WQ0010583_Residual Annual Report 2019_20200224

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/24/2020
Received:*
Project Number* WQ0010583
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0010583
Applicant\Permittee * Davie County Water System
Facility Name * Davie County Water System
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Davie County Water System Annual Report -
10.39MB
WQ0010583. pdf
upload only 1 RDF docurrent. Nlaltiple docurrents rust be corrbined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0010583
Facility Name (as shown on permit):
Land Application Operator:
County:
Davie
Year: 2019
Davie County Water System
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes © No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in thepermit-.[
19
Total number of fields utilized for land application during the year:
6
Total amount of dry tons applied during the year for all application sites:
442.31
Total number of acres utilizes for land application during the year:
99.2
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1 t 05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. I I l I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false i formation, including the possibility
of fines and imprisonment for knowing violations."
Johnny Lambert - Utilities Director 0, _17- Zo z cl
Permittee Name and Title (type or print) fg7niokiof Permittee Date
l [ • a 7 ��a �a 1/3/2020
Signature of Pre+rer,4* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T
Signature of Land Applier Date
(if different from Permittee and Preparer)
.1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010583 Laboratory: 1)
Facility blame: Davie County Water Systems 2)
Residual Source WQ # or NCO024872 3)
NPDES #: 4)
WWTP Name: Cooleemee W WTP 5)
Dari:A1 Anolcrcic Nita
Parameter
(mg/kg)
Conc.
Limit
m � a
Sam le or Composite Date
4/9119
4/17/19
4/24/19
5/6/19
Average
Percent Solids {%)
NA
6.5
7.1
4.99
7.22
6.45
Arsenic
75
10.3
8.03
9.38
5.82
8.38
Cadmium
85
2.43
1.12
1.47
1.14
1.54
Copper
4,300
322
286
368
210
296.5
Chromium
NA
61.1
61.8
65
41.1
57.25
Lead
840
70.6
62.3
60.2
35.1
57.05
Mercury
57
0.826
0.849
1.42
1.19
1.07
Molybdenum
75
4.17
5.58
5.86
3.42
4.76
Nickel
420
31.4
29
32.2
21.3
28.5
Selenium
100
7.54
6.9
9.8
6.81
7.76
Zinc
7,500
1200
1080
1340
818
1109.5
Total Phosphorus
NA
12700
10800
13600
8500
11400
TKN
NA
26600
22500
30800
26500
26600
Ammonia -Nitrogen
NA
8760
5010
6660
11000
7857.5
Nitrate and Nitrite
NA
569
102
196
66.9
233.5
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false_ information, including the possibility of fines and imprisonment for knowing violations."
Signature of Pre*er
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T J t02 (26)
-a-v4-0
Date
DENR FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010583
Facility Name: Davie County Water Systems
Residual Source
NPDES # or WQ#:
WWTP Name:
R,—irlvial Annivcic nnta
NCO024872
Cooleemee WWTP
Laboratory: 1) 0
2)
3)
4)
5)
Parameter
(mg/kg)
Sam le or Com osite Date
419/19
4117/19
4/24/19
5/6/19
Average
Aluminum
52800
42800
44600
28500
42175
Calcium
8880
7730
10500
6680
8447.5
Magnesium
3170
2720
2960
2000
2712.5
pH
6.7
6.9
6.8
6.9
6.825
Potassium
2200
2110
2060
1460
1957.5
Sodium
1330
1100
1590
1130
1287.5
PAN
10301
7854
10768
10217
9784.98
SAR
0.78
0.73
0.79
0.83
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prep�rer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series:
Acres Used: 18 Acres Permitted: 18 Site #: NC-DVO08 Field #:
101.39
CeB2
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
5.63
Arsenic
0.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Cadmium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Copper
3.346
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.346
Chromiuni
0.645
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.645
Lead
0.643
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.643
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
denum
Nickel
0.321
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.321
Selenium
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
Zinc
12.505
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.505
Total
Phos-
128.432
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
128.432
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Roger Spillman
Operator: Roger Spillman
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 101.39 Site #:
Predominant Soil Series: Ce132
Crop 1 Name: Fescue - Hay Crop 1 Max. PAN:
209 Crop 2 Name:
4
NC-DVO08
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
18
18
o
QLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
�e '
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
c
?.
* �'
p
o
TKN
mg/kg
Z a
o
ac o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/17/19
149500
6.45
2.234
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
43.716
NA
Fescue
4/18/19
26000
6.45
0.389
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
7.603
NA
Fescue
4/26/19
32500
6.45
0.486
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
9.503
NA
Fescue
4/29/19
97500
6.45
1.457
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
28.510
NA
Fescue
4/30/19
1
71500
6.45
1.068
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
20.908
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
377000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
110.2401
0.000
Lime Applied
Annuallbs/acre
0.094
0.017
3.346
0.645
0.643
0.012
0.054
0.321
0.087
12.505
128.432
Date
lbs/ac
Prior Years Cumulative lbs/ac
5.1
1
105
0
41.5
0.0423
2.5
11.8
5
320
Current Cumulative lbs/ac
5.194
1.017
108.346
0.645
42.143
0.054
2.554
12.121
5.087
332.505
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
F 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series:
Acres Used: 18 Acres Permitted: 18 Site #: NC-DVO08 Field #:
94.41
M rC2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WINE
Com-
posite
Date
NEWEEMEM
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
5.25
Arsenic
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Cadmium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
3.116
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.116
Chromiuni
0.601
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.601
Lead
0.598
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.598
Mercury
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Molyb-
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
denum
Nickel
0.299
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.299
Selenium
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Zinc
11.644
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.644
Total
Phos-
119.586
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
119.586
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Roger Spillman
Operator: Roger Spillman
Crop 1 Name: Sudex
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 94.41 Site #:
Predominant Soil Series: MrC2
Crop 1 Max. PAN:
186
Crop 2 Name:
NC-DVO08
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
18
18
o
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
(Dry,
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
*
c
?.
* �'
�
p
o
TKN
mg/kg
Z a
o I
ac o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/2/19
6500
6.45
0.097
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
1.901
NA
Sudex
5/3/19
117000
6.45
1.748
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
34.212
NA
Sudex
5/7/19
227500
6.45
3.399
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
66.524
NA
Sudex
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
351000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
102.6371
0.000
Lime Applied
Annuallbs/acre
0.088
0.016
3.116
0.601
0.598
0.011
0.050
0.299
0.081
11.644
119.586
Date
lbs/ac
Prior Years Cumulative lbs/ac
1.4
1
105
0
41.5
0.0423
2.5
11.8
5
320
Current Cumulative lbs/ac
1.488
1.016
108.116
0.601
42.098
0.054
2.550
12.099
5.081
331.644
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 186
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series:
Acres Used: 20 Acres Permitted: 20 Site #: NC-DVO08 Field #:
108.40
M rB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
5.42
Arsenic
0.091
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Cadmium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Copper
3.219
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.219
Chromiuni
0.621
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.621
Lead
0.618
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.618
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
denum
Nickel
0.309
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.309
Selenium
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.084
Zinc
12.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.032
Total
Phos-
123.576
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
123.576
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Roger Spillman
Operator: Roger Spillman
Crop 1 Name: Sudex
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 108.40 Site #:
Predominant Soil Series: Mr132
Crop 1 Max. PAN:
221 Crop 2 Name:
6
NC-DVO08
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
20
20
o
QLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
�e '
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
c
?.
* �'
p
o
TKN
mg/kg
Z a
o
ac o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/30/19
71500
6.45
0.962
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
18.817
NA
Sudex
5/1/19
130000
6.45
1.748
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
34.212
NA
Sudex
5/2/19
110500
6.45
1.486
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
29.080
NA
Sudex
5/9/19
91000
6.45
1.224
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
23.949
NA
Sudex
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
403000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
106.0581
0.000
Lime Applied
Annuallbs/acre
0.091
0.017
3.219
0.621
0.618
0.012
0.052
0.309
0.084
12.032
123.576
Date
lbs/ac
Prior Years Cumulative lbs/ac
5.1
1
105
0
41.5
0.0423
2.5
11.8
5
320
Current Cumulative lbs/ac
5.191
1.017
108.219
0.621
42.118
0.054
2.552
12.109
5.084
332.032
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
F 221
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series:
Acres Used: 18.2 Acres Permitted: 18.2 Site #: NC-DVO08 Field #:
47.21
M rB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.59
Arsenic
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.541
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.541
Chromiuni
0.297
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.297
Lead
0.296
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.296
Mercury
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
denum
Nickel
0.148
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.148
Selenium
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Zinc
5.759
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.759
Total
Phos-
59.143
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
59.143
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Roger Spillman
Operator: Roger Spillman
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 47.21 Site #:
Predominant Soil Series: Mr132
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
188
Crop 2 Name:
NC-DVO08
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
18.2
18.2
o
Qac
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
�e '
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
c
?.
* �'
o
TKN
mg/kg
Z a
o o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/18/19
169000
6.45
2.498
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
48.875
NA
Fescue
4/22/19
6500
6.45
0.096
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
1.880
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
175500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
50.755
0.000
Lime Applied
Annuallbs/acre
0.043
0.008
1.541
0.297
0.296
0.006
0.025
0.148
0.040
5.759
59.143
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.419
0.173
16.654
4.708
3.914
0.087
0.662
2.214
0.432
66.771
Current Cumulative lbs/ac
0.462
0.181
18.195
5.005
4.210
0.093
0.687
2.362
0.472
72.530
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
41.95
Operator: Herbert Dooley Owner: Herbert Dooley Predominant Soil Series: CfB2
Acres Used: 16 Acres Permitted: 16 Site #: NC-DV12 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.62
Arsenic
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.557
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.557
Chromiuni
0.300
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.300
Lead
0.299
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.299
Mercury
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
denum
Nickel
0.149
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.149
Selenium
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Zinc
5.821
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.821
Total
Phos-
59.782
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
59.782
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Herbert Dooley
Operator: Herbert Dooley
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 41.95 Site #:
Predominant Soil Series: CfB2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
209
Crop 2 Name:
NC -DV 12
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
16
16
o
Qac
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
�e '
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
c
?.
* �'
o
TKN
mg/kg
Z a
o o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/24/19
123500
6.45
2.076
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
40.627
NA
Fescue
4/26/19
32500
6.45
0.546
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
10.691
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
156000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
51.318
0.000
Lime Applied
Annuallbs/acre
0.044
0.008
1.557
0.300
0.299
0.006
0.025
0.149
0.041
5.821
59.782
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.015
0.009
3.343
0.068
0.126
0.001
0.017
0.047
0.017
0.7
6/25/19
2000
Current Cumulative lbs/ac
0.059
0.017
4.900
0.368
0.425
0.007
0.042
0.196
0.058
6.521
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual):
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
48.95
Operator: Herbert Dooley Owner: Herbert Dooley Predominant Soil Series: FeC2
Acres Used: 9 Acres Permitted: 9 Site #: NC -DV 12 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phoms
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
5.44
Arsenic
0.091
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Cadmium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Copper
3.231
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.231
Chromiuni
0.623
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.623
Lead
0.621
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.621
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
denum
Nickel
0.310
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.310
Selenium
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.084
Zinc
12.075
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.075
Total
Phos-
124.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
124.009
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
1/3/2020
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System
Land Owner: Herbert Dooley
Operator: Herbert Dooley
WQ Permit #: WQ0010583 Field #:
Annual Dry Tons Applied: 48.95 Site #:
Predominant Soil Series: FeC2
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN:
158 Crop 2 Name:
2
NC -DV 12
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
o
Qac
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
coo
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Co it
�e '
Moist)
Precip.
Past 24
Hrs.
inches
�
0 w
c
?.
* �'
o
TKN
mg/kg
Z a
o o
5.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/23/19
65000
6.45
1.943
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
38.014
NA
Fescue
4/25/19
117000
6.45
3.497
Davie County
Dry
<.5"
S
0.5
0.3
26600
7858
233
68.425
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
o
ia2000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
106.438
0.000
Lime Applied
Annuallbs/acre
0.091
0.017
3.231
0.623
0.621
0.012
0.052
0.310
0.084
12.075
124.009
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.063
0.039
13.97
0.282
0.525
0.006
0.073
0.198
0.073
2.925
Current Cumulative lbs/ac
0.154
0.056
17.201
0.905
1.146
0.018
0.125
0.508
0.157
15.000
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 158
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/3/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypoint
ANALYTICAL
4/17/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-100-0216
Client Project Description: Analytical Testing
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/10/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
. L +� i vxu
CL
Page 1 of 5

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
Brent Collins Project Analytical Testing Report Date : 04/17/2019
755 Yadkinville Rd Information : Received : 04/10/2019
Mocksville , NC 27028
Report Number : 19-100-0216 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 95123
Matrix: Solids
Sample ID : Davie County - Cooleemee
Sampled:
4/9/2019
8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
93.5
%
0.010
1
04/12/19 12:34
CJR
SW-DRYWT
Ammonia Nitrogen
0.876
% - dry
0.030
0.153
1
04/16/19 16:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
569
mg/Kg -
dry
73.5
73.5
1
04/15/19 12:55
ZBD
4500NO3F-2011
pH
6.7
S.U.
1
04/16/19 07:31
JSL
9045D
Total Solids
6.50
%
0.010
0.010
1
04/12/19 12:34
CJR
2540G-2011
Total Volatile Solids
70.6
%
0.010
0.010
1
04/12/19 12:34
CJR
2540G-2011
Total Kjeldahl Nitrogen
2.66
% - dry
0.015
0.384
1
04/17/19 09:00
CLP
4500NH3C-2011
Phosphorus
12700
mg/Kg -
dry
39.5
76.9
1
04/15/19 19:46
BKN
6010D
Aluminum
52800
mg/Kg -
dry
31.2
76.9
1
04/17/19 15:03
BKN
6010D
Arsenic
10.3
mg/Kg -
dry
6.45
7.69
1
04/15/19 19:46
BKN
6010D
Cadmium
2.43
mg/Kg -
dry
0.762
1.54
1
04/15/19 19:46
BKN
6010D
Calcium
8880
mg/Kg -
dry
258
385
1
04/15/19 19:46
BKN
6010D
Chromium
61.1
mg/Kg -
dry
2.92
3.85
1
04/15/19 19:46
BKN
6010D
Copper
322
mg/Kg -
dry
2.23
3.85
1
04/15/19 19:46
BKN
6010D
Iron
110000
mg/Kg -
dry
65.2
76.9
1
04/15/19 19:46
BKN
6010D
Lead
70.6
mg/Kg -
dry
2.29
4.62
1
04/15/19 19:46
BKN
6010D
Magnesium
3170
mg/Kg -
dry
34.2
76.9
1
04/15/19 19:46
BKN
6010D
Manganese
1060
mg/Kg -
dry
2.82
7.69
1
04/15/19 19:46
BKN
6010D
Mercury
0.826
mg/Kg -
dry
0.0514
0.232
1
04/16/19 13:01
KKM
7471A
Molybdenum
4.17
mg/Kg -
dry
2.00
3.85
1
04/15/19 19:46
BKN
6010D
Nickel
31.4
mg/Kg -
dry
2.54
3.85
1
04/15/19 19:46
BKN
6010D
Potassium
2200
mg/Kg -
dry
45.8
76.9
1
04/15/19 19:46
BKN
6010D
Selenium
<7.54
mg/Kg -
dry
7.54
7.69
1
04/15/19 19:46
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 2 of 5

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-100-0216
Lab No : 95123
Sample ID : Davie County - Cooleemee
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Analytical Testing
Information :
REPORT OFANALYSIS
Report Date : 04/17/2019
Received : 04/10/2019
Qa"
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/9/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Sodium
1330
mg/Kg - dry
119
385
1
04/15/19 19:46
BKN
6010D
Zinc
1200
mg/Kg - dry
16.6
19.2
1
04/15/19 19:46
BKN
6010D
Sulfur
6110
mg/Kg - dry
75.2
76.9
1
04/15/19 19:46
BKN
6010D
Organic N
1.78
% - dry
0.030
0.153
1
04/16/19 16:00
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 5

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-100-0216
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 04/10/2019 13:21:08
Page 4 of 5

Client Name/Address
Client Project Manager/Contact
Billing Information
EMA Resources Inc
Brent Collins
Account #46245
For Laboratory Use Only
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
H RUSH —Additional charges apply
Method of Shi ment
Matrix Key
Special Detection Limit(s)
Fed Ex [5uPS EjuSPS
WW —Wastewater GW —Groundwater
Date Results Needed
Courier Client Drop Off
DW — Drinking Water S— Soil /Solid O— Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
[e-mail]
M
Z
(n
A Cool < 10C Na25203 (Micro Only)
Waypoint
:
-
0
E
a Cool <= 6C
ANALYTICAL
Y
o
p
O
CD
E
vt
,/0
C H2SO4 pH<2
D None Required
2790 Whitten Road
°
u
a
0
u
!n
E
O
vJ
I_
u)
t'
L U
E NaOH pH>10
Memphis, TN 38133
Unless noted, all containers
°
W
0
(t7
z
z
@
M
\
U
� HCL 3H z<2
[phone]
per Table II of 40 CFR Part
135.
a
Z
x
;�
4l
(---
Z
O
^
LL
/
H H3PO4 P H<Z
I Cool <= 6C NA25203
Date
Time
Required
Analysis / Preservative
Comments/Notes
4l9
8.3
Sample Identification
�
ewnce
I
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,MO,Hg,Ni,Se,Na,P,S,K,Zn
IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII IIIIIIIIIIIIIIIIIIIIIIIIN 46 o° 0196
EMA Resources Inc 132050
Analvtical Testino
For
Laboratory Use Only
Sampled by (Name — Print)
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
/ N
Custody
Seals
Lab Comments
Relinq
Date Time
t/9 )C.)" '
—
Receive by: IGNATURE)
Date Time
y/9 /0;3ooM
v
f__ *'�
Blank Cooler Tern
Relin ed by: (SIGNAT RE)
Dajse Time
Received by: (SIGNATURE)
Date Time
y/9 3.-09o„.,
Relinquished by: (SIGNATURE)
Date Time
Receiv by: (SIGNATURE)
D t Time
v lc

Waypoint
ANALYTICAL
4/26/2019
EMA Resources Inc
755 Yadkinville Road
Mocksville, NC, 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Lab Report Number: 19-108-0265
Client Project Description: Analytical Testing
Davie County/ NC
Waypoint Analytical, LLC. received sample(s) on 4/18/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
. L +� i vxu
CL
Page 1 of 6

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Analytical Testing
Lab Report Number: 19-108-0265
Date: 4/25/2019
Metals Analysis Method 6010D
Sample 89683 (Cooleemee)
Analyte: Aluminum
QC Batch No: 1-432092/1-431893
MS/MSD Recovery failed, DT confirmed matrix interference
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Analyte: Potassium
QC Batch No: 1-432092/1-431893
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 2 of 6

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
755 Yadkinville Road Project Analytical Testing Report Date : 04/26/2019
Information : Davie County/ NC Received : 04/18/2019
Mocksville , NC 27028
Report Number : 19-108-0265 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 89683
Matrix: Solids
Sample ID : Cooleemee
Sampled:
4/17/2019
11:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
92.9
%
0.010
1
04/22/19 16:32
ADM
SW-DRYWT
Ammonia Nitrogen
5010
mg/Kg -
dry
352
1
04/24/19 11:15
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
102
mg/Kg -
dry
68.9
68.9
1
04/24/19 14:25
ZBD
4500NO3F-2011
Organic N
17500
mg/Kg -
dry
704
1
ACA
CALCULATION -
pH
6.9
S.U.
1
04/24/19 06:53
JSL
9045D
Total Solids
7.10
%
0.010
0.010
1
04/22/19 16:32
ADM
2540G-2011
Total Volatile Solids
38.1
%
0.010
0.010
1
04/22/19 16:32
ADM
2540G-2011
Total Kjeldahl Nitrogen
22500
mg/Kg -
dry
704
704
1
04/24/19 09:30
JPJ
4500NH3C-2011
Phosphorus
10800
mg/Kg -
dry
36.2
70.4
1
04/19/19 19:34
BKN
6010D
Aluminum
42800
mg/Kg -
dry
28.6
70.4
1
04/19/19 19:34
BKN
6010D
Arsenic
8.03
mg/Kg -
dry
5.90
7.04
1
04/19/19 19:34
BKN
6010D
Cadmium
1.123
mg/Kg -
dry
0.697
1.41
1
04/19/19 19:34
BKN
6010D
Calcium
7730
mg/Kg -
dry
237
352
1
04/19/19 19:34
BKN
6010D
Chromium
61.8
mg/Kg -
dry
2.68
3.52
1
04/19/19 19:34
BKN
6010D
Copper
286
mg/Kg -
dry
2.04
3.52
1
04/19/19 19:34
BKN
6010D
Iron
95100
mg/Kg -
dry
59.7
70.4
1
04/19/19 19:34
BKN
6010D
Lead
62.3
mg/Kg -
dry
2.10
4.23
1
04/19/19 19:34
BKN
6010D
Magnesium
2720
mg/Kg -
dry
31.3
70.4
1
04/19/19 19:34
BKN
6010D
Manganese
958
mg/Kg -
dry
2.58
7.04
1
04/19/19 19:34
BKN
6010D
Mercury
0.849
mg/Kg -
dry
0.0449
0.204
1
04/19/19 14:45
TJS
7471A
Molybdenum
5.58
mg/Kg -
dry
1.83
3.52
1
04/19/19 19:34
BKN
6010D
Nickel
29.0
mg/Kg -
dry
2.32
3.52
1
04/19/19 19:34
BKN
6010D
Potassium
2110
mg/Kg -
dry
42.0
70.4
1
04/19/19 19:34
BKN
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 3 of 6

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 19-108-0265
Lab No : 89683
Sample ID : Cooleemee
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Analytical Testing
Information : Davie County/ NC
REPORT OFANALYSIS
Report Date : 04/26/2019
Received : 04/18/2019
Q0"
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/17/2019 11:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<6.90
mg/Kg -
dry
6.90
7.04
1
04/19/19 19:34
BKN
6010D
Sodium
1100
mg/Kg -
dry
109
352
1
04/19/19 19:34
BKN
6010D
Zinc
1080
mg/Kg -
dry
15.2
17.6
1
04/19/19 19:34
BKN
6010D
Sulfur
5010
mg/Kg -
dry
68.9
70.4
1
04/19/19 19:34
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 4 of 6

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-108-0265
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ISovanchampa Yos Date & Time: 04/18/2019 12:13:07
Page 5 of 6

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH — Additional charges apply
Me[ d of Shipment
Matrix Key
jv; e- l /� o"47 /N L
��1R
Special Detection Limit(s)
Date Results Needed
Fed Ex UPS �USPS
rier El Client Drop Off
WW —Wastewater GW —Groundwater
DW — Drinking Water S —Soil /Solid 0 — Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone p
Project Manager Email
Purchase Order Number
Site/Facility ID Ji
336-399-3646
[e-mail]
0
M
z
in
A Cool < 10C Na2S203 (Micro Only)
O
�
B Cool a 6C
Waypoint
c
.q
a+
Y
0
O
o
C
C
M
C H2504pH<2
D None Required
ANALYTICAL
o
S
o
E
°1
(n
�//��
W
E NaOH pH>10
2790 Whitten Road
Unless noted, all containers
_
°
w
N
ea
Q
_
ca
T
V J
\
U
F HNO3 pH<2
G HCL pH<2
Memphis, TN 38133
S
Z
/�
[phone]
per Table II of 40 CFR Part
E
x
Q
U
H H3Po4 pH<2
I
136.
�
Z
A
`
Z
10
Cool — 6C NA25203
Date
Time
Sample Identification
Required
Analysis / Preservative
Comments/Notes
y117
II:Door►
('ooI ee,-ne e-
I
\
C_
XX
X
X
Meta Is:AI,As,Ca, Cd,Cr,Cu,Fe, Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
11111111111 11111 Jill 11111111146245
04 -820196
EMA Resources Inc 12 08 08
Analytical Testing
For Laboratory Use Only
Sampled by (Name — Print)
ji>'n-� ts
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Lab Comments
Y J N
J
Relinq fished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Y(,,,
ylll 3�«>pH
Blank/Coo r Te p
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
ff o L'
Relinquished by: (SIGNATURE)
Date Time
Receive�IGpI URE)
Date Time
l � r
�J

Waypoint
ANALYTICAL
4/30/2019
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-115-0250
Client Project Description: Analytical Testing
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/25/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
. L +� i vxu
CL
Page 1 of 5

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
Brent Collins Project Analytical Testing Report Date : 04/30/2019
755 Yadkinville Rd Information : Received : 04/25/2019
Mocksville , NC 27028
Report Number : 19-115-0250 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 91672
Matrix: Solids
Sample ID : Cooleemee
Sampled:
4/24/2019
9:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
95.0
%
0.010
1
04/25/19 16:30
ADM
SW-DRYWT
Ammonia Nitrogen
6660
mg/Kg -
dry
500
1
04/26/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
196
mg/Kg -
dry
87.8
87.8
1
04/26/19 12:06
ZBD
4500NO3F-2011
Organic N
24200
mg/Kg -
dry
20.0
1000
1
04/26/19 15:00
CALCULATION -
pH
6.8
S.U.
1
04/26/19 07:01
JSL
9045D
Total Solids
4.99
%
0.010
0.010
1
04/25/19 16:30
ADM
2540G-2011
Total Volatile Solids
43.2
%
0.010
0.010
1
04/25/19 16:30
ADM
2540G-2011
Total Kjeldahl Nitrogen
30800
mg/Kg -
dry
1000
1
04/26/19 16:28
CLP 4500NORGD-2011
Phosphorus
13600
mg/Kg -
dry
51.4
100
1
04/27/19 20:46
KKM
6010D
Aluminum
44600
mg/Kg -
dry
40.6
100
1
04/28/19 19:19
KKM
6010D
Arsenic
9.383
mg/Kg -
dry
8.38
10.0
1
04/27/19 20:46
KKM
6010D
Cadmium
1.473
mg/Kg -
dry
0.990
2.00
1
04/27/19 20:46
KKM
6010D
Calcium
10500
mg/Kg -
dry
336
500
1
04/28/19 19:19
KKM
6010D
Chromium
65.0
mg/Kg -
dry
3.80
5.00
1
04/28/19 19:19
KKM
6010D
Copper
368
mg/Kg -
dry
2.90
5.00
1
04/27/19 20:46
KKM
6010D
Iron
93400
mg/Kg -
dry
84.8
100
1
04/27/19 20:46
KKM
6010D
Lead
60.2
mg/Kg -
dry
2.98
6.00
1
04/27/19 20:46
KKM
6010D
Magnesium
2960
mg/Kg -
dry
44.4
100
1
04/27/19 20:46
KKM
6010D
Manganese
1230
mg/Kg -
dry
3.66
10.0
1
04/27/19 20:46
KKM
6010D
Mercury
1.42
mg/Kg -
dry
0.0642
0.290
1
04/26/19 15:47
TJS
7471A
Molybdenum
5.86
mg/Kg -
dry
2.60
5.00
1
04/27/19 20:46
KKM
6010D
Nickel
32.2
mg/Kg -
dry
3.30
5.00
1
04/27/19 20:46
KKM
6010D
Potassium
2060
mg/Kg -
dry
59.6
100
1
04/27/19 20:46
KKM
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 2 of 5

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-115-0250
Lab No : 91672
Sample ID : Cooleemee
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Analytical Testing
Information :
REPORT OFANALYSIS
Report Date : 04/30/2019
Received : 04/25/2019
Q0"
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/24/2019 9:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<9.80
mg/Kg -
dry
9.80
10.0
1
04/27/19 20:46
KKM
6010D
Sodium
1590
mg/Kg -
dry
154
500
1
04/27/19 20:46
KKM
6010D
Zinc
1340
mg/Kg -
dry
21.6
25.0
1
04/27/19 20:46
KKM
6010D
Sulfur
6800
mg/Kg -
dry
97.8
100
1
04/27/19 20:46
KKM
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 3 of 5

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-115-0250
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: IDanyale Love Date & Time: 04/25/2019 10:39:02
Page 4 of 5

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (city/State)
RUSH -Additional charges apply
Special Detection Limit(s)
Method of Shipment
1:1Fed Ex UPS F-1USPS
Matrix Key
Ww -Wastewater GW - Groundwater
Date Results Needed
Courier Client Drop Off
DW - Drinking Water S -Soil /Solid 0 - Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
[e-mail]
_
0
Z
0
A Cool < 10C Na25203 (Micro Only)
B Cool c 6C
�
-
O
v
M
�
C H250None
Waypoi nt
y°1,
n
0
c
C
0
Required
D None Required
ANALYTICAL
0
°
o
O
Q
O
!^
W
E NaOH pH>10
F HNO3 pH<2
2790 Whitten Road
Memphis, 'IN 38133
Unless noted, all containers
°
`u
a
z
-
tts
z
Z
T
2
V)
\\
/
G HCL 4 p
H H3PO4 pH<2
[phone]
per Table II of 40 CFR Part
£
x
`
`
Y
w
Z
/'1
U
Cool <= 6C NA26203
136.
Z
Required
Analysis / Preservative
Comments/Notes
Date
Time
Sample Identification
y�Ly
0D"m
V
X
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,PbA
y�1y
93aar+
C
ooe�hLnI-
I
ti
G
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
IIIIIIIIIIIII�IIIII�IIIIIIIINIIIIIIIIIIII
IIIIIIIIXIIII
IIIIIIIIIXX
io-ii5-0222
EMA Resources Inc
Analytical Testino
IIIIII IIIII III IIIIII IIIII IIII
IIII IIIIII IIIII
0
5
I III IIIII III II11
019
EMA Resources Inc
10,3839
Analytical Testinq
Sampled by (N.
eIt"A5
Sludge Samples - Report Dry Weight
For Laboratory Use Only
Ice
Custody
Lab Comments
CSeals
N
LrM+
Relin 'shed by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
/ N
I/N /2 • copra
Relinquished by: (SIGNATURE)
Date Time
Received by: (SI
ATURE)
Date Time
Blank oolerTemp
r
Relinquished by: (SIGNATURE)
Date Time
Rece' d b (SIG
URE) Da Timms
��,
S cI

Waypoint
ANALYTICAL
5/ 16/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-127-0222
Client Project Description: Cooleemee WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 5/7/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
. L +� i vxu
CL
Page 1 of 7

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Cooleemee WWTP
Lab Report Number: 19-127-0222
Date: 5/16/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L435277
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 2 of 7

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample 94721 (Cooleemee WWTP)
Analyte: Calcium
QC Batch No: L435414/L434996
Target analyte(s) was identified in the method blank associated with this project. Per laboratory protocol any
associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Page 3 of 7

Wa OI �� ' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Y ANALYTICAL www.wa ointanal tical.com
Yp Y
46245
EMA Resources Inc
Mr. Brent Collins Project Cooleemee WWTP Report Date : 05/16/2019
755 Yadkinville Road Information : Received : 05/07/2019
Mocksville , NC 27028
Report Number : 19-127-0222 REPORT OFANAL YSIS Danyale Love
Project Manager
Lab No : 94721
Matrix: Solids
Sample ID : Cooleemee WWTP
Sampled:
5/6/2019
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
92.8
%
0.010
1
05/08/19 15:15
CJR
SW-DRYWT
Ammonia Nitrogen
11000
mg/Kg -
dry
347
1
05/16/19 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<66.9
mg/Kg -
dry
66.9
66.9
1
05/16/19 12:49
ZBD
4500NO3F-2011
Organic N
15600
mg/Kg -
dry
14.0
701
1
05/13/19 15:06
CALCULATION -
pH
6.9
S.U.
1
05/15/19 08:21
JSL
9045D
Total Solids
7.22
%
0.010
0.010
1
05/08/19 15:15
CJR
2540G-2011
Total Volatile Solids
38.8
%
0.010
0.010
1
05/08/19 15:15
CJR
2540G-2011
Total Kjeldahl Nitrogen
26500
mg/Kg -
dry
701
1
05/13/19 15:06
CLP 4500NORGD-2011
Phosphorus
8500
mg/Kg -
dry
35.7
69.4
1
05/09/19 21:15
KKM
6010D
Aluminum
28500
mg/Kg -
dry
28.2
69.4
1
05/09/19 21:15
KKM
6010D
Arsenic
<5.82
mg/Kg -
dry
5.82
6.94
1
05/09/19 21:15
KKM
6010D
Cadmium
1.143
mg/Kg -
dry
0.688
1.39
1
05/09/19 21:15
KKM
6010D
Calcium
6680 B
mg/Kg -
dry
233
347
1
05/10/19 14:22
KKM
6010D
Chromium
41.1
mg/Kg -
dry
2.64
3.47
1
05/09/19 21:15
KKM
6010D
Copper
210
mg/Kg -
dry
2.01
3.47
1
05/09/19 21:15
KKM
6010D
Iron
66700
mg/Kg -
dry
58.9
69.4
1
05/09/19 21:15
KKM
6010D
Lead
35.1
mg/Kg -
dry
2.07
4.17
1
05/09/19 21:15
KKM
6010D
Magnesium
2000
mg/Kg -
dry
30.8
69.4
1
05/09/19 21:15
KKM
6010D
Manganese
857
mg/Kg -
dry
2.54
6.94
1
05/09/19 21:15
KKM
6010D
Mercury
1.19
mg/Kg -
dry
0.0486
0.221
1
05/08/19 12:03
TJS
7471A
Molybdenum
3.423
mg/Kg -
dry
1.81
3.47
1
05/09/19 21:15
KKM
6010D
Nickel
21.3
mg/Kg -
dry
2.29
3.47
1
05/09/19 21:15
KKM
6010D
Potassium
1460
mg/Kg -
dry
41.4
69.4
1
05/09/19 21:15
KKM
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 4 of 7

Waypoint,
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 19-127-0222
Lab No : 94721
Sample ID : Cooleemee WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Cooleemee WWTP
Information :
REPORT OFANALYSIS
Report Date : 05/16/2019
Received : 05/07/2019
Qa"
Danyale Love
Project Manager
Matrix: Solids
Sampled: 5/6/2019 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<6.81
mg/Kg -
dry
6.81
6.94
1
05/09/19 21:15
KKM
6010D
Sodium
1130
mg/Kg -
dry
107
347
1
05/09/19 21:15
KKM
6010D
Zinc
818
mg/Kg -
dry
15.0
17.4
1
05/09/19 21:15
KKM
6010D
Sulfur
4320
mg/Kg -
dry
67.9
69.4
1
05/09/19 21:15
KKM
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
05/09/19 21:15
CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 5 of 7

(2)W•
ayPoi nt 2790 Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-127-0222
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: Rory Phillips Date & Time: 05/07/2019 09:52:00
Page 6 of 7

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Page 7 of 7

aceAnalytical a ANALYTICAL REPORT
National Center for Testing &Innovation April 19, 2019
EMA Resources
Sample Delivery Group: L1087575
Samples Received: 04/10/2019
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
Stacy Kennedy
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures:060302, 060303,and 060304.
II.
F +

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
COOLEEMEE WWTP L1087575-01
5
Fn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FC
Wet Chemistry by Method D93/1010A
10
F
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
[Al
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
RC
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1037575
04/19/1917:12 2 of 21

I
SAMPLE SUMMARY
Collected by
COOLEEMEE WWTP L1087575-01 Waste Roy Whitaker
ONE LAB. NATIONWIDE. *
Collected date/time Received date/time
04/09/19 08:45 04/10/19 08:45
Cp
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1266334
1 04/15/1914:45
04/15/1914:45
TM
Preparation by Method 1311
WG1266387
1 04/15/1915:47
04/15/1915:47
CGD
Wet Chemistry by Method 9012 B
WG1265448
1 04/16/19 08:49
04/16/1913:42
JER
Wet Chemistry by Method 9034-9030B
WG1266106
1 04/17/1914:25
04/17/1914:25
TCC
Wet Chemistry by Method 9045D
WG1265297
1 04/13/1915:56
04/13/1916:27
TH
Wet Chemistry by Method D93/1010A
WG1264165
1 04/11/19 23:03
04/11/19 23:03
TCC
Mercury by Method 7470A
WG1266788
1 04/16/191143
04/17/1910:35
ABL
Metals (ICP) by Method 6010D
WG1266828
1 04/17/1915:55
04/18/19 09:29
TRB
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1266887
1 04/16/19 20:39
04/16/19 20:39
JHH
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1267252
1 04/18/19 05:44
04/18/1916:27
KLM
Pesticides (GC) by Method 8081B
WG1266504
1 04/17/19 07:23
04/17/1916:28
LEL
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1266499
1 04/17/1912:20
04/18/19 04:23
AO
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1037575 04/19/1917:12
PAGE:
3 of 21

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
F,
Stacy Kennedy [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 4 of 21

COOLEEMEE WWTP
Collected date/time: 04/09/19 08:45
Preparation by Method 1311
SAMPLE RESULTS - 01
L1087575
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
4/15/2019 2:45:29 PM
WG1266334
TCLP ZHE Extraction -
4/15/2019 3:47:29 PM
WG1266387
Fluid 1
4/15/2019 2:45:29 PM
WG1266334
Initial pH 6.81
4/15/2019 2:45:29 PM
WG1266334
Final pH 4.89
4/15/2019 2:45:29 PM
WG1266334
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
04/16/201913:42
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide 60.7 25.0
Wet Chemistry by Method 9045D
Batch
WG1265448
Dilution Analysis Batch
date / time
1 04/17/201914:25 WG1266106
Result Qualifier Dilution Analysis
Analyte su date / time
Corrosivity by pH 7.17 T8 1 04/13/201916:27
Sample Narrative:
L1087575-01 WG1265297: 7.17 at19.4C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis
Analyte Deg. F date / time
Ignitability DNI at170 1 04/11/2019 23:03
Mercury by Method 7470A
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.334
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
6.85
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Batch
WG1265297
Batch
WG1264165
Dilution Analysis Batch
date / time
1 04/17/201910:35 WG1266788
Dilution Analysis
Batch
date / time
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
1 04/18/2019 09:29
WG1266828
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 04/16/2019 20:39
WG1266887
1 04/16/2019 20:39
WG1266887
1 04/16/2019 20:39
WG1266887
1 04/16/2019 20:39
WG1266887
SDG:
DATE/TIME: PAGE:
L1037575
04/19/1917:12 5 of 21

COOLEEMEE WWTP SAMPLE RESULTS
Collected date/time: 04/09/19 08:45 L1087575
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
04/16/2019 20:39
WG1266887
1,1-Dichloroethene
ND
0.0500 0.70 1
04/16/2019 20:39
WG1266887
2-Butanone (MEK)
ND
0.500 200 1
04/16/2019 20:39
WG1266887
Tetrachloroethene
ND
0.0500 0.70 1
04/16/2019 20:39
WG1266887
Trichloroethene
ND
0.0500 0.50 1
04/16/2019 20:39
WG1266887
Vinyl chloride
ND
0.0500 0.20 1
04/16/2019 20:39
WG1266887
(S) Toluene-dH
100
80.0-120
0411612019 20.39
WG1266887
(S)c,a,o-Trifluorotoluene
100
80.0-120
041161201920.39
WG1266887
(S) 4-Bromofluorobenzene
93.1
77.0-126
0411612019 20.39
WG1266887
(S) 1,2-Dichloroethane-d4
97.7
70.0-130
041161201920.39
WG1266887
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S)2,4-DichlorophenylAcetic Acid 81.2
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
E7.6
(S) Tetrochloro-m-xylene
74.1
Qualifier RDL
Limit
mg/I
mg/I
0.00200
1
0.00200
10
14.0-158
Qualifier RDL
Limit
mg/I
mg/I
0.00500 0.03
0.00500 0.02
0.00500 0.0080
0.00500 0.40
0.00500 10
0.0100 0.50
10.0-128
10.0-127
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Dilution Analysis
date / time
1 04/18/201916:27
1 04/18/201916:27
041181201916.27
Dilution Analysis
date / time
04/17/201916:28
04/17/201916:28
04/17/201916:28
04/17/201916:28
04/17/201916:28
04/17/201916:28
041171201916.28
041171201916.28
Batch
WG1267252
WG1267252
WG1267252
Batch
WG1266504
WG1266504
WG1266504
WG1266504
WG1266504
WG1266504
WG1266504
WG1266504
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 04/18/2019 04:23
WG1266499
2,4-Dinitrotoluene
ND
0.100
0.13
1 04/18/2019 04:23
WG1266499
Hexachlorobenzene
ND
0.100
0.13
1 04/18/2019 04:23
WG1266499
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 04/18/2019 04:23
WG1266499
Hexachloroethane
ND
0.100
3
1 04/18/2019 04:23
WG1266499
Nitrobenzene
ND
0.100
2
1 04/18/2019 04:23
WG1266499
Pyridine
ND
0.100
5
1 04/18/2019 04:23
WG1266499
3&4-Methyl Phenol
ND
0.100
400
1 04/18/2019 04:23
WG1266499
2-Methylphenol
ND
0.100
200
1 04/18/2019 04:23
WG1266499
Pentachlorophenol
ND
0.100
100
1 04/18/2019 04:23
WG1266499
2,4,5-Trichlorophenol
ND
0.100
400
1 04/18/2019 04:23
WG1266499
2,4,6-Trichlorophenol
ND
0.100
2
1 04/18/2019 04:23
WG1266499
(S) 2-Fluorophenol
39.1
10.0-120
0411812019 04.23
WG1266499
(S) Phenol-d5
22.5
10.0-120
0411812019 04.23
WG1266499
(S) Nitrobenzene-d5
60.2
10.0-127
0411812019 04.23
WG1266499
(S) 2-Fluorobiphenyl
60.8
10.0-130
0411812019 04.23
WG1266499
(S) 2,4, 6-Tribromophenol
66.0
10.0-155
0411812019 04.23
WG1266499
(S) p-Terphenyl-d14
60.4
10.0-128
0411812019 04.23
WG1266499
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 6 of 21

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WG1266788 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1087575-01
Method Blank (MB)
(MB) R3402550-1 04/17/19 09:59
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
Mercury U 0.00330
0.0100
Laboratory Control Sample (LCS) • Laboratory Control
Sample Duplicate (LCSD)
(LCS) R3402550-2 04/17/1910:01 • (LCSD) R3402550-3 04/17/19 10:04
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0293 0.0290
97.8 96.7 80.0-120 1.14 20
L1087426-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1037426-04 04/17/19 10:07 • (MS) R3402550-4 04/17/19 10:09 • (MSD) R3402550-5 04/17/19 1012
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0298
0.0297 99.3 99.1 1 75.0-125 0.198 20
L1087764-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1037764-02 04/17/19 10:14 • (MS) R3402550-6 04/17/19 1017 • (MSD) R3402550-7 04/17/19 1019
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0290
0.0302 96.6 101 1 75.0-125 3.95 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 11 of 21

WG1266828
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1087575-01
ONE LAB. NATIONWIDE. *
(MB) R3402991-1 04/13/19 0911
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Arsenic U 0.0333 0.100
Barium U 0.0333 0.100
Cadmium U 0.0333 0.100
Chromium U 0.0333 0.100
Lead U 0.0333 0.100
Selenium U 0.0333 0.100
Silver U 0.0333 0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3402991-2 04/13/19 09:14 • (LCSD) R3402991-3 04/13/19 0916
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte mg/I mg/I mg/I
Arsenic 10.0 9.71 9.78
97.1
97.8
80.0-120
0.677
20
Barium 10.0 9.88 9.87
98.8
98.7
80.0-120
0.0464
20
Cadmium 10.0 9.69 9.66
96.9
96.6
80.0-120
0.245
20
Chromium 10.0 9.55 9.53
95.5
95.3
80.0-120
0.214
20
Lead 10.0 10.0 9.97
100
99.7
80.0-120
0.457
20
Selenium 10.0 9.86 9.83
98.6
98.3
80.0-120
0.234
20
Silver 2.00 1.94 1.94
97.1
97.1
80.0-120
0.0135
20
L1088224-03 Original Sample (OS) • Matrix Spike (MS) • Matrix
Spike Duplicate (MSD)
(OS) L1033224-03 04/13/19 09:19 • (MS) R3402991-5 04/13/19 09:24 • (MSD) R3402991-6 04/13/19 09:26
Spike Amount Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier
MSD Qualifier
RPD
RPD Limits
Analyte mg/I mg/I mg/I
mg/I
Arsenic 10.0 ND 9.71
9.55
97.1
95.5
1 75.0-125
1.64
20
Barium 10.0 0.907 10.8
10.7
98.9
98.1
1 75.0-125
0.766
20
Cadmium 10.0 ND 9.61
9.63
96.1
96.3
1 75.0-125
0.158
20
Chromium 10.0 ND 9.45
9.49
94.5
94.9
1 75.0-125
0.408
20
Lead 10.0 ND 10.1
9.97
101
99.7
1 75.0-125
0.819
20
Selenium 10.0 ND 9.79
9.79
97.9
97.9
1 75.0-125
0.0830
20
Silver 2.00 ND 1.93
1.92
96.6
96.2
1 75.0-125
0.401
20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1037575
04/19/1917:12
12 of 21

WG1266887 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1087575-01
Method Blank (MB)
(MB) R3402291-3 04/16/191457
MB Result
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
104
(S) a, a, a- Trifluorotoluene 97.8
(S) 4-Bromofluorobenzene 97.8
(S) 1,2-Dichloroethane-d4 94.8
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
0.0833
0.250
0.0167
0.0500
0.0167
0.0500
0.167
0.500
0.0167
0.0500
0.0167
0.0500
0.0167
0.0500
80.0-120
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3402291-1 04/16/1911:33 • (LCSD) R3402291-2 04/16/191155
Spike Amount LCS Result LCSD Result
Analyte mg/I mg/I mg/I
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Benzene
0.0250
0.0238
0.0246
95.4
98.4
70.0-123
3.18
20
Carbon tetrachloride
0.0250
0.0251
0.0260
101
104
68.0-126
3.39
20
Chlorobenzene
0.0250
0.0233
0.0227
93.3
91.0
80.0-121
2.55
20
Chloroform
0.0250
0.0243
0.0245
97.4
97.9
73.0-120
0.540
20
1,2-Dichloroethane
0.0250
0.0215
0.0216
86.0
86.2
70.0-128
0.300
20
1,1-Dichloroethene
0.0250
0.0280
0.0279
112
112
71.0-124
0.222
20
2-Butanone (MEK)
0.125
0.117
0.120
93.8
95.7
44.0-160
1.96
20
Tetrachloroethene
0.0250
0.0235
0.0232
94.1
92.9
72.0-132
1.28
20
Trichloroethene
0.0250
0.0253
0.0253
101
101
78.0-124
0.0285
20
Vinyl chloride
0.0250
0.0280
0.0290
112
116
67.0-131
3.50
20
(S) Toluene-d8
94.5
94.7
80.0-120
(S) a, a, a- Trifluorotoluene
97.7
100
80.0-120
(S) 4-Bromofluorobenzene
94.2
93.0
77.0-126
(S) 1,2-Dichloroethane-d4
102
104
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 13 of 21

WG1266887
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D
L1087575-01
L1087393-01 Original Sample (OS) • Matrix Spike (MS)
C p
(OS) L1087393-01 04/16/19 2143 • (MS) R3402291-4 04/16/19 2226
Spike Amount Original Result MS Result
MS Rec.
Dilution
Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
%
%
z
TC
Benzene 1.25 ND 1.28
103
1
17.0-158
Carbon tetrachloride 1.25 ND 1.45
116
1
23.0-159
FS
Chlorobenzene 1.25 ND 1.28
102
1
33.0-152
Chloroform 1.25 ND 1.36
109
1
29.0-154
1,2-Dichloroethane 1.25 ND 1.14
91.6
1
29.0-151
[Cn
1,1-Dichloroethene 1.25 ND 1.52
122
1
11.0-160
2-Butanone (MEK) 6.25 ND 6.33
101
1
10.0-160
FrTetrachloroethene
1.25 ND 1.34
107
1
10.0-160
Trichloroethene 1.25 ND 1.43
115
1
10.0-160
Vinyl chloride 1.25 ND 1.47
118
1
10.0-160
(S) Toluene-d8
96.6
80.0-120
(S) a, a, a- Trifluorotoluene
99.8
80.0-120
7 GI
(S) 4-Bromofluorobenzene
95.9
77.0-126
(S) 1,2-Dichloroethane-d4
105
70.0-130
FAI
L1087737-01 Original Sample (OS) • Matrix Spike (MS) • Matrix
Spike Duplicate (MSD)
Fc
(OS) L1037737-01 04/16/19 22:05 • (MS) R3402291-6 04/16/19 22:43 • (MSD) R3402291-7 04/16/19 23:09
Spike Amount Original Result MS Result
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte mg/I mg/I mg/I
mg/I
Benzene 1.25 ND 1.34
1.32
105
102 1
17.0-158
1.97
27
Carbon tetrachloride 1.25 ND 1.48
1.43
118
114 1
23.0-159
3.08
28
Chlorobenzene 1.25 ND 1.17
1.28
93.8
102 1
33.0-152
8.36
27
Chloroform 1.25 ND 1.35
1.34
108
107 1
29.0-154
0.656
28
1,2-Dichloroethane 1.25 ND 1.17
1.14
93.9
91.0 1
29.0-151
3.10
27
1,1-Dichloroethene 1.25 ND 1.56
1.53
125
122 1
11.0-160
1.74
29
2-Butanone (MEK) 6.25 ND 6.25
6.19
100
99.0 1
10.0-160
1.08
32
Tetrachloroethene 1.25 ND 1.22
1.32
97.4
106 1
10.0-160
8.24
27
Trichloroethene 1.25 ND 1.38
1.36
110
109 1
10.0-160
1.20
25
Vinyl chloride 1.25 ND 1.47
1.48
118
118 1
10.0-160
0.348
27
(S) Toluene-d8
91.5
99.2
80.0-120
(S) a, a, a- Trifluorotoluene
102
99.8
80.0-120
(S) 4-Bromofluorobenzene
90.5
97.5
77.0-126
(S) 1,2-Dichloroethane-d4
106
103
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1037575
04/19/1917:12
14 of 21

WG1267252
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3403149-1 04/13/1912:44
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 61.2
Acid
QUALITY CONTROL SUMMARY
L1087575-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3403149-2 04/13/19 12:53
Spike Amount LCS Result
Analyte mg/I mg/I
2,4-D 0.0500 0.0472
2,4,5-TP (Silvex) 0.0500 0.0482
(S) Z4-Dichlorophenyl Acetic
Acid
LCS Rec.
Rec. Limits LCS Qualifier
94.4
50.0-120 P
96.4
50.0-125 P
�JL�EEI]FI-Si
L1087593-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1037593-10 04/13/19 17:09 • (MS) R3403149-3 04/13/19 17:23 • (MSD) R3403149-4 04/13/19 17:37
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4-D
0.0500
ND
0.0450
0.0473
90.0
94.6
1 50.0-120
4.98
20
2,4,5-TP (Silvex)
0.0500
ND
0.0457
0.0484
91.4
96.8
1 50.0-125
5.74
20
(S) Z4-Dichlorophenyl Acetic
80.0
84.8
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 15 of 21

WG1266504 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method 8081B L1087575-01
Method Blank (MB)
(MB) R3402825-2 04/17/19 1411
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
93.7
10.0-128
(S) Tetrochloro-m-xylene
80.8
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3402825-1 04/17/191359
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.0101
101
55.0-129
Endrin
0.0100
0.00986
98.6
57.0-134
Heptachlor
0.0100
0.00766
76.6
27.0-132
Methoxychlor
0.0100
0.00940
94.0
54.0-155
(S) Decachlorobiphenyl
93.7
10.0-128
(S) Tetrochloro-m-xylene
83.2
10.0-127
L1087593-10 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1037593-10 04/17/19 17:05 • (MS) R3402325-3 04/17/19 1717 • (MSD) R3402325-4 04/17/19 17:30
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00957
0.00971
95.7
97.1
1 14.0-141
Endrin
0.0100
ND
0.00954
0.00972
95.4
97.2
1 10.0-160
Heptachlor
0.0100
ND
0.00734
0.00726
73.4
72.6
1 16.0-136
Methoxychlor
0.0100
ND
0.00913
0.00923
91.3
92.3
1 10.0-160
(S) Decachlorobiphenyl
90.2
91.6
10.0-128
(S) Tetrochloro-m-xylene
75.4
75.1
10.0-127
ONE LAB. NATIONWIDE. *
MS Qualifier MSD Qualifier RPD RPD Limits
1.45 40
1.87 39
1.10 40
1.09 34
FP1
ITC
FS-1
[Cn]
Fr
�GI
FAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 16 of 21

WG1266499 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1087575-01
Method Blank (MB)
(MB) R3402887-2 04/13/19 0039
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
Pyridine
U
0.0333
0.100
(S) 2-Fluorophenol
37.2
10.0-120
(S) Phenol-d5
22.4
10.0-120
(S) Nitrobenzene-d5
473
10.0-127
(S) 2-Fluorobiphenyl
56.1
10.0-130
(S) Z4, 6-Tribromophenol
67.5
10. 0-155
(S) p-Terphenyl-d14
65.0
10.0-128
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3402887-1 04/18/19 0019
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.294
58.8
18.0-120
2,4-Dinitrotoluene 0.500
0.373
74.6
49.0-124
Hexachlorobenzene 0.500
0.380
76.0
44.0-120
Hexachloro-1,3-butadiene 0.500
0.303
60.6
19.0-120
Hexachloroethane 0.500
0.282
56.4
15.0-120
Nitrobenzene 0.500
0.293
58.6
27.0-120
2-Methylphenol 0.500
0.290
58.0
28.0-120
3&4-Methyl Phenol 0.500
0.285
57.0
31.0-120
Pentachlorophenol 0.500
0.346
69.2
23.0-120
2,4,5-Trichlorophenol 0.500
0.393
78.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.377
75.4
42.0-120
Pyridine 0.500
0.144
28.8
10.0-120
(S) 2-Fluorophenol
43.0
10.0-120
(S) Phenol-d5
24.3
10.0-120
(S) Nitrobenzene-d5
59.1
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1087575 04/19/1917:12 17 of 21

I
WG1266499 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1087575-01
Laboratory Control Sample (LCS)
(LCS) R3402887-1 04/18/19 0019
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) 2-Fluorobiphenyl 677 10.0-130
(S) 2,4, 6-Tribromophenol 77.0 10. 0-155
(S) p-Terphenyl-d14 65.1 10.0-128
L1087318-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1037313-01 04/13/19 00:59 • (MS) R3402337-3 04/13/19 0120 • (MSD) R3402337-4 04/13/19 0140
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.270
0.251
54.0
50.2
2,4-Dinitrotoluene
0.500
ND
0.408
0.391
81.6
78.2
Hexachlorobenzene
0.500
ND
0.421
0.403
84.2
80.6
HexachIoro-1,3-butadiene
0.500
ND
0.274
0.254
54.8
50.8
Hexachloroethane
0.500
ND
0.235
0.229
47.0
45.8
Nitrobenzene
0.500
ND
0.324
0.316
64.8
63.2
2-Methylphenol
0.500
ND
0.313
0.297
62.6
59.4
3&4-Methyl Phenol
0.500
ND
0.307
0.291
61.4
58.2
Pentachlorophenol
0.500
ND
0.374
0.352
74.8
70.4
2,4,5-Trichlorophenol
0.500
ND
0.442
0.424
88.4
84.8
2,4,6-Trichlorophenol
0.500
ND
0.419
0.402
83.8
80.4
Pyridine
0.500
ND
0.180
0.183
36.0
36.6
(S) 2-Fluorophenol
44.5
41.6
(S) Phenol-d5
26.0
23.6
(S) Nitrobenzene-d5
63.6
62.7
(S) 2-Fluorobiphenyl
74.4
70.3
(S)2,4,6-Tribromophenol
83.5
83.5
(S) p-Terphenyl-d14
68.6
66.3
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
7.29
1 39.0-125
4.26
1 35.0-122
4.37
1 12.0-120
7.58
1 10.0-120
2.59
1 12.0-120
2.5C
1 10.0-120
5.25
1 10.0-120
5.35
1 10.0-128
6.06
1 33.0-120
4.16
1 26.0-120
4.14
1 10.0-120
1.65
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
30
36
37
31
31
37
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1037575 04/19/1917:12 13 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Abbreviations and Definitions
u
Fc
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
FS
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard Anal es added to eve blank, sample, Laboratory Control Sample/Duplicate and
9 ( 9 )- Yt n1 P n1
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
F
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
e
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
AI
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Rc
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
P
RPD between the primary and confirmatory analysis exceeded 40%.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1037575 04/19/1917:12 19 of 21

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1037575 04/19/1917:12 20 of 21

Billing Information:
Analysis
/
Container
/ Preservative
Chain of Custody Page _ of _
EMA Resources
Mr. Brent Collins Pres
755 Yadkinville Road Chk
8CB1y'�e}ICai�
755 Yadkinville Road
Mocksville, NC 27028
Haro vu Ce a rw r.va Mnonx an
Mocksville, NC 27028
12065 Lebanon Rd r r�
Report to:
Finail To, [e-mail]
Mr. Brent Collins
Phone.6unt 1518-5858et, TN z
Phune 51s�7sa-sass s�,r
Phone-800767-SRS9 nS .
Fax: [phone]
Project
City/State �,,{{
Collected: frloCiCS� I�C/N�
Description'
L # 81 5-7-5
Client Project p
Lab Project a
Phone: [phone]
A233
Fax: [phone]
uz
v
li
Collected by (print):
Site/Facility ID #
P.Q. #
0
Acctnum: EMARES
Temp late:T11413
Collected by (signature):
Rush? {Lab MUST Be Notified} Quote #
Same Day Five Day
CL
O
U
-L!
Prelogin: P689638
_ Next Day _ 5 Day (Rad Only) Date Results Needed
Z
~
TSR: 702 - Cassandra Foster
Immediately
Two Day 10 Day (Rad Only) No.
L
w
PS: 11
Packed on Ice N _ Y_
_Three Day of
J
'i
a
J
Snipped via: FedEX Ground
Sample ID
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
Rr-1,,
samnlep(lab.nly)
Cooleew,re Wti^1r`A
C
SS
3'
y/9�/9
$:5►So,n
2
X
X
r p
I
i
i
_
' Matrix: emarks. Sample F-ecel-- C-PG
SS - Soil AIR - Air -Filter c�* ' Fa Temp COC Seal Present/Intact:--NP _Y
FN
�w
GW- Groundwater B Bioassay s7s�RCCt�i
COC Signed/Accurare: �t _1
Bottles arrave intact: td
WW - Wastewater Flow Other Correct bottles used: _N
DW - Drinking Water Samples ret rned via: Sufficient volume sent: Y _N
jArolicd:ble
OT Other _UPS FedEx ,Courier _ Tracking #
VOA Zero Headspace: Y N
Relinquish Date: Time: Received by: (Signaturej Trip BI nk ceived: Ye N Preservation Correct/Checked: _Y _N
Q ! HCL / MeoH
TBR
Relinquish by : (Signature)
Date:
Time:
Received by: (Signature)
em otfles Received:
If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date:
Time:
Receiv or lab by: nature}
Date: Time:
Hold:
Conditi :
L;_Jd_ JG 81LIS--
NCF / U

aceAnalytical ® ANALYTICAL REPORT
National Center for Testing & Innovation May 08, 2019
FC
FS
EMA Resources
Sample Delivery Group: L1091344 Fn
Samples Received: 04/10/2019
Project Number: Fr
Description: Sludge FC
GI
Report To: Mr. Brent Collins
755 Yadkinville Road [Al
Mocksville, NC 27028
RC
Entire Report Reviewed By:
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures:060302, 060303,and 060304.
4
AP- 40MENN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091344 05/03/1911:20 1 of 10

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
COOLEEMEE WWTP L1091344-01
5
Fn
Qc: Quality Control Summary
Metals (ICP) by Method 6010D
6
Fr
GI: Glossary of Terms
7
Al: Accreditations & Locations
8
FC
Sc: Sample Chain of Custody
9
GI
[Al
RC
ACCOUNT: PROJECT:
SDG: DATE/TIME:
PAGE:
EMA Resources
L1091344 05/03/1911:20
2 of 10

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
COOLEEMEE WWTP L1091344-01 Waste Roy Whitaker 04/09/19 08:45 04/10/19 08:45 , C
P
Method
Preparation by Method 1311
Metals (ICP) by Method 6010D
Batch Dilution Preparation
date/time
W G1270724 1 04/23/1918:10
WG1271406 1 04/24/19 22:07
Analysis
date/time
04/23/1918:10
04/25/19 07:14
Analyst
CGD
TRB
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Fr
FC
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1091344 05/03/1911:20
PAGE:
3 of 10

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Cassandra Foster
Project Manager
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091344 05/03/1911:20 4 of 10

COOLEEMEE WWTP
Collected date/time: 04/09/19 08:45
Preparation by Method 1311
SAMPLE RESULTS - 01
L1091344
Result
Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction -
4/23/2019 6:10:51 PM
WG1270724
Fluid 1
4/23/2019 6:10:51 PM
WG1270724
Initial pH 6.76
4/23/2019 6:10:51 PM
WG1270724
Final pH 4.98
4/23/2019 6:10:51 PM
WG1270724
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Lead ND 0.100 5
Dilution Analysis Batch
date / time
1 04/25/2019 07:14 WG1271406
ONE LAB. NATIONWIDE. *
Fp
FC
FS
Fn
FA
FC
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091344 05/03/1911:20 5 of 10

WG1271406
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3405204-1 04/25/19 0707
MB Result
Analyte mg/I
Lead U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0333 0.100
QUALITY CONTROL SUMMARY
L1091344-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3405204-2 04/25/19 07:09 • (LCSD) R3405204-3 04/25/19 0712
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Lead 10.0 9.43 9.39 94.3 93.9 80.0-120 0.377 20
L1091344-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1091344-01 04/25/19 07:14 • (MS) R3405204-5 04/25/19 07:20 • (MSD) R3405204-6 04/25/19 07:22
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Lead 10.0
ND
9.31
9.39 93.1 93.9 1 75.0-125 0.929 20
FP1
ITC
FS-1
[Cn]
Fr
�GI
SAI
Fc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091344 05/03/1911:20 6 of 10

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Abbreviations and Definitions
u
Fc
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
FS
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fn
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fr
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
El
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
R
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1091344 05/03/1911:20 7 of 10

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
ID SD
VWY
` NV T NE
T UT
CA co
KS
W o �AZ NM O�
T TX
AK
� . b
C,
fo • B HI 4 S
ACCOUNT: V PROJECT:
EMA Resources
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR
Ms AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1091344 05/03/1911:20 3 of 10

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Andy Vann
From: Cassandra Foster
Sent: Monday, April 22, 2019 10:48 AM
To: Login; Sample Storage; TCLP
Subject: L1087575 RElog for TCLP Lead
Please relog for TCLP PSICP to a new SDG#. Standard turn.
Thank you,
Cassandra (Kc) Foster
Project Manager
Pace Analytical National Center for Testing & Innovation
12065 Lebanon Road I Mt. Juliet, TN 37122
615-773-9665
[e-mail] j pacenational.com
ESC Lab Sciences is now Pace Analytical National Center for Testing & Innovation! Please
make note of my new email address and website.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Davie County Water System WQ Permit Number: WQ0010583
WWTP Name: Cooleemee WWTP NPDES Number: NCO024872
Monitoring Period:
From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat DryinM ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Rav ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
JAerob1c Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative pe med Class A or Class B complete the folllowing.F.F
monitor
in data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Excee- Number o
ences-
Frequency
of Analysis
Sample
Type
Analytical
Tech nique
Minimum
Geo. Mean
Maximuml
Units
Fecal Coliform
2 x 10 to the
6th power
per of
otals olds
MPN
CFU
10802
15625
24217
col/g
0
Quarterly
C
SM9222D
1000 mpn per grain
oftotal solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Aik. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
reauirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tim Smith - WWTP ORC
Preparer Name and Title (type or print)
Signature of P parer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
� 4;: 1 /3/2020
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02i (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Davie County Water System WQ Permit Number:
WWTP Name: Cooleemee WWTP NPDES Number:
Monitoring Period:
From 1/1/2019
To 12/31/2019
WQ0010583
NCO024872
Pathosen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑ 1
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Com ost ❑
Heat Drying ❑
Heat Treatment ❑
Then-nophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density 211
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Si nificaatly Reduce Pathogens":
Lime Stabilization ❑
Air Drying, ❑
Composting ❑ jAcrobic
Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed Class A or Class B complete the folIowingFF
monitorin data:
Parameter
Allowable Level
in Sludge
Pathogen Density
o
NumberFrequency
Fxcee-
dendences
of Analysis
Sample
Type
Analytical
Tech-niqueinimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFL�
6640
12489
19841
col/ g
0
Quarterly
Q y
C
SM9222D
1000 mpn per gram
of total solid (dn-
wei t)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O-, uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
17 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tim Smith - WWTP ORC
Preparer Name and Title (type or print)
UA,. �.
Signature of reparer* Date
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
2!y-i w1 /3/2020
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Davie County Water System WQ Permit Number: WQ0010583
WWTP Name: Cooleemee WWTP NPDES Number: NCO024872
Monitoring Period: From 1/1/2019 To 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑ I Alt. C (Prior Testing)[]
Alt.D (No Prior Test) ❑
T Process to Further Reduce Pathogcngs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Dryin ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Garnma Ray ❑
Pasteurization ❑
Class B:
At. (1) Fecal Density r❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the following.
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
o
NumberFrequency
Excee-
of Analysis
Sample
Type
Analytical
Tech-ni ue
q
MinimumGeo.
Mean
aximu
Unitsences.
Fecal Coliform
2 x l 0 to the
6th power
per gram of
total solids
MPN
CFU
359
472
713
col/g
0
Quarterly
C
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
0
Alt. 2 (40-day bench)
JAlt. 3 (30-day bench) ❑ JAIL 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization ❑
JAR 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation) ❑
JNo vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tim Smith - WWTP ORC Brent Collins; Director of Technical Services
Prep r Name and Title (type or print)
JL
Signature of eparer* Date
Land Applier Name and Title (if applicable)(type or print)
Z�i"' 1 /3/2020
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Davie County Water System
WWTP Name: Cooleemee WWTP
Monitoring Period: From l/i/2019 To
WQ Permit Number:
NPDES Number:
12/31/2019
WQ0010583
NCO024872
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑ 1
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 0
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density RI
Alt_ (2) Process to Significantly Reduce Pathogens LJ
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative pe med Class A or Class B complete the followinj
1, monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Excee- Number o
ences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
260
465
709
col/g
0
Quarterly
C
SM9222D
1000 mpn per gam
of total solid (dry
wei t)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) r❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
I Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ jAlt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tim Smith - WWTP ORC
Preparer Name and Title (type or print)
Signature of P parer*
Brent Collins; Director of Technical Services
Land Applier Name and Title(ifapplicable)(type or print)
—1t ]tom G;2� - 1/3/2020
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 IO2 (26)
Date
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Brent Collins
Client: FMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech Work Order # 04091907 Sample: Cooleemee WWTP 1 Grab
Parameters
Page 1
Report Date: 4/24/2019
Date Sample Rcvd: 4/9/2019
4/9/19
Result Analysis Date Reporting Limit Method
% Total Solids 6.31 % 4/10/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 12678 col/g dry wt 4/9/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04091908 Sample: Cooleemee WWTP 2 Grab 4/9/19
Parameters ResuIt Analysis Date Reporting Limit Method
%Total Solids 6.48 % 4/10/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 10802 col/g dry wt 4/9/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04091909 Sample: Cooleemee WWTP 3 Grab 4/9/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.83 % 4/10/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 14641 col/g dry wt 4/9/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04091910 Sample: Cooleemee WWTP 4 Grab 4/9/19
Parameters Result Analysis Date Reporting limit Method
% Total Solids 6.92 % 4/10/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 14451 col/g dry wt 4/9/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04091911 Sample: Cooleemee WWTP 5 Grab 4/9/19
Parameters Result Analysis Date Reporting_ Limit Method
% Total Solids 6.94 % 4/10/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 21614 col/g dry wt 4/9/19 431 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Brent Collins Report Date: 4/24/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 4/9/2019
Meritech Work Order # 040919112 Sample: Cooleemee WWTP 6 Grab 4/9/19
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
6.67 %
4/10/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
14993 col/g dry wt
4/9/19
431 col/g dry wt
SM 9222D
Meritech Work Order # 040919113 Sample: Cooleemee WWTP 7 Grab
4/9/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
7.02 %
4/10/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
24217 col/g dry wt
4/9/19
431 col/g dry wt
SM 9222D
I hereby certify that 1 have reviewed and approve these data. _-Z
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

59-2016 Chain of Custody Record (COC)
NPDES#:
Client. EMA Resources Inc. Phone:_336-751-1441
M E RITECH INC.
J
Address:_ 755 Yadkinville Rd Fax: [phone]
ENVIRONMENTAL LABORATORIES
Mocksville NC 27028 Email:bl(ar txoliins a Pin 31 e5purCeSlnc.M11
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Brent Collins Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
www.meritechlabs.comCircle
all that apply Email (p eferred), Fax, Mail Std 10 da s) 3 - 5 Da s 24-bS Hrs
Sampling Dates & Times
Person Taking Sample (Sign/Print):
y Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
Tests) Req u i red
On Ice?
e Ys No
pH OK?
Date
Time
Date
Time
Grab?
Cont.t
CIOK.
CCd�ee-nee- WkJTP I
y�9�Irj
g.oia�
G
�
�ec4 [ ��; �or..-.
Z
3
Lf
i
(e
1
7
V
l
Temperature Upon
Receipt:
*** be done in field ***
Method Of
Dechlorination (<0.5 pm)of Ammonia, C nide, Phenol and TKN samples must the prior to preservation.
Comments:
Compositor #
Shipment:
EJ UPS
Jug#
Fed Ex
Are these rcqults f r egul ory purposes? Yes No 15
Report results in: mg/L mg/kg - ug/L
Hand Delivery
Relinquished by:, Dat�4/fig Time: .ys
Received by: Date:4/`g Time:
Other
Relinquished by: DaN /,3 Time: db, as
/
Received by: Date: Time:
Relinquished by: Date: Time:
ewe b:

Page 1
Contact: Brent Collins Report Date: 5/1/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksvilie, NC 27028 Date Sample Rcvd: 4/18/2019
Meritech Work Order # 04181907 Sample: Cooleemee WWTP 1 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 7.23 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 15214 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04181908 Sample: Cooleemee WWTP 2 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 7.23 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 12448 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04181909 Sample: Cooleemee WWTP 3 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.73 % 4/23/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 11887 col/g dry wt 4/15/19 431 cal/g dry wt SM 9222D
Meritech Work Order # 04181910 Sample: Cooleemee WWTP 4 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
%Total Solids 7.53 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 6640 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04181911 Sample: Cooleemee WWTP 5 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.59 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 13657 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
642 Tameo Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 2
Report Date: 5/1/2019
Date Sample Rcvd: 4/18/2019
Meritech Work Order # 04181912 Sample: Cooleemee WWTP 6 Grab 4/18/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 7.56 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 19841 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04181913 Sample: Cooleemee WWTP 7 Grab 4/18/19
Parameters Re. sult Analysis Date Reporting Limit Method
% Total Solids 6.41 % 4/23/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 11700 col/g dry wt 4/15/19 431 col/g dry wt SM 9222D
I hereby certify that have reviewed and approve these data.
Laboratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

ss-2016
Sample Locatio
Method of
Shipment:
UPS
Fed Ex
Hand Delivery
Other
Chain of Custody Record (COC)
MERITECH, INC.
ENVIRONMENTAL_ LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sampling Dates & Times
n and/or ID # Start End
gDate Time Date Time
L
7-
3
�r
7
*** Dechiorination (<0.5
Comments:
Are these results for
nquished by:
nquished by:
nquished by
Client: EMA Resources Inc.
Address: 755 Yadkinville Rd
Mocksville NC 27028
Attention: Brent Collins
NPDES#:
Phone: [phone]
Fax: [phone]
Email:_ brent.WfinsC er res© arc irac.cUm
Project:
P.O.#:
How would you like your report sent?
Circle all that apply: mail referred) , Fax, Mail
Person Taking Sample (Sign/Print):
Comp? Of
Grab? Cont.t Test(s) Required
Fecal
and TKN samples must be done in the field prior to preservation. ***
es? Yes No
Dy Time:
Date: Time:
by:
by:
ort results in: mg/L
Turn Around Time*
*RUSH work needs prior approval.
Std (10 days) 13 - 5 Days I �a - d$ 44-
Lab Use Only
,Gn,Ice? pH OK?
Yes)/ No Cl OK?
Temperature Upon
Receipt:-
Compositor #
JJug #
mg/kg ug/L
pale Time:
,fli 1 004~
Date: Tiimee:

Page 1
Contact: Brent Collins Report Date: 5/6/2019
Client: BMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 4/24/2019
Meritech Work Order # 04241926 Sample: Cooleemee WWTP 1 Grab 4/24/19
Parameters Result Analysis Date Reporting -Limit Method
% Total Solids 4.98 % 4/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 365 col/g dry wt 4/24/19 431 cal/g dry wt SM 9222D
Meritech Work Order # 04241927 Sample: Cooleemee WWTP 2 Grab 4/24/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 5.07 % 4/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 359 col/g dry wt 4/24/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04241928 Sample: Cooleemee WWTP 3 Grab 4/24/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 5,11 % 4/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 534 col/g dry wt 4/24/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04241929 Sample: Cooleemee WWTP 4 Grab 4/24/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 5.05 % 4/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 540 col/g dry wt 4/24/19 431 col/g dry wt SM 9222D
Meritech Work Order # 04241930 Sample: Cooleemee WWTP 5 Grab 4/24/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 5.10 % 4/25/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 713 col/g dry wt 4/24/19 431 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Brent Collins Report Date: 5/6/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 4/24/2019
Meritech Work Order # 04241931 Sample: Cooleemee WWTP 6 Grab 4/24/19
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
5.06 %
4/25/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
359 col/g dry wt
4/24/19
431 col/g dry wt
SM 9222D
Meritech Work Order # 04241932 Sample: Cooleemee WWTP 7 Grab
Parameters
4/24/19
Result Analysis Date Reporting Limit Method
% Total Solids
5.08 %
4/25/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
537 col/g dry wt
4/24/19
431 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

&9-2016
Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc_ Phone:— 336-751-1441
Address:_755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email:_ biem_ gM astl�--_,n esourcesuic-corn;
Project:
P.O.#:
Attention: Brent Collins Turn around rime*
ap
approval.
Haw would you like your report sent? *RUSH work needs p_
Std 10da s] 3-5 Da s 24-41Hrs
Circle all that apply Email (pr (erred] , Fax, Mail
.E
II/� E R �T E C H1 INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
w. I .
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample {sign/Print :
Lab Use Only
Start
End
Comp?
Grab?
# of
Cont.
Test (s) Required
On Ice?
'�e/ No
pH OK?
Cl OK?
Date
Time
Date
Time
z
..
11
S
G
7
14
Temperature Upon
Receipt:.
;
Method of
Shipment:
*** Dechlori
nation( <Q.5 m) of Ammonia, Cyanide,
Phenol and TKN
sam les must be done in the field prior to preservation.***
Comments:
ljug#
Compositor #
UPS
Q Fed Ex
Are these results for regulatory purposes? Yes
No
Report results in:
mg/t
mg/kg ug/L
Wand Delivery
Relinquished by: Date; ®
T,un�e 1
Received by:
Dat Tim
�. -
Other
Reiinquis .by: 4D
/9rf
Time:, ���
Received by:
Date: Time:
Relinquished by' Date: Time:
R ceive La
a{e r -

Page 1
Contact: Brent Collins Report Date: 5/14/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 5/3/2019
Meritech Work Order # 05031902 Sample: Cooleemee WWTP 1 Grab 5/3/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.36 % 5/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 572 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D
Meritech Work Order # 05031903 Sample: Cooleemee WWTP 2 Grab 5/3/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.61 % 5/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 413 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D
Meritech Work Order # 05031904 Sample: Cooleemee WWTP 3 Grab 5/3/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 6.21 % 5/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 439 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D _
Meritech Work Order # 05031905 Sample: Cooleemee WWTP 4 Grab 5/3/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 7.17 % 5/6/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 380 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D
Meritech Work Order # 05031906 Sample: Cooleemee WWTP 5 Grab 5/3/19
Parameters Result Analysis _Date Reporting Limit Method
% Total Solids 5.13 % 5/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 709 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Page 2
Contact: Brent Collins Report Date: 5/14/2019
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 5/3/2019
Meritech Work Order # OSQ31907 Sample: Cooleemee WWTP 6 Grab 5/3/19
Parameters Result Analysis Date Reporting limit Method
% Total Solids 7.00 % 5/6/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 649 col/g dry wt 5/3/19 130 col/g dry wt SM 9222D
Meritech Work Order # 05031908 Sample: Cooleemee WWTP 7 Grab 5/3/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
6.98 %
5/6/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
260 col/g dry wt
5/3/19
130 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. jW'- J9
Laboratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

:ors
Chain of Custody Record (COC)
NPpES#: ...
.......... a..........i................................ a................................ ....................................................... ...............
Client: '• EMA Resources Inc. Phone: -336-751-1441
Address:�................................................................................—s.
's755 Yadkinville Rd Fax: :[phone]
--Mocksville NC 27028 Email: brent.coilins erni«5ourcesinc.com
.......•••--•----..............._.---.............._.......--.... ......--- �...m.......x.y......... 7.... x.y..-.-.w,.M.:.,...a.........
Project:642
.........................................................................._
............-- -...-_..................................._....................._............. P.Q.#:
Attention: Brent Collins Turn Around Time*
-- work nee or ova
How would you like your report sentwww.mer? *Rusty k needs prior approval.
Circle all that apply: ail preferred) , Fax, Mail 5�s) aas s 1�s
MERITECI;� C.
ENVIRONMENTAL LABORATORIES
...........................................................................................................
Al
Tamco Rd. Phone: [phone]i .............
Reidsville INC 27320 Fax: [phone]
.................. ..... ..... ............ ..... .............................................. .. ......... ........
Email: [e-mail]
... •..............................._...................._...............................................................
$h° C
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample rvsof
Lab Use Only
Start
End
Grab?Cont.
Test(s) Required
on Ice?
Yes / No
pH OK?
CI OK?
Date
Time
Date
Time
��pp
e0l ee�?�e.
VJ 'rP I
�31��1
a
eca (rfE,4e%
3
Temperature Upon
Receipt:
s
Method of
Shipment:
*** Dechlorination <0.5 m) of Ammonia, Cyanide,
Phenol and TKN sam les must be done in the field priorto preservation.***
Comments:
:.................... :..................... :....................
:............. ............ ........... ........... ..
Compositor#
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
No ❑
Report results in: mg/I_ ❑
mg/kg
ug/L ❑
❑ Hand Delivery
Relinquished by: pa
Time: J Oda
Received by:
gate:
Time:
❑ Other
..........................
Relinquished by: Date:
Time:
Receiv d�y:
Date:
Time:
.....
Relinquished by: Date:
Time:
Receive
t
Tin-@: cj,,4,
i ,
J

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 04/09/2019
Reported: 04/ 11 /2019
For: Cooleemee
Comments:
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190409-26-01
30 Day Benchscale
Eff
% EPA625-R-92/0
190409-26-02
% Volatile Solids
IN
0.71
% SM2540G
190409-26-02
Percent Solids
IN
0.99
% SM2540B-2011
190409-26-03
% Volatile Solids
OUT
2.25
% SM2540G
190409-26-03
Percent Solids
OUT
5.67
% SM2540B-2011
Respectfully submitted,
(0P,'W/Ou j-"� I
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
04/10/2019 WC
04/10/2019 WC
04/10/2019 WC
04/10/2019 WC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

Client: c
STATF.SVILLF,ANALYTICAI.
Address:
/Q ( K2f: ✓ZCCe
O fi�
122 Court Street P.O. Box 228
Statesville.NC 28687
"ockW r C
G
-7b .X
(7tMl872-4697
Contact Person: Phone
#
FAX#
Chain of
Custody Record
PO # J �� ' Requisitioned by: (Time Date)
Customer
Sample IN
La 4D M
Time Sampled
(Grab Onty)
Date Sampled
(Grab Only)
M
Matrix
Parameters requested for analysis
s—
w
wry
Caoc'r'C-A+ e w
► OU 41
,
o
Coec"* ec- w r
CC r
S
6jR !E2
C-ctCcnw wwf
(: ���R^1
!,
✓
oc
t�E SoLr�S
c�c«,tic Wry,
. 0
�t
� 9
✓
o �
tc - rSoc —
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date _/_!_
Time end am, pm Date _/_/_
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date
Time 5�.30 0>pm Date
(� �'
Time -{ am, pm Date-VI-7 / �
Time am, pm Date _/_/_
Time am, pm Date _/_/_
Lab Comments:
Sampled by: RV t
Transported by:�p t
Holding times met:
Compliance work:
Non-compliance work:
i
rn
04
[V O
r- (V
00
O d
n
n
00
1.0
00
(V
z
ai
00
(V
CV
X
O
m
0
d

Volatile Solids IN 0.71
%Total Solids IN 0.99
Fractional Volatile Solids IN 0.717
Volatile Solids OUT 2.25
Total Solids OUT 5.67
Fractional Volatile Solids OUT 0.397
Volatile Solids
As a decimal
Volatile Solids In 0.717
Volatile Solids Out 0.397
Volatile Solids Reduction 1 74.1

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 04/17/2019
Reported: 04/22/2019
For: Davie Co Cooleemee WWTP
Comments:
STATESVILLE
C ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190417-37-01
% Volatile Solids
Dig In
0.39
%
SM2540G
04/18/2019
CL
190417-37-01
Percent Solids
Dig In
0.64
%
SM2540B-2011
04/17/2019
CL
190417-37-02
% Volatile Solids
Dig Out
2.18
%
SM2540G
04/18/2019
CL
190417-37-02
Percent Solids
Dig Out
4.71
%
SM2540B-2011
04/17/2019
CL
Respectfully submitted,
�0P --WVG j '
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Condition of Receipt
Sample Number 190417-37-01 Temp on Arrival: 3.4
Parameter Schedule: Percent Solids
Parameter Schedule:
Sample Number 190417-37-02 Temp on Arrival: 3.4
Parameter Schedule:
Received on Ice
Received on Ice
Received on Ice
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

O
00
0
x
N
N
00
to
rt
Sv
r�
z
n
N
00
0)
00
Client: /1 -50 s
G J
STATESVII.LEANALYTICAL
Address:
122 Court Street P.O. Box Z8
Statesville, NC 28687
A /
[phone]
Contact Person:
Phone # jqge,?67_11/9¢( FAX#
[
Chain of
Custody Record
PO #=C /W�� Requisitioned by: (rime Dale)
L.D
Customer
Sample ON
LabI #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
Matrix
Pararequested for analysis
s
w
ww
L'aoCC�5'latEi' s,
: O l �4
o vG i CCU csoG
Ii
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date /_/_
Time end am, pm Date --//
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date
a p Date U-1 Sampled by: #yr,(
Time �VZS an(','� Date Transported by �
Time am, pm Date _/_/_ Holding times met:
Time am, pm Date �!/_
Compliance work:
Non-compliance work:
Lab Comments: Samples Transported On Ice:
Initials:

Volatile Solids IN 0.39
%Total Solids IN 0.64
Fractional Volatile Solids IN 0.609
Volatile Solids OUT 2.18
Total Solids OUT 4.71
Fractional Volatile Solids OUT 0.463
Volatile Solids
As a decimal
Volatile Solids In 0.609
Volatile Solids Out 0.463
Volatile Solids Reduction 1 44.8

EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date:
Reported:
For:
Comments:
Analytical Results
04/24/2019
04/25/2019
Davie County
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190424-17-01
% Volatile Solids
IN
0.65
% SM2540G
04/24/2019
WC
190424-17-01
Percent Solids
IN
0.76
% SM2540B-2011
04/24/2019
WC
190424-17-02
% Volatile Solids
OUT
2.24
% SM2540G
04/24/2019
WC
190424-17-02
Percent Solids
OUT
4.47
% SM2540B-2011
04/24/2019
WC
Respectfully submitted,
�0P --WVG j '
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 3

Condition of Receipt
Sample Number 190424-17-01 Temp on Arrival: 3.3
Parameter Schedule:
Parameter Schedule:
Sample Number 190424-17-02 Temp on Arrival: 3.3
Parameter Schedule:
Parameter Schedule:
Received on Ice
Received on Ice
Received on Ice
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 3

O
00
0
x
N
N
00
V)
sv
rt
rl)
r�
z
n
N
00
rn
00
v
Client: �vS �1s�fC
STATESVILLE ANALYTICAL
122 Court Street P.O. Box 228
Statesville, NC 28ti8787
Address: !S
J
[phone]
Contact Person: Phone #
FAX#
Chain of
Custody Record
PO # ✓t r Requisitioned by: (rime Dale)
Customer
Sample ID#
Lab_IO
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
m
o
S".
Matrix
w
ww
Parameters requested for analysis
44a,ww
1�,��
O"_1_ G5F_ Sow S
Coo a
'7: Q W
Relinquished by: Time IQS am, m Date ' w /L( Sampled by: tby:a
P r � r
Received by: Time p � am, pm Date 7 Zil j Transported �02.
Relinquished by: Time am, pm Date _/—/� Holding times met:
Received by: Time am, pm Date _/ J—
Compliance work:
Composite Sampling #1:
Time begin am, pm Date _/_/_ _ Non-compliance work:
Time end am, pm Date _
Lab Comments: Samples Transported On Ice:
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date _/_/_ Initials:

Volatile Solids IN 0.65
%Total Solids IN 0.76
Fractional Volatile Solids IN 0.855
Volatile Solids OUT 2.24
Total Solids OUT 4.47
Fractional Volatile Solids OUT 0.501
Volatile Solids
As a decimal
Volatile Solids In 0.855
Volatile Solids Out 0.501
Volatile Solids Reduction 1 83.0

Meritech, Inc.
Environmental. Laboratory
Laboratory Certification No, 165
Contact: $rent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Report Date: 5/14/2019
Mocksville, NC 27028 Date Sample Rcvd: 5/3/2019
Meritech Work Order # 05031909 Sample: Davie County VS In Composite 5/3/19
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
0.79 %
5/7/19
0-100 %
SM 2540E
% Volatile Solids
0.47 %
5/7/19
0-100 %
SM 2540E
Meritech Work Order #
05031910
Sample: Davie County VS Out Composite
5/3/19
Parameters
Result
Analysis Date
Reporting Limit
Method
%Total Solids
5.55 %
5/7/19
0-100 %
SM 2540B
% Volatile Solids
2.31 %
5/7/19
0-100 %
SM 2540E
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#-,
........... . ........ . . ................ -.1 ...... ..... .... .............................. ..................... ....................... . ................... . ... ...........
Client EMA Resources Inc. Phone: -336-751-1441
.......... ........ . ................... .. ................................. .......... ...... . ............... . ..... . ............ ....................
Address: -755 Yadkinville Rd Fax: -336-751-1442
--- ......... . ..... ...................................... . .................... .. .................. ......................... ........ . ......... ...................
.Mocksvi li.e NC 27028
............ —.1 ...................................... .............................. .. . .......
Project:
............ . .......... ................................. . .. . ............................... .................... . ..... ......... .... . ...................
............ ...... .............. . .............. ........ ........... ....... P.O.#:
Attention: Brent Collins Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
............... ..................... . .........................................................
Circle all that apply: ma preferred) Fax, Mail S S) 48 Hrs
tn—
MERITECH., INC.
....................... . .................... . ..................... ................................ --------
ENVIRONMENTAL LABORATORIES
'N. ....................... . ...... ............. . ........................................................ . ....
... �12mco Rd. Phone: [phone]
---------------- -- ............... . .................... ....................
Reidsville NC 27320 Fax.- 336-342-1522
....................... . ..................... .......................... .. ....... . .......... ...
Email: [e-mail]
..... . ........ . ................... . .................................. . ............... ...... ­­_­ ........................................
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print):::
Lab Use Only
Start
End
comp?
Grab?
Cont.On
ont
Test(s) Required
Ice?
Yes No
pH OK?
CI OK?
Date
Time
Date
Time
V5 zv
543!17
r-*8.
Vo a e le -50/' C/-C li
VS OV
T 04�
Vf
Temperature Upon
Receipt: lj
Method of
Shipment:
Dechlo rination (Z.S pprn),of Ammonia, Cyanide, Phenol and TKN sarnRles
must be done in the field priorto preservation.
Comments:
L .............. ................................................. Z _...4 ............
............................. ............. ........................................... .......................
Compositor #
Jug #
El UPS
El Fed Ex
Are these results for regulatory purposes? Yes No ❑
Report results in: mg/L ❑ mg/kg S"' ug/L ❑
❑ Hand Delivery
Relinquished by: Dat— 10, rime:
Flo - 0000-n
Received by: Date: Time:
Aeceyejs Date: Time:
0 Other
.................I............
Relinquished by: Date: Time:
Relinquished by: Date: Time:
/i) 7T11 TI-q:
Rec y Lab A-<�

Volatile Solids IN 0.47
%Total Solids IN 0.79
Fractional Volatile Solids IN 0.595
Volatile Solids OUT 2.31
Total Solids OUT 5.55
Fractional Volatile Solids OUT 0.416
Volatile Solids
As a decimal
Volatile Solids In 0.595
Volatile Solids Out 0.416
Volatile Solids Reduction 1 51.5

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY19-SL032178
C'°°'"T°"F�a� Predictive
Client:
Roger Spillman
Advisor:
Brent Collins
PO Box 378
EMA Resources Inc
Soil Report
Mehlich-3 Extraction
Cooleemee, NC 27014
755 Yadkinville Rd
b
Mocksville, NC 27028
Sampled County: Davie
Fo Links to Helpful Information
Sampled: Not Provided
Received: 05/15/2019
Farm: NC-DV-08
Completed: 05/24/2019
Client ID: 411288
Advisor ID: 405413
Sample ID: 00004
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M
0.0 180-220 110
110 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dnfl:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.51 1.00 6.2 81 1.2 6.0
15 52 48 29
36 312 204
175
175
35 0.1 2
Sample ID: 00005
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Sudan/Sorghum silage
0.0 180-220 70
130 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.22 1.03 14.6 91 1.3 6.4
33 36 57 33
48 1075 656
431
431
180 0.1 1
Sample ID: 00006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Sudan/Sorghum silage
0.0 180-220 40
130 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dnfl:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP
SS -I NO3-N
0.18 1.01 16.7 94 1.1 6.4
50 33 56 36
32 659 406
431
431
125 0.1 1
North Carolina
x
AL
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL032178
Roger Spillman
Page 2 of 3
Sample ID: 00007
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0
120-200 100
40
0
0
pH$
0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.22 0.97 15.2
95 0.8 6.6 17 48
64 30
37
558
343
384
384
182 0.1
1
Sample ID: 00008
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 120
90
0
0
0
0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.32 1.04 7.7
89 0.9 6.3 10 26
61 26
35
1396
850
115
115
104 0.1
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY19-SL030864
CU)-ToegPredictive
Client:
Herbert Dooley
Advisor:
Brent Collins
�C,
241 Parker Rd
EMA Resources Inc
Soil Report
Mehlich-3 Extraction
Mocksville, NC 27028
755 Yadkinville Rd
b
Mocksville, NC 27028
Sampled County: Davie
F� x7- Links to Helpful Information
Sampled: Not Provided
Received: 04/26/2019
Farm: DV12
Completed: 05/08/2019
Client ID: 442169
Advisor ID: 405413
Sample ID: 00001
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M
0.5 120-200 70
70 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.51 1.03 7.9 80 1.6 5.7
29 36 55 23
51 796 495
154
154
176 0.1 1
Sample ID: 00002
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M
0.0 120-200 60
60 0 0
0
0
0 0
Note: 12
2 -
0.0
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.56 0.99 10.3 86 1.4 6.0
34 41 58 26
37 316 207
304
304
218 0.1 1
North Carolina
x
AL
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

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►4CCOLJNTihFO cos'Y No.113 8 8 9
0 SOUTHERN STATES
DAVIE FARM SERVICE, INC.
PHONE. [phone] P.D. BOX 911 MOCKSVILLE, NC 27028
FEED • SEEDS . FERTILIZERS . FARM CHEMICALS . FARM & GARDEN SUPPLIES
DATE ON ACCOUNTS OVER 30 DAYS 01-0 A 1.112°I, PER MONTH SERVICE CHARGE
,iorE S ED. %ANNUALLY. MIN. $1.00 PER MONTH,
------------- ----------------------------------------
CUSTOMER
PLEASE --- - - --- ---- -- ---- - ------------------------------ PRODUCER
PRINT
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CGOLEEWUL, INC 27oi4
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17 17 - 17
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FIEC EIVED BY
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Alt clalm ..d -wmd jpad& MUST be 6WOmpaied by IRIS W.

AMOUNTING COPY No. 96400
fn SOUTHERN FATES
DAVIE FARM SERVICE, INC.
PHONE: �336j 751-5021 P.O. BOX 911 MOCKSVILLE, NC 27028
F
I—iVA
•SEE•FERTILIZERS • FARM CHEMICALS • FARM & GARDEN SUPPLIES
GATE ON ACCOUNTS OVER 30 DAYS OLD A 1.112% PER MONTH SERVICE CHARGE
WILL BE ADDED. 18% ANNUALLY. MIN. $1.00 PER MONTH.
- ------ _ _ CUSTOMER NP.
PRINT �C --------�----------- J--------�+- . P#iOC3UCER❑
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CLERK [ PXD I CHARGE I ON
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