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HomeMy WebLinkAboutNCG030027_COMPLETE FILE - HISTORICAL_20160126STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV CIS 6 3 n o a� DOC TYPE HISTORICAL FILE ❑ MONITORING REPORTS DOC DATE ❑ J b 1�(2 I a YYYYM M D D E:i•N .(ji;YEMIg&IILW%tbt/ti'AL'2 December 18, 2015 Eaton Corporation Attn: AP Process Support Analyst NoM American Financial Services Center 2000 Apollo Drive Brook Park, OH 44142 Faa: 216-416-2604 Email: ProcessSupport@Eaton.com NORTH CAROLINA DEPARTMENT OF ENVIROMENTAL & NATURAL RESOURCES NCDENR ATTN STORMWATER BILLING DIV ENERGY MINERAL & LAND RESOURCES 1612 MAIL SERVICE CENTER RALEIGH NC 27699 Dear Sir or Madam: E Our records indicate -that the-fellowing check(s)-was issued to.you and, as of -today, it -,has not -been cashed. -- Nature of Funds: Check #2101122909 Date Issued: 3/19/2015 Amount: $100.00 USD Invoice Number(s): MVSS1275016REENTRY Description or Reference: PERMIT NCG030027 - INVOICE 2015PR000205 If you have an interest in these funds and wish to prevent such funds from being reported as Unclaimed Property and remitted to the state of NC, please indicate the disposition of these items on the bottom of this form. After you have completed this form, please return the signed form immediately either by fax to number 216-416-2604 or email to ProcessSupport@Eaton.com. If you don't have access to a fax machine or scanner, please return a signed copy of this letter by mail to the address above. Disposition of Outstanding Items ❑ The above check(s) was cashed. ❑ Check(s) was received, but not cashed. (If you still have the check(s) please return the check(s) along with this letter indicating if you are still entitled to this money). ❑ Check(s) is no longer required. There are no outstanding invoices for this amount and the / obligation has been satisfied. /``K�,J• This checks) was not received and our records indicate the amount is still due. Please issue a -- - repleeement-cheek------- ❑ Other Signature: Print Name: fi%(.-WkV ft tt 7 uLA ^ 1-" Address (if different �f7r(}om above). Title: f iMdlll� Phone:t o SSN%Federal ID No. Date: Your assistance is greatly appreciated. Please respond no later than 311812015. Sincerely, ease yna,�e � io�ce °r Accounts Payable Process Support Analyst Eaton - N.A. Financial Services Center T - 1 ✓`"'— Y /1 ! Yliw A NCDENR North Carolina Department of Environment and Natural Resources Division of Energy, Mineral, and Land Resources Land Quality Section Tracy E. Davis, PE, CPM Pat McCrory, Governor Director John E. Skvarla, III, Secretary March 10,:2014 Glenn McLean Eaton Corporation - - 2564 Durham Road Roxboro, NC 27573 Subject: General Permit No. NCG030000 Eaton Corporation - Roxboro Facility COC NCG030027 Person County Dear Mr. McLean: In accordance with your application for a stormwater discharge permit received on February 11, 2014 we are forwarding herewith the modified certificate of coverage to discharge under the subject state NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1, the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended) and in accordance with the November 14, 2013 Settlement Agreement between Eaton Corporation and NCDENR. This permit modification clarifies that the permit covers all stormwater discharges from industrial activities at the facility, including the discharges from your onsite stormwater retention pond. The engineer's statement included with your recent application has certified that work has been completed to change onsite stormwater drainage to assure that impacted groundwater is no longer infiltrating into the storm drain system. You should note that this permit is for stormwater discharges only and any wastewaters from your site, now or in the future, would need to be addressed by permit coverage through the NC Division of Water Resources (DWR). It is our understanding of the November 14, 2013 Settlement Agreement that adherence to the conditions of the agreement and issuance of this stormwater permit supersedes previous permit coverage, including NC0003379. This approval letter is copied to staff of DWR so they can address any necessary final procedures for rescission of their permit coverage. 1612 Mail Service Center, Raleigh, North Carolina 27699.1612 • Telephone 919-707-9220 / FAX: 919-733-2876 512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://ponal.ncdenr.org/web/[rAand-ouality An Equal Opportunity 1 Affirmative Action Employer - 50%Recycled 110% Post Consumer Paper Glenn McLean C NCG030027 March 10, 2014 Page 2 of 2 Please take note that this certificate of coverage is not transferable except after notice to the Division of Energy, Mineral and Land Resources (DEMLR). The Division may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DEMLR or permits required by the Division of Water Resources, or any other federal, state or local governmental permit that may be required. If you have any questions concerning this permit, please contact Bradley Bennett at - telephone number (919) 807-6378 -Sincerely, for Tracy E. Davis, P.E., CPM cc: Raleigh Regional Office, John Holley Central Files Stormwater Permitting Unit Files Tom Belnick - DWR - NPDES Wastewater Carolyn McLain - NCDOJ Jimmy Kirkland - Womble Carlyle Sandridge & Rice, LLP 1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone 919-707-92201 FAX: 919-733-2876 512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http //portal nodenr ora/web/lrfand-guality An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No NCG030027 STORMWATER DISCHARGES -NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance`with the provision of North Carolina General Statute 143-215.1, other lawful standards and`regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Eaton Corporation is hereby authorized to discharge stormwater from a facility located at Eaton Corporation - Roxboro Facility 2564 Durham Road Roxboro Person County to receiving waters designated as UT to North Flat River, a class WS-111, NSW water in the Neuse River Basin, in accordance with the effluent limitations; monitoring requirements, and other conditions set forth in Parts 1,11, III, IV, V, and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective March 10, 2014. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day March 10, 2014. for Tracy E. bavis, P.E., Director Division of Energy, Mineral, and Land Resources By the Authority of the Environmental Management Commission LOCATION MAP: USGS Map: Timberlake Latitude: 36°21'31" N NCG030027 Facility W Longitude: 78°59'04" W County: Person Eaton Corporation — Roxboro Location Stream Class: WS-III, NSW Receiving Stream: UT to North Flat River Sub -basin: 03-04-01 (Neuse River Basin) [)VOttli Not to Scale LEGGETTE, BRASHEARS & GRAHAM, INC. Professional Groundwater and Environmental Consultants 104 Mill Street, Suite I Gahanna, Ohio 43230 (614)416-9100 ((i l4) 416-9101 — Pax v@9T 09 February 7, 2014 F EB 14 2014 Mr. Bradley Bennett DENR.WAT `. W E gFANC1 Supervisor, Stormwater Permitting Program WETLANDS AND STORt North Carolina Division of Energy, Mineral and Land Resources 1612 Mail Service Center Raleigh, North Carolina 27699-1612 Subject: Settlement Agreement Submissions Eaton Corporation Roxboro Facility — 2564 Durham Road, Person County, NC Dear Mr. Bennett: In accordance with the November 14, 2013 Settlement Agreement, I am submitting the following documents on behalf of Eaton Corporation: • Engineer's Statement of Completion of the Storm Sewer Work • Notice of Intent for NCG030000 for coverage of the entire facility and a check for $100.00 • Stormwater Pollution Prevention Plan that incorporates discharges from the stormwater retention pond. It is Eaton's understanding that a Certificate of Coverage under NPDES General Permit NCG030000 will be issued which includes discharges from the stormwater retention pond. Additionally, we understand that the Certificate of Coverage will supersede all previously issued NPDES permits including individual NPDES Permit No. NC0003379. In accordance with Paragraph E. of the Settlement Agreement, please provide three days prior notice of the issuance of the Certificate of Coverage to StevenFesko@Eaton.com with a copy to JKirkland@wcsr.com. If you have any questions regarding this submittal, please contact me at (614) 416-9100 or jtschick@lbgcmh.com. cc: Connecticut New Jersey Sincerely, LEGGETTE, BRASHEARS & GRAHAM, INC. Vl_ Jeffrey T. Schick Eaton Project Coordinator Mr. Steve Fesko — Eaton Corporation Mr. Glenn McLean — Eaton Corporation Mr. Jimmy Kirkland — Womble,Carlyle Sandridge & Rice, LLP Florida Georgia Illinois Michigan New York Ohio Pennsylvania South Dakota Z014 DENR-WATCRCDALLTY WETLANDS ANDSTORIL77 ATERgtyCN Minnesota Missouri North Dakota Texas Vermont Wisconsin Division of Water Quality / Surface Water Protection Section i� NC®ENR National Pollutant Discharge Elimination System Np CM — CEP4rtMEM W EMnROxMCi? /YD NrtUR4 RE-AMCES NCG030000 NOTICE OF INTENT FOR AGENCY USE ONLY Date Received Year Month Day Certificate ofCovera e N 3 Check H Arnowt Permit Assigrtcd to National Pollutant Discharge Elimination System application for coverage under General Permit NCG030000: STORMWATER DISCHARGES associated with activities classified as: SIC (Standard Industrial Classification) 335 Rolling, Drawing, and Extruding of Nonferrous Metal c� tir.t SIC 3398 Metal Heat Treating SIC 34 Fabricated Metal Products ►u)� 1 SIC 35 Industrial and Commercial Machinery IUn\U 1 ?014 SIC 36 Electronic and Other Electrical Equipment FEB SIC 37 Transportation Equipment DEWWAT`RppERBpµ SIC 38 Measuring, Analyzing, and Controlling Instruments WETL*pSAND STOk �E,l For questions, please contact the DWQ Regional Office for your area. See page 4. (Please print or type) 1) Mailing address of ownerloperator (address to which all permit correspondence will be mailed): Name EATON CORPORATION Street Address 2564 DURHAM ROAD City ROXBORO State NC ZIP Code 27573 Telephone No. (336) 503-6538 Fax: 2) Location of facility producing discharge: Facility Name EATON CORPORATION Facility Contact KIM WITKOWSKI Street Address 2564 DURHAM ROAD City ROXBORO State NC ZIP Code 27573 County PERSON Telephone No. (336) 503-6538 Fax: Email KIM BERLYWITKOWSKI@EATON.COM 3) Physical Location Information: Please provide a narrative description of how to get to the facility (use street names, state road numbers, and distance and direction from a roadway intersection). THE EATON ROXBORO FACILITY IS LOCATED AT INTERSECTION OF DURHAM ROAD (US HIGHWAY 501) AND INDUSTRIAL DRIVE. (A copy of a county map or USGS quad sheet with the facility clearly located must be submitted with this application.) 4) Latitude 36021' 31" N Longitude 78059' 4" W (deg, min, sec) Page 1 of 4 S W U-218-071408 Last revised 7/14/08 NCG030000 N.O.I. 5) This NPDES Permit Application appliesto which of the following: ❑ New or Proposed Facility Date operation is to begin X Existing 6) Standard Industrial Classification: Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial activity at this facility. SIC Code: 3714 7) Provide a.brief narrative description of the types of industrial activities and products manufactured at this facility: THE EATON ROXBORO FACILITY IS PRIMARILY ENGAGED IN THE MANUFACTURE OF MOTOR VEHICLE PARTS. 8) Discharge points / Receiving waters: How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? 3 What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater discharges, end up in? UNNAMED TRIBUTARY TO THE NORTH FLAT RIVER IN NUESE RIVER BASIN Receiving water classification: WS-III NSW Is this a 303(d) listed stream? NO Has a TMDL been approved for this watershed? NO If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm sewer system (e.g. City of Raleigh municipal storm sewer). 9) Does this facility have any other NPDES permits? ❑ No X Yes If yes, list the permit numbers for all current NPDES permits for this facility: NC0003379 10) Does this facility have any Non -Discharge permits (ex: recycle permit)? X No ❑ Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility: _ 11) Does this facility employ any best management practices for stormwater control? ❑ No X Yes (Show any structural BMPs on the site diagram.) If yes, please briefly describe: A STORMWATER RETENTION POND WAS INSTALLED 12) Does this facility have a Stormwater Pollution Prevention Plan? ❑ No X Yes If yes, when was it implemented? JANUARY 1, 2014 13) Are vehicle maintenance activities occurring at this facility? X No ❑ Yes 14) Hazardous Waste: a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? X No ❑ Yes Page 2 of 4 SWU-218-071408 Last revised 7/14/08 NCG030000 N.O.I. b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of hazardous waste? X No ❑ Yes c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? X No ❑ Yes d) Is hazardous waste stored in the 100-year flood plain? X No ❑ Yes If yes, include information to demonstrate protection from flooding. e) If you answered yes to questions b. or c., please provide the following information: Type(s) of waste: How is material stored: Where is material stored: How many disposal shipments per year: Name of transport / disposal vendor: Vendor address: 15) Certification: North Carolina General Statute 143-215.6B (i) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request coverage under the referenced General Permit. I understand that coverage under this permit will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an individual permit. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and /accurate. Printed Name of Pers—on Siing: GI erm Title: CYn ero,IY7 'yG r/ (Signature of Applicant) 5-F�6 001V (Date Signed) This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to: NCDENR Page 3 of 4 SWU-218-071408 Last revised 7114/08 NCG030000 N.O.I. Final Checklist This application will be returned as incomplete unless all of the following items have been included: X Check for $100 made payable to NCDENR. X This completed application and all supporting documents. X A site diagram showing, at a minimum, (existing or proposed): (a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materials are stored, (f) impervious areas, (g) site property lines. X Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map. Mail the entire package to: Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Note The submission of this document does not guarantee coverage under the General Permit. For questions, please contact the DWQ Regional Office for your area. DWQ Regional Office Contact Information: Asheville Office ...:.. (828) 296-4500 Fayetteville Office,... (910) 433-3300 Mooresville Office... (704) 663-1699 --Raleigh Office ....:... (919) 791-4200 Washington Office ...(252) 946-6481 - - Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central'Office .........(919) 807-6300 Page 4 of 4 SWU-218-071408 Last revised 7114/08 LEGEND -'- APPROXIMATE PROPERTY LINE STORM SEWER STORMWATER DRAINAGE SWALE ASTORM WATER OUTFALL ®POTENTIAL STORMWATER POLLUTANT AREA DIRECTION OF SURFACE WATER ROW ---DRAINAGE AREA (APPROX.) � TREE LINE © GENERATOR © CHILLER UNIT O TRASH DUMPSTERS OTRANSFORMER NW HAZARDOUS WASTE STORAGE uan r -� �Ro ' ORS i _ (lam ;. ' i' o l� �% � !'- "-,j v /t '✓' r r\' r_./i f/--J ! ( r;�, \ � •t i�..i~�i:: M1"Z jJ rIa `j I {l fl// J TankSite Jass r ` ,.I �" ASll r, /! I `-� } -( t.• •.. ' .i; �.� H1Jif'_- Y� L.� .:•, Ladd .. ,{ er /� � ''� �~ ,\IS �� ! _ems _ ��~• D. ' 1 ~ �^rr J��.(�� _ ttw ! `—!•_-'-�ti r. .� r �' I•�^ til> �, �� C � �_( 1. ' '�.1 ` J � ,' U !u FIGURE 2 - SITE EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC TOPOGRAPHICAL MAP AND ONE 625 HUNTSMAN COURT MILE RADIUS GASTONIA, NC 28054 853-08000 N (704) Excel Project No. 28091 Source: USGS N3615 — W7852 Timberlake NC, 1981 ENGINEER'S STATEMENT OF COMPLETION Lm_ineer's statement of Completion I hereby coil, that I have deigned and supen isal the follm img NNork which was completsl at the Eatcm Corporetiun facility. 2564 Durham Road. Roxboro. North Carolina: replacement of norm savers and catch basins with welded hi_h-dcnsit polyethylene piping in the buck scale and truck dock area. 8y: Michael J. Lyc n, P.:. Principal Civil Engineer The Kelly -Buck Company 1048 Literary Road Cleveland, OH 44113 NC Engineering Firm UC-2692 Date �o'o� SSd-4/V SEAL 028510 ctigEL .J. Ly STATE OF NORTH CAROLINA COUNTY OF PERSON Eaton Corporation Petitioner, V. NC Dept. of Environment and Natural Resources, Division of Water Resources, Respondent. IN THE OFFICE OF ADMINISTRATIVE HEARINGS 13 EHR 16402 Settlement Agreement The North Carolina Department of Environment and Natural Resources ("DENR"), through its Division of Water Resources (the "Respondent") and Eaton Corporation ("Petitioner") hereby enter into this Settlement Agreement pursuant to N.C. Gen. Stat. § 150E- 3l(b) in order to amicably resolve matters in controversy between them. This matter arose out of the Petitioners filing a Petition for Contested Case Hearing (13 EHR 16402) on August 19, 2013, challenging the Respondent's July 12, 2013 issuance of National Pollutant Discharge Elimination System ("NPDES") permit No. NC0003379 to Petitioner. Without any trial of fact or law in a contested case hearing, and without any admissions of liability, the Respondent and Petitioner have reached the following agreement: A. In order to avoid the cost and delay of litigation, Petitioner and Respondent have entered into this Agreement and have agreed that all parties have been correctly designated and that there is no question as to misjoinder or nonjoinder. B. The stormwater from certain areas of the facility discharge to the stormwater retention pond which discharges under individual NPDES permit No. NC0003379. Petitioner has determined that impacted groundwater is apparently infiltrating into the storm sewer in the area of the truck scale and truck dock in the northeast part of the site. To prevent this impacted groundwater infiltration into the storm sewer, the Parties hereto agree that Petitioner will retain a civil engineering firm to design and supervise the replacement of the storm sewer and catch basins with welded high -density polyethylene piping in the truck scale and truck dock area of the site (the "Storm Sewer Work"). Petitioner shall complete the Storm Sewer Work by February 14, 2014. Petitioner will submit an engineer's statement of completion to Respondent no later than 10 business days following completion of the Storm Sewer Work. C. The Parties recognize that the water being discharged under NPDES permit No. NC0003379 is primarily stormwater and once the Storm Sewer Work is completed, that coverage under General Permit NCG030000 is more appropriate for this discharge from the stormwater retention pond. Respondent agrees to rescind the July 12, 2013 NPDES permit NC0003379 upon execution of this Settlement Agreement. Upon rescission of NPDES Permit No. NC0003379, Petitioner would continue to operate under the expired April 1, 2008 NPDES permit which shall remain in effect, except as described in Paragraph E below, until completion of the Storm Sewer Work and issuance of a certificate of coverage under the General Permit NCG030000. t+w` Cmftr LL,4r Mc-&036(5.7 1 D. Petitioner will submit at the same time as submittal of the engineer's statement of completion a revised Notice of Intent ("NOI") form for coverage under NPDES General Permit NCG030000. Included with this submittal will be an updated Stonnwater Pollution Prevention Plan ("SPPP") to account for the changes made at the site. -2- E. Upon receipt of the engineer's statement of completion documentation, updated SPPP and NOI, Respondent will issue a Certificate of Coverage ("Certificate of Coverage") for coverage under NPDES General Permit NCG030000 to include discharges from the stormwater retention pond (the "Coverage Letter"). The Certificate of Coverage will indicate that it supersedes all previously issued NPDES permits, including NPDES Permit No. NC0003379. Respondent will provide Petitioner at least three business days prior notice of the issuance of the Certificate of Coverage by email to: SteveFesko@Eaton.com with a copy to JKirkland@wcsr.com. F. Beginning on the effective date of this Settlement Agreement and continuing until a Certificate of Coverage under NCG030000 is issued, Petitioner will continue to comply with the expired April 1, 2008 individual NPDES permit No. NC0003379, including the monthly collection of samples, continuous measurement of flow and submittal of Discharge Monitoring Reports. The permit conditions will be in effect with the exception of the monthly average flow limit contained in permit Section A. (1). G. Within ten days of the full execution of this Settlement Agreement, Petitioner shall file with the Office of Administrative Hearings a Notice of Voluntary Dismissal With Prejudice of this Contested Case, Eaton Corporation v. NC Department of Environment and Natural Resources, Division of Water Quality, 13 EHR 16402 (the "Contested Case"), with each Party to bear its own costs and attorney's fees. H. The Parties agree to cooperate fully in executing any and all supplementary documents and in taking all additional actions that may be necessary to give full force and effect to the terms of this Settlement Agreement. 3 I. Petitioner expressly stipulates and acknowledges that, by entering into this Settlement Agreement, on behalf of itself, its successors and assigns, and any person or entity claiming through them, it settles and releases Respondent from any and all claims, demands, actions or causes of action that were raised or could have been raised or asserted in this Contested Case concerning the challenge to the July 12, 2013 NPDES Permit NC0003379. Petitioner specifically does not release or otherwise waive any claims, actions, rights, or challenges with respect to the expired April 1, 2008 NPDES Permit, any future individual NPDES permits issued to Petitioner, the Coverage Letter, or enforcement of the terms of this Settlement Agreement. J. It is understood and agreed that this settlement is not to be construed as an admission of liability on the part of the Panics and that this settlement is a compromise of a disputed claim. None of the foregoing agreements, statements and actions by the Parties shall be deemed an admission. K. This Settlement Agreement constitutes the entire agreement between the Parties pertaining to the subject matter contained herein. The invalidity or unenforecability of any particular provision of this Settlement Agreement shall not affect the other provisions herein, and this Settlement Agreement shall be construed in all respects as if such invalid or unenforceable provisions were omitted. 11. The Parties represent that all necessary corporate and governmental formalities have been complied with for purposes of them signing and entering into this Settlement Agreement. M. This Settlement Agreement may be executed in separate counterparts and together shall constitute one agreement. M N. This Settlement Agreement shall be binding upon the Parties and their successors and assigns and shall inure to the benefit of each Party's successes and assigns. O. Petitioner and Respondent agree that, for purposes of any future bankruptcy proceeding, this Agreement is not intended as, nor shall it be deemed to constitute, a novation of any claims asserted by the Respondent pursuant to this Agreement are nondischargeable in bankruptcy under I U.S.C. § 523. Nothing in this Agreement releases any nondischargeability claims that may be asserted by the Respondent in any bankruptcy proceeding, and nothing in this Agreement shall be deemed a waiver of the Respondent's right to rely on the nature of any claim or debt released in this Agreement to show that the claim or debt is nondischargeable. �>t This the 14 day of November, 2013. Eaton Corporation By:-Stf�en Gle/tr7 Its: nl a n-t- Aai�' ,z �tr Division of Water Resources, NC Department Of Environment nd Natural Resources By: Its: jpf r(- , �la5re v✓d7Lo Q�an� Stiperv,s�T -5- currmk} Uvr4 Vt�,br NC6,030oal _ dvl(cw ,hva;« -0 9 0013PR000a88 2/1/)3 - 101t-I A'100 Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Tuesday, February 25, 2014 11:22 AM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission I wouldn't worry too much about the fee question. I spoke with the attorney about the fee and he was totally OK with using the fee for the other outstanding fees. This looks good to me. Minor edits in the last paragraph: remove the period from the beginning of the first sentence and did you mean to write "notice" or "note" in that first sentence? Thanks! Carolyn From: Bennett, Bradley [mailto:brad ley. bennett(c ncdenr.gov] Sent: Tuesday, February 25, 2014 10:58 AM To: McLain, Carolyn Subject: FW: Eaton Corporation Roxboro Submission Carolyn, Still haven't received confirmation from them on the fee question in my email, but I have drafted the modification letter. Can you please take a look and see if you think this is okay. Thanks M Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradley.bennett(a)ncdencgov Raleigh, NC 27699-1612 Web: http://portal.ncdenr.org/web/ir/stormwater Email correspondence to and from this address may be subject to public records laws From: Jeff Schick fmaiIto: itschick0lbecmh.com] Sent: Friday, February 21, 2014 4:42 PM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission Received ok. Thanks. From: Bennett, Bradley [mailto: brad ley. ben nett(ancdenr.00v] Sent: Friday, February 21, 2014 4:41 PM To: jtschick(allbecmh.com Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: RE: Eaton Corporation Roxboro Submission Mr. Schick, Second try. Sorry I got the email wrong the first time. Gil Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradlev.bennettla)ncdenr.00v Raleigh, NC 27699-1612 Web: hUo://Portal.ncdenr.org/web/Ir/stormwater Email correspondence to and from this address may be subject to public records laws From: Bennett, Bradley Sent: Friday, February 21, 2014 2:52 PM To: 'jtschick@lbgmh.com' Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Serge! Subject: Eaton Corporation Roxboro Submission Mr. Schick, I just wanted to touch base with you concerning our discussion today on the submittal. As we discussed, the Stormwater Program will not be issuing a new permit coverage for the Roxboro facility. We will be sending a letter that essentially reissues the existing coverage and clarifies that it includes the discharge from the sites stormwater pond now that work from the settlement agreement has been completed to exclude the impacted groundwater from entering the storm sewer. We will also work with the NPDES Wastewater Staff in DWR to assure that coverage under NC0003379 is rescinded. , In addition, as we discussed, the Eaton facility stormwater permit— NCG030027 — currently has an outstanding annual fee of $100 for the time period feb 2013-Jan 2014. The $100 fee submitted with the N01 package will be applied to this overdue annual fee.. Please confirm that this is appropriate. I have attached the invoice for this annual fee. If there are any changes needed in the contact information for this please let me know. m Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradley.bennettancdenr.00v Raleigh, NC 27699-1612 Web: http://oortal.nedenr.org/web/Ir/stormwater Email correspondence to and from this address may be subject to public records laws Bennett, Bradley From: Jeff Schick [jtschick@lbecmh.com] Sent: Friday, February 21, 2014 4:42 PM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission Received ok. Thanks. From: Bennett, Bradley[mailto:bradley.bennett(abncdenr.00v] Sent: Friday, February 21, 2014 4:41 PM To: itschick(a)lbecmh.com Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: RE: Eaton Corporation Roxboro Submission Mr. Schick, Second try. Sorry I got the email wrong the first time. m Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Faz: (919) 807-6494 1612 Mail Service Center Email: bradlev.bennett aMcdenr.00v Raleigh, NC 27699-1612 Web: httoaloortal.ncdenr.orc/web/Ir/stormwater Email correspondence to and from this address may be subject to public records laws From: Bennett, Bradley Sent: Friday, February 21, 2014 2:52 PM To: 'jtschick@lbgmh.com' Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: Eaton Corporation Roxboro Submission Mr. Schick, I just wanted to touch base with you concerning our discussion today on the submittal. As we discussed, the Stormwater Program will not be issuing a new permit coverage for the Roxboro facility. We will be sending a letter that essentially reissues the existing coverage and clarifies that it includes the discharge from the sites stormwater pond now that work from the settlement agreement has been completed to exclude the impacted groundwater from entering the storm sewer. We will also work with the NPDES Wastewater Staff in DWR to assure that coverage under NC0003379 is rescinded. In addition, as we discussed, the Eaton facility stormwater permit — NCG030027 — currently has an outstanding annual fee of $100 for the time period feb 2013-Jan 2014. The $100 fee submitted with the N01 package will be applied to this overdue annual fee. Please confirm that this is appropriate. I have attached the invoice for this annual fee. If there are any changes needed in the contact information for this please let me know. W Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradlev.bennettPncdenr.00v Raleigh, NC 27699-1612 Web: http://portal.ncdenr.orclweb/Ir/stormwater Email correspondence to and from this address may be subject to public records laws F Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Tuesday, February 11, 2014 1:14 PM To: Bennett, Bradley Subject: RE: Eaton - Roxboro - Settlement Agreement Attachments: FullyExec_11-14-13 Eaton Settlement.pdf Great. See attached for the agreement in full. Let me know if you have questions. I can walk you through the particulars, if you need. Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclain@ncdoj.gov IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email maybe subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Bennett, Bradley [mailto:bradley.bennett@ncdenr.gov] Sent: Tuesday, February 11; 2014 1:12 PM To: McLain, Carolyn Subject: RE: Eaton - Roxboro - Settlement Agreement Carolyn, Got the package today. If the agreement isn't too long, could your forward a copy to me? Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradley.bennett(a ncdenr.gov Raleigh, NC 27699-1612 Web: htto:/Iportal.ncdenr,org/web/Ir/stormwater Email correspondence to and from this address may be subject to public records laws From: McLain, Carolyn [mailto:CMcLain(@ncdoj.gov] Sent: Monday, February 03, 2014 10:44 AM To: Bennett, Bradley Subject: FW: Eaton - Roxboro - Settlement Agreement 1 Hi Bradley— I hope you are doing well. I don't know if you recall this case (initially Tom BeInick and Serge C.) but Eaton is now in the phase where they need to work with you a bit, I think. They were operating under individual NPDES permit but now only need coverage under existing/modified General SW permit. Sergei tells me that all of this needs to be sent to you but I just wanted to confirm with you and also give you a heads up that this is coming your way. Also — can you please include the best address to send this to? ' I'm happy to discuss further if you need. Appreciate your help in this matter. Thank you, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclaina.ncdoi.00v IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to -10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Kirkland, Jimmy [mailto:JKirkland(d)wcsr com] Sent: Monday, February 03, 2014 10:18 AM To: McLain, Carolyn Subject: Eaton - Roxboro - Settlement Agreement Carolyn, 1 hope you are doing well. Eaton is ready to make the notifications required under the Settlement Agreement. Under the terms of the agreement Eaton is required to submit the following; • Storm Water Work Statement of Completion • Stormwater Notice of Intent • Stormwater Pollution Prevention Plan Who should these be submitted to? The Stormwater N01 has instructions for mailing but we want to determine if it should be mailed differently. Also, do you want them all mailed at the same time or can they be submitted separately? Thanks, Jimmy Jimmy Kirkland Womble Carlyle Sandridge & Rice, LLP 271 17th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax 8""v.wcsr.com IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements imposed by the IRS, we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matleraddressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential, privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it. or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission, There is no intent on the part of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. Bennett, Bradley From: McLain, Carolyn (CMcLain@ncdoj.gov] Sent: Monday, February 10, 2014 10:04 AM To: Bennett, Bradley Subject: FW: Eaton Roxboro Settlement Agreement Submittals Hey Bradley — hope you're doing well. See attached. It looks like all of the appropriate materials are headed your way. I removed the attachments since they were 6 MB and you'll be receiving the hardcopies. Please let me know if/when you would like to chat about this project. I'm more than happy to fill you in on the details but I also don't want to waste your time if you feel you've got sufficient information for this project. I'm pretty open this week, so let me know. Thanks again, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone - (919) 716-6766 Fax cmclain(ancdoi.00v IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. 4 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919).716-6600.:. From: Kirkland, Jimmy [mailto:JKirkland(a)wcsr.com) Sent: Friday, February 07, 2014 4:03 PM To: McLain, Carolyn Subject: Eaton Roxboro Settlement Agreement Submittals Carolyn, Earlier today the submittals required pursuant to the Settlement Agreement were mailed to Bradley Bennett. Copies of the submittals are attached. We look forward to receiving the Certificate of Coverage for the facility. If you have any questions, please let me know. Regards, Jimmy Jimmy Kirldand Womble Carlyle Sandridge & Rice, LLP 271 17th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax www.wcsr.conn IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements imposed by the IRS, we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matter addressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential, privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message. any part of it, or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the part of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Monday, February 03, 2014 10:44 AM To: Bennett, Bradley Subject: FW: Eaton - Roxboro - Settlement Agreement Hi Bradley — I hope you are doing well. I don't know if you recall this case (initially Tom Belnick and Sergei C.) but Eaton is now in the phase where they need to work with you a bit, I think. They were operating under individual NPDES permit but now only need coverage under existing/modified General SW permit. Sergei tells me that all of this needs to be sent to you but I just wanted to confirm with you and also give you a heads up that this is coming your way. Also — can you please include the best address to send this to? I'm happy to discuss further if you need. Appreciate your help in this matter. Thank you, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclain(d).ncdoi.00v IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Kirkland, Jimmy [mailto:JKirkland(cbwcsr.com] Sent: Monday, February 03, 2014 10:18 AM To: McLain, Carolyn Subject; Eaton - Roxboro - Settlement Agreement Carolyn, I hope you are doing well. Eaton is ready to make the notifications required under the Settlement Agreement. Under the terms of the agreement Eaton is required to submit the following; Storm Water Work Statement of Completion Stormwater Notice of Intent Stormwater Pollution Prevention Plan Who should these be submitted to? The Stormwater NOI has instructions for mailing but we want to determine if it should be mailed differently. Also, do you want them all mailed at the same time or can they be submitted separately? Thanks, Jimmy Jimmy Kirkland Womble Carlyle Sandridge & Rice, LLP 27117th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements imposed by the IRS, we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used. and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matter addressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential. privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it, or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the part of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. Permit Number NCG030027 Program Category NPDES SW Permit Type Metal Fabrication Stormwater Discharge CDC Primary Reviewer bradley.bennett Coastal SWRule Permitted Flow 0 Facility RECEIVED MAR 10 Z014 CEDW !Q!Q BOGES Central Files: APS _ SWP _ 3/10/2014 Permit Tracking Slip Status Project Type Active Minor modification Version Permit Classification 4.10 COC Permit Contact Affiliation Facility Name Major/Minor Region Roxboro plant - Minor Raleigh Location Address County 2564 Durham Rd Person Roxboro NC 27573 Facility Contact Affiliation Brian J. Phillips PO Box 241 Owner Roxboro NC 27573 Owner Name Owner Type Eaton Corporation Non -Government Owner Affiliation Pathrico J. McClain 744 S Battleground Ave Dates/Events Kings Mtn NC 28086 Scheduled Ong Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration 4/16/1993 2/11/2014 3/10/2014 3/10/2014 10/31/2017 Regulated Activities Requested /Received Events Electronic equipment manufacture RO staff report received Industrial and commercial machinery manu RO staff report requested Measuring and analyzing instruments manu Additional information requested 2/12114 Metal products manufacture Additional information received 2/21114 Rolling, drawing, and extruding of nonfe Transportation equipment manufacture Vehicle maintenance Outfall 001 Waterbody Name Streamindex Number Current Class Subbasin North Flat River 27-3-2 WS-III;NSW 03-04-01 r NCDENR North Carolina Department of Environment and Natural Resources Division of Energy, Mineral, and Land Resources Land Quality Section Tracy E. Davis, PE, CPM Pat McCrory, Governor Director John E. Skvarla, III, Secretary March 10, 2014 Glenn McLean Eaton Corporation 2564 Durham Road Roxboro, NC 27573 Subject: General Permit No. NCG030000 Eaton Corporation - Roxboro Facility COC NCG030027 Person County Dear Mr. McLean: In accordance with your application for a stormwater discharge permit received on February 11, 2014 we are forwarding herewith the modified certificate of coverage to discharge under the subject state NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1, the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended) and in accordance with the November 14, 2013 Settlement Agreement between Eaton Corporation and NCDENR. This permit modification clarifies that the permit covers all stormwater discharges from industrial activities at the facility, including the discharges from your onsite stormwater retention pond. The engineer's statement included with your recent application has certified that work has been completed to change onsite stormwater drainage to assure that impacted groundwater is no longer infiltrating into the storm drain system. You should note that this permit is for stormwater discharges only and any wastewaters from your site, now or in the future, would need to be addressed by permit coverage through the NC Division of Water Resources (DWR). It is our understanding of the November 14, 2013 Settlement Agreement that adherence to the conditions of the agreement and issuance of this stormwater permit supersedes previous permit coverage, including NC0003379. This approval letter is copied to staff of DWR so they can address any necessary final procedures for rescission of their permit coverage. 1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone 919-707-9220 / FAX: 919-733-2876 512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: htto://portal.nedenr.org/web/ir/land-quality An Equal Opportunity 1 Affirmative Action Employer - 50% Recycled 110% Post Consumer Paper Glenn McLean NCG030027 March 10, 2014 Page 2 of 2 Please take note that this certificate of coverage is not transferable except after notice to the Division of Energy, Mineral and Land Resources (DEMLR). The Division may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DEMLR or permits required by the Division of Water Resources, or any other federal, state or local governmental permit that may be required. If you have any questions concerning this permit, please contact Bradley Bennett at telephone number (919) 807-6378 Sincerely, '94*2�n for Tracy E. Davis, P.E., CPM cc: Raleigh Regional Office, John Holley Central Files Stormwater Permitting Unit Files Tom Belnick - DWR - NPDES Wastewater Carolyn McLain - NCDOJ Jimmy Kirkland - Womble Carlyle Sandridge & Rice, LLP 1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone 919-707-9220 / FAX: 919-733-2876 512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://portal.ncdenr.org/web/Ir/land-guality An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES GENERAL PERMIT NO. NCG03000Q CERTIFICATE OF COVERAGE No. NCG030027 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Eaton Corporation is hereby authorized to discharge stormwater from a facility located at Eaton Corporation - Roxboro Facility 2564 Durham Road Roxboro Person County to receiving waters designated as UT to North Flat River, a class WS-111, NSW water in the Neuse River Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, 111, IV, V, and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective March 10, 2014. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day March 10, 2014. for Tracy E. Davis, P.E., Director Division of Energy, Mineral, and Land Resources By the Authority of the Environmental Management Commission LOCATION MAP: USGS Map: Timberlake Latitude: 36'21'31" N NCG030027 Facility Longitude: 78°59'04" W �Y Eaton Corporation County: Person - Location Stream Class: WS-III, NSW Roxboro Receiving Stream: UT to North Flat River Sub -basin: 03-04-01 (Neuse River Basin) avottli Not to Scale Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Tuesday, February 25, 2014 11:22 AM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission I wouldn't worry too much about the fee question. I spoke with the attorney about the fee and he was totally CK with using the fee for the other outstanding fees. This looks good to me. Minor edits in the last paragraph: remove the period from the beginning of the first sentence and did you mean to write "notice" or "note" in that first sentence? Thanks! Carolyn From: Bennett, Bradley[mailto:brad ley. ben nett(a)ncdenr.gov] Sent: Tuesday, February 25, 2014 10:58 AM To: McLain, Carolyn Subject: FW: Eaton Corporation Roxboro Submission Carolyn, Still haven't received confirmation from them on the fee question in my email, but I have drafted the modification letter. Can you please take a look and see if you think this is okay. Thanks 32 Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradley.bennett(a)ncdenr.gov Raleigh, NC 27699-1612 Web: htto://nortal.ncdenr.org/web/Ir/stormwater Email correspondence to and from this address maybe subject to public records laws From: Jeff Schick [mailto:itschickCallbocmh.com] Sent: Friday, February 21, 2014 4:42 PM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission Received ok. Thanks. From: Bennett, Bradley[ma !Ito:brad ley. ben nettftncdenr.gov] Sent: Friday, February 21, 2014 4:41 PM To: itschick0)lbecmh.com Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: RE: Eaton Corporation Roxboro Submission Mr. Schick, Second try. Sorry I got the email wrong the first time. M.- Bradley Bennett Stormwater Permitting Program NC Division of Energy, Mineral and Land Resources 1612 Mail Service Center Raleigh, NC 27699-1612 Phone: (919) 807-6378 Fax: (919) 807-6494 Email: bradlev.bennett(@.ncdenr.gov Web: http://portal.ncdenr.org/web/Irlstormwater Email correspondence to and from this address may be subject to public records laws From: Bennett, Bradley Sent: Friday, February 21, 2014 2:52 PM To: 'jtschick@lbgmh.com' Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: Eaton Corporation Roxboro Submission Mr. Schick, I just wanted to touch base with you concerning our discussion today on the submittal. As we discussed, the Stormwater Program will not be issuing a new permit coverage for the Roxboro facility. We will be sending a letter that essentially reissues the existing coverage and clarifies that it includes the discharge from the sites stormwater pond now that work from the settlement agreement has been completed to exclude the impacted groundwater from entering the storm sewer. We will also work with the NPDES Wastewater Staff in DWR to assure that coverage under NC0003379 is rescinded. In addition, as we discussed, the Eaton facility stormwater permit — NCG030027 — currently has an outstanding annual fee of $100 for the time period feb 2013-Jan 2014. The $100 fee submitted with the N01 package will be applied to this overdue annual fee. Please confirm that this is appropriate. I have attached the invoice for this annual fee. If there are any changes needed in the contact information for this please let me know. fl: Bradley Bennett Stormwater Permitting Program NC Division of Energy, Mineral and Land Resources 1612 Mail Service Center Raleigh, NC 27699-1612 Phone: (919)807-6378 Fax: (919) 807-6494 Email: bradley.bennett(o@cdenr.gov Web: http://portal.ncdenr.orglweb/Ir/stormwater Email correspondence to and from this address may be subject to public records laws Bennett, Bradley From: Jeff Schick Otschick@lbecmh.com] Sent: Friday, February 21, 2014 4:42 PM To: Bennett, Bradley Subject: RE: Eaton Corporation Roxboro Submission Received ok. Thanks. From: Bennett, Bradley[ma ilto:brad ley. ben nett@ncdenr.gov] Sent: Friday, February 21, 2014 4:41 PM To: itschickZlbecmh.com Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: RE: Eaton Corporation Roxboro Submission Mr. Schick, Second try. Sorry I got the email wrong the first time. m Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradlev.ben nett(a)ncdenr.gov Raleigh, NC 27699-1612 Web: httn://I)ortal.ncdenr.org/web/ir/stormwater Email correspondence to and from this address may be subject to public records laws From: Bennett, Bradley Sent: Friday, February 21, 2014 2:52 PM To: 'jtschick@lbgmh.com' Cc: McLain, Carolyn; Belnick, Tom; Chernikov, Sergei Subject: Eaton Corporation Roxboro Submission Mr. Schick, I just wanted to touch base with you concerning our discussion today on the submittal. As we discussed, the Stormwater Program will not be issuing a new permit coverage for the Roxboro facility. We will be sending a letter that essentially reissues the existing coverage and clarifies that it includes the discharge from the sites stormwater pond now that work from the settlement agreement has been completed to exclude the impacted groundwater from entering the storm sewer. We will also work with the NPDES Wastewater Staff in DWR to assure that coverage under NC0003379 is rescinded. In addition, as we discussed, the Eaton facility stormwater permit — NCG030027 — currently has an outstanding annual fee of $100 for the time period feb 2013-Jan 2014. The $100 fee submitted with the N01 package will be applied to this overdue annual fee. Please confirm that this is appropriate. I have attached the invoice for this annual fee. If there are any changes needed in the contact information for this please let me know. m Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 1612 Mail Service Center Email: bradlev.bennett(�ncdenr.00v 'Raleigh, NC 27699-1612 Web: hUp://portal.ncdenr.org/web/Ir/stormwater Email correspondence to and from this address may be subject to public records laws Bennett, Bradley From: McLain, Carolyn (CMcLain@ncdoj.gov] Sent: Tuesday, February 11, 2014 1:14 PM To: Bennett, Bradley Subject: RE: Eaton - Roxboro - Settlement Agreement Attachments: FullyExec_11-14-13 Eaton Settlement.pdf Great. See attached for the agreement in full. Let me know if you have questions. I can walk you through the particulars, if you need. Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919)716-6766 Fax cmclain@ncdoj.gov IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. 4132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Bennett, Bradley [mailto:bradley.bennett@ncdenr.gov] Sent: Tuesday, February 11, 2014 1:12 PM To: McLain, Carolyn Subject: RE: Eaton - Roxboro - Settlement Agreement Carolyn, Got the package today. If the agreement isn't too long, could your forward a copy to me? 01 Bradley Bennett Stormwater Permitting Program Phone: (919) 807-6378 NC Division of Energy, Mineral and Land Resources Fax: (919) 807-6494 - 1612 Mail Service Center Email: bradley.bennett(ancdencoov Raleigh, NC 27699-1612 Web: http://portal.ncdenr.org/webllr/stormwater Email correspondence to and from this address may be subject to public records laws From: McLain, Carolyn [mailto:CMcLain(alncdoi.00v] Sent: Monday, February 03, 2014 10:44 AM To: Bennett, Bradley Subject: FW: Eaton - Roxboro - Settlement Agreement Hi Bradley— I hope you are doing well. I don't know if you recall this case (initially Tom Belnick and Sergei C.) but Eaton is now in the phase where they need to work with you a bit, I think. They were operating under individual NPDES permit but now only need coverage under existing/modified General SW permit. Sergei tells me that all of this needs to be sent to you but I just wanted to confirm with you and also give you a heads up that this is coming your way. Also — can you please include the best address to send this to? I'm happy to discuss further if you need. Appreciate your help in this matter. Thank you, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclainencdoi.00v IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Kirkland, Jimmy [mailto:JKirklandCalwcsr.com] Sent: Monday, February 03, 2014 10:18 AM To: McLain, Carolyn Subject: Eaton - Roxboro - Settlement Agreement Carolyn, I hope you are doing well. Eaton is ready to make the notifications required under the Settlement Agreement. Under the terms of the agreement Eaton is required to submit the following; Storm Water Work Statement of Completion Stormwater Notice of Intent Stormwater Pollution Prevention Plan Who should these be submitted to? The Stormwater NCI has instructions for mailing but we want to determine if it should be mailed differently. Also, do you want them all mailed at the same time or can they be submitted separately? Thanks, Jimmy Jimmy Kirkland Womble Carlyle Sandridge & Rice, LLP 271 17th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax www.wcsr.com IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements imposed by the IRS, we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used. and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matter addressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential, privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it. or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the part of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Monday, February 10, 2014 10:04 AM To: Bennett, Bradley Subject: FW: Eaton Roxboro Settlement Agreement Submittals Hey Bradley — hope you're doing well. See attached. It looks like all of the appropriate materials are headed your way. I removed the attachments since they were 6 MB and you'll be receiving the hardcopies. Please let me know if/when you would like to chat about this project. I'm more than happy to fill you in on the details but I also don't want to waste your time if you feel you've got sufficient information for this project. I'm pretty open this week, so let me know. Thanks again, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclainno ncdoi.4ov IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Kirkland, Jimmy [mailto:JKirkland(a)wcsr.com] Sent: Friday, February 07, 2014 4:03 PM To: McLain, Carolyn Subject: Eaton Roxboro Settlement Agreement Submittals Carolyn, Earlier today the submittals required pursuant to the Settlement Agreement were mailed to Bradley Bennett. Copies of the submittals are attached. We look forward to receiving the Certificate of Coverage for the facility. If you have any questions, please let me know. Regards, Jimmy Jimmy Kirkland Womble Carlyle Sandridge & Rice, LLP 271 t7th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax www.wcsr.com IRS CIRCULAR 230 NOTICE. To ensure compliance with requirements imposed by the IRS, we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matter addressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential, privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient. you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it. or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the part of the sender to waive any privilege, including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. Bennett, Bradley From: McLain, Carolyn [CMcLain@ncdoj.gov] Sent: Monday, February 03, 2014 10:44 AM To: Bennett, Bradley Subject: FW: Eaton - Roxboro - Settlement Agreement Hi Bradley — I hope you are doing well. I don't know if you recall this case (initially Tom Belnick and Sergei C.) but Eaton is now in the phase where they need to work with you a bit, I think. They were operating under individual NPDES permit but now only need coverage under existing/modified General SW permit. Sergei tells me that all of this needs to be sent to you but I just wanted to confirm with you and also give you a heads up that this is coming your way. Also — can you please include the best address to send this to? I'm happy to discuss further if you need. Appreciate your help in this matter. Thank you, Carolyn Carolyn McLain Assistant Attorney General North Carolina Department of Justice P. O. Box 629 Raleigh, NC 27602-0629 (919) 716-6600 Phone (919) 716-6766 Fax cmclain(a)ncdoi.gov IMPORTANT: This email message is intended solely for the individual or individuals to whom it is addressed. It may contain confidential attorney -client privileged information and attorney work product. Information contained in this email may be subject to North Carolina Public Records Act requests under N.C. Gen. Stat. § 132-1 to - 10. If the reader of this message is not the intended recipient, you are requested not to read, copy or distribute it or any of the information it contains. Please delete the message immediately and notify the Attorney General's Office by return e-mail or by telephone (919) 716-6600. From: Kirkland, Jimmy [mailto:JKirkland(o)wcsr.com] Sent: Monday, February 03, 2014 10:18 AM To: McLain, Carolyn Subject: Eaton - Roxboro - Settlement Agreement Carolyn, I hope you are doing well. Eaton is ready to make the notifications required under the Settlement Agreement. Under the terms of the agreement Eaton is required to submit the following; Storm Water Work Statement of Completion Stormwater Notice of Intent Stormwater Pollution Prevention Plan Who should these be submitted to? The Stormwater NOI has instructions for mailing but we want to determine if it should be mailed differently. Also, do you want them all mailed at the same time or can they be submitted separately? Thanks, Jimmy Jimmy Kirkland Womble Carlyle Sandridge & Rice, LLP 271 17th Street NW Suite 2400 Atlanta, Georgia 30363 404.879.2460 phone 404.870.8223 fax IRS CIRCULAR 230 NOTICE: To ensure compliance with requirements imposed by the IRS. we inform you that any U.S. tax advice contained in this communication (or in any attachment) is not intended or written to be used, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code or (ii) promoting, marketing or recommending to another party any transaction or matter addressed in this communication (or in any attachment). CONFIDENTIALITY NOTICE: This electronic mail transmission has been sent by a lawyer. It may contain information that is confidential. privileged, proprietary, or otherwise legally exempt from disclosure. If you are not the intended recipient, you are hereby notified that you are not authorized to read, print, retain, copy or disseminate this message, any part of it, or any attachments. If you have received this message in error, please delete this message and any attachments from your system without reading the content and notify the sender immediately of the inadvertent transmission. There is no intent on the pan of the sender to waive any privilege. including the attorney -client privilege, that may attach to this communication. Thank you for your cooperation. LEGGETTE, BRASHEARS & GRAHAM, INC. Professional Groundwater and Environmental Consultants 104 Mill Street, Suite 1 Gahanna, Ohio 43230 (614)416-9100 (614) 416-9101 -Fax February 7, 2014 Mr. Bradley Bennett Supervisor, Stormwater Permitting Program North Carolina Division of Energy, Mineral and Land Resources 1612 Mail Service Center Raleigh, North Carolina 27699-1612 113 §VXV D FEB 14 M4 DENR-WAT-4Dl1ALtT� WETLANDS AND STORNATERD�' Subject: Settlement Agreement Submissions Eaton Corporation Roxboro Facility - 2564 Durham Road, Person County, NC Dear Mr. Bennett: In accordance with the November 14, 2013 Settlement Agreement, I am submitting the following documents on behalf of Eaton Corporation: Engineer's Statement of Completion of the Storm Sewer Work • Notice of Intent for NCG030000 for coverage of the entire facility and a check for $100.00 • Stormwater Pollution Prevention Plan that incorporates discharges from the stormwater retention pond. —P So.4 fo SRO w(KvAiSMh, c&py- It is Eaton's understanding that a Certificate of Coverage under NPDES General Permit NCG030000 will be issued which includes discharges from the stormwater retention pond. Additionally, we understand that the Certificate of Coverage will supersede all previously issued NPDES permits including individual NPDES Permit No. NC0003379. In accordance with Paragraph E. of the Settlement Agreement, please provide three days prior notice of the issuance of the Certificate of Coverage to StevenFesko@Eaton.com with a copy to JKirkland@wcsr.com. If you have any questions regarding this submittal, please contact me at (614) 416-9100 or jtschick@lbgcmh.com. cc: Connecticut New Jersey Sincerely, LEGGETTE, BRASHEARS & GRAHAM, INC. I!" - Jeffrey Schick Eaton Project Coordinator Mr. Steve Fesko - Eaton Corporation Mr. Glenn McLean - Eaton Corporation Mr. Jimmy Kirkland - Womble,Carlyle Sandridge & Rice, LLP Florida Georgia Illinois Michigan New York Ohio Pennsylvania South Dakota FEB 1 : ZW4 DENR-WAT:R��E gtpttGN WETLANDS AND STDR' Minnesota Missouri North Dakota Texas Vermont Wisconsin ALYCRA of Water Quality / Surface Water Protection Section NC®ENR National Pollutant Discharge Elimination System Nw+P ciPoux. or P�xr o. ExviPpxxEM W D NYW Y FEXNIRCES NCG030000 NOTICE OF INTENT FOR AGENCY USE ONLY Date Received Year I Month I Dav Certificate ofC.vc.,,e N C G 0 ' Check H Amount Permit A.ivued to National Pollutant Discharge Elimination System application for coverage under General Permit NCG030000: STORMWATER DISCHARGES associated with activities classified as: SIC (Standard Industrial Classification) 335 Rolling, Drawing, and Extruding of Nonferrous Metal SIC 3398 Metal Heat Treating �, t' SIC 34 Fabricated Metal Products 0 SvL�� SIC 35 Industrial and Commercial Machinery SIC 36 Electronic and Other Electrical Equipment FEB SIC 37 Transportation Equipment WpT.ROIWIT GH SIC 38 Measuring, Analyzing, and Controlling Instruments WETLANOSWdDS70Rt iER6FAN V\f For questions, please contact the DWQ Regional Office for your area. See page 4. = (Please print or type) 1) Mailing address of owner/operator (address to which all permit correspondence will be mailed): Name EATON CORPORATION Street Address 2564 DURHAM ROAD City ROXBORO State NC Telephone No. (336) 503-6538 Fax: 2) Location of facility producing discharge: Facility Name EATON CORPORATION Facility Contact KIM WITKOWSKI Street Address 2564 DURHAM ROAD City ROXBORO State NC County PERSON Telephone No. (336) 503-6538 Fax: Email KIM BERLYWITKOWSKI@EATON.COM ZIP Code 27573 ZIP Code 27573 3) Physical Location Information: Please provide a narrative description of how to get to the facility (use street names, state road numbers, and distance and direction from a roadway intersection). THE EATON ROXBORO FACILITY IS LOCATED AT INTERSECTION OF DURHAM ROAD (US HIGHWAY 501) AND INDUSTRIAL DRIVE. (A copy of a county map or USGS quad sheet with the facility clearly located must be submitted with this application.) 4) Latitude 36° 21' 31" N Longitude 78° 59' 4" W (deg, min, sec) Page 1 of 4 SWU-218-071408 Last revised 7/14/08 NCG030000 N.O.I. 5) This NPDES Permit Application appliesto which of the following: ❑ New or Proposed Facility Date operation is to begin X Existing 6) Standard Industrial Classification: Provide the 4-digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial activity at this facility. SIC Code: 3714 7) Provide a brief narrative description of the types of industrial activities and products manufactured at this facility: THE EATON ROXBORO FACILITY IS PRIMARILY ENGAGED IN THE MANUFACTURE OF MOTOR VEHICLE PARTS. 8) Discharge points / Receiving waters: How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? 2 What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater discharges end up in? UNNAMED TRIBUTARY TO THE NORTH FLAT RIVER IN NUESE RIVER BASIN Receiving water classification: WS-III NSW Is this a 303(d) listed stream? NO Has a TMDL been approved for this watershed? NO If the site stormwater discharges to a separate storm sewer system, name the operator of the separate storm sewer system (e.g. City of Raleigh municipal storm sewer). 9) Does this facility have any other NPDES permits? ❑ No X Yes If yes, list the permit numbers for all current NPDES permits for this facility: NC0003379 10) Does this facility have any Non -Discharge permits (ex: recycle permit)? X No ❑ Yes If yes, list the permit numbers for all current Non -Discharge permits for this facility: 11) Does this facility employ any best management practices for stormwater control? ❑ No X Yes (Show any structural BMPs on the site diagram.) If yes, please briefly describe: A STORMWATER RETENTION POND WAS INSTALLED 12) Does this facility have a Stormwater Pollution Prevention Plan? ❑ No X Yes If yes, when was it implemented? JANUARY 1, 2014 13) Are vehicle maintenance activities occurring at this facility? X No ❑ Yes 14) Hazardous Waste: a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? X No ❑ Yes Page 2 of 4 SWU-218-071408 Last revised 7/14/08 NCG030000 N.O.I. b) Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste generated per month) of hazardous waste? X No ❑ Yes c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? X No ❑ Yes d) Is hazardous waste stored in the 100-year flood plain? X No ❑ Yes If yes, include information to demonstrate protection from flooding. e) If you answered yes to questions b. or c., please provide the following information: Type(s) of waste: How is material stored: Where is material stored: How many disposal shipments per year: Name of transport / disposal vendor: Vendor address: 15) Certification: North Carolina General Statute 143-215.6B (i) provides that: Any person who knowingly makes any false statement. representation, or certification in any application, record, report, plan, or other document fled or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request coverage under the referenced General Permit. I understand that coverage under this permit will constitute the permit requirements for the discharge(s) and is enforceable in the same manner as an individual permit. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and /accurate. Printed Name of Person Sim/ ing: l� 1en'o -- M/ �/ C Le4✓I Title: PIC117- a"Ill rYI/_ P. P— (Signature of Applicant) 5-F�b zoi� (Date Signed) This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to: NCDENR Page 3 of 4 SWU-218-071408 Last revised 7/14/08 NCG030000 N.O.I. Final Checklist This application will be returned as incomplete unless all of the following items have been included: X Check for $100 made payable to NCDENR. X This completed application and all supporting documents. X A site diagram showing, at a minimum, (existing or proposed): (a) outline of drainage areas, (b) stormwater management structures, (c) location of stormwater outfalls corresponding to the drainage areas, (d) runoff conveyance features, (e) areas where materials are stored, (f) impervious areas, (g) site property lines. X Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map. Mail the entire package to: Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Note The submission of this document does not guarantee coverage under the General Permit. For questions, please contact the DWQ Regional Office for your area. DWQ Regional Office Contact Information: Asheville Office ...... (828) 296-4500 Fayetteville Office ... (910) 433-3300 Mooresville Office ... (704) 663-1699 Raleigh Office ........ (919) 791-4200 Washington Office ...(252) 946-6481 Wilmington Office ... (910) 796-7215 Winston-Salem ...... (336) 771-5000 Central Office .........(919) 807-6300 Page 4 of 4 SWU-218-071408 Last revised 7/14108 LEGEND -'- APPROXIMATE PROPERTY LINE STORM SEWER STORMWATER DRAINAGE SWALE ®i STORM WATER OUTFALL ®POTENTIAL STORM WATER POLLUTANT AREA DIRECTION OF SURFACE WATER FLOW --- DRAINAGE AREA (APPROX.) � TREE LINE © GENERATOR © CHILLER UNIT OTRASH DUMPSTERS OTRANSFORMER HAZARDOUS WASTE STORAGE .a x.M m , '�C'`RU BOftb• %'•;: � �I (f C�'�I ��c-'�`\;' •• ok dale, �J Radio, I `� � i / `.• �''J� .. � {{�]\ c (WRXo) '�-•., Leo\ " '�... ( Tank f \ Site O f •':l• E...* \,/ Y.: !.. \'t. `.y :. • • .i p Hill V 4 (. `4`� Tra 1 r r � - P2f - it I. •$ "� 1 f-� Si1i•15L3t 0 ..._ - y-... � - low Vf tfRi� •gr i ('fJ FIGURE 2 - SITE EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC 625 HUNTSMAN COURT TOPOGRAPHICAL MAP AND ONE GASTONIA, NC 28054 MILE RADIUS N (704) 853-08000 Excel Project No. 28091 Source: USGS N3615 — W7852 Timberlake NC, 1981 I-m-,ineer's Statement of Completion I hereby ccrtifi` that I have designed and supervised the following work which was completed at the Eaton Corporation facility, 2564 Durham Road. Roxboro. North Carolina: replacement of storm sewers and catch basins with welded high -density polyethylene piping in the tuck scale and truck clock area. 02103100l9 By: Michael J. L y-d LM, P. -,. Date Principal Civil Engineer The Kelly -Suck Company 1048 Literary Road Cleveland, 011 44113 NC Engineering Firm #C-2692 oA CAR =OPoFESSip <�2` SEAL 028510 � .FyG I Attachment 1 —Training Logs E_T*N Roxboro MESH Document 3.0 Water Management Powering Business Worldwide Stormwater Pollution Prevention Plan (SWPPP) TRAINING LOG AND MODULE Training Completed By: Signature: Title: Date: Printed Name Department Signature Training Topics Covered: Overview of applicable permit requirements • Contents and goals of the stormwater pollution prevention plan • Potential pollutants and minimization of exposure Manufacturing and maintenance activities Good housekeeping Clean-up, disposal, and organization Preventative maintenance • Inspection and maintenance of control equipment Spill prevention, response and reporting Spill equipment, procedures and cleanup Attachment 2 — Blank Forms FffeN ®� w � se Powering Business Worldwide NCDENR Eaton Corporation - Roxboro, North Carolina Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out th isform, please visit.- htto://oorta1.ncdenr.org/web/Ir/npdes-stormwater/ Permit No.: N/C/C/0/3/0/0/0/0/ or Certificate of Coverage No.: Facility Name: Eaton Corporation - Engine Components Division County: Person Phone No. (336) 599-1141 Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): Was this a "Measureable Storm Event" as defined by the permit? (See information below.) ❑ Yes ❑ No A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 6 SWU-242, Customized For Eaton, Last modified 10/31/2013 1. Outfall Description: Outfall No. 001 Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 6 SWU-242, Customized for Eaton, Last modified 10/31/2013 1. Outfall Description: Outfall No. 004 Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of Floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 3 of 6 SW U-242, Customized for Eaton, Last modified 10/31/2013 1. Outfall Description: Outfall No. 005 Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 4 of 6 SWU-242, Customized for Eaton, Last modified 10/31/2013 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Supplement SWU-242A: Guidance for Rating Stormwater Discharge This supplement is intended only as a guide for rating visually observed parameters on a scale of 1-5. The inspector should use best professional judgment when characterizing the quality of stormwater discharge. Also, the pictures included here do not necessarily show stormwater discharges but serve to illustrate the characteristics described. Clarity, (I is clear, and 5 is very opaque or cloudy) 1 3 Floating Solids ( I is no solids, and 5 is the surface covered with Floating solids or significant trash/debris) 1 3 Page I of 10 5 5 SWU-242A-061808 Suspended Solids (I is no solids, and 5 is extremely muddy or clouded with other •o� F'7i � o` � � r VI�. particles) T • �' mot' TM 1 3 5 Tannic Water Water naturally high in tannins in the eastern part of North Carolina may still have low amounts of suspended solids and high clarity but not appear "clear" because of coloration. The examples below will help rate discharges that must be observed in tannic waters. Clear tannic water may look like tea or coffee, but waters that look more "milky" or like "chocolate milk" have less clarity and higher suspended solids. Suspended Solids / Clarity in waterbodies namr illy high in tannins 1/1 3/3 Page 2 of 10 5/5 SwU-242A-061808 Example I 1. Outfall Description: Example 1 of 4 Outfall No. 001 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: light brown 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: I G 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 O 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 2 O 4 5 Page 3 of 10 Swu-2 t2n-oe t s0s Example 1 of 4, cont. 7. Is there any foam in the stormwater discharge? 8. Is there an oil sheen in the stormwater discharge? 9. Is there evidence of erosion or deposition at the outfall? 10. Other Obvious Indicators of Stormwater Pollution: List and describe N/A Page 4 of 10 Possibly small amount of Yes No foam near pipe outlet. Yes No Yes No Deposition of sand to the right of pipe outlet. SwU-242A-061808 Example 2 Outfall Description: Example 2 of 4 Outfall No. 001 Structure (pipe, ditch, etc.) Ditch Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: medium erav-ereen 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 Note in lower right corner picture, leaf shadow is visible on the botttt om of outlet. Clarity decreases beyond outlet. 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 3 4 5 Floating solids observed here are mostly tree debris that fell in after discharge. 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: I O 3 4 5 Page 5 of 10 Solids have settled out near outfall and are more "dissolved" out in the water netu the top of the picture (where water appears more Bray). At the outlet. there are not any swirls, clouds, or suspended particles. S W U-242A-061808 Example 2 of 4, cont. 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the cattail? Yes No Itl. Other Obvious Indicators of Stormwater Pollution: List and describe Some displacement of gravel and sediment observed at the outfall. Also. lots of solids that have settled. The water becomes more turbid/cloudv bevond the outfall (i.e.. clarity decreases). Evidence of excessive solids being carried into receiving water. This example illustrates how additional information in number 10. can be important to characterizing stormwater discharge impacts. Page 6 of 10 SwU-242A-061808 Example 3 1. Outfall Description: Example 3 of 4 Outfall No. 001 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: medium brown/tan 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): oily smell 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: I 2 3 O 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: Rating based on amount of scum/oil 1 2 3 4 5 covering surface, not tree debris. 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 O 4 5 Page 7 of 10 S W U-242A-a6 t 808 Example 3 of 4, cont. 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Oil and scummv substance floating on top. Dead duck found. Page 8 of 10 S W U-242A-061808 Excimple 4 1. Outfall Description: Example 4 of 4 Outfall No. 001 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: clear 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): none 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: O 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: O 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: O 2 3 4 5 Page 9 of 10 S W U-242A-061808 Lxample 4 of 4, cunt. 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe N/A Pave 10 of 10 S W U-242A-061808 Semi -Annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG030027 FACILITY NAME Eaton Corporation — Engine Components Division COUNTY Person PERSON COLLECTING SAMPLES LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply [—]SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) No discharge this period?Z Date Sample 24-hour rainfall pH, Non -Polar O&G/Total Toxic Outfall No. Total Suspended Solids Copper Lead zinc Total Petroleum Collected' amount, Standard units Hydrocarbons Organicss (mo/dd/yr) Inches; Benchmarks 100 mg/L or 50 mg/L' 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 0016 004 005 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is waived if a current, detailed Solvent Management Plan is on file at the facility. If this is the case, sign/certify page 2. 6 If combined with monthly monitoring as required by the facility's individual NPDES permit NC0003379, any duplicated parameters (i.e. pH, oil & grease, settleable solids) need not be re -analyzed, but must still be reported. Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Permit Date:11/1/2012-10/31/2017 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SWU-245, last revised 10/2S/2012 Page 2 of 3 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 STORMWATER DISCHARGE OUTFALL (SDO) ANNUAL SUMMARY DATA MONITORING REPORT (DMR) / SPPP Annual Update DATA REVIEW FORM Calendar Year Certificate of Coverage (COC) No. NCG030027 This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP. Facility Name: Eaton Corporation — Engine Components Division County: Person Phone Number: Total no. of SDOs monitored Outfall No. 001 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑ Parameter, (units) Total Rainfall, inches. Total Suspended ..solids, �; -pH, Standard units,; Copper Lead Zinc Non-Polar O&G/ Total Petroleum Hydrocarbons. Total Toxic Organics Benchmark N/A 100 mg/L or SO mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L - 1 mg/L Date Sample Collected, mmlddlyy ■ SWU-264— Eaton Customized Annual DMR Last revised 1013112013 Additional Outfall Attachment Outfall No. 004 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑ Parameter, (units) Total. Rainfall, inches Total Suspended Solids ,`.. -. ,.pH, Standard units Copper Lead Zinc ' Non -Polar 0&G/ Total Petroleum. Hydrocarbons Total Toxic Organics Benchmark N/A 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Date Sample Collected, mmlddlyy ® ---- Outfall No. 005 Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑ Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑ If this outfall was in Tier 2 last year, why was monthly monitoring discontinued? Enough consecutive samples below benchmarks to decrease frequency ❑ Received approval from DWQ to reduce monitoring frequency ❑ Other ❑ Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑ SWU-264 — Eaton Customized Annual DMR Last revised 1013112013 > Parameter, (units) Total Rainfall; inches Total Suspended - 'Solids ` pH, _?. Standard units : . Copper ,:. Lead. " - "Zinc Non -Polar O&G/Total :� Petroleum Hydrocarbons' Total Toxic Organics Benchmark N/A 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L Date mm/dd/ dSample Col lecte, mmldd/yy "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature Date DWQ_Regional Office Contact Information: For questions, contact your local Regional Office: RALEIGH4ECI0NAL OFFICE 3800 Barrett Drive Raleigh, NC 27609 (919) 791-4200 SWU-264 - Eaton Customized Annual DMR Last revised 1013112013 NCDENR ExvinOxn[H' wO NutAµ RC9gIwC[] Division of Water Quality / Surface Water Protection National Pollutant Discharge Elimination System REPRESENTATIVE OUTFALL STATUS (ROS) REQUEST FORM FOR AGENCYUSE ONLY Datc Rcccircd Y= Month Day If a facility is required to sample multiple discharge locations with very similar stormwater discharges, the permittee may petition the Director for Representative Outfall Status (ROS). DWQ may grant Representative Outfall Status if stormwater discharges from a single outfall are representative of discharges from multiple outfalls. Approved ROS will reduce the number of outfalls where analytical sampling requirements apply. If Representative Outfall Status is granted, ALL outfalls are still subject to the qualitative monitoring requirements of the facility's permit —unless otherwise allowed by the permit (such as NCGO20000) and DWQ approval. The approval letter from D WQ must be kept on site with the facility's Storm water Pollution Prevention Plan. The facility must notify DWQ in writing if any changes affect representative status. For questions, please contact the DWQ Regional Office for your area (seepage 3). (Please print or type) 1) Enter the permit number to which this ROS request applies: Individual Permit (or) Certificate of Coverage N C S I I I I I I N C G 2) Facility Information: Owner/Facility Name Facility Contact Street Address City County Telephone No. State ZIP Code E-mail Address Fax: 3) List the representative outfall(s) information (attach additional sheets if necessary): Outfall(s) is representative of Outfall(s) Outfalls' drainage areas have the same or similar activities? Outfalls' drainage areas contain the same or similar materials? Outfalls have similar monitoring results? Outfall(s) is representative of Outfall(s) Outfalls' drainage areas have the same or similar activities? Outfalls' drainage areas contain the same or similar materials? Outfalls have similar monitoring results? Outfall(s) is representative of Outfall(s) ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No ❑ No data* ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No ❑ No data* Outfalls' drainage areas have the same or similar activities? ❑ Yes ❑ No Outfalls' drainage areas contain the same or similar materials? ❑ Yes ❑ No Outfalls have similar monitoring results? ❑ Yes ❑ No ❑ No data* *Non-compliance with analytical monitoring prior to this request may prevent FOS approval. Specific circumstances will be considered by the Regional Office responsible for review. Page 1 of 4 SWU-ROS-2009 Last revised 12/30/2009 Representative Outfall Status Request 4) Detailed explanation about why the outfalls above should be granted Representative Status: (Or, attach a letter or narrative to discuss this information.) For example, describe how activities and/or materials are similar. 5) Certification: North Carolina General Statute 143-215.6 B(i) provides that: Any person who knowingly makes any false statement, representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the [Environmental Management] Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). I hereby request Representative Outfall Status for my NPDES Permit. I understand that ALL outfalls are still subject to the qualitative monitoring requirements of the permit, unless otherwise allowed by the permit and regional office approval. I must notify DWQ in writing if any changes to the facility or its operations take place after ROS is granted that may affect this status. If ROS no longer applies, I understand I must resume monitoring of all outfalls as specified in my NPDES permit. I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Title: (Signature of Applicant) (Date Signed) Please note: This application for Representative Outfa115tatus is subject to approval by the NCDENR Regional Office. The Regional Office may inspect your facility for compliance with the conditions of the permit prior to that approval. Final Checklist for ROS Request This application should include the following items: ❑ This completed form. ❑ Letter or narrative elaborating on the reasons why specified outfalls should be granted representative status, unless all information can be included in Question 4. ❑ Two (2) copies of a site map of the facility with the location of all outfalls clearly marked, including the drainage areas, industrial activities, and raw materials/finished products within each drainage area. o Summary of results from monitoring conducted at the outfalls listed in Question 3. ❑ Any other supporting documentation. Page 2 of 4 SWU-ROS-2009 Last revised 12/30/2009 Representative Outfall Status Request Mail the entire package to: NC DENR Division of Water Quality Surface Water Protection Section at the appropriate Regional Office (See map and addresses below) Notes The submission of this document does not guarantee Representative Outfall Status (ROS) will be granted as requested. Analytical monitoring as per your current permit must be continued, at all outfalls, until written approval of this request is granted by DWQ. Non-compliance with analytical monitoring prior to this request may prevent ROS approval. Specific circumstances will be considered by the Regional Office responsible for review. For questions, please contact the DWQ Regional Office for your area. Asheville Regional Office 2090 U.S. Highway 70 Swannanoa, NC 28778 Phone (828) 296-4500 FAX (828) 299-7043 Fayetteville Regional Office Systel Building, 225 Green St., Suite 714 Fayetteville, NC 28301-5094 Phone (910) 433-3300 FAX 910/ 486-0707 Mooresville Regional Office 610 East Center Ave. Mooresville, NC 28115 Phone (704) 663-1699 FAX (704) 663-6040 Raleigh Regional Office 1628 Mail Service Center Raleigh, NC 27699-1628 FAX (919) 571-4718 Washington Regional Office 943 Washington Square Mall Washington, NC 27889 Phone (252) 946-6481 FAX (252) 975-3716 Wilmington Regional Office 127 Cardinal Drive Extension Wilmington, NC 28405 Phone (910) 796-7215 FAX (910) 350-2004 Winston-Salem Regional Office 585 Waughtown Street Winston-Salem, NC 27107 Phone (336) 771-5000 Water Quality Main FAX (336) 771-4630 Central Office 1617 Mail Service Center Raleigh, NC 27699-1617 Page 3 of 4 SWU-ROS-2009 Last revised 12/30/2009 Attachment 3 — Completed Qualitative Monitoring Forms ATFR Or 11 BRIAN PHILLIPS EATON CORP - ROXBORO PO BOX 241 ROXBORO, NC 27573 Dear Permittee: Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality August 23, 2002 Subject: NPDES Stormwater Permit Renewal EATON CORP - ROXBORO COC Number NCG030027 Person County In response to your renewal application for continued coverage under general permit NCG030000, the Division of Water Quality (DWQ) is forwarding herewith the reissued Stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983. The following information is included with your permit package: * A new Certificate of Coverage * A copy of General Stormwater Permit NCG030000 * A copy of the Analytical Monitoring Form (DMR) * A copy of a Technical Bulletin for the general permit Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater and General Permits Unit at (919) 733-5083, ext. 548 Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Stormwater & General Permits Unit Files Raleigh Regional Office MA NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1- 800-623-7748 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030027 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, EATON CORP is hereby authorized to discharge stormwater from a facility located at EATON CORP - ROXBORO 2564 DURHAM ROAD ROXBORO PERSON COUNTY to receiving waters designated as a UT to the North Flat River, a class WS-111 NSW stream, in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11. III, IV, V, and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective September 1, 2002. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 23, 2002. b� . I / svy 'e-&— for Alan W. Klimek, P.E.. Director Division of Water Quality By Authority of the Environmental Management Commission WATc9 Q Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources 9 JAMES FESPERMAN AIR CONTROLS DIVISION PO BOX 241 ROXBORO, NC 27573 Dear Permittee: Gregory J. Thorpe, Ph.D. Acting Director Division of Water Quality December 27, 2001 Subject: NPDES Stormwater Permit Renewal AIR CONTROLS DIVISION COC Number NCG030027 Person County Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires on August 31, 2002. The Division slaff is currently in the process of rewriting this permit and is scheduled to have the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for continued coverage under the reissued permit. In order to assure your continued coverage under the general permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued coverage under the general permit. Failure to request renewal within this time period may result in a civil assessment of at (cast $250.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could result in assessments of civil penalties of up to $10,000 per day. Please note that recent federal legislation has extended the "no exposure exclusion' to all operators of industrial facilities in any of the I I categories of "storm water discharges associated with industrial activity," (except construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General Permits Unit Web Site at http://h2o.cnr.state.nc.us/su/storrnwatcr.htmi If the subject stormwater discharvc to waters of the state has been terminated, please complete the enclosed Rescission Request Form. Mailing instructions are listed on the bottom of ll e form. You will be notified when the rescission process has been completed. If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at (919) 733-5083, ext. 548 Sincerely, �/,cLCC/..�U �f�,7•i��f/l Bradley Bennett. Supervisor Stormwater and General Permits Unit cc: Central Files Raleigh Regional Office ern NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1-800-623-7748 State of North Carolina Department of Environment, Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director October 1, 1997 JAMES FESPERMAN EATON CORP-ROXBORO PLANT PO BOX 241 ROXBORO, NC 27573 A14y IDFEE HNFi Subject: Reissued Stormwater General Permit for Certificate of Coverage No. NCG030027 Person County Dear Permittee: In response to your renewal application for continued coverage under the subject permit, the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This pemut is reissued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. The following information is included with your permit package: ■ A copy of the stormwater general permit. ■ A Stormwater Pollution Prevention Plan Certification Form. This form certifies that you have developed and implemented the Stormwater Pollution Prevention Plan (SPPP) required in your permit. This form must be completed and retumed to the Division within 30 days of receipt of this letter. DO NOT send the SPPP with the signed form. ■ Five copies of Analytical Monitoring forms. ■ Five copies of Qualitative Monitoring forms. ■ A copy of a Technical Bulletin on the stormwater program with outlines program components and addresses frequently asked questions. ■ A corrected Certificate of Coverage if you indicated a name or address change on the Renewal Form returned to the Division. Your certificate of coverage is not transferable except after notice to DWQ. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DWQ or permits required by the Division of Land Resources, Division of Air Quality, Coastal Area Management Act or any other Federal or Local governmental permits that may be required. If you have any questions concerning this permit or other attached documents, please contact the Stormwater Group at telephone number (919) 733-5083 Sincerely, for O A. Preston Howard, Jr., P. E. P.O. Box 29535, Ralei,-h, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE NO. NCG030027 STORMWATER DISCHARGES In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, EATON CORP-ROXBORO PLANT is herby authorized to discharge stormwater from a facility located at: 2564 DURHAM ROAD ROXBORO,NC PERSON COUNTY to receiving waters designated as UT To North Flat River in the NEUSE River Basin in accordance with the effluent limitations, monitoring requirements and other conditions set forth in Parts I, 11, 111 and IV of General Permit No. NCG030000 as attached. This Certificate of Coverage shall become effective September 15, 1997 This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day October 1,1997 (or A Preston Howard, Jr., P.E., Director Division of Water Quality By Authorization of the Environmental Management Commission 01 State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management 512 North Salisbury Street • Raleigh, North Carolina 27604 James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary April 16, 1993 James Fesperman Eaton Corporation Eaton Center Cleveland, OH 44114 A. Preston Howard, Jr., P. E. Director Subject: General Permit No. NCG030000 Eaton Corporation COC NCG030027 Person County Dear Mr. Fesperman: In accordance with your application for discharge permit received on September 21, 1992, we are forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Environmental Management. The Division of Environmental Management may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 9191133- 5083. cc Sincerely, Original Signed By A. PreS4bPftegIowarOdltIrs., P.E. Raleigh Regional Office Pollution Prevention Pays P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT STORMWATER DISCHARGES In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Eaton Corporation is hereby authorized to discharge stormwater from a facility located at Eaton Corporation US Hwy 501 South - Two miles south of Roxboro Roxboro Person County to receiving waters designated as an unnamed tributary to Flat River in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II,1I1 and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective April 16, 1993. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day April 16, 1993. Original Signed By Coleen H. Sullins A. Preston Howard, Jr., P.E., Director Division of Environmental Management By Authority of the Environmental Management Commission UNITED STATES =" DEPARTMENT OF THE INTERIOR GEOLOGICAL SURVEY ` 1 57' 30" SOUTH BO$]ON (VT.) ]I ML A1 a a82 79i 00' egpoaomE ROXBORO fP.0.1 36°z2'30" <, � '-o 0 le . -SRO BDR-'`„��- / �;--y.--- _ 11 �\BM I` V .IC Radio 4 (WR7C01 �I� • �� ru p , xz \ �1 '. •v I� / 1�'` 4-�chln-� i � 1,\��f �A� _' u , � �\\\_v/��_�y �� \J��/� cn / r 65 r/:T Tan 'o25I PIPELINE)/ Q\ \J �. 7 Gn \ n r�\ 1 �j. ��.� J " ( / lir �i, 1 ff 1) ei set \ �, l� IwTI N/'��— /pa Pa / Pa j o In "Memoria `24 j - _ T"�( 1 by i�t " \�'- I / (, —_;•\ 7 lru 12. BN > I I cd c, - i FAC L.;Ti vnl cvrzpoeA Tnnl COUNTY �ERSti�( NPGES ~. N C C-1 V'3 L MAP 4 ?� 23 5 V`( DSN ELO4.' N /A 1 SUI,SASIN LATTITUDE LONGITUDE;. =�3 RECEIVING STREAM u N N AM �-b Tlzl (3uTA72,Y Tb ND2r-F� STREXIA CLASS 4 W S L N S W DISCHARGE CLASS SyZW?-MWAT-Fa EXPIRATION DATE o 6 - 31- Cl j �O 1 G G� y�F 79 36"22'30. UNITED STATES DEPARTMENT OF THE INTERIOR r:F.OLOOICAL SURVEY llln-7 *ESC ANALYTICAL REPORT November 22, 2016 M1 Eaton Corporation Sample Delivery Group: L872799 RECEIVED Samples Received: 11/15/2016 DEC 2 1 Z016 Project Number: Description: 28091-R CENTRAL FILES Eaton Corp Semi -Annual Stormwater PWR SECTION Report To: Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: r 41AJ- Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This zest report shall not be reproduced, except in full, wi:hoot written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. '. t TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cover Page 2Tc: Table of Contents 'Ss; Sample Summary 4Cn: Case Narrative 'Sr: Sample Results 2016-11-14-001 (POND) L872799-01 2016-11-14-005 (TOOL ROOM TRENCH) L872799-02 'Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 Volatile Organic Compounds (GC/MS) by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 'GI: Glossary of Terms 8AI: Accreditations & Locations 9Sc: Chain of Custody 1 2 3 4 5 5 8 11 11 12 13 14 16 18 19 25 26 27 ACCOUNT: PROJECT: SDG: DATETIM PAGE: I SAMPLE SUMMARY - -- - TI - ._ ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time 2016-11-14-001(POND) L872799-01 WW Kirk Spicer 11/14/161100 17n5/1609:00 FC Method Batch Dilution Preparation Analysis Analyst P date/time date/time Tc 6ravimetric Analysis by Method 2540 D-2011 WG927865 1 11/18/1614:11 11/18/1615:04 MMF Metals (ICP) by Method 200.7 WG926979 1 11/1611617:45 11/16116 21:41 LTB Pesticides (GC) by Method EPA 608 WG927281 1 11/17/16 00:51 11/17/1615.36 VKS Polychlonnated Biphenyls (GC) by Method EPA-608 W6926876 1 11/15/16 23:55 11/16/1616:37 JNS Semi Volatile Organic Compounds (GC/MS) by Method 625 WG927135 1 11/15/1619:00 11/18/16 16 32 SNR a Cn Volatile Organic Compounds (GC/MS) by Method 624 WG926511 1 11/17/16 2105 11/17/16 2105 JHH Wet Chemistry by Method 1664A WG926999 1 11/1611612:41 11/16/1617:19 SHG 5 Sf Collected by Collected date/time Received date/time 6qC 2016-11-14-005 (TOOL ROOM TRENCH) L872799-02 WW Kirk Spicer 11n4161100 11n5n609:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time GI 6ravimetric Analysis by Method 2540 D-2011 WG927865 1 11/18/1614:11 11/18/1615,04 MMF Metals (ICP) by Method 2007 WG926979 1 11/16/1617:45 11/16/16 2149 LTB aAl Pesticides (GC) by Method EPA 608 WG927281 1 11117/1600:51 11/17/1615.49 VKS Polychlorinated Biphenyls (GC) by Method EPA-608 WG926876 1 11/15/16 23:55 11/16/1616:49 JNS 5 Semi Volatile Organic Compounds (DOME) by Method 625 WG926871 1 11/15/1619:00 11/20/1623.22 JF SC Volatile Organic Compounds (GC/MS) by Method 624 WG926511 1 11/17/16 2125 11/17/16 2125 JHH Wet Chemistry by Method 1664A WG926999 1 11/16/1612:41 11/1611617:20 SHC ACCOUNT: PROJECT: SDG: DATEITIME: .PAGE: CASE NARRATIVE ONE LAB. NATIONWIDE. V All sample aliquots were received at the correct temperature, in the proper containers, with the Cp appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the FTCanalysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the Fs as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. eSr Lj- 6 QC FGI Jimmy Hunt a Technical Service Representative AI ACCOUNT: PROJECT: sDG' DATECIME: PAGE: 2016-11-14-001 (POND) SAMPLE RESULTS - 01 ONE LAB. NATIOINWIDE. Collected date/time: 11/14/16 11:00 _ L872799 Additional Information C Result Units p Analyte z pH (On Site) Z2 an TC Temperature (on -site) 14.5 Deg.0 D-2011 Gravimetric Analysis by Method 2540 Result Oualifer MDL RDL Dilution Analysis Batch ^ Cn Analyte mgA mgA mgA date/time Suspended Solids 2.30 J 0350 2.50 1 11118/201615:04 WG927865 Wet Chemistry by Method 1664A 6 Result Qualifier MDL RDL Dilution Analysis Batch QC Analyte mgA mgA mg/I date/time TPH -Oil&Grease 0.889 J 0325 5.56 1 11116/201617:19 WG926999 7GI Metals (ICP) by Method 200.7 SAI Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mg/I date/time 9 Copper U 0.00700 0.0100 1 11/16/2016 21:41 WG926979 SC lead U 0.00200 0.00500 1 11/16M16 21:41 WG926979 Zinc 0,0267 J MOW 0.0500 1 11/16/2016 21,41 WG926979 Volatile Organic Compounds (GC/MS) by Method 624 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mgA date/time Acrolein U J4 0,00887 0.0500 1 11/17/20162105 WG926511 Acrylonitrile U 0.M187 a0100 1 11/17/M16 21:05 WG926511 Benzene U 0.000331 0.00100 1 11/17/2016 21:05 WG926511 'Bromodichloromethane U 0.000380 0.00100 1 107/201621:05 WG926511 Bromoform U 0.000469 U0100 1 11/i7/20162105 WG926511 'Bromomethane U OA00866 0.00500 1 11/17/201621:05 WG926511 Carbon tetrachloride U 0.000379 0.00100 1 11/17/2016 21.05 WG926511 Chlarohenzene U 0.000348 0.00100 1 11/17/2016 21:65 WG926511 Chlorodibromomethane U 0M0327 0.00100 1 11/17/201621,05 WG926511 ,Chloroethane - ._U ,. - _ _.-_ . 0A00453 0.005W _ . 1 11117/201621:05 _. WG926511 ... I 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 11/17/2016 21:05 WG926511 'Chloroform U H00324 0.00500 1 11/17/2016 2105 WG926511 Chloromethane U H00276 0,00250 1 iV17/2M 2105 WG926511 ,1.2-Dichlorobenzene U 0.000349 0.00100 - 1 11/17/2016 2105 WG926511 1,3-01chiorobenzene U H00220 0.00100 1 11/17/2016 2105 WG926511 ,1,4-Dichlorobenzene U O000274 0.00100 1 11/17/2016 2105 WG926511 , Dichlorodifluoromethane U 0.000551 0.00500 1 11/17/2016 2105 WG926511 11 1-Dichloroe[hane U 0-000259 0.00100 1 11/17/2016 2105 WG926511 1,2-Dichloroethane U J4 0.000361 0,00100 1 11117/201621:05 WG926511 11,1-Dichloroethene - U 0.000398 0.00100 _ i 11/17/2016 2105 WG926511 trans-1,2-Dichloroethene U 0.000396 0.00100 1 11/17120162105 WG926511 ,12 Dichloropropane U 0.000306 0.00100 1 11/17/2016 21:05 WG926511 cis-1,3-Dichloropropene U 0.000418 0.00100 1 11/17/2016 21:05 WG926511 trt ans13-Dichloropropene^ U 0.000419 0.00100 1 11/17/20162105 WG92661 - - Ethylbenzene U 0.000384 - 0,00100 1 11/17/20162105 WG926511 Chloride U _ 0.00100 0A0500 - - 1� 11/17/2016 21_05- - _ -WG926511 .Methylene _ _ - _ _ _ 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 11/17120162105 WG926511 ITettachloroethene U 0.000372 0.00100 1 11/17/201621:05 WG926511 Toluene U 0.000780 0.00500 1 11/17/2016 21:05 WG926511 L11-Trichloroe,hane U _ 0.000319 000100 1 11/17/20163105 WG926511 - 1,12-Trichlorcethane U 0.000383 0.00100 1 11/17/2616 I65 WG926511 iACCOUNT. PROJECT: SDG: DATE/TIME: PAGE: ONE LAB. NATIONWIDE. 2016-11-14-001 (POND) SAMPLE RESULTS - 01 Collected date/time: 11/14/16 11:00 L_872799 Volatile Organic Compounds (GC/MS) by Method 624 Analyte Result Qualifier mgA MDL mg4 RDL mg4 Dilution Analysis date/time Batch Trichloroethene U 0.000398 0.00100 1 11/17/201621:05 WG926511 Trichlorofluoromethane U 0,00120 0.00500 1 11/17/201621.05 WG926511 Vinyl chloride U 0.000259 0.00100 1 11/17/2016 2105 WG926511 (S)Toluene-d8 108 90.0-115 111171201621.05 WG926511 SJDibramofluoromethone 99.2 79.0-121 111171201621.05 WG926511 (S)0,o,o-Trlfluorololuene 103 90.4-116 11117201621.05 WG926511 (S)4-Bromofluorobenzene 99.8 80.1-120 111171201621.05 WG926511 Pesticides (GC) by Method EPA 608 Result Qualifier MDL RDL Analyte mgA mgA mgA Mond U 0.00000813 0.0000500 Alpha BHC _ U J3 0.0000166 0.0000500 Beta BHC U 0,0000184 0.0000500 Delta BHC 0.000139 0.0000197 0.0000500 Gamma BHC U J3 0.0000176 0.0000500 Chlordane _ U 0.0000977 01.000500 4,4-DOD U 0.0000170 0,0000500 4,4-DDE U 4,4-DDT U Dieldrin U _ Endosulfan I U Endosulfan II U Endosulfan sulfate U Endrin U Endrin aldehyde U Enc in Ketone U Heptachlor U Heptachlor epoxide U Hexachlofobenzene U J3 Methoxychlor U Toxaphene U (S)Oemchlorc iphenyl 66.6 (SJ Tetrochloro-m-rylene 60.1 0.0600164 0.0000500 0.0000177 0.0000500 0.00000751 0-0000500 0.0000179 0.0000500 0.0000176 6.0006500 0.0000196 0.0000500 _ 0.6000189 0.0000500 0.0000142 0.0000500 0.0000170 0.0000500 0.0000108 0.0000500 0.0000175 0.0000500 0.0000134 0.0000500 0.0000193 0.0006560 0.000168 0.000500 10.0456 13.9-137 Polychlorinated Biphenyls (GC) by Method EPA-608 Dilution Analysis date / time 1 11/17/2016 15:36 1 11/17/201615:36 - 1 11/17/261615:36 1 11/17Mi 15:36 1 11/17/2016 15:36 1 11/17/201615:36 1 11/171201615:36 1 11/17/20161536 1 11/17/201615:36 1 11/17/201615.36 1 11/17/201615:36 1 11/17/201615:36 1 11/17/2016 15:36 1 11/17/201615:36 1 11/17/2016 15:36 1 1117/201615:36 1 11/17/2016 15:36 1 11/17/2016 1546 1 11/17/2016 15:36 - 1 11/17/201615:36 _ 1 11/17/2016 15:36 11111201615.36 111771201515:36 Batch WG927281 413927281 WG927281 WG927281 WG927281 WG927281 WG927281 WG927281 WG927281 WG927281 WG927281 --W(3927281 WG927281 WG927281 WG927281 WG927281 WG927281 WG927291 WG927281 WG927281 WG927281 WG927281 WG927281 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mgA date/time PCB 1016 U 0.000100 0.000500 1 11/16/2016 16 37 WG926876 PCB 1221 U 0.0000730 0.000500 1 11/16/201616:37 WG926876 PCB 1232 U 0.0000420 0.000500 1 11/16/201616:37 WG926876 -__. . ,PCB 1242 U __ 0.0000470 __._._._ 0.000500 1 fl1161201616:37 WGG 926876 I PCB 1248 U _.__._.____ 0.0000860 ,_-_ _ .- 0.000500 .- 1 11116/201616:37 WG926876 IPCB 454 U - 0.0000470 0.000500 1 11/16/201616:37 WG926876 PCB 1260 U 0.000120 0.000500 1 11/16/201616.37 WG926876 Oemchlorobi hen I 61.9 1 __ O ____.___.-_ 00-156 _ _.. 11/]620161637 .__. .___. WG926876 (SJ Tetrochlorom-xylene 51.2 13.9-137 11/161201616.37 WG926876 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Oualifier MDL Analyte mgA mgA Acenaphthene U 0.000316 Acenaphthylene U 0.000309 Anthracene U 0.000291 Ben2idme U 0.00432 ACCOUNT: RDL Dilution Analysis Batch mgA date/time 0.00100 1 11118/201616:32 WG927135 0.00100 1 11/18/201616:32 WG927135 0,00100 1 11/18/201616:32 WG927135 6.6100 1 11/18/201616:32 WG927135 PROJECT: SDG: DATE/TIME: PAGE: ONE LAB. NATIONWIDE. 2016-11-14-001 (POND) " SAMPLE RESULTS - 01 Collectetl dateltime: _11/14/16 11:00 L872799 _.__..-_.-_._..____-_ Semi'Volatile Organic Compounds (GC/MS) by Method 625 Result Qualifier MDL RDL Dilution Analysis Batch Anilyte mg/I mgA mg/I date/time Benzo(a)anthracene 0.000185 J 0.0000975 0.00100 1 11/18/201616:32 WG927135 Benzo(b)fluoranihene 0.000117, J 0.0000896 -0.00100 1 11/18/201616,32 WG927735_ Benzo(k)0uoranthene U J3 0.000355 0-00100 1 11/18/201616:32 WG927135 Benza(g,h i)perylene U 0.000161 0.00100 1 11/18/201616.32 WG927135 Benzo(a)pyrene U 0.000340 0.00100 1 11/18/201616:32 WG927135 s(- - -- Bis(2chlorethoxy)methane -- U� � - 0000329 - 0.0100 1 - --- _ 11118/201616:32 --- -- WG927735 , Bai2-chloroethyl)ether U 0,00162 0.0100 1 11/18/201616:32 WG927135 Bis(2-chloroisopropypether U 0.000445 0.0100 1 11/181201616:32 WG927135 - 4-Bromophenyl-phenylether U 0,000335 0.0100 1 11/18/201616:32 WG927135 2-Chloronaphthalene U 0.000336 _ 0.00100 _. 1 _ ii/18/201616:32 WG927735 _ _- __ 4-Chlorophenyl phenylether _._._ __ U _ _. 0-000303 -___ 0.0100 1 11118/201616.32 WG927135 1Chrysene U 0.000332 0.00100 1 11/18/2016 16:32 WG927735 Dibenz(a,h)anthracene U 0.000279 0.00100 1 11/18/201616:32 WG927135 333 Dichlorohenzldine U 000202 0.0100 1 11/18/201616:32 WG927135 - 2,4-Dinitrotoluene U 0.00165 0.0100 1 11/18/2016 16 32 WG927135 _.-._ _- - - 2 6-Dinitrotoluene - U - .. _ -- 0.000279 -- 0.0100 7 - - 11I78I201fi 1fi:32 - -_. - WG927735 �. 12-Diphenylhydrazine _ U 0.000318 0.0100 1 11/18/20161632 WG927135 Fluorantheme U 0,000310 0,00100 1 _ 11/18/201616:32 - WG927135 Fluorene U 0000323 0.00100 1 11/18/201616:32 WG927135 . _ _ Hexachloroheniene U � - 0.000341 _._-_ ._ 0.00700 1 .. ..___ - 11I18/20161fi:32 _ _.. -- _. WG927735 ._ .. ... � Hexachloro-1,3-butadiene U 0.000329 0.0100 1 11/18/201616:32 WG927135 Hexachlorocyclopentadiene U 0.00233 0.0100 1 11118/201616:32 W(3927735 Hexachloroethane U 0.00036E 0.0100 1 11/181201616:32 WG927135 Jndedo(1,2,3-cd)pyrene U 0.000279 0.00100 1 11/18/201616:32 WG927135 ' sophorone U 0.000272 0.0100 1 11/18/201616:32 WG927135 _-__.-____ Naphthalene -_____. U __.___-__.__ 0.000372 000100 1 _-_..________-. it/18/215116.32 -- ____ WG927135 Nitrobenzene U 0.000367 0,0100 1 11/18/201616:32 WG927135 n-Nitrosodimethylamine U 0,00126 0.0100 1 _.-------- .___-_- - 71118/201616:32 WG927135 n-Nltroscdlphenylamine U 0,000304 0.0100 1 11/18/201616:32 WG927135 n-Nitrosodi-n-propylamine U 0.000403 0-0100 1 111181201616:32 WG927135 Phenanthrene U 0.000366 0,00100 1 11/18/201616:32 WG927135 Benzylbutyl phthalate U 0.00027E 0.00300 1 11I18I201fi 16:32 WG927735 Bis(2-ethylhexyl)phthalate 0-00107 B J 0.000709 090300 1 11/18/201616,32 WG927135 Di-n-butyl phthalate U 0.000266 0-00300 1 11/18/2016 16:32 WG927135 ' Diethyl phthalate _ U 0.000282 0,00300 1 11/18/201616:32 WG927135 Dimethyl phthalate U 0000283 0-00300i 1 11I1820161632 WG927135 Di-n-octyl phthalate U 0.000278 0-00300 1 11/18/201616.32 WG927135 __._._._______ __ _-.___._. ... _. ___..____.__ _yrene ,P U____.-_ _ _ _.____-_. _..-.__-._._--_._ 0.000330 -____ 0.00100 ___ 1 _-____w___ 11/18/201616:32 WG927135 L2,4-TrichIorobenzene U 0,000355 0-0100 1 11/18/20161692 WG927135 4-Chloro73,methylphenol U 0.000263 00100 _ 1 11/1820167692 .WG927735 2-Chlorophenol U 0.000283 0.0100 1 11/18/201616:32 WG927135 12,4-Dichlorophenol U 0.000284 "0.0100 1 11/18/201616:32 WG927135 2,4-Dimethylphenol U 0.000624 0,0100 1 11/18/201616:32 WG927135 phenol U 0DG262_-_ 0.0100 -1__ 11/18/201616:32 �1DnDinitFo-2-methyl _ --_WG927135 _ - 2,4-Dinilrophenol U J3 0.0032E 0,0100 1 11/18/201616:32 WG927135 T2-Nitropdenpl U - 0.000320 Q,0100 1 11l_78/201616 32 WG927135 4-Nitrophenol It 0.00201 0.0100 1 11/18/201616:32 WG927135 ,__^_-_.._.-_-___-._____._T._.___�._______.-._____. Pentachlorophenol U 0.000313 0.0100 7 11I78I20161fi32 WG927735 - I Phenol U 0,000334 0.0100 1 11/18/201616:32 WG927135 , _-.__-_09_ _r4,6-Trcha _0__00 1 _... _ _11_�820r616.32 WG_9.-271�35 (S)2-Fluorophenol 254 10.0-779 111181261616:32 WG927135 I_S)Phenold5 15.] - 50070.1 111181201616,32 WG927135 (S) Mhobenzener75 679 27..8-123 1081206 16.32 WG927135 �V(S)2-Fluorobiphenyl- 789 - 295-131 . 71118201616:32 WG927735 (S)2,4,6-Tribromophenol 878 112-130 1111820167532 WG927135 t {SJ p-Terphenyl d14 171 29.3 137 1117820161632 WG927135 ' ACCOUNT: PROJECT: _ SDG, DATE/TIME: PAGE: 2016-11-14-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - o2 ONELAe.NATIONwIOE. collected date/time:- 11/14/16 11:00 L872799 Additional Information Result Units C P Analyle ZTc PH (On Site) 7.5 su Temperature (on -site) - 131 Deg.0 - - - Gravimetric Analysis by Method 2540 D-2011 S Result Oualifier MDL ROL Dilution Analysis Batch Analyte mg/l mg/l mg/I date/time Cn Suspended Solids 6.31 0.350 2.50 1 11/18/201615:04 WG927865 Wet Chemistry by Method 1664A Result Oualifier MDL RDL Dilution Analysis Batch Qc Analyte mgll mgA mgll date Mime TPH -Oil&Grease 1.65 J 0.725 5,88 1 11/16/201617:20 WG926999 7GI Metals (ICP) by Method 200.7 a Result Qualifier MDL RDL Dilution Analysis Batch AI Analyte mg/I mg/I mg/1 date/time 9 Copper 0,0230 0.00700 0.0100 1 11/16/20162149 WG926979 SC F Lead J 0.00200 0.00500 1 11/16/2016 21:49 WG926979. Zinc 0.0352 J 000340 0.0500 1 11/16/201621:49 WG926979 Volatile Organic Compounds (GC/MS) by Method 624 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/1 mg/I date/time Acrolein U J4 0,00887 0.0500 1 11/17/2016 2125 WG926511 Acrylanitnle U _ 0.00187 0.0100 1 IMN01621,25 WG926511 Benzene U 0.000331 0.00100 1 11/17/2016 2125 WG926511 Bromodichloromethane U 0.000380 0.00100 1 11/17/201621:25 WG926511 Bromoform U 0.000469 0,00100 1 11/17/201621:25 WG926511 Bromomethane U 0.000866 Ti.60500 1 11/17/201621.25 WG926511 Carbon tetrachloride U 0,000379 0.00100 1 11/17/2016 2125 WG926511 Chlorobenzene U 0000348 0.00100 1 11/17/20162125 WG926511 Chlorodibromomethane U 0,000327 0.00100 1 11/17/20162125 WG926511 ;Chloroethane _.. - U ._. _ . . _� ..0.000453 _0.00500_ __._.1 .._ .11177/20162125 �.. __ - _ W6926511 2-Chlorcethyl vinyl ether U 0.00301 M500 1 11/17/201621:25 WG926511 Chloroform U 0.000324 0.00500 1 11/1700162t25 W6926511 I Chloromelhane U 0.000276 0.00250 1 11/17/20162125 WG926511 i______. ___ __. 12 Dichlorobenzene _ U ___. 0.000349 _. -__-____�___ 0.00100 1 _.. 11/17/201621:25 _____._. WG926511 j 1,3-Dichlorobenzene U 0,000220 0.00100 1 IV17/20162125 WG926511 114Dichlorobenzene Ll -0.000274 000100 1 11/17/20162125 WG9265fl ! Dichlorodifluoromethane U 0.000551 0.00500 1 11/17/20162125 WG926511 ___.___._,..__..__o_ 1, Dichlgroethane ,U' 0.000259- ._..__-__. 0.00100' 1 - __ _ 11/17/20162125 ._ ____ WG926511 1,2-Dichloroethane U J4 0.000361 0.00100 1 11/171201621:25 WG926511 ri t Dichloroethene U_ J 0.000398 0.00100 1 11/17/2016 2125 WG926511 trans-1,2-Dichloroethene U 0.000396 0,00100 1 11117/201621,25 WG926511 11Z Dichloiopropane U - 0D00306 0,00100 1 11/17/2016 2125 WG926517 - cis-13-Olchloropropene U 0,000418 0.00100 1 11/17/201621,25 WG926511 trans-1,3-Dichloropropene .__ U d.000419 ____. 0.00100 1 11/17001621.25 WG926511 - -, Ethylbenzene U 0.000384 _ __ _0, 0.00100 1 11I77I201621:25 WG926511 iMethylene Chloride .0 0.00100 0.00500 1 11/17120162t25 WG926511 ' 1,1,2,2-Tetrachloroethane U 0,000130 0,00100 1 11/17/2016 2125 WG926511 iTetr&chloroethene U - 0.000372 0.00100 1 11/17/2016 21:25 92 WG926511 1 Toluene U 0.000780 0.00500 1 11/17/20162125 WG926511 ,1,1,1-Tnchloroethane �u 0000319 0.00100 1 11/17/20162125 WG926511 1 11,2-Trichloroethane U 0.000383 0.00100 1 11117/201621:25 WG926511 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: r ONE LAB. NATIONWIDE. 2016-11-14-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - 02 Collected date/time: 11/14/16 11:00 L_87.2799 Volatile Organic Compounds (GC/MS) by Method 624 Analyte Result mg4 Qualifier MDL mgn RDL mg/I Dilution Analysis date/time Batch Trichloroethene U 0.000398 0.00100 1 IIY17/2016 21:25 WG926511 TrichloroRuoromethane U 0.00120 0.00500 1 11/17120162125 WG926511 Vinyl chloride U 0,000259 0.00100 1 11/17/201621:25 WG926511 (S Toluene-d8 168 90.0-115 11/17201621..25 WG926511 (S)Dibromolluoromethane 160 79.0-121 11177201621.25 WG926511 (So,a,o-Trilluoro(oluene� 103 90.4-116 111171201621.25 WG926511 (S)4-Bromo8uorobenzene _ 102 80.1 l20 117J720162125 WG926511 Pesticides (GC) by Method EPA 608 Result Qualifier MDL RDL Dilution Analysis Batch Aldrin U Alpha BHC U Beta BHC U Delta BHC 0.0000843 Gamma BHC U Chlordane U 4,4-DDD U 4,4-DDT U Dieldrin U Endosulfan I U Endosullan II U Endosulfan sulfate _ _ U Endrin U Endrin aldehyde U Endrin ketone U Heptachlor U Heptachlor epoxide U Hexachlorobenzene U Methoxyc'Nor U Toxaphene U (SJ Decochlorobiphenyl 52.3 (S) Tetrachloro-m-aylene 56 1 mgn ni date/time 0.00000813 0.0000500 1 11/171201615:49 WG927281 J3 0.0000166 0.0000500 t 11/17/201615:49 WG927281 0.0000184 0.0000500 1 11/17/201615:49 WG927281 0 0000197 - 0.0000500 1 - 11/17/201615:49 WG927281 J3 0.0000176 0.0000500 1 11/17/201615:49 WG927281 0.0000977 0.000500 1 11/17/201615:49 W3927281 _ 0.0000170 0.0000500 1 11/17/201615:49 WG927281 0.0000164 0.0000500 1 11/17/201615:49 WG927281 H000177 0.0000500 1 11/17/201615:49 WG927281 0.00000751 0.0000500 1 11/17/201615:49 WG927281 0.0000179 0.0000500 1 11117/201615:49 WG927281 0.0000176 0.0000506 1 11/17/201615:49 WG927281 0.0000196 0,0000500 1 11/17/201615:49 WG927281 0.0000189 0.0000500 1 11/17/201615:49 WG927281 0.0000142 0.0000500 1 11/17/201615:49 WG927281 0.0000170 0.0000500 1 11/171201615:49 WG927281 0.0000108 0.0000500 1 11/17/201615:49 WG927281 0.0000175 0.0000500 1 11/17/201615:49 WG927281 J3 0,0000134 0.0000500 1 11/17/201615:49 WG927281 0.0000193 0.0000500 1 11/17/201615:49 WG927281 0.000168 0.000500 1 11/17/201615:49 WG927281 - - 10.0-156 17717201615.49 _ WG927281 _ 13.9-137 111172016 15.49 WG927281 Polychlorinated Biphenyls (GC) by Method EPA-608 Result Qualifier MDL RDL Dilution Analysis Batch Analyte all mgn mg4 date/time PCB 1016 U 0.000100 0.000500 1 11/16/201616:49 WG926876 PCB 1221 U 0.0000730 0.000500 1 17/16/201616:49 WG926876 PCB 1232 U 0,0000420 0.000500 1 11/16/201616:49 WG926876 '.PCB1242 U 0.0000470 0.000500 1 11/16/201616:49 - WG926876 PCB 1248 U 0.0000860 0,000500 1 11/16/201616:49 WG926876 'PCB 1254 U - 0.0000470 0.000500 7 11/76201616:49 WG926876 PCB 1260 U 0,000120 0.000500 1 11/16/201616:49 WG926876 (SJDecachloroblphenyl 66.3 10.0-156 111161201616,49 WG926876 I (S) Tetrachloro-m-xylene 63.7 139-137 77/162076 16:49 WG926876 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ni mg/I mgll date/time Acenaphthene U 0.000316 0.00100 1 11120/201623:22 WG926871 r____________ AcenapBthylene U 0.000309 ____-_.. 0.00100 -____ -_ 1 11/20/201623:22 _.__ NC26871 Anthracene U 0000291 0.00100 1 11/20/201623:22 WG926871 Benzidine U 0.00432 6.6100 1 11/20601623:22 WG926871 ACCOUNT: PROJECT: SDG: DATEMME PAGE: 2016-11-141605 (TOOL ROOM TRENCH) SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 11/14/16 11:00 L872799 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Qualifier MDL RDL Dilution Analysis Batch CF Analyte mg/I mg/I mg/I date/time Benzo(a)anthracene U 0.0000975 0.00100 1 11/20/2016 23:22 WG926871 ITC Benzo(b)Fluoranthene 0.000108 J 0.6000896 0.00100 1 11/20/201623:212 WG926877 Benzo(k)iluoranthene U 0.000355 0.00100 1 11/20/2016 23:22 WG926871 3SS Benzo(g,h,i)perylene _ U 0.000161 0.00100 1 11/20/20162322 WG926871 Benzo(a)pyrene U 0.000340 0.00100 1 11/20/201623:22 WG926871 Bis(2-chlorethoxy)methane - U 0.000329 0.0100 1 11/20/2016 23:22 WG926871 4 cr Bis(2-chloroethyl)ether U 0.00162 0,0100 1 11/20/2016 23:22 WG926871 Bis(2-chlormsopropypether U 0.000445 0.0100 1 11/20/20163322 WG926871 4-Bromophenyl phenylether U 0.000335 0.0700 1 11/20/2016 23.22 WG926871 2-Chloronaphthalene U 0.000336 0.00100 1 11/20/2016 23:22 WG926877 _ 4-Chlorophenylphenylether U 0.000303 0.0100 1 11120/201623:22 WG926871 6^ F ' hrysene U 0.000332 0.00100 1 11/20/2016 23:22 WG926871 lM Dibenz(a,h)anthracene U 0,000279 0.00100 1 11/20/201623:22 WG926871 3,3-61chlorobenzicine U 0.00262 0.0100 1 11/20/2016 23:22 WG926877 GI 2,4-Dimtrotoluene U 0.00165 0.0100 1 11/20/2016 23:22 WG926871 2 6-Dinitrotoluene -_ .0029 00100 1 11/20/2016 23:22 WG926871 AI Di,_y,___ 12 phe U 0.000318 __. . 0.0100 1 _ __ 11/20/201623:22 WG926871 Fluoranthene U 0.006310 o.do100 1 11/20/201623:22 WG92B871 rIyC^JC Fluorene U 0.000323 0.00100 1 11/20/2016 23:22 WG926871 ( Hexachlorobenzene U 6000341 0.00100 1 11/20/2016 23:22 WG926871 Hexachloro-1,3-butadiene U 0,060329 0.0100 1 11/20/2016 23:22 WG926871 Hexachlorocyclopenta_dien_e U 0.00233 00100 1 11/20I201623:22 WG926871 Hexachloroelhane U 0.000365 0.0100 1 11/20/2016 23:22 WG926871 Indeno(L2,3-cd)pyre_ne U _ 0.000279 0.00100 1 11/20/201623:22 WG926871 Isophorone U 0.000272 0.0100 1 11/20/20162322 WG926871 Naphthalene U 0.000372 0.00100 1 11/20/2016 23:22 WG926871 Nitrobenzene U 0.000367 0.0100 1 11/20/2016 23:22 WG926871 n-Nitrosodimethylamine U _ 0.004_ .. __6 0.0100 1 11I20I20-1623:_22 WG926871 n-Nitrosodiphenyla mine U 0.000304 0.0100 1 11/20/2016 23:22 WG926871 n-Nitrosodi-n-propylamine U 0.000403 0,0100 1 11/20/2016 23 22 WG926871 Phenanthrene U 0.000366 0.00100 1 11/20/201623:22 WG926871 Benzylbutyl phthalate U 0.06027; 0.00300 1 11/20/201623:22 WG926871 Bis(2-ethylhexypphthalate 0,00130 J_ 0.000709 0.00300 1 11/20/2016 23:22 WG926871 'Di-n-butyl phthalate U 0.000266 0.00300 1 71120/2016 23:22 WG926871 Diethyl phthalate U 6.060282 0.00300 1 11/20/201623,22 WG926871 .�-_._.______.__-_-..�.___....r__.,_�._-_.__� Dimethyl phthalate U 0.000283 __..__-__ 0.00300 1 .., 11/20I2016 2322 - WG926877 e Di-n-octyl phthalate 0.00134 B J 0.000278 0.00300 1 11/2W2016 2322 WG926871 Pyrene U 0.000330 0,00100 1 11/20/2016 23:22 WG926871 1 .2,4-Trichlorobenzene U 0.000355 0.0100 1 11/20/2016 23:22 WG926871 4-Chloro-3-methylphenol U 0.060263 0.0100 1 11/20/2016 23:22 WG926871 2-Chlorophenol u 0.000283 0.0100 1 11/20/2016 2322 WG926877 2,4-Dichlorcphenol _ 0.00.0337 J 0.000284 0.0100 1 11/20/2016 23:22 WG926877 2,4-Dimethylphenol _ _ _ U 0.000624 0,0100 1 11/20/2016 23:22 WG926871 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 11/20I20162322 WG926877 2,4-Dinitrophenol U J3 0.00325 0.0100 1 11/201201623:22 WG926871 2-Nitrophenol U 0.000320 0.0100 1 11/20/2016 23:22 WG926877 , 4-Nitrophenol U 0.00201 0.0100 1 11/20/201623:22 WG926871 IPentachlorophenol U 0.000313 6.0106 1 11/20/201623:22 WG926871 Phenol U 0.000334 0.0100 1 11/20/2016 23:22 WG926871 ;2,4,6-Trichlorophenol U 0.000297 0.0700 1 11/20/2016 23.22 WG926871 (S)2-Fluorophenol 24.1 10.0-77.9 1112012016 23 22 WG926871 (S)Phenol-d5 - 6..4 500-70.1 1120/201623.22 WG926871 (S) Nitrobenzene-d5 79.8 21.8-123 111201201623:22 WG926871 (SJ 2-Fluorobiphenyl 846 295-131 11/20/20162322 WG926871 (S)2,4,6-Tribromophenol 50.5 1t2-130 1112020162322 WG926871 (S)p-Terphenyl-d14 104 _ - 29.3-137 _ 11/2020162322 WG926877 1 ACCOUNT: PROJECT: SDG: DATE7rIME: PAGE' WG927865 _ QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE. -Gravirr,etnc_Agalysis,by_M ethod:2540,;D_2011_,__--____-- _. ---_ _ __- L872799-01,02-_._- - Method Blank (MB) Cp (MB) R3179518-1 11/18/1615:04 MB Result MB Qualifier MB MDL MB RDL Analyte mg/1 mg/l ni TC Suspended Solids U 0,350 2,50 3Ss L872716-01 Original Sample (OS) • Duplicate (DUP) nCn (OS) L872716-01 11/18/1615.04 • (DUP) P3179518-4 11/18/1615:04 Original Result DUP Result Dilution DUP RPD Analyte ni mg/I % DUP Qualifier DUP RPD Limits % Sr Suspended Solids 77.0 72.0 1 6,71 J3 5 ce L873415-02 Original Sample (OS) •Duplicate (DUP) 7G (OS) L873415-02 11/18/1615.04 • (DUP) P3179518-5 11/18/1615.04 - Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/l mg/l % % gA Suspended Solids 511 49.7 1 2.83 5 BSc Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3179518-2 11/18/16 15:04 • (LCSD) R3179518-3 11/18/16 15:04 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/l ni % % % % % Suspended Solids 773 736 736 95.2 95.2 85.0-115 0,000 5 ACCOUNT: :PROJECT: SDG: DATEMME: PAGE: WG926999 _Wet Chemistry_by_Method ,1664A Method Blank (MB) QUALITY CONTROL SUMMARY 0NELAB. N.ATioNWIOE. 1-872799-01,02 (MB) R3178549-1 11/16/1617:16 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 2 TC TPH - Oil & Grease 0 0.725 5.00 Ss 3n Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3178549-2 11/16/1617:16 • (LCSD) R3178549-3 11/16/1617:16 Cn Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I ni % % % % % 'Sr TPH -Oil&Grease 20G 19.6 20.3 98.0 102 78.0-114 3.51 18 N [GI $AI eSc ACCOUNT: - ,PROJECT: SDG: DATE/TIME: PAGE: WG926979 _ Metals (ICP)_by_Metfiod_200.7 Method Blank (MB) -QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. —._.__..—__. - _ ___- ...-_ _LB72799-01,02 _ (MB) R3178663-1 11/16/16 20:46 MB Result MB Qualifier MB MDL MB RDL Copper U 0.007 0.0100 Lead U _0.002 0.00500,. Zinc - U 0. 0034 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3178663-2 11/16/16 20:48 • (LCSD) R3178663-3 11/16/16 20:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte mgA mg/I mg/I % % % Copper 1.00 0.990 0.993 99 99 85-115 Leatl 7.00 _ 0999 0.995 106 too 85.115 Zinc 1.00 0.999 0.996 100 100 85-115 L872605-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) LCS Qualifier LCSD Qualifier RPD RPD Limits 0 20 0 20 0 20 (OS) L872605-01 11/16/16 20:53 • (MS) R3178663-5 11/16/16 20:59 • (MSD) P3178663-6 11/16/16 21:01 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits Analyte mg/I mg/I nigh mg/I % % % Copper 1.00 0.0168 1.03 1.04 102 102 1 70-130 ,Lead 1,00 ND 1.02. 1.02 102 102 1 70-130 Zinc 1.00 NO 1.01 1.01 100 100 1 70-130 L872984-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 9 MS Qualifier MSD Qualifier RPD RPD Limits SC 0 20 ....0. 20-.. . . 0 - 20 (OS) L872984-02 11/16/16 21:04 • (MS) R3178663-7 11/16/16 21:06 • (MSD) R3178663-8 11/16/16 21:09 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mgl mg/I % % % % % Copper 1.00 ND 1.00 1.01 100 101 1 70-130 1 20 Lead - _ _ -1.00 -- -_-ND 1.62 1.02 102 102 1 70-130 1 20 - Zinc 1.00 0.0644 1.06 1.07 100 101 1 70-130 1 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG926511 QUALITY CONTROL SUMMARY _ - � -- � ONE LAB, NATIONWIDE. 0 Volatile Organic Compounds_(GC/MS) by, Method 624 _ _ - - 1-872799-01,02 Method Blank (MB) Cp (MB) R3179168-3 11117/1612:35 MB Result MB Oualifier MB MDL MB RDL Analyse mgA mgll mg/I EC: U 0.00887 0.0500 Acrylonitrlle U 0.00187 0.0100 - -' - - Benzene U 0.000331 0.00100 FS Bromodichloromethanc U 0.000.380 ._. .. 0.00100 __ - - Bromoform U 0000469 0,00100 - QCn !Bromomethane U 0.000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 -- - - Chlorahenzene U _. 0.000348 _ 0.00100 Chlorodibromomethane U 0.000327 0.00100 - - Chloroethane U 0.000453 0.00500 2-Chloroethyl vinyl ether U 0.00301 0.0500 Chloroform U 0.000324 0.005001 - --- - Chloromethane U 0.000276 0.00250 - .. 12 Drchlorobenzene A U _ ___. 0000349 __ 0:00100- 13Dichlorobenzene U _ 0000220 0.00100 a/a 14 Dichlorobenzene U 0000274 0.00100 , - - Dichlorodi8uoromethane U _ . 0.000551 0.00500 ,1,1-Dichloroethane U _ 0.000259 0.00100 C 1,2-Dichloroethane _ _ U 0.000361 0.00100 - 1,1-Dichloroethene U 0.000398 0.00100 ' trans-1,2-Dichloroethene U 0.000396 0,00100 .__ .-prop_ __. A,2-Dichloropropane _ _ _. U _____ _ 0.000306 .. 0,00100 cis-1,3-Dichloropropene _ _ _ U _ 0.000418 _ 0.00100 ,trans-1,3-Dichloropropene _.. .. -_ U - 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0.00100 0.00500 1,1,2,2-7etrachloroethane U 0.000130 0.00100 Tetrachloroethene U _ 0.000372 0.00100 ; - -- Toluene U _ 0.000780 0.00500 4,1,1-Trichloroethane U 0.000319 0.00100 ' 1,1,2-Trichloroethane U 0.000383 0.00100 . - . _ Trichloroethene U 0.000398 0.00100'. - -. Trichlorofluorome[hane U 0.00120 0.00500 Vinyl chloride � U 0.000259 0.00700 (S) Toluene-d8 707 90.0-715 __ (S)Dibromolluorome(hone ._ .. __.._ 99.3 ...�. ."._ __. 79.0-121 (S)o,a.o-TriOuorotoluene 103 90.4-116 (S)4-BromoAuorobenzene 985 80.1-120 ACCOUNT: PROJECT: SDG DATE/TIME: PAGE: WG926511 QUALITY CONTROL SUMMARY Volatile Organic Compounds_(GC/MS)Lby_Method 624 __. 1.872799-01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3179168-1 11/17/16 11:32 • (LCSD) R3179168-2 11/17/16 1153 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I MO LCS Rec. % LCSD Rec % Rec. Limits % LCS Qualifier LCSD Oualifier RPD % RPD Limits % p ,TC Acrolein 0.125 1.88 177 1510 1410 88.0-118 E J4 E J4 6.51 28.1 Acrylonitrile 0125 - 0135 0126 108 101 71.0-135 7.06 20 SS Benzene 0.0250 00749 0.0254 995 102 73.0-122 2.22 20 Bromotlicheromethane 00250. 00270 00272 108 109 75.5-121 _ 0.670 _ 20 _ _ _ 4Cn Bromoform 00250 00200 0.0209 80.1 83.6 71.5-131 4.31 20 Bromomeihane 0.0250 0.0228 0.0229 91.1 91.8 22.4-187 0.670_ 20 Carbon tetrachloride 00250 _ 00243 00247 _ 97.0 98.8 _ 70.9-129 _ _ 1.84 20 6Sr Chlorobenzene _. 00250 00223 00225 89.3 89.8 79.7-122 0.530 20 Chlorodibromomethane iChloroethane _. _ 00250 0 0250; _ . _. 00227 00245 .___.. ___ 0,0230 0:0250 _.._....� 90.8 96.0 � _... 91.8 99.9 _ 78.2-124 41.2-153 1.11 1.95 20 20 � • 2-ChlorOethyl vinyl ether 0.125 0.166 OJ69 __ 733 .. __ 136 _. _ 23.4-162 _ 1.81 _ ..... _ 23.5 .Chloroform_ 00250 00266 00266 107 107 73.2-125 0.0100 20 7GI Chloromethane 0 0250 0 0275 0 0280 110 112 55.8-134 _ 2.06 20 112 Dichlorobenzene 13Dichlorobenzene _ 0.0250 00250 0,0232 00211 0.0245 0,0219 _ 92.9 84.5 _ 98.1 BT7 84.7-118 77.6-127 5.36 3.71 20 20 P, 9,4 Dichlorobenzene 0.0250. 0.0229 0.0233 91.7 93.1 82.2-114 1.53 20 Dichlorodifluoromethane 00250 00252 00265 101 106 56.0-134 5.35 20 SC 11-Dichloroethane . _ 00250 _ 00263 _. 0.0267 105 107 71.7-127 1.69 _ 20 1,2-Dichloroethane 0.0250 0.0303 0,0317 121 127 65.3-126 J4 455 - 20 _._.._______.________.-_._ 4,1-Dichloroethene 0.0250 0.0219 0.0229 _ 67.6 _. 91.6 59.9-137 4.40 20 trans-1,2-Dichloroethene 0.0250 0.0230 0.0235 91.9 94.1 72.6-125 2.42 20 1,2-Dichloropropane 0.0250 0.0270 0.0275 108 110 77.4-125 1.56 20 cis-13-Dich1oropropene 0.0250 0.0274 0.0278 110 ill 77.7-124 1.37 20 _. . __._.._ _p_ trans-1,3-Dlchloropropene _.________ 0.0250 ___. _.. 0.0272 _ _..____ _ 0.0279 ._. 109 112 73.5-127 2.51 _ .. 20 Ethylbenzene 0.0250 0.0220 0.0222 87.8 88.6 80.9-121 0.890 20 .Methylene Chloride 0.0250 0.0226 0.0245 90.4 97.8 69.5-120 7.87 20 1,1,2,2-Tetrachlomethane 0.0250 0.0221 00229 884 91.6 79.3-123 3.47 20 detrachloroethene 0.0250 -0220 V 0.0227 88,0 90.9 73.5130 3.15 20 Toluene 0D250 0.0248 0.0250 99.0 99.9 77.9-116 0.850 20 d,1,LTrichloroethane 0.0250- .. � OA267 _.___ 0.0271 _ 107 ,. 109 71.1-129 1.76 20 1,1,2-Trichlorcethane 0.0250 0.0230 0.0237 92.0 95.0 81.6-120 3.17 20 __.___-____-_--__-__- rTrichloroethene 0.0250 0.0239 0.0242 95.5 96.7 79.5-121 _ .. T 20 Trichlorofluoromethane 0,0250 0.0243 0.0252 97.1 101 49.1-157 3.86 20 Vinyl chloride 0.0250 0.0258 0.0262 103 105 61.5-134 1.59 20 (SJ Toluene-d8 106 105 90.0-115 (S) Dibromofluorome(hane 100 101 79.0-721 (S)a,a,o-7rilluorotoluene 102 101 90.4-116 (S)4-Bromolluorobenzene 99.5 i 97.0 80.1-120 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG927281 _Pesticldes_(GC). by. Method EPA 608____ Method Blank (MB) QUALITY CONTROL SUMMARY - ONE LAB. NATioNW1 E. L872799.01,02-..- (MB) R3178862-3 11/17/1612:32 Analyte M8 Result mg/I MB Oualifler MB MDL mg/I MB RDL mg/I Aldrin U 0.00000813 0.0000500 Alpha BHC _ U _ 0.0600166 a0000500 Beta BHC U _ 0.0000184 0,0000500 '0elta BHC U 0.0000197 0.0000560 Gamma BHC U 0.0000176 0.0000500 44-DDD U - 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 '4,4-DDT U O.00D0177 0,0000560 Dieldrin U 0.00000751 0.0000500 .Endosulfan I _ U 0.0000M 0,0000560 Endosulfan II _ U _ _ _ 0.0000176 0.0000500 Endosulfan sulfate U 0.0000196 Endrin _ _ U _ 0.0000189 _0.0000500 0.0000500 J _ - IEndrin aldehyde U _ _ _ _ _ (.0000142 - 0.0000500 Endrin ketone U 0.0000170 0.00OD500 'Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide _ _ U _ _ _ _ 0.0000175 0.0000500 'Hexachlorobenzene U 0.0000134 0.0000500 Methoxychlor _ _ _ U _ _ _ 0.0000193 0,0000500 Chlordane U 0.0000977 0.000500 Toxaphene U 0.000168 0,000500 (5) Decochlorobiphenyl 81.0 70.0-156 (S)Tetrochloro-m-x)lene 72.7 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3178862-1 11/17/16 12:05 • (LCSD) R3178862-2 11/17/16 12:18 Fp ITC 3Ss QCn Fr E - - - aAl . 9Sc Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Oualifier LCSD Oualifer RPD RPD Limits Analyte mgll mg/1 mg/1 % % % % % Aldrin 0.00100 0.000925 0.000751 92.5 75.1 10.0-120 20.7 33.9 Alpha BHC 0.00100 0.000999 0.000751 99.9 75.1 53.6-125 J3 28.4 22.3 Beta BHC 0,00100 0.000976 0,000830 97.6 83.0 55,8-130 162 20.6 ;Delta BHC 0.00100 0.000990 0,000855 99.0 85.5 42.2-135 14.7 23.3 Gamma BHC 0,00100 0.000995 0.000796 99.5 79.6 54.7-125 J3 22.2 21.1 '4,4-DDD 0.00700 0.000963 0.000857 96.3 85.7 47.6-144 11:7 24.3 44-DDE 0.00100 0.000937 0.000819 93.7 81.9 45.0-124 _ _ 13.4 _ 25.7 '4,4-DDT 0.00100 0.000922 _ 0.000820 92.2 82.0 49.8-130 11.7 25A Dieldrin O.00100 0.000952 0.000835 95.2 83.5 55.0-127 _ _ 13.1 _ 22.9 Endosulfan 1 0.00100 �0.000974 0,000 445 97.4 84.5 54.7-127 14.2 24.3 ACCOUNT: .PROJECT: SDG: DATE/TIME: PAGE: WG927281 QUALITY CONTROL SUMMARY _Pesticides_,(GC) by_Method_EPA 608_ _ _ L872799-01602 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3178862-1 11/17/16 12:05 • (LCSD) R3178662-2 11/17/16 12:18 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyte mg/I mg/I mg/I % % % % Endosulfan II 0.00100 0.000963 0,000860 96.3 86.0 53.1-135 Endosulfan sulfate 000100 0.000960 0.000858 96.0 85.8 51.5-132 _ Endrin 000100 0000975 0.000861 975 86.1 50.1-131 _ .Endrin aldehyde _ _ _ 0.00100 !_ _ 0.000905 0.000784 r 90.5 _ 78.4 _ 39.5-137 Endrin ketone 0,00100 O.OD101 0.000902 101 90.2 53.5-139 ,Heptachlor 0.00100 0.000842 0.000661 84.2 66.1 20.7-127 Heptachlor epoxide 0.00100 0.000970 0.000832 97.0 83.2 564-124 -Hexachlorobenzene 0.06100 0.000848 0.000636 84.8 63.6 26.7-114 Methoxychlor 0,00100 0,000942 O.00D864 _ 94.2 86.4 48.2-144 (S) Decochlorobiphenyl 876 79.1 70.6-156 (5)Te(rochloro-m-xylene 83.3 60.3 13.9437 ONE LAB. NATIONWIDE. V RPD Limits TA 23.5 _. 11.1 26.3 _. 12.4_ _... 29.1 . 14.4 HA 10.9 28.4 - 24.1 305 15.2 23.1 J3 28.6 27.6 - - - 8.72 27.8 v FTC ass �Cn 6Sr 0 7GI aAl BSc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG926876 QUALITY CONTROL SUMMARY - ONE LAB. NATIONWIDE. _Polychlorinated_Biphenyls-((;C),by Method_EPA-608,. _ 1-872799-01,02_ - Method Blank (MB) F- (Mat R31/8503-1 11/16/161101 MB Result MB Ouali(ier MB MDL MB RDL Analyte mg/I mg/I mg/I PCB 1260 U 0.000120 0.000500 ,PC8 1016_ _ U 0.000100 0.000506 PCB 1221 U 0,0000730 0.000500 'PCB 1232 U _ 0.0000420 0.000500 PCB 1242 U 0.0000470 0.000500 PCB 1248 _ _ U _ 0.0000860_ _ 0.000500 PCB1254 U _ 0.0000470 0.000500 (S) Decachlorobiphenyl 55.4 10.0-156 (S)Tetrochloro-m-xylene 46.3 _ 13.9437 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Tc 3SS En Fr ce (LCS) R3178503-2 11/16/16 11:14 • (LCSD) R3178503-3 11/16/16 11:26 1 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Oualifer LCSD OualiFler RPD RPD Limits aAI Analyte mg4 mg4 mg4 % % % % % PCB 1260 0.00250 0,00172 0.00197 69.0 78.7 477-149 13.2 28.8 _ ___. ____._ .__. _ -_' __ PCB 1616 0 00250 0.00187 0.00207 _. 75.0 82.9 24.7-128 10.0 34.9 SC (S) Decachlorobiphenyl 59.1 67.3 10,0-156 (S) reVachlam-m-rylene 50.1 55.6 13.9-137 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG926871 _ QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. � Semi Volatile Or,ganlc Compounds_(GC/.MS) by_Melhod 625 - _ _ 1872799-02 Method Blank (MB) F (MB) R3178733-3 11/16/16 12:04 MB Result MB Qualifier MB MDL MB RDL z Analyte mg/1 mg/I mg/I TC Acenaphthene U 0.000316 0.00100 'Acenaphthylene U 0000309 0.00100; 3 S Anthracene U 0 000297 0.00100 Benzidine U 000432 O.O100 4Cn Benzo(a)anthracena U 00000975 0.00100 'Benzolb)fluoranthene U 00000896 0.00100 Benzo(k)fluoranthene U 0000355 0.00100 8enzc(g;hJ)pery1ene U 0 00016-1 0.00100 8enzo(a)pyrene U Bis(2-chlorethoxy)methane U 0.000340 0000329 0.00100 0.0100 �• Bis(2-chloroethypelher U 0.00162 0.0100 fBis(2-chlaroisopropyl)ether U 0.000445 0.0100 7 4 Bromophenyl phenylether U 0.000335 0.0100 .__ _.-- 2 Chloronaphthalene U 4 Chlorophenyl phenylether U - _ 0.000330 0.000303 __ 0.00106 0.0100 A Cf rysene U 0 000332 0 00100 T - - - - - - Dibenz(a.h)anthracene U 0.000279 0 00100 Sc 33 Dichlorobenzidine U 0,00202 0 0100 , 24-Dinilrotoluene U 0.00165 0.0100 - 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.000310 0,00100 Fluorene U 0.000323 0.00100 - Hexachlorobenzene U 0.000341 0.00100 .Hexa'hlor0-1,3-butathen e U 0.0 0032 9 0.0100 Hexachlorocyclopentad iene U 0,00233 0.0100 'Hexachloroethane U 0.000365 0.0100 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 sophorone U 0.000272 0.0100 Naphthalene U 0.000372 0,00100 iNitrobenzene U - 0,000367 0.0100 }. n-Nitrosodimethylamine U 0.00126 0.0100 ;n-Nhrosodiphenylamine U 0.000304 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 -Phenanthrene U 0.000366 0,00100 Benzylbutyl phthalate U 0,000275 0.00300 'Bis(2- ethyl hexyl)phthalate U 0.000709 0.00300' Di-n-butyl phthalate U 0.000266 0.00300 ;Diethyphthalate U 0.000282 0.00300r Dimethyl phthalate U 0.000283 0.00300 (Di-n-octyl phthalate 0,00207 J 0.000278 0.00300 .ACCOUNT: -PROJECT: SDG: DATE/TMME: PAGE: WG926871 QUALITY CONTROL SUMMARY -_Semi Volatile Organic Compounds _(GC/MS)_by Method 625 _ - L972799-02 Method Blank (MB) (MB) R3178733-3 11/16/16 12:04 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Pyrene U 0.000330 0.00100 1,24-Trichlorobenzene U 0.600355 0.0100 4-Chloro-3-methylphenol _ U _ _ _ _ 0.000263 0.0100 2-61orophenol _ U 0.000283 0.0100 2,4-Dichlorophencl U _ 0.000284 0.0100 ';2,4-Dimethylphenol U 0.000624 0.0100 4,6-Dinum-2-methylphenol U 0.00262 0.0100 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U _ _ _ 0.00201 0.0100 Pentachlorophenol U 0.000313 _ 0.0100 Phenol U 0.000334 0.0100 2,4,6-Trichiorophenol U 0.000297 0.0100 (S) Nitrobenzene-d5 62.0 21.8-123 (S) 2-Fluorobiphenyl 725 29.5-131 (S) p- Terphenyl-dN 79.5 _ _ 29.3-137 (5)phenol-d5 16.1 5,00-70.1 (S)2-Fluorophenol 26.7 �- - _ 10.0-7791 (S) 24, 6-TrIbromophenol 724 11.2-130 ONE LAB. NATIONWIDE. FP �Tc - 3SS QCn . 7 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG927135 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile_ Organic Compounds :(GC/MS)_by-Method 625 _ _ - _ L872799-01 Method Blank (MB) (MB) R3179125-3 11/17/161749 Cp MB Result MB Qualifier MB MDL MB RDL z Analyte mgA mg/I mg/I TC Acenaphthene U 0.000316 0.00100 'Acenaphthylene U 0000309 0.00100 3S5 Anthracene U 0000291 0.00100 Benzidine _-_ U - _. 000432 _.__ 0.0100 Benzo(a)anthracene U 00000975 0.00100 Cn IBenzo(b)fluoranthene U 0.0000896 0.00100 Benzo(k)fluoranthene U 0,000355 0.00100 'Sr Benzo(g,h,i)perylene U 0.000161 0.00100 . Benzo(a)pyrene U - 0.000340 _ 0.0D100 'Bis(2-chlorethoxy)methane U - 0.000329 0.0100 BiSl2-chloroethyllether U 0.00162 0.0100 Bis(2-chloroisopropyl)ether U 0.000445 0.0100 GI 4-Bromophenyl phenylether U 0.000335 0.0100 2 Chloronaphtfialene U 0000330 0.001001 ' 4Chlorophenylphenylether U 00003D3 00100 A� Chrysene U 0.000332 0.00100 Dibenz(a,h)anthracene U 0000279 0,00100 SC 33 Dn:hlorobenzidine U 0.00202 0.0100 2,4-Dinitrotoluene U 0.00165 0.0100 2,6-D Drivel-o lue- U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 ,Fluorene U 0,000323 0,00100 Hexachlorobenzene U 0.000341 0.00100 ,Hexachloro-13-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0.00233 0,0100 Hexachloroethane U 0000365 0.0100 Indeno(t2,3-cd)pyrene U 0.000279 0.00100 ,Isophorone a 0.000272 0.0100 Naphthalene U 0.000372 0.00100 - Nitrobenzene U 0.000367 0.0100 n-Nitrosodimethylamine U 0.00126 0.0100 n-Nitrosodiphenylamine U _ 0,000304 0,0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 0.00100 Benzylbulyl phthalate U 0.000275 0.00300 IBisl2-ethylhexygphthalate 0.00109 J 0.000709 0.00300T Di-n-butyl phthalate U 0.000266 0,00300 Diethyl phthalate U 0.000282 0.00300 . Dimethyl phthalate U 0.000283 0.00300 Di-n-octyl phthalate HUM J 0.000278 0.00300 , ACCOUNT: PROJECT: SDG: DATEfrIME: PAGE: WG927135 v QUALITY CONTROL SUMMARY Semi Volatile Organic, Compounds-.(GC/MS) by Method 625 L872799-01 Method Blank (MB) ONE LAB. NATIONWIDE. (MB) R3179125-3 11/17/161749 MB Result MB Qualifier MB MDL MB RDL Analyte mgll mg/I mgll Pyrene U 0,000330 0.00100 1,2,4drichlorobenzene J 0-.000355 0.0100 - 1,2-Diphenylhydrazine U 0.000318 0.0100 - 4-61oro-3-methylphenol U 0.000263 0.0100 -- 2-Chlorophenol U 0.000283 0.0100 2-Nilrophenol U - 0.000320 0,0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0.0100 Phenol U 0.600334 0.0100 2 4 6-Trichlorophenol U 0.000297 0.0100 24-Dichlorophenol U 0.000284 0.0100 '24-Dimethyl Phenol U 0.000624 0.0100 4,6-Dinitro-2>methylphenol U 0.00262 0.0100 2,4-Dinitrophenol -U 0.00325 - O.0100 SJ Nitrobenzene-d5 _ 68.0 _ 21.8-123 (S)2-Fiuorobiphenyl 73.1 .. _ . 29.5-131- (S) p-Terphenyl-d14 - 81.2 . 29.3-137 _ (S) Phenol-d5 19.8 5.00-70.1, - - -- - - - - (S)2-Fluorophenol 29.8 10.0-779 - ._ _ - (S) 2,4.6-Tribromophenol . 61.5 11.2-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3179125-1 11/17/1617:02 • (LCSD) R3179125-2 11/17/16 17:26 Spike Amount LCS Result LCSD Result Analyte mgll mgll mg/I LCS Rec. % LCSD Rec % Rec. Limits % LCS Oualifier LCSD Qualifier RPD % RPD Limits % Acenaphthene 0.0500 0.0308 0.0370 61.6 74.0 38.7-109 18.2 21.5 Acenaphthylene 0.0500 _ 0.0326 _ _ 0.0391 65.2 _ 78.2 36.0-106 18.1 21 Anthracene 0.0500 0.0325 0,0386 65.1 77.1 43.6-113 _ 17.0 18.8 ;Benzidine 6.0500 _ 0.0249 _ 0.0297 49.7 59.4 10.0-165 17.8 40 Benzo(a)anthracene 0.0500 0.0313 0.0377 62.5 75A 51.2-112 _ _ 18.7 _ 20 Benzo(b)fluoranthene _ 0.050_0 0.0315 _ 0.0380 63.1 76.0 47.6-111 18.6 20 - Benzo(k)Fluoranthene 0.0500 0,0318 0.0393 63.7 78.6 49.4-114 J3 21.0 20 Benzo(g,h,i)perylene 0.0500 -0.0330 0.0397 66.0 79.5 45.2-117 18.5 20 Benzo(a)pyrene 0.0500 0,0287 0.0347 57.4 69.3 45.6-106 18.8 20 Bis(2-chlorethoxy)methane 0.0500 0,0305 0.0375 60.9 74.9 37.2-111 26.6 24.1 Bis(2-chloroethyl)ether 0.0500 0.0275 0.0327 55.0 65.4 22.6-108 17.2 27.9 'Bis(2-chloroisopropyl)ethei 0.0500 0.0304 0.0371 60.7 _ 74.2 32.9-100 20.0 25.1 4-Bromophenyl-phenylether 0.0500 0.0314 0.0369 62.8 73.8 40.7-116 _ _ 16.1 21 Cp z Tc 3C$ QCn SSf ce 7GI aAl 9Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: QUALITY CONTROL SUMMARY ONE LAB, NaTioNwTDE. WG927135 �?�� LSemi Volatile-Or;ga nic Compou nds_(GC/M S) by_Method-625 L872799-01_ Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3179125-1 11/17/1617:02 • (LCSD) R3179125-2 11/17/1617:26 Cp Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 2 Analyte mg/I mg/I mg/I % % % % % TC 2-Chloronaphthalene - 0,0500 0,0282 0.0339 56.4 1 67.9 33.6-105 18.4 23 - 4Chlorophenylphenylether 0,0500 0,0309 00364 618 723 39.0113 163 2(1 3SS _ Lhrysene 0.0500. .03 _ 00330 __ 00401 659 80.3 54.6120 _ 197 20 l Dibenz(ah)anthracene 0.0500 0.0297 00363 594 72.5 42.8118 199 20 4Cn 33Dichlorobenzidine 00500 0.0316 00389 631 778 27.2-142 209 223 2,4-Dinitrotoluene 0.0500 0.0307 0.0369 61.3 73.9 31.2-105 18.6 22 126Dmitrotoluene 0:0500 00295 00365 59.0 73.0 30.6106 212 231 r Fluoranthene 0.0500 0.0326 0.0385 65.2 77.0 45.9115 16.6 20 Fluprene .____ 0.0500 _.__ 0 0321 - ::_ 0,0380 ._ 64.2 __ 76.0 __ 41.0-112 _ _- _.. -._. _. - . __ 16.8 _ _ __ 20.2 Hexachlorobenzene 00500 00312 00378 62.4 75.6 38.5-116 191 201 �• _ IHexachloro-1,3butadlare. ,_- 0-0500 T.s.__. 00219, _. _ 0:0283 _ 437 56.6 761-104 - 257 312 ' Hexachlorocyclopentadiene 00500 0,0251 0.0311 50.2 62.2 10.0-121 21.3 279 Ne�xachloroethane'- 0.0500, 0.0204 0.0259 40.9 51.7 16.5-898 23.5 307 nden o(123cd)pyrene sophorone ' 0.0500 0,0304 00369 607 64.4_ 73.8 �r __ _- 78.6 v 45.0116 _ _._ .._ _ 35.4112 _ _ _ 19.5 _199 20 2L5 IE s AI ___._ 00500 _ ..__ 0.0322 �..�,- 0.0393 Naphthalene 0,0500 0,0272 0.0341 54.3 68.2 32.2-101 22.6 23.8 Mitrobenzene 0.0500 -0:0286 00352 571 r 70.5 31.4-106 209 257, 5 SC n NihosodimethY lamloe 0.0500 00161 00179 32.1 359 100-801 11.0 37.5 n Nitrosodiphenylamthe. 00500 0:0328 0.0392 fi5.6 78.4 44.4113 - 179 20 n-Nltrosodl-n-propylamine 0.0500 0.0319 0,0381 ISIS 76.3 33.2-106 - 17.8 23.7 ;Pherommene 0.0500 0.0313 - 0.0372 62.6 74.5 4fi.4-113 17.4 20 Benzylbutyl phthalate 0,0500 0,0305 0.0374 61.0 74.8 31.8-123 20.3 20.7 l_ ___-__ __-.__._ Bls(2 ethylhexyl)phthalate 0.05D0 T_3-- 0.0323 - ___ __ 0.0394 .__. 646 __. 78.9 36.9134 _. 199 236 - 1 Di-n-butyl phthalate 0.0500 0.0342 0.0404 68.5 80.8 41.8-120 16.5 20.2 (Diethyl phthalate. 0.0506 .0:0322 0.0367. 64.5 77.3 36.5-129 18.1 20 Dimethyl phthalate 0,0500 0,0324 0.0381 64.7 76.2 35.3-128 16.2 20.8 ,Di -n-octylphthalate 0,0500 0.0301 0.0363 60.2 72.6 - 39.7-112 187 21.1 Pyrene 0.0500 0.0334 0.0406 66.8 81.2 46.3-117 19.5 20 124Trichlorobenzene 00500 _ 0,0232 00302 46A 60.4 22.9-96.1 26.2 27.5 _ 1,2-Diphenylhydrazlne 0.0500 0.0291 0.0345 58.3 691 37.6-111 17.0 21.1 4-Chlor0-3-methylphenof 0.0500 0.0290 0.0333 57.9 66.7 35.7-100 14.0 22.9 2-Chlorophenol 0.0500 0.0254 0.0282 50.8 56.4 262-91.5 10A 26.5 2,4-Dichlorophenol 0.0500 : 0.0302 0.0356 60.3 71.2 31.4-103 16.6 24.9 2,4-Dim ethyl phenol a0500 0,0289 0.0325 5Z8 65.0 31.9-107 11.7 257 ;4,6-Dinitro-2-methylphenol 0.0500 -0,0304 0.0332 60.7 66.4 18.4-148 8.92 24.4 2,4-DinitropInena1 0.0500 0.0208 0.0158 41.6 31.6 24.2-128 J3 27.3 20.5 2-Nitrophenol 0.0500 0.0276 0.0347 55.1. 69.5 25.9-106 23.1 26.9 4-Nitrophenol 0.0500 0.00950 0.00955 19.0 19.1 10.0-527 0.520 40 Penmchloroteinof 0.0500 0.0281' 0.0320 56.3 63.9 10.9-974 12.7 35.1 Phenol 0.0500 0,0118 0.0109 23.6 21.8 10.0-57.9 7,84 35 ACCOUNT:. 'PROJECT: SDG: DATE/TIME: PAGE: WG927135 QUALITY CONTROL SUMMARY ONEiAe.NATIONwibE. _Seml-Volatile Organic Compounds _(GC/MS)_by, Method. 625 - _ ,.,.. L872799.07_ Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3179125-1 11/17/16 17:02 • (LCSD) R3179125-2 11/17/16 17:26 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % 2,4,6-Trichlorophenol 0.0500 0.0318 0.0376 63.6 75.2 29.8-107 16.7 24.1 (SJ Nitrobenzene-d5 63.7 756 21.8-123 Fluorobiphenyl 68.5 77.5 29.5-131 - - (5)p-Terphenyl-d74 70.6 80.0 29.3-137 - l51 Phenol-d5 - 26.9 22.8 5.00-70.7 (5) 2-Fluorophenal 374 354 100-779 - ---- (5)2,4,6-Tribromophenol 671 75,0 11.2-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. Cp MDL _ Method Detection Limit. _ z RDL Reported Detection Limit. Tc U Not detected at the Reporting Limit_ (or MDL where applicable) RPD Relative Percent Difference. Original Sample The non spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) Ss from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control En Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring - - Rec. recovery_ Surrogates are not expected to be detected in all environmental media. - - - - - Recovery _ s Sr Qualifier Description roc B E The same analyte is found in the associated blank. The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL) J The identification of the analyte is acceptable, the reported value is an estimate 8AI J3 The associated batch_OC was outside the established quality control range for precision. J4 The associated batch CC was outside the established quality control range for accuracy. e Sc ACCOUNT: PROJECT: SDG DATEfrIME: PAGE: ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. 0 ESC Lab Sciences is the only environmental laboratory accreditedkertified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle our needs throughout the country. capacity and capability from our single location laboratory is comparable to the collective totals of the <es P P Y 9 ry P Y P Y 9 ry P network laboratories in our industry. The most significant benefit to our `one location' design is the design oPour laboratory campus. The model is conducive to accelerated productivity, decreasing turnaround time, and preventing cross contamination, thus protect ng sample integrity, Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. ' Not all certi Oca Lions held by the laboratory are amuIca ble to the results reported in the attached report. State Accreditations Alabama 40660 _ Nevada TN-03-2002-34 Alaska _ UST-080 _ New Hampshire 2975 Arizona AZ0612 New Jersey NELAP TNO02 Arkansas 98_0469 New Mexico _ TN00003 California 01157CA New York 11742 Colorado TN00003 North Carolina _ Env375 Conneticut PH-0197 North Carolina' _ _ _ DW21704 _ ___ Florida _ _ _ E87487 _ North Carolina' 41 Georgia NELAP North Dakota —_ R-140 Georgia' 923 Ohio—VAP___ _ _ CL0069 _ Idaho _ TN00003 ____ Oklahoma _ _ _ _ 9915 Illinois 200008 ---------- Oregon TN200002 --- -- Indiana C-TN-01 Pennsylvania _ _ _ _ 68-02979 Iowa _ 364 Rhode Island _ _ 221_ Kansas _ E-10277 South Carolina 84004 Kentucky' _ _ _ 90010 South Dakota _ nla Kentucky' 16 _ Tennessee" _ _ __ _ 2006 Louisiana A130792 Texas T104704245-07-T% Maine TN0002 Texas' _ LABO152 Maryland 324 Utah 6157585858 Massachusetts _ _ _ M-TNO03 Vermont _VT2006 _ _ Michigan _ — 9958 ---- Virginia--------—_-- 109 Minnesota 047-999-395 Washington C1915 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 _ Montana CERT0086 _Wyomi n_g_ ____ A21LA _ Nebraska _ _ NE-OS-15-05 Third Party & Federal Accreditations A2LA—ISO 17025 1461.01 AIHA-------078 -109--_------- A2LA—ISO 17025' 1461.02 DOD 1461.01 Canada 14fi1.01 - USDA ��-—--5-67674--_-----------_ EPA_Crypto_ _ TN00003 `Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ' ChemicallMicrobiological s Mold " Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. T W4 MT ryD N.E OR • MN T ID • SD WI v• NY • n Tm T T T ? G • T T A T NV NET T UT T T T T T 16 Ile CA T CO • KSM• • VA T • KV • _ T T •_r-Q • •l—TR N T AZ OT T • NM An? SC T • T T M.5 AL G4 T IX TT f LA �• • �T e AK t • p FL ro B HI `> P CCp 2Tc 3Ss 4Cn SSr 6QC rGI 9Sc ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Billing lnfarmation; Anal tit/ Contalrscr/Preserwtive Chain oI Cui:odY Company Name/Address: � C Eaton'Corporation NAFinanciai�PO Boz 818024 OJJ,�� 2564 Durham Rd . Cleveland, OH 44181-8024 i ( L-A o Roxboro; NC127573 11 ,m"'I 1 ❑Ob la non Ad �! Qi ' i N •N' O off'+ '. h+uf UdeltnD101 Emell TM r ., Repon to: f - r.a` 1~0 L O' Pl L1 ces9 Dustin LaClair ustinlaclair@Eaton.com- t c>9 u o 7 7^t 61slStlErs9 cu4/state x. xzr:_- Profe¢. Cg4lected: ROXboro,lNIC �. '• _ EafoniCorp.;Seml Annual Stom+water tm, z c ho) Q t•d%M�% ,.9 Deudptian:: CllentProJceto '•tabPriapa9' ... r km. a0 Qi,l ,;, ` B 0 vhene:336 599,1141 28091-R EATONRNC?28091SW t± 3 -- I.E �L,. , 3 Fa:: ° m o E 'Wti m �? 11 AianumfATONRNC; sitq/Fadlity IDR P.O.a �� rv'. o r._e, E ,E {ayge+aetl oY lPrintl: IW 1ca, 'N jEr, c r`o rl r { sl natD'r Rush?- MUST, Notific II Date Results Needed % �t y Q) Vrelagln Collected by,l C x K' x % vi, TSfld~ Hunt tmmailla i. ?t°av ...........:40% Email? YiS V No�.YCS' No. � rpi a �� O �. � 3ht Ped tFAX? XNd a p via.,, alol h $erv,, �/ lhrra Dal _::2S% o I'll,N !i o•• i . r' fn• rL- . ..w 'l inae ntrs to aJ' 7 ♦tNO tN0 •lb •� tlamlCwim l•.m LrrgY OnbonMl Sample ID. tComp/Grab' . MatriM • Depth Dare. 4 1 9.p16`.=li-tH-Oo5 � Gc��t�j: ;wW 1 .i— ,pH Temp _ GW Groundwater 'w: olt WW-WasteWtter DW-DrinkingWarer.OT Other Matrlss SNoltla4 C' Flow- Otherall a a••.. - ' Remarks 'Replace kit upon;arrival at lab` (pV S b3 -i 5ampies rewrned via: ❑uPs ' Relinqurched by:{Signal i Date:, Time: RetClvrd ayrlSlgnat4Eei Condition:' ilab usq only) //y�O �i 1 FedEs ❑Ctlurier ❑� �IL8. . .E L. _ry. . +- �gpttles RCcelvedt Date: Time: Received bY ISlgnatVroTT� T mp - eiinquishea ny:151 atutel[ �, " , ,.�., "; _. CO[ Seel lntatt YI Nr "NA'' DAM',—H Checkad NCi S natural" Date: Time: Rgcerved for.lab by (IB Rellnquishad by:'ISIHnat!;r.�) Wy,,o u,FL-,L-A 13 �O,P,�! •s - eteipt Fole. sacra G87Z �99 Cooler. Received/QpcneB On:-111.IS /16 f'empetnture Upon Receipt: Z •z. °c Received By:, signature: ^No Receipt Check List Yes N%A y seals on outside:of cooler and intact? y.papers prs arrive in good condition? F�_6 'bottlesused for'tfie_analyses;requeat amount of sample sent in each bottle? / Were all applicable sample containers;correctlyjpreservedfan'dl' clleckedafor preservaLion7 {Anylriot In acceptedrange noted'onfGOC)' _ _: if applicable, was amo6seru6ble VOA headspace present? `�eii,n�CnnfririnancetGerierated'>(If;.vessee:attaciied.NGF)� ,, REAL TIME OPiA PGGE55 M F•'' r ANALYTICAL REPORT September 26, 2016 .?al lv VCG- 0366a_7 RECEIVED Eaton Corporation OCT 2 4 Z016 Sample Delivery Group: L860714 Samples Received: 09/20/2016 CENTRAL FILES DWR SECTION Project Number: 28091-R Description: Eaton Corp Semi -Annual Stormwater Site: ROXBORO, NC Report To: Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: / LJ- Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures'. 060302, 060303, and 060304) TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cover Page 'Tc: Table of Contents 'Ss: Sample Summary 'Cn: Case Narrative 5Sr: Sample Results 2016-09-19-005 (TOOL ROOM TRENCH) L860714-01 `Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 Volatile Organic Compounds (GC/MS)by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 'Gl: Glossary of Terms "Al: Accreditations & Locations 9Sc: Chain of Custody 1 2 3 4 5 5 9 9 10 11 12 14 16 17 21 22 23 11 ACCOUNT: Eaton Corporation PROJECT: 28091-R SDG: L860714 DATEMME: PAGE: 09/26A6 14:55 2 of 24 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected dateltime Received date/time 2016-09-19-005 (TOOL ROOM TRENCH) L860714-01 WW Kirk Spicer 091191160915 09120/1609:00 C P Method Batch Dilution Preparation Analysis Analyst date/time date/time a Tc Gravinetric Analysis by Method 2540 D-2011 WG910335 1 09/23/1600:24 09/23/1605:20 1M Metals lCP) by Method 200.7 WG909855 1 09/22/16 09:15 09/22/1616:48 ST Pesticides (GC) by Method EPA 608 WG909588 142 09/20116 21:07 09/2111616:25 VKS Polychlorinated Biphenyls (GC) by Method EPA-608 WG909588 L42 09/20116 2107 09/21/1619:11 JNS Semi Volatile Organic Compounds (GC/MS) by Method 625 WG910521 1.11 09/2311618:13 09/25/16 2117 JF ° Cn Volatile Organic Compounds (GUMS) by Method 624 WG910110 1 09/21/16 23:59 09/21116 23:59 DAH Wet Chemistry by Method 1664A WG909710 1 0921116 11:06 09/21It616:29 SHG s $f ACCOUNT: PROJECT: BEG: DATE/rIME: PAGE: Eaton Corporation 28091-R L860714 09Y26YI614:55 3 of 24 CASE NARRATIVE ONE LAB. NATIONWIDE. ' All sample aliquots were received at the correct temperature, in the proper containers, with the c p appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOO) values reported for environmental samples have been corrected for the dilution factor used in the jTc analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the 3S5 laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Fri I�� 6QC JIF � G I Jimmy Hunt eAl Technical Service Representative } t � ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L860714 09/26/1614:55 4 of 24 20,16-09-19-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 09/19/16 09:15 L860714 Additional Information Result Units Cp Analyle pH (On Site) 6.6 all FTCTemperature (on -site) 24.5 Deg. C aSs Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch ° Cn Analyze mgA mgA mgA date/time Suspended Solids 5.27 0.350 2.50 1 09/23R016 05:20 WG910335 Wet Chemistry by Method 1664A 6 Result Qualifier MOILRDL Dilution Analysis Batch QC Analyte mgA mgA mgA date/time TPH -Oil&Grease U 0725 SR8 1 09/21/201616:29 WG909710 7GI Metals (ICP) by Method 200.7 eAl Result Oualifer MDL RDL Dilution Analysis Batch 9 Analyze mgA mill mgA date/time Copper 0.0333 0.00700 0.0100 1 09/22/201616:48 WG909855 SC Lead 0.00296 J 0.00200 0.00500 1 09/22/201616:48 WG909855 Zinc 0.0359 J 6.00340 0.0500 1 09/22/201616:48 WG909855 Volatile Organic Compounds (GC/MS) by Method 624 Analyze Result mgA Qualifier MDL mg4 RDL mgA Dilution Analysis date/time Batch Acrolein U J4 0MSK 0.0500 1 09/211201623:59 WG910110 Acrylonitrile U 0.0016 0.0100 1 09/2l/201623:59 WG910110 Benzene U 0.000331 0,00100 1 09/21/201623:59 WG910110 Bromodichloromethane U 0.006380 0.00100 1 09/21/201623:59 WG910110 Bromoform ._ U 0,000469 0.00100 1 09/21/201623:59 VIG910110 Bromomeihane U 0.006866 0.00500 1 09/21/201623:59 VIG910110 Carbon tetrachloride U 0000379 0.00100 1 09/21/201623:59 WG910110 Chlorobenzene U 0A00348 0.00100 1 09/21001623:59 WG910110 Chlorodibromomethane U 0.000327 0.00100 1 09/21/2016 23:59 WG910110 y Chlomethane U 0.000453 0.00500 1 09/21/2616 23:59 WG910110 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 09/21/2016 23:59 WG910110 Chloroform U 0.000324 0.00500 1 09/21/2016 23:59 WG910110 Chloromethane U 0.000276 0,00250 T 09121/201623:59 WG910110 1,2-Dlchl6robenzene U 0.000349 0,00100 1, 09/2l/2016 23:59 WG910110 N 1,3-Dichlorohenzene U 0.000220 0,00100 1 09/21/2016 23:59 WG910110 1,4-Dichlorobenzene U 0.000274 0.00100 1 09/21/201623:59 WG910110 Dichlorodifuoromethane U 0.000551 0.00500 1 09/21/201623:59 WG910110 1,1-Dichloroethane U 0.000259 0.00100 1 69121/201623:59 VIG910110 1,2-Dichloroethane U 0,000361 0.00100 .1 09/21/201623:59 P/G910110 1,1-Dichloroethene U 0,000398 0.0010o 1 09/21/201623:59 WG910110 Vans-1,2-Dichloroethene U 0,000396 0.00100 1 09/21/201623:59 VJG910110 1,2-Dichloropropane U 0000306 0.00100 1 09/21R01623:59 WG910110 cls-1,3-Dichloropropene U 0,000418 0.00100 1 09121/201623:59 WG910110 trans-1,3-Dichloropropene U 0.000419 0.00100 1 09121/201623:59 WG910110 Ethylhenzene U 0.000384 0.00100 1 09121/20162359 WG910110 Methylene Chloride 7U _ 0.WOO 0.00500 1 09/21/201623:59 VVG910110 1,1,2,2-Tetrachlorcethana U 0,000130 0.00100 1 09/21/201623:59 WG910110 Tetrachlomethene U 0.0003R o.00100 L 09/21/201623:59 WG910110 Toluene'+ U 0,000780 0.00500 J. .' 09121/201623:59 WG910110 "- 1,1,1-Trichloroethane U 0.000319 0.001o0 1 090/201623:59 W6910110 1,1,2-Trichloroethane U 0.000383 0.00100 1 09121/201623:59 WG910110 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L860714 09126/1614:55 5 of 24 2016-09-19-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. ' Collected dale/lime: 09/19/16 09:15 L860714 Volatile Organic Compounds (GC/MS) by Method 624 Analyte Result mgfl Qualifier MOIL mgA ROL mg/I Dilution Analysis date/time Batch Trichloroethene U 0.000398 CD0100 1 09/21/2016 23:59 WG910110 Trichlorofluoromethane U 0.00120 0,00500 1 09/21/201623:59 WG910110 Vinyl chloride U 0,000259 0,00100 1 09/21/201623.59 - WG910110 (S)Toluene-d8 107 90.0-715 09121201623:59 WG910110 (S) Dibromofluommethone 965 79.0-121. 0972U20762359 WG916110 (S) o,o,o- Trifluorotoluene 965 90.4-116 0927201623.59 WG910110 (S)4-BmmoOuorobenzene 95.0 80.1-120 0921201623.59 WG910110 Pesticides (GC) by Method EPA 608 Result Qualifier MDL ROL Dilution Analysis Batch Analyte mgA mgA mgfl date/time Aldrin U 0.0000115 0.0000710 1,42 09/21/201616:25 WG909588 Alpha BHC U J3 0.0000236 0.0000710 1.42 09/21/261616:25 WG909588 Beta BHC U J3 0,0000261 0.0000710 1.42 09/211201616:25 WG909588 Delta BHC U 0.0000280 6.6000710 1.42 69/2V201616:25 WG909588 Gamma BHC U J3 0.0000250 0.0000710 1.42 09/21/201616:25 WG909588 Chlordane _ U 0.000139 0MO710 L42 09121/201616:25 VJG909588 4,4-DDD U 0.0000241 0.0000710 142 09/21/201616:25 WG909588 4,4DDE _ U 0.0000233 0.6000716 1.42 09t2V201616:25 WG909588 4A-DDT U 0.0000251 0.0000710 1.42 091211201616:25 WG909588 Dieldrin U 0.0000107 0.0000710 1.42 091211201616:25 WG909588 Endosulfan I U 0.0000254 0.0000710 T42 09121/201616:25 WG909588 Endosulfan II U 0.0000250 0,6000710 1.42 09121/201616:25 WG909588 Endosulfan sulfate U 0.0000278 0.0000710 1.42 09/21/201616:25 WG909588 Endrin U 0.0000268 0.0000710 1.42 0901/201616:25 VJG909588 Endrin aldehyde U 0.0000202 00000710 1.42 09/211201616:25 WG909588 Endrin ketone U 0.0000241 0.0000710 142 09121120161625 WG909588 Heptachlor U 0.0000153 0.0000716 1,42 09/21/201616:25 WG909588 Heptachlor epoxide U 0.0000248 0.6000710 142 09/211201616:25 WG909588 Hexachlorobenzene_: U 0.0000190 0.0000710 1.42 09/21/201616:25 WG909588 Methoxychlor U 0.0000274 0.0000710 1.42 09T2l/20161625 WG909588 Toxaphene U 0.000238 0.000710 1.42 09121/201616:25 VIG909588 (S) Decochlorobiphenyl 89.8 10.0-756 0921201616.25 VIG909588 'V)Tetrochloro-m-xylene 727 139-137 0912V201616:25 VIG909588 Polychlorinated Biphenyls (GC) by Method EPA-608 Result OualiOer MDL RDL , Dilution Analysis Batch Analyte. mg/1 mg/I mg/I date/time PCB 1016 U 0.000142 0.000710 1.42 09/21/201619:11 WG909586 PCB 1221 U 0.000104 6,600710 1.42 09/211201619:11 WG909588 PCB 1232 U 0.0000596 0.000710 1.42 09121/201619:11 WG909588 PCB 1242 U 0.0000667 0.000710 1.42 09/211201619:11 WG909588 PC81248 U 0.000122 0.600710 1.42 09/21/201619:11 WG909588 PCB 1254 U 0.0000667 0.000710 1,42 09/21/2016 19 11 WG909588 PCB 1260 U 0.000170 0.000710 1.42 09/21/201619:11 WG909588 (S) Decochlorobiphenyl 82.4 10.6-156 0912U201619: 11 VJG909588 (S) Tetrochloro-m-xylene 83.8 13.9-137 09121WO1619: 11 VIG909588 Semi Volatile Organic Compounds (GC/MS) by Method 625 Analyte Result mg/1 Qualifier MDL mg/I RDL mgA Dilution Analysis date/time Batch Acenaphthene U 0.000351 0.00111 1.11 09/25/2016 2117 WG91OS21 Aceliaphthylene U 0.000343 0,00111 1.11 09/25/2016 2117 WG91OS21 Anthracene U 0000323 0.00111 111 09/25/2016 2117 WG910521 Benzidine U 0.00480 0.0111 1.11 09/25/2016 2117 WG910521 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 2809i-R L860714 09/26/16 14 55 6 of 24 2016-09-19-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dale/time: 09/19/16 09:15 L860714 Semi Volatile Organic Compounds (GC/MS) by Method 625 I Result 0ua6rier MDL RDL Dilution Analysis Batch Cp Analyte mg4 mg4 mg/l date/time Benzo(a)anthracene U 0000108 0.00111 1.11 09/25/2016 2117 WG910521 Benzo(b)Fluoranthene U 0.0000994 0,00111 1.11 09/25/2016 2117 WG910521 Benzo(k)huoranthene U 0.000394 0.00111 1.11 09/25/2016 2117 WG910521 Benzo(g.h,i)perylene U 0.600179 0.00111 1.11 09/25/2016 21:17 WG916521 Benzo(a)pyrene U 0.000377 0.00111 1.11 09/25/2016 21:17 WG910521 Bis(2-chlorethoxAmethane U 0,000365 0.0111 1.11 09/25/2016 21:17 WG910521 Bis(2-chloroethypether U 000180 0.0111 1.11 09/25/2016 2117 WG910521 Bis(2-chloroisopropyl)ether U 0M0494 0.0111 1.11 09/25/2016 21:17 WG910521 4-Bromophenyl-phenylether U 0.000372 0,0111 1.11 09125/2016 2117 WG910521 2-Chloronaphthalene U 0.000366 0.00111 1.11 09R5/20162117 WG910521 4 Chlorophenyl-phenylether U 0.000336 0.0111 1.11 09/25/2016 21:17 WG910521 Chrysene U 0.000368 a00111 1.11 09252016 21:17 WG910521 Dibenz(a,h)anthracene U 0.000310 0.00111 1.11 09/25/2016 21:17 WG910521 3,3-Dichlorobenzidine U 0.00224 0.0111 1AI 09125120162117 WG910521 2,4-Dlnitrotoluene U 0.00182 0.0111 111 09/25/2016 2117 WG910521 2,6-Dinitrotoluene U JD06310 0.0111 1.11 0965/2016 2117 WG916521 1,2-Diphenylhydrazlne U 0.000353 0.0111 1.11 09/25/2016 2117 WG910521 Fluoranthene U 0.000344 0.00111 111 09/2512016 2117 WG910521 Fluorene U 0.000358 0.00111 1.11 09/25/2016 2117 WG910521 Hexachlorobenzene U 0.000378 000111 1.11 09t25/20162117 WG910521 Hexachloro-1,3-butadiene U 0.000365 0.0111 Til 09/25/2016 21:17 WG910521 Hexachlorocyclopentadiene U 0.00259 0.0111 1JI 09/25/2016 21:17 VIG910521 Hexachloroethane U 0,000405 0.0111 111 09/25/2016 2117 WG910521 Indeno(1,2,3-cd)pyrene U 0,000310 0.00111 ill 09/25/2016 2117 VJG910521 Isophorone U 0.000302 0.0111 1.11 09/25/2016 2117 VIG910521 Naphthalene U 0.000413 0,00111 1.11 09/2512016 2117 WG910521 Nitrobenzene U 0.000407 0.0111 1.11 09/25/2016 2117 VIG910521 n-Nitrosodimethylamine U 0.00140 00111 1.11 09/2512016 2117 VJG910521 n-Nihosodiphenylarnme U 0.000337 0,0111 1.11 09/25/2016 21:17 VIG910521 n-Nitrosodi-n-propylamine U 0.000447 0.0111 111 09/25/2016 21:17 WG910521 Phenanthrene U 0.000406 0.00111 ill 09/2512016 2117 VIG910521 Benzylbutyl phthalate U 0.000305 0.00333 1.11 09/25/2016 2117 VIG910521 81s(2-ethylhexyl)phthalate U 0.000787 0.00333 1.11 09/25/2016 2117 VIG910521 Di n-butyl phthalate 0.00107 J 0.000295 0,00333 1.11 09M120162117 VIG910521 Diethyl phthalate U 0.000313 0,00333 1.11 09/25/2016 21:17 WG910521 Dimethyl phthalate U 0.000314 000333 1.11 09/25/2016 21:17 VIG910521 Di-n-octyl phthalate U 0.000308 000333 1.11 09/2512016 21:17 VIG910521 Pyrene U 0.000366 0.00111 1.11 69/25/20162117 WG910521 1,2,4-Trichlorobenzene -. U 0.000394 00111 1.11 09/25/2016 2 M7 VJG910521 4-Chloro-3-methylphenol U 0.000292 00111 1.11 09/25/2016 2117 VIG910521 2-Chorophenol U 0.000314 00111 111 09/2512016 2117 VIG910521 2,4-Dichlorophenol U 0.000315 mill 1.11 096ci/201621:17 WG910521 2,4-Dimethylphenol U 0.000693 0,0111 1.11 09125/2016 2117 UG910521 4,6-Dinitro-2-methylphenol U 0,06291 0.0111 111 09125201621:17 V1G910521 24-Dinitrophenol U J3 J4 0.00361 0.0111 1.11 09/25/2016 2117 VIG910521 2-Nitrophenol U 0.000355 0.0111 ill 09/2512016 2117 VIG910521 4-Nitrophenol U 0.00223 0.0111 ill 69/25/2016 2117 UG910521 Pentachlorophenol U 0.000347 0.0111 1.11 09/25/2016 21:17 VJG910521 Phenol U 6.000371 0.0111 1.11 09125/2016 21:17 WG910521 2,4,6-Trichlorophenol U 0.000330 0.0111 1.11 09125/2016 2117 WG916521 (S)1-Fluorophenol 15.9 10.0-77.9 09125201621,O WG910521 (S)Phenoli 9.73 5.00-70.1 012520162L7 WG910521 (S) N7trobenzene-tl5 47.8 27.8-123 0912520162f 17 VIG910521 (S)2-Fluarobiphenyl 67.3 2fl5-131 092520182i17 WG910521 (S)2,4,6-Tribromophenol 42.0 U2430 0912520162LI7 WG910521 (S) pi- Terphenyl-d74 69.5 N4137 0925IM621.17 WG910521 ACCOUNT: PROJECT: SDG: DATEMME PAGE: Eaton Corporation 28091-R L860714 09/26/16 14:55 7 of 24 2016-09-19-005 (TOOL ROOM TRENCH) SAMPLE RESULTS - 01 ONELAS.NATIONWIDE. •� Collected date/time: 09/19/16 09:15 L860714 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg4 mg/l mg4 date/lime z Tc Sample Narrative: 625 L860714-01 WG910521: Dilution due to sample volume 3 SS �Cn FOCI 7G1 BAI 9Sc cI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L8607I4 09/26/1614'55 8 of 24 WG910335 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Gravimetrlc Analysis by Method 2540 D-2011 _ L860714-01 - Method Blank (MB) Cp (ME) R3165901-1 09/23/16 05:20 ❑ MB Result MB Qualifier MB MDL MB RDL Analyte mg/1 mg/1 mg/l x TC Suspended Solids u 0.350 2.50 aSs L86O669-01 Original Sample (OS) • Duplicate (DUP) 4Cn (OS) L860669-01 09/23/16 05:20 • (DUP) R3165901-4 09/23/16 05:20 Original Result DUP Result Dilution DUP RPD DUP Qualifier Analyte mg/l mg/I % DUP RPD Limits % 5 Sr Suspended Solids 229 249 1 8.37 J3 5 L86O91O-03 Original Sample (OS) •Duplicate (DUP) (OS) L860910-03 09/23/16 05:20 • (DUP) R3165901-5 09/23/16 05:20 G Original Result DUP Result Dilution DUPRPD DUP Qualifier DUP RPD Limits Analyte mgll mg/1 % % aAl Suspended Solids 78.0 76.7 1 1.72 5 9Sc Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3165901-2 09/23/16 05:20 • (LCSD) R3165901-3 09/23/16 05:20 Spike Amount LCS Result LCSD Result LCS Rea. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/l mg/1 % % % % % Suspended Solids 773 852 888 110 115 85.0-115 4.14 5 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L860714 DATE/TIME: 09/26A614:55 PAGE: 9 of 24 WG909710 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Wet Chemistry by Method 1664A L860714-01 Method Blank (MB) (MB) R316b1b1-1 09/2U1616:26 MB Result MB Oualifier MB MDL MB ROL Analyte mg/I mg/I mg/I TPH -Oil&Grease U 0.725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3165151-2--09/21/16 16:27 • (LCSD) R3165151-3 09/2111616*28 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Oualifier RPD RPD Limits Analyte mgR mg/I mgA % % % % % TPH -Oil&Grease 20.0 19.3 18.8 96.5 94.0 78.0-114 2,62 18 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L860714 DATE/TIME: 09/26/1614,55 PAGE: 10 of 24 WG909855 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICP) by Method 200.7 L860714-01 Method Blank (MB) (MB) R3165507-1 09/22/16 1559 MB Result Copper U Lead U Zinc U MB Oualifer MB MDL MB RDL mg/I mg/I 0.007 0.0100 0.002 0.00500 0.0034 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3165507-2 09/22/1616:02 • (LCSD) R3165507-3 09/22/16 16:04 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Copper 1.00 1.02 1.04 102 ' 104 85-115 2 20 Lead 1.00 1.01. 1.04 101 104 85-115 3 20 Zinc tA0 1,01 1.03 101 103 85-115 3 20 L860648-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L860648-01 09/22/1616:07 • (MS) R3165507-5 09/22/161692 - (MSD) R3165507-6 09/22/16 16:15 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/1 mg/I mgA men % % % % % Copper 1.00 0.0380 1.11 1.15 107 ill 1 70-130 4 20 Lead 1.00 ND 1.03 W2 103 102 1 70-130 0 20 Zinc 1.00 ND 1.06 1.05 102 102 1 70-130 0 20 L860844-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L860844-01 09/22/1617:16 • (MS) R316SS07-7 09/22/1617:18 • (MSD) R3165507-8 09/22/1617:20 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits MS OuallBer MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Copper 1.00 0.0456 1.09 110 105 105 1 70-130 1 20 Lead 1.00 ND LD2 1.02 102 102 1 70-130 0 20 Zinc 1.00 0.0865 1.08 1.10 100 101 1 70-130 1 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L860714 0926/16 14:55 11 of 24 WG910110 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 L860714-01 Method Blank (MB) (MB) R3165387-4 09/21/1615:08 MB Result MB OuallBer MB MDL MB RDL Analyte mg/I mg/I mg/I Acroleln U 0.00887 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0.00100 'Bromodichloromethane U 0.000380 0.00100 Bromoform U 0.000469 0,00100 Bromomethane U 0,000866 0,00500 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethahe- U 0.000327 0,00100 Chloroethane t t U 0.000453; 0.00500 2-Chloroethyl vinyl ether U 0.00301 0,0500 Chloroform U 0,000324 0.00500 Chloromethane U 0,000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 - 1,3-Dichloroben2ene U 0.000220 0,00100 1,4.Dichlorobenzene U 0.000274 0.00100 Dichlorodifluoromethane U 0.000551 0.00500 1.1-Dichloroethane U 0.000259 '0.00100 1,2-Dichloroethane U 0.000361 0,00100 91-Dichloroethene U 0.000398 0.00100 trans-1,2.Dichloroethene U 0.000396 0,00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0,000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0.00100 OA0500 1,1,2.2-Tetrachloroethane U 0.000130 0,00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0,000760 0.00500 4,1,1.Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0,00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 _ `0.00500 Vinyl chloride U 0.000259"� 0.00100 (S) Toluene-d8 101 90.0-115 (S) Dibromofluoromethone 92.9 79.0-121 - (S)0,o,o-Trifluomtoluene 975 90.4416 (S) 4-8romolluorobenzene 98.0 80.1-120 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L860714 DATEMME: 09/26,1614:55 PAGE: 12 of 24 WG910110 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organlc_Compounds (GC/MS) by Method 624 ,. L860714-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Cp (LCS) �R3165387-1 09/21/1613:23 • (LCSD) R3165387-2 09/21/16 13:44 Spike Amount LCS Result LCSD Result LCS Red. LCSD Red. Red. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 2 Analyze mg/I mg4 hill% % % % % TC Acrolein 0.125 0.350 0.371 280 297 88.0-118 J4 J4 5.65 281 Acrylonitrlle 0.125 0.131 0.141 105 113 71.0-135 6.91 20 a SS Benzene 0.0250 0.0227 0.0243 90.7 97.0 73.0.122 6.72 20 Bromodichloromethane 6.0250 0,0214 0.0230 854 91.8 75.5-121 7.23 20 4 Bromoform 0.0250 0,0217 0.0233 86.6 934 71.5-131 7,51 20 Cn Bromomethane 0,0250 0.0155 0.0171 62.0 68.4 22.4-187 9.77 20 Carbon tetrachloride 0,0250 0.0211 0.0230 84.5 92A 70.9-129 8.66 20 Fri Chlorobenzene 0.0250 0.0232 0.0253 92.9 101 79.7-122 SAS 20 Chlorodibromomethane 0,0250 0,0238 0.0249 95.1 99.6 78.2-124 4.66 20 Chloroethane 0.0250 0.0156 0,0160 62.4 64.1 41.2-153 2.72 20 2-Chioroethyl vinyl ether 0.125 0.122 0.130 97.7 104 234-162 6.58 23S Chloroform 0.0250 0.0211 0,0225 64.3 90.1 73.2-125 6.65 20 7GI Chloromethane 0.0250 0.0235 0.0269 94.0 108 55.8-134 13.7 20 1,2-Dichlorobenzene, 0,0250 0.0236 0.0252 94.3 101 84.7-118 671 20 s 13-Dichlorobenzefie' 0.0250 0,0210 0.0226 84.1 90.4 77.6-127 7.28 20 AI 1,4-Dichlorobenzenc 0.0250 0,0222 0.0235 88.8 94.1 82.2-114 5.75 20 Dichlorodifluoromethane 0.0250 0.0269 0.0294 107 118 56.0-134 9.13 20 e SC 1,1-Dichloroethane 0.0250 0.0238 0.0256 95.2 103 71.7-127 7.45 20 1,2-Dichloroethane 0,0250 0.0207 0.0222 82.9 88.6 65.3-126 6.63 20 1,1-Dichloroelhene 0,0250 0.0237 0.0260 94.7 104 59.9.137 9.37 20 trans-1.2-Dichloroelhene 0,0250 0.0225-" DC241 90.1 96.6 72.6-125 r 6.94 20 1,2-Dichloropropane 0.0250 0.0261 0.0283 104 113 774-125 7.92 20 cis-1,3-Dichloropropene 0.0250 0.0236 0.0252 94.4 101 77.7-124 6.39 20 trans-1,3-Dichloropropene 0.0250 0.0225 0.0238 89.9 951 73.5-127 5.64 20 Ethylbenzene 0.0250 0,0228 0.0246 91,2 98.4 80.9.121 7.54 20 Methylene Chloride 0.0250 0.0223 0.0234 89.3 93.7 69.5-120 4.87 20 1,1,2,2-Tetrachioroethane 0,0250 0.0226 0.0242 90.5 96.9 79.3.123 6.87 20 Tetrachloroethene 0.0250 0.0226 0.0244 90.3 97,8 735-130 7.93 20 _ Toluene 0.0250 0.0224 0.0241 89.5 96.3 779-116 7.27 20 1,1,1-Trichloroelhane 0.0250 0.0213 0.0232 85.3 92.8 71.1-129 8A5 20 1,1,2-Trichloroethane 0.0250 0.0223 0.0243 89.3 97.0 81.6-120 8.25 20 Trichlorotimene 00250 DM31 0.0247 923 98.9 79.5-121 6.93 20 Trichlorofluoramethane 0.0250 0.0193 0.0207 77.1 82.9 49.1-157 T24 20 Vinyl chloride _ 0,0250 0.0242 0.0266 96.8 106 61.5.134 9.42 20 (S) Toluene-tl8 104 105 90.0-115 (S) Dibromolluoromethone 93.3 92.6 79.0.121 (S)c,o.o-Trilluoroto7uene 977 99.2 90.4-116 (S)4-8romoflluorobenzene 107 99.4 80.1-120 ACCOUNT: PROJECT: 5DG: DATE/TIME: PAGE: Eaton Corporation 28091-R L860714 09/2611614:55 13 of 24 WG909588 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608 L860714.01 Method Blank (MB) (MB) R3165305-2 09/21/161458 Analyte MB Result mg4 MB Qualifier MB MDL ni MB RDL mg1l Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0,0000184 O.OD00500 Delta BHC U 0.0000197 0,0000500 Gamma BHC U 0.0000176 0,0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0,0000177 0.0000500 Dieltlrin U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0.0000500 Endosulfan II U 0,0000176 0.0000500 Endosulfan sulfate U 0.0000196 0,0000500 - Endrin U 0,0000189 0.0000500 Endrin aldehyde ,- U 0.0000142 0.0000500 Endrin ketone U 0.0000170, 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene U 0.0000134 0.0000500 Methoxychlor U 0.0000193 0.0000500 Chlordane U 0.0000977 0.000500 Toxapherie " U 0.600168 0.000500 (S) Decochlorobfphenyl 58.7 10.0-156 (S) Tetrachloro-m-xylene 46.0 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3165305-3 09/2111615:10 • (LCSD) R3165305-1 09/21/1614:45 Spike Amount LCS Result LCSD Result LCS Rea LCSD Rem. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/l % % % % % Aldrin 0.00100 0,000611 0.000753 61.1 75.3 10.0-120 20.8 33.9 Alpha BHC 0.00100 0,000604 0.000757 BOA 75.7 53.6-125 J3 22.5 22.3 Beta BHC 0.00100 0.000610 0.000752 61.0 75.2 55.8-130 J3 20.8 20.6 Delta BHC 0.00100 0.000639 0.000793 63.9 79.3 42.2.135 21.4 23.3 Gamma BHC 0.00100 0,000613 0.000769 61.3 76.9 54.7-125 J3 22.5 21.1 4,4-DDD 0.00100 0.000720 0.000882 72.0 88.2 47.6-144 20.2 24.3 4,4-DDE 0.00100 0.000672 0,000827 67.2 82.7 45.0-124 20.7 25.7 4,4-DDT -- 0.00100 0.000708 0.000857 70.8 -85.7 49.8-130 19.1 25.4 N' Dieltlrin 0,00100 0.000697 0.000856 69.7 85.6 55.0-127 20.5 22S Endosulfan 1 0.00100 0.000685 0.000838 68.5 83.8 54.7-127 20.1 24.3 ACCOUNT: Eaton Corporation PROJECT: SDG: 28091-R L860714 DATE/TIME: 09/26A614:55 PAGE: 14 of 24 WG909588 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides_ (GC) by Method EPA 608 L860714.01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3165305=3 09/21/l6l5:10 • (LCSD) R3165305-1 09/21/1614:45 Cp. Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/I mg11 mg/I % % % % % TC Endosulfan ll 0.00100 0,000705 0000859 70.5 85.9 53.1-135 19.7 23.5 Endosulfan sulfate 0.00100 0.000715 0.000870 71.5 87.0 51.5-132 19.5 26.3 a SS Ellerin 0.00100 0.000691 0.000643 69.1 84.3 50.1-131 19.8 29.1 'Endrin aldehyde 0.00100 0.000666 0.000813 66.6 81.3 39.5-137 19.9 28A y Endrin ketone 0.00100 0.000690 0.000834 69.0 83.4 53.5-139 189 28.4 Cn Heptachlor 0.00100 0.000613 0.000742 61.3 74.2 20.7-127 19.0 30.5 Heptachlor epoxide 0.00100 0.000624 MOMS 624 76.5 56.4-124 20.3 23.1 s Sr Hexachlorobenzene _ 0.00100 0.000545 0.000668 54.5 66.6 26.7-114 20.2 27.6 Methoxychlor 0.00100 0.000756 0.000897 75.6 89.7 48.2-144 17.0 27.8 - (5) Decochlorobiphenyl 70.5 85.4 10.0-156 (S) Tetrachloro-m-xylene 51.1 60.8 13.9-137 r .r ACCOUNT: Eaton Corporation 4? PROJECT: SDG: DATE/TIME: PAGE: 28091-R L860714 09/26/1614:55 15 of 24 WG909588 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Polychlorinated Biphenyle (GC) by Method EPA-608 _ LB60714-01 Method Blink (MB) c Cp (MB) R3165256-1 09/2111611:06 MB Result MB Qualifier MB MDL MS RDL Analyte mg/I mg/I mg/I TC PCB 1260 U 0.000120 0.000500 PCB 10'16. U 0.000100 0.000500 3SS PCB 1221 U 0.0000730 0.000500 PCB 1232 U 0,0000420 PCB 1242 U 0.0000470 0.000500 0.00D500 4 Cn PCB 1248 U 0.0000860 0,000500 PCB 1254 U 0.0000470 0.000500 6Sr (S) Decochlorobiphenyl 42.0 10.0-156 (S)Tetrochloro-m-xylene 427 )3.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) GI (LCS) R3165256-2 09/21/1611:19 • (LCSD) P3165256-3 09/21/16 11:31 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits B Analyte mg/I mg4 mg4 % % % % % P,I PCB 1260 0.00250 0.00144 0.00178 57.5 71.2 473-149 21.1 28.8 PCB 7016 0.00250 0.00169 0.00194 67.7 77.5 24.7-128 13.5 34.9 SC (S) Decochlorobiphenvl 46.5 52.7 10 0-156 (S) Tetrochloro-in-xylene 39.7 45.6 13.9-137 D'. ACCOUNT: Eaton Corporation PROJECT: 28091-R SDG: DATE/TIME: L860714 09/26/16 14.55 PAGE: 16 of 24 WG910521 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Seml Volatile Organic Compounds. (GC/MS). by. Method 625 L860714.01 Method Blank (MB) 1 (MB) R3166056-3 09/25/161550 Cp• MB Result MB Qualifier MB MDL MB RDL z Analyte mg/I mg/I mg/I TC Acenaphthene U 0.000316 0,00100 'Acenaphthylene�F. U 0.000309 0.00100 3S5 Anthracene U 0.000291 0.00100 Benzidine U _ _ 0,00432 0.0100 4 Benzo(a)anthracene U 0,0000975 0.00100 Cn Benzo(h)fluoranthene U 0.0000896 0.00100 Benzo(k)guoranthene U 0.000355 0.00100 6SF Benzo(g,Ni)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0.00100 'Bis(2-chlorethoxy)methane U 0.000329 0.0100 Bis(2-chloroethypether U 0,00162 0.0100 Bis(2-chloroisopropyl)ether U - 0.000445 0.0100 7G) 4-Bromophenyl phenylether U 0.000335 0.0100 2-Chloronaphlhalene U 0,000330 0.00100 e 4-Chlorophenyl-phenylether U 0.000303 0.0100 AI Chrysene U 0.000332 0.00100 Dibenz(a,h)anNracene U 0.000279 0.00100 0 _ SC .. 3,3 Dichlorobenzidine U' 0.00202 0.0100 2,4-Dinitrotoluene U _ 0,00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 'Fluorene U 0,000323 0.00100 Hexachlorobenzene U 0.000341 0.00100 Hexachloro-1,3-butadiene U 0,000329 0.0100 Hexachlorocyclopentadiene U 0.00233 OA100 Haxe hloroethane . U O.OD0365 •' 0.0100 Indeno(1.2,3-cd)pyrene U 0.000279 0.00100 Isophorone U 0.000272 0.0100 Naphthalene U 0.000372 0,00100 Nitrobenzene U _ 0.000367 0.0100 _ n-Nitrosodimethylamine U 0.00126 0.0100 1,2-Diphenylhydrazine U 0.000318 0.0100 , n-Nitrosodiphenylamine U 0.000304 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 O.OD100 Benzylbutyl phthalate U 0.000275 0.00300 Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0,000282 0,00300 Dlmethyl phthalate U 0.000283 0.00300 ACCOUNT: PROJECT: Eaton Corporation 28091 R SDG: L860714 DATE7TIME: 09/26/1614:55 PAGE: 17 of 24 WG910521 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE: x Seml Volatile Organic Compounds (GC/MS) by Method 625 L860714-01 Method Blank (MB) (MB) R3166056-3 09/25/1615:50 MB Result MBOualifer MB MDL MB RDL Analyte mg/I mg)] mg/I Di-n-octyl phthalate, U 0.000278 0.00300 - Pyrene Ll 0.000330 5 0.00100 1.2,4-Trichlorobenzene U 0.000355 0.0100 - 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0,000283 0.0100 2,4-Dichlorophenol U 0.000284 0.0100 2,4-Dimethylphenol U 0.000624 0.0100� 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0,0100 Phenol U 0.000334 0,0160 2A6-Trichlorophenol U 0.000297 0.0100 (S) Nitrobenzene-d5 35.2 21.8-123 (5) 2-Fluorobiphenyl 46.6 29.5-131 (S)p-Terphenyl-di4 69.9 29.3-137- (S) Phenol-d5 12.4 5.00-70.1 (S) 2-Fluorophenol 20.5 10.0-729 (S) 2,4,6-Trlbromophenol 55.7 112-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3166056_b 09/25/1615:03 • (LCSD) R3166056-2 09/25/16 15:26 Spike Amount LCS Result LCSD Result = LCS Rea. LCSD Rea. Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mgll % % % % % Acenaphthene 0.0500 0.0321 0.0314 64.3 62.9 38.7-109 2.23 21,5 Acenaphthylene 0.0500 0.0345 0.0331 69.1 66.3 36.0-106 4.11 21 , Anthracene 0.0500 0.0337 0,0341 67.4 68.1 43.6-113 1.04 18.8 Benzidine 0.0500 0.0154' 0,0174 30.9 34.8 10.0-165 -`-12.0 40 Benzo(a)anthracene 0.0500 0.0325 0.0343 65.0 68.5 51.2-112 5.24 20 Benzo(b)fluoranthene 0.0500 0.0322 0.0329 64A 65.9 4Z6-111 2.22 20 Benzo(k)fluoranthene 0.0500 0.0321 0.0353 64.2 70.6 49.4-114 9.48 20 Benzo(g,h,i)perylene 0.0500 0.0360 0.0377 72.1 75A 45.2-117 4.55 20 Benzo(a)pyrene 0.0500 0.0329 0.0346 65.9 69.2 45.6-106 4.92 20 Bis(2-chlorethoxy)methane 0.0500 0.0269 0.0264 53.7 52.9 37.2-111 1.57 24.1 BiS(2-chlorcethyl)ether 0.0500 0.0211 0,0186 42.1 37.1 22.6-108 12.7 27.9 Bis)2-chloroisopropyl)ether 0.0500 0.0280 0,0244 56.0 48.8 32.9-100 13.6 25.1 4-Bromophenyl-phenylether 0.0500 0.0365 0.0366 72.9 73.2 40.7-116 0.410 21 ACCOUNT: Eaton Corporation PROJECT: SDG: 28091-R L860714 DATE/TIME: 09/26/1614:55 PAGE: 18 of 24 WG910521 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds ,(GC/MS) by Method 625 L860714-01 . Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) r (LCS) R3166056-1 09/25/1615:03 • (LCSD) R3166056-2 09/25/1615:26 Cp' Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/I mgA mg4 % % % % % TC 2-Chloronaphthalene 0,0500 0.0300 0.0282 60.1 56.4 33.6-105 6.33 23 4-Chlorophenyl-phenylether 0,0500 0.0348 0.0345 69.6 69.0 39.0-113 0.880 20.9 a SS 1,2-Dlphenylhydra7lne _ 0.0500 0.0291 0.0284 56.2 56.8 37.6-111 2.37 21.1 Chysene 0.0500 0,0349 0.0363 69.8 72.6 54.6-120 3.97 20 4 Dibenz(a,h)anthracene 0.0500 0.0350 0.0369 70.0 73.8 42.8-118 5.34 20 Cn 3,3-Dichlorobenzidine 0.0500 0.0244 0.0366 68.8 732 27.2-142 6,24 22.3 2,4-Dinitrotoluene 0.0500 0.0389 0.0392 77.8 78.5 3L2-105 0.900 22 6 Sr 2,6-Dinitrotoluene� 0.0500 0.0358 0.0352 � 71.5 704 30.6-706 1.55 23.1 Fluoranthene 0.05o0 0.0336 0,0358 57.3 71.7 45.9-115 6.34 20 Fluorene 0,0500 0.0344 0.0341 68.6 68.3 41.0-112 0.770 20.2 'Hexachlorobenzene 0.0500 0.0370 0.0391 73.9 761 - 38.5-116 5.49 20.1 Hexachloro-1,3-butadiene 0.0500 0.0264 0.0237 52.8 47.5 16.1-104 10.6 31.2 7Gl Hexachlorocyclopenladiene 0.0500 0.0298 0.0268 59.5 53.5 10.0-121 10.7 27.9 Hexachloroethane 0.0500 0.0220 0.0191 44.0 38.2 16.5-89.8 14.1 30.7 a Indeno(1,2,3-cd)pyrene 6.0500 0,0358 0,0376 71.6 75.2 45.0-116 5.01 20 AI Isophorone O.D500 0,0297 0,0294 59.5 58.9 35,4-112 0,990 21.5 Naphthalene 0.0500 0.0277 0.0252 55.3 50A 32.2-101 9.31 23.8 SC Nitrobenzene OA500 0.0254 0.0239 50.6 47.8 31.4-106 6.75 25.7 n-Nitrosodimethylamine 0.0500 0.0118 0.0104 23.6 20.8 10.0-80.1 12.6 37.5 n-Nitrosodiphenylamine 0,0500 0.0346 0.0344 69.2 687 44.4-113 0.670 20 -n-Nitrosodi-n-propylamine 0.0500 0.0288 0.0276 57.6 55.2 33.2-106 4,32 23.7 Phenanthrone 0,0500 0.0316 0.0320 63.2 64.1 46.4-113 1,40 20 Benzylbutyl phthalate 0.0500 0.0335 0.0358 67.0 71.6 31.8-123 6.63 20.7 Bis(2-ethylhexyl)phthalate 0.0500 0.0327 0.0342 65 4 68.3 36.9-134 4.33 23.6 M-n-butyl phthalate 0.0500 0,0337 0.0358 67.3 71.7 41.8-120 6,27 20.2 Diethyl phthalate 0.0500 0,0360 0.0366 72.0 73.2 36.5-129 1.69 20 Dimethyl phthalate 0.0500 0,0351 0.0352 70.2 70.4 35.3-128 0,280 20.8 Di-n-octyl phthalate 0.0500 0.0328 0.0350 65.7 70.0 39.7-112 6.34 21.1 Pyrene 0.0500 0.0334 0.0340 66.7 68.0 46.3-117 1.91 20 1,2,4-Trichlorobenzene 0 0500 0.0268 0.0243 53.5 487 22.9 96.1 9.46 27.5 4-Chloro-3-methylphenol 0.0500 0.0284 0.0297 -' 56.9 594 357-100 4.30 22.9 2-Chlorophenol 0.0500 0,0237 0,0214 47.4 42.9 26.2-91.5 10.1 26.5 2,4-Dichlorophenol 0.0500 0.0289 0.0287 57.9 57.4 31.4-103 0.900 24.9 2,4-Dimethylphenol 0.0500 0.0248 0.0254 49.6 50.8 .;. 31.9-107 2.42 25.7 - 4,6-Dinitro-2-methylphenol 0.0500 0.0326 0.0316 65.1 63.1 18.4-148 3.15 24.4 2,4-Dinitrophenol 0.0500 0.0140 0.0113 28.0 22.5 24.2-128 J3 J4 21.8 20.5 2-Nitrophenol 0.0500 0.0312 0,0295 62.4 58.9 25.9-106 5.79 26.9 4-Nitrophenol 0.0500 0.00937 0.0101 18.7 20.1 10.0-527 7,14 40 Pentachlorophenol 0.0500 0.0283 0.0292 56.5 58A 10.9-97A 3,22 35.1 Phenol 0.0500 0.00998 0.0103 20.0 20.5 10.0 57A 2.89 35 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporatlon 28091-R L860714 0926/1614:55 19 of 24 WG910521 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS).,by Method 625 L860714-01 Laboratory Control Sample (LCS) - Laboratory Control Sample Duplicate (LCSD) (LCS) R3166056-1 09/25/16 15:03 • (LCSD) R3166056-2 09/25/16 15:26 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Anaiyte mg/I mgll mg/1 % % % % % 2,4,6-Trichlorophenol 0.0500 0.0337 0.0325 67.5 65.0 29.8-107 3.72 24.1 (S)Nitrobenzene-d5 53.3 475 218-123 (S) 2-Fluorohiphenyl 65.7 60,4 29.5-131 (5)p-Terphenyl-d14 73,8 781 29.3-137 (S) Phenol-d5 20.2 20.7 5.00-70.1 (S)2-Fluorophenof 314 29.1 10.0-779 (S)2,4,6-Trlbro`m1phenol 86.9 89.0 11.2-130 '-f 's: CP zTc 3Ss 4Cn 6Sr 7G1 aAl 95c ACCOUNT: PROJECT: SDG: DATE7TIME: PAGE: Eaton Corporation 28091-R L860714 09/26/1614:55 20 of 24 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions Cp SDG Sample Delivery Group. MDL Method Detection Limit. a RDL Reported Detection limit. Tc U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) Rs _ from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) -Anal es added to eve ryblank, sample, Laboratory Control Cn Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. s Rec. Recovery. Sr 6Qc Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch OC was outside the established quality control range for precision. J4 The associated batch OC was outside the established quality control range for accuracy. BAI s—C ACCOUNT: PROJECT: SDG: DATERIME: PAGE: Eaton Corporation 28091-R L860714 09/26/1614'.55 21 of 24 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences is the only environmental laboratory accred ited/cedifed to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capablllty from our single location laboratory is comparable to the collective totals of the network laboratories in our industry The most significant benefit to our'ome location' design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turnaround time, and preventing cross contamination, thus protecting Sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all ceradcatlons held by the laboratory are applicable to the results opened in the attached report State Accreditations Alabama 40660 Alaska --- UST-080 Arizona_-- _ _ A20612 Arkansas 88-0469 California _ 01157CA Colorado _ -- ----- -_ TN00003 Conneticut - - --- - - -- -__ _PH-0197 _--_ Florida _- ---�- E87487 Georgia__,___ _ ___ NELAP Georgia 923 Idaho __ ___ ___ ___ TN00003 Illinois ------�-- -- 200008 Indiana----- C-TN-01 Iowa 364 Kansas _ _ E-10277 -_ -_ - _ Kentucky_ _ _ _ _ _ 90010 Kentucky° _ - 16 Louisiana A130792 Maine _ _ TN0002_ _ Maryland _ _ _ _ 324 Massachusetts _ KTN iO3 Michigan - _ _ _ _ __ _ _ __ 9958 Minnesota 047-999-395 Mississippi TN00003 Missouri 340 Montana CERT0086 Third Party & Federal Accreditations Nevada _ _ _ _ TN_03-2002-34 New Hampshire _ -de 2975 _ New rsey-N ELAP __. -.. TNO02 New Mexico -_-- TN00003_ --11742 New York North Carolina _ Env375 North Carolina' DW21704 _ _ North Carolina' _ _ _ 41 North Dakota _ R-140 Ohio-VAP CL0069 Oklahoma ___ 9915 ____ _ Oregon _ _ _ ____ — TN 200002 Pennsylvania 68-02979 Rhode Island - - - -- -- 221 - - South Carolina 84004-_— - SouthDakota_ nra Tennessee" _ 2006 Texas _ - --- T1047_04245-07-TX__ Texas s -� - _- - ----__ _ LAB0152---__ _ Utah _ _ __ _ _ 6157585658 Vermont VT2006 Virginia _ _. _ 109_-- Washington _ _ _ C1915 West Virginia _ _ 233 Wisconsin 9980939910 Wyoming A21-A A2LA-ISO 17025 1461.01 AIHA 100789 A21LA - 15017625` 1461.02 _ DOD _ - - 14fi1.01 Canada _-- 1461.01 _-- -- -TN - - ---- USDA -- - - - - S-67674 ---- -_-- EPA -Crypt_o 00003 _-- --- -- `Drinking Water Underground Storage Tanks ° Aquatic Toxicity ' ChemlcaliMicrobiological ' Mold * Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/orthe delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory, wA O MT NV OR • 4N ! n' SV ! 1Vl T NY' vaY � !ai ! T IA T NV T NG • ! T T •iT ! RA ! • !- T ! • i • O T.i VT N LYn cf T co ! Ks Mc!i • vn! ! • T KYAZ •�T _ N • ! MS x'L GA ! rx ! ! LA ! •--.t'! ! r• • � AK ! • • O FL ACCOUNT: PROJECT: SDG: DATE/TIME: Eaton Corporation 28091-R L860714 09/2611614:55 N.E PAGE: 22 of 24 �_1 Company Name/Address: Billing Information: A alysis Coma ner Preservat e a, " . I . - : a.. Eaton, Coeporatidn,,- NA Financial — A PO Box 024 V�J`M 2564 Durham Rd Cleveland, OH "181-8024 Roxboro, NC 27573 L- A- B S- C- I -E! N: C-EIS r nt Juk% 7N 37122 ILL LL� Email TO: Report to: 0 11�_;61S.751158 ; : bustin'LaClair �ustinlaclalr@Eaton.com 3�, 0 Z z z I.M.5.1118 _2 as Project Eaton Corp.,§em!.Annual Storrnwater.� city/stale Collected: Roxboro, NC' Description: 7 'k -�. ! so 0-- > 0 M -0 .0 1Z11 Imp I - 141', client Project 9,1', Lab Project 4 J I ' Phone:336-59 7 L 'R 2809T. EATON RN C-28091 SW I Table's J a. 0 z , '0. ". N — E,� 0, , �OE;,!' E M E t Collected bylprii Ste/Facility ID N P.O. # A'oCtnuAATONRNC- EL IF, E E Q Template, "ll X 0 C!. 4: Collected by (signalure): —Rush?-(Lab MUST Be Notiflid)— __Date Results Needle -*— T7 Prefogin:- Sam. Day.......-. 200146 lo(X4 X TSR: Hunt - Im diately , e Next Day. ............................ �­ T.0 D.y,. .............................. SM 2 5)ii , mail? —No )4i.68 FAX? )CNO YeSr No. �,�; X i♦ N .6 ' . . 0 0 'r %A lz�) Z. Z, Cooler e Shippedv6: Ralellgh'Seirv, pa ed on Ice N y Three Day .......... .............. nr 6 0, on 6 ILI, 0 N us Z Sample 10 comp/Grab matrix Depth rate Time mrs WW VM e, It 1==� 16 •Gw •main.: ss - Soil -Groundwater ww - wastewater DW Drinking Water Or - Other ph, Temp5 rr Remarlks�;Replace kit upon arrival at lab* Flow— Other Mold E: Relinquished by:(Sl atur e Relinquished Date: Time: Received by: (Signature) I , 0 Samples returned via: 13 UPS Condition' (lab use only) � 1/4 10"00 XFedEx OCcurier 0— Relinquished by: (Signature).'Uate: :2", Ime; Received by: (Sign�tkurr)� CDC Sea] Intact:V. N V1t­V _NA T P C, Bot es Received: Relinquished by.7(Sgnature)t Date: ff Time: Re c!iyel [6r Iatibj� (Sig a D p une: .11 Checked Wc, I ; Client cooler Receipt'Form SDGt1 'Cooler.Received/O ened On:9/20/16...__. P_.__ _ _ _TemperatureUpon-Receipt:— ,Receive d.Dy Timiesha Scott Signatur 71 Receipt Check List Yes No N/A Were custody seals on outside of cooler and intact? Were custody'papers propely;filled out?: ' v Did all bottles arrive in'good condition? ,Were correct bottles used for the analyses requested? Was sufficient amount of sample sent in each bottle? Were all applicable;sample containers correctly preserved and, checked for preservation?'(Anynot iroaccepted.range noted omCOC)., If applicable, was an observable VOA headspace present? _ Non Conforirnance,Genefated.-(I£.yes see attached NCF) L'*ESC ANALYTICAL REPORT my® Entire Report Reviewed By: it Jimmy Hunt Technical Service Representative Results relate only c the items tested or calibrated and are reported as rounded values. This test report shall not be ' reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC Is performed per guidance provided in laboratory standard operating procedures: 060302. 060303, and 060304, ffi f• (�'r F TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cover Page 'Tc: Table of Contents 'Ss: Sample Summary 4Cn: Case Narrative 'Sr: Sample Results 2016-06-22-005 L843453-01 'Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 Volatile Organic Compounds (GC/MS) by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Corilpounds (GC/MS) by Method 625 'GI: Glossary of Terms aAl: Accreditations & Locations 'Sc: Chain of Custody tl 1 CP 2 3 4 3SS 5 5 4Cn 8 Sr 8 g 6Qc 10 11 I G 14 eAl 16 17 9Sc 21 22 23 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: 2016-06-22-005 L843453-01 WW Method SAMPLE SUMMARY Collected by Dustin A. LaClalr Batch Dilution Preparation dateltime ONE LAB. NATIONWIDE. V Collected dateltime Received date/time 06/22/1617:25 06124/1609:00 Analysis Analyst date/time Gravimetric Analysis by Method 2540 D-2011 WG883640 1 06129/161133 06129/1612:06 MMF Metals (ICPI by Method 200.7 WG883795 1 06/28/1617:43 06/29/16 01:12 LTB Pesticides GC) by Method EPA 608 WG883337 1 06/26/16 23:05 06/27/1612:03 VKS Polychlorinated Biphenyls (GC) by Method EPA-608 WG883337 1 06/26/16 23:05 06/2711614:21 JNS Semi Volatile Organic Compounds (GC)MS) by Method 625 WG883348 1 06/25/161101 06/26/1611:26 JF Volatile Organic Compounds (GOMS) by Method 624 WG883472 1 06125/1617:50 06/25/1617:50 EMS Wet Chemistry by Method 1664A WG883623 1 06/27/1610:18 06/27/1613:49 SHG ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the ID appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the Tc analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the Ss laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. SSr 6 L it ,GIGl Jimmy Hunt eAl Technical Service Representative 9Sc ACCOUNT: PROJECT: SDG: DATMIME: PAGE SAMPLE RESULTS - 01 L843453 ONE LAB. NATIONWIDE. V 2016-06-22-005 Collected date/time: 06/22/16 17:25 Additional Information Result Units Analyte pH (On Site) 72 su Temperature (on -site) 30.2 Deg. C Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgll mg/I mg/1 date/time Suspended Solids 94.3 J3 0.350 2.50 1 06/291201612:06 WG883640 Wet Chemistry by Method 1664A Result Qualifier MDL ROL Dilution Analysis Batch Analyte mgA mgA mgA date/time TPH - Oil & Grease U 0.725 5.56 1 06127/201613*49 WG883623 Metals (ICP) by Method 200.7 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mgA date/time Copper 0.0418 0.00700 0.0100 1 ` 06/29/2016 0112 WG883795 Lead 0.00707 0.00200 0.00500 1 06/29/2016 0112 WG883795 Zinc 0.133 0.00340 0,0500 1 06129/20160112 WG883795 Volatile Organic Compounds (GC/MS) by Method 624 Analyte Result mgA Qualifier MDL mgA RDL mgA Dilution Analysis date/time Batch Acrolein U J4 0,00887 0.0500 1 06/251201617:50 WG883472 Acrylonitrile U 0.00187 0.0100 1 06/251201617:50 WG883472 Benzene U 0.000331 0,00100 1 06/251201617:50 WG883472 Bromodichlorcmethane U 0.000380 0.00100 1 06/251201617:50 WG883472 Bromoform U 0.000469 0.00100 1 06/25/201617:50 WG883472 Bromomethane U 0.000866 0.00500 1 06/25/201617:50 WG883472 Carbon tetrachloride U 0.000379 0,00100 1 06/251201617:50 WG883472 Chlorobenzene U 0.000348 0,00100 1 06/25/201617:50 WG883472 Chlorodibromomethane U 0.000327 0,00100 1 06/25/201617:50 WG883472 Chloroethane U 0,000453 0.00500 1 06/25/201617:50 WG883472 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 06/25/201617.50 WG883472 Chloroform U 0.000324 0.00500 1 06/25/201617:50 WG883472 Chloromethane U 0.000276 0.00250 1 06/25/201617:50 WG883472 1,2-Dichlorobenzene U 0.000349 0-00100 1 06/25/201617:50 WG883472 1,3-Dichlorobenzene U 0.000220 0.00100 1 06/25/201617:50 WG883472 1,4-Dichlorobenzene U 0.000274 0.00100 1 06/25/201617:50 WG883472 Dichloroditlucromelhane U J4 0.000551 0.00500 1 06/25/201617:50 WG883472 1,1-Dichloroethane U 0.000259 mol00 1 06/251201617:50 WG883472 1,2-Dichloroethane U 0.000361 0.00100 1 06/25/201617:50 WG883472 1,1-Dichloroethene U 0.000398 0.00100 1 06125/201617:50 WG883472 trans-1,2-Dichloroethene U 0.000396 0.00100 1 06125/201617:50 WG883472 1,2-Dichloropropane U 0.000306 0,00100 1 06/25/201617:50 WG883472 cis-1,3-Dichloropropene U 0.000418 0.00100 1 06/25/201617:50 WG883472 trans-1,3-Dichloropropene U 0.000419 0.00100 1 06/25/201617:50 WG883472 Ethylbenzene U 0.000384 0.00100 1 06/25/201617:50 WG883472 Methylene Chloride U 0.00100 - 0.00500 1 06/25/201617:50 WG883472 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 06/25/201617:50 WG883472 Tetrachloroethene U 0.006372 0,00100 1 06/25201617:50 WG883472 Toluene U 0,000780 0.00500 1 0625201617:50 WG883472 1,1,1-Trichloroethane U 6.000319 0.00100 1 06/251201617:50 WG883472 1.1.2-Trichloroethane U 0.000383 0.00100 1 06/25/201617:50 WG883472 FCp FTC as$ 4Cn 6QC 7GI aAl 9Sc ACCOUNT: PROJECT: SDG: DATEMME PAGE: 2016-06-22-005 SAMPLE RESULTS - 01 Collected date/time: 06/22/16 17:25 L843453 Volatile Organic Compounds (GC/MS) by Method 624 ONE LAB. NATIONWIDE. Analyte Result mgA Oualifer MDL mgA RDL mg/I Dilution Analysis date/time Batch Trichloroethene U 0.000398 0.00100 1 06/25201617:50 WG883472 Trichloroll ad rometh a ne U 0,00120 0,00500 1 06/25/201617:50 WG883472 Vinyl chloride U 0.000259 0.00100 1 06/25/201617:50 WG883472 (S)Toluene-tl8 101 90.0-115 06251201617.50 WG883472 (S) Dibromoflluoromethone 101 79.0-121 062512016 1750 WG883472 (S)oo,o-Tri(Iuorololuene 975 90.4-116 062520161750 WG883472 (S)4-Bmmorluorobenzene 99.1 80.1-120 06251201617.50 WG883472 Pesticides (GC) by Method EPA 608 Result Oualifer. MDL RDL Dilution Analysis Batch Analyte mg4 mgA mgA date/time Aldrin U 0.00000813 0.0000500 1 06/27/201612:03 WG883337 Alpha BHC U 0.0000166 0.0000500 1 06/27/201612:03 WG883337 Beta BHC U 0.0000184 0.0000500 1 06/27/201612:03 WG883337 Delta BHC U 0.0000197 0.0000500 1 06/27/201612:03 WG883337 Gamma BHC U 0.0000176 0.0000500 1 06/27/201612:03 WG883337 Chlordane U 0.0000977 0.0o0500 1 06/27/201612:03 WG883337 4,4-DDD U 0.0000170 0.0000500 1 06/27/201612:03 WG883337 4,4-DDE U 0.0000164 0.0000500 -1 06/27/201612:03 WG883337 4,4-DDT U 0,0000177 0.0000500 1 06/27/201612:03 WG883337 Dieli rin U 0.00000751 0.0000500 1 06/27/201612:03 WG883337 Endosulfan I U 0.0000179 0,0000500 1 06/271201612:03 WG883337 Endosulfan II U 0.0000176 0.0000500 1 06/27/201612:03 WG883337 Endosulfan sulfate U 0-0000196 0.0000500 1 06127/201612:03 WG883337 Endrin U 0.0000189 0.0000500 1 06/27/201612:03 WG883337 Endrin aldehyde U 0.0000142 0.0000500 1 06/27/201612:03 WG883337 Endrin ketone U 0.0000170 0,0000500 1 061271201612:03 WG883337 Heptachlor U 0.0000108 0.0000500 1 06127/201612:03 WG883337 Heptachlor epoxide U 0,0000175 0.0000500 1 06/27/201612*03 WG883337 He$achlorobenzene U 0,0000134 0.0000500 1 06/27/201612:03 WG883337 Methoxychlor U 0A000193 0.0000500 1 06/27/201612:03 WG883337 Toxapheno U 0.000168 0.000500 1 06/27/201612:03 WG883337 (S) Decochlorobiphenyl 575 10.0-156 0627201612:03 WG883337 - (S)Tetrochloro-m-*ene 658 13.9-137 06127201612.03 WG883337 Polychlorinated Biphenyls (GC) by Method EPA-608 Result Oualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mg4 date/time PCB 1016 U 0.000100 0.000500 1 06/271201614:21 WG883337 PCB 1221 U 0.0000730 0.000500 1 06/27/201614:21 WG883337 PCB 1232 U 0.0000420 0.000500 1 06/27/201614:21 WG883337 PCB 1242 U 0.0000470 0,000500 1 06/27/201614:21 WG883337 PCB 1248 U 0.0000860 0,000500 1 06/27/201614:21 WG883337 PC81254 U 0.0000470 0,000500 1 06/27/201614:21 WG883337 PCB 1260 U 0.000120 0.000500 1 06/27/201614:21 WG883337 (S) Decochlorobiphenyl 59.6 700-756 06127207614: 21 WG883337 (S)Tetrochloro-m-xylene 660 13.9-137 0627201614.21 WG883337 Semi Volatile Organic Compounds (GC/MS) by Method 625 Analyte Result mg4 Oualifier MDL mgA RDL mgA Dilution Analysis date/time Batch Acena dithene U 0.000316 0.00100 1 06126/20161126 WG883348 Acenaphthylene U 0.000309 0.00100 1 06/26/201611:26 WG883348 Anthracene U 0,000291 0.00100 1 06/26/20161126 WG883348 Benzidine U 0.00432 0,0100 1 06/26/201611:26 WG883348 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: ICp 2Tc aSs 4 Cn I 6QC FGI aAl 9Sc ONE LAB. NATIONWIDE. JR 2016-06-22-005 SAMPLE RESULTS - 01 Collected dateitime: 06i22/16 17:25 L843453 Semi Volatile Organic Compounds (GC/MS) by Method 625 ' Analyte Result mgA Qualifier MDL mgA RDL mgA Dilution Analysis date/time Batch Benzo(a)anthracene U 0.0000975 0.00100 1 06/26120161126 WG883348 Benzo(b)0uoranthene U 0.0000896 0.00100 1 06/26/20161126 WG883348 Benzo(k)Buoranthene U 0.000355 0.00100 1 06/26201611:26 WG883348 Benzo(g,h,i)perylene U 0.000161 0.00100 1 06/261201611:26 WG883348 Benzo(a)pyrene U 0.000340 0,00100 1 06/26/20161126 WG883348 Bis(2-chlorethoxylmethane U 0.000329 0.0100 1 062620161126 WG883348 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 06/26/20161126 WG883348 Bis(2-chloroisopropyl)ether U 0.000445 0.0100 1 06/26/201611:26 WG883348 4-Bromophenyl-phenylether U 0,000335 0.0100 1 06/26201611:26 WG883348 2-Chloronaphthalene U 0.600330 0,00100 1 06/26/201611:26 _ WG883348 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 06126/20161126 WG883348 Chrysene U 0.000332 0.00100 1 06/26/201611:26 WG883348 Diben2(a,hlanthracene U 0.000279 0.00100 1 06261201611:26 WG883348 3,3-Dichlorobenzidine U 0,00202 0.0100 1 06/2620161126 WG883348 2,4-Dinitrotoluene U 0.00165 0.0100 1 06/2620161126 WG883348 2,6-Dinitrotoluene U 0.000279 HIM 1 06/26001611:26 WG883348 1,2-Diphenylhydrazine U 0.000318 0.0100 1 06/26201611:26 WG883348 Fluoranthene U 0.000310 0.00100 1 06/26/20161126 WG883348 Fluorene U 0.000323 0.00100 1 06/26/20161126 WG883348 Hexachlorobenzene U 0.000341 0.00100 1 061261201611:26 WG883348 Hexachloro-1,3-butadiene U 0.000329 0.0100 1 06/26/201611:26 WG883348 Hexachlorocyclopentadiene U 0.00233 0.0100 1 06/26/20161126 WG883348 Hexachloroethane U 0.000365 0.0100 1 06/26/20161126 WG883348 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 06126/201611:26 WG883348 Isophorone U 0,000272 0.0100 1 06/26/201611:26 WG883348 Naphthalene U 0000372 0.00100 1 06/26/20161126 WG883348 Nitrobenzene U 0,000367 0.0100 1 06/26/20161126 WG883348 n-Nitrosodimethylamine U 0.00126 0.0100 1 06/26120161126 WG883348 n-Nitrosodiphenylamine U 0.000304 0.0100 1 06/26/201611:26 WG883348 n-Nitrosodi-n-propylamine U 0000403 0.0100 1 06/26/201611:26 WG883348 Phenanthrene U 0.000366 0.00100 1 06/26/20161126 WG883348 Benzylbutyl phthalate U 0.060275 0.00300 1 06/26/20161126 WG883348 8is(2-ethylhexyl)phthalate 0.00155 B J 0.000709 0.00300 1 06126120161126 WG883348 Di-n-butyl phthalate a00117 B J 0.006266 0.00300 1 06/26/201611:26 WG883348 Diethyl phthalate U 0.000282 0.00300 1 06/26/201611:26 WG883348 Dimethyl phthalate U 0.000283 0.00300 1 06126/20161126 WG883348 Di-n-octyl phthalate U - 0.000278 0,00300 1 \ 06/26/20161126 WG883348 Pyrene U 0.000330 0.00100 1. 06/26/201611:26 WG883348 1,2,4-Trichlorobenzene U 0.000355 0.0100 1 06/26/20161126 WG883348 4-Chloro-3-methyl phenol U 0.600263 0.0100 1 06i26/20161126 WG883348 2-Chlorophenol U 0.000283 0.0100 1 06126/201611:26 WG883348 2,4-Dichlorophenol U 0.000284 0.01o0 1 06/26/2016 it 26 WG883348 2,4-Dimethylphenol U 0.00062.4 0.0100 1 06/26/20161126 WG883348 4,6-Dinitro-2-methylphenol U J3 0.00262 M100 1 06/26/201611:26 WG883348 24-Dinitrophenol U J3 0.00325 0.0100 1 06126120161126 WG883348 2-Nitrophenol U 0.000320 0.0100 1 06/26/20161126 WG883348 4-Nitrophenol U 0.00201 HIM 1 06/26/20161126 WG883348 Pentachlorophenol U 0,060313 0.0100 1 06/26/201611:26 WG883348 Phenol 0.00137 J 0.000334 0.0100 1 06/26/201611:26 WG883348 2,4,6-Trichlorophenol U 0.060297 0.0100 1 0666/20161126 WG883348 (S)2-Fluorophenol 422 10.0-779 06126120161126 WG883348 (S) Phenol -d5 32.1 5.06-701 062612016it26 WG883348 (5)Nitrobenzene-d5 63.2 218-123 06262015 n126 WG883348 (SJ 2-Fluorobiphenyl 682 29.5-131 062620161126 WG883348 (S)2,4,6-Tribromophenol 73.7 112-130 062612015lt26 WG883348 /S)p-Terphenyl-dl4 76.9 29.3-137 06262016 h26 WG883348 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: WG883640 QUALITY CONTROL SUMMARY G ravimetrlc Anal�sis by Method 2540 D-2011 L843453-01 Method Blank (MB) C` (MB) R3146705-1 06/29/1612:06 MB Result MB Qualifier MB MDL MB RDL .-Analyte mgll mgR mgA Suspended Solids U, 0.350 2.50 L843453-01 Original Sample (OS) • Duplicate (DUP) (OS) L843453-01 06/29/16 12:06 • (DUP) R3146705-4 06/29/16 12:06 Original Result DUP Result Dilution DUP RPD DUP Oualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Solids 94.3 99.7 1 5.50 J3 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. V (LCS) R3146705-2 06/29/16 12:06 • (LCSD) R31467OS-3 06/29/16 12:06 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Oualifier RPD RPD Limits Analyte mg/I mg/I mgll % % % % % Suspended Solids 773 776 780 100 101 85.0-115 0.514 5 L. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG883623 QUALITY CONTROL SUMMARY Wet Chemistry by, Method 1664A L843453-01 Method Blank (MB) (MB) R3146048-1 06/27/16 13:48 MB Result MB Qualifier MB MDL MB ROL Analyte mg/I mg/I mg/I - TPH -Oil&Grease U 0.725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3146048-2 06/27/16 13:48 - (LCSD) R3146048-3 06/27/16 13:48 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % TPH -Oil&Grease 20.0 19,8 19.7 99A 985 78.0-114 0.506 18 ONE LAB. NATIOtyWIDE. V ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG883795 Metals_TCP) by Method 200.7 Method Blank (MB) QUALITY CONTROL SUMMARY L843453-01 ONE LAB. NATIONWIDE. (ME) R3146404-1 06/29/16 00:22 MB Result MB Qualifier MB MDL MB ROL Analyte mg/1 mg/I mg/I - Copper U 0.007 t 0.0100 Lead U 0.002 0.00500 Zinc U 0.0034 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3146404-2 06/29/16 00:24 • (LCSD) R3146404-3 06/29/16 00:27 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec, Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgA mg/I mgA % % % % % Copper 1.00 1.02 1.03 102 103 85 115 1 20 Lead 1.00 1.03 1.05 103 105 85-115 2 20 Zinc 1.00 (1 1.00 99 100 85-115 1 20 L843445-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L843445-01 06/29/16 00:29 • (MS) R3146404-5 06/29/16 00:35 • (MSD) R3146404-6 06/29/16 00:37 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/1 ri mg/I % % % % % Copper 1.00 NO 1.04 1.03 104 103 1 70-130 1 20 Lead 1.00 NO 1.03 1.02 103 102 1 70-130 1 20 Zinc 1.00 NO 1.02 Lot 1101 100 1 70-130 1 20 L843458-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L843458-01 06/29/16 00:40 • (MS) R3146404-7 06/29/16 OOA2 • (MSD) R3146404-8 06/29/16 00:45 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/1 mg/I mgA mgA % % % % % Copper 1.00 ND 1.05 IDS 105 105 1 70-130 0 20 Lead 1.00 NO 1.06 LOS 106 105 1 70-130 1 20 Zinc 1.00 NO 1.02 1.02 100 99 1 70-130 0 20 ACCOUNT: PROJECT: SDG' DATE/TIME PAGE: WG883472 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. ` Volatile Organic Compounds (GC/MS) by Method 624 L843453-01 _ Method Blank (MB) (MB) R3145844-3 06/25/1616:55 MB Result MB Oualifer MB MDL M8 RDL Analyte mg/I mg/1 mg/1 Acrolein U 0.00987 0.0500 Acrylonitrlle U 0.00187 0.0100 Benzene U 0,000331 0.00100 Bromodichloromethane U 0,000380 0.00100 Bromoform U 0,000469 0.00100 Bromomethane U 0.000866 0.00500 Carbon tetrachloride U 0,000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chiorodibromomethane U 0.000327 0.00100 �Chloroethane U 0.000453 0,00500 2-Chlorcethyl vinyl ether U 0.00301 0.0500 Chloroform U _ 0.000324 0.00500 Chloiomethane U _ 0.000276 0.00250 1,2-Dichlorobenzene U t 0.000349 0.00100 1,3-Dichlorobenzene U 0,000220 0.00100 1,4-Dichlorobenzene U 0.000274 0.00100 Dichlorodilluoromethane U 0.000551 0.00500 1,1-Dlchloroethane U 0,000259 0.00100 1,2-Dichloroethane U 0.000361 0,00100 1,1-Dichloroethene U 0,000398 0.00100 trans-1,2-Dichloroethene U 0,000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1.3-Dichloropropene U 0.000418 0.00100 trans-1,3.Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0.00100 0.00500 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0,000780 0.00500 1,1,1-Trichloroelhane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichlofoethene U 0.000398 0,00100 Trichlorofluoromethane U 0.00120 0,00500 Vinyl chloride U 0.000259 0.00100 (S) Toluene -dB 101 90.0-115 (S) Dibromo/luoromethone 98.1 79.0-121 (S)o,o,o-Trilluorotoluene 99,2 90.4-116 (S) 4-Bromofluorobenzene 102 801-120 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG883472 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS( by Method 624 L843453-01 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) LCS) P3145844-1 06/25/16 15:35 • (LCSD) R3145844-2 06/25/1615:55 Analyte Spike Amount mg/I LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rec. % Rec. Limits % Acrolein 0.125 0.102 0,0908 81.9 72.7 88.0-118 Acrylonitrile 0.125 0,131 _ 0.120 105 96.0 71.0-135 Benzene 0.0250 0.0269 0.0252 108 101 73.0-122 Bromodichloromethane 0.0250 0.0264 0.0250 106 100 75.5-121 Bromoform - 0.0250 0,0274 0,0247 110 98.9 7L5-131 Bromomethane 0.0250 0.0444 0.0424 178 170 22.4-187 Carbon tetrachloride 0.0250 0.0245 0.0229 97.9 917 70.9-129 Chlorobenzene 0,0250 0.0282 0.0269 113 107 79.7-122 Chlorodibromomethane 0.0250 0.0279 0.0261 112 104 78.2-124 Chloroethane 0.0250 0.0301 0.0288 121 115 41.2-153 2-Chloroethyl vinyl ether 0,125 0,185 0.159 148 127 23A-162 Chloroform _ 0.0250 0,0269 0.0255 108 102 73.2-125 Chloromethane 0.0250 0.0285 0.0270 114 108 55.8-134 1.2-Dichlorobenzene 0.0250 0,0279 0.0266 112 106 84.7-118 13-0ichlorobenzene 0.0250 0,0274 0.0260 110 104 77.6-127 1,4-Dichlorobenzene 0.0250 0.0275 0.0261 110 104 82.2-114 Dichlorodifluoromethane 0.0250 0.0343 0.0324 137 130 56.0-134 1.UDlchloroethane 0.0250 0,0269 0.0258 108 103 71.7-127 1,2-Dichloroethane 0.0250 0.0253 0.0237 101 94.8 65.3-126 11-Dlchloroethene 0.0250 0,0263 0.0250 105 100 59.9-137 trans-1,2-Dlchloroethene 0.0250 0.0283 0.0265 113 106 72.6125 1,2-Dichloropropane 0.0250 0.0267 0.0252 107 101 77A-125 cis-1,3-Dichloropropene 0.0250 0.0280 0.0266 112 106 77,7-124 trans-1,3-Dichloropropene 0.0250 0.0271 0.0257 108 103 73.5-127 Ethylbenzene 0.0250 0.0283 0.0273 113 109 80.9-121 'Methylene Chloride 0.0250 0.0262 0.0248 105 99.3 69.5-120 1,1,2,2-Tetrachloroethane 0.0250 0.0266 0.0247 106 98.8 79.3-123 Tetrachloroethene 0.0250 0.0279 0.0270 111 108 73.5-130 Toluene 0.0250 0.0249 0.0238 99.6 95.3 77.9-116 1,1,1-Trichloroethane 0.0250 0.0281 0.0273 112 109 71.1-129 1,1,2-Trichloroethane 0.0250 0.0270 0.0251 108 100 81.6-120 Trichloroethene 0.0250 0,0273 0.0261 109 105 79.5-121 Trichloroflucromethane 0.0250 0.0294 0.0276 118 110 49.1-157 Vinyl chloride 0.0250 0.0269 0.0257 108 103 61.5-134 (S)Toluene-d8 102 104 90.0-115 (S) Dibromotluoromethone 107 99.0 79.0-121 (S)0, 0, n- Trifluorotoluene 97.6 99.9 90.4-116 (S)4-Bromofluorobenzene 976 99.0 80.1-120 LCS Qualifier LCSD Oualifier J4 J4 J4 FCp RPD RPD Limits z TC 11.9 8.66 6.56 28.1 20 20 35S 5.45 1D.5 4A8 6.57 4.92 20 20 20 20 20 Cn Sr 6.72 4.44 15.2 20 20 23.5 5.57 5,27 4.80 5.29 20 20 20 20 GI eAl 5.03 5.65 4.18 20 20 20 9SC 6.60 5.16 6.62 5.59 20 20 20 20 5.06 5.26 3.80 5.54 20 20 20 20 7.49 3,06 4.44 20 20 20 2.83 7.44 4.36 20 20 20 6.39 4.85 20 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PACE: WG883472 QUALITY CONTROL SUMMARY Volatile. Organic Compounds (GC/MS) by Method 624 L843453-01 L843188-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L843188-07 06/25/16 19:09 - (MS) R3145844-4 06/25/16 18:10 - (MSD) R3145844-5 06/25/1618:30 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Analyte mg/I mg/I mg/I mg/I % % Dilution Rec. Limits MS Oualifer MSD Oualifer % Acrolein 0.125 ND 0.0944 0.0923 75.5 73.9 1 10.0-200 Acrylonitrile 0.125 NO 0.130 0.126 104 101 1 494-133 Benzene 0.0250 ND 0.0241 0.0244 96.5 97.8 1 58.6-133 IBromodichloromethane O.D250 NO 0.0249 0.0249 99.6 99.7 1 69.2-127 Bromoform 0.0250 ND 0.0259 0.0263 104 105 1 66.3-140 Bromomethane 0.0250 ND 0.0344 0,0345 138 138 1 16,6-183, Carbon tetrachloride 0.0250 ND 0.0224 0.0224 89.4 89.4 1 60.6-139 Chlorobenzene 0.0250 ND 0,0262 OD266 105 107 1 70.1-130 Chlorodibromomethane 0.0250 ND 0.0261 0.0269 , 104 108 1 71.6-132 Chloroethane '• 0,0250 ND 0,0248 0.0250 99.3 100 1 33.3-155 2-Chloroethyl vinyl ether 0.125 ND OD0518 0,00304 4.14 2.43 1 5,00-149 J6 J3 J6 Chloroform _ 0.0250 ND OA248 0,0253 99.1 101 1 66.1-133 Chloromethane 0,0250 ND 0,0214 0,0211 85.5 842 1 40.7-139 1,2-Dichlorobenzene 0.0250 ND 0.0261 0.0266 104 106 1 77.4-127 1,3-Dichlorobenzene 0,0250 NO 0.0261 0.0264 104 106 1 67.9-136 1,4-Dichlorobenzene 0,0250 ND O.0255 0.0261 102 104 1 74A-123 Dichlorodifluoromethane 0.0250 ND 0.0277 0.0269 ill 108 1 42.2-146 1,1-Dichloroethane 0.0250 NO OD251 OD252 100 101 1 64.0-124 1,2-Dichloroethane 0.0250 ND OD234 0.0236 93.6 94.2 1 60.7-132 11-Dichloroethene 0,0250 NO 0.0224 0.0225 89.6 90.1 1 48.8-144 trans-1,2-Dichloroethene 0,0250 ND 0.0241 0.0243 96.4 97.2 1 61.0-132 1,2-Dichloropropane 0.0250 ND 0.0251 0.0250 100 99.8 1 69.7-130 cis-1,3-Dlchloropropene 0.0250 ND 0.0254 0.0255 102 102 1 71.1-129 trans-1,3-Dichloropropene 0.0250 ND 0.0252 0.0256 101 102 1 66.3-136 Ethylbenzene 0.0250 ND 0.0262 OD268 105 107 1 62.7-136 Methylene Chloride 0.0250 ND 0.0236 0,0235 94,6 94.2 1 61.5-125 11,2,2-Tetrachloroethane 0,0250 ND 0,0261 0,0263 104 105 1 64.9-145 Tetrachloroethene OD250 NO 0.0251 OD258 100 103 1 57.4-141 Toluene 0.0250 ND OD227 OD233 90.9 93.3 1 67.8-124 11,1-fichloroethane 0.0250 ND 0,0258 0,0265 103 106 1 58.7-134 1,1,2-Trichloroethane 0.0250 ND OD257 0.0257 103 103 1 74-1-130 Trichlomethene 0.0250 NO 0.0240 0.0244 96.1 97.4 1 48.9-148 Trichlomfluoromethane 0.0250 ND 0.0253 0,0255 101 102 1 39.9-165 Vinyl chloride 0.0250 ND 0.0213 0.0213 85.3 85.2 1 44.3-143 (S) Toluene-d8 102 103 90.0-115 (S) Dibromofluoromethone 101 994 79.0-121 . (S)oo,a-Trlfluorotoluene 98,0 98,5 90.4-116 (S)4-Sromofluorobenzene 99.4 99.6 80.1-120 ONE LAB, NATIONWIDE. M RPD RPD Limits 2.24 27.7 3.12 25.3 1.35 20 0.0700 20 1.40 20 0,450 20.5 0.0100 20 1.69 20 2.87 20 0.740 20 52.0 40 2.22 20 148 20 1.86 20 1.10 20 2.30 20 2.61 20 0.280 20 H90 20 0500 20 0.850 20 0.450 20 0.540 20 1.83 20 2,52 20 0440 20 0.690 20 2.85 20 2.57 20 2.66 20 0.0900 20 T39 20 0.800 20 0.0900 20 rCp ZTc aS5 4Cn Fr 0 FGI $AI 9Sc ACCOUNT: PROJECT: BOG: DATE7TIME: PAGE: WG883337 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608 L843453-01 Method Blank (MB) (MB) R3146014-1 06/27/16 Analyte 09:58 MB Result mg/I MB Qualifier MB MDL mg/I MB RDL mg/I Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0.0000184 0.0000500 Delta BHC U 0.0000197 0.0000500 Gamma BHC U 0.0000176 0.0000500 4.4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0.0000177 0.0000500 Dieldrin - U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0.0000500 Endosulfan II U 0.0000176 0.0000500 Endosulfan sulfate U 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500 Endrin ketone U 0.0000170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U a0000175 0.0000500 Hexachlorobenzene U 0.0000134 0.000D500 Methoxychlor U 0.0000193 0.0000500 Chlordane U 0,0000977 0,000500 Toxaphene U 0,000168 0.000500 (5) Decochlorobiphenyl 717 10.0-156 (S) Tetrochloro-m-xylene 81.2 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3146014-2 06/27/1610:23 • (LCSD) P3146014-3 06127/1610:36 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Aldrin 0.00100 0.000776 0,000746 77.6 74.6 10.0-120 3.91 33.9 Alpha BHC - 0.00100 0,000936 0.000883 93.6 88.3 53.6-125 5.82 22.3 Beta BHC 0,00100 0.000933 0.000891 93.3 89.1 55.8-130 4.58 20.6 Delta BHC 0.00100 0.000880 0.000805 88,0 80.5 42,2-135 8.90 23.3 Gamma BHC 0.00100 0.000925 0,000874 92.5 87.4 54.7-125 5.64 21.1 4,4-DDD 0.00100 0,000880 0.000808 88.0 80.8 - 47.6-144 P 8.47 24.3 4,4-DDE 0.00100 0.000841 0.000774 84.1 77.4 45.0-124 8.27 25.7 4,4-DDT 0.00100 0,000898 0.000842 89,8 84.2 49.8-130 6,46 25.4 Dieldrin 0.00100 0.000899 0.000842 89.9 84.2 55.0-127 6.53 22.9 Endosulfan I 0.00100 0.000903 0.000846 90.3 84.6 54.7-127 6,47 24.3 Fp zTc aSs 4Cn Fr ce [GI 8AI 9Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG883337 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608 _ _ _. L843453-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3146014-2 06/27/16 10:23 - (LCSD) R3146014-3 Spike Amount LCS Result Analyte mg/I mg/I 06/27/16 10:36 LCSD Result mg/I LCS Res. % LCSD Rec. % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % Endosulfan II 0.00100 0.000886 0.000837 88.6 83.7 53.1-135 5.75 23.5 ;Endosulfan sulfate 0.00100 0,000944 0.000880 944 88.0 51.5-132 7.02 26.3 Endrin 0.00100 0.000900 0,000843 90.0 94.3 50.1-131 6.54 29.1 Endrin aldehyde 0,00100 0.000867 0.000826 867 82.6 39.5-137 4.89 28A Endrin ketone 0,00100 0.000882 0.000840 88.2 84.0 53.5-139 4,91 284 Heptachlor 0.00H00 0.000871 0.000807 87.1 80.7 20.7-127 T64 30.5 Heptachlor epoxide 0.00100 0.000881 0.000809 88.1 80.9 56.4-124 8,58 23.1 Hexachlorobenzene 0.00100 0.000844 0.000807 84.4 80.7 26.7-114 4.44 27.6 Methoxychlor 0.00100 0.000955 0.000928 95.5 92.8 48.2-144 2.83 27.8 ' is) Decochlorobiphenyl 65.3 67.0 70.0-156 iS/ Tetrochloro-m-xylene 87.4 77.5 139.137 ACCOUNT: PROJECT: SDG: DATEl1'IME: PAGE: WG883337 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Polychlorinated Biphenyls (GC) by Method EPA-608 L843453-01 Method Blank (MB) (MB) R3145972-1 06/27/16 0947 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/1 PCB 1260 U 0.000120 0.000500 PCB 1016 _ U 0.000100 0,000500 PCB 1221 U 0.0000730 0.000500 PCB 1232 U 0.0000420 0.000500 PCB 1242 U 0.0000470 0.000500 PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 (S) Decochlorobiphenyl 83.2 10.0-156 (S)Tetrochloro-m-xylene 77.7 13.9-137 1CP ZTc aSs 4Cn SSr Ed FGI aAl 9Sc ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: WG883348 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds ,(GC/MS) by Method 625 L843453-01 Method Blank (MB) (MB) R3145855-3 06/26/16 04:29 MB Result Analyte mg/I Acenaphthene U 'Acenaphthylene U Anthracene U 'Benzidine U Benzo(a(anthracene U :Benzo(b)Ouoranthene U Benzo(k)fluoranthene U �Benzo(g,h,i)perylene U Benzo(a)pyrene U Bis(2-chlorethoxy)methane U Bis(2-chloroethyl)ether U Bis(2-chloroisopropyl)ether U 4-Bromophenybphenylether U 2-Chloronaphthalene U 4-Chlorophenyl-phenylether U Chrysene U Dibenz(a,h)anthracene U 33-Dichlorobenzidine U 2,4-Dlnitrotoluene U 2,6-Dinitrotoluene U Fluoranthene U Fluorene U Hexachlorobenzene U Hexachloro-1,3-butadiene U Hexachlorocydopentadiene U '..Hexachloroethane U Indeno(1,2,3-cd)pyrene U Isophorone U Naphthalene U Nitrobenzene U n-Nitrosodimethylamine U 1,2-6iphenylhydrazine U n-Nitrosodiphenylamine U n-Nitrosodi-n-piopylamine U Phenanthrene U Benrylbutyl phthalate U Bis(2-ethylhexyl)phthalate 0.00140 Di-n-butyl phthalate 0.00101 Diethyl phthalate U Dimethyl phthalate U MB Qualifier MB MDL mg/I MB RDL mg/I 0.000316 0,00100 0.000309 0.00100 0,000291 0.00100 0,00432 0,0100 0.0000975 0.00100 0.0000896 0.00100 0.000355 0.00100 0.000161 0.00100 0.000340 0.00100 0.000329 0,0100 0,00162 0.0100 0.000445 0.0100 _ 0.000335 0.0100 0.000330 0,00100 0.000303 0,0100 0,000332 0.00100 0.000279 0,00100 0.00202 0.0100 0.00165 0.0100 0.000279 0.0100 0,000310 0.00100 0,000323 0.00100 0.000341 0.00100 0.000329 0.0100 0.00233 0.0100 0.000365 0.0100 0.000279 0,00100 0.000272 0.0100 0.000372 0.00100 0.000367 0.0100 0.00126 0.0100 0.000318 0,0100 0.000304 0,0100 0.000403 0,0100 0.00D366 0.00100 0.000275 0,00300 1 0.000709 0.00300 1_ 0.000266 0.00300 0.000282 0.00300 0.000283 0.00300 tCp zTc 3$5 4Cn SSr 0 rGI eAl 9Sc ACCOUNT: PROJECT: SDG: DATEfrlME: PAGE: WG883348 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625 L843453-01 Method Blank (MB) (MB) R3145855-3 06/26/16 04:29 MB Result Analyte mg4 MB Qualifier MB MDL mgA MB RDL mg/I Di-n-octyl phthalate 0,000969 J 0,000278 0.00300 -Pyrene U. 0.000330 0.00100 1,24-Trichlorobenzene U 0.000355 0.0100 4-Chlorc-3-methylphenol U 0.000263 0.0100 2-Chorophenol U 0.000283 0.0100 2,4-Dichlorophenol U 0.000284 0,0100 2.4-Dimethylphenol U 0.000624 0.0100 4.6-Dinitro-2-methylphenol U 0.00262 0.0100 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0.0100 Phenol U 0.000334 0.0100 2,4,6-Trichlorophenol U 0.000297 0.0100 (S)Nitrobenzene-d5 56.3 21.8-123 (S) 2-Fluorobiphenyl 64.3 29.5-131 (S)p-Terpheoyl-dN 74.9 29.3-137 (S) Phenol-d5 _. 23.1 5.00-70.1 (S) 2-Fluorophenol 33.3 10.0-77.9 (S) 2,4,6-Trtbromophenol 58.4 11.2-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3145855-1 06/26/16 03:19 • (LCSD) R3145855-2 06/26/16 04:06 Analyte Spike Amount mg/I LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rec % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % Acenaphthene 0,0500 0.0373 0.0379 74.6 75.8 387-109 1.61 21.5 Acenaphthylene 0,0500 0.0386 0.0401 77.3 80.1 36.0-106 3.58 21 Amhracene 0.0500 0.0389 0.0396 77.8 79.2 43.6-113 1.75 18.8 Benzidine 0,0500 0.0215 0.0267 43.1 53.5 10.0-165 21.5 40 Benzo(a)anthracene 0,0500 0.0371 0,0369 74.2 73.7 51.2-112 0,710 20 Benzo(b(fluoranthene 0,0500 0.0386 0.0390 77.2 78,0 47.6-111 1.07 .20 Benzo(k)fluoranthene 0,0500 0.0377 0.0379 75.5 75.8 49.4-114 0.440 20 Benzo(g,h,i)perylene 0.0500 0.0386 0.0381 77.1 76.2 45.2-117 1.14 20 Benzo(a)pyrene 0.0500 0.0390 0,0391 78.0 78.3 45.6-106 0.350 20 Bis(2-chlorethoxy)methane 0.0500 0.0332 0.0335 66.5 66.9 37.2-111 0.720 24.1 Bis(2-chlorcethyi)ether 0.0500 0.0296 0,0281 59.2 56.3 22.6-108 5.09 27.9 Bis(2-chloroisopropyl)ether 0.0500 0.0345 0.0319 69.0 63.8 32.9-100 7.81 25.1 4-Bromophenyl-phenylether 0.0500 0.0364 0.0363 72.8 72.5 403-116 0.360 21 Cp FTC 3Ss 4Cn Fr 0 [GI aAl ySc ACCOUNT: PROJECT: SDG: DATE[UME: PAGE: WG883348 QUALITY CONTROL SUMMARY Semi Volatile.Organic Compounds (GC/MS)_by Method. 625 L843453-01 ONE LAB. NATIONyJIDE. v Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (1-CS) R3145855-1 06/26/16 03:19 • (LCSD) R3145855-2 06/26/16 04:06 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I mg/I 2-Chloronaphthalene. .' 0,0500 0.0333 0.0346 4-Chlorophenyl-phenylether 0.0500 0.0365 0.0375 1,2-Diphenylhydrazine 0.0500 0.0396 0.0400 Chrysene 0.0500 0.0376 0.0378 Dibenz(a,nanthracene 0,0500 0.0387 0.0384 3.3-Dichlorobenzidine 0.0560 0.0478 0,0503 24-Dinitrotoluene 0.0500 0.0391 0.0420 2,6-Dinitrotoluene 0.0500 0.0356 0,0371 Flucranthene 0.0500 0.0400 0.0414 _ _ _ _ _ Flucrene 0.0500 0.0363 0.0389 Hexachlorobenzene 0.0500 0.0351 0.0362 Hexachloro-1,3-butadiene 0.0500 0.0297 0.0295 IHexachlorocyclopentadiene 0.0500 0.0277 0.0290 Hexachloroethane 0.0500 0.0272 0.0267 Ilndeno(L2,3-cd(pyrene 0.0500 0.0397 0.0393 Isophorone 0.0500 0.0348 0.0357 Naphthalene 0,0500 0.0314 0.0318 n-Nitrosodimethylamine 0,0500 0.0222 0,0207 Nitrobenzene 0.0500 0.0309 0.0311 n-Nitrosodiphenylamine 0.0500 0.0375 0.0389 �n-Nitrosodi-n-propylamine 0.0500 0.0308 0.031i Phenanthrene 0.0500 0,0356 0,0373 Benzylbutyl phthalate 0.0500 0.0400 0,0389 Bis(2-ethylhexyl(phthalaie 0.0500 0.0404 0.0397 Di-n-butyl phthalate 0.0500 0.0384 0.0395 Diethyl phthalate 0,0500 0.0416 0.0418 Dimethyl phthalate 0.0500 0.0384 0.0388 DIT-octyl phthalate 0.0500 0.0389 0.0388 IPyrene 0.0500 0,0399 0.0386 1,2,4-Trichlorobenzene 0.0500 0.0283 0.0283 4-Ch loro-3-methylp hen ol 0.0500 0.0364 0.0381 2-Chlorophenol 0.0500 0.0277 0.0281 2,4-Dichloiophenol 0.0500 0,0347 0.0354 24-Dlmethylphenol 0.0500 0.0342 0.0353 4.6-Dinitro-2-methylphenol 0.0500 0.0232 0.0329 24-0initrophenol 0.0500 0,0149 0.0186 2-Nitrophenol 0.0500 0.0333 0.0351 4-Nitrophenol 0.0500 0.0129 0.0164 ,Pentachlorophenol 0.0500 0.0321 0.0348 Phenol 0,0500 0.0141 0,0154 LCS Rec. LCSD Rec. Res. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 66.6 69.2 33.6-105 3,83 23 73.0 74.9 39.0-113 2.58 20.9 79.2 79.9 37.6-111 0,820 21.1 75.2 75.5 54.6-120 0.460 20 77.4 76.8 42.8-118 0,750 20 95.7 101 27.2-142 4.91 22.3 78.2 84.0 31.2-105 7.13 22 71.2 74.2 30.6-106 4,21 23.1 80.0 82.9 45.9-115 3.50 20 76.6 77.9 41.0-112 1.63 20.2 70.2 72,4 38.5-116 3,01 20.1 59.4 59.0 16.1-104 0.580 31.2 55A 58.0 10.0-121 4.59 27.9 54.5 53.4 16.5-89.8 2.03 30.7 79.4 78.6 45.0-116 0.950 20 69.5 71.4 35.4-112 2.62 21.5 62.8 63.5 32.2-101 1.06 23.8 44.5 41.3 10.0-80.1 7.28 37.5 61.9 62.1 31.4-106 0.400 25.7 75.0 77.8 44.4-113 3,65 20 61.5 62.2 33.2-106 1.10 23.7 71.2 74.5 46.4-113 4.57 20 80.0 77.9 31.8-123 2.69 20.7 80.8 79.3 36.9-134 1.84 23.6 76.9 78.9 41.8-120 2.60 20.2 83.3 83.6 36.5-129 0.390 20 76.8 77.6 35.3-128 1.07 20.8 77.8 77.6 397-112 0.160 21.1 79.7 77.3 46.3-117 311 20 56.6 56.6 22.9-96.1 0.0300 27.5 72.8 76.2 35.7-100 4.58 22.9 55.5 56.1 26.2-91.5 1.16 26.5 69.4 70.8 31.4-103 2.02 24.9 68A 70.6 31.9-107 3.15 25.7 46.3 65.9 18.4-148 J3 34.9 24.4 29.8 37.2 24.2-128 J3 22.2 20.5 66.5 70.2 25.9-106 5.31 26.9 25.8 32.8 10.0-52.7 24.1 40 64.2 69.6 10.9 974 8.06 35.1 28.2 30.9 10.0-57.9 8.91 35 ACCOUNT: PROJECT. SDG: DATE/TIME: PAGE: WG883348 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 625 L843453-01 ONE LAB. NATIONWIDE. V Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3145855-1 06/26/16 03:19 • (LCSD) R3145855-2 06/26/16 04:06 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Oualifier LCSD Oualifer RPD RPD Limits Analyte _ mg4 mg4 mg/I % . % % % % 2,4,6-Trichlorophenol 0.0500 0,0343 0.0366 68.5 73.3 29.8-107 6.71 24.1 (S) Nitrobenzene-d5 62.0 62.2 21.8-123 (S)2-Fluorobiphenyl 68.9 68.9 29,5-131 - (S)p-Terphenyl-dN 774 74.5 29.3437 (S)Phenol-d5 25.5 277 5,00-70.1 (S)2-Fluorophenol 34.7 35.9 10.0-779 (S)2,4,6-Trlbromophenal 677 73.1 11.2-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Defnitions C SDG Sample Delivery Group. p MDL Method Detection Limit. z RDL Reported Detection Limit. Tc U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. 3S5 Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) (S) from a quality control sample. The Original Sample may not be included within the reported SDG. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control 4Cn Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. 5 Rec. Recovery. Sr Qualifier Description 6Qc B The same analyte is found in the associated blank. J The identification of the analyte is acceptable; the reported value is an estimate. J3 J4 The associated batch OC was outside the established quality control range for precision. The associated batch CC was outside the established quality control range for accuracy. El: The sample matrix interfered with the ability to make any accurate determination, spike value is low. 9Sc ACCOUNTPROJECT: SDG: DATE/TIME: PAGE: ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. 0 ESC Lab Sciences is the only environmental laboratory accreditedhertilied to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the - network laboratories in our industry. The most significant benefit to our "one location' design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time. and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. ' Not all certifications held by the laboratory are applicable to the results reported in the attached report. State Accreditations I Cp TC Alabama 40660 Nevada TN-03-2002-34 3SS Alaska _ _ UST-080_ New Hampshire _ 2975 Arizona_ AZ0612 New Jersey_NELAP _ _ Arkansas -_ _ _ _ 88 0469 _ -_ -__ _ New _Mexico _TNO02 _ TN00003 ° Cn California 07157CA _ _ New York 17742 Colorado TN00003 North Carolina Env375 ConnetiCut_ --_ PH_0197 North Carolina' DW21704 _-. _.. s Sr Florida _ E87487--- North Carolina' _ _._. _41_ _-_ Georgia_— _ _ NELAP _ North Dakota _ _ _ _ R-140 5Qc Georgia 923 Ohio-VAP CLOO69 Idaho TN00003 m laho_a 9915 _ _ _ Illinois _ _ _ 200008 _ Oregon TN200002 Indiana _ _ _ C TN 01_ Pennsylvania _ _ _ 68-02979 _ GI Iowa - 364 Rhode Island 221 Kansas E-10277 South Carolina B4004 Kentucky' _ _ 90010 South Dakota_ _ nla _ Kentucky' _ _ _ 16 _ _ To 4 _ 20_06 Louisiana - -_-_- - _---_--_ A130792 Texas T104704245-07-TX y - ----- Maine TN00_02 LA80152 SC Maryland - 324 Utah 6157585858 Massachusetts M-TN603 Vermont VT2006 Michigan 9958 Virginia _ 109 Minnesota 047-999-395 Washington C1915 Mississippi -_ TN00003 -_ -- West Virginia_ - _ _233 Missouri _ 340 Wisconsin 9980939910 Montana C_FR_T0086_ Wyoming _ A21-A Nebraska NE-OS-15-05 Third Party & Federal Accreditations A2LA-IS017025 1461.01 AIHA_ 1007_89 A2LA-ISO 17025s 1461.02 - - _ DOD _ 1461.01 Canada 1461.01 _ USDA S-67674 EPA-Crypto _ TN00003 'Drinking Water' Underground Storage Tanks 3Aquapc Toxicity ' Chemical/Microbiological `Mold " Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. WA O " MT NO OR 'AN T IO SO T WI T ryy �•rr � TaI T t rA T • RA A • T Nv T OF • T T cTI l UT CO •T, • b✓V VAT � T KS ? '(V• • T • T T f— act T •Az NM �? ArT • T T sc TNAS AL GA T X IFT LA •.__sT T 'f' • • AK T • • "C' FL T • ...n B HI i i ACCOUNT: PROJECT: EGG: DATEIFIME: ME PAGE: d t' tornparry-NaMe/Add 'Wng-Infwmatiom Analysis/ -Container -!-Preservative ChJinol.Caatody—Falle_ _ j Eaton Corporation NA Flnarclal J. ',' PO Box 618024 l i j J* E,S�;'c 2564; Durham'Rd Cleveland; OH 44181-8024 _ Rozlioro'NC•27573 4 ` i ,L .. / y .13 S. C'I. C'N.C. E-$ d' .n -J' ]J0651b -nRtlM1r �.■• ■ - RePorlto - - - Email To t4„•.v �-. 0I 0�. �•V r' a .- DustinLaCI r-1— .;_. .,, ustinlaclair@Eaton.com " .. i'4 Y' [ ++ i§ V., i ZI 2 fl L 0 { Z m t Z ~1', ,Z S„ 3� �� N n, , "W; '' Mount i l t TN 37122 PM 61s)sa6659 PM R90 )6>.SBs9 J, Fa 615)5a5a59 Project ✓ - City/State Eaton Corp Annual,,Stormwater Roxboro -,NC a N ,Q n d, 1 ,Semi Description Collected: ., - u v, Z 'o ,C: - w. .. r. ire y+s ^. •� d ,� d '- j LN ' 336 599 1141 Client Projectp ;Lab Project.g A126 Phone a 2809t W, - EATONRNC-28091SW h' 1A �gz a .! d o Z r� X'E I N: _ o t ,; tp i m tPlE., . i :o _ AcctnemEATONRNC �'i° Collected by (print): ,- s ;_ Site/Facility ID a w. P.O. p i e, _ k, w rJ, vJ E E r PR r = :s X, �. K " o i -at m o r ao ' 4 Template ,• S i R'.^ri. _• fi 1x 6 Call d b signature Rush7'(Lab MUST 8e Notifietl) :Date Results Needed 5imebaY„ .....2W% � o 81Sf Email? No es i No _Next Day- ......100% i-. �° X = t N A, TSR tj , Hunt ur' ' ImmedlatelYJ. °..•,. w, / ...:--7wa Day..............................StM6 ✓No Yes , d-'., kip ] x- j �, d O of Cooler pt ay Packed on Ice N_ Y_ _Three Day....... ..35% •:' ........... ;.,,•FART — of ,• , ,.„O' k' to i = a..' c v s N co, bj Shipped Vla Raleigh Si!m k -� .Sample ID Comp/Grab Matrix' ,Depth Date Time, nVs a F �a.� H. 7 U rl ) Rem/eani.m o.m smP�e RP.b o�Ml ZDlto ; --27- ODs;— : via '-!^;W - -•N n_ - o(a zz (&. .1 125 _ r9 ", � X IJO a X. vX .. X:'►r1. _ bi'1 +: 'rOOI-:R OOM'CR6+kC:H .. WW. -i F _ y t 6 .,1' y. 1' i -,, - _.' 4 . ..". 5 c,!^.,t C✓Y. .h .., : '� :., RCr.t9 �, % A • N it _ni Y, - 'Matrix: SS - Soil GW-Groundwater WW WasteWater DW- Drinking Water OT - Other _ pH '-Temp' ,.. Remarks:c .. =.' s ,, ;. ,. Flow Other Hold p. •- ,, r �,. �. c Relin hed I atttuurre) ,k Dare - Time: Received by: (Signature) Samples returned via: ❑ UPS - r _ Conditlon rr„ (lati use only) • . - u�"t" Ob 1+'S; lb: �3� •, " . ,-_. Ex ❑Couiiei. ❑ Z28 ' • y Relinquishedby '(Signature)Fw.n Date: a Time Received t,, by: (Signature) q' Te p tJ Bottles Received:--„9 r :i ,.' F "'.�..w. WC -Seal ln`[aCl�f� Y'_:� ry. .; Relinquished by :'(Signatu)'•, Date: .i-Time: RYecelved for labb Signaure)1 �. Date:' •' Time: ,u'I` pCheckedt"�. ,y, NCf ;. c a ANALYTICAL REPORT myESC May 25, 2016 NC.Gd 36�ar7 Eaton Corporation Sample Delivery Group: Samples Received: Project Number: Description: Site: L836370 05/18/2016 28091-R' Eaton Corp Semi -Annual Stormwater ROXBORO,NC Report To: Dustin LaClair ` Fc S/Vj 2564 Durham Road 5 ZO) Roxboro, NC 27573 CANT CwR 82-C7.10A Entire Report Reviewed By: 41t"Vp Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This lest report shall not be reproduced, except In full, without when approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. } { i v TABLE OF CONTENTS ONE LAB. NATIONWIDE. V 'Cp: Cover Page 2Tc: Table of Contents 'Ss: Sample Summary 'Cn: Case Narrative 'Sr: Sample Results 2016-5-17-001 POND L836370-01 2016-5-17-005 TOOL ROOM TRENCH L836370-02 6Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 U^ Volatile Organic Compounds (GC/MS) by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 'GI: Glossary of Terms 'Al: Accreditations & Locations 9Sc: Chain of Custody 1 2 3 .4 5 5 9 13 13 14 15 16 21 23 24 28 29 30 ACCOUNT: PROJECT: SDG: DATEMME: 2016-5-17-001 POND L836370-01 WW Method Gravimetric Analysis by Method 2540 D-2011 Metals (ICP) by Method 200.7 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 Volatile Organic Compounds (GUMS) by Method 624 Volatile Organic Compounds (GC/MS) by Method 624 Wet Chemistry by Method 1664A SAMPLE SUMMARY Collected by Kirk Spicer Balch Dilution Preparation t'1 date/time WG874188, '� 1 05/21/1604:18 WG 874021 1 05/22/1619:32 WG873940 1 05/20/1613:40 WG873940 1 05/20/161140 WG873716 1 05/19/16 09:17 WG873315 1 05/19/16 03:25 WG874261 1 05/20/16 20:44 WG874876 1 05/24/16 08:18 2016-5-17-005 TOOL ROOM TRENCH L836370-02 WW Method Gravimetric Analysis by Method 2540 D-2011 Metals (ICP) by Method 2003 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 Volatile Organic Compounds (GC/MS) by Method 624 Volatile Organic Compounds (GC/MS) by Method 624 Wet Chemistry by Method 1664A Collected by Kirk Spicer Batch Dilution Preparation date/time WG874188 1 05/21/16 04:18 WG874021 1 05/221619:32 WG873940 1 05/20/1613:40 WG873940 1 05/20/1613:40 WG873716` 1 05/1911609:17 WG873315 1 05/19,16 03:45 WG874261 1 05/20/16 2103 WG874876 1 05/24/16 08:18 ONE LAB. NATIONWIDE. Collected date/time Received date/time 05/17/1611:55 05/18/16 09:00 ID IC Analysis Analyst date/time Tic 0512111605:57 --- 05/2/163 LTB 05/20/161616:33 VKS 05/2311614:22 CLG 0520/1613:59 JF 4Cn 05/19/1603:25 BMB 05/2011620:44 BMB s 05/24/1615:51 SHG Sf Collected date/time Received date/time 6QC 05/17/1612:19 05/18/16 09:00 61 Analysis Analyst date/time 05/21/16 05:57 aA( 05/2311609:55 LTB 05/20/1616:46 VKS 9SC 0523/1614:34 ADF 05120/1612 03 JF 05/19/1603:45 BMB 05/20/1621:03 BMB 05/24/1615:51 A SHE ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the: , -, analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualifed within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. ' LVIL- Jimmy Hunt Technical Service Representative ICp FTC 3Ss SSr 6Q� �GI BAI 9SC ACCOUNT: PROJECT: SDG: DATEKIME: PAGE: 2016-5-17,D01•POND SAMPLE RESULTS - Q1 ONE LAB. NATIONWIDE. - Collected date/time: 05/17/16 11:55 L836370 - Additional Information C Result Units - p Analyte pH (On Site) 7.1 su TC ,Temperature (on -site) 18.4 Deg C - ' Gravimetric Analysis by Method 2540 D-2011 3Ss Result Qualifier MDL RDL Dilution Analysis Batch 4 Cn Analyte mgA mgA mgA date/time Suspended Solids 103 0.350 2.50 1 051211201605:57� WG874188 Wet Chemistry by Method 1664A 6 Result Qualifier MDL RDL Dilution Analysis Batch � QC Analyte mg/1 mgA mg/I date/time TPH- Oil&Grease iU 0325 5.26-_-_1�_- 05/24/201615:51 �-WG874876 V [GI Metals (ICP) by Method 200.7 s AI Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgA mgA mg/I date/time s Copper U 0.00700 0.0100 1 05/23/201609:52 WG874021 SC Lead U 0.00200 0.00500 1 05f23/201609:52 WG874021- Zinc 0.0859 0.00340 0.0500 1 05/23/201609:52 WG874021 Volatile Organic Compounds (GC/MS) by Method 624 Analyte Result mg/I Qualifier MDL mgA RDL mg/I Dilution Analysis date/time Batch Acrolein U J4 MOM 0.0500 1 05/20201620:44 WG874261 Acrylonitrile U DD0187 0.0100 1 05/19201603:25 WG873315 Benzene U 0.000331 0.00100 1 05/19/201603:25 WG873315 Bromodichloromethame U 0.000380 0.00100 1 05/191201603:25 WG873315 Bromoform U 0,D00469 0.00100 1 05119/201603:25 WG873315 Bromomethane U 0.000866 0.00500 1 05119201603:25 WG873315 Carbon tetrachloride U 0,000379 0.00100 1 05/19/2016 03:25 WG873315 Chlorobenzene U 0.000348 0,00100 1 05A9/201603:25 WG873315 Chlorodibromomethane U 0.000327 0.00100 1 05/19/201603:25 WG873315 Chtoroethane U 0.000453 0,00500 1 05/19201603:25 WG873315 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 05/192016 03:25 WG873315 Chloroform U 0.000324 0.00500 1 05/19/2016 03:25 WG873315 Chloromethane U 0,000276 0.00250 1 D5/191201603:25 WG873315 1,2-Dichlorobenzene U 0.000349 0.00100 1 05119201603:25 WG873315 1,3-Dichlorobenzene U 0.000220 0.00100 1 05/19/2016 03:25 WG873315 1,4-Dichlorobenzene U 0.000274 0.00100 1. 05/19/201603:25 WG03315. Dichlorodifl uo rom ethane U 0.000551 0.00500 1 05119/201603:25 WG873315 1,1-Dichloroethane U 0.000259 0.00100 1 05/19201603*25 WG873315 1,2-Dichloroethane U 0.000361 0.00100 1 05/19201603:25 WG873315 I,i-Dichtoroethene U 0.000398 0.00100 1 05/192016 03:25 WG873315 [tans-1,2-1)ichlomethene U 0.000396 0.00100 1 05/19/201603:25 WG873315 1,2-Dichloropropane U 0.000306 0,00100 1 05119/201603:25 WG873315 _Is-73-Dichloropropene U 0.000418 0.00100 1 051191201603:25 WG873315 trans-1 3-Dichloropropene U 0.000419 0,00100 1 05/19/2016 03:25 WG873315 thylhenzene U 0.000384 0.00100 1 05/19/201603:25 WG873315 Methylene Chloride U 0.00100 0.00500 1 0S/192016 D3:25 WG873315 1,1,2,2-Tetrachloroethane U 0,000130 0.00100 1 05/192016 D3:25 WG873315 retrachloroethene 0.00148 0.D00372 0.00100 1 05/19/201603:25 WG873315 roluene U 0.000780 0.00500 1 05/19/201603:25 WG873315 1,11-Trichloroethane U 0.000319 0.00100 1 05/19/2016 03:25 WG873315 1.1.2-Trichloroethane U 0.000383 0.00100 1 05/192016 03:25 WG873315 ACCOUNT: PROJECT: SDG: DATEMME: PAGE 2016-5-17-,001 POND SAMPLE Collected date/time: 05/17/16 11.55 Volatile Organic Compounds (GC/MS) by Method 624 RESULTS - 01 L836370 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgn mgh mg/I date/time Trichloraemene 0.000599 J 0.000398 0.00100 1 05/19201603:25 WG873315 Trichlorofluoromethane U 0.00120 0.00500 1 05/19201603:25 WG873315* Vinyl chloride U 0000259 0.00100 1 05/191201603:25 WG873315 (S)Toluene-d8 101 90.0-115 0-10920160325 WG873315 (S)Toluene-dB102- - 90.0-115 - 05201201620..44 WG874261 (S) Dibromolluoromethone 93.4 79.0-121 05201201620.44 WG874261 (S) DlbromoPluoromethooe 98.8 79.0-121 051191201603r25 WG873315 (S)a,o, o-TriOuorotoluene 102 90.4-116 051191201603:25 WG873315 '. (5/a,o,a-Trilluorotoluene, 97.6 90.4-116 05201207620.44 WG874261 (S)4-Bromotluorobenzene .96..7 80.1-120 05201201620:44 WG874261 (S)4-Bromo7luorabenzene 97.9 sai-bo 05119201603.25 WG873315 Pesticides (GC) by Method EPA 608 Analyte Result mg/I Qualifier MDL mgll RDL mgll Dilution Analysis date/time Batch Aldrin U 0.00000813 0.0000500 1 0520/201616:33 WG873940 T Alpha BHC U 0.0000166 -0.0000500 1 0520/201616:33 WG873940 Beta BHC U 0.0000184 0.0000500 1 05/20/201616*33 WG873940 Delta BHC U 0.0000197 0.0000500 1 05120/201616:33 WG873M0 Gamma BHC U 0.0000176 0,0000500 1 05120/201616:33 WG873940 Chlordane U 0.0000977 0.000500 1 05/201201616:33 WG873940 4,4-DDD U 0.0000170 0.0000500 1 05120/201616:33 WG873940 4,4-DDE U 0.0000164 0.0000500 1 05/2012016 16:33 , WG873940 - 4,4-DDT U 0.0000177 0.0000500 1 05/20/201616:33 WG873940 Dleldrin U 0.00000751 0,0000500 1 05/201201616:33 WG873940 EndosalfanI U 0,0000179 0.0000500 1 05/20/201616:33 WG873940 Endosulfan II U 0,0000176 0.0000500 1 0520/201616:33 WG873940 Endosulfan sulfate U 0,0000196 0.0000500 1 05/20/201616:33 WG873940 Endrin U 0,0000189 0.0000500 1 051201201616:33 WG873940 Endrin aldehyde U 0.0000142 0.0000500 1 05/20/201616:33 WG873940 Endrin ketone U 0.0000170 0,0000500 1 0520/201616:33 WGB73940 Heptachlor U 0.0000108 0.0000500 1 05/20/201616:33 WG873940 Heptachlor epoxlde U 0.0000175 0.0000500 1 05120/201616:33 WG873940 Hexachlorobenzene U 0.0000134 0,0000500 1 05/20/201616:33 WG873940 Methoxychlor U 0.0000193 0.0000500 1 05/20/201616:33 WG873940 Toxaphene U 0.000168 0.000500 1 0520201616:33 WG873940 (S)De ochlorobiphenyl 93.2 10.0-156 OW0201616:33 WG873946 (S)Tetrochloro-m-xylene 81.8 13.9-137 0520201616.33 WG873940 Polychlorinated Biphenyls (GC) by Method EPA-608 Analyte PCB 1016 PCB 1221 PCB 1232 PCB 1242 PCB 1248 PCB 1254 PCB 1260 (S) Decochlorobiphenyl (S) Tetrachloro-m-xylene Result mg/I U U U U U U u 74,7 77.6 Qualifier ONE LAB. NATIONWIDE: ,* MDL RDL Dilution Analysis Batch mg/I mg/I date/time �WGB73940 0.000100 0.000500 1 05/231201614:22 0.0000730 0.000500 1 05/23/201614:22 WG873940 0.0000420 0.000500 1 05/23/201614:22 WG873940 0.0000470 0.000500 1 0523201614:22 WG873940 0.0000860 0.000500 1 05/23201614:22 WG873940 0.0000470 0.000500 1 0523201614:22 WG873940 0.000120 0,000500 1 0523/201614:22 WG873940 10.0-156 052320161422 WG873940 13.9-137 05231201614.22 WG873940 tCF rTc aSs Fr 6QL [GI 6AI 9Sc ACCOUNT: PROJECT: SDG: DATEMME: PAGE: ONE LAB: NATIONWIDE., 2016-54-T00120ND SAMPLE RESULTS -.01 Collecied dateltime. 05/17/16 11.55. - L836370' Semi Volatile Organic Compounds (GC/MS) by Method 625 Analyte Result mgA Qualifier MDL mgA RDL mgA Dilution Analysis date / time Batch Acenaphthene U 0.000316 0.00100 1 05120/201613:59 WG873716 Acenaphthylene U 0.000309 0.00100 1 05120/201613:59 WG873716 . Anthracene U 0.000291 0,00100 1 05/20/201613:59 WG873716 Benildlne U 0.00432 0.0100 1 05R0001613:59 WG873716 Benzo(a)anthracene U 0.0000975 0.00100 1 05/20/201613:59 WG873716 Benzo(b)8uoranthene U 0.0000896 0.00100 1 05201201613:59 WG873716 Benzo(k)lluoranthene U 0.000355 0.00100 1 0520/201613:59 WG873716 ,Benzo(g,h,i)perylene U 0.000161 0.00100 1 0520201613:59 WG873716 Benzo(a)pyrene U 0.000340 0.00100 1 05/20/201613:59 WG873716 'BIs(2-chlorethoxy)methane U 0.000329 0.0100 1 05/20201613:59 WG873716 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 05/20/201613:59 WG873716 8IS(2-chloroisopropyl)ether U 0.000445 0.0100 1 051201201613*59 WG873716 4-Bromophenyl-phenylether U 0.000335 0.0100 1 05/20/201613:59 WG873716 .2-Chloronaphthalene U 0.000330 0.00100 1 05/20/201613*59 WG873716 4-Chlorophenyl-phenylether U 0.000303 HIM 1 05/20/201613:59 WG873716 Chiysene U 0.000332 0.00100 1 05/20/201613:59 WG873716 Dibenz(a,h)anthracene U 0.000279 0.00100 1 05/201201613:59 WG873716 33-Dichlorobenzidine U 0.00202 0.0100 1 05120/201613:59 WG873716 2,4-Dinitrotoluene U 0.00165 0.0100 1 0520/201613:59 WG873716 2,6-Dinitrotoluene U 0.000279 0.0100 1 05/201201613:59 ING873716 1,2-Diphenylhydrazine U 0.00031B 0,0100 1 05/20/201613:59 WG873716 Fluoranthene U 0.000310 0.00100 1 05120/201613:59 WG873716 Fluorene U. 0.000323 0.00100 1 05/201201613:59 WG873716 Hexachlorobenzene U 0.000341 0.00100 1 05/20201613:59 WG873716 Hexachloro-1,3-butadiene U 0.000329 0.0100 1 051201201613:59 WG873716 Hexachlorocydopentadlene U 0,00233 0.0100 1 05/20201613:59 WG873716 Hexachloroethane U 0.000365 0.0100 1 05/201201613:59 WG873716 Indeno(1,2,3-4pyrene U 0.000279 0.00100 1 0520/201613:59 WG873716 Isophorone U 0.000272 0.0100 1 D520/201613:59 WG873716 Naphthalene U 0.000372 0.00100 1 05/20201613:59 WG873716 Nitrobenzene U 0.000367 0.0100 1 05120/201613:59 WG873716 n-Nltrosodlmethylamine U 0.00126 0.0100 1 05/20/201613:59 WG873716 n-Nitrosodiphenylamine U T - 0.000304 0.0100 1 051201201613:59 WG873716 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 05/20/201613:59 WG873716 Phenanthrene U 0.000366 0.00100 1 05/20/201613:59 WG873716 Benzylbutyl phthalate 0.000997 J 0.000275 0.00300 1 05/20201613:59 WG873716 Bis(2-ethylhexyl)phthalate 0.00141 B J 0.000709 0.00300 1 05/20/201613:59 WG873716 DI-n-butyl phthalate 0.000861 B J 0.000266 0.00300 1 DS/20/201613:59 WG873716 Diethyl phthalate U 0.000282 0,00300 1 05/20/201613:59 WG873716 Dimethyl phthalate U 0.000283 0.00300 1 05/20/201613:59 WG873716 Di-n-octyl phthalate 0.00124 B J 0.000278 0.00300 1 05/20/201613:59 WG873716 Pyrene U 0.000330 0.00100 1 05120/201613:59 WG873716 1,2,4-Trichlorobenzene U 0.000355 0.0100 1 05/20/201613:59 WG873716 4-Chloro-3-methylphenol U 0.000263 0.0100 1 05120201613:59 WG873716 2-Chlorophenol U 0.000283 0.0100 1 05/20/2016 13:59 WG873716 2,4-Dichlorophenol U 0.000284 0.0100 1 D5/20/201613:59 WG873716 2,4-Dimethylphenol U 0.000624 0.0100 1 0520/201613:59 WG873716 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 05/201201613:59 WG873716 2,4-Dinitrophenol U 0.00325 0.0100 1 05/201201613:59 WG873716 2-Nitrophenol U 0.000320 0.0100 1 05/201201613:59 WG873716 4-Nitrophenol U 0.00201 0.0100 1 05/201201613:59 WG873716 Pentachlorophenol U 0.000313 0.0100 1 05/201201613:59 WG873716 Phenol U 0.000334 0.0100 1 05/201201613:59 WG873716 2,4,6-Trlchlorophenol U _ 0.000297 0.0100 1 051201201613:59 WG873716 (S)2-Fluorophenol 56.3 = 10.0-77.9 05201201613.59 WG873716 (S)Phenol-d5 41.2 500-70.1 0520201613:59 WG873716 tCP FTC aS5 4Cn 6QC 7GI BAI 9SC ACCOUNT:, PROJECT: SDG: DATE/TIME: PAGE: 2016-5-17-001 POND SAMPLE RESULTS- 01 Collected date/time: 05/17/16 11:55 LB36370 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Oualifier MDL RDL Dilution Analysis Analyte _ mgll ----_— _ mgll mgll --____--�----� —_- — date/time (SJ Nitrobenzene-d5 l�71.2 218-123 051202016,13.59 (S) 2-Fluoroblphenyl 76.3 29.5-131 0520201613.59 (S)2,4,6-Tribromophenol 65.6 71.2-130 0520201613.59 (S) p-Terphenyl-dN 92.3 29.3-137 OW0201613.59 ONE LAB. NATIONWIDE. Batch WGB73716 WG873716 WG873716 WG873716 _ ,CF rTc 3SS QCr 6nL 7 �GYYI BAI 9S� ACCOUNT: PROJECT: SDG: DATE(TIME: PAGE: ;2016-5,17-00.5 TooL;RooM TRENCH SAMPLERESULTS -. 02 ONE LAB. NATIONWIDE. Collected date/time: OS/17/1612:19 "• -L836370 Additional Information Result Units FP Analyte - pH On site) �.� �. 7 su _ _ 2 TC Temperature (on -site) . 18.6 _• Deg C Gravimetric Analysis by Method 2540 D-2011 3Ss Result Qualifier MDL RDL Dilution Analysis Batch 4Gn Analyte mg/I - mgfl mg/I date/time Suspended Solids 7.56 P1 0.350 2.50 1 05/21/2016 05:57 y_WGB74188 Wet Chemistry by Method 1664A Result Qualifier MDL RDL Dilution Analysis Batch 6 QC Analyte mg/I mg/I mg/I date/time - 1PH-Oil &Grease U 0.725 5.26 1 05/24/201615:51 WG874876 7GI Metals (ICP)'by Method 200.7 gA•I. - Result Qualifier MDL RDL - Dilution Analysis Batch lnaly[e mg/I mg/I v mg/I date/time :upper 0.0142 0,00700 0.0100 1 05/23/201609:55 WG674021 v� u� 9SC _ead 0.00300 - J- 0.00200 0,00500 1 05;231201609:55 WG874021 'inc 0,0329 J 0.00340 0.0500 1 05123/201609:55 WG874021 ✓olatile Organic Compounds (GC/MS) by Method 624 - Result Qualifier MDL RDL Dilution Analysis Batch - tnalyte mg/I mg/I mg/I date/time wolein U J4 0.00887 0.0500 -1 05/20/211621:03 WG874261 'crylonitrile U 0.00187 0.0100 1 05/19/2016 03:45 WG873315' lenzene U 0.000331 0.00100 1 05/19/2016 03:45 WG873315 'romodichloromethane U 0.000380 0.00100 1 05t19/201603:45 WG873315 romoform U 0.000469 0.00100 1 05/19/2016 03:45 WG873315 romomethane U 0.000866 0.00500 1 05/19/2016 03:45 WG873315 arbon tetrachloride U 0.000379 0.00100 1 05119/201603:45 WG873315 - hlorobenzene U 0.000348 0.00100 1 05/19/2016 03:45 WG873315 hlorodibromomethane U - 0.000327 0.00100 1 05/19/2016 03:45 WG873315 hloroethane U_ 0.000453 0.00500 1 05/19/2016 03:45 WG873315 -Chloroethyl vinyl ether U 0.00301 0.0500 1 05/19/2016 03:45 WG873315 hloroform U 0.000324 0.00500 1 05/19/2016 03:45 WG873315 hloromethane U 0.000276 0,00250- 1 05/19/2016 03:45 _ WG873315 2-Dichlorobenzene U 0.000349 0,00100 1 05/19/2016 03:45 WG873315 - 3-Dichlorobenzene U 0.000220 0.00100 1 05/19/2016 03:45 WG873315 1-Dichlorobenzene U _ - 0.000274 -_ 0.00100 1. 05/191201603:45 WG873315 chlorodifluoromethane U 0.000551 0.00500 1 051191201603:45 WG873315 _ I-Dichloroethane U 0.000259 0.00100 1 05/19/2016 DIAS - WG873315 2-Dichloroethane U 0.000361 0.00100 1 05/19/2016 03:45 WG873315 =Dichloroethene U _ 0.000398 0,00100 1 05/191201603:45 WG873315 - 3ns-1,2-Dichloroethene U 0.000396 0.00100 1 05/19/2016 03:45 - WG873315 i-Dichloropropane U 0.000306 0.00100 1 05/191201603:45 WG873315 ;71,3-Dichloropropene U 0.000418 0-00100 1 05/19/2016 03.45 WG873315 ins-1.3-Dichloropropene U - 0.060419 '0.00100 1, .05/19/2016 03:45 WG873315 ,ylbenzene U 0.000384 0.00100 1 05/19/2016 03:45 WG873315 a[hylene Chloride U 0.00100 0.00500 1 05/191201603:45 WG873315 ,2,2-Tetrachloroethane U 0,000130 0,00100 1 05/19/2016 03:45 WG873315 trachloroethene 0 0.000372 0.00100 1 05/19/2016 03:45 WG873315 luene U - 0.000780 0.00500 1 05/191201603:45 WG873315 i-Trichloroethane U 0.000319 0.00100 1 05/191201603:45 WG873315 2-Trichloroethane U 0.000383 0.00100 1 05/19/2016 03:45 WG873315. - ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: 2016-5-17.-005 TOOL ROOM TRENCH SAMPLE RESULTS ' 02 Collected dateltime: 05/17/16 12:19 L836370 Volatile Organic Compounds (GC/MS) by Method 624 ONE LAB. NATIONWIDE:' Analyte Result Qualifier mg/I MDL mg/I RDL mg/1 Dilution Analysis date/time Batch Trichloro-et liene U ,0.000398 0.00100 1.1.'t 05/191201603:45 .WG873315 Trichlorofluoromethane U - 0.00120 0.00500 1 Q5119/2016 D3:45 WG873315 Vinyl chloride U 0,000259 0.00100 1 05/19/2016 03:45 WGB73315 (S)Toluene-d8 99.7 90.0-n5 0511WO1603.45 WG873315 (S)Toluene-d8 105- - 90.0-115 05201201621:03 -WG874261- - -- - ' (S) Dibromofluoromethone 93.3 79,0-121. 0512012016 21.03 WG874261 (SJ,Dibromofluoromethone 98.0 79.0-121 0549201603.45 WG873316 (S)o,o,o-Tafluorotoluene 102 90.4-116 0511WO7603.45 WG873315 (S)o.go-Tr7fluorotoluene 101 90.4-116 0520/201621.03 WG874261. -. (5)4-Bromofluorobenzene 972 80.1-120 05120201621.03 WG874261 (S) 4-Bromofluorobenzene 95.7 80.1-120 0511912016 03.45 ,WG873315 - - Pesticides (GC) by Method EPA 608 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mch mg/l mg/I - date/time �,. Aldrin U 0.00000813 _ 0.0000500 1 05120/201616:46� WG873940 Alpha BHC U 0.0000166 0.0000500 1 05/20/201616:46 WG973940 Beta BHC U O.00D0184 0.0000500 1 05/20/201616:46 WG873940 Delta BHO U 0,0000197 0.0000500 1 05/20/201616:46 WG873940 _ Gamma BHC U 0.0000176 0.0000500 1 05/20/201616:46 WG873940 Chlordane U 0.0000977 0.000500 1 05/20/201616:46 WG873940 4,4-ODD U - - 0.0000170 0.0000500 1 05/20/201616:46 WG873940 4,4-DDE- - U 0.0000164 0.000D500 1 -. 05/20/201616:46 WG873940 - •' 4,4-DDT U 0.0000177 0.0000500 1 05/20/201616:46 WG873940 Dieldrin U 0.00000751 0.0000500 1 05/2001616:46 WG873940 Endosulfan I U 0.0000179 0.0000500 1 05/20/201616:46 WG873940 Endosulfan 11 U 0.0600176 - 0,0000500 1 05/20/201616:46 WG873940 Endosulfan sulfate U . 0.0000196 0.000D500 1 05/20/201616:46 WG873940 Endrin U 00000189 0.0000500 1 05/20/2016161.46 WG873940 Endrin aldehyde U 0.0000142 0.0000500 1 05/20/201616:46 WG873940 Endrin ketone U 0.0000170 0.0000500 1 05/20/201616:46 WG873940 Heptachlor U 0.0000109 0.0000500 1 05/20/201616:46 WG873940 . Heptachlor epoxide U 0,0000175 0,0000500 1 05/20/201616:46 WG873940 Hexachlorobenzene U 0.0000134 0.0000500 1 05/201201616:46 WG873940 Methoxychlor U 0.0000193 0.0000500 1 05/20/201616:46 WG873940 '. Toxaphene U 0.000168 0.000500 1 05/20/201616:46 WG873940 (S) Decochlorobiphenyl 69.4 10.0-156 0520201616.46 WG873940 (S)Tetrochloro-m-xylene 64.6 13.9-137 05120201615,46 WG873940 Polychlorinated Biphenyls (GC) by Method EPA-608 Result Qualifier MDL RDL Dilution Analysis Anal e m /I mg/l mg/I date/time Y 9 PCB 1016 -U - 0.000100 0.000500 1 PCB 1221 U 0.0000730 0,000500 1 PCB 1232 0 0.0000420 0.000500 1 PCB 1242 U 0.0000470 0.0DO500 1 PCB 1248 U 0.0000860 0,000500 1 PCB 1254 U 0.0000470 0.000500 1 PCB 1260 U - 0,000120 0,000500 1 (S) Decochlorobiphenyl 63.2 10.0-156 (S) Teeachloro-m-xylene 68.8 13.9-137 05/23/201614:34 05123/201614:34 05/231201614:34 05/23/201614:34 D5/23/201614:34 05/23/201614:34 05/23/201614:34 0523201614:34 051231201614.34 Batch WG873940 WG873940 WG873940 WG873940 WG873940 WG873940 WG873940 WG873940 WG873940 ACCOUNT: PROJECT: SDG: DATE/TIME. PAGE: ONE LAB. NATIONWIDE. 2016-5-17-005 TOOL ROOM TRENCH SAMPLE RESULTS.- 02 Collected date/time: 05/17/16 12:19 L836370 Semi Volatile Organic Compounds (GC/MS) by Method 625 Analyte Result mgA Oualifier MDL mgA RDL mgA Dilution Analysis date/time Balch Acenaphthene U 0.000316 0,00100 t %d 05/20/201612:03 WG873716 Acenaphthylene U 0.000309 0.00100 1. 051201201612:03 WG873716 Anthracene U 0.000291 0.00100 1 0520201612:03 WG873716 Benzidme U 0.00432 0,0100 1 0520/201612:03 W13873716 Benzo(a)anthracene U 0.0000975 0,00100 1 05120/201612:03 WG873716 Benzo(b)fluoranthene U 0.0000896 0.00100 1 05120/201612:03 WG973716 Benzo(k)Fluoranthene U 0,000355 0.00100 1 05/20/201612:03 WG873716 Bynzo(g,h,i)perylene U 0.000161 0.00100 1 0520/201612:03 WG873716 Benzo(a)pyrene U 0.000340 0.00100 1 0520/201612:03 WG873716 6s(2-chlorethoxy)methane U 0.000329 0.0100 1 05/201201612:03 WG873716 Bis(2-chloroethyi)ether U 0.00162 0.0100 1 05/20201612:03 WG873716 Bis(2-chloroisopropyl)ether U 0.000445 0.0100 1 05I20/201612:03 WG873716 4-Bromophenyl-phenylether U 0.000335 0.0100 1 051201201612:03 WG873716 2-Chloronaphthalene U 0.600330 0.00100 1 05R0/201612:03 WG873716 4-Chlorophenyl-phenylether U r 0.000303 0.0100 r;c 1 051201201612:03 WG873716 Chrysene U 0.000332 0.00100 1 0520/201612:03 WG873716 Dibenz(a,h)anthracene U 0.000279 0.00100 1 05/20/201612:03 WG873716 3,3 Dichlorobenzoine U 0.00202 0.0100 1 05/20/201612:03 WG873716 2,4-Dinitrotoluene U 0.00165 0.0100 1 05/20/201612:03 WG873716 2,6-Dini6otoluene U 0.000279 0.0100 1 05/201201612:03 WG873716 1,2-Diphenylhydrazine U 0.000318 0.0100 1 05/20/201612:03 WG873716 Ftuoranthene U 0.000310 0.00100 1 05/201201612:03 WG873716 Fluorene U 0.000323 :0.00100 1 05/20/201612:03 WG873716 Hexachlorobenzene U 0.000341 -0.00100 1 05201201612:03 WG873716 Hexachloro-1,3-butadiene U 0.000329 0.0100 1 05/20/201612:03 WG873716 Hexachlorocyclopentadlene U 0.00233 0.0100 1 0520201612:03 WG873716 Hexachloroethane U 0.000365 0.0100 1 05/20/201612:03 WG873716 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 05/20/201612:03 WG873716 Isophorone U 0.000272 0.0100 1 05/20/201612:03 WG873716 Naphthalene U 0.000372 0.00100 1 05/20/201612:03 WG873716 Nitrobenzene U 0.000367 0.0100 1 05/20/201612:03 WG873716 n-Nitrosodlmethylamine U 0.00126 0.0100 1 05/201201612:03 WG873716 n-Nitrosodiphenylamine U 0,000304 0.0100 1 05120/201612:03 WG873716 n-Nitrosodl-n-propylamine U 0.000403 0.0100 1 05/20/201612:03 WG873716 Phenanthrene U 0.000366 0.00100 1 05/20/201612:03 WG873716 Benzylbutyl phthalate U 0.000275 0.00300 1 05/20/201612:03 WG873716 Bisl2-ethylhexypphthala1e 0.00129 B J 0.000709 0.00300 1 - 05/20/201612:03 WG873716 Di-n-butyl phthalate 0.000884 B J 0.000266 0.00300 1 05/20/201612:03 WG873716 Diethyl phthalate U 0.000282 0,00300 1 05/20/201612:03 WG873716 Dimethyl phthalate U 0.000283 0.00300 1 05/20/201612:03 WG873716 Di-n-octyl phthalate 0.00122 B J 0.000278 0.00300 1 05/201201612:03 WG873716 Pyrene U 0.000330 0.00100 1 0520/201612:03 WG873716 1,2,4-Trichlorobenzene U D.000355 0,0100 1 05/20/201612:03 WG873716 4-Chloro-3-methylphenol U 0.000263 0,0100 1 05/20/201612:03 WG873716 2-Chlorophenol U 0.000283 0,0100 1 05/20/201612:03 WG873716 2,4-Dichlorophenol U 0.000284 0,0100 1 05/20/201612:03 WG873716 2,4-DimethylphenDI U 0.000624 0.0100 1 05/20/201612:03 WG873716 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 05120/201612:03 WG873716 2,4-Dinitrophenol U 0.00325 0.0100 1 05/20/201612:03 WGB73716 2-Nitrophenol U 0,000320 0.0100 1 0520/201612:03 WG873716 4-Nitrophenol U 0.00201 0.0100 1 05/20201612:03 WG873716 Pentachlorophenol U 0.000313 0.0100 1 05/201201612:03 WG873716 Phenol U 0.000334 0.0100 1 05/20/201612:03 WG873716 2,4,6-Trichlorophenol U 0.000297 0.0100 1 05/20/201612:03 WG873716 (5)2-Fluorophenol 573 10.0-77.9 05201201612:03 WG873716 (S) Phenol-d5 42.0 500-70.1 0520201612:03 WG873716 1Cp ' ?TC 3S5 4Cn 6QC 7 GI r1C aAl 9Sc ACCOUNT: -I PROJECT: SDG: DATE/TIME: PAGE: 2016-5-17-'005 TOOL ROOM TRENCH SAMPLE RESULTS = 02 Collected date/time: 05/17/16 12:19 LB36330 Semi Volatile Organic Compounds (GC/MS) by Method 625 ONE LAB. NATIONWIDE. Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgh mg/I mg/I date / time (SJ Nitrobenzene-d5 _ 74.8 A^ �t`-1 21.8-123 _ __, 0520201612.03 T ^ WG873716 (SJ 2-Fluorobiphenyl 79.6 29.5-131 0520201612:03 WG873716 (S)$4,6-Trlbromophenol 819 71.2-130 0520/201612:03 WG873716 (S)p-Terphenyl-d14 92.0 - 29.3-137 0520/201612.03 WG873716 4 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Gravimetrlc Analysis by Method 2540 D-2011 1.836370-01,02 Method Blank (MB) (MB) R3138886-1 05/21/16 0557 MB Result MB Qualifier MB MOIL MB ROL Analyte mg/I mg/I mg/I Suspended Solids U 0.350 ! 2.50""-- L836299-02 Original Sample (OS) • Duplicate (DUP) (OS) L836299-02 05/21/16 05:57 • (DUP) R3138886-4 05/21/16 05:57 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Sollds 37.5 37.8 1 0.664 5 —' L836370-02 Original Sample (OS) • Duplicate (DUP) twr 4-0�0a/U-UZ v0rty lb Ub:b/ • (UUP) R3138886-5 05/21/16 05:57 - Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Solids 7.56 6.89 7 9.23 Pi 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) k—1 �ou00e0-n UDr<V 10 Uo:W • ll-UCU) H3136886-3 05/21/16 05:57 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Suspended Solids 773 788 820 102 106 85.0-115 3.98 5 ,nc Inc. rv, i 111lvc. 4w, LOS ACCOUNT: PROJECT_--_—SDG:--_---- DATERIME: -- -_-- PAGE___--- WG874876 Wet Chemistry by Method 1664A Method Blank (MB) QUALITY CONTROL SUMMARY L836370-01,02 ONE LAB. NATIONWIDE. IV (MB) R3139427-1 05/24/1615:49 MB Result MB Qualifier MB MDL MB RDL Analyte mg/1 mg/I T mg/I TPH - oil & Grease A U 0.725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3139427-2 05/24/16 15:50 • (LCSD) R3139427-3 05/2411615:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyte mg/I mg/I mg/I % % % % TPH QII & Grease _ 20.0 18.2 17.9 91.0 89.5 78.0-114 1.66. RPD Limits 18 Ar cni JNT PROJECT: SDG: DATE/TIME: PAGE; IN 11\VL ju lyl lvl/-Ar\ 1 L836370.01,02 vrvc u D. rvH I IUINVVIvc: _4K, Metals (JCP) by Method 200.7 Method Blank (MB) (MB) R3139058-1 05/23/16 09:30 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Copper U 0.007 0.0100 Lead U 0.002 0.00500 Zinc U 0,0034 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Iw01 n000DD0-< UDr<ono UV:sJ - tLl.SU) H3139U58-3 05/23/16 09:35 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Copper 1.00 0.995 0.999 100 100 85-115 0 20 Lead 1.00 1.01 1.01 101 101 85-115 1 Y0 Zinc 1.00 0.986 0.986 99 99 85-115 0 20 L836409-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) Iw) caaowU7-v1 v5i[snb U9:38 • (MS) R3139058-5 05/23/16 09:44 • (MSD) R3139058-6 05/23/16 09:46 Spike Amount Original Result ME Result MSD Result MS Rec. MSD Rec. Dilution Analyte mg/I mgll mg/I mg/I % % Rec. Limits MS Oualifier MSD Qualifier RPD % % RPD Limits % Copper 'Do NO 0.990 0.984 99 96 1 70-130 1 20 Lead 1.00 NO 1.00 1.00 100 100 1 70-130 0 20 Zinc 1.00 ND 0.984 0,976 98 98 1 70-130 1 20 L836438-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) Iwl L0004J0-v1 voi<ano Ivu • trv15) H3139U68-/ U523/1610:29 • (MSD) R3139058-8 05/23/1610:37 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Copper 1.00 NO 1.00 1.01 too 101 1 70-130 1 20 Lead 1.00 ND 1.03 1.03 103 103 1 70-130 1 _ 20 Zinc 1.00 ND 0,984 1.00 98 100 1 70-130 2 20 ACCOUNT: PROJECT:, SDG: DATE/TIME- PAGE: WG873315 Volatile Organic Compounds (GC/MS) by Method 624 Method Blank (MB) (i R3138314-3 05/18/1618:26 MB Result MS Qualifier MB MDL Analyte ri J mg/I Acrylonitrlle y ^U 0.00187 Benzene U 0.000331 Bromodichloromethane U 0.000380 Bromoform U 0.000469 Bromomethane U 0.000866 Carbon tetrachloride U 0.000379 Chlorobenzene U 0.000348 Chlorodibromomethane U 0.000327 Chloroethane U 0.000453 2-Chloroethyl vinyl ether U 0.00301 Chloroform U 0.000324 Chloromethane U 0.000276 1,2-Dichlorobenzene U 0.000349 1,3-Dichlorobenzene U 0.000220 1,4-Dichlorobenzene U 0.000274 Dichlorodifluoromethane U 0.000551 1,1-Dichloroethane U 0.000259 1,2-Dichloroethane U 0.000361 1,1-Dichloroethene U 0.000398 trans-1,2-Dichloroethene - U 0.000396 1,2-Dichloropropane U 0.000306 cis-1,3-Dichloropropene U 0.000418 trans-1,3-Dichloropropene U 0,000419 Ethylbenzene U 0.000384 Methylene Chloride U 0,00100 1,1,2,2-Tetrachloroethane U 0.000130 Tetracharoethene U 0.000372 Toluene U 0.00078D 1,1,1-Trichloroethane U 0.000319 1,1,2-Trichloroethane U 0.000383 Trichloroethene U 0.000398 Trichlorofluonomethane U 0.00120 Vinyl chloride U 0.000259 (S)Toluene-d8 98.8 (S) Dibromolluoromethone 98.6 (S)a,a,a-Tritluorcroluene 102 QUALITY CONTROL SUMMARY L836370-01,02 MB RDL mg/I 0.0100 0.00100 0.00100 0.00100 0.00500 0.00100 0.00100 0.00100 0.00500 0.0500 0,00500 0.00250 0.00100 0.00100 0.00100 0.00500 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00500 0.00100 0.00100 0,00500 0.00100 0.00100 0.00100 0.00500 0.00100 90.0-115 79.0-121 90.4-116 I ONE LAB. NATIONWIDE. ACCOUNT: PROJECT: SDG: DATEMME: GAGE: Volatile Organic Compounds.(GC/MS) by Method 624 L836370-01,07 .. ♦' ` Method Blank (MB) (MB) R3138314-3 05/18/1618:28 M8 Result MB Qualifier MB MDL MB RDL Analyte mg/I - mg/I mgA XU.I-ILD Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138314-1 05/18/16 16:48 - (LCSD) R3138314-2 05/18/1617:09 Analyte Spike Amount mg/I LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rix. % Rec. Limits % LCS Qualifier LCSD Qualifler RPD % RPD Limits % Acrylonitrile 0.125 0.112 0.112 89.3 89.2 71.0-135 0,130 20 Benzene 0.0256 0.0245 0.0243 98.0 97.1 73.0-122 0.900 20 Bromodichloromethane 0.0250 0.0248 0,0247 99.4 98.7 75.5-121 0.740 20 Bromoform 0.0250 0.0276 0.0273 110 109 71.5-131 0.960 20 Bromomethane 0.0250 0.0241 0.0239 96.5 95.5 22.4-187 1.77 1.11 20 Carbon tetrachloride . 0.0250 0.0238 0.0245 95.0 98.2 70.9-129 20 ' Chlorobenzene 0.0250 0.0273 0.0273 709 109 79.7-122 - 0.0500 20 Chlorodibromomethane 0.0250 0.0266 0,0265 106 106 78.2-124 0.220 20 Chloroethane 0,0250 0.0220 0.0217 88.0 86.8 41.2-153 1.40 20 2-Chloroethyl vinyl ether 0,125 0.119 0.119 95.5 95.0 23.4-162 0.560 23.5 Chloroform 0.0250 0.0239 0.0239 95.5 95.7 73.2-125 0.280 20 Chloromethane 0.0250 0.0246 0.0245 98.5 98J 55.8-134 0.480 20 1,2-Dichlorobenzene 0.0250 0.0261 0.0263 _ 104 105 84.7-118 _ 0.900 20 1,3-Dichlorobenzene 0.0250 0.0279 0.0277 111 111 77.6-127 0.720 20 1,4-Dichlorobenzene 0.0250 0.0264 0.0263 106 105 82.2-114 0.340 20 Dichlorodinuoromethane 0.0250 0.0301 0.0301 120 120 56.0-134 0.0500 2D 1,1-Dichloroethane 0.0250 0.0239 0.0234 95.5 93.6 71.7-127 2.60 20 ' 1.2-Dichlorbethane 0.0250 0.0216 0.0217 86A 86.7 65.3-126 0.340 20 1,1-Dichloroethene 0.0250 0.0227 0.0234 90.9 93.4 59.9-137 2.72 20 trans-1 MbIfiloroethene 0,0250 0,0252 0.0252 101 101 72.6-125 0.220 20 1,2-Dichloropropane 0.0250 0.0252 0.0245 101 98.2 77.4-125 2.74 20 . cis-1,3-Dlchloropropene 0.0250 0.0254 0.0252 101 101 77.7-124 0.740 20 trans-1,3-Dichloropropene 0.0250 0.0226 0.0226 90.5 90.5 73.5-127 0.000 20 Ethylbenzene 0.0250 0.0276 6.0272 110 109 80.9-121 747 20 Methylene Chloride 0.0250 0.0247 0.0248 98.8 99.4 69.5-120 0.610 20 1,1,2,2-Tetrachloroethane 0.0250 0.0251 0.0255 101 102 79.3-123 1.25 20 Tetrachloroethene 0.D250 0.0285 0.0275 114 110 73.5-130 3.58 20 Toluene 0.0250 0.0257 0.0252 103 101 77.9-116 1.92 20 , 1,1,1-Trichloroethane 0.0250 0.0249 0.0252 99.6 101 71.1129 1.09 20 ACCOUNT:. PROJECT: 3DG: DAT&TIME: PAGE:- WG873315 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 624-L836370.01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138314-1 05/18/16 16:48 • (LCSD) R3138314-2 05/18/1617:09 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I mgll LCS Rec. % LCSD Rec. % Rec Limits % LCS Oualifier LCSD Oualifier RPD % RPD Limits % 1,1,2-Trichloroethane 0.0250 0.0258 0.0255 103 102 v 81.6-120 -1.44 20 Trlchlorcethene 0.0250 0.0266 0.0259 106 104 79.5-121 2.59 20 Trlchlorofluoromethane 0.0250 0.0218 0.0215 87.0 85.9 49.1-157 1.30 20 Vinyl chloride 0.0250 0.0234 0,0230 93.5 91.8 61.5-134 1.86 20 (5)Toluene-d8 100 too 90.0-115 (S) DibromoBuoromethone 98.4 98.2 79.0-121 (S) c c o-Trifluorotoluene 102 102 90.4-116 (S)4-Bromofluorobenzene 97.1 978 80.1-120 L835775-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (05) L835775-01 05/18/16 23:43 • (MS) R3138314-4 05/18/16 19:45 • (MSD) R3138314-5 05/18/16 20:05 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Analyte mg/I mg/I Mgt[ mg/I % % AcryloniMle - 0,125 U 0.128 0.118 103 94.1 1 Benzene 0.0250 U 0,0230 0.0220 92.2 88.0 1 Bromodichloromethane 0,0250 U 0.0249 0,0236 99.6 94.4 1 Bromoform 0.0250 U 0.0286 0.0270 114 108 1 Bromomethane 0.0250 U 0.0192 0.0184 76.8 73.4 1 Carbon tetrachloride 0.0250 U 0.0227 0.0220 91.0 88.1 1 Chlorobenzene 0.0250 U 0.0260 0.0252 104 101 1 Chlorodibromomethane 0.0250 U 0.0270 0.0256 108 103 1 Chloroethane 0,0250 U 0.0189 0.0181 75.6 72.2 1 2-Chlomethyl vinyl ether 0.125 U 0.0132 0.00786 10.6 6.29 1 Chloroform 0.025D U 0.0234 0.0224 937 89.7 1 Chloromethane 0.0250 U 0.0183 0.0179 73.1 71.7 1 1,2-Dichlorobenzene 0.0250 U 0.0259 0.0254 104 101 1 1,3-Dichlorobenzene 0.0250 U 0.0267 0.0260 107 104 1 1,4-Dichlorobenzene 0.0250 U-;0.0262 0,0254 105 102 1 Dichlorodifluoromethane 0.0250 U 0.0249 0.0242 99.6 96.7 1 1,1-Dichloroethane 0.0250 U 0.0229 0.0220 91.5 BT9 1 1,2-Dichloroethane 0.0250. U 0.0218 0.0208 87.3 83.1 1 1,1-Dlchloroethene 0.6256 U 0.0208 0.0199 83.2 79.5 1 trans-1,2-Dichloroethene 0.0250 U 0,0224 0.0213 89.7 85.0 1 1,2-Dichloropropane 0.0250 U 0.0245 0,0237 _ 98.0 95.0 1 cis-13-Dichloropropene 0.0250 U 0.0245 0.0237 98.5 94.8 1 ONE LAB. NATIONWIDE. ' Rec. Limits MS Qualifier MSD Oualifier RPD RPD Limits 49A-133 8.81 25.3 . 58.6-133 4.70 20 69.2-127 5.32 20 66.3-140 5.89 20 16.6-183 4.49 20.5 KIS-139 3.24 20 70.1-130 3.30 20 . 71.6-132 5.10 20 , 33.3-155 4.60 20 5.00-149 J3 51.0 40 66.1-133 4A0 20 403-139 1.98 20 77A-127 2.25 20 67.9-136 2.84 20 74.4-123 ., 2.95 20 42.2-146 2.93 20 64.0-134 4.03 20 603-132 4.88 20 48.8-144 4.55 20 61.0-132 5,30 20 69.7-130 3.13 20 71.1-129 3.78 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: VV VaJ/ JJ Iu k-,1 CJHL1 I T k-; IJ IN 1 M%jL JU IVI IVIHK T Volatile Organic Compounds (GC/MS) by Method 624 L836370-01,02 L835775-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L835775-01 0S/18/16 23:43 - (MS) R3138314-4 05/18/16 19:45 • (MSD) R3138314-5 05/18/16 20:05 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier Analyte mg/I mg/l mg/l mg/I % % % trans-1,3-Dichloropropene 0,0250 U 0.0226 0.0214 90.5! - 85.7 1 66.3-136 Ethylbenzene 0.0250 U 0,0261 0,0250 104 99.9 1 62.7-136 Methylene Chloride 0,0250 U 0.0231 0.0219 92.4 87.4 1 61.5425 11.2,2-Tetrachloroethane 0.0250 U 0.0274 0.0259 110 103 1 64.9-145 Tetrachloroethene 0,0250 U 0,0254 0.0243 102 97.2 1 57.4-141 Toluene 0.0250 U _ 0.0240 0.0230 96.0 92.0 1 67.8-124 1,1.1-Trichloroethane 0.0250 U 0.0237 0.0228 94.7 91.1 1 58.7-134 1,1,2-Trlchloroethane 0.0250 U 0.0277 0.0264 ill 105 1 74.1-130 Trichloroethene 0.0250 U 0.0243 0.0236 97.1 94.4 1 48.9-148 Trlchlorolluoromethane 0.0250 U 0,0196 0.0190 78.3 76.1 1 39.9-165 Vinyl chloride 0.0250 U 0.0185 0.0178 74.1 71.4 1 44.3-143 (S)Toluene-d8 99.4 99.8 90.0-115 (5) Dibromofluoromethone 99.0 99.4 79.0-121 (5) ox.&Trifluoratoluene 102 102 - 90.4-116 (5)4-Bromolluorobenzene 97.0 96.1 60.1-120 virc I..i,ii wc. AK MSD Qualifier RPD RPD Limits 5.50 20 4.33 20 5.53 20 5.91 20 4.38 20 4.19 20 3.89 20 5.13 20 2.84 20 2.83 20 3.69 20 rCp 2 TC aSs 4Cn aSr C. /GI- 6AI aSc .. ACCOUNT: PROJECT: SDG: DATEMME: PAGE:, ' ` WG874261 Volatile Organic Compounds (GC/MS) by Method 624 Method Blank (MB) QUALITY CONTROL SUMMARY 1.836370-01,02 (MB) R3138924-3 05/20/16 20:08 MB Result MB Qualifier M8 MDL MB RDL Analyte mg/I mgll mg/1 Acrolein J 0.00887 0.0500 (S) Toluene-d8 103 90.0-115 (S) Dibromolluoromethone 94.7 79.0-121 (S)a,a,a-Tritluorotoluene 100 90.4-116 (S)4-Bromotluorobenzene 102 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138924-1 05/20/16 18:22 • (LCSD) R3138924-2 05/20/1618:41 _ Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Oualifer RPD RPD Limits Analyte mgll mg/I mg/I % % % % % Acrolein 0,125 0.105 0.113 83.9 90.1 88.0-118 J4 7.21 28.1 (5) Totuene-d8 101 101 90.0415 ' (S) Dibromolluoromethane 95.7 93.0 79.0-121 (S)au. o-TriRuorotoluene 100 95.2 90.4-116 (S)4-BromotNorobenzene 98.2 99.1 80.1-120 ONELAB.NATIONWIDE. tCp 2Tc 3Ss QCn 6Sr 7GI aAl 9SC i ACCOUNT: PROJECT: - SDG: DATE/TIME: PAGE: �^� •�-, �.vry i\vL JVIVI IVIIYI\ - vo Lr,o.Ivnli Vw v r wc:' :�� Pesticides (GC) by Method EPA 608 L836370.01,02 - Method Blank (MB) Irvior rtoi�7t�u-I UW/ Uhb Analyte _ lb:bb MB Result mg/I MB Quaffler MB MDL mg/I _ MB RDL mg/I Afdrin U 0.00000813 0700500--- Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0.0000184 0.0000500 Delta BHC U 0.0000197 0.0000500 Gamma BHC U 0.0000176 0.0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0.0000177 0.00OD500 Dieldrin U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0.0000500 Endosulfan II U 0.0000176 0.000D500 Endosulfan sulfate U 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500 Endrin ketone U 0,0000170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene U 0,0000134 0.0000500 Methoxychlor U 0.0000193 0.0000500 Chlordane U O.00D0977 0.000500 Toxaphene U 0.000168 0.000500 (5) Decochloroblphenyl 99.6 10.0-156 (S)Tetrochloro-m-xylene 82.2 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R313929O-2 05/20/1616:08 • (LCSD) R313929O-3 05/20/16 16:21 Spike Amount LCS Result LCSD Result LCS Rec, LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mgh mg/I % % % % % - Aldrin 0.00100 0.000941 0.000 441 94.1 94.1 10.0-120 0.0700 33.9 Alpha. BHC o.00100 0.000944 0.000940 94.4 94.0 53.6-125 0.480 22.3 Beta BHC 0.00100 0.000914 0.000934 91.4 93.4 55.8-130 2.23 20.6 Delta BHC 0,00100 0.00100 0.06101 160 101 42.2-135 01810 23.3 Gamma BHC 0.00100 0.000937 0.000938 93.7 93.8 54.7-125 0.0900 21.1 4,4-DDD 0.00100 0.06107 0.00107 107 107 47.6-144 D.0900 24.3 4,4-DDE 0.00100 0.00101 0.00101 101 101 45.0-124 0.260 25.7 ACCOUNT: PROJECT: SDG: - DATE/TIME: PAGE: WG873940 QUALITY CONTROL SUMMARY Pesticides (GC) by Method EPA 608 LB36370.01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. 4V (LCS) R3139290-2 05/20/16 16:08 • (LCSD) R3139290-3 Spike Amount LCS Result Analyte mg/I mg/1 05/20/16 16:21 LCSD Result mg/I LCS Rec.. % LCSD Rec. % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits 4,4-DDT 0.00100 0.00104 0.00103 104 103 - 49.8-130 0.440 , 25.4 Dieldrin 0.00100 0.00105 0.00105 105 105 55.0-127 0.4B0 22.9 Endosulfan 1 0.00100 0,00106 0.06105 106 105 54.7-127 0.820 24.3 Endosulfan II 0.00100 0.00107 0.00107 107 107 53.1-135 - 0.340 23.5 Endosulfan sulfate 0.00100 0.00109 0.00169 109 109 51.5-132 0.460 26.3 Endrin 0.00100 0.00104 0.00104 104 104 50.1-131 0.200 29.1 Endrin aldehyde - 0.00100 0.06104 0.00105 104 105 39.5-137 0.890 28.4 Endrin ketone 0,00100 0.00107 0.00108 107 108 53.5-139 - 0.420 28.4 Heptachlor 0.00100 0.000985 0.000987 98.5 -98.7 20.7-127 0.19D-- 30.5 - - -- Heptachlorepox1de 0.00100 0.00101 0.00101 101 101 56.4-124 0.180 23.1 Hexachlorobenzene 0.00100 0.000860 0.000851 86.0 85.1 26.7-114 1.04 27.6 Methoxychlor 0.00100 0,00109 0.00109 109 109 48.2-144 0.190 27.8 (5) 0ecochlorobiphenyl 97.3 99.2 10.0-156 (5) refrachloro-m-xylene 81.9 79.8 13.9-137 ACCOUNT' PROJECT: SDG: DATE/TIME: PAGE: VV VDo/ oz `tu Polychlorinated Blphenyls (GC) by Method EPA-608 Method Blank (MB) UU/ALI I Y I.,VIV I KVL DUIVIIVIHKY- LB36370.01,02 UIVt WV.NAIIUNVVHUt. 44K (Mb) H3139329-1 05/23/16 Analyze 13:44 MB Result mg/I MB Qualifier MB MDL mg/I MB RDL mgll PCB 1260 U 0.000120 0,000500 PCB 1016 U 0.000100 0.000500 PCB 1221 U 0.0000730 OD00500 PCB 1232 U 0.0000420 0.000500 PCB 1242 U 0.0000470 0.060500 PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 •- (S) Decochlorobiphenyl 79.2 10.0-156 (S) Tefrochloro-m-xylene 76.2 73.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3139329-2 05/23/16 13:57 • (LCSD) R3139329-3 05/23/1614:09 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % PCB 1260 0.00250 0.00241 0.00251 96.2 100 47.7-149 4.10 28.8 PCB 1016 0.00250 0.00228 0.00234 91.1 93.6 24.7-128 2.70 34.9 (S) Decochlorobiphenyl 79.4 82.2 10.0-156 (S)Tetmchloro-m-xylene 79.8 77.7 13.9-137 ACCOUNT: PROJECT: SDG: '• DATE7TIME: ! PAGE: WG873716 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 625 1836370-01,02 ONE. LAB. NATIONWIDE: Method Blank (MB) (MB) R3138611-1 05/20/16 04:17 Analyte MB Result mg/I MS Qualifer MB MDL mg/I v MB RDL mg/1 Acenaphthene U 0.000316 0.00100 Acenaphthylene U 0.000309 0,00100 Anthracene U 0.000291 0,00100 Azobenzene U 0,000318 0.0100 Benzidine U 0.00432 0.0100 Benzo(a)anthracene U 0.0000975 0.00100 Benzo(b)fluoranthene U 0.0000896 0.00100 Benzo(k)fluoranthene U 0.000355 0.00100 3enzo(g,h,1)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0.00100 Bis(2-chlorethoxy)methane U 0.000329 0,0100 Bis(2-chloroethyl)ethat U 0.00162 0.0100 Bis(2-chIoroisopropyl)ether U 0.000445 0.0100 4-Brom oph enyl-phenylether U 0.000335 0.0100 2-Chloronaphthalene U OA00330 0.00100 4-Chloro phenyl -ph enylether U 0.000303 0.0100 Chrysene U 0.000332 0.00100 Dibenz(a,h)anthracene U 0.000279 0.00100 3,3-Dichlorobenzidine U 0.00202 0.0100 2,4-Dinitrotoluene U 0.00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 Fluorene U 0.0OD323 0.00100 Hexachldrobenzene U 6.060341 0.00160 Hexachloro-1,3-butadiene U 0.000329 0,0100 - Hexachlorocyclopentadlene U 0.00233 0.0100 Hexachloroethane U 0.000365 0.0100 In deno(1,2,3-cd)pyrene U 0.000279 0.00100 Isophorone U 0.000272 0.0100 - Naphthalene U 0.000372 0.00100 - Nitrobenzene U 0.000367 0.0100 n-Nitrosodimelhylamine U 0.00126 0.0100 n-Nitrosodiphenylamine U 0.000304 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0,000366 0.00100 Benzylbutyl phthalate U 0,000275 0.00300 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: - - V...vly 11\VL JVIVI IVIHf\ I - Vlvc'Wo..IVMIIVIVVVIUC. �I Semi Volatile Organic Compounds (GC/MS) by Method 623 v L836370-01,02 .. Method Blank (MB) I01 KOIJao11-1 VJ/GU/lb U4:l/ MB Result Bis(2-ethylhexyl)phthalate .0.00143 Di-n-butyl phthalate 0.000778 Diethyl phthalate U Dimethyl phthalate U Di-n-octyl phthalate 0.00123 Pyrene U 1,2,4-Trichlorobenzene U 4-Chloro-3-methylphenol U 2-Chlorophenol U 2,4-Dichlorophenol U 2,4-Dimethylphenol U 4,6-Dinitro-2-methylphenol U 2,4-Dinitrophenol U 2-Nitrophenol U' 4-Nitrophenol U Pentachlorophenol U Phenol U 2AFY-Trlchlorophenol U (S) Nitrobenzene-d5 679 (S) 2-Fluorobipheayl 75.6 (S)p-Terphenyl-d14 86.3 (S)Phenol-d5 3Z2 (5) 2-Fluorophenol 5t 9 (S) 2,4,6-Tribromophenol 72.3 MB Qualifier MB MDL mg/I MB RDL mg/I J 0.000709 0.00300 J 0.000266 0.00300 0.000282 0,00300 0.000283 0.00300 J 0.000278 0.00300 0.000330.- 0.00100 0.000355' . 0.0100 0.006263 0.0100 0.000283 0.0100 0.000284 0.0100 0.000624 0,0100 0.00262 0.0100 6.00325 0.0100 0.000320 0.0100 i' 0,00201 0.0100 0.000313 0.0100 0.000334 0.0100 0.000297 0.0100 21.8-123 29.5-131 29.3-137 5.00-70.1 10.0-7Z9 IL2-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138611-2 05/20/16 03:31 • (LCSD) R3138611-3 05/20/16 03:54 0 Spike Amount . LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mgll mg/I % % % % % Acenaphthene O.D500 0.0390 0.0393 78.0 78.5 38.7-109 0.600 21.5 Acenaphthylene 0.0500 0.0407 0.0411 81.4 82.3 36.0-106 1.01 21 Anthracene 0.0500 0.0416 0,0423 83.2 84.5 43.6-113 1.56 18.8 Azobenzene 0.0500 0,0406 0.0419 81.1 83.8 37.6-111 3.31 21.1 Benzidine 0.0500 0.0209 0,0246 41.9 49.1 10.0-165 15.9 40 Benzo(a)anthrecene 0,0500 0.0401 0.0405 60.1 81.0 51.2-112 1.13 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG873716 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 625 L836370-01,02 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138611-2 05/20/16 03:31 • (LCSD) R3138611-3 05/20/16 03:54 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I mg/I LCS Rec. % LCSD Rec % Rec. Limits % LCS Qualifier LCSD Qualifier RPD % RPD Limits % v_ Benzo(b)fluoranlhene _ 0,0500 0.0414 0.0407 82.7 81.5 47.6-111 _ 1.54 20 Benzo(k)fiuoranthene 0,0500 0.0412 0.0422 82.5 84.5 49.4-114 - 2.39 20 Benzo(g.h,lIperylene 0.0500 0.0419 0.0420 83.7 84.1 45.2-117 0.430 - 20 Benzo(a)pyrene , 0.0500 0.0412 0.0415 82.3 83.1 45.6-106 - 0.920 20 Bis(2-chlorethoxy)methane 0.0500 0,0390 0.0382 78.0 76.3 37.2-111 2.17 24.1 Bls(2-chloroethyl)ether 0.0500 0.0349 0.0349 69.9 69.8 22.6-108 .. _ - 0.110 27.9 815(2-chlomisopropyl)ether 0,0500 0.0377 0.0375 75.3 75.0 32.9-100 0.380 25.1 4-Brom6phenyl-phenylether 0.0500 0.0395 0.0408 79.0 81.6 40.7-116 3.31 21 2-Chloronaphthalene 0.0500 0.0365 0.0373 72.9 74.7 33.6-105 2.42 23 4-Chlorophenyl-phenylether 0.0500 0.0390 0.0404 78.0 80.9 39.D-113 3.58 20.9 Chrysene 0,0500 0.0405 0.0408 81.0 81.6 54.6-120 0,800 20 Dibenz(a.h)anthracene 0.0500 0.0418 0.0424 83.6 84.7 42.8-118 1.32 20 33-Dichlorobenzidine 0,0500 0.0529 0.0557 106 ill 27.2-142 5.19 22.3 2,4-Dinitrotoluene 0.0500 0.0414 0.0431 82.7 86.1 31.2-105 4.07 22 2,6-Dinitrotoluene 0.0500 0.0371 0,0384 74.2 76.8 30.6-106 3.36 23.1 Fluoranthene 0.0500 0.0412 0.0429 82.4 85.7 45.9-115 3.97 20 Fluorene 0.0500 0.0391 0.0400 78.2 79.9 41.0-112 2.17 20.2 Hexachlorobenzene 0.0500 0.0391 0.0394 78.2 78.8 38.5-116 0.740 20.1 Hexachloro-1,3-butadiene 0.0500 0.0330 0.0320 65.9 64.0 16.1-104 3.02 31.2 Hexachlorocyclopentadiene 0.0500 0.0335 0.0317 66.9 63.5 10.0-121 5.30 27.9 Hexachloroethane 0.0500 0.0296 0,0297 59.3 59.4 16.5-89.8 0,220 30.7 Indeno(1,2,3-cd)pyrene 0.0500 0.0424 6.0427 84.8 85.5 '45.0-116 0.820 20 Isophorone 0.0500 0.0399 0.0405 79.9 80.9 35.4-112 1.27 21.5 Naphthalene 0.0500 0.0351 0.0349 - 70.3 69.7 32.2-101 0,730 23.8 . n-Nitrosodimethylamine 0.0500 0.0223 0.0214 44.6 42.7 10.0-80.1 4.42 37.5 Nitrobenzene 0.0500 0,0360 0.0350 72.0 70.0 31.4-106 2.74 25.7 n-Nitrosodiphenylamine 0,0500 0,0414 0.0423 827 84.5 44A-113 2.18 20 n-Nitrosodi-n-propylamine 0.0500 0.0359 0.0365 71.8 73.0 33.2-106 1.73 23.7 Phenanlhrene 0.0500 0.0383 0.0394 76.6 78.9 46.4-113 2.89 20 Benzylbutyl phthalate 0.0500 0.0405 0,0409 81.0 81.8 37.6-123 0.990 20T" - Bis(2-enylhexypphthalale 0.0500 0,0408 0.0405 81.5 81.2 36.9-134 0.420 23.6 Di-n-butyl phthalate 0.0500 0.0395 0.0403 78.9 80.5 41.8-120 L99 20.2 Diethyl phthalate 0.0500 0.0414 0.0426 82.7 85.3 36.5-129 3.03 20 Dlir l phthalate 0.0500 0.0403 0.0414 80.5 82.8 35.3-128 - 2.83 20.8 Di-n-octyl phthalate 0.0500 0.0397 0.0400 79.5 80.0 39.7-112 0.690 21.1 Pyrene 0.0500 0.0423 0.0425 84.6 84.9 46.3-117 0.320 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE W68/3/16 UUALI I Y UUIN I KUL 5UIVIIVIAKY.' )NbLNtl.NAIIUINYVIvt: 41K,. Semi Volatile Organic Compounds (GC/MS) by Method 625 1.836370-01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3138611-2 05/20/16 03:31 • (LCSD) R3138611-3 05/20/16 03:54 C 2 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Ouali0er LCSD OualiRer RPD RPD Limits Armyte mg/1 mg/1 mg/I % % % % % TIC 1,2,4-Trichlorobenzene O.D500 0.0325 0.0325 64.9 65.0 22.9-96.1 0.0900 27.5 = 4-Chloro-3-methylphenol 0.0500 0,0398 0.0400 79.7 _ 80.0 35.7-100 0.380 22.9 355 2-Chlorophenol 0.0500 0.0344 0,0326 68.9 65.2 26.7-91.5 5.48 26.5 2,4-Dichlorophenol 0.0500 0.0398 0.0385 79.7 77.0 31.4-103 3.38 24.9 y 2,4.Dimethylphenol 0.0500 0.0385 OA380 77.0 75.9 31.9-107 1.31 25.7 Cn 4,6-D1nitro-2-methylphenol 0.0500 0.0374 0.0370 74.8 74.0 18.4-148 0.990 24.4 2,4-Din1trophenol 0.0500 0.0282 0.0260 56.4 52.0 24.2-128 8.15 20.5 65f 2-Nitrophenol 0.0500 0.0397 0.0389 79.4 77.8 25.9-106 2.04 26.9 4-Nitrophenol 0.0500 0.0206 0,0190 41.2 38.0 10.0-52.7 7.90 40 Pentachlorophenol 0.0500 0.0385 0.0393 76.9 78.7 10.9-97.4 2.28 35.1 Phenol 0,0500 0.0201 0.0190 40.3 37.9 10.0-57.9 5.92 35 2,4,6-Trichlorophenol 0.0500 0.0408 0.0411 81.7 82.3 29.8-107 0.700 24.1 7GI (S)Nitrobenzene-d5 72.7 68.2 21.8-123 (S)2-Fluorobiphenyl 73.4 73.5 29.5-131 - eAI (S)p-Terphenyl414 84.6 828 29.3-137 (S) Phenol-d5 37.4 34.0 5.00-70.1 (S)2-Fluorophenol 51.0 45.7 10.0-779 9p CC (S)2,4,6-Tribromophenol 84.8 81.4 11.2-130 ACCOUNT: PROJECT: . SDG: DATE/TIME: PAGE: GLOSSARY OF TERMS ONE LAB. NATIONWIDE. V Abbreviations and Definitions � SDG Sample Delivery Group. C MDL Method Detection Limit. RDL Reported Detection Limit. EC Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. s (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry Ss report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) 4Cn from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control s Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring Sr recovery. Surrogates are not expected to be detected in all environmental media. Rec. Recovery. e SDL Sample Detection Limit. I QC MQL Method Quantitation Limit. LLL___ Unadj. MQL Unadjusted Method Ouantitation Limit. Qualifier Description BAI B J The same analyte is found in the associated blank. The identification of the analyte is acceptable; the reported value is an estimate. ECJ3 The associated batch OC was outside the established quality control range for precision. J4 The associated batch OC was outside the established quality control range for accuracy. Pi RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATEMME: PAGE: ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences Is the only environmental laboratory accredited/certlfied to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other ' lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the Cp network laboratories in our industry. The most significant bereft to Our 'one location" design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. ' Not all certifications held by the laboratory are applicable to, the results reported in the attached report. T State Accreditations c Alabama_ 40660 Nevada _ _ _ T_N-03-2002-34 3 SS F - _ _ _ Alaska UST-080 New Hampshire _ _ 2975 _ _ _ _ _ Arizona Arkansas AZO612 88-0469 New Jersey-NELAP New Mexico TNO02 TN00003 ° Cn -- - - California _ 01157CA New York _ 11742 � _ Colorado TN00003 North Carolina E.nv375 Conneticut PH-0197 North Carolina DW21704 r Florida_ E87487 North Carolina 2_ 41 Georgia NELAP North Dakota- -- -- - ._ R-140. __. Georgia 923 Ohio-VAP CL0069 - QC Idaho TN00003 Oklahoma 9915 . _ _ Illinois 200008 Oregon TN200002 [GI _ _ Indiana C-TN-01 Pennsylvania 68-02979 _ Iowa 364 Rhode Island 221 ._ Kansas E-10277 South Carolina 840C4 Kentucky' 90010 South Dakota _ n/a Kentucky.' 16 Tennessee " _ 2006 _ Louisiana_ AI30792 Texas T104704245-07-T% y Marne TN0002 Texans LA60152 SC _ Maryland 324' Utah 6157585858 Massachusetts M-TNO03 Vermont _ VT2006 Michigan 9958 Virginia.,, ., ,_.._.. 109 .'i Minnesota 047-999-395 Washington C1915 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA Nebraska _ NE-OS-15-05 Third Parry & Federal Accreditations A2LA-IS017025 1461.01 — AIHA 106789 A21_A - IS017025s 1461.02 DOD 1461.01 Canada 1461.61 USDA S-67674 EPA-Crypto _ TN00003 'Drinking Water ° Underground Storage Tanks ' Aquatic Toxicity ' Chemicalmlicrobiological Mold '-Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. a WA ` OR MT NO MN WE T ID SD T V.II r T' NY Y T wv Y aaI T T NE If T T PA T a T NV • T CT, T ` R Vv T CA T C T KS M� T� VAT T KY ! T ad? .N T ?AZ NM pk T T sc T o MS 4L GA T T rX T LA T • T �• :T\ AK a t FL O m B Hu p PROJECT: SDG: DATEMME: PAGE: ACCOUNT: Company Name/Address. airline Information: .I Analysii l Container/PreservaifGe lChainGfOxii Page Eaton Corporation NA Financial �of— 2564 Durham Rd PO Box 8580 Roxboro, NC 27573 Cleveland, ON44181 8024 J y' Li O �' Ifi65lrbanke a! O`-- Report to: Email To: Dustin LeClair ustiniaeialr@Eaton.eom o = •D• o - xWnl lul k�IN 3JI IN T} 37i _ U' U Z: "N Z "? e�.atyy none: eoo-m.sa51 >. • Project Eaton Corp.,Semi•Annual Stormwater Descdption: Ci /State - ty Roxboro• NC Collected: r' ... a' `,. W .O; _.m IHV�g:�Vl3Tf/... '� . Phorne:336-599-1141 Client Project Lab Project Faac 28091-R EATONRNC 28091SW a, m • u 1073 Z_ On .E is eO' -tp R .s, i*�_--, Collected by 1pdnik Site/Fadfill"I :: P.O: gt. Z` .i T IICP.� w'. Ac numb k`rof4 C ' _'J . _ _. .., m.l O c��3 v�i •N M E o; E o E o Collected): Rush? (Lab MUST Be Notified) Date Results Needed .�J • J�"'! _same my .......................... xao>< X t- �lxl; K nse j Prelogint Email? No Yes — — Immediately _Rvs a, .._..•............lows _Two Day ..... _ .__._SIML • - M y;='� `allo. N N'' O' N .- 4N F••.. �j TSR .HURL.. ,^. "r_' 2 Packed on Ice N _ Y �thrte Day.._.__.......-....-.25R FAX? i(No —Yes T Intri DO X as 4. 7 �' N, N '00 �.' - F �""9 Samplel6 Comp/Grab Matrix• Depth Date TimeD1 ShippotlVo Ralel hiSery i6- ��" ?,o s— J7— oo.i v ww S i7 6 X F XI U X O 7c m X r0_ aX 7a 1 ) 4mXnn amaum smp,a 5eenld �d6_-5�17-oos - Cmxki ►"rn s;l:�.:_ 12:IQpr OR •.ate 6n .- u Sr � ' •• - p'. Sin-+ i rs 1 'Matrix; Ss - Sall GW-Groundwater WW- Wastewater DW- Drinking Water OT: Other pH Temp Remarks: _.-.7% '.t -..- ,.` Flow .:.Ocher xgten, * I Relinquished by I gnature Date: Time: Received bj-(Slgnature) Sarnplet: relurned via: Q UP d CondlNon;• - (lab use only)12, -+ r 5 b 0/p�y ..w,, r S/!(Ir tb f;x7 �t _a: FiFedEe ❑.Warier Q -' y RellnqulsAetl byi (atureJ ` Date: Time: Received try:JSi@namrnJ:' - �, Tem •� =Doefles RKelved; i aK- p: T T CCC S6WInta3 r''ye N:r. Relinquished by i(5(gnatuyej Date: Time: RKerved fd . b V. 151 azure r - '• - _ - — ••,F I, Datc., SGne�s• pHCheticr. a rrcr:i =o 300 0Q,7 20vx� ANALYTICAL REPORT March 04, 2016 myESC Eaton Corporation Sample Delivery Group: L819665 _ Samples Received: 02/24/2016 Project Number: 28091-R Description: Eaton Corp Semi -Annual Stormwater Site: - ROXBORO, NC Report To: Dustin LaClair 2564 Durham Road Roxboro, NC 27573 4 Entire Report Reviewed By: / LJ— Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures. 060302, 060303, and 060304. N, TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cp Cover Page 1 2Tc: Table of Contents 2 "'+ 'Ss: Sample Summary 3 'Cn: Case Narrative 4 3Ss 'Sr: Sample Results 5 4Cn 2016-2-22-005 L819665-01 5 60c: Quality Control Summary 8 Sr Gravimetric Analysis by Method 2540 D-2011 8 Wet Chemistry by Method 1664A 9 e QC Metals (ICP) by Method 200.7 10 Volatile Organic Compounds (GC/MS) by Method 624 it,. [GI Pesticides (GC) by Method EPA 608 15 eAl Polychlorinated Biphenyls (GC) by Method EPA-608 16 • Semi Volatile Organic Compounds (GC/MS) by Method 625 _ 18 9 Sc 'GI: Glossary of Terms _ - - 22 8AL Accreditations & Locations 23 9Sc: Chain of Custody 24 ACCOUNT: PROJECT: SDG: DATE/TIME: -PAGE: Eaton Corporation 28091-R L819665 03/04/1611V28 2 of 24 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected datehime Received dateltime Kirk Spicer 0222tI616:43 02t24A609:00 + 2016-2-22-005 L819665-01 WW � Cp Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 D-2011 WG851881 1 02/25/1605:23 02/25/1606:06 JM Metals (ICP) by Method 200.7 WG851929 1 02/25/1610:43 02/2511619:01 ST Pesticides (GC) by Method EPA 608 WG851913 1 02/25116 23:50 03/OV1619:09 ADF Polychlorinated Biphenyls (GC) by Method EPA-608 WG851913 1 02/25116 23:50 02/2611615:17 LKO Semi Volatile Organic Compounds(GUMS) by Method 625 WG852131 1 0212811619:13 02129r162149 JF Volatile Organic Compounds(GC/MS) by Method 624 WG852162 1 02/2511622:34 02/25I1622*34 ACG Wet Chemistry by Method 1664A WG852994 1 03/01/1614:53 03/01/1616:33 JM 2' ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L819665 DATE/TIME: PAGE: 03/04/16 11:28 3 of 24 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the C p appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the ' zTc analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the 3SB laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. s$r U r' 'G Jimmy Hunt BAI Technical Service Representative 9Sc ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:26 4 of 24 2016-2-22-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 02/22/16 16:43 L819665 Additional Information C Result Units 2 Analyte pH (On site) 7.7 so Tc Temperature (on -site) 12.3 Deg.0 2540 D-2011 3Ss Gravimet Tic Analysis by Method Result Oualifer MDL RDL Dilution Analysis Batch ° Cn Analyte mg/I mg/I mgA date/time Suspended Solids 18.2 :. 0.350 2.50 1 02/25/201606:06 WG851881 Wet Chemistry by Method 1664A 6 Result Oualifier MDL RDL Dilution Analysis Batch QC Analyte mg/I mgll 'mg/I date/time TPH -Oil&Grease 1.38 J 0.725 5.75 1 03101/201616:33 WG852994 rGI Metals (ICP) by Method 200.7 aAl Result Ouallfer MDL RDL Dilution Analysis Batch 9 Analyze mgA mg/I mgA date/time Copper 0.0416 0,00700 DOM 1 02/25/201619.01 WG851928 SC Lead 0,00613 O00200 0.00500 1 02125/201619:01 WGSS1928 Zinc 0.0482 J 0.0034D 0A500 1 02/25/201619:01 WG851928 Volatile Organic Compounds (GC/MS) by Method 624 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ri mgA mgA date l time Acrolein U J4 0.00887 0.0500 1 02/25/201622:34 WG852162 Acrylonitrile U 0.00187 0.0100 1 02/25/201622:34 WG852162 Benzene U 0.000331 0.00100 1 02/25/2016 22:34 WG852162 Bromodichloromethane U 0.000380 0.00100 1 02/25/201622:34 WG852162 Bromoform U 0.000469 0.00100 1 02/25/201622:34 WG852162 IBromomethane U 0.000866 0.00500 1 02/25/201622:34 WG852162 Carbon tetrachloride U 0.000379 0.00100 1 02/25/2016 22:34 WG852162 . "Chlorobenzene U 0,000348 0.00100 1 02/25/201622:34 WG852162 Chlorodibromomethane U 0.000327 0.00100 1 02/25/201622:34 WG852162 Chioroethane U 0.000453'0.00500 1 02/25/201622:34 WG852162 _ 2-Chlomethyl vinyl ether U 0,00301 0.0500 1 02/2512016 22:34 WG852162 Chloroform U 0.000324 0.00500 1 021251201622:34 WG852162 Chloromethane U 0,000276 0.00250 1 021251201622:34 WG852162 ,-Dihlarbenzene WG85216212 1,3-Dlchlorobenzene U 0,000220 0,00100 1 02/251201622:34 WG852162 �74-Dichlorobenzene U 0.000274 0.00100 1 021251201622:34 WG852162 Dichlorodifluoromethane U 0,000551 0,00500 1 02/25/201622:34 WG852162 1,1-Dichloroethane U 0.000259 0.00700 1 02125/201622:34 WG852162 _ 1,2-Dichloroethane U 0.000361 0.00100 1 02/25/201622:34 WG852162 d,t-Dichloroethene U 0.000398 0.00100 1 02/25/201622:34 WG852162" trans-1,2-Dichloroethene U 0.000396 000M 1 02125/201622:34 WG852162 1,2-6ichloropropane U 0.000306 0.0010D 1 02/25/201622:34 WG852162 cis-1.3-Dichloropropene U 0.000418 0.00100 1 02/25/201622:34 WG852162 tans-1,3-Dichloropropene U 0.000419 0.0010D 1 02/25/201622:34 WG852162 Ethylbenzene U 0.000384 0.00100 1 02/251201622:34 WG852162 !Methylene Chloride U 0.00100 0.00500 1 02/25/201622:34 WG852162 1,1,2,2-Tetrachloroezhane U 0.000130 0,00100 1 02/25/201622:34 WG852162 Tetrachloroethene U 0.000372 Oloolo0 1 02125/201622:34 WG852162 Toluene U 0.000780 0.00500 1 02/25/201622:34 WG852162 �1,1,1-Trichloroethane U - 0.000319 0.00100 1 02/25/20162234 W6852162 1,1,2-Trichloroethane U 0.000383 0.00100 1 02/25/2016 22:34 WG852162 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03104/1611:28 5 of 24 2016-2-22-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dateltime: 02122/1616:43 L819665 Volatile Organic Compounds (GC/MS) by Method 624 Result Oualifier MDL RDL Dilution Analysis Batch _ Cp Analyte mg/1 mg/I mg/I date/time Trichloroethene U 0.000398 0.00100 1 02125/201622:34 WG852162 Tc Trichlorofluoromethane U 0.00120 0.00500 7 02/25I201622:34 WG852162 Vinyl chloride U 0.000259 0.00100 1 02/25/2016 22:34 WG852162 a (S)Toluene-d8 104 90.04/5 02125201622.34 WG852162 SS (S) Dibromofluoromethone 105 79.0-121 0225201622.34 WG852162 (S)o,o,a-Trifluorotoluene 102 90.4-116 0225201622.34 WG852162 Cn (S)4-Bromolluorobenzene 702 80.1-120 0225201622:34 W6652162 Pesticides (GC) by Method EPA 608 Result Oualifer MDL RDL Dilution Analysis Batch 6 Analyte allmg/I mg/I date/time QC Aldrin U 0.00000813 0.0000500 1 03101/201619:09 WG851913 Alpha BHC U 0.0000166 0.0000506 1 03/01/201619.09 WG851913 �GI Beta BHC U 0.0000184 0.0000500 1 03/01/201619:09 _ WG851913 Delta BHC U 0.0000197 OD000500 1 03/01/201619:09 WG851913 a Gamma BHC U 0,0000176 0.0000500 1 03/01/201619:09 WG851913 AI Chlordane U 0.0000977 0.000500 1 03/01/201619:09 WG851913 4,4-DDD U 0.0000170 a0000500 1 03/01/201619:09 WG851913 9 ScS ,4-DDE U 0.0000164 0.0000500 1 03/07/201619:09 W6851913 4,4-DDT U 0.0000177 0,0000500 1 03/01/201619:09 WG851913 Dieldrin U 0,00000751 0.0000500 1 03/0l/201619:09 WG851913 Endosulfan 1 U 0.0000179 0.0000500 1 03/01/201619:09 WG851913 Endosulfan II a 0.0000176 0,0000500 1 03/011201619:09 WG851913 Endosulfan sulfate U 0.0000196 00000500 1 03/01201619.09 WG851913 'Endrin U 0.0000189 0.0000500 1 03/01/201616.09 WG851913 Endrin aldehyde U 0.0000142 0.0000500 1 03/01/201619:09 WG851913 Endrin ketone U 0.0000170 0.0000500 1 03/01/201619:09 WG851913 Heptachlor U 0.0000108 0.0000500 1 03/01/201619:09 WG851913 Heptachlor epoxide U 0.0000175 0.0000500 1 03/01/201619:09 WG851913 Hexachlorobenzene U 0.0000134 0,0000500 1 03/01/201619:09 WG851913 Methoxychlor U 0.0000193 0.0000500 1 03/01/201619:09 WG851913 Toxaphene U 0.000168 0000500 1 03/01/201619:09 WG851913 ICI Polychlorinated Biphenyls (GC) by Method EPA-608 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mgn mg/l date/time , PCB 1016 U 0.000100 0.000500 1 02/26/201615:17 WG851913 PCB 1221 U 0.0000730 0.000500 1 02/26/201615:17 WG851913 PCB 1232 U 0,0000420 0.000500 1 62/26/201615:17 WG851913 PCB 1242 U 0.0000470 0.000500 1 02126/201615:17 WG851913 PCB 1248 U 0.0000860 0.000500 1 02/26/201615:17 WG851913 PCB1254 U 0.0000470 0.000500 1 02/261201615:17 W13851913 PCB1260 U 0.000120 0.000500 1 02/26/20161517 WG851913 (S) Decachlorobiphenyl 36.0 10.0-156 02126120161597 WG851913 (S) relrochloro-m-xylene 43.3 13.9-137 02262016 15: 17 WG851913 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Oualifler MDL RDL Analyle Acenaphthene Acenaphthylene Anthracene Benadine Benzo(a)anthracene Benzo(b)fluoranthene U 0,000316 MOM U 0.000309 OD0100 U 0.000291 0.00100 U 0.00432 0.0100 U 0.0000975 0.00100 u 0.0000896 0,00100 ACCOUNT: Eaton Corporation Dilution Analysis date / time 1 02/29/2016 2149 1 02/29/2016 21:49 1 02/29/2016 2149 1 02/29/2016 2149 1 02/29/2016 2149 1 02/29/2016 21'.49 PROJECT: SDG: 28091-R L819665 Batch WG852131 WG852131 WG852131 WG852131 WG852131 - WG852131 DATEMME: 03/04/16 1126 PAGE: 6 of 24 2016-2-22-005 SAMPLE RESULTS - 01 ONE LAB, NATIONWIDE. Collected da Le/time: 02/2211616:43 L819665 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result ''Oualifer MDL RBL Dilution Analysis Balch Cp Analyle mg/I mgA mgll date/lime Benzo(k)fluoranthene U 0.000355 0.00100 1 02/29/20162149 WG852131 2TC Benzo(g,h,Ilperylene U 0.000161 0,00100 1 02/29/2016 21:49 WG852131 Benzo(a)pyrene U 0,000340 0.00100 1 02129/20162149 WG852131 a Bisi2-chlorethoxyimethane U 0,000329 0.0100 1 02/29/20162149 WG852131 SS Bis(2-chloroethy)ether U 0.00162 0.0100 1 02/29/2016 2149 WG852131 Bis(2-chloroisopropyl)ether U 0,000445 0.0100 1 02/29120162149 WG852131 Cn 4-Bromophenyl-phenylether U 0.000335 0.0100 1 02/29/2016 2149 WG852131 ,2-61oronaphthalene U 0,000330 0,00100 1 02/29/2016 21:49 WG852131 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 02/29/20162149 WG852131 Chrysene U 0.000332 0.00100 1 0229/2016 21:49 WG852131 Dibenz(a,h)amhracene U 0.000279 0.00100 1 02/29/2016 2149 WG852131 6 OC 3,373ichlorobenzidine U J3 0.00202 0.0100 1 0229/201621:49 WG852131 2,4-Dinitfotoluene U 0.00165 0.0100 1 0209/201621:49 WG852131 FGI 2,6-Dinitrotoluene U 0.000279 0.0100 1 02/29/20162149 WG952131 1,2-Diphenylhydrazlne U 0.000318 0.0100 1 02/29/2016 2149 WG852131 Fluoramhene U 0.000310 0.00100 1 02/29/20162149 WG852131 aA.l Fluorene U 0.000323 0.00100 1 02/29/2016 2149 WG852131 Hexachlorobenzene U 0.000341 0.00100 1 02/29120162149 WG852131 y Hexachloro-1,3-butadiene U 0.000329 0.0100 1 02/29/2016 2149 WG852131 SC Hexachlorocydopentadie ne U 060233 0.0100 1 02/291201621:49 WG852131 Hexachloroethane U 0,000365 0.0100 1 021291201621:49 WG852131 Indeno(1,2,3-cd)pyrene U _ 0.000279 0.00100 1 02/29/2016 21:49 WG852131 Isophorone U 0.000272 0.0100 1 02/29120162149 WG852131 Naphthalene U 0.000372 MOM 1 02129/20162149 WG852131 Nitrobenzene U 0.000367 0.0100 1 02/29/2016 2149 WG852131 n-Nitrosodimethylamine U 0.00126 0.0100 1 02/29120162149 WG852131 n-Nitrosodiphenylamine U 0,000304 0,0100 1 02/29/20162149 WG852131 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 02129/20162149 WG852131 Phenanthfene U 0,000366 0.00100 1 02/29/20162149 WG852131 Benzylbmyl phthalate _ U 0,000275 0.00300 1 02/29/2016 2149 WG852131 Sisl2-ethylhexylta thalate U 0.000709 0.00300 1 02/29/20162149 WG852131 6-11-6utyl phthalate 0.00116 1_ 0.000266 0.00300 1 02/29/2016 2149 WG952131 Diethyl phthalate U 0.000282 0.00300 1 02/29/2016 21:49 WG852131 Dimethyl phthalate U 0M0283 0.00300 1 02/29/2016 21:49 WG852131 Dl-n-octyl phthalate U 0.000278 0.00300 1 0229/20162149 WG852131 IPyrene U 0.000330 0.00100 1 02/29/2016 2149 WG852131 _ 1,2,4-Trichlofobenzene U 0.000355 0.0100 1 0229120162149 WG852131 4-Chloro-3-methylphenol U 0.000263 0.0100 1 02/29/20162149 WG852131 2-Chloraphenol U 0.000283 0,0100 1 0229120162149 WG852131 2,4-Dichloropher l U _ 0.000284 0.0100 1 02/29120162149 WG852131 2,4-Dimethylphenol U 0.000624 0.0100 1 02/29/2016 21,49 WG852131 4,6-Dinitro-2-methylphenol U 0.00262 _ 0.0100 1 02/291201621:49 WG852131 2,4-Dinitrophenol U J3 0.00325 0,0100 1 02/29120162149 WG852131 12-Nitrophenol U 0.000320 0.0100 1 02/291201621:49 WG852131 4-Nitrophenol U ,,.. 0.00201 0,0100 1 02/29120162149 WG852131 'Pentachlorophenol U 0.000313 0,0100 1 02/29/2016 2149 WG852131 Phenol U 0.000334 0.0100 1 02/29120162149 WG852131 2,4,6-irichlorophenol U 0.000297 0.0100 1 02/29/20162149 WG852131 ' (S)2-Fluorophenol 49.2 - - - - _ - 10.0-729 0212WO162149 ---WG852131-- (S)Phenol-d5 38.5 - _ 5.00-70.1 022WO162749 WG852131 (S) Nitrobenzene-d5 785 21.8-123 02129120162749 WG852131 (S)2-Fluorobiphenyl 75.1 29.5-131 0212920162749 WG852131 IS)2,4,6-Tribromophenol 80.5 11.2-130 0229201627:49 WG852131 (S)p-Terphenyl-d14 84.3 29.3-137 02129201621.49 WG852131 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 7 of 24 WG851881 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. .� Gravimetric Analysis by Method 2540 0-2011 LE19665-01 Method Blank (MB) (MB) 02/25/16 06:06 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Suspended Solids U 0.350 2.50 L819345-04 Original Sample (OS) • Duplicate (DUP) (OS) 02/25/16 06:06 • (DUP) 02/25/16 06:06 Original Result DUP Result Dilution DUP RPD OUR Qualifier OUR RPD Limits Analyte mg/I mg/I % % Suspended Solids 50.3 52.3 1 3.90 5 L819669-02 Original Sample (OS) • Duplicate (DUP) (OS) 02/25/16 06.06 - (DUP) 02/25/16 06:06 Original Result OUR Result Dilution DUP RPD DUP Qualifier OUR RPD Limits Analyte mg/l mg/I % % Suspended Solids 461 443 1 3.98 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/25/16 06:06 • (LCSD) 02/25/16 06:06 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I MV % % % % % Suspended Solids 773 876 864 113 112 85.0-115 1.38 5 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 8 of 24 WG852994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method 1664A _ L819665-01 Method Blank (MB) C (MB) 03/01/16 16:32 p MB Result MB Qualifier MB MDL Analyte in TPH - Oil & Grease U 0.725 MB RDL nlyl 5.00 Laboratory Control Sample (LCS) - Laboratory Control Sample Duplicate (LCSD) (LCS) 03/01/16 16:32 • (LCSD) 03/01/16 16:33 _ Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyle mg/I mg/I mg/I % % % % % TPH -Oil&Grease 20.0 18.7 17.7 93.5 88.5 78.0-114 5.49 18 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/16 11:28 9 of 24 WG851928 QUALITY CONTROL SUMMARY ONELAB.NATIONwIDE. Metals (ICP) by Method 200.7 L819665.01 Method Blank (MB) 1 Cp (MB) 02/25/1618:06 MB Result Analyte mg/I MB Qualifier MB MDL mg/I MB ROL mg/I ITC] Copper U 0.007 0.0100 Lead U 0.002 0,00500 3 $S Zinc U 0.0034 0.0500 QCn Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/25/16 18:09 • (LCSD) 02/25/1618:12 6 $r Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % ' % Copper 1.00 1.04 1.04 104 104 85-115 1 20 Lead Zinc 1.00 1.02 1.00 0.975 1.01 0.961 102 98 101 96 85-115 85-115 1 1 20 20 �GI L819637-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) aAl (OS) 02/25/16 18:15 • (MS) 02/25/1618:21 • (MSD) 02/25/1618:24 y Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits SC Analyte mg/I mg/I mg/I mg/I % % % % % Copper 1.00 0-00201 1.04 1.05 104 105 1 75-125 1 20 Lead 1.00 0.00117 1.02 1.03 102 103 1 75-125 2 20 Zinc 1.00 0.0406 1.00 1.02 96 98 1 75-125 2 20 L819706-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 02/25/1619:35 • (MS) 02/25/16 19:38 • (MSD) 02/25/16 19:40 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mgh rag/I % % % % % Copper 1.00 0,00882 1.05 1.07 104 106 1 75-125 1 20 Lead 1.00 0.00446 LO0 1.02 101 102 1 75-125 1 20 Zinc 1.00 0.0474 1.01 1.01 96 97 1 75-125 0 20 ACCOUNT: PROJECT: SDG: DATE IME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 10 of 24 WG852162 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 - L819665.01 Method Blank (MB) (MB) 02/25/16 21:46 MB Re5ult MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mgh Acrolein U 0.00887 0.0500 Benzene U 0.000331 0.00100 Acrylombile U 0.00187 0.0100 Bromodichloromethane U 0.000380 0.00100 Bromoform U _ 0.000469 0,00100 Bromomethana - U 0.000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 - Chlorobenzene U 6.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0,000453 0.00500 - 2-Chloroethyl vinyl ether U 0.00301 0,0500 Chloroform U 6.000324 0.00500 Chloromethane U 0.000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 1,3-Dichlorobenzene U 0.000220 0.00100 1,4-Dichlorobenzene U o 060274 0.00100 Dichlorodifluoromethane U 0.000551 0,00500 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene U ODOM% 0.00100 1,2-Dichloropropane U 0.000306 0,00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0,000384 0.00100 Methylene Chloride U 0.00100 0.00500 I,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0,00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 0.00500 Vinyl chloride U 0.000259 0.00100 (S) Toluene-d8 102 88.5-111 (S) Dibromolluoromethone 105 78,3-121 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 11 of 24 WG852162 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. volatile Organic Compounds (GC/MS) by Method 624 L819665-01 Method Blank (MB) (MB) 02/25/16 21:46 MB Result MB Qualifier MBMDL MB RDL (S)o,oa-Tofluorotoluene 101 850-114 (S)4-8romolNorobenzene 103 71.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/25/1619:54 - (LCSD) 02/25/16 20:15 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier Analyte mg/I mg/I mgn % % % Acrolein 0.125 0.219" 0.222 175 178 88.0-118 J4 Benzene 0.0250 6.0249 0.0259 99A 103 73.0-122 Acrylonitrile 0.125 0.136 0.138 109 110 7L0-135 Bromodlchloromethane 0.0250 0.0261 0,0264 104 106 75.5-121 Bromoform 0.0250 0.0265 0.0288 106 115 71.5-131 Bromomethane 0.0250 0.0277 0.0285 ill 114 224-187 Carbon tetrachloride 0.0250 0.0261 0.0265 104 106 70.9-129 Chlorobenzene 6.0250 0.0245 0.0256 98.1 102 79.7-122 Chlorodibromomethane 0.0250 0.0271 0,0271 109 108 78.2-124 Chloroethane 0.0250 0.0263 0.0266 105 107 41.2-153 2-Chloroethyl vinyl ether 0.125 0.144 0.153 115 122 23.4-162 Chloroform 0.0250 0.0259 0.6272 104 109 73.2-125 Chloromethane 0.0250 '0.0252 0.0258 101 103 55.8-134 1,2-Dichlorobenzene 0.0250 0.0253 0.0268 101 107 84.7-118 1,3-Dichlorobenzene 0.0250 0,0250 0.0263 100 105 77.6-127 1,4-Dichlorobenzene 0.0250 0,0241 0.0256 96.4 102 82.2-114 Dichlorodifluoromethane--0.0250 0.0256 0.0261 102 104 56.0-134 1,2-Dichloroethane 0.0250 0.0258 0.0266 103 106 65.3-126 1,1-Dichloroethane 0.0250 0.0267 0.0274 107 110 71.7-127 1,1-Dichloroethene 0.0250 OrOM7 0.0272 167 109 59.9-137 trans-1,2-Dichloroethene 0.0250 0,0261 0.0268 105 107 72.6-125 1.2-Dichloropropane 0.6250 0.0251 0.0268 100 107 77.4-125 cis-1,3-Dichloropropene 0,0250 0,0264 0.0272 106 109 77.7-124 trans-1,3-Dichloropropene 0-0250 0.0276 0.0288 110 115 73.5-127 Ethylbenzene 0.0250 0,0246 0.0253 98.2 101 80.9-121 Methylene Chloride 0,0250 0,0256 0.0265 103 106 69.5-120 lj. ,2-Tetrachloroethane 0.0250 0.0246 0.0264 98.6 105 79.3-123 Tetrachloroethene 0.0250 0.0246 0,0248 98.3 99.1 73.5-130 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L819665 LC5D Qualifier RPD RPD Limits J4 1.54 28.1 3.99 20 1.26 20 1.24 20 8.57 20 2.86 20 1.59 20 4'.14 20 0,320 20 1.96 20 5.91 23.5 5.06 20 2.37 20 5.73 20 5.03 20 5.93 20 1,88 20 3.09 20 2.71 20 1.82 20 2.38 20 6.74 20 2.99 20 4.42 20 2.98 20 3.28 20 6.76 20 0.890 20 DATErTIME: 031041161126 PAGE: 12 of 24 WG852162 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. Volatile, Organic Compounds (GC/MS) by Method 624 L819665-01 _ Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/25/16 19:54 - (LCSD) 02/25/16 20J5 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Res. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Toluene 0,0250 0.0243 0.0248 97.1 99.3 77.9-116 2.22 20 1,11-Trichloroethane 0.0250 0.0248 0.0263 994 105 71.1-129 570 20 1,1,2-Trichloroethane 0.0250 0.0241 0.0254 96.5 102 81.6-120 5.21 20 Trichloroethene 0.0250 0.0251 0.0259 101 103 79.5-121 2.93 20 Trichlorofluoromethane 6.0250 0.0265 0.0271 106 108 49.1-157 2,31 20 Vinyl chloride 0.0250 0.0265 ., 0.0266 106 106 61.5-134 0.320 20 (S)Toluene-d8 100 702 88.5-111 /S/ Dibmmohuoromefhone - 103 105 78.3421 (S)zo,o-TrilNorotoluene 99.0 100 85.0-114 Q4-8romoBuorobenzene 99.3 99.1 71.0-126 L819193-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 02/26/16 02.54 - (MS) 02/26/16 05:15 - (MSD) 02/26/16 05:35 1 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Per. Limits MS Qualifier MSD Quallfer RPD RPD Limits Analyte mg/I mgh mg/1 mg/1 % % % % % Benzene 0.0250 ND 0.0262 0.0268 105 107 1 58.6-133 2.02 20 Acrolein 0.125 ND 0.195 0.212 156 170 1 10.0-200 8.66 27.7 Acrylonitrile 0.125 ND 0.153 0.150 123 120 1 49A-133 2.42 25.3 Bromodichloromethane 6.0250 ND 0.0264 0.0271 106 109 1 69.2-127 2.60 20 Bromoform 0.0250 ND 0.0271 0.0281 108 113 1 66.3-140 3.84 20 Bromomethane 0,0250 ND 0.0235 0.0243 94.0 97.3 1 16.6-183 i,12 20.5 Carbon tetrachloride 0.0250 ND 0.0242 0,0255 96.8 102 1 60.6-139 5.11 20 Chlorobenzene 0.0250 0,0612 0,0706 0.0717 37.6 42.2 1 70.1-130 J6 J6 1.60 20 Chlorodibromomethane 0.0250 ND 0.0278 0,0287 ill 115 1 71.6-132 3.24 20 Chloroethane 0.0250 ND 0.0264 0.0275 106 110 1 33.3-155 3.99 20 2-Chloroethyl vinyl ether 0.125 ND ND ND 0.333 0293 1 5.00-149 J6 J6 12.8 40 Chloroform 0.0250 ND O.N65 0.0276 106 110 1 66.1-133 3.94 20 Chloromethane 0.0250 ND 0.0246 0.0256 95.9 102 1 40.7-139 6.54 20 1,2-Dichlorobenzene 0.0250 ND 0.0254 0.0253 102 101 1 77.4-127 0.630 20 1,3-Dichlorobenzene 0.0250 ND 0.0233 0,0249 93.1 99.7 1 67.9-136 6.87 20 0-Dichlorobenzene 6.0256 ND 0.0239 6.0238 95.5 95.1 1 74.4-123 0.380 20 Dichlorodifiuoromethane 0.0250 ND 0,0260 0.0277 104 ill 1 42.2-146 6.48 20 1,2-Dlchloroethane 0.0250 0.0241 0.0473 0.0483 92.7 96.7 1 60.7-132 2.09 20 1,1-Dichloroethane 0,0250 0.000556 0,0274 0.0285 107 112 1 64.0-134 3,96 20 1,1-Dichlorcethene 0.0250 0.60374 0.0289 0.0307 100 108 1 48.8-144 6.31 20 ACCOUNT: PROJECT: SDG: DATErrlME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 13 of 24 WG852162 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 L819665-01 L819193-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 02/26/16 02:54 • (MS) 02/26/16 05:15 • (MSD) 02/2G/16 05:35 Cp Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Oualifer MSD Oualifer RPD RPD Limits 2 Analyte mg/I mg/I mg/I mg/I % % % % % TC trans-1,2-Dichloroethene 0.0250 0.000398 0,0266 0.0280 105 ill 1 61.0-132 5.18 20 1,2-Dichloropropene 0.0250 ND 0.0274 0.0273 109 109 1 69.7-130 0.350 20 a SS cis-1,3-Dichloropropene 0.0250 ND 0.0271 0.0268 108 107 1 711-129 0.970 20 trans-1,3-Dichloropropene 0.0250 ND 0.0292 0.0294 117 117 1 66.3-136 0.390 20 4 Ethylbenzene 0.0250 0.000488 0.0254 0.0261 99.7 103 1 627-136 2.82 20 Cn Methylene Chloride 0.0250 ND 0.0255 0.0274 102 110 1 6L5-126 7,48 20 1,1,2,2-Tetrachloroethane 0.0256 ND 0.0249 0.0270 99.6 108 1 _ 64.9-145 &31 20 5 Sr Toluene 0.0250 0.00142 0.0257 0.0258 97.1 977 1 67.8-124 0.620 20 Tetrachloroethene 0.0250 0,000187 0.0247 0.0257 97.9 102 1 57.4-141 4.05 20 1,1,1-Trichloroethane _ 0.0250 NO 0.0264 0.0267 105 107 1 58.7-134 L28 20 1.1,2-Trichloroethane 0.0250 ND 0.0261 0.0264 104 106 1 741-130 1.23 20 Trichloroethene 0.0256 0.00140 0.0256 0.0267 96.8 101 1 48.9-148 4,32 20 rGI TrichloroFluoromethane 0,0250 ND 0,0263 0,0270 105 108 1 39.9-165 2A3 20 Vinyl chloride 0.0250 0.00184 0.0273 0.0292 102 109 1 44.3-143 6.60 20 a (S) Toluene-d8 107 102 88.5-111 A (S) Dibromolluoromethane 101 166 78,3-121 (S)0,0.a-Trilluorololuene 96.2 988 850-114 SC (S)4-Bromolluorobenzene 93.8 100 7LO-126 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 14 0/ 24 WG851913 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. _ Pesticides.(GC). by Method EPA 608 L819665-01 Method Blank (MB) (MB) 03/02/1614:26 Analyte MB Result mg/I MB Qualifier MB MDL nigh MB RDL mg/I Aldrin U 0,00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 Beta BHC U 0.0000184 0.0000500 Delta BHC U 0.0000197 0.0000500 Gamma OHC U 0.0000176 0.0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0.0000177 ___. 0.0000500 Dieldrin U _._. .0 0.00000751 --._.._ -. __ _ _. ... 0.0000500 Endosulfan I U 0.0000179 0.0000500 Endosulfan 11 U 0.0000176 0,0000500 Endosulfan sulfate U 0.0000196 0.0000500 Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500 _ Endrin ketone U 0.0000170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene U 0.0000134 0.0000500 Methoxychlor U 0,0000193 0.0000500 Chlordane U 0.0000977 0.000500 Toxaphene U 0.000168 0.000500 (SJ Decochlorobiphenyl 64.1 10.0-156 (S) Tetrachloro-m-xvlene 68.5 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 03/01/1617:16 Analyte • (LCSD) 03/O1/16 17:29 Spike Amount mg/I LCS Result mg/I LCSD Result mg/I LCS Rea, % LCSD Rec. % Rec. Limits LCS Qualifier % LCSD Oualifler RPD % RPD Limits % Aldrin 0.00100 0.000470 0.000531 47.0 53.1 10.0-120 12.1 33.9 Alpha BHC 0.00100 0.000883 0.000824 88.3 82.4 53.6-125 6.97 22.3 Beta BHC 0.00100 0.000959 0.000898 95.9 89.8 55.8-130 6.59 20.6 Delta BHC 0.00100 0.00103 0.00095E 103 95.8 42.2-135 6.82 23.3 Gamma BHC 0.00100 0.000982 0.000913 98.2 91.3 54.7-125 7.25 _ 21.1 4,4-DDD 0.00100 0.00110 0.00102 110 i02 47.6-144 7.49 24.3 44-DDE 6.60100 0.00092E 0,000874 92.8 87.4 45.0-124 5.99 257 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L819665 03/0411611:28 15 of 24 WG851913 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 606 L819665-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 03/01/16 17:16 • (LCSD) 03/0111617:29 Spike Amount Analyte mg/I LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rec. % Rec. Limits LCS Qualifier % LCSD Qualifier RPD % RPD Limits % 4.4-DDT 0.00100 0.000977 0.000904 97.7 90.4 49.8-130 7.82 25.4 Dieldrin 0.00100 0.00103 0.000967 103 967 55.0-127 6.77 22.9 Endosulfan I 0.00100 0.00103 0.000959 103 95.9 54.7-127 7.22 24.3 Endosulfan II 0.00100 0.00104 0.000970 104 97.0 53.1-135 714 23.5 Endosulfan sulfate 0.00100 0.00107 0.000995 107 99.5 51.5-132 Z15 26.3 Endrin 0.00100 0.00101 0.000943 101 94.3 50.1-131 7.14 29.1 Endrin aldehyde 0.00100 0.000915 0.000837 91.5 83.7 39.5-137 8.87 28.4 Endrin ketone 0.00100 6.000907 0.000857 90.7 85.7 53.5-139 5.67 28.4 Heptachlor 0.00100 0.000588 0.000627 58-8 62.7 20.7-127 6.48 30.5 Heptachlor epoxide 0.00100 0.000986 0.000920 98.6 92.0 564-124 6.94 231 Hexachlorobenzene 0.00100 0.000520 0.000574 52.0 57.4 26.7-114 9.85 27.6 Methoxychlor 0.00100 0.00104 0.000958 104 95.8 48.2-144 7.84 27.8 (S) Decachlorobiphenyl 69.9 56.7 10.0-7S6 (S) retrochlom m-xylene BE5 783 13.9-137 Method Blank (MB) (MB) 02/26/1610:32 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mgA PCB 1260 U 0.000120 0.000500 PCB 1016 U 0.000100 0.000500 PCB 1221 U 0,0000730 0.000500 PCB 1232 U 0.0000420 0.000500 PCB 1242 U 0,0000470 0.000500 PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 (S) Decachlorobiphenyl 72,5 10.0-156 (S) Tefrachloro-m-xylene 71.4 139-i37 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/26/1610:44 • (LCSD) 02/2611610:57 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mgll mgll % % % % % PCB 1260 0.00250 0.00235 0,00230 93.9 91.9 477-149 2.11 28.8 ACCOUNT: PROJECT: SDG: Eaton Corporation 26091-R L819665 DATE/TIME: 03/04/161128 PAGE: 16 of 24 WG851913 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Polychlorinated Biphenyls (GC) by Method EPA-608 _- _ _ 1-819665-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) C (LCS) 02/26/16 10:44 • (LCSD) 02/26/16 10:57 p Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/1 mg/I mg/I % % % % % TC PCB 1016 0,00250 0.00190 0.00193 76.0 771 24.7-128 140 34.9 (S)Decochlorobiphenyl 76.7 75,9 10.6156 _ a SS ..- etrachl..ara�m-xyl.... _ -ene 81.3 79.7 (S) T 18.9-137 4Cn 6Sr 7GI 6AI 9Sc ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 17 of 24 WG852131 QUALITY CONTROL SUMMARY ONELAB.NATIONWIDE. .� Semi Volatile Organic Compounds UGC/MS) by Method 625 L819665-01 Method Blank (MB) (MB) 02/29/1611:15 Analyte MB Result mg/I MB Qualifier MBMDL mg/I MB RDL mg/I Acenaphthene U 0.000316 0.00100 Acenaphi hylene U 0,000309 0.001DD Anthracene U 0.000291 0,00100 Benzidme U 0,00432 0.0100 Benzo(a)anthracene U 0.0000975 0.00100 Benzo(b)fiucranthene U 0.0000896 0.0o100 Benzo(k)fluoranthene U 0.000355 0.00100 Benzo(g,hJ)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0.00100 Eis(2-0lorethoxy)methane U 0.000329 0.0100 Bis(2-chloroethyl)ether U 0.00162 0.0100 Bis(2-chloroisopropyl)ether U 0.000445 0,0100 4-Bromophenyl-phenylether U 0.000335 0.0100 2-61oronaphthalene U 0.000330 0.00100 4-Chlorophenyl-phenylether U 0.000303 0.0100 Chrysene U 6.00D332 0.00100 Dibenz(a,h)anthracene U 0.000279 0,00100 3,3-Dichlorobenzidine U 0.00202 0.0100 2.4-Dinitrotoluene U 0.00165 0.0100 2.6-Dinitrotoluene U 0.000279 0,0100 Fluoranthene U 0.000310 0.00100 Fluorene U 0.000323 6.00100 Hexachlorobenzene U 0.000341 0.00100 Hexachloro-13-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0,00233 0.0100 Hexachloroethane U 0.000365 0.0100 ' Indenc(1,2,3-cd)pyrene U 0.000279 0.00100 Isophorone U 0.000272 0.0100 Naphthalene U 0.000372 0.00100 Nitrobenzene U 0.000367 0.0100 n-Nitrosodimethylamine U 0.00126 0.0100 1,2-Diphenylhydrazine U 0.000318 0,0100 n-Nitrosodiphenylamine U 0.00M04 0.01oo n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 0.00100 Benzylburyl phthalate U 0.000275 0.00300 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 18 of 24 WG852131 QUALITY CONTROL SUMMARY ONELAS.NATIONWIDE. Semi Volatile Organic Compounds. (GC/MS)_by.Method 625 _ _ L819665-01 Method Blank (MB) (ME) 02/29/1611:15 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 8is(2-ethylhexypphthalate .. 0,00126 0.000709 ...-_60 -_.- 0.00300 -'-_. _ ... .._ ._. - _... .. - ... - ----_. Di-n-butyl phthalate ..-_... U _ 0.000266 0.00300 Diethyl phthalate U 0.000282 0.00300 Dimethyl phthalate U -. 0.000263 0.00300 Di-n-octyl phthalate U 0.000278 0.00300 Pyrene U 0.000330 0.00100 1,2,4=Trichlorobenzene U 0.DD0355 0.0100 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0.000283 0.0100 24-Dichlorophenol U 0000284 0.0100 2,4-Dimethylphenol U 0.000624 0.0100 4,6-Dimtro-2-methy1phenol U 0.00262 0.0100 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0.0100 Phenol U 0.00M34 0.0100 2 4,6-Trichlorophenol U 0.000297 0.0100 (S)Nitrobenzene-d5 508 2LS-123 (S)2-Fluorobiphenyl 680 29.5-131 (S)p-Terpheny1-d14 _ 71.9 293-137 (S)Phenal-d5 272 5.00-70.1 (S) 2-Fluorophenol 43.4 10.0-77.9 (S) Z4,6 Trlbromophenol 527 71.2-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/29/16 10:28 • (LCSD) 02/29/1610:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/1 mg/I al % % % % % Acenaphthene 0.0500 0.0349 0.0383 69.8 76.6 38.7-109 9.19 21.5 Acenaphthylene 0.0500 0.0367 0.0402 73.4 60.3 36.0-106 9.06 21 Anthracene 0.0500 0.0364 cw412 72.8 82.4 43.6-113 12 5 18,8 Benzidine 0.0500 0.0215 60269 43.1 53.7 10.0-165 22.0 40 Benzo(a)anthracene 0.0500 0.0360 0.0408 72.1 81.5 51.2-112 12.3 20 Benzo(b)fiuoranthene 0.05o0 0,0365 0.0418 73.0 33.5 47.6-111 13.4 20 ACCOUNT: PROJECT: SDG', DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03104/1611:28 19 of 24 WG852131 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625 L819665-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/29/16 10:28 • (LCSD) 02/29/16 10:51 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Oualifier RPD RPD Limits Analyte mg/1 mg/1 mg/I % % % % % Benzo(k)Fluoranthene 0.0500 0.0349 0,0393 69.8 78.7 494-114 11.9 20 Benzo(g.h,i)perylene 0.0500 0.0359 0.0414 71.7 82.9 45.2-117 14.4 20 Benzo(a)pyrene 0.0500 0.0357 0,0409 71.5 81.8 45.6-106 13.5 20 Bis(2-chlorethoxy)methane 0.0500 0.0333 0.0367 66.6 73.3 37.2-111 957 24.1 Bis(2-chloroethyl)ether 0.0500 0.0314 0.0326 62.9 65.3 22.6-108 3.79 27.9 Bi5(2-chloroisopropyl)ether 0.0500 0.0359 0.0371 71.7 74.1 32.9-100 3.28 25.1 4-Bromophenyl-phenylether 0.0500 0.0356 0.0406 71.2 81.2 40.7-116 13.7 21 2-Chloronaphthalene 0.0500 0.0358 0.0385 71.7 77.0 33.6-105 712 23 4-Chlorophenyl-phenylether 0,0500 0-0349 0.0386 •69.8 77.2 39.0-113 10.1 20.9 1,2-Diphenylhydrazme 0.0500 0.0359 0.0464 71.8 80.8 37.6-111 11.8 21.1 Chrysene 0.0500 0.0350 0.0395 70.0 78.9 54.6-120 12.0 20 Dibenz(a,h)anthracene 0,0500 0.cm8 0.0406 71.6 81.3 42.8-118 12.8 20 33-Dichlorobenzid1ne 0.0500 0.0322 0.0409 64.4 81.8 272-142 J3 23,8 22.3 2,4-Dinitrotoluene 0.0500 60349 0.0404 69.7 80.8 3L2-105 14.7 22 2,6-Dinitrotoluene 0.0500 0.0349 0.0399 69.8 79.9 30.6-106 136 23.1 Fluoranthene 0.0500 0.0360 0.0405 71.9 81.0 45.9-115 11.9 20 Fluorene 0.0500 0.0361 0.0396 72.1 79.3 41.0-112 9.45 20.2 Hexachlorobenzene 0.0500 0.0367 0.0403 73.4 80.6 38.5-116 9.30 20.1 Hexachloro-13-butadiene 0.0500 0.0290 0,0320 58.1 63.9 16.1-104 9.57 3L2 Hexachlorocyclopentadiene 0.0500 0.0217 0.0226 43.5 45.3 10.0-121 4,03 27.9 Hexachloroethane 0,0500 0.0293 0.0323 58.7 64.5 16.5-89.8 9AS 30.7 Indeno(1,2,3-cd)pyrene 0.0500 0.0363 0.W5 72.6 83.1 45.0-116 13.5 20 Isophorone 0.0500 0,0365 0.0403 73.0 80.5 3SA-112 9.85 21.5 Naphthalene 0.0500 0.0313 0.0347 62.7 69.4 32.2-101 10.1 23.8 Nitrobenzene 0,0500 0.0344 0.0369 68.9 73.8 31.4-106 7.00 25.7 n-Nitrosodimethylamine 0.0500 0.0147 0.0161 29A 32.3 10.0-80.1 9.27 37.5 n-Nurosodiphenyla mine 0.0500 0.0380 0.0418 76.0 83.6 44.4-113 949 20 n-Nitrosodi-n-propylamine 0.0500 0,0383 0.0415 76.5 83.0 33-2-106 8,12 23.7 Phenanthrene 0.0500 0.0351 0.0366 70.3 77.3 46.4-113 _ 9.47 20 Benzylbutyl phthalate 0.0500 0.0343 0,0392 68.7 78.3 31.8-123 13.1 20.7 Bis(2-ethylhexy1)phtha1ate 0.0500 0.0339 0.0383 67.8 76.6 36.9-134 12.1 23.6 Di-n-butyl phthalate 0.0500 0,0349 0.0395 69.7 79.6 41.8-120 12.5 202 Diethyl phthalate 0,0500 0.0380 0,0431 75.9 86.3 36.5-129 12.7 20 Dlmethyl phthalate 0.0500 0.0376 0.0419 75.2 83.7 35.3-128 107 20.8 Di-n-octyl phthalate 0.0500 0,0323 0,0372 64.5 74.5 39.7-112 14.3 21.1 Pyrene 0.0500 0.0370 0.0417 73.9 83.5 46,3-117 12.1 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE' Eaton Corporation 28091-R L819665 03/0411611'28 20 of 24 WG852131 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. -Semi Volatile Organif_Compountls. (GC/MS)_by Method 625-- -,. _ _L819665-07__ _ _- _ _ _ _ •. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 02/29/16 10:28 - (LCSD) 02/29/16 10:51 Spike Amount Analyte mg/I LCS Result mg/I LCSD Result high LCS Rec. % LCSD Rec % Rec. Limits % 1,2,4-Trichlorobenzene 0.0500 0.0298 0.0323 59.5 64.6 22.9-96.1 '4-Chloro-3-methylphenol 00500 0.0370 0.0425 73.9 84.9 35.7-100 2-Chloropheno1 00500 0.0331 0.0344 66.3 68.7 26.2-91.5 �24-Dichlorophenol 00500 00365 0.0404 72.9 80.8 31.4-103 2,4-Dimethylphenol 00500 00353 0,0395 70.6 79.1 319-107 4,6-Dinitro-2-methylphenol 0.0500 00384 0.0453 76.7 90.6 18.4-148 2,4-Dlnitrophenol 0.0500 0.0234 0.0318 467 63.6 242-128 �2-Nitrophenol O0500 0.0358 0.0383 717 76.6 25.9-106 4-Nitrophenol 0.0500 0.0153 0.0195 30.5 39.0 10.0-527 Pentachlorophenol 0.0500 0.0343 0.0390 68.6 78.6 10.9-97.4 Phenol 0.0500 0.0149 0.0168 29.7 33.6 10.0-57.9 0.0500 O6363 0.0403 72.6 80.6 29.8-107 ,2A,64richlorophenol (S)Nitrobenzene-d5 55.5 67.5 27.8-123 - (S)2-Fluorobiphenyl - - _ - - - _ -- 68.7 73.5 29.5-131 (Slp-Terphenyl-d74 72.6 81.3 29.3-137 (S) Phenol-d5 286 3t3 5M-70.1 (S)2-Fluorophenol 44.5 451 10.077.9 /SJ2,4,6-Tribromophenol 75.5 7918 11.2-130 LCS Qualifier LCSD Oualifier RPD RPD Limits 8.22 27.5 - - - 13.8 22.9 3.66 26.5 10.2 N.9 lL3 25.7 16G NA J3 30.7 20.5 6.68 26.9 24.4 40 - 12.7 35.1 - 12.2 35 10.5 - _. 24.7 ACCOUNT: PROJECT: SEE: Eaton Corporation 28091-R L819665 DATEMME: 03/04/1611'.28 PAGE: 21 of 24 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. Cp MDL - RDL _ Method Detection Limit. - - Reported Detection Limit. TC ❑ ND,U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. a (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry Ss report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) aCn from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control s Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring Sr recovery. Surrogates are not expected to be detected m all environmental media. Rec. Recovery. e SDL Sample Detection Limit. Qc VOL Method Ouantitation Limit. Unadj. MOL Unadjusted Method Ouantitation Limit. a[Al Qualifier Description J _ The identification of the analyte is acceptable; the reported value is an estimate. aSc J3 The associated batch OC was outside the established quality control range for precision. J4 The associated batch OC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L819665 03/04/1611:28 22 o124 ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE. 10 • ESC Lab Sciences is the only environmental laboratory accredited/cenified to support your work nationwide from one location. One phone call, one point of contact. one laboratory. No other lab Is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory Is comparable to the collective totals of the network laboratories In our industry, The most significant benefit to our 'one location' design is the resin n of our laboratory campus. the model Is conducive to accelerated productivity, decreasl ng turn -around time, and preventing cross contamination, thus protecting sample integrity, Our focus on premium quality antl prompt service allows us to be YOUR LAB OF CHOICE. • Not all certifications held by the laboratory are applicable to the results reported in the attached report. State Accreditations Alabama 40660 Nevada_ __ TN-03-2002-34 Alaska _ UST_080 _ ___ New Hampshire _ _2975 --- Arizona AZ0612_ ___ _ _ __ New Jersey_NE_LAP __ _ _ _ _ _ _ _ TN002__ _ Arkansas _ 88-0469_ New Mexico TN00003 California 01157CA New York 11742 Colorado TN00003 __ _North Carolina_ Env375 Conneticut PH-0197 _ _ North Carolina_ _DW21704 _ Florida E87487 North_ Carolina'_ _ 41 Georgia NELAP North Dakota _ _ _ _ _ R_140 Georgia 923 _Ohio—VAP Idaho TN00003 Oklahoma __CL0069 _ __9915___ Illinois Oregon___. __ TN2000D2 Indiana _200008 C TN-01 Pennsylvania 68-02979 _ Iowa 364,- _Rhode Island 221 Kansas E-10277 South Carolina 94004 Kentucky' 90010 South Dakota n/a _ Kentucky' 16 Tennessee" _ 2006 Louisiana A130792 _ Jexas _ _ _ _ _ _T 104704IN5_07-T%__ Maine TN0002 Texas' LAB0152 ___ Maryland 324 Utah_ _ 6157585858 Massachusetts M-TNO03 Vermont VT2006 _ Michigan_ 9958 --_ _ Virginia_ 109 Minnesota 047-999-395 _ Washington_ C1915 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin _ 9980939910__ Montana CERT0086 _ Wyoming _ _ ____ AKA _ Nebraska NE-OS-15-05 Third Party & Federal Accreditations A2LA—IS017025 1461.01 AIHA 100789 A2LA—ISO 17025' 1461.02 DOD 1461.01 _ Canada 1461,01 USDA _ S-67674 EPA —Cry to TN00003_ ` Drinking Water 2-Underground Storage Tanks 1 Aquatic toxicity ' Chemicanvicroblological ` Mold ° Acc edaation not applicable Our Locations ESC Lab Sciences has sixy--four client support centers that provide sample plckup and/oche delivery of sampling supplies. It you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. wA O �• MT N[] OR • MIN T IIJ sO T wl T T NY 4 wr Tal ! o NV T • IT N[ T T T T � „• T VA ! �!r T �T T O • yw • T T KS MT • •VVA! _CA T T •r9 N • •� ice! T : NM 0� ArT • T sc • • MS AL CA e • AK !T • • ! O $O FL �o B HI i ACCOUNT: PROJECT: SDG: DATEMME: Eaton Corporation 28091-R L819665 03/04/161128 Me PAGE: 23 of 24 6 Company Name/Address: Eaton Corporation NA Financial Po Box 818024 2564 Durham Rd Cleveland, CH 44181-B024. Roxboro, NC 27573 Re port to: ErtWIi To: ustlnla4.liir@Eaton.com Dustin LaClair Project Citylstate Roxboro, NC Eaton Corp.,Semi-Annual Stormwater 6nifected: 9 Pho.036-59911-ill I Client Project 0 Lob Project EAT6NRNC-28091S 28091 -R Fax: collected by (Pginl)- Site/Facifity to 0 P.O. # Date Results Nettle r Collected by (sipature)' Rush? (Lab MUST Be Nolffied) same Day. .......... ---.100% Next Day .... ...... ...... Emad? —No _ CS inunedialekV D" No Thee FAX? 2�No --- �ye$ 'of Packed on Ice N— V nin Sample to Comp/Gran matrix • Depth Date nun,.: CIO Pirm Ttv'lek WW •L�3,nx: Si- SoIIGW.GroundwaterVVW-wa.st,W3ter,DW-CrinkinoWater OT-q[hV'F' Rematks; ed Refinxials attire Rerewed DY; Dat Time: (Signature) TIA.1% L4 Relmquished by tSignaturejt Time: ReCeWedb ;(ST (Signature) Date: W Relinquished by: ISfilifatfMily Cale: Time: eeG!C' "Y' Ili O z 0 E E X 6 ESC L% rnun.:.wl6Ysess S. F090 pH TemiP Flow Hold 0 "—A UPS samples returned viat COMItion: (lab .Ib fed Ea bc-UrLer gvdature)T Date:� - MIR NA:` M~ n .volu roc<e�o rir�'o'rre e't ANALYTICAL REPORT January 26, 2016 h3Doll Eaton Corporation Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L812515 01/16/2016 28091-R Eaton Corp Semi -Annual Stormwater ROXBORO,NC Dustin LeClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: P Ld V Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test rupon shall not be reproduced, except in full. without written approval of the laboratory, Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. myESC TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: 'c p Cover Page 'Tc: Table of Contents 2 'Ss: Sample Summary 3 4Cn: Case Narrative 4 3S5 'Sr: Sample Results 5 , 2016-01-15-005 L812515-01 5 Cn 60c: Quality Control Summary 8 Sr Gravimetric Analysis by Method 2540 D-2011 8 Wet Chemistry by Method 1664A 9 6 Oc Metals (ICP) by Method 200.7 10 �GI Volatile Organic Compounds (GC/MS) by Method 624 11 Pesticides (GC) by Method EPA 608 15 EAI Polychlorinated Eiphenyls (GC) by Method EPA-608 16 Semi Volatile Organic Compounds (GC/MS) by Method 625 18 s Sc 'GI: Glossary of Terms 22 8AI: Accreditations & Locations 23 9Sc: Chain of Custody 24 ACCOUNT: PROJECT: SDG: DATEMME: Eaton Corporation 28091-R L812515 01126/1616:57 PAGE: 2 of 24 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time 2016-01-15-0 '05 L812515-01 WW P D. LeClair OV15A615:00 OV16/16 09:00 i G Method Batch Dilution Preparation Analysis Analyst date/time date/time 2T Gravimetric Analysis by Method 2540 D-2011 WG843133 1 01I19I1614:56 01/19I7675:33 ME Metals (ICP) by Method 200.7 WG843305 1 OV19/I6 20:34 01/20/1613:57 WBD Pesticides (GC) by Method EPA 608 WG842947 1 01/19116 08:35 01/20/1618:34 ADF Polychlorinated Biphenyls (GC) by Method EPA-608 WG842947 5 01/19116 08:35 01/26/1611:27 LKD Semi Volatile Organic Compounds (GC/MS) by Method 625 WG843233 1 OW91160924 01/20r619:27 JF ° Cn Volatile Organic Compounds (GC/MS) by Method 624 WG842965 1 01/17/16 07:20 01/17/16 07:20 ACG Wet Chemistry by Method 1664A WG843527 1 01120/161352 01120/1615:It JM a SF 6QC 7G1 eAl 95C v i 1 ACCOUNT: PROJECT: SDG: DATERIME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 3 of 24 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the I C p appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the ITC] analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the 3SS laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. aSr 6 41XJ- QC 7G1 Jimmy Hunt eAl Technical Service Representative ACCOUNT: PROJECT: SDGDATEMME: PAGE: Eaton Corporation 28091-R L812515 01126/1616:57 4 of 24 2016-01-15-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 01115/16 15:00 L812515 Additional Information Cp Result Units z Analyte pH (On Site) 7 su TC Temperature (on -site) 10.1 Deg C 2540 D-2011 _ aSs Gravimetric Analysis by Method Result Qualifier MDL ROL Dilution Analysis Batch Gn Analyte mgA mgA mgA date/time Suspended Solids 18A 0.350 2.50 1 01/19/201615:33 WG843133 Wet Chemistry by Method 1664A 6 Result Qualifier MDL RDL Dilution Analysis Batch QC Analyte mgA mgA mgA date/time TPH -Oil&Grease U 0.725 5.81 1 011201201615:11 WG843527 7GI Metals (ICP) by Method 200.7 s A Result Qualifier MDL RDL Dilution Analysis Batch s Analyte mgA mgA mgA date/time Copper 0.0161 0,00700 0.0100 1 01/20/201613:57 WG843305 SC Lead 0.00440 J 0.00200 0.00500 1 01/201201613:57 WG943305 Zinc 0,0616 0.00340 0.0500 1 01/20/201613:57 WG843305 Volatile Organic Compounds (GC/MS) by Method 624 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mgA date/time Acrolein U J4 0.00887 OD500 1 01/17/201607:20 WG842965 AcrylonitNe U 0.00187 0.0100 1 01/17/2016 07:20 WG842965 Benzene U 0.000331 0.00100 1 01/17/201607:20 WG842965 Bmmodichloromethane U 0.000380 o.o61oo 1 0IJ17/2016 07:20 WG842965 Bromoform U 0.000469 0.00100 1 01AW201607:20 WG842965 Bromomethane U 0.000966 0,00500 1 01117/201607:20 WG842965 Carbon tetrachloride U 0.000379 0.00100 1 01117/201607:20 WG842965 Chlarobenzene U 0.000346 0.00100 1 01117/201607:20 WG842965 Chloroduromomelhane U 0,600327 000100 1 01/17/201607:20 WG842965 Chloroethane U 0,000453 0.00500 1 0107/2016 07:20 WG842965 2-Chloroethyl vinyl ether U 0,00301 0.0500 1 01117/201607:20 WG842965 Chloroform U 0.000324 0.00500 1 OIY17/2616 0720 WG842965 Chloromethane U 0,000276 0.00250 1 01117/201607:20 WG842965 1.2-Dichlorobenzene U 0.000349 0.00100 1 0111V2016 07:20 WG842965 1,3-Dichlorobenzene U 0,000220 0.00100 1 01117/201607:20 WG842965 1.ADichlorobenzene U 0.000274 0.00100 1 01117/201607:20 WG842965 Dichlorodifluoromethane U 0,000551 0.00500 1 01/17/2016 07 20 WG842965 'Ll-Dichloroelhane U 0.000259 0.00100 1 0111MO16 07:26 WG842965 L2-Dichlorcethane U 0,000361 0.00100 1 01/171201607:20 WG842965 L1-Dichloroelhene U 0.000398 0.00100 1 01117/201607:20 WG842965' trans-1,2-Dichloroethene U 0,000396 0.00100 1 01/171201607:20 WG842965 1,2-Dichloropropane U 0.000306 0.00100 1 01/17/201607:20 WG842965 cis-1,3-Dichloropropene U 0,000418 0.00100 1 01/17/201607:20 WG842965 Vans-1,3-Dichloropropene U 0.000419 0.00100 1 01/17/201667:20 WG842965 Ethylbenzene U 0.000384 0.00100 1 01117/201607:20 WG842965 Methylene Chloride U 0.00100 0.00506 1 01/17/201607:20 WG842965 11,2,2-Tetrachloroethane U 0.000130 0.00100 1 01/17/201607:20 WG842965 Tetra chloroethene U 0.000372 0.00100 1 01/17)201667:20' ,_� WG842965 _. Toluene U ` 0.006780 0.00500 1 01/17/201607:20 WG842965 1,1,1-Trichloroethane U 0.006319 0.00100 1 OM7/20160720 WG842965 I.I.2-Trichloroethane U 6.000363 0,00100 1 01/17/201607,20 WG842965 ACCOUNT: PROJECT: SDG: DATE/TIME. PAGE: Eaton Corporation 28091-R L812515 01/26/1616: 57 5 of 24 2016-01-15-005 SAMPLE RESULTS - 01 Collected Dale/lime 01/15/16 15:00 L812515 Volatile Organic Compounds (GC/MS) by Method 624 ONE LAB. NATIONWIDE. 0 Analyte Result mgA Dualifer MDL mgA RDL mgA Dilution Analysis date/time Hatch Trichloroethene if 0.000398 0.00100 1 OVI7/201607:20 WG842965 Trichlorofluoromethane U 0.00120 0.00500 1 O1h7/201607:20 WG842965 Vinyl chloride U 0.000259 0.00100 1 OM71201607:20 WG842965 (S)Toluene-d8 103 90.0-115 01117201607,20 WG842965 (S)Dibromofluoromethone 99.9 79.0-121 OY17201607.20 WG842965 (A o,n.a- Trilluorotoluene 101 90.4-116 01117201607.20 WG842965 (S)4-Bromo;luorobenzene 96.9 80.1420 007201607.20 WG842965 Pesticides (GC) by Method EPA 608 Analyte Result mgA Qualifier MDL mgA RDL mgA Dilution Analysis date/lime Batch Aldrin U 0.00000813 0.0000500 1 01/20/201618:34 WG842947 Alpha BHC U 0.0000166 0,0000500 1 01/20/201618:34 WG842947 Beta BHC U 6.0000184 0.0000500 1 01/20/201618:34 WG842947 Delta BHC U 0,0000197 OA000500 1 01/20/201618:34 WG842947 Gamma BHC U 0,0000176 0.0000500 1 01120/201618:34 WG842947 Chlordane u 0.0000977 0.000500 1 01/20/201618:34 WG842947 4,4-DDD U 0.0000170 0.0000500 1 01/20/201618:34 WG842947 4,4-DDE u 00000164 0.0000500 1 011201201618:34 WG842947 4,4-DDT U 0.0000177 0.0000500 1 01120/201618:34 WG842947 Dleldrin U 0D0000751 0.0000500 1 01/20/201618:34 WG842947 Endosulfan I U 0.0000179 0A00500 1 01120201618:34 WG842947 Endosulfan 11 U 0,0000176 0.0000500 1 01120201618:34 WG842947 Endosulfan sulfate U 0.0000196 0.0000500 1 011201201618:34 VIG842947 Endrin U 0,0000189 a000 500 1 01120/201618:34 WG842947 Endrin aldehyde U 0.0000142 0.0000500 1 01/201201618:34 WG842947 Endrin ketone U 0.0000170 0.0000500 1 01/20/201618:34 WG842947 Heptachlor U 0.0000108 0.0000500 1 01/20/201618:34 WG842947 Heptachlor epoxide U 0.0000175 0.0000500 1 01/20/201618:34 WG842947 Hexachlorobenzene U 0,0000134 0.0000500 1 01/20201618:34 WG842947 Methoxychlor U 0.0000193 0.0000500 1 01120/201618:34 WG842947 Toxaphene U 0-000168 0.000500 1 01/20201618:34 WG842947 (5) Demchlorobiphenyl 57.4 10.0-156 0120120161834 WG842947 (S) Telrochloro-m-xylene 84.6 139-137 OV20201618.34• VIG842947 Polychlorinated Biphenyls (GC) by Method EPA-608 Analyte Result mg/I Qualifier MDL mgA RDL mgA Dilution Analysis date/lime Batch PCB 1016 U 0.000500 0.00250 5 01/26/20161127 WG842947 PCB 1221 U 0.000365 0.00250 5 01/26/20161127 WG842947 PCB 1232 U 0,000210 0.00250 5 01126/20161127 - WG842947 PCB 1242 u 0,060235 0.00250 5 OIJ26/201611'.27 WG842947 PCB 1248 U 6.000430 0.00250 5 01126/20161127 WG842947 PCB 1254 U 0.000235 0,00250 5 01126/201611,27 VIG842947 PCB 1260 U 0.600600 0.00250 5 01/2620161127 WG842947 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Oualifier MDL RDL Dilution Analysis Batch Analyle mgA mgA mgA date/time Acenaphthene U 0.000316 0.00100 1 01120/201619:27 WG843233 Acenaphthylene U 0.000309 0.00100 1 01/20/201619:27 WG843233 Anthracene U 0.000291 0.00100 1 01/20201619:27 LVG843233 Benzidme U _ 0.00432 0.0100 1 01/20/201619:27 WG843233 Ben2o(a)anthracene U 0,0000975 0.00100 1 01/20/201619:27 WG843233 Benzo(b)Ruoranlhene U 0.0000896 aoolo0 1 01/201201619:27 WG843233 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 6 of 24 2016-01-15-005 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 01115/16 15:00 L812515 Semi Volatilp Organic Compounds (GC/MS) by Method 625 Analyte Result mg4 Oualifer MOL mg/1 RDL mg4 Dilution Analysis date/time Batch Benzo(k)8uoranthene U 0,000355 0.00100 1 01120/201619:27 WG843233 Benzolg,h,llperylene U 0.000161 MOM 1 01120/201619:27 WG843233 Benza(a)pyrene U 0.000340 0.00100 1 01/20/2016 19:27 WG843233 Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 01/20/2016 19:27 WG843233 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 01120/2016 19 27 WG843233 Bis(2-chloroisopropAether U 0.060445 0.0100 1 01/20/201619:27 WG843233 4-Bromophenyl-phenylether U 0.000335 0.0100 1 0120/201619:27 WG843233 2-Chloronaphthalene U 0.000330 0.00100 1 01/20/2016 19:27 WG843233 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 01/20/2016 19:27 WG843233 Chrysene U 0.000332 0.00100 1 01/20/201619:27 WG843233 Nbenz(a,h)anthracene U 0.000279 0.00100 1 01/20201619:27 WG843233 3,3-Dichlorobemadine U 0.00202 0,0100 1 01/20201619:27 WG843233 2,4-Dinitrotoluene U 0.00165 0.0100 1 01/201201619:27 WG843233 2,6-Dinitrotoluene U 0.000279 0.0100 1 01/20201619:27 WG843233 1,2-Diphenylhydrazine U 0.000318 O0100 1 01/20/201619:27 WG843233 Fluoranthene U 0.000310 0.00100 1 0120201619:27 WG843233 Fluorene U 0.000323 0.00100 1 01/20/201619.27 WG843233 Hexachlorohenzene U 0.000341 0.00100 1 0120120161127 WG843233 Hexachloro-1,3-hutadiene U 0.000329 0.0100 1 0120/201619:27 WG843233 Hexachlorocyclopentadiene U 0.00233 0.0100 1 0120201619:27 WG843233 , Hexachloroethane U 0.000365 0.0100 1 01120/201619:27 WG843233 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 0120/201619:27 WG843233 Isophorone U 0.000272 0,0100 1 0120/201619:27 WG843233 Naphthalene U 0.000372 0.00100 1 0120201619:27 WG843233 Nitrobenzene U 0.000367 0.0100 1 011201201619:27 WG843233 n-NTrosadimethylamine U 0.00126 0.0100 1 01120/201619:27 WG843233 n-Nitrosadiphenylamine U 0.000304 0.0100 1 0120/201619:27 VIG843233 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 0120/201619:27 VIG843233 Phenantmene U 0,000366 0.00100 1 011201201619:27 VIG843233 Benzylbutyl phthalate 0.00131 J 0,0002715 0.00300 1 01/201201619:27 WG843233 8is(2-ethylhexyI)phthalate 0.00150 J 0.000709 0.00300 1 01/201201619.27 WG843233 Dim -butyl phthalate 0.00151 J 0.000266 0.00300 1 0120/201619:27 WG843233 Diethyl phthalate 0.00215 J 0,000282 0.00300 1 012012016 19:27 VJG843233 Dimethyl phthalate U 0.000283 0.00300 1 01/20/201619:27 VJG843233 Di-n-octyl phthalate 0.00131 J J3 0.000278 0.00300 1 0120/201619:27 VIG843233 Pyrene U 0.000330 0.00100 1 O120/201619:27 VIG843233 1,2,4-Trichlorobenzene U 0.000355 0,0100 1 0120/201619:27 V16843233 4-Chloro-3-methylphenol U 0.000263 0.0160 1 0120/201619:27 VJG843233 2-Chlorophenol U 0.000283 0.0100 1 01/201201619:27 WG843233 .. 2,4-Dichlorophenol U 0.000284 0,0100 1 01/20/201619:27 VIG843233 2,4-Dimethylphenol U 0.000624 0,0100 1 0120/201619:27 VIC843233 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 01120/201619:27 WG843233 2,4-Dinitrophenol U J3 0.00325 0,0100 1 01/201201619:27 WG843233 2-Nitrophenal U 0.000320 0.0100 1 01/20/20161927 WG843233 4-Nitrophenal U 0,00201 00100 1 01/20/201619:27 VIG843233 Pentachlorophemol U 0.000313 0.0100 1 01/20/2016 19:27 WG843233 Phenol U 0,000334 0.0100 1 01/20/201619:27 WG843233 2,4,6-Trichlorophenol U 0.000297 0.0100 1 01120/201619:27 WG843233 (S)2-Fluorophenol 450 10.0-77.9 01120201619.27 WG843233 (S) Pheno145 325 5.00-70.1 01120201619:27 VIG843233 (S) Nitrobenzene-d5 69.9 21.8-123 0120120161,97 WG843233 (S)2-Fluorobiphenyl 693 29.5-21 01/20120161927 WG843233 (S)24.6-Tribromcphenol 6t7 11.2-130 011201201619.27 WG843233 (S)p-Terphenyl-d14_ 84.2 _ � 295-137 011201201619. 27 WG843233 ACCOUNT: PROJECT: BEG: DATEMME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 7 of 24 WG843133 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Gravimetrlc Analysis by Method 2540 D-2011 1812515-01 Method Blank (MB) (MB) 01/19/16 15:33 Cp MIS Result MR Qualifier MR MOIL Me RDL Analyte mg/I mg4 rig/I Suspended Solids U 0.350 2.50 L812431-01 Original Sample (OS) • Duplicate (DUP) (US) 01/19/16 15:33 • (DUP) O1119/16 15:33 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte C ni mg/I % % Suspended Solids 5.00 5.00 1 0.000 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/19/16 15:33 • (LCSD) 01/19/16 15:33 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mgA mg/I % % % % % Suspended Solids 773 736 744 95.2 96.2 85.0-115 1.08 5 rl . ACCOUNT: Eaton. Corporation PROJECT: 28091-R SDG: L812515 DATEITIME: 01/26/1616:57 PAGE: 8 of 24 WG843527 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet.Chemistry by Method 1664A L812515-01 _ Method Blank (MB) Rp (MB) 01/20/1615,01 MB Result MB Qualifier MB MDL MB RDL - 2 Analyte mg/I mg/I mgn TC TPH - Oil & Grease U 0.725 5.00 3S$ Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 4Cn (LCS) 01/20/1615:03 • (LCSD) 01/20/1615,04 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 5 Analyte mgll mq/I Mg/1 % T. % % %Sr TPH - Oil & Grease 20.0 18.6 19.2 93.0 96.0 78.0-114 3.17 18 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L812515 01/2611616:57 9 of 24 0 WG843305 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals QCP) by Method 200.7 L812515-01 Method Blank (MB) (MB) 01/20/1612:55 Cp MB Result MB Qualifier MB MOIL MB ROL Analyte mg/I mg/I mgA Copper u 0.007 0.0100 Lead u 0.002 0.00500 Zinc u 0.0034 0.0500 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/1612:58 • (LC5D) 01/2011613:01 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg/I ni % % % % % Copper 1,00 1.01 LOO 101 100 85-115 1 20 Lead 1.00 1.02 LOO 102 100 85-115 1 20 Zinc 1.00 1.00 2991 100 99 85-115 1 20 L812218-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 01/20/16 13:10 • (MS) 01/20/16 13:16 • (MSD) 01/20/16 13.19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/l mgn mall mg/l % % % % % Copper 1.00 0.0418 L05 1.05 101 101 1 75-125 1 20 Lead L00 0.00650 LOS 1.05 104 104 1 75-125 0 20 Zinc 1.00 0.230 124 1.24 101 101 1 75-125 0 20 L812577-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 01/20/1614:04 • (MS) 01/20/1614:07 • (MSD) 01/20/1614:10 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I % % % % % Copper 1.00 0.00314 1.01 1.00 101 100 1 75-125 1 20 Lead LOO 0.00114 L03 1.01 102 101 1 75-125 1 20 Zinc 1.00 0.0191 103 1.01 101 99 1 75-125 2 20 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R - L812515 DATE/TIME: 01/26n616:57 PAGE: 10 of 24 WG842965 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Orgdric Compounds (GC/MS) by Method 624 _ _ L812515-01 Method Blank (MB) (MB) 01/16/1613.33 Analyte MB Result mg1l MB Oualifer MB MDL mg/I MB RDL mgA Acrolein U 0,00887 0.0500 Acrylonitrile U 0.00187 0.0100 Benzene U 0.000331 0,00100 Bromodichloromelhane U 0,000380 0,00100 Bromoform U 0.000469 0.00100 Bromomethane U 0,000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 ,Chlorobenzcne U 0.000348 0.00100 _ Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500 2-Chlcrcethyl vinyl ether U 0.00301 0,0500 Chloroform U 0.000324 0.00500 Chloromethane U 0.000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 1,3-Dichlorobenzene U 0.000220 0,00100 1,4-Dichlorobenzene U 0,000274 0.00100 Dichlorodiflueromethane U 0.000551 0.00500 .1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 LI-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene _ _ U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 _ cis-1,3-Dichloropropene U _ 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0,00100 Ethylbenzene U 0,000384 0,00100 Methylene Chloride U 0.00100 0.00500 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000780 0.00500 1,1,1-Trichloroethane U 0,000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0,00100 Trichlorofluoromethane U 0.00120 0.00500 Vinyl chloride U 0.000259 0.00100 (S) Tofuene-d8 104 90.0-115 (S) DibromolWorome(hone 105 79.0.121 ACCOUNT: PROJECT: SDG: DATE/TIME: Eaton Corporation t 28091-R L812515 01/26/1616'57 PAGE: 11 of 24 WG842,9.65 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 L812515-01 Method Blank (MB) (ME) 01/16/16 13.33 MB Result MB Qualifier MB MDL MB RDL Analyte mg1l mg/I ri (i zac-Trifluorotoluene 975 904-116 (S)4-Bromol/uorobenzene 91.0 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/16/1611:50 • (LCSD) 01/16/1612:11 Spike Amount Analyte mgll LCS Result mg/l LCSD Result mg/I LCS Rec. % LCSD Rea. % Rec. Limits LCS Qualifier % LCSD Qualifier RPD is RPD Limits % Acrolein 0.125 1.23 1.24 985 991 88.0-118 J4 J4 0.630 28.1 Acrylonitrile 0.125 0.123 0.126 98.7 100 71.0-135 1.75 20 Benzene 0.0250 0.0254 0,0251 101 100 73.0-122 1,05 20 Bromodichloromethane 0.0250 0.0250 0,0251 100 100 75.5-121 0,400 20 Bromoform 0,0250 0.0242 0.0246 96.7 98.4 71.5-131 1.78 20 Bromomethane 0.0250 0.0278 0.0283 Ill 113 22.4-187 1.74 20 Carbon tetrachloride 0.0250 0.0263 0,0292 105 117 70.9-129 10.6 20 Chlorobenzene 0.0250 0.0232 0.0241 92.9 96.4 79.7-122 3.61 20 Chlorodibromomethane 0.0250 0.0233 0.0242 93.2 96.9 78.2-124 3.96 20 Chloroethane 0,0250 0.0271 0,0275 108 110 41.2-153 1.48 20 2-Chloroethyl vinyl ether 0.125 0,139 0.139 ill Ill 23.4-162 0,310 23.5 Chloroform 0.0250 0.0274 0.0274 110 110 73.2-125 0.120 20 Chloromethane 0.0250 0.0236 0.0234 94.3 -93.5 55.8-134 0.890 20 1,2-Dichlorobenzene 0.0250 0.0244 0.0247 97.7 98.8 84.7-118 L09 20 1,3-Dichlorobenzene 0.0250 0.0233 0.0234 93.0 93.7 77.6-127 0.760 20 1,4-Dichlorobenzene 0.0250 0.0246 0.0246 98.5 98.4 82.2-114 0.0600 20 Dichlorodifluoromethane 0.0250 0.0270 0,0269 108 108 56.0-134 0.190 20 Lt-Dichloroet4ane 0.0250 0.0260 0.0263 104 105 71.7-127 1.20 20 1,2-Dichloroethane 0,0250 0.0267 0.0267 107 107 65.3-126 0.240 20 1,1-Dichloroethene 0.0250 0.0279 0.0285 ill 114 59.9-137 2,30 20 trans-1,2-Dichloroethene 0.0250 0.0249 0.0255 99.7 102 72.6-125 2.24 20 1,2-Dichloropropane 0.0250 0.0238 0.0240 95A 95.8 77.4-125 0,480 20 cis-13-Dichloropropene 0,0250 0,0246 0.0252 98.3 101 77.7-124 2.35 20 trans-1,3-Dichloropropene 0,0250 0.0245 0.0250 98.0 99.9 73.5-127 1.91 20 Ethylbenzene 0.0250 0,0234 0.0239 93.5 95.6 80.9-121 2.19 20 'Methylene Chloride 0,0250 0.0232 0.0232 93.0 92.6 69.5-120 0.370 20 1,1,2,2-Tetrachloroethane 0.0250 0.0239 0.0240 95.5 96.1 79.3-123 0.650 20 Tetrachloroethene 0.0250 0.0229 0.0235 91.5 93.8 73.5-130 2.45 20 ACCOUNT: PROJECT: SDG'. DATE/TIME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 12 of 24 WG842965 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE, Volatile, Organic Compounds (GC/MS) by Method 624 L812515.01 Laboratory Control Sample (LCS) (LCS) 01/16/1611:50 - (LCSD) 01/16/16 12 11 Spike Amount Laboratory Control Sample Duplicate (LCSD) LCS Result Toluene - 0.0250 0.0245 1,1,1-Trichloroethane 0.0250 0.0284 1,1,2-Trichloroethane 0.0250 0.0226 Trichloroethene 0,0250 0,0242 Trichlorofluoromethane 0.0250 0.0289 Vinyl chloride 0.0250 0.0254 (S) Toluene d8 (S) Oibromolluoromethone (S) o,o,o-Trieuorotoluene (S) 4Bromolluorobenzene LCSD Result mg/ LCS Rec. .% LCSD Rec. % Rec. Limits % 3.0.0251 98.0 100 77.9-116 0,0281 114 113 71.1-129 0,0232 90.4 92.8 81.6-120 0.0250 96.6 99.8 79.5-121 0.0291 115 117 49.1-157 0.0261 102 104 61.5-134 101 101 900-115 103 100 79.0-721 952 96.3 90.4-116 92.1 92.8 80.1-120 L812401-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) LCS OualiOer LCSD Oualifler RED RPD Limits % % 2.35 20 0.890 20 2,64 20 3.28 20 0.920 20 2.60 20 (OS) 01/17/16 01:13 - (MS) 01/17/16 0092 - (MSD) 01/17/16 00:32 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits MS Oualifler MSD Oualifler RPD RPD Limits Analyte mull mull mg/I mg/I % - % % % % Acrolein 0125 0.0103 T98 1.75 1570 1390 1 10.0-200 J5 JS 12.3 277 Acrylonitrile 0.125 0.00187 0.147 0.133 116 - 105 1 49.4-133 10.1 25.3 Benzene 0.0250 ND 0.0246 0,0239 98.5 95.6 1 58.6-133 3.04 20 Bromodichloromethane 0.0250 0.000453 0.0246 0.0245 96.5 96.1 1 69.2-127 0.380 20 Bromoform 0,0250 ND 0.0233 0.0226 93.1 90.5 1 66.3-140 2.77 20 Bromomethene 0,0250 ND 0.0294 0.0292 118 117 1 16.6-183 0.590 20.5 Carbon tetrachloride 0.025D ND 0,0239 0.0225 95.7 90.1 1 60.6-139 6,06 20 Chlorobenzen6 0.0250 ND 0.0214 0.0211 85.6 84.3 1 70.1-130 T53 20 Chlorodibromomethane 0.0250 ND 0.0224 0.0229 89.6 91.7 1 71.6-132 2AO 20 Chloroethane 0.0250 ND 0,0283 0.0282 113 113 1 33.3-155 0.350 20 2-Chloroethyl vinyl ether 0.125 ND 0.0728 0.0250 58.2 20.0 1 5.00-149 J3 97.6 40 Chloroform 6.0256 0.0228 0.0487 0,0465 104 94.8 1 66.1-133 4.58 20 Chloromethane 0.0250 0.000170 0,0244 0.0239 96.9 94.9 1 40.7-139 2.08 20 1,2-Dichlorobenzene 0,0250 ND 0.0233 0.0231 93.1 92.3 1 77A-127 0,770 20 1,3-Dichlorobenzene 0.0250 ND 0.0156 0.0141 62.4 56.2 1 67.9-136 J6 J6 10.3 20 1,4-Dichlorobenzene 0.0250 0.000360 0.0233 0.0233 91.6 91.9 1 74.4-123 0,320 20 Dichlorodifluoromethane 0.0250 ND 0.0295 0.0295 11B 118 1 42.2-146 0.0200 20 1,1-Dichloroethane 0.0250 ND 0.0257 0.0250 103 99.8 1 64.0-134 3.12 20 1,2-Dichloroethane 0.0250 ND 0.0272 0.0254 109 102 1 60.7-132 6.96 20 1,1-Dichloroethene 0.0250 ND 0.0275 0.0278 110 ill 1 48.8-144 1.25 20 FP �Tc 3Ss 4Cn 6Sr 2GI eAl aSc ACCOUNT: Eaton Corporation PROJECT: SDG: 28091-R L812515 DATE/TIME: 01/26/16 16:57 PAGE: 13 of 24 WG842965 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic,Compounds (GC/MS) by Method 624 L812515-01 L812401-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 01/17/16 01:13 •, (MS) 01/17/16 00:12 • (MSD) 01/17/16 00:32 k. r Spike Amount Original Result Analyte mg/I mgll MS Result mi MSD Result mg/I MS Rec. % MSD Rec, Dilution % Rec. Limits MS Qualifier % MSD Oualifier RPD % RPD Limits % trans-1,2-Dichloroethene &0250 ND 0.0250 0.0245 100 97.9 1 61.0-132 2.23 20 1,2-Dichloropropane 0.0250 0.00111 0.0234 0.0226 89.3 86.0 1 69.7-130 3,56 20 cis-1,3-Dichloropropene 0.0250 NO 0.0243 0,0239 97.1 95.5 1 71.1-129 1.68 20 trans-1,3-Dichloropropene 0,0250 0.000529 0.0250 0.0245 97.9 96.1 1 66.3-136 L87 20 Ethylbenzene 0,0250 0.00468 0.0226 0.0234 71.6 74.8 1 62.7-66 3.51 20 .Methylene Chloride 0.0250 0.000159 0.0238 0.0235 94.7 93A 1 6LS-125 1,41 20 1,1,2,2-Tetrachloroethane 0.0250 DOD502 0.0273 0.0284 89.1 93A 1 64.9-145 3.87 20 Tetrachlorcethene 0,0250 0.0641 0.0671 0.0839 11.8 79.2 1 57.4-141 J6 J3 22.3 20 Toluene 0,0250 0.0374 0.0552 0.0587 7L3 - 85.3 1 67.8-124 6.16 20 1,1,1-Trichloroethane 0,0250 ND O.0272 0.0263 109 105 1 58.7-134 3.35 20 1,1,2-Trichloroethane 0,0250 0.000665 0.0222 0.0224 86.1 86.8 1 _ 74.1-130 0.810 20 Trichloroethene 0,0250 ND 0.0227 0.0227 90.7 90.7 1 48.9-146 0.0500 20 Trichloro0uoromethane 0.0250 IND 0,0285 0,0287 114 115 1 39.9-165 0,600 20 .Vinyl chloride 0.0250 ND 0.0263 0.0257 105 103 1 44.3-143 2.24 20 (S) Toluene-d8 101 96.4 90.0-115 (S) Dibromolluoromethone 109 104 79.0-121 (S)a.a,o Trllluoro(oluene 90.7 869 90A-116 J2 (S)4-Bromolluorobenzene 82.9 79.5 80.1-120 J2 ACCOUNT: PROJECT: Eaton Corporation 2809I R SDG'. L812515 DATE/TIME'. 01/26/1616:57 PAGE: 14 of 24 WG842947 Pesticides (GC) by Method EPA 608 Method Blank (MB) (MB) 01/20/16 14:37 Aldrin Alpha BHC Beta BHC Della BHC Gamma BHC 4,4-DDD 4,4-DDE 4,4-DDT Dleldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Chlordane Toxaphene (S) Decochlorobiphenyl (S) 7etrachloro-m-xylene MB Result mg/I U U U U U U U __.. .. _U_.. _ U U U U U U U U U U U U 7L7 89.3 QUALITY CONTROL SUMMARY L812515-01 MB Qualifier MB MDL MB RDL mg/I mg/I 0.00000813 0,0000500 0.0000166 0,0000500 0.0000184 0.0000500 0.0000197 0.0000500 0.0000176 0.0000500 0.0000170 0.0000500 0.0000164 0.0000500 0.0000177 0.0000500 _ 0.00000751 0.0000500 0.0000179 0.0000500 0.0000176 0.0000500 0.0000196 0,0000500 0.0000189 0.0000500 0,0000142 0,0000500 0.0000170 0,0000500 0.0000108 0.0000500 0.0000175 0.0000500 0.0000134 0.0000500 0,0000193 0.0000500 0.0000977 0.000500 0.000168 0.000500 10.0-156 139-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/1614,12 • (LCSD) 01/20/1614:25 Spike Amount LCS Result A-1,,Ie .. mrdl -11 Aldrin Alpha BHC Beta BHC Delta BHC Gamma BHC 4,4-DDD 4 4-DDE - - 0.00100 0.000751 0,00100 0.000917 0,00100 0.000872 0.00100 0.000983 0.00100 0.000914 0.00100 _ 0.000885 0.00100 0.000836 LCSD Result mg/I LCS Rec. % LCSD Rec. % Rec. Limits LCS Oualifier % LCSD Ouallfler RPD % RPD Limits % 0.000567 75.1 56.7 10.0-120 27.9 33.9 0.000854 91.7 85.4 53,6-125 7.15 22.3 0.000825 87.2 82.5 55.8-130 5,62 20.6 0.000924 98.3 92.4 42.2-135 6.27 23.3 0.000855 91A 85.5 547-125 6.57 21.1 0.000814 88.5 81.4 47.6-144 8.42 24.3 0.000763 83.6 76.3 45.0-124 9.09 25.7 ONE LAB. NATIONWIDE. 0 ACCOUNT: PROJECT: SDG', Eaton Corporation 28091-R L812515 DATE/TIME: 01/26/1616:57 PAGE: 15 of 24 WG842947 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Pesticides (GC) by Method EPA 608 L812515-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/16 14:12 • (LCSD) 01/20/16 14:25 Spike Amount Analyte mgll LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rea. % Rea. Limits LCS Qualifier % LCSD Qualifier RPD % RPD Limits % 4,4-DDT 0.00100 0.000736 0.000673 73.6 67.3 49.8-130 9.92 25.4 Dieldrin 0.00100 0.000884 0.000819 88.4 81.9 55.0-127 Z60 22.9 Endosulfan 1 0.00100 0.000893 0,000827 89.3 82.7 54.7-127 774 24.3 Endosulfan II 0.00100 0.000886 0.000825 88.6 82.5 53.1-135 7.23 23.5 Endosulfan sulfate 0.00100 0.000911 0.000845 91.1 84.5 51.5-132 7,57 26.3 Endrin 0.00100 0.000865 0.000797 86.5 79.7 50.1-131 8.15 29.1 Endrin aldehyde 0.00100 0.000831 0.000760 63.1 76.0 39.5-137 8,89 28.4 Endrin ketone 0,00100 0.000876 0.000809 87.6 -80.9 53.5-139 7.88 28.4 Heptachlor 0.00100 0.000822 0.000627 82.2 62.7 20.7-127 27.0 30.5 Heptachlor epoxide 0.00100 0.000898 0.000830 Pad 83.0 56.4-124 7.90 23.1 Hexachlorobenzene 0.00100 0.000667 0.000526 66.7 52.6 26.7-114 23.6 27.6 Methoxychlor 0.00100 0,000824 0,000773 82.4 77.3 48.2-144 645 27.8 (S) Decochlorobiphenyl 722 64.5 100156 (S)Telrachloro-m-xylene 876 804 13.9137 Method Blank (MB) (MU) 012111b 12:bU Analyte MB Result mgll MB Qualifier MB MDL mg/I AB RDL mg/I PCB 1260 U 0,000120 0.000500 PCB 1016 U 0,000100 0.000500 PCB 1221 U 0.0000730 0.000500 '.PCB 1232 U 0.0000420 0.000500 PCB 1242 U 0.0000470 0.000500 .PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 (5) Decochlorobiphenyl 51.6 s 10.0456 (S) Telrochloro-m-�Ilene 876 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/21/16 13:03 - (LCSD) 01/21/16 13:15 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rea, Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/1 % % % % % PCB 1260 0,00250 0.00220 0.00218 88.1 87,1 47.7-149 1.09 28.8 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R - L812515 DATE/ IIAE: 01/26/16 16:57 PAGE: 16 of 24 WG842947 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Polychlorinated Biphenyls (GC) by Method EPA-608_ L812515-01 _ Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/21/16 13:03 • (LCSD) 01/21/1613:15 Spike Amount LCS Result PCB 1016 0,00250 0.00195 (5) Decorhlorobiphenyl (5) Tetrachloro.m-xylene LCSD Result LCS Rea. LCSD Rea. Rea. Limits LCS Oualifer mg/I % % % 0.00179 78.2 7L5 24.7-128 55.5 54.6 10.0-156 88.3 86.8 13 9-137 LCSD OuallOer RPD RPD Limits 8.95 34.9 L ACCOUNT: PROJECT: SEE: DATEMME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 17 of 24 WG843233 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625 L812515-01 Method Blank (MB) (MB) 01/20/1614:00 Analyte MB Result mg/I MB Oualifer MB MDL mg/I . MB RDL mgA Acenaphthene U 0.000316 0.00100 Acenaphthylene U 0.000309 0.00100 Anthracene U 0,000291 0,00100 Benzidine U 0.00432 0.0100 Benzo(a)anthracene U 0.0000975 0.00100 Benzo(b)fluoranthene U 0.0000896 0.00100 Benzo(k)fluoranthene U _ 0.000355 0.00100 :Benzo(g,h,i)perylene U 0.000161 0,00100 Benzo(a)pyrenIe U 0.000340 0.00100 Bis(2-chlorethoxy)methane U 0,000329 0.0100 Bis(2-chloroethyl)ether U 0.00162 0,0100 Bis(2-chloroisopropytether U 0.000445 0,0100 4-Bromo0enyl-phenylether U _ 0.000335 0.0100 2-Chloronaphthalene U 0,000330 0.00100 4-Chlorophenyl-phenylether U 0.000303 0.0100 Chrysene U 0.000332 0.00100 Dibenz(a,h)anthracene U 0.000279 0.00100 3,3-Dichlorobenzidine U 0,00202 0.0100 - 2,4-Dinitrotoluene U 0.00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 Fluorene _ U 0.000323 0.00100 Hexachlorobenzene U 0,000341 0.00100 Hexachloro-1,3-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0,00233 0.0100 Hexachloroethane U 0.000365 0.0100 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 'lsophorone U 0.000272 0.0100 Naphthalene U 0.000372 MOM Nitrobenzene U 0.000367 0.0100 n-Nitrosodimethylamine U 0.00126 0.0100 o-Nitrosodiphenylamine U 0000304 0.0100 1,2-Diphenylhydrazine U 0.000318 0.0100 n-Nitrosodi-n-propyla mine U 0.000403 0.0100 Phenanthrene U _ 0.000366 0,00100 Benzylburyl phthalate U 0.000275 0.00300 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L812515 DATEITIME: 01/26/1616:57 PAGE: 18 of 24 WG843233 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625 L812515-01 - Method Blank (MB) C (MB) 01/20/1614,00 MB Result MB Cualilier MB MDL MB REAL Analyte mg/I mg/I all Bis(2-ethylhexyI)phtha late 0.00109 0,000709 0.00300 Di-n-butyl phthalate 0.00100 0.000266 0.00300 ., Diethyl phthalate U 0.000282 0.00200 Dirri phthalate U 0.000283 0.00300 Di-n-octyl phthalate U 0.000278 0.00300 Pyrene U 0,000330 0.00100 1,24-Tnchlorobenzene U 0,000355 0,0100 4-Chlorci3 methylphenol U 0.000263 0,0100 2-Chlorophenol _ U 0.000283 0.0100 2,4-Dichlorophenol U 0.000284 0.0100 2 4-Dimethylphenol U 0.000624 0.0100 '4,6-6initro-2-methylphenol U 0,00262 0,0100 2 4-Dinitrophenol -_ U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 _ _ _ _ 4-Nitrophenol - _ _ _ U _ 0.00201 - _ 0.0100 IPentachlorophenol U 0.000313 0.0100 Phenol U 0,000234 0,0100 2,4,6-Trichlorophenol _ U - - 0.000297 _ - _ - 0.0100 (5) Nitrobenzene-d5 767 218-123 (S) 2-Fluoroblphenyl 79.7 29,5131 (5)p-Terphenyl-d14 102 293-137 (S) Phenol-d5 - 33,0 5.00-701 (5) 2-Fluorophencl 439 10.0-779 (S)1,Q6-Tribromophenol 62.8 112-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/1613.13 • (LCSD) 01/20/1613.36 Spike Amount LCS Result LCSD Result LCS Rec, LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgh mgh mg/I % % % % % Acenaphthene 0.0500 0.0403 0.0400 80.5 80.0 38.7-109 0.620 21.5 ____ _._._....._._ 'Ace--aphthylene _0_.. 0.0500 __.... 0.0385 _... 0.0409 76.9 81.8 36.0-106 6.10 _. 21 Anthracene 0,0500 0.0445 0,0447 89.0 89A 43.6-113 0.440 18.8 I,Benzidine 0.0500 0.0410 0.0423 82.0 84.6 10.0-165 3.14 40 Benzo(a)anthracene 0,0500 0.0521 0.0463 104 92.6 51.2-112 11.7 20 iBenzo(b)Fluoranthene 0.0500 0.0509 0.0540 102 108 4Z6-111 5.81 20 ACCOUNT: PROJECT: SDG'. DATE/TIME'. PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 19 of 24 WG843233 QUALITY CONTROL SUMMARY ONE LAD NATIONWIDE. Semi VolatileOrganicCompounds (GC/MS). by Method 625 L812515-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/1613.13 • (LCSD) 01/20/16 13,36 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I mg/I % % % Benzo(k)fluoranthene 0,0500 0.0392 0.0400 78.4 79.9 49.4-114 Benzo(g,L,,i)perylene 0.0560 0.0474 0.0489 94.8 97.7 45.2-117 Benzo(a)pyrene 0,0500 0.0483 0.0482 96.6 96.3 45.6-106 Bis(2-chlorethoxy)methane 0.0500 0.0365 0.0379 73.1 75.8 37.2-111 Bis(2-chloroethyl)ether 0,0500 0.0396 0.0367 79.3 73.5 22.6-108 :Bis(2-chloroisopropyl)ether 0. 0500 0.0362 0.0387 72.5 77.4 32.9-100 4-Bromophenyl-phenylether 0.0500 0.0453 004SO 90.7 90.0 40.7-116 2-Chloronaphthalene 0.0500 0.0427 0.0399 85.4 79.9 33.6-105 4-Chlorophenyl-phenylether 0.0500 0.0407 0.0432 81.4 86.3 39.0-113 . .L2-Diphenylhydrazine 0.0500 0.0449 0.0480 89.8 961 37.6-111 Chesene 0.0500 0.0431 0,0437 81 87.4 54,6-120 IDibenz(a,h)anthracene 0.0500 0.0495 0.0460 99.0 91.9 42.8-118 3,3-Dichlorobenzidine 0,0500 0.0419 0.0436 83.8 87.2 27.2-142 �2,4-Dmitrotoiil 0.0500 0.0446 0.0464 892 92.9 372-105 2,6-Dinitrotoluene 00500 0.0462 10.0409 92.4 81.8 30.6-106 Fluoranthene 00500 0.0452 0.0477 90.4 95A 45.9-115 Fluorene 0.0500 0.0446 0.0449 89.2 897 41.0-112 jHexachlorobenzcne 0,0500 6.0479 0.0443 91 88.6 38.5-116 Hexachloro-1,3-butadiene 0,0500 0,0357 0.0339 71.4 67.7 16.1-104 1Hexachlorocyclopentadiene 0,0500 0.0183 0.0206 36.6 412 10.0-121 Hexachloroethane 0.0500 0.0356 0.0340 71.3 68.0 16.5-89.8 lndeno(1,2,3-cd)pyrene 0.0500 0.0484 0,0465 96.7 93.0 45.0-116 sophorone 0.0500 0.0488 0,0439 97.6 87.7 354-112 ,Naphthalene 0.0500 0.0382 0,0369 76.4 73.7 32.2-101 Nitrobenzene 0.0500 0.0415 0,0413 83.0 82.6 31.4-106 :n-Nitrosodimethylamine 0,0500 0.0286 0,0240 57.2 48.1 10.0-80.1 n-Nitrosodiphenylamine 0.0500 0.0413 0,0433 82.7 86.6 44.4-113 n-Nitrosodi-n-propyla mine 0.0500 0.0409 0,0432 81.9 86.3 33.2-106 Phenanthrene 0.0500 0.0438 0.0414 87.6 82.8 46.4-113 .Benzylbutyl phthalate 0.0500 0,0411 0.0435 82.2 86.9 31.8-123 Bis(2-ethylhexypphthalate 0.0500 0,0454 0.0437 90.8 87.4 36.9-134 Di-n-butyl phthalate 0,0500 0.0400 0.0423 80.0 84.6 41.8-120 Diethyl phthalate 0,0500 0.0576 0.0490 115 98.0 36.5-129 iDimethyl phthalate 0,0500 0.0448 0.0420 89.5 83.9 35.3-128 LCSD Qualifier RPD RPD Limits 1,88 20 3.07 20 0,240 20 3.62 24.1 - 7.61 27.9 - - 1 25.1 0720 21 23 - _673 594 20.9 - 6.70 21.1 1,30 20 7.36 20 3.88 22.3 4.06 22 . - .. .. 12.2 231 5.39 - - 20 _ 0 590 20.2 786 20.1 5.36 312 -_ 11.8 27.9 4.62 30.7 - 3.97 - - 20 10.7 21.5 3,52 - - - 23.8 0.460 25.7 - 17.3 37.5 4.67 . 20 _ - 1 23.7 5,58 20 _ 5.64 20.7 3.83 23.6 5.56 20.2 161 20 646 20.8 Di-n-octyl phthalate 0.0500 0.0527 0.0417 105 83.4 39.7-112 J3 23.3 21.1 Pyrene 0,0500 0,0580 0.0500 116 100 46.3-117 14.7 20 t` ACCOUNT: PROJECT: SDG'. DATE/TIME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 20 of 24 WG843233 QUALITY CONTROL SUMMARY - Semi Volatile Organic. Compounds (GC/MS).by Method 625 L812515.01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 01/20/1613:13 • (LCSD) 01/2011613:36 w Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/l mg11 mg/I % % % % % 1,2,4-Trichlorobenzene 0.0500 0.0356 0.0347 71.3 -,69.4 22.9-96.1 2.61 27.5 4-Chloro-3-methylphenol 0.0500 0.0411 0.0433 82.2 86.6 35.7-100 5.25 22.9 2-Chlorophenol 0.0500 '0.0331 0.0342 66.1 68.3 26.2-91.5 3.27 26.5 2,4-Dlchlorophenol 0.0500 0.0371 0.0396 74.3 79.2 31.4-103 6,44 24.9 2,4-Dimethylphenol 0.0500 0,0392 0.0411 78.4 82.2 31.9-107 4.67 25.7 4,6-Dinitro-2-methylphenol 0,0500 0.0321 0,0277 64.3 55.5 18.4-148 147 24.4 2,4-Dinitrophenol 0,0500 0,0181 0.0132 36.1 26.4 24.2-128 J3 31.3 20.5 2-Nitrophenol 0.0500 0.0366 0.0386 73.1 77.2 25.9-106 5.34 26.9 4-Nitrophenol 0.0500 0.0159 0.0141 31.7 28.1 10.0-52.7 12.0 40 Pentachlorophenol 0.0500 0.0349 0,0353 69.9 70.5 10.9-97.4 0.950 35.1 Phenol 0.0500 0,0179 0.0188 35.8 37.7 10.0-57.9 5.01 35 2,4,6-Trichlorophenol 0.0500 0.0348 0.0369 69.6 73.7 29.8-107 5.77 24.1 (S) Nitrobenzene-d5 742 90.6 218.123 (S)2-Fluorobiphenyl - _ 71.5 74.1 29.5-131 _ (S)p-Terphenyl-d14 95.8 96.9 29.3-137 (S)Phenol-d5 33.6 359 15. 00-70.1 (S)2-Fluomphenol 46.0 439 10.077.9 (S)2,4,6-Tribromophenol 73.3 76,0 11.2-130 ONE LAB, NATIONWIDE. ACCOUNT: PROJECT: SDG: DATErTIME: PAGE: Eaton Corporation 28091-R L812515 01/26/161&57 21 of 24 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. Cp MDL RDL Method Detection Limit. _ Reported Detection Limit. ETC ND,U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. 3S5 (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) aCn from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control s Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring Sr recovery. Surrogates are not expected to be detected in all environmental media. Rec. Recovery. e SDL Sample Detection Limit. -- QC MQL Methodtedtod Limit. Unadj. MOIL UnadjustedMethod Ouantitation Limit. Qualifier Description qAl J The identification of the analyte is acceptable, the reported value is an estimate. s J2 Surrogate recovery limits have been exceeded, values are outside lower control limits. Sc J3 The associated batch OC was outside the established quality control range for precision. J4 The associated batch OC was outside the established quality control range for accuracy_. J5 The sample matrix interfered with the ability to make any accurate determination, Spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L812515 01/26/1616:57 22 of 24 ACCREDITATIONS & LOCATIONS ONE LAB NATIONWIDE. E$C gab Sciences is the only environmental laboratory accredited/cergfied to support your work nationwide from one location. One phone call, one point of conact. one laboratory. No ether tab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the ' network laboratories in our Industry. The most significant benefit to our 'one location' design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination. thus protecting sample integrity. Our focus on premium quality and prompt seMce allows us to be YOUR LAB OF CHOICE. 'Not all ce ulcaOans held by the laboratory are applicable to the results reported in the attached report. z State Accreditations TC —------------- • Alabama -- 40660 -- — - ---- --- Nevada _ _ _ _ _ _ — ----- ----------- _ TN-03-2002-34 3S5 Alaska _ UST-080 _ New Hampshire 2975 Arizona AZ0612 New Jersey NELAP TNO02 _ Arkansas ---_ _ 88-0469 _ _ _ _ New Mexico - -- _ TN00003 -- - ° CD California_ —_ 07157CA _ New Yark-- 11742 Colorado TN00003 North Carolina Env375 Conneticut PH-0197 North Carol ina' DW21704_ Sr _ _ _ _ _ E87487 North Carolina 41 _Florida North Dakota----- Georgia' 923 Ohio-VAP CL0069_ CLOO Idaho — _ _ TN 00003 Oklahoma — _ 9915 _ Illinois 200008 _ Oregon 02- _ _ Indiana C-TN-01 lva Pennsy nia 68-02979 68-029 _ Iowa 364 Rhode Island _ _ 221 _ _ Kansas _ — E-10277 South Carolina 84004 Kentucky' _ _ _ 90010 7 South Dakota nla Kentucky' 16 Tennessee" 2006 _ _. Louisiana _ — A130792 Texas T104704245-07-TX y Maine TN0002 Texas _ _ _ _ _ _ LA80152 _ _ _ _ Maryland _ ___ __ __ ____ _ __ 324 _ _ _ Utah _ _ _ _ _ _ 6157585858 Massachusetts M-TNO03 Vermont — VT2006 Michigan 9958 Virginia 109 Minnesota 047-999-395 Washington _ _ C1915 _ Mississippi__ _ ___ __ TNO0.0.03 _ West Virginia__ _ 233 _ _ Missouri 340 W_sconsin 9980939910 Montana —�- CERT0086 Wyoming_ A2LA Nebraska _ _ NE-OS-15_-05 Third Party & Federal Accreditations A2LA-ISO 17025 1461.01 AIHA 100789 EA - 1SO 170255 14fi1.02 __ DOD 1461,01- Canada 1461.01_ - _ _ _ _ USDA _ SS-67674 EPA-Crypto --_ TN00003 __._._ — `Drinking Water r Underground Storage Tanks ' Aquatic Toxicity ' ChemicallMicroblological ° Mold "- Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup anchor the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. T \^IA MT ND ♦ ^1 N.E OR µN T 'D SD T V.'I NY • v+Y � T.n • NL IT T • PF T NV ♦ L '� T u CO ♦ KS VAT' T T M KY ♦ T �•Q N i T •A2 Nh1 OT Art SC T • j1.5 AL GA • IX ♦ ♦ LA T •-�-T � AK • Ir, T T • ♦ ♦ • Q 0 �05� FL • � �u .. HI ACCOUNT: PROJECT: SDG: DATE/rIME: PAGE: Eaton Corporation 28091-R L812515 01/2611616:57 23 of 24 •rW� ESC ANALYTICAL REPORT m ESC L.,.a s.�.,.E.N . E.s ��� December 29, 2015 MM Eaton Corporation Sample Delivery Group: L808032 Samples Received: 12/18/2015 Project Number: 28091-R Description: Eaton Corp Semi -Annual Stormwater �® Site: ROXBORO, NC Report To: Dustin LaClair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: Jason Romer Technical Service Representative Results relate onlyto the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302. 060303. and 060304. M TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cover Page 'Tc: Table of Contents 'Ss: Sample Summary `Cn: Case Narrative 5Sr: Sample Results 2015-12-17-005 TOOL ROOM TRENCH L808032-01 'Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 Volatile Organic Compounds (GC/MS) by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 'Gl: Glossary of Terms sAl: Accreditations & Locations 'Sc: Chain of Custody 1 tCp 2 3 3 4 SS 5 5 FCn 8 Fr 8 9 fiQC 10 GI 11 15 EAI 16 17 9Sc 21 22 23 ACCOUNT: PROJECT: sDG DATE/TIME: PAGE: Eaton Corporation 28091-R J808032 12/29/15 17:03 2 of 23 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received datehime 2615-12-17-005 TOOL ROOM TRENCH L808032-01 WW Kirk Spicer 12/17/1507:00 12/18/1509:00 C P Method Batch Dilution Preparation Analysis Analyst date/time date/time FT, Gravimetric Analysis by Method 2540 D-2011 WG837411 1 12/2211510:22 12/22/151102 JER Metals(ICP) by Method 2007 WG837604 1 12/2311510.16 12/24/1516:12 WBD Pesticides (GC) by Method EPA 608 WG837190 1 12/21/15 07:39 12/23/1519:49 LKD Polychlorinated Biphenyls (GC) by Method EPA-608 VIG837190 1 12/21/15 07:39 12/24/1514:20 EGR Semi Volatile Organic Compounds(GC/MS) by Method 625 WG837944 1 12/23/1516:20 12/24/1519.30 JF Cn Volatile Organic Compounds (GC/MS( by Method 624 WG834853 1 12/19/1517:34 12119/1517:34 ACG Wet Chemistry by Method 1664A WG838260 1 12/24/1507:49 12124/1515:03 JIM Fr 6QC TGI BAI 9Sc n v ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L809032 12/29/151703 3 of 23 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the C p appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the ITC] analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my 3S5 digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. SSr FOCI FGI Jason Romer r.-- Technical Service Representative ASc N ACCOUNT: PROJECT: SDGDATEMME: PAGE: Eaton Corporallon 28091-R L808032 12/29/15IT03 4 of 23 2015-12-17-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 12/17/15 07:00 L808032 Additional Information Result Units Cp Analyte pH (On Site) 7.3 su TC Flow Measure 13.4 Deg. C 3Ss Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch Cn Analyte moll mg/I mgll date/time Suspended Solids 7,60 0.350 2.50 1 12/22/201511:02 WG837411 Wet Chemistry by Method 1664A 6 Result Ouarfler MDL RDL Dilution Analysis Batch QC Analyte al all mg/I date/time TPH- Oil&Grease 0.737 J 0.725 5.26 1 1224201515:03 WG838260 7GI Metals (ICP) by Method 200.7 eAl Result Qualifier MDL ROL Dilution Analysis Batch 9 Analyte mg/I hill moll date/time Copper 0.0189 0.00700 0,0100 1 1224201516:12 WG837604 SC Lead U 0.00200 0.00500 1 12/24/201516:12 WG837604 Zinc 0.0317 J 0.00340 0.0500 1 12124/201516:12 WG837604 Volatile Organic Compounds (GC/MS) by Method 624 Result Qualifier MDL RDL Dilution Analysis Batch Analyle mg/I moll mg/I date/time Acrolein U 0.00887 0.0500 1 12119/201517:34 WG834853 Acrylonitrile U 0.00187 0.0100 1 12119/201517:34 WG834853 Benzene U 0.000331 0.00100 1 12119/201517.34 WG834853 Bromodichloromethane U 0.000380 0.00100 1 19J79/201517:34 WG834853 Bromoform U 0.000469 0.00100 1 12119/201517:34 WG834853 Bromomethane Ll 0.000866 0.00500 1 12JI91201517:34 WG834853 Carbon tetrachloride U 0.000379 0.00100 1 121191201517:34 WG834853 Chlorobenzene U 0,000348 0.00100 1 121191201517:34 WG834853 Chlorodibromomethane U 0,000327 0.00100 1 121191201517:34 WG834853 Chloroemane U 0.000453 0.00500 1 12119/201517:34 WG834853 2-Chloroethyl vinyl ether U J4 0,00301 0,0500 1 l21l9i201517:34 WG834853 chloroform U 0.000324 0.00500 1 1D19/201517:34 WG834853 Chloromethane U 0,000276 0,00250 1 12/19/201517:34 VIG834853 1,2-Dichlorobenzene U 0.000349 0,00100 1 12/19201517:34 WG834853 ' 1,3-Dichlorobenzene U 0.000220 0,00100 1 12119/201517:34 WG834853 1,4-Dichlorobenzene U 6,000274 0,00100 1 QP9/201517:34 WG834853 DIChI0rodlilUoromelhdne U 0.000551 0,00500 1 12/191201517:34 WG834853 'LI Dichloroethane U 0.000259 OD0100 1 12119/2015 17:34 WG834853 1,2-Dichloroethane U 0DC0361 0.00100 1 12/19/2015 17:34 WG834853 1,f Dichloroethene U 0.000398 0.00100 1 12119/2015 17:34 VIG834853 trans-1,2-Dichloroethene U 0.000396 0.00100 1 12/19/201517:34 WG834853 �1,2-Dichloropropane U 0.006306 oDo100 1 12/19/201; 17.34 WG834853 cis-1,3-Dichloropropene U 0.000418 0.00100 1 12/19/201517:34 N/G834853 trans-1,3-Dichloropropene U 0.000419 0.00100 1 12/19/2015 17:34 WG834853 Ethylbenzene U 0.000384 0.00100 1 12/191201517:34 WG834853 Methylene Chloride U 0.00100 0.00500 1 1211912201517:34 WG834853 1,1,2,2-Tetrachloroethane U 0000130 0.06100 1 12/19/201517:34 WG834853 Tetrachloroethene U 0.000372 0.06100 1 12/19/2015 17:34 WG834853 _ Toluene U 0.001 0780 0.00500 1 12I19201517:34 WG834853 ,1,11-Trichloroethane U 0.000319 0.00100 1 12119/201517:34 WG834853 1.1.2-Trichloroethane U 0-Doo83 0.00100 1 12119/201517:34 WG834853 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L808032 12/2911517:03 5 of 23 2015-12-17-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 Collected date/time: 12/17/15 07:00 LE08032 Volatile Organic Compounds (GC/MS) by Method 624 ONE LAB. NATIONWIDE. Result Qualifier MDL RDL Dilution Analysis Batch Analyte mgA m04 mgA date/time Trichloroemene U 0.000398 0.00100 1 12119/201517:34 WG834853 Trichlorofluoromethane U 0.00120 0.00500 1 12/19/201517:34 WG834853 Vinyl chloride U 0,000259 0.00100 1 12/19/2015 17:34 WG834853 (S) Toluene-d8 103 90.0415 12179120151734 WG834853 (S) Dibromoluoromethone 105 79.0-121 12179QO151734 WG834853 (S)0,,a,0- Trihunrotoluene 104 9,9A-116 72179.201517.34 WG834853 /S)4-Bromolluorobenzene 79.7 J2 80.1-110 1217912015 17 34 WG834853 Pesticides (GC) by Method EPA 608 Analyze Result mgA Qualifier MDL mgA RDL mgn Dilution Analysis date/time Batch Aldrin U 0.00000813 0.0000500 1 12/23/201519:49 WG837190 Alpha BHC U 0.0000166 0.0000500 1 12/23/201519:49 WG837190 Beta BHC U 0.0000184 0.0000500 1 12/23/201519:49 WG837190 DeltaBHC U 0.0000197 0.0000500 1 12/23/20151!1.49 WG837190 Gamma BHC U 0,0000176 0.0000500 1 12123201519:49 WG837190 'Chlordane U 0.0000977 0.000560 1 12/231201519.49 WG837190 4,4-DDD U 0.0000170 0.0000500 1 12/23/201519:49 VIG837190 4,4-DDE U 0.0000164 0.0000500 1 121231201519:49 WG837190 4,4-DDT U 0.0000177 0.0000500 1 12/23/201519:49 WG837190 Dieldrin U 0.00000751 0.0000500 1 12/231201519:49 WG837190 Endosulfan I U 0,0000179 0.0000500 1 12/231201519:49 WG837190 Endosulfan ll U 0.0000176 0.0000500 1 12/23/20151949 WG837190 Endosulfan sulfate U 0.0000196 0.0000500 1 12/23/201519:49 VIG837190 Endrin U 0.0000189 0.0000500 1 12/23/201519:49 WG837190 Endrin aldehyde U 0.6000142 0.0000500 1 12/23/201519:49 WG837190 Endrin ketone U 0,0000170 0.0000500 1 12/23/201519:49 WG837190 Heptachlor U 0.0000108 0.0600500 1 12/23/2015 19:49 WG837190 Heptachlor epoxide U 0.0000175 6.0000500 1 12/23/201519:49 WG837190 Hexachlorobenzene U 0,0000134 :0.0000500 1 12/23/20151949 WG837190 Methoxychlor U 0,0000193 0.0000500 1 12/23/201516:49 WG837190 Toxaphene U 0.000168 0.000500 1 12/23/201519:49 VIG837190 (S) Decochlorobiphenyl 149 10,0-156 121231201519,49 WG837190 (S) Telrochloro-m-*ene 132 139437 121231201519.49 WG837190 Polychlorinated Biphenyls (GC) by Method EPA-608 Analyze Result mgA Qualifier MOL mgA RDL mg/I Dilution Analysis date/time Batch PCB 1016 U 0,000100 0.000500 1 12/24/201514:20 WG837190 PCB 1221 U 0,0000730 0.000500 1 12/24/201514:20 VIG837190 PCB 1232 U 0,0000420 0.000500 1 12/24/201514:20 WG837190 PCB 1242 U 0.0000470 0.000500 1 12/24/201514:20 WG837190 ' PCB 124E U 0,0000860 0.000500 1 12/24/201514:20 WG837190 PCB 1254 U 0.0000470 0.000506 1 12/24/201514:20 WG837190 PCB 1260 U 0000120 0.000500 1 12/241201514:20 WG837190 Semi Volatile Organic Compounds (GC/MS) by Method 625 Analyte Result i g/I Qualifier MDL hod RDL mg/I Dilution Analysis date / lime Balch Acenaphthene U 0.000316 0.00100 1 12/24/201519:30 WG837944 Acenaphlhylene U 0.000309 0.00100 1 12/24/201519:30 WG837944 Anthracene U 0.000291 000100 1 12/24/201519:30 WG837944 Benzin ine U 0.60432 0.0100 1 12/241201519.30 WG837944 Benzo(a)anthracene U 0.0000975 0,00100 1 12/24/2015 19.30 WG837944 Benzo(b)fluoranthene U 0.0000896 0.00100 1 12/2412015 19.30 WG837944 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L808032 12/29/1517:03 6 of 23 2015-12-17-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dateltime: 12/17/15 07:00 L808032 Semi Volatile Organic Compounds (GC/MS) by Method 625 1 Analyte Result mgn ouali8er MDL ni RDL mgfl Dilution Analysis date/time Batch Gp Benzolklfluoranthene U 0.000355 0.00100 1 12/24/201519:30 WG837944 z Tc Benzo(g,h,l)peryiene U 0.000161 0.00100 1 12/241201519:30 WG837944 Benzolalpyrene U 0.000340 0.00100 1 12/24201519:30 WG837944 3 Bisi2-chlorethoxyimethane U 0.000329 0.0100 1 12/24/201519:30 WG837944 $S Bis(2-chloroethyl)ether U 0.00162 0,0100 1 12/24201519:30 WG837944 Bisl2-chioroisopropyllether U 0.000445 0,0100 1 12/24/201519:30 WG837944 ° Cn 4 Bromophenyl-phenylether U 0,000335 0.0100 1 12/24/201519:36 WG837944 2-Chloronaphthalene U 0,000330 0.00100 1 12/24/201519:30 WG837944 4-6hlorophenyl-phenylether U 0.000303 0.0100 1 12/24/201519:30 WG837944 Chrysene U 0.600332 0.00100 1 12/241201519:36 WG837944 Dibenz(a,h)anthracene U 0.000279 0.00100 1 12124/201519:30 WG837944 a QC 3,3-Dichlorobenzidine U 0.00202 0.0100 1 12/241261519:30 WG837944 2,4-Dinitrotoluene U 0.00165 0.0100 1 12/24/201519:30 WG837944 7GI 2,6-Dinitrotoluene U 0.000279 0,0100 1 12/241201519:30 WG837944 1 2-Diphenylhydrazine U 0.000318 0,0100 1 12/24/201519:30 WG837944 Fluoranthene U 0.000310 0.00100 1 12/24/201519:30 WG837944 eAl Flumene U OA00323 0,00100 1 12/24/201519:30 WG837944 Hexachlorobenzene U 0.000341 0.00100 1 12/24/201519:30 WG837944 y Hexachloro-1,3-butadiene U OA00329 0.0100 1 12/24/201519:30 VIG637944 $C Hexachlarocyclopentadiene U 0.00233 0.0100 1 12/24/201519:30 WG837944 Hexachloroethane U 0.000365 0.0100 1 12/24/201519:30 WG837944 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 12/24201519:30 WG837944 Isophorone U 0.000272 0.0100 1 12/24/201519:30 WG837944 Naphthalene U 0.000372 0.00100 1 12124201519:30 WG837944 Nitrobenzene U 0.000367 0.0100 1 12/24/201519:30 WG837944 n-Nitrosodimethylamine U 0,00126 00100 1 12/24/201519:30 WG837944 n-Nitrasodiphenylamine U 0.000304 00100 1 121241201519:30 WG837944 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 12724201519:30 VIG837944 Phenanthrene U 0.000366 0,00100 1 12/24/201519:30 VIG837944 Benzylbutyl phthalate U 0.000275 0.06300 1 12124201519:30 WG837944 Bis(2-ethylhexypphthalate U 0.000709 0,00300 1 12124/201519:30 WG837944 Di-n-butyl phthalate U 0.000266 0,00300 1 12/24/201519:30 VIG837944 Diethyl phthalate U 0.000282 0.00300 1 121241201519:30 VIG837944 Dimethyl phthalate U 0.000283 0.00300 1 12/24/201519:30 VIG837944 DI-n-octyl phthalate U 0.000278 000300 1 12/24/201519:30 WG837944 , Pyrene U 0.000330 0.00100 1 12124201519:30 WG837944 1,2A Trichlorobenzene U 0,000355 0,0100 1 12124/201519:30 WG837944 4-Chloro-3-methylphenol U 0.000263 0.0106 1 1224201519:30 WG837944 2-Chlorophenol U 0.000283 0.0100 1 12124201519:30 VIG837944 __ n a.. 2,4-Dichloiophenol U 0,000284 0,0100 1 12124/201519:30 WG837944 2,4-Dimethylphenol U 0.000624 0,0100 1 IM4201519:30 VIG837944 4,6-Dinitro-2-methylphenol U 0.00262 0.01o0 1 12/24201519:30 WG837944 2,4-Dinitrophenol U 0,00325 0,0100 1 12/24/201519:30 WG837944 2-Nitrophenol U o.000320 0.0100 1 1224/201519:30 WG837944 4-Nitrophenol U 0.00201 0.0100 1 12/24/201519:30 WG837944 Pentachlorophenol U - 0.000313 0.0100 1 12/24/201519:30 WG837944 Phenol U 0,000334 0.0100 1 12/24/201519:30 WG837944 24,6-Trichlorophenol U 0.000297 0.0100 1 12/24/201519:30 WG837944 /SI2-FRrorophenol 52.2 10.0-7Z9 121241202519:30 WG837944 (S)Pherri 36.3 500-70.1 121,,001519.30 WG837944 (S) Nitrobenzene-6 843 21.8-123 12724/291519:30 WG837944 (S) 2-Fluorobiphenyl 80.1 29.5-131 1272420151930 WG837944 (5) 2.46-Tribromophenol 92.5 112-130 121241201511 WG837944 w (S)p-Terphenyl-d14 90.4 293-137, _ 12/24/201519.30 WG837944 ,wj ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L808032 12/29/151703 7of23 r , WG837411 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. _Gravimetrlc Analysis by Method 2540 D-2011- LBOBD32-01 Method Blank (MB) (MB) 12/22/1511:02 CP MB Result MB Qualifier MB MDL Analyte mg/I mg/I MB RDL mg4 TC Suspended Solids U 0.350 2,50 aSs, L8O8O31-02 Original Sample (OS) • Duplicate (DUP) (0S)12/22/15 11:02 • (DUP) 12/22/15 11:02 Cn Original Result DUP Result Dilution DUPRPD DUP Qualifier DUP RPD Limits Analyze mg/l mg/I % % s Sr Suspended Solids 183 180 1 T34 5 Laboratory Control Sample (LCS) •Laboratory Control Sample Duplicate (LCSD) 7 (LCS)12/22/15 11:02 • (LCSD)12/22/15 11:02 G Spike Amount LCS Result LCSD Result LCS Red. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % BA Suspended ds So 773 852 888 110 115 85.0-115 414 5 aSc k ACCOUNT: PROJECT: SDG DATE/TIME: PAGE: Eaton Corporation 28091-R L808032 12/2911517.03 8 of 23 WG838260 QUALITY CONTROL SUMMARY Wet Chemistry by Method 1664A _ _ LBOBD32-01 Method Blank (MB) (MB) 12/24/1514:59 t MB Result MB OualiRer MIIMDL MB RDL Analyze mg/I r ll mg4 TPH - Oil & Grease u 0.725 5.00 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/24/1515:00 - (LCSD)12/24/15 15:00 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rea. Limits LCS Oualifer LCSD Oualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % TPH - 0il & Grease MO 16.5 18.2 82.5 91,0 78.0-114 9.80 18 3' ONE LAB. NATIONWIDE, 1Cp 2Tc aSs 4Cn s$r �GI BAI eSc ACCOUNT: PROJECT: SDG'. DATE/TIME: PAGE: Eaton Corporation 28091-R L808032 12/29/1517:03 9 of 23 WG837604 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICP) by Method 200.7 L808032.01 Method Blank (MB) (MB) 12/24/1514:43 " Cp Analyte ME Result mg/I MB Qualifier MB MDL mg/I MB RDL mg/I TC Copper U 0.007 0.0100 Lead U 0.002 0.00500 a -11 Zinc U � 0.0034 0.0500 ' SS Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)12/24/15 14:45 • (LCSD)12/24/15 14:46 Spike Amount LCS Result LCSD Result LCS Rec. LCSD per. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I rri % % % % % Copper 1.00 1.02 1.02 102 102 85-115 0 20 Lead LOO 1,00 1.01 100 101 85-115 1 20 Zinc 1.00 1.00 1.01 100 101 85-115 0 20 L807837-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12/24/1514:51 • (MS) 12/24/15 14.57 • (MSD) 12/24/1515:00 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mgp mg/I mg/I % % % % % Copper f 1.00 0.00734 1.03 1.04 102 104 1 75-125 1 20 Lead ' 1.00 0.000729 t01 1.02 101 102 1 75-125 1 20 Zinc 1.00 0.00182 1,01 1.02 101 102 1 75-125 1 20 L808007-01 Original Sample (OS) - Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12./24/1516:03 • (MS) 12/24/1516:06 • (MSD) 12/24/1516:09 Spike Amount Original Result MS Result MSD Result MS Rec MSD per. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte li mg/I mg/I mg/I % % % % % Copper 1.00 0.0143 1.05 L02 104 101 1 75-125 3 20 .Lead 1.00 ND 1.04 1.02 104 102 1 75-125 2 20 Zinc 1.00 0.00990 L04 1. Lot 103 106 1 75-125 2 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L809032 12/29/1517:03 10 o123 1 v €' WG834853 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 L808032-01 Method Blank (MB) (MB)12119/15 09.56 Analyze MB Result my/I MB Qualifier MB MDL tri MB RDL all Acrolein U 0,00887 0.0500 'Acrylonitrile U 0.00187 0,0100 Benzene e- U 0.000331 0.00100 �Bromodichloroniethane U 0.D00380 0.00100 Bromo(orm U 0.000469 0.00100 Bromomethane U 0.000866 0,00500 Carbon tetrachloride U 0.000379 0.00100 Chlorobenzene U 0.000348 0.00100 Chlorodibromomethone U 0,000327 0.00100 Chloroethane _ _U 0.000453 0.00500 2-Chloroethyl vinyl ether _ U 0.00301 0.0500 Chloroform U 0.000324 0.00500 Chloromethane U 0,000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 6-Dichlorobenzene U 0.000220 0.00100 1,4-Dichlorobenzene U 0,000274 0.00100 Dichlorodifluoromethane U 0.000551 0.00500 .1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene_ U 0.000398 0.00100 trans-1,2-Dichloroethene U 0,000396 _ 0,00100 L2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0,000419 0.00100 Bthylbenzene U _ 0.000384 0.00100 'Methylene Chloride U 0.00100 0.00500 _ 1,1,2,2-Tetrachloroethane U OA00130 0.00100 Tetrachloroethene U 0.000372 Toluene U _ _ 0.000780 _0.00100 _ 0.00500 1,1,1-Trichloroethane U _ 0,000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorcfluoromethane U 0.00120 0,00500 Vinyl chloride U 0.000259 0,00100 Q Toluene-d8 104 90.0.115 (S) Dibromofluoromefhone, 103 79.0-121 ACCOUNT: PROJECT: SOG: Eaton Corporation 28091-R L808032 DATE/TIME 12/29/1517:03 PAGE: 11 of 23 WG834853 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, volatile Organic Compounds_(GC/MS) by Method 624 L808032-01 Method Blank (MB) (MB)12/19/15 09:56 MB Result MB Qualifier MB MDL MB RDL Analyte mgh mg/I mg/I (si o,o,o-Trilluorotoluene 105 90.4-116 /5/4-8romo/lugrobenzene 81.2 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/19/15 08:45 - (LCSD) 12/19/15 09:04 Spike Amount Analyte mg/I LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rec. % Rec. Limits LCS Qualifier % LCSD Qualifier RPD % RPD Limits % Acrolein 0.125 0,119 0,118 95.3 94.4 88.0-118 0,860 28.1 Acrylonitrile 0.125 0.140 0.140 112 112 71.0-135 0,0600 20 Benzene 0.0250 0.0251 0.0253 100 101 73.0-122 0,970 20 Bromodichloromethane 0,0250 0.0260 0.0267 104 107 75.5-121 2.36 20 Bromoform 0.0250 0,0268 0.0281 107 112 71.5-131 4.69 20 Bromomethane 0.0250 0.0261 0.0252 105 101 22.4-187 3.52 20 Carbon tetrachloride 0.0250 0.0274 0.0272 109 109 70.9-129 0.780 2.0 Chlorobenzene 0.0250 0.0239 0.0252 95.5 101 79.7-122 5A7 20 Chlorodibromomethane 0.0250 0,0252 0.0267 101 107 78.2-124 5.69 20 'Chloroethane 0.0250 0.0222 0.0215 88.9 86.0 4T2-153 3.41 20 2-Chloroethyl vinyl ether 0.125 0.429 0.409 343 328 23.4-162 J4 J4 4.70 23.5 ;Chloroform 0.0250 0.0256 0.0255 103 102 73.2-125 0.640 20 Chloromethane 0.0250 0.0271 0.0261 108 104 55.8-134 - 3.76 20 1,2-Dichlorobenzene 0.0250 0.0257 0,0256 103 102 84.7-118 0.200 20 I.3-Dichlorobenzene 0,0250 0.0239 0.0249 95.7 99.5 _ 77.6-127 3,99 20 1,4-Dichlorobenzene 0.0250 0.0238 0.0242 95.1 96.9 82.2-114 T88 20 Dichlorodifluoiomethane 0.0250 0.0223 .0.0223 ' 89A 89.0 56.0-134 0.360 20 1,1-Dichloroethane 0.0250 0.0259 `OJ0261 104 105 71.7-127 0.860 20 1,2-Dichloroethane 0.0250 0.0231 0.0229 92.6 91.5 65.3-126 1.23 20 1,1-Dichloroethene 0.0250 0.0217 0.0220 86.8 88.0 59.9-137 1.32 20 trans-1,2-Dichloroethene 0.0250 0.0244 0.0243 97.6 -97A 72.6-125 0,230 20 ;1,2-Dichloropropane 0.0250 0.0282 0.0286" 113 114 77.4-125 1.37 20 cis-1,3-Dichloropropene 0.0250 0,0282 0.0283 113 113 77.7-124 0.570 20 trans-13-Dichloropropene 0,0250 0.0266 0,0285 106 114 73.5-127 7.01 20 Ethylbenzene 0.0250 0.0232 0.0251 92.9 100 80.9-121 7,72 20 Methylene Chloride 0.0250 0.0216 0.0221 86.5 88.3 69.5-120 2.10 20 1,1,2,2-Tetrachloroethane 0.0250 0.0237 0.0259 94.9 104 79.3-123 8.78 20 Tetra chloroethene 0.0250 0.0245 0,0242 97.9 97.0 73.5-130 0.940 20 ACCOUNT: PROJECT. SDG: DATE/TIME: PAGE' Eaton Corporation 28091-R L808032 12/29/1517.03 12 of 23 WG834853 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Volatlle Organic Compounds.(GC/MS) by. Method 624 L808032-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)12/19/15 08:45 • (LCSD)12/19/15 09:04 C p Spike Amount LCS Result LCSD Result LCS Rea. LCSD Rec. Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/1 mgll ri % % % % % TC Toluene 0.0250 0.0252 0.0254 101 102 77.9-116 0.930 20 111-Trichloroethane 0.0250 0,0247 0.0256 98.6 102 71.1-129 3.72 20 3 SSI 11,2-Trichloroethane 0.0250 0.0235 0.0249 93.8 99.4 81.6-120 5.78 20 0.. Trichloroethene .0250 0.0264 0.0264 105 106 79.5-121 0.210 20 y Trichlorofluoromethane -00250 0.0245 0.0232 97.9 920 49.1-157 5,16 20 Cn 'Vinyl chlonde 0.0250 0.6220 0.0225 87.9 89.9 61.5-134 2.26 20 (S) Toluene d8 105 104 90.0-115 - _ s Sr (S)Dibronolluoromethanc_. _ _ _ -. _ .- 101 98.0 790-121 _ (S) o.a o TnBuorololueno 105 105 90.4-116 (5) 4 Bromohuorobenzene 87.1 89,5 60,1-120 7GI L805952-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12/19/15 11:57 • (MS) 12/19/15 11:05 - (MSD) 12/19/15 11:22 aAl Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I rai ni mg/I % % % % % 9 Acrolein 0,125 ND 0.121 0.106 9Z0 84.7 1 10.0-200 13.6 27.7 SC Acrylonitrile 0.125 ND 0.172 0.151 137 120 1 49.4-133 JS 13.2 25.3 Benzene 0,0250 ND 0.0263 0.0266 105 106 1 58.6-133 1.17 20 IDromodichloromethane 0.0250 ND 0.0262 0.0262 105 105 1 69.2-127 0,180 20 Brom dorm 0.0250 ND 0.0298 0.0277 119 111 1 66.3-140 Z27 20 'Bromomethane 0.0250 ND 0.0273 0.0267 109 107 1 16.6-183 2.16 20.5 Carbon tetrachloride 0.0250 ND 0.0280 0.0285 112 114 1 60.6-139 1.53 20 Chlorobenzene 0.0250 ND 0,0255 0.0255 102 102 1 70.1-130 0.170 20 Chlorodibromornethane 0.0250 ND 0,0272 0,0264 109 106 1 71.6-132 2.95 20 Chloroethane 0.0250 0.00034E 0.0235 0,0234 92.5 92.2 1 33.3-155 0.310 20 2-Chloroethyl vinyl ether 0.125 ND 0.0125 0.0136 10.0 10.9 1 5,00-149 8.23 40 'Chloroform 0.0250 ND 0.0260 0.0260 104 104 1 66.1-133 0.0300 20 Chloromethane 0,0250 ND _ 0.0281 0.0282 113 113 1 407-139 0.390 20 ,1,2-Dichlorobenzene 0.0250 ND 0.0263 0.0256 105 102 1 77.4-127 2.83 20 1,3-Dichlorobenzene 0.0250 ND 0.0256 0.0247 103 98.7 1 67.9-136 3.84 20 4,4-Dichlorobenzene 0,0250 ND 6.0249 0.0246 99.4 98A 1 74.4-123 1.01 20 Dichlorodifluoromethane 0.0250 ND 0.0252 0.0240 101 96.1 1 42.2-146 4.86 20 1,1-Dichloroethane 0.0250 0.0168 0,0376 0,0371 83.4 81.4 1 64.0-134 1.29 20 1,2-Dichloroethane 0.0250 ND 0.0244 0.0239 97.4 95.5 1 50.7-132 1,97 20 1,1-Dichloroethene 0.6250 0.0103 0.0265 0.0264 64.6 64.1 1 48.8-144 0.500 20 ACCOUNT: PROJECT: SDG'. DATE/TIME : PAGE: Eaton Corporation 28091 R L808032 12/29/1517:03 13 of 23 WG834853 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Volatile Organic Compounds. (GC/MS), by Method 624 L808032.01 L805952-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) 12A9/1511:57 • (MS)12/19/15 11:05 • (MSD)12/19/15 11:22 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/l mg/I mg/I % % % % % Ira ns-1,2-Dichloroethene 0,0250 NO 0.0252 0.0259 101 104 1 61.0-132 2.95 20 1,2-Dlchloropropane 0,0250 ND 0,0286 0,0292 115 117 1 697-130 2.05 20 cis-1,3-Dichloropropene 0.0250 NO 0.0276 0.0274 1fl 110 1 711-129 0770 20 trans-1,3-D[chi oroprop ene 0,0250 ND 0.0279 0.0276 112 110 1 66.3-136 1.20 20 Ethylbenzene 0.0250 ND 0.0280 0.0259 112 104 1 62.7-136 7.89 20 '.Methylene Chloride 0.0250 0.000283 C.0235 0.0229 93.0 90.5 1 61.5-125 2.62 20 1,1,2,2-Tetrachloroethane 0.0250 ND 0.0284 0.0258 114 103 1 64.9-145 9.47 20 Tetrachloroethane 0.0250 ND _ 6b255 0.0252 102 101 1 57.4-141 1.21 20 Toluene 0.0250 ND 0.0252 0.0256 101 102 1 67.8-124 1.56 20 1,1,1-Trichloroethane 0,0250 ND 0.0260 0.0267 104 107 1 58.7-134 2.53 20 1,1,2-Trichloroethane 0.0250 NO 0.0260 0,0250 104 99.8 1 74.1-130 3.89 20 Trichloroethene 0.0250 ND 0,0258 0.0267 103 107 1 48.9-148 3.62 20 Trichlorofluoromethane 0.0250 NO 0.0257 0.0255 103 102 1 39.9-165 0.820 20 Vinyl chloride 0.0250 0.000651 0.0241 0.0234 93.7 90.9 1 44.3-143 2,89 20 (S) Toluene-d8 102 102 90.0-115 (S) Dibromolluoromelhane_ 101 100 79.0 12.1 (S)ca,u-Trifluorotoluene _ 101 103 90.4-116 /S)4-BromoBuorobenzene 918 89.4 80.1-120 ACCOUNT: PROJECT: SDG' Eaton Corporation 28091-R L808032 DATE/ IME: 12/29/1517:03 PAGE: 14 of 23 WG837190 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. x Pesticides (GC) by Method EPA _608 _ - L808032.01 Method Blank (MB) Cp (ME) 12/23/1511:53 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/1 mg/I TC Aldrin U 0.00000813 0,0000500 Alpha BHC U 0.0000166 0.0000500 a SS Beta BHC U 0.0000184 0.0000500 .Delta BHC U 0.0000197 0.0000500 _ q Gamma BHC U 0.0000176 OJ0000500 Cn 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 Sr 4,4-DDT U 0.0000177 0.0000500 Dieldrin U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0,0000500 Endosulfan II U 0.0000176 0,0000500 �Endosulfan sulfate U 0.0000196 0.0000500 7G Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0600142 0.0000500 a Endrin ketone U O'0000170 0.0000500 A Heptachlor U 0,0000108 0.0000500 Heptachlor epoxide U _ 0.0000175 0.0000500 a Sc Hexachlorobenzene U 0.0000134 0.0000500 _ Methoxychlor U _ 0.0000193 0.0000500 ,Chlordane U 0.0000977 0.000500 Toxaphene U 0,000168 0.000500 (S) Decachlorobiphonyl 70.9 10.0-156 (S) Tetrochloro-m-xylene 60.2 13.9-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/23/1512,06 • (LCSD) 12/23/15 12:18 Spike Amount LCS Result LCSD Result LCS Red. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Aldrin 0.00100 0.000813 0.000804 81.3 80A 10.0-120 1.07 339 Alpha BHC 0.00100 0.00103 0.00106 103 106 53.6-125 2.76 22.3 Beta BHC 0.00100 0.000999 0.00103 99.9 103 55.8-130 3.21 20.6 Delta BHC 0.00100 0.00117 0,00120 117 120 42.2-135 2.38 233 Gamma BHC 0.00160 0.00103 0.00106 103 106 54.7-125 2.46 2Ll 4,4-DDD 0,00100 0.00111 0,00106 Ill 106 47.6-144 4.79 24.3 4,4-DDE „_ 0.00100 0.00113 0.00107 113 107 45.0-124 4.56 25J ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L808032 DATE/TIME' 12/29/15 17:03 PAGE: 15 of 23 WG837190 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Pesticides (GC) by Method EPA 608 L808032-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/23/15 12:06 - (LCSD) 12123/15 12.18 Spike Amount Analyte mgA LCS Result mg/I LCSD Result mg/I LCS Rec. % LCSD Rec. % Rec. Limits LCS Qualifier % LCSD Qualifier RPD % RPD Limits % 4,4-DDT 0,00100 0.00118 0.00109 118 109 49.8-130 8.16 25.4 Dieldrin 0.00100 0,00116 0.00112 116 112 55.0-127 3.36 22.9 Endosultan 1 0.00100 0.00113 0.00111 113 Ill 54.7-127 1.66 24.3 Endosulfan II 0.00100 0.00117 0.00111 117 ill 53.1-135 4.57 23.5 Endosulfan sulfate 0.00106 0,00122 0.00115 122 115 51.5-132 6.04 26.3 Endrin 0,00100 0.00113 0.00107 113 107 50.1-131 5.24 29.1 £ndrin aldehyde 0.00100 0,00113 0.00109 113 109 39.5-137 3,12 28A Endrin ketone 0.00100 0.00120 0,00111 120 Ill 53.5-139 7,25 28A Heptachlor 0.00100 0.000941 0.000948 94.1 94.8 20.7-127 0.790 30.5_ Heptachlor epoxide 0,00100 0.00110 0.00109 110 109 56A-124 _ 1.01 23.1 Hexachlorobenzene 0.00100 0.000750 0.000779 75.0 77.9 26.7-114 3.84 27.6 Methoxychlor,F - 0,00100 0.00132 0,00115 . 132 115 48.2-144 13.0 27.8 (S) Decochlorobiphenyl 1- 99A 85.1 10.0156 (S)Tetrochloro-m-xylene - - - 71.4 73.4 739137 - - - - Method Blank (MB) (MB)12/24/15 11:26 Analyte MB Result mg/I MB Qualifier MB MDL mg/I MB RDL mgA ' PCB 1260 U 0.000120 0.000500 'PCB 1016 U 0.000100 0,000500 PCB 1221 U 0.0000730 0,000500 'PCB 1232 U 0.0000420 0,000500 PCB 1242 U 0.0000470 0.000500 !PCB 1248 U 0.0000860 0.000500 PCB 1254 u 0.0000470 0.000500 (S Decochlorobiphenvl 87.7 10.0-156 (S) Telrochloro-m-xylene 74.1 13.9-137 ACCOUNT: Eaton Corporation PROJECT: 28091-R SDG. DATE/TIME'. L808032 12129/1517:03 PAGE: 16 of 23 WG837944 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE, Semi Volatil e,0•rganic Compounds (GC/MS),by Method 625 LBOB032-01 - Method Blank (MB) (MB) 12/24/1511:22 MB Result MB Oualifer MB MDL MB RDL Analyte my/I mg/l mg/I - Acenaphthene U 0.000316 0,00100 Acenaphthylene U 0.000309 0,00100 Anthracene U 0.000291 0.00100 'Azobenzene U 0.000318 0.0100 - Benzidine U 0.00432 0.0100 Benzo(a)anthracene _ U 0.0000975 0.00100 _ Benzo(b)fluoranthene _ U 0.0000896 0.00100 Benzo(b)fuoranthene U 0.000355 0.00100 Benzo(g,hJ)perylene U 0,000161 0,00100 ,Benzo(a)pyrene U 0,000340 0.00100 Bis(2-chlorethoxy)methane U 0.000329 0.0100 is (2-chloroethyl)ether U 0,00162 0.0100 Bis(._-. -. 2-chloroisopropypether U .. _ 0.000445 0.0100 4-Bromophenyl-phenylether U 0.000235 0.0100 2-Chloronaphthalene U 0.000330 0,00100 4-Chlorophenyl-phenylether U 0.000303 0,0100 Chrysene U 0.000332 0.00100 of benz(a,h)a nth racene U 6.000279 _ 0.0010_0 3,3-Dichlorobenzidine U 0.00202 O.Choo 2,4-Dinitrotoluene U 0,00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0,000310 0.00100 Fiuorene U 0.000323 O.00100 Hexachlorobenzene U 0,000341 0.00100 Hexachloro-13-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0.00233 0.0100 Hexachloroethane U 0,000363 0.0100 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 Isophorone U 0,000272 0.0100 -Naphthalene U 0.000372 0.00100 Nitrobenzene U 0.000367 0.0100 in-Nitrosodimethylamine U 0.00126 0,0100 n-Nitrosodiphenylamine U 0.000304 0.0100 In-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 0.00100 �Benzylbutyl phthalate U 0.000275 0,00300 Cp 2Tc a55 Fn sSf 7GI aAl 9SC ACCOUNT: PROJECT: SDG: DATEPnME: PAGE: Eaton Corporation 28091-R L808032 12/29/1517:03 17 of 23 WG837944 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 6�5 L808032-01 Method Blank (MB) (MB) 12/24/1511:22 Anayte MB Result mg/I MB Qualifier MB MDL mgll MB RDL mg/I Bis(2-ethyl hexyl)phtha late U 0.000709 0.00300 Di-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0.000282 0.00300 '.Dimethyl phthalate U 0,000283 0.00300 Dl-n-octyl phthalate U 0.000278 0.00300 Pyrene U 0.000330 0.00100 1,2,4-Trichlorobenzone U 0.000355 0.0100 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0.000283 0,0100 2,4-Dlchlorophenol U 0.000284 0.0100 2,4-Dimethylphenol U 0.000624 0,0100 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 2,4-Dinitrophenol U 0.00325 0.0100 - 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.000313 0.0100 Phenol U 0.000334 0.0100 2,4,6-Trichlorophenol U O.D00297 0.0100 (5) Nitrobenzene-d5 816 218-113 (S 2-Fluorobiphenyl 75.8 295-131 (S) p-Terphenyl-dN 85.2 293-137 (S) Phenol-d5 317 5.00-70.1 (S) 2-Fluorophenol 48.1 10.0-77.9 • 246-Tabromophenol 83.5 11.1-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/24/1510:36 • (LCSD)12/24/15 10:59 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgll mg/I mg/1 % % % % % Acenaphthene 0.0500 0.0410 0.0361 82.0 72.2 38.7-109 12.6 21.5 Acenaphthylene 0.0500 0.0433 0.0372 86.6 74.4 36.0-106 15.1 21 Azobenzene 0.0500 0.6483 0.0417 96.5 83.4 3T6-111 14.6 21.1 Anthracene 0,0500 0.0420 0.0365 83.9 73.0 43.6-113 13.9 18.8 Benzidine 0.0500 0,0229 Ob248 45.8 49.6 10.0-165 7.88 40 Benzo(a)anthracene 0.0500 0.0388 0.0346 77.7 69.2 51.2-112 11.5 20 ACCOUNT: ' PROJECT: SDG: Eaton Corporation 28091-R L808032 DATEIRIME: 12/29/1517'.03 PAGE: 18 of 23 WG837944 QUALITY CONTROL SUMMARY _. Semi Volatile Organic Compounds (GC/MS) by -Method. 625 _ L808032-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS)12124/1510:36 • (LCSD)12/24/1510:59 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec Limits LCS Oualifier LCSD Ouaffler RPD RPD Limits Analyte mg/I mg/1 mg/I . , % % % % % Benzo(b)fluoranthene 0.0500 0.0397 'iD.0367 79.3 73.3 47.6-111 7,85 20 iBenzo(k)Fluoranthene 0.0500 0.0399 0.0350 79.7 70.0 49.4-114 13.0 20 Benzo(g,h,i)perylene 0.0500 0.0407 0.0367 61.5 73.3 45.2-117 10.5 20 Senzo(a)pyrene 0.0500 0,0414 0.0369 82.9 73.9 45.6-106 11.5 20 Bis(2-chlorethoxy)methane 0,0500 0.0382 0.0337 76.4 �" 67.3 37,2-111 12.6 24.1 Bis(2-chloroethyl)ether 0.0500 .0.0392 0.0347 78.3 69.5 22.6-108 12.0 27.9 Bis(2-chloroisopropypether 0.0500 0,0393 0,0348 78.6 69.7 32.9-100 12.1 25.1 4-Bromophenyl-phenylether 0.0500 0.0423 0.0375 84.6 75.1 40.7-116 12.0 21 2-Chloronaphthalene O.0500 0.0414 0.0360 82.9 72.0 33.6-105 14.1 23 i4-Chlorophenykphenylether 0.0500 0.0460 0.0355 80.1 71.1 39.0-113 11.9 20.9 Chrysene 0.0500 0.0391 0.0356 78.2 71.1 54.6-120 9.40 20 Dibenz(a,h)anthracene 0.0500 0.0410 0.0369 81.9 73.8 42.8-118 10.5 20 3,3-Dichlorobenzidine 0.0500 0,0432 0.0382 86.4 76.3 27.2-142 12.3 22.3 2,4-Dinitrotoluene 0.0500 0.0434 0,0384 66.9 76.7 31.2-105 124 22 2,6-Dlnitrotoluene 0,0500 0,0446 0.0393 892 78.6 30.6-106 12.6 23.1 Fluoranthene 0.0500 0.0426 0.0373 85.2 74.6 45.9-115 13.3 20 Fluorene 0.0500 0.0404 0.0360 80.8 72.1 41.0-112 1L4 20.2 Hexachlorobenzene 0,0500 0.0449 0.0384 89.8 76.8 38.5-116 15.6 20.1 Hexachloro-1,3-butadiene 0,0500 0.0389 0.0349 77.8 69.8 16.1-104 10.8 31.2 Hexachlorocyclopentadiene 0.0500 0.0260 0.0223 52.1 44.6 10.0-121 15A 27.9 Hexachloroethane 0.0500 0,0384 0.0338 76.8 67.6 16.5-89.8 12.8 30.7 Indeno(1,2,3-cd)pyrene 0.0500 0.0415 0.0372 83.0 74.4 45.0-116 10.9 20 Isophorone 0.0500 0.0446 0.0399 99.1 -79.8 35.4-112 11.1 21.5 Naphthalene : _ 0.0500 0.0368 ;0.0320 73.6 64.1 322-101 13.9 23.8 Nitrobenzene 0.0500 0.0431 �0.0379 86.3 75.9 31.4-106 12.8 25.7 n-Nitrosodimethylamine 0,0500 0.0230 0,0199 45.9 39.8 10.0-80.1 14A 37.5 n-Nitroscdiphenylamine 0.0500 0,0415 0,0367 829 73.3 44A-113 12.3 20 n-Nitrosodi-n-propylamine 0,0500 0.0408 0.0367 81.6 734 33.2-106 10.5 23.7 Phenanthrene 0.0500 .0,0388 0.0339 77.5 67.8 46A-113 13.4 20 Benzylburyl phthalate 0.0500 0,0481 0.0430 96.2 86.1 31.8-123 11.1 20.7 Bis(2-ethylhexyl)phthalate 0.0500 0.0440 0.0390 87.9 78.0 36.9-134 12.0 23.6 Di-n-butyl phthalate 0.0500 0.0472 0.0412 94A 82.3 41.8-120 13.7 20.2 Diethyl phthalate 0.0500 0.0463 0.0410 92.6 82.1 36.5-129 12.1 20 'Dimethyl phthalate 0.0500 0.0447 0,0392 89.4 78.5 35.3-128 13.0 20.8 Di-n-octyl phthalate 0.0500 _ 0.0483 0.0424 96.6 84.8 39.7-112 13-0 21.1 'Pyrene 0.0500 0.0406 0.0373 81.2 74.6 46.3-117 8,47 20 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L608032 12/29/1517:03 19 of 23 WG837944 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625 L808032-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 12/24/15 1036 • (LCSD) 12/24/15 10:59 Spike Amount Analyte mg/I LCS Result mg11 LCSD Result img/I LCS Rec. % LCSD Rea. % Rec. Limits LCS Qualifier % LCSD Qualifier RPD % RPD Limits % 1,2,4-Trichlorobenzene 0.0500 0.0339 0.0310 67.8 62.0 22.9-96.1 8.92 27.5 4-Chloro-3-methylphenol 0,0500 0.0460 0.0401 91.9 80.3 35.7-100 13.5 22.9 2-Chlorophenol 0.0500 0.0374 0.0327 74.7 65A 262-91.5 13.3 26.5 2,4-Dichlorophenol 0,0500 0.0422 0.0375 84.4 75.0 31.4-103 IL7 24.9 2,4-Dimethylphenol 0,0500 0.0417 0.0381 83.4 76.3 31.9-107 8.94 25.7 4,6-Dinitro-2-methylphenol 0,0500 0.0432 0.0392 86.4 78.4 18.4-148 9.73 24A 24-Dinitrophenol 0,0500 0.0247 0.0292 49.4 58.5 24.2-128 16.9 20.5 2-Nitrophenol 0.0500 0.0442 0.0390 88A 78.1 25.9-106 12A 26.9 4-Nitrophenol OOSOO 0.0197 0.0185 _ 39.4 37.0 10.0-52.7 647 40 Pentachlorophenol_ 0.0500 0.0430 0.0372 85.9 74.5 10.9-97.4 14.3 35.1 Phenol 0.0500 0.0189 0,0169 37.8 33.8 10.0-57.9 11.4 35 2,4,6-Trichlorophenol 0.0500 0.0440 0.0391 88.0 78.3 29.8-107 117 24.1 (S) Nitrobenzene-d5 79.6 760 218-123 (S) 2-Fluorobiphenyl 76.9 678 29.5-131 (S)p-Terphenyl-dN 848 786 293-137 (5) Phenol-d5 34.5 30.4 5.00-70.1 (S) 2-Fluorophenol 53.8 47.3 10.0-77.9 (S)2.4.6-Tribromopheaol 9Zo 84.0 11.2-130 ACCOUNT: PROJECT: SDG: DATErrIME PAGE: Eaton Corporation 28091-R L808032 12/291151703 20 of 23 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. 'MDL Method Detection Limit. RDL Reported Detection Limit. ND,U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. Results are reported based on the dry weight of the sample. [this will only be present on a dry ,(dry) report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate, used to evaluate analytical efficiency by measuring _ recovery. S_u_rrogates are not expected to be detected in all environmental media. _ Rec. Recovery. SDL Sample Detection Limit. - _ MQL Method Ouantitation Limit. Unadj. MQL Unadjusted Method Ouantitation Limit. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J4 The associated batch OC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination, spike value is high. ACCOUNT: PROJECT: SDG. DATEMME Eaton Corporation 28091-R L808032 12/29/1517.03 PAGE: 21 of 23 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one paint of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry The most significant benefit to our -one location- design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing turn around time. and preventing cross contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE, Not all certifications held by the laboratory are applicable to the results reported in the attached report. State Accreditations Alabama 40660 Nevada TN-03-2002-34 Alaska UST-080 __ New Hampshire 2975 __ Arizona _- __ _ _ _ AZ0612 _ _ _ New Jersey-NELAP _ Arkansas 88-0469 New Mexico _ _ _TNO02__- TNO0003 California 01157CA New York 11742 Colorado TN00003 North Carolina _ Env375 Conneticut PH-0197 North Carolina DN/21704 Florida E87487 _ _ North Carolina' _ _ 41 Georgia NELAP North Dakota _ R-140 Georgia' _ 923 Ohio-VAP _ CLOO69 _ Idaho _ _ _ TN00003 Oklahoma _ _ _ !_ 9915 Illinois 200008 Oregon TWHO02 Indiana C-1`19-01 ___ Pennsylvania _ _ _ _ 68-02979_ Iowa 364 Rhode Island _ 221 Kansas ____.__.._.- _ .E-10277 _ South Carolina — _ _ _ __- . _ 84004 Kentucky' _ _ _ 90010 .- South Dakota_ _ - — - n/a Kentucky'___— _ _ 16 — Tennessee" - 2006 _ Louisiana ._ AI30792 __- Texas T 104704245-07-TK Maine TN0002 Texas s LABO152 Maryland - _ 324 Utah 6157585858 Massachusetts M-TN003 Vermont _ VT2006 Michigan - _ - --_ 9958 _. _-- Virginia 109 Minnesota _ _ _ _047-999-395 _ Washington _ 0915_ Mississippi _ TN00003 _ West Virginia _ 233 Missouri 340 Wisconsin 9980929910 Montana _ _ _ CERT0086 Wyoming _ _ _ A21-A - Nebraska NE-OS-15-05 Third Party & Federal Accreditations A2LA-ISO 17025 1461.01 AIHA 100789 A2LA- ISO 17025' 1461.02 DOD 1461.01 Canada 1461.01 — -- -- - USDA _ S-67674------- - EPA-Crypto _ _ TN00003 'Drinking Water `Underground Storage Tanks °- Aquatic Toxicity' Chemicalifocroblological SMoltl "' Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. N/A / O " MT riD OR • ff.N T IIJ SD T lVl TNY MY Tar T T NE IA T T T ! PA T • T NV ! T Ir �LTI UT T T T C ! xw T' CA T CO • KS M• • VAT T KY —� _ T T T •.�--yN • l—:mot t T •AZ N. �? Arlp • • T sc T Ms At GA • T T t Ix Ln •—tT 9 T' • T AK O FL � BO • • �n HI ACCOUNT: PROJECT: SDG: DATE7TIME% Eaton Corporation 28091-R L808032 12/291151703 N.E PAGE: 22 of 23 _ Gain WCuttady page of + Anal SIS / Container J PreservallveT'1 ,C) Company Name/Address: Billing Information: Eaton Corporation NA Financial PO Box 818024 I i ..-� ..,.,o o.c.,.c•r+ c s-o . 2564 Durham Rd . Cleveland, OH 441BI.8024 k _ Roxboro, NC 27573: bass TW t.wwm1 n • . Tu O.yv G rfawl slYTsesese, \.} Email To: d A �.: Pbrr.: eoo:Yateess rr ". RCPorl ta: i., U,-' U O z v • ,:(� q (sis)e4se1? [i]y 1.' Dustin LeClair ustinlaclair@Eaton.com _ ? mx h Protect City/State Roxboro, NC z a; o o' Lan l +U$03oi Eaton,Corp.,Seml-Annual Stormwater 6aiioued: or. a 'a ' LD f� Description:: ' q o J005 Clieni Prole[tu Lab Proie[lA -' so Phcnc:336.599-1141 EATONRNC-28091SW. m v' _ E E 28091-R a No E m •m gCClnbmEATONRNG Fqa:. Z o'I E !�' j r ' _Collected by In Site/FbrililV.IDA P'C'k I W M, N 0E .C, � 0; Ics'I 7emPute { -X1 t� k P S t(�r o ,< to, d a eiogln Date Results Needed = X• R k i .�'. Couetled by(si nature): Rush? (lab MUST Be Noliied) J 'IX C AN (NI N TSA iHUtlt+ semc Div .._____......._. Z00% `' s- -W', .1 ....10^% EmellT _ND yes le �'. YlO 0.. �• CoolCr __.. _Neat OaY••••^- N0� i. IFFF_ /1"�' '� % dfa:,RaleigFt SOrw Two Day _ ....... _. ..__sox FA%3'NO �Y2F I ti0 .a j Y ShiPPed, immediately bt . O rrs 1a� Packed On lW N_� Y� _Thrcn bay. .... .. ...._IS% !' N •.S i N: N ''� ~`' - AemlPPnr"'^'^' s+mNc glue onNT Time ntn H •F •,. U '.!?r , sD .. Date . • - 5nmplel0; CV i ome/Grab Maa' DeOth . 13. - --- 3 . Tnol � Rmd4 lrtncLL WW " 4 ! • .w 1 _ 4 r . - 1 73 'Matrix:SS - Soil GW-Groundwa[cry WW'WastewDW- Drinking Water oT - other Hold N` • Flow Other � ConAltWd; .Pqb use,onryl Remarks: Samples relumecivia:. d UPS Time: - .Date _ Received by (Signs re) ,,t (T• RCi/ljnquished.by ignatu rA�'-\�FedEa ❑Courier •��� QI(••• ' [ :Bottles ecefved . Time Recelvedhy IsIon,a M) Temp: ^ RN ✓ nNA;. Relinquished by (5lengtarel Date. < '" qs� - CoWeal Intact . - 1 \ I `2 pH checked,-NCF - s Date. _ Timc: of for (SigT atur 1.2• Relupulshed by : (Slgnat f Dater _ [ . a S ESC CIS - ANALYTICAL REPORT November 30, 2015 Eaton Corporation Sample Delivery Group: L802563 Samples Received: 11/20/2015 Project Number: 28091-R 0 Description: Eaton Corp Semi -Annual Stormwater Site: ROXBORO, NC Report To: Dustin La Clair 2564 Durham Road Roxboro, NC 27573 Entire Report Reviewed By: 41AJ- Jimmy Hunt Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced. except in full, Without written approval of the laboratory. Where applicable. sampling conducted by ESC is performed per guidance provided In laboratory standard operating procedures: 060302, 060303, and 060304. r r� J II. REPL iIME DATA ACCESS r1 I TABLE OF CONTENTS ONE LAB NATIONWIDE. 'Cp: Cover Page 2Tc: Table of Contents 'Ss: Sample Summary "Cn: Case Narrative 'Sr: Sample Results 2015-11-19-005 TOOL ROOM TRENCH L802563-01 60c: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664A Metals (ICP) by Method 200.7 Volatile Organic Compounds (GC/MS) by Method 624 Pesticides (GC) by Method EPA 608 Polychlorinated Biphenyls (GC) by Method EPA-608 Semi Volatile Organic Compounds (GC/MS) by Method 625 'GI: Glossary of Terms "Al: Accreditations & Locations 9Sc: Chain of Custody 1 2 3 4 5 5 8 8 9 10 11 15 15 17 21 22 23 Cp 3$5 aCn SSr 6Oc [GI eAl BSc ACCOUNT: PROJECT: SOG: Eaton Corporation 28091-R L802563 DATEMME: PAGE: 11/30/15 21:07 2 of 23 SAMPLE SUMMARY ONE LAB. NATIONWIDE. 2015-11-19-005 TOOL ROOM TRENCH L8O2563-01 WW Collected by Collected dateRime Received date/time Kirk Spicer 11/1911507:15 11/20/1509:00 Method Batch Dilution Preparation date/time Analysis date/lime Analyst Gravir is Analysis by Method 2540 D-2011 WG831428 1 11/25/1513:16 11/251514:11 MF Metals (ICP) by Method 200.7 WG831726 1 1112511517:04 11/26/1504:11 CCE Pesticides (GC) by Method EPA 608 WG830650 1 11/22/15 20:00 11/23/1517:41 ADF Polychlorinated Biphenyls (GC) by Method EPA-608 WG830650 1 11/22/15 20:00 11/24/1518:14 LKO Semi Volatile Organic Compounds (GC/MS) by Method 625 WG831669 1 11/24/1512:00 1112511522:56 ADF Volatile Organic Compounds(GC/MS) by Method 624 W6830844 1 11/22/1512:29 11/22/1512:29 JHH Wet Chemistry by Method 1664A WG832228 1 11/30/1514:22 11/30/15 17:14 1M �J ACCOUNT: PROJECT: SDG: Eaton Corporation 28091R L802563 DATE/TIME: PAGE: 11/30/15 21:07 3 of 23 CASE NARRATIVE ONELAs.NAnoNwIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOO) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. P7 4-�Zj- Jimmy Hunt Technical Service Representative ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21'07 4 of 23 2Q15-11-19'-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected dale/lime: 11/19/15 07:15 L802563 Additional Information C Result Units Analyte pH (On Site) 7 su TC Temperature (on -site) 17.2 Deg. C D-2011 _ aSs Gravimetric Analysis by Method 2540 Result Qualifier MOIL RDL Dilution Analysis Batch ° Cn Analyte mg/I mg/1 Fogg date/time Suspended Solids 8.82 0.350 2.50 1 11/25/201514:11 WG831428 Wet Chemistry by Method 1664A 6 Result Oualifler MOIL RDL Dilution Analysis Batch OC Analyte mg4 mg4 mg4 date/time TPH -Oil&Grease U 0725 5.56 1 11/30/20151714 WG832228 [GI Metals (ICP) by Method 200.7 aAl Result Qualifier MOIL RDL Dilution Analysis Batch s Analyze mg4 mg/l mg4 date/time Copper 0.0161 0.00700 0.0100 1 11/261201504:11 WG831726 SC Lead U 0.00200 600500 1 11/261201504:11 WG831726 Zinc 0.0281 J 0.00340 00500 1 11/261201504:11 WG831726 Volatile Organic Compounds (GC/MS) by Method 624 Result Qualifier MOIL RDL Dilution Analysis Batch Analyte mg4 mad mg4 date/time Acrolein U J4 0.00887 0,0500 1 11/22/20151229 WG830844 Acrylonilrile U 0.60187 0,0100 1 11/22/20151229 WG830844 Benzene U 0.000331 0.00100 1 11/22/201512:29 UGE30844 Bromodichloromethane U 0.000380 0,00100 1 11/22/201512:29 WG830W Bromoform U 0.000469 0.00100 1 11122/201512:29 VIG830844 Bromomethane U 0.000666 0.00500 1 11122/2M 12:29 WG830844 Carbon tetrachloride U 0.000379 0.00100 1 11122/201512:29 WG830844 Chlorchenzene U 0000348 0.00100 1 11122201512:29 WG830844 Chlorodibromomethane U 0000327 0.00100 1 11122/201512:29 WG830844 Chloroethane U 0.000453 0.00500 1 11122/2015 12 29 WG830844 2-Chloroethyl vinyl ether U J4 0.00301 0,0500 1 11/22/2015 12: 2 9 WG830844 Chloroform U 0.000324 0,60500 1 11122/20151229 WG830844 Chloromethane U 0.000276 0.00250 1 11122/2015 12 :29 WG830844 1,2-Dichlorobenzene U 0.0100349 0.00100 1 11/22/2015 12:29 VJG830844 1,3-Dichlorobenzene U 0.000220 0.00100 1 11/22/201512:29 VIG830844 1,4-Dichlorobenzene U 0.000274 0.00100 1 11/22/201512.29 WG830844 Dichlorodifluoromethane U 0.000551 6Q0560 1 11/22120151229 VIG830844 11-Dichloroethane U 0.000259 0.06100 1 11/22/20151229 WG830844 1,2-Dichloroethane U 0.000361 0.00100 1 11/22/2015 12 29 N/GS30844 11-Dichloroethene U 0.000398 0.00100 1 11/22/201512:29 WG830844 trans-1,2-Dichloroethene U 0.000396 0.00100 1 11/22/201512:29 WG830844 1,2-Di0hloropropane U 0.000305 0.00100 1 11/22/201512:29 WG830844 cis-1,3-Dichloropropene U 0.000418 0.00100 1 11/22/2015 12 29 WG830844 trans-1,3-Dichloropropene U 0.000416 0.00100 1 11/251201512:29 WG830844 - Ethylhenzene U 0.000364 0.00100 1 11/22/201512:29 WG830844 Methylene Chloride U 0.00100 0.00506 i 11/22/201512.26 WG830844 , 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 11/221201512:29 WG830844 'Tetrachloroethene U 0.0o0372 0.00100 1 11/22/201512:29 WG830844 i Toluene U 0.000780 0.00500 1 11/22120151229 WG830844 v 1,1,1-Trichloroethane U 6.000319 0.00100 ,1 11/22/201512:29 WG830844 �. 1,1,2-Trichloroethane U 0.000383 0.00100 1 11/22/201512:29 WG830844 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21:07 5 of 23 2015-11-19-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 ONE LAB. NATIOf WIDE. Collected dateltime: 11/19115 07:15 L902563 Volatile Organic Compounds (GC/MS) by Method 624 t Col Result Qualifier MDL RDL Dilution Analysis Batch Analyze mgA mg/l mgA date/time Trichloroethene U 0.000398 0.00100 1 11/22/201512:29 WG830844 Tc Trichlorofiuoromethane U 0.00120 0.00500 1 11/22I201512:29 WG830844 Vinyl chloride U 0.000259 0.00100 1 11122120151129 WG830844 3 (S)Toluene-d8 987 90.0-115 1U22201512.29 WG830S44 $5 (S) Dibromolluoromelhone 9L9 79.0-121 1U2220151229 WG830844 (S 4rzo- Aitluorotoluene 109 904-116 1V22201512.29 WG830844 Cn (S) 9-eramo0uoraben7ene 102 80.1-110 11127201512:79 WG830844 Pesticides (GC) by Method EPA 608 Result Qualifier MDL RDL Dilution Analysis Batch 5 Analyte mg/I mg/I mga date/time QC Aldrin U 0,00000813 0.0000500 1 11/23/201517:41 WG830650 Alpha BHC U 00000166 0.0000500 1 11/23/201517:41 WG830650 7GI Beta BHC U 0.0000184 0.0000500 1 11/23201517:41 WG830650 Delta BHC U 0.0000197 0.0000500 1 11/23/201517:41 WG830650 a Gamma BHC U 0.6060176 0.0000500 1 11/23/201517:41 WG830650 A Chlordane U 0.0000977 0.000500 1 11/23/201517:41 WG830650 4,4-DDD U 0,0000170 0.0000500 1 111231201517:41 WG830650 0 Sc 4,4-DDE U 0.0000164 0.0000500 1 11/23/201517:41 WG8306506830650 4,4-DDT U 0,0000177 0.0000500 1 11123/201517:41 WG830650 Dieldrin U 0.00000751 0.0000500 1 111231201517:41 WG830650 Endosulfan I U 0.0000179 0.0000500 1 111231201517:41 WG830650 Endosulfan II U 0.0000176 0.0000500 1 11123/201517:41 VIG830650 Endosulfan sulfate U 0.0000196 0.0000500 1 11/23/201517:41 VIG830650 Endrin U 0.0000189 0.0000500 1 11/23/201517:41 VIG830650 Endrin aldehyde U 0.0000142 0.0000500 1 11123/201517.41 WG830650 Endrin ketone U 0.0006176 0.0000500 1 11/23/201517:41 WG830650 Heptachlor U 0.0000108 0.0000500 1 11/23/201517:41 WG8306SO Heptachlor epoxide U 0.0000175 0.0000500 1 11/23/2M 17:41 WG830650 Hexachlorobenzene U 0.0000134 0.0000500 1 11/23/2015 17:41 VIG830650 Methoxychlor U 0.0000193 0,0000500 1 11/23/2015 IT41 WG830650 Toxaphene U 0.000168 0.000500 1 11/23/201517:41 WG830650 (S) Decoo5forobiphenyf 72.1 10.0-156 1112312015 IZ41 WG830650 (S)Telrochforo-no-zylene 796 13.9-137 1112311201577.41 VIG830650 � Polychlorinated Biphenyls (GC) by Method EPA-608 Result Qualifier MDL RDL Dilution Analysis Batch Analyze mgA '. mgA mgA date/lime PC81016 U 0,000100 0.000500 1 111241201518:14 WG830650 PC81221 U 0.0000736 0.000500 1 W24/201518:14 WG630650 PCB 1232 U 0,0000420 0.000500 1 11/241201518:14 WG830650 PCB1242 U 0.0000470 0,000500 1 11/241201518:14 VIG830650 PCB 1248 U 0.0000860 0.000500 1 11/24/201518:14 VIG830650 ,PCB 1254 U 0.0000470 0.0005m 1 11/24/261518:14 WG830650 PCB 1260 _ U 0.000120 0.000500 1 11/24/201518:14 WG830650 Semi Volatile Organic Compounds (GC/MS) by Method 625 Result Qualifier MDL RDL Dilution Analysis Balch Analyze mg/I mg/l mg/I date/time Acenaphthene U 0.000316 0,00100 1 11/25/2015 22:56 VIG831669 Acenaphthylene U 0.000306 000100 1 11/25/201522:56 WG831669 Anthracene U 0.600291 000100 1 11/25/201522:56 VJG831669 Benzidine U 0.00432 0.0100 1 11/25/201522:56 WG831669 ` Benzo(ahmthraceoe U 0.0000975 000100 1 11125/201522:56 WG831669 Benzo(b)fluoranthene U 0.0000896 000100 1 11125/20152256 WG831669 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21:07 6 of 23 2Q15-11-19'-005 TOOL ROOM TRENCH SAMPLE RESULTS - 01 ONE LAB .NATIONWIDE. Collected date/time: 11/19/15 07:15 L802563 Semi Volatile Organic Compounds (GC/MS) by Method 625 l Result Qualifier MDL RDL Dilution Analysis Batch CPI Analyte mgA mgA mgA date/time Benzo(k)Iluoranthene U 0000355 0.00100 1 11/25201522:56 WG831669 z Tc Benzo(g,hJ)perylene U 0.000161 0.00100 1 11/25/2015 22:56 WG831669 Benzo(a)pyrene U 0.000340 0.00100 1 11125/20152M6 WG831669 a Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 11/251201522:56 WG831669 SS Bis(2-chloroethyl)elher U 0.00162 0.0160 1 1125201522:56 WG831669 Bis(ichloroisopropyllether U 6.000445 o.0100 1 11/25/201522:56 WG831669 ° Cn 4-Bromophenyl-phenylether U 0.006335 0.0100 1 11/25/2015 22:56 WG831669 2-Chloronaphlhalene U 0.000330 0.00160 _ 1 11/25/201522:56 WG831669 4-61oraphenyl-phenylether U 0.000303 0.0100 1 11/25/2015 22:56 WG931669 Chrysene U 0.000332 0.00100 1 W25/201522 5(3 WG831669 Dibenz(ah)anth race ne U 0.000279 0,00100 1 11/251201522:56 WG831669 a QC 3,3-6ichlorobenzidine U 0.00202 0.0100 1 11/25/201522.56 WG831669 - 2,4-Dinitrotoluene U 0.00165 0.0100 1 11/2S/2015 22:56 WG831669 7GI 2,6-Dinitrotoluene U 6.600279 0.0100 1 11/251201522:56 WG831669 1,2-Diphenylhydrazlne U 0,000318 0.0100 1 111251201522:56 WG831669 Fluoranthene U 0.000310 0.00100 1 11/25/2015 22:56 WG831669 eAl Fluorene U 0.000323 0.00100 1 11/25/201522:56 VlG831669 Hexachlorobenzene U 0.000341 0.00100 1 11/252015 22:56 VIGS31669 y Hexachloro-1,3-butadiene U 0.000329 0.0100 1 11/251201522:56 WG831669 SC Hexachlorocyclopentadiene U 0.00233 0.0100 1 1125/2015 22:56 VIG831669 Hexachloroethane U 0.000365 0,0100 1 11/25/2015 22:56 WG831669 , Indeno(1,2,3-cd)pyrene U 0.000279 0,00100 1 11/25/2015 22:56 VIG831669 Isophorone U 0.000272 0.0100 1 11/25/2015 22:56 VIG831669 Naphthalene U 0,060372 0.0600 1 IIJ25/2015 22:56 VIG831669 Nitrobenzene U 0.000367 0.0100 1 11/25/201522:56 WG831669 n-Nitrosodimethylamine U 0.00126 0.0100 1 11/25/2015 22 56 WG831669 n-Nitrosodiphenylamine U 0.000304 0.0100 1 11/25201522.56 WG831669 n-NiUosodi-n-propylamine U 0.000403 0,0100 1 1105/20152156 WG831669 Phenanthrene U 0.000366 0.00100 1 11125/2015 22:56 VJG831669 Benzylbulyl phthalate U 0,000275 0.00300 1 11125/201S 22:56 WG831669 Bis(2-ettlylhex)egphthalate U 0.000709 0.00300 1 11/25/2015 22:56 WG831669 Di-n-butyl phthalate U 0000266 0.00306 1 1125/201522:56 WG831669 Diethyl phthalate U 0.000282 0.00300 1 11/2512015 2256 VIG831669 Dimethyl phthalate U 0,000283 0.00300 1 11125/201522:56 WG831669 Di-n-octyl phthalate U 0,000278 0.00300 1 11/25/2015 22.56 WG831669 Pyrene U 0.000330 0.00100 1 11125/201522,56 WG831669 1,2,4-Trichlorobenzene U 0.600355 0.0100 1 11/25/201522.56 WG831669 4-Chloro-3-methylphenol U 0.000263 0.0100 1 11/25/201522.56 WG831669 2-Chlorophenol U 0.000283 0.0100 1 11/25/2015 22:56 WG831669 2,4-Dichlorophenol U 0.000284 0.0100 1 1125/201522.56 WG831669 2,4-Dimethylphenol U 0.000624 0.0100 1 11/25/201522:56 WG831669 4,6-Dimtro-2-methylphenol U 0.00262 0.0100 1 11/25/201522:56 WG831669 2,4-Dinitrophenol U J3 0.00325 0.0100 1 11125/201522:56 WG831669 2-Nitrophenol U 0,000320 0.0100 1 11/25/201522:56 V/G831669 4-Nitrophenol U 0.00201 0QP00 1 111251201522:56 VIG831669 Pentachlorophenol U 0.000313 0.0100 1 11/25/201522:56 WG831669 Phenol U 0.000334 0.0100 1 1125/201522:56 WG931669 2,4,6-Trichlorophenol U 0.000297 0.0100 1 11/25/201522:56 WG831669 (5)2-Fluorophenol 43.5 10.0-729 112520152255 WG831669 IS) Phenol -d5 34.5 5.00-701 112520152255 ING831669 (5) Nirobenzened5 49.6 21.8-123 1112520152256 WG831669 (S)2-Fluorobiphenyl 562 195-131 1112520152256 WG831669 , (S)2,4.6-Tribron7ophenol 69.2 11.2-130 112520151256 WG831669 (S)p-Terpheny1-d14 58.8_ 293-137 112520752256 WG831669 ACCOUNT: PROJECT: SDG DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21.07 7 of 23 WG831428 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Gravimetric Analysis by Method 2540 D-2011 L902563-01 Method Blank (MB) (MB)11125/15 14:11 MB Result MB Qualifier MB MOIL MB ROT Analyte mg/I mg/l mg/I Suspended Solids U 0,350 2.50 L8O2571-01 Original Sample (OS) • Duplicate (DUP) (0S)11/25115 14:11 • (DUP) 11/25/15 14:11 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Solids 7,11 7.33 1 3.08 5 L8O2579-04 Original Sample (OS) • Duplicate (DUP) OS) 11/25/1514:11 • (DUP)11/25/15 14:11 Original Result DUP Result Dilution DUPRPD DUP Qualifier DUP RPD Limits Analyte mg/I mg/I % % Suspended Solids 27.5 27.8 1 0.905 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)11/25/15 14:11 • (LCSD) 11/25/15 14:11 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Oualifier RPD RPD Limits Analyte mgn mg/I mgA % % % % % Suspended Solids 773 756 764 SITE 98.8 85.0-115 1.05 5 ACCOUNT: PROJECT: SDG'. Eaton Corporation 28091R L802563 DATE/TIME: 11/30/15 2107 PAGE: 8 of 23; WG832228 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. ,y1 Wet Chemistry 5y Method 1664A - L802563-01 _ Method Blank (MB) (MB)11130/15 17:10 Cp z MB Result MB Qualifier MB MDL MB RDL Analyte mg/I myll nig/I TC TPH - Oil & Grease U 0.725 5.00 3Ss ^Cn Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)11/30/15 17:11 • (LCSD) 11/30/1517:12 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 5 Analyte mgll mg/I mg/I % % % % % Sf TPH - Oil & Grease 20.0 17.2 17.3 86.0 86.5 78.0-114 0.580 18 7GI eAl 9SG ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 1V30/15 21:07 9 of 23 WG831726 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICP( by Method 200.7 L802563-01 Method Blank (MB) 1 (MB) 11/26/15 03:13 Cp MB Result MB Qualifier MD MB RDL Analyze mg/I mg/l mg/I - TC Copper U 0.007 0.0100 Lead U 0.002 0.00500 3$S Zinc U 0.0034 0.0500 _ �Cn Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)11/26/15 03:16 • (LCSD) 11/26/15 03:19 5 $r Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mgA % % % % % Copper 1.00 1.06 1.05 106 105 85-115 1 20 Lead 1.00 1.07 1.06 107 106 85-115 1 20 Zinc 1.00 1.02 1.01 102 101 85-115 1 20 7G1 L8O2477-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) aAl (OS) 11/26/15 03:22 • (MS) 11/26/15 03.2E • (MSD)11/26/15 03:31 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits $C Analyze ! mg/I mg/l mg/I mgA % % % % % Copper -- 4.00 0.0313 Lit 1.13 107 110 1 75-125 2 20 Lead 1.00 0.00250 w8 1.09 107 109 1 75-125 1 20 Zinc 1.00 0.368 1.36 1.38 99 101 1 75-125 1 20 L8O2655-01 Original Sample (OS) •.Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS)11/26/15 04:42 • (MS) 11/26/15 04:45 • (MSD) 11/26/15 04:48 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mgll mg/I mg/I % % % % % Copper 1,00 0.417 1.56 1.46 115 104 1 75-125 7 20 Lead 1.00 0,000835 1.16 1.14 116 114 1 75-125 2 20 Zinc 1.00 0.0127 1.09 1.08 108 107 1 75-125 1 20 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L802563 DATE/TIME: 1V30/15 21'.07 PAGE: 1Dof23 WG830844 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 624 L802563-01 - - Method Blank (MB) (MB)11/22/15 09:32 CP MB Result Analyte mg/l Acrolein U 'Acrylonitrile U Benzene U IBromodichloromelhane U Bromoform U �Bromomethane U Carbon tetrachloride U �Chlorobenzene U Chlorodibromomethene U Chloroethane U 2-61oroethyl vinyl ether U Chloroform U Chlorcmethane U d,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodigucromethane U ;1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U trans-1,2-Dichloroethene U �1,2-Dichloropropane U cis-1,3-Dichloropropene U trans-13-Dichloropropene U Ethylbenzene, U Methylene Chloride U 11,2.2-Tetra chloroethane U Tetrachloroethene U Toluene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichloroflucromethane U ,Vinyl chloride U (S)Tofuene-d8 98.4 (S) Dibrornofluorome(hone 97.8 MB Qualifier MS MDL MB RDL mg/I mgll 0.00887 0.05p0 _ 0.00187 0,0100 0.000331 0.00100 0,000380 0.00100 0.000469 0.00100 _ 0.000866 _0.00500 0.000379 0.00100 0.000348 0,00100 0.000327 0.00100 0.000453 0.00500 0,00301 0.0500 _ 0.000324 0.00500 0.000276 0.00250 0.000349 0,00100 0,000220 0.00100 0.000274 0,00100 0.000551 0.00500 0,000259 0.00100 0,000361 0,00100 0,000398 0.00100 0,000396 0.00100 0.000306 0.00100 0.000418 0.00100 0,000419 0.00100 0,000384 0.00100 _ 0,00100 0.00500 0.000130 0,00100 0.000372 0.00100 0.000780 0.00500 0.000319 .0.00100 0.000383 0.00100 _ 6.000398 0.00100 0.00120 0.00500 0.000259 0.00100 90.0-115 79.0-121 ACCOUNT: PROJECT: SDG'. DATErTIME: PAGE: Eaton Corporation 28091.R L602563 11/30/15 21:07 11 of 23 WG830844 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by,Method 624 L902563-01 Method Blank (MB) (MB)11/22/15 09:32' MB Result MB Qualifier MBMDL MB RDL Analyte _ mg/1 mg/I mg/I (S)cec-TriAuoromluene 107 _ 90.4-176 (S)4-BromoOuorobenzene 103 80.1-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/22/15 06:57 • (LCSD)11/22115 07:17 -- Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % Acrolein 0.125 0103 0110 82.3 87.9 88.0-118 J4 J4 6.60 28.1 Acrylonitrile 0.125 0.119 0127 94.9 102 71.0-135 6.74 20 Benzene 0.0250 0.0240 0,0236 95.8 94.4 73.0-122 _ 144 20 IBromodichloromethane 0.0250 0.0266 0.0263 106 105 75.5-121 1.02 20 Bromoform 0,0250 0.0308 0.0297 123 119 71.5-131 3.68 20 IBromomethane 0.0250 0.0219 0.0213 87.6 85.4 22.4-187 2.58 20 Carbon tetrachloride 0.0250 0.0231 0.0235 92.5 94.1 70.9-129 1.71 20 Chlorobenzene 0.0250 0.0283 0.0272 113 109 79.7-122 3.79 20 Chlorodibromomethane 0.0250 0-0298 0.0291 119 117 78.2-124 2.37 20 Chloroethane 0,0250 0.0235 0.0234 94.0 93.4 41.2-153 0,610 20 2-Chloreethyl vinyl ether 0.125 0,222 0.220 178 176 23.4-162 J4 J4 0.970 23.5 Chloroform 0.0250 0,0239 0.0236 95.4 94.5 73.2-125 0.910 20 Chloromethane 0,0250 0.0210 0.0207 84.2 82.6 55.8-134 1,90 20 ,1,2-Dichlorobenzene 0.0250 0.0267 0.0264 107 106 84.7-118 1.15 20 1,3-Dichlorobenzene 0.0250 0.0286 0.0281 114 112 77.6-127 1.81 20 '1,4-Dichlorobenzene 0.0250 0.0260 -0.0255 104 102 82.2-114 2.05 20 Dichlorodinuoromethane 0,0250 0.0229 0.0224 91.8 89.5 56.0-134 2.47 20 -1,1-Dichloroethane 0,0250 0.0237 0,0236 95.0 94.5 71.7-127 0.470 20 12-Dichloroethane 0.0250 0.0228 0.0228 91.3 91.3 65.3-126 0,0600 20 4,1-Dichloroethene 0.0250 0.0239 0.0234 95.5 93.6 59.9-137 1.93 20 trans-1,2-Dichloroethene 0.0250 0,0253 0.0250 101 100 72.6-125 1.23 20 1,2-Dlchloropropane 0,0250 0,0263 0.0261 105 104 77.4-125 0,750 20 cis-1.3-Dichloropropene 0.0250 0,0273 0.0269 109 108 77.7-124 T45 20 trans-1,3-Dichloropropene 0.0250 0,0247 0.0247 98.8 98.8 73.5-127 0.000 20 Ethylbenzene 0.0250 0.0261 0.0253 104 101 80.9-121 2.93 20 Methylene Chloride 0.0250 0.0223 0.0219 89.1 87.7 69.5-120 149 20 1,1,2,2-Tetrachloroethone 0,0250 0.0282 0.0281 113 113 79.3-123 0.220 20 Tetrachloroethene 0.0250 0.0296 0.0287 119 115 73.5-130 3.32 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporatlon 28091 R L802563 1830/15 21:07 12 of 23 WG830844 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. volatile_ Orga nic Compounds (GC/MS) by Method 624 L802563-01 - Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)11/22/15 0657 - (LCSD)11/22/15 07:17 CP Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec Limits LCS Oualifler LCSD Oualifler RPD RPD Limits z Analyze mg/I mg/I mg/I % % % % % TC Toluene 0.0250 0.0259 0,0254 103 102 77.9-116 1.70 20 LLt-Trichloroethane 0.0250 0,0244 0.0240 97.4 96.1 71.1-129 1,40 20 a SS 1,1,2-Trlchloroe[hane 0.0250 0.0283 0.0276 113 111 81.6-120 229 20 Trichloroethene 0.0250 0.0280 0.0274 112 109 79.5-121 2.47 20 y Trichlorofluoromethane 0,0250 0.0239 0.0233 95.7 93.0 49.1-157 2.85 20 Cn Vinyl chloride 0.0250 0.0237 0,0235 94.8 94.1 61.5-134 0.710 20 /S)Todrene-ds..,r 98.9 99.8 90.0-115 s r (S) Dibromolluoromethane 91.4 91.6 79.0121 Q eo,a- rrifluorotoluene - 106 105 90.4-176 (S) 4-6romolluorobenzene 102 101 80,1120 GI L802395-10 Original Sample (OS) Matrix Spike (MS) Matrix Spike Duplicate (MSD) (OS) 11/22/1513:07 - (MS)11/22/15 09:52 • (MSD)11/22/15 10:11 eAl Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Oualifer MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I men % % % % % 9 Acrolein 0.125 ND 0.106 0.119 85.0 95.0 1 10.0-200 11.1 27.7 SC Acrylonitrile 0.125 ND 0.123 0,135 98B 108 1 49.4-133 9.39 25.3 Benzene 0.0250 ND 0.0219 0.0226 87.5 90.6 1 58.6-133 3.41 20 IBromodichloromethane 0.0250 ND 0.0257 0.0275 103 110 1 69.2-127 6.92 20 Bromoform 0.0250 ND 0.0329 0.0383 132 153 1 66.3-140 J5 15.1 20 Bromomethane 6.0250 ND 0.0187 0.0194 74.7 77.7 1 16.6-183 3.97 20.5 Carbon tetrachloride 0.0250 ND 0.0223 0.0229 89.3 91.8 1 60.6-139 2.72 20 Chlorobenzene 0,0250 ND 0.0276 0.0296 110 118 1 70.1-130 7.14 20 Chlorodibromomethane 0.0250 ND 0,0302 0.0338 121 135 1 71.6-132 J5 11.4 20 Chloroethane 0,0250 ND 0.0202 0.0211 80.9 84.4 1 33.3-155 4.20 20 2-Chloroethyl vinyl ether 0.125 ND 0.0135 0.00833 10.8 6.66 1 5.00-149 J3 471 40 Chloroform 0.0250 ND 0.0228 0.0234 91.2 93.5 1 66.1-133 2.49 20 Chloromethane - 0.0250 ND 0.0170 0,0176 68.1 70.5 1 40.7-139 3.50 20 1,2-Dichiorobenzene - 0.0250 ND 0.0280 0.0333 112 133 1 77.4-127 J5 17.3 20 1,3-Dichlorobenzene 0.02SO ND 0.0300 0.0350 120 140 1 67.9-136 J5 15.6 20 T ZI-Dichiorobenzene 0.0250 ND 0.0270 0.0319 108 128 1 74.4-123 JS 16.5 20 Dichlorodifluoromethane 0.0250 ND 0,0184 0,0192 73.5 76.8 1 42.2-146 4,44 20 4,1-Dichloroethane 0,0250 ND 0.0220 0.0227 88.2 90.9 1 64.0-134 3.06 20 1,2-Dichloroethane 0.0250 ND 0.0221 0.0229 88.2 91.5 1 60.7-132 3.67 20 4,1-Dichlorcethene 0.0250 ND 0.0203 0.0208 81.4 83.2 1 48.8-144 2.23 20 ACCOUNT. PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 IV30/15 21:07 13 of 23 WG830844 QUALITY CONTROL SUMMARY ONELAa.NATIONWIDE. Volatile Organic Compounds (GC/MS). by Method 624 - _ _ L802563-01 L8O2395-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (0S)11/22/15 L':07 • (MS)11/22/15 09:52 • (MSD) 11/22/1510:11 Spike Amount Original Result MS Result Analyte mg/1 mg4 trans-1,2-Dichloroethene 0.0250 ND 9,2-Dichloropropane 0.0250 ND cis-1,3-Dichloropropene 0,0250 ND trans-1,3-Dichloropropene 0,0250 0.000694 Ethylbenzene 0.0250 NO 'Methylene Chloride 0.0250 ND 11,2.2-Tetrachloroethane 0.0250 ND Tetrachloroethen_e 0.0250 ND Toluene 0.0250 ND 1,1,1-Trichloroethane 0,0250 ND 1,1,2-Trichloroethane 0.0250 ND Trichloroethene 0,0250 ND Trichlorofluoromethane 0.0250 ND Vinyl chloride 0.0250 ND (S) Toluene-d8 (S) Dlbromolluoromethone (S) o,o,o-T(iT1uoroto)uene (S) 4-Bromofluorobenzene 0.0251 0.0256 0.0242 0.0251 0,0203 0.0326 0,0284 0.0243 0.0229 0.0286 0.0263 0,0219 0.0198 MSD Result mg/I MS Red. % MSD Rec. Dilution % Rec. Limits MS Oualifler % MSD Oualifier RPD % RPD Limits % 0.0229 88.6 914 1 61.0-132 3,19 20 0.0257 100 103 1 69.7-130 2,62 20 0.0268 102 107 1 71.1-129 4,67 20 0.0262 93,8 102 1 66.3-136 7.96 20 0,0270 100 108 1 _ 62.7-136 7.25 20 0,0209 81.1 83.7 1 - 615-125 3,15 20 0.0385 130 154 1 64.9-145 J5 16.6 20 0.0289 114 116 1 57.4-141 T. 5 20 0.0250 97.4 99.8 1 67.8-124 2.48 20 0.0238 91.6 95.0 1 58.7-134 3.71 20 0.0315 115 126 1 _ 74.1-130 9.62 20 0.0268 105 107 1 48.9-148 1.77 20 0,0227 - 87.7 91.0 1 39.9-165 - 3.67 20 0.0204 79.0 81.8 1 44.3-143 3.40 20 98.7 98.5 90.0115 90.8 92.1 79.0-121 107 107 90.4-116 101 102 _ 80.1-120 - Cp 2Tc 3Ss 4Cn 6Sr 7GI aAl aSc ACCOUNT: PROJECT: SDG: DATErHME: PAGE: Eaton Corporation 28091-R L802563 11/30115 21:07 14 of 23 WG830650 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. Pesticides (GC) by Method EPA 608 _ L802563-01 Method Blank (MB) (MB) 11/23/15 12:17 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0,0000500 Beta BHC U 0.0006184 0.0000500 'Delta BHC U 0.0000197 0.0000500 Gamma BHC U 0.0000176 0.0000500 4,4-DDD U 0.0000170 0.0000500 4,4-DDE U 0.0000164 0.0000500 4,4-DDT U 0,0000177 0.0000500 _ _ Dieldrin U 0.00000731 0,0000500 Endosulfan 1 0.0000179 0.0000500 Endosulfan 11 _ _U U 0,0000176 0.0000500 Endosulfan sulfate U 0.0000196 0.0000500 _ Endrin U 0.0000189 0.0000500 'Encirin aldehyde U 0,0000142 0.0000500 Endrin ketone U 0.0D00170 0.0000500 Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorohenzene U 0.0000134 0,0000500 Methoxychlor U 0.0000193 0,0000500 'Chlordane U 0,0600977 0.000500 Toxaphene U 0.000168 0.000500 (S) Decochlombiphenyl 76.1 10.0-156 (S) ietrachloro-m-x7lene 83.3 13.9-137 Method Blank (MB) (MB)11/24/15 09:44 MB Result MB OualiOer MB MDL MB RDL Analyte mg/l my/I mg/I PCB 1260 U 0,000120 0,000500 PCB 1016 U 0,000100 0.000500 PCB 1221 U 0.0000730 0.000500 PCB1232 _ 0.0000420. 0,000500 _ PCB 1242 _ _U U _ 0.0000470 0,000500 ;PCB 1248 1 U 0.0000860 0,000500 PCB 1254 U 0.0000470 0.000500 ACCOUNT: PROJECT: SDG: Eaton Corporation 28091-R L802563 DATE/TIME: 1V30/15 21:07 PAGE: 15 of 23 WG830650 QUALITY CONTROL SUMMARY ONE LAa. NATIONWIDE. Polychlorinated Biphenyls_(GC) by Method EPA-608 _ L802563-01 Method Blank (MB) (ME) 11/24/15 09:44 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I (S) Demchloroblphenyl 950 10.0-156 (S)Tetrachloro-m-xylene 103 139-137 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS)11/24/15 09:56 - (LCSD) 11/24/15 10:09 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % PCB 1260 0,00250 0.00303 0.00303 121 121 47.7-149 0,0300 28.8 PCB 1016 0.00250 0,00262 0.00269 105 108 24.7-128- 2,67 34.9 (5) Decochlorobiphenyl 94.3 93.0 100-156 (S) Tetrachloro-m-xylene 104 105 13,9 137 ACCOUNT: PROJECT: SDG'. Eaton Corporation 28091-R L602563 DATE/TIME: 11/30AS 2107 PAGE: 16 of 23 WG831669 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 625 L802563-01 Method Blank (MB) (MB) 11/25/1513:58 MB Result MB Oualifer MB MDL MB RDL Analyte ri mgll mg/I ONE LAB. NATIONWIDE. 0 Acenaphthene U 0.000316 0.00100 'Acenaphthylene U 0.000309 0,00100 Anthracene U 0.000291 0,00100 Benzidine U 0.00432 0.0100 Benzo(a)anthracene u 0.0000975 0.00100 'Benzo(b)Fluoranthene U _ _ 0.0000896 0.00100 Benzo(k)fluoranthene U 0.000355 0.00100 !Benzo(g,h,i)perylene U 0.000161 0.00100 Benzo(a)pyrene U 0.000340 0.00100 Bis(2-chlorethoxy)methane U 0.000329 0,0100 Bis(2-chlorcethyl)ether U 0,00162 0.0100 '.Bis(2-chloroisopropyl)ether U 0.000445 0.0100 4-Bromophenyl-phenylether U 0,000335 0,0100 '2-Chloronaphthalene U 0.000330 0.00100 4-Chlorophenyl-phenylether U 0.000303 0.0100 '.Chrysene U 0.000332 0.00100 Dibenz(a,h)an,hracene U 0.000279 0.00100 3,3-Dichlorobenzidine U O.00202 0,0100 2,4-Dinitrotoluene - U 0.00165 0,0100 2,6-6initrotoluene U 0.000279 0,0100 Fluoranthene U 0.000310 0.00100 iFluorene L) 0.000323 0.00100 _ Hexachlorobenzene U _ 0.000341 0.00100 iHexachloro-13-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0.00233 0,0100 Hexachloroethane _U_ 0.000365 0.0100 _ _ Indeno(1,2,3-cd)pyrene _ U 0.000279 0.00100 Isophorone _ L1 _ _ 0.000272 0.0100 _ Naphthalene U 0.000372 0.00100 :Nitrobenzene U 0.000367 0.0100 _ n-Nitrosodlmethylamine _ U 0.00126 0.0100 1,2-Diphenylhydrazine U 0,000318 0.0100 n-Nitrosodiphenylamine U 0.000304 0,0100 n-Nitrosodi-n-propylamine U 0.000403 0,0100 Phenanthrene U 0.000366 0.00100 IBenzylbutyl phthalate U 0.000275 0.00300 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091 R L802563 11/30/15 21.07 17 of 23 WG831669 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. x _Semi Volatile Organic Compounds _ (GC/MS)_by.Method 625 L802563-01 Method Blank (MB) 1 (MB) 11/25/1513:56 Analyte MB Result mg/I MB Oualifer MB MDL mg/I MB RDL Mgt 8is(2-ethyl1­exyl)phthalate U 0.000709 0.00300 Di-n-butyl phthalate U _ 0.000266 0.00300 Diethyl phthalate U 0.000282 0,00300 Dimethyl phthalate U 0,000283 0.00300 Di-n-octyl phthalate U 0.000278 0.00300 'Pyrene - U 0.000330 0,00100 1,2,4-Trichlorobeozene U 0,000355 0,0100 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chlorophenol U 0.000283 0.0100 2,4-Dichlorophenol _ U 0.000284 0.0100 2,4-Dimethylphenol _ U 0.000624 0,0100 4,6-Dinitro-2-methylphenol U 0.00262 0,0100 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0,000320 0.0100 4-Nitrophenol U 0.00201 0.0100 Pentachlorophenol U 0.D00313 0.0100 Phenol U O.000334 0.0100 24,6-Trichlorophenol U 0.000297 0.0100 (S) Nitrobenzene-d5 60.3 21.8-123 (S) 2-Fluorobiphcnyl 64.0 295-131 (S)p-Terphenyl-04 77.4 293-137. _ (5) Phenol-d5 33.6 5.00-70.1 (S) 2-Fluorophenol _ 44.8 10.0-77.9 (S) 2.4,6-Tribromophenol 662 11.2-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/25/15 1112 • (LCSD) 11/25/1513:35 Spike Amount LCS Result LCSD Result LCS Rea. LCSD Rec. Rea. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mgA mg/I mg/I % % % % % Acenaphthene 0.0500 0.0303 0.0292 60.5 58A 38.7-109 3.57 21.5 Acenaphthylene 0.0500 0.0322 0.0315 64.5 62.9 36.0-106 2.41 21 Anthracene 0.0500 0.0346 0.0345 69.2 69.1 43.6-113 0.190 18.8 Benzidine 0.0500 0,0319 0.0325 63.8 65.0 10.0-165 1,83 40 Benzo(a)anthracene 0,0500 0.0334 0.0324 66.9 64.8 51.2-112 3.12 20 :Benzo(b)Fluoranthene 0,0500 0.0336 0.0348 67.2 69.6 47.6-111 3.53 20 V C ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 2107 18 of 23 WG831669 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds.-(GC/MS). by Method 625 L802563-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/25/15 13:12 • (LCSD)11/25/15 13,35 _ CD] C_ Spike Amount LCS Result ;LCSD Result LCS Rec. LCSD Rec. Rec. Limits .LCS Qualifier LCSD Qualifier RPD RPD Limits 2 Analyte mgll mgh "mgll % % % % % TC Benzo(k)fiuoranthene 0.0500 0.0359 0.0365 71.8 73.0 49.4-114 1.56 20 Benzo(g,h,i)perylene _ 0.0500 0.0361 0.0359 72.1 71.7 45.2-117 0.550 20 3$S Benzo(a)pyrene 0.0500 0.0341 0,0350 58.3 '70.0 45.6-106 _ 243 20 Bis(2-chlorethoxy)methane 0.0500 , 0.0318 0.0302 63.7 60.3 37.2-111 5.41 24.1 a Bis(2-chioroethyl)ether 0.0500 0.0298 0.02B1 59.6 56.2 22.6-108 5,76 27.9 Cn Bis(2-clip1misopropygether 0.0500 0.0347 0.0303 69.3 60.5 32.9-100 13.6 25.1 4-Bromophenyl-phenylether _ 0.0500 0.0330 0.0344 66.0 68.8 _ 40.7-116 4.12 21 Fri '2-Chloronaphthalene 0.0500 0.0314 0.0305 62.8 60.9 33.E-105 3.00 23 1,2-Dipheny1hydrazine 0.0500 0.0330 0.0339 66.1 673 37.6-111 2.56 21.1 4-Chlorophenyl-phenylether 0,05.00 0.0310 0.0308 62.0 61.6 39.0-113 0,660 20.9 Chrysene 0,0500 0.0326 0.0324 65.2 643 54.6-120 0.610 20 Dibenz(a,h)anthracene 0.0500 0.0343 0.0354 68.7 70.8 42.8-118 2,99 20 7GI 3.3-Dichlorobenzidine 0.0500 0.0375 0.0357 74.9 71.4 27.2-142 4.78 22.3 '.2,4-Dinitrotoluene 0,0500 0.0376 0.0364 75.3 727 31.2-105 3.47 22 a 2,6-Dinitrotoluene 0.0500 0.0378 0.0370 75.5 74.0 30.6.106 2.02 23.1 AI Fluoranthene 0.0500 0.0344 0,0348 683 69.6 45.9-115 1.18 20 _ Fluorene _ _ 0.0500 0.0313 0.0315 62.6 63.1 41.0-112 0.770 20.2 SC iHexachlorob_enzene 0.0500 0.0358 0.0364 71.E 72.8 36.5-116 1.6E 20.1 Hexachloro-1,3-butadiene 6.0500 0.0269 0.0252 53.8 50.5 16.1-lD4 _ 6.27 31.2 Hexachlorocyclopentadiene 0.0500 0.0155 0.0150 31.0 30.1 10.0-121 3.12 27.9 Hexachloroethane 0.0500 0.026E 0.0242 _ 53.2 48.3 16.5.89.8 9.68 30.7 Indeno(1,2,3-Cd pyren_e _ 0,0500 0.0358 _ , 0.0364 71.5 72.9 45.0-116 1,88 20 Isophorone 0.0500 0.0356 `0.0344 71.2 68.9 35.4-112 3.38 21.5 'Naphthalene 0.0500 0.0282 0.0258 56.3 51.5 32.2-101 8.86_ 23.8 Nitrobenzene _ 0.0500 0.0336 _ 0.0306 67.1 61.2 314-106 919 257 m-Nitrosodimethylamine 0.0500 0.0181 0.0173 36.3 .34.5 10.0-80.1 5.00 37.5 n-Nitrosodlphenyla mine 0,0500 0.0336 0.0345 67.1 69.0 44A-113 2.81 20 n-Nitrosodi-n-propylamine 0.0500 0.0294 0.0297 58.7 59.3 33.2-106 1.05 23.7 Phenanthrene 0.0500 0.0330 0.0332 66.0 66.3 46.4-113 0.440 20 Benzylbutyl phthalate 0.0500 0,0368 _ 0.0367 73.5 73.4 31.8-123 0.150 20.7 Bis(2-ethylhexypphthalate _ 0.0500 0.0369 _ 0.0372 73.8 74.4 36.9-134 0.750 23.6 DI-n-butyl phthalate_ 0.0500 0.0368 0.0370 73.6 73.9 41.8-120 0.350 20.2 Diethyl phthalate 0,0500 0.0371 0.0375 74.3 74.9 36.5-129 0.860 20 Dimethyl phthalate _ _ _ 0.0500 0,0367 0.0368 73.5 73.7 35.3-128 0.210 20.8 Di-n-octyl phthalate 0.0500 0.0363 0.0367 72.6 73.4 39.7-112 1,13 21.1 IPyrene 0.0500 0.0319 0,0322 63.8 64.4 463-117 1.02 20 ACCOUNT: PROJECT: SDG: DATE/TIME' PAGE: Eaton Corporation 28091-R L802563 11/30/15 21:07 19 of 23 WG831669 QUALITY CONTROL SUMMARY ONE LAB. NATI0NWIDE. Semi Volatile_ Organic Compounds-(GC/MS) by. Method 625 L802563-01 - Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) 11/25/1513:12 - (LCSD) 11/25/1513:35 Spike Amount LCS Result 'LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD Oualifier RPD RPD Limits z Analyze al mg/I mgp % % % % % TC 1,2,4-Trichlorobenzene 0.0500 0.0270 0.0246 53.9 49.3 22.9-96.1 8.92 27.5 4-Chloro-3-methylphenol 0.0500 0.0360 0.0365 72.0 73.0 35.7-100 1.31 22.9 - 3 SS 2-Chlorophenol 0.0500 0.0322 0.0298 644 59.7 26.2-91.5 7.60 26.5 2,4-Dichlorophenol 0,0500 0.0353 0.0331 70.6 66.2 31.4403 6.45 24.9 a 24-Dimethylphenol 0.0500 0.0355 0.0301 70.9 60.2 3L9-107 16.3 25.7 Cn 4,6-Dinitro-2-methylphenol 0.0500 0.0383 0.0349 76.6 59.9 18.4-148 9.25 24A 2,4-Dinitropheno) 0.0500 0.0258 0.0191 51.5 38.1 242-128 J3 29.9 20.5 6 $r 2-Nitrophenol _ _ 0.0500 0.0365 0.0322 73.0 64.4 25.9-106 12.5 26.9 4-Nitrophenol 0.0500 0.0188 0.0171 37.6 34.3 10.0.52.7 9.07 40 Pentachlorophenol 0.0500 0.0372 0.0376 74.4 75.1 10.9-97.4 0.990 35.1 Phenol 0,0500 0.0187 0.0180 37.4 36.0 _ 10.0-5Z9 3,88 35 2,4,6-Trichlorophenol 00500 0.0362 0.0346 72.5 69.7 29.8-107 3.94 24.1 RG (S) Nitrobenzene,d5 64.6 62.0 21.8-123 (S)2-Fluoroblphenyl (S)P-Terphenyl-d14 _ 66.1 68.8 64.7 69.0 29.5.131 29.3-137 (S) Phenol-d5 361 35.0 5.00-70.1 (s)2-FluoroPhenol 49.2 472 10.0779 (S)2,4,6-Tribromopheool - - - - - - - 76.2 713 112-130 $C ACCOUNT: PROJECT: Eaton Corporation 28091-R SDG'. L802563 DATE/TIME'. 11/30/15 21.07 PAGE: 20 of 23 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. MDL Method Detection Limit. RDL Reported Detection Limit. ND,U Not detected at the Reporting Limit (or MDL where applicable). RPD Relative Percent Difference. '(dry) _ Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate, used to evaluate analytical efficiency by measuring _ recovery. Surrogates are not expected to be detected in all environmental media. Rec. Recovery. SDL _ Sample Detection Limit. MOL Method Ouantitation Limit. Unadj. VOL Unadjusted Method Ouantitation Limit. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J3 The associated batch OC was outside the established quality control range for precision. J4 The associated batch OC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination, spike value is high. a ACCOUNT: PROJECT: 80G: DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21,07 21 of 23 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. 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State Accreditations Alabama _ _ 40660 Nevada _ TN-03-2002-34 Alaska --_ UST-080 New Hampshire _ 2975 Arizona _ AZO612 _--_ New Jersey-NELAP Arkansas 88-0469 -__ New Mexico _TN002 TN00003 carfornia _ _ _ _ ______ 01157CA Colorado TN00003 Conneticut _PH-0197 _ --_--_-_—____ Florida - -- E87487 Georgia_ NELAP Georgia' 923 Idaho _ _ _ _ _ TN00003 Illinois _ _ _ _ 200008 Indiana C-TN-01 Iowa _ 364 Kansas E-10277 Kentucky_ _ _____ _ 90010_ Kentucky' _ 16 Louisiana A130792 Maine TN0002 Maryland 324 Massachusetts M-TNO03 Michigan _ __ _ 9958 Minnesota _ _047-999-395 Mississippi _ _ _ TN00003 Missouri _ 340 Montana CERT0096 Nebraska _ _ _ NE-OS_15:05 Third Party & Federal Accreditations North Carolina Env375 North Carolina DW21704 North Carolina' 41 North Dakota R-140 Ohio-VAP CL0069 Oklahoma _ __ 9915 Oregon TN200002 Pennsylvania 68-02979 Rhode Island _ _ _ _ 221 South Carolina _ ____ ________ 84004______ South Dakota _ _ War Tennessee 14 2006 Texas - --_ - -_ -- T104704245-07-T% _ ----—LA80152 Texas' Vermont_ VT2006 _ Virginia _ _ 109_ Washington__ __ __ __ _ __ _ C1915 West Virginia 233 Wisconsin _ 998C939910 Wyoming_.____ ___ __ _ A2LA A2LA-ISO 17025 1461.01 AIHA 100789 A2LA - 150 17025' _ 1461.02-� - — - - � _ DOD --- _ — 146t01 Canada _ _ _ 1461.01 _ _ _ _ USDA 5-67674 EPA-Crypto_ -1100003�______—__.___._ Drinking Water ' Underground Storage Tanks " Aquatic Toxicity ' Chemical/Microbialogical ' Mold "'Accreditation not applicable Our Locations ESC Lab Stlences has sixty-four client suppon centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. N/A O Ml" ND OR • M.V T 'D SO T Wh Y T' NY vm • Tnr T T • T GA t NE • T T T L•1T • NV OT T T T• • T T R TL� U T CO • KS MV' • wV V KY��- T T T T T.�g T •: •`T N +'Z NM Or T AIT • IF SC T M$ AL GA T T Tx T LA T •-�rT T ~• • AK T • T • .O FL �.o • �_ • T Hi 1 -r' N.E ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L802563 11/30/15 21'07 22 of 23 Rllling information: Ana sls/Container/Preservative Chain of Custody Pare_et_ Company Name/Address: r C Eaton Corporation NA Financial �V Po Box MOM- J 2564 Durham Rd Cleveland, OH 44181-8024 1 L•�•B 5 C•�•fi N-C•R-9 Roxboro, NC 27573 4 N Email To: 6. wmume�tunm Report to: _ rfd O Pne".:ms.ru vss Dustin LaClalr ustinlaciairQEaton.com v u i z �^ ^•marcnsau iu ala]aLiri] O- project eltYeRoxboro,.NC _5 H` ° ;d fl: •- - Eaton Corp.,Semi-Annual Stormwater Collected: z Descnptntm: �� " LLI OS l d '� ON. •m �y• > 0 C100l Phone 336.599-1141,m -28091SW 280n91-R EATONRNC- E E to to z Nt o A 4 n�anum£ATONRNC Collected by.lprtntl: fitelFadlltVlD!1 P.O.n _ S •y - s ff OL �'�I N ILE o �oE t Tenrl Collected by (signature).`te Fesults Needed'- O .- ,t? i. a�%C ` p�CloBin Hush? 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