road, Memphis, TN 39133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/10/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
'The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN0001--
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #802-15 PA CEP #69-03195
Page 1 of 7

Way oi nt � 27901HIP�itten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.corn
Sample Summary Table
Repcprt Number: 20-010-0059
Clieret Project Description: Guilfield Mills
Kenansville, NC
Lab Np Client Sample 1D Matrix Date Collected Date Received
92916 Guilford Mills WWTP Solids 01/09/2020 08:00 01/10/2020
Page 2 of 7

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Guilfield Kills
Lab Report Number: 20-010-0059
Date: 1 /22/2020
2790 Whitten Road, Memphis, Tltl 38133
Mgain 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92916 (Guilford Mills WVVI-P)
Analyte: Aluminum
QC Batch No: 1-472729/1-472416
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
vvas performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 3 of 7

A
�
2790 Whitten Road, Memphis, TN 38133
'
Main
901.213.2400
°
Fax [phone]
ANALYTICAL
www.waypointanalyfical.com
46245
Er4i1 Resources Inc
Mr- Br'entCollins
Project Guilfield Kills
Report Date : 01/22/2020
755 Yadbnville Rd
Information : Kenansville, NC
Received : 01/10/2020
MoCksvile , NC 27028
Report Number: 20-010-0059
RERORTOFANALYSFS
Danyale Love
Project
Manager
Lab INo : 92916
Matrix:
Solids
Sample ID: Guilford Mills WWTP
Sampled:
2/9/2020 8:00
Test
ResuHs
Units
MDL
MQL
DF
Date I Time
By
Ana"cal
Analyzed
Method
Moisture
97.4
%
0.010
1
01/13/20 16:26
ADM
SW-DRYWT
Ammonia Nitrogen
5350
mg/Kg - dry
962
1
01/21/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<192
mg/Kg - dry
192
192
1
01/20/20 16:10
ZBD
4500NO3F-2011
Organic N
25230
mg/Kg - dry
55.00
2754
1
01/14/20 16:16
CALCULATION
pH
6.8
S.U.
1
01/21/20 05:24
JSL
9045D
Total Solids
2.64
%
0.010
0.010
1
01/13/20 16:26
ADM
254OG-2011
Total Volatile Solids
69.5
%
0.010
0.010
1
01/13/20 16:26
ADM
254OG-2011
Total Kjeldahl Nitrogen
30600
mg/Kg - dry
2750
1
01/14/20 16:16
CLP 4500NORGD-2011
Phosphorus
13300
mg/Kg - dry
98.8
192
1
01/14/20 02:28
BKN
6010D
Aluminum
98500
mg/Kg - dry
78.1
192
1
01/14/20 02:28
BKN
6010D
Arsenic
<16.1
mg/Kg - dry
16.1
19.2
1
01/14/20 02:28
BKN
6010D
Cadmium
<1.90
mg/Kg - dry
1.90
3.85
1
01/14/20 02:28
BKN
6010D
Calcium
7150
mg/Kg - dry
646
962
1
01/14/20 02:28
BKN
6010D
Chronnium
<7.31
mg/Kg - dry
7.31
9.62
1
01/14/20 02:28
BKN
6010D
Copper
48.1
mg/Kg - dry
5.58
9.62
1
01/14/20 02:28
BKN
6010D
Iron
361
mg/Kg - dry
163
192
1
01/14/20 02:28
BKN
6010D
Lead
<5.73
mg/Kg - dry
5.73
11.5
1
01/14/20 02:28
BKN
6010D
Magnesium
1540
mg/Kg - dry
85.4
192
1
01/14/20 02:28
BKN
6010D
Manganese
36.9
mg/Kg - dry
7.04
19.2
1
01/14/20 02:28
BKN
6010D
Mercury
<0.125
mg/Kg - dry
0.125
0.565
1
01/15/20 16:22
TJS
7471A
Molybdenum
12.7
mg/Kg - dry
5.00
9.62
1
01/14/20 02:28
BKN
6010D
Nickel
<6.35
mg/Kg - dry
6.35
9.62
1
01/14/20 02:28
BKN
6010D
Potassium
2010
mg/Kg - dry
115
192
1
01/14/20 02:28
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 4 of 7

!ti
0y
Waypoint,
rt.
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax [phone]
www.waypointanalytical.com
46Z45
EMA Resources Inc
Mr- Brent Collins Project Guilfield Kills
Report Date : 01/22/2020
755 Yadkinville Rd Information : Kenansville, NC
Received : 01/10/2020
Mocksviile , NC 27028
Report Number: 20-010-0059 REPORT OFANAL YSIS
Danyale LoveProject Manager
Lab IYO : 92915
Matrix: Solids
Sam2ple ID : Guilford Mills WWTP
Sampled: 1/9/2020 8.00
Test
Results
Units
MDL
MQL
DF
Date I Time
Analyzed
By
Analytical
Method
Selenium
<18.8
mg/Kg - dry
18.8
19.2
1
01/14/20 02:28
BKN
6010D
Sodium
2070
mg/Kg - dry
297
962
1
01/14/20 02:28
BKN
6010D
Zinc
41.53
mg/Kg - dry
41.5
48.1
1
01/14/20 02:28
BKN
6010D
Sulfur
14400
mg/Kg - dry
188
192
1
01/14/20 02:28
BKN
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
01/14/20 02:28
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
Estimated value
Page 5 of 7

Wa,avaint.
2790 Whitten Road, Memphis, TN38133
0
ANALYTICAL
Main 901.213.2400 Fax [phone]
unvw.waypointanalytical.com
Shipment
Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-010-0059
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 Other:
0 UPS 0 Client 0 Courier
Thermometer ID: �70
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
r 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No Not Present
Custody seals intact on sample bottles?
0 Yes
0 No Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
* Yes
0 No
COC properly completed
* Yes
0 No
Samples in proper containers?
0 Yes
No
Sample containers intact?
* Yes
0 No
Sufficient sample volume for indicated test(s)?
* Yes
0 No
All samples received within holding time?
* Yes
0 No
Cooler temperature in compliance?
i Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
* Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No * N/A
Water - VOA vials free of headspace
0 Yes
0 No * N/A
Trip Blanks received with VOAs
0 Yes
0 No * N/A
Soil VOA method 5035 — compliance criteria met
Yes
0 No * N/A
High concentration container (48 hr)
— Low
concentration EnCore samplers (48 hr)
r High concentration pre -weighed (methanol -14 d)
— Low
conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments
Signature: (Tory Phillips Date & Time: 01/10/2020 10:50:20 it
Page 6 of 7

Went Nawwe/Address
EMA ResOurces I-
755 Yadoclm lle Rd
Client Project Manager/Contact
Brent Collins
1111"Ag trdormation
Account #46245
For laboratory Use Only
MocksAMO, NC 27028
Project DaS1:611110o
t 1U o rC r
Project/site Location {City/sate)
l
A ! �{/ (�
RUSH -Additional charges apply
Spedal Detection Umit(s)
Date Results Needed
Me of Shipppment
Fed Ex ' (t1P5 ❑USPS
Courier rU{pfent Drop OH
Other
Matrix Key
WW -Wastewater GW-Gmtmdwater
DW- Drinking Water s-Safi /5otad p_Did
P - Product M • Misc
Project Nuxlnber
Project Manager Phone a
Project Manager Email
Purchase Order Number
site/Facifty ID M
336-399-3646
[e-mail]
pant.
2790 Whitlen Road
Memphis. TN 38733
[phone]
Unless rested, all containers
per Table ltof 136�CFR Part
ai
'
Z
o
„mu„
z
=E
=
o
as
o
-'
Ut
/6
Cu
O
Q
Z
Z
C
rn
0
w
Z
in
I -
�
�
�1
' +
v
A Cod c 10C Na?MO3 (hWo Only)
e s6C
C m2see
o More Requk
edANALYTICAL
E Na"pW10
F HNO3 PH<2
c _
H �r �
08ie
me
Sample Identirrcatron
Re
wired A at sis / PreservaN
a
Comments/Notes
:ep
f,(,(r« t J
t
"`
GV,
Metals:AI,As,Ca,Cd,Cr,CU,Fe,Pb
Mn,Mg,Mo, Hg,Ni,Se,Na,P,S,K,Zn
20-01 I II�I�� �iI�I��i1�1 �N 111 ��9�°
Gui Wd Miles„
For laboratory Use only
Sampled by (Name -Print)
Client Remario/Comments
Sludge Samples - Report Dry Weight
Ice Custody
V / N
Y
Lab Comments
Relinqui RE) _ _
—
i
�hne
a.•ao
Received try: (smNA RE)
Date Time
,l9 z'oo
8fank twkr
ReRrpuis by: ( ATURE)
a Time
Real by: SIGNATURE)
Date Time
tV!
Relinquished by. ISIGNATURE)
Date rime
Rea : (SIG TURE)
Dace TI . e
O
C)'�- . 05
Page 7 of 7

SAR
SAR Calculation _ Nam /g 1 Ca mg/I Mg mg/1—
54-64 88 188.76 40.656
Na Ca_ T Mg SAR fi
2.376 9.438 3.388 0.938 Na mil eq Ca mil eq 'IWg mil ec
1 - -2.376 9.438 G 3.388
Enter{ Enter .% TS
Data _ Na_m kk�
- - - — -- Ca ma/ka
i
Job Name: 'Guilford Performance Textiles
' I
2.64
?070
7150
1540
Page 1

Analytical Results
Epic A Resources, Inc.
755-Yadkinville Rd.
Mocl<sville, NC 27028
Receive Date:
- 01/09/2020
Reported:
01/10/2020
For:
Guliford Mills
Comments:
Geometric Mean= <764 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200109-23-01
Fecal Coliforms
GM-1
<763
MPN/g
sM92210E-20W
01/09/2020
CL
200109-23-01
Percent Solids
GM-1
2.62
%
SM254OB-2011
01/09/2020
CL
200109-23-02
Fecal Coliforms
GM-2
<766
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-02
Percent Solids
GM-2
2.61
%
SM25406-2011
01/09/2020
CL
200109-23-03
Fecal Coliforms
GM-3
<752
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-03
Percent Solids
GM-3
2.66
%
SM264OB-2011
01/09/2020
CL
200109-23-04
Fecal Coliforms
GM-4
<766
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-04
Percent Solids
GM-4
2.61
%
sM254o6-2011
01/09/2020
CL
?00109-23-05
Fecal Coliforms
GM-5
<775
MPN/g
SMMICE-20W
01/09/2020
CL
200109-23-05
Percent Solids
GM-5
2.58
%
SM25406-2011
01/09/2020
CL
200109-23-06
Fecal Coliforms
GM-6
<769
MPNlg
SM92210E-2006
01/09/2020
CL
200109-23-06
Percent Solids
GM-6
2.60
%
SM254OB-2011
01/09/2020
CL
200109-23-07
Fecal Coliforms
GM-7
<784
MPN/g
SM92210E-2006
01/09/2020
CL
200109-23-07
Percent Solids
GM-7
2.55
%
SM254OB-2011
01/09/2020
CL
Respectfully submitted,
LP.,-vt^ ';Y �' ,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 1 of 4

Condition of Receipt
Sam ple Number 200109-23-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-02 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-03 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-04 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-05 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-06 Temp on Arrival:
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 200109-23-07 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 3 of 4

O
(30
x
N
N
00
•
rt
0)
m
m
Z
N
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tT
00
V
V
o
to �
140
?
V
o, N
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t.p
V
Contact Person:
PO #
custormf
Sample IN
_ CO e
Lab-10 N (Gwb Onty)�
-a L9 /-G4 . z 3. 'rao
- 2.
;aG
pq
-S- [I
Relinquished by:
or
Received by: -
Relinquished by:
— Phone # 336-� X#
Requisitioned by: (Tine —Dais)
— ra
We Onli/) tl MaMx Parameters requested lw ana s
_ (Grab OnlY1 ,� , � awdpe W ww �
Received by:
Composite Sampling #11
Time begin am, pm Date I_I_
Time and am, pm Date
Composite Sampling_#2:
Time begin am, pm Date —I I
Time end —am, pm Date
A 0
Time
Time 12-6�am, 1
Time am, I
Time am, I
Lab Comments:
STATESVILLE ANALYTICAL
122 Coon Sit= • P,O. Box 228
Statesville, NC 28687
[phone]
i
Chain of
Custody Record
1

Residuals Information Sheet
Generator:
Lear Corporation, Guilford Performance Textiles
Facility:
Guilford Performance Textiles WWTP
Address:
1754 NC 903/11 North
Kenansville, NC 28349
Phone:
910-296-5201 336-909-1718
Contact:
Steve Molino (Lear) Roy Whitaker (EMA)
Land Application
Contractor: EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
Phone:
336-751-1441
Contact:
Roy Whitaker
Please Note: The application of these residuals is only allowed in accordance with
subject permit. (To Be Issued)
All applicable setbacks in accordance with 15A NCAC 02T .l 108(b) will be
adhered and is the responsibility of the land application contractor.
Application rates shall be applied at agronomic rates for intended uses.
No residuals shall be applied to any site that is flooded, frozen or snow covered.
Adequate procedures will be implemented to prevent surface runoff of residuals in
any surface waters.
The Attached Residuals Analysis Report is a summary of major and micro
nutrients available in the residuals.
If you have any question concerning this information, you may contact EMA
Resources Inc. at the numbers listed above.

Standard Operating Procedure and Operation and
Maintenance Plan for the LCFWSA - Bladen Bluffs
Regional WTP Land Application Program
1. Purpose
a. Ensure the requirements of the Guilford Performance Textiles Distribution of
Class A Residuals Permit# WQ............. (when issued) are met.
2. Personnel
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources Inc.
Boger Hartsell - Project Manager
2. Roy Whitaker - Director of Business Development/Ops.
3. Brent Collins - Director of Technical Services
ii. Guilford Performance Textiles WWTP
1. Steve Molino - Plant Maintenance Manager
3. Operational Functions
a. The operational function of this project it going to involve mixing the residuals
storage basin via pump recirculation to achieve a well -mixed and consistent
material that is suitable for land application. It is going to be spread at
agronomic rates that are determined using the Realistic Yield Expectations
(RYE) as outlined in the permit, the amount of other nutrient sources the
landowner and operator has applied, and the residuals nutrient and metal
sample that is current for that monitoring period. It is going to be spread with
a liquid applicator that will use pressure to spread the material in such a way
as to achieve a consistent spread pattern. The material is going to be land
applied on fields that have a crop growing on them that are going to either
be grazed or cut for animal feed. Application rates will be reduced by 25%

on fields that are primarily used for grazing in accordance with USDA-NRCS
590. Grazed fields will be determined by the farmers and EMA project
managers.
4. Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended
by the EMA Resources Operations Director (Roy Whitaker) for the equipment
necessary to complete the job.
5. Safety Measures
a. EMA Resources Inc. believe in operating in a safety conscious manner and all
employees participate in safety training that is designed to help employees
recognize safety issues and take steps to prevent accidents from occurring. In
addition, EMA Resources employees have the authority to stop operations if
they think any aspect of the operation is going to cause environmental or
personal harm.
6. Spill Response Plan
a. In the unlikely event of a spill, the following action shall be taken immediately.
i. Management of Spill Clean-up Activities: The EMA Resources Project
Manager shall take immediate charge and initiate clean-up activities.
EMA Resources labor and equipment is to be utilized. In the event
additional labor and equipment is required, assistance may be
requested from Guilford Performance Textiles, The NC Department of
Transportation, and other private contractors as necessary.
ii. Halt the Source of the Spill: Such as a ruptured container or damaged
transport unit.
iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall be
used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The Operations
Manager or the person in charge on the spill site will be advise the
clean-up personnel where to get the straw, lime, and other items
necessary to complete the clean-up operation. ie. local farmers, farm
supply centers, nurseries.
iv. Initial Clean -Up.- Employ front-end loaders, vacuum equipment,
sludge application vehicles, and/or local septic tank service to remove
as much of the spilled material as possible. Straw and/or sand should
be scattered in the spill area to soak up the remaining material. The

straw and sand soaked material will be collected and removed to a
disposal area approved by representatives of the state regulatory
agency.
v. Final Clean -Up: Employ rotary brush sweeper if needed and apply
lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private property,
the clean-up will be completed to the satisfactory of the property
owner and state regulatory representatives. The ultimate goal will be
restore the spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the Guilford
Performance Textiles and the EMA Resources main office. EMA
Resources office staff are then responsible for notifying other key EMA
Resources personnel.
vii. Reporting_ EMA Resources staff will notify the Wilmington Regional
office of the NCDENR by telephone [phone] as soon as
possible, but not more than 24 hours after, or on the next working day
following the occurrence. The EMA Project Manager shall provide a
written report with 48 hours of the spill to the EMA Resources Director
of Technical Services and Guilford Performance Textile staff. The report
shall list all relative information and actions taken. With the assistance
of EMA Resources personnel, and the Guilford Performance Textile
personnel, a written report will be filed with the Wilmington Regional
office within 5 days of the occurrence. For after hours reporting, the
Division's emergency number shall be called to report all incidences
[phone].
7. Inspection Plan
a. Inspection for the land application of residuals will conducted on a minimum
of a weekly basis at the land application site during land application activities.
The inspection frequency is based on the time frame that it is going to take to
complete the project and the amount of dry tons to be land applied from this
facility. The inspections will consist of inspecting a current field that is being
applied as well as inspecting random fields that have been completed.
Inspections will be conducted by Boger Hartsell - Project Manager. These
inspections will consist of the following:

8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for land
application.
b. The samples will be collected from the storage basin that holds the residuals
c. Roy Whitaker, Boger Hartsell, Brent Collins, or other designee will be
responsible for sample collection for nutrient and metal, TCLP, and fecal
coliform.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and
consist of at least 7 individual aliquots mixed together in order to get the
composite sample for these parameters.
e. The residuals will be sampled annually for TCLP including the RClls.
f. Metal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
g. Residuals will be sampled for fecal coliform to demonstrate pathogen
requirements have been met. Seven separate samples will be collected and
analyzed.
9. Environmental Impacts
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner while ensuring compliance with the laws and regulations and
to minimize exposure, negative environmental impacts and public relation
concerns.

State of North Carolina
DW.
Department of Environmental Quality RDivision of Water Resources
Div Ision of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instroctions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
inforrrnation requested. Failure to submit all of the required items will lead to additional processing and review time for the
perm, it application. Unless otherwise noted the Applicant shall submit one original and two copies of fte_application and
supnarting documentation
For more information, visit the Water Quality Permitting Section's Non-Dischar a Permittin , Unit
Gene K'al -- This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
[] Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Man Guidance for
Residuals Land Application Permits'
❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: EMA Resources, Inc.
umber
2305
Maximum Dry Tons Per Year
Current b
318
Proposed
318
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

wislon of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Guilford Performance Textiles
2. Facility permit holder is: [ Federal, 0 State, E] Local Government, or Private.
Facility permit issued by: Div. of Water Resources, ❑ Div. of Environmental Health,
or Other (explain:).
3. Facility contact person and title: Steve Molino
Complete mailing address: 1754 NC 903/11 North
City: Kenansville State: NC Zip: 28349-
relephone number: 910 296-5201 E-mail address: smolino Cwlear.com
4. Facility physical address: 1754 NC 903/11 North
City: Kenansville State: NC Zip: 28349-
Coordinates: Latitude: 35' 01' 04" Longitude: 77" 51' 32"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
5. Purpose of the facility:
Q treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: 99 % industrial and <1 % domestic)
other (explain:._ _ . ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: _ 1.5 MGD and facility average daily flow: .9 MGD
8. Average amount of residuals being generated at this facility, 318 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Tv
pe and volume of residuals treatment: I MG Aerobic Digeste
Type and volume of residuals storage (i.e., outside of residuals treatment units): 500K Aerated Storage Tank
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
D 40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257,
2. Specify if residuals are defined under 15A NCAC 02T.1102 6 as:
Biological Q Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-hazaxdous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: Q yes 0 no.
If yes, list the number(s): L ;_ v
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: a yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Anal ical and Date of analysis: January 21, 2020
Passed corrosivity test: yes] no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes no. Flashpoint: DNI at 170 OF (> 140°F)
Passed reactivity test: 19yes Ono. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
1'mg1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land A licadon: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 1/22/2020
Parameter Ceiling
Concentration Limits
(C1assA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic 75 41
<16.1
Cadmium 85 39
<1.9
Copper 4,300
1,500
48.1
Lead 840
300
<5.73
Mercury 57
17
<0.125
Molybdenum 75
n/a
12.7 '
Nickel 420
420
<6.35
Selenium 100
100
<18.8
Zinc 7,500 21800
41.5
b. For Surface Disposal Unit (landfilll: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: .
Distance from Disposal { Arsenic
Unit to Boundary to
Closest Property Line
(meters, check one) (mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kgj
E] > 0 but <25
30
200
210
❑ > 25 but < 50
34
220
240
> 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
[] > 100 but < 125 53
360
390
Q > 125 62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.64 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Wavpoint Analytical and Date of analysis: 1 /22/2020
Parameter
Result
(mg/k9)
Aluminum
98500
Ammonia -Nitrogen
5350
Calcium
7150
Magnesium
1540
Nitrate -Nitrite Nitrogen
<192
pH (Standard Unit)
6.8
Phosphorus
13300
Potassium
2010
Sodium
2070
Total Kjeldahl Nitrogen
30600
c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0.938
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): 0 default value, or El actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: Aerobic Digestion.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method I First (1") Year PAN I Five -Year
Maximum Adjusted PAN
(mg/k� (mg/kg)
Surface 10442 14992
I Injection/Incorporation 1 13117 1 17667 1
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: NA
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For DistributionlLandAgElicalion of Class A or E uivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
0 Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
n Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
[] Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
[] Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 0 composting, n heat drying, ❑ heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
gamma ray irradiation, or ❑ pasteurization.
b. For Land A lication of Class B:
Q Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: 0 aerobic digestion, 0 air drying, ❑ anaerobic digestion,
0 composting, or 0 lime stabilization.
c. For Surface DisnasaL
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
0 Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
Exempt -If Daily Cover Alternative is chosen in Item I1.8. below [15A NCAC 02T.1106(a)(2)].
0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Vector Attraction Reduction (VARk: Per 15A NCAC 02T.1107. specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
j] Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
n Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying ofUnstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
E3 Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
® Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I5A NCAC 02T.1107(b)(2)].
M Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

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Guilford Performance Textiles WWTP
Quantitative Justification for Residuals Production Rate
The annual dry ton calculation is based on the projected percent solids of the
thickened residuals (3.0%) and the removal of 500,000 gallons per event (5
times per year).
Gallons lbs/Gal. %Solids Drylbs. lbs/ton Dry Tons
2,500,000 x 8.34 x 0.03 = 625,500 _ 2000 = 313