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HomeMy WebLinkAboutNCG030427_MONITORING INFO_20190926Vv52 0 STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑ HISTORICAL FILE E� MONITORING REPORTS DOC DATE ❑ 90 0 U YYYYMMDD Stormwater Discharge Monitoring; Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted V2.1/2 CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 SAMPLE COLLECTION YEAR 2019 FACILITY NAME GKN 06veline Alamance SAMPLE PERIOD ❑ Jan -June ❑ July -Dec COUNTY Alamance or Q Monthly' /i 35 "_ (month) PERSON COLLECTING SAMPLES Ricky Hiatt �rCEI�IFnDISCHARGINGTOCLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert. # 12; 40 r ❑Zero -flow ®❑Water Supply ❑SA Comments on sample collection or analysis: SEP 26 2019 ❑Other Part A: Stormwater Benchmarks and Monitoring Results ;ENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION X No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 01 N/A 02 N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page i of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ricky Hiatt Name (Print name) EHS Coordinator Title (Print title) Signa re Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L'. where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. * No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMUR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR including all 'No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee Permit Date: 11/1/2018-05/31/2021 1, ry Date SWU-245, last revised 11/1/2018 Page 3 of 3 Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted 8/12/2019 CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 FACILITY NAME GKN Driveline Alamance COUNTY Alamance PERSON COLLECTING SAMPLES Ricky Hiatt LABORATORY Pace Analytical Lab Cert. # 12; 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Q Monthly' %/y (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ®❑Water Supply [_]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --) No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 01 7/22119 0.8" 5.8mg/I 6.5 0.0078 mg/I <0.005mg/I 0.0576mg/I <0.005mg/I N/A 02 7/22/2019 0.8" 12.2 mg/I 6.6 0.0069 mg/I <0.005mg/I 0.0408 mg/i <0.005mg/1 N/A ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Section B, Table 1 to identifythe especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Ricky Hiatt Name (Print name) EHS Coordinator Title (Print title) / Signal re Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑■ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMUR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this MR, including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge' reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." I Signature of Permittee Permit Date: 11/1/2018-05/31/2021 % V e2 Date SWU-245, last revised 11/1/2018 Page 3 of 3 ace Analytical ww 001abs.wm August 06, 2019 Ricky Hiatt GKN Driveline 1067 Trollingwood Hawfield Rd Mebane, NC 27302 RE: Project: Monthly Stormwater Pace Project No.: 92438449 Dear Ricky Hiatt: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 I Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2019. This report is a summary of the results based upon our understanding of your data quality objectives. Please contact us if itemized quality control results are needed. These results relate only to the samples included in this report. Outfall 001 samples were received outside of required temperature range. Analysis was completed upon client approval. If you have any questions concerning this report, please feel free to contact me. Sincerely, ti� b��--D Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Dave Bruce, GKN Driveline REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical e .pacelabs.wm CERTIFICATIONS Project: Monthly Stormwater Pace Project No.: 92438449 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirgmiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical .eacelsbscem SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Monthly Stormwater 92438449 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92438449001 Outfall 001 EPA 1664B JMS 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.4 1994 IDS 3 PASI-A EPA 625.1 PKS 58 PASI-C EPA 624.1 CL 34 PASI-C SM 2540D-2011 MJP 1 PASI-A SM 4500-H+B-2011 SMK 1 PASI-A EPA 420.4 Rev 1.0 1993 DMN 1 PASI-A 92438449002 Outfall 002 EPA 1664B JMS 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.4 1994 DS 3 PASI-A EPA 625.1 PKS 58 PASI-C EPA 624.1 CL 34 PASI-C SM 254OD-2011 MJP 1 PASI-A SM 4500-H+B-2011 SMK 1 PASI-A EPA 420.4 Rev 1.0 1993 DMN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalyical wawpacelabs.com ANALYTICAL RESULTS Project: Monthly Slormwaler Pace Project No.: 92438449 Sample: Outfall 001 Parameters Lab ID: 92438449001 Results Units Collected: 07/22119 13:20 Report Limit OF Oil and Grease NO mg/L 4.9 1 Aldrin NO ug/L 0.050 1 alpha-BHC NO ug/L 0.050 1 beta-BHC NO ug/L 0.050 1 delta-BHC NO ug/L 0.050 1 gamma-BHC (Lindane) NO ug/L 0.050 1 Chlordane (Technical) NO ug/L 0.50 1 alpha -Chlordane NO ug/L 0.050 1 gamma -Chlordane NO ug/L 0.050 1 4,4'-DDD NO ug/L 0.050 1 4,4'-DDE NO ug/L 0.050 1 4,4'-DDT 0.052 ug/L 0.050 1 Dieldrin NO ug/L 0.050 1 Endosulfan I NO ug/L 0.050 1 Endosulfan II NO ug/L 0.050 1 Endosulfan sulfate NO ug/L 0.050 1 Endrin NO ug/L 0.050 1 Endrin aldehyde NO ug/L 0.050 1 Heptachlor NO ug/L 0.050 1 Heptachlor epoxide NO ug/L 0.050 1 PC13-1016 (Aroclor 1016) NO ug/L 0.50 1 PCB-1221(Aroclor 1221) NO ug/L 0.50 1 PCB-1232 (Aroclor 1232) ND ug/L 6.50 1 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 PCB-1248 (Aroclor 1248) NO ug/L 0.50 1 PCB-1254 (Aroclor 1254) NO ug/L 0.50 1 PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 Toxaphene NO ug/L 0.50 1 Tetrachloro-m-xylene (S) 67 % 10-130 1 Decachlorobiphenyl (S) 24 % 10-130 1 Copper 7.8 ug/L 5.0 1 Lead NO ug/L 5.0 1 Zinc 57.6 ug/L 10.0 1 Acenaphthene NO ug/L 5.0 1 Acenaphthylene NO ug/L 5.0 1 Anthracene NO ug/L 5.0 1 Benzo(a)anthracene NO ug/L 5.0 1 Benzo(a)pyrene NO ug/L 5.0 1 Benzo(b)8uoranthene NO ug/L 5.0 1 Benzo(g,h,i)perylene NO ug/L 5.0 1 Benzo(k)8uoranlhene NO ug/L 5.0 1 4-Bromophenylphenyl ether NO ug/L 5.0 1 Butylbenzylphlhalate NO ug/L 5.0 1 4-Chloro-3-methylphenol NO ug/L 5.0 1 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 2-Chloronaphthalene NO ug/L 5.0 1 2-Chlorophenol NO ug/L 5.0 1 4-Chlorophenylphenyl ether NO ug/L 5.0 1 Ill REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunters,11c, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Dale: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, -LC. Page 4 of 13 aceAnalytical wwnpacelabs.com ANALYTICAL RESULTS Project: Monthly Slormwater Pace Project No.: 92438449 Sample: Outfall 001 Lab ID: 92438449001 Collected: 07/22/19 13:20 Parameters Results Units Report Limit OF Chrysene NO ug/L 5.0 1 Dibenz(a,h)anthracene NO ug/L 5.0 1 3,3'-Dichlorobenzidine NO ug/L 25.0 1 2,4-Dichlorophenol ND ug/L 5.0 1 Diethylphthalate NO ug/L 5.0 1 2,4-Dimethylphenol NO ug/L 10.0 1 Dimethylphthalate NO ug/L 5.0 1 Di-n-butylphthalate ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol NO ug/L 20.0 1 2,4-Dinitrophenol NO ug/L 50.0 1 2,4-Dinitrololuene NO ug/L 5.0 1 2,6-Dinitrololuene NO ug/L 5.0 1 Di-n-octylphthalate NO ug/L 5.0 1 bis(2-Ethylhexyl)phthalate NO ug/L 5.0 1 Fluoranthene NO ug/L 5.0 1 Fluorene NO ug/L 5.0 1 Hexachloro-1,3-butadiene NO ug/L 5.0 1 Hexachlorobenzene NO ug/L 5.0 1 Hexachlorocyclopentatiene NO ug/L 10.0 1 Hexachloroethane NO ug/L 5.0 1 Indeno(1,2,3-cd)pyrene NO ug/L 5.0 1 Sophorone NO ug/L 10.0 1 Naphthalene NO ug/L 5.0 1 Nitrobenzene NO ug/L 5.0 1 2-Nitrophenol NO ug/L 5.0 1 4-Nitrophenol NO ug/L 50.0 1 N-Nitrosodimethylamine NO ug/L 5.0 1 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 N-Nitrosodiphenylamine ND ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 Pentachlorophenol ND ug/L 10.0 1 Phenanthrene NO ug/L 5.0 1 Phenol NO ug/L 5.0 1 Pyrene NO ug/L 5.0 1 1,2,4-Trichlorobenzene NO ug/L 5.0 1 2,4,6-Trichlorophenol NO ug/L 10.0 1 Nitrobenzene-d5 (S) 66 % 10-120 1 2-Fluorobiphenyl (S) 60 % 15-120 1 Terphenyl-dib (S) 93 % 11-131 1 Phenol-d6 (S) 15 % 10-120 1 2-Fluorophenol(S) 6 % 10-120 1 SO 2,4,6-Tribromophenol (S) 30 % 10-137 1 Benzene NO ug/L 1.0 1 Bromodichloromethane NO ug/L 2.0 1 Bromoform NO ug/L 2.0 1 Bromomethane NO ug/L 2.0 1 Carbon tetrachloride NO ug/L 2.0 1 Chlorobenzene NO ug/L 2.0 1 Chloroethane NO ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Ana lyti c al Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, U.C. Page 5 of 13 aceAnalytical w pacelabs.ccnt ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92438449 Sample: Outfall 001 Parameters Lab ID: 92438449001 Results Units Collected: 07/22/19 13:20 Report Limit DF Chloroform ND ug/L 5.0 1 Chloromelhane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 1,2-Dichlorobenzene ND ug/L 2.0 1 1,3-Dichlorobenzene ND ug/L 2.0 1 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroelhane ND ug/L 2.0 1 1,2-Dichloroelhane ND ug/L 2.0 1 1,1-Dichloroelhene ND ug/L 2.0 1 cis-1,2-Dichloroelhene ND ug/L 2.0 1 trans-1,2-Dichloroethene ND ug/L 2.0 1 1,2-Dichloropropane ND ug/L 2.0 1 cis-1,3-Dichloropropene ND ug/L 2.0 1 trans-1,3-Dichloropropene ND ug/L 2.0 1 Elhylbenzene ND ug/L 1.0 1 Methylene Chloride ND ug/L 5.0 1 1,1,2,2-Tetrachloroelhane ND ug/L 2.0 1 Tetrachloroethene ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 1,1,2-Trichloroethane ND ug/L 2.0 1 Trichloroethene ND ug/L 2.0 1 Trichloro8uoromethane ND ug/L 2.0 1 Vinyl chloride ND ug/L 2.0 1 4-Bromofluorobenzene(S) 100 % 70-130 1 Toluene-d8 (S) 100 % 70-130 1 1,2-Dichloroelhane-d4 (S) 94 % 70-130 1 Total Suspended Solids 5.8 mg/L 4.2 1 pH at 25 Degrees C 6.5 Sid. Units 1.0 1 Phenol ND mg/L 0,020 1 H3 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced except in full, Dale: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, L-C. Page 6 of 13 aceAnalytical w Paoelabs.mm ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92438449 Sample: Outfall 002 Parameters Lab ID: 92438449002 Results Units Collected: 07/22/19 13:40 Report Limit DF Oil and Grease NO mg/L 4.8 1 Aldrin NO ug/L 0.050 1 alpha-BHC NO ug/L 0.050 1 beta-BHC NO ug/L 0.050 1 delta-BHC NO ug/L 0.050 1 gamma-BHC (Lindane) NO ug/L 0.050 1 Chlordane (Technical) NO ug/L 0.50 1 alpha -Chlordane NO ug/L 0.050 1 gamma -Chlordane NO ug/L 0.050 1 4,4'-DDD NO ug/L 0.050 1 4,4'-DDE NO ug/L 0.050 1 4,4'-DDT 0.055 ug/L 0.050 1 Dieldrin NO ug/L 0.050 1 Endosulfan I ND ug/L 0.050 1 Endosulfan If NO ug/L 0.050 1 Endosulfan sulfate NO ug/L 0.050 1 Endrin NO ug/L 0.050 1 Endrin aldehyde NO ug/L 0.050 1 Heptachlor NO ug/L 0.050 1 Heptachlor epoxide NO ug/L 0.050 1 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 PCB-1221 (Aroclor 1221) NO ug/L 0.50 1 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 PCB-1260 (Aroclor 1260) NO ug/L 0.50 1 Toxaphene NO ug/L 0.50 1 Tetrachloro-m-xylene (S) 70 % 10-130 1 Decachlorobiphenyl(S) 55 % 10-130 1 Copper 6.9 ug/L 5.0 1 Lead NO ug/L 5.0 1 Zinc 40.8 ug/L 10.0 1 Acenaphthene NO ug/L 5.0 1 Acenaphthylene NO ug/L 5.0 1 Anthracene NO ug/L 5.0 1 Benzo(a)anlhracene NO ug/L 5.0 1 Benzo(a)pyrene NO ug/L 5.0 1 Benzo(b)8uoranthene ND ug/L 5.0 1 Benzo(g,h,i)perylene ND ug/L 5.0 1 Benzo(k)8uoranthene NO ug/L 5.0 1 4-Bromophenylphenyl ether NO ug/L 5.0 1 Butylbenzylphthalate NO ug/L 5.0 1 4-Chloro-3-methylphenol NO ug/L 5.0 1 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 bis(2-Chloroelhyl) ether ND ug/L 5.0 1 2-Chloronaphthalene NO ug/L 5.0 1 2-Chlorophenol NO ug/L 5.0 1 4-Chlorophenylphenyl ether NO ug/L 5.0 1 116, REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9600 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, I.I.C. Page 7 of 13 aceAnalytical wwwpacelabs.can ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92438449 Sample: Outfall 002 Parameters Lab ID: 92438449002 Results Units Collected: 07/22119 13:40 Report Limit OF Chrysene ND ug/L 5.0 1 Dibenz(a,h)anthracene ND ug/L 5.0 1 3,3'-Dichlorobenzidine ND ug/L 25.0 1 2,4-Dichlorophenol ND ug/L 5.0 1 Dielhylphlhalate NO ug/L 5.0 1 2,4-Dimethylphenol ND ug/L 10.0 1 Dimethylphthalate ND ug/L 5.0 1 Di-n-butylphthalate ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 2,4-Dinitrophenol NO ug/L 50.0 1 2,4-Dinitrotoluene ND ug/L 5.0 1 2,6-Dinitrotoluene NO ug/L 5.0 1 Di-n-octylphthalate NO ug/L 5.0 1 bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 Fluoranthene NO ug/L 5.0 1 Fluorene NO ug/L 5.0 1 Hexachloro-1,3-butadiene NO ug/L 5.0 1 Hexachlorobenzene NO ug/L 5.0 1 Hexachlorocyclopentadiene NO ug/L 10.0 1 Hexachloroethane NO ug/L 5.0 1 Indeno(1,2,3-cd)pyrene NO ug/L 5.0 1 Isophorone ND ug/L 10.0 1 Naphthalene ND ug/L 5.0 1 Nitrobenzene NO ug/L 5.0 1 2-Nitrophenol ND ug/L 5.0 1 4-Nitrophenol ND ug/L 50.0 1 N-Nitrosodimethylamine NO ug/L 5.0 1 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 N-Nitrosodiphenylamine NO ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 Pentachlorophenol NO ug/L 10.0 1 Phenanthrene NO ug/L 5.0 1 Phenol ND ug/L 5.0 1 Pyrene ND ug/L 5.0 1 1,2,4-Tdchlorobenzene ND ug/L 5.0 1 2,4,6-Tnchlorophenol NO ug/L 10.0 1 Nitrobenzene-d5(S) 64 % 10-120 1 2-Fluorobiphenyl (S) 67 % 15-120 1 Terphenyl-d14 (S) 94 % 11-131 1 Phenol-d6 (S) 45 % 10-120 1 2-Fluorophenol(S) 58 % 10-120 1 2,4,6-Tdbromophenol (S) 105 % 10-137 1 Benzene ND ug/L 1.0 1 Bromodichloromethane NO ug/L 2.0 1 Bromoform NO ug/L 2.0 1 Bromomethane NO ug/L 2.0 1 Carbon tetrachloride ND ug/L 2.0 1 Chlorobenzene ND ug/L 2.0 1 Chloroethane ND ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnaVical mrwpacelabs.cont ANALYTICAL RESULTS Project: Monthly Slormwater Pace Project No.: 92438449 Sample: Outfall 002 Lab ID: 92438449002 Collected: 07/22/19 13:40 Parameters Results Units Report Limit DF Chloroform ND ug/L 5.0 1 Chloromethane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 1,2-Dichlorobenzene ND ug/L 2.0 1 1,3-Dichlorobenzene ND ug/L 2.0 1 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 1,2-Dichloroethane ND ug/L 2.0 1 1,1-Dichloroethene ND ug/L 2.0 1 cis-1,2-Dichloroethene ND ug/L 2.0 1 trans-1,2-Dichloroethene ND ug/L 2.0 1 1,2-Dichloropropane ND ug/L 2.0 1 cis-1,3-Dichloropropene ND ug/L 2.0 1 trans-1,3-Dichloropropene ND ug/L 2.0 1 Ethylbenzene ND ug/L 1.0 1 Methylene Chloride ND ug/L 5.0 1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 Tetrachloroethene ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 1,1,2-Trichloroethane ND ug/L 2.0 1 Trichloroethene ND ug/L 2.0 1 Trichlorolluoromethane ND ug/L 2.0 1 Vinyl chloride ND ug/L 2.0 1 4-BromaBuorobenzene(S) 100 % 70-130 1 Toluene-d8 (S) 99 % 70-130 1 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 Total Suspended Solids 12.2 mg/L 4.2 1 pH at 25 Degrees C 6.6 Sid. Units 1.0 1 Phenol ND mg/L 0.020 1 H3 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, -LC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, -LC. Page 9 of 13 aceAnalytical w xpecelabs.mm QUALIFIERS Project: Monthly Stormwater Pace Project No.: 92438449 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantilation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolem and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. H3 Sample was received or analysis requested beyond the recognized method holding time. SO Surrogate recovery outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/06/2019 03:09 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 aceAnalytical� Sample Condition Upon Reel t(SCUR) Page 1 of 2 Document No,: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality OK ice Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ Client Name: 2 q Project If: Courier: LJ�pd-Ex ❑UPS ❑USPS ❑Client ❑ Commercial ❑' Pace ,_,[/� ❑Other._ Custody Seal Present? []Yes ND Seals Intact? (—]Yes ON, Packing Material: ❑' Bubble wrap []Bubble Bags ❑None/. ElOther Thermometer:' Type of ice: dew t Delve ❑IRGunW Z1.r,o 8 i Cooler Temp ('C): '' Correction Factor: Add/Subtract ('C) 0.0 Cooler Temp Corrected IQ USDA Regulated II (❑ N/A, water sample) Did samples on " ate in a quarantine tone within the United Stales: CA, NY, or SC (check maps)? rlve' Nn WO#:92433449 92438449 Date/In ilia is Person Examining Contents: I'I-> '71 (//C Biological TissueeFF pien? [-] Yes ❑No LJN/A ❑None Temp ould be above freezing to 6'C mples out of temp criteria. Samples on ice, cooling process �f. hasbegun �ld�iilfl Did samples originate from a foreign source (Internal any, Including Hawaii and Puerto Rico)?FlYes 11 a Comments/DlScre anC : Chain of Custody Present? 2 Yes ONO ❑N/A 1. Samples Arrived within Hold Time? clyes EN / ❑N/A 2. Short Hold Time Analysis e72 hr.)? Yes N N/A 3. Rush Turn Around Tlme Requested? ❑Yes No ❑N/A 4. SuRident Volume? EK' No N/A S. Correct Containers Used? -Pace Containers Used] YP' ONO No ❑N/A N A 6. Containers Intact? Yes ONO N/A 7. Dissolved analysis: Samples Field Filtered? ❑vei ON. ! N/A S. Sample Labels Match CDC? -Includes Date/Time/ID/analysis Matrix: Yes illy ON. ❑N/A 9. Headspace in VDA Vials(>S-6mm)? dles ❑ ❑N/A 10. Trip Blank Present? TO p Blank Custody Seals Prose nt? ❑Yes Yes ONO No ❑N/ N/A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESDLUTIDN Person contacted: Project Manager SCURF Review: Project Manager SRF Review: tr Oate/Tlme: Field Data Required? ❑Yes [-]NO Date: I Date: (2-1 I Pagel 1 of 13 Document Name: Document Revised: February 7, 2018 aceAnalytieal x Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rey.06 Pace Carolinas Quality Office "Check mark top half of box if pH and/or dechlarinatien is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project # WO# : 92438449 PM: MWB Due Date: 08/07/19 CLIENT: 92-0KN m _ .1".. \ Z c E n a z o of i'in n m a z a o a. m a a " n m n n JI n m _ O Z n c a m z' n n N a m o E u m a u n n 0 E 4 3 _ ¢ n ¢ _ ti L7 a - ¢ _ la a — z c = E a c m a 01 i ,A a Ji N E a of N ¢ z E E a n m T l7 �¢ Z a E q i3n a O E 4 T > 2. a O E Y P > O E 4 m ii N ¢ a ° < n 3 Y to � n N E N H y N E N N N m x a E x5 `m c a E o a - E tp > a ` E m o /� la 2 i I Z u N 3 \N+ 6 fi 7 R 9 11 k1210 pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon mcelpl Date preservation adjusted Time p reservalian adjusted Amount of Preservative added Lot No[e: vvnenever mere is a mscrepaney affecting Norin t.araima compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 12 of 13 /12AW -1 CHAIN -OF -CUSTODY I Analytical Request Document ------^• The Chain-Df-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Sec ,on A e—lnn R cc or, Required Client Information: Required Project Information: Invoice Iniarmatian: l PDge Company. GKN Drivehno. Alamance Robert To: Ricky Hiatt Attention: Address: 1067 Trolln wood HoWrelds Rd Copy To: Company Name. Mebane. NC 22302 Address: Email, ry� ,A/W eti„y�,yer. Purchase Order#: Pace Olpte: _ f. Re Mato A enc Ph..: 1919)215-1066 Fax x Ponied m Naa: Mmihly Stormwater Pace Ponieo Manager,Rd pacelabz.rom, State I L«ation Requested Due Date: Project #: Pace Profile #: 4SN-5 _ . NC - -Rc u<stetl Anal sls Filtered _ A Z .or. coos COLLECTED Preservatives - awry wa vw o U pine s Walern wx Pimw P - GV p w SAMPLE ID sx. SL 3 dre START END F One Character per boa. C a1. q (A-Z, 0.91. Sample Ids must be unique In— 1a � TOATeTIMS zO 2 m0 - is Lj ti 9W ~ rei f W O i V O L LQ. DATE TIME o z z i i f o n r f o m m m `a I,�Lj tlFL. L, ' 1 Oudali 001 �LL I yU J / iz 1:20 l t y�q x x x x x x x x Cu, Pb, Zn (dQ i z o�dan 002 ��u � :. wr % X % X % % X x Cu. Pb. Zn 3 _ 4 6 6 7 . 8 9 0 lit 32 " p ADDITIONAL COMMENTS. RELINOUISHEDGYIAFFIWT0N .GATE TIME - :gt EPTEDBYIAFFlLIATgxI DATE 11ME SAMPLECONOmONS SAMPLER NAME AND,SIGNAT_URE PRINT Name of SAMPLER Trr tD _ - m _ E �+ i SIGNATDRE of SAMPLER: V �— DATE Signed: Z y