NCG200477_COMPLETE FILE - HISTORICAL_20110810

VV I hC4 EJ�Ve-
STORMWATER DIVISION CODING SHEET
RESCISSIONS.
PERMIT NO.
N C otLi-�
DOC TYPE
l` COMPLETE FILE - HISTORICAL
DATE OF
RESCISSION
❑ 0b l 1 D� 10
YYYYMMDD

�r
NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Colleen H. Sullins Dee Freeman
Governor Director Secretary
August 10, 2011
Rocky Mount Recyclers
Attn: Michael Avent
PO Box 7186
Rocky Mount, NC 27804-7186
Subject: Representative Outfall Status Request
Rocky Mount Recyclers/Fayetteville Metal Recyclers
NPDES Stormwater Permit NCG200000, COC-NCG200477
Cumberland County
Dear Mr.Avent:
Staff with the Fayetteville Regional Office of the Division of Water Quality have reviewed your request received on August
4, 2011 for a determination that stormwater discharge outfall (SDO) #1 be granted representative outfall status for
stormwater outfalls #1 and #2. Based on the information provided as well as a previous site visit conducted by Mike
Lawyer on February 24, 2011, we are approving this request. In accordance with 40 CFR §122.21(g)(7), you are
authorized to sample outfall number #1 as a representative outfall. This approval is effective with the next sampling event.
Please be reminded that the permit requires Qualitative Monitoring to be performed at all stormwater discharge outfalls,
regardless of representative outfall status.
Please remember that any actions you initiate in response to benchmark exceedances as directed in the tiered response
provisions of your permit must address all drainage areas represented by SDO #1, where appropriate.
Please append this letter to your Stormwater Pollution Prevention Plan (SPPP) to document that representative outfall
status has been approved. If changes in drainage areas, structures, processes, storage practices, or other activities occur
that significantly alter the basis of this approval, representative outfall status is no longer valid. In that case, you should
resume sampling at all SDOs, or reapply to this office for representative outfall status based on updated information. If
you have any questions or comments concerning this letter, please contact Mr. Lawyer at [phone] or by e-mail at
[e-mail].
Sincerely,
ACCreD
Belinda S. Henson
Regional Supervisor
Surface Water Protection Section
BSH: ML/ml
cc: FRO -Surface Water Protection-Stormwater Files
Stormwater Permitting Unit t
Location. 225 Green Street, Suite 714, Fayetteville, North Carolina 28301
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: httpi/ponal.ncdenr.otg/web/wq
An Equal Opportunity \ Affirmative Action Employer
NorthCarolina
Naturally

■ ■■■
■■ ■■
■ ■ ■
DWQ
1617 Mail Service Center
Raleigh, NC 27699-1617
July 10, 2014
Attention: Central Files
To whom it may concern:
REGIONAL
MATERIALS
RECOVERY, INC
R,CE.IWED
JUL 17 2014
CEWES
01BOG
There was no discharge recorded during the 91" monitoring event (January 1, 2014-June 30, 2014) for
general permit No. NCG 200000 and Certificate of Coverage NC200477. N(§� P-00 L/7
Sincerely,
Bo Brown

STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #S
RECEIVED
AUG 18 2014
NPOES PERMIT NO. NC 4 03001-L
FACILITY: /✓Ma ck e.�?' 0
COUNTY:
L g e,
PHONE /41 774— / / PE
INSPECTOR:
DATE: z 2, 0 I
OUTFALL No.
OUTFALL TYPE:
RECEMNG STREAM:
SD _ O-00
D INLET .PE t t FLUME
✓rivet weather obsorvation a Drywoator observallon
i Flow during dry weather u No flow during dry weather a Starrding water during dry weather
Describe the industrial acUvlties occurring within the ouufall drainage area.
COLOR - Describe the discharge color (e.g. red, brown, green, blue) and tint (e.g., tight, medium, dark).
C-1 C ."
ODOR - Describe airy distinctodors (e.g. gasoline, rotten eggs, chlorine) the discharge may hove.
pjv
CLARITY . Choose the number that beat ranks the clarity of the discharge, where 1 19Clear and 10 le very
cloudy-
1 2 6) 4 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of fleeting solids in the discharge.
where t Is no solids and 10 Is the surface covered with floating solids.
1 2 (�) 4 5 5 7 S 9 10
SUSPENDED SOLIDS - Choose the number that beat ranks the amount of suspended solids In tho discharge,
where t le no suitde and 10le kaemety muddy.
1 r 3 4 5 S 7 a 9 10
FOAM -
Is there any foam on or In the stormwater discharge? yes
OIL SHEEN -
Is there c0 shown visible In the sbormwater discharge or at the outafl? yq
DEPOSITION AT OUTFALL -
Aretore sedtmont ar citron materlel deposits "maw outfatl? yes no
EROSION AT OUTFALL -
le tore erosion at or Immediately below the outail? yes
List and describe ctor obvlow irrditsters of a0ommratar pollution:
By this signature, I certify trot this report Is accurate a wmplete ro "thee` off"''
MaaAJ. Monett, a.41�rd
Pe - 'a Signafura L11 Invedwi Siydafure
aury
MITTING

219 S. Steele SU.
Sanford, NC 27330
Phone:.[phone]
Cameron Testing' Services,,Inc. 'Chain of Custody
kc WWI I GW'66n. #654'NC PHHS Cin # 3779� us EPA . N . C . 01918 Page Of
Cknpihy:a
neti-Marelli
E A—'if
jmes
S,[e-mail]
qTSja-b i1s-0'..I
76My
Contact:
Phono:_
(c) -5
liames-Siler
919-�721-1353
" T,13A 6
i(Y/ . NINA)
12101 Nash St.
(City, State,
'
zip)
Sanford, NC 27330
No tes:
: Due:
Regulatory Rush .1
11 jYIN) A, /11 (YIN) i
ZwC4 so t*--- 1
collect Ndnre�.` -b
lure
-UffioWinfohnnAtion.
Nurnbdr;bf:hdMes
-
Sample ID
1-7
x
Requested Analysis
'CTSIL:ab
115
E
E
0
0
C)j
'b
jTO
os
7-
Aelknouishecl:ll
44
!Received:,,
Vateffinne
Rush work will requir6 prior ippr'oval. Additional charges will apply

Cameron Testing Services, Inc. Laboratory Report
Client: Magneti-Marelli CTS f'Foj.
Project: 2014 SW #1 Regulatory
Sample Information
Sampled J. Sller Date 02I03114 Reeolved
Analyses and Results
NC DENR 4654
NC PHHS 037799
US EPA #NC01918
140096
Yes
C. Cameron -Data 02103114
Lab'ID-
Sample lD
x
g
.a a
:U•�
Analyte
Result
=
j
'" m
o.
c'
Std. Methods
Reference
a
140096, 01
Outfall A
sw
C.
pit
60
S u
o
021D4114
DPK
45DO H 8 • pH
TSS
32.3
aget
26
02M7114
DPK
2540 D - TSS
02
Outfall B
sw
a
O&G-W
<5.0
"A.
s
02105/14
DPK
EPA 1664A
03
Outfall C
sw
Gr
EPA 6241625
04
Outfall D
sw
or
EPA 608
05
Outfall E
SW
M
Metals
TTO for samples -03 and •04 analyzed by ENCO; report attached.
Metals analyzed by FAQ; report attached.
Metals = Cu, Pb, Zn
Data
Review
Lab�"Teee��ljf�� n(/icla�n
Report
Review
/
—
Lab Director
219 S. Steele Su.
S:mioid NC 21330
may— -
oz.�/z1/9 ---
Date
91!1-20s-t240
d risqgcammmnasdtro.com

CHAIN -OF -CUSTODY .! .RECORD'
,6,wimi
wiwii.iiniolibCi6tn
I
N, 310131

�. FIRST ANALYTICAL LABORATORIES
billing: Pi) box 110272 - Research Trimigle Park, NC 277i 19
rbilyi..g. 7517 Precision Drive, Suile 101 - Raleigh NC 27C17
EPA Method 200 Analysis Report
FAL Project #: 140221.1
Client: Cameron Testing Services
Client Project ID: 140096
Sample Name: 140096-05 - SW#1
TEL: 919 942 W7
RAN: 919 882 1603,
n1nc. fuxmnah'tica I labs.com
Report Date: 2/20/2014
Date Received: 2/10/2014
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Copper(Cu)
0.018
0.001
Lead (Pb)
0.009
0.001
Zinc (Zn)
0.142
0.005
Approved by:
Matt Loftis, Laboratory Manager

®FIRST ANALYTICAL LABORATORIES
+ „r F'JEocllrP) Rexnmh'rri.ugle{'mk.N:,,,;,v CHAIN OF CUSTODY
✓,,,1.,,p .a -flee' n[pne.Smel01-R'vlegJ�. Ni ]-GI- F.lA)1•)Ys^_IMP
+c fua �ab»G"'llnbs :rm
Client:
Cameron Testing
Prol. Name/No: 140096
Contact:
Chris Cameron
Address:
219 S. Steele St.
Sanford, NC 27330
Phone No.
919-208-4240
email: chrisCalcamerontestina.com
Purchase Order#:
Note To Lab:
Collection
No. Sample ID Description Date Time Matrix Preservative
140221
Analysis Required
1
140096-05
SW #1
2/3/2014
1107
WW
NN03
Cu, Pb, Zn
2
3
4
5
6
7
8
9
10
vistrd er/ D te/Ti e:
1014, 'oU
Page I of
ae<ewea ey, ate/Time;
Reuegvished By: Date/Time:
Re,eived lob, Date/Time•
i ,r-r /'o'l ,j�e�/.�

� plr rVriiV- la
A'ArceTrtev.: Respvrsive:. Innovative
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, February 21, 2014
Cameron Testing Services, Inc. (CA039)
Attn: Chris Cameron
219 South Steele Street
Sanford, NC 27330
RE: Laboratory Results for
Project Number: 140096, Project Name/Desc: TTO
ENCO Workorder(s): C401556
Dear Chris Cameron,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, February 7, 2014.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Link Thrower
Project Manager
Enclosure(s)
RN0 lNs report relates only to the sample as recdved W the lab000M, and may only t,e reooxt i m Mi. Page 1 of 21

v .encolalmcom
ANALYTICAL RESULTS
Description: Trip Blank
Lab Sample ID:C401556-03
Received: 02/07/14 15:55
Matrix: Water
Sampled: 02/03/14 11:02
Work Order. C401556
project: TTO
Sampled By: Cameron Testing
Volatile Organic Compounds by GCMS
,-eon( Yry tadam44e(AC Oil
Anahne rCAS Number]
Results
fin
1111131
Bi
MU
ML
Ant
Hem
Analyzed
IN Notes
1,1,1-Trichlora:thane[71-55-6]^
<0.12
u9/1-
1
0.12
1.0
4810032
EPA 624
02/1111411:07
REF
1,1,2,2-Tetrachbroethane[79-34-5]^
<0.28
ug/L
1
0.28
1.0
QW032
EPA 624
02/11/14 11:07
REF
1,1,2-TriWaaetham[79-00-S]^
<0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1-Dkhkmoethane[75-34-3]^
<0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1-Dichloroethene[75-35-4]^
<0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02111/1411:07
REF
1,2-Didtlorpbenzene [95-50-1]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,2-Didtkaoetharte[307-06-2]^
<0.21
ug/L
1
0.21
1.0
4B30032
EPA 624
02/11/14 11:07
REF
1,2-Diddoropropa e[7R87-5]A
<0.10
ug/L
1
0.10
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,3-Dichlorobemene [541-73-1]A
< 0.15
ug/L
1
0.15
1.0
4BID032
EPA 624
02/1111411:07
REF
1,4-Di(hbrohemtene [106-46-7]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
2-Odmethyl Vinyl Ether [110-75-8]^
< 1.1
ug/L
1
Ll
5.0
4B10032
EPA 624
02/11/14 11:07
REF
Acrolein[107-02-8]A
<4.0
ug/L
1
4.0
10
4BI0032
EPA 624
02111/1411:07
REF
Attylonibile [107-13-I]A
< 3.5
ug/L
1
3.5
10
4B1D032
EPA 624
02111/1411:07
REF
Benzene[7143-2]A
<0.15
ug/L
1
0.15
1.0
4810032
EPA 624
02/1111411:07
REF
Broniodkhloromethane[75-27-4]^
<0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02111/1411:07
REF
Bnomoform[75-25-2]^
<0.22
ug/L
1
0.22
1.0
4B10032
EPA 624
02/1111411:07
REF
Bronnow,e ttate [74-83-9]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Carbon Tetrechbride[56-23-5]^
<0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chbrobenzene[108.9R7]A
<0.17
ug/L
1
0.17
1.0
4810032
EPA 624
02/11/14 11:07
REF
Chlo oethane [75-00-3]^
< 0.23
ug/L
1
0.23
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chloroform [67-66.3]A
0.53
3
u9/L
1
0.18
1.0
4BID032
EPA 624
02/11/14 11:07
REF
Chbromethane[7487-3]^
<0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02111/1411:07
REF
as-1,3-Dkhlorepropene[I0061-01-5]^
<0.20
ug/L
1
0.20
1.0
4BI0032
EPA 624
02/1111411:07
REF
Dbornochioane0iane[12448-1]^
<0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02111/1411:07
REF
Ethylbenzene[10R414]^
<0.13
ug/L
1
0.13
1.0
4BID032
EPA 624
02/11/14 11:07
REF
Methylene Oiloride[75-09-2]^
<0.23
ug/L
1
0.23
1.0
4830032
EPA 624
02/1111411:07
REF
Teboadtkroethene[127-184]^
<0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Toluene [108-8R3]^
< 0.14
ug/L
1
0.14
1.0
4BID032
EPA 624
02/11/1411:07
NET
tram-1,2-Dkhloroettene,[156-60-5]^
<0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 11:07
REF
trans-1,3-Dichlaroprapene[10061-02-61^
<0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02111/1411:07
REF
Trichkoroethene [79-01-61A
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Vinyl ddoride [75-01-4]^
< 0.32
ug/L
1
0.32
1.0
4B10032
EPA 624
02/11/14 11:07
REF
SIt1ouffief
HeStllf
' 9f
Svike-Ld
96
%Ref
Umlrs
an
1lElhffi
AmA2Cd
AY No
4-Broox&VADbenzene
38
I
50.0
76%
51-122
4BI0032
EPA 624
0211111411:07
REF
Dibwrp/kzaomefhax
43
1
50.0
85 %
68-117
4BI0032
EPA 624
0211111411.07
REF
Toluene-&
43
1
50.0
86 %
67-127
4810032
EPA 624
02/1111411.07
REF
FINAL This report relates mty to the sample as receiveil by the laboratory, and may only be repo iuoe in full. Page 8 021

C�
v .encolabs.com
ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID:C401556-02 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/1411:03 Work Order. C401556
Project: TTO Sampled By: lames Slier
NEENNIN
Semivolatile Organic Compounds by GC
^-9,CO2 qt fiN Jr Dry /AC 5911
Anabne FCAS Numberl
PCB-1260 [11096-82-5]A
Tomphene[BW1-35-21^
Surroaa[es
2,4,5,E-7CMX
2,4,5,6-7640(
OeYaorbVb#P yl
Oeeadrbmbp*nyl
BssWts
ELM
1lnits
12E
H" P41
A=
Method
Analyzed
By Notes
<0.45
ug/L
1
0.45 0.50
4809004
EPA 608
02/14/1413:16
MWC
<0.22
ug/L
1
0.22 1.0
4BO9003
EPA 608
02/14/1413:16
MWC
g�r(CF'
RE
Spike LN
%aer
%Rec Umlts
1=
6
By No
0.99
1
1.00
99 %
44-134
4BO9003
EPA 608
0211411413.16
MWC
0.99
1
1.00
99 %
45-ISI
4BO9004
EPA 608
07/1411413:16
MWC
0.96
1
1.00
96 %
37-149
4809003
EPA 606
0Z/14/1413:16
MWC
a96
1
1.00
96 %
42-159
4809004
EPA 608
0211411413:16
MWC
HI 7Ns repel rtlates 0* t0 the empk a aeheil by pie bWatM, aM may only Ee Mpr00 in fW. Page 7 0/ 21

1RWW.encolabs.com
ANALYTICAL RESULTS
Description: 140096-04
Lab Sample ID:C401556-02 Received: 02/07/14 15:55
Matrix: Water
Sampled:02/03/1411:03 Work Order: C401556
Project: TTO
Sampled By:lames Siler
Semivolatile Organic Compounds by GCMS
pnaMe IGeS Nemberl
Bg7Als
Haa LBiti
PE
llBS
PA
AaUh
ldathad
Analyz
Q[t yags
Hexachbmcydopentadiene [77-47A]A
< 1.3
ug/L
1
1.3
10
4808010
EPA 625
02/11/14 18:07
DFM
Hexachloroethane [67-72-11^
< 1.1
ug/L
1
1.1
10
4808010
EPA 625
02/11/1418:07
DFM
1nderlo(1,2,3-W)pyrene1193-39-5]1
<2.2
ug/L
1
2.2
10
4BOB010
EPA 625
02/11/1418:07
DFM
Isophomm [78-59-1)^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/1418:07
DFM
Naphthalene [91-20.3]^
< 1.3
ug/L
1
1.3
10
4B08010
EPA 625
02/11/1418:07
DFM
Nitrobenzene [98-95-3]A
< 1.2
ug/L
1
1.2
10
4BOB010
EPA 625
02/ll/1418:07
DFM
N-NkrosodimeMylamirre(fi2-75-9)^
<1.3
ug/L
1
1.3
10
4BOB010
EPA 625
0211111418:07
DFM
N-Nitros &- propyhmine [621-64-7)^
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/1418:07
DFM
N-Nitrosodiphmylamine/Diphenylamine
< 2.1
ug/L
1
2.1
10
4BO8010
EPA 625
02/11/1418:07
OFM
[86-30-6/122-394]^
Pentachlorophmol [87-86-5]A
< 1.8
U91L
1
1.8
10
4008010
EPA 625
02/11/14 18:07
DFM
Phmanthrene [85-01-8]^
< 1.4
ug/L
1
1.4
10
4808010
EPA 625
02/11/14 18:07
DFM
Phertol [108-95-21^
< 1.4
ug/L
1
1.4
10
4808010
EPA 625
02/11/1418:07
DFM
Pyrene [129-00-01^
< 2.1
ug/L
1
2.1
10
4BO8010
EPA 625
02111/14 18:07
DFM
59�ffi4 8eF(!(Jx'
O£
SWke LN
"
%Rec Lim/Cr
ANO
B
fir tl4tL5
2,4,6-Tndonppyr 1 82
1
100
52%
I9-157
48MIO
EPA 625
0271171418:07
DFM
2-R--bldrenyl 33
I
50.0
67%
15-139
48OW10
EPA 625
0211111418:07
DFM
2-Flu gahenol 46
1
100
46 %
10-104
4808010
EPA 625
0211111418.07
DFM
ffiftb�d5 30
I
50.0
60%
16-140
4B08010
EPA 625
01711/1418. 07
DFM
Plxml-d5 36
I
100
36 %
10-83
4A78010
EPA 62S
02111114 /8:07
DFM
757x'x "14 45
1
50.0
91 %
23-164
4BO8010
EPA 625
0211111418:07
DFM
Semivolatile Organic Compounds by GC
^ -F bry remred dro44e/AC s
Analyte [CAS Numberl
4,4'-DDD [72-548]A
4,4'-1)DE [72-55-91^
4,4'-DDT [50-29-31^
Aldrin [309.00-21^
alpha-BHC[319-846]A
beta-BHC [319-85-71^
Chlordane (n.o.s.) [57-749]^
Chlordane (teed [12789-03-6]^
deka-BHC[319.86-B]A
Dieldrin [60-57-1]^
Endosukan 1 (959-98-81
Endo%Van 11 [33213-65-9]A
Endosut[an sukate [1031-07-81^
Endrin [72-20-8]A
Endrin aldehyde [7421-934]^
gamma-BHC [58-89-9]A
Heptachlor[7644-8]^
Heptachlor epoxide [1024-57-31A
PCB-1016/1242[12674-11-2/53469-21-9]A
PCB-1221[11104284]A
PCB-1232[11141-16.5]^
PCB-1248[12672-29.6]A
PCB-1254 (11097-69.1]A
FINAL
itesult4 Eta
Mavis
QE
Ku
EQl
9ittrdl
Method
ABalyz
al H=
<0.041
ug/L
1
0,044
0.050
4BO9003
EPA 608
02/14/1413:16
MWC
<0.048
ug/L
1
0.048
0.050
4BO9003
EPA 608
02114/1413:16
MWC
<0.049
ug/L
1
0.049
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.041
ug/L
1
0.041
0.050
4BO9003
EPA 608
02/1411413:16
MWC
< 0.036
ug/L
1
0.036
0.050
4609003
EPA 608
02/14/14 13:16
MWC
<0.036
ug/L
1
0.036
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.020
ug/L
1
0.020
1.0
4BO9003
EPA 608
02/14/14 13:16
MWC
< 0.20
ug/L
1
0.20
0.50
4B09003
EPA 608
02/14/14 13:16
MWC
<0.048
ug/L
1
0.048
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.045
u91L
1
0.015
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.045
ug/L
1
0.045
0.050
4809003
EPA 608
02/14/14 13:16
MWC
<0.036
ug/L
1
0.036
0.050
4B09003
EPA 608
02/14/14 13:16
MWC
< 0.032
ug/L
1
0.032
0.050
4609003
EPA 608
02/14/14 13:16
MWC
< 0.041
u9/L
t
0.041
0.050
4809003
EPA 608
02/14/14 13:16
MWC
< 0.042
ug/L
1
0.042
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.034
ug/L
1
0.034
0.050
4B09003
EPA 608
02/14/1413:16
MWC
< 0.030
ug/L
1
0.030
0.050
4809D03
EPA 608
02/14/14 13:16
MWC
<0.037
Ig/L
1
0.037
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
<0.43
ug/L
1
0.43
0.50
4009004
EPA 603
02/14/14 13:16
MWC
< 0.37
❑9/L
1
0.37
0.50
4B09004
EPA 608
02/14/14 13:16
MWC
<0.45
u91L
1
0.45
0.50
4B09004
EPA 608
02/1411413:16
MWC
<0.014
ug/L
1
0.014
0.50
4BO9004
EPA 608
02/1411413:16
MWC
<-0.37
ug/L
1
0.37
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
This repot rdet ordl'to the sample as re,dv by the
laboratory,
and may a
dy be relxaduml in 6d1.
Pepe 6 0 21

v .encelabacom
ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID:C401556-02 Received: 02/07/14 15:55
Matrix: Water Sampled: 02/03/14 11:03 Work Order. C401556
Project: TTO Sampled ByJames Sher
ISemivolatile Organic Compounds by GCMS
AnaMe MAS Numbed
Rend
fin Una
j1I
Hu
Em
fttrh
Method
AnaBarA
BY
H=
1,2,4-Trkhlorobenzene[120-82-1]A
<1.2
ug/L
1
1.2
10
4808010
EPA 625
02111/1418:07
DFM
1,2-Didlkxobena ne [95-50.1]A
< 1.1
ug/L
1
1.1
10
4308010
EPA 625
02/11/14 18:07
DFM
1,3-Dichbrobenzene [541-73-1]A
< 1.1
u9/1.
1
1.1
10
4808010
EPA 625
02/11/14 18:07
DFM
1,4-Didtbrubenzene [106-46-M
< 1.0
ug/L
1
1.0
10
4808DIO
EPA 625
02/11/14 18:07
DFM
- 14lethyraphthaksle[9D-12-0]A
<1.7
ug/L
1
1.7
10
4BOB010
EPA 625
02111/1418:07
DFM
QL-02
- "2,4,5-Trkh1cxopheno1 [%,95-4]A
< 1.0
ug/L
1
1.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
2,4,6-Tnch1oropheno1 [0&06-2]A
< 1.1
ug/L
1
1.1
30
4BOB010
EPA 625
02/11/14 18:07
DFM
2,4-Dichlomphenol [120-83-21A
< 1.4
ug/L
1
1.4
30
41308010
EPA 625
02/11/14 18:07
DFM
2,4-Dimethylpheml [105-67-9]A
< 1.3
ug/L
1
1.3
10
4B09010
EPA 625
02/11/14 18:07
DFM
2,4-Dinitrophenol [51-28-5]A
< 2.6
ug/L
1
2.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4Dndmtduene[121-14-2]A
<2.4
ug/L
1
2.4
10
4BOR010
EPA 625
02/11/14 18:07
DFM
2,6-Dinitrotoluene [606-20.2]A
< 1.5
ug/L
1
1.5
10
4808010
EPA 625
02/11/14 18:07
DFM
2-Mlomnaphthalene [91-58-7]A
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2-Chloropt r l [95-57-81A
< 1.2
ug/L
1
1.2
10
4BOB010
EPA 625
02/11/14 18:07
DFM
2-MettrA4,6dinib'opheno1[53452-1]A
<2.9
ug/L
1
2.9
10
4BOB010
EPA 625
02111/1418:07
DFM
2-Methylnaphthalene[91-57-6]A
<1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2-Nitmpt a of [88-75-5]A
< 1.1
ug/L
1
1.1
10
4BOB010
EPA 625
02/11/14 18:07
DFM
3,T-DichbrobenzWhe [91-94-1]A
< 3.3
ug/L
1
3.3
30
4B08010
EPA 625
02/11/14 18:07
DFM
4BramophmyFpheny1ether [101-55-3]A
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
4-Chlcr 3-methylphenol [59-50-7]A
< 1.5
ug/L
1
1.5
10
4808010
EPA 625
02/11/14 18:07
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
<1.6
ug/L
1
1.6
10
4B08010
EPA 625
02111/1418:07
DFM
4Nitrophenol [100-02-7]A
< 2.0
ug/L
1
2.0
10
4BO8010
EPA 625
02/11/1418:07
DFM
Acenaph&h [83-32-9]A
<1.4
u9/L
1
1.4
10
4BOB010
EPA 625
02/11/1418:07
DFM
Aceaaphthylene [208-96.81A
< 1.2
u9/L
1
1.2
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Anthracene [120.12-7]A
< 1.6
ug/L
1
1.6
10
4BOBD10
EPA 625
02/11/14 18:07
DFM
Benzldine[92-87-5]A
<1.6
ug/L
1
1.6
10
4808010
EPA 625
02/11/14 18:07
DFM
Beoao(a)anthmcene 156-55-31A
<1.3
ug/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Benzo(a)pyrene [50-32-B]A
< 1.3
u9/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Berrzu(b)fluorenthene [205-99.2]A
< 1.0
u9/1.
1
1.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Benzo(g,hj)perylene [191-24-2]1
< 2.4
ug/L
1
2.4
30
4B08010
EPA 625
02/11/14 18:07
DFM
QV-01
Benzo(k)Ouoranthene [207-08-9]A
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzoic acid[65-85-0]A
<1.0
u9/L
1
1.0
50
4BOB010
EPA 625
02/11/14 18:07
DFM
Bis(2chkxcethoxy)meth3ne[111-91-1]A
<1.4
ug/L
1
1.4
10
480NIO
EPA 625
02/11/14 18:07
DFM
Bis(2ch1cmethy1)ether[111i 4]A
<1.2
ug/L
1
1.2
10
4BO8010
EPA 625
02/1111418:07
DFM
Bis(2cldamiscpm )ettw [108-60-11A
< 1.3
ug/L
1
1.3
10
4BOS010
EPA 625
02/11/14 18:07
DFM
81s(2-eth0hexy1)phtha1ate [117-81-7]A
< 1.7
u9/L
1
1.7
5.0
4808010
EPA 625
02/11/14 18:07
DFM
&itymenzy¢ththalate [85-68-7]A
< 2.0
ug/L
1
2.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
a.ysere[218-01-9]A
<2.0
ug/L
1
2.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Dibemo(a,h)anthracene (53.7D-3]A
< 2.3
ug/L
1
2.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
DiedrAphthalate [84-66-2]A
< 2.1
ug/L
1
2.1
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Dimethylphthalate [131-I1-31A
< 1.4
ug/L
1
1.4
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Di-n-butylphthalate [8474-21A
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/1111418:07
DFM
Di-n-octylphthalate[117-840]A
<3.1
ug/L
t
3.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
DPH (as Azobenzene) [103-33-3]A
< 1.9
ug/L
1
1.9
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Fhxxanthene [206-44-0]A
< 2.1
ug/L
1
2.1
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Fhxuene [86-73-7]A
< 1.7
ug/L
1
1.7
10
4808010
EPA 625
02/11/14 18:07
DFM
Hexachktmbezene [318-74.1]A
< LO
ug/L
1
1.0
10
4BOB010
EPA 625
02/1111418:07
DFM
Hexachlombutadiene [87-68-3]A
< 1.2
ug/L
1
1.2
10
4BOB010
EPA 625
02/11/1418:07
DFM
FINAL
This repot relates o * to the samde as recti ed by the laboratory, and may uriy be rew rimed In AdL
Page
5 d 21

1vIRW.encolabs.com
ANALYTICAL RESULTS
Description: 140096-03 Lab Sample ID:C401556-01 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/1411:02 Work Order: C401556
project: TTO Sampled By:lames Siler
(Volatile Organic Compounds by GCMS
^ -EAC'O prynv00M aruMa iM1C 5911
Analvte ICAS Numherl
Results flag
Ihdto
2E
MIX
EM
&atch
[Method
Analinzed
BY KQW
1,1,1-Tnchloroethane[71-55-6]^
<0.12
ug/L
1
0.12
1.0
4B10032
EPA 624
02111/1410:37
REF
1,1,2,2-Tetradibroethane[793451^
<0.28
ug/L
1
0.28
1.0
4B10032
EPA 624
0211111410:37
REF
1,1,2-Tdchloroethane[79.00-5]^
<0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 10:37
REF
- 1,1-Dichloroethane[75-34-3]^
<0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02111/1410:37
REF
_ - 1,1-Dichlon ethenre [75-35-4]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 10:37
REF
12-Dkhbrobenzene [95-SUM]^
< 0.19
ug/L
1
0.19
1.0
41310032
EPA 624
02/11/14 10:37
REF
y
1,2-Dirhloroethane [107-06-2]^
< 0.21
ug/L
1
0.21
1.0
4810032
EPA 624
02/11/14 10:37
REF
1,2-Dichbroixopane [I8-87-5]^
< 0.10
ug/L
1
0.10
1.0
4810032
EPA 624
02/11/14 10:37
REF
1,3-Dichlorobenzene[541-73-1]^
<0.15
ug/L
1
0.15
1.0
4B10D32
EPA 624
02/11/1410:37
REF
1,4Dichbrobenzene[106-46-71^
<D.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/1111410:37
REF
2-Chlome61y1 Vinyl Ether [110-75-8]^
< 1.1
ug/L
1
1.1
5.0
4B10032
EPA 624
02/11/14 10:37
REF
Acrolein[107-02-8]^
<4.0
ug/L
1
4.0
10
4BID032
EPA 624
02/11/14 10:37
REF
Acrylonitnle [107-13-11^
< 3.5
ug/L
1
3.5
10
4610032
EPA 624
02/11/14 10:37
REF
Benzene [71-43-2]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Bromodichbromethane[75-27-4]^
<0.17
ug/L
1
0.17
1.0
4BID032
EPA 624
02/11/14 10:37
REF
Bromofonn [75-25-2]^
< 0.22
ug/L
1
0.22
1.0
4810032
EPA 624
02/11/14 10:37
REF
DvnDmethane [74-83-9]^
< 0.14
ug/L
1
0.14
1.0
4810032
EPA 624
02/11/14 10:37
REF
Carbon Tetrachloride [56-23-5]^
< 0.17
ug/L
1
0.17
1.0
41310032
EPA 624
02/11/14 10:37
REF
Chlorobenzene [108-90-7]^
< 0.17
ug/L
1
0.17
1.0
4BID032
EPA 624
02/11/14 10:37
REF
Chloroethane [7500-3]^
< 0.23
ug/L
1
0.23
1.0
4BI0032
EPA 624
02/11/14 10:37
REF
Chloroform[67-66-3]^
<0.18
ug/L
1
0.18
1.0
4B10032
EPA 624
02111/1410:37
REF
Chloromethane [74-87-3]^
< 0.13
ug/L
1
0.13
1.0
4810032
EPA 624
02/1111410:37
REF
cis-1,3-Dichlompropene [I0061-01-5]^
< 0.20
ug/L
1
0.20
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Dibromodlbtornethane [124-48-1]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Ethylbenzene [100-41-4]^
< 0.13
ug/L
1
0.13
1.0
4BID032
EPA 624
02/11/14 10:37
REF
Methylene Chloride [75-09-2]^
< 0.23
ug/L
1
0.23
1.0
4010032
EPA 624
02/11/14 10:37
REF
Tebachloroethene [127-18-4]^
< 0.17
u9/L
1
0.17
1.0
4BID032
EPA 624
02/1111410:37
REF
Toluene [308-88-3]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 10:37
REF
trans-1,2-Dichbrcethene [156-60-5]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 30:37
REF
trans-1,3-Dichloropropene[10061-02-6]^
<0.15
ug/L
1
0.15
1.0
4BI0032
EPA 624
02111/1410:37
REF
Trichloroethene[79-01-6]^
<0.15
ug/L
1
0.15
1.0
4BI0032
EPA 624
02/11/14 10:37
REF
Vinyl chloride (75-01-41^
< 0.32
ug/L
1
0.32
1.0
4B10032
EPA 624
02/11/14 10:37
REF
5urrooates
FzfL(Lf
Rf
Spike L14
%Rec
%Rrl
NY Rotes
4-BromoMpmbenzere
37
1
50.0
74 %
51-122
4BI0032
EPA 624
0211111410:37
REF
Dion noflu0m Mane
41
1
50.0
82 %
68-117
4810032
EPA 624
0211111410.'37
REF
T010 08
42
1
50.0
83 %
67-127
4B10032
EPA 624
021111141027
REF
RI This report mates only to the sample as rt d� by the laboratory, aM may or 1, be reprodeeej in fiAL Page 4 of 21

www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
ClientlD: 140096-03
lab ID:
C401556-01
Sampled:
02/03/1411:02 Received: 02/07/14 15:SS
Parameter Hold Date/Time(s)
EPA 624 02/17/14
Prep Date/Time(s)
OZ/07/14
10:31
Analysis Date/Time(s)
02/11/14 10:37
ClientlD: 140096-04
Lab ID:
C401556.02
Sampled:
02/03/14 11:03 Received: 02/07/14 35:SS
Pammeter Hold Date/Time(s)
EPA 608 02/10/14
03/21/14
Prep Date/Time(s)
02/09/14
07:54
Analysis Date/Time(s)
02/14/14 13:16
EPA 608
EPA 625
02/03/15 03/21/14 02/09/14 08:00 02/14/14 13:16
02/10/14 03/20/14 02/08/14 22:53 OZ/11/14 18:07
Client ID:
Trip Blank
Lab ID: C401556-03
Sampled:
02/03/14 11:02 Received:
02/07/14 15:55
Parameter
EPA 624
Hold Date/Time(s)
02/17/14
Prep Date/Time(s)
OZ/07/14
10:31
Analysis Date/Time(s)
02/11/14 11:07
FINK nis report relates only to the sample as recd� by the laboratory, and may orgy Ee repmEycerJ in U. Page 2 0/ 21