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HomeMy WebLinkAboutNCG030006_MONITORING INFO_20190326STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V DOC TYPE ❑ HISTORICAL FILE � MONITORING REPORTS DOC DATE ❑ Dol � V -'�;060 YYYYM M DD Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 0 0 0 6 FACILITY NAME ABB Inc. - Edkecombe COUNTY Edgecombe PERSON COLLECTING SAMPLES Geoffrey Murphrey LABORATORY Pace Analytical National Lab Cert. fi 41 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD Q Jan -June ❑ July -Dec or ❑ Monthly' (month) RECEEN9SCHARGING TO CLASS ❑ORW ❑HQW [—]Trout❑PNA C ll��L {{�^ 0 ❑Zero -flaw ❑Water Supply ❑SA MAR 2 B 2019 QOther NSW CEN I}.WL FILE PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTIOIH n No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> - - 100 mg/L or 50 mg/L 6.0 —9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 02/20/19 0.3 4.15 8.7 0.0028 <0.005 <0.050 <5.88 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?Z Outfall No. Date Sample , Collected (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B . See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports/ to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are signifiSant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012 Page 3 of 3 aceAnalytical Naaonzn cenow for res!;ng 6lo nrau0n x "1 ANALYTICAL REPORT March 01. 2019 Piedmont Geologic Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L1072167 02/21/2019 1913 ABB Inc. PINETOPS, NC Pete Dressel 6003 Chapel Hill Rd Ste 145 Raleigh, NC 27607 Entire Report Reviewed By: r dl Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable. sampling conducted by Pace National Is performed per guidance provided In laboratory standard operating procedures: 060302, 060303. and 060304. Y TABLE OF CONTENTS ONE LAB. NATIONWIDE. 0 Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results OUTFALL-001 L1072167-01 Oc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664E Metals (ICP) by Method 200.7 Metals (ICPMS) by Method 200.8 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 CJ 2 4 4 3S$ 5 5 , Cn 6 6 Sr 7 60c 8 9 7GI 10 11 AI 12 9Sc ACCOUNT: PROJECT: SDG: DATEMME: Piedmont Geologic 1913 L1072167 03/0V1914:14 PAGE: 2 of 12 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time OUTFALL-001 L1072167-01 WW Geoffrey Murphrey 02120/1909:45 02121/1908:45 a Method Batch Dilution Preparation Analysis Analyst Location date/time dateltime Gravimetric Analysis by Method 2540 D-2011 WG1240467 1 02/23/1909:59 02/23/1911:07 AEC Mt. Juliet, TN Wet Chemistry by Method 1664E WG1242277 1 02/26119 09:21 02/26/1915:40 DAD Mt. Juliet, TN Metals (ICP) by Method 200.7 WG1240181 1 02/27/19 06:22 0212711918:22 TRB Mt. Juliet, TN Metals (ICPMS) by Method 200.8 WG1241620 1 02127/19 09:48 03/0111910:34 JPD Mt. Juliet, TN nCn SSr H �GI CAI BSc ACCOUNT: PROJECT: SDG: DATE7TIME: PAGE: Piedmont Geologic 1913 - L1072167 03/0111914:14 3 of 12 CASE NARRATIVE ONE LAB. NATIONWIDE. 0 the All sample aliquots were received at the correct temperature, in the proper containers, with appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Ouality Control are within established criteria except where addressed in this case narrative, a non-conformance form 3 or properly qualified within the sample results. By my digital signature below, I affirm to the best of my S5 knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. aSr Heather J Wagner AI Project Manager 9Sc ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Piedmont Geologic 1913 L1072167 03101/1914,14 4of 12 OUTFALL-001 SAMPLE RESULTS - 01 ONE LAB, NATIONWIDE. Collected date/time: 02/20/19 09:45 L1072167 Additional Information l-J Result Units Analyte C pH (On Site) 8.7 su Gravimetric Analysis by Method 2540 D-2011 ass Result Qualifier ROL Dilution Analysis Batch Analyle ugA ugA date/time ° Cn Suspended Solids 4150 3850 1 02/231201911:07 WG1240467 Wet Chemistry by Method 1664E Result Qualifier RDL Dilution Analysis Batch VQC Analyte ugA ugA date/time TPH - Oil & Grease NO 5B80 1 02/26/201915:40 WG1242277 GI Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch AI Analyze ug/I ugA date/time Lead NO 5.00 1 02/27/201918:22 VVGi240181 9 Zinc NO 50.0 1 02/27/201918:22 WG1240181 $C Metals (ICPMS) by Method 200.8 Result Qualifier RDL Dilution Analysis Batch Analyze UV ugA date/time Copper 2.80 B 1.00 1 03/01/201910:34 WG1241620 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Piedmont Geologic 1913 L1072167 03/011914:14 5 of 12 WG1240467 Gravimetric Analysis by Method 2540 D-2011 Method Blank (MB) (MB) R3386413-1 02/23/19 11:07 M8 Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ugll Suspended Solids U 350 2500 L1072166-01 Original Sample (OS) • Duplicate (DUP) QUALITY CONTROL SUMMARY L1072167-01 (OS) L1072166-01 02/23/19 11:07 • (DUP) R3386413-3 02/23/19 11:07 Original Result DUP Result Dilution DUPRPD DUP Qualifier Limi DUPtRPD Analyte ug/I ug/I % % Suspended Solids`W 37000 37500 1 1.34 5 L1072187-04 Original Sample (OS) • Duplicate (DUP) (OS) L1072187-04 02/23/19 11:07 • (DUP) R3386413-4 02/23/19 11:07 Original Result DUP Result Dilution DUP RPD DUP Qualifier D IPIRPD Urnin.. a,.., nn4 un/I % % Suspended Solids 54000 46000 1 16.0 J3 5 Laboratory Control Sample (LCS) ONE LAB. NATIONWIDE. 0 -Tc 3S$ 4Cn ssf �GI ,A cSC (LCS) R3386413-2 02/2311911:07 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyze ug/I ugh % % Suspended Solids 773000 800000 103 85.0-115 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Piedmont Geologic 1913 L1072167 03/01/19 14:14 6 of 12 WG1242277 QUALITY CONTROL SUMMARY Wet Chemistry by Method 1664B L1072167-01 Method Blank (MB) (MB) R3387027-1 02/26/19 15:40 MB Result MB Qualifier MB MDL MB ROL Analyte ugll ugll ugll TPH - Oil & Grease U 725 5000 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3387027-2 02/26/19 15:40 • (LCSD) R3387027-3 02/26/1915:40 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ugll % % % % % TPH - Oil & Grease 20000 18400 19600 92.0 98.0 64.0-132 6.32 34 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pledmom Geoloolc 1913 L1072167 03/0111914:14 7 of 12 WG1240181 QUALITY CONTROL SUMMARY Metals (ICP) by Method 200.7 L1072167-01 Method Blank (MB) (MB) R3387441-1 02/27/19 17:38 MB Result MB Qualifier MB MDL M8 RDL Analyte ugn ugll ugA Lead U 2.00 5.00 Zinc U 3.40 50.0 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3387441-2 02/27/19 17:40 • (LCSD) R3387441-3 02/27/19 17:43 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec, Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyle ugn ugli ugll % % % % % Lead 1000 1020 1050 102 105 85.0-115 2.70 20 Zinc 1000 1020 1040 102 104 85.0-115 1.71 20 L1071651-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike. Duplicate (MSD) (OS) L1071651-01 02/27/19 17:45 • (MS) R3387441-5 02/27/19 17:50 • (MSD) R3387441-6 02/27/19 17:53 Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits All ugA ug/I ugA fri % % % % % Lead 1000 NO 1030 1010 103 101 1 70.0-130 2.19 20 Zinc 1000 ND 1020 999 101 99.4 1 70.0-130 1.70 20 L1072196-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1072196-01 02/27/19 17:56 - (MS) R3387441-7 02127/1917:56 - (MSD) R3387441-8 02/27/1918:01 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec. Limits MS Oualifier MSD Qualifier RPD RPD Limits All ugA ug/I ugA ugA % % % % % Lead 1000 NO 1090 1080 109 108 1 70.0-130 0.679 20 Zinc 1000 58.8 1120 1110 106 105 1 70.0-130 0.729 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Piedmont Geoloqic 1913 L1072167 03/01/1914:14 8 of 12 WG1241620 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICPMS) by Method 200.8 L1072167-01 Method Blank (MB) Cp (MB) R3387924-1 03/01/19 10:20 MB Result M8 Qualifier MB MDL MB RDL ,TC Analyte ug/I ug/1 ug/1 Copper 0.790 J 0.270 1.00 3SS Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) , Cn (LCS) R3387924-2 03/O1/19 10:25 - (LCSD) R3387924-3 03/01/1910:29 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugll ug/I ug/I % % % % % Sr Copper 50.0 52.7 52.6 105 105 85.0-115 0.250 20 L1O72167-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 7GI (OS) L1072167-01 03/01/1910:34 • (MS) R3387924-5 03/01/1910:43 • (MSD) R3387924-6 03/01/1910:48 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyze ugll ug/l ug/I ugll % % % — % % Copper 50.0 2.80 55.5 58.0� 105 110 1 70.0-130 4.43 20 ISc L1O72874-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1072874-01 03/01/1910:52 - (MS) R3387924-7 03/O1/19 10:57 • (MSD) R3387924-8 03/01/19 11:01 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyze ug4 ug/1 ug/l ugll % % % % % Copper 50.0 6.38 59.0 57.6 . 105 102 1 70.0-130 2.43 20 ACCOUNT: PROJECT: SOG: DATE/TIME: Piedmont Geoloaic 1913 L1072167 03/O1/191414 PAGE: 9 of 12 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. 0 Guide to Reading and Understanding Your Laboratory Report o The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions FTC] MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). 3 Ss RDL Reported Detection Limit. Rec. Recovery. a Cn RPD Relative Percent Difference, SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). s Sr The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes Analyte reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the QC standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the Dilution laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field. the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyze being reported. Successful OC Sample analysis will target all analytes recovered or duplicated within these ranges. aA' The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control Original Sample sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional Information concerning the result71 SC Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cl observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. This section of the report includes the results of the laboratory quality control analyses required by procedure or Quality Control analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not Summary Qc) being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and Sample Summary (Ss) times of preparation and/or analysis. Qualifier Description B The same analyte is found in the associated blank. J The identification of the analy[e is acceptable; the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. ACCOUNT: PROJECT: SDG: DATEfIME: PAGE: Piedmont Geologic 1913 L1072167 03/01/1914.14 10 of 12 ACCREDITATIONS & LOCATIONS Pace National Is the only environmental laboratory accreditedlcertifed to support your work nationwide from one location. accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and ' Not all certifications held by the laboratory are applicable to the results reported in the attached report. ' Accreditation is only applicable to the lest Methods specified an each scope of accreditation held by Pace National. State rA.cctedit8tions la Alabama 40660 _ _____—___. Alaska 17-026 Arizona AZOfi12 Arkansas 88-0469 2932 _California Colorado _ TN00003 Connecticut Florida Georgia PH-0197 E87487 __. NELAP Georgia'— — _ _ - 923 Illinois_ 200008 Indiana C-TN O1 Iowa _,._ .... 364 .._. Kansas E-10277 Kentucky1°__ 90010 Kentucky _ 16 _ Louisiana A130792 LA180010 _Louisiana Maine TN0002 Maryland 324 Massachusetts M-TNO03 Michigan 9958 _. Minnesota 047-999-395 Mississippi .._......... TN00003 _.....__... _.......... _.._... ___. ONE LAB. NATIONWIDE. One phone call, one point of contact, one laboratory. No other lab Is as boratory is comparable to the collective totals ofthe network The model is conducive to accelerated productivity, decreasing CO prompt service allows us to be YOUR LAB OF CHOICE. 1Tc 3 Nebraska NE-OS-15-05 SS Nevada TN-03-2002-34 New Hampshire -._._ _— __. New Jersey NELAP TN002 TN-0 Cn New Mexico Me New York North Carolina Env375 _ 6 Sr rth Carolina DW21704 --No ._...._ __.. North Carolina _ __. 41 North Dakota _ R 140 �QC Ohio VAP CL0069 Oklahoma 9915- Oregon_ TN200002 Pennsylvania 68 02979 Rhode Island LA000356 South Carolina _ 84004 South Dakota--- _ Na Tennessee 2006 _...... texas ..... ...._. _.. i104704245 1815 _- g SC Texas'— -- --- LABO152--- Utah TN00003 Vermont _ VT2006 _Virginia ------�� — 460132 Washington C847 West Virginia 233 Missouri 340 __.._ Wisconsin ........_._.. __-_ . _ . _........ .. _........... 9980939910 ... ..___._.... Montana _._ ____..... .... ....._._.. ._.__._". CERT0086 Wyoming__ AKA _ Thll'td Party Cr9C.ril i,)i Accreditdticnis A2LA-ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA-ISO 7025° 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA Crypto TN00003 'Drinking Water 'Underground Storage Tanks 'Aquatic Toxicity 4Chem Ica l/Microbiological 'Mold `Wastewater Me Accreditation not applicable Our LocS%ons Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central Laboratory. NIA OR IAT f NO 4 ID SO o OAC NV ) DT ' R�AZ Ntl OK b AK t \ T O HI ME MN ill = NY tdI IA 4 4 PA I • l o OH T `JN MO T VA� p^KY • r�T AR • SC • 615 AZ GA LA _ FL ACCOUNT: PROJECT: Piedmont Geologic 1913 SDG: DATETIME: PAGE: L1072167 03/01/19 14:14 11 of 12 • Billing Information: Analysis Chain of Custody Pace _ol PiedmontGeologic" g Accounts Payable Pre: d'k 6003 Chapel Hill Rd Ste 145 6003 Chapel Hill Rd Raleigh, NC 27607 Ste 145 Raipioh Nr 776n7 t �= 1t0a5leearon 0.d 1.1bkt Tv 3jlil 1 Report to: Email To: pjdressel@pledmontgeoiogic•com Pete Cressel Imurphrey@pledmongeoiogic.com a . tret _ PMaa. tts-na-ssu n - O u' ; aeoaa. aoo Tn.sess F e1S y5&5a59 1] City/State Project • Description. ASO Inc. Collected: ,.�.� A)L - d . - t R �O�LU7 E235 Phone:919-854.9700 Client Project R Lab Project R PIEGEO-ABB Fax: 919-854AS32 O. Collected by (print)-: - Site/Facility to If P.O.f! Acctnum:PIEGEO ` p� iih-P,Y lvtld+ tfi PINETOPS,.NC ' j ti U • eb' O- ' d• a` o '' Z ' f` TempltifiM29400 4', 11 ° Prelogin: P679700; "' ! C ected by i,nature)- Rush? (Lab MUST Be Notified) Quote R •'No. _ Same Oay _. Five Day Next Day Day Iliad OnNi Date Results Needed p, . U" Z X LI TSR.873-Heath FWagner. . Irrlmedi _5 _Two Day _10 Day Iliad Only) Z`. S i -- PBI O Packed on ice N_ Y� _Three Day of d','; CW" l7 O a J• +, 'un ..,. Stiippe Via:F dE%Ground Sample ID Comp/Grab Matrix' Depth Date Time firs Rrmarb Samele a the onhl .. - OUTFALL-001 n '- (� � WW 2aO 3 xr X X de .ri a r.. t 'Matrix: Remarks: +IMF '� c r i R tot of COC Sae 1,. PreaeutlinGaci P _Y _N_ SS - Soil AIR - Air F- filter 'y pH Temp CCC Sf gncdlAccurace:? , r{" X_y GW- Groundwater B- Bioassay Flow_ Other Bottles arrive lntec T N Cotroct' bottles 'used:'t •r _D WW-Wastewater OW - Drinking Water Samples reumedva ( �nd.tiS- .,, O ( `_ sufficient volume aertt ' 1y _N 11 s1t A ii� a t ' .. OT - Other q /• _UPS Q Fed£x _Courler Trackin p 1 Y/� 7, 101 `- - 8 l 1"L ' VOA zero Readapace:. ,1 Y .N Preservation Correcd/Checked:'�T` N rz n� 4a,ln i{ {}. f[I hF ;F q q fished nawrej Date: Time. Received by. (S -ur Trip. Blank Received_:_ Yes / N - HCL/MeoH n RI �q �3�f� TBR {i Ifpreservat(onrequiredby Login:.Date/rime-' _ ISig / Date: Time: Rec dby' atur Temp: '� Bottles Recerred: cur y: - Rin ' elature) Date: Time: Received fo ab by: nature) -.. Date: .Time Hold Condiuo r !f,NCF / 61s, Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03 0 0 0 6 FACILITY NAME ABB Inc. - Edgecorn e COUNTY Edgecombe PERSON COLLECTING SAMPLES Geoffrey Murphrey LABORATORY Pace Analytical National Lab Cent. # 41 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑X July -Dec CE�v� or ❑ Monthly' (month) RE t V TS HARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA 0 16 ZQ ❑Zero -flow ❑Water Supply ❑SA L-FILES ®Other NSW CENT SEC -VIOLA pWR PLEASE REMEMBER TO SIGN ON PAGES ZAND/OR 3 4 No discharge this period: Outfal6No Date Sam ,le pr - Collected (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids p pH'Co ;'pper Standard units' -, _ , - Lead Zinc N on -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss - Benchmarks ---> _. - r 50 m L ° 6.0 - 9.0 0.007 m L g/ 0.03 mg/L�_� 0.067.mg/L . - ;`35 mg/L'.?�, 1;,mg/L ;y 001 10/11/18 0.8 <6.75 8.8 0.00135 <0.005 <0.050 <5.56 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." -A . F 1 Name (Print name) Title Print title r (Si nature) '(Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/U' where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. FI a:_ L _ .&._ - Outfall No. ' Date`Sampie Collected' (mo/dd/yr) - 24-hour rainfall amount, ' Inches , .. Non-polar,0&G/TPH by „CEPA °1664 SGT-.HEM ( ) LJ IVU UIJLIIUI Total Suspended Solids „ ., ,. + L,C LIII� JJUIIUU. H sr r P `Benchmarks 100 mg/L or 50 mg/L* 6.0-9.0SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 aceAnalytical Nabbnal Cenfarlar Tazarg B lonowdon ANALYTICAL REPORT October 22. 2018 Piedmont Geologic Sample Delivery Group: L1034475 Samples Received: 10/13/2018 , Project Number: -1751 Description: ABB Inc. Site: _.PINETOPS, NC Report To: Pete Dressel 6003 Chapel Hill Rd Ste 145 Raleigh, NC 27607 Entire Report Reviewed By: Heather J Wagner Project Manager Results relate only to the items tested or calibrated and are reposed as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National �- Is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 0603K ti Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copv of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results /or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are signific nalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (S�gnature of Permi(tee) Da e Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 TABLE OF CUNTENT S ONE LAB. NATIONWIDE. 4R Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results OUTFALL-001 L1034475-01 Qc: Quality Control Summary Gravimetric Analysis by Method 2540 D-2011 Wet Chemistry by Method 1664E Metals (ICP) by Method 200.7 Metals (ICPMS) by Method 200.8 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 2 �F 3 4 5 3SS 5 6 QCr 6 SSr 7 6 8 QC 9 rGI 10 11 eAl 12 ACCOUNT: PROJECT: SDG: DATETIME: PAGE: OUTFALL-001 L1034475-01 WW SAMPLE SUMMARY Collected by Geoffrey Murphey ONE LAB. NATIONWIDE. Collected date/time Received date/time 10/11/1813:15 10A3A8 08:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 D-2011 WGI182090 1 10/181812:04 1018I1813:05 MMF Wet Chemistry by Method 1664B WG1182655 1 10l18A808:38 10/18/181131 DAD Metals (ICP) by Method 200.7 WGI180493 1 10/15/1817:10 10/16/18 08:54 CCE Metals (ICPMS) by Method 200.8 WG1180596 1 10/16/18 06:30 10/1611815:21 JPD ACCOUNT: PROJECT: SDG: DATE7TIME: PAGE: CASE NARRATIVE ONE LAB. NATIONWIDE. 4R All sample aliquots were received at the correct temperature, in the proper containers, with the ICF appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and ROL (LOQ) values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my S5 knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 6Sr 6 c Heather J Wagner eAl Project Manager 9SC ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: ONE LAB. NATIONWIDE. W OUTFALL-001 SAMPLE RESULTS - 01 Collected date/time: 10/11/18 13:15 L1034475 Additional Information Result Units CF Analyte pH (On Site) 8.8 su ETC Gravimetric Analysis by Method 2540 D-2011 3Ss Result Qualifier RDL Dilution Analysis Batch Analyze ugh ug/I date/time aCr Suspended Solids ND 6750 1 10A8/201813:05 WG1182090 Sample Narrative: L1034475-01 WGI182090: 370mis All that would filter. Wet Chemistry by Method 1664B C)C Result Qualifer RDL Dilution Analysis Batch 7GI Analyte ugA ugA date/time TPH -Oil&Grease ND 5560 1 10/18/201813:31 WG1182655 [Al Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch 9SC Analyze ug/I ug/I date/time Lead ND 5.00 1 10/16201808:54 WG1180493 Zinc ND 50.0 1 10/16201808:54 WG1180493 Metals (ICPMS) by Method 200.8 Analyte Result ugA Qualifier RDL ugA Dilution Analysis Batch date/time Copper 1.35 1.00 1 10/16/201815:21 WGI180596 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1182090 Gravimelric Analysis oy Method 2540 D-2011 Method Blank (MB) (MB) R3352248-1 10/18/1813:05 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I Suspended Solids U 350 2500 L1O34483-01 Original Sample (OS) • Duplicate (DUP) DUALITY CONTROL SUMMARY L1034475-01 (OS) L1034483-01 10/18/1813:05 • (DUP) R3352248-4 10/18/18 13:05 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA uwl % % Suspended Solids 133000 147000 1 10.5 J3 5 L1O34569-01 Original Sample (OS) • Duplicate (DUP) (OS) L1034569-01 10/18/1813:05 • (DUP) R3352248-5 10/18/18 13:05 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ug/I % % Suspended Solids 2800 1800 1 43.5 J PI 5 Laboratory Control Sample (LCS) (LCS) R3352248-2 10/18/1813:05 Spike Amount LCS Result LCS Rec, Rec. Limits LCS Qualifier Analyte ugA ug/I % % Suspended Solids 773000 804000 104 85.0-115 ONE LAB. NATIONWIDE. AR 1CP zTc aSs 4Cr s $r N FGI aAl 9SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1182655 Wet Chemistry by Method 1664B Method Blank (MB) (MC) H33519 /3-1 IU/18/18 I/:I/ MB Result MB Qualifier MB MDL MB ROL Analyte ug4 Ug4 ug/I TPH - Oil & Grease U 725 5000 QUALITY CONTROL SUMMARY L1034475-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (L(-S) H33S19/3-2 10/18/1817:18 • (LCSD) R3351973-3 10/18/18 17:18 Spike Amount LCS Result LCSD Result LCS Rec, LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyse ug4 ugA ugA % % % % TPH - Oil & Grease 20000 19200 17800 96.0 89.0 78.0-114 7.57 ONE LAB. NATIONWIDE. 4R RPD Limits 18 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1180493 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals )ICP) by Meth,d 200.7 L1034475-01 Method Blank (MB) (MB) R3351038-1 10/16/18 08:33 C� MB Result MB Qualifier MB MOIL MB ROL Analyte ugA ugA ug/I ZTC Lead U 2.00 5.00 Zinc U 3.40 SOO aSS Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Er(LCS) R3351038-2 10/16/18 08:35 • (LCSD) R3351038-3 10/16/18 0838 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec Limits LCS Qualifier LCSD Qualifier RPD RPD Limits s Sr Analyte ugA ugA ugA % % % % % Lead 1000 1010 988 101 98.8 85.0-115 2.60 20 Zinc 1000 1000 976 100 97.6 85.0-115 2.63 20 L1034466-01 Original Sample Matrix 7GI (OS) • Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1034466-01 10/16/18 08:40 • (MS) R3351038-5 10/16/18 08:48 • (MSD) R3351038-6 10/16/18 08:51 aAl Spike Amount Original Result MS Result MSD Result MS Rec MSD Rec. Dilution Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ug/I ug4 ug/1 % % % % % 95e Lead 1000 U 1010 1010 101 101 1 70.0-130 0.419 20 Zinc 1000 U 993 985 99.3 98.5 1 70.0-130 0.806 20 L1034475-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1034475-01 10/16/18 08:54 • (MS) R3351038-7 10/16/18 08:56 • (MSD) R3351038-8 10/16/18 08:59 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyle ugA ugA ugA ugA % % % % % Lead 1000 ND 999 987 99.9 98.7 1 70.0-130 1.23 20 Zinc 1000 NO 984 976 98.4 97.6 1 70.0-130 0.802 20 L1034679-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1034679-15 10/16/18 09:07 • (MS) R3351038-9 10/16/18 09:09 - (MSD) R3351038-10 10/16/18 09:12 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I ug/I % % % % % Lead 1000 U 1020 1010 102 101 1 70.0-130 0.546 20 Zinc 1000 5.25 1010 1000 100 99.6 1 70.0-130 0.677 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: WG1180596 Metals (ICPMS) by Method 200.8 Method Blank (MB) (MB) R3351194-1 10/16/1814:17 MB Result Analyte ugA Copper tl MB Qualfer MB MDL MB RDL ugA ug/I 0.270 1.00 QUALITY CONTROL SUMMARY L1034475-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. 4R (LC�,) k33b1194-2 10/16/1814:21 • (LCSD) R3351194-3 10/16/18 14:25 - Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec Rec. Limits LCS Qualifier LCSD OuallRer RPD RPD Limits Analyte ugA ug/I ugA % % % % % Copper 50.0 48.8 50.5 9T5 101 85.0-115 3.45 20 L1032775-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (US) L1032//5-03 10/16/1814:29 • (MS) R3351194-5 10/16/18 14:37 • (MSD) R3351194-6 10/16/18 14:41 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA - ugll ugA ug/I % % % % % Copper 50.0 4.72 52.8 52.3 96.2 95.2 1 70.0-130 0.924 20 L1034416-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (US) UU34416-01 10/16/1814:45 • (MS) R3351194-7 10/16/1814:49 • (MSD) R3351194-8 10/16/1814:53 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec Dilution Rec, Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ug/I ugA ug/I % % % % % Copper 50.0 ND 49.4 49.4 97.8 97.9 1 70.0-130 0.0574 20 rCF 2Tc aSs 4Cr SSr 7GI aAl 9Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: GLOSSARY CIF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not CF intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions �Tc MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). a SS RDL Reported Detection Limit. Rec. Recovery. a RPD Relative Percent Difference. cr SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). s $r Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. 6 If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Q� Dilution standard, or if concentrations of analyses in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than I is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful OC Sample analysis will target all analyses recovered or duplicated within these ranges. a Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control Ai sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and Sc potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Oc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the feld when your samples were initially collected. This is used to verify the time and Sample Chain of sate of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable: the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. Pt RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AC.C.REDITAT IONS & LOCATIONS IONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accrel ited/certifed to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab k as accessible or prepared to handle your needs throughout the country. Our capacity and cape billy, from our single location labo mtory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productbity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. State Accreditations _Alabama 40660 Nebraska NE-OS-15-05___ Alaska 17-026 _ Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TN002 California 2932 New Mexico' Na Colorado TN00003 Connecticut _ PH-0197 Florida FR74R7 Georgia NELAP Georgia' 923 Idaho TN00003 Illiiwis 200008 Indiana C TN-01 Iowa 364 Kansas Kentucky'" — -- E-10277 ---- 90010—_---- Kentucky 2 16 Louisiana A130792 Louisiana' _ LA180010 Maine TN0002 Maryland 324 Massachusetts M-TNO03 Minnesota 047-999-395 _Mississippi TN00003 Missouri 340 Montana CERT0086 Third Partv Federal Accreditations A21-A — 15017025 AAA — ISO 17025 "— -- 1461.01 1461.02 -- ----- — -- Canada 1461.01 EPA —Crypt. TN00003 New Yark 11742 North Carolina Env375 North Carolina DW21704 North Carolina ° 47 North Dakota R-140 Ohio—VAP CL0069 _Oklahoma 9915 Oregon TN200002 Pennsylvania 68-02979 Rhode Island LA000356 South Carolina 84004 South Dakota Tennessee 14 Texas T104704245-17-14 —__LAB0152 Utah TN00003 Vermont VT2006 _Virginia 460132 Washington C847 West Virginia 233 Wisconsin 9980939910 Wyoming AKA AIHA-LAP,LLC EMLAP 100789 DOD ---— 1461.01—_-- _MA P330-15-00234 Drinking Water 2 Underground Storage Tanks °Aquatic Toxicity 40hemical/Microbiological "Mold "Wastewater Na Accreditation not applicable Our Locations Pace National has soty-four dlent support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main offde. Pace National performs all testing at our central laboratory. WA MT OR T ID WY T NV T UT T • CA CO' T • T� NM b AK IQ 4 B H1 �.o HI tSDND NE EKS T Tx T MN T WI NY MI T A T T PA 4 • IL Ii OH T MO VAT T �, k N T TAT AR • T T SC MS AL GA R ME cP 2Tc 8J$ 4Cr 6$r 6Qk 7GI 9SD ACCOUNT: PROJECT: SDG: DATEr-IME: PAGE: Billing Information: Ana s Contalner PceservatNe ' rlialn of tus+ody -Pale M Piedmont Geologic P es Accounes Payable 6003 Chapel Hill Rd Ste 145 �'k SC 6003 Chapel Hid Rd Raleigh, NC 27607 Ste 145 Ratesoh Nf P7W17 tm631abaaat ea ❑i LTti❑i Repon to Cmail To: pjdresml®pledmomgeotoglc.com; rl Pete Dfessel jmprphrorVptodmontgeotog(d.com ' " wum hlletTN sTua r On O rhme.81Yr945a5a'' Project ON/Stale Callactod: Nl.l 1 q �` Description ABB Inc, I^G.+.O , _ _ client Project a lab Project a Phone: 919 854 9700 17S1 PIEGEOFABB 4 Fax:- 919-Ma9532 ;Y .,,I£ J C07rJ Collected Site/Facility ID it P.O..P ,by(prfn*- PINETOPS, NC N A a A'tmmmrrtrocv.---- beo4m - 17 ' 'O a` O tdmpintp;T129400 Co :[tad (signdture)i - Rush7ltaDMVSTBeHoti0eol. Quote ,' _4mo Day _tarn oay' •. - - .ud,- z m Pralogtn;';P652173 ' _rlexteaY _50ay 1Rad earl Data Results Needed U' S 0- 1SR 887h3;,H)eantherl Wo nc ,; tmmed. a _l"vie Day �Iptrav (R dDM') 40• �'.Z, T' .S' Pk.".' Packed on" N_'Y_ _Thnn Day C tD L 5hippedvia4edEXGround _ _ d 'v O. - its ' 'Sample 10 Comp/Grab Matrix Depth Date 11me to = un.niu;. .`'UN* - x 4+n W*1 H r, OUTFALL-001 GKC�. WW ��+�� �Q i „3. X X X it -- - tMatriw•,:, emarks: - Hereto YeCaiot -LT yr SaP]"ieteynar t/incdact _: s _°Y. 1^'t tt SS,•Soi1 AIR -Air F- Filter •,',',}p�, pN temp. - -' •"" GW-_Groundwatai B•BloassaY tf �� • is <0 5 mR t Flow Other eotrlea ar iso rfreacc: GY 1 WIN -wastewater ivw-SCr* r _— Ger rotE:ba rt.lna-P4aiir'. DW-Drlekiog Water Samples:(efu "ed via:, {� [� 07-Other UPS;_ edEa,•._Courie: Tracking N. Su3 eicf!n: vpIum9 addL GY -�U _= YDA ax0 itl0aJapata. •., Y gip. R u'nh S�gnaturo) Dale: Tfine: ReceHW bytl two ip Blank Rae'wd:'Yes /No PYa BrvpCan7 Cdreec_E/Chacknd ,Fi'�:. Hall elinquished by Date, Time: R Rat Temp[ !C aatdn RecNved;. It:presarvatjon required by login; Date/Time Rel at '" DaW lime:, Recel-Wier tab by 15igharure) Dar x Time: - Hold; Condition;' 4s Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG( Date submitted CERTIFICATE OF COVERAGE No. N0003 0 0 0 6 FACILITY NAME ABB Inc. - Edeecombe COUNTY Edgecombe PERSON COLLECTING SAMPLES Nathan Beauchamp LABORATORY ESC Labs Lab Cert. A 41 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD X❑ Jan -June ❑ July -Dec E�_ {{... or ❑ Monthly' (month) '^ uISC�ARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA MAY 1 0 tote ❑Zero -flow ❑Watersupply ❑SA CENP ®Other NSW FILCwR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 n Nn rlisrhnrna thic narinrl?2 Outfall No. Date Sample. P Collected (mo/dd/yr) 24-hour rainfall amount, inches 3 Total Suspended Solids � � .?H�. -standard units `Copper Lead Zinc _Non -Polar, 0&G/ 'Total Petroleum Hydrocarbons Total Toxic Organics=' Benchmarks ==> d: _ 100 mg/L or50 mg/L . 60-9.0-, 0.007,mg/L. 0.03 mg/L +0.067 mg/G ,,- 15 mg/L, ',,I mg/L n. 001 04/24/18 1.2 5.6 8.7 <0.010 <0.005 <0.050 <5.75 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ./Drees-, fi 5�,te�s, CSC Name (Print name) ,q_S QY\T_ 4atitletinttitle) ure) - (Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n Nn f icrhnrno Chic narinrl2' Outfall No. '. -'Date Sample - collected' -(mo/dd/yr),Inches 24-hour rainfall. - ' amount, , a Non -polar O&G/TPH by EPA 1664(SGT-HEM) -'" Total Suspended Solids pH - Benchmarks===>- '� "' 15.mg/L 100mg/L or.50 mg/L• '6.0-9.0 SU"- Footnotes from Part A also apply to this Part B . See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 , Page 2 of 3 OESC ANALYTICAL REPORT myESC Piedmont Geologic Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L988357 04/25/2018 1751 ABB Inc. PINETOPS, NC Pete Dressel 6003 Chapel Hill Rd Ste 145 Raleigh, NC 27607 Entire Report Reviewed By: Ll h� Heather J Wagner Technical Service Representative Results relate only to the Items tasted or calibrated and are reported as rounded values This test report shall not be reproduced. except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is { performed per guidance provided in laboratory standard operating procedures060302, 066303, and 060304. � { a t `V lit". - . . Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Pq IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 f. BIBin In!ormatlon: Ana '-s/.Containm Presemt lve chain of 'wBeLa, _ � Piedmont Geologic a ablRd3te;195 es AaoDnu vayablr ISC 6003Cha P 44 6003 ChaPel,Hill Rd:" Rale)gN .NC 27607 • ''r, .. �." •»'a.:::i/�%.e^, Ste 145 ; � R�loloh Nh77fn7• - - ".- R - uevattiu rr»w �. � Repoato ,.; -.- -_ Email to: PldressNGpledmongeoloiicfom, 1 Pete Gressel 41 )murDhrey@Diodmon'tgeologicrom 1 1 .b V. r nw.:e so-sasa , rFro,aWDJtx SaH `rr rutcia tsa sus ;QQ _ .. PUrendptl fJtY/State �' xok:A881nt. W r p 9 Qg. r ID q�, Phone;919:854 9700 Qllet.GmllctD 1751 tO .' Lab Project PIEGEO; ABB �- D06`S . E .+ Collened by IDrintJ: - Slte/Faulhy ID D° P.O.. a . _ - nccmgm`S PIEGEO - h%oC.t. ' - PINETOPS NCt - uu,- M, w . � 7u' 2 7empla.e.T129400, rrclrigtr. P624228.: Collwed_ by.(signature)i Rush? lLab;MUST Be Notified) Quote p t 'Samotuv-.,,— Fpa Der -••,, ty- f6R:'I10`Br'idJn((F�o�rd rt Na.t Oay _5011tsd Only) "D9te Results Needed x W - r �71 tmmedlately' ✓ =T•'o,oar._.iO pav lRad Onkl, : _ _ J0. fw x l7 S. Pot' " (11 !' l Sblpped wai Fed&Ground: Packed, on Ice N 'Y' ' �Tnrae Day ,.. ff U )=_ J' N - - itry 'Sample ID Comp/Grab bLi[ilti i° Depth Date Time: OUTFALU001 SEAS 3] 'XV ' % x I', r: k { AAt C MatrM Remarks:j(2 ] .. S Soll gIR�•A)x F Fiter M�t.��- YetD��kad r 1r • pH CJ.r! .Temp 3'ste we SOQ] P:caenVincace; rP^p. COC Of ntamccurate � 8 . GW Groundwater B BIo9ssayA " BDttlon o i sa t. NasteWater Flow Other cdzrort Eottieo nsrid)t 4 UW Drinking rlae Saihpies returned vta; „ q LtVC VIM r.Lit 5uF(Ida t volan, aantr :! AcpiL h�O 07 Other UDS fed6,—Courier --_ 7fetklnBb I — — - o IteadaDaent _N r ,, Time: ReOcivetl byt,(S )`TNawwa Relinquished by (S'Bnature) , "Oau! - - ufie Trip Received: Yes/CIA_ ipD. Ca eNC'neekedc •-- -+N eoH •` z4 I$ - alJ'u- l_. PeBnq-uishW - - BON bisl De_C 1D1 DtCServatlon_ fe o r 8 n,Date n1!> nme; RDOnqunh ne '. - Ode: . Time.. flue! _.eNVY.-9'natur ),,,,. .... Hold: - CprMlilq-' �D�atte. 1 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE, ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab Is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory 6 comparable to the collective totals of the network laboratories In our industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model is conducive to accelerated productMty, decreasing Wmaraund time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached repod. ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. State Accreditations Alaska 17-026 Colorado TN00003 Connecticut PH-0197 Florida E87487 Georgia _ NELAP Georgia 923 Idaho _ _ TN00003 Iowa 364 Kansas E-102➢ Kentucky1B 90010 _ tuck Keny --_--- 16 -_--- - Louisiana A130792 Marylantl 324 Massachusetts Michigan _ _ M-TNO03 _ 9958 Minnesota 047-999-395 Mississippi ____ TN00003 _Missouri _ 340 Montana Third Party CERT0086 Federal Accreditations A2A - ISO 17025 146L01 A2LA-ISO 17025' 1461 no -- Nebraska NE-OS-15-05 Nevada _ _ _ New Hampshire TN ;03-2002 34 2975 New Jersey-_NELAP TNO02 New Mexico' _ Na New Y_ork 11742 North Carolina North Carolina' DW21704 North Conlin 83 _ _ 41 North Dakota _ R-140 Ohio-VAP CL0069 _ Oklahoma Oregon Pennsylvania 68 02979 Rhode Island South Carolina _ _ South Dakota LA000356 _ 84004 No Tennessee10 Texas 2006 _ T104704245-17-14 Texas' _ LABO152 Utah TN00(T3 _Vermont Virginia _ _._ VT2006 460132 Washington _ C847 West VI glue 233 Wisconsin _ 9980939910 Wyoming _ _ A2LA AIHA-LAP,LLC EMI -AP 100789 DOD 1461.01 USDA P330-15-00234 'Drinking Water 'Underground Storage Tanks 3Aquatic Toxicity °ChemicallMicrobiological "Mold "Wastewater No Accreditation not applicable Our Locations ESC Lab Sciences has sory four client support centers that provide sample pickup anchor the delivery of sampling supplies. If you would like assistance from one of our support odes, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. WA MT NO ME OR MN T IO SO T YA NY YYY MI T T w T ISE IA T T PA T T IL 1l� OM UT cA T VAT T OO KS MC) IL • T INT T TLT • T� N1.1 OK AR SC MS AT TGA T TX LA T ° AK T T O L � � T o HI C�l i ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Piedmont Geologic 1751 L988357 05/02/1808:49 10 of 11 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Cp Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 3Ss OUTFALL-001 L988357-01 _ 5 4Cn Qc: Quality Control Summary 6 Gravimetric Analysis by Method 2540 D-2011 6 5Sr Wet Chemistry by Method 1664B 7 Metals (ICP) by Method 200.7 8 roc GI: Glossary of Terms 9 Al: Accreditations &Locations 10 GI Sc: Sample Chain of Custody 11 eAl ACCOUNT: PROJECT: SOG: DATErIME: PAGE: Piedmont Geologic 1751 L988357 05/02/1808:49 2ofi1 SAMPLE SUMMARY ONE LAB. NATIONWIDE. OUTFALL-001 L988357-01 WW Collected by Nathan Beauchamp Collected datehime 04124/1911:08 Received datehime 04/251808:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 D-2011 WG1103085 1 04/25/1820:39 04125/1822:02 BS Wet Chemistry by Method 16648 WG1105123 1 05/0V808:48 05/01/1817:42 JM Metals (lCP) by Method 200.7 WG1102844 1 04125/1813:44 0427/1801:02 TRB ACCOUNT: PROJECT: SDG: DATE/rlME: PAGE: Piedmont Geologic 1751 L988357 05/02/1808:49 3or 11 CASE NARRATIVE ONE LAB. NATIONWIDE. RP All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within ETC the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by the client. All Method and Batch Quality Control are within established Ss criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. SSr aQC lVi 'GI Heather J Wagner s Technical Service Representative AI ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Piedmont Geologic 1751 L988357 05/02t1808:49 4of11 OUTFALL-001 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 04/24/18 11:08 L988357 Additional Information Result Units Analyte pH (On Site) 8.7 su Gravimetric Analysis by Method 2540 D-2011 Result Qualifier RDL Dilution Analysis Batch Anatyte ug/I ugll date/time Suspended Solids 5500 2500 1 04/251201922:02 WG1103085 Wet Chemistry by Method 1664E Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date/time TPH -Oil&Grease NO 5750 1 05/01/201817:42 WG1105123 Metals (ICP) by Method 200.7 Result Qualifier RDL Dilution Analysis Batch Anatyte ug/I ug/I date/time Copper NO 10.0 1 04/271201801:02 WG1102844 Lead NO 5.00 1 04/27/201801:02 WG1102844 Zinc ND 50.0 1 04/27/201801:02 WG1102844 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Piedmont Geologic 1751 L988357 05/02/1808.49 5of11 WG1102844 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Metals (ICP) by Method 200.7 L988357-01 Method Blank (MB) (MB) R3305159-1 04/27/18 00:28 MB Result Copper J Lead U Zinc u MB Qualifier MB MDL MB RDL ugll ug/I Zoo 10.0 2.00 5.00 340 50.0 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3305150-2 04/27/18 00:30 • (LCSD) R3305159-3 04/27/18 00:33 Spike Amount LCS Result LCSD Result LCS Rec LCSD Rec. Rec Limits LCS Oualier LCSD Qualifier RPD RPD Limits Analyte ugll ugll ugll % % % % % Copper 1000 1000 1000 100 100 85.0-115 0.151 20 Lead 1000 1020 1030 102 103 85.0-115 0.67E 20 Zinc 1000 1010 1010 101 101 85.0-115 0.450 20 L988366-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L988366-01 04/27/18 00:35 • (MS) R3305159-5 04/27/18 00:41 • (MSD) R3305159-6 04/27/18 00:43 Spike Amount Original Result MS Result MSD Result MS Rec, MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugh ugh ug/I ugll % % % % % Copper 1000 ND 1040 1040 104 104 1 70.0-130 0.783 20 Lead 1000 ND 1080 1090 108 109 1 70.0-130 0A24 20 Zinc 1000 90.7 1150 1160 106 107 1 70.0-130 0.407 20 L988372-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (05) L988372-01 04/27/18 00:46 • (MS) R3305159-7 04/27/18 00:48 • (MSD) R3305159-8 04/27/18 00:51 Spike Amount Original Result MS Result MSD Rewlt MS Rec. MSD Rec. Citron Rec Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/1 ug/I % % % % % Copper 1000 ND 1040 1020 104 102 1 70.0-130 1.82 20 Lead 1000 ND 1090 1080 109 106 1 70,0130 1.02 20 Zinc 1000 ND 1080 1070 107 106 1 700130 1.05 20 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Piedmont Geologic 1751 L988357 05/02/18 09:49 8 of 11 GLOSSARY OF TERMS ONE LAB. NATIONWIDE, 40 Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). Analyze The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyze being reported. Successful CC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was Result no measurable result returned for a specific analyte, the result in this column may state "ND' (Not Detected) or "BDL" (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Cc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This Is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed an each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Piedmont Geologic 1751 L988357 05/02/1808:49 9ofn WG1103085 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Gravimetric Analysis by Method 2540 D-2011 L988357-01 Method Blank (MB) (MB) R3305085-1 04/25/18 2202 - MB Result MB Qualifier MB MDL MB RDL Analyze ug/I ugtl ug/I Suspended Solids U 350 2500 L988361-05 Original Sample (OS) • Duplicate (DUP) (OS) L988361-05 04/25/18 22:02 - (DUP) R3305085-5 04/25/18 22:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyze ug/I ug/I % % Suspended Solids 137000 138000 1 0.727 5 L988367-01 Original Sample (OS) • Duplicate (DUP) (OS) L988367-01 04/25/18 22:02 • (DUP) R3305085-4 04/25/18 22:02 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ugll % % Suspended Solids 78600 80000 1 1.80 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3305085-2 04/25/18 22:02 - (LCSD) R3305085-3 04/25/18 22:02 Spike Amount LCS Result LCSD Result LCS Rea LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ugh ug/I ug/I % % % % % Suspended Solids 773000 796000 800000 103 103 85.0-115 0.501 5 ACCOUNT: Piedmont Geologic PROJECT: SDG: DATE/TIME: 1751 L988357 05/02/18 08:49 PAGE 6 of 11 WG1105123 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method 1664B L988357-01 Method Blank (MB) (MB)HJJ(Jbl/19 0b/01/1817:40 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I i TPH -Oil&Grease U 725 5000 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (i KJCutiI/1¢ Ub/Ul/1817:40 • (LCSD) R3306171-3 05/01/1817:42 Spike Amount LCS Result LCSD Result LCS Rec. LCSD sec. Rec. Lim Rs LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I i % % % % % TPH -Oil&Grease 20000 18700 19500 93.5 97.5 78.0-114 4.19 18 ACCOUNT: PROJECT: SDG: Piedmont Geologic 1751 L988357 DATE/TIME: 05/02/18 08:49 PAGE: 7 of 11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water �Qualit r General Permit No. NCG( Date submitted CERTIFICATE OF COVERAGE NO. N0003_Q _ __D-6 FACILITY NAME ARR Inc COUNTY Edgecombe PERSON COLLECTING SAMPLES no digrhnrga LABORATORY _ _ - Lab Cert. q Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR c-�`J 1 -7 SAMPLE PERIOD ❑ Jan -June July -Dec r n or ❑ Monthly' (month) R C I`/ DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow [:]Water Supply ❑SA DEC 1 /(:j' ❑Other CIENTIRAL crl-�-^ DWR„ PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 D No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24•hour rainfall amount, Inches3 Total Suspended Solids Total pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> _ - 100 mg/L or 50 mg/L° 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L r, •ter✓ L I J Z017 ' Monthly sampling (instead of semi-annual) must begin with the second consecufi'velbenchmark exceedance for the same parameter at the same outfall. ft'r rn �� r'llk-S z For sampling periods with no discharge at any single outfall, you must still submitthis'dlsehargelmonitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic -compounds -used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Doreen Shiers Name (Print name) HSE Manacler Tit e (Print title) 7 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1—Tier-2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑,No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664(SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 444 �: (7 CERTIFICATE OF COV[[PEJJtAGE No. NCG03 L Q FACILITY NAME .TT` COUNTY kO PERSON COLLECTING SAMPLES _ LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR - '�© 1-1 SAMPLE PERIOD Jan -June ❑ July -Dec or []Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ECEIVED ❑Zero -flow ❑Water Supply ❑SA ❑Other DEC 13 Z017 CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 XNo discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L' 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) —BS ,(— Title (Print title) Pgnature) /a LA (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/I.", where XX•is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No dischome this neriod?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids PH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications_where the mcce protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE of COVERAGE NO- NCG03 0 O o FACILITY NAME F�C�Fi3. c COUNTY a, PERSON COLLECTING SAMPLES LABORATORY Y�� 'c'.�e Lab er fF Lit D Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR o'Q(S SAMPLE PERIOD ❑ 1an=June E'luly-Dec �/� or , ❑ Monthly' (month) ®® r'EECEOISCFARDINGTOCLASS ❑ORW ❑HCtW ❑Trout ❑PNA FEB .0 9 2016 ❑Zero -flow, [:]WaterSupply ❑SA it k ®0thei­47 Tn iLkD:e ccnP z CENTRAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 �tk�ray, �rlyi si p y 1 . { Ilya R�.+t) 4.I��r114v S {,.�� •c. k �.�Y �I. HI^�PI�. b rt ..I w i5 tiii?•'7nn'� �46'�:I>E. „ Een 5n t P45 d ,�'t,u. t its itl� , .r., .. rs l' (i 1� �i riill•,ila No Iy`x' A$nt'[ 1y� 7)at discharge �W�•en Y, r i,d, L thrs period vli El: I' olp v.: e"Klr L '..:r n. r,r iX ULnf•d'�,td5,�, iy r w��aO�itfall No �, � t D;ate ,ample:. .. '.. 24h nal f'il�' � o r, ? a ��ainnulnt "�"`Total .krh.p,,.,4I,t E • ,., a wtW SUspended„'Soltdskl,a� �1P� 1 1iS !w o+•=�'a'dly`�`,ICtlpper'`'��ta'r�a��d�` �. FI* Y(;:,a,.... � , �i nd t'fmOd/yr) 11 v v , T drOCarbOn4Wi Hy iiy I J Benchmarks�t a w Sd, L 4` i1 mP✓L=;. 1 kit -a-t5 R R.,1;5m;; Monthl 1' d f samp Ing (Instea o semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 E }o Z aged ZTOZ/sZ/oT paslnaJ iSe1'sbZ-nms L1OZ/1£/0T-ZiOZ/T/TT:aWU l!wJad 'salldde �!lewy]uaq anl;]a;wd aloes ayi aiaym suolle]gIMP Ja3em gwnla]aJ anl;lsuas Apeloadso aq3 BulA;guapl's algel'ixal llwiad leiauag aas g lied sly; of Aldde osle y lied woJ; saloulood fls 0 6 ,Q 4 J l+ x/gwrOS io�l gw OOI 5 ,' w ` > -1- =zv t H drs, D �� " WIoS paP dsns4 a}a r i I o- e , `'�az I,l i!s A4Hdl/�J'gA"iefod � v f9, RRl t a�,t •4+1s1 R�t�"°'.`w �l'-i` ��'��hli�. :y?w �(nFS tHir Lillo7. � i Iv, (n 'is lrt� �•}.�. �np ` IKt �Jry i P;�, d °1 . i n I�1:«��'�P ^�� .:,, ��a��'4• �,:nfF t 4 ��_17r I 1` , y, �rPouad swl abiou7slo oni I-1 . .. u •y;uow Jad HO mau JO 10 gg <flulgeiane salllp3ej.lo}Aluo:sllnsall OupolluoW eaJyaaueualuleW alalyaA :g Ind 'lxal l!wiad;nJauag aag •sasuodsai g Jall Jo Z iaLL'T Ja1 L ivawa;dwl lsnw noA 9iJawy]uaq aq7 fo ssaaxa ui an;on a;dwos o wodaJ no f fj :aloN uo!loa3a a ; o an en eouawnu a sl '-I/gw ul •ola'3!wll gullJodai';!wll P 4 } I I yi XX aiaym „� w xx>,� lewJof ay; ul pa;Jo aJ aq lsnw --Ka— ,, alge]gdde aq;molaq ale sllnsai uaym -lewio; leouawnu-uou Jellwls Jaylo JO'QN 'halap-uoN 'lbd>'109 'l!Wll uollaaiap molag lJo a�J iou od •iewio; le]uawnu ul paiJodaJ a q isnw s41nsel1 :aloN (a3eO) (ainleug!s) Ia1i!i 3ulJ 1i1 '-Ilrll%VIh[v� -5-f7 (aweu luud) oweN „-ueld uo!;uanaJd uognpod Ja;emwiols ayl ul papnl]ul ueld luawa8euew luanlos ayl }o suolslnad ayi Ile ayl 8w;uawaldwl sl Ai!IPe; sly;;eyl A;l;ia] Ja43Jn; I •�odaj 8uuo3!uow agieq]slp isel ayi Bully aouls paJJno]o sey gouni Jalemwols Jo lle;uleJ of pasodxa aie y]lym seaie Jo Jalemwiols ayl olul soluegJo ]lxol pa3eJ;ua3uoo4o 8uldwnp ou'}allaq pue a8palmou5l Aui;o isaq aql of ley; A;llia] I'(O.LL) sJweBJo ]lxol lelol Jo; luawannbw 8ulio;!uow l!wiad aql yl!M anelldwoo gulgeuew Jo; alglsuodsai Ap]ailp suosiad Jo uosiad ayi}o AJlnbul Aw uodn pase% quawale;s uol;eaylliaa gulmollo; ayl ugls Ileys JagJeq]slp agl'Janlem guuolluow OLL ay; Aoldwa of gul;gala salitilae; asoyl Jod llwiad Ieiauag ayl ul pals!I sluawala Jay;o ay; pue pasn spunodwoa aluegio �lxol lelol ayl;o Is!1 a apnpul peps ueld;uawa8euew luanlos el aa4i •panlem aq Aew guuolluow p11Jo; luawannbaJ ayl pue'A}!liaa os Am veld uolluanaJd uoljnIlOd JalemwJo;g ayl olul ueld wawageuew luanlos a a;eiodioaw leyl sal;•ylaed Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SEC11ON B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS' SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO t REGIONAL OFFICE CONTACT NAME: Mail an orlainal and one copy of this DMR Including all "No Discharge" reports within 30 days of receipt of the lab results far at end of monitoring period to the case of No Discharge reports) to: Division of Water Quality Attn: OWq Central Files e 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." l / J ✓ � (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 3 I -4-o ) '(Date) SWU-245, last revised 10/25/2012 Page 3 of 3 WORK Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidanceonfillingourthisform,pleasevisit,Z//nortalnedenror/web/wq/ws/Jnpde w#ta 4 Permit No.: Facility Name: PrP County: Inspector:. 0 Date of Inspection: _ Time of Inspection: _ or certificate of Coverage No.: NIVI / 0/-4� Cam C� Phbne No. Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or measureable storm event"(requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. , A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: w1s4lnLwc Ut rermaree or uesignee) Page 1 of SWU-242, Last modified 10/25/2D12 aceAnalyticaie maspacefebacvm Project: ABB - 2nd Annual 2015 Pace Project No.: 92274347 Charlotte Certification Me 9800 Kincey Ave. Ste 100, Huntemvnle, NC 28078 North Caroline Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification M 12 South Carolina Certification #: 9900SM1 1;x )s' CERTIFICATIONS hCG-e3 oaf Florlda/NELAP Certification #: E87627 Kentucky UST Certificatlon #: 84 West Virginia CertlBcation M 357 VirglnlaNELAP Certification #: 480221 Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, INC 20076 (704)875-9092 Asheville Certification Me ' 2225 Riverside Drhre, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridafNEIAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 West Virginia Certification M 358 North Carolina Drinking Water Certification #: 37712 VirginlarVEIAP Certification M 400222 REPORT OF LABORATORY, ANALYSIS This report shag not he reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 25 aceAnalytrcal" wwamoefabssoro SAMPLE ANALYTE COUNT i Pace Analytical Services, Inc. 980D ICincey Ave. Suh* too Huntertville, NC 28157s (704)875.9092 Project: Pace Project No.: ABB-2nd Annual 2015 92274347 Lab ID Sample ID - Mothod Analysts Analysts Reported Laboratory 92274347001 SDO.1 EPA 1884E JMS 1 PASI-C EPA 8010 CDF 1 PASI-A EPA 8270 RES 74 PASI-C EPA 8260 GAW 71 PASI-C SM 2540D SAM 1 PASI-A REPORT OF LABORATORY ANALYSIS This report $hall hot be reproduced, except In run, without the written consent of Pars Analytical SerNcea, Inc.. Page 3 of 25 Paco Analytical Services, Inc. 0 ( lee Analyticala98001(Incey Ave. Suite 100 n yaac®aaamaHunters7NC 078 74)875-9-9092 ANALYTICAL RESULTS Project: ABB-2nd Annual 2015 Pace Project No.: =74347 Sample: SOO.1 LablD: 92274347001 Collected: 11/0211509:15 Received: 11/03/1509:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO M91L 5.0 1 11/12/15 07:39 5010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead . NO ug/L 5.0 1 11/07/15 20:00 11/09/15 14:57 7439-92-1 8270 IMISSV HVI Somivol Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene NO ug/L 10.0 1 11/05/1615:57 11/11/15 12:15 83-32.9 Acenaphthylene NO ug/L 10.0 1 1110511516:57 11111/1512:16 208-96-8 Aniline NO ug/L 10.0 1 11/05/15 16:57 11111/1512:15 62-53-3 Anthracerie ND ug/L 10.0 1 11/06/16 16:57 11/11/15 12:15 120-12-7 Benzo(a)an0tracene NO ug/L 10,0 1 11/0511516:57 11/11/1512:15 56-55-3 Benzo(a)pyrene NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 5D-32-8 Behzo(b)Ouoranlhene NO ug/L 10.0 1 11105/16 16:57 11/11/15 12:15 205-99-2 Benzo(g,h,l)perylene NO ug/L 10.0 1 11/05/15 16:57 11/11115 12:15 191.24-2 8enzoNfiuoranthene ND ug/L 10.0 1 11/05/15 16:57 11/11115 12:15 207-08-9 Benzoic Acid NO ug/L 50.0 1 11105/15 16:57 11111/15 12:15 65-85-0 Senzyl alcohol NO ug/L 20.0 1 11/0511516:57 11/11/1512:15 10051-6 4-Brornopherrylphenyl ether NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 101-55-3 Butylbenzylphthalate NO, ug/L 10.0 1 11/05/15 15:57 11/11/15 12:15 85-68-7 4-Chioro3methylphenol ND ug(L 20.0 1 11/05/15 16:57 11/11/15 12:15 59-50-7 4-Chloroanl8ne NO ug/L 20.0 1 11105/1516:57 11/11/15 12:15 106-47-6 bfs(2-0)darcethoxy)methane ND ug/L 10.0 1 11/05/1516:67 1111V751215 111-91-1 bis(2-Chloroethy) ether NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 111-44-4 bis(2-Chlorolsopropyp ether NO ug/L 10.0 1 11/05/15 16:57 11111/15 12:15 108-50-1 2-Chlomnaphthalene NO ug/L 10.0 1 11/06/16 16:57 11/11/15 12:15 91-56-7 2-Chlorophenol ND ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 95-57-8 4-Chlorophenylphenyl ether NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 7005-72-3 Chrysene NO ug/L 10.0 1 11/0511516:57 1111111612:15 21Ml-9 Dlbenz(a,h)anthracene NO ug/L 10.0 1 11/05115 16:57 11/11/16 12:15 53-70-3 Dibenzoluran ND ug/L 10.0 1 11/05/15 16,57 11111/16 12:15 132-64-9 1,2-1)ichlorobenzene NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 95.50-1 1,3-Dichlorobenzene NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 541-73.1 14-Dichlombenzene ND ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 106-46-7 3,T-Dichlorobenadne ND ug/L 20.0 1 1110511516:57 11/11/1612:16 91-94-1 2,4-Dichlorophenol NO ug1L 10.0 1 11/05/15 15:57 11/11/15 12:15 120-83.2 Dlethylphthalafe NO ug1L 10.0 1 11/05/15 16:57 11/11/15 12:15 64-56-2 2,4-Dimethylphenol ND ug/L 10.0 1 11/05M5 16:57 11/11/15 12:16 105.67-9 Dimethylphthalate NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 131-11-3 Di-n-butylphthalate NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 84-74-2 4,6-Dtnitrc-2-methylphenol NO ug/L 20.0 1 11/05/15 16:57 11/11/15 12:15 534-52-1 2,4-Dinitrophenal ND WL 50.0 1 11/05/15 16:57 11/11/15 12:15 51-28-5 2,4-Diralrololuene NO ug/L 10.0 1 11/06/15 16:57 11/11/15 12:15 121-14-2 2,6-DINtrotoluene NO ug/L 10,0 1 1110511516:57 IiMV1512:15 60620.2 Dt-n-octytphthalate NO ug/L 10.0 1 1110511516:57 11111/1512:15 117-84-0 bis(2-Ethylhexyl)phthalate ND ug/L 6.0 1 1110511516:57 11111/1512:15 117-81-7 Fluoranthene NO ug/L 10.0 1 11/05/15 1657 11/11/15 12:15 206-44-0 REPORT OF LABORATORY ANALYSIS This report oral not be roproduced, except In fur, Date: 11/13/2016 05:33 PM without the wrilten consent of Pace Analytical Services, Inc.. Page 4 of 25 ® Pace Analytical Services, Inc. aceAnalyfical 9800Klncey Ave. Sulfetoo xnvrpsrdelu.cum Hunteraville. NC 28b78 (7e4)878-9092 ANALYTICAL RESULTS Project ABB - 2nd Annual 2015 Pace Project No.: 92274347 Sample: SDO.1 Lab 10: 92.274347001 Collected: IV02115 09:15 Received: 1110311509:30 Matrix: Water Parameters 8270 MSSV HVI Semivol Organic Fluorene HexaGUoro-1, 3-buladiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane fndeno(1,2,3-cd)pymre Isophorone 1-Methyinaphtholene 2-Methylnaphthalene 2-Methyiphenol(o-Cresoo 3&4-Methylphenol(m&p CresoD Naphthalene 2-Nitroaniline 3-NilroaNfine 4-Nitroantline Nitrobenzene 2-Nilrophend 4-NI(rophenol N-Nllrosodimethylamine N-Nitroso-di-n-propylamine N-Nitrosoc iphenylemine -Pentachlorophenol Phenanthrene Phenol Pyrene 1,2,4-Trtchiorobenzene 2,4,5-Trichlomphencl 2,4,6-Trichlomphenof Surrogates Nltrobenzened5 (S) 2-Ruorobiphenyi (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol(S) 2,4,6-Trtbromophenol (S) Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ Analytical Method: EPA8270 Preparation Method: EPA3510 NO ug/L 10.0 1 11/05/15 16:57 11111/15 12:15 86-73-7 NO ug/L 10.0 1 11/05/15 16:57 11/11115 12:15 87-68.3 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 118-74-1 NO ug/L 10.0 1 11/05/15 16:57 11/11/16 12:16 7747-4 NO ug/L 10.0 1 11/0511516:57 11/11/1512:15 67-72.1 NO ug/L 10.0 1 11/05/15 16:57 11111/15 12:15 193-39-6 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 78.59-1 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 90-12-0 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 91-57-6 NO uglL 10.0 1 11/05/15 16:57 11/11/15 12:15 -95-48.7 NO ug1L 10.0 1 11/05/15 16:57 11/11/15 121f NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 91-20-3 NO ug1L 50.0 1 11105/1516:57 11111/15 12:15 88-744 NO ug/L 50.0 1 11105/1516:57 11/1111512:15 99-09-2 NO ug/L 20.0 1 11/05/15 16:67 11/11/15 12:15 100-01-6 NO ug/L 10.0 1 11/06/15 16:57 11/11/15 12:15 98-95-3 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 88-75-5 NO ug/L 50.0 1 11/05/15 16:57 11/11/15 12:15 100-02-7 NO ug/L 10.0 1 11/05/15 16:57 11/11115 12:15 62-75-9 NO ug1L 10.0 1 11/05/15 16:57 11/11/15 12:15 621-64-7 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 88-30-6 NO ug/L 25.0 1 11105/1516:57 11/1111512:15 87-86-5 NO ug/L 10.0 1 1110511516:57 1111111512:15 85-01-8 NO ug/L 10.0 1 11/D5/1516:57 1111111512:15 108-95-2 NO ug/L 10.0 1 11/05/15 16:57 11/11/15 12:15 129-00-0 NO u9/1. 10.0 1 11105/15 16:57 11/11/15 12:15 120-82-1 NO ug1L 10.0 1 11105/16 16:57 11/11/15 12:15 95.954 NO uglL 10.0 1 11/05/15 18:57 11111/15 12:15 88-06-2 41 % 21-110 1 11/05/15 16:57 11/11/15 12:15 4165.60-0 39 % 27-110 1 11/05115 16:57 11/11/16 12:15 321-60-8 78 % 31-107 1 11/05/15 16:57 11/11/15 12:15 1718-51-0 14 % 10-110 1 11/05/15 16:57 11/11115 12:15 13127-88-3 12 % 12-110 1 11/05/15 16:67 11/11/15 12:15 367-12-4 28 % 27-110 1 11/05/15 16:57 11111/15 12:15 118-79-6 8260 MSV Anarytloal Method: EPA 8260 Acetone NO ug1L 25.0 1 11/13/15 06:49 67-64-1 Benzene NO ug/L 5.0 1 11113/15 05:49 71.43-2 Bromobenzane NO ug/L 5.0 1 11/13/15 06:49 108-86-1 Bromodlloromefhane - NO ug/L 5.0 1 11/13/15 06:49 74-975 Bromodchloromethane NO ug/L 5.0 1 11113115 DSA9 75-27.4 Bromoform NO uglL '"'5.D 1 11/13/1506:49 75-25-2 Bromomethane NO ug/L 10.0 1 11/13/15 06:49 74-83-9 2-Butanone (MEK) NO ug/L 10.0 1 11/13/15 06:49 7B-93-3 tert-Butyl Alcohol NO ug/L 100 1 11113/1508:49 75-65-0 L3 n-Butylbenzene - NO ug1L 5.0 1 11/13/15 06:49 104-51-8 REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in full, Date: 11/13/2015 05:33 PM without the wdden consent of Paco Analytical Services, Inc. Page 5 of 25 Pace Analytical Services, Inc, AnalXicala 990o ncay Ave. Suitetea xwwparea' b&= Huntersvtle, NO 28078 aF poa)ms-eoez ANALYTICAL RESULTS Project ABB-2nd Annual2015 Pace Project No.: 92274347 Sample: SDO.1 Lab ID: 92274347001 Collected: 11102/1509:15 Received: 11/03/1509:30 Mat0x: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Dual 8260 MSV Analytical Method: EPA 8260 - seo-Butylbenzene NO ug/L 5.0 1 11/13/15 06:49 135-98-8 tert-Butylbenzene NO ug/L 5.0 1 11/13/1506:49 98-06.6 Carbon tetrachloride ND ug/L 6.0 1 11113/1506:49 56-23-5 Chlorobenzene NO ug/L 5.0 1 11/13115 06:49 108-90-7 Chloroethane ND ug/L 10.0 1 11113/15 D6:49 75-00-3 Chloroform ND ug/L 5.0 1 1111311506:49 67-663 Chloromethane NO ug/L 5.0 1 11/13/1506:49 74-87-3 2-Chlarotoluene ND ug/L 5.0 1 11/13/15 06:49 95.49-8 4-Ohlorotoluene ND ug/L 5.0 1 11113/15 06:49 106-43-4 12-Dlbromo-3-cltoropropahe NO ug/L 2.0 1 11/1311506:49 96-12-8 Dibromochloromethane NO ug/L 5.0 1 11/13/15 06:49 124-4B-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1 11/13/15 06:49 106-93-4 Dlbronlomethane ND ug/L 5.0 1 11/13115 06:49 74-95-3 1,2-Dichlorobenzene NO ug/L 5.0 1 11/13/15 06:49 95-50-1 1,3-Dichlorobenzene NO ug/L 5.0 1 11/13/15 06:49 541-73-1 1,4-01chlorobenzene NO ugA 5.0 1 11/1311505:49 106-46-7 Dichlorodifluoromethene NO 'ugA 5.0 1 11/13/15 06:49 75-71-8 1,1-Dirhlorcetharle NO ug/L 5.0 1 11/13/15 06:49 75-34-3 1,2-0tchloroethane ND ugA 5.0 1 11/13/15 06:49 107-06-2 1,2-01chloruethene (Total) NO uglL- 5.0 1 11/13115 08:49 540-59-0 1.1-Dichloroethene NO ug/L 5.0 1 11/13115 0BA9 75.35-4 cis-1,2-Dichloroethene NO ugA 5.0 1 11/13/15 06:49 156-59-2 trans-1,2-Dicttoroethene NO ug/L 5.0 1 11/13/16 06:49 156-60-5 1,2-Dlchloropropane ND ugA 5.0 1 11/13/15 06:49 78-87-5 1,3-Dichloropropane NO ug/L 5.0 1 11/13/15 06:49 142-28-9 22-Dichloropropane NO ugA 5.0 1 11/13/15 06:49 594-20-7 1,1-Diddoropropene NO ug/L 5.0 1 11/13/15 06:49 503-58-6 cis-1,3-01chlorapropene NO ug/L 5.0 1 11/13/15 06:49 10061-01-5 trans-1,3-Dlchloropropene ND ug/L 5.0 1 fill 3/1506:49 10061-02-6 05sopropyl ether NO ugA &0 1 11/13115 06:49 108-2D-3 Ethylbenzerhe NO ugA 5.0 1 11113/15 06:49 100-41.4 Hexachlmr 1,3-buttdiene ND ug/L 5.0 1 11/13/15 06:49 67-68-3 2-Hexanone NO ug/L 10.0 1 11/13/1506:49 591-78-6 Isopropylbertzene (Cumene) NO ug/L 5.0 1 11/13/15 06:49 98-82-8 p-Isopropyltoluerhe ND ug/L 5.0 1 11113/1606:49 99-87-6 Methylene Chloride NO ug/L 5.0 1 11/13/15 06:49 75-09-2 4-Methyl-2-pentanone(MIBK) ND ugA 10.D 1 11113/15 06:49 108-10.1 Methyl-tert-butyl ether NO ugA 5.0 1 11113/15 06:49 1634-04-4 Naphthalene NO ug/L 5.0 1 11/13/15 06:49 91-20-3 n-Propylbenzene ND ug/L 5.0 1 11/13/15 08:49 103-65-1 Styrene NO ug/L 5.0 1 11/13/15 06:49 10042-5 1,1,1,2-Tetrachloroethane NO ug/L 5.0 1 11/13M5 08:49 630-2D-6 1,12,2-Tetrarhloroethane ND ugA 5.0 1 1111311506:49 79-34-5 Tebachloroethene NO ugA 5.0 1 11113/1506:49 127-18-4 Toluene NO ug/L 5.0 1 11113/15 06:49 108-88-3 1,2,3-Tdchlorobenzene NO ug/L 5.0 1 11/13/15 06:49 87-61-6 1,2,4-Tdchlorobenzene NO ug/L 5.0 1 11113/15 06:49 120.62-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fWl, Date: 11/13/2015 05:33 PM without the writen consent of Pace Analytical Services. Inc.. Page 6 of 25 aceAnalytical amwya®1Msbwa ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Sufte100 HunterWIle, NC 28078 (704)875-9a92 Project: ASS - 2nd Annual 2015 Pace Project No.: 92274347 Sample: SDD-1 Lab ID: 92274347001 C011e0ted: 11/0211609:16 Received: 11/0311509:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSv Analytical Method: EPA 8260 t,1.1-Tdchlomethane NO ug/L 5.0 1 11/13/15 06:49 71-55-6 1,12-Tdchlomethane NO ug1L 5.0 1 11/13/1506:49 79-064 Tdchloroethene NO ug1L 5.0 1 1111311506:49 794)1.6 Tdchlorofluommethane NO ug/L 10.0 1 11/1311506:49 75-89-4 1,2,3-Trichloropropane NO ug/L 5.0 1 11/13/15 06:49 96-184 1,2,4-Trimethylbenzene NO ug/L 5.0 1 11/13/15 D6:49 95-63.6 1,3,5-Tdmethylbenzene NO ug/L 5.0 1 11113/1506:49 108-67-8 Vinyl acetate Vinyl chloride NO ug/L 10.0 1 11/13/15 06:49 108-054 nrAp-Xylem NO NO ug/L 5.0 1 11/13/15 06:49 75.014 0-Xylene ug/L 10.0 1 11113/1506:49 179801-23-1 Surrogates NO ug/L 5.0 1 11/13/15 06:49 95-47-6 4-Sromolluorobenzene (S) 101 % 74130 1 11/13115 06:49 460-00-4 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 11/13/15 06:49 17060-07-0 Toluene-dll (S) 105 % 70-130 1 11/13/15 06:49 2037.26-5 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.2 mg/L 5.0 1 11/04/1510:20 t REPORT OF LABORATORY ANALYSIS This report Shan not be reproduced, except in full, Date: 11113/2015 05:33 PM without the written consent of Pace Analytical Servicea, Inc.. Page 7 of 25 aceAnalytical mrntpampoebi am QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kinney Ave. Sidle 100 1 Huntersmi le, NC 29078 (704)875-9092 Project ASS - 2nd Annual 2015 Pace Project No.: 92274347 QC Batch: GCSV/23181 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92274347001 METHOD BLANK 1604434 MatdK: Water Associated Lab Samples: 92274347001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L NO 5.0 11/12/15 07:35 LABORATORY CONTROL SAMPLE: 1604435 Spike LCS LCS % Rae Parameter Units Cone. Result %Rae Limits Qualifiers Oti and Grease mg/L 40 33.7 84 78-114 MATRIX SPIKE SAMPLE: 1604436 92275153001 Spike MS MS % Rae Parameter Units Result Conc. Result %Rec Limits Quallfiers Oil and Grease mglL ND 40 35.0 88 78-114 Results pmeented on this page ate in me unlls indicated by the" UnIW' calumn except Where an alternate unit In presentad to the right of the reaull. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, meept In full, Date: 11113/2015 05:33 PM wllhout the written consent of Pace Analytical SeMces, Inc. Page 8 of 25 �aceAnapical'a aox'pacele0t seen QUALITY CONTROL DATA Pace Analytical SoMme, Inc. 9000 Kincey Ave. Suite lo0 HuntmMile, NC 28376 (704)975-9092 Project: ABB - 2ndAnnual 2015 Pace Project No.: 92274347 CC Batch: MPRP/19985 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92274347001 METHOD BLANK: 1601584 Associated Lab Samples: 92274347001 Parameter Units Lead u9/L LABORATORY CONTROL SAMPLE: 1601585 Parameter Units Lead ug/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND - 5.0. 11/0911513:52 Spike LCS LCS %Rec Conc. Result % Rec Limits Qualifiers 500 471 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1601586 1601587 MS MSD 92273821001 Spike Spike- MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Lead uglL - 8.2 500 . 500 466 470 92 92 75-125 1 tureens nexanted an this papa are In the unite Indluted by Cho "UNta' column except where an ethernet, unit Is Presented to the rIght of the result REPORT OF LABORATORY ANALYSIS - This report shag not he reproduced, except in full, Date: 11113/2015 05:33 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 25 5ceAna1j&ca1. ~petelebs QUALITY CONTROL DATA Pace Analytical 8ervlces, Inc. 9800 Kincey Ave. Suite 100 Huntersulle, NC 29078 (704)B75.9092 Project: ABB-2nd Annual 2015 Pace Project No.: 92274347 QC Batch: MSV/34264 Analysis Method: EPA 8260 QC Batch Method: . EPA 8260 Analysis Description: 8260 MSV Associated Lab Samples: 92274347001 METHOD BLANK 1605554 Associated Lab Samples: 92274347001 Parameter Units Matrix: Water Blank Reporting Result Limit _ Analyzed 1, 1, 12-Tetmchloroethane ug/L NO 5.0 11/1311506:15 1,1,1-Tdchloroethane ug/L NO 5.0 11/13/15 06:15 1,1,2,2-Te rachloroe0wle ug/L NO 5.0 11113/15 06:15 1,1,2-Tdchtoroethane uglL NO 5.0 11/13/15 06:15 1,1-Dlchlomelhane ug1L NO 5.0 11113/15 06:15 1,1-131chloroethene ugli- NO 5.0 11/13/15 06:15 1,1-Dichloropropene ug/L NO 5.0 11/1311506:15 1,2,3-Tdchlorobenzene ug/L ND 5.0 11/13/15 06:15 1,2,3-Trichloropropane - ug/L NO 5.0 11/13/15 06:15 1,2,4-Tdchlombenzene ug/L NO 5.0 11/13/15 06:15 1,2,4-Tdmethylbenzen s ug/L ND 5.0 11/13115 06:15 1,2-Dibromo-3-chloropropane ug/L NO 2.0 11113115 06:15 1,2-Dlbromoethane (EDB) ug/L NO 5.0 11/13/15 05:16 1,2-Dichlorobenzene ug/L NO 5.0 11/13115 06:15 1,2-Dlchiorcethane ug/L NO 5.0 11113115 06:15 1,2-Dichloroethene (Total) ug/L NO 5.0 11113115 66:15 1,2-Dichloropropone ug/L ND 5.0 11/13/15 06:15 1,3,5-Tdmethylbenzene ug(L NO 5.0 11/13/16 06:15 1,3-DlcNarobenzene ug1L NO 5.0 1111311506: 15 1,3-Dicdoropropane ug/L NO 6.0 11113/15 06:15 1,4-Dichlorobenzene ug/L NO 5.0 11/13/15 06:15 2,2-Dichloropropane ug/L NO 5.0 11/13/15 06:15 2-Butanone (MEH) _ ug/L NO 10.0 11/13/15 06:15 2-Chlorotoluene ug)L NO 5.0 11/13/16 06:15 2-Hexanone ug/L NO 10.0 11113115 06:15 4-Chiomtoluene ug/L NO 5.0 11113115 06:15 4-Methyl-2-pentanone(MIBK) ug/L NO 10.0 11/l 3/1506:15 Acetone ug/L NO 25.0 11/13/1506:15 Benzene ug/L NO 5.0 11/13/15 06:15 Bromobenzene ug/L ND 5.0 11/1311506:15 Bromtchloromethane ug/L ND 5.0 11/13/15 05:15 Bromodichloromethane ug/L NO 5.0 11/1311506:15 Brumoform ug/L NO 5.0 11/1311506:15 Bromomethane ug/L NO 10.0 11/13/1506:15 Carbon tetrachloride ug/L NO 5.0 11113/15 06:15 Chlorobenzene ug/L NO 5.0 1111311506:18 Chloroethane ug/L NO 10.0 11/13/15 06:15 Chloroform ug/L NO 5.0 11113/15 06:15 Chlommethane ug/L NO 5.0 11113/15 06:15 d8-1,2-Dlchlomethene ug1L NO 5.0 11/13115 06:15 cis-1,3-Dichloropropene ug/L NO 5.0 1111311506:16 Qualifiers Results presented on this page are In the unite Indicated by the"Unix" column except where an alternate emit is presented to the front of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, excnpl In full, Date: 11/13/2015 05:33 PM vdthout the written consent of Pace Analytical Services, Inc., page 10 of 25 aceAnalytical wnlapsro66swm QUALITY CONTROL DATA Project: . ABB-2nd Annual2015 Pace Project No.: 92274347 - METHOD BLANK: 1605554 Associated Lab Samples: 92274347001 Parameter ' Units Matra: Blank Result Water ' Reporting Limit Analyzed Dibromochlorortethane ug/L NO 5.0 11/1311506:15 _ Dibromomethane ug/L NO 6.0 11/13/15 06:15 Oichlorodi9uoromethane ug/L NO 5.0 11/13/15 06:15 Diisopropyl ether ug/L NO 5.0 11/13/15 06:15 Ethylbenzene ug/L NO 5.0 -11/13/15 06:15 Hezachloro-1,3-butediene ug/L NO 5.0 11/13/16 b6:15 Isopropylbenzene(Cumene) ug/L ND 5.0 11113/1506:15 m&p-Xylene - ug/L NO 10.0 11113/15 06:15 Methyl-tert-butyl ether ug/L NO 5.0 11/13/15 06:15 Me(hylene Chloride - ug1L NO 5.0 11/1311506:15 n-Buly(benzene ug1L NO 5.0 11113/15 06:15 n-Propylbemene ug/L NO 5.0 11/13/15 06:15 Naphthalene ug/L NO 5.0 1111311506i15 o-Xylene - ug/L ND 5.0 11/13/15 06:15 p4sopropyltoluene ug/L NO 5.0 11/13/15 06:15 sec-Butylbenzene- ug/L NO 5.0 11/13/1506:15 Styrene ug/L NO 5.0 11113/1506:15 tert-Butyl Alcohol ug/L NO 100 11/13/15 06:15 tert-Butylbemene ug/L NO 5.0 11/13/15 06:15 Tetrachloroethene ug/L NO 5.0 11/13/15 06:15 Toluene ug/L NO 5.0 11/13/15 08:15 trans-1,2-1)ichloroethone ug/L NO 6.0 11/13/16 06:15 trans-1,3-Dichloropropene ug1L NO 5.0 1ill 311506:15 Trichloroethene ug/L ND 5.0 11/1311506:15 Trichlom8uoromethane ug/L NO 10.0 11113/1506:15 Vinyl acetate ug/L NO 10.0 11/13/15 06:15 Vinyl chloride ug/L NO 5.0 11/13/15 06:15 1,2-Dichloroethane-d4(S) % 96 70-130 11/13/16 06,15 4-Bronmfluorobemene (S) % 101 70-130 11/13/15 06:15 Toluene-d8 (S) % 105 70-130 11/13/15 08:15 Qualifiers Pace Analytical services, Inc. 9800 Klncey Ave. sufte 10o Huntersville, NC 28078 (704)875-e092 LABORATORY CONTROL SAMPLE: 1605555 Spike 1-CS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 44.6 89 80-125 1,1,1-Tdchloreethane ug/L 50 44.6 s9 71-129 1,1,2,2-Telrachloroethene ug/L 50 52.1 104 79-124 1,1,2-Trtchloroethane ug/L - 50 47.0 94 85-125 1,1-Dichloroethane ug/L 50 44.9 90 73.126 1,1-Dichioroethene ug/L 50 37.6 75 66-135 1,1-Dlclderopropene ug/L 50 44.2 88 74-135 1,2,3-Tdchlorobemene ug/L 50 47.9 96 73-135 1,2,3-Tdchloropropone ug/L 50 54.0 108 75-130 12,4-Trichlorobemene ug1L 50 45.9 92 75-134 Rmuae prosantad on M. pap. are In the units In4lcatee by tho'Units- column •%aapt when so anematt unit is prasented to the daht of the revulL REPORT OF LABORATORY ANALYSIS This report shall not be roproduced, excopt In rub, Date: 1111312015 W:33 PM without the written consent of Pace Analytical services, Inc.. Page 11 of 25 aceAnatXical vnvapam,46xtwn QUALITY CONTROL DATA Project ABB-2nd Annual 2015 Pace Project No.: 92274347 Pace Analytical Services, Inc. 980D Kincey Ave. Suite 100 Huntersvile, NC 28078 (704)875-9092 LABORATORY CONTROL SMAPLE: Parameter 1605555 Units Spike Conc. ' LCS Result LCS % Rec % Rec - Limits Qualifiers 1,2,4-Tdmethylbenzene ug/L 50 49.0 98 79-125 1,2-Dibromo-3-chloropropane ug/L_ 50 47.9 96 71-133 1,2-Dibromoethane (EDB) ug/L 50 52.4 105 83-124 1,2-Dlchlorobenzene ug/L 51) 47.3 - 95 . . 80.133 1,2-Dichlomethane ug/L 50 47.8 96 - 67-128 1,2-Dichioreethene (Total) ug/L 100 90.3 - 90 73-128 1,2-Diehloropropane ug/L 50 47.5 - - 95 75-132 1;3,5-Tdmethyibenzene ug/L 50 ' 47.9 - 96 79-123 1,3-Dlchlorobenzene ug/L 50 47.5 95 77-130 1,3-Dichloropropane ug/L 50 51.3 103 76-131 1,4-Dichiorobenzene uglL 50 _ 46.8 94 78-130 2,2-01chioropropane ug/L 50 _ 35.6 71 40-160 2-Butanone (MEK) ug/L 100 122 122 61-144 2-Chlorololuene ug/L 50 46.4 93, 74-132 12-Hexanone ug/L 100 126 126 68-143 4-Chlorotoluene ug/L 50 49.1 98 76-133 4-Methyl-2-pentanonli(MIBip ug/L 100 117 117 72A35 Acetone ug/L 100 119 119 48-146 Benzene ug/L 60 4T.9 - 96 . 80-125 Bromobenzene ug/L 50 44.8 90 75-125 Bromochloromethane ug/L 60 48.8 98 71-125 Bromodlchloromethane ug/L 50 48.2 96 78-124 Bromoform ug/L 50 36.0 72 7/-128 Bromomethane ug/L 50 21.7 43 40-160 Carbon tetrachloride ug/L 50 45.1 90 69-131 Chlombenzene ug/L 50 454 91 81-122 Chloroethane ug/L 50 27.9 56 39-148 Chloroform ug/L 50 42.9 88 73-127 Chloromethane ug/L 50 40.5 81 44-146 cis-1,2-Dichloroethene ug/L 50 44.9 90 74-124 cis-1,3-Dichioropropene ug/L 50 45.3 91 72-132 Dbromochloromelhane ug/L 50 42.4 85 78-125 Dibromomethane ug/L 50 46.2 92 82-120 Dirhlorodi0uoromethane ug/L 50 50.1 IOU 34-157 Dlisopropyl ether ug/L 50 _ 54.0 108 69-136 Ethylbenzen , ug/L 50 44.0 88 79-121 Hexachloro-1,3-butedlene ug/L 50 52.6 105 72-131 lsopropyibenzene (Cumene) ug/L 50 44.8 90 81-132 m8p-Xyiene ug/L 100 92.9 93 81-124 Methyl -ten -butyl ether ug/L 50 65.3 111 74-131 Methyiene Chloride ug/L 50 51.1 102 64-133 n-Butylbenzene ug/L 50 45.8 92 78-127 n-Propylbenzene ug/L 50 47.1 94 78-130 Naphthalene ug/L 50 51.7 103 73-133 o-Xylene ug/L 50 47.2 94 79-131 p4sopropyltoluene ug/L 5o 47.1 94 80-131 sec-Butylbenzene ug/L 50 46.4 93 80-133 Results presented on this page are In the units Indlceted by the "Units" column exceptxltere an aeernsh, It Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Dale: 11/1312015 05:33 PM without the written consent of Pace Analytcal Services, Inc.. Page 12 of 25 aceAnapical. wew.pecabDs.can Pace Analytical Services, Inc. 980010ncey Ave, Suite too Huntersvllle, NC 28678 (704)875-9092 Project: ASS - 2nd Annual 2015 Pace Project No.: 92274347 QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: 1605555 Spike LCS LCS % Rec Parameter Units Conc. Result % Rao Limits Qualifiers Styrene ug/L 50 48.2 96 84.126 tert-Butyl Alcohol u9/1- 500 834 167 36-136 LO ten-Sutylbenzene ug/L 50 40.3 81 77-1 33 Tetrachloroetherle uglL 50 42.2 84 78-133 Toluene ug/L 50 43.7 87 80-121 trans-1,2-Dichbroethene ug/L 50 45.3 91 71-127 trans-1,3-Dichlompmpene ug/L 50 45.8 92 69-141 Trichloroethene ug/L 50 43.5 87 78-122 Trichlorofluorornethane uglL 50 36.8 78 53-137 tlnyl acetate ug/L 100 98.4 98 40-160 Vinyl chloride ug/L 50 44.6 89 58-137 1.2-Dichloroethane-d4 (S) % 109 70.130 4-Bromo6uorobenzene(S) % 101 70-130 Toluene-d8 (S) % 97 70-130 Revolts preaanted an this page are In the unit- Indicated by the "Unite" column except Mere an.Item-te unit Is pre-ented to the right of the S.H.v REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Data: 11/131201505:33 PM without the written consent of Paco Analytical Services,Inc.. Page 13 of 25 ace Analytical' ' twty{amLDscnn Project: ABE-2nd Annua12015 Pace Project No.: 92274347 QC Batch: OEXT1381i QC Batch Method: EPA 3510 Associated Lab Samples: 92274347001 QUALITY CONTROL DATA Analysis Method: EPA8270 . Analysis Description: 8270 Water MSSV HVI METHOD BLANK: 1600243 Associated Lab Samples: 92274347001 - Parameter Units Matrix: Water _ Blank Reporting Result Limit Analyzed 1,2,4-Trichlorobenzene ug/L NO %0 11106/1617:10 1,2-01ctdorobenzene ug/L NO 10.0 11/06/15 17:10 1,3-DicNorobenzene uglL NO 10.0 11106N5 17:10 1,4-Dlchlorabenzene ug/L ND lax 1V06/1517:10 1-Methylnaphthalene ug1L ND 10.0 1110611517:10 2,4,5-Trichlorophenol ug/L ND 10.0 1110611517:10 2,4,6-Trlchlorophenol ug/L NO 10.0 11/06116 17:10 2,4-DlcHarophenol ug/L ND 10.0 11106/1517:10 2,4-Dlmethylphenol ug/L NO 10.0 11/06/15 17:10 2,4-Dinitrophenol ug/L ND 50.0 11f06/1517:10 2,4-Dlnitrotoluene ug/L NO 10.0 11/06/15 17:10 2,6-Olnibotoiuene ug/L NO 10.0 11/06/1617:10 2-Chloronaphthalene ug/L ND 10.0 11/06/15 17:10 2-Chlorophenol ug/L NO 10.0 11/06/15 17:10 2-Meihylnaphthalene ug/L NO 10,0 11/0511517:10 2-Methyiphencl(o-Creso[I ug/L NO 10.0 11106/1517:10 2-Nitroaniline ug/L NO 50.0 1110611517:10 2-Nibophenol ug/L ND 10.0 11/06115 17:10 3&4-Mett"henol(m&p Cresoq ug/L ND 10.0 11/06/15 17:10 3,3'-Dltlllorobenzldlne ug/L ND 20.0 11/06/15 17:10 3-Nltroanlline ug/L ND 50.0 11/06/15 17:10 4,6-Dlydtro-2-mettlylphenol ug/L NO 20.0 11/06/1517:10 4-Bramophenylphenyl ether ug/L NO 10.0 11/06/15 17:10 4-Chloro-3-methylphenol ug/L ND 20.0 11/0611517:10 4-ChlomaNOne ug/L NO 20.0 1110511517:10 4-Chlorophenylphenyl ether ug/L ND %0 11/08/15 17:10 4-Nitroaniline ug/L ND 20.0 11/0611517:10 4-Nitrophenol ug/L NO 50.0 11106/1517:10 Acenaphthene ug/L NO 10.0 11/06/15 -17:10 Acenaphthylene ug/L NO 10.0 11/0611517:10. Aniline ug/L NO 10.0 11/0511517:10 Anthrecene ug/L NO 10.0 11/06/15 17:10 Senzo(a)enthrawne ug/L NO 10.0 11/0611517:10 Benzo(a)pyrene ug/L ND 10.0 11/06/15 17:10 Benzo(b)fluoranthene ug/L NO 10.0 11/06/15 17:10 Benzo(g,h,l)perylene ug/L NO 10.0 11/06/15 17:10 Benzo(b)fluomnthene ug/L ND 10.0 11/0611517:10 Benzoic Acid ug/L NO 50.0 11/06/15 17:10 Benzyl alcohol ug/L NO 20.0 11/08/15 17:10 bis(2-Chloroethoxy)methane uglL ND 10.0 11108/1517:10 bis(2-Chlomethyl) ether ug/L NO 10.0 11/06/15 17:10 Qualifiers Pace Analytical Services, Inc. 9800 IOncey Ave. Suite 100 HuntersWite, NC 25076 (704)8754092 Resulta presented on this page am In the units Indicated by We "Unite" cahunn except where an alternate unit Is posented to the right of toe result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11113/2015 05:33 PM Without the written consent of Pace Analytical Services, Inc.. Page 14 of 25 aceAnalytfcale m Pece66tcom Paco Ana lyticai Servlaae, Inc. 9800 Klncay Ave. Suite 100 Huntersvnle, NC 21168 (704)876-9092 QUALITY CONTROL DATA Project: A813 - 2nd Annual 2015 Pace Project No.: 92274347 METHOD BLANK 1600243 Matrix: Water Associated Lab Samples: 92274347001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers bls(2,-Ch(oroisopropyl) ether uglL NO - 10.0 1110651517:10 bls(2-Ethylhexypphthalate ug/L NO 6.0 ll/D6/15 17:10 Butylbenzylphthalate . ug/L NO 10.0 11/06/15 17:10 Chrysene ug/L ND 10.0 11/06/15 f7:10 Dfn-butylphthalate_ ug/L NO 10.0 11/0611517:fO Okn-octylphlhalafe ug/L ND 10.0 1110611517:10 Dibenz(a,h)anthracene ug/L NO 10.0 11106/15 17:10 Dibenzoluran - ug/L ND 10.0 1.1106115 17:10 _ Dielhylphthelate ug/L ND 10.0 1110WIS 17:10 - - Dimethylphlhalate ug/L NO 10.0 W06/1517:10 Fluorantherle ug/L ND 10.0 11/06/15 17:10 Fluorene . ug/L ND 10.0 11/06/15 17:10 Hexachloro-1,3-butadfene uglL NO 10.0 11/06/15 17:10 - Hexachlorobenzene ug/L ND 10.0 11/0611517:10 Hezachlorocyclopentadiene ug/L ND 10.0 11/06/15 17:10 Hexachloroethane uglL NO 10.0 11/06/15 17:10 Indeno(1,2-,3-cd)pyrene uglL NO 10.0 11/06115 17:10 Isophorone ug/L NO 10.0 11/06/15 17:10 N-Nitroso-di-n-propylamine ug/L ND 10.0 11/06/15 17:10 N-Nitrosodirrelhylemine ug1L NO 10.0 11/0611517:10 N-Nltrosodiphenylamine ug/L ND 10.0 11/0611517:10 Naphthalene ug/L NO 10.0 11/06/1517:10 Nitrobenzene ug/L NO 10.0 1110611517:10 PentachWophenol ug/L ND 25.0 1110CV1517:10 Phenanthrene ug/L NO 10.0 11/06/15 17:10 Phenol ug/L NO 10.0 11/06/16 17:10 PYmne ug/L ND 10.0 1110511517:10 2,4,6-Tdbromophenol(S) % 47 27-110 11/06/15 17:10 2-Fluorobiphenyl(S) % 46 27-110 11/06/15 17:10 2-Fluorophenol(S) % - 11 12-110 11/06/15 17:10 So Nltrobenzene-d5 (S) % 43 21-110 11/06/15 17:10 Pher l-d6 (S) % 12 10-110 11/06/15 17:10 Teryherlyl-04 (S) % 71 31-107 11/06/15 17:10 LABORATORY CONTROL SAMPLE: 1600244 Spike LCS LCS % Rec - Parameter Units Conc. Result %Rec Limits Qualifiers 1,24-Tdchlombenzene ug/L 50 42.7 85 31-120 1,2-Dichlorobenzene ug/L 50 39.5 79 38-120 1,3-111chlorobenzene ug/L 50 37.1 74 30-122 1,4-DIChlorobenzene ug/L 50 38.6 77 37-120 1-Methyinaphthaiene ug/L 50 48.1 95 34-113 2,4,5-Trlchlomphenol ug/L 50 44.3 89 43-113 2,4,6-Tdchlurophenol ug/L 50 44.1 88 42-120 Rasuea presented on Nis page are In Me unim inaleated by the "Units" column 00cept vdnre an a111a10 unit is preaentetl to the 49ht of the nault. REPORT OF LABORATORY ANALYSIS This report Shan not he reprc6uud, except in fun, Dale: 11/13/2015 05:33 PM Without the written consent of Pau Analy4cel Sen1ces, Inc.. Page 15 of 25 ceAnalytical ' wwprecefaW.mm QUALITY CONTROL DATA Project: ABB-2nd Annual 2015 Pace Project No.: 92274347 LABORATORY CONTROL SAMPLE: Parameter 1600244 Units Spike Conc. LCS Result LCS %Rec % Rao Limits 2,4-Dichlorophenol ug/L 50 36.2 - 72 3D-120 2,4-Dlmethldphenol ug/L 50 47.2 94 29-111 2,4-Dlnitrophenol ug/L 25D 175 70 19-132 2,4-Dinitrotoh erte ug/L 50 41.7 83 58-128 2,6-Dinitrotoluene ug/L 50 40.2 80 54-129 2Chloranaphthalene ug/L 50 41.6 B3, 43-117 2Chlorcphenol ug/L 50 34.3 69 37-120 2-Methyinaphthalene ug/L 50 44.8 90 33-120 2-Methyiphenol(o-Cresol) ug/L 50 33.3, 67 31-120 2-1,11troanilins ug/L 100 66.2 66 _. 48-121 2-Nltrophenol ug/L 50 - 34.9 70 25-116 384-Methyiphenol(mBp Cresol) ug/L 50 29.4 59 23-120 3.T-Dichiorobenzidine ug/L. 100 85.4 - 65 10-154 3-NltroaNltne ugfl 100 66.5 67 43-115 4,05-Dinitro-2-methylphenol ug/L 100 -93.4 93 44-124 4-Bromophenylphenyl ether. ug/L 50 48.0 96 34-113 4-Chloro-3-methylphenol ug1L 100 91.2 91 31-110 4Chloroanillne ug/L 100 83.0 83 _ . 20-120 4-Chlorophenyiphenyl ether ug/L 50 41.5 '83 34116 4Nltroiniline ug/L 100 65.7 55 46-128 4-Nitrophenol ug/L 250 94.1 - 38 11-120 Acenaphthene ug/L 50 46.2 92 48-114 Acenaphthylene ug/L 50 45.7 91 48-112 Anigne ug/L 60 28.0 56 26-120 Anthracene _ ug/L 50 50.9 102 57-118 Benzo(a)anthracerte ug/L 50 53.5 107 56-121 Benzo(e)pyrene ug/L 50 50.2 100 55-127 Benzo(b)fiuoranthene ug/L 50 48.3 97 53-128 . Senzo(g,h,i)perylene ug/L 50 48.2 98 54A25 Benzo(k)Ouoranthene ug/L 51) 57.1 114 51-123 Benzoic Acid ug/L 250 126 50 10-120 Benzyl alcohol ug/L 100 68.6 89 27-120 bis(2-Chlomethoxy)methane ug/L 50 44.7 89 32-120 bis(2-Chiotoethyl) ether ug/L 50 39.9 80 33-111 bis(2-CMoroisopropyo ether ug/L 50 31.9 64 15-120 bis(2-Elhylhexyl)phthalate ug/L 50 60.3 121 50-145 Butylbenzylphthaiate ug/L 50 58.4 117 54.138 Chrysene ug/L so 52A 104 58-127 DI-n-butylphthalate ug/L 50 50.9 102 66-125 Dl-n-aciylphihalate ug/L 50 66.2 132 5D-134 Dlbenz(a,h)anihracene ug/L 50 49.4 99 53-129 Dit erizefuran ug(L 50 43.7 87 45-120 Diethylphthalale ug/L 50 43.2 86 53-120 Dimethylphthalate ug/L 50 43.0 86 55-116 Fluorenthene ug/L 50 50.7 101 57-125 Flucrene ug/L 50 46.6 93 53-118 Hexachloro-1,3.buladiene ug/L 50 39.4 79 23-120 Pace Ans"zal SeMcea, Inc. 980010ncey Ave. Suite too HuntarsAle, NC 28076 (704)875.9092 Qualifiers Results presented on this page ere In the units Indicated by file 'enlb" caluren except where an alternate unit le presented to the right of the resulL REPORT OF LABORATORY ANALYSIS ' This report shag not be reproduced, except in full, Date: 1111312015 05:33 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 25 Analytical ® .� .Project: ABB-2nd Annual 2015 Pace Project No.: 92274347 ' QUALITY CONTROL DATA Pace Analytical Services, Inc. 9600Kinsey Hunterav ue, Suite C 28C788 (704)875-e092 LABORATORY CONTROL SAMPLE: 1600244 Spike LCS LCS %Rec . Parameter Units Conc. Result %Rec Limits Qualifiers Hexachlorobenzene ug/L 50 58.2 116 49.116 Hexarhlorocyclopentadiene ug/L 50 3D.7 61 26-158 Hexarhlomethane ug/L 50 37.1 74 30-114 Indeno(1,2,3-cd)pyrene ug/L 50 48.4 97 55-128 Isophorone ug/L 50 50.2 100. 31-118 N-Nitroso-di-n-propylamine ug/L 50 38.0 76 32-119 N-Nitroso limethylamine uglL 50 30.1 60 13-120 N-Nitrosocilphertylamine ug/L 50 45.6 91 43.120 Naphthalene ug/L 50 42.9 86 32-120 Nitrobenzene - ug/L 5o _ 43.1 Bar 33-110 Pentachloropherrol ug/L 100 93.3 93 10-137 Phenanthrone ug(L 50 49.1 98 57-117 Phenol ug/L 50 19.0 38 10-120 P'rome ug/L 50 51.2 102 55.122 2,4,6-Tribramophenol(3) % - _ 103 27-110 2-Fluoroblphenyl(S) % - 85 27-110 2-Fluorophenol(S) % 43 12-110 Nitrobenzene-d5 (S) % 86 21-110 Phenol-d5 (S) _ % - 36 10-110 TerphenylW14 (S) % 91 31-107 ace MATRIX SPIKE SAMPLE: Parameter 1WO245 Units 92274187002 Spike MS MS %Rec Result Conc. Result %Rec Limits Qualifiers 1,2,4-TNchtorobenzene ug/L 479 1,2-Dichlorobenzene ug/L 45.2 1,3-01chlorobenzene ug/L 42.5 1,4-01chlorobenzene ug/L 44 8 i-Methylnaphthalene ug/L - 577 M1 2,4,5-Tdchlomphenol ug/L 41.1 2,4,6-Tdchlorophenol ug/L _ 34.8 2,4-Dichlomphenol _u9/L 42.5 44-Dimethylphenol ug/L ND 52.2 - ..---_ M1 2A-Dinilrophenol ug/L 55.7 2,4-Dinitrotoluene ug/L 41 9 - 2,6-Dinitrotoluene ug/L 44.5 2-Chioronaphthalene ug/L 46.6 2-Chlorophenol ug/L 39.7 2-Methyinaphthalene ug/L 55.0 2-Mefl ylphenol(c-Cresog ug/L 38.2 2-Nitroaniline ug1L 75.3 2-Nitrophencl ug/L 39.4 3&4-Me1hylphenol(m&p Cresol) ug/L NO 36.0 3,3'-DidJorobenzid'ne ug/L 85.5 3-Nitroanifine uglL 72.6 Rnuha presented on this page an to the unite Indicated by the "Unna" column oxcept where an alternate unit le presented to the dght stirs resurb REPORT OF LABORATORY ANALYSIS This report shall not be raproduced, except In full, Date: 11/13/2015 05:33 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 25 lceAnalyfical- QUALITY CONTROL DATA Project: ABB-2nd Annua12015 Pace Projecl No.: 92274347 Pace Analytical Sawices, Inc 9800 Kincey Ave. Suite 100 Huntersvl9e, NC 26078 (704)875-9D92 MATRIX SPIKE SAMPLE: Parameter 1600245 Units 92274187002 Spike MS MS Result Conc. Result. %Rec %Rec Limits Qualifiers 4,6-Dlnl1ro-2-methylphenol ug/L 39.3 - 4-Bromophenylphenyl ether ug/L 50.4 4-Chloro-3-methylphenol ug/L 112 - M1 4-ChbroaNline ug/L. 102 Mt - 4-Chlomphenylphenyl ether ugn. - 46.3 4-Nilroanlline ug/L 66.3 4-Nltrophenol ug/L 35.3J Acanaphthene ug/L 52.5 M1 Acenaphthylerie ug/L 62.2 Mi Aniline ug/L - 34.1 Anthracene ug/L 53.8 Benzo(a)anthracene ug/L _ 54.7 Benzo(a)pyrene ug/L 52.2 Benzo(b)fluoranthene ug/L 50.3 Benzo(g,h,i)peryiene ug/L 52.3 Benzo(k)fiuoramhene ug/L 60.7 Mt Benzoic Acid ug/L 45.3J Benzyl alcohol ug/L _ 87.7 bis(2-Chloroethoxy)methan , ug/L 52.0 bls(2-Chloroelhyl) ether ug/L 47.8 bis(2-Chlomisopropyp ether ug/L _ 30.2 bis(2-EthylhexAphthalate ug/L 61.6 M1 Burylbenzylphihalate _ ug/L - 61.8 Mt Chrysene ug/L 54.9 DI-n,butylphthalate ug/L 51.3 DI-n-aclytphthalate U91L 69.6 Mi Dibenz(a,h)anthracene ug/L 63.1 Dibenzofuran ug/L 49.0 DieBfylphthalate ug/L ND 46.5 Dimethylphthalale ug/L 47,7 - Fluoranthene ug/L 60.6 Fluerene ug/L 52.7 M1 Hexachloro-1,3-butadiene ug/L 42.6 Hlexachlorobenzene ug/L 62.5 M1 Hexachlomcyclopenladiene ug/L 33.5 Hexachloroethane ug/L 42.2 Indeno(1,2,3-cd)pyrene ug/L 52.6 Isophorone ug/L 60.5 N-Nltroso-di-n-prepylamine ug/L 49.3 N-Nitrosocilmethylamine ug/L 32.0 N-NRrosociphenylanline ug/L 51.2 Naphthalene ug/L 48.7 Ndrobenzene ug/L 47.3 Pentarhlorophenol ug/L ND 34.3 Phenanthnme ug/L 51.2 Phenol ug/L 20.8 Pyrene ug/L 56.7 Results presented on this papa ere In the units Indicated by too 'V n@Y column exeeptwhere an aitemato uM is presented to the right of are out, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Poll. Date: 11/13/2015 05:33 PM without the written consent or Pam Analytical Services, Inc.. Page IS of 25 aceMalytical" mvwpeca�Ws.cbm QUALITY CONTROL DATA Pace Analytical Services, Inc. ea00 lQncey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: ABE-2nd Annual 2015 Pace Project No.: 92274347 MATRIX SPIKE SAMPLE: 1600245 92274187002 Spike MS MS %Rec Parameter Units Result Conn. Result % Rec Limits Qualifiers 2,4,6-Tdbromophenol(8) % 2-Fluorobipherryl (S) % 77 27-110 2-Fluorophenol(8) % 88 27 110 Nitrobenzene-d5 (S) % -41 12-110 Phenol-d6 (S) % 90 21-110 Terpheny1414 (S) % 36 10-110 - 78 31-107 SAMPLE DUPLICATE: 1600246 Parameter Units 92274180004 Dup Result Result 1,2,4-hichlorobenzene ug/L NO 1,2-01chlorobenzene ug/L ND 1,3-Dichlorobenzene ug/L - NO 1,4-Dichlombenzens ug/L NO 1-Mathylnaphthalene ug/L NO 2,4,5-Trichlorophenol ug/L ND 2,4,8-Trichloropherlol ug/L NO 2,4-Dichlorophenol ug/L NO 2,4-DSnethylphenol _ ug/L NO NO 2,4-Dinteophenol ug/L ND 2,4-Dlnitrotoluene ug/L NO 2,6-Dinitrotoluene ug/L NO 2-Chioronaphthalene ug/L - _ NO 2-Chlorophenol ug/L NO 2-Methylnaphthalene ug/L NO 2-Methylphenoi(o-Cresol) ug/L NO 2-Nitroahitine uglL - NO 2-Nitrophenol ug/L NO 3&4-Methyiphenol(m&p CresoQ ug/L NO NO 3,T-DlUlombenzidine ug/L ND 3-Nitroanlifne ug/L NO 4,6-Dinibo-2-methylphenol ug/L NO 4-Brornophenylphenyl ether ug/L NO 4-Chloro-3-me1hylphenol ug/L ND 4-Chlereeniline ug/L NO 4-Chlorophenyipherlyl ether ugli- NO 4-Nltroanillne ug/L NO 4-Nllrophenol ug/L NO Acenaphlhene ug/L NO Acenaphthylene ug/L NO Ariline ug/L NO Anthracene ug/L NO Benzo(a)anthracene ug/L ND Benzo(a)pyrene ug/L NO Benzo(b)fluoranthene ug/L ND RPD Qualifiers Results presented on Una pope an in the unite Indlcated by Ne'UnU' column exceplwharo an altemata unli is presented to the dghl or Me rpeult. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced. except In fun, Date: 11/13/2015 05:33 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 25 lCeAnalAcal' mnvpeushflao0rq QUALITY CONTROL DATA Project ABB-2nd Annual 2015 Pace Project No.: 92274347 SAMPLE DUPLICATE: 1600246 - Parameter - Units 92274180004 Result Dup Result RPD Senzo(g,h,i)perylene ug/L NO Benzo(k)guoranthens ug/L NO Benzoic Acid ug/L NO Benzyi alcohol uglL NO bis(2-Chloroethoxy)methane uglL r NO bis(2-Chlomethyl) ether ugfL NO bis(2-Chloroisoprepyl) ether ug/L NO bis(2-Ethylhexygphthalate ug/L 160 Butylbenzylphthalate ug/L NO Chrysene ug/L NO Di-n-butylphthalate ug/L NO DIo-octylphthalate uglL NO Dlbenz(a,h)anthrecene ug/L NO Dibenzofuran ug/L ND Diethytphthalate ugfL NO NO Dimethylphthalate ug/L NO Fluomnthene ug/L NO Fluonme ugf- NO HexacNorc-1,3-butadiene uglL NO Hexactllorobenzene ug/L NO HexacNarocydopentadierle ug/L NO Hexachloroethane ug/L ND Indeno(1,2,3-cd)pynew ugtL NO Isophorone ug/L NO N-Nitroso-di-n-propylemine ug/L NO NO N-Nitrosodimethylamine ug/L NO N-Mbasodiphelrylamine ug/L NO Naphthalene ug/L NO Nitrobenzene ug/L NO Pentachlorophend ug/L NO NO Phenanthrene uglL NO Phenol uglL NO Pyrene ug/L NO 2,4,6-Trlbromophenol (S) % 0 2-Fluorobiphenyl (S) % 65 2-Fluorophenol (S) % 0 Nitrobenzene-d6(S) % 66 Phenol-d6 (S) % 0 Terphenyl-dl4 (S) % 55 SO SO 6141 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suits 100 Huntersvllle, NC 28W8 (704)875-9092 Results presenmd on this page are In the units Indlceted by the 'Wits" oclunn except where an slbmate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/131201505:33 PM without the written consent of Pace Analytical Servkea,Inc.. Page 20 of 25 aceAna/Acal e wwwpaaela[a.am QUALITY CONTROL DATA Project ABB - 2nd Annual 2015 Pace Project No.: 92274347 QC Batch: WETl41198 Analysis Method: SM 2540D QC Balch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92274347001 Mt I HUD BLANK 1598226 Associated Lab Samples: 92274347001 Parameter Units Total Suspended Solids _ mg/L LABORATORY CONTROL SAMPLE: 1598227 Parameter Units Total Suspended Solids mglL Pace Analytical services, Inc. 9800 Kmcay Ave. Suite too Huntersvine. NC 2a078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2.5 11l04715 10:18 Spike LCS LCS %Rec Cone. Result %Rec Limits Qualifiers 250 242 97 90-110 SAMPLE DUPLICATE: 1598228 92274504001 Dup Parameter Units Result Result Total Suspended Solids mg/L 78.0 78,0 SAMPLE DUPLICATE: 1598229 92274481001 Dup Parameter Units Result Result Total Suspended Solids mgf- 28.4 7.0 RPD Qualifiers 0 RPD Qualifiers 121 06 9aauire p aluell d an NB page M N Ina units Indlutad by that "tines" column except where an ae.a,a ana B pmeentetl b the right of the reaulL REPORT OF LABORATORY ANALYSIS This report Shan not he reproduced, except in full, Date: 11l1312015 05:33 PM without the written consent of Pace Analytical Services, Inc. Page 21 of 25 Ice Analytical ' mlwpecekDaroat QUALIFIERS Project: ABB - 2nd Annual 2015 Pace Project No.: 92274347 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot, NO - Not Detected at or above adjusted reporting limit. J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. - PQL- Practical Quantftation UrruL RL - Reporting Limit. Pace Analytical Services, Ina 98001dncey Ave. Suite 100 Hunlenwi9e, NC 2807a (704)875.9092 S - Surrogate - - 1,2-Oipherlylhydmzine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte Is a combined concentration. - Consislent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D)- Laboratory Control Sample(Duplicate) MS(D)- Matrix Spike (Duplicate) ' DUP - Sample Duplicate _ RPD - Relative Percent Difference NC - Not Calculable. SG - Slllca Gel - Clean -Up U.- Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis ofAcroleln and Acrylonitrlle by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Dlphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS DO The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L3 Analyte recovery in the laboratory central sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. Mt Matra spike recovery exceeded QC Omits. Batch accepted based on laboratory control sample (LCS) recovery. SO Surrogate recovery outside laboratory control limits. Date: 11/13/2015 05:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent or PaceAnalytical Services, Inc.. Page 22 of 25 uocument Name: 6 Client Name: EoHln Fes; . rv�yN,- vwmi corn nowaou. may w, �� , Pace 1 of 2' Page 2 of 2 Is for Internal Use Only Courier: Fed E ❑ UP❑ USP❑ Clle ❑ C mmerci[I Pace Other Custody Seal on Cooler/BoxPresent: [I yes ne Seale Intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑ Other. Thermometer Used: IR Gun 140 Type of Ice: et Blue None Temp Correction Factor T 2 No Correction , m : M,. ro ?"M12 ❑ S9 plea on Ice, cooling process has begun Corrected Cooler Temp.:,�c ' C Biological Tissue is Frozen: Yes No. WA Date and Initials of person axemining P contents: A Tamp should be above freezing to 6°C Comments: Chain of CustodV Present: ea No ONfA 1. Chain of Custody Filled Out: ea ON. ❑N/A 2. Chain of Custody Relinquished: - t7Yee ONIA 3. Sampler Name & Sf nature on COG: es No ❑ WA 4. Samples Arrived within Hold Time; 216, [IN. PNfA 5. Short Hold Time AnaWsia <72hr : OYes Q o ON/A, 6. Rush Turn Around Time Requested: OYea Q o ONIA 7, Sufficient Volume: Zfes V No OWA 8. Correct Containers Used: O ", ONO ❑NIA 9. -Pace Containers Used: t32ea OLNO ONrA Containers Intact: I k'e's: ONO ON/A 10 Filtered volume received for Dissolved tests ❑Yes Mo O A 11. Sample Labels match COC: es QNo ONIA Q. - -Includes date/tlmeADlAnal is Matrix: tJ All containers needing preservation have been checked. _ 0ec ON, ❑NfA 13. All containers needing preservation are found to be In LJYes LJNo ❑NIA compllance with EPA recommendation. // exce dons: VOA, millarnr, Too, O&O. WI-DRO ate!) 1O'& No Samples checked for dechlorination: I_tYea [IN. OwA 14. Heed's ace in VOA Vials >6mm : OYes O too ONIA 15. Trip Blank Present: OYes ONO OZA 16. Trip Blank Custody Seals Present OYes ONO Ow Pace Trip Blank Lot If ifpurchased): Client Notiflcationl Resolution: Field Data Required? Y I N Person Contacted: Date rims: Comments/ Resolution: SCURF Review: Date: I II SRF Review: Date: I I Note: Whenever there Is a iscrepsncy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cef iOeatian Office (Le out of hold, Incorrect preservative, out of temp, Incorrect containers) WO# : 92274347 II I III II I II II Illlll III 92274347 Paae 24 of 25 Paokialytical` . ..wasaNm.mm CHAIN -OF -CUSTODY / Analytical Request Document The ChAh -Q gopy is a LEGAL DOCVMENT. AN relevam flews mutt becmnplebC accuratary. N `0 N SoctionA Raqulme cowl lMmaallon: Rse�clr ^yD SacSonC PrPjemhe avn Inwim Wohcakn: Page: 01 1 1 OI °gin Reom Ta: Marti n: 1842625 Cary To: Company Name: REGDL RYAGENCY ' Maass)CY_JD NPDES I- GROUNGp*D WATER r DRINKING WATER r UST (' RCRA r OTHER MW La.U. STATE: To: e.L.l Haquoctal Duo DalelTAT: RyrJlare OM¢r No: Project Number: (li.i, �e((JJ--LL Pew Owm PIXA PWOtl Mhn?0ar Paw Pm@a Y. C'C� l/7•./ Requested 'gnalysis:FReied (YM) a w setl D Matrla Copse AVWhMLTFIrI ygmrs Dar-Jrg wamr DW water WT Waste wa8 WW Pmaum P S HMQ a. SL SAMPLE ID °" a. W2. Di 1:1 Air AR Air .. AR SvnpW ala MUST BE UNIDUE Tleaue Ts Dam DT .� 2 g S C w O X o 0 m O v w w COLLECTED 0 F j 0 U < n I' E m w Z r z O x Preservatives z OMOONre araPf muvaPra' m¢ag v m m 7 y T C i S psL.r 2 S. c i O y W. m. = .y ✓ j^ Z L U w y/�p -1 l`IJ 1 Pace Project Nm.l Lab I.D. DATE EMU DATE TIME 2 I 3 t 5 6 T E 9 10 N 4 12 ADDIDONAL COMMENTS RELINMNSNED. BY I AFFILIAEVW DATE TIME ACCEP DSYIAFPILIATICN DATE Ttm5 SAMPLECONDRI°Ns n/ J ORIGINAL lnparunlNMe: BYe9^ee welam Yauaee aaeWm Powl NETaO Mvmxv.nrxm..r SAMPLER NAME"AND.SIGNATURE n 8 18L GGW r}- ^£r $L PRWT Name aI SAMPLER: L. SIGNATt1RE.'of SAMPLER; MW_-._v �_____, _ _ DAM SI(MMOD", 1rr1 ( ,..-•-..-..•« r --..'c .-. soya. FALL-0A20nv.07.15-May-2007 1. Outfall Description: Outfall No. 5WI Structure,(pipe, ditch, etc.) r� i�1 Receiving Stream: t-x T T, r ,a'rP C Describe the industrial activities that occur within the outfall'drainage area: r--, Sre=i,\1 �'iLtr�S cstc��f s o-def 6c IYJI.e� 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark), as descriptors: sk 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Ih�E 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: P 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: P 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 1 V 8. Is there an oil sheen in the stormwater discharge? Yes �� 9. Is there evidence of erosion or deposition at the cutfall? Yes 10. Other Obvious. Indicators of Stormwater Pollution: l , List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU•242, Last modified 10/25/2012 8XAna1y6ca1e W-A—fos.uao November 13, 2015 Mr. Johnny Baines Eastern Environmental Management PO Box 4030 518 S. Pearl Street Rocky Mount, NC 27803 RE: Project: ABB - 2nd Annual 2015 Pace Project No.: 92274347 Dear Mr. Baines: Pace analytical Services, Ina 9800 KIncey Ave. Suite loo Hunteravllle. NC 25078 (704)875.9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most currentTNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, 7�V Taylor Ezell taylor.ezell@pacelabs.com Project Manager Enclosures cc: Ms. Cathy Baines, Eastern Environmental Management REPORT OF LABORATORY ANALYSIS This report $hall not be reproduced, except in fug, 9. without the written consent of Pace Analytical Services, in, Page 1 of 25 AF T WA NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Governor Mr. Faheem Amod Environmental & Safety Supervisor Clarcor Engine Mobile Solutions 230 Clarks Neck Rd Washington, NC 27889 Dear Mr. Amod: John E. Skvarla, III Secretary June 13, 2014 Subject: NPDES General Permit NCG030000 Clarcor Engine Mobile Solutions, LLC Formerly Stanadyne Corporation Certificate of Coverage NCG030005 Beaufort County Division personnel received your request to revise your stormwater permit Certificate of Coverage to accurately reflect your new company and/or facility name. Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the General Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued under the requirements of North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency. If you have any questions or need further information, please contact the Stormwater Permitting Program at (919) 707-9220. Sincerely, ( Q� C� for Tracy E. Davis, P.E., CPM, Director Division of Energy, Mineral and Land Resources cc: Washington Regional Office, T. Edgerton Stormwater Permitting Program Files Central Files Division of Energy, Mineral, and Land Resources Energy Section • Geological Survey Section - Land Quality Section 1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919707-9200 / FAX: 919-715-8801 512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http-//Portal.ncdenr.org/web/ir/ An Equal Opportunity \ Affirmative Action Employer — 50% Recycled \ 10% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND.NATURAL RESOURCES DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030005 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Clarcor Engine Mobile Solutions, LLC is hereby authorized to discharge stormwater from a facility located at Clarcor Engine Mobile Solutions, LLC 230 Clarks Neck Road Washington Beaufort County to receiving waters designated as Tranters Creek, a class C;Sw;NSW water in the Tar -Pamlico River Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective June 13, 2014. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day June 13, 2014. for Tracy E. Davis, P.E., Director Division of Energy, Mineral, and Land Resources By the Authority of the Environmental Management Commission �^ Division of Energy, Mineral & Land Resources 474/;r Land Quality Section/Stormwater Permitting NC®ENR National Pollutant Discharge Elimination System x o� Ermnoxx[mm .wv Nuw.0 aEx.�xrca PERMIT NAME/OWNERSHIP CHANGE FORM FOR AGENCY USE ONLY Date Received Year I Month Day 1. Please enter the permit number for which the change is requested. NPDES Permit (or) Certificate of Coverage Vq. I C 1111 0 1 3 1 0 1 0 10 1 S 11. Permit status prior to requested change. a. Permit issued to (company name): Stanadyne Corporation b. Person legally responsible for permit: WMAY 1 4 2014 pENR p ST RtRNA E bpmr" yVETIANOS O c. Facility name (discharge): d. Facility address: e. Facility contact person: Curtis Ryan First MI Last Plant Manager Title 230 Clarks Neck Road Permit Holder Mailing Address Washington NC 27889 City State Zip (252)975-9260 (252)975-9229 Phone Fax Stanadyne Corporation 230 Clarks Neck Road Address Washington NC 27889 City State Zip Faheem Amod (252) 975-9224 First / MI / Last Phone 111. Please provide the following for the requested change (revised permit). a. Request for change is a rdsult of: M Change in ownership of the facility ❑ Name change of the facility or owner If other please explain b. Permit issued to (company name): Clarcor Engine Mobile Solutions, LLC c. Person legally responsible for permit: Curtis Ryan First Ml Last Plant Manager Title 230 Clarks Neck Road Permit Holder Mailing Address Washington NC 27889 City State Zip (252) 975-9260 cryan(a)stanadyne.com Phone E-mail Address d. Facility name (discharge): Clarcor Engine Mobile Solutions, LLC e. Facility address: 230 Clarks Neck Road Address Washington NC 27889 City State Zip f. Facility contact person: Faheem Amod First MI Last (252) 975-9224 famod(a,stanadyne.com Phone E-mail Address 0Ir� 'p l l q IV. Permit contact information (if different from the person legally responsible for the permit) Revised Jan. 27, 2014 �PDESPERMIT NAME/OWNERSHIP CHANGE FORM y Page 2 of 2 Permit contact: Faheem Amod First MI Last Environmental And Safety Supervisor Title 230 Clarks Neck Road Mailing Address Washington NC 27889 City State Zip (252) 975-9224 famodnastanadyne.com Phone E-mail Address V. Will the permitted facility continue to conduct the same industrial activities conducted prior to this ownership or name change? ® Yes ❑ No (please explain) VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS ARE INCOMPLETE OR MISSING: ❑ This completed application is required for both name change and/or ownership change requests. ❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed, or a bill of sale) is required for an ownership change request. Articles of incorporation are not sufficient for an ownership change. The certifications below must be completed and signed by both the permit holder prior to the change, and the new applicant in the case of an ownership change request. For a name change request, the signed Applicant's Certification is sufficient. PERMITTEE CERTIFICATION (Permit holder prior to ownership change): 1, Curtis Ryan, attest that this application for a name/ownership change has been reviewed and is accurate and complete to the best of my knowledge. I understand that if all required parts of this application are not completed and that if all required supporting information is not included, this application package will be returned as incomplete. 14��tbll= - �7 - � I 11V Signature Date APPLICANT CERTIFICATION 1, Curtis Ryan, attest that this application for a name/ownership change has been reviewed and is accurate and complete to the best of my knowledge. 1 understand that if all required parts of this application are not completed and that if all required supporting information is not included, this application package will be returned as incompI t /� 164`� s�- 6 - tly Signature Date PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO: Division of Energy, Mineral and Land Resources Stormwater Permitting Program 1612 Mail Service Center Raleigh, North Carolina 27699-1612 Revised Jan. 27, 2014 NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Governor Director December 4, 2012 Phil Vick Stanadyne Corporation 230 Clarks Neck Rd Washington, NC 27889 Dee Freeman Secretary Subject: NPDES Stormwater Permit Coverage Renewal Stanadyne Corporation COC Number NCG030005 Beaufort County Dear Permittee: In response to your renewal application for continued coverage under stormwater General Permit NCG030000 the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October 15, 2007 (or as subsequently amended). The following information is included with your permit package: • A new Certificate of Coverage (COC) • A copy of General Permit NCG030000 • A copy of the Technical Bulletin for the General Permit • Two copies of the Discharge Monitoring Report (DMR) Form • Two copies of the Qualitative Monitoring Report Form The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the permit to update your current SPPP to reflect all new permit requirements. The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable, report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this permit and do not count prior exceedances. The more significant changes in the General Permit since your last COC was issued are noted either in the Draft Permit Fact Sheet that accompanied the public notice (http://portal.ncdenr.org/web/wg/ws/su/current- notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit http://portal.ncdenr.org/web/wq/ws/su/npdessw (click on 'General Permits' tab) to review that information for your specific General Permit carefully. 1617 Mail Service Center, Ralegh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Ralegh, North Carolina 27604 Phone: 919-807-63001 FAX: 919-807-6492 Internet: www.ncwaterouality om An Equal Opportunity 1 Affirmative Action Employer NorthCarolina Naturallrf Phil Vick December 4, 2012 Page 2 of 2 Some of the changes include: • Part II: • Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated to the most current language of our permits. Additional conditions for specific industry sectors have been added to the SPPP requirements in some cases. • Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring that the permittee begin a monthly sampling scheme. • Sections B, C: A lower TSS benchmark of 50 mg/I for HOW, ORW, PNA and Tr Waters applies to these more sensitive waters. • Sections B, C., The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other analytical monitoring requirements. • Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined in the "Definitions" section of the permit. • Sections 8, C: The term "Representative Storm Event" has been replaced by "Measurable Storm Event." A measurable storm event is defined in the permit. • Section D: If the permittee fails to respond effectively to problems identified by qualitative monitoring, DWQ may require the permittee to perform corrective action. Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit, including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than 30 days from the date the facility receives the sampling results from the laboratory. Also note that existing permittees do not need to submit a renewal request prior to expiration unless directed by the Division. Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package, please contact the Division's Stormwater Permitting Unit at (919) 807-6300. Sincerely, for Charles Wakild, P.E. cc: DWQ Central Files Stormwater Permitting Unit Files Washington Regional Office STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030005 STORMWATER NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Stanadyne Corporation is hereby authorized to discharge stormwater from a facility located at: Stanadyne Corporation 230 Clarks Neck Rd Washington Beaufort County to receiving waters designated as Tranters Creek, a class C;Sw,NSW waterbody in the Tar - Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, 111, and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective December 4, 2012. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this 4�h day of December, 2012. for Charles Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission sec rn�� NCG- oloo9 S STANADYNE ■ NG(r�3�bo5 Effective May 31, 2006 Please update your records to reflect our Current information: Billing and Shipping Address: Stanadyne Corporation 405 White Street Jacksonville, NC 28546 (P.O. Box has been eliminated) o dm p � C'-3 lfLflJ w m m ND 01 O _I �0� m v o o Stanadyne Corporation 405 White Street Jacksonville, NC 28546, USA Tel: (910) 353-3606: Fax: (910) 353-6807; www.stanadyne.com Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources IJ � —1 CHA -LES WATSON STANADYNE CORPORATION PO BOX 1105 WASHINGTON. NC 27889 Dear Permittee: Alan W. Klimek, P.E., Director Division of Water Quality August 23, 2002 Subject: NPDES Stormwater Permit Renewal STANADYNE CORPORATION COC Number NCG030005 Beaufort County In response to your renewal application for continued coverage under general permit NCG030000, the Division of Water Quality (DWQ) is forwarding herewith the reissued stoimwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983. The following information is included with your permit package: * A new Certificate of Coverage * A copy of General Stormwater Permit NCG030000 * A copy of the Analytical Monitoring Form (DMR) * A copy of a Technical Bulletin for the general permit Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable federal. state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this per package please contact Bill Mills of the Central Office Stormwater and General Permits Unit at (919) 733-5083, ext. 548 Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Stormwater & General Permits Unit Files Washington Regional Office NNA NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NO 27699-1617 (919) 733-7015 Customer Service 1- 800-623-7748 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030006 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, ABB INC is hereby authorized to discharge stormwater from a facility located at ABB INC-EDGECOMBE HWY 43 NORTH PINETOPS EDGECOMBE COUNTY to receiving waters designated as a UT to Towne Creek, a class C NSW stream, in the Tar - Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, IV. V, and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective September I, 2002. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 23, 2002. for Alan W. Klimek, P.E.. Director Division of Water Quality By Authority of the Environmental Management Commission STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030005 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, STANADYNE CORPORATION is hereby authorized to discharge stormwater from a facility located at STANADYNE CORPORATION 230 CLARKS NECK ROAD WASHINGTON BEAUFORT COUNTY to receiving waters desi=nated as Tranters Creek, a class WS-IV SW NSW CA stream, in the Tar - Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, IV, V. and VI of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective September 1, 2002. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 23, 2002. for Alan W. Klimek, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality August 23, 2002 TOM BOYLAN ABB INC-EDGECOMBE PO BOX 687 PINE TOPS, NC 27864 Subject: NPDES Stormwater Permit Renewal ABB INC-EDGECOMBE COC Number NCG030006 Edgecombe County Dear Permittee: In response to your renewal application for continued coverage under general permit NCG030000. the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1981 The following information is included with your permit package: * A new Certificate of Coverage * A copy of General Stormwater Permit NCG030000 * A copy of the Analytical Monitoring Form (DMR) A copy of a Technical Bulletin for the general permit Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule. standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater and General Permits Unit at (919) 733-5083, ext. 548 Sincerely. Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Stormwater & General Permits Unit Files Raleigh Regional Office ITMAW NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1-800-623-7748 WA7F9 11'' ' r r ■ � —1 ® 'C TOM BOYLAN ABB POWER T&D CO INC-EDGECOMBE PO BOX 687 PINE TOPS. NC 27864 Dcar Pennittee: Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Gregory J. Thorpe, Ph.D. Acting Director Division of Water Quality December 27, 2001 Subject: NPDES Stormwater Permit Renewal ABB POWER T&D CO INC-EDGECOMBE COC Number NCG030006 Edgecombe County Your facility is currently covered for stor nwater discharge under General Permit NCG030000. This permit expires on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for continued coverage under the reissued permit. In order to assure your continued coverage under the general permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued coverage under the general permit. Failure to request renewal within this time period may result in a civil -assessment of at least $250.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could result in assessments of civil penalties of up to $10.000 per day. Please note that recent federal legislation has extended the "no exposure exclusion' to all operators of industrial facilities in any of the I I categories of "storm water discharges associated with industrial activity," (except construction activities). If you Ieel your facility can certify a condition of "no exposure", i.e. the facifty industrial materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional information contact the Central Office Stormwater Staff member listed below or check the Smrmwater & General Permits Unit Web Site at htip://h2o.enr.state.nc.us/su/stormwater.html If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the rescission process has been completed. If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at (919) 733-5083. ext. 548 Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Raleigh Regional Offce ern NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1- 800-623-7748 Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources 9 r Gregory J. Thorpe, Ph.D. "1 Acting Director Division of Water Quality December 27, 2001 CHARLES WATSON STANADYNE AU"fOMOTIVE CORPORATION PO BOX 1 105 WASHINGTON, NC 27889 Subject: NPDES Stormwater Permit Renewal STANADYNE AUTOMOTIVE CORPORATION CDC Number NCG030005 Beaufort County Dear Permittee: Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for continued coverage under the reissued permit. In order to assure your continued coverage under the general permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued coverage under the general permit. Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could result in assessments of civil penalties of up to $10,000 per day. Please note that recent federal legislation has extended the "no exposure exclusion' to all operators of industrial facilities in any of the I I categories of "storm water discharges associated with industrial activity," (except construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General Permits Unit Web Site at hnp:Hh2o.err.state.nc.us/su/stormwater.litml If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the rescission process has been completed. if you have any questions regarding the permit renewal procedures please contact Robert Tankard of the Washington Regional Office at 252-946-6481 or Bill Mills of the Central Office Stormwater Unit at (919) 733-5083, ext. 548 Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Washington Regional Office dwA NCDENR N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 Customer Service 1-800-623-7748 _ State of North Carolina Department of Environment, Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director October 1, 1997 TOM BOYLAN ABB POWER T&D CO INC-EDGECOMBE P O BOX 687 PINE TOPS, NC 27864 IDFEE HNF1 Subject: Reissued Stormwater General Permit for Certificate of Coverage No. NCG030006 Edgecombe County Dear Permittee: In response to your renewal application for continued coverage under the subject permit, the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. The following information is included with your permit package: o A copy of the stormwater general permit. ■ A Stormwater Pollution Prevention Plan Certification Form. This form certifies that you have developed and implemented the Stormwater Pollution Prevention Plan (SPPP) required in your permit. This form must be completed and returned to the Division within 30 days of receipt of this letter. DO NOT send the SPPP with the signed form. ■ Five copies of Analytical Monitoring forms. ■ Five copies of Qualitative Monitoring forms. ■ A copy of a Technical Bulletin on the stormwater program with outlines program components and addresses frequently asked questions. m A corrected Certificate of Coverage if you indicated a name or address change on the Renewal Form returned to the Division. Your certificate of coverage is not transferable except after notice to DWQ. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DWQ or permits required by the Division of Land Resources, Division of Air Quality, Coastal Area Management Act or any other Federal or Local governmental permits that may be required. If you have any questions conceming this permit or other attached documents, please contact the Stormwater Group at telephone number (919) 733-5083 Sincerely, for A. Preston Howard, Jr., P. E. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE NO. NCG030006 STOR,MWATER DISCHARGES In compliance with the provision of Notch Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, ABB POWER T&D CO INC-EDGECOMBE is herby authorized to discharge stormwater from a facility located at: HIGHWAY 43 NORTH PINETOPS, NC EDGECOMBE COUNTY to receiving waters designated as UT To Towne Creek in the TAR-PAMLICO River Basin in accordance with the effluent limitations, monitoring requirements and other conditions set forth in Parts I, II, III and IV of General Permit No. NCG030000 as attached. This Certificate of Coverage shall become effective September 15, 1997 This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day October 1,1997 for A. Preston Howard, Jr., P.E.. Director Division of Water Quality By Authorization of the Environmental Management Commission i 1�Q.V 4 - State of North Carolina Department of Environment, Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director October 1, 1997 CHARLES WATSON STANADYNE AUTOMOTIVE CORP. P. O. BOX 1105 WASHINGTON, NC 27889 A1kT:.W;VA IT IDFEE HNFi Subject: Reissued Stormwater General Permit for Certificate of Coverage No. NCG030005 Beaufort County Dear Permittee: In response to your renewal application for continued coverage under the subject permit, the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. The following information is included with your permit package: ■ A copy of the stormwater general permit. ■ A Stormwater Pollution Prevention Plan Certification Form. This form certifies that you have developed and implemented the Stormwater Pollution Prevention Plan (SPPP) required in your permit. This form must be completed and returned to the Division within 30 days of receipt of this letter. DO NOT send the SPPP with the signed form. Five copies of Analytical Monitoring forms. ■ Five copies of Qualitative Monitoring forms. ■ A copy of a Technical Bulletin on the stormwater program with outlines program components and addresses frequently asked questions. • A corrected Certificate of Coverage if you indicated a name or address change on the Renewal Form returned to the Division. Your certificate of coverage is not transferable except after notice to DWQ. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by DWQ or permits required by the Division of Land Resources, Division of Air Quality, Coastal Area Management Act or any other Federal or Local governmental permits that may be required. If you have any questions concerning this permit or other attached documents, please contact the Stormwater Group at telephone number (919) 733-5083 Sincerely, for A. Preston Howard, Jr., P. E. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE NO. NCG030005 STOR,MWATER DISCHARGES In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, STANADYNE AUTOMOTIVE CORP. is herby authorized to discharge stormwater from a facility located at: 230 CLARKS NECK ROAD WASHINGTON, NC BEAUFORT COUNTY to receiving waters designated as Trainers Cr.-Tar River -Cherry Run in the TAR-PAMLICO River Basin in accordance with the effluent limitations, monitoring requirements and other conditions set forth in Parts I, II, I11 and IV of General Permit No. NCG030000 as attached. This Certificate of Coverage shall become effective September 15, 1997 This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day October 1,1997 for A. Preston Howard, Jr., P.E., Director Division of Water Quality By Authorization of the Environmental Management Commission State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary A. Preston Howard, Jr., P.E., Director Randy Varni Stanadyne Automotive Corporation P O Box 1105 Washington, NC 27889 Dear Mr. Varni: July 30, 1993 Subject: General Permit No. NCG030000 Stanadyne Automotive Corporation COC NCG030005 Beaufort County In accordance with your application for discharge permit received on August 31, 1992, we are forwarding herewith the subject certificate of coverage to discharge under the subject state NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Environmental Management. The Division of Environmental Management may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Mr. Steve Ulmer at telephone number 919n33- 5083. cc: Sincerely, Original Signed BY Coleen H. Sullins A. Preston Howard, Jr., P. E. Washington Regional Office P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919.733.5083 FAX 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAGEMENT STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Stanadyne Automotive Corporation is hereby authorized to discharge stormwater from a facility located at Stanadyne Automotive Corporation Clarks Neck Road (SR 1403) Washington Beaufort County to receiving waters designated as Tranters Creek in the Tar -Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Pans I, 11, III and IV of General Permit No. NCG030000 as attached. This Certificate of Coverage shall become effective July 30, 1993. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day July 30, 1993. Original Signed By Coleen H. Sullins A. Preston Howard, Jr., P.E., Director Division of Environmental Management By Authority of the Environmental Management Commission ,y e. — d, �• ,O,tu "� a t.. _ f i�_ _ _.i �\�, lat?,(�� :^\ 0 : •� �/ �.� \��l V \y/\�\ y ---f-= __'=`•~ __._�° c�/��'___--_ � '���' j�. !fit ��� rp Jt,� o- \ IyY���J ��CC f �xV �• ��, 2-.o� n �• ��A DaybeScoR o 'oUaybeaton ._ ,s (�jj�^V�).f�( I .e9, W�1 DaYbeacon nh �-x '•�v -.-DaYb acaGlen.(G) °• e�3.n�♦_ 14 �� '� \ / -P antic _ ,� q Daybeacori�o Pile _ \// ` ,._SO �I r c_Inpoin � � 7 / ' Y ! 7. -{yJHED) BM` /l—NOFFOLK1 - IId3 Janctfon/l Radio Ton eaF)s Y ♦' oji ifl . (w/ Sll f/ 08 , J(`<'�� 0: F•�--ifp� ( �Yi�(I V/�\`- �•!,-.� \CreeF, /C� J _ BM �f t3g Marsden \ c�.\ h- Qx l A._ .. Station .�� � ��. • ��q • � Cam- ��_ ���1\. - �M`v t7 -_. s. .s U\ Tnn�� v� n 25 r����VA ins �b�o l_� T blor"Cr. F�ytir Ch 'CHOC i. � FACILITY J COUra�i a NPDES MAP # DSN FLOW STANp.p�'NE GFUr�rtio-ii V� CveP�t���r� �;eA-L4 rvpl- NCc�o�boo� �3�sc SITS BASIN R LATTITUDE ' LONGITUDE RECEIVING STREW STREAM CLASS 4 4 DISCHARGE CLASS EXPIMATION DATE 03-03--d(p 356351 50 i M w4--rE7L- erg— 31 9-1 I EM State of North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management 512 North Salisbury Street • Raleigh, North Carolina 27604 James B. Hunt, Jr., Governor _ Jonathan B. Howes, Secretary April 16, 1993 Wayne D. Nock ABB Power T&D Company, Inc. 630 Sentry Park Blue Bell, PA 19422 Dear Mr. Nock: A. Preston Howard, Jr., P. E. Director Subject: General Permit No. NCG030000 ABB Power T&D Company, Inc. COC NCG030006 Edgecombe County In accordance with your application for discharge permit received on September 8, 1992, we are forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983. If any parts, measurement frequencies or sampling. requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Environmental Management. The Division of Environmental Management may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 919/733- 5083. Sincerely, U;;gtriai Signed By Coleen H. Sullins A. Preston Howard, Jr., P.E. Raleigh Regional Office Pollution Prevention Pays P.O. Box 20535, Raleigh, North Carolina 27626-0535 Telephone 919-733-7015 An Equal Opportunity Affirmative Action Employer STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES DMSION OF ENVIRONMENTAL MANAGEMENT STORMWATER DISCHARGES NATIONAL POLI UTANT DIS HARCE LIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, ABB Power T & D Company, Inc. is hereby authorized to discharge stormwater from a facility located at ABB Power T & D Company, Inc. NC Hwy 43 N, approx. one mile north Pinetops Edgecombe County to receiving waters designated as an unnamed tributary to Town Creek in the Tar -Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, III and IV of General Permit No. NCG030000 as attached. This certificate of coverage shall become effective April 16, 1993. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day April 16, 1993. Original Signed By Coleen H. Sullins A. Preston Howard, Jr., P.E., Director. Division of Environmental Management By Authority of the Environmental Management Commission =I� 4, Cem NJ Town Creek _I ' 1 =es7 t : •, — 2500 8000 i i 7000 !% v 2000 6000 — r y„ o� _ .. o .7 4 - r 1 5000 1500 O o, 4000 1000 �yl 3000 900 — 00 \ +r — 7 00 Z 3965 2000 Epp 500 Sewage Di pal al ly 1000 300 100 0 100 �„„ �•o I x` 0 0 Feet Meters ,64 1 .30/8 C 1.2192 7 P5336 • • • •Il: r J 8 21394 9 2,7432 10 30480 �.72 � TO Moved feet to meters r - r z multiply M 30e8 to fat is I.ed meters mulfipltipy M 3.2808 o / /k FACILITY cOUNIy , ' O:L Cj- 35 o Co NPDES MAP DSN FLOW v3 l Sl B i'nv: Z l l Lp�'TITUDE �, 35v 48 13 a1 ° LONGITUDE o 2t5' 3�5 uN�n M STREAM RECEIVING STREAM CLASS ! G N CLASS S� � 0 A7� DISCHARGE I:_,. DATE n8- 3I -q EXPIRATION 1 III/ \ •Lower Town Creek is / (IN21I /.. Cem I ��_ r� II 1141 /•'-� \ n - Af5F3'v � Y / l =� `Q}k , it Cems .... 30 11 _—_.__._ _ , .� err 1 • l l lil q / Cem : �Ce\tn �P 'a � - - FFF✓FF°� rl'�; n �� II ?.. .3" C� I' nary%�N� .._ _ I � C n' ° I' Cem �/ Cem \ , 1'er`✓.. i i�� • _ ��r /!( Cem`, 0 , 9000 i 3967 2500 8000 120 7000 re 1, z N 60DO _ o � a 6000 I I500 I _ Qi / I 4000 -' - i r;{ 1000 3000 900 /I Q 800 ?DO 3965 2000— 600 800 lwage Dis lsposall= IDDD 3Do , 200 100 0 0 Feet Melers ashy 1 6096 9 .9144 q / / 47'39' 4 1.2192 6 1.82 / 6 1828886 7 � 2.336 8 241U81 2In/ 9 2,7432 / I ID 70480 J To mpveM1 fort to meters Is, mm7 byaatip6 t x, )PS �� ( H 3o wsrsd metro I. feel / o mullipry 61328U ate` II ' STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. n c6 D 3 coo f DOC TYPE STORICAL FILE MONITORING REPORTS DOC DATE ❑ YYYYM M D D STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. IV U& W -7 DOC TYPE ❑ HISTORICAL FILE L` MONITORING REPORTS DOC DATE YYYYM M DD - . Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted S—1 7- I S CERTIFICATE OF COVERAGE NO. NCG03 D 3 O % FACILITY NAME rni�-ed Tco) I S'-raw,0i r,C (o, aF AJC COUNTY Cuwtbtr PERSON COLLECTING SAMPLES TIn/ 0Le_- LABORATORY V{�irYO hiAG Lab Cert. # NCON& #!l Comments on sample collection or analysts: 4X PO/'/ 3i 37-71 c( Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Zo / 9 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or [Z Monthly' rl month REMSSCH�ARGINGTOCLASS ❑ORW HQW ❑❑ Trout PNA LJ ❑Zero -flow ❑Water Supply ❑SA MAY 2 3.2019 ❑other. CEN7NAL FILE$ . PLEASELREMEM13ER TO SIGN ON PAGES 2 AND/OR 3 4 DVVR SECTION ❑ No discharge this period. Outfall No`- Benchmarks -_> Date3ample Collected i (mo/dd/yrl, '' 5 —�'1 24 hour rainfall amount,, '- Inches3', 405 Total 9uspended'Solids 100 m-/L or 50'mg/L G 1 P H Standard units;. 5 �r Copper LO.ZS?2 Lead 0.03:0L ca-OSO Zinc . ' 9i067 mg/Lr cO.azg Non Pola�;0&G/ Total Petroleiim Hydrocarbons . g 1 m /L': c5 O Total Toxic Organics 1 mg/L 'Month samcling linsiead of cami_annuall z — - a , cn'--V anLC ,u, Lift same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling Is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that Incorporate a solvent management plan Into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit,.BDL, <PQL, Non -detect, ND, or other similar non -numerical format: When results are below the applicable limits, they must be reported in the format. "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report.a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Footnotesfr No discharge this period?Z. Outfall No Date Sample 24 hour rainfall Collected' amount,1 Non polarO&G/TPHby 9 - Total Suspended solids - pH (rno/dd/yr) Inches. EPA 1664'(SGT-HEM) Benchmarks >,•..:: :is mg/L 100 mg/L or SQmg/O 6.0-9:o Su am Part A also aooly to this Part e `.See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: - "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, including the passibility of fines and Imprisonment for knowing violations." Permittee) Permit Date:11/1/2012-10/31/2017 5-1-7-15 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 �VMICROBACg Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9D0078 United Tool & Stamping Project Name: United Tool & Stamping Mr. Justin Hoover Project / PO Number: N/A 2817 Enterprise Avenue Received: 04/05/2019 Fayetteville, NC 28306 Reported: 04/19/2019 Case Narrative Field pH (by client): 5.8 Analytical Testing Parameters Client Sample ID: Stormwater, grab Sample Matrix: Stormwater Collected By: Hoover Lab Sample ID: K9D0078-01 Collection Date: 04/05/2019 10:45 Wet Chemistry Result RL Units Note Prepared Analyzed Analyst Method: EPA 1664 Rev. B Oil & Grease (SGT-HEM) <5.00 5.00 mg/L 04/16/19 1113 TAB Method: SM 2540 D-2011 Total Suspended Solids <4.17 4.17 - mg/L 04/08/19 1543 TMC Metals Result RL Units Note Prepared Analyzed Analyst Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994 Capper <0.250 0.250 mg/L 04/12/19 1318 04/12/19 1318 TAB Lead <0.050 0.050 mg/L 04/12/19 1318 04/12/19 1318 TAB Zinc <0.025 0.025 mg/L 04/12/19 1318 04/12/19 1318 TAB Definitions RL: Reporting Limit Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to/��f vQ�Ldrl applicable accreditation standard unless otherwise noted. �(j/f C/ The data and information on this, and other accompanying documents, represents only the samples) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental Reported: 04/192019 09:02 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I w .microbac.com Page 1 of 2 (§DMICROBACO Fayetteville DMsIo . n 2592 Hope NMs Road — Fayeffevifle . NC 2830S (9 *K9DO078* Fax CHAIN OF CUSTODY RECORD F f_y,-Jr.Vjjj& A)f =3 D6 0 0 TYPE OF ANALYSIS PRESERVATION (CODE) r4 010 32,3 L wv 9At6 WPS At YM DATE TIME 01 9-n n Lo I ft rpy"A"11 E111 11 m- m 11110 ft �,, , 1016% i Xg mo IS DATA FOR REG. COMPLIANCE PURPOSE? NO Pk 5.9 YES. WHICH: mmam� TurnmDund time: REGULAR RUSH Comments w Spedal H—rd : Ua rcL REVIEWED Page 2 of 2 Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. htM:1/12ortal.ncdenr.org/web/ir/npdes-stormwater/­ Permit No.: N/C/V Facility Name:.�J. County: Uuwh, Inspector: �1us Date of Inspection: Time of Inspection: 30 Total Event Precipitation (inches): 1,0S i.: N/C/fim/3-/0/3/O/Z/ n c. 9l o— 323 — 9,5Y9 Was this a "Representative Storm Event" or "Measureable Storm Event' as defined by the permit? (See information below.) M Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event' or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event' or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatWq, I certify that this report is accurate and complete to the best of my knowledge: or Designee) Pagel of 2 1. Outfall Description: p Outfall No. Structure (pipe, ditch, etc.) e- rui 7&7gL P ' . Receiving Stream: R/ouka-r Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: n Io rn /o r 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A %6 r9i�ao 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Floating solids: 1.. 0 2 3 4 5 Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU•242, Last modified 7/31/2013