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HomeMy WebLinkAboutWQ0002834_2019 Residual Annual Report_20200224Theresa Coletta Mayor Jeanne Martin Torn Clerk Ms. Sonya Gregory Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 Ms. Gregory, Town of Burnsville 02/13/2020 Councilors: Judy Buchanan Denise Collier Qussell Fox Bunnie McIntosh Please find enclosed the original and two copies of the Town of Burnsville's Biosolids Annual Report for your review and approval. There was not a compost pile built in 2019. This information is a new analysis from the pile built in 2018. If you have any questions please call the ORC at 828-260-2027. Thank you, P blic Works Director DEB w � 2Q perm��t�nq FFg S 4 2020 t. P.O. Box 97 0 Burnsville, North Carolina 2874 0 Phone (828) 682-2420 • PAX (828) 682-7757 Facility Name: Town of Burnsville WWTP Name: Town of Burnsville WQ Permit Number: W00002834 NPDES Number: NCO020290 Monitoring Period: From 1/1/2019 To 12/31/2019 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt. A (time/temp) Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed Class A or Class B complete the following monit ring data: Parameter Allowable Level iaof n Slud g Pathogen Density Number Excee- dences Frequency of Analysis Sample Type Analytical Tech- ni ue inim Geo. Mean aximu Units 2 x 10 to the 6th power MP N per gram of Fecal Coliform total solids CFU 1000 mpn per m of total solid 21.7 40.2 mpn/kg 0 only pile G sm9221 e2 (dry weight) Salmonella 3 MPN per 4 bacteria (in lieu of grams total solid fecal coliform) (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative nerformed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) Alt. 6 (Alk. Stabilization ❑ It. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) Alt 7 (Drying - Stable) [IAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) CR "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." N Signature *Preparer is i Brewer, ORC and Title (< e or Land Applier Name and Title (if applicable)(type or print) ,parer* Date Signature of Land Applier (if applicable) in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date BRLPAASTER FECAL LITY LAS & OPERATIONS; INC. PO. BOX 1167 aNNER ELK, NC 28604 (828)898-6277 CLIENT: TOWN OF I LOGIN TIME: ADDRESS: SAMPLER: Steve Taylor CITY: RECEIVED DATE: 6-Mar-19 STATE: NC REPORTED DATE: 15-Mar-19 !D#: NCO020290 ANALYSIS LSID# ANALYSIS MOL's UNITS METHOD SAMPLE ANALYSIS INT RESULTS LOCATION DATE TOTAL SOLIDS 33 °h BURN. SLUDGE FECAL 1 <7 1.00 MPN/G SM9221E2 #3 7-Mar-19 PUPY TOTAL SOLIDS 26.4 % BURN. SLUDGE FECAL 2 <8 1.00 MPN/G SM9221E2 #3 7-Mar-19 P[/PY TOTAL SOLIDS 21.7 OA BURN. SLUDGE FECAL 3 <9 1.00 1 MPN/G SM9221E2 #3 7-Mar-19 PUPY TOTAL SOLIDS 33.1 % BURN. SLUDGE FECAL 4 <7 1.00 1 MPN/G SM9221E2 #3 7-Mar-19 PI/PY TOTAL SOLIDS 30A % BURN. SLUDGE FECAL 5 <7 1.00 MPN/G SM9221E2 #3 7-Mar-19 PI/PY TOTAL SOLIDS 29.8 % BURN. SLUDGE FECAL 6 <7 i.00 MPNIG SM9221E2 #3 7-Mar-19 PI /PY TOTAL SOLIDS 40.2 % BURN. SLUDGE FECAL. 7 <5 1.00 MPN1G SM9221E2 #3 7-Mar-19 PI REPORTED BY: NC CERTIFIED LAB # 544 PAUL ISENHOUR.. SUPERVISOR CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: W00002834 FACILITY NAME: Town of Burnsville PHONE: 828-682-2420 COUNTY: Yancey OPERATOR: Jadd Brewer FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ® Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes ka No ❑ If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) V lume (dry tons Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons Intended use(s) January NCO020290POTW 40 20.62 60.62 TERRY MILLER 0.69 NONROOT/LEF CROP February Digester CHAD PRISK 0.13 SOIL CONDITIONER March JAQUELINE THOMAS 0.77 POTTING SOIL/MULCH April JEFF TRUIT 0.25 May RANDY BAKER 6.25 PASTURE June WILLARD JOBE 4.14 PASTURE July BILLY RATHBURN 1.03 MULCH August STEVE TONY 0.25 NONROOT/LEAF CROP September RUSSELL BANKS 0.13 NONROOT/LEAF CROP October LEE RULE 0.17 POTTING SOIL/MULCH November WILLIAM MEEHAN 0.04 MULCH December H.C. MARTIN 0.04 MULCH Total from FORM DMSDF (sup) 40 20.62 60.62 Totals: Annual (drytons : 80 I 41.24 121.24 13.89 Amendment(s) used: I Bulking Agent(s) used: wood chips * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Part C: Total Number of Form DMSDF (Supp) Facility was compliant during the past calendar year with all conditions of the land application 14 Yes permit (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No - If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submi 'ng fats formation, including the possibility of fines and impri ment for knowin " -1--, Signature ermittee Date Signature eparer** Date **Pr er is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) (if dill t from Permittee) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0002834 FACILITY NAME: PHONE: 828-682-2420 COUNTY: Yancey FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A -"Month", 1 Distribution and Marketinm (complete Parts A Town of Burnsville OPERATOR: Jadd Brewer "Source(s)" and "Residual In" columns only) and B) Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) 40 20.62 60.62 LILIANA GUTIERREZ 0.21 NONROOT/LEAF CROP JOE HENSLEY 0.21 POTTING SOIL DALE BOLE 0.47 SOIL BOLE JIMMY AYER 12.07 POTTING SOIL/MULCH ALEX CHAPPELEAR 2.04 SOIL CONDITIONER RICHARD YORK 0.64 MULCH WAYNE RATHBURN 4.85 MULCH JOE GIARDINA 0.3 MULCH Totals: Annual (dry tons): 40 20.62 60.62 20.79 Amendment(s) used: I Bulking Agent(s) used: WOOD CHIPS * If more space is required, attach additional information sheets (FORM DMSDF (supp# Total Number of Form DMSDF (Supp) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0002834 Laboratory: 1) Envionmental Testing Solutions Facility Name: Town of Burnsville 2) Water Quality Labs Residual Source WQ # or NPDES #: NCO020290 WWTP Name: Town of Burnsville Residual Analysis Data 3) 4) 5) Parameter (mg/kg) Ceiling Conc. Limit (mg/kg)a Sam le or Com osite Date 07/11/19 Percent Solids % NA 22 Arsenic 75 <6.29 Cadmium 85 <2.52 Copper 4,300 132 Chromium NA NA Lead 840 13.4 Mercury 57 1.6 Molybdenum 75 <6.29 Nickel 420 30.8 Selenium 100 <6.29 Zinc 7,500 270 Total Phosphorus NA 7390 TKN 1370 21900 Ammonia -Nitrogen 8.7 0.6 Nitrate and Nitrite 30 <30 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly pAered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of f es and finprisonment forjuwW'n,A violations." Signature of Preparer * *Preparer is defined in 40 CFR Part 5 .9 and 15A NCAC 2T .1102 (26) L�� �Z Date ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0002834 Laboratory: 1) Environmental Testing Solutions Facility Name: Town of Burnsville 2) Water Quality Labs Residual Source NPDES # or WQ#: WWTP Name: Residual Analysis Data NCO020290 Town of Burnsville 3) 4) 5) Parameter M Sample or p. Date - .. ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure t at qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaffies Ar submitting falsginfoVmation, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * *Preparer is defined in Part 503.9(r) and 15A NCAC 2T .1102 (26) Date Pile Number 2u 1 6{ TOWN OF BURNSVILLE Date Initials Tempt Temp 2 Temp 3 Temp 4 Temp 5 Temp 6 Temp 7 Temp 8 2 (`{� ( 3 1 F 3 of G-r F Y F 6 F 3 S F l 35 F F F o f (ott F t F 1 (p F 3 F `3 F F F I JLF i i C, F IZ-1, F t�i F _7 F ' F F Zj 3U F F F F F J F F F 17 F F I 7Z F ";' F 1 2 F F L: Z....F F F F LF F F F F F F F F L Z- F Of 4 F L F F S-'--F Z F G F 3 2_-.F S—\—F F F F '�"-F ( F F F F S"rF F F �F F F F F F F Z F F F F F F F F 6 F :)A F F F -3 3 F F F F F F F 1 33 F 1 5> F I D F F �G y11 F (3-T F C) F 6 F F Sf F F F 2-7 yS F F / F Gf F F ) F y F F Z F t3S�F /'ZO F / F 3 F `"F IV3 F F �1 �iF F( C,> F t-16 F F F 15-5 F F z Z e57y VO 1-/-1 F F L-1 6 F F F( 6 F F 3 6z--p q6 F 31' F 16 F 15A F( F F J F F 2-1 LA GL`Z F I S F ` F( ZS F 1� Z F F KF F F �F TD F F F —F F F I GL ( F 3 `" F 6 F H� F J �12 F J� F (,J�F F F �� F F Cj F /�{ Z F_ F F F �j"F 0 3 Z F I F jqy F{Ll 2 F o- F F F Z GG If-? F FI 6Z, F i—(2—F F F F -( F f 3 v F (i't _ F I L& F 1,-CQ F F O F F Z ` F 2 i-+ F 160 F JLJ F F F j J F F 12Lj F F FI q-0 F I F( F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F F Sampling Date Sampling Depth Number of Samples Taken Page of 1 Environmental Testing Solutions, Inc. Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project name: Town of Burnsville WWTP Project number: 190711.508 Collection date: 11-Jtd-19 Date received: l l-Jul-19 Sample identification: 2017-2018 Compost Pile - Grab Sample number: 170493 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Arsenic 6010 C <6.29 6.29 mg/kg 16-Jul-19 MLR 1 Cadmium 6010 C <2.52 2.52 mg/kg 16-Jul-19 MLR 1 Copper 6010 C 132 2.52 mg/kg 16-1ul-19 MLR 1 Lead 6010 C 13.4 6.29 mg/kg 16-1ul-19 MLR 1 Molybdenum 6010 C <6.29 6.29 mg/kg 16-Jul-19 MLR 1 Nickel 6010 C 30.8 2.52 mg/kg 16-Jul-19 MLR 1 Selenium 6010 C <6.29 6.29 mg/kg 16-Jul-19 MLR 1 Aluminium 6010 C 8540 629 mg/kg 16-1ul-19 MLR 1 Calcium 6010 C 14800 1390 mg/kg 16-Jul-19 MLR 1 Magnesium 6010 C 3180 62.9 mg/kg 16-Jul-19 MLR 1 Potassium 6010 C 3080 12.6 mg/kg 16-1ul-19 MLR 1 Sodium 6010 C 127 13.9 mg/kg 16-Jul.19 MLR 1 Mercury 7471B 1.6 0.080 mg/kg I6-Jul-19 TLT 1 Total Kjeldahl Nitrogen 351.2 21900 1370 mg/kg 17-1ul-19 NCR 1 Nitrate + Nitrate 300.0 <30.0 30.0 mg/kg 16-Jul-19 LBW 1 Total Nitrogen Calculation 21900 42.6 mg/kg 17-Jul-i9 NCR 1 Total Phosphorus 200.7 7390 629 mg/kg 16-Jul-19 LMC 1 Total Solids SM2540 G 23.5 0.10 % 16-Jul-19 MLR 1 pH in Soil SW 846 9045D 6.6 0.10 S.U. I I-Jul-I9 MS 2 % Total Solid SM 2540 G 22 0.10 % 11-Jul-19 MS Ammonia Nitrogen EPA 350.3 0.60 8.7 mg/kg 18-Jul-19 KEK 3 Plant Avaliable Nitrogen CALC 2193 mg/kg 20-Jul-19 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by Rogers & Callcott Environmental. 2. Sample analyzed outside holding time. The duplicate result was 6.7 S.U. 3. Duplicate was outside established limits. Validity of data is not affected. Date reviewed: Data reviewed by: Kelley E. Keenan Signature: NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. Rogers & Callcott ENVIRONMENTAL Client Environmental Testing Solutions Kelley E. Keenan 351 Depot St. Asheville, NC 28801-4310 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory Services Burnsville WWTP 9070827 07/12/2019 11:30 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on July 12, 2019. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Lauren Woodrum, your Project Manager, at lauren.woodrum(cz)rogersandcallcott.com or (864)-232-1556 if you have any questions about this report. Report Approved By Lauren Woodrum Project Manager This report inav not be reproduced, except in full, without written perinission from Rogers & Collcotl. Inc. --P0--8ox3655 1 Grtsenvitle. SC 29606 ! 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company Page 1 of 11 _ Rogers &Callcott A. ENVIRONMENTAL Certificate of Analysis South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Client Environmental Testing Solutions Project: Burnsville WWTP Kelley E. Keenan Rork Order: 9070827 351 Depot St. Received: 07/12/2019 11.30 Asheville, NC 28801-4310 Sample Number Sample Description Matrix Sampled 9070827-01 Burnsville WWTP 2017-2018 Compost Pile Solid 07/11/19 09:00 Type Grab PO Box 5655 Greenville, SC 29606 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 r'Ogen Sap d Ca.11COtt. om 0- 19 2019 16:14 This report mqv not be reproduced, except in full, without written permission from Rogers X Callcott, hic. Page 2 ff 1 1 Rogers & Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 Sample Data Sample Number 9070827-01 Sample Description Burnsville WWTP 2017-2018 Compost Pile collected on 07/11/19 08:00 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analvst Batch General Chemistry Parameters Nitrate asN ND 25.0 mg/kgdry 5.00 07/16/19 18:31 EPA300.0 X LBW B9G0852 Nitrite asN ND 5.0 mg/kgdry 5.00 07/16/19 18:31 EPA300.0 X LBW B9G0852 Total Kjeldahl Nitrogen 21900 1370 mg/kg dry 10.0 07/17/19 17:48 EPA351.2 NCR B9G0771 Total Nitrogen (TKN+Nitrate+Nitrite) 21900 42.6 mg/kg dry 1.00 07/17/19 17:48 NCR B9G1033 Total Solids 23.5 0.10 % 1.00 07/16/19 16:00 SM2540G MLR B9G0811 Total Metals Mercury 1.6 0.080 mg/kgdry 1.00 07/16/19 09:38 EPA7471B TLT B9G0682 Aluminum 8540 629 mg/kgdry 100 07/16/19 20:24 EPA6010D LMC B9G0736 Arsenic ND 6.29 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Cadmium ND 2.52 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Calcium 14800 1390 mg/kgdry 100 07/19/19 13:16 EPA6010D LMC B9G0912 Copper 132 2.52 mg/kg dry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Lead 13.4 6.29 mgngdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Magnesium 3180 62.9 mg/kgdry 10.0 07/16/10 20:28 EPA6010D LMC B9G0736 Molybdenum ND 6.29 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Nickel 30.8 2.52 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Potassium 3080 12.6 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Selenium ND 6.29 mg/kgdry 1.00 07/16/19 20:44 EPA6010D LMC B9G0736 Sodium 127 13.9 mg/kgdry 1.00 07/19/19 13:20 EPA6010D LMC B9G0912 Total Phosphorus as P 7390 629 mg/kg dry 100 07/16/19 20:24 EPA6010D LMC B9G0736 PO Box 5655 I Greenville, SC 29606 ` 426 Fairforest Way I Greenville, SC 29607 i main 864.232.1556 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 07 19 2019 16: I4 This report may not be reproduced, except in full, without H ritten permission from Rogers R Callcolt, Inc. Page 3 of 11 -- - - - - - -- - -- - Rogers & Cal[cott -- ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 General Chemistry Parameters Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B9G0771 - EPA 351.2-TKN Blank (B9G0771-BLKI) Total Kjeldahl Nitrogen ND 875 nig/kg wet LCS (B9G0771-BSI) Total Kjeldahl Nitrogen 245 879 mg/kg wet 264 93 0-200 Reference (B9G0771-SRMI) Total Kjeldahl Nitrogen 1060 33 2 mg/kg wet 1090 97 53 6-146 8 Batch B9G0852 - IC Soil Blank (B9G0852-BLKI) Nitrate as N ND 0 5 mg/kg dry Nitrite as N ND 0 1 mg/kg dry Blank (B9G0852-BLK2) Nitrate as N ND 5.0 mg/kg dry Nitrite as N ND l 0 mg/kg dry LCS (B9G0852-BSI) Nitrate as N 24 0.5 mg/kg dry 250 95 90-I10 Nitrite as N 05 0 1 mg/kg dry 0 500 99 90-I10 Duplicate (B9G0852-DUPI) Source: 9070827-01 Nitrate as N ND 25 0 mg/kg dry ND 30 Nitrite as N ND 50 mg/kg dry ND 30 Matrix Spike (B9G0852-MSI) Source: 9070827-01 Nitrate as N 902 5.0 mg/kg dry 747 ND 94 65-130 N1 g Reference (B9G0852-SRMI) Nitrate as N 197 5.0 nig/kg dry 237 83 66.2-109.8 PO Box 5655 • Greenville, SC 29606 1 426 Fairforest Way ' Greenville, SC 29607 ' main 864.232.1556 i fax 864,232.614E rogersandeallcott.com an employee -owned company 0- 19 2019 16 14 This report rrury nol be reproduced, except infull, without xr» ten pernussron from Roger, & Cullcorl, Lrc Page 4 of 11 Rogers &Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 General Chemistry Parameters Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B9G0852 - IC Soil Reference (B9G0852-SRN,l2) Nitrite as N 4 5 1 0 mg/kg dry 458 98 0-200 PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way ! Greenville, SC 29607 1 main 864.232.1556 ! fax 864.232.6140 rogersandealleott.eom an employee -owned company 0- 19 2019 16-14 This report may not be reproduced, except ur full, without a riven pernurcron fr-orn Rogers & Callcott, 1ne Page 5 of 11 Rogers & Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 Total Metals Quality Control Summary Reporting Spike Source % REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B9G0682 - EPA 7471 B Blank (B9G0682-BLKI) Mercury ND 0.00020 mg/kg wet Blank (B9G0682-BLK2) Mercury ND 0.019 mg/kg wet LCS (B9G0682-BSI) Mercury 0.0046 0.00020 mg/kg wet 0.00500 92 80-120 LCS (B9G0682-BS2) Mercury 0.49 0.020 mg/kg wet 0.497 100 80-120 Reference (B9G0682-SRMI) Mercury 13 0.040 mg/kg wet 12.5 102 60.3-140 Batch B9G0736 - EPA 3050B Blank (139430736-BLKI) Aluminum ND 0.05 mg/kg wet Arsenic ND 0.05 mg/kg wet Cadmium ND 0.02 mg/kg wet Copper ND 0.02 mg/kg wet Lead ND 0.05 mg/kg wet Magnesium ND 0.05 mg/kg wet Molybdenum ND 0.05 mg/kg wet Nickel ND 0.02 mg/kg wet Potassium ND 0.10 mg/kg wet Selenium ND 0.05 mg/kg wet Total Phosphorus as P ND 0.05 mg/kg wet LCS (1119430736-BSI) Aluminum 0.53 0.05 mg/kg wet 0.500 106 80-120 Arsenic 0.52 0.05 mg/kg wet 0.500 103 80-120 Cadmium 0.52 0.02 mg/kg wet 0.500 105 80-120 Copper 0.54 0.02 mg/kg wet 0.500 l08 80-120 Lead 0.52 0.05 mg/kg wet 0.500 104 80-120 Magnesium 0.55 0.05 mg/kg wet 0.500 111 80-120 Molybdenum 0.52 0.05 mg/kg wet 0.500 104 80-120 PO Box 5655 ' Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 s main 864.232.1556 I fax 864.232.6140 rogersandealleott.eom an employee -owned company 0- 19 2019 16:14 This report muv not be reproduced, except in full, without wrillen permission from Rogers d Cullcott, Inc. Page 6 of 11 Rogers & Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 Total Metals Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit L'nits Level Result '% REC Limits RPD Limit Flags Batch B9G0736 - EPA 3050B LCS (B9G0736-BSI) Nickel 0.51 0.02 mg/kg wet 0.500 103 80-120 Potassium 4.75 0.10 mg/kg wet 5.00 95 80-120 Selenium 0.51 0.05 mg/kg wet 0.500 103 80-120 Total Phosphorus as P 0.54 0.05 mg/kg wet 0.500 107 80-120 Reference (B9G0736-SRMI) Aluminum 9830 231 mg/kg wet 7900 124 46.71-153.2 Arsenic 166 4,62 mg/kg wet 166 100 83.13-116.9 Cadmium 124 1.85 mg/kg wet 129 96 82.17-117.1 Copper 113 1.85 nig/kg wet 110 103 83.55-116.4 Lead 194 4.62 mg/kg wet 203 96 92.27-I17.2 Magnesium 2640 231 nig/kg wet 2290 115 75.55-124.5 Molybdenum 33.7 4.62 mg/kg wet 32.4 104 78.7-121 Nickel 87.2 1.85 mg/kg wet 87.1 100 82.43-117.1 Potassium 2110 9.24 mg/kg wet 1990 106 69.35-131.2 Selenium 115 4.62 mg/kg wet 117 98 78.46-120.5 Reference (B9G0736-SRM2) Total Phosphorus as P 951 23.0 mg/kg wet 866 110 19.86-159.35 Batch B9G0912 - EPA 3050B Blank (B9G0912-BLKI) Calcium ND 0.10 mg/kg wet Sodium ND 0.10 mg/kg wet LCS (B9G0912-BSI) C.Atl`i"_ n Sc n to Qtg . n son ' t to An-I20 Sodium 0.54 0.10 mg/kg wet 0.500 109 80-120 Reference (B9G0912-SRMI) Calcium 4750 484 mg/kg wet 4720 101 81,36-118.4 Sodium 625 484 mg/kg wet 621 101 73.75-126.4 PO Box 5655 Greenville, SC 29606 ; 426 Fairforest Way I Greenville, SC 29607 ': main 864.232.1556 ! fax 864,232.6140 rogersandealleott.eom an employee -owned company 0- 19 2019 16:14 This report mqv not be reproduced, except in full, without written permission from Rogers X Callcon. Inc. Page 7 of 11 } Rogers &Cakott ,,,_._ _ ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville W WTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 Sample Preparation Data Parameter Batch Sample ID Prepared Analvst EPA 3050B Metal Digestion EPA 3050B B9G0736 9070827-01 07/16/2019 08:00 LMC EPA 3050B B9G0912 9070827-01 07/18/20 N 08:42 LMC EPA 7471B Mercury Digestion EPA 7471B B9G0682 9070827-01 07/15/2019 09:52 TLT PO Box 5655 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 i tax 864.232.6140 rogersandealleott.eom an employee -owned company 07 192019 16:14 This report muv not be reproduced, except in fill, without written permission from Rogers X Collcott, Inc. Page 8 of 11 Rogers & Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Burnsville WWTP 351 Depot St. Work Order: 9070827 Asheville, NC 28801-4310 Reported: 07/19/19 16:14 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference X Result subject to sample matrix interference. Reporting limit has been adjusted where applicable. PO Box 5655 1 Greenville, SC 29606 ; 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 ' fax 864.232.6140 rogersandcalleott.eom an employee -owned company p- 19 2019 lh:I; This report mo, not be reproduced, except in fdl, without written permissionfrom Rogers <& Callcon. Inc. Page 9 of 11 Rogers Callcott CHAIN OF CUSTODY RECORD d- EI VIRONMENTAL Mailing Po B 5655 Shipping 426 Falrforest Way 215E Stoneridge Drive Address: Gree iRe, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phon (864)232-1556 Flax (864)232-6140 Phone (803) 509-8999 Client Name Address Report To: Email Addr Telephone PO # I�— WORK ORI 4LIND C Y:Y:: 7. Possible Hazards ssoclat TIME BY: e 16 with samples: El c t IT ` o o v v G _ Project # z E SAMPLE DESCRIPTION DATE/TIME: RECEIVED BY: &11.1g 2. (f LAP DATE/TIME. RECEIVED 4. �RECEI DATE/TIME: . 6. DATE/TIME: RECEIVED BY: 8. ❑Flammable 0Skin Irritant OPolson e DATE/T ME Pq I.) DATE/TIME: DATE/TIME: Unknown ❑Other DATE/TIME: WORK ORDER 610 _ O CO Z`j Filtered (Yes/ ) Cooled(_es _o) Container Type !Kas c/G(assj Container Volume (mL) 6w Sample Typ Grab omposite) Sample Source (WW, GW, DW, SW S�7_ther. Preservation Code(s) A —None E—HCI I — ZnAcetate'' B—HNO3 F—Na2S203 1—H3PO4 C—H2SO4 G — Boric Acid K-MCAA D—NaOH H—Ascorbic Acid L- COMMENTS r?SV, IQ II ) A. I Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: Temperature of blank or representave sample At time of collection 1 '°C At time of lab receipt l °C Form Revised July, 2014 Page Paqe 10 of111 }� t ' CA fifit '..� � Sample Receipt Verification Date Client: S Received: Z . Carrier Name: Client FedHx UPS US Mail Courier Tracking Number: Receipt Criteria Y N N Shipping container / cooler intact? Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Sample M on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Samples cooled? T=p at receipt recorded on COC Temp measured with IR thermometer - SN: 97050057 Samples requiring pH preservation at proper pH? Note. Samples for metals analysis may be preserved upon receipt in the lab. Note: Samples for O&G and VOA analysis — preservation checked at bench, Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? Note: Chlorine checked at bench for samples requiring Bacterial, VOA,and HAA .,....1.m... Work Order: 0 -4 0 22-�- Field Services Other: so A Comments X X Damaged Leaking Other: Damaged Leaking Other: Ice ) Cold Packs Dry Ice None If in-house preservation used — record Lot # HCL A0th0erA_ H2SO4 HNO3 - — �vuuu�uw. Were non-conformance issues noted at sample receipt? —Yes -ter Non -Conformance issue other than noted above: Revised February 2018 Completed by: Page 11 of 11