WQ0038580_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0038580
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0038580
Applicant\Permittee * Town of Hillsborough
Facility Name * City of Hillsborough
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Hillsborough Annual Report - WQ0038580.pdf 3.82MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0038580 FACILITY NAME: Town of Hillsborough WTP
PHONE: COUNTY: Orange OPERATOR: Town of Hillsborough WTP
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
© Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar ear? Yes r❑ No ❑ —i If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPD1rS # if
applicable)
(dry tons)
Recipient Information
AAmendment/Volume
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF (sup)
0
0
133.42
133.42
Totals:
Annual (dry tons):
0
0
133.42
133.42
Amendment()used:
Bulking Agent(s) used:
tsuonb: Total Numher of Fnrm r)McnF Minnl n
* if more space is required. attach additional information sheets (FORM DMSDF
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit © Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ip If No, Explain in Narrative
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date ignature of Prep er * Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0038580 FACILITY NAME: Town of Hillsborough WTP
PHONE: COUNTY: Orange OPERATOR: Town of Hillsborough WTP
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
V Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume ( dry
tons)
Intended use(s)
August
Town of Hillsborough WTP
46.66
David Poe
46.66
Soil Amendment
September
Town of Hillsborough WTP
86.76
David Pope
86.76
Soil Amendment
Totals:
Annual (dry tons):
0
0
133.42 133.42
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESEDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - E
WQ Permit Number: WQ0038580 Laboratory:
Facility Name: Town of Hillsborough WTP
Residual Source WQ # or
NPDES #:
PWS#0368015
WWTP Name: Town of Hillsborough WTP
Residual Ana sis Data
1} Waypoint Analytical
2)
3)
4}
5)
Parameter
Limit
Sampleor . .. ite Date
I all
Selenium
'For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Deference the individual permit for metals limits,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Q,
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
- _Zo
Date
QENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0038580
Laboratory: 1)
Facility Name:
Torun of Hillsborough WTP
2)
Residual Source
PWS#0368015
3)
NPDES # or WQ#:
4)
WWTP Name:
Torun of Hillsborough WTP
5)
Re'ddlial Analvrds Data
Waypoint Analytical
Parameter
CompositeSample or Date
ff ' 111
-----_-----
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
M
*
*Preparer is defined in 40 CFR part 503.9(r) and 15A NCAC 2T . 1102 (26)
1;,-2 ;-.2-e
Hate
❑ENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Hillsborough Total Dry Tons Applied (Annual):
Permit #: WQ0038580 Cation Exchange Capacity (non 503 only):
62.71
Operator: D. Pope Owner: D. Pope Predominant Soil Series: HrB
Acres Used: 24 Acres Permitted: 24 Site #: OR02 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.61
Arsenic
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
0.335
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.335
Chromiuni
0.173
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.173
Lead
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
denum
Nickel
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Selenium
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.095
Zinc
0.747
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.747
Total
Phos-
10.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.034
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Hillsborough
D. Pope
Operator: D. Pope
WQ Permit #: WQ0038580 Field #:
Annual Dry Tons Applied: 62.71 Site #:
Predominant Soil Series: HrB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
211
Crop 2 Name:
Acres Utilized: 24
OR02 Acres Permitted: 24
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
-t
� �
*
c
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
8/20
71500
2.69
0.334
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
2.653
NA
Fescue
8/21
123500
2.69
0.577
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
4.583
NA
Fescue
8/27
71500
2.69
0.334
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
2.653
NA
Fescue
8/28
58500
2.69
0.273
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
2.171
NA
Fescue
8/29
1
58500
1 2.69
0.273
Hillsborough WTP
D
<.5"
S
0.5
0.1
1 7330
7630
185
2.171
NA
Fescue
8/30
32500
2.69
0.152
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
1 185
1.206
NA
Fescue
9/3
123500
2.69
0.577
Hillsborough WTP
D
<S"
S
0.5
0.1
7330
7630
185
4.583
NA
Fescue
9/4
19500
2.69
0.091
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
0.724
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
0
559000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
20.745
0.000
Lime Applied
Annuallbs/acre
0.083
0.010
0.335
0.173
0.074
0.001
0.025
0.086
0.095
0.747 10.034
0
0.747
2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.083
0.010
0.335
0.173
0.074
0.001
0.025
0.086
0.095
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
Permit PAN Limit 1 st/2nd Crop
1
211
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Hillsborough Total Dry Tons Applied (Annual):
Permit #: WQ0038580 Cation Exchange Capacity (non 503 only):
16.78
Operator: D. Pope Owner: D. Pope Predominant Soil Series: HrB
Acres Used: 11 Acres Permitted: 11 Site #: OR02 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.53
Arsenic
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.196
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.196
Chromiuni
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Lead
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
denum
Nickel
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Selenium
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Zinc
0.436
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.436
Total
Phos-
5.856
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.856
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/10/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Hillsborough
D. Pope
Operator: D. Pope
WQ Permit #: WQ0038580 Field #:
Annual Dry Tons Applied: 16.78 Site #:
Predominant Soil Series: HrB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
211
Crop 2 Name:
Acres Utilized: 11
OR02 Acres Permitted: 11
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
-t
� �
*
c
* �'
o'
p
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/4
149500
2.69
1.525
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
12.105
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
t49soo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
12.105
o.000
Lime Applied
Annuallbs/acre
0.048
0.006
0.196
0.101
0.043
0.000
0.015
0.050
0.055
0.436 5.856
0
0.436
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.048
0.006
0.196
0.101
0.043
0.000
0.015
0.050
0.055
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
211
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/10/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Hillsborough Total Dry Tons Applied (Annual):
Permit #: WQ0038580 Cation Exchange Capacity (non 503 only):
21.87
Operator: D. Pope Owner: D. Pope Predominant Soil Series: GeB
Acres Used: 14 Acres Permitted: 14 Site #: OR02 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.56
Arsenic
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.200
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.200
Chromiuni
0.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.103
Lead
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
denum
Nickel
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Selenium
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Zinc
0.447
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.447
Total
Phos-
5.998
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.998
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Hillsborough
D. Pope
Operator: D. Pope
WQ Permit #: WQ0038580 Field #:
Annual Dry Tons Applied: 21.87 Site #:
Predominant Soil Series: GeB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
211
Crop 2 Name:
Acres Utilized: 14
OR02 Acres Permitted: 14
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
c
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/4
58500
2.69
0.469
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
3.722
NA
Fescue
9/5
91000
2.69
0.729
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
5.789
NA
Fescue
9/9
45500
2.69
0.365
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
2.895
NA
Fescue
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
t95000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
12.406
o.000
Lime Applied
Annuallbs/acre
0.049
0.006
0.200
0.103
0.044
0.000
0.015
0.052
0.057
0.447 5.998
0
0.447
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.049
0.006
0.200
0.103
0.044
0.000
0.015
0.052
0.057
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
211
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Hillsborough Total Dry Tons Applied (Annual):
Permit #: WQ0038580 Cation Exchange Capacity (non 503 only):
17.50
Operator: D. Pope Owner: D. Pope Predominant Soil Series: GeB
Acres Used: 9 Acres Permitted: 9 Site #: OR02 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.94
Arsenic
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.249
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.249
Chromiuni
0.129
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.129
Lead
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
denum
Nickel
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
0.556
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.556
Total
Phos-
7.465
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.465
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Hillsborough
D. Pope
Operator: D. Pope
WQ Permit #: WQ0038580 Field #:
Annual Dry Tons Applied: 17.50 Site #:
Predominant Soil Series: GeB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
211
Crop 2 Name:
4 Acres Utilized: 9
OR02 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
0
0
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
4 -t
� �
*
c
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/9
65000
2.69
0.810
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
6.432
NA
Fescue
9/10
91000
2.69
1.134
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
9.005
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
ts6000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
15.438
o.000
Lime Applied
Annuallbs/acre
0.061
0.007
0.249
0.129
0.055
0.000
0.019
0.064
0.070
0.556 7.465
0
0.556
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.061
0.007
0.249
0.129
0.055
0.000
0.019
0.064
0.070
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
211
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Hillsborough Total Dry Tons Applied (Annual):
Permit #: WQ0038580 Cation Exchange Capacity (non 503 only):
14.58
Operator: D. Pope Owner: D. Pope Predominant Soil Series: HrB
Acres Used: 8 Acres Permitted: 8 Site #: OR02 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.82
Arsenic
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.234
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.234
Chromiuni
0.121
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.121
Lead
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denum
Nickel
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Selenium
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Zinc
0.521
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.521
Total
Phos-
7.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.000
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 1/11/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Hillsborough
D. Pope
Operator: D. Pope
WQ Permit #: WQ0038580 Field #:
Annual Dry Tons Applied: 14.58 Site #:
Predominant Soil Series: HrB
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
211
Crop 2 Name:
OR02
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
o
Volume applied
(enter one) Solids/
Liquid
4
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
-t
� �
*
c
* �'
o'
- ~
�. �
a•
o
TKN
mg/kg
a
o
aQ 5
� �.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/10
110500
2.69
1.549
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
12.302
NA
Fescue
9/11
19500
2.69
0.273
Hillsborough WTP
D
<.5"
S
0.5
0.1
7330
7630
185
2.171
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
o
t30000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
14.473
o.000
Lime Applied
Annuallbs/acre
0.058
0.007
0.234
0.121
0.052
0.000
0.018
0.060
0.066
0.521 7.000
0
0.521
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.058
0.007
0.234
0.121
0.052
0.000
0.018
0.060
0.066
Permitted C. P. L. R.****1
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
1
211
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/11/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
8/29/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-228-0032
Client Project Description: Hillsborough
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/16/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Hillsborough
Lab Report Number: 19-228-0032
Date: 8/27/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L450743
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 2 of 6

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Hillsborough Report Date : 08/29/2019
755 Yadkinville Road Information : Received : 08/16/2019
Mocksville , NC 27028
Report Number : 19-228-0032 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 93637
Matrix: Solids
Sample ID : Hillsborough
Sampled:
8/15/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
97.3
%
0.010
1
08/16/19 16:20
ADM
SW-DRYWT
Ammonia Nitrogen
7630
mg/Kg -
dry
926
1
08/27/19 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<185
mg/Kg -
dry
185
185
1
08/27/19 12:36
ZBD
4500NO3F-2011
Organic N
<1910
mg/Kg -
dry
1910
1
ACA
CALCULATION
pH
6.2
S.U.
1
08/22/19 07:40
JSL
9045D
Total Solids
2.69
%
0.010
0.010
1
08/16/19 16:20
ADM
2540G-2011
Total Volatile Solids
32.5
%
0.010
0.010
1
08/16/19 16:20
ADM
2540G-2011
Total Kjeldahl Nitrogen
7330
mg/Kg -
dry
1910
1
08/26/19 15:30
CLP 4500NORGD-2011
Phosphorus
1920
mg/Kg -
dry
95.2
185
1
08/22/19 20:35
BKN
6010D
Aluminum
197000
mg/Kg -
dry
75.2
185
1
08/22/19 20:35
BKN
6010D
Arsenic
15.83
mg/Kg -
dry
15.5
18.5
1
08/22/19 20:35
BKN
6010D
Cadmium
<1.83
mg/Kg -
dry
1.83
3.70
1
08/22/19 20:35
BKN
6010D
Calcium
2090
mg/Kg -
dry
622
926
1
08/23/19 20:10
BKN
6010D
Chromium
33.1
mg/Kg -
dry
7.04
9.26
1
08/22/19 20:35
BKN
6010D
Copper
64.1
mg/Kg -
dry
5.37
9.26
1
08/22/19 20:35
BKN
6010D
Iron
61100
mg/Kg -
dry
157
185
1
08/22/19 20:35
BKN
6010D
Lead
14.2
mg/Kg -
dry
5.52
11.1
1
08/22/19 20:35
BKN
6010D
Magnesium
1730
mg/Kg -
dry
82.2
185
1
08/22/19 20:35
BKN
6010D
Manganese
5630
mg/Kg -
dry
6.78
18.5
1
08/22/19 20:35
BKN
6010D
Mercury
<0.118
mg/Kg -
dry
0.118
0.533
1
08/22/19 09:00
TJS
7471A
Molybdenum
<4.81
mg/Kg -
dry
4.81
9.26
1
08/22/19 20:35
BKN
6010D
Nickel
16.5
mg/Kg -
dry
6.11
9.26
1
08/22/19 20:35
BKN
6010D
Potassium
930
mg/Kg -
dry
110
185
1
08/22/19 20:35
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 19-228-0032
Lab No : 93637
Sample ID : Hillsborough
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Hillsborough
Information :
REPORT OFANALYSIS
Report Date : 08/29/2019
Received : 08/16/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 8/15/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<18.1
mg/Kg - dry
18.1
18.5
1
08/22/19 20:35
BKN
6010D
Sodium
5963
mg/Kg - dry
286
926
1
08/22/19 20:35
BKN
6010D
Zinc
143
mg/Kg - dry
40.0
46.3
1
08/27/19 15:21
BKN
6010D
Sulfur
6630
mg/Kg - dry
181
185
1
08/22/19 20:35
BKN
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1
08/22/19 20:35
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-228-0032
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 08/16/2019 09:11:09
Page 5 of 6

Client Name/Address
Client Project Manager/Contact
Billing information
For Laboratory Use Only
E=MA Resources inc
Brent Collins
Account #45245
755 Yadklnville Rd
Mocksvdle, 127028
Project Description
Project/site Location (City/State)
BUSH -Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limit{s)
0 Fed E- UPS E]USPS
WW -Wastewater GW --Groundwater
Date Results Needed
1:1 Ccurier E] Client Drop Off
OW - Drinking Water S- Soil /Solid 0 -Oil
P - Product M • Misc
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID q
336-399-3646
[e-mail]
M
Z
W
A Cool < 10c Na25Zd3 (Micro oniy)
+���
0
B Cool r- 5C
/�
fLJ � r
aIY
'Y
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Q
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�
0
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ANALYTICAL
c
$
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CD
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E li pH,la
27St1 WE=itten iloati
Unless noted, all containers
o
-
�j
to
[tf
Q
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F HNO3 Ht2
P
G H3PO4
Memphis, TN 38133
C
z
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[phone]
per Table II of 40 CFR Part
a
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H3POa pHc2
P
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236,
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Date
Time
Sam le Identification
Required
Analysis 1 Preservative
Comments/Notes
C
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✓
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MetalsAl,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,H9,Ni,Se, Na, P,S,K,Zn
Illli I� IIII ��I� III �II I!I I III IT II 46245&-0U32
I i ill IIII 08-16-2019
E NIA Rrscvu ces irir, 0910.45
10.45
Hillsborauoh
For Laboratory Use Only
Sampled by (Name - Prmli
Ld��b� ��:;t�k
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
L
Seals
Seals
Lab
{{��
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Da/3Le Time
Received by: (SIGNATURE)
Date Time
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Relin i In by: (SIGNATURE)
Date Time
Recei d by: (SIGNATURE)
Date Time
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Date Time
VRIa y: { ATUREj
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0'?.5 s

aceAnalytical
National Center for Testing & Innovation
ANALYTICAL REPORT
August 26, 2019
EMA Resources
Sample Delivery Group: L1129947
Samples Received: 08/16/2019
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
HILLSBOROUGH L1129947-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
9
10
11
12
13
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1129947 03/26/19 16:41
PAGE:
2 of 22

HILLSBOROUGH L1129947-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
Landon Whitaker 08/15/19 08:30 08/16/19 09:00
Cp
Batch
Dilution Preparation
date/time
W G1331785
1 08/20/1914:2 0
WG1332728
1 08/21/1917:18
WG1333521
1 08/22/19 22:55
WG1332229
1 08/21/1919:18
W G1333140
1 08/23/1913:19
W G1332 965
1 08/23/1913:45
WG1333707
1 08/23/19 08:34
WG1333743
1 08/23/19 09:04
W G1332 983
1 08/22/1918:45
WG1333658
1 08/23/19 08:27
WG1334090
1 08/26/19 07:09
WG1334093
1 08/25/19 08:23
Analysis
date/time
08/20/1914:20
08/21/1917:18
08/23/1912:57
08/21/1919:18
08/23/1914:48
08/23/1913:45
08/23/1912:15
08/23/191100
08/22/1918:45
08/24/1916:00
08/26/1915:07
08/26/19 03:56
Analyst
CGD
CGD
JER
MJA
JIC
MJA
ABL
CCE
BMB
MT-1
LEL
AO
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 4 of 22

HILLSBOROUGH
Collected date/time: 08/15/19 08:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1129947
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
8/21/2019 5:18:37 PM
WG1332728
TCLP ZHE Extraction -
8/20/2019 2:20:50 PM
WG1331785
Fluid 1
8/21/2019 5:18:37 PM
WG1332728
Initial pH 7.43
8/21/2019 5:18:37 PM
WG1332728
Final pH 4.81
8/21/2019 5:18:37 PM
WG1332728
Wet Chemistry by Method 9012 B
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Cyanide ND 0.250 1 08/23/201912:57 WG1333521
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/21/201919:18 WG1332229
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.86 T8 1 08/23/201914:48 WG1333140
Sample Narrative:
L1129947-01 WG1333140: 6.86 at 23.9C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 08/23/201913:45 WG1332965
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 08/23/201912:15 WG1333707
Dilution Analysis
Batch
date / time
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
1 08/23/201911:00
WG1333743
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
1 08/22/201918:45
WG1332983
SDG:
DATE/TIME: PAGE:
L1129947
03/26/19 16:41 5 of 22

HILLSBOROUGH SAMPLE RESULTS
Collected date/time: 08/15/19 08:30 L1129947
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
08/22/201918:45
WG1332983
1,1-Dichloroethene
ND
0.0500 0.70 1
08/22/201918:45
WG1332983
2-Butanone (MEK)
ND
0.500 200 1
08/22/201918:45
WG1332983
Tetrachloroethene
ND
0.0500 0.70 1
08/22/201918:45
WG1332983
Trichloroethene
ND
0.0500 0.50 1
08/22/201918:45
WG1332983
Vinyl chloride
ND
0.0500 0.20 1
08/22/201918:45
WG1332983
(S) Toluene-dH
103
80.0-120
081221201918.45
WG1332983
(S) 4-Bromofluorobenzene
96.2
77.0-126
081221201918.45
WG1332983
(S) 1,2-Dichloroethane-d4
103
70.0-130
0812212019 18.45
WG1332983
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S)2,4-DichlorophenylAcetic Acid 81.8
Pesticides (GC) by Method 8081B
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 08/24/201916:00
WG1333658
0.00200
10
1 08/24/201916:00
WG1333658
14.0-158
081241201916.00
WG1333658
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 08/26/201915:07
WG1334090
Endrin
ND
0.00500
0.02
1 08/26/201915:07
WG1334090
Heptachlor
ND
0.00500
0.0080
1 08/26/201915:07
WG1334090
Lindane
ND
0.00500
0.40
1 08/26/201915:07
WG1334090
Methoxychlor
ND
0.00500
10
1 08/26/201915:07
WG1334090
Toxaphene
ND
0.0100
0.50
1 08/26/201915:07
WG1334090
(S) Decochlorobiphenyl
71.9
10.0-128
081261201915.07
WG1334090
(S) Tetrochloro-m-xylene
67.3
10.0-127
081261201915.07
WG1334090
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 08/26/2019 03:56
WG1334093
2,4-Dinitrotoluene
ND
0.100
0.13
1 08/26/2019 03:56
WG1334093
Hexachlorobenzene
ND
0.100
0.13
1 08/26/2019 03:56
WG1334093
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 08/26/2019 03:56
WG1334093
Hexachloroethane
ND
0.100
3
1 08/26/2019 03:56
WG1334093
Nitrobenzene
ND
0.100
2
1 08/26/2019 03:56
WG1334093
Pyridine
ND
0.100
5
1 08/26/2019 03:56
WG1334093
3&4-Methyl Phenol
ND
0.100
400
1 08/26/2019 03:56
WG1334093
2-Methylphenol
ND
0.100
200
1 08/26/2019 03:56
WG1334093
Pentachlorophenol
ND
0.100
100
1 08/26/2019 03:56
WG1334093
2,4,5-Trichlorophenol
ND
0.100
400
1 08/26/2019 03:56
WG1334093
2,4,6-Trichlorophenol
ND
0.100
2
1 08/26/2019 03:56
WG1334093
(S) 2-Fluorophenol
19.6
10.0-120
0812612019 03.56
WG1334093
(S) Phenol-d5
13.9
10.0-120
0812612019 03.56
WG1334093
(S) Nitrobenzene-d5
34.4
10.0-127
0812612019 03.56
WG1334093
(S) 2-Fluorobiphenyl
39.7
10.0-130
0812612019 03.56
WG1334093
(S) 2,4, 6-Tribromophenol
55.0
10.0-155
0812612019 03.56
WG1334093
(S) p-Terphenyl-d14
68.6
10.0-128
0812612019 03.56
WG1334093
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 6 of 22

WG1333521 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1129947-01
Method Blank (MB)
(MB) R3443599-1 03/23/1912:27
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1129818-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1129313-03 03/23/1912:32 • (DUP) R3443599-3 03/23/1912:33
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
(dry) (dry) Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide U 0.000 1 0.000 20
L1129818-33 Original Sample (OS) • Duplicate (DUP)
(OS) L1129313-33 03/23/1912:42 • (DUP) R3443599-6 03/23/1912:43
Original Result DUP Result DUP RPD
Dilution DUP RPD DUP Qualifier
(dry) (dry) Limits
Analyte mg/kg mg/kg
Reactive Cyanide 0.0849 0.0891 1 4.86 J 20
Laboratory Control Sample (LCS)
(LCS) R3443599-2 08/23/19 12:28
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.67 107
Rec. Limits LCS Qualifier
50.0-150
L1129818-32 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1129313-32 03/23/19 12:36 • (MS) R3443599-4 03/23/19 12:40 • (MSD) R3443599-5 03/23/19 12:41
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 U 0.871 0.650 52.1 38.9 1 75.0-125 J6 J3 J6 29.1 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 7 of 22

WG1333521 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B L1129947-01
L1129818-41 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129313-41 03/23/19 12:51 • (MS) R3443599-7 03/23/19 12:52 • (MSD) R3443599-3 03/23/19 12:54
Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
(dry) (dry) (dry)
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.72 0.206 1.38 1.26 68.6 61.2 1 75.0-125 J6 J6 9.66
ONE LAB. NATIONWIDE. *
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 3 of 22

WG1332229
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3442971-1 03/21/191913
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1129198-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1129947-01
(OS) L1129193-02 03/21/1919:13 • (DUP) R3442971-3 03/21/1919:13
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg _ %_
Reactive Sulfide 29.5 29.5 1 0.176 20
Laboratory Control Sample (LCS)
(LCS) R3442971-2 03/21/19 1913
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 112 112 70.0-130
ONE LAB. NATIONWIDE. *
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 9 of 22

WG1333140 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1129947-01
Laboratory Control Sample (LCS)
(LCS) R3443630-1 03/23/19 1443
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.94 99.4 99.0-101
Sample Narrative:
LCS: 9.94 at 23.1C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 10 of 22

WG1332965
Wet Chemistry by Method D93/1010A
L1129887-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1129337-01 03/23/1913:45 • (DUP) R3443639-2 03/23/1913:45
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000
L1130263-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1129947-01
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1130263-01 03/23/1913:45 • (DUP) R3443639-3 03/23/1913:45
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3443639-1 08/23/19 13:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 83.8 102 96.0-104
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 11 of 22

WG1333707 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1129947-01
Method Blank (MB)
(MB) R3443590-1 03/23/191151
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control
Sample Duplicate (LCSD)
(LCS) R3443590-2 03/23/1911:53 • (LCSD) R3443590-3 03/23/191155
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0318 0.0323
106 108 80.0-120 1.59 20
L1129911-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1129911-01 03/23/19 1157 • (MS) R3443590-4 03/23/19 12:03 • (MSD) R3443590-5 03/23/19 12:05
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0317
0.0311 106 104 1 75.0-125 1.84 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 12 of 22

WG1333743
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1129947-01
(MB) R3443547-1 03/23/1910:52
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic 0.0355
J 0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead U
0.0330
0.100
Selenium U
0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3443547-2 08/23/1910:55 • (LCSD) R3443547-3 08/23/1910:57
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.73
9.87
97.3
98.7
80.0-120
Barium
10.0
9.99
10.1
99.9
101
80.0-120
Cadmium
10.0
9.81
9.92
98.1
99.2
80.0-120
Chromium
10.0
9.65
9.84
96.5
98.4
80.0-120
Lead
10.0
9.90
10.0
99.0
100
80.0-120
Selenium
10.0
9.78
9.94
97.8
99.4
80.0-120
Silver
2.00
1.81
1.83
90.4
91.6
80.0-120
L1129947-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129947-01 03/23/19 1100 • (MS) R3443547-5 03/23/19 1106 • (MSD) R3443547-6 03/23/19 1109
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.89
9.84
98.3
97.8
Barium
10.0
ND
10.2
10.2
102
101
Cadmium
10.0
ND
9.94
9.94
99.4
99.4
Chromium
10.0
ND
9.87
9.81
98.7
98.1
Lead
10.0
ND
10.1
9.97
101
99.7
Selenium
10.0
ND
9.89
9.88
98.9
98.8
Silver
2.00
ND
1.83
1.83
91.7
91.7
ACCOUNT: PROJECT:
EMA Resources
LCS Qualifier LCSD Qualifier RPD
RPD Limits
1.46
20
1.30
20
1.12
20
1.96
20
1.09
20
1.64
20
1.32
20
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.495
20
1 75.0-125
0.263
20
1 75.0-125
0.0219
20
1 75.0-125
0.526
20
1 75.0-125
0.981
20
1 75.0-125
0.0332
20
1 75.0-125
0.0317
20
SDG:
DATE/TIME:
PAGE:
L1129947
03/26/19 16:41
13 of 22

WG1332983
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS)
by Method
8260D
L1129947-01
Method Blank (MB)
C p
(MB) R3443293-2 03/22/191134
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
z
TC
Benzene U
0.0167
0.0500
Carbon tetrachloride U
0.0167
0.0500
FS
Chlorobenzene U
0.0167
0.0500
Chloroform U
0.0833
0.250
1,2-Dichloroethane U
0.0167
0.0500
[Cn
1,1-Dichloroethene U
0.0167
0.0500
2-Butanone (MEK) U
0.167
0.500
FrTetrachloroethene
U
0.0167
0.0500
Trichloroethene U
0.0167
0.0500
Vinyl chloride U
0.0167
0.0500
(S) Toluene-d8 102
80.0-120
(S) 4-Bromofluorobenzene 100
77.0-126
F
(S) 1,2-Dichloroethane-d4 102
70.0-130
SAI
11
Laboratory Control Sample (LCS)
(LCS) R3443293-1 03/22/19 09:55
FC
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
Benzene 0.0250
0.0234
93.6
70.0-123
Carbon tetrachloride 0.0250
0.0230
91.8
68.0-126
Chlorobenzene 0.0250
0.0229
91.5
80.0-121
Chloroform 0.0250
0.0239
95.7
73.0-120
1,2-Dichloroethane 0.0250
0.0239
95.7
70.0-128
1,1-Dichloroethene 0.0250
0.0232
92.8
71.0-124
2-Butanone (MEK) 0.125
0.127
101
44.0-160
Tetrachloroethene 0.0250
0.0227
90.7
72.0-132
Trichloroethene 0.0250
0.0244
97.5
78.0-124
Vinyl chloride 0.0250
0.0221
88.4
67.0-131
(S) Toluene-d8
101
80.0-120
(S) 4-Bromofluorobenzene
98.7
77.0-126
(S) 1,2-Dichloroethane-d4
102
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
L1129947
03/26/19 16:41 14 of 22

WG1332983 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1129947-01
L1129911-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129911-03 03/22/19 18:25 • (MS) R3443293-3 03/22/19 20:44 • (MSD) R3443293-4 03/22/19 2104
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
1.25
ND
0.697
0.820
55.1
65.0
Carbon tetrachloride
1.25
ND
0.467
0.620
37.4
49.6
Chlorobenzene
1.25
ND
0.882
0.957
70.5
76.5
Chloroform
1.25
ND
0.790
0.876
63.2
70.1
1,2-Dichloroethane
1.25
ND
1.01
1.08
81.2
86.2
1,1-Dichloroethene
1.25
ND
0.369
0.503
29.5
40.3
2-Butanone (MEK)
6.25
ND
6.59
6.41
105
103
Tetrachloroethene
1.25
ND
0.574
0.723
45.9
57.8
Trichloroethene
1.25
ND
0.647
0.771
51.8
61.7
Vinyl chloride
1.25
ND
0.262
0.353
21.0
28.3
(S) Toluene-d8
104
103
(S) 4-Bromofluorobenzene
99.6
102
(S) 1,2-Dichloroethane-d4
97.5
105
ACCOUNT:
EMA Resources
PROJECT:
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
16.3
27
1 23.0-159
J3 28.2
28
1 33.0-152
8.14
27
1 29.0-154
10.3
28
1 29.0-151
6.00
27
1 11.0-160
J3 30.7
29
1 10.0-160
2.74
32
1 10.0-160
22.9
27
1 10.0-160
17.5
25
1 10.0-160
J3 29.7
27
80.0-120
77.0-126
70.0-130
SDG:
DATE/TIME:
PAGE:
L1129947
03/26/19 16:41
15 of 22

WG1333658
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1129947-01
(MB) R3444010-1 03/24/1910:02
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 62.8
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3444010-2 03/24/191017
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
2,4-D 0.0500
0.0364
72.8
50.0-120
2,4,5-TP (Silvex) 0.0500
0.0358
71.6
50.0-125
(S) Z4-Dichlorophenyl Acetic
670
14. 0-158
Acid
LCS Qualifier
L1129693-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1129693-04 03/24/19 11:46 • (MS) R3444010-3 03/24/19 12:01 • (MSD) R3444010-4 03/24/19 12:15
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0390
0.0398
78.0
79.6
1 50.0-120
2.03
20
2,4,5-TP (Silvex)
0.0500
ND
0.0395
0.0407
79.0
81.4
1 50.0-125
2.99
20
(S) Z4-Dichlorophenyl Acetic
71.2
73.0
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 16 of 22

WG1334090 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method 8081B L1129947-01
Method Blank (MB)
(MB) R3444319-2 03/26/191303
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
89.3
10.0-128
(S) Tetrochloro-m-xylene
71.7
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3444319-1 08/26/1912:50
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.0102
102
55.0-129
Endrin
0.0100
0.00944
94.4
57.0-134
Heptachlor
0.0100
0.00895
89.5
27.0-132
Methoxychlor
0.0100
0.00957
95.7
54.0-155
(S) Decachlorobiphenyl
84.7
10.0-128
(S) Tetrochloro-m-xylene
76.6
10.0-127
L1129737-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1129737-01 03/26/19 13:15 • (MS) R3444319-3 03/26/19 13:27 • (MSD) R3444319-4 03/26/19 13:40
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.0107
0.00888
107
88.8
1 14.0-141
Endrin
0.0100
ND
0.0103
0.00849
103
84.9
1 10.0-160
Heptachlor
0.0100
ND
0.00852
0.00703
85.2
70.3
1 16.0-136
Methoxychlor
0.0100
ND
0.0103
0.00841
103
84.1
1 10.0-160
(S) Decachlorobiphenyl
89.2
73.4
10.0-128
(S) Tetrochloro-m-xylene
86.3
65.7
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
18.6 40
19.3 39
19.2 40
20.2 34
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 17 of 22

WG1334093 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1129947-01
Method Blank (MB)
(MB) R3444119-1 03/25/19 23:43
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
44.1
10.0-127
(S) 2-Fluorobiphenyl
48.9
10.0-130
(S) p-Terphenyl-d14
65.0
10.0-128
(S) Phenol-d5
10.3
10.0-120
(S) 2-Fluorophenol
18.5
10.0-120
(S) Z4, 6-Tribromophenol
49.2
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3444119-2 08/26/19 00:05
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.195
39.0
18.0-120
2,4-Dinitrotoluene 0.500
0.386
77.2
49.0-124
Hexachlorobenzene 0.500
0.344
68.8
44.0-120
Hexachloro-1,3-butadiene 0.500
0.189
37.8
19.0-120
Hexachloroethane 0.500
0.167
33.4
15.0-120
Nitrobenzene 0.500
0.234
46.8
27.0-120
Pyridine 0.500
0.155
31.0
10.0-120
2-Methylphenol 0.500
0.180
36.0
28.0-120
3&4-Methyl Phenol 0.500
0.192
38.4
31.0-120
Pentachlorophenol 0.500
0.370
74.0
23.0-120
2,4,5-Trichlorophenol 0.500
0.354
70.8
44.0-120
2,4,6-Trichlorophenol 0.500
0.328
65.6
42.0-120
(S) Nitrobenzene-d5
37.4
10.0-127
(S) 2-Fluorobiphenyl
55.5
10.0-130
(S) p-Terphenyl-d14
69.5
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1129947 08/26/19 16:41 18 of 22

WG1334093 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1129947-01
Laboratory Control Sample (LCS)
(LCS) R3444119-2 08/26/19 00:05
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 12.4 10.0-120
(S) 2-Fluorophenol 19.6 10.0-120
(S) 2,4, 6-Tribromophenol 70.0 10. 0-155
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1129947 03/26/19 16:41 19 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
F
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
Rc
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
Case Narrative (Cn)
Quality Control
Summary (Qc)
Sample Chain of
Custody (Sc)
Sample Results (Sr)
Sample Summary (Ss)
Qualifier
J
J3
J6
T8
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Description
The identification ofthe analyte is acceptable, the reported value is an estimate.
The associated batch QC was outside the established quality control range for precision.
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1129947 03/26/19 16:41 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1129947 03/26/19 16:41 21 of 22

Billing Information:
Analysis
/
Container
Preservative
Chain of Custody Page _ of
EMA Resources
Mr. Brent Collins IPres
755 Yadkinville Road chk
�2ceks!ical'
8
755 Yadkinville Road
Mocksville, NC 27028
7r11n0 fmrneMvn
Mocksville, NC 27028
I
12065 Lebanon Rd Rim
Report to:
Email To: brent.collins@emaresourcesinc, com
Mr. Brent Collins
Mount luiiet, TN 37122
Phone'515-758-5858 �4�
I
�r
Fa. o 615OS$ses559 ❑11 0.
Project
City/State
Description:
Collected: I
L k
Client Project #
Lab Project #
Phone : [phone]
B 50
Fax: [phone]
-
Ac ril EMARES
Collected by (print),
Site/Facility ID #
P O a
o
1f1
Z
U
Template:711413
Collected by (signature):
hush? (Lab MUST Be Notified) Quote #
O
PrelDgin: P689629
Same Day Five Day
Z,
Next Day 5 Day (Rad Onlv) Date Results Needed
TSR: 702 - Cassandra Foster
Immediately
_
—TwoDay _ 10 Day Only) No.
�
w
+'
PB:
Packed on Ice N Y ✓
Ta y of
J
.-4
Shipped Via: FedEX Ground
Sample ID
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
d
U
Remarks
Sar,piea{iabo++iyl
ix
X
H
X
SS
r
fl�/'S�!°J
'Er.`.3ool
2
I
- — - _.... _....... ... . .
x Sample Recein-„.1€cklys.
Matrix: Remarks: ✓
SS -Soil AIR - Air F- Filter pH Temp CGG Seal Present/Intact: _NP _Y N
CGC Signed/Accurate: ./f N
GW- Groundwater 8-Bloassay Bottles arrive intact: :/7r �N
WW - WasteWater Flow Other Correct bottles used: t/s _r
DW- Grinkin ateff Samples returned via: Sufficient volume sent: TX_N
OT-Other 5(Ud9-e_, _UPS _Fed Ex _Courier Tracking# If Applicable
VOA Zero Headspace: Y _N
r q sFi y. Date:Time: Received by: (signature) Trip Blank Received: Ye / No Preservation Correct/Checked:_N
p►_Y
eoH RAD SORES: Cli.5 r
Tl'iR
Re uish by : (Signatur
pate:
Time:
Received by: (SignabJrei
Temp: ,r��c Bottles Received:
f preservation required by Login, Date/Time
Relinquished by : (Signature)
Date:
Time:
ftel:eiv d for lab y: (Signal
Date: Time]
Hold:
Calo�'?
NCI , t361

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Hillsborough WQ Permit Number:
WWTP Name: Town of Hillsborough WTP PWS Number:
Monitoring Period: From
I/112019 To 12/31/2019
WQ0038580
360915
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timeltemp) ❑
Alt B (Alk Treatment)❑
T Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑ 1
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Patba ens":
Com ost ❑
Heat Drying ❑
Heat Treattnent ❑
Thermophilic ❑
Beta Rav IT
Gamma Ray ❑
Pasteurization ❑
Class B:
All. (1) Fecal Density El
Alt. (2) Process to Significantly Deduce Pathogens []
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying [3 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number ot
Excee-
es
Frequency
of Analysis
Y
Sample
yp
Type
Analytical
Tech-ni ue
4
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
62
70
80
MPNIg
0
Annually
Grab
SM922ICE
CFCI
1000 mpn per gram
of total so] id (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Aft. 2 (40-day bench) ❑
jAlt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
jAlt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
INo vector attraction reduction alternatives were performed 21
CERTIFICATION STATEMENT (please check the appropriate statement)
21 " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met."' (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.]
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Howard Hobson - Water Plant ORC Brent Collins - Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
C-� �— / :x� .c 1/11/2020
Signs o Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l IO2 (26)
❑ENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
08/22/2019
Reported:
08/23/2019
For:
Hillsborough
Comments:
Geometric Mean <70 MPN/g
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190822-16-01
Fecal Coliforms
1
<67
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-01
Percent Solids
1
3.00
%
SM2540B-2011
08/22/2019
WC
190822-16-02
Fecal Coliforms
2
<62
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-02
Percent Solids
2
3.22
%
SM2540B-2011
08/22/2019
WC
190822-16-03
Fecal Coliforms
3
<69
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-03
Percent Solids
3
2.88
%
SM2540B-2011
08/22/2019
WC
190822-16-04
Fecal Coliforms
4
<75
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-04
Percent Solids
4
2.67
%
SM2540B-2011
08/22/2019
WC
190822-16-05
Fecal Coliforms
5
<69
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-05
Percent Solids
5
2.88
%
SM2540B-2011
08/22/2019
WC
190822-16-06
Fecal Coliforms
6
<80
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-06
Percent Solids
6
2.50
%
SM2540B-2011
08/22/2019
WC
190822-16-07
Fecal Coliforms
7
<71
MPN/g
SM92210E-2006
08/22/2019
WC
190822-16-07
Percent Solids
7
2.80
%
SM2540B-2011
08/22/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 190822-16-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-02 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-03 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-04 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-05 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-06 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 190822-16-07 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

Client: �JA -�
STATFSVILLE ANALYTICAL
Address: 1
XV.
122 Court Street • P.O. Box 228
/el( Ct Y:1�G--
Statesville, NC 28687
[phone]
��//
JYi.Mayrtly - 2702r
Contact Person: �r #
Phone # FAX#
Chain of
PO #
Requisitioned by: (Time
Date)
Custody Record
Customer
Sample to#
Lab -ID#
Time Sampled
(Grab Only)
Dateamp Sled
(Grab Only)
a
@
Matrix
mdv w ww
Parameters requested for analysis
7. mso.,,
Va.:/"7
?�
X
qca I 'A-
2-
3
s
Qri
(o00L
7
0
V
Relinquished by:
Time 9'�f7 > pm Date r/ 22119
Sampled by: /3�[
Received by:
Timeqa , pm Date/4 lq
Transported'by:
Relinquished by:
Time am, pm Date /�/
Holding times met: V-1,
Received by:
Time am, pm Date
_/_J_
Compliance work: t/
Composite Sampling #1:
Time begin am, prn Date /
/_
Non-compliance work:
Time end am, pm Date _/_/
lab Comments:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date
r,
00
t9
00
eV
U
Z
N
N
4-
Ln
00
tV
CV
X
0
m
0
a-

Page 1 of 1
Report Number: 19-255-0518
Account Number:46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
•
Waypoint,,
ANALYTICAL
"Every acre... Every year. "rM
SOIL ANALYSIS REPORT
Date Received: 09/12/2019 Date Of Analysis: 09/13/2019 Date Of Report: 09/16/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: David Pope
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
INC = North Carolina Fertility Index Value
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
1
10662
7.0
VH
150
321 VH
INC = 267
67 L
INC = 34
278 VH
819 L
10
VL
5.5
6.70
2.3
8.9
MIN
2
10663
5.5
H
148
258 VH
INC = 215
42 VL
INC = 21
319 VH
898 M
11
VL
6.2
1.0
8.3
MIN
3
10664
5.1
H
139
319 VH
INC = 266
28 VL
NC = 14
298 VH
919 M
10
VL
5.8
6.76
1.7
8.9
MIN
4
10666
5.1
H
141
173 VH
INC = 144
27 VL
INC = 14
286 VH
859 M
10
VL
6.1
6.82
1.1
7.9
MIN
5
10667
6.3
H
150
173 VH
INC = 144
35 VL
INC = 18
286 VH
891 M
10
VL
5.8
6.77
1.6
8.6
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NO3 N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm
Rate
SS
ms/cm Rate
1
1.9
26.0
46.0
0.5
25.8
17 M
INC =35
44.9 VH
INC =1122.5
28 H
INC =175
266 VH
3.1 VH
INC =155.0
0.4
L
0.16
VL
2
1.3
32.0
54.1
0.6
12.0
12 L
INC =25
37.7 VH
INC =942.5
48 H
NC=300
147 VH
3.2 VH
INC =160.0
0.4
L
0.13
VL
3
0.8
27.9
51.6
0.5
19.1
15 L
INC =31
49.3 VH
INC =1232.5
27 H
INC=169
170 VH
4.5 VH
INC =225.0
0.4
L
0.17
VL
4
0.9
30.2
54.4
0.6
13.9
10 L
INC =21
24.2 VH
INC =605.0
32 H
NC=200
122 VH
2.8 H
INC =140.0
0.4
L
0.14
VL
5
1.0
27.7
51.8
0.5
18.6
12 L
NC=25
30.2 VH
NC=755.0
31 H
NC=194
180 VH
3.1 VH
NC=155.0
0.4
L
0.16
VL
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �Aylic m� %�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary