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WQ0006594_Regional Office Historical File Pre 2016
North Carolina Department of Environmental Quality Pat McCrory Donald R.van der Vaart Governor Secretary October 2, 2015 Ms. Lisa Haynes, Corporate Environmental Manager Unifi, Inc. P.O. Box 1437 Reidsville,NC 27323 SUBJECT: 2014 Annual Report Review Unifi, Inc., Distribution of Industrial Pretreatment Residuals Permit No. WQ0006594 Rockingham County Dear Ms. Haynes: The Division of Water Resources (DWR) acknowledges receipt of your 2014 annual report for the subject permit. A review of this report was conducted by DWR staff person Jim Gonsiewski. Review of the subject annual report reflects compliance with Permit No. WQ0006594. An announced routine facility compliance inspection is planned to be scheduled within the next 12 months. If you or your staff have any questions, please contact Jim Gonsiewski or me at 336-776-9800. Sincerely, • Sherri V. Knight, PE Assistant Supervisor Water Quality Regional Operations Division of Water Resources cc: Brent Collins, EMA Resources, Inc. Rockingham County Environmental Health DWR Central Office—Permit File WQ0006594 �A�1Z'U'Ftks 450 W Hanes Mill Rd.,Suite 300,Winston-Salem,NC 27105 Phone:336-776-9800\Internet:www.ncdenr.gov An Equal Opportunity\Affirmative Action Employer—Made in part by recycled paper Compliance Inspection Report Permit: WQ0006594 Effective: 10/02/14 Expiration: 09/30/19 Owner: Unifi Inc SOC: Effective: Expiration: Facility: Unifi,Inc.Distribution of Residual Solids County: Rockingham PO Box 698 Region: Winston-Salem Yadkinville NC 27055 Contact Person: Timothy Cole Title: Phone: 910-679-8891 Directions to Facility: WSRO-US 52N-BUS 40E-HWY 158N-Left on Reid School Rd.-Right on Vance Street Ext.(Facility on left/north side) System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): Related Permits: NC0021873 Town of Mayodan-Mayodan WWTP NC0024881 City of Reidsville-Reidsville WWTP Inspection Date: 09/28/2015 Entry Time: 02:30PM Exit Time: 03:15PM Primary Inspector: Jim J Gonsiewski Phone: 336-776-9704 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Annual Report Review Permit Inspection Type: Distribution of Residual Solids(503 Exempt) Facility Status: Compliant Not Compliant Question Areas: Miscellaneous Questions (See attachment summary) Page: 1 Permit: W00006594 Owner-Facility:Unifi Inc Inspection Date: 09/28/2015 Inspection Type:Annual Report Review Reason for Visit: Routine Inspection Summary: This inspection consisted of a review of the 2014 Annual Report only. No site visit was conducted as part of this compliance inspection. No land application was conducted in 2014. Review of the subject annual report reflects compliance with Permit No.WQ0006594. See the files for additional details of the review. Page: 2 Permit: WO0006594 Owner-Facility:Unit Inc Inspection Date: 09/28/2015 Inspection Type:Annual Report Review Reason for Visit: Routine Type Yes No NA NE Land Application • ❑ Distribution and Marketing El Page: 3 ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0006594 County: ROCKINGHAM Year: 2014 Facility Name(as shown on permit): UNIFI, INC. Land Application Operator: LISA HAYNES Phone: 336-348-6516 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes No -If No,skip Part A, and Part B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the residuals were haStVEDIDENRIDWR Part A-Residuals Application Summary: r Total number of application fields in the permit: i :- j0 - Total number of fields utilized for land application during the year: Water Quail Total amount of dry tons applied during the year for all application sites: Permitting Section Total number of acres utilizes for land application during the year: Part B-Annual Compiance Statement: Facility was compliant during calendar year with all conditions of the land application permit (including but not limited to items 1-13 below)issued by the Division of Water Resources. _1 Yes .a No If no please, provide a written description why the facility was not compliant,the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3) copies of laboratory results are attached. 4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a)or the Pollutant Loading Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C-Certification: "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate, and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." LISA HAYNES, CORP ENV MGR RECEIVED--1 Val 16 N.C.Dept.of ENR Permittee Name and Title (type or prat) Y 0 6 2015 Signature of PeAa:-.4.voixj) ee ate Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RECEIVED ATA N.C. Dept.of ENR APR242015 — WINSTON-SALEM NCDENR REGIONAL OFFfrth Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der Vaart Governor Secretary April 20, 2015 CERTIFIED MAIL # 7010 0780 0001 7057 5228 RETURN RECIEPT REQUESTED Lisa M. Haynes Unifi, Inc. Post Office Box 1437 Reidsville, NC 27323 q- r?'1.4r.ti Subject: NOTICE OF DEFICIENCY (NOD-2015-PC-0092) PERMIT CONDITIONS VIOLATIONS Permit No. WQ0006594 Unifi, Inc. Distribution of Residual Solids Rockingham County Dear Ms. Haynes: This Notice of Deficiency is being sent to you for failure to submit the 2014 annual report. One of the requirements of your non-discharge permit is the submittal of an annual report to the Division of Water Resources by March 1st of each year. As of this date, our records indicate that the 2014 annual report has not been submitted for the subject facility. Failure to act in accordance with the terms, conditions, or requirements of your permit may result in a recommendation of enforcement action, in accordance with North Carolina General Statute §143-215.6A. Please respond to this Notice of Deficiency within 15 calendar days of its receipt, either by submitting three copies of the annual report or records indicating the report was submitted. Submit to: Ed Hardee Division of Water Resources Non-Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Non-Discharge Permitting Unit 1617 Mail Service Center,Raleigh,North Carolina 27699-1617 Phone:919-807.64641 Internet:htt ://oortalncdenr.ora/web/wq An Equal Opportunity\Affirmative Action Employer—Made in part with recycled paper Nothing in this letter should be taken as relieving from you the responsibility for failing to submit the annual report in a timely manner. A decision as to the appropriateness of an enforcement action will be made.following the receipt of your response. If you have any questions regarding this letter, please contact Ed Hardee of our Central Office staff at ed.hardeea_ncdenr.gov or (919) 807-6319. Sincerely, on Ri aard, Branch Manager Division of Water Resources Permit Files iv.e i s o.594 North Carolina Department of Environment and Natural Resources Pat McCrory John E. Skvarla, III Governor Secretary October 2,2014 Lisa Haynes—Corporate Environmental Manager Unifi, Inc. P.O.Box 1437 Reidsville,NC 27323 Subject: Permit No. WQ0006594 Unifi,Inc.Distribution of Industrial Pretreatment Residuals Rockingham County Dear Ms. Haynes: In accordance with your permit renewal request received June 26, 2014, and subsequent additional information received September 15,2014,we are forwarding herewith Permit No.WQ0006594 dated October 2, 2014, to Unifi, Inc. for the continued operation of the subject residuals management program.Note that plant No. 15 is no longer owned by the Permittee and removed from the permit. This permit shall be effective from the date of issuance until September 30, 2019, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachments A for they may differ from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note that on September 1, 2006, North Carolina Administrative Code Title 15A Subchapter 02T — Waste not Discharged to Surface Waters was adopted. Accordingly, this permit incorporates the requirements of these rules, therefore, please take the time to review this permit thoroughly. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this matter, please contact Chonticha McDaniel at (919)807-6337 or chonticha.mcdaniel@ncdenr.gov. Sincerely, r Thom s A.Reeder,Director Division of Water Resources 1636 Mail Service Center,Raleigh,North Carolina 27699-1636 Phone:919.807-64641 Internet:httmlloortal.ncdenr.orohueblwq An Equal Opportunity i ANirmative Action Employer-Made in part with recycled paper Ms.Haynes October 2,2014 Page 2 of 2 cc: Rockingham County Health Department(Electronic Copy) Winston-Salem Regional Office,Water Quality Regional Operations Section(Electronic Copy) Roy Whitaker—EMA Resources,Inc.(Electronic Copy) Beth Buffington—Protection and Enforcement Branch(Electronic Copy) Digital Permit Archive(Electronic Copy) Central Files If you have any questions regarding this letter, please contact Ed Hardee of our Central Office staff at(919) 715-6189. Sincerely Kim H. Colson, P.E., Supervisor Land Application Unit KHC:eh cc: 11.111101111.110.1111111.1111. APS Central Files Land Application Unit FWaTF O�� RpL Michael F.Easley,Governor y William G.Ross Jr.,Secretary r North Carolina Department of Environment and Natural Resources -S" Coleen H.Sullins,Director Division of Water Quality June 11, 2008 RECEIVED N.C.Dept.of ENR CERTIFIED MAIL#7006 2150 0003 5466 7356 JUN 1 3 2008 RETURN RECEIPT REOUESTED Winston-Salem Regional Office Lisa M. Haynes «l Unifi Inc. Post Office Box 1437 Reidsville, NC 27323-1437 Subject: NOTICE OF VIOLATION (NOV-2008-PC-0410) FAILURE TO SUBMIT ANNUAL REPORT Permit No. WQ0006594 Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids Rockingham County Dear Ms. Haynes: One of the requirements of your non-discharge permit is the submittal of an annual report to the Division of Water Quality by March 1st of each year. As of this date, our records indicate that the 2007 annual report has not been submitted for the subject facility. Failure to act in accordance with the terms, conditions, or requirements of your permit may result in the assessment of civil penalties of up to $25,000.00 per violation per day, in accordance with North Carolina General Statute §143-215.6A. Please respond to this notice of violation within 15 calendar days of its receipt, either by submitting three copies of the annual report or records, indicating the report was submitted. Submit to: Ed Hardee Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Nothing in this letter should be taken as relieving from you the responsibility for failing to submit the annual report in a timely manner. A decision as to the appropriateness of an enforcement action will be made following the receipt of your response. Nam` Carolina Vaturall Aquifer Protection Section 1636 Mail Service Center Raleigh,NC 27699-1636 Telephone: (919)733-3221 Internet:http://h2o.enr.state.nc.us 2728 Capital Boulevard Raleigh,NC 27604 Fax 1: (919)715-0588 Fax 2: (919)715-6048 An Equal Opportunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper Customer Service: (877)623-6748 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH DISTRIBUTION OF INDUSTRIAL PRETREATMENT RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143,General Statutes of North Carolina as amended,and other applicable Laws,Rules,and Regulations PERMISSION IS HEREBY GRANTED TO Unifi, Inc. Rockingham County FOR THE continued operation of a residuals management program for Unifi, Inc. and consisting of the distribution of industrial pretreatment residuals generated by the approved facilities listed in Attachment A with no discharge of wastes to surface waters,pursuant to the application received June 26, 2014,and subsequent additional information received by the Division of Water Resources, and in conformity with other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Pennittee from complying with the federal regulations. This permit shall be effective from the date of issuance until September 30, 2019, and shall be subject to the following specified conditions and limitations: SCHEDULES 1. No later than 180 days of following the effective date of this permit, the Permittee shall be able to demonstrate compliance and meet the monitoring and reporting requirements of pathogen and vector attraction reduction. Exception from meeting the vector attraction reduction requirement may be granted if the Permittee is able to provide documentation to justify that vector attracting potential in the residuals is not present or insignificant. 2. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein,and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. WQ0006594 Version 3.0 Shell Version 140324 Page 1 of 10 II. PERFORMANCE STANDARDS 1. The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Winston-Salem regional office supervisor, and take any immediate corrective actions. 2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. 3. Only residuals generated by the facilities listed in Attachment A are approved for distribution in accordance with this permit. 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations(i.e.,dry weight basis): Ceiling Concentration Monthly Average Parameter Concentration (milligrams per kilogram) (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106(a)and(b). Exceptions to this requirement shall be specified in Attachment A. 6. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are distributed shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. WQ0006594 Version 3.0 Shell Version 140324 Page 2 of 10 7. Setbacks for Class A land applied bulk residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake* Private or public water supply 100 100 Surface waters(streams—intermittent and perennial, 100 25 perennial waterbodies,and wetlands) Surface water diversions(ephemeral streams, 25 0 waterways,ditches) Groundwater lowering ditches(where the bottom of • 25 0 the ditch intersects the SHWT) Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 * Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing,as well as can be handled, transported and spread as a solid(e.g., using a backhoe, front end loader, clinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind. 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre-approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.php). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods(a)or(b)above,the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service,or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document:Chapter 1 (http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100 109.pdf). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. WQ0006594 Version 3.0 Shell Version 140324 Page 3 of 10 9. The Permittee shall not distribute industrial pretreatment residuals that have a sodium adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content; has agreed on proper residual application rates;and has agreed to operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service,a North Carolina Licensed Soil Scientist,or an agronomist. III. OPERATION AND MAINTENANCE REOUIREMENTS 1. The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non-discharge system to prevent any contravention of surface water or groundwater standards. 2. The Permittee shall maintain an approved Operation and Maintenance Plan(O&M Plan)pursuant to 15A NCAC 02T .1110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan.The O&M Plan,at the minimum,shall include: a) Operational functions; b) Maintenance schedules; c) Safety measures; d) Spill response plan; e) Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f) Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). 3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,or as specified in the most recently approved O&M plan(i.e.,see Condition 111.2), and shall comply with all other conditions of 15A NCAC 08G.0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Technical Assistance&Certification.Unit at(919)733-0026. WQ0006594 Version 3.0 Shell Version 140324 Page 4 of 10 4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. 6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. 7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. 8. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; £ During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18%for injected or incorporated bulk liquid residuals; h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0,or if an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations to the acceptable soil pH(6.0)will be noted in this permit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no-till program shall be exempted from meeting this vegetative cover requirement; j. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 1. Application exceeds agronomic rates. 9. A Utilization Agreement between the Permittee and the entity agreeing to accept and distribute Class A bulk residuals shall be in place prior to distribution of the bulk residuals. The agreement shall specify the agreeing entity's responsibilities. The Permittee or his designee and the person responsible for application of the residuals shall sign the Utilization Agreement, which shall be considered expired concurrent with the permit expiration date,and shall be renewed during the permit renewal process. WQ0006594 Version 3.0 Shell Version 140324 Page 5 of 10 • 10. At a minimum,the Utilization Agreement shall stipulate the following: a. By agreeing to accept the bulk Class A residuals, it is recognized that the application of these residuals is allowed under the conditions of this agreement.Land application of Class A residuals is considered the beneficial reuse of a waste under 15A NCAC 02T .1100, and has been deemed permitted under 15A NCAC 02T.1103(4)provided the conditions of this agreement are met.Any action resulting in damages to surface water or groundwater, caused by failure to follow the conditions of this agreement, is subject to Division enforcement action; b. The person or entity accepting the bulk Class A residuals shall to the best of their knowledge meet the following application requirements: i. List all prohibitions under Condition 111.8 with a statement that bulk residuals shall not be land applied under these conditions. ii. Industrial Pretreatment Residuals shall not be stockpiled for more than 30 days prior to land application; iii. Application of bulk residuals shall not occur within 100 feet of a public or private water supply source; iv. Application of bulk residuals shall not occur within 100 feet of any well, with the exception of Division approved monitoring wells; v. Application of bulk residuals shall not occur within 25 feet of surface waters. c. The generator of the Class A bulk residuals shall provide information on the proper use of the residuals, including information on the nutrient quantities within the residuals and recommended application rates. A copy of the label or information sheet attached to bags or other containers,as specified in the labeling requirements under Condition 1II.12, is sufficient; d. The applicator or party accepting bulk residuals from the Permittee shall supply all third parties receiving bulk residuals with documentation specifying that application shall occur consistent with the utilization agreement; e. Instructions, including contact information for key personnel, shall be provided to the applicator or party receiving bulk residuals in the event that any requirements specified in the utilization agreement are not met. f. A copy of the Utilization Agreement shall be maintained at the land application sites when bulk residuals are being applied. 11. All residuals shall be adequately stored to prevent untreated leachate runoff. The fmished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to the buyer. If an alternate storage site is used,approval must be obtained from the Division. 12. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum,the label or information sheet shall contain the following: a. The name and address of the person who prepared the residuals; b. A statement that residual land application is prohibited except in accordance with the instructions on the label or information sheet; c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use. 13. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement. WQ0006594 Version 3.0 Shell Version 140324 Page 6 of 10 14. All leachate shall be reused as a wetting agent for the processing of residuals or routed to the head of the treatment plant. IV. MONITORING AND REPORTING REQUIREMENTS 1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. 2. Residuals shall be analyzed to demonstrate they are non-hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)I shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters(the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene(7.5) Nitrobenzene(2.0) Barium(100.0) 1,2-Dichloroethane(0.5) entachlorophenol(100.0)' Benzene(0.5) 1,1-Dichloroethylene(0.7) yridine .0)-` Cadmium(1.0) 2,4-Dinitrotoluene(0.13) Selenium(1.0) Carbon tetrachloride(0.5) Endrin(0.02) Silver(5.0) Chlordane(0.03) Hexachlorobenzene(0.13) 4etrachloroethylene 7) Heptachlor(and its hydroxide) Chlorobenzene(100.0) (0.008) Toxaphene(0.5) Chloroform(6.0) Hexachloro-1,3-butadiene(0.5) (richl ero 0o thylene(0j Chromium(5.0) Hexachloroethane(3.0) 2,4,5-Trichlorophenol(400.0) Tm-Cresol 0 0) Lead(5.0) 2,4,6-Trichlorophenol(2.0) o-Cresol(200.0)\\ Lindane(0.4) 2,4,5-TP(Silvex)(1.0) p-Cresol(200.0) Mercury(0.2) Vinyl chloride(0.2) Cresol(200.0)1 Methoxychlor(10.0) 2,415{ .0) (--ethyl ethyl ketone(200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A,the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. WQ0006594 Version 3.0 Shell Version 140324 Page 7 of 10 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia-Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate-Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. 5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. 6. The Permittee shall maintain records tracking all bulk residual distribution or land application events performed by the Permittee. At a minimum,these records shall include the following: a. Source of residuals; b. Date of distribution/land application; c. Name and address of recipient of residuals; d. Volume of residuals distributed to each recipient; e. Intended use of residuals; f. If land application events performed by the Permittee - Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website,the printout page shall be kept on file and reprinted every five years). 7. Three copies of an annual report shall be submitted on or before March 1st. The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http://portal.ncdenr.org/web/wq/aps/lau/reporting, or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh,North Carolina 27699-1617 WQ0006594 Version 3.0 Shell Version 140324 Page 8 of 10 8. Noncompliance Notification The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (336) 771-5000, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the distribution program resulting in the land application of significant amounts of wastes that are abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to surface waters. c. Any time self-monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting(e.g.,discharges to surface waters,imminent failure of a storage structure, etc.)outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number(800)662-7956,(800)858-0368,or(919)733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. 2. When the Permittee land applies bulk residuals, prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. 3. Any duly authorized Division representative may, upon presentation of credentials,enter and inspect any property,premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater,surface water or leachate samples. VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215.6C. 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. WQ0006594 Version 3.0 Shell Version 140324 Page 9 of 10 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state,and federal). Of particular concern to the Division are applicable river buffer rules in I5A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000;any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. 5. In the event the residuals program changes ownership or the Permittee changes their name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. 6. This permit is subject to revocation or unilateral modification upon 60 days notice from the Division Director,in whole or part for the requirements listed in 15A NCAC 02T.0110. 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T.0120(b). 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit pursuant to 15A NCAC 02T.0105(e)(3). Permit issued this the 2"d day of October 2014 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION „r £ cder,Director Divi ion of Water Resources By Authority of the Environmental Management Commission Permit Number WQ0006594 WQ0006594 Version 3.0 Shell Version 140324 Page 10 of 10 ATTACHMENT A-Approved Residual Sources Certification Date: October 2,2014 Unify Inc. Permit Number: WQ0006594 Version:3.0 Monitoring Monitoring Monitoring Approved Maximum Frequency for Owner Facility Name County Permit Number Biological Dry Tons Frequency for Frequency for Pathogen& Mineralization Residuals Per Year' Non-hazardous Metals and Rate Characteristics 2 Nutrients 3 Vector Attraction Reductions Unifi,Inc. Unifi,Inc.Dyed Operations Reidsville Rockingham R-0002 Yes 100 Annually Annually Annually 0.30 Total 100 I. Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility. 2. Analyses to demonstrate that residuals are non-hazardous(i.e.,TCLP,ignitability,reactivity,and corrosivity)as stipulated under permit Condition 1V.2. 3. Testing of metals and nutrients as stipulated under permit Condition 1V.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition 1V.4. Page 1 of 1 Compliance Inspection Report Permit: WQ0006594 Effective: 08/26/05 Expiration: 07/31/14 Owner: Unifi Inc SOC: Effective: Expiration: Facility: Unifi,Inc.Plants 2 and 15 Distribution of Residual Sc County: Rockingham PO Box 698 Region: Winston-Salem Yadkinville NC 27055 Contact Person: Timothy Cole Title: Phone: 910-679-8891 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): L1 s� Hay nc s - 33c •3 8LSIIr 9-050Y- doh s°,^ 33(2 41 ;•8812-(vv.) ✓�0-7-33,16s+) Related Permits: NC0021873 Town of Mayodan-Mayodan VWVTP NC0024881 City of Reidsville-Reidsville WWTP o4(ue 64 01 Entry f gyp, 3L1 PC Inspection Date: --0,084f1977- Ent ime: ?J0A. - Exit Time: Primary Inspector: Stephen Berry Phone: 336-771-5000 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Distribution of Residual Solids(503 Exempt) Facility Status: ❑ Compliant ❑ Not Compliant Question Areas: ▪ Miscellaneous Questions II Record Keeping Treatment ▪ Sampling Transport aLt)Dyevs (See attachment summary) \orty /wk - „ ralim 3w/ix/opts Irla . y vv ,f ooK avl I�1os N ; � +2 tad s Z b1�� r-fit- ifav,ilt; Vilks eykiim.41,c) p„0-1- 1,4m&D,) I•.. 41 o' Z - �«f�row•^- v d �� V�(� �(M"�}�i G '[a �l S - 1VIkia I 0). t-JL L„,_ I � J�`C Iy C�✓ I`I�'�tiJ \4).%. I;eV S fi flekbliCrnt (ryf'. ri,t40) Page: 1 N'cV, daivit14 1ciciodivv13 kty zPv"'fS Tor l&Ac ri( l_ ,. Li I f: r.-- L, Permit WO0006594 Owner-Facility:Unifi Inc Inspection Date: 07/04/1976 Inspection Type:Compliance Evaluation Reason for Visit: Routine Inspection Summary: Page: 2 Permit: W00006594 Owner-Facility:Unifi Inc Inspection Date: 07/04/1976 Inspection Type:Compliance Evaluation Reason for Visit: Routine Record Keeping Yes No NA NE Is GW monitoring being conducted,if required? 0 ❑ 0 Are GW samples from all MWs sampled for all required parameters? 0 0 Q ❑ Are there any GW quality violations? 0 ❑ 0 0 Is GW-59A certification form completed for facility? 1 0 ❑ Q 0 Is a copy of current permit on-site? j, �► i N w tow r JO1bv. S Are current metals and nutrient analysis available? 000Y Are nutrient and metal loading calculating most limiting parameters? El o ❑ a. TCLP analysis? 0 ❑ 0 b. SSFA(Standard Soil Fertility Analysis)? El ❑ d Are PAN balances being maintained? 0 0 ❑ Are PAN balances within permit limits? ID El Has land application equipment been calibrated? 0 ❑ Are there pH records for alkaline stabilization? El 0 ❑ Are there pH records for the land application site? ❑ El Elio Are nutrient/crop removal practices in place? ❑ [!l CI Do lab sheets support data reported on Residual Analysis Summary? 0 ❑ 0 Er Are hauling records available? d Are hauling records maintained and up-to-date? ❑ 0 ❑ #Has permittee been free of public complaints in last 12 months? d Has application occurred during Seasonal Restriction window? @❑ Comment: Treatment Yes No NA NE Check all that apply Aerobic Digestion Anaerobic Digestion Alkaline Pasteurization(Class A) Alkaline Stabilization(Class B) Compost El Drying Beds Other Comment: Sampling Yes No NA NE Describe sampling: Is sampling adequate? Page: 3 Permit: WQ0006594 Owner-Facility:Unifi Inc Inspection Date: 07/04/1976 Inspection Type:Compliance Evaluation Reason for Visit: Routine Is sampling representative? ❑ ❑ ❑ ❑ Comment: Transport Yes No N•,�'h Is a copy of the permit in the transport vehicle? 0 0 P! II Is a copy of the spill control plan in the vehicle? 0 0 !! II Is the spill control plan satisfactory? 0 0 Pi II Does transport vehicle appear to be maintained? 0 0 f i i1 Comment: Page: 4 State of North Carolina P Department of Environment and Natural Resources RDivision of Water Resources Division of Water Resources Water Quality Regional Operations Section Staff Report To: Non-Discharge Permitting Unit Application No.: WQ0006594 Attn: Chonticha McDaniel Regional Login No.: From: Stephen Berry Choose an item. Regional Office I. GENERAL SITE VISIT INFORMATION 1. Was a site visit conducted? ® Yes or❑ No a. Date of site visit: 08/26/2014 b. Site visit conducted by: Stephen Berry c. Inspection report attached? ❑ Yes or® No d. Person contacted: Lisa Haynes and their contact information: (336)348 - 6516 ext. n/a e. Driving directions: WSRO — US 52N — Bus40E- HWY 158N- Left on Reid School Rd. — Right on Vance Street Ext. (Facility on left/north side) II. PROPOSED FACILITIES FOR NEW AND MODIFICATION APPLICATIONS 1. Facility Classification: (Please attach completed rating sheet to be attached to issued pe • 2. Are the new treatment facilities adequate for the type of waste and disposal system? ❑ Yes / No If no, explain: 3. Are site conditions(soils,depth to water table, etc)consistent with the submitte• sorts? ❑ Yes ❑No ❑N/A If no, please explain: 4. Do the plans and site map represent the actual site(property lines,w- , etc.)? ❑ Yes ❑No ❑N/A If no, please explain: 5. Is the proposed residuals management plan adequate? • s ❑No ❑N/A If no, please explain: 6. Are the proposed application rates(e.g., hydra • ,nutrient)acceptable? ❑ Yes ❑No ❑ N/A If no, please explain: 7. Are there any setback conflicts for pr• ..sed treatment, storage and disposal sites? ❑ Yes or❑No If yes, attach a map showing con • areas. 8. Is the proposed or existing • .undwater monitoring program adequate? ❑ Yes ❑No ❑N/A If no, explain and reco s• end any changes to the groundwater monitoring program: 9. For residuals,wi easonal or other restrictions be required? ❑ Yes ❑ No ❑ N/A If yes, attac of sites with restrictions(Certification B) FORM: WQROSSR 02-14 Page 1 of 3 III.EXISTING FACILITIES FOR MODIFICATION AND RENEWAL APPLICATIONS 1. Are there appropriately certified Operators in Charge(ORCs)for the facility? ❑ Yes ®No❑N/A ORC: Certificate#: Backup ORC: Certificate#: 2. Are the design,maintenance and operation of the treatment facilities adequate for the type of waste and disposal system? ® Yes or❑No If no,please explain: n/a 3. Are the site conditions(e.g., soils,topography, depth to water table, etc)maintained appropriately and adequately assimilating the waste? ❑ Yes or❑No 503 Exempt If no, please explain: n/a 4. Has the site changed in any way that may affect the permit(e.g., drainage added,new wells inside the compliance boundary, new development,etc.)? ❑ Yes or❑No 503 Exempt If yes, please explain: n/a 5. Is the residuals management plan adequate? ® Yes or❑ No If no,please explain: n/a 6. Are the existing application rates(e.g., hydraulic,nutrient) still acceptable? ❑ Yes or❑No 503 Exempt If no, please explain: SAR/ESP may be an issue 7. Is the existing groundwater monitoring program adequate? ❑ Yes❑No ®N/A If no, explain and recommend any changes to the groundwater monitoring program: n/a 8. Are there any setback conflicts for existing treatment, storage and disposal sites? ❑ Yes or®No If yes,attach a map showing conflict areas. 9. Is the description of the facilities as written in the existing permit correct? ❑Yes or®No If no, please explain: No description in permit;treatment works last updated— 1996 10. Were monitoring wells properly constructed and located? ❑ Yes❑No ®N/A If no,please explain: n/a 11. Are the monitoring well coordinates correct in BIMS? ❑ Yes ❑No ®N/A If no,please complete the'following(expand table if necessary): Monitoring Well Latitude Longitude O , „ 0 , „ O , If 0 , „ O , „ 0 , „ O , „ 0 , „ O , „ 0 , „ 12. Has a review of all self-monitoring data been conducted(e.g.,NDMR,NDAR, GW)? ❑Yes or®No Please summarize any findings resulting from this review: n/a 13. Are there any permit changes needed in order to address ongoing BIMS violations? ❑ Yes or®No If yes,please explain: Only violations(in BIMS)were failure to submit Annual Report 14. Check all that apply: ®No compliance issues ❑ Current enforcement action(s) ❑ Currently under JOC ❑Notice(s)of violation ❑ Currently under SOC ❑ Currently under moratorium Please explain and attach any documents that may help clarify answer/comments(i.e.,NOV,NOD,etc.) 15. Have all compliance dates/conditions in the existing permit been satisfied? ® Yes ❑No ❑N/A If no,please explain: n/a �.. 16. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit? ❑ Yes ®No ❑N/A If yes,please explain: n/a FORM: WQROSSR 02-14 Page 2 of 3 IV. REGIONAL OFFICE RECOMMENDATIONS 1. Do you foresee any problems with issuance/renewal of this permit? n Yes or® No If yes,please explain: n/a 2. List any items that you would like APS Central Office to obtain through an additional information request: Item Reason ORC Designation Form WSRO does not have record of ORC/back-up on file;BIMS does not list an ORC. Update SOP/O&M Tab 6 of Application Packet, under 7.6(Inspection Plan): Lists incorrect number document for DENR; should be 800-858-0368. Narrative Description of Current permit does not include a narrative of treatment works(EQ basin, Treatment Works lagoon, clarifier,digester). 3. List specific permit conditions recommended to be removed from the permit when issued: Condition Reason II.2. Plant No. 15 is no longer owned by Unifi(as of 2012); remove Mayodan plant as a source. 4. List specific special conditions or compliance schedules recommended to be included in the permit when issued: Condition Reason 5. Recommendation: n Hold,pending receipt and review of additional information by regional office ® Hold, pending review of draft permit by regional office ❑ Issue upon receipt of needed additional information n Issue ❑ Deny(Please state asons: )(7 6. Signature of report preparer: //// Q-✓ Signature of APS regional supervisor: Date: 08/26/2014 V. ADDITIONAL REGIONAL STAFF REVIEW ITEMS Patrick Mitchell will be reviewing the draft permit FORM: WQROSSR 02-14 Page 3 of 3 WATER QUALITY REGIONAL OPERATIONS SECTION APPLICATION REVIEW REQUEST FORM Date: July 9, 2014 RECEIVED N.C.Dept.of ENR To: WSRO-WQROS: Corey Basinger/ Sherri Knight JUL 1 1 2014 WI ton-Salem From: Chonticha McDaniel, Water Quality Permitting Section-Non-Discharge P rmitti office Telephone: (919) 807-6337 Fax: (919) 807-6496 E-Mail: chonticha.mcdaniel@ncdenr.gov A. Permit Number: WQ0006594 B. Applicant: Unifi Inc C. Facility Name: Unifi,Inc.,Plants 2 and 15 Residuals Distribution D. Application: Permit Type: Distribution of Residual Solids (503 Exempt) Project Type:Renewal E. Comments/Other Information: ❑ I would like to accompany you on a site visit. Attached, you will find all information submitted in support of the above-referenced application for your review, comment, and/or action. Within 45 calendar days, please take the following actions: ® Return a completed WQROSARR Form. ® Return a completed WQROSRSR Staff Report ❑ Attach a classification rating sheet. ❑ Attach Well Construction Data Sheet. ❑ Attach Attachment B for Certification. ❑ Issue an Attachment B Certification. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: S+42.4)L.le"r1(4—‘ Date: 416-1i L't 1 /L 011 , .` , '/21 ,007 A�-.".r..7� i��/� �'Vtl / FORM: WQROSARR 02-14 Page 1 of 1 ArtA NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory John E. Skvarla, III Governor Secretary July 9,2014 Lisa Haynes—Corp. Environmental Management Unifi, Inc PO Box 1437 Reidsville,NC 27323 Subject: Acknowledgement of Application No. WQ0006594 Unify Inc. Residuals Management System Scotland County Dear Ms. Haynes: The Water Quality Permitting Section acknowledges receipt of your permit application and supporting documentation received on June 26, 2014. Your application package has been assigned the number listed above, and the primary reviewer is Chonticha McDaniel. Central and Winston-Salem Regional Office staff will perform a detailed review of the provided application, and may contact you with a request for additional information. To ensure maximum efficiency in processing permit applications, the Division of Water Resources requests your assistance in providing a timely and complete response to any additional information requests. Please note that processing standard review permit applications may take as long as 60 to 90 days after receipt of a complete application. If you have any questions, please contact Chonticha McDaniel at(919) 807-6337 or chonticha.mcdaniel@ncdenr.gov. Sincerely, Jon Risgaard, Supervisor Division of Water Resources cc: iiiimainftimilmiumillift Water Quality Regional Operations Section Roy Whitaker—EMA Resources, Inc., 755 Yadkinville Rd, Mocksville NC 27028 Permit File WQ0006594 • 1636 Mail Service Center,Raleigh,North Carolina 27699-1636 Phone:919-807-64641 Internet:http:llportal.ncdenr.oro/weblwq An Equal Opportunity\Affirmative Action Employer—Made in part with recycled paper N2. = Z3 Ca = 4J 2 11 - = z" 2 M47L- ivto L-4-- Ca ',tool = 5�a Skg bEj ys(cc�i-, +Mi1)f `i 297V J .S-(c,t,�,t z s s N a - Cct!5,c, � 2°115 ZS era 37z. s 11, 3 lsy. Ip s Z1, 1%o Ec P ,,,/ Gz L �f S = 5' 5-4.d Z. Z -- /'l ts loo 7� —Resources, Inc. Permit Renewal Application For Unifi, Inc. WQ0006594 Unifi WWTP Distribution of Residual Solids (503 Exempt) Prepared By: EMA Resources Inc. 755 Yadkinville Road Mocksville, NC 27028 336-751-1441 June 27, 2014 Phone 336.751.1441 —Fax 336.751.1442 755 Yadkinville Road—Mocksville,NC 27028 TEMA Inc. ry RECEIVED June27, 2014 N.C.Dept.of ENR JUL 112014 Division of Water Resources Winston-Salem R-!Tonal Office Aquifer Protection Section Land Application Unit 512 N. Salisbury Street RECEi��Ft��C►ENh�/D�R Raleigh, NC 27604 JUN 2 6 2014 RE: Permit Renewal Application, Permit No. WQ0006594 Water Quality Permitting Section Mr. Jon Risgaard, Unit Supervisor On behalf of Unifi, Inc, you will find included in this permit application the following: Cover Letter, Distribution of Residuals Solids Form (503 Exempt), and supporting documentation. Please note that each form is supplemented with its accompanying attachments and are clearly identified on the accompanying tab. If you have any questions concerning this application, please contact Roy Whitaker at: office: 336-751-1441 or mobile: 336-909-1718. Respectfully, EMA Resources Inc. Roy L. Whitaker Director Business Development/Operations Phone 336.751.1441 - Fax 336.751.1442 755 Yadkinville Road— Mocksville,NC 27028 Roy Whitaker .om: Haynes, Lisa - Reidsville <LHAYNES@UNIFI.COM> Thursday,June 12, 2014 9:34 AM To: 'roy.whitaker@emaresourcesinc.com'; brent.collins@emaresourcesinc.com Subject: FW: Permit renewal WQ0006594 Importance: High Gentlemen: Please see response from DENR regarding permit renewal application. Are we still on schedule for June 27`h? Sincerely, Lisa Haynes Corporate Environmental Manager Unifi Manufacturing, Inc. Phone: 336.348.6516 Mobile: 336.580.7334 Fax: 336.348.6586 Web: www.unifi.com R CR6VRDiDENR/p R web: www.repreve.com JUN 2G 2014 Water Quality Permitting Section From: Risgaard, Jon [mailto:jon.risgaard@ncdenr.gov] Sent: Thursday, June 12, 2014 9:30 AM To: Haynes, Lisa - Reidsville Cc: Mitchell, Patrick; Knight, Sherri Subject: Permit renewal WQ0006594 Lisa, Thank you for sending the written request for an extension of the Distribution of Residual Solids permit renewal date for permit#WQ0006594 issued to Unifi, Inc. With this email your permit renewal date is extended to June 27, 2014. Please note that your permit expires on 7/31/2014,and if the permit renewal application is not received prior to permit expiration you will be operating without a valid permit, and any residuals application that occurs without a valid permit would be subject to enforcement. Please keep a copy of this email for your records, and include a copy of it with your renewal application. Jon n Risgaard - Supervisor, Non-Discharge Permitting Unit ter Quality Permitting Section 1636 Mail Service Center Raleigh, NC 27699-1636 1 \ 1 FORM DCAR \ J I 2 EXISTING PERMIT J ( \ 3 SITE LOCATION/PROCESS FLOW \ 1 ( \ 4 PROGRAM INFO SHEET \ J ( \ 5 RESIDUALS INFO SHEET \ J ( \ 6 OPERATIONS AND MAINTENANCE PLAN \ J I \ 7 NUTRIENTS& METALS ANALYSIS \ J I 8 TCLP ANALYSIS \ J State of North Carolina Dw R Department of Environment and Natural Resources Division of Water Resources Division of Water Resources 15A NCAC 02T.1100—DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 11-13&SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non-Discharge Permitting Unit website at: http://portalncdenr.org/web/wq/aps/lau General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)residuals under 15A NCAC 02T.1100. Unless otherwise noted,the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals(FORM: DCAR 11-13): ® Submit the completed and appropriately executed Distribution of Class A Residuals(FORM: DCAR 11-13) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans,specifications,etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T.0106(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies)for application packages involving new or changes to treatment and storage units. B. Application Fee(New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environment and Natural Resources(NCDENR). ❑ STANDARD REVIEW — Submit the appropriate fee for all new and major modification applications as listed in the table below. STANDARD APPLICATION REVIEW FEES: Facility Classification New Permit I Major Modification ' Major(residuals permitted for distribution >3,000 dry tons/year) $1,310 $395 Minor(residuals permitted for distribution<3,000 dry tons/year) $810 $245 -A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter(All Application Packages) ® List all items included in the application package,as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 11-13 Page I of 3 D. Program Information(All Application Packages) ® Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. ®How the residuals will be processed/treated(attach process flow diagram). ® How leachate collection will be handled. ®Where the residuals will be stored until processed. ®How the final product will be distributed(packaging,bulk,etc.) ®What nutrients or other constituents(i.e. nitrogen, phosphorous, aluminum,calcium, etc.)are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth,or adversely impact soil quality. ® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: Name and address of the person who prepared the residual that is sold or given away. ® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ®A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ®Information on all applicable setbacks in accordance with 15A NCAC 02T.1 108(b). ®A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications(Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications,but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T.1108(a)on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T.1 104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN—NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations(Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 104(a). G. Environmental Assessments(May be Required—See 15A NCAC IC .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 11-13 Page 2 of 3 H. Operation and Maintenance Plan(New and Renewal Application Packages) ❑ For Modification Application, if there are any changes to the existing plan,submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T.1 110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs,etc. ® Safety measures; may include safety training program,manuals,signs,etc. ® Spill response plan; including control,containment,remediation,emergency contact information,etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s)and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements(e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE,INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS,SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON-DISCHARGE PERMITTING UNIT By U.S. Postal Service: By Courier/Special Delivery: 1636 MAIL SERVICE CENTER 512 N.SALISBURY STREET RALEIGH,NORTH CAROLINA 27699-1636 RALEIGH,NORTH CAROLINA 27604 TELEPHONE NUMBER: (919)807-6300 FAX NUMBER: (919)807-6496 INSTRUCTIONS FOR FORM: DCAR 1 1-13 Page 3 of 3 State of North Carolina Department of Environment and Natural Resources Division of Water Resources DWR Ivlslon of Water Resources 15A NCAC 02T.1100—DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 08-13 I. APPLICANT INFORMATION: I. Applicant's name: Unifi, Inc. Applicant type: ❑ Individual ®Corporation ❑General Partnership ❑ Privately-Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑County Signature authority's name per 1 5A NCAC 02T .0106: Lisa Haynes Title:Corporate Environmental Manager Applicant's mailing address: P.O.Box 1437 City: Reidsville State:NC Zip:27323- Telephone number: (336)348-6516 Email Address: lhaynes@unifi.com 2. Consultant's name: Roy Whitaker License Number(for P.E.): NA Affiliation: El On Staff ® Retained(Firm: EMA Resources, Inc.) Consultant's mailing address: 755 Yadkinville Road City: Mocksville State:NC Zip: 27028- Telephone number:(336)751-1441 Email Address: roy.whitakere,emaresourcesinc.com 3. Fee submitted:NA(See Instruction B) PERMIT INFORMATION: 1. Application is for(check all that apply):❑ new, El modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit,provide the following: Permit number: W00006594 Date of most-recently issued permit: August 26,2005 Date of most-recently certified Attachment A(if different than the permit): NA III. FACILITY INFORMATION: 1. Name of residuals processing facility: Unifi, Inc.—Dyed Operations City: Reidsville State:NC Zip:27323- Coordinates: Latitude: 36°21' 11.83" Longitude: 79°41'49.37" Datum:NAD83 Level of accuracy: .01" Method of measurement: GPS County where facility is located: Rockingham 2. Facility contact(person familiar with residuals preparation): Name: Lisa Haynes Title:Corporate Environmental Manager Mailing address: P.O. Box 1437 City: Reidsville State: NC Zip: 27323- Telephone number: (336)348-6516 E-mail address: lhaynes@unifi.com FORM: DCAR 11-13 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 730 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers,aeration basins,etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn(bulk); ❑home garden(bulk); other(explain); Bulk land application of liquid on crop and hay/pasture land. Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added per 1.0 dry ton of residuals(dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 50 dry tons per year. 4. Approximate amounts of the final product(processed residuals)to be.distributed: 50 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): The Unifi WWTP has a 0.5MG Aerobic Digester which also serves as the residuals storage tank. Currently, the residuals are thickened in the tank and lend application take place every 2-3 years, dependent on solids build-up. 6. Does the facility have a stormwater management plan? ® Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: The storage is in a tank and decant is pump back to the aeration basin. V. RESIDUALS SOURCE INFORMATION: (Not required if no new,renewed,or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. sS Residuals Source Certification FORM: DCAR 11-13 Page 2 of 3 Professional Engineer's Certification:(Application Involving New or Changes to Treatment or Storage Units) of Applicable ,attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal,Signature,and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule,and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ®Yes ❑ No, Explain; I, Lisa Haynes,Corporate Environmental Manager (Signature Authority's Name—PLEASE PRINT) (Title) :st that this application for Unifi Manufacturing, Inc. (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further,any discharge of residuals to surface waters or the land will result in an immediate enforcement action,which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed$10,000 as well as civil penalties up to$25,000 per violation. Signature: -LgaAlfr.2.5 Date: (e/Z./ t FORM: DCAR 11-13 Page 3 of 3 Of V4AT6'9 Michael F.Easley,Governor �O pG William G.Ross Jr.,Secretary r North Carolina Department of Environment and Natural Resources 0 Alan W.Klimek,P.E.,Director Division of Water Quality August 26,2005 MS. LISA HAYNES, ENVIRONMENTAL BIOLOGIST UNIFI,INCORPORATED POST OFFICE BOX 737 MADISON,NC 27027 Subject: Permit No. WQ0006594 Unifi,Incorporated Unifi,Inc. Plants 2 and 15 Distribution of Residual Solids Distribution/Land Application of Residuals from the Treatment of Other Wastewater Rockingham County Dear Ms.Haynes: In accordance with your permit renewal application package received on March 25, 2002 as well as the additional information received on October 29, 2003,we are forwarding herewith a renewed Permit No. WQ0006594, dated August 26, 2005, to Unifi, Incorporated for the operation of a program to • distribute residuals from the treatment of other wastewater. The product is a residual that is generated from the treatment of industrial wastewaters at the Unifi,Inc.Plant#2 at Reidsville,North Carolina under pre-treatment program permit R-0002 and at the Unifi Inc. Plant#15 at Mayodan, North Carolina under pre-treatment program permit M-0104. This permit shall be effective from the date of issuance until July 31,2010; shall void Permit No. WQ0006594, issued on April 22, 1997; and shall be subject to the conditions and limitations as specified therein. Make note of this permit's expiration date and the fact that a permit renewal application is due to the Division of Water Quality(Division)no later than six months prior to that date(i.e.,see Condition,VI. 7.), as the Division does not send reminders to apply for permit renewal. This permit approves the continued operation of the residuals land application program for another five-year cycle. As always, remember to take the time to review this permit thoroughly, as some of the conditions contained therein may have been added, changed, or deleted since the last issuance. Pay particular attention to the monitoring requirements in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. Please note that all domestic wastewater shall be kept separated from the subject industrial wastewaters at both Unifi Plants. A permit modification is required if domestic wastewater is ever mixed with the subject industrial residuals. Additional treatment facilities may be necessary to meet the requirements for Processes to Further Reduce Pathogens(PFRP)with domestic wastewater residuals. &DEEI Non-Discharge Permitting Unit Internet http://h2o.enr.state.nc.us/ndpu 1617 Mail Service Center,Raleigh,NC 27699-1617 Telephone (919)733-5083 Fax (919)715-6048 DENR Customer Service Center Telephone 1 800 623-7748 An Equal Opportunity Action Employer 50%recycled/10%post-consumer paper Ms. Lisa Haynes Page 2 August 26, 2005 If any parts, requirements, and/or limitations contained in this permit are unacceptable,you have the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the from of a written petition, conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need any additional information concerning this matter,please contact Mr. Duane Leith by telephone at(919)715-6186,or via e-mail at duane.leith@ncmail.net. Sincerely for Alan W. Klimek,P.E. cc: Mr. Chris Alexander,Precision Land Application, Inc. Rockingham County.Health Department Winston-Salem Regional Office-Aquifer Protection Section Technical Assistance and Certification Unit APS Central Files LAU Files LAU Residuals Program Coordinator 2 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH PERMIT FOR THE DISTRIBUTION/LAND APPLICATION OF RESIDUALS FROM THE TREATMENT OF OTHER WASTEWATER In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended,and other applicable Laws,Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Unifi, Incorporated Rockingham County FOR THE continued operation of a wastewater residuals facility for the distribution and marketing of residuals which meet exceptional quality standards throughout the State of North Carolina, consisting of the distribution of 200 dry tons per year of residuals from the sources listed in Condition II 2, with no discharge of wastes to surface waters, pursuant to the permit renewal application package received on March 25, 2002 as well as the additional information received on October 29, 2003 and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until July 31, 2010; shall void Permit No. WQ0006594, issued on April 22, 1997; and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS 1. The program for the distribution/land application of the residual product shall be effectively maintained and operated as a non-discharge system to prevent the discharge of any wastes to waters of the state resulting from the operation of this program. 2. This permit shall become voidable in the event of failure of the distribution/land application program to protect the assigned water quality standards of the surface waters and groundwater adequately. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwater resulting from the operation of the distribution/land application program. 1 4. In the event that the residuals distribution/land application program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall cease distributing/land applying residuals to the site, contact the Aquifer Protection Section of the appropriate Division of Water Quality's (Division) regional office, and take any immediate corrective actions as may be required by the Division. 5. Diversion or bypassing of untreated residuals or leachate from the wastewater and/or residuals treatment facilities shall be prohibited. 6. No residuals shall be stored at any location other than at the wastewater treatment facility at any time,unless approval has been requested and obtained from the Division. 7. All leachate must be reused as a wetting agent for the processing of residuals or routed to the head of the treatment plant. II. OPERATION AND MAINTENANCE REQUIREMENTS 1. The facilities and program shall be properly maintained and operated at all times. 2. No residuals other than the following are hereby approved for distribution in accordance with this permit: Permit Volume Source County Number (Dry Tons/Year) Unifi,Inc.Plant No.2 Reidsville Rockingham M-0104 100 City of Reidsville Unifi, Inc. Plant No. 15 Mayodan Rockingham R-0002 100 Town of Mayodan 3. Upon classification of the facilities by the Water Pollution Control System Operators Certification Commission (WPCSOCC), the Permittee shall employ a certified operator to be in responsible charge (ORC) of the residuals distribution/land application program. The operator shall hold a certificate of the type classification assigned to the residuals distribution/land application program by the WPCSOCC. The Permittee shall also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8G .0202. 4. For the residuals of exceptional quality to be distributed/land applied, the following shall be satisfied: 2 The Ceiling Concentrations(i.e., on a dry weight basis) and the Pollutant Monthly Average Concentrations(i.e., on a dry weight basis) shall be maintained: Ceiling Monthly Average Concentrations Concentrations Parameters (m2/kg) (m2/k2) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 --- Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 5. All residuals shall be adequately stored to prevent leachate runoff prior to and following treatment. The residuals may be stored in an elevated silo, placed on a concrete pad, kept under shelter, or covered until such time as it is distributed/land applied. If an alternative storage site is to be used,approval shall first be obtained from the Division. 6. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals treatment,storage,and/or distribution/land application fields onto adjacent property or into any surface waters. 7. A label shall be affixed to the bag or other container in which residuals that are sold or given away for application to the land, or an information sheet shall be provided to the person who receives the residuals sold or given away in an other container for application to the land. The label or information sheet shall contain the following information: a. The name and address of the person who prepared the residuals that is sold or given • away in a bag or other container for application to the land. b. A statement that application of the residuals to the land is prohibited except in accordance with the instructions on the label or information sheet. c. A statement which identifies that this material shall be prevented from entering any public or private water supply source(including wells) and any stream, lake,or river. d. Residuals shall not be applied to any site that is flooded,frozen or snow-covered. e. Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. III. MONITORING AND REPORTING REQUIREMENTS • 1. Any monitoring (i.e., including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to ensure protection of the environment shall be established and an acceptable sampling and reporting schedule shall be followed. 3 2. Proper records shall be maintained by the Permittee tracking all distribution/land application activities. The Permittee shall be responsible for developing and maintaining a consistent field numbering/identification system. Records shall contain, but shall not be necessarily limited to,the following information: a. Source,volume and analysis of each residuals, and b. Name of residuals' recipient, volume received and intended use 3. A residuals analysis shall be conducted annually from the date of permit issuance and any time that a change in the manufacturing process occurs. The results of all residuals analyses shall be maintained on file by the Permittee for a minimum of five years. If distribution/land application occurs at a frequency less than annually, a residuals analysis will be required for each instance of distribution/land application. The residuals analysis shall include, but shall not necessarily be limited to,the following parameters: Aluminum Magnesium Phosphorus msI k9 Ammonia-Nitrogen Mercury Potassium Arsenic Molybdenum Selenium Cadmium Nickel Sodium Calcium Nitrate-Nitrite Nitrogen Total Kjeldahl Nitrogen Copper Percent Total Solids Zinc Lead pH Plant Available Nitrogen (by calculation) 4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): rrn I 4. Arsenic (5.0) 1,4-Dichlorobenzene(7.5) Nitrobenzene(2.0) Barium(100.0) 1,2-Dichloroethane(0.5) Pentachlorophenol(100.0) Benzene(0.5) 1,1-Dichloroethylene(0.7) Pyridine(5.0) Cadmium(1.0) 2,4-Dinitrotoluene(0.13) Selenium(1.0) Carbon tetrachloride(0.5) Endrin(0.02) Silver(5.0) Chlordane(0.03) Hexachlorobenzene (0.13) Tetrachloroethylene(0.7) Chlorobenzene(100.0) Heptachlor(and its hydroxide) (0.008) Toxaphene(0.5) Chloroform(6.0) Hexachloro-1,3-butadiene(0.5) Trichloroethylene(0.5) Chromium(5.0) Hexachloroethane(3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol(200.0) Lead(5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol(200.0) Lindane (0.4) 2,4,5-TP(Silvex)(1.0) p-Cresol (200.0) Mercury(0.2) Vinyl chloride(0.2) Cresol(200.0) Methoxychlor(10.0) 2,4-D(10.0) Methyl ethyl ketone(200.0) -A After the residuals have been monitored annually for two ears the Permittee may submit a request to the Division for a permit modification to reduce the frequency of the TCLP analysis. In no case, however, shall the frequency of TCLP monitoring be less than once per permit cycle when residuals are distributed/land applied. 5. Three copies of all required monitoring and reporting requirements as specified in Condition III. 1., Condition III. 2., Condition III. 3., and Condition III. 4. shall be submitted annually on or before March 1s` of the year following the distribution/land application event to the following address: 4 Division of Water Quality Information ProcessingUnit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 6. Noncompliance Notification: The Permittee shall report by telephone to the Aquifer Protection Section of the Division's Winston-Salem Regional Office at telephone number(336)771-4600, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the residuals land application program that results in the land application of significant amounts of residuals that are abnormal in quantity or characteristic. b. Any failure of the residuals land application program resulting in a release of material to receiving waters. c. Any time that self-monitoring information indicates that the residuals land application program has gone out of compliance with the conditions and limitations of this permit or the parameters on which the program system was designed. d. Any process unit failure, due to known or unknown reasons, that render the residuals land application program incapable of adequate residuals treatment. e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site. Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS 1. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. V. INSPECTIONS • 1. The Permittee or his designee shall inspect the residuals storage, transport, and treatment facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority, upon request. 5 2. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property,premises or place on or related to the treatment site or facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS 1. This permit shall become voidable unless the residuals land application events are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by the Division. 2. This permit shall be effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes §143-215.6A through §143-215.6C. 4. The annual administering and compliance fee shall be paid by the Pennittee within 30 days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit, as specified by 15 NCAC 2H.0205 (c)(4). 5. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances that may be imposed by other government agencies (i.e., local, state, and federal)which have jurisdiction, including,but not limited to,applicable river buffer rules in 15A NCAC 2B .0200, soil erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000, and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 15A NCAC .0500. 6. This permit may be modified, revoked, and/or reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to protect the environment and public health adequately. 7. The Permittee, at least six months prior to the expiration of this permit, shall request its extension. Upon receipt of the request,the Division shall review the adequacy of the facilities and residuals land application program described therein, and if warranted, shall extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit shall not be automatically transferable. In the event that there is a desire for the residuals Iand application program to change ownership or to change the name of the Permittee, a formal permit request shall be submitted to the Division documentation from the parties involved and other supporting materials as may be appropriate. The approval of this request shall be considered on its merits and may or may not be approved. 6 Permit issued this the 26th day of August 2005. 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V? A I• {.11- 0 ik-,- ---• * .. CAMP DA1/19 TRL?: • telb, k . .. . Data use subject to license TN Scale 1 16,000 * 0 000 $OO 1200 1600 an 11 ©DeLorme Topo USA®8. mm(11 5.W)A 0 , as 420—see 700 ' ,_ www delorme corn ' 1"=1,333 3 ft Data Zoom 13-6 (----- ----------- Sta. 1 Sta. 2 18 il10=87 8t, n AEROBIC 14 DIGESTER To City ^ 15 Sta. 3 a19 17 �" , A j 16 � >' 1 I L. i Drain to Gravity #1 Station Feeed f Normal Flow Basin 11 Ij A i : „ I A f i 1 I A 12'Overflow 1MG —1 \ Bypass 710'Meter 9I-X _1 - B Meter ., > > > Sta. 5 2 ^ >3 Way Valve 8"Back 3 Way Volvos Porte & Flow / Sta. 6 Wash -->--'5r 4 ^ 20/ 5 / Bypass 2MG Overflow Bock Flush or Gravity Blow Drain Down {� Tank i From Reclaim Sys. From Plant 4 ate wge\Water_Waste Water\ Waste Water\ All Waste Water Tanks.dwg Program Information 1. Provide a narrative explaining the following: a. How will the materials be handled and transported from where the residuals were produced to where it will be treated? The wastewater plant residuals are solids that have been aerobically digested and thickened All residuals are handled by pumps and pipe lines onsite. b. How will the residuals be processed/treated(attach process flow diagram). The residuals are aerobically treated c. How will leachate collection be handled? Not Applicable. d. Where will the residuals be stored until processed? The residuals will be stored in the 0.5MG aerobic digester tank. e. How will the final product be distributed(packaging)? The residuals will be delivered to local farmers via 6500 gallon tanker loads. Each load will be off-loaded to a high flotation applicator for application on a receiver site (grassland or row crop). 2. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. The residuals have mainly nitrogen value,but they have additional micro nutrients that can be utilized by crops for optimum plant growth. The program will recruit local farmers to participate in the bulk land application program. They will be advised as to the nutrient value of the residuals,but they will be offered up to one ton of agricultural lime for soil pH adjustment where soil analysis indicates a need 3. Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain,at a minimum,the following information: Note:Residuals will be distributed through bulk land application of liquid managed by a contracted land application firm. See Attached Information Sheet (Attachment Order 1-d:Information Sheets) Residuals Information Sheet Generator: Unifi, Inc. Facility: Unifi, Inc. — Dyed Operations WWTP Address: P.O. Box 1437 (Vance Street) Reidsville, NC 27323 Phone: 336-348-6516 Contact: Lisa Haynes Land Application Contractor: EMA Resources Inc. 755 Yadkinville Road Mocksville, NC 27028 Phone: 336-751-1441 Contact: Roy Whitaker Please Note: The application of these residuals is only allowed in accordance with subject permit. (WQ0006594) All applicable setbacks in accordance with 15A NCAC 02T .1108(b) will be adhered and is the responsibility of the land application contractor. Application rates shall be applied at agronomic rates for intended uses. No residuals shall be applied to any site that is flooded, frozen or snow covered. Adequate procedures will be implemented to prevent surface runoff of residuals in any surface waters. The Attached Residuals Analysis Report is a summary of major and micro nutrients available in the residuals. If you have any question concerning this information, you may contact Unifi Manufacturing, Inc. or EMA Resources Inc. at the numbers listed above. RESIDUALS ANALYSIS REPORT PROJECT: Unifi, Inc Sample Date: 8/22/13 %Solids 1.14 pH: 8.07 CONVERSION TABLE PARAMETER % X 10000 = ppm dry wt. X 0.002 = lbs/dt Nitrogen TKN 4.74 47400 94.8 Phosphorus 0.79 7900 15.8 Potassium 0.29 2900 5.8 Sulfur 2.24 22400 44.8 Calcium 1.04 10400 20.8 Magnesium 0.27 2700 5.4 Sodium 6.85 68500 137 Ammonia N 0.35 3500 7 Nitrate N 1.77 17700.00 35.4 Iron 0.304 Ceiling 3040.00 6.08 Concent. Aluminum 0.31 m 3100.00 6.2 Chromium 0.0073 pp 73.00 0.146 Manganese 0.064 640.00 1.28 Copper 0.038 4300.00 380.00 0.76 Zinc 0.018 7500.00 180.00 0.36 Cadmium 0.0002 85.00 2.00 0.004 Nickel 0.0032 420.00 32.00 0.064 Lead 0.0007 840.00 7.00 0.014 Arsenic 0.0003 75.00 3.00 0.006 Mercury 0.00004 57.00 0.40 0.0008 Selenium 0.0005 175 00 5.00 0.01 Molybdenum 0.0005 75.00 5.00 0.01 PLANT AVAILABLE NITROGEN CALCULATION (PAN) MR (TKN-AmN) + .5(AmN) + NO3N X.002 = lbs. PAN/dt Surface 13170 1750 17700 65.24 MR (TKN-AmN) + AmN + NO3N X.002 = lbs. PAN/dt Injection 13170 3500 17700 68.74 Standard Operating Procedure and Operation and Maintenance Plan for the Unifi Manufacturing, Inc. Distribution of Class A Residuals Land Application Program 1. Purpose a. Ensure the requirements of the Unifi, Inc. Distribution of Class A Residuals Permit# W00006594 are met. 2. Personnel a. The following is a list of personnel in order they are to be contacted when information needs to be shared. i. EMA Resources inc. 1. Jeff Thompson - Project Manager 2. Roy Whitaker - Director of Business Development 3. Brent Collins - Director of Technical Services ii. Unifi Manufacturing, Inc. 1. Lisa Haynes, Corporate Environmental Manager 3. Operational Functions a. The operational function of this project it going to involve the aerobic digestion/mixing of the residuals via diffused air to achieve a well-mixed and consistent material that is suitable for land application. It is going to be spread at agronomic rates that are determined using the Realistic Yield Expectations (RYE) as outlined in the permit, the amount of other nutrient sources the landowner and operator has applied, and the residuals nutrient and metal sample that is current for that monitoring period. It is going to be spread with a liquid applicator that will use pressure to spread the material in such a way as to achieve a consistent spread pattern. The material is going to be land applied on fields that have a crop growing on them that are going to either be grazed or cut for animal feed. Application rates will be reduced by 25% on fields that are primarily used for grazing in accordance with USDA-NRCS 590. Grazed fields will be determined by the farmers and EMA project managers. 4. Maintenance Schedule a. EMA Resources Inc. will follow the maintenance schedule as recommended by the EMA Resources Operations Director (Mike Collins) for the equipment necessary to complete the job. 5. Safety Measures a. Unifi, Inc. and EMA Resources Inc. believe in operating in a safety conscious manner and all employees participate in safety training that is designed to help employees recognize safety issues and take steps to prevent accidents from occurring. In addition, EMA Resources employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. 6. Spill Response Plan a. In the unlikely event of a spill, the following action shall be taken immediately. i. Management of Spill Clean-up Activities: The EMA Resources Project Manager shall take immediate charge and initiate clean-up activities. EMA Resources labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from Unifi, Inc., The NC Department of Transportation, and other private contractors as necessary. ii. Halt the Source of the Spill: Such as a ruptured container or damaged transport unit. iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will be advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation. Ie. local farmers, farm supply centers, nurseries. iv. Initial Clean-Up: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw and sand soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. v. Final Clean-Up: Employ rotary brush sweeper if needed and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfactory of the property owner and state regulatory representatives. The ultimate goal will be restore the spill area to its original condition if possible. vi. Notification: As soon as possible after the spill occurs, the EMA Resources Project Manager or designee will notify the Unifi, Inc. and the EMA Resources main office. EMA Resources office staff is then responsible for notifying other key EMA Resources personnel. vii. Reporting: EMA Resources staff will notify the Winston Salem regional office of the NCDENR by telephone (336) 771-5000 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The EMA Project Manager shall provide a written report with 48 hours of the spill to the EMA Resources Director of Technical Services and Unifi, Inc. staff. The report shall list all relative information and actions taken. With the assistance of EMA Resources personnel, and the Unifi, Inc. personnel, a written report will be filed with the Winston Salem regional office within 5 days of the occurrence. For after hours reporting, the Division's emergency number shall be called to report all incidences (800) 662-7956. 7. Inspection Plan a. Inspection for the land application of residuals will conducted on a minimum of a weekly basis at the land application site during land application activities. The inspection frequency is based on the time frame that it is going to take to complete the project and the amount of dry tons to be land applied from this facility. The inspections will consist of inspecting a current field that is being applied as well as inspecting random fields that have been completed. Inspections will be conducted by Jeff Thompson - Project Manager. These inspections will consist of the following: i. Verifying the application rates for each field that plan on receiving material. ii. Checking the calculated loads to ensure the correct amount of residuals are being land applied. iii. Ensure that all manned equipment has a copy of the permit and the operation and maintenance plan. iv. Ensure that the field has been flagged properly and that all buffers are being adhered to. v. Ensure proper signage has been posted vi. Verify that the proper number of samples of the residuals have been taken and that it meets the criteria for land application. vii. The records will be kept in the EMA Resources project files in the main office. Copies of all analyses and records will be forwarded to Unifi, Inc. and kept on file. viii. EMA Resources and Unifi, Inc. staff will immediately inform the other party if any of the following conditions are noted. 1. Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. 2. Any failure of the distribution system that results in the release to surface waters. 3. Any time that self-monitoring indicates that the facility has gone out of compliance with the permit. 4. Any process failure that results in the system not adequately treating the residuals. 5. Any spill or discharge from a vehicle or piping system during residuals transportation. 6. Any release that requires immediate reporting outside normal business hours shall be called in by EMA Resources staff to DENR at (800) 662-795 This nu e called in the event of a release to surface waters or imminent failure o storage system when the event occurs outside of normal business hours. 0000.0051 • tg6t3 (11^1W)tr 8. Sampling and Monitoring Plan a. Sampling for this project consists of sampling the residuals prior to land application occurring in order to ensure that the residuals are suitable for land application. b. The samples will be collected from the storage tank that holds the residuals c. Jeff Thompson, Brent Collins, or other designee will be responsible for sample collection for nutrient and metal, and TCLP analysis. d. Nutrient, metal and TCLP sample aliquots will be collected randomly and consist of at least individual aliquots mixed together in order to get the composite sample for these parameters. e. The residuals will be sampled annually for TCLP including the RCIls. f. Metal and nutrient parameters will be collected and analyzed based on the requested dry ton numbers in the permit application. 9. Environmental Impacts a. The environmental impacts for residuals may be affected by this procedure. b. This procedure helps assure that land application is conducted in a safe and efficient manner while ensuring compliance with the laws and regulations and to minimize exposure, negative environmental impacts and public relation concerns. Page: 1 of 2 Report Number: 13-235-0206 in A&L Eastern Laboratories, Inc. Account Number: 46245 7621 Whitepme Road Richmond.Virginia 23237 (904)743-9401 Fax(804)271-6446 Submitted By: ROY WHITAKER wwtw.aleasbracom Send To: EMA RESOURCES INC Project:UNIFI REIDSVILLE 755 YADKINVILLE RD NC CERT#257 MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 8/22/2013 10:30:00 Lab Number: 95160 Date Received: 08/23/2013 00:00 Sample Id : UNIFI REIDSVILLE Date Reported: 08/28/2013 PARAMETER RESULT RESULT QUANTITATION LIMIT ANALYSIS (%) (mg/kg) (mg/kg`) ANALYST DATE/TIME METHOD Total Solids" 1.14 11400 100.0 JM 08/23/2013 14:15 SM-2540G Moisture* 98.86 100.0 JM 08/23/2013 14:15 SM-2540G Total Kjeldahl Nitrogen 4.74 47400 10.0 JM 08/26/2013 08:10 SM-4500-NH3C-TKN Total Phosphorus 0.79 7870 100 KM 08/26/2013 14:21 SW 6010C Total Potassium 0.29 2870 100 KM 08/26/2013 14:21 SW 6010C Total Sulfur 2.24 22400 100 KM 08/26/2013 14:21 SW 6010C Total Calcium 1.04 10400 0,0'10' 100 KM 08/26/2013 14:21 SW 6010C Total Magnesium 0.27 2700 3°11 f(''.100 KM 08/26/2013 14:21 SW 6010C Total Sodium 6.85 68500 1 O61O e 100 KM 08/26/2013 14:21 SW 6010C Total Iron 3040 100 KM 08/26/2013 14:21 SW 6010C Total Aluminum 3100 100 KM 08/26/2013 14:21 SW 6010C Total Manganese 640 5 KM 08/26/2013 14:21 SW 6010C Total Copper 380 5 KM 08/26/2013 14:21 SW 6010C Total Zinc 180 5 KM 08/26/2013 14:21 SW 6010C Ammonia Nitrogen 0.35 3510 10.0 JM 08/26/2013 08:10 SM-4500-NH3C Organic N 4.39 43890 10.0 08/26/2013 08:10 CALCULATION Nitrate+Nitrite-N 17700 2.00 JM 08/26/2013 08:10 SM-4500NO3F Total Cadmium <2.0 2.0 KM 08/26/2013 14:21 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 42/24 Cur reports and letters are for the exclusive and confidential use of our clients.and may not be reproduced in whole or pad,nor may any reference be made ,azi.m. to the ore me tesults,or the company in any advertising,news release,or other public announcements without obtaining our prior written authorization. S :�\ 10 Debbie Holt Page: 2 of 2 Report Number: 13-235-0206 ilL A&L Eastern Laboratories, Inc. Account Number: 46245 7621 Whitepine Road Richmond,Virginia 23237 (804)743-9401 Fax(804)271.6446 Submitted By: ROY WHITAKER wWw:atl uten1.com Send To: EMA RESOURCES INC Project:UNIFI REIDSVILLE 755 YADKINVILLE RD NC CERT#257 MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 8/22/2013 10:30:00 Lab Number: 95160 Date Received: 08/23/2013 00:00 Sample Id : UNIFI REIDSVILLE Date Reported: 08/28/2013 RESULT RESULT QUANTITATION LIMIT ANALYSIS PARAMETER (%) (mg/kg) (mg/kg`) ANALYST DATE/TIME METHOD Total Chromium 73 5 KM 08/26/2013 14:21 SW 6010C Total Nickel 32 5 KM 08/26/2013 14:21 SW 6010C Total Lead 7 5 KM 08/26/2013 14:21 SW 6010C Total Arsenic 3.0 3.0 KM 08/26/2013 14:21 SW 6010C Total Mercury <0.4 0.4 KM 08/26/2013 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 08/26/2013 14:21 SW 6010C pH (Standard Units)* 8.07 2.00 JM 08/26/2013 08:10 SW-9045D Total Volatile Solids 74.51 745100 100.0 JM 08/23/2013 14:15 SM-2540G Total Molybdenum <5 5 KM 08/26/2013 14:21 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR"Cr"AND"Ni". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. a.,reports and letters are for the exclusive and confidential use of our clients.and may not be reproduced in whole or part.nor may any reference be made 64.16.fizei. 'o;ne,::orx,Inc results,or the company in any advertising.news release,or other public announcements without obtaining our prior written authorization. Debbie Holt BIOSOLIDS SAMPLE TRANSMITTAL FORM/CHAIN OF CUSTODY I Act:otint it At A&L Eastern Agricultural Laboratories, Inc. 7621 Whitopine Road Richmond VA 23237 Tel:804-743.9401 Fax:804.271.6446 Email:ofQccQlal-labs-castan.cum Customer Information Submitted By Charge To I Coov To EMA Resources Inc EMA Resources Inc 755 Yadkinvi le Rd 755 Yedkinvllle Rd «11111111111111 1IJIYl141i1206 46246 ELIA RESOURCES INC 08-23-2013 Mocksville,NC 27028 Mocksville,NC 27028 UN'Ft R1EOS\1LLE 1322.01 1 1 Project • Sample Information Lab Number Collection Information Container IMorrnathm Please Chad;Desired Tests Sample ID (Lab Use Number 603 Nitrogen Type Veins SLI SL2 ChMTN* Date limeof Botilw metals pH CCE Ag CIVSaYds Others • UNZ Z l413 Grab - of 4 sYrur O V.Gornpoelte 144413/r3 1°:364.4` l o w rr ✓ ✓ ✓ fib — o: Composite ._Plastic _Pint at —_Grab _Giese c= ___Composite _Plssta �int Grab _Composite ___ pkd nt _ l 8 .(S re) DaNe Tints Received By;�ipnetum) Date Tine >r 2 , coPat 4/2=�-A3 y 1o• - Ex lIs-�; . /3 ` n;30 � ..�---, . C Test Package Details Special Instructions or Remarks SL I t Total Solids(Moisture)Total fJeldsld Nitrogen,Phosphonu and Potassium 8L2t Stale Test SL I plus Sulfur.Calcium.Magnaslean,Sodlum,Iron,Alumioum.Mangsncee,Copper And Zinc 803 Metal.:Areenlo,OWN"Chromium,Mercury,Moybdenum,Lead,Nickel,Selenium. (Copper&Zinc included In SL2) NIIroom Narks:Intel KJoldohl.Ammonium,Nitrate do OrganicNltrogm. CCE:Culdwlt Carbonate Equivalent or Total neutralization Value(For Lime Treated Sludge) RESIDUALS ANALYSIS REPORT PROJECT: Unifi, Inc Sample Date: 8/22/13 %Solids 1.14 pH: 8.07 CONVERSION TABLE PARAMETER % X 10000 =ppm dry wt. X 0.002 = lbs/dt Nitrogen TKN 4.74 47400 94.8 Phosphorus 0.79 7900 15.8 Potassium 0.29 2900 5.8 Sulfur 2.24 22400 44.8 Calcium 1.04 10400 20.8 Magnesium 0.27 2700 5.4 Sodium 6.85 68500 137 Ammonia N 0.35 3500 7 Nitrate N 1.77 17700.00 35.4 Iron 0.304 Ceiling 3040.00 6.08 Concent. Aluminum 0.31 3100.00 6.2 Chromium 0.0073 ppm 73.00 0.146 Manganese 0.064 640.00 1.28 Copper 0.038 4300.00 380.00 0.76 Zinc 0.018 7500.00 180.00 0.36 Cadmium 0.0002 85.00 2.00 0.004 Nickel 0.0032 420.00 32.00 0.064 Lead 0.0007 840.00 7.00 0.014 Arsenic 0.0003 75.00 3.00 0.006 Mercury 0.00004 57.00 0.40 0.0008 Selenium 0.0005 1 5.00 0.01 75 00 75.00 Molybdenum 0.0005 5.00 0.01 PLANT AVAILABLE NITROGEN CALCULATION (PAN) MR (TKN-AmN) + .5(AmN) + NO3N X.002= lbs. PAN/dt Surface 13170 1750 17700 65.24 MR (TKN-AmN) + AmN + NO3N X .002= lbs. PAN/dt Injection 13170 3500 17700 68.74 12065 Lebanon Rd. *ESC Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L•A.9 S•C•I•E•N•C•E•S Tax I.D. 62-0814289 YOUR L A© OF CHOICE Est. 1970 Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 Report Summary Friday September 06, 2013 Report Number: L653712 Samples Received: 08/23/13 Client Project: Description: Unifi-Reidsville The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. • Entire Report Reviewed By: Terrie Fudg , ESC resentative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 3 12065 Lebanon Rd. *ESC Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L•A•B S•C•I.E•N•C•E•5 Tax I.D. 62-0814289 YOUR LAB OF CHOICE Est. 1970 REPORT OF ANALYSIS Mr. Brent Collins September 06,2013 EMA Resources 755 Yadkinville Road Mocksville, NC 27028 ESC Sample # : L653712-01 Date Received August 23, 2013 Description Unifi-Reidsville Site ID : Sample ID UNIFI-REIDSVILLE Project : Collected By Roy Whitaker Collection Date : 08/21/13 10:30 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Corrosivity Non-Corrosiv 9045D 08/29/13 1540 JW 1 Ignitability See Footnote Deg. F D93/101 08/30/13 1645 MCG 1 Reactive CN (SW846 7.3.3.2) BDL 0.125 mg/kg 9012B 08/28/13 1131 JAL 1 Reactive Sulf. (SW846 7.3.4.1) BDL 25. mg/kg 9034/90 08/27/13 1531 DRK 1 TCLP Extraction - 1311 08/27/13 0651 MJF 1 Mercury BDL 0.0010 mg/1 0.20 7470A 08/28/13 1103 CAF 1 Arsenic BDL 0.050 mg/1 5.0 6010E 08/28/13 1428 ST 1 Barium BDL 0.15 mg/1 100 6010B 08/28/13 1428 ST 1 Cadmium BDL 0.050 mg/1 1.0 6010B 08/28/13 1428 ST 1 Chromium BDL 0.050 mg/1 5.0 6010B 08/28/13 1428 ST 1 Lead BDL 0.050 mg/1 5.0 6010B 08/28/13 1428 ST 1 Selenium BDL 0.050 mg/1 1.0 6010B 08/28/13 1428 ST 1 Silver BDL 0.050 mg/1 5.0 6010B 08/28/13 1428 ST 1 TCLP ZHE Extraction - 1311 08/29/13 0647 MJF 1 TCLP Volatiles Benzene BDL 0.050 mg/1 0.50 8260B 08/30/13 0044 DP 1 Carbon tetrachloride BDL 0.050 mg/1 0.50 8260B 08/30/13 0044 DP 1 Chlorobenzene BDL 0.050 mg/1 100 8260B 08/30/13 0044 DP 1 Chloroform BDL 0.25 mg/1 6.0 8260B 08/30/13 0044 DP 1 1,2-Dichloroethane BDL 0.050 mg/1 0.50 8260B 08/30/13 0044 DP 1 1,1-Dichloroethene BDL 0.050 mg/1 0.70 8260B 08/30/13 0044 DP 1 2-Butanone (MEK) BDL 0.50 mg/1 200 8260B 08/30/13 0044 DP 1 Tetrachloroethene BDL 0.050 mg/1 0.70 8260B 08/30/13 0044 DP 1 Trichloroethene BDL 0.050 mg/1 0.50 8260B 08/30/13 0044 DP 1 Vinyl chloride BDL 0.050 mg/1 0.20 8260B 08/30/13 0044 DP 1 Surrogate Recovery Toluene-d8 98.9 t Rec. 114. 8260B 08/30/13 0044 DP 1 Dibromofluoromethane 92.2 % Rec. 125. 8260B 08/30/13 0044 DP 1 a,a,a-Trifluorotoluene 101. % Rec. 114. 8260B 08/30/13 0044 DP 1 4-Bromofluorobenzene 95.7 % Rec. 128. 8260B 08/30/13 0044 DP 1 TCLP Pesticides Chlordane BDL 0.0050 mg/1 0.030 8081A 09/03/13 1417 CBB 1 Endrin BDL 0.0050 mg/1 0.020 8081A 09/03/13 1417 CBB 1 Heptachlor BDL 0.0050 mg/1 0.0080 8081A 09/03/13 1417 CBB 1 L653712-01 (IGNITABILITY) - Did Not Ignite @ 170 F Page 2 of 3 12065 Lebanon Rd. *ESC Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L.A•9 S.C•f•E•N•C•E•$ Tax I.D. 62-0814289 YOUR LAB OF CHOICE Est. 1970 REPORT OF ANALYSIS Mr. Brent Collins September 06,2013 EMA Resources 755 Yadkinville Road Mocksville, NC 27028 ESC Sample # : L653712-01 Date Received August 23, 2013 Description Unifi-Reidsville Site ID : Sample ID UNIFI-REIDSVILLE Project : Collected By Roy Whitaker Collection Date : 08/21/13 10:30 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Lindane BDL 0.0050 mg/1 0.40 8081A 09/03/13 1417 CBB 1 Methoxychlor BDL 0.0050 mg/1 10. 8081A 09/03/13 1417 CBB 1 Toxaphene BDL 0.010 mg/1 0.50 8081A 09/03/13 1417 CBB 1 Surrogate Recovery Decachlorobiphenyl 86.2 % Rec. 123. 8081A 09/03/13 1417 CBB 1 Tetrachloro-m-xylene 85.5 % Rec. 114. 8081A 09/03/13 1417 CBB 1 TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.0020 mg/1 1.0 8151A 09/04/13 2121 KLM 1 2,4-D BDL 0.0020 mg/1 10. 8151A 09/04/13 2121 KLM 1 Surrogate Recovery 2,4-Dichlorophenyi Acetic Acid 82.4 % Rec. 8151A 09/04/13 2121 KLM 1 TCLP Semi-Volatiles 1,4-Dichlorobenzene BDL 0.10 mg/1 7.5 8270D 08/29/13 0119 KMF 1 2,4-Dinitrotoluene BDL 0.10 mg/1 0.13 8270D 08/29/13 0119 KMF 1 Hexachlorobenzene BDL 0.10 mg/1 0.13 8270D 08/29/13 0119 KMF 1 Hexachloro-1,3-butadiene BDL 0.10 mg/1 0.50 8270D 08/29/13 0119 KMF 1 Hexachloroethane BDL 0.10 mg/1 3.0 8270D 08/29/13 0119 KMF 1 Nitrobenzene BDL 0.10 mg/1 2.0 8270D 08/29/13 0119 KMF 1 Pyridine BDL 0.10 mg/1 5.0 8270D 08/29/13 0119 KMF 1 3&4-Methyl Phenol BDL 0.10 mg/1 400 8270D 08/29/13 0119 KMF 1 2-Methylphenol BDL 0.10 mg/1 200 8270D 08/29/13 0119 KMF 1 Pentachlorophenol BDL 0.10 mg/1 100 8270D 08/29/13 0119 KMF 1 2,4,5-Trichlorophenol BDL 0.10 mg/1 400 8270D 08/29/13 0119 KMF 1 2,4,6-Trichlorophenol BDL 0.10 mg/1 2.0 8270D 08/29/13 0119 KMF 1 Surrogate Recovery 2-Fluorophenol 32.9 % Rec. 87.0 8270D 08/29/13 0119 KMF 1 Phenol-d5 23.1 % Rec. 67.0 8270D 08/29/13 0119 KMF 1 Nitrobenzene-d5 57.9 % Rec. 120. 8270D 08/29/13 0119 KMF 1 2-Fluorobiphenyl 69.4 % Rec. 122. 8270D 08/29/13 0119 KMF 1 2,4,6-Tribromophenol 61.4 % Rec. 148. 8270D 08/29/13 0119 KMF 1 p-Terphenyl-d14 88.1 % Rec. 149. 8270D 08/29/13 0119 KMF 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 09/06/13 13:42 Printed: 09/06/13 13:56 L653712-01 (IGNITABILITY) - Did Not Ignite © 170 F Page 3 of 3 Billing information: Analysis'Container/Prgskarvativ Cha istody EMA Resources Page_i_of_i_ Mr. Brent Collins 755 Yadkinville Road 755 Yadkinville Road Mocksville,NC 27028 Mocksville,NC 27028 . - *ESC ,„„ . . ,.: 'O'a' L-A-S S•C-I-E•N•C•E•S Report to: Email • 12065 Lebanon Road Mr. Brent Collins brent.collins@etnaresourcestt - Mt. uliet,TH 37122 pro ectCity/State Description: J�7 ri -REs73yte eE L'dlete f►.,� //' Phone:(8001 767.5859 vl �w� t`� ,Ir ` t Phone.(615)758-5858 Client Project#: Lab Project# u� shone: (3361751-1441 Fax (615)758 5859 =A: (3361751-1442 rlt:S o E016 :oilecte�v(print): Site/Facility IDS: P.O.S: ° zi Ko4 GJt{ZT..Ved i2 Rush? (Lab MUST Be NoGr U Collected at ): _ Date Results Needed ..l AC suet ''EMA#ES u,rt only) Same Day 200% t1 mmcdiat y Next Day 100% . — r, T ln T1 1413/P42818 packed on Ice N Y �� —Two Day 50% Email? _No X Yes ('-' Coo4r#� _Three Day 25% FAX? _No _Yes of - CL. • - i'Y;iff 17 ' Shipped Vipl .f edEX Gr Cntrs 1 Sample ID Comp/Grab _ Matrix* Depth Date Time AC F-• Remarks/Contaminant Sample#(lab Doty) tiAJZFZ-lerasvccce COmk(' _ TCLP Vat1(_ in:3oRu. 2 •X X L�37)Z-o( Ltn)tFr-RenSvtccr Cause . ,,. '^ • '. ' - 'Matrix: SS-Soil GW-Groundwater WIN-WasteWater DW-Drinking Water OT-Other pH Temp Remarks: Flow Other R-. = • �u�•° Date: Time: Recei'edb : Si•nature �' � �` / Y ( ) Sarpptes returned via: LJ UPS Condttign: (lab use only), ` ' /.?Z !3 y�p/tl . a �� �e1/FedEx❑Courier 0 •elfin• fished b (Sins(# Date: Time: 'ecery:': •Y( ,• ,., ) Temp: Bottles Received: ‘ 3 6 af.. ' coc sea)Intact:,.....•,V N 1'NA' e squished bigigdoliUre) Date: Time: Received for lab by.(Signature) Date: .TimO pH Chocked. 4/. 11;', c43'3. ate,: ATA NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory John E. Skvarla, Ill Governor Secretary May 30, 2014 Lisa Haynes Unifi, Inc. PO Box 737 Madison, NC 27027 SUBJECT: 2013 Annual Report Review Unifi, Inc. Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County • Dear Ms. Haynes: The Division of Water Resources (DWR) acknowledges receipt of your 2013 annual report for the subject permit. A review of this report was conducted by DWR staff. Review of the subject annual report and additional information received on May 30, 2014 reflects compliance with Permit No. WQ0006594. Please note: Your permit expires July 31, 2014 and to date DWR has not received a permit renewal application. If you or your staff have any questions, please contact Stephen Berry at 336-771-5288. Sincerely, Sherri V. Knight, PE"6 Assistant Supervisor Division of a er esources, NCDENR Cc: Brent Collins, EMA, 755 Yadkinville Road, Mocksville, NC 27208 Rockingham County Health Department Non-Discharge Permitting Unit— Permit File WQ0006594 585 Waughtown Street,Winston-Salem,North Carolina 27107 Phone:336-771-50001 Internet:www.ncdenr.gov An Equal Opportunity 1 Affirmative Action Employer—Made in part by recycled paper wA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Pat McCrory Thomas A. Reeder John E. Skvarla, Ill Governor Acting Director Secretary June 19,2013 Lisa Haynes Unifi, Inc. PO Box 737 Madison,NC 27027 SUBJECT: Annual Report Additional Information Acknowledgment Unifi,Inc. Unifi,Inc.Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County Dear Ms. Haynes: Additional information was requested on April 16,2013 for the 2011 and 2012 annual reports. Forms DMSF for 2011 and 2012 were received on May 23,2013. Thank you for your quick response. The additional information was found to be compliant with permit WQ0006594. If you or your staff have any questions,please call Derek Denard at 336-771-5286. Sincerely, „it k. Sherri V. Knight,P.E. Regional Supervisor,Aquifer Protection Section cc: Rockingham County Health Department APS Central Office-Permit File WQ0006594 Winston-Salem Regional Office 585 Waughtown Street,Winston-Salem,North Carolina 27107 One Phone:336-771-5000 FAX:336-77146311 Customer Service:1-877-623-6748 NorthCarolina Internet:http:llportal.ncdenr.orglweb/wq ���'/��//� An Equal Opportunity\Affirmative Action Employer [�l t` RECEIVED N.C.Dept.of ENh ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM MAY 2.3 2013 PERMIT#: WQ0006594 FACILITY NAME: UNIFI MANUFACTURING, INC. REIDSVILLE Winston-Salem PHONE: 336-348-6516 COUNTY: ROCKINGHAM OPERATOR: LISA HAYNES - Ropional offioo FACILITY TYPE (please check one): It urface Disposal(complete Part A(Source(s)and "Residual In" Volume only)and Part C) Distribution and Marketing(complete Parts A,B,and C) Was the facility in operation during the past calendar year? ❑ Yes OKo No If No skip parts A,B,C and certify form below Part A*: Part B*: Sources s (include NPDES#if Volume(dry tons) Recipient Information Month ( ) Amendment/ Volume(dry applicable) Bulking Agent Residual In Product Out Name(s) tons) Intended use(s) January February March April May June July August September October November December Totals: Annual(dry tons): 0 0 0 0 Amendment(s)used:I Bulking Agent(s)used:I * If more space than given is required,please attach additional information sheet(s). 0 Check box if additional sheet(s)are attached Part C: Facility was compliant during calendar year XI cL, with all conditions of the permit(including but not limited to items 1-3 below) issued by the Division of Water Quality. ® Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation,prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify,un. •r penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate and complete. I am aware that .ere ar significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." • 5/aa/i3 signature of Permi e Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF(11/2005) r CliClVCU N.C.Dept.of ENF ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM MAY 2 3 2013 PERMIT#: WQ0006594 FACILITY NAME: UNIFI MANUFACTURING, INC. REIDSVILLE Winston-saiem fteaional Office PHONE: 336-348-6516 COUNTY: ROCKINGHAM OPERATOR: LISA HAYNES FACILITY TYPE(please check one): 0 Surface Disposal(complete Part A(Source(s)and "Residual In" Volume only) and Part C) it Distribution and Marketing(complete Parts A,B,and C) Was the facility in operation during the past calendar year? 0 Yes 0No No If No skip parts A,B,C and certify form below Part A*: Part B*: Sources s (include NPDES#if Volume(dry tons) Recipient Information Month ( ) Amendment/ Volume(dry applicable) Bulking Agent Residual In Product Out Name(s) tons) Intended use(s) January February March April May June July August September October November December totals: Annual(dry tons): 0 0 0 0 Amendment(s)used:I Bulking Agent(s)used:I * If more space than given is required,please attach additional information sheet(s). 0 Check box if additional sheet(s)are attached Part C: Facility was compliant during calendar year 2011 with all conditions of the permit(including but not limited to items 1-3 below) issued by the Division of Water Quality. 0'Yes ❑ No If No,please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation,prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate and complete. I am aware thhere ar significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." çPLI1a gnature of Pe ee Da a Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF(11/2005) Av7A NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Pat McCrory Charles Wakild, P. E. John E. Skvarla, Ill Governor Director Secretary April 16, 2013 Lisa Haynes Unifi, Inc. PO Box 737 Madison,NC 27027 SUBJECT: 2011 &2012 Annual Report Review/Additional Information Request Unifi,Inc. Unifi,Inc.Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County Dear Ms. Haynes: Enclosed please find a copy of the Annual Report Review conducted on April 16, 2013. The review was conducted by Derek Denard of the Winston-Salem Regional Office. The Annual Report was reviewed for the years 2011 and 2012, which were received on February 1, 2012 and February 15, 2013. The facility was found to be in compliance with permit WQ0006594. The following was noted from the review: A cover letter indicated that residuals were not distributed in 2011 and 2012. Please fill out the attached FORM DMSDF with this information for the years 2011 and 2012. Writeable copies of this form can be found on our website at: http://portal.ncdenr.org/web/wq/aps/lau/reporting Please send the additional information requested in writing within thirty(30)days following receipt of this letter. Please refer to the enclosed report form for additional observations and comments. If you or your staff have any questions, please call Derek Denard at 336-771-5286. Sincerely, ).• t 4)1"-:c Sherri V.Knight,P.E. Regional Supervisor,Aquifer Protection Section cc: Rockingham County Health Department APS Central Office-Permit File WQ0006594 Winston-Salem Regional Office 585 Waughtown Street,Winston-Salem,North Carolina 27107 One Phone:336-771-5000 FAX:336-771-4631 I Customer Service:1-877-623-6748 North Carolina Internet http:llportal.ncdenr.org/weblwq �atura!!t� An Equal Opportunity 1 Affirmative Action Employer ( > 67 RECEIVED N.0 Dept of ENR UN/Jr/® FEB 2 2013 • Winston-Salem Regional Office February 8,2013 Mr. Ed Hardee Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh,NC 27699-1636 RE: Permit No. WQ0006594 Unifi,Inc. Plants 2 and 15 Distribution of Residual Solids Rockingham County Dear Mr.Hardee: In accordance with Permit No. WQ0006594 reporting condition the following information is being provided. During the calendar year January -December 2012 there was no distribution of residual solids from Plants 2 or 15. If you require additional information please contact me at 336-348-6516 or lhaynes@unifi.com. Sincerely, 0q4d1 Lisa Haynes Corporate Environmental Manager RECEIVEDIDENRIDWQ FEB 15 2013 Aquifer Protection Section DC_D RECEIVED N.C.Dept.of ENR 'IL"IN' FEB 0 71012 WWII® Winston-Salem Regional Office January 31, 2012 Mr. Ed Hardee Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh,NC 27699-1636 RE: Permit No. WQ0006594 Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids Rockingham County Dear Mr. Hardee: In accordance with Permit No. WQ0006594 reporting condition the following information is being provided. During the calendar year January-December 2011 there was no distribution of residual solids from Plants 2 or 15. If you require additional information please contact me at 336-348-6516 or lhaynes@unifi.com. Sincerely, _� _ Lisa Haynes V Corporate Environmental Manager R&M North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleen H. Sullins Dee Freeman Governor Director Secretary October 13, 2011 Lisa Haynes Unifi,Inc. PO Box 737 Madison,NC 27027 SUBJECT: Annual Report Review Unifi Inc Unifi,Inc.Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County Dear Ms. Haynes: Enclosed please find a copy of the Annual Report Review conducted on October 13,2011. The review was conducted by Derek Denard of the Winston-Salem Regional Office. The Annual Report was reviewed for the year 2010,which was received on August 22,2011. The facility was found to be in compliance with permit WQ0006594. Please refer to the enclosed report form for additional observations and comments. If you or your staff have any questions, please call Derek Denard at 336-771-5286. Sincerely, 4 .1 - Sherri V.Knight,P.E. Regional Supervisor,Aquifer Protection Section cc: Rockingham County Health Department APS Central Office-Permit File WQ0006594 Winston-Salem Regional Office • 585 Waughtown Street Winston-Salem,North Carolina 27107 One Phone:336-771-50001 FAX:336-771.46311 Customer Service:1-877.623-6748 NorthCarolina Internet:http:l/portal.ncdenr.org/wet><wq Natural/ An Equal Opportunity 1 Affirmative Action Employer State of North Carolina O�GF VVATF,S) Department of Environment and Natural Resources Division of Water Quality G Beverly Eaves Purdue, Governor — - Dee Freeman, Secretary 0 Coleen H. Sullins, Director Annual Report Review Distribution/Surface Disposal of Residuals Facility Name: Unifi, Inc. Reporting Period: 2010 Permit No.: WO000659 Counties that land is permitted for: N/A Maximum Dry Tons Per Year: 200 Dry tons distributed: 33.78 Acres permitted: N/A Acres applied on: N/A Dry tons per acre applied: N/A Number of fields in permit: N/A Number of fields applied on: N/A Monitoring Frequency: <319(1/Year)® Z319—<1,650(1/Quarter)❑ a1,650—<16,500(1/60Days)❑ z16,500(1/,Month)❑ Monitoring Frequency for TCLP: Annually ® Permit Cycle ❑ Groundwater monitoring: ❑Yes No 1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form Was a certification form submitted? ®Yes ONo ONA ONE Was distribution conducted during the reported period? ®Yes ONo ONA ONE Were the distributions with the permitted amount? ®Yes ONo DNA ONE Were recipients information listed? ®Yes ONo ONA ONE Did it indicate compliance? ®Yes ONo ONA ONE Was form complete? ZYes ONo DNA ONE Was it signed by the appropriate people? ZYes ONo ONA ONE Comments: 2. Monitoring Were the analyses conducted at the required frequency? ®Yes ONo ONA ONE Was an analyses taken for each source that was distributed? ®Yes ONo ONA ONE Were the metals analyses reported on the Residual Sampling Summary Form? ®Yes ONo ONA ONE Were the results reported in mg/kg? ®Yes ONo ONA ONE Were the pH's 6.0 or greater for each residual sample? ZYes ONo ONA ONE Were the heavy metals within ceiling concentration permit limits? ®Yes ONo ONA ONE Were the lab analyses attached? ®Yes ONo DNA ONE Were all the required parameters tested? ®Yes ONo ONA ONE Was TCLP analysis conducted? ZYes ONo ONA ONE Were the TCLP contaminants within regulatory limits? ®Yes ONo ONA ONE Was a corrosivity, ignitability, and reactivity analysis conducted? ®Yes ONo ONA ONE Comments: 3. Pathogen and Vector Attraction Reduction Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? Oyes ONo ZNA ONE Did the form provide all the required information? Oyes ONo ZNA ONE Was pathogen and vector attraction reduction documented? OYes ONo ®NA ONES Was pathogen/vector demonstrated according to 40 CFR Part 503? Oyes ONo ZNA ONE Class A Pathogen Review To be Class A, residuals shall meet either fecal Coliform density or salmonella density. Fecal Coliform density Was the sampling conducted at the required frequency? Oyes ❑No ZNA ONE Were multiple samples taken? Oyes ONo ®NA ONE Was each sample less than 1000 MPN/gram of total solids? Oyes ONo ZNA ONE OR Salmonella density Was the sampling conducted at the required frequency? Oyes [No ZNA ONE Were multiple samples taken? Oyes ONo ZNA ONE Was each sample less than 3 MPN/4 grams of total solids? Oyes ONo ZNA ONE nifi, Inc. (Plant 2) Permit No WQ0006594 Annual Report Review October 13, 2011 To be Class A, residuals shall meet one of the following alternatives: Alternative 1— Time/Temperature Were the residuals maintained for correct time and temperature? OYes ONo ZNA ONE Were logs submitted showing time and temperature? OYes ONo ZNA ONE Were temperatures within range for complete time period? OYes ONo ZNA ONE Alternative 2—Alkaline Treatment Were logs submitted showing time and temperature? OYes ONo ®NA ONE Was the pH raised to 12 or greater and maintained for 72 hours or longer? OYes [No ®NA ONE Was the temperature 52°C (126°F)for 12 hours or longer while the pH was z12? OYes ONo ZNA ONE Were logs submitted showing time and pH? OYes ONo ®NA ONE Was the temperature corrected to 25°C (77°F)? OYes ONo ®NA ONE Alternative 5—Process To Further Reduce Pathogens PFRP Composting Were the within-vessel method or static aerated pile methods used? OYes ONo ZNA ONE Was temp. Z55°C(131°F)for z3 days in within-vessel or static aerated pile method? OYes ONo ®NA ONE OR Was the windrow composting method used? OYes ONo ®NA ONE Was the temp. at z55°C for z15 days in windrows and turned a minimum of 5 times? OYes ONo ZNA ONE PFRP Heat Drying Was drying by direct or indirect contact w/hot gases& moisture reduced to 510%? OYes ONo ZNA ONE Was temp. of residuals or temp. of the gas in contact w/residuals at exit>80°C(176°F)? OYes ONo ®NA ONE Vector Attraction Reduction Review Was the sampling conducted at the required frequency? ['Yes ONo ®NA ONE Option 1 —38% Volatile Solids Reduction Was there 38% reduction? OYes ONo ZNA ONE Were lab sheets/calculations in report? OYes ONo ZNA ONE Was the reduction on volatile solids(not total solids)? OYes ONo ZNA ONE Were samples taken at beginning of digestion process &before application (Inspection)? :Wes ONo ®NA ONE Were calculations correct? OYes ONo ZNA ONE Option 2—40-Day Bench Scale Test Were residuals from anaerobically digested treatment(Inspection)? OYes ONo ZNA ONE Were residuals anaerobically digested in lab? OYes ONo ZNA ONE Was the test run for 40 days? OYes ONo ZNA ONE Was the test done between 30°C (86°F)and 37°C(99°F)? OYes ONo ®NA ONE Was the reduction of on volatile solids(not total solids)? ['Yes ONo ®NA ONE Was the reduction less than 17%? OYes ONo ®NA ONE Were lab sheets/calculations in report? OYes ONo ZNA ONE Were calculations correct? OYes ONo ZNA ONE Option 3—30-Day Bench Scale Test Were residuals from aerobically digested treatment(Inspection)? OYes ONo ZNA ONE Were residuals aerobically digested in lab? Oyes ONo ZNA ONE Were residuals 2% or less total solids? OYes ONo ZNA ONE If not 2%total solids, was the test ron a sample diluted to 2%w/unchlorinated effluent? OYes ONo ®NA ONE Was the test run for 30 days? DYes ONo ®NA ONE Was the test done at 20°C (68°F)? OYes ONo ZNA ONE Was the reduction of on volatile solids (not total solids)? OYes ONo ZNA ONE Was the reduction less than 15%? OYes ONo ZNA ONE Were lab sheets/calculations in report? OYes ONo ZNA ONE Were calculations correct? OYes ONo ®NA ONE Page 2 of 3 Unifi, Inc. (Plant 2) Permit No WQ0006594 Annual Report Review October 13, 2011 Option 4—Specific Oxygen Uptake Rate (SOUR) Were residuals form aerobically digested treatment(Inspection)? :Yes ❑No ZNA ONE Were residuals 2% or less total solids(dry weight basis) (not diluted)? OYes ONo ®NA ONE Was the test done between 10°C (50°F)and 30°C(86°F)? OYes ONo ZNA ONE Was the temperature corrected to 20°C (68°F)? OYes ONo ZNA ONE Was SOUR 51.5 mg of oxygen per hour/gram of total residual solids(dry weight basis)? OYes ONo ZNA ONE Was the sampling holding time two hours? OYes ONo ZNA ONE Was the test started within 15 minutes of sampling or aeration maintained? OYes ONo ZNA ONE Option 5— 14-Day Aerobic Process Were the residuals from aerobically digested treatment(Inspection)? OYes ONo ®NA ONE Were the residuals treated for 14 days? OYes ONo ZNA ONE Was the residuals temperature higher than 40°C(104°F)for a 14-day period? OYes ❑No ZNA ONE Was the average residuals temperature higher than 45°C (113°F)? OYes ONo ZNA ONE Option 6—Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? OYes ONo ®NA ONE Did the pH of residuals remain at z12 for two hours without the addition of more alkali? OYes ONo ZNA ONE Did the pH remain at z11.5 for an additional 22 hours w/out the addition of more alkali? OYes ONo ZNA ONE Was the pH corrected to 25°C (77°F)? OYes ONo ZNA ONE Option 7—Drying of Stabilized Residuals Does the residuals contain any unstabilized residuals? OYes ONo ®NA ONE Were the residuals mixed with any other materials? OYes ONo ZNA ONE Were the residuals dried up to 75%total solids? OYes ONo ZNA ONE Option 8—Drying of Unstabilized Residuals Were the residuals mixed with any other materials? OYes ONo ZNA ONE Were the residuals dried to 90%total solids? OYes ONo ZNA ONE Option 9—Injection Was any significant amount of residuals on surface one hour after injection (Inspection)? OYes ONo ZNA ONE Was injection done on pasture or hay field? OYes ONo ZNA ONE Was injection done at time that crop was growing? OYes ONo ®NA ONE If Class A, were residuals injected with 8 hours after discharge from pathogen treatment? OYes ONo ZNA ONE Comments: 4. General Was the report in the proper format? ®Yes ONo ONA ONE Was the annual report complete? ZYes ONo ONA ONE Was the report submitted on time? OYes ZNo ONA ONE Comments: Received on Aug 22, 2011. Page 3 of 3 lir UNIFI. N.C.Dept.of ENR AUG 24 2011 - W.nston-Salem Regional Office AQUIFFIR PPM -,,- rr,, „I,rCTlO August 17, 2011 AUG 2 2 z-,:a Mr. Ed Hardee NCDENR Division of Water Quality Aquifer Protection 1601 Mail Service Center Raleigh, NC 27699-1601 RE: Unifi, Inc.: Permit# WQ0006594 Distribution of Class A Residuals 2010 Annual Report Dear Mr. Hardee: Please find attached the 2010 Annual Report for Distribution of Class A Residuals from our facility located in Reidsville,NC. If you have any questions or require additional information please advise. AO Sincerely, .....1hApt Lisa Haynes Corporate Environmental Manager PPir Unifi, Inc. Distribution of Class A Residuals 2010 Annual Report NC Permit WQ0006594 (111111111 QUALITY THROUGH PRIDE Prepared by: Precision Land Application, Inc. 4022 White Plains Rd. Roaring River, NC 28669 (336) 957-8839 Precision Land Application, Inc. 2010 Annual Report Unifi, Inc. NC Permit WQ0006594 Enclosed is the Annual Monitoring Report as required by the above referenced permit. In 2010 Unifi, Inc. distributed 810,000 gallons (33.78 dry tons)of biosolids under their distribution and marketing program. If there are any questions or comments concerning this report,please contact me. Sin - ely, J. % es C. Alexander esident 4022 White Plains Rd. • Roaring River,NC 28669 • (336)957-8839 ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT#: WQ0006594 FACILITY NAME: Unifi, Inc. (Plant 2) PHONE failiraffillaig COUNTY: Rockingham OPERATOR: Unifi,Inc. 'N FACILITY TYPE (please check one): 0 Surface Disposal(complete Part A(Source(s) and "Residual In" Volume only) and Part C) ! ' Distribution and Marketing(complete Parts A,B,and C) Was the facility in operation during the past calendar year? L'Yes ❑No No If No skip parts A,B,C and certify form below Part A*: Part B*: Sources s include NPDES#if Volume(dry tons) Recipient Information Month ( ) ( Amendment/ applicable) Bulking Agent Residual In Product Out Name(s) Volume(dry tons) Intended use(s) • January Unifi,Inc. N/A Fertilize February " March II " " April " May " " '1 June " " " July 7.76 7.76 Ronald O'Quinn 7.76 " August " September _ 26.02 26.02 Ronald O'Quinn 26.02II October " " I,November I ," " " December " " II Totals: Annual(dry tons): 0 33.78 33.78 33.78 Amendment(s)used:I None Bulking Agent(s)used:1 None * If more space than given is required,please attach additional information sheet(s). 0 Check box if additional sheet(s)are attached Part C: Facility was compliant during calendar year 2010 with all conditions of the permit(including but not limited to items 1-3 below) issued by the Division of Water Quality. Ea' Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3)copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation,prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law,that the above information is, to the best of my knowledge and belief,true,accurate and complete. I am aware th there a pi significant enalties for submitting false information,mation, including the possibility of fines and imprisonment for knowing violations."l Signature of Pe Date Signature of Preparer Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF(11/2005) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please dote that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006594 Laboratory: 1) Meritech, Inc. Facility Name: Unifi,Inc(Plant 2) 2) NPDES#or 3) WQ#: 4) WWTP Name: Unifi,Inc. (Plant 2) 5) Residual Analysis Data Sample or 9/21/10 Composite Date Percent Solids 1 Arsenic 5.00 Cadmium 1.00 Chromium 28 or) Copper 222.00 Lead 5.00 Mercury 0.10 a Molybdenum 2.50 Nickel 13.00 Selenium 5.20 Zinc 88.50 Total Phosphorus 5970 TKN 19600 Ammonia-Nitrogen 14 Nitrate and Nitrite 11300 "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signi ant pen Ities for submitting false information,including the possibility of fines and imprisonment for knowing violations." Signature of Prepare Date DENR FORM RSSF(5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Igi Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006594 Laboratory: 1) Meritech, Inc. Facility Name: Unifi, Inc. (Plant 2) 2) NPI)ES#or 3) WQ#: 4) WWTP Name: Unifi, Inc. (Plant 2) 5) Residual Analysis Data Sample or 9/21/10 Composite Date Aluminum 21,800 Calcium 5960 Magnesium 1970 Sodium 117,000 „� pH 9.52 5 PAN(Surface) /-7 i V.g a e9 to 0 Z "I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to ass re that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are signif ant pen hies for submitting false information,including the possibility of fines and imprisonment for knowing violations." Ma 10411_ Signature of Prep r Date r DENR FORM RSSF-B(5/2003) Pr Precision Land Application, Inc. Operations Report Unifi,Inc. Plant 2 (Reidsville,NC) Site No. Farmer Date Weather Method Crop Gallons/Yards GDU6-4 O'Quinn 7/29/10 Dry _ Surface Fescue 114,000 GDU6-4 O'Quinn 7/30/10 Dry Surface Fescue 72,000 GDU6-4 O'Quinn 9/16/10 Dry Surface Fescue 84,000 GDU6-4 O'Quinn 9/17/10 Dry Surface Fescue 102,000 GDU6-4 O'Quinn 9/21/10 Dry Surface Fescue 120,000 GDU6-4 O'Quinn 9/22/10 Dry Surface Fescue 114,000 GDU6-4 O'Quinn 9/24/10 Dry Surface Fescue 126,000 GDU6-4 O'Quinn 9/25/10 Dry Surface Fescue 78,000 Total 810,000 4022 White Plains Rd. • Roaring River,NC 28669 • (336) 957-8839 I Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 141 • Contact: Chris Alexander Report Date: 10/19/10 Client PLA 4022 White Plains Road Roaring River,NC 28669 Date Sample Rcvd: 9/21/10 Meritech Work Order# 09211037 Sample: U-1 Grab 9/21/10 parameters Result Analysis Date Reporting Limit Method %Solids 1.0 % 9/28/10 0-100 % SM 2540E Ammonia,Nitrogen 14 mg/kg 9/22/10 10 mg/kg . EPA 350.1 TKN 19,600 mg/kg 10/1/10 20 mg/kg EPA 351.1 Nitrate/Nitrite,Nitrogen 11,300 mg/kg 9/23/10 10 mg/kg EPA 353.2 Arsenic,total <5.00.mg/kg 9/27/10 5.00 mg/kg EPA 200.7 Cadmium,total < 1.00 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 Calcium,total 5,960 mg/kg 9/27/10 0.500 mg/kg EPA 200.7 Chromium,total . 28.0 mg/kg 9/27/10 0.500 mg/kg EPA 200.7 Copper,total 222 mg/kg 9/27/10 0.010 mg/kg EPA 200.7 Lead,total <5.00 mg/kg 9/27/10 0.050 mg/kg EPA 200.7 . Magnesium,total 1,970 mg/kg 9/27/10 0.500 mg/kg EPA 200.7 Mercury,total 0.1000 mg/kg 9/28/10 0.0100 frig/kg EPA 245.1 Molybdenum,total <2.50 mg/kg 9/27/10 0,025 mg/kg EPA 200.7 Nickel,total 13.0 mg/kg 9/27/10 .0.050 mg/kg EPA 200.7 Phosphorus,total 5970 mg/kg 9/27/10 0.100 mg/kg EPA 200.7 Potassium,total 3,760 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 Selenium,total 5.20 mg/kg 9/27/10 5.56 mg/kg EPA 200.7 Sodium,total 117,000 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 pH 9.52 S.U. 10/7/10 1.0 14.0 S.U. SM 4500 H B I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 4 ,-s s .-1 t 0 - 3.-'+- Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Chris Alexander Report Date: 10/19/10 Client: PLA Revision Date: 8/11/11 4022 White Plains Road Roaring River,NC 28669 Date Sample Rcvd: 9/21/10 Meritech Work Order# 09211037 Sample: U-1 Grab 9/21/10 Parameters Result Analysis Date Reporting Limit Method %Solids 1.0 % 9/28/10 0- 100 % SM 2540B Ammonia,Nitrogen 14 mg/kg 9/22/10 10 mg/kg EPA 350.1 TKN 19,600 mg/kg 10/1/10 20 mg/kg EPA 351.1 Nitrate/Nitrite,Nitrogen 11,300 mg/kg 9/23/10 10 mg/kg EPA 353.2 q� Aluminum,total 21,800 mg/kg 9/27/10 0.250 mg/kg EPA 200.7 Arsenic,total <5.00 mg/kg 9/27/10 5.00 mg/kg EPA 200.7 Cadmium,total < 1.00 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 Calcium,total 5,960 mg/kg 9/27/10 0.500 mg/kg EPA 200.7 Chromium,total 28.0 mg/kg 9/27/10 0.025 mg/kg EPA 200.7 Copper,total 222 mg/kg 9/27/10 0.010 mg/kg EPA 200.7 Lead,total <5.00 mg/kg 9/27/10 5.00 mg/kg EPA 200.7 Magnesium,total 1,970 mg/kg 9/27/10 0.500 mg/kg EPA 200.7 Mercury,total 0.1000 mg/kg 9/28/10 0.0200 mg/kg EPA 245.1 Molybdenum,total <2.50 mg/kg 9/27/10 2.50 mg/kg EPA 200.7 Nickel,total 13.0 mg/kg 9/27/10 0.050 mg/kg EPA 200.7 Phosphorus,total 5,970 mg/kg 9/27/10 0.100 mg/kg EPA 200.7 Potassium,total 3,760 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 Selenium,total 5.20 mg/kg 9/27/10 0.050 mg/kg EPA 200.7 Sodium,total 117,000 mg/kg 9/27/10 1.00 mg/kg EPA 200.7 * Zinc,total 88.5 mg/kg 9/27/10 0.050 mg/kg EPA 200.7 pH 9.52 S.U. 10/7/10 1.0- 14.0 S.U. SM 4500 H B I hereby certify that I have reviewed and approve these data. • arna,ndtd Aii004 foa noL cLt Laboratory Representative 642 Tamco Road, Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 1 MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls,Inc. ` Cl PLA Project: Unifi Client Sample ID: U-1 Sample Collection: 09/21/10 Meritech Sample ID: 09211037 1311 - TCLP Organics Volatiles:SW-846 8260 Analysis: 09/30/10 Date Extracted: . 09/22/10 Analyst: V W V Parameter Result Units pet.Limit Rea.Limit Dilution Factor Benzene <0.0100 mg/L 0.0100 0.50 1 Carbon Tetrachloride <0.0700 mg/L 0.0100 0.50 1 Chlorobenzene <0.0100 mg/L 0.0100 100 1 Chloroform <0.0100 mg/L 0.0100 6.0 1 I,2-Dichloroethane `<0.0100 mg/I. 0.0100 0.50 1 1.,1-Dichlomethene <0.0100 mg/L 0.0100 0.70 I Methyl Ethyl Keane <0.100 mg/L 0.100 200 . 1 Tetrachloroethylene <0.0I00 mg/L 0.0100 . 0.70 1 Trichlomethene <0.0100 mg/L. 0.0100 0.50 1 . Vinyl Chloride <0.0200 mg/L 0.020 0.20 1 Sean-Volatiles:SW-846 8270 Extraction: 09/27/10 Analysis: - 10/18/10 Analyst: MC Parameter &RA Units Det.Limit Rea.Limit Dilution Factor 1,4-Dichlorobenzene <0.100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L. 0.100 3.00 10 o-cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridinc <0.100 mg/L 0.100 5.0 10 2.4.5-Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6-Thchlorophenoli <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 • I hereby certify that I have reviewed and approve these data. (p.-2a.VI Laboratory Representative • 642 Tamco Road* Reidsville, NC 27320 (336)342-4748 Ph* (336)342-1622 Fax 1 i • MERITECH, INC. *, Environmental.Laboratories _ . A Division of Water Technology and Controls,Inc. gir Client PLA Attn:Chris Alexander j Address: 4022 White Plains Road Roaring River,NC 28669 Client Sample ID: U-1 Sample Collection: 9/21/2010 Meritech Sample ID: 09211037 1311-TCLP Metals Metals-EPA 200.7 Extraction: 9/22/2010 Analyst:• BD Analysis: 9/23/2010 Parameter Result Units Det.Limit Reg.Limit Dilution Factor Arsenic <0.100 mg/L 0.100 5.0 1 Barium 0.442 mg/L 0.050 100.0 1 • Cadmium <0.020. mg/L 0.020 1.0 1 Chromium <0.050 mg/L 0.050 5.0 1 Lead 0.111 mg/L 0.100 5.0 1 Selenium 0.112 mg/L 0.100 1.0 1 Silver <0.050 mg/L 0.050 5.0 1 Metals-EPA 245.1 Extraction: 9/28/2010 Analyst: BD Analysis: 9/28/2010 Parameter Result Units Det.Limit Reg.Limit Dilution Factor Mercury <0.020 mg/L 0.020 0.2 1 Parameter Method Result Units Det.Limit Reg,Limit Date Analyzed Total Sulfide SM 4500 S D 6.05 mg/L 0.010 NA 9/23/2010 Total Cyanide EPA 335.4 <0.005 mg/L 0.005 NA 10/11/2010 • I hereby certify that I have reviewed and approve these data. - n f2d6) Laboratory Representative 642 Tamco Road* Reidsville, NC 27320 (336)342-4748 Ph* (336)342-1522 Fax MERI TECH, INC. y.c Environmental Laboratories _ AirA Division of Water Technology and Controls, Inc. Client: PLA Project: TCLP Client Sample ID: U-1 Grab Sample Collection: 9/21/2010 Meritech Sample ID: 9211037 Method 1311 - TCLP Pesticides & Herbicides Pesticide-SW-846 8081A Extraction: 10/4/2010 • Analyst Summit Analysis: 10/4/2010 Parameter Result Units Det.Limit Reg.Limit Dilution Factor Linda* <0.005 mg/L 0.005 0.40 1 Chlordane <0.01 mg/L 0.01 0.03 1 Endrin <0.005 mg/L 0.005 0.02 1 Heptachlor <0.002 mg/L 0.002 0.008 1 - Methoxychlor <0.005 mg/L 0.005 10.0 1 Toxaphene <0.02 mg/L 0.02 0.5 1 Herbicides-SW-846 8151A, Extraction: 10/4/2010 Analysis: 10/4/2010 Analyst Summit Parameter Result Units Det.Limit Reg.Limit Dilution Factor 2,4-D <0.005 mg/L 0.005 1.0 1 2,4,5-TP(Silvex) <0.005 mg/L 0.005 0.10 1 Other Parameters Method Date Analyzed Ignitability 1010 *WNI °C N/A N/A 10/19/2010 "Will Not Ignite I hereby certify that I have reviewed and approve these data 2, Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax • 1 A 'A NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleen H.Sullins Dee Freeman Governor Director —__ _ Secretary RECEIVED N.C.Dept.of ENR June 9, 2011 JUN 14 2011 Winston-Salem CERTIFIED MAIL# 7010 0780 0001 7057 5556 Regional Office RETURN RECEIPT REQUESTED Lisa M. Haynes Unifi, Inc. Post Office Box 1437 Reidsville, NC 27323 Subject: NOTICE OF VIOLATION (NOV-2011-PC-0353) FAILURE TO SUBMIT ANNUAL REPORT Permit No. WQ0006594 Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids Rockingham County Dear Ms. Haynes: This Notice of Violation is being sent to you for failure to submit the 2010 annual report. One of the requirements of your non-discharge permit is the submittal of an annual report to the Division of Water Quality by March 1st of each year. As of this date, our records indicate that the 2010 annual report has not been submitted for the subject facility. Failure to act in accordance with the terms, conditions, or requirements of your permit may result in the assessment of civil penalties of up to $25,000.00 per violation per day, in accordance with North Carolina General Statute §143-215.6A. Please respond to this notice of violation within 15 calendar days of its receipt, either by submitting three copies of the annual report or records, indicating the report was submitted. Submit to: Ed Hardee Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 AQUFER PROTECTION SECTION 1636 Mail Service Center,Raieian,North Caroiina 27699-1636 Location:2728 Capital Bouievarc.Raleigh North Carolina 27604 One G arc :3 1 91q 71' 0 8 non. 33-322 FAX 5.058E FAX 19-7 5-6048',Customer Service 1- --623-6748 North Carolina interne::avwri ncwaterauality orG Naturally u pan ci; Nothing in this letter should be taken as relieving from you the responsibility for failing to submit the annual report in a timely manner. A decision as to the appropriateness of an enforcement action will be made following the receipt of your response. If you have any questions regarding this letter, please contact Ed Hardee of our Central Office staff at (919) 715-6189. Sincerely, • Jon Risgaard, Supervisor Land Application Unit JR:eh cc: Permit Files WQ0006594 Land Application Unit EMA Resources, Inc. January 30, 2014 DENR/Water Quality Section Non-Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2013 Annual Report—Unifi, Incorporated Treatment and Land Application of Residuals Permit No. WQ0006594 Dear Sir or Madam: Enclosed are three copies of the 2013 Annual Report for the above referenced land application permit. During 2013 EMA Resources, Inc. land applied 18.86 dry tons of wastewater residuals to 48.5 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Since ly, Brent Collins Director of Technical Services brent.collins@emaresourcesinc.com REDEIVEDIDENRIDWR JAN - 3 2014 Water Quality Permitting Section Phone 336.751.1441 -Fax 336.751.1442 755 Yadkinville Road-Mocksville,NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM Q0006594 County: Rockingham Year: 2009 e(as shown on permit): Unifi, Inc. Plants 2 and 15 nd Application Operator: Chris Alexander, PLA, Inc. Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? , .,civtu;DENR 1 UWQ 0 Yes rfflNo - If No,skip Part A,and Part B and proceed to Part C. Also, If residuals weiAlli=P tiPfTt"TInN gFCTION generated but not land applied, please attach an explanation on how the residuals were handled. AUG 0 4 2010 Part A-Residuals Application Summary: Total number of application fields in the permit: N/A Total number of fields utilized for land application during the year: Total amount of dry tons applied during the year for all application sites: Total number of acres utilizes for land application during the year: Part B-Annual Compiance Statement: Facility was compliant during calendar year with all conditions of the land application permit • (including but not limited to items 1-13 below)issued by the Division of Water Quality. 0 Yes ❑ No If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory results are attached. 4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a)or the Pollutant Loading Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals,as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C-Certification: "I certify, under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." RECEIVED Lisa Haynes, Environmental Mana er N.C.Dept o(ENR b (3/b 0 Permittee Name and Title (type or print) " AUG 0 9 2010 Signature o Pe 'nee Date Winston-Salem Regional Office Signature of Preparer* Date `Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACE (12/2006) I I111\II/I WI/1M® August 3, 2010 Mr. Ed Hardee DENR Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh,NC 27699-1636 RE: Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids NOTICE OF VIOLATION (NOV-2010-PC-0899) Dear Mr. Hardee: In response to the NOV noted above the following information is being provided. Please find attached a completed Annual Land Application Certification Form. As indicated on the attached form residual solids were not land applied during the calendar year 2009. The residual solids generated were held in an aerobic digester during this period. If you have any questions or require additional information please contact me at (336) 348-6516 or Ihaynesa,,unifi.com Sincerely, Q isa Haynes Environmental Manager RECEIVED I DENR/DWQ AQUIFER PRnTFrTln!V gFCTION AUG 0 4 2010 NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beveriv Eaves Perdue Coieen H. Sullins Dee Freeman Governor Director Secretary July 28, 2010 CERTIFIED MAIL#7008 1140 0002 6736 8726 RETURN RECEIPT REQUESTED Lisa M. Haynes Unifi, Inc. Post Office Box 1437 Reidsville, NC 27323 Subject: NOTICE OF VIOLATION (NOV-2010-PC-0899) FAILURE TO SUBMIT ANNUAL REPORT Permit No. WQ0006594 Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids Rockingham County Dear Ms. Haynes: This Notice of Violation is being sent to you for failure to submit the 2009 annual report. One of the requirements of your non-discharge permit is the submittal of an annual report to the Division of Water Quality by March 1st of each year. As of this date, our records indicate that the 2009 annual report has not been submitted for the subject facility. Failure to act in accordance with the terms, conditions, or requirements of your permit may result in the assessment of civil penalties of up to $25,000.00 per violation per day, in accordance with North Carolina General Statute §143-215.6A. Please respond to this notice of violation within 15 calendar days of its receipt, either by submitting three copies of the annual report or records, indicating the report was submitted. Submit to: • Ed Hardee Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 AQUIFER PROTECTION SECTION 1636 Mail Service Center.Raleigh,North Carolina 2769N-163: Location:2728 Capital 6ourevard.Raleigh.North Carolina 27604 �Jn: Phone:919-733-3221 FAX 1:919 715-058E:FAX,2:915-715-6048',Customer Service:1-877-623-674E T Internet:www.ncwaterouality.orc �I 01't�7 Carolina Natwatik An Coua!VpporIunit':`Affirmative H.cuon Employe' Nothing in this letter should be taken as relieving from you the responsibility for failing to submit the annual report in a timely manner. A decision as to the appropriateness of an enforcement action will be made following the receipt of your response. If you have any questions regarding this letter, please contact Ed Hardee of our Central Office staff at (919) 715-6189. Sincerely, Jon Risgaard, Supervisor Land Application Unit JR:eh cc atilaffaiiffargaraW S Permit Files WQ0006594 Land Application Unit W A 7 Michael F.Easley,Governor WO* William G.Ross Jr.,Secretary GNorth Carolina Department of Environment and Natural Resources CqrColeen H.Sullins,Director Division of Water Quality August 16,2008 Lisa M.Haynes Unifi,Inc. Post Office Box 1437 Reidsville,NC 27323-1437 SUBJECT: Annual Report Reivew Unifi,Inc. Unifi,Inc.Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County Dear Ms. Haynes: Enclosed please find a copy of the annual report review conducted on June 30,2008. The review was conducted by Derek Denard of the Winston-Salem Regional Office. The annual report was reviewed for the year 2007,which was received on June 24,2008. The facility was found to be in Compliance with monitoring requirements in permit WQ0006594. Please refer to the enclosed inspection report for additional observations and comments. If you or your staff have any questions,please call Derek Denard at 336-771-5286. Sincerely, ) I Y. ..�. Sherri V.Knight,P.E. Regional Aquifer Protection Supervisor cc: James C.Alexander,Precision Land Application,Inc., 4022 White Plains Rd.,Roaring River,NC 28669 Rockingham County Health Department Ed Hardee,AP Program Section LAU APS Central Files Nor Carolina Naturall Division of Water Quality/Aquifer Protection Section Customer Service 585 Waughtown Street,Winston-Salem NC 27107 1-877-623-6748 Phone: (336)771-5000 Fax: (336)7714631 Internet: http:i/ww w.ncwaterqualit‘.org An Equal Opportunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper Compliance Inspection Report Permit: WQ0006594 Effective: 08/26/05 Expiration: 07/31/10 Owner: Unifi Inc SOC: Effective: Expiration: Facility: Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids County: Rockingham PO Box 698 Region: Winston-Salem Yadkinville NC 27055 Contact Person: Timothy Cole Title: Phone:910-679-8891 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): Related Permits: NC0021873 Town of Mayodan-Mayodan WWTP NC0024881 City of Reidsville-Reidsville WWTP Inspection Date: 06/30/2008 Entry Time: 10:00 AM Exit Time: 07:00 PM Primary Inspector: Derek Denard Phone:336-771-5000 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type:Compliance Evaluation • Permit Inspection Type: Distribution of Residual Solids(503 exempt) Facility Status: ■Compliant 0 Not Compliant Question Areas: III Miscellaneous Questions •Record Keeping (See attachment summary) Page: 1 Permit:WQ0006594 Owner-Facility: Unifi Inc ' Inspection Date: 06/30/2008 inspection Type:Compliance Evaluation Reason for Visit:Routine inspection Summary: ANNUAL REPORT REVIEW Reporting Period: 2007 Permit Details: • Land Application or Distribution? Distribution • Is 503? N/A • Class A or B? A • Maximum Dry Tons Per Year: 200 • Monitoring Frequency for TCLP:Annually • Monitoring Frequency for Residuals Analysis:Annually and any time that a change in the manufacturing process occurs. • Monitoring Frequency for Pathogen &Vector Attraction Reduction: N/A Annual Report Review Class A Distribution 1. Class A Annual Distribution and Marketing/Surface Disposal Certification Form • Was a certification form submitted?YES • Was distribution conducted during the reported period?YES • How many dry tons were distributed? 88.8 • Were the distributions with the permitted amount?YES • Were recipients information listed?YES • Did it indicate compliance?YES • • Was form complete?YES •Was it signed by the appropriate people? The preparer's signature was not on the Certification Form. However, the preparer signed a cover letter. 2. Monitoring Were the analyses conducted at the required frequency?YES • Were the metals analyses reported on the Residual Sampling Summary Form?YES • Were the results reported in mg/kg?YES • Were the metals within ceiling concentration permit limits?YES Were the metals within monthly average concentration permit limits?YES If no,were the lab analyses attached? N/A, but YES • Were all the required parameters tested?YES •Was TCLP analysis conducted?YES • Were the TLCP contaminants with regulatory limits?YES 3. Pathogen and Vector Attraction Reduction • Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? N/A • Did the form indicate the period of coverage, the residual class, and the pathogen reduction alternative and the vector attraction reduction option used? N/A • Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? N/A • Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? N/A 4.General • Was the report in the proper format?YES • Were any parts of the annual report missing?YES • Was the report submitted on time? NO, Notice of Voliation was issued by the Central Office on 6/11/08. Report was received on 6/24/08. Page: 2 Permit:WQ0006594 Owner-Facility: Unifi Inc Inspection Date: 06/30/2008 Inspection Type:Compliance Evaluation Reason for Visit:Routine Type Yes No NA NE Land Application ❑ Distribution and Marketing • Record Keeping Yes No NA NE Is GW monitoring being conducted, if required? 0 0 • 0 Are GW samples from all MWs sampled for all required parameters? 0 0 • 0 Are there any GW quality violations? ❑ ❑ U ❑ Is GW-59A certification form completed for facility? 0 0 ■ 0 Is a copy of current permit on-site? 0 0 0 ■ Are current metals and nutrient analysis available? U ❑ ❑ ❑ Are nutrient and metal loading calculating most limiting parameters? U ❑ ❑ ❑ a. TCLP analysis? 11000 b. SSFA(Standard Soil Fertility Analysis)? 0 0 ■ 0 Are PAN balances being maintained? 0 0 • 0 Are PAN balances within permit limits? 0 0 ■ 0 Has land application equipment been calibrated? 0 0 ■ 0 Are there pH records for alkaline stabilization? 0 0 • 0 Are there pH records for the land application site? 0 0 ■ 0 Are nutrient/crop removal practices in place? 0 0 • 0 Do lab sheets support data reported on Residual Analysis Summary? ■ ❑ ❑ ❑ Are hauling records available? ■ ❑ ❑ ❑ Are hauling records maintained and up-to-date? ■ ❑ ❑ ❑ #Has permittee been free of public complaints in last 12 months? ■ ❑ ❑ ❑ • Has application occurred during Seasonal Restriction window? ❑ ❑ ■ ❑ Comment: See summary for comments. Page: 3 W A TZ. Michael F.Easley,Governor Q 9 William G.Ross Jr.,Secretary OCR QG North Carolina Department of Environment and Natural Resources G7 Coleen H.Sullins,Director Division of Water Quality O '< September 26,2007 Ms.Lisa Haynes,Environmental Biologist Unifi,Incorportated Post Office Box 737 Madison,NC 27027 SUBJECT: September 21,2007 Compliance Evaluation Inspection Unifi,Inc Unifi,Inc.Plants 2 and 15 Distribution of Residual Solids Permit No: WQ0006594 Rockingham County Dear Ms.Haynes: Enclosed please find a copy of the Compliance Evaluation Inspection form from the inspection conducted on September 21, 2007. The Compliance Evaluation Inspection was conducted by Derek Denard of the Winston-Salem Regional Office. Present for the inspection was Chris Alexander,Precision Land Application,Inc. The facility was found to be in Compliance with permit WQ0006594. Please refer to the enclosed inspection report for additional observations and comments. If you or your staff have any questions,please call Derek Denard at 336-771-5286. Sincerely, j6eu )'T 14ft Sherri V.Knight,P.E. Regional Aquifer Protection Supervisor cc: James C.Alexander,4022 White Plains Rd.,Roaring River,NC 28669 Rockingham County Health Department APS Central Files s Nye Carolina turn!!y Division of Water Quality/Aquifer Protection Section Customer Service 585 Waughtown Street,Winston-Salem NC 27107 1-877-623-6748 Phone: (336)771-5000 Fax: (336)771-4631 Internet: http://WWNN.ncwaterqualitv.org An Equal Opportunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper Compliance Inspection Report Permit: WQ0006594 Effective: 08/26/05 Expiration: 07/31/10 Owner: Unifi Inc SOC: Effective: Expiration: Facility: Unifi, Inc. Plants 2 and 15 Distribution of Residual Solids County: Rockingham PO Box 698 Region: Winston-Salem Yadkinville NC 27055 Contact Person: Timothy Cole Title: Phone:910-679-8891 Directions to Facility: System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On-Site Representative(s): Related Permits: NC0021873 Town of Mayodan-Mayodan VWVTP NC0024881 City of Reidsville-Reidsville WWTP Inspection Date: 09/21/2007 Entry Time: 10:00 AM Exit Time: 12:30 PM Primary Inspector: Derek Denard Phone:336-771-5000 Secondary Inspector(s): Reason for Inspection: Routine Inspection Type:Compliance Evaluation Permit Inspection Type: Distribution of Residual Solids(503 exempt) Facility Status: IN Compliant 0 Not Compliant Question Areas: •Miscellaneous Questions III Record Keeping •Treatment II Sampling II Land Application Site •Transport (See attachment summary) Page: 1 Permit:W00006594 Owner-Facility: Unifi Inc Inspection Date:09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine Inspection Summary: PERMIT • Land Application or Distribution? Distribution • Is 503? NO • Class A or B?A • Maximum Dry Tons Per Year: 200 Number of acres permitted: N/A • Total number of fields in permit: N/A • Counties that land is permitted for: N/A • Other Description: Residuals for this permit are primary land applied (distributed) in Rockingham County. RECORD KEEPING • Comments for record keeping: No comments. • For further details on record keeping see questions on the inspection form. SELF-MONITORING • Upon Review of the annual report(s)for 2005 and 2006 the facility was found to be compliant with monitoring requirements. • Details noted from Annual Report Review: In the 2006 no Aluminum was reported on the residuals sampling summary form or the in lab report for metals analyses. The 2005 report was missing PAN,which can be calculated from nutrient data. The 2005 report was received on April 5, 2006 and the 2006 report was received on March 15, 2007. • For further details see Annual Report Review below. PATOGEN AND VECTOR ATTRACTION N/A Page: 2 Permit:W00006594 Owner-Facility: Unifi Inc Inspection Date: 09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine TREATMENT Aerobic Digestion STORAGE Aerobic digester SAMPLING During the inspection a grab sampling was taken by the operator for the following parameters: Total metals, NH3,TP, TKN,TCLP. The grab sample was taken from aerobic digester,which was well mixed, so the grab should be representative of the entire volume. Contract labs used for analysis include TRITEST and Statesville Analytical. TRANSPORT The contractor, PLA, keeps two transport forms. The loading form is kept at the loading site at the Unifi plant near the aerobic digester tracking the volume of sludge that is loaded on the tanker truck. Another form is kept in the contractor's pick-up truck at the land application site with the spreaders. Copies of the permits and spill control plans are kept on the tanker truck driver's clipboard and in the contractor's pick-up at the site with the spreaders. LAND APPLICATION SITE Ronald O'Quinn farm application site was to review compliance of the distribution program with performance standards and operation and maintenance requirements. Buffers appeared to be adequate for a Class B permit although these buffers are not required for Class A permit. OTHER N/A ANNUAL REPORT REVIEW Reporting Period: 2005 and 2006 Monitoring Frequency for Condition III. 2. (TCLP): Annually Monitoring Frequency for Condition III. 3. (Residuals Analysis) and Condition III. 4. (Pathogen &Vector Attraction Reduction):Annually 1.Annual Land Application OR Annual Distribution and Marketing/Surface Disposal Certification Form Was a certification form submitted?YES • Did it indicate compliance?YES •Was it signed by the appropriate people?YES • If permitted for distribution how many dry tons per year was distributed? See below. • Was land application conducted during the reported year? N/A • What is the total number of fields in permit? N/A Page: 3 Permit:WQ0006594 Owner-Facility: Unifi Inc Inspection Date:09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine •What was the total number of fields land application occurred during the year? N/A • What was the total acres land application occurred on this year? N/A • How many dry tons and dry tons per acre were applied? N/A • Were the applications within the permitted amount? N/A •Verify PAN if more than 10 tons/acre. N/A • Comments: 102.76 dry tons in 2005 and 17.95 dry tons 2006. 2. Monitoring • Were the analyses conducted at the required frequency?YES • Were the metals analyses reported on the Residual Sampling Summary Form?YES • Were the results reported in mg/kg?YES • Were the heavy metals within ceiling concentration permit limits?YES • If no,were the lab analyses attached?YES • Were all the required parameters tested? NO • Was TCLP analysis conducted?YES • Comments: In the 2006 no Aluminum was reported on the residuals sampling summary form or the in lab report for metals analyses. The 2005 report was missing PAN which can be calculated from nutrient data. 3. Field Summary Were the land application events recorded on the Field Summary Forms? N/A •Was a Field Summary Form submitted for each field? N/A •Were all the residuals applied to permitted land? N/A • Were all the residuals applied from permitted sources? N/A •Were the field loading rates for each metal and PAN calculated (year to date)? N/A Were the cumulative pollutant loading rates calculated? N/A • Were the calculations correct? N/A • Were the PAN loading rates within permit limits? N/A • Were the heavy metal cumulative pollutant loading rates within permit limits? N/A •Were the residuals applied on a suitable crop? N/A • Were the applications conducted during the crop's growing season? N/A • Were the Field Summary Forms complete? N/A • Comments: N/A 4. Pathogen and Vector Attraction Reduction • Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? N/A • Did the form indicate the period of coverage,the residual class, and the pathogen reduction alternative and the vector attraction reduction option used? N/A • Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? N/A • Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? N/A • If lime stabilization was used was the pH temperature corrected? N/A • Comments: N/A 5. Soil Tests • Was a Standard Soil Fertility Analysis conducted for each application field? N/A •Were the soil pH's 6.0 or greater for each application field? N/A Were the copper and zinc indexes in the soil less than 3000 for each application field? N/A • Comments: N/A 6. General • Was the report in the proper format?YES •Were any parts of the annual report missing? NO Was the report submitted on time? NO • Comments: The 2005 report was received on April 5, 2006 and the 2006 report was received on March 15, 2007. • Page: 4 Permit:WQ0006594 Owner-Facility: Unifi Inc Inspection Date:09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine Page: 5 Permit:WO0006594 Owner-Facility: Unifi Inc Inspection Date:09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine Type Yes No NA NE Land Application 0 Distribution and Marketing ■ Record Keeping Yes No NA NE Is GW monitoring being conducted, if required? n ❑ • ❑ Are GW samples from all MWs sampled for all required parameters? 0 ❑ • 0 Are there any GW quality violations? ❑ ❑ • Is GW-59A certification form completed for facility? ❑ ❑ • ❑ Is a copy of current permit on-site? ■ ❑ ❑ ❑ Are current metals and nutrient analysis available? ■ ❑ ❑ ❑ Are nutrient and metal loading calculating most limiting parameters? ■ ❑ ❑ ❑ a. TCLP analysis? • ❑ ❑ ❑ b. SSFA(Standard Soil Fertility Analysis)? ■ ❑ ❑ ❑ Are PAN balances being maintained? • ❑ ❑ ❑ Are PAN balances within permit limits? ■ ❑ ❑ ❑ Has land application equipment been calibrated? ❑ ❑ ❑ • Are there pH records for alkaline stabilization? ❑ ❑ • ❑ Are there pH records for the land application site? ❑ ❑ ■ ❑ Are nutrient/crop removal practices in place? ■ ❑ ❑ ❑ Do lab sheets support data reported on Residual Analysis Summary? • ❑ ❑ ❑ Are hauling records available? • 0 ❑ ❑ Are hauling records maintained and up-to-date? ■ ❑ ❑ ❑ #Has permittee been free of public complaints in last 12 months? ■ ❑ ❑ ❑ Has application occurred during Seasonal Restriction window? M ❑ ❑ ❑ Comment: No comments. Treatment Yes No NA NE Check all that apply Aerobic Digestion Anaerobic Digestion ❑ Alkaline Pasteurization(Class A) ❑ Page: 6 Permit:W00006594 Owner-Facility: Unifi Inc Inspection Date: 09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine Alkaline Stabilization(Class B) 0 Compost Drying Beds n Other Comment: Sampling Yes No NA NE Describe sampling: During the inspection a grab sampling was taken by the operator for the following parameters:Total metals, NH3,TP,TKN,TCLP. The grab sample was taken from aerobic digester,which was well mixed,so the grab should be representative of the entire volume. Is sampling adequate? • n 0 n Is sampling representative? • n ❑ Comment: No comments. Transport Yes No NA NE Is a copy of the permit in the transport vehicle? 0 0 0 • Is a copy of the spill control plan in the vehicle? n ❑ ❑ • Is the spill control plan satisfactory? 0 0 0 • Does transport vehicle appear to be maintained? ■ n ❑ 0 Comment: See summary for comments. Land Application Site Yes No NA NE Is a copy of the permit on-site during application events? • n n Q Is the application site in overall good condition? ■ n n 0 Is the site free of runoff/ponding? • n ❑ n If present, is the application equipment in good operating condition? • 000 Are buffers being maintained? i• n ❑ ❑ Are limiting slopes buffered? 10%for surface application 0 0 ■ n 18%for subsurface application 0 0 • 0 Are there access restrictions and/or signs? M 0 n Is the application site free of odors or vectors? ■ n n n Have performance requirements for application method been met? For injection? O n • 0 Page: 7 Permit:WO0006594 Owner-Facility: Unifi Inc Inspection Date: 09/21/2007 Inspection Type:Compliance Evaluation Reason for Visit:Routine For incorporation? ❑ ❑ ■ ❑ Does permit require monitoring wells? ❑ ■ ❑ ❑ Have required MWs been installed? onion Are MWs properly located w/respect to RB and CB? 0 ❑ R ❑ Are MWs properly constructed(including screened interval)? 0 0 • ❑ Is the surrounding area served by public water? ❑ ■ ❑ 0 If Annual Report indicates overapplication of PAN,are wells nearby that may be impacted? ❑ ❑ ■ ❑ Are soil types consistent w/Soil Scientist report/evaluation? U ❑ ❑ ❑ Is the water table greater than 1'/3'bls. 0 0 • 0 Is application occurring at the time of the inspection? ❑ ■ ❑ ❑ Comment: See summary for comments. Page: 8 o f WArFR Michael F.Easley,Governor C� 0 William G.Ross Jr.,Secretary 0 7 North Carolina Department of Environment and Natural Resources Alan W.Klimek,P.E.,Director 0 C Division of Water Quality RECEIVED October 2, 2003 N.Q. Dept. of EHNT1 MS.LISA HAYNES,ENVIRONMENTAL BIOLOGIST OCT - 7 2003 UNIFI, INC. P.O. BOX698 Winsterl-� ter YADKINVILLE, NC 27055 Region.. Subject: Application No. WQ0006594 Additional Information Request#2 Unifi, Inc. Plants 2 & 15 Distribution of Residual Solids Distribution of Residual Solids (503 exempt) Rockingham County Dear Ms. Haynes: The Non-Discharge Permitting Unit has requested that additional information be submitted in response to a preliminary review of the subject permit application package. The application was received March 25, 2002 and was held in our backlog of permit reviews. It was reviewed this summer and a letter requesting additional information was sent August 7, 2003. The required information has not yet been received. Please address the following items no later than November 3, 2003. 1. The application must be signed by an appropriate person in accordance with 15A NCAC 2H .0206. This regulation states that, for a corporation, it must be signed by a principal executive officer of at least the level of vice-president, or his duly authorized representative. Please verify that the signer meets the regulatory requirement above or sign the application following the above requirement. Alternatively, you may provide documentation the signer, or any employee holding the position of the signer, is a duly authorized representative through a letter of delegation from someone meeting the above requirement. 2. In reference to application item III.2., I was unable to obtain any information for permits under 0002 or 0104. Please check the permit numbers for the generating facilities and provide all facility permit numbers and the issuing authorities. 3. In reference to application item VI.3., please revise the Biosolids Information Sheets to show the name and address of the entity who prepared the residual. That would appear to be Unifi, Inc. Plant 2 with the Reidsville address and Unifi, Inc. Plant 15 with the Mayodan address. Please be aware that you are responsible for meeting all requirements set forth in North Carolina rules and regulations. Any oversights that occurred in the review of the subject application package are still the responsibility of the applicant. In addition, any omissions made in responding to the above items may result in future requests for additional information. Please reference the subject application number when providing the requested information. Two copies of all revised and/or additional documentation should be signed, sealed,dated, and submitted to my attention at the address above/below. Please note that failure to provide this additional information on or before the above requested date may result in your application being denied. •i. Non-Discharge Permitting Unit Internet http://h2o.enr.state.nc.us/ndpu 1617 Mail Service Center,Raleigh,NC 27699-1617 Telephone (919)733-5083 Fax (919)715-6048 DENR Customer Service Center Telephone 1 800 623-7748 An Equal Opportunity Action Employer 50%recycled/10%post-consumer paper Ms. Lisa Haynes Page 2 October 2, 2003 If you have any questions regarding this request,please do not hesitate to contact me at duane.leith@ncmail.net or(919)733-5083, extension 370. You may also check the future status of this project online at http://h2o.enr.state.nc.us/bims/Reports/reportsPermits.html. Thank you for your cooperation. Sincerely, Duane Leith Non-Discharge Permitting Unit Cc: Mr. Chris • - • s._ • - e• • .. .• .. • . 'fit . Permit Application File WQ0006594 RECEWED NON-DISCHARGE APPLICATION REVIEW REQUEST FORM.C. Dept.of EHNR AUG 1 1 2003 Date: August 7, 2003 To: ❑ Forrest Westall, ARO-WQS ❑ Debra Watts, CO-GWinSton-Salem ❑ Paul Rawls,FRO-WQS Regional Office ❑ Rex Gleason, MRO-WQS Copies Sent to CO-GWS: ❑ Ken Schuster,RRO-WQS ❑ Jim Mulligan,WaRO-WQS ❑ Rick Shiver,WiRO-WQS Copies Sent to RO-WQS: 1 ' QS ® Distribute 1 Copies to RO-GWS From: Duane Leith,Non-Discharge Permitting Unit Telephone: (919)733-5083 ext. 370 Fax: (919)715-6048 E-Mail: duane.leith@ncmail.net 3 �� A. Permit Number: W00006594 ASSIGNED TO / B. Owner: t DUE DATE C. Facility/Operation: Unit-1Incorporated-A Sludge/Plant#2 and#15 Distribution of Res. Solids ❑ Proposed ® Existing ❑ Facility ® Operation D. Application: 1. Permit Type: ❑ CS (O&M) ❑ Surface Irrigation ❑ Reuse ❑ H-R Infiltration ❑ Recycle ❑ I/E Lagoon ❑ GW Remediation (ND) For Residuals: ❑ Land App. ® D&M ❑ Surface Disposal ❑ 503 ❑ 503 Exempt ❑ Animal 2. Project Type: ❑ New ❑ Major Mod. ❑ Minor Mod. ® Renewal ❑ Renewal w/Mod. E. Comments/Other Information: ® I would like to accompany you on a site visit. Waste is industrial Class A equivalent. This is a very old application which I am trying to clear up. BIMS shows that RO comments have been requested, but I have no form NDARR in the file and no response, so I'm sending another request. Attached, you will find all information submitted in support of the above-referenced application for your review,comment, and/or action. Within 30 calendar days,please take the following actions: For RO-WQS: ® Return a Completed Form NDSRR. ❑ Attach Attachment B for Certification by the NDPU. ❑ Issue an Attachment B Certification from the RO*. * Remember that you will be responsible for coordinating site visits, reviews, as well as additional information requests with other RO-WQS and RO-GWS representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for additional detail. For CO-GWS: ❑ Return a Memorandum with Permit Condition Recommendations. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Non-Discharge Permitting Unit contact person listed above. RO-WQS Reviewer: Date: FORM: NDARR 09/02 Page 1 of 1 r i NON-DISCHARGE REGIONAL WATLI QUALITY STAFF REPORT AND RECOMMENDATIONS Date: -Ser° t ` D c 3 County: /QQ ,',"h,l-I'"1 To: Non-Discharge Permitting Unit Permitee: (,z,✓� ; A/c. NDPU Reviewer: Application No.: W000 D 6 S g y Regional Login No: GENERAL INFORMATION 1. This application is(check all that apply): ❑ New n Renewal ❑ Minor Modification ❑ Major Modification ❑ Surface Irrigation ❑ Reuse ❑ Recycle ❑ High Rate Infiltration ❑ Evaporation/Infiltration Lagoon FLand Application of Residuals ❑ Attachment B included as appropriate ❑ 503 regulated ❑ 503 exempt ❑ Distribution of Residuals ❑ Surface Disposal 2. Was a site visit conducted in order to prepare this report? ❑ Yes or rig No. a. Date of site visit: b. Person contacted and contact information: c. Site visit conducted by: d. Inspection Report Attached: ❑ Yes or❑ No. 3. Is the following information entered into the BIMS record for this application correct? Yes or ❑ No. If no, please complete the following or indicate that it is correct on the current application. For Treatment Facilities: a. Location: b. Driving Directions: c. USGS Quadrangle Map name and number: d. Latitude: Longitude: e. Regulated Activities/Type of Wastes (e.g., subdivision, food processing, municipal wastewater): For Disposal Sites: (If multiple sites either indicate which sites the information applies to, copy and paste a new section into the document for each site, or attach additional pages for each site) a. Location(s): b. Driving Directions: c. USGS Quadrangle Map name and number: d. Latitude: Longitude: FORM:NDSRR 03/02 1 iiiiii NON-DISCHARGE REGIONAL WATER QUALITY STAFF REPORT AND RECOMMENDATIONS RENEWAL AND MODIFICATION APPLICATIONS(use previous section for new or major modification systems) DESCRIPTION OF WASTE(S)AND FACILITIES 1. Are there an appr9Priantely certified ORCs for the facilities?0Yes or❑ No. �Zi s �7'A jCANO eft Operator in Charge: Certificate#: Back-Operator in Charge: Certificate#: 2. Is the design, maintenance and operation (e.g. adequate aeration, sludge wasting, sludge storage, effluent storage, etc) of the treatment facilities adequate for the type of waste and disposal system? Vil Yes or❑ No. If no,please explain: 3. Are the site conditions (soils, topography, etc) maintained appropriately and adequately assimilating the waste?® Yes or❑ No. If no, please explain: 4. Is the residuals management plan for the facility adequate and/or acceptable to the Division? Yes or❑ No. If no, please explain: 5. Are the existing application rates (hydraulic or nutrient) still acceptable? 12 Yes or ❑ No. If no, please explain: 6. Are there any buffer conflicts (treatment facilities or disposal sites)? ❑ Yes or al No. If yes, please attach a map showing conflict areas or attach any new maps you have received from the applicant to be incorporated into the permit: 7. Is the type and/or volume of waste(s) as written in the existing permit correct? ( ] Yes or ❑ No. If no,please explain: 8. Is the description of the facilities as written in the existing permit correct? rjg Yes or E No. If no, please explain: 9. Has a review of all self monitoring data been conducted? ❑ Yes or ❑ No. Please summarize any findings resulting from this review: 10. Check all that apply: ❑ No compliance issues; ❑ Notice(s)of violation within the last permit cycle; ❑ Current enforcement action(s) ❑ Currently under SOC; 0 Currently under JOC; 0 Currently under moratorium. If any items checked, please explain and attach any documents that may help clarify answer/comments (such as NOV,NOD etc): 11. Have all compliance dates/conditions in the existing permit, SOC, JOC, etc. been complied with? ❑ Yes or 0 No. If no,please explain: 12. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit?❑ Yes or 71 No. If yes, please explain: FORM:NDSRR 03/02 3 NON-DISCHARGE REGIONAL WATI,J. QUALITY STAFF REPORT AND RECOMMENDATIONS ADDITIONAL REGIONAL STAFF REVIEW ITEMS 27-tiz-2—r A,; )04-‘ rta—r21-4.rel 4- A.-12 7 FORM:NDSRR 03/02 5 NON-DISCHARGE REGIONAL WATEJ. QUALITY STAFF REPORT AND RECOMMENDATIONS EVALUATION AND RECOMMENDATIONS 1. Provide any additional narrative regarding your review of the application.: 2. List any items that you would like NDPU to obtain through an additional information request. Make sure that you provide a reason for each item: Item Reason 3. List specific Permit conditions that you recommend to be removed from the permit when issued. Make sure that you provide a reason for each condition: Condition Reason 4. List specific special conditions or compliance schedules that you recommend to be included in the permit when issued. Make sure that you provide a reason for each special condition: Condition Reason • 5. Recommendation: ❑ Hold,pending receipt and review of additional information by regional office; ❑ Hold, pending review of draft permit by regional office;g Issue; ❑ Deny. If deny,please state reasons: �"� 6. Signature of report preparers +_ / • Signature of WQS regional supervisor: •i Date: O 3 a, / S FORM:NDSRR 03/02 4 RECEIVED ri Dept. f Gti N . 04/02/02 Permit Number WQ0006594 N.C. Permit Tracking S] Program Category AUG t i 2003 Status Project Type Non-discharge �J�J ,��$ In review Renewal Permit Type �`,n stO n:t �j y{^^��4S � �t Version Permit Classification Distribution of Residual Soli3P5�3 exempt) Individual Primary Reviewer Permit Contact Affiliation shannon.thornburg Timothy Cole Permitted Flow PO Box 698 Yadkinville NC 27055 Facility Facility Name Major/Minor Region Unifi Incorporated-A Sludge/Plant #2 Minor Winston-Salem Location Address County PO Box 698 Rockingham Yadkinville NC 27055 Facility Contact Affiliation Owner Owner Name Owner Type • Unifi Inc Non-Government Owner Affiliation Timothy Cole PO Box 698 Yadkinville NC 27055 Dates/Events Draft Scheduled Public Orig Issue App Received Initiated Issuance Notice Issue Effective Expiration 03/25/02 Regulated Activities Requested/Received Events ;Textile manufacturing RO staff report received RO staff report requested V- 7-U 3 Additional information requested Additional information received Grouri \ comments requested Gro d comments received A/ Outfall r : 51-Cz..�- - = 0( J23i:200e Waterbody Name Stream Index Number Current Class Subbasin OF W A 7'69 Michael F.Easley,Governor O QG William G.Ross Jr.,Secretary North Carolina Department of Environment and Natural Resources > _� Gregory J.Thorpe,Ph.D.,Acting Director 0 -c Division of Water Quality RFC`F;VZD April 2,2002 N.C. L) %t. ;.?;• EHNR UNIFI, INC. APR 0 5 2002 LISA HAYNES P.O. BOX 737 MADISON NC 27025 ReQ oAla1 C ff f Subject: Acknowledgemen o pp is io WQ0006594 Distribution of Other Residual Solids Rockingham County Dear Mrs.Haynes: The Non-Discharge Permitting Unit of the Division of Water Quality (Division)acknowledges receipt of your permit application and supporting materials on January 25,2002. This application package has been assigned the number listed above. Your application package has been assigned to Shannon Thornburg for a detailed review. The reviewer will contact you with a request for additional information if there are any questions concerning your submittal. If you have any questions, please contact Shannon Thornburg at 919-733-5083 extension 353, or via email at Shannon.Thomburg@ncmail.net. If the reviewer is unavailable, you may leave a message on their voice mail, and they will respond promptly. PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES ON THIS PROJECT. Sipcerely, i—K-im H. Colson,P.E. Supervisor,Non-Discharge Permitting Unit cc: ' .4 .,op Permit Application File WQ0006594 at co Non-Discharge Permitting Unit Internet http://h2o.enr.nc.state.us/ndpu 1617 Mail Service Center,Raleigh,NC 27699-1617 Telephone (919)733-5083 Fax (919)715-6048 DENR Customer Service Center Telephone 1 800 623-7748 An Equal Opportunity Action Employer 50%recycled/10%post-consumer paper 04/02/02 Permit Number ` Permit Tracking S] Program Category Status Project Type Non-discharge In review Renewal Permit Type Version Permit Classification Distribution of Residual Solids (503 exempt) Individual Primary Reviewer Permit Contact Affiliation shannon.thornburg Timothy Cole Permitted Flow PO Box 698 Yadkinville NC 27055 Facility Facility Name Major/Minor Region Unifi Incorporated-A Sludge/Plant #2 Minor Winston-Salem Location Address County PO Box 698 Rockingham Yadkinville NC 27055 Facility Contact Affiliation Owner Owner Name Owner Type Unifi Inc Non-Government Owner Affiliation Timothy Cole PO Box 698 Yadkinville NC 27055 Dates/Events Draft Scheduled Public Orig Issue App Received Initiated Issuance Notice Issue Effective Expiration 03/25/02 Regulated Activities Requested/Received Events Textile manufacturing RO staff report received RO staff report requested Additional information requested Additional information received Groundwater comments requested Groundwater comments received Outfall Waterbody Name Stream Index Number Current Class Subbasin State of North Carolina Department of Environment, Health and Natural Resources 7;7;:iirA Division of Water Quality p - James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary p E H N F A. Preston Howard, Jr., P.E., Director April 22, 1997 Mr. Tim Cole, Environmental Affairs Manager UNIFI, Inc. Post Office Box 698 Yadkinville, North Carolina 27055 Subject: Permit No. WQ0006594 Unifi, Inc. Plant#2 Reidsville Unifi, Inc. Plant#15 Mayodan Distribution of Class A Wastewater Residuals Rockingham County Dear Mr. Cole: In accordance with your application received on January 30, 1997, we are forwarding herewith • Permit No. WQ0006594 dated April 22, 1997, to Unifi, Incorporated for the operation of a wastewater residuals facility for the distribution of residuals. Please note, your previous permits were conditioned for a limited land application of residuals program. Please be advised, this permit contains several different conditions for your new residuals distribution program. It is understood, the wastewater treatment facilities,processing the subject residuals, are already permitted under a pre-treatment program permit. It is noted that all domestic wastewater is kept separated from the subject industrial wastewaters at both Unifi Plants. Please note, a permit modification is required, if domestic wastewater is ever mixed with the subject industrial residuals. Additional treatment facilities may be necessary, to meet the requirements for PFRP with domestic wastewater residuals. This permit shall be effective from the date of issuance until March 31, 2002, shall void Permit No. WQ0006594 issued June 28, 1993, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring and reporting requirements contained in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447, Raleigh, NC 276 1 1-7447. Unless such demands are made this permit shall be final and binding. P.O. Box 29535,Raleigh, North Carolina 27626-0535 Telephone(919)733-5083 FAX(919)733-0719 An Equal Opportunity Affirmative Action Employer 50%recycled/10%post-consumer paper If you need additional information concerning this matter, please contact . John (919) 733-5083 extension 546. Sey at • Sincerely, A. Preston Howard, Jr., .E. cc: Rockingham County Health Department Environmental waste Recycling Incorporated Winston-Salem Regional Office, Water Quality Section Winston-Salem Regional Office, Groundwater Section Bob Cheek, Groundwater Section, Central Office Training and Certification Unit Facilities Assessment Unit ' `J NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES RALEIGH PERMIT FOR THE DISTRIBUTION OF RESIDUALS In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended,and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Unifi, Incorporated Rockingham County FOR THE operation of a facility for the distribution of residuals of exceptional quality consisting of the distribution of 200 dry tons per year of residuals from the sources listed in Condition II 2, with no discharge of wastes to the surface waters, pursuant to the application received on January 30, 1997, and in conformity with the — project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment,Health and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until March 31, 2002, shall void Permit No. WQ0006594 issued June 28, 1993, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS 1. The distribution residuals program shall be effectively maintained and operated as a non- discharge system to prevent the discharge of any wastes resulting from the operation of this program. 2. This permit shall become voidable in the event of failure of the residuals program to adequately protect the assigned water quality standards of the surface waters and • groundwaters. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. 4. In the event that the residuals program is not operated satisfactorily,including the creation of nuisance conditions,the Permittee shall take any immediate corrective actions as may be required by the Division. 5. Diversion or bypassing of the untreated residuals or leachate from the residual treatment facilities is prohibited. 6. All leachate must be reused as a wetting agent for the processing of residuals or routed to the head of the treatment plant. 1 II. OPERATION AND MAINTENANCE REQUIREMENTS 1 . The residuals treatment facilities shall be properly maintained and operated at all times. 2. No residuals other than the following are hereby approved for distribution in accordance with this permit: Permit Volume Source County Number (Dry Tons/Year) Unifi, Inc., Plant No. 2 Rockingham City of Reidsville 100 Reidsville WWTP Unifi, Inc. Plant No. 15 Rockingham Town of Mayodan 100 Mayodan WWTP Total 200 3. All residuals shall be adequately stored to prevent leachate runoff until treated. The finished product may be placed on a concrete pad, placed under shelter or covered until such time as it is distributed to the buyer. If an alternate storage site is to be used, approval must be obtained from the Division of Water Quality. 4. No other residuals other than those specified under Condition II 2 above may be distributed. The Permittee shall request and obtain a permit amendment from the Division of Water Quality for each additional residual source prior to acceptance of that residual. 5. For a wastewater residual of exceptional quality to be sold or given away in bags or other container for application to the land,the following must be satisfied:The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly Average Concentrations (Dry Weight Basis) must be maintained: Ceiling Monthly Average Concentrations Concentrations Parameters mg/kg mg/kg Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Nickel 420 420 Zinc 7,500 2,800 6. Upon classification of the facility by the Certification Commission, the Permittee shall employ a certified residuals operator to be in responsible charge (ORC) of the residuals program. The operator must hold a certificate of the type classification assigned to the residuals program by the Certification Commission. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of Title 15A NCAC 8A, .0202. 7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals treatment area onto the adjacent property or into any surface waters. 2 8. A label shall be affixed to the bag or other container in which residuals that are sold or given'away for application to the land, or an information sheet shall be provided to the person who receives the residuals sold or given away in an other container for application to the land. The label or information sheet shall contain the following information: a. The name and address of the person who prepared the residuals that is sold or given away in a bag or other container for application to the land. b. A statement that application of the residuals to the land is prohibited except in accordance with the instructions on the label or information sheet. c. Information on all applicable buffers including a 10 foot buffer between application site and any public or private water supply source (including wells) and any stream, lake, or river. d. Residuals shall not be applied to any site that is flooded,frozen or snow-covered. e Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. III. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division of Water Quality to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee tracking all residual activities. These records shall include,but are not necessarily limited to the following information: a. source,volume and analysis of each residuals b. name of residuals'recipient,volume received,and intended use 3. A residual analysis shall be conducted annually from the date of permit issuance by the Permittee. The results of all analysis shall be maintained on file by the Permittee for a minimum of five years.The residuals analysis shall include the following parameters: Cadmium Nickel Copper Lead Zinc Aluminum _ pH . . Ammonia-Nitrogen Phosphorus Calcium Plant Available Nitrogen(by calculation) Magnesium Potassium Nitrate-Nitrite Nitrogen Sodium Total Solids TKN 3 4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) o-Cresol (200.0) m-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5) 1,1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13) Endrin (0.02) Heptachlor(and its hydroxide)(0.008) Hexachlorobenzene (0.13) Hexachloro-1,3-butadiene(0.5) Hexachloroethane (3.0) Lead(5.0) Lindane (0.4) Mercury (0.2) Methoxychlor(10.0) Methyl ethyl ketone(200.0) Nitrobenzene(2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium(1.0) Silver(5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene(0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride(0.2) 5. Three copies of all required monitoring and reporting requirements as specified in conditions III 1, III 2, III 3,and III 4 shall be submitted annually on or before March 1 of the following year to the following address: NC Division of Water Quality -- � Water Quality Section Facility Assessment Unit PO Box 29535 Raleigh,NC 27626-0535 6. Noncompliance Notification: The Permittee shall report by telephone to the Winston-Salem Regional Office,telephone number 910/ 771-4600 as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the distribution program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to receiving waters. c. Any time that self-monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system during transportation of residuals. Persons reporting such occurrences by telephone shall also file a written report in letter - form within five (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. 4 I V. GROUNDWATER REQUIREMENTS 1 . The COMPLIANCE BOUNDARY for the disposal system is specified by regulations in 15A NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary is for the disposal system constructed after December 31, 1983 is established at either(1) 250 feet from the waste disposal area, or(2) 50 feet within the property boundary, whichever is closest to the waste disposal area. An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to immediate remediation action in addition to the penalty provisions applicable under General Statute 143-215.6A(a)(1). In accordance with 15A NCAC 2L, a REVIEW BOUNDARY is established around the disposal systems midway between the Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards at the Review Boundary shall require remediation action on the part of the penmittee. 2. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. V. INSPECTIONS 1. The Permittee or his designee shall inspect the residuals storage, transport, and treatment facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health,or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance,repairs,or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division of Water Quality or other permitting authority,upon request. 2. Any duly authorized officer, employee, or representative of the Division of Water Quality may,upon presentation of credentials,enter and inspect any property,premises or place on or related to the treatment site or facility at any reasonable time for the purpose of determining compliance with this permit;may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. V I. GENERAL CONDITIONS 1. This permit shall become voidable unless the distribution activities are carried out in accordance with the conditions of this permit,the supporting materials, and in the manner approved by this Division. 2. This permit is effective only with respect to the nature and volume of residuals described in the application and other supporting data. 3. This permit is not automatically transferable. In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division of Water Quality accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. -- 4. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the.Division of Water Quality in accordance with North Carolina General Statute 143-215.6(a)to 143-215.6(c). 5 5. The annual administering and compliance fee must be paid by the Permittee within thirty (30) days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205 (c)(4). 6. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local, state,and federal)which have jurisdiction. 7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the Division of Water Quality deems necessary in order to adequately protect the environment and public health. Permit issued this the 22nd day of April, 1997 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION 4/./i4 A. reston Howard, Jr., P.E., Director vision of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0006594 • • Unifi, Inc. Application for Permit Renewal NC Permit WQ0006594 OM QUALITY THROUGH PRIDE Prepared by: Precision Land Application, Inc. 4022 White Plains Rd. Roaring River, NC 28669 (336) 957-8839 C , N.0 RE Dept.EIV ff Precision Land Application, Inc. APR 0 5 2002 Application for Renewal FiC. nai Offices Permit No. WQ0006594 Unifi, Inc. Distribution of Other Residual Solids (DORS) March 2002 Introduction Unifi, Inc. is requesting the renewal of its existing DORS permit. Unifi currently produces approximately 175 dry tons of residuals from two of its manufacturing plants. These residuals are the result of the treatment of wastewater generated by wet textile processing. Table of Contents 1. This section contains general project information including Form: DORS 06/94, and its attachments. 2. Current Permit 3. Biosolids Analysis RECEIVED WATER QUALITY SECTION MAR 2 5 2002 NON-DISCHARGE PERMITTING 4022 White Plains Rd. • Roaring River,NC 28669 • (336) 957-8839 State of North Carolina Department of Environment, Health and Natural e +sicklED q ,(TYSECT(Gr Division of Environmental Managemen i ). • !`on-1Jischaree Permit Application Form MAR 2 5 200Z • (T BIS FORM MAY BE PHOTOCOPIED FOR USE AS E' ORIGI 'AL) DISTRIBUTION OF OTHER RESIDUAL S `r &SCH GE PERMITTING This application is intended for facilities which are EXEMPT from 40 I. GENERAL INFORMATION: 1. Af;.ir.a.nt's name (please specify the name of the municipality,corporation, individual, etc.): Unif:i, Inc. 2. Prim owners or signing official's name and title(the person who is legally responsible for the facility and its compliance): Lisa Haynes, Environmental Biologist 3. ?r;ai1Lg address: >?0 Box 737 Cirv: Madison State: NC 27025 Zip: • Teie:,hone Number: ( 336 ) 427-1144 4. Application Date:• March 2002 5. Fee Submitted: S 0 .0 0 [The permit processing fee should be as specified in 15A NCAC 2H.0205(c)(5).) • 6. Specify how these residuals will be distributed: sold or given away in bags or other containers; lawn (bull:): horse garden (bulk): X other. Bulk Liquid 7. if the a.�..,,�..�.... for residual disposal consists of"surface disposal"as defined under 40 CFR Part 503.please complete the application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify if there is any storage of residuals in a s_face impoundment or disposal thru landfilling. Explain: N/A E. Is the residual process facility also the generator? X Yes; No R— 36°21 ' 58"N 79°39 5�� 9. Lail ude: M— 3 0°2 9 ' 6 0" N Longitude: 8 0°5 7 ' 3 0" PI of residual process facility private; state;Xlocal government, 10. Specify whether the process facility is owned by: federal; 11. Co:�.:y where facility is located: Rockingham County • II. PERMIT INFORMATION: • • 1. Application No. twill be completed by DEM): 2. Specify whether project is: new; X renewal'; modification • For renewals, complete all sections included in the application. Engineering Signature and Seal not required for renewals or if there is not any construction involved with the subject project 3. If this application is being submitted a_s a result of a renewal or modification rilto22 an existing permit. list the existing permit numberWQ 0 0 0 6 5 9 4 and its issue date P FORM: DORS 06194 Pane 1 of 7 III. FACILITY INFORMATION (attach additional pages for additional sources of residuals): :,. ; `� . � _ ; €c:,cratedorprepar,:d:Unifi, INC. Mayodan & Reidsville Plant: 2. Facility permit number: M-0104 ; facility permit bolder: Unifi, Inc . 3. Sp_cify whether facility in Section III.] is owned by: federal; X private; state; local government; R— 3. Omgd R— .8idgd C. Specify facility design flow: M— 1. 5mgd red; facility average daily flow: M— .7mcid mgd; • Type of residual storage: Steel & Concrete Tanks V'oiu.-me of residual storage: 250 , 000 & 500, 000 gal , Length of residuals storage at facility: 90 & 90 days (the Division requires a minimum 30 days storage in units that are separate from treatment system, i.e.not in clarifiers,aeration basins,etc.); Estimated volume of residuals: 150 — 200 (city tons/yr.); 5. If the residual process facility is not the same as the generator,please specify delivery frequency and quantity of residual to •• be processed: N/A 6. Facility contact(person familiar with residuals preparation): Lisa Haynes , 7. Facility contact's telephone number: ( 336 ) 4 2 7—114 4 Reidsville 8. Location of treatment facility: & Mayodan State; NC Rock ingha uary 9. Malincaddress: PO Box 787 Madison, NC 27025 10. Specify the source of the residuals: treanent of water (alum sludges); X treatment of industrial wastewater (100 w industrial residuals); treatment of industrial wastewater mixed with domestic wastewater (please specify a.prorzte percentages of %industrial wastewater, %domestic wastewater); other(explain): - Attach explanation of either the treatment process,manufacturing process, or bow the waste is generated. Provide full and complete details of the entire process. See Attachment 11. Does the facility which generates the residuals have an approved pretreatment program? Yes; No. N/A This includes facilities which are classified as a"Class I"facility (any publicly owned treatment works required,under 40 CFR 403.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as "Class I" b* the appropriate federal or State authority) IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals): 1. Information for Hazardous Waste (RCRA)Determination. The information requested on the limitations specified below pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contribution or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources. a. Are any of the residuals covered by this application listed in 40 CFR 261.31 261.33? Yes; X ,No. If Yes. list the number(s): b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? Yes; X No. Attach laboratory results for the Toxicity Characteristic Leaching Procedure Analyses, Reactivity, Ignitability, and Corrosivity for each residual. FORM: DORS 06/94 Page 2 of 7 ote• If the following constituent levels(as determined by the Toxicity Characteristic Leaching Procedure Analyses)arc exceeded in the residuals or if the pH of the residual is not within the range listed below, the residual is b. definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels. PPM PPM Arsenic 5.0 Barium 100.0 Benzene 0.5 Cadmium 1.0 Carbon tetrachloride 0.5 Chlordane 0.03 Chlorobenzene 100.0 Chloroform 6.0 Chromium 5.0 o-Cresol 200.0 m-Cresol 20v^.0 p-Cresol 200.0 Cresol 200.0 2,4-D 10.0 1,4-Dichlorobenzene 7.5 1,2-Dichloroethane 0.5 • 1,1-Dichloroethylene 0.7 2,4-Dinitrotoluene 0.13 Endrin 0.02 Heptachlor(and its hydroxide) 0.008 = Hexachlorobenzene 0.13 Hexachloro-1,3-butadiene 0.5 . Hexachloroethane 3.0 Lead 5.0 Lindane 0.4 Mercury 0.2 Methexychlor 10.0 Methyl ethyl ketone 200.0 , Nitrobenzene 2.0 Pentachlorophenol 100.0 Pyridine 5.0 Selenium 1.0 Silver 5.0 Tetrachloroethylene 0.7 Toxaphene . 0.5 Trichloroetbylene • 0.5 2,4,5-Trichlorophenol 400.0 2,4,6-Trichlorophenol 2.0 2,4,5-TP (Silvex) 1.0 Vinyl chloride 0.2 pH (2:1 volJwt.): >2.0 s.u. - <12.5 s.u. NOTE: IF ANY OF THE RESIDUALS MEET THE DEFINITIONS OF A HAZARDOUS WASTE, AS NOTED IN EITHER "A" OR "B" ABOVE, A PERMIT CANNOT BE ISSUED FOR THAT MATERIAL AND IT SHOULD NOT BE INCLUDED' AS PART OF THIS APPLICATION. 2. For each residual,please attach a complete chemical analysis of the material. This analysis must be comprehensive enough to completely characterize the residual and must be based upon a review of the process that generates the material. If the facility that will generate the residual is not yet in operation, the characterization must be based on similar existing facilities and projection based on the type of facility. The analysis must include a minimum of the following parameters and any other}mown and suspected contaminants that are tributary to the system. Cadmium Aluminum pH Copper Ammonia-Nitrogen Phosphorus Lead Calcium Potassium Nickel Magnesium Sodium . Zinc Nitrate-Nitrite Nitrogen TICN . %Total Solids Plant Available Nitrogen(by calculation) • 3. Wastew•ater residuals can not be sold or given away if the concentration of any pollutant in the residuals exceeds the ceiling concentrations specified in the table below. Specify the pollutant concentration of these residuals(attach lab analysis): Pollutant Pollutant Ceiling Concentration (mg/kg) Pollutant Concentration (mg/kg) Dry Weight Basis Dry Weight Basis Cadmium 85 See Analysis Section Copper 4300 . - . - Lead 840 • " Nickel 420 " Zinc 7500 " FORM: DORS 06/94 Pane 3 of 7 = Provide. all applicable pilot studies and any bench scale tests performed on each residual source and the results,includin, ' the approximate fertilizer equivalent. r 5. Wastewater residuals can't be sold or given away in bags or other containers for application to the land unless one of tyc following options is satisfied. A Specify either A or B. Please be advise. if the residuals are to be sold or given away in bulk for application tc lawn or home garden then Option A is the only option. A . The pollutant concentration of the residuals must be less than Pollutant Monthly Average Concentrations listed in the table below. Monthly Average Concentrations Pollutant Concentration I Pollutant Dry Weight Basis (mg/kg) Dry Weight Basis (mg/kg) Cadmium Copper 39 See Analysis Section II 1500 Lead 300 , I Nickel 420 II Zinc 2800 I B. The product of the concentration of each pollutant in the residual and the annual.whole residual application rate for the residual shall not cause the Annual Pollutant Loading Rate to be exceeded. In order for the Annual Whole Residual Application Rate (AWRAR) to be calculated the Annual Pollutant - Loading Rate (APLR) is divided by the pollutant concentration (PC) times 0.001 (a conversion factor) as s follows: I AWRAR= APLR , - PC * 0.001 Pollutant Annual Pollutant Annual Whole Residual I Pollutant Concentration Loading Rates Application Rate Dry Weight Basis - (APLLR) (AWRAR) (mg/kg) kg/hectare _ Cadmium 1 .9 -... Copper 75 Lead 15 Nickel 21 Zinc 140 The AWRAR for the residual is the lowest AWRAR calculated. This is the maximum rate at which the subject residual can be applied (to convert ke/bectare to lbs/acre multiply'by 0.8924). Please specify kg/yectare or lbsfacre: AWRAR= N/A V. PATHOGEN REDLUCTION INFORMATION (attach add. pages for additional sources of residuals) In accordance with 15A NCAC 2H .0200,pathogen reduction can be achieved using either 40 CFR Part 257 or 40 CFR Part 503. Since the pathogen reduction requirements found in 40 CFR Part 257 (note, "Processes to Further Reduce Pathogens" or PFRP) are incorporated into 40 CFR Part 503, only Part 503 is listed below. Please check which of the following applies to the subject residual: • FORM: DORS 06/94 Page 4 of 7 • • 1. in order for the residuals to be Class A, in accordance with the pathogen requirements in 40 CFR 503.32(a).either Part a or . Part b Lad one of the options in Part c must be completed (please submit all lab analysis.test results and calculations): N/A a. A Fe`:, cnlifrrm density less than 1000 Most Probable Number per gram of total dry solids, or b. A 521-nnnetla sp. density less than 3 Most Probable Number per 4 grams of total dry solids. c. In addition to Part a or Part b being met,one of the following alternatives must also be completed. Please specify 1, 2, 3,4, 5a, 5b, 5c, 5d, 5e, 5f, 5g or 6 below being met _ 1. Iirne/te^,^t'att"_e - an increased residuals temperature should be maintained fur a prescribed period of time, in accordance with the following guidelines. The results (D) shall be the amount of time, in days, that the residuals shall remain at the given temperature: Time and Temxrature Guidelines • Total Solids I Temoerarure (t) I Minimum Time 1 Equation Notes • No beating of crn21l > or=7% > or=50° C > or= 20 minutes D=13 j.700.E particles by warmed 100.14 t gases or immiscible liquid. > or=7% > or=50° C > or= 15 seconds D= 131.700.000 , Small particles heated by 100.14 t warmed gases or immiscible liquid. < 7% > or= 50° C > or= 15 seconds D=1;1.700.000 to 100.14 t < 30 minutes < 7% > or= 50° C >or= 30 minutes I D=50.070.000 100.14 t • 2. .Lkaline treannent- the pH of the residuals is raised to greater than 12 for at least 72 hours. During this time, the temperature of the residuals should be greater than 52° C for at least 12 hours. In addition, after the 72 hour period, the residuals are to be air dried to at least 50%total solids. 3. prior testing for Enteric VirusNiable Helminth Ova -the residuals are analyzed for the presence of enteric viruses (Plaque-forming units) [pfu]and viable belminth ova. If the residuals are analyzed before the pathogen reduction process and found to have densities of enteric virus <1 pfu/4 grams of total solids and viable belminth dva<1/4g total solids, the residuals are Class A with respect to enteric virus and viable belminth ova until the next monitoring episode. If the residuals are analyzed before the pathogen reduction process and found to have densities of enteric virus > or= 1 pfu/4 g total solids or viable belminth ova> or= 1/4 g total solids, and tested again after processing and found to meet the enteric virus and viable belminth ova levels listed under "4" below, then the processed residuals will be Class A with respect to enteric viruses and viable belminth ova when the operating parameters for the pathogen reduction process are monitored and shown to he consistent with the values or ranges of values documented. 4. no prior tegin2 for Enteric VirusNiable Helminth Ova-if the residuals are not analyzed before pathogen reduction processing for enteric viruses and viable helminth ova, the density of enteric viruses must be less than 1 pfu/4 g of total dry solids and the density of viable helminth ova must be less than 1/4 g of total dry solids, or the residuals must be treated by a"Process to Further Reduce Pathogens"or a"Process to Further Reduce Pathogens" equivalent process.. 5. The"Processes to Further Reduce Pathogens" (PFRP)are described as follows: a. Composting,- using either the within-vessel or static aerated pile composting methods, the temperature of the residuals are raised to 55°C or higher for three days. Using the windrow composting method, the residuals are raised to 55°C or higher for fifteen days. During the high temperature period,there will be 2 minimum of five turnings of the windrow. rnpmt DORS 06/94 Page 5 of 7 b. ti-a• Dr in; - residuals are dried by direct or indirect contact with bot gases to reduce the moisture content o the residuals to 10' or lower. Either the temperature of the gas in contact with the residuals exceeds 80°C o the .vet h::!h temneratt:re of the gas in contact with the residuals. when the residuals leave the.dryer. except 80° C. c. Heat Treatment- liquid residuals are heated to a temperature of 180°C or higher for thirty minutes. • Aerobic Digestion -liouid residuals are agitated with air or oxygen to maintain aerobic condition, at residence times of ten days at temperatures of 55°C to 60°C. e. Beta Ray Irradiation - residuals are irradiated with beta rays from an accelerator at dosages of at least 1.( megarad at room temperature (ca.20°C). f. Ga. •tea Rey Irradiation -residuals are irradiated with gamma rays from certain isotopes such as 60Co and 13'Cc, at dosages of at least 1.0 megarad at room temperature (ca. 20°C). - g. Pasteurization - the temperature of the residuals is maintained at 70°C or higher for at least thirty minutes. 6. The residuals shall be treated in a process that is equivalent to a"Processes to Further Reduce Pathogens" (PFRP). as determined by the permitting authority based on evaluations of the recommendations provided by the Pathogen Equivalency Committee. VI. GENERAL INFORMATION: 1. Please provide a brief narrative concerning materials handling,including the following: a. How will the materials will be handled and transported from where the residuals were produced to where it will be coated? N/A b. Where will the residuals be stored until processed? N/A c. How will leachate collection be handled? N/A I _ d What will be the duration of treatment? N/A e. Where will the final product be stored? On Site f How lcnc will the final product be stored before being distributed? 3 Months E. How will the final product he distributed (packaging)? Bulk. Liquid 2. Please attach a marketability statement detailing destinations and approximate amounts of the final product to be di; bred. 150 -- 200 DT/YR; Bulk. Liquid on area farm land and forest land 3. Please provide either a label which shall be affixed to the bagged processed residual or an information sheet which shall be provi ed to the person who receives the processed residual. The label or information sheet shall contain,at a minimum,the following information: See Attachment a. The name and address of the person who prepared the residual that is sold or given away in a bag or other container for application to the land. b. A statement that application of the residual to the land is prohibited except in accordance with the instructions on the label or information sheet.- c. A statement that the residuals shall not be applied to any site that is flooded, frozea or snow-covered.' • d A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. e. Information on all applicable buffers including a 10 foot buffer between application site and any public or private water supply source (including wells)and any stream,lake,river,or natural drainage way. f. The Annual Whole Residual Application Rate(AWRAR)for the residual that does not cause any of the annual pollutant loading rates to be exceeded(if necessary). • FORM: DORS 06/94 Page 6 of 7 • • Name and Ccmp;e.ic Address of Enp.ineering Firm: N/A • City;: State: Zip: Telephone Number: ( Professional Engineer's Certification: I. . attest that this application for has•been reviewed by me and is accurate and complete to the best of my}mowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals,inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: • Applicant's Certification: Lisa Haynes . attest that this application for DORS Permit • • has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that if all required parts of this application are not completed and that if all required supportinginformation-tid attachments are not included, this application package will be returned to me as yiincomp te. • Signature A/5Carta) Date 3 5 Oa THE COMPLETED APPLICATION PACKAGE. INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHOULD BE SENT TO THE FOLLOWING ADDRESS: • NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY SECTION PERMITS AND ENGINEERING UNIT POST OFFICE BOX 29535 RALEIGH, NORTH CAROLINA 27626-0535 TELEPHONE NUMBER: (919) 733-50S3 • • FORM: DORS 06i94 P.: : 7 of 7 A Process Description for Unifi's Reidsville & Mayodan Manufacturing Facilities Unifi's Reidsville Manufacturing facility texturizes approximately 170,000 pounds of polyester yarn each day. About 100,000 pounds of textured polyester yarn is package dyed daily along with small amounts of textured nylon and cotton blend yarns. Unifi's Mayodan Manufacturing facility package dyes about 100,000 pounds of textured polyester yarn daily. Dyed yarns are rewound onto paper cones for sale. In the texturing process,packages of textured yarn are placed in vessels called dye kierns. Under pressure,heated water and various organic compounds are used to disperse pigments into the yarn. Several dyeing batches may be running at the same time while other kierns are being unloaded or cleaned. Normally, at the Reidsville Plant one million gallons of industrial wastewater is discharged to the pretreatment process daily. The Mayodan Plant normally discharges 700,000 gallons of industrial wastewater to the pretreatment process daily. About 90%of the industrial wastewater is generated by the dyeing process with the balance from air washer, cooling tower, and boiler blowdown. No domestic or sanitary waste is discharged to the pretreatment process. The wastewater pretreatment process at the Reidsville Plant is an activated sludge system consisting of 1-two million gallon equalization basin, a one million gallon aeration basin, a 165,000 gallon final clarifier, and a 500,000 gallon aerobic digester. The clarifier effluent combines with the sanitary wastewater before discharging into the City of Reidsville's collection system. The pretreatment process typically reduces the industrial wastewater BOD5 from 360 to 15 mg/L. The Mayodan Plant pretreatment process is an activated sludge system consisting of a 1.5 million gallon aeration basin and a 250,000 gallon clarifier. A Dissolved Air Floatation treats a segregated wastestream that discharges into the aeration basin for treatment prior to discharge to Town of Mayodan collection system. The clarifier effluent combines with the sanitary wastewater before discharging into the Town of Mayodan's collection system. The process typically reduces the industrial wastewater BOD5 from 285 to 34 mg/L. At the Mayodan Plant, tankers for disposing of waste sludge are loaded from the aeration basin sludge return line. The tanker fill station is diked for spill containment. I estimate that the wasting of 500,00 gallons every 3 months at the Mayodan Plant will be necessary to maintain acceptable process operations. At the Reidsville Plant,waste sludge is loaded from the digester into tankers. The tanker fill station is diked for spill containment. I estimate that the digester sludge will require removal at least every 6 months to maintain acceptable process operations. Sincerely, Wteia.‘liatlinta) Lisa Haynes Environmental Manager Precision Land Application, Inc. Biosolids Analysis Report Project: Unifi, Inc. Plant 2 Sample Date: 1/28/02 %Solids: 1.3 Type of Sample Taken: Grab pH: 7.2 Conversion Table Parameter Mg/Kg X 0.002 = lbs/dry ton Nitrogen TKN 30,615.39 61.23 Ammonia N 3,715.39 7.43 Nitrate N 5453.85 10.9077 Phosphorus 4,738.46 9.48 Ceiling Concentration Mg/Kg Arsenic 0.00 OK 75.00 0.0000 Cadmium 0.00 OK 85.00 0.0000 Chromium 0 Copper 70.31 OK 4300.00 0.1406 Lead 2.54 OK 840.00 0.0051 Mercury 0.00 OK 57.00 0.0000 Molybdenum 0.00 OK 75.00 0.0000 Nickel 3.15 OK 420.00' 0.0063 Selenium 1.62 OK 100.00 0.0032 Zinc 22.92 OK 7500.00 0.0458 Aluminum 360.00 0.7200 Calcium 2,976.92 5.95 Chlorides 0.0000 Iron 0.0000 Magnesium 976.92 1.95 Manganese 51.00 0.1020 Potassium 3,238.46 6.48 Sodium 21,615.39 43.23 Sulfur 0.00 Plant Available Nitrogen (PAN) Mineralization Rate: 0.3 Unstabilized Primary&Secondary Residuals 0.4 Aerobically Digested Residuals 0.3 Anaerobically Digested Residuals 0.2 Composted Residuals 0.1 [(MR x (TKN -AmN))+ (.5 x AmN)+ NO3N] x .002 =lbs. PAN/dry ton Surface 15,381.54 Mg/Kg 30.76 lbs PAN/dry ton [(MR x (TKN -AmN))+AmN + NO3N] x .002 =lbs. PAN /dry ton Injection 17,239.23 Mg/Kg 34.48 lbs PAN/dry ton Page 1 of 1 Precision Land Application, Inc. Biosolids Information Sheet Nutrients Provided at 20,000 Gallons / Acre Project: Unifi, Inc. Plant 2 1.08 Dry tons/Acre pH: 7.2 Sample Date: 1/28/02 lbs./acre Parameter applied Nitrogen(PAN) 33.35 Phosphorus(P) 10.27 Potassium (K) 7.02 Sulfur 0.000 Calcium 6.455 Magnesium 2.118 Copper 0.152 Zinc 0.050 Cadmium 0.000 Nickel 0.007 Lead 0.006 Biosolid Value Unit cost/lb* $Iacre Nitrogen (N) $0.20 $6.57 Phosphate(P) $0.20 $2.02 Potash (K) $0.20 $1.38 Spreading Cost per acre: $5.30 Total value per acre: $15.28 Note: Application of this residual to the land is prohibited except in accordance with instructions on this sheet. Note: State regulations require a minimum of a 10'buffer between the application area and any public or private water supply source, including wells, and any stream, lake, river,or natural dranage way. In addition, residuals shall not be applied to a site when it is flooded,frozen,or snow-covered. Adequate procedures must be provided to prevent surface runoff from carrrying any applied residuals into any surface waters I Page 1 of 1 Precision Land Application, Inc. Biosolids Analysis Report Project: Unifi, Inc. Plant 15 Sample Date: 1/28/02 %Solids: 0.82 Type of Sample Taken: Grab pH: 7.3 Conversion Table Parameter Mg/Kg X 0.002 = lbs/dry ton Nitrogen TKN 43,765.28 87.53 Ammonia N 2,640.59 5.28 Nitrate N 0.00 0.0000 Phosphorus 4,914.43 9.83 Ceiling Concentration Mg/Kg Arsenic 0.00 OK 75.00 0.0000 Cadmium 0.00 OK 85.00 0.0000 Chromium 0 Copper 30.32 OK 4300.00 0.0606 Lead 1.22 OK 840.00 0.0024 Mercury 0.26 OK 57.00 0.0005 Molybdenum 0.00 OK 75.00 0.0000 Nickel 5.62 OK 420.00- 0.0112 Selenium 3.18 OK 100.00 0.0064 Zinc 20.54 OK 7500.00 0.0411 Aluminum 266.50 0.5330 Calcium 5,281.17 10.56 Chlorides 0.0000 Iron 0.0000 Magnesium 1,860.64 3.72 Manganese 51.00 0.1020 Potassium 63.80 0.13 Sodium 51,833.74 103.67 Sulfur 0.00 Plant Available Nitrogen (PAN) Mineralization Rate: 0.3 Unstabilized Primary&Secondary Residuals 0.4 Aerobically Digested Residuals 0.3 Anaerobically Digested Residuals 0.2 Composted Residuals 0.1 [(MR x(TKN -AmN))+(.5 x AmN)+ NO3N] x .002 =lbs. PAN/dry ton Surface 13,657.70 Mg/Kg 27.32 lbs PAN/dry ton [(MR x(TKN -AmN))+AmN + NO3N] x .002 =lbs. PAN /dry ton Injection 14,978.00 Mg/Kg 29.96 lbs PAN/dry ton Page 1 of 1 Precision Land Application, Inc. Biosolids Information Sheet Nutrients Provided at 20,000 Gallons /Acre Project: Unifi, Inc. Plant 15 0.68 Dry tons/Acre pH: 7.3 Sample Date: 1/28/02 lbs.I acre Parameter applied Nitrogen (PAN) 18.68 Phosphorus(P) 6.72 Potassium (K) 0.09 Sulfur 0.000 Calcium 7.223 Magnesium 2.545 Copper 0.041 Zinc 0.028 Cadmium 0.000 Nickel 0.008 Lead 0.002 Biosolid Value Unit cost/lb* $/acre Nitrogen (N) $0.20 $3.68 Phosphate (P) $0.20 $1.32 Potash (K) $0.20 $0.02 Spreading Cost per acre: $5.30 Total value per acre: $10.32 Note: Application of this residual to the land is prohibited except in accordance with instructions on this sheet. Note: State regulations require a minimum of a 10'buffer between the application area and any public or private water supply source, including wells,and any stream, lake, river,or natural dranage way. In addition, residuals shall not be applied to a site when it is flooded,frozen, or snow-covered. Adequate procedures must be provided to prevent surface runoff from carrrying any applied residuals into any surface waters Page 1 of 1 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES RALEIGH PERMIT FOR THE DISTRIBUTION OF RESIDUALS In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Re ns RECEIVED IVATER QUALITY SECTION PERMISSION IS HEREBY GRANTED T Unifi, Incorporated • • MAR 2 5 2002 Rockingham County NON-DISCHARGE PERMITTING FOR THE operation of a facility for the distribution of residuals of exceptional quality consisting of the distribution of 200 dry tons per year of residuals from the sources listed in Condition II 2, with no discharge of wastes to the surface waters, pursuant to the application received on January 30, 1997, and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department • of Environment, Health and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until March 31, 2002, shall void Permit No. WQ0006594 issued June 28, 1993, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS 1. The distribution residuals program shall be effectively maintained and operated as a non- discharge system to prevent the discharge of any wastes resulting from the operation of this program. • 2. This permit shall become voidable in the event of failure of the residuals program to adequately protect the assigned water quality standards of the surface waters and groundwaters. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. 4. In the event that the residuals program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall take any immediate corrective actions as may be required by the Division. 5. Diversion or bypassing.of the untreated residuals or leachate from the residual treatment facilities is prohibited. 6. All leachate must be reused as a wetting agent for the processing of residuals or routed to the head of the treatment plant. l I • II. OPERATION AND MAINTENANCE REQUIREMENTS l . The residuals treatment facilities shall be properly maintained and operated at all times. 2. No residuals other than the following are hereby approved for distribution in accordance with this permit: Volume olume Source County Number (Dry Tons/Year) Unifi, Inc., Plant No. 2 Rockingham City of Reidsville 100 Reidsville Unifi, Inc. Plant No. 15 Rockingham Town of MayodanP 100 Mayodan WWT Total 200 3. All residuals shall be adequately stored to prevent leachate•runoff until'treated. The ' finished product may be placed on a concrete pad, placed under shelter or covered until such time as it is distributed to the buyer: If an alternate storage site is to be used, approval must be obtained from the Division of Water Quality. 4. No other residuals other than those specified under Condition II 2 above may be distributed. The Permittee shall request and obtain a permit amendment from the Division of Water Quality for each additional residual source prior to acceptance of that residual. 5. For a wastewater residual of exceptional quality to be sold or given away in bags or other container for application to the land, the following must be satisfied: The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly Average Concentrations (Dry Weight Basis) must be maintained: Ceiling Monthly Average Concentrations Concentrations Parameters mg/kg mg/kg Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Nickel 420 420 • Zinc 7,500 2,800 6. Upon classification of the facility by the Certification Commission, the Permittee shall employ a certified residuals operator to be in responsible charge (ORC) of the residuals program. The operator must hold a certificate of the type classification assigned to the • residuals program by the Certification Commission. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of Title . 15A NCAC 8A, .0202. • 7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants.from the residuals treatment area onto the adjacent property or into any surface waters. 2 8. A label shall be affixed to the bag or other container in which residuals that are sold or given away for application to the land, or an information sheet shall be provided to the person who receives the residuals sold or given away in an other container for application to the land. The label or information sheet shall contain the following information: a. The name and address of the person who prepared the residuals that is sold or given away in a bag or other container for application to the land. b. A statement that application of the residuals to the land is prohibited except in accordance with the instructions on the label or information sheet. c. Information on all applicable buffers including a 10 foot buffer between application site and any public or private water supply source (including wells) and any stream, lake, or river. d. Residuals-shall not be applied to any site that is flooded, frozen or snow-covered. e Adequate procedures shall be provided to prevent surface runoff from carrying any di:.po;.ed or stored residuals irito any surface waters. III. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division of Water Quality to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee tracking all residual activities. These records shall include,but are not necessarily limited to the following information: a. source, volume and analysis of each residuals b. name of residuals'recipient, volume received,and intended use 3. A residual analysis shall be conducted annually from the date of permit issuance by the Permittee. The results of all analysis shall be maintained on file by the Permittee for a minimum of five years.The residuals analysis shall include the following parameters: Cadmium Nickel Copper Lead Zinc Aluminum pH • • - Ammonia-Nitrogen Phosphorus Calcium . Plant Available Nitrogen (by calculation) Magnesium Potassium Nitrate-Nitrite Nitrogen Sodium Total Solids TKN • 3 4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually. The TCLP analysis shall include the following parameters (please note the regulatory level in mg/L in parentheses): Arsenic (5.0) Barium (100.0') Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) o-Cresol (200.0) m-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5) 1,1-Dichloroethylene (0.7) 2,4-Dinitrotoluene (0.13) Endrin (0.02) Heptachlor(and its hydroxide) (0.008) Hexachlorobenzene (0.13) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxynhlnr.(111D) Methyl ethyl ketone(200 D) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) .Selenium (1.0) • Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorop1enol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) 5. Three copies of all required monitoring and reporting requirements as specified in conditions III 1, III 2, III 3, and III 4 shall be submitted annually on or before March 1 of the following year to the following address: NC Division of Water Quality Water Quality Section Facility Assessment Unit PO Box 29535 Raleigh, NC 27626-0535 6. Noncompliance Notification: The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number 910/ 771-4600 as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the distribution program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to receiving waters. c. Any time that self-monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed. . d. Any.process unit failure, due to known or unknown reasons, that render the facility incapable of-adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system during transportation of residuals. Persons reporting such occurrences by telephone also Tale=a-written report in letter form v ithin ve (5).aays-following first know1e3ge oT•the occur-Terme. This report must outline the actions taken or_proposed to'be taken to ensure that the_prdblem does not recur. -4 IV. GROUNDWATER REOUIREMENTS 1 . The C MP IA BOUNDARY for the disposal system is specified by regulations in 15A NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary is for the disposal system constructed after December 31, 1983 is established at ewhichever50 feet from the waste disposal area, or (2) 50 feet within of Groundwater Quality boundary,tandards at or is closest to the waste disposal area. An exceedance beyond the Compliance Boundary is subject to immediate remediation action in addition to the penalty provisions applicable under General Statute 143-215.6A(a)(1). In accordance with 15A NCAC 2L, a REVIEW BOUNDARY is established around the disposal systems midway between the Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards at the Review Boundary shall require remediation action on the part of the permittee. 2. Any groundwater quality monitoring, as deemed necessary-by the Division, shall-be • provided. V. INSPECTIONS transport., and treatment 1. The Permittee or his designee shall inspect the residuals storage, trans p facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health,or he a nuisance. The Permittee shall maintain an inspection log or summaryincluding date and time of inspection, observations made, and any maintenance, repairs,or corrective actions taken by the Permittee. This log of inspections-shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division of Water Quality or other permitting authority,upon request. 2. Any duly authorized officer, employee, or representative of the Division of Water place Quality may, upon presentation of credentials, enter and inspect any property, p of or related to the treatment site or facility at any reasonable time for the purpose determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater, surface water, or leachate. VI. GENERAL CONDITIONS 1. This permit shall become voidable unless t the supporting distribution materials, and in the manner ut in accordance with the conditions of this permit, approved by this Division. 2. This permit is effective only with respect to the nature and volume of residuals described in the application and other supporting data. here is a sire for the 3. This permit is not automatically transferable. change of the Permittee,ta formal peernut request facilities to change ownership or a nameg application on fee,t must be submitted to the Division of Water Quality accompanied byan a P documentation from the parties involved, ther ns considorting materials ered itsmerits and may or may as may be appropriate. The approval of this request will be o not be approved. 4. Failure to abideby the conditions and limitations contained in this permit may subject the Permittee.toan‘enforcement action by the Division of Water Quality in accordance with North Carolina General Statute 143-215.6(a)ro 143-2T5.6(c). 3 I 5. The annual administering and compliance fee must be p,..d by the Permittee within thirty (30) days after being billed by the Division. Failure to pay b accordinglye fee I S NC 2mH .0205 cause the Division to initiate action to revoke this permit as specifiedY (c)(4). 6. The issuance of this permit does not preclude the Permitteebe imposed complying l ingrgovernmentya all statutes, rules, regulations, or ordinances which may P Y agencies (local, state, and federal) which have jurisdiction. 7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit may be modified, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the and Division sio of �.Water Quality deems necessary in Drdertomdequately protect theenvironment Permit issued this the 22nd day of April, 1997 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION • A. reston Howard,.Jr., P.E., Director vision of Water Quality By Authority of the Environmental Management Commission Permit Number WQ0006594 • • • • • lestAim rica ___._�. __ _ e RECEIVED INCORPORATED WATEROUALITYSECTION VAR 2 5 2002 NON-DISCHARGE PERMITTING ANALYTICAL REPORT PLA 9471 Lab Number: 02-A13413 CHRIS ALEXANDER Sample ID: UN-2 4022 WHITE PLAINS ROAD Sample Type: Water ROARING RIVER, NC 28669 Site ID: Date Collected: 1/28/02 Project : Time Collected: 14:37 Project Name: Date Received: 1/29/02 Sampler: JAMES ALEXANDER Time Received: 9 :00 Page: 1 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *METALS* Mercury ND mg/1 0.00200 0.00020 1 1/31/02 9:43 C. Martin 7470 6139 Aluminum 4.68 mg/1 0.050 0.050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Arsenic ND mg/1 0.0050 0.0050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Cadmium ND mg/1 0.0010 0.0010 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Calcium, total 38.70 mg/1 1.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Copper 0.9140 mg/1 0.0100 0.0100 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Lead 0.0330 mg/1 0.0030 0.0030 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Magnesium 12.70 mg/1 1.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Molybdenum ND mg/1 0.0500 0.0500 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Nickel 0.0410 mg/1 0.0100 0.0100 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Potassium 42.10 mg/1 1.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Selenium 0.0210 mg/1 0.0050 0.0050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Sodium, total 281. mg/1 10.0 1.00 10 2/ 1/02 15:07 Rob Hunt 200.7 6912 Zinc 0.2980 mg/1 0.0200 0.0200 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 *MISCELLANEOUS CHEMISTRY* pH 7.20 pH Units 1 2/ 4/02 15:40 B. Powell 9040/150.1 6304 Nitrate-N as N 70.9 mg/1 1.00 0.100 10 1/29/02 22:16 A.Bamarni 353.2 6016 Nitrite-N as N ND mg/1 0.100 0.100 1 1/29/02 23:11 A.Bamarni 353.2 6012 Phosphorus 61.6 mg/1 0.100 0.100 1 1/30/02 20:00 S. Prayter 365.4 6706 Ammonia Nitrogen as N 48.3 mg/1 1.00 0.100 10 2/ 1/02 11:00 S. Prayter 350.1M 7323 Solids, total 13000 mg/1 20.0 20.0 1 1/30/02 20:00 D. Hessin SM2540G 6568 Sample report continued . . . 2960 FOSTER CREIGIITON DRIVE / NASIIVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13413 Sample ID: UN-2 Project : Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch Kjeldahl Nitrogen as N 398. mg/1 0.100 0.100 1 1/30/02 20:00 S. Prayter 351.2 6707 LABORATORY COMMENTS: ND - Not detected at the report limit. # - Recovery outside Laboratory historical or method prescribed limits. M - Method 350.1 modified for manual distillation with Lachat procedure. End of Sample Report. 2960 FOSTER CREI GHTON DRIVE / NAsIIVILLE,TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 TestA merica INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 02-A13411 CHRIS ALEXANDER Sample ID: UN-2 4022 WHITE PLAINS ROAD Sample Type: Sludge ROARING RIVER, NC 28669 Site ID: Date Collected: 1/28/02 Project : Time Collected: 14 :37 Project Name: Date Received: 1/29/02 Sampler: JAMES ALEXANDER Time Received: 9 :00 Page: 1 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch • TCLP Pesticide LCS for sample batch 274 outside QC limits. Samples were re-extracted outside of holding time with all LCS recoveries within QC limits. All samples confirmed on re-extraction and original data was reported. TCLP Herbicide LCS for sample batch 9904 outside QC limits. Samples were re-extracted outside of holding time with all LCS recoveries within QC limits. All samples confirmed on re-extraction and original data was reported. TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (%) Date Method Arsenic < 0.100 mg/1 5.0 104 2/ 1/02 6010E Barium < 1.00 mg/1 100 88 2/ 1/02 6010B Cadmium 0.100 mg/1 1.0 96 2/ 1/02 6010B Chromium < 0.500 mg/1 5.0 91 2/ 1/02 6010B Lead < 0.5000 mg/1 5.0 93 2/ 1/02 6010B Mercury < 0.0100 mg/1 0.2 105 2/ 2/02 7470A Selenium < 0.100 mg/1 1.0 109 2/ 1/02 6010B Silver < 0.100 mg/1 5.0 93 2/ 1/02 6010B Benzene < 0.0200 mg/1 0.5 102 2/ 1/02 8260 Carbon tetrachloride < 0.0200 mg/1 0.5 111 2/ 1/02 8260 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NAsm ILI,E,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 l es t merica INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13411 Sample ID: UN-2 Project : Page 2 TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (%) Date Method Chlorobenzene < 0.0200 mg/1 100 96 2/ 1/02 8260 Chloroform < 0.0200 mg/1 6.0 127 2/ 1/02 8260 1,2-Dichloroethane < 0.0200 mg/1 0.5 96 2/ 1/02 8260 1,1-Dichloroethene < 0.0200 mg/1 0.7 100 2/ 1/02 8260 Methylethylketone 0.270 mg/1 200 129 2/ 1/02 8260 Tetrachloroethene < 0.0200 mg/1 0.7 106 2/ 1/02 8260 Trichloroethene < 0.0200 mg/1 0.5 100 2/ 1102 8260 Vinyl Chloride < 0.0200 mg/1 0.2 101 2/ 1/02 8260 Cresols < 0.0100 mg/1 200 66 2/ 4/02 8270 1,4-Dichlorobenzene < 0.0100 mg/1 7.5 70 2/ 4/02 8270 2,4-Dinitrotoluene < 0.0100 mg/1 0.13 80 2/ 4/02 8270 Hexachlorobenzene < 0.0100 - mg/1 0.13 50 2/ 4/02 8270 Hexchlor-1,3-butadien < 0.0100 mg/1 0.5 68 2/ 4/02 8270 Hexachloroethane < 0.0100 mg/1 3.0 68 2/ 4/02 8270 Nitrobenzene < 0.0100 mg/1 2.0 82 2/ 4/02 8270 Pentachlorophenol < 0.0100 mg/1 100 90 2/ 4/02 8270 Pyridine < 0.0100 mg/1 5.0 28 2/ 4/02 8270 2,4,5-Trichlorophenol < 0.0100 mg/1 400 92 2/ 4/02 8270 2,4,6-Trichlorophenol < 0.0100 mg/1 2.0 92 2/ 4/02 8270 Chlordane < 0.00050 mg/1 0.030 92 2/ 6/02 8081A 2,4-0 < 0.100 mg/1 10.0 156 2/ 5/02 8151A Endrin < 0.00050 mg/1 0.02 94 2/ 6/02 8081A Heptachlor < 0.00050 mg/1 0.008 78 2/ 6/02 8081A Lindane < 0.00050 mg/1 0.4 104 2/ 6/02 8081A Methoxychlor < 0.00050 mg/1 10.0 71 2/ 6/02 8081A Toxaphene < 0.010 mg/1 0.50 58 2/ 6/02 8081A Silvex < 0.0100 mg/1 1.0 120 2/ 5/02 8151A Heptachlor epoxide < 0.00050 mg/1 0.008 106 2/ 6/02 8081A TCLP Extraction Initiated 1/31/02 1311 Zero Headspace Extraction Initiated 1/31/02 1311 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NAsIIvILI,E,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 • • 'festA imer ca INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13411 Sample ID: UN-2 Project : Page 3 Sample Extraction Data Wt/Vol Parameter Extracted Extract Vol Date Time Analyst Method TCLP Herbicides 5.0 ml 5.00 ml 2/ 2/02 D. Harris 3510 TCLP Pesticides 100. ml 10.0 ml 2/ 4/02 D. Harris 3510 TCLP BNA's 500. ml 1.0 ml 2/ 1/02 D.Yeager 3510 Surrogate % Recovery Target Range VOA Surr 1,2-DCA-d4 99. 60. - 158. VOA Surr Toluene-d8 98. 82. - 127. VOA Surr, 4-BFB 108. 72. - 136. BNA Surr-Nitrobenzene-d5 86. 24. - 128. BNA Surr-2-Fluorobiphenyl 84. 33. - 118. BNA Surr-Terphenyl-d14 82. 27. - 142. BNA Surr-Phenol-d5 64. 1. - 72. BNA Surr-2-Fluorophenol 74. 1. - 99. BNA Surr-2,4,6-Tribromophenol 112. 45. - 157. pest surr-TCMX 46. I 53. - 125. surr-Dibutylchlorendate 28. 10. - 117. surr-DCAA 108. 24. - 173. LABORATORY COMMENTS: ND - Not detected at the report limit. 8 - Recovery outside Laboratory historical or method prescribed limits. All results reported on a wet weight basis. End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NAs11vIiLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 U3/21/02 U4: 40 PM lestAmerica, Inc. TestAmerica, Inc. Page 2 of 4 #838388= TEST AMERICA INC ANAYLTICAL REPORT 2960 Foster Creighton Drive Nashville, Tennessee 37204 ** Original report and a copy of the chain of custody will follow by mail . PLA 9471 CHRIS ALEXANDER 4022 WHITE PLAINS ROAD Lab Number: 02-A42739 ROARING RIVER, NC 28669 Sample ID: UN2-1 Date Collected: 3/15/02 Project : PLANT 2 & 15 Time Collected: 11 :57 Project Name: UNIFI, INC Date Received: 3/18/02 Sampler: JAMES ALEXANDER Time Received: 9 : 00 State Certification: 387 Sample. Type : Liquid waste Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* Reactive Cyanide ND mg/kg 50.0 50.0 1 3/20/02 15:15 S. Prayter SW-846 1547 Reactive Sulfide ND mg/kg 100. 100. 1 3/20/02 15:15 S. Prayter SW-846 1547 Ignitability not ignitable up to 200f 3/19/02 17:30 R. Coleman l01CM 2345 Corrosivity Not Corrosive 3/21/02 8:53 T. Beverly 1110 3044 LABORATORY COMMENTS: ND - Not detected at the report limit. / - Recovery outside Laboratory historical or method prescribed limits. Flash point/ignitability reported to the nearest 10 deg F. All results reported on a uet weight basis. festAmerica INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 02-A13412 CHRIS ALEXANDER Sample ID: UN-15 4022 WHITE PLAINS ROAD Sample Type: Water ROARING RIVER, NC 28669 Site ID: Date Collected: 1/28/02 Project : Time Collected: 11 :30 Project Name: Date Received: 1/29/02 Sampler: JAMES ALEXANDER Time Received: 9:00 Page: 1 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method . Batch *METALS* - Mercury 0.00210 mg/1 0.00200 0.00020 1 1/31/02 9:43 C. Martin 7470 6139 Aluminum 2.18 mg/1 0.100 0.050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Arsenic ND mg/1 0.0100 0.0050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Cadmium ND mg/1 0.0020 0.0010 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Calcium, total 43.20 mg/1 2.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Copper 0.2480 mg/1 0.0200 0.0100 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Lead 0.0100 mg/1 0.0060 0.0030 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Magnesium 15.22 mg/1 2.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Molybdenum ND mg/1 0.100 0.0500 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Nickel 0.0460 mg/1 0.0200 0.0100 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Potassium 63.80 mg/1 2.000 1.000 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Selenium 0.0260 mg/1 0.0100 0.0050 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 Sodium, total 424. mg/1 20.0 1.00 10 2/ 1/02 15:07 Rob Hunt 200.7 6912 Zinc 0.1680 mg/1 0.0400 0.0200 1 2/ 1/02 15:07 Rob Hunt 200.7 6912 *MISCELLANEOUS CHEMISTRY* pH 7.30 pH Units. 1 2/ 4/02 15:35 B. Powell 9040/150.1 6304 Nitrate-N as N ND mg/1 0.100 0.100 1 1/29/02 22:09 A.Bamarni 353.2 6016 Nitrite-N as N ND mg/1 0.100 0.100 1 1/29/02 23:13 A.Bamarni 353.2 6012 Phosphorus 40.2 mg/1 0.100 0.100 1 1/30/02 20:00 S. Prayter 365.4 6706 Ammonia Nitrogen as N 21.6 mg/1 0.200 0.100 2 2/ 1/02 11:00 S. Prayter 350.1M 7323 Solids, total 8180 mg/1 20.0 20.0 1 1/29/02 18:25 D. Hessin SM2540G 5825 Sample report continued . . . 2960 FOSTER CREIGIITON DRIVE / NASIIVILLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13412 Sample ID: UN-15 Project : Page 2 Report Quan Dil Analysis Analysis Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch Kjeldahl Nitrogen as N 358. mg/1 0.100 0.100 1 1/30/02 20:00 S. Prayter 351.2 6707 LABORATORY COMMENTS: ND - Not detected at the report limit. # - Recovery outside Laboratory historical or method prescribed limits. M - Method 350.1 modified for manual distillation with Lachat procedure. End of Sample Report. 2960 FOSTER CREIGIrroN DRIVE / N.AsiiviLLE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 rica I . . • lest me IINCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 02-A13410 CHRIS ALEXANDER Sample ID: UN-15 4022 WHITE PLAINS ROAD Sample Type: Sludge ROARING RIVER, NC 28669 Site ID: Date Collected: 1/28/02 Project : Time Collected: 11 :30 Project Name: Date Received: 1/29/02 Sampler: JAMES ALEXANDER Time Received: 9:00 Page: 1 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch TCLP Pesticide LCS for sample batch 274 outside QC limits. Samples were re-extracted outside of holding time with all LCS recoveries within QC limits. All samples confirmed on re-extraction and original data was reported. TCLP Herbicide LCS for sample batch 9904 outside QC limits. Samples were re-extracted outside of holding time with all LCS recoveries within QC limits. All samples confirmed on re-extraction and original data was reported. TCLP Results Matrix Spike IAnalyte Result Units Reg Limit Recovery (%) Date Method Arsenic < 0.100 mg/1 5.0 104 2/ 1/02 6010B Barium < 1.00 mg/1 100 88 2/ 1/02 6010B Cadmium < 0.100 mg/1 1.0 96 2/ 1/02 6010B Chromium < 0.500 mg/1 5.0 91 2/ 1/02 6010B Lead 0.5000 mg/1 5.0 93 2/ 1/02 6010B Mercury < 0.0100 mg/1 0.2 105 2/ 2/02 7470A Selenium < 0.100 mg/1 1.0 109 2/ 1/02 6010B Silver < 0.100 mg/1 5.0 93 2/ 1/02 6010B Benzene < 0.0200 mg/1 0.5 102 2/ 1/02 8260 Carbon tetrachloride < 0.0200 mg/1 0.5 111 2/ 1/02 8260 Sample report continued . . . 2960 FOSTER CREIGHTON DRIVE / NASHVILI,E,TN 37204 / 615-726-0177 / FAN: 615-726-0954 / 800-765-0980 L ri lest me ca INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13410 Sample ID: UN-15 Project : Page 2 TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (%) Date Method Chlorobenzene < 0.0200 mg/1 100 96 2/ 1/02 8260 Chloroform < 0.0200 mg/1 6.0 127 2/ 1/02 8260 1,2-Dichloroethane < 0.0200 mg/1 0.5 96 2/ 1/02 8260 1,1-Dichloroethene < 0.0200 mg/1 0.7 100 2/ 1/02 8260 Methylethylketone 0.470 mg/1 200 129 2/ 1/02 8260 Tetrachloroethene < 0.0200 mg/1 0.7 106 2/ 1/02 8260 Trichloroethene < 0.0200 mg/1 0.5 100 2/ 1102 8260 Vinyl Chloride < 0.0200 mg/1 0.2 101 2/ 1/02 8260 Cresols < 0.0100 mg/1 200 65 2/ 4/02 8270 1,4-Dichlorobenzene < 0.0100 mg/1 7.5 56 2/ 4/02 8270 2,4-Dinitrotoluene < 0.0100 mg/1 0.13 82 2/ 4/02 8270 Hexachlorobenzene < 0.0100 - mg/1 0.13 46 2/ 4/02 8270 Hexchlor-1,3-butadien < 0.0100 mg/1 0.5 54 2/ 4/02 8270 Hexachloroethane < 0.0100 mg/1 3.0 54 2/ 4/02 8270 Nitrobenzene < 0.0100 mg/1 2.0 68 2/ 4/02 8270 Pentachlorophenol < 0.0100 mg/1 100 92 2/ 4/02 8270 Pyridine < 0.0100 mg/1 5.0 34 2/ 4/02 8270 2,4,5-Trichlorophenol < 0.0100 mg/1 400 92 2/ 4/02 8270 2,4,6-Trichlorophenol < 0.0100 mg/1 2.0 88 2/ 4/02 8270 Chlordane < 0.00050 mg/1 0.030 92 2/ 6/02 8081A 2,4-D 0.350 mg/1 10.0 156 2/ 5/02 8151A Endrin < 0.00050 mg/1 0.02 94 2/ 6/02 8081A Heptachlor < 0.00050 mg/1 0.008 78 2/ 6/02 8081A Lindane < 0.00050 mg/1 0.4 104 2/ 6/02 8081A Methoxychlor < 0.00050 mg/1 10.0 71 2/ 6/02 8081A Toxaphene < 0.010 mg/1 0.50 58 2/ 6/02 8081A Siivex < 0.0100 mg/1 1.0 120 2/ 5/02 8151A Heptachlor epoxide < 0.00050 mg/1 0.008 106 2/ 6/02 8081A TCLP Extraction Initiated 1/31/02 1311 Zero Headspace Extraction Initiated 1/31/02 1311 Sample report continued . . . 2960 FOSTER CREI(GHTON DRIVE / Nnsnvn.1,E,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica INCORPORATED ANALYTICAL REPORT Laboratory Number: 02-A13410 Sample ID: UN-15 Project : Page 3 Sample Extraction Data Wt/Vol Parameter Extracted Extract Vol Date Time Analyst Method TCLP Herbicides 5.0 ml 5.00 ml 2/ 2/02 D. Harris 3510 TCLP Pesticides 100. ml 10.0 ml 2/ 4/02 D. Harris 3510 TCLP BNA's 500. ml 1.0 ml 2/ 1/02 D.Yeager 3510 Surrogate % Recovery Target Range • VOA Surr 1,2-DCA-d4 96. 60. - 158. VOA Surr Toluene-d8 98. 82. - 127. VOA Surr, 4-BFB 109. 72. - 136. BNA Surr-Nitrobenzene-d5 84. 24. - 128. BNA Surr-2-Fluorobiphenyl 82. 33. - 118. BNA Surr-Terphenyl-d14 64. 27. - 142. BNA Surr-Phenol-d5 52. 1. - 72. BNA Surr-2-Fluorophenol 56. 1. - 99. BNA Surr-2,4,6-Tribromophenol 110. 45. - 157. pest surr-TCMX 32. # 53. - 125. surr-Dibutylchlorendate 34. 10. - 117. surr-DCAA 108. 24. - 173. LABORATORY COMMENTS: ND - Not detected at the report limit. # - Recovery outside Laboratory historical or method prescribed limits. All results reported on a wet weight basis. End of Sample Report. 2960 FOSTER CREIGHTON DRIVE / NAsnvH.i.E,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 03/22/02 04: 40 PH TestAmerica, Inc. TestAmerica, Inc. Page 3 of 4 #838380= TEST AMERICA INC ANAYLTICAL REPORT 2960 Foster Creighton Drive Nashville, Tennessee 37204 ** Original report and a copy of the chain of custody will follow by mail. PLA 9471 CHRIS ALEXANDER 4022 WHITE PLAINS ROAD Lab Number: 02-A42740 ROARING RIVER, NC 28669 Sample ID: UN15-1 Date Collected: 3/15/02 Project: PLANT 2 & 15 Time Collected: 11:20 Project Name: UNIFI,INC Date Received: 3/18/02 Sampler: JAMES ALEXANDER Time Received: 9:00 State Certification: 387 Sample Type: Liquid waste Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* Reactive Cyanide ND mg/kg 50.0 50.0 1 3/20/02 15:15 S. Prayter SW-846 1547 Reactive Sulfide ND mg/kg 100. 100. 1 3/20/02 15:15 S. Prayter SW-846 1547 Ignitability not ignitable up to 200f 3/19/02 17:30 R. Coleman 1010M 2345 Corrosivity Not Corrosive 3/21/02 8:53 T. Beverly 1110 3044 LABORATORY COMMENTS: ND - Not detected at the report limit. / - Recovery outside Laboratory historical or method prescribed limits. Flash point/ignitability reported to the nearest 10 deg F. All results reported on a wet weight basis. — CHAIN OF CUSTODY RECORD PCB krnerica Nashville Division Phone: 615-726-0177 To assist ups in usingthe ro''' Testi 2960 Foster Creighton Toll Free: 800-765-0980 proper analytical t.; "' Nashville,TN 37204 regulator is this work being conducted for Fax: 615-726-34rJ4 regulatory purposes? Client Name/Account 0: P(-19 C1(-11 1 r ^� Address: y 02Z Compliance Monitoring? No (,vHlTrc eL ' -') iO nJ Enforcement Action? Yes 0 City1StateiZIp: >Za�ti,_� v-` N c n � Project Manager: � � � ` o)�'(c(� 1 Report To: • T ger /�mES }aL fs,, oF_ Invoice To: Telephone Number: (33(..%) 95-1-ksn FaxNo.: (33C,) ',Si- ”'"1(, — = TA Quote X: Sampler Name:(Print) ,'• .r•4 S C. �#t..�E` Pro'ecilD: Sampler Signature: p 1 n = / ,0^P Project ii: z Preservative Matrix Anal.2e For J limim3 .tc) C. — co N B TAo4, miS1 : o r J t tQ a m m `o a v a 1 a H 3 3 - Sam ID/Desert Liono I z 6 = z = z z -ES a R = O / gc93otnv38 � c � v, 1;•`s I S- 1 13410 1341Z i-rr-a� 11:3o f V ✓ �'Dow"- -... N • • N.: Ut3-/>- Z. I• i�:3o 1 ✓ a r • U''J i S-- 3 J i13c o ✓ • > • e a 0••4 2 - 1 l 3411 1341' 1-zs-4-1y:37 1 V ✓ . ^ A U++ 2 -Z !rl Yv Z 3 l4'sry I a � ul UN 2- , /41.31 1 a 111111111111111111 Special instructions: o �� Z� �� C� /�•rti•:tE r T ' ' `' Mcj , �, �J�. ��-! I / 14si.Cc ) C 6, Di. 1-15, Mc)IJi Labe 5 S E�,as{ {ti« LP story Comments: Rail - ;S by Method of Sh(• ant: FEDD( Temperature Upon Receipt 3 f' ime a ' / Date Time Received Oats 1 1/OCs Free of Headspaoe? y N nqufshed try _allillt_c_c:, /-e. - Li Z. /,5"•'&io f26 n • Date • . Received by TestArne : • Date Time , • 112c11c` t1-a. P State of North Carolinap r iv FA Department of Environment Alf • and Natural Resources Division of Water Quality Michael F. Easley, Governor NCDENR William G. Ross Jr.,Secretary Gregory J. Thorpe,Ph.D.,Acting Director NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES January 28, 2002 E TIMOTHY COLS ` UNIFI,Inc. \2 Dept. • . E PO Box 698 Yadkinville,NC 27055 t" ' `�{ � '� Subject: Annual Monitoring and Reporting Requirements Treatment,Distribution and Marketing of Residual. ,z Permit Number: WQ0006594 UNIFI,Inc. Rockingham County Dear TIMOTHY COLE, The purpose of this letter is a reminder that the monitoring reports required by the subject permit must be submitted as an Annual Report for calendar year 2001 by no later than March 1, 2002. The report must be submitted(in triplicate)to the following address: DENR/DWQ/Water Quality Section Non-Discharge Compliance Unit 1617 Mail Service Center Raleigh,N.C. 27699-1617 Due to limitations in storage space, please submit the reports in bound form rather than in notebook form. Permittees are subject to civil penalty for failing to submit the Annual Report as required by their permit. Enclosed are the summary and certification sheets that must be used for your annual report depending on whether your residual is Class A or Class B.Please complete the necessary sheets and if necessary make copies of the blank forms if extras are needed. The information on these forms has not changed since last year (although minor aesthetic changes have been made)so you may use those you already have on hand. You will however note that the forms include additional information required by EPA as outlined in 40 CFR Part 503. Since the requirements of 40 CFR Part 503 are self implementing, they are legally binding and enforceable Federal requirements for all persons subject to the requirements of 40 CFR Part 503,even if these requirements are not currently contained in the State permit.The annual reports for the EPA must be received by EPA at the following address on or before Febuary 19, 2002. Hector Danois Clean Water Act Enforcement Section Water Programs Enforcement Branch Water Management Division U.S. EPA Region 4 61 Forsyth Street,S.W. Atlanta, Ga. 30303-3104 1617 Mail Service Center,Raleigh,North Carolina 27699-1617 Telephone 919-733-5083 Fax 919-733-0059 An Equal Opportunity Affirmative Action Employer 50%recycled/10%post-consumer paper Annual Monitoring and Reporting Requirements Page 2 If there is a need for any information or clarification on the State reporting requirements,please do not hesitate to contact me at (919) 733-5083 extension 581. For further information on the Federal requirements, you should call Madolyn Dominy of the Environmental Protection Agency at 404-562-9305. ely, 14/f/fid. •.''� Wit, Environmental Specialist I cc: Vince Miller,EPA Region IV WSRO Regional Supervisor Non-Discharge Compliance/Enforcement File Central Files ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM RECEIVED FACILITY NAME Unifi, Inc.(Plants 2&15) PERMIT# WQ0006594 COUNTY Rockingham N.C. ritpt.of ENR FACILITY TYPE(please check one): r Surface Disposal(complete Part A(Source(s)and"Residual IN"Volume only)and Part C F C b 0 4 2002 F Distribution and Marketing(complete Parts A,B,and C) sit ..,.-• „„ r (Ofn /�c 3 • Y+;O ia4; �vs 1'7I14c WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? F YES r NO. If NO,skip Parts A,B,and C and certify form below.^J PART A* PART B* Source(s) Volume(dry tons) Recipient Information Month (includes NPDES#if applicable) Amendment/Bulking Name(s) Volume Intended use(s) agent IN Residual IN Product OUT dry tons January Unifi,Inc. Plants 2&15 N/A 16.33 16.33 See Attachments Fertilize February 5.18 5.18 Fertilize March 0 0 Fertilize April If 90 32.03 32.03 90 Fertilize May 0 0 Fertilize June 14.33 14.33 Fertilize July 22.82 22.82 Fertilize AugustII 00 14.5 14.5 Fertilize September 0 0 " Fertilize October 23.06 23.06 Fertilize November 14.5 14.5 Fertilize December 0 0 Fertilize Totals: Annual(dry tons) 142.75 MMIIIIIIIII9.a Amendments)used: N/A Bulking Agent(s)used: N/A *If more space is required than given,please use the comment space provided below or attach additional sheet(s). F Check box if additional sheet(s)are attached. Comments 0 PART C , a Facility was compliant during calendar year 2001 with all conditions of the permit(including but not limited to items 1-3 below)issued by the in' :1 ,,.tl„ vs Division of Water Quality F YES NO. If NO,please provide a written description why the facility was not compliant. -3 G. m 1. All monitoring was performed in accordance with the permit and reported during the year as required and three(3)copies of the certified laboratory results are attached. m D 2::. 0 2. All operations and maintenance requirements were complied with or,in the case of a deviation,prior authorization was received from the Division of Water Quality. g) r Csv m 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. --- . g en v 1< "I CERTIFY UNDER PENALTY OF LAW,THAT THE ABOVE INFORMATION IS,TO THE BEST OF MY KNOWLEDGE AND BELIEF,TRUE,ACCURATE AND g v m = COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION,INCLUDING THE POSSIBILITY OF FINES O 0 AND IMPRISONMENT FOR KNOWING VIOLATIONS." =Z 4sa'Alaidintoi ilagloa, e. /—...7r-- d z_ SIGNATURE OF PERMITTEE DATE S N RE OF PREPARE DATE (f • erent from Permittee) *Preparer is defined in 40 CFR Part 503.9(r) PLIk Precision Land Application, Inc. Operations Report i/1/01 to 12/31/01 Unifi,Inc. Plant 2 (Reidsville,NC) Site No. Farmer Date Weather Method Crop Gallons/Yards Dry Tons GDU9-1 Isley Jan 01 Moist Surface Fescue 258,000 10.33 GDU9-2 Isley Jan 01 Moist Surface Fescue 138,000 5.52 GDU10-1 Garrison Jan 01 Moist Surface Fescue 12,000 0.48 GDU6-2 O'Quinn Apr 01 Dry Surface Fescue 204,000 8.17 GDU6-3 O'Quinn Apr 01 Dry Surface Fescue 204,000 8.17 GDU6-4 O'Quinn Apr 01 Dry Surface Fescue 30,000 1.20 UN1-21 Hanks Jul 01 Dry Surface Wheat 252,000 10.09 UN1-24 Hanks Jul 01 Dry Surface Wheat 90,000 3.60 UN1-25 Hanks Jul 01 Dry Surface Wheat 132,000 5.28 UN1-26 Hanks Jul 01 Dry Surface Wheat 96,000 3.84 GDU6-3 O'Quinn Oct 01 Dry Surface Fescue 576,000 23.06 Total 1,992,000 gal 79.74 dry/tons 4022 White Plains Rd. • Roaring River,NC 28669 • (336) 957-8839 PLIk Precision Land Application, Inc. Operations Report 1/1/01 to 12/31/01 Unifi, Inc. Plant 15 (Mayodan,NC) Site No. Farmer Date Weather Method Crop Gallons/Yards Dry Tons GDU8-1 Purgason Feb 01 Dry Surface Fescue 90,000 2.59 GDU8-2 Purgason Feb 01 Dry Surface Fescue 90,000 2.59 GDU8-1 Purgason Apr 01 Dry Surface Fescue 210,000 6.04 GDU8-2 Purgason Apr 01 Dry Surface Fescue 138,000 3.97 GDU5-3 Purgason Apr 01 Dry Surface Fescue 96,000 2.76 GDU5-2 Purgason Apr 01 Dry Surface Fescue 60,000 1.73 GDU7-1 Green Jun 01 Dry Surface Fescue 228,000 6.56 GDU7-2 Green Jun 01 Dry Surface Fescue 270,000 7.77 GDU5-7 Purgason Aug 01 Dry Surface Fescue 504,000 14.50 GDU5-4 Purgason Nov 01 Dry Surface Fescue 336,000 9.67 GDU5-8 Purgason Nov 01 Dry Surface Fescue 168,000 4.83 Total 2,190,000 gal 63.01 dry/tons 4022 White Plains Rd. • Roaring River,NC 28669 • (336) 957-8839 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number Laboratory 1) Unifi,Inc. Facility Name Unifi,Inc. 2) Test America(Nashville,TN) NPDES# WQ0006594 3) or WQ#(residual only facilities) WWTP Name Unifi, Inc. Plants 2&15 Residual Analysis Data Date Sampled(grab)or 3/1ro1 Grab 3/1ro1 Grab Date Composited (Plant 2 , (Plant 15) Percent Solids 0.96 0.69 Parameters(mg/kg dry weight) Arsenic 0.52 0.00 Cadmium o.00 o.00 Chromium o.00 o.00 Copper 41.35 23.19 Lead 0.63 1.45 Mercury o.00 o.00 Molybdenum o.00 o.00 Nickel 3.54 3.19 Selenium 1.25 2.03 Zinc 19.06 14.49 TKN 32,812.50 25,072.46 Ammonia Nitrogen 4,718.75 1,652.17 Nitrate-Nitrogen 4,708.33 0.00 Total Phosphorus 2,916.66 ,•,072.46 X _ J-2r-ae (SIG' E OF PREPAR ) �~ DATE nder penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,induding the possibility of fines and imprisonment for knowing violations." DEM FORM SSF(10/94) Precision Land Application, Inc. Biosolids Analysis Report Project: Unifi, Inc. Plant 2 Sample Date: 3/1/01 %Solids: 0.96 Type of Sample Taken: Grab pH: 8.4 Conversion Table Parameter Mg/Kg X 0.002 = lbs/dry ton Nitrogen TKN 32,812.50 65.63 Ammonia N 4,718.75 9.44 Nitrate N 4708.33 9.4167 Phosphorus 2,916.66 5.83 Ceiling Concentration Mg/Kg Arsenic 0.52 OK 75.00 0.0010 Cadmium 0.00 OK 85.00 0.0000 Chromium 0 0 Copper 41.35 OK 4300.00 0.0827 Lead 0.63 OK 840.00 0.0013 Mercury 0.00 OK 57.00 0.0000 Molybdenum 0.00 OK 75.00 0.0000 Nickel 3.54 OK 420.00 0.0071 Selenium 1.25 OK 100.00 0.0025 Zinc 19.06 OK 7500.00 0.0381 Aluminum 0.00 0.0000 Calcium 2,968.75 5.94 Chlorides 0.00 0.0000 iron 0.00 0.0000 Magnesium 988.54 1.98 Manganese 0.00 0.0000 Potassium 4,302.08 8.60 Sodium 30,312.50 60.63 Sulfur - 0.00 Plant Available Nitrogen(PAN) Mineralization Rate: 0.3 Unstabilized Primary&Secondary Residuals 0.4 Aerobically Digested Residuals 0.3 Anaerobically Digested Residuals 0.2 Composted Residuals 0.1 [(MR x(TKN -AmN))+ (.5 x AmN) + NO3N]x .002=lbs. PAN/dry ton Surface 15,495.83 Mg/Kg 30.99 lbs PAN I dry ton [(MR x(TKN -AmN)) +AmN + NO3N]x .002=lbs. PAN/dry ton Injection 17,855.21 Mg/Kg 35.71 lbs PAN I dry ton Page 1 of 3 Precision Land Application, Inc. Biosolids Analysis Report (Continued) Project: Unifi, Inc. Plant 2 Sample Date: 3/1/01 Type of Samples Taken: Grab Pathogen Reduction Not Applicable Sodium Absorption Ratio(SAR): 12.02 Approaching Limit Vector Attraction Reduction Not Applicable Page 2 of 3 Precision Land Application, Inc. Biosolids Information Sheet Nutrients Provided at 20,000 Gallons/Acre Project: Unifi, Inc. Plant 2 0.80 Dry tons/Acre pH: 8.4 Sample Date: 3/1/01 lbs./acre Parameter applied Nitrogen(PAN) 24.81 Phosphorus(P) 4.67 Potassium(K) 6.89 Sulfur 0.000 Calcium 4.754 Magnesium 1.583 Copper 0.066 Zinc 0.031 Cadmium 0.000 Nickel 0.006 Lead 0.001 Biosolid Value Unit cost/lb* $/acre Nitrogen (N) $0.17 $4.27 Phosphate(P) $0.17 $0.80 Potash (K) $0.17 $1.18 •Costs based on 17-17-17 purchased by the ton and spread by Southern States,Inc. $211.00 per ton,of which$35.00 was spreading cost. Cost dated:June 1999 Spreading Cost per acre: $5.30 Total value per acre: $11.56 Note: Application of this residual to the land is prohibited except in accordance with the instructions on this sheet. Note: State regulations require that at least 10'buffer zone between the application site and any public or private water supply source(including wells)and any stream,lake,river,or natural drainage way. This residual shall not be applied to any frozen,flooded,or snow covered area. Note: Adequate procedures must be taken to prevent surface runoff from carying any applied or stored residuals into any surface water. Page 3 of 3 Limn. QUALITY THROUGH PRIDE 2920 Vance St. P.O. Box 1437 27323 Reidsville,NC 27320 Certificate#: 68 Analysis performed by: Darlene Moore Sample Location: Digested Sludge Date Collected: 3-5-01 Date Analyzed: 3-5-01 Analysis Result Method pH 8.4 4500-H+ B Total Solids .96 2540 B festAmer!ct• INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 01-A26679 CHRIS ALEXANDER Sample ID: UN2-2 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Project : PLANTS 2 & 15 Time Collected: 11 :00 Project Name: UNIFI,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* Nitrate/Nitrite-N as N 45.2 mg/1 0.500 0.100 5 3/ 3/01 0:49 A.Bamarni 353.2 2666 Phosphorus 28.0 mg/1 0.100 0.100 1 3/ 8/01 22:00 Hardcastle 365.4 5811 Ammonia Nitrogen as N 45.3 mg/1 1.00 0.100 10 3/ 5/01 9:00 Hardcastle 350.1M 3783 Kjeldahl Nitrogen as N 315. mg/1 0.100 0.100 1 3/ 6/01 9:30 Hardcastle 351.2 3794 ND - Not detected at the report limit. # - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Method 350.1 modified for midi-distillation with Lachat procedure. Sample report continued . . 2960 FnsTKK CRKU;II iw DRI I / Nasnkn.i,E.TN 37204 / 615-726-0177 / F\x: 615-726-0954 / 800-765-0980 TestAmerica' INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26679 Sample ID: UN2-2 Project : PLANTS 2 & 15 Page 2 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: C Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FosTIK (;KRu;IITon DRIVE / NAs►nvn,1,E.TN 37204 / 615-726-0177 / FAx: 615-726-0954 / 800-765-0980 • 1 f'' festAmer!cà INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: O1-A26680 CHRIS ALEXANDER Sample ID: UN2-3 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Project : PLANTS 2 & 15 Time Collected: 11 :00 Project Name: UNIFI,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *METALS* Mercury ND mg/1 0.0020 0.0002 1 3/ 5/01 14:06 G.McCord 245.1 3804 Arsenic 0.0050 mg/1 0.0050 0.0050 1 3/ 4/01 13:25 G.McCord 200.7 2976 Cadmium ND mg/1 0.0010 0.0010 1 3/ 4/01 13:25 G.McCord 200.7 2976 Calcium, total 28.5 mg/1 1.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Copper 0.397 mg/1 0.0100 0.0100 1 3/ 4/01 13:25 G.McCord 200.7 2976 Lead 0,0060 mg/1 0.0030 0.0030 1 3/ 4/01 13:25 G.McCord 200.7 2976 Magnesium 9.49 mg/1 1.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Molybdenum ND mg/1 0.0500 0.0500 1 3/ 4/01 13:25 G.McCord 200.7 2976 Nickel 0.0340 mg/1 0.0100 0.0100 1 3/ 4/01 13:25 G.McCord 200.7 2976 Potassium 41.3 mg/1 1.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Selenium 0.0120 mg/1 0.0050 0.0050 1 3/ 4/01 13:25 G.McCord 200.7 2976 Sodium, total 291. mg/1 10.0 1.00 10 3/ 4/01 13:25 G.McCord 200.7 2976 Zinc 0.183 mg/1 0.0200 0.0200 1 3/ 4/01 13:25 G.McCord 200.7 2976 ND - Not detected at the report limit. I - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Sample report continued . . . 2960 FOsrh.K (:KKIGt1r(1S DKIkE / Nns►1vn,i.E.TN 37204 / 615-726-0177 / Fnx: 615-726-0954 / 800-765-0980 festAmericâ INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26680 Sample ID: UN2-3 Project : PLANTS 2 & 15 Page 2 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 Fo,TISK CKKImIroN DKIv / NAsn Im,K,TN 37204 / 615-726-0177 / Fax: 615-726-0954 / 800-765-0980 • Precision Land Application, Inc. Biosolids Analysis Report Project: Unifi, Inc. Plant 15 Sample Date: 3/1/01 % Solids: 0.69 Type of Sample Taken: Grab pH: 7.2 Conversion Table Parameter Mg/Kg X 0.002 = lbs/dry ton Nitrogen TKN 25,072.46 50.14 Ammonia N 1,652.17 3.30 Nitrate N 0.00 0.0000 Phosphorus 4,072.46 8.14 Ceiling Concentration Mg/Kg Arsenic 0.00 OK 75.00 0.0000 Cadmium 0.00 OK 85.00 0.0000 Chromium 0 0 Copper 23.19 OK 4300.00 0.0464 Lead 1.45 OK 840.00 0.0029 Mercury 0.00 OK 57.00 0.0000 Molybdenum 0.00 OK 75.00 0.0000 Nickel 3.19 OK 420.00 0.0064 Selenium 2.03 OK 100.00 0.0041 Zinc 14.49 OK 7500.00 0.0290 Aluminum 0.00 0.0000 Calcium 20.60 0.04 Chlorides 0.00 0.0000 Iron 0.00 0.0000 Magnesium 1,089.86 2.18 Manganese 0.00 0.0000 Potassium 6,666.67 13.33 Sodium 55,652.17 111.30 Sulfur - 0.00 Plant Available Nitrogen(PAN) Mineralization Rate: 0.3 Unstabilized Primary&Secondary Residuals 0.4 Aerobically Digested Residuals 0.3 Anaerobically Digested Residuals 0.2 Composted Residuals 0.1 [(MR x(TKN -AmN)) +(.5 x AmN)+ NO3N]x.002=lbs. PAN/dry ton Surface 7,852.17 Mg/Kg 15.70 lbs PAN/dry ton [(MR x(TKN -AmN)) +AmN + NO3N]x .002 =lbs. PAN/dry ton Injection 8,67826 Mg/Kg 17.36 lbs PAN I dry ton Page 1 of 3 Precision Land Application, Inc. Biosolids Analysis Report (Continued) Project: Unifi, Inc. Plant 15 Sample Date: 3/1/01 Type of Samples Taken: Grab Pathogen Reduction Not Applicable Sodium Absorption Ratio(SAR): 29.66 Approaching omit Vector Attraction Reduction Not Applicable Page 2 of 3 Precision Land Application, Inc. Biosolids Information Sheet Nutrients Provided at 20,000 Gallons /Acre Project: Unifi, Inc. Plant 15 0.58 Dry tons/Acre pH: 7.2 Sample Date: 3/1/01 lbs./acre Parameter applied Nitrogen(PAN) 9.04 Phosphorus(P) 4.69 Potassium(K) 7.67 Sulfur 0.000 Calcium 0.024 Magnesium 1.254 Copper 0.027 Zinc 0.017 Cadmium 0.000 Nickel 0.004 Lead 0.002 Biosolid Value Unit cost/lb* S/acre Nitrogen(N) $0.17 $1.55 Phosphate(P) $0.17 $0.81 Potash (K) $0.17 $1.32 *Costs based on 17-17-17 purchased by the ton and spread by Southern States,Inc. $211.00 per ton,of which$35.00 was spreading cost. Cost dated:June 1999 Spreading Cost per acre: $5.30 Total value per acre: $8.98 Note: Application of this residual to the land is prohibited except in accordance with the instructions on this sheet. Note: State regulations require that at least 10'buffer zone between the application site and any public or private water supply source(including wells)and any stream,lake,river,or natural drainage way. This residual shall not be applied to any frozen,flooded,or snow covered area. Note: Adequate procedures must be taken to prevent surface runoff from carying any applied or stored residuals into any surface water. Page 3 of 3 • vnriri QUALITY THROUGH PRIDE 271 Cardwell Rd. P.O. Box 250 Mayodan, NC 27027 Certificate#: 334 68 Analysis performed by: Darlene Moore John Allen Sample Location: Return Sludge Date Collected: 3-29-01, 4-9-01 Date Analyzed: 4-2-01, 4-9-01 Analysis Result Method pH 7.2 4500-H+B Total Solids .69 2540 B TestAmericä INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 01-A26682 CHRIS ALEXANDER Sample ID: UN15-2 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Project : PLANTS 2 & 15 Time Collected: 9:45 Project Name: UNIFI,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* Nitrate/Nitrite-N as N ND mg/1 0.100 0.100 1 3/ 3/01 0:50 A.Bamarni 353.2 2666 Phosphorus 28.1 mg/1 0.100 0.100 1 3/ 8/01 22:00 Hardcastle 365.4 5811 Ammonia Nitrogen as N 11.4 mg/1 0.100 0.100 1 3/ 5/01 9:00 Hardcastle 350.1M 3783 Kjeldahl Nitrogen as N 173. mg/1 0.100 0.100 1 3/ 6/01 9:30 Hardcastle 351.2 3794 ND - Not detected at the report limit. / - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Method 350.1 modified for midi-distillation with Lachat procedure. Sample report continued . . . 2960 Fos•rI R CkRu:IlTo1 DKI%E / N.Asncn.i,N;.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 ��m rl• est e ca INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26682 Sample ID: UN15-2 Project : PLANTS 2 & 15 Page 2 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER C;REIG,IITON DRIVE / NASHVII,1.E.TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 . . ThstAmer!cit' INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 01-A26683 CHRIS ALEXANDER Sample ID: UN15-3 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Protect : PLANTS 2 & 15 Time Collected: 9:45 Project Name: UNIFI ,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *METALS* Mercury ND mg/1 0.0004 0.0002 1 3/ 5/01 14:06 G.McCord 245.1 3804 Arsenic ND mg/1 0.0100 0.0050 1 3/ 4/01 13:25 G.McCord 200.7 2976 Cadmium ND mg/1 0.0020 0.0010 1 3/ 4/01 13:25 G.McCord 200.7 2976 Calcium, total 20.6 mg/1 2.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Copper 0.160 mg/1 0.0200 0.0100 1 3/ 4/01 13:25 G.McCord 200.7 2976 Lead 0.0100 mg/1 0.0060 0.0030 1 3/ 4/01 13:25 G.McCord 200.7 2976 Magnesium 7.52 mg/1 2.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Molybdenum ND mg/1 0.100 0.0500 1 3/ 4/01 13:25 G.McCord 200.7 2976 Nickel 0.0220 mg/1 0.0200 0.0100 1 3/ 4/01 13:25 G.McCord 200.7 2976 Potassium 46.0 mg/1 2.00 1.00 1 3/ 4/01 13:25 G.McCord 200.7 2976 Selenium 0.0140 mg/1 0.0100 0.0050 1 3/ 4/01 13:25 G.McCord 200.7 2976 Sodium, total 384. mg/1 20.0 1.00 10 3/ 4/01 13:25 G.McCord 200.7 2976 Zinc 0.100 mg/1 0.0400 0,0200 1 3/ 4/01 13:25 G.McCord 200.7 2976 ND - Not detected at the report limit. 0 - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Sample report continued . . . 2960 FOSTER CKN;mnrnr I)aivI / NAsIlvii,i,K,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmerica INCORPOR ATED ANALYTICAL REPORT Laboratory Number: O1-A26683 Sample ID: UN15-3 Project : PLANTS 2 & 15 Page 2 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FosTKk CRKimiroN DRIYK / NAsNYILLR.TN 37204 / 615-728-0177 / FA‘: 615-726-0954 / 800-765-0980 Lim r est e Ica INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: 01-A26678 CHRIS ALEXANDER Sample ID: UN2-1 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Project : PLANTS 2 & 15 Time Collected: 11 :00 Project Name: UNIFI,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* pH 7.50 pH Units 1 3/ 5/01 12:35 K. Stewart 9040/150.1 2649 TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (Y.) Date Time Analyst Method QC Batch Arsenic < 0.100 mg/1 5.0 106 3/ 7/01 10:25 G.Robinson 6010E 3278 Barium < 1.00 mg/1 100 95 3/ 7/01 10:25 G.Robinson 6010B 3278 Cadmium < 0.100 mg/1 1.0 100 3/ 7/01 10:25 G.Robinson 6010B 3278 Chromium < 0.500 mg/1 5.0 95 3/ 7/01 10:25 G.Robinson 6010B 3278 Lead < 0.500 mg/1 5.0 103 3/ 7/01 10:25 G.Robinson 6010B 3278 Mercury < 0.0100 mg/1 0.20 98 3/ 5/01 11:53 G.McCord 7470A 3426 Selenium < 0.100 mg/1 1.0 113 3/ 7/01 10:25 G.Robinson 6010E 3278 Silver < 0.100 mg/1 5.0 98 3/ 7/01 10:25 G.Robinson 6010B 3278 Benzene < 0.0200 mg/1 0.5 102 3/ 6/01 8:47 C.Bates 8260 4399 Carbon tetrachloride c 0.0200 mg/1 0.5 82 3/ 6/01 8:47 C.Bates 8260 4399 Chlorobenzene < 0.0200 mg/1 100 104 3/ 6/01 8:47 C.Bates 8260 4399 Chloroform < 0.0200 mg/1 6.0 114 3/ 6/01 8:47 C.Bates 8260 4399 1,2-Dichloroethane < 0.0200 mg/1 0.5 114 3/ 6/01 8:47 C.Bates 8260 4399 1,1-Dichloroethene < 0.0200 mg/1 0.7 124 3/ 6/01 8:47 C.Bates 8260 4399 Methylethylketone < 0.100 mg/1 200 89 3/ 6/01 8:47 C.Bates 8260 4399 Tetrachloroethene < 0.0200 mg/1 0.7 104 3/ 6/01 8:47 C.Bates 8260 4399 Sample report continued . . . 2960 FOSTER CREIGHTn' OR14M: / N,ksii%ILLK,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 im eatL erica INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26678 Sample ID: UN2-1 Project : PLANTS 2 & 15 Page 2 TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (Y.) Date Time Analyst Method QC Batch Trichloroethene < 0.0200 mg/1 0.5 114 3/ 6/01 8:47 C.Bates 8260 4399 Vinyl Chloride < 0.0200 mg/1 0.2 104 3/ 6/01 8:47 C.Bates 8260 4399 Cresols < 0.0100 mg/1 200 91 3/ 7/01 20:44 J.Fuqua 8270 6176 1,4-Dichlorobenzene < 0.0100 mg/1 7.5 102 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4-Dinitrotoluene < 0.0100 mg/1 0.13 112 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexachlorobenzene c 0.0100 mg/1 0.13 78 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexchlor-1,3-butadien < 0.0100 mg/1 0.5 106 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexachloroethane < 0.0100 mg/1 3.0 90 3/ 7/01 20:44 J.Fuqua 8270 6176 Nitrobenzene < 0.0100 mg/1 2.0 96 3/ 7/01 20:44 J.Fuqua 8270 6176 Pentachlorophenol < 0.0100 mg/1 100 70 3/ 7/01 20:44 J.Fuqua 8270 6176 Pyridine < 0.0100 mg/1 5.0 96 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4,5-Trichlorophenol < 0.0100 mg/1 400 116 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4,6-Trichlorophenol < 0.0100 mg/1 2.0 98 3/ 7/01 20:44 J.Fuqua 8270 6176 Chlordane < 0.0005 mg/1 0.030 125 3/ 8/01 14:49 R. Hunt 8081A 6124 2,4-D < 0.100 mg/1 10.0 78 3/ 7/01 16:17 R. Hunt 8151A 5252 Endrin < 0.0005 mg/1 0.02 115 3/ 8/01 14:49 R. Hunt 8081A 6124 Heptachlor < 0.0005 mg/1 0.008 101 3/ 8/01 14:49 R. Hunt 8081A 6124 Lindane < 0.0005 mg/1 0.4 102 3/ 8/01 14:49 R. Hunt 8081A 6124 Methoxychlor < 0.0005 mg/1 10.0 118 3/ 8/01 14:49 R. Hunt 8081A 6124 Toxaphene < 0.0100 mg/1 0.50 85 3/ 8/01 14:49 R. Hunt 8081A 6124 Silvex < 0.0100 mg/1 1.0 65 3/ 7/01 16:17 R. Hunt 8151A 5252 Heptachlor epoxide < 0.0005 mg/1 0.008 102 3/ 8/01 14:49 R. Hunt 8081A 6124 TCLP Extraction Initiated 3/ 2/01 15:40 K.Bundy 1311 2590 Zero Headspace Extraction Initiated 3/ 2/01 15:40 K.Bundy 1311 2590 ND - Not detected at the report limit. Matrix Spike Recovery for TCLP analytes reported from Batch QC TCLP prepartion follows method 1311, SW-846 Revision 3. Sample report continued . . . 2960 FusTER CREIGIIToN DRIvt / NASH1'ILLF:,TN 37204 / 615-726-0177 / FAN: 615-726-0954 / 800-765-0980 festAmericâ' INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26678 Sample ID: UN2-1 Project : PLANTS 2 & 15 Page 3 Sample Extraction Data Wt/Vol Parameter Extracted Extract Vol Date Time Analyst Method TCLP Herbicides 5.0 ml 5.00 ml 3/ 5/01 J. Rudden 3510 TCLP Pesticides 100. ml 10.0 ml 3/ 6/01 J. Rudden 3510 TCLP BNA's 500. ml 1.0 ml 3/ 6/01 J. Rudden 3510 Surrogate % Recovery Target Range BTEX/GRO Surr., a,a,a-TFT 131. 50. - 150. VOA Surr, 1,2-DCA, d4 130. 71. - 136. VOA Surr, Toluene d8 99. 69. - 129. VOA Surr, 4-BFB 93. 65. - 122. surr-Nitrobenzene-d5 72. 16. - 120. surr-2-Fluorobiphenyl 78. 10. - 136. surr-Terphenyl d14 78. 10. - 119. surr-Phenol d5 44. 10. - 69. surr-2-Fluorophenol 50. 10. - 148. surr-2,4,6-Tribromophenol 98. 11. - 144. pest surr-TCMX 50. 23. - 150. surr-Dibutylchlorendate 36. 10. - 120. surr-DCAA 94. 10. - 161. 0 - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Sample for pH analysis received outside method prescribed holding time. Sample report continued . . . 2960 FOSTER CREIGIITON DRIVE; / N.a,Inn.I.K,TN 37204 / 615-726-0177 / F,1x: 615-726-0954 / 800-765-0980 TestAmericà INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26678 Sample ID: UN2-1 Project : PLANTS 2 & 15 Page 4 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (7, Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 End of Sample Report. 2960 FOSTER CREIGHTON DKpvI / N,ASH%11,LE,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 TestAmericà ' INCORPORATED ANALYTICAL REPORT PLA 9471 Lab Number: O1-A26681 CHRIS ALEXANDER Sample ID: UN15-1 4022 WHITE PLAINS ROAD Sample Type: Liquid waste ROARING RIVER, NC 28669 Site ID: Date Collected: 3/ 1/01 Project : PLANTS 2 & 15 Time Collected: 9:45 Project Name: UNIFI,INC. Date Received: 3/ 2/01 Sampler: JAMES ALEXANDER Time Received: 9:00 Report Quan Dil Analyte Result Units Limit Limit Factor Date Time Analyst Method Batch *GENERAL CHEMISTRY PARAMETERS* pH 6.90 pH Units 1 3/ 5/01 12:35 K. Stewart 9040/150.1 2649 TCLP Results Matrix Spike Analyte Result Units Reg Limit Recovery (Y.) Date Time Analyst Method QC Batch Arsenic < 0.100 mg/1 5.0 106 3/ 7/01 10:25 G.Robinson 6010E 3278 Barium < 1.00 mg/1 100 95 3/ 7/01 10:25 G.Robinson 6010B 3278 Cadmium < 0.100 mg/1 1.0 100 3/ 7/01 10:25 G.Robinson 6010B 3278 Chromium < 0.500 mg/1 5.0 95 3/ 7/01 10:25 G.Robinson 6010B 3278 Lead < 0.500 mg/1 5.0 103 3/ 7/01 10:25 G.Robinson 6010B 3278 Mercury < 0.0100 mg/1 0.20 98 3/ 5/01 11:53 G.McCord 7470A 3426 Selenium < 0.100 mg/1 1.0 113 3/ 7/01 10:25 G.Robinson 6010B 3278 Silver < 0.100 mg/1 5.0 98 3/ 7/01 10:25 G.Robinson 6010B 3278 Benzene < 0.0200 mg/1 0.5 102 3/ 6/01 8:47 C.Bates 8260 4399 Carbon tetrachloride < 0.0200 mg/1 0.5 82 3/ 6/01 8:47 C.Bates 8260 4399 Chlorobenzene < 0.0200 mg/1 100 104 3/ 6/01 8:47 C.Bates 8260 4399 Chloroform < 0.0200 mg/1 6.0 114 3/ 6/01 8:47 C.Bates 8260 4399 1,2-Dichloroethane < 0.0200 mg/1 0.5 114 3/ 6/01 8:47 C.Bates 8260 4399 1,1-Dichloroethene < 0.0200 mg/1 0.7 124 3/ 6/01 8:47 C.Bates 8260 4399 Methylethylketone c 0.100 mg/1 200 89 3/ 6/01 8:47 C.Bates 8260 4399 Tetrachloroethene < 0.0200 mg/1 0.7 104 3/ 6/01 8:47 C.Bates 8260 4399 Sample report continued . . . 2960 FOSTER (NEIGHToM1 DKIxK / N.AsIixu.I.K.TN 37204 / 615-726-0177 / Fm 615-726-0954 / 800-765-0980 . . 1'estA meric t INCORPORATED ANALYTICAL REPORT Laboratory Number: O1-A26681 Sample ID: UN15-1 Project : PLANTS 2 & 15 Page 2 TCLP Results Matrix Spike Analyte , Result Units Reg Limit Recovery (Z) Date Time Analyst Method QC Batch Trichloroethene < 0.0200 mg/1 0.5 114 3/ 6/01 8:47 C.Bates 8260 4399 Vinyl Chloride < 0.0200 mg/1 0.2 104 3/ 6/01 8:47 C.Bates 8260 4399 Cresols < 0.0100 mg/1 200 91 3/ 7/01 20:44 J.Fuqua 8270 6176 1,4-Dichlorobenzene < 0.0100 mg/1 7.5 102 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4-Dinitrotoluene < 0.0100 mg/1 0.13 114 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexachlorobenzene < 0.0100 mg/1 0.13 82 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexchlor-1,3-butadien < 0.0100 mg/1 0.5 108 3/ 7/01 20:44 J.Fuqua 8270 6176 Hexachloroethane < 0.0100 mg/1 3.0 90 3/ 7/01 20:44 J.Fuqua 8270 6176 Nitrobenzene < 0.0100 mg/1 2.0 96 3/ 7/01 20:44 J.Fuqua 8270 6176 Pentachlorophenol < 0.0100 mg/1 100 96 3/ 7/01 20:44 J.Fuqua 8270 6176 Pyridine < 0.0100 mg/1 5.0 96 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4,5-Trichlorophenol < 0.0100 mg/1 400 116 3/ 7/01 20:44 J.Fuqua 8270 6176 2,4,6-Trichlorophenol < 0.0100 mg/1 2.0 100 3/ 7/01 20:44 J.Fuqua 8270 6176 Chlordane < 0.0005 mg/1 0.030 125 3/ 8/01 14:49 R. Hunt 8081A 6124 2,4-D < 0.100 mg/1 10.0 78 3/ 7/01 16:17 R. Hunt 8151A 5252 Endrin < 0.0005 mg/1 0.02 115 3/ 8/01 14:49 R. Hunt 8081A 6124 Heptachlor < 0.0005 mg/1 0.008 101 3/ 8/01 14:49 R. Hunt 8081A 6124 Lindane < 0.0005 mg/1 0.4 102 3/ 8/01 14:49 R. Hunt 8081A 6124 Methoxychlor < 0.0005 mg/1 10.0 118 3/ 8/01 14:49 R. Hunt 8081A 6124 Toxaphene < 0.0100 mg/1 0.50 85 3/ 8/01 14:49 R. Hunt 8081A 6124 Silvex < 0.0100 mg/1 1.0 65 3/ 7/01 16:17 R. Hunt 8151A 5252 Heptachlor epoxide < 0.0005 mg/1 0.008 102 3/ 8/01 14:49 R. Hunt 8081A 6124 TCLP Extraction Initiated 3/ 2/01 15:40 K.Bundy 1311 2590 Zero Headspace Extraction Initiated 3/ 2/01 15:40 K.Bundy 1311 2590 ND - Not detected at the report limit. Matrix Spike Recovery for TCLP analytes reported from Batch QC TCLP prepartion follows method 1311, SW-846 Revision 3. I I Sample report continued . . . 2960 FOSTER CREIGIIT(ln DRIVE / N.Asuen,i,E,TN 37204 / 615-726-0177 / Fir, 615-726-0954 / 800-765-0980 TestAmerict INCORPORATED ANALYTICAL REPORT Laboratory Number: 01-A26681 Sample ID: UN15-1 Project : PLANTS 2 & 15 Page 3 Sample Extraction Data Ht/Vol Parameter Extracted Extract Vol Date Time Analyst Method TCLP Herbicides 5.0 ml 5.00 ml 3/ 5/01 J. Rudden 3510 TCLP Pesticides 100. ml 10.0 ml 3/ 6/01 J. Rudden 3510 TCLP BNA's 500. ml 1.0 ml 3/ 6/01 J. Rudden 3510 Surrogate % Recovery Target Range BTEX/GRO Surr., a,a,a-TFT 130. 50. - 150. VOA Surr, 1,2-DCA, d4 130. 71. - 136. VOA Surr, Toluene d8 100. 69. - 129. VOA Surr, 4-BFB 95. 65. - 122. surr-Nitrobenzene-d5 80. 16. - 120. surr-2-Fluorobiphenyl 90. 10. - 136. surr-Terphenyl d14 76. 10. - 119. surr-Phenol d5 54. 10. - 69. surr-2-Fluorophenol 62. 10. - 148. surr-2,4,6-Tribromophenol 110. 11. - 144. pest surr-TCMX 48. 23. - 150. surr-Dibutylchlorendate 46. 10. - 120. surr-DCAA 97. 10. - 161. I - Recovery outside Laboratory historical limits. All results reported on a wet weight basis. Sample for pH analysis received outside method prescribed holding time. Sample report continued . . 2960 FOSTER CREIGHTOS DRIVK / NASHIILLR,TN 37204 / 615-726-0177 / FAX: 615-726-0954 / 800-765-0980 Lim rl est e ca I N C O R P O R A T E D ANALYTICAL REPORT Laboratory Number: O1-A26681 Sample ID: UN15-1 Project : PLANTS 2 & 15 Page 4 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Report Date: 3/12/01 Paul E. Lane, Jr. , Lab Director Gail A. Lage, Technical Serv. Michael H. Dunn, M.S. , Technical Director Glenn L. Norton, Technical Serv. Johnny A. Mitchell, Dir. Technical Serv. Kelly S. Comstock, Technical Serv. Eric S. Smith, Assistant Technical Director Pamela A. Langford, Technical Serv. Laboratory Certification Number: 387 I I End of Sample Report. 2960 FosTM:R CHPanu ffi I)RIVM: / NAs►ivH,i,r:,TN 37204 / 615-726-0177 / Fax: 815-726-0954 / 800-765-0980 5.726-0177 a Test rrierica Nashville960 F Nashvi 3� Phone:615-- . is b using proper for regulatory methods. o N C,.., Compliance Monitoring 4 E S ��d�ob Client Name PaEcsSie4 Lpao APPr.,c,�siu , 1..+c '1. Client PLA 94I Z� Address: I/42z r.Jr' T'E PA.A,..s a.. Project Name: J.. 1:.i , 1.+c. City/State/ZipCode: QoA0,,...(, 2.Jea.-) r k.. at1.0(DS Project*: Pu►...n ) d— 1S Project Manager. ,Sn.nes e• Ac4,.. am- Site/Location ID: State: NJL Telephone Number: (3 Ka) 1 1 y y 39 Fax C 31') q s i-rsr q t Report To: Sampler Name: (Print Name) _NateoE s C C. P1 A-,0E-- Invoice To: 1 Sampler Signature: L' . oat' Quote#: POO: Matrbc Preservation&it of Contahark Analyze For 1 TAT 1 i . 7D erabies Rush('surcharges may aPPIY) g , V ///// _Level 2 i III vilit ' (Batch QC) Oats Needed: ; b v, iF 7 Level 3 Fax Results: Y a ; 4 OtherLevel 4 rn U 3 3y 7l vim x � • i rSAMPLE ID p O x " Z REMARKS 0 0 a-z \ tit... 6. 9- ✓ ✓ 99 Ur,►a- 3 iI ac. G sc. / J ./ g0 U a ►S- 1 waS G SL Ni 31 v ra i S.- a q:ti5— G. 51. ✓ J '0- 0,1 IS -3 3-1-41 cjtc41* G s` ✓ ✓ I P-Ze$A Special Instructions: LABORATORY COMMENTS: Init Lab Temp: Rec Lab Temp: 3 G • Relinquished a ,c yo Date: Time: Received By Feel eic Date: Time: Custody Seals: Y N N/A Bottles Supplied by TestAmerica: Y N Retinquia Date: Time: Received By. C7-ejania2r Date:S/ r lime: 90t) Relinquished By: Date: Time: Received By: Date: Tune: Method of Shipment ..ice sari mows i.. — ...— .e of North Carolina 46?egyivii Iepartment of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor NCDENR Sherri Evans-Stanton,Acting Secretary NORTH CAROLINA DEPARTMENT OF Kerr T. Stevens,Director ENVIRONMENT AND NATURAL RESOURCES January 12,2001 TIMOTHY COLS RFC"" 1',` _._ UNIFI,INC-A SLUDGE/PLANT#2 's PO BOX 698 C y YADKINVILLE,NC 27055 FEB 0 `;0 tls 1 Subject: Annual Monitoring and Reporting Requirements Treatment and Land Application of Residuals Permit Number:WQ0006594 . 51., UNIFI,INC-A SLUDGE/PLANT#2 '..''-1' ROCKINGHAM County Dear TIMOTHY COLE, The purpose of this letter is a reminder that the monitoring reports required by the subject permit must be submitted as an Annual Report for calendar year 2000 by no later than March 1,2001. The report must be submitted(in triplicate) to the following address: DENR/DWQ/Water Quality Section Non-Discharge Compliance Unit 1617 Mail Service Center Raleigh,N.C.27699-1617 Due to limitations in storage space,please submit the reports in bound form rather than in notebook form. Permittees are subject to civil penalty for failing to submit the Annual Report as required by their permit. Enclosed are the summary and certification sheets that must be used for your annual report.Please complete these sheets and if necessary make copies of the blank forms if extras are needed. The forms have not changed since last year,so you may use those you already have on hand. You will however note that the forms include additional information required by EPA as outlined in 40 CFR Part 503. Since the requirements of 40 CFR Part 503 are self implementing, they are legally binding and enforceable Federal requirements for all persons subject to the requirements of 40 CFR Part 503,even if these requirements are not currently contained in the State permit.The annual reports for the EPA must be received by EPA at the following address on or before Febuary 19,2001. Hector Danois Clean Water Act Enforcement Section Water Programs Enforcement Branch Water Management Division U.S.EPA Region 4 61 Forsyth Street,S.W. Atlanta,Ga. 30303-3104 1617 Mail Service Center,Raleigh,North Carolina 27699-1617 Telephone 919-733-5083 Fax 919-733-0059 An Equal Opportunity Affirmative Action Employer 50%recycled/10%post-consumer paper Monitoring and Reporting Requirements Page 2. If there is a need for any information or clarification on the State reporting requirements,please do not hesitate to contact me at(919)733-5083 extension 529. For further information on the Federal requirements, you should call Madolyn Dominy of the Environmental Protection Agency at 404-562-9305. Sincer, Brian L.Wrenn, Environmental Specialist III cc: Vince Miller,EPA Region IV WSRO Regional Supervisor Non Discharge Compliance/Enforcement File Central Files F'' r a01NORTH CAROLINA DEPARTMENT OF 7i, ENVIRONMENT AND NATURAL RESOURCES ;` W DIVISION OF WATER QUALITY :, . • p R April 1, 1999 c ,= r. < J - 334 JAMCS B.FIUNY JR._ Pik''' Ms. Lisa K. Haynes f.�' ' I:j..j GOVERNOR -1 'R:`- Unifi, Inc., Mayodan P.O. Box 737 Winston. _ : 4 Madison, NC 27025- Regional • -I - ,: WAYNEMCDEVI7T Dear Ms. Haynes: i.SzcoiRY rA ,:,,,i=..ti Y , r''! It Your letter, received February 24, 1999, concerning corrective actions for your .4.,' t analytical procedures has been reviewed. The quality control measures taken in 4,• 4 ":� ‘- reference to the violations cited in the December 16, 1998 inspection report are A.rozoroN ow o- ,R.7 ..- :F acceptable. Your laboratory continues to meet the requirements of 15A NCAC 2H • �� • w11* *Si "• 0800 for the analysis of environmental samples. If a future inspection should reveal z+ -� ,�„ I` Y P P ,-•' K that the violations cited in the inspection report were not corrected, enforcement ;,•, actions will be recommended. ,vim ! ''w` ' ' : Thank you again for your cooperation during the inspection. Contact us at 919- r � 733-3908, extension 252, ifyou have anyquestions or need additional information � � �� tr' regarding our requirements. l':5r 14 1.!11§X 1 -.V Sincerely, �� ACam - V -� .� w Connie U. Brower 4. *:°t Laboratory Section r' , 4s cc: James W. Meyer .. Marilyn Deaver limi...f--,_,. ..:--- Winston-Salem Regional Office 7 Y ' ry-, N % , a1 Iz:a- s" r LABORATORY SECTION ^„ .. 'it,;": -j 4405 REEDY CREEK ROAD,RALEIGH,NORTH CAROLINA 27607-6445 a°`° "� PHONE 919-733-3908 FAX 919-733-6241 ' AN EQUAL OPPORTUNITY/AFFIRMATIVE ACTION EMPLOYER-S0%RECYCLED/10%POST-CONSUMER PAPER .. `:T�=:'W.R':s:...�Zi..a fafii.ld' ct NORTH c..AROLINA DEPARTMENT OF t„ ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY i�,�', A -'--1 mmmo Np R April 1, 1999 RECFrVED ~- f1.C. DLF. ,. .Jf EHNP ; ` : ;Y 68 JAMESB--HUNTJR: - Ms. Lisa K. Haynes APR 0 7 1999 GOVERNOR ":Y`- Unifi, Inc., Reidsville, NC -_ P.O. Box 737 Winston-Salea i Madison, NC 27025- Regional Of tei WAYNE MCDEVITT Dear Ms. Haynes: SECRETARY ',..-c .0 7 Your letter, received February 24, 1999, concerning corrective actions for your gip` analytical procedures has been reviewed. The quality control measures taken in b . : reference to the violations cited in the December 16, 1998 inspection report are A.PRESTON. 7'H i acceptable. Your laboratory continues to meet the requirements of 15A NCAC 2H JR-,.PE ,,'-)x ; D a ;t:' .0800 for the analysis of environmental samples. If a future inspection should reveal '' •� , y , that the violations cited in the inspection report were not corrected, enforcement °c actions will be recommended. pi 4 :` Thank you again for your cooperation during the inspection. Contact us at 919- ,. "J 733-3908, extension 252, if you have any questions or need additional information 1 regarding our requirements. K ok Sincerely, C,CIAL a-Le��- Connie U. Brower -4' Laboratory Section :. i t h ', cc: James W. Meyer .:--- Marilyn Deaver -..,:�:--•• Winston-Salem Regional Office - = _ , ,., :, $ LABORATORY SECTION ^ 4405 REEDY CREEK ROAD,RALEIGH, NORTH CAROLINA 27607-6445 r ` PHONE 919-733-3908 FAX 919-733-6241 - AN EQUAL OPPORTUNITY/AFFIRMATIVE ACTION EMPLOYER-S0%RECYCLED/IO%POST-CONSUMER PAPER