WQ0003035_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0003035
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0003035
Applicant\Permittee * SYNAGRO
Facility Name * City of Eden
Phone Number*
4434899026
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for City of Eden
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
EDEN NC 2019 Annual Report FINAL.pdf 22.77MB
Upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020

435 Williams Court, Suite 100
Baltimore, MD 21220
�V�v�u synagro. com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0003035
Dear NCDEQ:
■
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Eden, NC.
If you have any questions or need additional information, please do not hesitate to contact
Melinda Ward at [phone] ext. 130 or Ryan Copeland at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Melinda Ward — City of Eden
Ryan Copeland — Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF EDEN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003035
2019 ANNUAL REPORT

City of Eden, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms & Metals Field
Loading Summary Forms
4. TCLP Analyses
5. Pathogen ReductionlVector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00003035 County Rockingham Year 2019
Facility Name (as shown on permit) Mebane Bridge WWTP NPDES No. NCO023841
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 76
Total number of fields utilized for land application during the year: 10
Total amount of dry tons applied during the year for all application sites: 450.42
Total number of acres utilized for Iand application during the year: 120,60
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items
I-13 below) issued by the Division of Water Quality YES X NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and time was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15.A NCAC 02T .1105 (a) or the Pollutant Loading
Rates in 15ANCAC 02T .I105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
II. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Melinda Ward, WWTP Superintendent
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
✓ ''Y ff,,
V �-1 do
Signature of Permittee Date
r r o d PDate
(if different from ei . r�per)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006:)

SYNAGRO
February 11, 2020
REFERENCE: EXPLINATION OF NON -COMPLIANT ANNUAL REPORT OF
PERMIT 4 WQ0003.035 City of Eden
On behalf of the City of Eden, Synagro is submitting an explanation of why the 2019
annual report is marked non -compliant.
In this annual report you will find 4 Nutrient & Metals Analysis however the 4" quarter
sample is dated 1/16/20. This is due to the original 4th quarter sample being lost in shipment to
the lab. When the mistake was realized a new sample was pulled and sent in for analysis. Due
to wet weather an unsuitable spreading conditions the storage pad had an abundance of older
material. When retaking this sample, I consulted with the belt press operator and he showed
me which material was made during the 4 h quarter of 2019. Even though this sample was
pulled in 20201 feel that it is a strong representation of the material produced in the 4' quarter
of 2019.
If you have any further questions, please contact me at [phone] or
rcopeland@synap,ro.com
Sincerely,
Ryan Copeland
Technical Services Specialist
Synagro
284 Boger Road, Mocksville, NC 27028 ® Phone: [phone] ® Fax: [phone]

2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
EDEN, NC
EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
DRY METRIC
MONTHNEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2019
720.00
W
125.28
D
113.63
April 2019
144.00
W
25.06
D
22.73
June 2019
84.00
W
15.20
D
13.79
July 2019
852.00
W
154,21
D
139.87
September 2019
360.00
W
87.11
D
79.01
November 2019
180.00
W
43.56
D
39.51
YEARLY TOTAL
2,340.00
W
450.42
D
408.54
1/30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: W00003035 Laboratory
Facility Name: EDEN, NC Waypoint Analytical Virginia Inc.
NPDES# : NCO023841 PACE ANALYTICAL SERVICE INC.
or WQ# (residual only)
WWTP Name: MEBANE BRIDGE WWTP
Residuals Analysis Data
Product Type AEDCAK AEDCAK AFDCAK AEDCAK
Date Sampled (grab) or 01/10/19 04/15/19 07/24/19 01/16/20
Date Composited
Percent Solids 17.40 18.10 24.20 17.60
PARAMETERS (mglkg dry weight)
Arsenic
12.3
13.8
13 . 1
12
Cadmium
3.7
2.71
3.05
3.81
Mercury
0.42
0.418
0.626
0.612
Chromium
NR
57.1
63.7
45
Copper
1720
1420
1620
1780
Lead
44.7
41.5
57.8
64.6
Molybdenum
16.3
12.3
13.7
12.6
Nickel
33.9
35.5
38.7
33.6
Selenium
11.1
8.19
10.8
9.49
Zinc
1150
1020
1230
1220
Total Phosphorus
17600
18300
20560
21700
TKN
30700
35900
26800
39500
Ammonia -Nitrogen
563
<100
1690
<562
Nitrate and Nitrite
<11.2
54.4
86.4
46.1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the Information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
M
(SIGNATURE OF PREPARER)
Date _12 !'
DENR FORM RSSF (5/2003) Printed: Wednesday - February 5 2020 at 13:23:53 for: 2013 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form
Permit Number WQ0003035 Laboratory
Facility Name EDEN, NC Waypoint Analytical Virginia Inc.
NPDES# NC0023841 PACE ANALYTICAL SERVICE INC.
or WQ# (residual only)
WWTP Name MEBANE BRIDGE WWTP
Residual Analysis Data
Product Type
AEDCAK
AEDCAK
AEDCAK
AEDCAK
Date Sampled
01/10/19
04/15/19
7/24/2019
1/16/2020
Date Composited
Percent Soilds
17.40
18.10
24.2
17.8
PARAMETERS (mg/kg dry weight)'
Aluminium
37900
39600
44900
46000
Calcium
8080
6880
6610
8030
Magnesium
2380
2400
2330
2840
pH
6.60
5.50
6.90
6.60
Potasium
2430
2280
1910
3320
Sodium
<1970
369
325
410
PAN
9334
10874
8464
12177
SAR
2.0588
0A139
0.4292
0.421
"l certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
X (J\�Q(, Date
(SIGNATCJRE OF PREPARER)
NR - Data Not Reported or Data Not Required Report Run Date:- 2/5/2020 1:49:05 PM

(�Iacmnalytical
www,pacelabs.com
January21, 2019
Nate Roth
Synagro Technologies Inc
284 Boger Rd
Mocksville, NC 27028
RE: Project: Eden
Pace Project No.: 92413584
Dear Nate Roth:
Pace Analytical Services, LLc
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen for
Lorri Patton
lorri,[e-mail]
1(828)254-7175
Project Manager
Enclosures
cc: Lysa Finnerty, Synagro
REPORT OF LABORATORY ANALYSIS
4Wo
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

_ aceAnalytical
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Project: Eden
Pace Project No.: 92413584
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 16

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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No,:
Eden
92413584
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92413584001
Edon 1 of 4
EPA 6010D
SH1
13
PASI-A
EPA 74718
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PAS I -A
SM 271OB-2011
EWS
1
PAS I -A
EPA 350.1 Rev 2.0 1993 Mod,
CJH1
1
PASI-A
EPA 351.2 Rev2.0 1993
MFO
1
PAS I -A
EPA353.2Rev 2.01993
MFO
3
PASI-A
EPA365.1 Rev 2.01993
MFO
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC, Page 3 of 16

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ANALYTICAL RESULTS
Pace Analytical Services, LLG
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Eden
Pace Project No.: 92413584
Sample: Eden 1 of 4
Lab ID: 92413584001 Collected:
01/10/19
11:30 Received: 01/10/19
12:38 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601OD Preparation Method: EPA 3050B
Aluminum
37900 mglkg
197
5 01/16/19 10:17
01/18/19 20:21
7429-90-5
Arsenic
12.3 mglkg
3.9
1 01/16/19 10:17
01/17/19 21:21
7440-38-2
Cadmium
3.7 mglkg
0.39
1 01/16/19 10:17
01/17/19 21:21
7440-43-9
Calcium
8080 mglkg
39.4
1 01/16/19 10:17
01/17/19 21:21
7440-70-2
Copper
1720 mglkg
2.0
1 01/16/19 10:17
01/17/19 21:21
7440-50-8
Lead
44.7 mglkg
2.0
1 01/16/19 10:17
01/17/19 21:21
7439-92-1
Magnesium
2380 mglkg
39.4
1 01/16/19 10:17
01/17/19 21:21
7439-95-4
Molybdenum
16.3 mglkg
2.0
1 01/16/19 10:17
01/17/19 21:21
7439-98-7
Nickel
33.9 mglkg
2.0
1 01/16/19 10:17
01/17/19 21:21
7440-02-0
Potassium
2430 mg/kg
1970
1 01/16/19 10:17
01/17/19 21:21
7440-09-7
Selenium
11.1 mg/kg
3.9
1 01/16/19 10:17
01/17/19 21:21
7782-49-2
Sodium
ND mglkg
1970
1 01/16/19 10:17
01/17/19 21:21
7440-23-5
Zinc
1150 mglkg
3.9
1 01/16/19 10:17
01/17/19 21:21
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation
Method: EPA 7471 B
Mercury
0.42 mg/kg
0,020
1 01/11/19 15:21
01/15/19 09:12
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
17.4 % 0.000010
1
01/11/19 16:09
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
82.6 %
0.10
1
01/11/1916:02
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
6.6 Std. Units
0.10
1
01/15/19 11:46
H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
PlantAvallable Nitrogen
9320 mg/kg
0.12
1
01/15/19 17:46
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0
1993 Mod.
Nitrogen, Ammonia
563 mglkg
39.4
1 0111211910:40
01112/1916:05
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
30700 mglkg
1200
5 01/14/19 11-34
01/15/19 06-03
7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mglkg
11.2
1 01/11/19 22:50
01/12/19 03:38
Nitrogen, Nitrate
ND mglkg
11.2
1 01/11/19 22:50
01/12/19 03:38
14797-55-8
Nitrogen, Nitrite
ND mglkg
5.6
1 01/11/19 22:50
01/12/19 03:38
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0
1993 Preparation Method: EPA 3651 Rev 2.0 1993
Phosphorus
17600 mglkg
282
50 01/14/1919:23
01/14/1923:27
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/21/2019 12:07 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 16

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QUALITY CONTROL DATA
Project: Eden
Pace Project No.: 92413584
QC Batch: 452021 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92413584001
METHOD BLANK: 2471568
Associated Lab Samples: 92413584001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2471669
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 01/1411915:21
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.083 0.070 84 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471570 2471571
MS MSD
92413583001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.46 2.7 2.6 2.5 2.7 76 86 75-125 7
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Eden
Pace Project No.: 92413584
QC Batch: 452712 Analysis Method: EPA 6010D
QC Batch Method: EPA 30508 Analysis Description: 6010 MET
Associated Lab Samples: 92413584001
METHOD BLANK: 2474452
Associated Lab Samples: 92413584001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Aluminum
mglkg
ND
10.0
01/17/19 20:52
Arsenic
mglkg
ND
1.0
01/17/19 20:52
Cadmium
mglkg
ND
0.10
01/17/19 20:52
Calcium
mglkg
ND
10.0
01/18/19 20:12
Copper
mglkg
ND
0.50
01/17/19 20:52
Lead
mglkg
ND
0.50
01/17/19 20:52
Magnesium
mg/kg
ND
10.0
01/17/19 20:52
Molybdenum
mglkg
ND
0.60
01/17/19 20:52
Nickel
mglkg
ND
0.50
01/17/19 20:52
Potassium
mglkg
ND
500
01/17/19 20:52
Selenium
mg/kg
ND
1.0
01/17/19 20:52
Sodium
mg/kg
ND
500
01/17/19 20:52
Zinc
mglkg
ND
1.0
01/17/19 20:52
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2474453
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mglkg
500
492
98
80-120
Arsenic
mg/kg
50
44.5
89
80-120
Cadmium
mglkg
50
46.2
92
80-120
Calcium
mg/kg
500
497
99
80-120
Copper
mg/kg
50
48.9
98
60-120
Lead
mg/kg
50
46.0
92
80-120
Magnesium
mg/kg
500
472
94
80-120
Molybdenum
mg/kg
50
50.0
100
80-120
Nickel
mg/kg
50
47.3
95
80-120
Potassium
mg/kg
500
ND
99
80-120
Selenium
mglkg
50
42.4
85
80-120
Sodium
mg/kg
500
488J
98
80-120
Zinc
mglkg
50
45.2
90
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2474454
MS
92413571001
Spike
Parameter Units
Result
Conc.
Aluminum mg/kg
9440
18500
Arsenic mglkg
ND
1850
Cadmium mg/kg
ND
1850
Pace Analytical Services, LLC
980o KinceyAve. Suite 100
Huntersville, NC 28076
[phone]
Qualifiers
2474455
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
17700
33800
31700
132
126
75-125
7 M1
1770
1660
1550
90
88
75-125
7
1770
1720
1620
93
91
75-125
6
Resuits presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /21 /2019 12:07 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

leAnalyticals
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Eden
Pace Project No.: 92413584
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2474454
2474455
MS
MSD
92413571001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Cone,
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
14800
18500
17700
33300
31000
100
92
75-125
7
Copper
mg/kg
289
1850
1770
2140
2000
100
97
75-125
7
Lead
mg/kg
ND
1850
1770
1740
1620
93
91
75-125
7
Magnesium
mg/kg
10100
18500
17700
28200
26200
98
91
75-126
7
Molybdenum
mg/kg
27.8
1850
1770
1890
1770
101
98
75-125
7
Nickel
mg/kg
24.3
1850
1770
1790
1680
96
94
75-125
6
Potassium
mglkg
ND
18500
17700
22400
20800
101
96
75-125
7
Selenium
mg/kg
ND
1850
1770
1580
1480
85
83
75-125
6
Sodium
mg/kg
ND
18500
17700
20200
18900
94
91
75-125
6
Zinc
mg/kg
869
1850
1770
2570
2400
92
87
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/21/2019 12:07 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

lCbAnalyfical
www.paeelabs,com
Project: Eden
Pace Project No.: 92413684
QC Batch: 452075
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92413584001
SAMPLE DUPLICATE: 2471918
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2471919
Parameter
Percent Moisture
Units
Units
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92413463001 Dup
Result Result RPD Qualifiers
19.8 20,0 1
92413803001 Dup
Result Result RPD Qualifiers
18.1 15.5 15
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit €s presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /21 /2019 12:07 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16

aceAnalyticat
wwwpacelabs.cam
QUALITY CONTROL DATA
Project: Eden
Pace Project No.: 92413584
QC Batch: 452172 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92413584001
SAMPLE DUPLICATE: 2472426
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2472427
Parameter
pH at 25 Degrees C
92413563001 Dup
Units Result Result
Std. Units 5.2 5.3
92413312001 Dup
Units Result Result
Std. Units 6.8 6.8
RPD Qualifiers
0 H3
RPD Qualifiers
0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvi€le, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01121 /2019 12:07 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16

aceAnalytical
mmpacelabs.com
QUALITY CONTROL DATA
Project: Eden
Pace Project No.: 92413584
QC Batch: 452023 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Hatch Method: EPA 350.1 Rev 2.0 1993 Mod, Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92413584001
METHOD BLANK: 2471582
Associated Lab Samples: 92413584001
Parameter Units
Nitrogen, Ammonia mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 8.9 01/12/19 15:09
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2471583
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 472 464 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471584 2471585
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Roc
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mglkg 13200 10300 10500 21800 22500 83 89 90-110 3 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2471586 2471587
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Roc % Rec Limits RPD Qua[
Nitrogen, Ammonia mg/kg ND 2320 2320 2210 2210 93 93 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shaft not be reproduced, except in full,
Date: 01/21/2019 12:07 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16

aceAnalytical
www,pacelabs.com
Project: Eden
Pace Project No.: 92413584
QC Batch: 452219
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92413584001
METHOD BLANK: 2472536
Associated Lab Samples: 92413584001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2472537
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Pace Analytica[ Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 2807E
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 01/15/19 04:45
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1000 967 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472538 2472539
MS MSD
92413357001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 62000 21200 19000 74700 74800 60 67 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2472540 2472541
MS MSD
92413358001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl,Total mg/kg 5230 5170 5170 8110 9500 56 83 90-110 16M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except to full,
Date: 01/21/2019 12:07 PM without the written consent of PaceAnaiytical Services, LLC. Page 11 of 16

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Eden
Pace Project No,: 92413584
QC Batch: 452122 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92413584001
METHOD BLANK: 2472244
Associated Lab Samples: 92413584001
Parameter Units
Nitrogen, Nitrate mglkg
Nitrogen, Nitrite mglkg
Nitrogen, NO2 plus NO3 mglkg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2,0 01/12/19 03:27
ND 0.99 01/12/19 03:27
ND 2.0 01/12/19 03:27
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2472245
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Nitrogen, Nitrate
mglkg
14.3
15.2 106 90-110
Nitrogen, Nitrite
mglkg
9.6
10.2 107 90-110
Nitrogen, NO2 plus NO3
mglkg
23.9
25.4 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2472246
2472247
MS
MSD
92413583001
Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mglkg
ND
522
529
374
401 72
76
90-110
7
Nitrogen, Nitrite
mg/kg
212
348
351
525
545 90
94
90-110
4
Nitrogen, NO2 plus NO3
mglkg
ND
870
880
899
946 99
103
90-110
5
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /21 /2019 12:07 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

IeAnalytical
Irwwpacelahs.com
QUALITY CONTROL DATA
Project: Eden
Pace Project No.: 92413584
QC Batch: 452341 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92413584001
METHOD BLANK: 2473119
Associated Lab Samples: 92413584001
Parameter Units
Phosphorus mglkg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 01/14/19 23:27
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hurtersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2473120
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mglkg 48.1 51.4 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2473121 2473122
MS MSD
92413583001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Phosphorus mglkg 2300 1580 1680 3650 3550 85 74 90-110 3 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /21 /2019 12:07 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16

IeAnalyt cal"
rrww.paGelabs.com
QUALIFIERS
Project: Eden
Pace Project No.: 92413584
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
Pace Analytical Services, LLC
9800 KirceyAve. Suite 100
Huntersville, NC 28078
[phone]
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyto is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenyiamine using Method 8270. The result reported for
each analyte is a combined concentration.
PaceAnalyt€cal is TNI accredited. Contact your Pace PM for the current Hst of accredited analytes.
TN€ - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditation slcertifications may apply. A
complete list of accreditationslcertifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall rat be reproduced, except in full,
Date: 01 /21/2019 12:07 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 16

Pace Analytical Services, LLC
® 9800 Kincey Ave. Suite 100
aceAnalyfrca! Huntersvllle, NC 28078
www.pacelabs.com (704)B75-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Eden
92413584
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92413584001
Eden 1
of 4
EPA 3050B
452712
EPA 601 OD
452810
92413584001
Eden 1
of 4
EPA 7471 B
452021
EPA 7471 B
452085
92413584001
Eden 1
of 4
SM 254OG-2011
452269
92413584001
Eden 1
of 4
ASTM D2974-87
452075
92413584001
Eden 1
of 4
EPA 9045D
452172
92413584001
Eden 1
of 4
SM 2710E-2011
452617
92413584001
Eden 1
of 4
EPA 350.1 Rev 2.0 1993
452023
EPA 350.1 Rev 2.0 1993
452144
Mod.
Mod,
92413584001
Eden 1
of 4
EPA 351.2 Rev 2.0 1993
452219
EPA 351.2 Rev 2.0 1993
452403
92413584001
Eden 1
of 4
EPA 353.2 Rev 2.0 1993
452122
EPA 353.2 Rev 2.0 1993
452124
92413584001
Eden 1
of 4
EPA 365.1 Rev 2.0 1993
452341
EPA 365.1 Rev 2.0 1993
452369
Date: 01/21/2019 12:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 16

CHAFE -OF -CUSTODY Analytical RegUest Document
u+a us�bN>y f(,cwarko ` "
ace,4nalytit;al'
W4# :
92413.584
Chainof-Custody is a LEGAL. DOCUMENT- Complete all relevent fiields"
Comp
Billing rnformatian:
Address:
Container Preservative TYR2l
92413384
RepoR To: _ g
Email To:
• Preservative Types: (2) n itnc add (21 sulfuric acid, (3) hyftchlnric add, (4) sodium hydroxide, (5) zinc acetatq
Co To-
pY -
Site Cgllection Inf%Address:
.16) methanul, (7) sodium bisulfate, (B)sod�um
thiosulfatn, (9) hexane, (A)ascnrhic acid, (Bl ammonium sulfate,
(C) ammonium
hydroxide, (o) TSP, (U) Unpresemed,
(D) Other
Customer Project Name/Number.
State: County/CLty: Time Zone Collected:
Analyses
Lab'Prof
yah Saatp7.e Receipt CheClclists -
Gustnr)y Sealsreseatllntaat iur`
Phone:
Email:
Site/Facility ID #: Compliance Monitoring?
yes [ ] ND
v
- •�
Y N
Litstodp $iyaatures P=eseat X N 2i�
Cn3lectnr sagaatare f�zeseat 3fli tiA
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Collected B jprintJ:
Purchase Order H: DW PWS ID #
Quote #:
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+
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`dflir
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DW Location Code:
L f ]
$r -:
SufTic}ea �"N ,NA
C ecte (s' ature]:
Tumaround Date Required: immedlate y Packed on Ice:
�7
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Sampled Rec�fved on ce �/2F 2IA
voa �eaasnace Acceptable Y N/^
Sample
Yes [ ] No
4)
�5� xega ater3 soils Y tq t#C
Samples in oldzag same �2'Ft Nii
is sal;
[ ) Dispose as appropriate 1 ] Return
Rush: Field Filtered (if applicable):
1 ] Same Day j ] Next Da Y L I Yes [] N n
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-itesxdual C;zYoza.ne 7hsesent " Y tr„Jr7+t�
t l steps:
l )Archive:
[ ]Hold:
L ] 2 Day I ] 3 Day I ] 4 Day [ ] 5 Day
AnaIYSLS:
c51
Sample pH;Aeeeptab3e �r n qra
(Expedite Charges Apply)
-7
Su fide Preser y
• Matrix Codes (Insert in Matrix box belovr): Drinkirig Water [DWI, Ground Water (GM, Wastewater (Vi1Wj,
.� '=
G
x-
ead Acetate straps
Product (P), Soil/Solid (SL}, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (81, Vapor (V), Other [OT)
I �: -
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* Comp/ Collected for Res # of Q
Matrix Grab Composite5tart) Composite End C)
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ab Sample ! comments
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Qate Time Date Time
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Customer Remarks / Special Conditions / Passible Hazards:
Date/Time, Received b mpany: (Signature)
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Date/Time: Received by/Comoanv: (SLenaturel
Date lime:
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Page: __/
0
f Pane 16 ol 16

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AERQB. 1110/2019 111/2019-413012019 2.0588
DIGESTED CAKE
Na mgll = (Na mg/kg x % Solids) + 100 = (1970 x 17,4000) + 100 = 342.78
Ca mgll = (Ca mg/kg x % Solids) � 100 = (8080 x 17.4000) 100 = 1405.92
Mg mgll = (mg mglkg x % Solids) : 100 = (2380 x 17.4000) + 100 = 414.12
Na meq = Na mgll + Molec.Wgt.Na = 342.78 + 23 = 14.9035
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1405.92 + 20 = 70.296
Mg meq = Mg mgll + Molec.Wgt.Mg = 414.12 + 12 = 34.51
SAR = Na meq ; SgrRoot[O.5 x (Ca meq + Mg meq)] = 14.9035 SgrRoot[0.5(70.296+34.51)] = 2.05878
Printed: 2/1/2020
Page 1 13:58

Waypoint"O
ANALYTICAL
4/25/2019
Synagro Central LLCI Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-107-0204
Project Description: Eden 2 of 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalvticai.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/1712019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p,,,,,. IV 6—dam
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 7

Waypoint,o
ANALYTICAL
Client: Synagro Central LLC/ Eden
Project: Eden 2 of 4
Lab Report Number: 19-107-0204
Date: 4/24/2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 65935
Analyte: Aluminum
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Arsenic
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the ana[yte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the Analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Selenium
QC Batch No: L432477
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L432519
MS/MSD Recovery failed, PDS confirmed matrix interference
Page 2 of 7

(2)
Waypoint. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-107-0204
Client Project Description: Eden 2 of 4
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
SM-4500-NH3C
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
9045D
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
4500NO3F-2011
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
6010D
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
SW-7471B
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
SM-4500-NH3C-TKN
WTN
65934
Eden WWTP
Solids
04/15/2019 12:35
04/17/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 3 of 7

Report Number: 19-107-0204
Account Number: 46452
Send To: Synagro Central LLC1 Eden
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65934
Sample Id : Eden WWTP
0
y�
Wa oint
ANALYTICAL
Project: Eden 2 of 4
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica Isom
Date Sampled: 411512019 12:35:00
Date Received: 04/17/2019 00:00
Date Reported: 04/25/2019
Total Solids *
18.10
181000
100.0
ADM
04/19/2019 15:34
Moisture *
81.90
100.0
ADM
04/19/2019 15:34
Total Kjeldahl Nitrogen
3.59
35900
250
JPJ
04/23/2019 10:00
Phosphorus
1.83
18300
50.0
BKN
04/23/2019 22:03
Potassium
0.23
2280
50.0
BKN
04/23/2019 22:03
Sulfur
0.49
4870
50.0
BKN
04/23/2019 22:03
Calcium
0.69
6880
250
BKN
04/23/2019 22:03
Magnesium
0.24
2400
50.0
BKN
04/23/2019 22:03
Sodium
0.04
369
250
BKN
04/23/2019 22:03
Iron
29200
50.0
BKN
04/23/2019 22:03
Aluminum
39600
50.0
BKN
04/23/2019 22:03
Manganese
1000
5.00
BKN
04/23/2019 22:03
Copper
1420
2.50
BKN
04/23/2019 22:03
Zinc
1020
12.5
BKN
04/23/2019 22:03
Ammonia Nitrogen
<0.01
<100
100
JPJ
04/21/2019 16:00
Organic N
3.59
35900
250
04/21/2019 16:00
Nitrate+Nitrite-N
54A
4.73
ZBD
04/24/201914:19
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
6010D
601 OD
601 OD
601 OD
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in bllank H - Beyond Holding Time
pwir-
P
oAl'rr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work, the results, or the company in any advertising; news release, or other public announcements without obtaining our prior written authorization_
Agronomist
Page 4 of 7

Report Number: 19-107-0204
Account Number: 46452
Send To: Synagro Central LLC/ Eden
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 65934
Sample Id : Eden WWTP
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH
Molybdenum
Comments:
s
41 Yp
Wa oint
ANALYTICAL
Project : Eden 2 of 4
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/15/2019 12:35:00
Date Received: 04/17/2019 00:00
Date Reported: 04/25/2019
2.71
1.00
BKN
04/23/2019 22:03
6010D
57.1
2.50
BKN
04/23/2019 22:03
6010D
35.5
2.50
BKN
04/23/2019 22:03
6010D
41.5
3.00
BKN
04/23/2019 22:03
601 OD
13.8
5.00
BKN
04/23/2019 22:03
6010D
0A18
0.0158
TJS
O4/23/2019 12:38
SW-7471 B
8.19
5.00
BKN
04/23/2019 22:03
6010D
5.5
JSL
04/23/2019 07:50
9045D
12.3
2.50
BKN
04/23/2019 22:03
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time pwic MC 1011rf
Our reports and fetters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising; news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 5 of 7

r
1 7621 Whitepine Road, Richmond, VA 23237
WayMain 804-743-9401 ° Fax [phone]
PA www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLCI Eden
Report Number: 19-107-0204
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
is Yes
0 No
Number of coolers received
0-9
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COG) present?
0 Yes
0 No
COC agrees with sample label(s)?
• Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
A[[ samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 NIA
High concentration container (48 hr) I- Low concentration
High concentration pre -weighed (methanol -14 d) F. Low conc
EnCore samplers (48 hr)
pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
g � � .....
Date &Time: 1712019 13.53:47
Signature: Brandi Watson
Page 6 of 7

m
0
V
SAMPLING LOG #
CRI
Svnclgl6CentrafLLC/Eden
CHAIN 0FCUST®®Y
CUSTOMER: S G" O'dAGRO
Eden 2Of4
0�2'-0204
72019
13:52:09
RECORD & ANALYSES
RECORD
PROJECT MANAGER.. �'"i�
1 �F
---- .
)roper field sampling procedures
f
W� — Li
��p O
were used during the collection of these samples.
Phone:(*)
iN _ur
A & iL CUSTOMER
LAS # SAMPLE I.D.
SAMPLING SAMPLE # OF
LOCATI®N E
SAMPLEl3
SAMPLING
METHOD METHOD
E0
CONTAINERS
5 SLjP
DATE TIME
PRESERVED SHIPPED
1135
Relinquished by Sampler: Date
Time Recieved b Y:
REMARKS:
Relinquished by:
Date
� PS
Time Recieved by:
Relinquished by:
I to
Ll 1
Time Rived by;
SPECIAL INSTRUCTIONS:
—�
{ 57ATE)
monitoring purposes.
PO#:
SAMPLE
ANALYSIS REQUEST
I.O SLI SL2 NH -N N® -N Organic
¢ a Cd cr Ni
Pb A5 R9 $e
CaCO ""a". Mo
PHequlv3
LO GA)
Solids CI NO2-N
W u3-y , ! 0 1-ow
PO PO ;0w ;00w pw
pow por J�w pw
SLI. Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2. Basic Test SL1 plus Sufrur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 4115/2019 51112019-713112019 0.4139
DIGESTED CAKE
Na mgll = (Na mg/kg x % Solids) + 100 = (369 x 18.1000) + 100 = 66.789
Ca mg/l = (Ca mg/kg x % Solids) + 100 = (6880 x 18.1000) + 100 = 1245.28
Mg mgll = (mg mglkg x % Solids) + 100 = (2400 x 18.1000) + 100 = 434.4
Na meq = Na mgll + Molec.Wgt.Na = 66.789 + 23 = 2,90387
Ca meq = Ca mgll + Moloc.Wgt.Ca = 1245.28 + 20 = 62.264
Mg meq - Mg mg/l + Molec.Wgt.Mg = 434.4 + 12 = 36.2
SAR = Na meq .: SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.90387 + SgrRoot[0.5(62.264+36.2)] = 0.41386
Printed: 2/1/2020
Page 1 13:58

Waypointo
ANALYTICAL
8/14/2019
Synagro Central LLCI Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 19-207-0004
Project Description: Eden N & M
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/5/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam- P 6-7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

(D
Waypoint, 76�1 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-207-0004
Client Project Description: Eden N & M
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
67549
Eden N
& M
Solids
07/24/2019
14:45
08/05/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
SM-4500-NN3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471 B
WTN
SM-4500-NN3C-TKN
WTN
SM-254OG
WTN
Page 2 of 6

Report Number: 19-207-0004
Account Number: 46452
Send To: Synagro Central LLC/ Eden
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 67549
Sample Id : Eden N & M
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
24.20
75.80
2.68
2.05
0.19
0.50
0.66
0.23
0.03
0.17
2.51
Waypointa (D
ANALYTICAL
26800
20500
1910
4990
6610
2330
325
29300
44900
1030
1620
1230
1690
25110
86.4
Project : Eden N & M
REPORT OFANALYSIS
250
50.0
50.0
50.0
250
50.0
250
50.0
50.0
5.00
2,50
12.5
100
250
4.70
ADM
ADM
JPJ
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
BKN
JPJ
ZBD
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 7/24/2019 14:45:00
Date Received: 08/05/2019 00:00
Date Reported: 08/14/2019
07/30/2019 15:06
07/30/2019 15:06
08/09/2019 11:30
08/01/2019 12:22
08/01/2019 12:22
08/01/2019 12:22
08/01/2019 12:22
08/01/2019 12:22
08/01/2019 12:22
08/01 /2019 1222
08/01/2019 12:22
08/01 /2019 12:22
08101 /2019 12:22
08/01 /2019 12:22
08/13/2019 12:00
08/09/2019 11:30
08/12/2019 15:09
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Cur reports and fetters are for the exclusive and conhdentiai use of our clients; and may not be reproduced in whole or part, nor may any reference be made
to the work, the resuits, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
SM-254OG
SM-2540G
SM-4500-NH3C-TKN
6010D
601OD
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
?W�a #1C V 011
Pauric McGroary
Agronomist
Page 3 of 6

Report Number: 19-207-0004
Account Number: 46452
Send To: Synagro Central LLCI Eden
Mary Brewer
284 Boger Road
Mocksville , NC 27028
Lab Number: 67549
Sample Id : Eden N & M
Waypoint,(b
ANALYTICAL
Project. Eden N & M
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytital.corn
Date Sampled: 7/24/2019 14:45:00
Date Received: 08/05/2019 00:00
Date Reported: 08/14/2019
Cadmium
3,05
1.00
BKN
08/01/201912:22
6010D
Chromium
63.7
2.50
BKN
08/011201912:22
6010D
Nickel
38.7
2.50
BKN
08/011201912:22
6010D
Lead
57.8
3.00
BKN
08/011201912:22
6010D
Arsenic
13.1
5.00
BKN
08/01/201912:22
6010D
Mercury
0.626
0.0142
TJS
08106/2019141-10
SW-7471B
Selenium
10.8
5.00
BKN
08101/201912:22
6010D
pH *
6.9
JSL
08/12/2019 07:57
9045D
Molybdenum
13.7
2.50
BKN
08/01/201912:22
601OD
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series
is on a wet basis.
B - Analyte detected in blank
H - Beyond holding time
� �
01C 1QOI4r
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work. the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Agronomist
Page 4 of 6

Waypoint,o
7621 Whltepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax $04-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLCI Eden
Report Number: 19-207-0004
Shipping Method
0 Fed Ex 0 US Postal (D Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
• NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 NIA
F_ High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: `'`MaiyAmend Date & Time: 08/05/2019 12:41:34
Page 5 of 6

SAMPLING LOG # INC. Clf�/aIN OF CUSTODY
111�11 III1IIIIIIIIIIII1IIII lllllll�llHlllHll 1111111 p�2� fl°g RECORD & ANALYSIS
CUSTOMER: SYNAGRO RECORD
Svnaera Central LLC! Eden ip�gF,.p4 _
EOEriI N&M
PROJECT MANAGEFI:. wN _- `"�'E: L t the proper fief sampling procedur$s
daring fho of these samples.
Phone:
�co�flection
SAMPLER
A & L CUSTOMER
LAB # SAMPLE I.D.
SAMPLING
LOCATION
SAMPLE
TYPE
*OF SAMPLING METHOD METHOD
CONTAINERS GATE TIME
PRESERVED SHIPPED
e0raj M
s5 �-
"SL/uw
'1`4/,y Wq5 �cc cX�OLGz
UPS
Relinquished by Sampler:
CopetArj0
Date
7125/+q
Time
Recieved by: REMARKS:
f =00
Relinquished by:
Date
Time
Recieved by:
Relinquished by:
Dale
'eta
Time
Reciev d by,
SPECIAL INS�TRUCT(ONS:
For E `�
�
monitoring purposes_
p0#
SAMPLE
ANALYSIS REQUEST
I.D. SLI SL2
NH4-N Nog-N Orgattls Cd
N
Cr NI
Pb
As H Se CaCoa Volatile
N
° PH equiv. Solids M❑ CI NOz1000
SLi: Total Solids (Moisture), Total Kjeldahl nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 7/24/2019 811I2019-12131I2019 0.4292
DIGESTED CAKE
Na mgll = (Na mg/kg x % Solids) =- 100 = (325 x 24.2000) + 100 = 78.65
Ca mg/l - (Ca mg/kg x % Solids) + 100 = (6610 x 24.2000) + 100 = 1599.62
Mg mg/1 = (mg mglkg x % Solids) + 100 = (2330 x 24.2000) -- 100 = 563.86
Na meq = Na mg1l + Molec.Wgt.Na = 78.65 + 23 = 3,41957
Ca meq = Ca mgll � Molec.Wgt.Ca = 1599,62 + 20 = 79.981
Mg meq = Mg mgll + Molec.Wgt.Mg = 563.86 + 12 = 46.9883
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.41957 + SgrRoot[0.5(79.981+46.9883)] = 0.429177
Printed: 2/1/2020
Page 1 13:58

Waypointo
ANALYTICAL
1/27/2020
Synagro Central LLC/ Eden
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 20-017-0004
Project Description: Eden 19
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/1712020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pam. tv &"r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page I of 6

Waypoint(D
ANALYTICAL
Report Number: 20-017-0004
Client Project Description: Eden 19
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
7D199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
SM-4500-1\11-13C
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
9045D
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
4500NO3F-2011
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2D20
6010D
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
SW-7471B
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
SM-4500-NH3C-TKN
WP MTN
70199
Eden 19
Solids
01/16/2020 11:51
01/17/2020
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

Waypoi t.G
ANALYTICAL
46452
Synagro Central LLC/ Eden Ryan
Mary Brewer Project Eden 19
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Submitted By: Ryan
Report Number : 20-017-0004 RL°POR)rOFANAIYSIS
Lab No : 70199
Sample ID : Eden 19
Report Date : 01/27/2020
Received : 01/17/2020
pau«G pr 6& r c/
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 111612020 11:51
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
82.2
%
0.010
1
01/22/2016:23
ADM
SM-254OG
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
<562
mg/Kg - dry
562
1
01/24/20 13:30
JPJ
SM-4500-NH3C
Nitrate Nitrite-N
46.1
mg/Kg - dry
27.1
1
01/24/20 13:36
ZBD
4500NO3F-2011
Organic N
39500
mg/Kg - dry
1400
1
01/24/20 10:00
CALCULATION
pH
6.6
S.U.
1
01/23/20 05:46
JSL
9045D
Total Solids
17.8
%
0.010
1
01/22/20 16:23
ADM
SM-2540G
Total Kjeldahl Nitrogen
39500
mg/Kg - dry
1400
1
01/24/20 10:00
JPJ iM-4500-NH3C-TKP
Phosphorus
21700
mg/Kg - dry
28.1
1
01/22/20 23:58
JTR
6010D
Aluminum
46000
mg/Kg - dry
28.1
1
01/22/20 23:58
JTR
6010D
Arsenic
12.0
mg/Kg - dry
2.81
1
01/22/20 23:58
JTR
6010D
Calcium
8030
mg/Kg - dry
140
1
01/22/20 23:58
JTR
6010D
Cadmium
3.81
mg/Kg - dry
0.562
1
01/22/20 23:58
JTR
6010D
Chromium
45.0
mg/Kg - dry
1,40
1
01/22/20 23:58
JTR
6010D
Copper
1780
mg/Kg - dry
1.40
1
01/22/20 23:58
JTR
601DD
Iron
27200
mg/Kg - dry
28.1
1
01/22/20 23:58
KKM
6010D
Lead
64.6
mg/Kg - dry
1.69
1
01/22/20 23:58
JTR
6010D
Magnesium
2840
mg/Kg - dry
28.1
1
01/22/20 23:58
JTR
6010D
Manganese
815
mg/Kg - dry
2.81
1
01/22/20 23:58
JTR
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 6

•
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401
° Fax [phone]
ANALYTICAL.
www.waypointanalytical.com
46452
Synagro Central LLC/ Eden
Ryan
Mary Brewer
Project
Eden 19
Report Date: 01/27/2020
284 Boger Road
Information :
Received : 01/17/2020
Mocksville , NC 27028
Pam« r (f��`'�
Submitted By : Ryan
P ry
Report Number : 20-017-0004
ALYSIS
REPORT OF AN
n
Agronomist
Lab No : 70199
Matrix: Solids
Sample ID : Eden 19
Sampled: 1/16/2020 11:51
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Mercury
0.612
mg/Kg - dry
0.0853
1 01/22/20 14:09 TJS SW-7471B
Molybdenum
12.6
mg/Kg - dry
1.40
1 01/22/20 23:58 JTR 6010D
Mickel
33.6
mg/Kg - dry
1.40
1 01/22/20 23:58 JTR 6010D
Potassium
3320
mg/Kg - dry
28.1
1 01/22/20 23:58 JTR 6010D
Selenium
9.49
mg/Kg - dry
2.81
1 01/22/20 23:58 JTR 6010D
Sodium
410
mg/Kg - dry
140
1 01/22/20 23:58 JTR 6010D
Zinc
1220
mg/Kg - dry
7,02
1 01/22/20 23:58 JTR 6010D
Sulfur
5730
mg/Kg - dry
28.1
1 01/22/20 23:58 JTR 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

Waypoint.(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-4401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46452
Customer Name: Synagro Central LLCI Eden
Report Number: 20-017-0004
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
• Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
,, Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COG) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
• Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
• NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 NIA
F- High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F- Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 49 No
Comments:
Signature: Brandi Watson Date & Time
Page 5 of 6
1 / 17/2020 11:21:14

SAMPLING LOG #
PROJECTMANAGER: Kw\j Cc*ahw
Phone:..
MLA&Ll
7621 Wt
Rlchmor
I111111I1111111l14111I1Ill E11113111111111111111111111I11117-0004
as32°
Svpj�aTc Central LLC,' Eden
Eden 19
A & L CUSTOMER SAMPLING SAMPLE # OF
LAB # SAMPLE LD. LOCATION TYPE CONTAINERS
Relinquished by Sampler: Date Time Recleved by:
Q
�
Relinquished by: Date Time R d by:
11�-1��
OF CUSTODY
! & ANALYSIS
ECO RD
1 attest that the proper fleld sampling procedures
were used daring the collection of these samples.
E YAQ QQA9 LAAD
SAMPLES
SAMPLING METHOD METHOD
DATE TIME PRESERVED SHIPPED
UPS
Relinquished by: I DAte Time Rbcleved 13y:
SPECIAL INSTRUCTIONS: �:-;-fLI L1I A--Ia�tL�
For
C, monitoring purposes. PO#:
SAMPLE
I.D.
r
1 C(
REMARKS:
ANALYSIS REQUEST
5L1
SI_2
NH4-N
NOS-N
()MMlc
Cd
Cr
NI
Pb
As
fig
Se
H
CaC v.
e uiv
Solids Volatile
Mo
Cl
M02 N
100
J000
A000,
100or
k;o
1,00r
1000,
1000
rO
SLI: Total Solids (Moisture), Total lgeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 1/16/2020 1 ! - 1 ! 0.4210
DIGESTED CAKE
Na mgll = (Na mg/kg x % Solids) + 100 = (410 x 17.8000) + 100 = 72.98
Ca mg1l = (Ca mg/kg x % Solids) + 100 = (8030 x 17.8000) + 100 = 1429.34
Mg mgll = (mg mg/kg x % Solids) � 100 = (2840 x 17,8000) + 100 = 505.52
Na meq = Na mgll + Molec.Wgt.Na = 72.98 _ 23 = 3.17304
Ca meq = Ca mg/l + Molec.Wgt.Ca = 1429.34 + 20 = 71.467
Mg meq = Mg mgll + Molec.Wgt.Mg = 505.52 + 12 = 42A267
SAR = Na meq + SgrRoct[0.5 x (Ca meq + Mg meq)] = 3,17304 + SgrRoot[0.5(71.467+42.1267)] = 0.421031
Printed: 2/5/2020
Page 1 13:12

SECTION 3

FACILITY NAME: EDEN,NC
OWNER: GRAY TUTTLE
SITE #: NC RC 00011 FIELD# : RC 00011 0001
RESIDUAL SOURCES): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLOVER
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 32.58
OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.00 ACRES PERMITTED: 9.00
Page: I
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
nation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(PP-)
Crop
Total
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/19/19
120,00 (W)
13.333
18.10
2.413
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0,30
35,900. p
100,00 p
54.40 p
10874
FESCUE HAY
7/20/19
60.00 (W)
6.6671
18.10
1.207
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE HAY
Jul-19
1 180.00 (W)
20.000
i'otal Gallons/Ac:
Total Wet Tons/Ac: 20.00
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 79
0.100 0.020 0,413 10.281 0.300 0.003 0.089 0.257 0.059 7.385 132.49
Cumulative lbs/acre 0.472 0.146 5.164 129,337 4.451 0.054 0.754 4.059 0.235 46.652
Permit PAN Limit (lbs/acre) 1st Cropl2nd Crop
3
146
,
FD Cumulative Pollutant Loading Rate Limit (Ibslacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
EDNIBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
�1Z-YT
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR —Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (.Annual): 32.58
Permit #: W Q000203 5
Operator: Gray Tuttle Owner:
Acres Used: 9 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Gray Tuttle Predominant Soil Series:
Clover
Site #: NC RC 00011 Field #: RC 00011 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
I 1 I
4/15/19
L2]3
j4
5
6
7
8]
L9J
LOJ
11 J
12
% Solids
18.1
Arsenic
13.8
Cadmium
2.71
Copper
1420
Chromium
57.1
Lead
41.5
Mercury
0.418
Molyb-
denum
12.3
Nickel
35.5
Selenium
8.19
Zinc
1020
Total
Phos-
horus
18300
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
I 1
2
3
4
5
6
7
8
9
1 D
11
12
DT/Ac./
App.
goy,
Event
3.62
Arsenic
0.100
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000 1
0.100
Cadmium
0.020
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.020
Copper
10.281
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.281
Chromium
0.413
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.413
Lead
0.300
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.300
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.089
denum
Nickel
0.257
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.257
Selenium
0.059
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.059
Zinc
7.385 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
7.385
Total
Phos-
132,492
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
132.492
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for ,submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�NN�) (fiw�Np
Signature of Land Applier
.1 Z9 In
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN,NC
OWNER: GRAY TUTTLE
SITE #: NC RC 00011 FIELD# : RC 00011 0002
RESIDUAL SOLRCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLOVER
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 28.24
OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.80 ACRES PERMITTED: 17.80
Page : 1
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Toth
DATE or
Solids
.Per
Residual
Dry; Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
I Per Acre
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/16/19
156.00 (W)
8,7641
I8.10
1.586
EDMB,F
DRY
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54,40 p
FESCUE PASTURE
Jul-19
156.00 (W)
8.764
1
T10874
Total Gallons/Ac:
Total Wet Tons/Ac: 8.76
Total Cubic Yds/Ac: 0.00
TOTALS:
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 34
0.044 0.009 0.181 4.505 0.132 0.001 0.039 0.113 0.026 3.236 58.06
Cumulative lbs/acre
0.548 0.164 7.235 192,509 5.713 0.073 0.987 6.999 0.279 53.315
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
'
90
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
2679
15.0
375.0
89.0
2500.0 i
'r
EDMBAEDC — EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAVE
E
i
A v
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p W pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit th
WQ000203 5
Eden, NC
Operator: Gray Tuttle Owner:
Acres Used: 17.8 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Gray Tuttle Predominant Soil Series
17.8 Site 4: NC RC 00011 Field 9
28.24
Clover
RC 00011 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
4/15/19
2
3
4
5
6
7
8
9
10
11
12
% Solids
18.1
Arsenic
13.8
Cadmium
2.71
Copper
1420
Clu-omium
57.1.
Lead
41.5
Mercury
0.418
Molyb-
denum
12.3
Nickel
35.5
Selenium
8.19
Zinc
1020
Total
Phos-
horus
18300
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1I
2
3
4
5
fi
7
8]
L9J
10
11
12
DT/Ao./
o
App
rt
Event
1.59
Arsenic
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Cadmium
0.009
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.009
Copper
4.504
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.504
Chromium
0.181
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.181
Lead
0.132
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.132
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
denum
Nickel
0.113
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Selenium
0.026
0.000
0.000
0.000
0.000
0.000
0M00
0.000
0.000
0.000
0.000
0.000
0.026
Zinc
3.235
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
3.235
Total
Phos-
58,448
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
58.048
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�N WVWM
Signature of Land Applier
,z- j zq a)
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN,NC
OWNER: GRAY TUTTLE
SITE #: NC RC 00011 FIELD# ; RC 00011 0006
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLOVER
PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 58.64
OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60
Page! I
Lime Applied ***
Date
LbsVAc
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
o�o
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
MI
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(PP-)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/17/19
9
16.552
18.10
2.996
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE EIAY
7/18119
72
6.207
18.10
1.123
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
35,400. p
100.00 p
54.4D p
10874
FESCUE HAY
7/19/19
60
:324:0:0](WW))
5A72
18,10
0.936
EDMBAE
MOIST
0-<I/2"
SUR
0.5
0.30
35,900.p
100.00 p
54.4D p
10874
FESCUE HAY
Jul-19
27.931
Total Gallons/Ac:
Total Wet Tons/AG: 27.93
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.140 0.027 0.577 14.358 0.420 0.004 0.124 0.359 0.083 10.313 185.03 110
Cumulative Ibs/acre 0 451 0.183 2.862 98.445 2.433 0.035 0.475 1.553 0.281 57.954
Permit PAN Limit (lbslacre) I st Crop/2nd Crop
r
I46
t
s
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
r
x d — CCII 2 Z
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation LO
Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (Annual): 58.64
Permit #:
Operator:
Acres Used:
WQ0002035
Gray Tuttle
Cation Exchange Capacity (non 503 only):
Owner: Gray Tuttle Predominant Soil Series:
Clover
11.6 Acres Permitted: 11.6 Site #: NC RC 00011 Field #: RC 00011 0006
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
L J
4/15/19
L2]3
4
5
6 j7
8
9
10
11
12
% Solids
18.1
Arsenic
13.8
Cadiniuml
2.71
Copper
1420
Chromium
57.1
Lead
41.5
Mercury
0.418
Molyb-
denum
12.3
Nickel
35,5
Selenium
8.19
Zinc
1020
Total
Phos-
horus
18300
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
11
L2]3
4
5
6
7
8
L9J
11
12
DT/Ac./
rt
App.
Event
5.06
Arsenic
0.140
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.140
Cadmium
0.027
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.027
Copper
14.356
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.356
Chromium
0.577
0M00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.577
Lead
0.420
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.600
0.000
0.420
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
1\4olyb-
0124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.124
denum
Nickel
0.359
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.359
Selenium
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Zinc
10.312
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
10.312
Total
Phos-
185.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
185.013
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Y6V A
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: CLAUDE FRENCH
SITE ff: NC RC 00026 FIELD# : RC 00026 0001 B
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FRD2
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 85.61
OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.10 ACRES PERMITTED: 20.10
Page: I
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip,
Past 24
Appli-
cation
Method
Vola-
tili-
nation
Miner -
ali-
nation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
Acre
Source
Moist
IIours
*
Rate**
Rate
Nitrite
3/18/19
156.00 (W)
7.761
17.40
1.350
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
11.20 p
9334
FESCUE PASTURE
3/19/19
156.00 (W)
7.761
17.40
1.350
EDMBAE
DRY
0-<112"
SUR
0.5
0.30
30,700. p
563.00 p
11.20 p
9334
FESCUE PASTURE
3/20/19
180.00 (W)
8.955
17A0
1.558
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
11.20 p
9334
FESCUE PASTURE
Mar-19
492.00 (W)
24.477
-i otal Nations/Ac:
Total Wet Tons/Ac: 24.48
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.105 0.032 NR 14.651 0.381 0.004 0.139 0.289 0.095 9.796 149,92 80
Cumulative Ibs/acre 0.968 0.344 8.568 232.350 7.271 0.080 1.298 6.146 0.501 94.924
Permit PAN Limit (lbslacre) 1st Crop/2nd Crop
,
115
35
h z
s
..71
i
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15 0
375.0
89.0
2500 0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
x�L� Z
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SUR1N - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (Annual): 85.61
Permit #:
Operator:
Acres Used:
WQ0002035 Cation Exchange Capacity (non 503 only):
Claude French Owner: Claude French Predominant Soil Series:
20.1 Acres Permitted:
Clover
20.1 Site #: NC RC 00026 Field #: RC 00026 0001B
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
1/10/19
L2]3
4
5
6
7
8
9
10
1l
12
% Solids
17.4
Arsenic
12.3
Cadmium
3.7
Copper
1720
Chromium
0
Lead
44.7
Mercury
0.42
Molyb-
denum
16.3
Nickel
33.9
Selenium
11.1
Zinc
1150
Total
Phos-
horus
17600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
11
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./ay,
App.
Event
4.26
'
Arsenic
0.105
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.105
Cadmium
0,032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.032
Copper
14.648
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.648
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.381
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.381
Mercury
0.004
0.000
0.000
0M00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.139
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.139
denum
Nickel
0.289
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.289
Selenium
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.095
Zinc
9.793
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
1 9.793
Total
Phos-
149.882
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
149.882
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
,J w uftlemon -
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: CLAUDE FRENCH
SITE #: NC RC 00026 FIELD# : RC 00026 0002 A
RESIDUAL SOURCE(S): See list at bottom of report
LfNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 46.46
OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.50 ACRES PERMITTED: 6.50
Page: I
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Voia-
Miner -
%
Tons
Cond.
Precip,
cation
till-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICK
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
9/25/19
72,00 (Vi)
11.0771
24.20
2.691
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
FESCUE MAY
Sep-19
72.00 (W)
11.077
11/6/19
60.00 (W)
9.231
24.20
2.234
EDMBAE
MOIST
"0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
( FESCUE HAY
11/22/19
60.00 (W)
9.2311
24.20
2.234
EDMBAE
MOIST
110-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
FESCUE HAY
Nov-19
120.00 (W)
18.462
L
Total Gallons/Ac:
Total Wet Tons/Ac: 29.54
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN
Annual lbs/acre 0.187 0.044 0.911 23.161 0.826 0.009 0.196 0.553 0.154 17.585 293.08 121
Cumulative lbs/acre 0.556 0.209 4,143 103.830 3.459 0.043 0.612 2.264 0.335 56.838
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
'
2 04
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0 i
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
x ev
Lill, _.
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injecticn/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (Annual): 46.46
Permit #:
Operator:
Acres Used:
WQ0002035
Claude French Owner:
Cation Exchange Capacity (non 503 only):
Claude French Predominant Soil Series: Clifford
6.5 Acres Permitted: 6.5 Site th NC RC 00026 Field 9: RC 00026 0002A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample or
Com-
posite
Date
1 11
7/24/19
2
3
4
5
6
7
8
9
10
11
12
% Solids
24.2
Arsenic
13.1
Cadn-dum
3.05
Copper
1620
Chromium
63.7
Lead
57.8
Mercury
0.626
Molyb-
denum
13.7
Nickel
38.7
Selenium
10.8
Zinc
1230
Total
Phos-
horus
20500
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
I 1 I
L2]3
4
5
6
7
8
9
10
11
12
r-3
DT/AcJ
¢
App .
14
Event
7.15
Arsenic
0.187
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.187
Cadmium
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Copper
23.163
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
23.163
Chromium
0.911
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0911
Lead
0.926
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.826
Mercury
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.196
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.196
denum
Nickel
0.553
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.553
Selenium
0.154
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.154
Zinc
17.587
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 17.587
Total
Phos-
293.109
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
293.109
11oruS
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
fV 4� ('vee-Gw)
Signature of Land Applier
4-Lv ho
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: CLAUDE FRENCH
SITE #: NC RC 00026 FIELD# : RC 00026 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 11.62
OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.90 ACRES PERMITTED: 11,90
Page: 1
Lime Applied
***
Date
LbslAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pptn)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
11/23/19
48.00 (W)
4.034
24.20
0.976
EDMBAE
DRY
"0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
FESCUE HAY
Nov-19
48.00 (W)
4.034
1
1
Total Gallons/Ac:
Total Wet Tons/Ac: 4.03
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.026 0.006 0.I24 3.163 0.113 0.001 0,027 0.076 0.021 2.401 40.02 17
Cumulative lbs/acre 0.441 0.197 4.011 96,816 3.084 0.042 0,580 1.922 0.229 48.157
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
2 09
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
I339.0
267.9
15.0 F
375.0
89.0
2500.0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB, DIGESTED CAKE
_(Uzt� 2%�412
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Eden, NC
WQ0002035
Claude French Owner:
11.9 Acres Permitted:
Total Dry Tons Applied (Annual): 11.62
Cation Exchange Capacity (non 503 only):
Claude French Predominant Soil Series: Clifford
11.9 Site #: NC RC 00026 Field #: RC 00026 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #i):
Sample or
Com-
posite
Date
1 11
7/24/19
L2]3
j4
5
6
7
8
9
10
11
12
% Solids
24.2
Arsenic
13.1
Cadmium
3.05
Copper
1620
Chromium
63.7
Lead
57.8
Mercury
0.626
Molyb-
denum
13.7
Nickel
38.7
Selenium
10.8
Zinc
1230
Total
Phos-
horus
20500
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
11
L 2-1
3
4
5
6
7
8
9
10
11
12
DT/Ac. /
c
App.
4
Event
0.98
Arsenic
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.026
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
3.162
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.162
Cliromiurn
0.124
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.124
Lead
0.113
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,027
denum
Nickel
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
Selenium
0.021
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Zinc
2.401
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
1 2,401
Total
Phos-
40,016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
40.016
horus
"l certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
cAr,4
Signature of Land Applier
-zZq bu
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME : EDEN, NC
OWNER: CLAUDE FRENCH
SITE #: NC RC 00026 FIELD# : RC 00026 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIFS: CLIFFORD
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 72.60
OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503):
ACRES.UTILIZED: 9.30 ACRES PERMITTED7 9.30
Page
Lune Applied ***
Date
Lb,/A,
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Tots
IMONTH Per Acre
➢ATE or
Solids
Per
Residual
Dry, Wet,
Past24
Method
zation
nation
TIN
Nitrogen
and
(Pp-)
Crop
Acre
Source
Moist
hours
Rate**
Rate
Nitrite
9/12/19
36.00 (W)
3.871
24.20
0,937
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
26,800, p
1,690.00 p
86.40 p
8464
FESCUE HAY
9/13/19
84.00 (W)
9.032
24.20
2.186
EDMBA.E
MOIST
0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
96.40 p
8464
FESCUE HAY
9/16/19
36.00 (W)
3.871
24.20
0.937
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
96.40 p
8464
FESCUE HAY
9/17/I9
12.00 (W)
L290
24.20
0.312
EDMBAE
DRY
0-<V2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
FESCUE HAY
9/19/19
24.00 (W)
2,581
24.20
0.625
EDMMAE
DRY
0-<1/2"
SUR
0.5
0.30
26,800.p
1,690.00 p
96.40 p
8464
FESCUE HAY
9/20/19
24.00 (W)
2.581
24.20
0.625
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
26,800. p
1,690.00 p
86.40 p
8464
FESCUE HAY
9/23/19
72.00 (W)
7.742
24.20
1.874
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
26,800. p
1,690,00 p
86.40 p
8464
FESCUE HAY
288.00 (W)
30.968
LSep-19
12.00 (W)
1.290124.20
0.312
EDM13AE
MOIST
"0QI2"
SUR
05
030
26SOOp
1,6110.00 p
86.40 p
8464
FESCUE HAY
12.00 (W)
1.290

FACILITY NAME: EDEN, NC
OWNER: CLAUDE FRENCH
SITE #: NC RC 00026 FIELD# : RC 00026 0005
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 72.60
OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.30 ACRES PERMITTED: 9.30
Page: 2
Lime Applied ***
Date
LbslAc
Gallons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
'Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
nation
TI{N
Nitrogen
and
(pp-)
Crop
MONTH
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
IUL� VWJVIIZI �L,
Total Wet Tons/Ac: 32.26
Total Cubic Yds/Ac: p,Op
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.205 0.048 0.995 25.293 0.902 0.010 0.214 0.604 0.169 19.204 320.06 132
Cumulative lbs/acre 0.520 0.167 3.477 88.277 2.844 0.030 0.682 1,956 0.324 47.652
Permit PAN Limit (Ibs/acre) 1st Cropl2nd Crop
209
FD Cumulative Pollutant Loading Rate Limit (lhslacre)
36.6
34.8
"
1339.0
267.9
15,0
375.0
89.0
2500.0 E
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
°I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mgNg ** Volatilization Rate: Surface 0.5, InjectionAncorporation LO
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation See Site pH & Lime Application. Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Eden, NC
WQ0002035
Claude French Owner:
9.3 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Claude French Predominant Soil Series:
9.3 Site #: NC RC 00026 Field #;
72.60
Clifford
RC 00026 0005
Residual Analvsis Data (Heavy Metals and Total Phosphorus use ma/kfa, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
7/24/ 19
L2J3
4
5
6
7
a
9
10 j
11
12
% Solids
24.2
Arsenic
13.1
Cadmium
3.05
Copper
1620
Chromium
63.7
Lead
57.8
Mercury
0.626
Molyb-
denum
13.7
Nickel
38.7
Selenium
10.8
Zinc
1230
Total
Phos-
horus
20500
Annual Heavv Metal Field Loadino (Calculated in lbs/acre):
Total
11
L2J3
4
5
5
7
8
9
D
11
12
DT/Ac./
App.
Event
7.81
'
Arsenic
0.205
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.205
Cadmium
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Copper
25.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
25.298
Chromium
0.995
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.995
Lead
0903
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.903
Mercury
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
0.214
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.214
denum
Nickel
0.604
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.604
Selenium
0.169
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.169
Zinc
19.208 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
19.208
Total
Phos-
320.128
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
320.128
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
VRO 0,pNA
Signature of Land Applier
W. � zv
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: BARRY KNIGHT
SITE #: NC RC 00105 FIELD# : RC 00105 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : CLOVER
PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 23.89
OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 13.40 ACRES PERMITTED: 13.40
Page: I
Lime Applied 4*4
Date
LWAc
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons {WT) (specify)
"a
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
MONTH
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
7/2/19
48.00 (W)
3.582
18,10
0.649
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE PASTURE
7/3/19
24.00 (W)
1.791
18.10
0.324
F,DMBAE
DRY
0-11/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE PASTURE
7/10/19
60,00 (W)
4.478
18.10
0.810
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE PASTURE
Jul-19
1 132.00 M
9.851
1
Total Gallons/Ac:
Total Wet Tons/Ac: 9.85
Total Cubic Yds/Ac: 0,00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 39
0,049 0.010 0.204 5.064 0.148 0.001 0.044 0.127 0.029 3.637 65.26
Cumulative lbs/acre 0.657 0.330 5.790 138.522 5.750 0.137 1.058 4.171 0.526 82.640
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
] 09
1
FD Cumulative Pollutant Loading Rate Limit Obs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR, Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/incorporation 1.0
* Application Mcthod: SUR - Surface, fNJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (Annual): 23.89
Permit #: WQ0002035
Cation Exchange Capacity (non 503 only):
Operator: Barry K'nigth Owner: Barry Knight Predominant Soil Series:
Acres Used: 13.4 Acres Permitted: 13.4 Site #: NC RC 00105 Field #:
Clover
RC 00105 0003
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
4/15/19
L2]
L3
L4
5
6
7
8
9
10
11
12
% Solids
18.1
Arsenic
13.8
Cadmium
2.71
Copper
1420
Chromium
57.1
Lead
41.5
Mercury
0.418
Molyb-
denum
12.3
Nickel
35.5
Selenium
8.19
Zinc
1 1020
Total
Phos-
horus
18300
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1
2
3
4
5
6
7
8 1
1911fl
11
12
DT/Ac./
rt
App-
Event
1.78
Arsenic
0.049
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
1 0.000
0.049
Cadmium
0.010
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.010
Copper
5.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.061
Chromium
0.204
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.204
Lead
0.148
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.148
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
denum
Nickel
0.127
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.127
Selenium
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Zinc
3.635
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 3.635
Total
Phos-
65.221
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
65.221
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zjz� /'u
Signature of Laird Applier
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: BARRY KNIGHT
SITE #: NC RC 00105 FIELD# : RC 00105 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLOVER
PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 26.06
OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED; 5.60 ACRES PERMITTED: 5.60
Page: I
Lime Applied ***
Date
LbsVAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Preeip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
6/29/19
84.00 (W)
15.000
18.10
2.715
EDMBAE
WET
0-<1/2"
SUR
0.5
0.30
35,900, p
100.00 p
54.40 p
I0874
FESCUE HAY
Jun-19
84.00 (W)
15.000
7/1/19
60.00 (W)
10.7141
18.10
1.939
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
35,900. p
100.00 p
54.40 p
10874
FESCUE HAY
Ju1-19
60.00 (W)
10.714
Total Gallons/Ac:
Total Wet Tons/AC: 25.71
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.128 0.025 0.532 13.218 0.386 0.004 0.115 0.330 0.076 9.495 170.35 101
Cumulative lbs/acre 0.763 0.271 5.775 146510 4.832 0.076 0.931 3.175 0A70 80.447 3
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
..............
, } r
146
1
.e.. .. ��
3 L
..:.. .,... ..
......
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
$9.0
2500.0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
X fS-` 17i \% (0` � ���Z,�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA — Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injeetion/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
WQ000203 5
Eden, NC
Operator: Barry Knight Owner:
Acres Used: 5.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Barry Knight Predominant Soil Series:
5.6 Site th NC RC 00105 Field #:
26.06
Clover
RC 00105 0004
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
I 1
4/15/19
2
3
4
5
6
7
&
9
10
11 J
12
% Solids
18.1
Arsenic
13.8
Cadmium
2.71
Copper
1420
Chromium
57.1
Lead
41.5
Mercury
0.418
Molyb-
den um
12.3
Nickel
35.5
Selenium
8.19
Zinc
1020
Total
Phos-
horus
18300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
LIJ
2
3
4 J
L5]6
7
8
9
10
11
12
DT/Ac./
App-
Event
4.65
Arsenic
0.128
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.128
Cadmium
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Copper
13.217
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
13.217
Chromium
0.531
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.531
Lead
0.386
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.386
Mercury
0.004
0.000
0.000
0.000
0M00
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.114
denum
Nickel
0.330
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.330
Selenium
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
Zinc
9.494
0.000
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
9.494
Total
Phos-
170.336
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
170,336
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
K�c y
Signature of Land AppIier
Z- 2 Zr�
Date
DENR FORM MFLSF (12/2006)

FACILITY NAME: EDEN, NC
OWNER: CHARLES O'BRYANT, JR.
SITE #: NC RC 00117 FIELD# : RC 00117 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 64.73
OPERATOR: CHARLES O'BRYANT, JR. CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.40 ACRES PERMITTED: 15.40
Page: I
Lime Applied
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
nation
TIN
Nitrogen
and
(PP-)
Crop
MONTH
Total
I Per Acre
Solids
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
3/28/19
84.00 (W)
5.455
17.40
0.949
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700.p
563.00 p
11,20 p
9334
FESCUE PASTURE
3/29/19
72.00 (W)
4.675
17.40
0.814
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
I L20 p
9334
FESCUE PASTURE
3/30/19
72.00 (W)
4.675
17.40
0.814
EDMBAE
MOIST
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
I L20 p
9334
FESCUE PASTURE
Mar-19
1 228.00 (W)
14.805
4/3/19
24.00 (W)
1.558
17.40
0.271
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700.p
563.00 p
11.20 p
9334
FESCUE PASTURE
4/4/19
36.00 (W)
2.338
17.40
0.407
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
1 11.20 p
9334
FESCUE PASTURE
4/11/19
84.00 (W)
5A55
17.40
0.949
EDMBAE
DRY
0-<1/2"
SUR
0.5
0.30
30,700. p
563.00 p
11.20 p
9334
FESCUE PASTURE
Apr-19
144.00 (W)
9.351
Total Gallons/Ac:
Total Wet Tons/Ac: 24.16
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.103 0.031 NR 14.459 0.376 0.004 0.137 0.285 0.093 9.667 147.95 78
Cumulative lbs/acre 0.768 0.501 5.860 166.704 9.013 0.179 L540 6.615 0,688 117 947
Permit PAN Limit (ibs/acre) 1st Crop/2nd Crop
.. . ...... . . .. .
110
FD Cumulative Pollutant Loading Rate Limit (lbsiacre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE
T
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Eden, NC Total Dry Tons Applied (Annual):
Permit #: WQ0002035 Cation Exchange Capacity (non 503 only):
Operator: Charles O'Bryant, Jr. Owner: Charles O'Bryant, Jr. Predominant Soil Series:
64.73
Clifford
Acres Used: 15.4 Acres Permitted: 15.4 Site #: NC RC 00117 Field #: RC 00117 0001
Residual Analvsis Data (Heavv Metals and Total Phosphorus use me/ka, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 11
1/10/19
L2]3
44
5
6
7
8
9 j10
11
12
% Solids
17.4
Arsenic
12.3
Cadmium
3.7
Copper
1720
Chromium
0
Lead
44.7
Mercury
0.42
Molyb-
denum
16.3
Nickel
33.9
Selenium
11.1
Zinc
1150
Total
Phos-
horus
17600
Annual Heavv Metal Field Loadinas (Calculated in lbs/acre):
Total
I 1 I
L2
4 J
5
6
L 7
L 8
L9J
LOJ
11 J
12
y
DT/Ac./
0
App.
Event
4.20
'
Arsenic
0.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
1 0.000
0.103
Cadmium
0.031
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0,000
0.031
Copper
14.462
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.462
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.376
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.376
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.137
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.137
denum
Nickel
0.285
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.285
Selenium
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Zinc
9.669
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
9.669
Total
Phos-
147.981
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
147.981
horus
"l certify, under penalty of law, that this document was prepares under my direction or supervision in accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
�/Ly `Zo
Date
DENR FORM MFLSF (12/2006)

SECTION 4

trill
lERV1f10Nf61rzNtAL T lit`�Ql.C1 l�$, thin;
AnafyNCM Lab6r,00669
October 01, 2019
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Eden
Dear Ryan Copeland:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX, [phone]
Website: httn://rvww.settelc.co7n
Order No.: 19090845
Summit Environmental Technologies, Inc. received 1 sample(s) on 9/12/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
�w W,.
A
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88.0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E97688, Georgia E87688, Idaho 01400923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania Q10, Rhodo Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OR00923201 1- 1, Virginia VELAP 9456, Washington C891
Page 1 of 39

UMMIT �`�"m'�zitEnvironnzentcrl Technologies, Inc. Case Narrative
S3310 Win St.
EMVNIOFJMENTA.L 1FM9INC31.C,fiGirs, 1NC Cuyahoga Falls, Ohio 44223 WO#: 19090845
rn kmiiyNoal Laboralorj6s TEL: [phone] FAX [phone]
Mehsite: httpJ/wivw.settek.conz Date: 10/1/2019
CLIENT: Synagro
Project: Eden
WorkOrder Narrative:
19090845: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies,_ Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19090845-001A TCLP-SVOC 8270E: Surrogate outside recovery limits. Minimum method criterion of
one surrogate within established recovery limits was met.
19090845-001a TCLP-SVOC-CPest(8081B): CCV exhibited high biased recoveries for several
analytes; associated sample results are N.D.
19090845-001A TCLP-SVOC-Herb_TCLP(8321): Sample exhibited outlying recovery of Surrogate:
DCAA.
Original
Page 2 of 39

MMIT
Sunnnit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
€NVIRQNWNTAL TLCHN01 G71:53, INC Cuyahoga Falls, Ohio 442� WO#: 19090845
Arralyff cal .Laboralanos TEL: [phone] FA: (330) 253-445
Data: 10/1/2019
Website: htts://www.settek.co
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution,
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
x The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
BIMB+ The analyte was detected in the associated blank,
G The ICB or CCB contained reportable amounts of analyte.
QC-1+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCSILCSD RPD was outside of accepted recovery limits.
QM-1+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-1+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits,
Z Deviation; A deviation from the method was performed, PIease refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL,
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLv1
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE,
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration BIank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 39

Sauazmit Environmental Technologies, Inc. WOrkOrder
SUMMIEF 3310 Win St.
ENVIRONMENTAL T��litt�l i�c�i��, iNr Cuyahoga Falls, Ohio 44223 Sample Summary
A.nafyfEcal tabaralarle'e TEL: [phone] FAX..- [phone] WO#: 19090845
Website: Mtn://ivivw.settek.coni 01-Oct-19
CLIENT: Synagro
Project: Eden
Lab Samplel[D Client Sample Ill Tag No Date Collected Date Received Matrix
19090845-001 Eden 9/11/2019 12:30:00 PM 9/12/2019 10:10:00 AM Sludge
Page 4 of 39

�' Summit Environmental Technologies, Inc. DATES REPORT
SUM3310 Win St.
EN-VIrtONmVNTAL Tr--cnrtot awes, ws Cuyahoga Falls, Ohio 44223
WO#: 19090845
Aua?Ocal Laboratarias TEL: [phone] FAX.- [phone] y
Website: hM:Ilwww.,Fettek.com 01-Oct-19
Client:
Proj ect:
Synagro
Eden
Sample ID
Client Sample ID
Collection Date Matrix Test Name Leachate Date Prep Date
Analysis Date
19090845-OOIA
Eden
9/11/2019 12:30:00 PM Sludge Flashpoint Detennination (1010)
9/27/2019 10:35:45 AM
Paint Filter Free Liquids Test (SW-846
9/17/2019 10:35:00 AM
9095)
pH (SW9045D)
9/26/2019 10:48:00 AM
Reactive Cyanide (90I4/7.3.3.2)-Solid
9/18/2019 5:17:00 PM
Reactive Sulfide (9034)/7.3.4.2
9/18/2019 5:I7:00 PM
SVOC SW-846: 8321 Herbicides-TCL
9/25/2919 11.12:00 AM
TCLP Mercury Analysis (SWI311/7479/15/2019 5:00:00 PM 9/17/2019 11:03:00 A 9/17/2019 4:24:00 PM
TCLP Metals Analysis (SW1311/6010'9/15/2019 5:00:00 PM 9/16/2019 1:45:00 PM 9/17/2019 3:51:55 PM
TCLP Pesticides Analysis (SW1311/8(9/15/2019 5.00:00 PM 9/18I2019 11:30:41 A 9/25/2019 9:49.00 AM
ER
TCLP Semi-Volatiles Analysis 9/15/2019 5:00:00 PM 9/16/2019 9:02:00 AM 9/18/2019 4:27:00 AM
(SW1311/8270)
TCLP Volatiles Analysis 9/15/20I9 5:00:00 PM 9/19/2019 5:45:00 PM
TCLP Volatiles Analysis 9/15/2019 5:00:00 PM 9/16/2019 4:08:00 PM
Original
Page 5 of 39

SUMM111
s207nnit Environmental Technologies, Inc.
3310 97in 51.
Analytical Report
EAt6�IltOtJMI M7Al t GliCdi7ti} ;{i$, ;�'
Cuyahoga Falls, Ohio 44223
(base report)
. mffyflcaf Lah6ratar6as TEL: [phone] FAX: [phone]
WO#: 19090845
YYebsite: httn:11)vivw,set1ek.com
Date Reported: 10/1/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
9/11/2019 12:30:00 PM
Lab ID:
19090845-001A
Project:
Eden
Client Sample
ID Eden
Analyses
Result RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: MJM
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND
0.00500
mglL
1
9/17/2019 4:24:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
0.500
mglL
1
9/17/2019 3:51:55 PM
TCLP Barium(Ba)
ND
5.00
mglL
1
9/17/2019 3:51:55 PM
TCLP Cadmium(Cd)
ND
0.100
mglL
1
9/17/2019 3:51:55 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
9/17/2019 3:51:55 PM
TCLP Lead(Pb)
ND
0.500
mglL
1
9/17/2019 3:51:55 PM
TCLP Selenium(Se)
ND
0.0500
mglL
1
9/17/2019 3:51:55 PM
TCLP Siiver(Ag)
ND
0.500
mglL
1
9/17/2019 3:51:55 PM
FLASHPOINT DETERMINATION (1010)
SW1010
Analyst: TAH
Flashpoint (140°F)
>140
°F
1
9/27/2019 10:35A5 AM
TCLP METALS, VOC, BNA, PEST, HERS -SOLID
SW8270
SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichloroberzene
ND
0.200
mglL
2
9/18/2019 4:27:00 AM
2,4,5-Trichlorophenol
ND
0.500
mg/L
2
9/18/2019 4:27:00 AM
2,4,6-Trichlorophenol
ND
0,500
mglL
2
9/18/2019 4:27:00 AM
2,4-Dinitrotoluene
ND
0.100
mg1L
2
9/18/2019 4:27:00 AM
Cresols, Total
ND
10.0
mglL
2
9/18/2019 4:27:00 AM
Hexachloro-1,3-butadiene
ND
0.0400
mglL
2
9/18/2019 4:27:00 AM
Hexachlorobenzene
ND
0.100
mglL
2
9/18/2019 4:27:00 AM
Hexachloroethane
ND
0.200
mglL
2
9/18/2019 4:27:00 AM
Nitrobenzene
ND
0.200
mglL
2
9/18/2019 4:27:00 AM
Pentachlorophonol
ND
0,500
mglL
2
9/18/2019 4:27:00 AM
Pyridine
ND
0.500
mglL
2
9/18/2019 4:27:00 AM
Surr: 2-Fluorophenol
15.7
10 - 109
%Rec
2
W18/2019 4:27:00 AM
Surr: Phenol-d6
20.1
10 - 109
%Rec
2
9/18/2019 4:27:00 AM
Surr: Nitrobenzene-d5
11.8
19 - 120
S %Rec
2
9/18/2019 4:27:00 AM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above guantitation range
H Folding times for preparation
or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation
exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CaleVal
< MDL
Page 6 of 39

ill SuzaatzaitEnrironzazezztal Technologies, Inc.
summ3310 YiTfra St.
Analytical Report
EkVlft l N h11 H i4L L 11Nf![ Cl4 � � *, F' ^.
Cuyahoga Falls, Ohio 44223
(base report)
Analy lcai LaboYaloriere TE-L: [phone] FLY: [phone]
WO#: 19090845
IYehsite: hyp:Mv1vw.se11ek.c0177
Date Reported: 101112019
CLIENT: Synagro
Tag Number:
Matrix: SLUDGE
Collection Date:
9/11/2019 12:30:00 PM
Lab ID: 19090845-OOIA
Project: Eden
Client Sample ID Eden
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr: 2,4,6-Tribromophenol 23.9
10 - 120
%Rec
2 9/18/2019 4:27:00 AM
Surr: 2-Fluorobiphenyl 10.2
22 - 117
S %Rec
2 9/18/2019 4:27:00 AM
Surr: p-Terphenyl-d14 12.7
34 - 116
S %Rec
2 9/18/2019 4:27:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: RIS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND
0.0250
mglL
10 9/25/2019 9:49:00 AM
Toxaphene ND
0.500
mglL
10 9/25/2019 9:49:00 AM
Endrin ND
0.00200
mglL
10 9/25/2019 9:49:00 AM
gamma-BHC ND
0.00200
mglL
10 9/25/2019 9AR00 AM
Heptachlor ND
0.00200
QC+ mglL
10 9/25/2019 9:49:00 AM
Heptachlor epoxide ND
0.00200
mglL
10 9/25/2019 9:49:00 AM
Methoxychlor ND
0.00200
dQC+ mglL
10 9/25/2019 9:49:00 AM
Surr. TCMX 54.2
10 - 119
%Rec
10 9/25/2019 9:49:00 AM
Surr: DCB 65.5
10 - 119
%Rec
10 9/25/2019 9:49:00 AM
TCLP HERBICIDES (SW846: 131118321)
SW8321A
Analyst: BJH
SVOC SW-846: 8321 HERBICIDES-TCLP
2,4-D ND
0.0100
mg1L
1 9/25/2019 11:12:00 AM
2,4,5-TP ND
0.0100
mglL
1 9/25/2019 11:12:00 AM
Surr: 2,4-Dichlorophenylacetle ad 0.190
70 - 130
S %Rec
1 9/25/2019 11:12:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311 M Analyst: RMT
TCLP VOLATILES ANALYSIS
1,1-Dichloroothene ND
0.500
mg1L
100 9/19/2019 5:45:00 PM
1,2-Dichloroethane ND
0.500
mglL
100 9/19/2019 6:45:00 PM
ME=K ND
10.0
mg/L
100 9/19/2019 5A5:00 PM
Benzene ND
0.500
mglL
100 9/19/2019 5:45:00 PM
Carbon tetrachloride ND
0.500
mglL
100 9/19/2019 5:45:00 PM
Chlorobenzene ND
5.00
mglL
100 9/19/2019 5:45:00 PM
Chloroform ND
0.500
mglL
100 9/19/2019 5:45:00 PM
Tetrachlomethere ND
0,500
mglL
100 9/19/2019 5:45:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding tines for preparation or analysis exceeded
M ManuaI Jntcgration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column confinnation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal
< MDT,
Page 7 of 39

SUMMIT
Summit Environmental Technologies, Inc.
3310 Yrjira St.
Analytical Report
-
ENVII OW&I�NTAL �FClill �e}�;a�^. 1W7
AnalyNC.?l LiabolraI0699
Ciryahoga falls, Ohio 44223
TEL: [phone] FAX..- [phone]
(base report}
WO#: 19090845
Website,- http:/hv,vw.settek.com
Date Reported: 10/1/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SLUDGE
Collection Date:
9/11/2019 12:30:00 PM
Lab ID:
19090845-001 A
Project:
Eden
Client Sample ID Eden
Analyses Result
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
94.9
Surr: Dibromofl uorom ethane
97.8
Surr: Toluene-d8
96.6
RCI-SOLID-Wl IGNITABILITY1030
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive
ND
PAINT FILTER FREE LIQUIDS TEST (SW-846: 9095)
Free Liquid pass
RCI-SOLID-WI IGNITABILITY1030
PH (SW9045D)
pH 6.6
RCI-SOLID-WI IGNITABILITY1030
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND
RL Qual Units
DF
Date Analyzed
SW8260 SW1311 M Analyst: RMT
0.500
mglL
100
0.200
mg/L
100
70 - 130
%Rec
100
70 - 130
%Rec
100
70 - 130
%Rec
100
SW9014
0.490
mg/Kg
1
SW9095
1
SW9045D
Qualifiers: B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit,
ND Not Detected
PL Permit Limit
RL Reporting Detection Limit
s,u.@19.6C 1
SW9034
25.0 mg/Kg 1
9/19/2019 5:45:00 PM
9/19/2019 5:45;00 PM
9/19/2019 5:46:00 PM
9/19/2019 5:45:00 PM
9/19/2019 5:45:00 PM
Analyst: MS
9/18/2019 5:17:00 PM
Analyst: DHC
9/17/2019 10:35:00 AM
Analyst: DHC
9/26/2019 10:48:00 AM
Analyst: MS
9/18/2019 5:17:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits Original
U Samples with CaleVal < MDL
Page 8 of 39

SUMMIEF
SunrnritL'nvironmerztal `Technologies, Inc. Accreditation Program
3310 Wiry St. Anal teS Report
EKV111ONh1ENTAL �ECtitw�l.t3C � G, INC Cuyahoga Falls, Ohio 44223 y p
AnafyOci?t Laboraloriox TEL: [phone] FAX.- [phone] WO#: 19090845
Website: http:11www.sette1c.cona 01-Oct-19
Client: Synagro
Project: Eden
State: NW
Program Name: NC_WW_SCM
Sample 1D Matrix
Test Name
Analyte
Status
19090845-001 A Sludge
Flashpo€nt Detertnination (1010)
Flashpoint (140°F)
A
Sludge
Paint Filter Free Liquids Test (SW-846: 9095)
Free Liquid
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2 -
Sulfide, Reactive
U
Sludge
SVOC SW-846: 8321 Herbicides-TCLP
2,4,5-TP
N
Sludge
SVOC SW-846: 8321 Herbicides-TCLP
2,4-D
N
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SWI311/60I0)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SWI311/60I0)
Lead
A
Sludge
TCLP Metals Analysis (SW I311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SWI311/60I0)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/9081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Lndrin
A
Sludge
TCLP Pesticides Analysis(SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SWI311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Nlethoxychlor
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW 131118270)
1,4-Dichlorobenzene
A
SIudge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
SIudge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzeue
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW131118270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
NC WW SCM A Accredited NC W W SCM N Not Accredited
NC W W SCM U Unavailabl
Version #3
Page 9 of 39

UMMIEFm
SumitFnvironmental Technologies, Inc. Accreditation Program
fr-S3310 Win St. Anal tes Report
ER VIROMMENTAL TECH OI OrIlf-S, INC Cuyahoga Falls, Ohio 44223 y p
ArWylical taboratarl6s TEL: [phone] FfLY. [phone] WO#: 19090845
Website: httn:11wwiv.settelccotn #1-Oct 19
Client: Synagro
Project: Eden
State: NW
Program Name: NCWW SCM
Sample ID Matrix
Test Name
AnaIyte
Status
19090845-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
II-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Te#rachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailab]
Version #3
Page 10 of 39

"ISUMMIT
Summit Environmental Technologies, .Inc.
3310 Win St.
QC SUMMARY REPORT
ENVITIOtWt:NTAL r-ECW G1,0Glf-7-1;, 1K(.
Cuyahoga Falls, Ohio 44223
WO#: 19D90845
.Arr&ipt€cal Laboralor)os
TEL: [phone] FAX..- [phone]
Website: hQ:Ilwivw.settek.com
01-Oct-19
Client:
Synagro
Project:
Eden
BatchID: 39425
Sample ID MB-39425
SampType: MBLK
TestCode: TCLP-VOC-M Units: mglL
Prep Date: 9/15/2019
RunNo: 103257
Client ID: PBS
Batch ID: 39425
TestNc: SW8260 SW1311M
Analysis Date: 911612019
SegNo: 2340758
Analyte
Result
PQL SPK value SPK Ref Vat
%REC Lowl-imit HighUmit RPD Ref Vai
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
474
Surr: Dibromofluoromethane
483
Surr: Toluene-d8
478
Qualifiers:
B Analyte detected in the associated Method Blank
7 Analyte detected below- quantitation limits
ND Not Detected
K RPD outside accepted recovery limits
500.0 94.8 70 130
500.0 96.5 70 130
500.0 95.6 70 130
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 11 of 39

l
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
"Isummo3310 Win St.
ENVIROAImr:mTAL racallof aGiaq, we Cuyahoga .Falls, Ohio 44223
WO#: 19090845
Anaiy lT cal Laborawkes TEL: [phone] FAY.- [phone]
Website: http:#Www.settek.com 01-Oct-19
Client: Synagro
Project: Eden EatebID: 39425
Sample ID LCS-103278
SampType: LCS
TestCode: TCLP-VOC-M Units: mglL
Prep Date:
RunNo: 103278
Client ID: LCSS
Batch ID: 39425
TestNo: SW8260 SW1311M
Analysis Date: 911612019
SegNo: 2344117
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.0207
0.00500
0.0200
0
103
79.4
131
1,2-Dichloroethane
0.0224
0.00500
0.0200
0
112
73.6
137
MEK
0.102
0.100
0.100
0
102
55.1
163
Benzene
0.0214
0.00500
0.0200
0
107
73.1
132
Carbon tetrachloride
0.0223
0.00500
0.0200
0
111
63.7
139
Chlorobenzene
ND
0.0500
0.0200
0
111
72.3
139
Chloroform
0.0213
0.00500
0.0200
0
107
79.3
129
Tetrachloroethene
0.0219
0.00500
0.0200
0
110
56.2
187
Trichloroethene
0.0234
0.00500
0.0200
0
117
64.1
138
Vinyl chloride
0.0161
0.00200
0.0200
0
80.4
22.1
147
Sum4-Bromofluorobenzene
51.1
50.00
102
80.4
126
Surr: Dibromofluorom ethane
49.8
50.00
99.7
70.3
125
Surr: Toluene-d8
49.6
50.00
99.3
82
117
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below gaantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 12 of 39

IT
Inc. QC SUMMARY REPORT
ffISUMM3310 Win St.
IERVIRONMEn7TALT-rCHN0L3GI!7;,;Kr. Cuyahoga Falls, Ohio44223
WO#_ 19090845
Ara?yrs,-.; t aboratormes TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 01-Oct-19
Client: Synagro
Project: Eden
BatchlD: 39428
Sample ID MB-39428
SampType: MBLK
TestCode:
SVOC-BNA_T Units: mg1L
Prep Date: 9116/2019
RunNo: 103423
Client ID; PBS
Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 911712019
SegNo: 2349918
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
N❑
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-FIuorophenol
0.382
Surr. Phenol-d6
0.441
Surr: Nitrobenzene-d5
0.215
Surr: 2,4,6-Tribromophenol
0.550
Surr: 2-Fluorobiphenyl
0.217
Surr: p-Terphenyl-d14
0.352
Qualifiers
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1.000
38.2
10
109
1.000
44.1
10
109
1.000
21.5
19
120
1.000
55.0
10
120
1.000
21.7
22
117
1.000
35.2
34
116
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reca
S
Original
Page 13 of 39

mmill
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffl su3310 Win St.
ENVI,tOfIMENTAL3cMhzKOf-CSGIE-7-ml, INC Cuyahoga Falls, Ohio44223
AF7atyFt;cal Labotatatlos TEL: [phone] FAX.- [phone] WO#: i9090845
Website: htfo:llwww.settek.com 01-Oct-19
Client: Synagro
Project: Eden BatchID: 39428
Sample ID LCS-39428
SampType: LCS
TestCode:
SVOC-BNA_T Units: mg1L
Prep Date: 9/16/2019
RunNo: 103423
Client ID: LCSS
Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 9/17/2019
SegNc: 2349919
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.261
C.100
0.8000
0
32.6
36.4
130 S
2,4,5-Trichlorophenol
0.481
0.250
0.8000
0
60.2
31.7
132
2,4,6-Trichlorophenol
0A81
0.250
0,8000
0
60.1
31.1
133
2,4-Dinitrctoluene
0.504
0.0500
0.8000
0
63.0
43.3
130
c-Cresol
0.383
0.250
0.8000
0
47.8
32.9
130
Cresols, Total
ND
5.00
1.600
0
49.3
31.7
130
Hexachloro-1,3-butadiene
0.249
0.0200
0.8000
0
31.1
31.4
130 S
Hexachlorobenzene
0.420
0.0500
0.8000
0
52.6
43.1
130
Hexachloroethane
0.243
0.100
0.8000
0
30.4
36.5
130 S
Nitrobenzene
0.331
0.100
0.8000
0
41.4
39.5
130
Pentachlorophenol
0.432
0.250
0.8000
0
54.0
34
130
Pyridine
0.301
0.250
0.8000
0
37.6
10
130 m
Surr: 2-FI uorop hen o I
0.430
1.000
43.0
17.1
130
Surr: Phenol-d6
0.480
1.000
48.0
10
130
Surr: Nitrobenzene-d5
0.242
1.000
24.2
32.6
130 S
Surr:2,4,6-Tribromophenol
0.629
1.000
62.9
4.43
130
Surr:2-Fluorobiphenyl
0.210
1.000
21.0
41.8
130 S
Surr: p-Terphenyl--d14
0.353
1.000
35.3
36.4
130 S
Qualifiers:
B Analyte detected in the associated Method Blank
3 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmat7on exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted recc
Original
Page 14 of 39

ly
Summit Lnvironmental Technologies, Inc. QC SUMMARY REPORT
fflsumm3310 Win St.
EW1iiOmPAENTAL TECH 3[5LL'rMUS, lht-.^. Giyahoga Falls, Ohio 44223
Anafy0Cal Laboralcrtoas TEL: [phone] FAX., [phone] WO#: 19090845
Website: httv:llwww.settek.com 0I-Oct-19
Client: Synagro
Project: Eden BatchlD: 39428
Sample ID 19090150-0DIAMS
SampType: MS
TestCode:
SVOC-BNA_T Units: mglL
Prep Date: 9/1612019
RunNo: 103423
Client ID: Batch=
Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 911712019
SegNo: 2349926
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimtt Qual
1,4-Dichlorobenzene
0.316
0.200
0.8000
0
39.5
33.8
126
2,4,5-Trichlorophenol
0.586
0.500
0.8000
0
73.2
28.7
144
2,4,6-Trichlorophenol
0.589
0.500
0,8000
0
73.6
12.8
153
2,4-Dinitrotcluene
0.628
C.100
0.8000
0
78.6
20.4
155
o-Cresol
ND
0.500
0.8000
0
57.4
10
148
Cresols, Total
ND
10.0
1.600
0
60.1
10
148
Hexachloro-1,3-butadiene
0.297
0.0400
0.8000
0
37.1
29
126
Hexachlorobenzene
0.547
0.100
0.8000
0
68.4
33.7
134
Hexachloroetharne
0.283
0.200
0.8000
0
35.4
32.8
132
Nitrobenzene
0.409
0.200
0.8000
0
51.2
20
158
Pentachlorophenol
ND
0.500
0.8000
0
60.4
10
176
Pyridine
ND
0.500
0.8000
0
43.6
10
130
Surr.2-Fluorophenol
0.510
1.000
51.0
3.39
130
Surr: Phenol-d6
0.578
1.000
57.8
5
130
Surr: Nitrobenzene-d5
0.282
1.000
28.2
14.5
154
Surr: 2,4,6-Tribromophenol
0.724
1.000
72.4
19.5
13C
Surr.2-Fluombiphenyl
0,266
1.000
26.6
34.4
130
Surr: p-Terphenyl-d14
0.438
1,000
43.8
8.86
156
Qualifiers:
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RFD outside accepted recovery limits
E Value above quantitation range H Holding tunes for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
m
S
Original
Page 15 of 39

'At Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffJ SUMM3310 Win St.
ENV[rtONP,iENTALTECHNo[,(rr.1-C-S, WC. Cuyahoga Falls, Ohio 44223
AnalyNca1 Laboratane� TEL: [phone] FAX.- [phone] WD#: 19090845
Website: hto.Ill wxcsettelccom 01-oct-19
Client: Synagro
Project: Eden
SatchID: 39428
Sample ID 19090150-001AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mglL
Prep Date: 9116/2019
RunNo: 103423
Client ID: BatchQC
Batch ID: 39428
TestNo: SW8270 SW3510C
Analysis Date: 9117/2019
SegNo: 2349938
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.307
0.200
0.8000
0
38.4
33.8
126
0.3156
2.83
30
2,4,5-Trichlorophero l
0.648
0.500
0.8000
0
81.0
28.7
144
0.5860
9.99
30
2,4,6-Trichlorophenol
0.654
0.500
0.8000
0
81.8
12.8
153
0,5892
10.5
30
2,4-Dinitrotoluene
0.662
0.100
0.8000
0
82.7
20.4
155
0.6284
5.15
30
c-Cresol
0.516
0.500
0.8000
0
64.6
10
148
0.4596
11.6
30
Cresols, Total
ND
10.0
1.600
0
67.5
10
148
0
0
30
Hexachloro-1,3-butadiene
0.267
0.0400
0.3000
0
33.4
29
126
0.2968
10.5
30
Hexachlorobenzene
0.582
0.100
0.8000
0
72.8
33.7
134
0.5472
6.16
30
Hexachloroethane
0.254
0.200
0.8000
0
31.7
32.8
132
0.2832
11.0
30 S
Nitrobenzene
0.446
0.200
0.8000
0
55.8
20
158
0.4092
8.61
30
Pentachlorophenol
0.526
0.500
0.8000
0
65.7
10
176
0.4832
8.41
30
Pyridine
ND
0.500
0.8000
0
42.6
10
130
0
0
30 m
Sum 2-Fluorophenol
0.549
1.000
54.9
3.39
130
0
Surr. Phenol-d6
0.624
1.000
62.4
10
130
0
Surr: Nitrobenzene-d5
0.301
1.000
30.1
14.5
154
0
Surr: 2,4,6-Tribromophenol
0.742
1.000
74.2
19.5
130
0
Sum 2-Flucrobiphenyl
0.284
1.000
28.4
34.4
130
0
S
Surr: p-Terphenyl-d14
0.441
1.000
44.1
8.86
156
0
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quamitation range H Holding times for preparation or anal!
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit Original
RL Reporting Detection Limit S Spike Recovery outside accepted recn
Page 16 of 39

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMI.EW
3310 Win St.
F-NV T ON14ENTAL T-ECM401 ,7., Cuyahoga Falls, Ohio 44223
WO#: 19090845
An$tyUCal Laboratonas TEL: [phone] FAX. [phone]
Websile: ht1n:1Avww.settek.com 01-Oct-19
Client: Synagro
Project: Eden
BatchID: 39428
Sample ID MB-39428
SampType: MBLK
TestCode:
TCLP-SVOC_ Units: mglL
Prep Date: 911612019
RunNo: 103423
Slient ID: PBS
Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 9/1712019
SegNo: 2349964
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.382
Surr: Phenol-d6
0.441
Surr: Nitrobenzene-d5
0.215
Surr: 2,4,6-Tribromophenol
0.550
Surr: 2-Fluorobiphenyi
0.217
Surr: p-Terphenyl-d14
0.352
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1.000
38.2
10
109
1.000
44.1
10
109
1.Ooc
21.5
19
120
1.000
55.0
10
120
1.000
21.7
22
117
1.000
35.2
34
116
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 17 of 39
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spilce Recovery outside accepted reco
Original

111
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
frSUMM3310 Win St.
EtWit'tOAMENTAL ZCINNO�00�S, WC. Cuyahoga Falls, Ohio 44223
WO#: 14090845
Agytical ab�rg1cwes TEL: [phone]] FAX- [phone] jf
Webshe: httn:llwww.settelc.coni 01-Oct-19
Client: Synagro
Project: Eden
BatchID: 39428
Sample ID LCS-39428
SampType: LCS
TestCode:
TCLP-SVOC_ Units: mglL
Prep Date: 9/16/2019
RunNo: 103423
Client ID: LCSS
Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 9/1712019
SegNo: 2349965
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qua{
1,4-Dichlorebenzene
0.261
0.100
0.8000
0
32.6
36.4
130
2,4,5-TricNorophenoI
0.481
0.250
0.8000
0
60.2
31.7
132
2.4,6-Trichlorophenol
0.481
0.250
0,8000
0
60.1
31.1
133
2,4-Dinitrotoluene
0.504
0.0500
0.8000
0
63.0
43.3
130
o-Cresol
0.383
0.250
0.8000
0
47.8
32.9
130
Cresols, Total
ND
5.00
1.600
0
49.3
31.7
130
Hexachloro-1,3-butadiene
0.249
0.0200
0.8000
0
31.1
31.4
130
Hexachlorobenzene
0.420
0.0500
0.8000
0
52.6
43.1
130
Hexachloroethane
0.243
0.100
0.8000
0
30.4
36.5
130
Nitrobenzene
0.331
0.100
0.8000
0
41.4
39.5
130
Pentachlorophenol
0.432
0.250
0.8000
0
54.0
34
130
Pyridine
0.301
0.250
0.8000
0
37.6
10
130
Surr: 2-Fluorophenoi
0.430
1.000
43.0
17.1
130
Surr: Phenol-d6
0.480
1.000
48.0
10
130
Sum Nitrobenzene-d5
0.242
1.000
24.2
32.6
130
Surr:2,4,6-Tribromophenol
0.629
1.000
62.9
4.43
130
Sum 2-Fluorobiphenyl
0.210
1.000
21.0
41.8
130
Surr: p-Terphenyl-d14
0.353
1.000
35.3
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantization range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
S
S
S
m
S
S
S
Original
Page 18 of 39

UMMIT Summit Environmental Technologies, Inc.
S3310 Win St.
ENVIiIONMEINTAL T2C}EIvIOi,DGIl -S, Ni7 Cuyahoga Falls, Ohio 44223
Anoty0ca1 Labotarone$ TEL: [phone] FAX: [phone]
Website: htW:Ilwww.settek.corn
QC SUMMARY REPORT
WO#: 19090845
01-Oct-19
Client: Synagro
Project: Eden Batch]D: 39428
Sample ID 19090150-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mglL
Prep Date: 9/16/2019
RunNo: 103423
Client ID: BatchQC
Batch ID: 39428
TestNo: SW8270 SW3510C
Analysis Date: 9/17/2019
SegNo: 2349966
Analyte
Result
PQL SPK value SPK Ref Val
%REC LcwLimit HlghUm1 RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.316
0.200
0.8000
0
39.5
15.2
124
2,4,5-Trichlorophenol
0.586
0.500
0.8000
0
73.2
30.6
152
2,4,6-Trichlorophenol
0.589
0.500
0.8000
0
73.6
27.6
150
2,4-Dinitrotoluene
0.628
0.100
0.8000
0
78.6
58
141
o-Cresol
ND
0.500
0.8000
0
57A
26.9
132
Cresols, Total
ND
10.0
1.600
0
60.1
27.6
132
Hexachloro-1,3-butadiene
0.297
0.0400
0.8000
0
37.1
-5.3
156
Hexachl oro benzene
0.547
0.100
0.8000
0
68.4
54.3
142
Hexachloroethane
0.283
0.200
0.8000
0
35.4
1.92
131
Nitrobenzene
0.409
0.200
0.8000
0
51.2
21
135
Pentachlorophenol
ND
0.600
0.8000
0
60.4
47.4
134
Pyridine
ND
0.500
0.8000
0
43.6
-10.3
64.2
Sum 2-FIuorophenol
0.510
1.000
51.0
9.77
146
Surr: Phenol-d6
0.578
1.000
57.8
20.7
130
Surr: Nitrobenzene-d5
0.282
1.000
28.2
13.9
156
Sum.2,4,6-Tribromophenol
0.724
1.000
72.4
27.3
183
Surr:2-FluoroNphenyl
0.266
1.000
26.6
21.4
153
Surr: p-Terphenyl-d14
0.438
1.000
43.8
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal`
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
m
S
Original
Page 19 of 39

int Summit Environmental Technologies, Inc. QC SUMMARY REPORT
summ3310 Win St.
E[w VIPIO14MENTAL 1rChNG1LOGIUt INC Cuyahoga Falls, Ohio 44223
WO#: 19090845
AnatyOcaP Laboratorlct TEL: [phone] FAX.- [phone]
Websile: hQ2.-1 www.settek.com of-Oct-19
Client: Synagro
Project: Eden
BatchlD: 39428
Sample ID
19090150-001AMSD SampType: MSD
TestCode:
TCLP-SVOC_ Units: mg1L
Prep Date: 9/16/2019
RunNc: 103423
Client ID:
BatchQC Batch ID: 39428
TestNo:
SW8270 SW3510C
Analysis Date: 911712019
SegNo: 2349967
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.307
0,200
0,8000
0
38A
15.2
124
0.3156
2.83
30
2,4,5-Trichlorophenol
0.648
0,500
0.8000
0
81.0
30.6
152
0.5860
9.99
30
2,4,6-Trichlorophenol
0.654
0.500
0.3000
0
81.8
27.6
150
0,5892
10.5
30
2,4-Dinitrotoluene
0.662
0.100
0.8000
0
82.7
58
141
0.6284
5.15
30
o-Cresol
0,516
0,500
0.8000
0
64.6
26.9
132
0.4596
11.6
30
Cresols, Total
ND
10.0
1.600
0
67.5
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.267
0.0400
0.8000
0
33A
-5.3
156
0,2968
10.5
30
Hexachlorobenzene
0.582
0A00
0.8000
0
72.8
54.3
142
0.5472
6.16
30
Hexachloroethane
0.254
0.200
0.8000
0
31.7
1.92
131
0.2832
11.0
30
Nitrobenzene
0.446
0,200
0,8000
0
55.8
21
135
0.4092
8.61
30
Pentachlorophenol
0.526
0.500
0.8000
0
65.7
47.4
134
0.4832
8A1
30
Pyridine
ND
0.500
0.8000
0
42.6
-10.3
64.2
0
0
30 m
Surr:2-Fluorophenol
0.549
1.000
54.9
9.77
146
0
Sum Phenol-d6
0.624
1.000
62.4
20.7
130
0
Sum Nitrobenzene-d5
0.301
1.000
30.1
13.9
156
0
Sum 2,4,6-Tribromophenol
0.742
1.000
74.2
27.3
183
0
Surr:2-Fluorobiphenyl
0.284
1.000
28.4
21.4
153
0
Sum p-Terphenyl-d14
0.441
1.000
44.1
54.8
154
0
S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal,
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 39

MMIT Summit Environmental Technologies, Inc.
ffISU3310 YVin St.
FENVIRt3JiMENTAL ��CttNa[ C'1 i ,,:Nfi Cuyahoga Falls, Ohio 44223
A'u±y-Oval Laboralorlos TEL: [phone] FAX., [phone]
Website: httn://www.settek.com
QC SUMMARY REPORT
WO#: 19090845
01-Oct-19
CIient: 5ynagro
Project: Eden BatchID: 39440
Sample 1D MB-39440
SampType: MBLK
TestCode:
Mtl-TCLP-7(6 Units: mglL
Prep Date: 9/1612019
RunNo: 103260
Client ID: PBS
Batch ID: 39440
TestNo:
SW6010D SW3010A
Analysis Date: 9/16/2019
SegNo: 2341242
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-39440
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mglL
Prep Date: 9/16/2019
RunNo: 103260
Client ID: LCSS
Batch ID: 39440
TestNo: SW6010D SW3010A
Analysis Date: 9116/2019
SegNo: 2341243
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Vai
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.08
0.500
2.000
0
104
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
107
80
120
TCLP Cadmium(Cd)
1.92
0.100
2.000
0
95.9
80
120
TCLP Chromium(Cr)
2.12
0.200
2,000
0
106
80
120
TCLP Lead(Pb)
2.18
0.500
2.000
0
109
80
120
TCLP Selenium(Se)
2.11
0.0500
2.000
0
105
80
120
TCLP Silver(Ag)
2.16
0.500
2.000
0
108
80
120
Qualifiers: B Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery Iimits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 21 of 39
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fflsummly 3310 Win St,
FR Vit-CO.MNI.5NTALT-.CHNCL[lGI�7_�, !W! Cuyahoga Falls, Ohio 44223
.dnWyt2�1 Labcratoner- TEL: [phone] FAX. [phone] WO#: 19090$45
Website: http://www.settek-.com 01-Oct-19
Client: Synagro
Project: Eden
BatchED: 39440
Sample [D 19090818-012AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mglL
Prep Date: 9116/2019
RunNo: 103320
Client ID: Batch=
Batch ID: 39440
TestNo: SW6010D SW3010A
Analysis Date: 9117/2019
SegNo: 2346875
Analyte
Result
PQL SPK value SPK Ref Val
%RFC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP ArseniC(As)
2.23
0.500
2.000
0
114
70
130
TCLP Barium(Ba)
ND
5.00
2.00C
2.874
98.9
70
130
TCLP Cadmium(Cd)
1.96
0.100
2.000
0.005326
97.8
70
130
TCLP Chromium(Cr)
2.06
0.200
2.000
0
103
70
130
TCLP Lead(Pb)
2.05
0.500
2.000
0
102
70
130 .
TCLP Selenium(Se)
2.34
0.0500
2.000
0
117
70
130
TCLP Silver(Ag)
2.26
0.500
2.000
0
113
70
130
Sample ID 19090818-012AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mglL
Prep Date: 9116/2019
RunNo: 103320
Client ID: Batch=
Batch ID: 39440
TestNo: SW6010D SW3010A
Analysis Date: 911712019
SegNo: 2346876
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.31
0.500
2.000
0
1'15
70
130
2.280
1.19
20
TCLP Barium(Ba)
ND
5.00
2.000
2.874
102
70
130
0
0
20
TCLP Cadmium(Cd)
2.00
0.100
2.000
0.005326
99.8
70
130
1.962
1.96
20
TCLP Chromium(Cr)
2.10
0.200
2.000
0
105
70
130
2.058
1.95
20
TCLP Lead(Pb)
2.09
0.500
2.000
0
104
70
130
2.048
1.93
20
TCLP Selenium (Se)
2.40
0.0500
2.000
0
120
70
130
2.344
2.52
20
TCLP Silver(Ag)
2,32
0.500
2.000
0
116
70
130
2.258
2.66
20
Qualifiers:
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 22 of 39

SUMMIEF Summit Environmental Technologies, Inc.
3310 Win St.
VI440NIdENTAL ITCHN04DGfrq, NC. Cuyahoga Falls, Ohio 44223
Arpa?yd al .Laboratarlts TEL: [phone] FAX.- [phone]
Website: htW:11www.settek.com
QC SUMMARY REPORT
WO#: 19090845
01 -Oct-19
CIient: Synagro
Project: Eden SatchID: 39461
Sample ID MB-39461
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prop Date: 9/1712019
RunNo: 103359
Client ID: PBS
Batch ID: 39461
TestNo: SW7470A SW7470A
Analysis Date: 9/1712019
SegNo: 2346192
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID LCS-39461
SampType: LCS
TestCode: HG TCLP(74 Units: PPM
Prep Date: 911712019
RunNo: 103359
Client ID: LOSS
Batch ID: 39461
TestNo: SW7470A SW7470A
Analysis Date: 911712019
SegNo: 2346193
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00446 0.00200 0.00400 0 112 80 120
Sample ID 19090845-OOIAMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 911712019
RunNo: 103359
Client ID: Eden
Batch ID: 39461
TestNo: SW7470A SW7470A
Analysis Date: 9/1712019
SegNo: 2346200
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.0111 0.00500 0.0100 0 111 75 125
Sample ID 19090845-001AMSD
SampType: MSD
TestCode: HG TCLP(74 Units: PPM
Prep Date: 911712019
RunNo: 103359
Client ID: Eden
Batch ID: 39461
TestNo: SW7470A SW7470A
Analysis Date: W1712019
SegNo: 2346201
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.0108 0.00500
Qualifiers: B Analyte detected in the associated Method BIank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0.0100 0 108 75 125 0.0111 2.75 20
E Value above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 23 of 39

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
summmir
, 9Ftr, Cuyahoga Falls. Ohio 44223 WO#: 1.9090845
A.r?afyNcal Laboretarles TEL: [phone] FAX. [phone]
Website: http://uwiv.settek.con7 01-Oct-19
Client: Synagro
Project: Eden
BatchID: 39461
Sample ID
19090845-001AMSD SampType: MSD
TestCode:
HG_TCLP(74 Units: PPM
Prep Date: 9117/2019
RunNo: 103359
Client ID:
Eden Batch ID: 39461
TestNo:
SW7470A SW7470A
Analysis Date: 911712019
SegNo: 2346201
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
II Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 24 of 39

MMIT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St,
Ei55wl1 OMNIENTAL rECHNOL0GiG_�, NC Cuyahoga Falls, Ohio 44223
A.rfadydc21 Laboratories TEL: [phone] F,4X..- [phone] WO#: 19090845
Website: http://www.settek.com 01-Oct-19
Client: Synagro
Project: Eden BatchED: 39480
Sample 1D 19090844-001amsd
SampType: MSS
TestCode:
TCLP-SVOC- Units: mg1L
Prep Date: 9/1812019
RunNo: 103682
Client ID: BatchQC
Batch ID: 39480
TestNo:
SW8081 SW3510C
Analysis Date: 9/2512019
SegNo: 2376755
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Endrin
0.00990
0.00500
0.0100
0
99.0
10
224
0.0110
10.4
gamma-BHC
0.00675
0,00500
0.0100
0
67.5
10
192
0.00752
10.8
Heptachlor
0.0103
0.00500
0.0100
0
103
10
197
0.0117
12.7
Heptachlor epoxide
0.00880
0,00500
0.0100
0
88.0
10
208
0.00965
9.25
Methoxychlor
0.0172
0.00500
0.0100
0
172
10
251
0.0188
9.23
Surr: TCMX
11.8
20.00
59.2
10
157
0
Surr: DCB
13.8
20.00
69.2
10
194
0
30
30
30 QC+
30
30 QC+
Sample ID 19090844-001ams
SampType: MS
TestCode:
TCLPSVOC- Units: mg1L
Prep Date: 911812019
RunNc: 103682
Client ID: BatchQC
Batch [D; 39480
TestNo:
SW8081 SW3510C
Analysis Date: 9125/2019
SegNo: 2376756
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.0110
0.00500
0.0100
0
110
10
224
gamma-BHC
0.00752
0.00500
0.0100
0
75.2
10
192
Heptachlor
0.0117
0.00500
0.0100
0
117
10
197
Heptachlor epoxide
0.00965
0.00500
0.0100
0
96.5
10
208
Methoxychlor
0,0188
0.00500
0.0100
0
188
10
251
Surr: TCMX
13.1
20.00
65.6
10
157
Surr. DCB
14.0
20.00
69.9
10
194
Qualifiers: B Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
QC+
QC+
Original
Page 25 of 39

I
Summit Environmental Technologies„ Inc. QC SUMMARY REPORT
ffl 3310 Win St.
E[h1V1,10NINIENTAL rr-chNoLt3Gir- Ltd.^ Cuyahoga Falls, Ohio 44223
A-tV? rtiCal Labcrator)e5 TEL: [phone] FAX.- [phone] WO#_ 19090$45
Wehsite: http Ilwww,.settek.com 01-Oct-19
Client: Synagro
Project: Eden
BatchED: 39480
Sample ID Ics-39480
SampType: LCS
TestCode:
TCLP-SVOC- Units: mg1L
Prep Date: 9/1812019
RunNo: 103682
Client ID: LCSS
Batch ID: 39480
TestNo:
SW8081 SW3510C
Analysis Date: 912512019
SegNo: 2376757
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.00596
0.000500
0.0100
0
59.6
10
130
gamma-BHC
0.00380
0.000500
0.0100
0
38.0
10
130
Heptachlor
0.00578
0.000500
0,0100
0
57.8
10
130 QC+
Heptachlor epoxide
0.00479
0.000500
0.0100
0
47.9
10
130
Methoxychlor
0.0130
0.000500
0.0100
0
130
10
178 QC+
Surr: TCMX
6.55
20.00
32.8
10
130
Surr: DCB
10.4
20.00
51.9
10
130
Sample ID mb-39480
SampType: MBLK
TestCode: TCLP-SVOC- Units: mglL
Prep Date: 9118/2019
RunNo: 103682
Client ID: PBS
Batch ID: 39480
TestNo: SW8081 SW3510C
Analysis Date: 9125/2019
SegNo: 2376758
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-Imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500 d
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500 dQC+
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500 dQC+
Surr: TCMX
6.51
20.00 32.6 10 119
Surr: DCB
10.7
20.00 53.7 10 119
Qualifiers: B Analyte detected in the associated Method Blank
3 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reca
Original
Page 26 of 39

l
Summit environmental Technologies, Inc. QC SUMMARY REPORT
summa3310 Win St.
!ENVInONMENTAL nGHND[Ot VFS, JfiC Cuyahoga Falls, Ohio 44223
WO#: 19090$45
An$r;,rtlt;a1 Calaoratrrrlfis TEL: [phone] FAX. [phone]
Website: httA_/1www.settek.com 01-0ct-19
Client: Synagro
Project: Eden Batch1l): R103314
Sample ID 19090731-001ADUP
SampType: DUP
TestCode:
FreeLiquid_S Units:
Prep Date:
RunNo: 103314
Client ID: BatchQC
Batch ID: R103314
TestNo:
SW9095
Analysis Date: 9/17/2019
SegNo: 2343874
Analyte
Result
PQL
5PK value SPK Ref Val
%REC Lowl-imit I-IighLimit RPD Ref Val
%RPD RPDLimit Qual
Free Liquid pass 0 0 20
Qualifiers
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S. Spike Recovery outside accepted reco
Original
Page 27 of 39

ffl'summiy
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVI ROA MENTAL I RECHNO WG 1ES, ANC
Cuyahoga Falls, Ohio 44223
WO#: 19090845
1lryaty6cal Laborala4os
TEL: [phone] FAX- [phone]
Website: hftp:llwww.settelc.coni
01-Oct-19
Client:
Synagro
Project:
Eden
Batch]D: R103463
Sample I❑ 19090844-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 103463
client ID: BatchQC
Batch ID: R103463
TestNo: SW9014
Analysis Date: 911812019
SegNo: 2351735
anaiyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.16 0.495 10.00 0.1092 90.5 81.6 122
Sample ID 19090844-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 103463
'fient ID: BatchQC
Batch ID: R103463
TestNo: SW9014
Analysis Date: 9118/2019
SegNo: 2351736
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowi-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.18 0.481
Qualifiers: B A.nalyte detected in the associated Method Blank
7 Analyte detected below quantitatiQn limits
ND Not Detected
R RPD outside accepted recovery limits
10.00 0.1092 90.7 81.6
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
122 9.156 0.275 5
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 28 of 39

IMF Summit Environmental Technologies, Inc. QC SUMMARY REPORT
InSUMM3310 Win St.
EFE HIONMENTAL TEC7 HOFt Grr. FS, IN-n Cuyahoga Falls, Ohio 44223
WOO: 19090845
.4�W1{t1cs? LabOrafYsrJort TEL: [phone]I1 F,4X.• [phone]
Website: htW://www.settelc.com 01-Oct-19
Client: Synagro
Project: Eden BatchID: R103463
Sample ID MBLK
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNc: 103463
Client iD: PBW
Batch ID: R103463
TestNo: SW9014
Analysis Date: 911812019
SegNo: 2351720
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.485
Sample ID LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 103463
Client ID: LCSW
Batch ID: R103463
TestNo: SW9014
Analysis Date: 9/18/2019
SegNo: 2351721
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.39 0.495 10.00 0 93.9 85 115
Sample ID RLC
SampType: RLC
TestCode:
Cyanide,Rea Units: mg1L
Prep Date:
RunNo: 103463
Client ID: SatchQC
Batch ID: R103463
TestNo:
SW9014
Analysis Date: 9/18/2019
SegNo: 2351723
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
0.543 0.495 0.5000 0 109 50 150
Qualifiers: B Anal Ae detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E VaIue above quantitation range H Holding times for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 29 of 39

ffl
SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
EW1i' ONMENTAL rrCHN0[XbGl5�.q, ;Kt.
Cuyahoga Falls, Ohio 44223
WO#: 19090845
Anaty l Laboraforleg
TEL: [phone] FAX.- [phone]
Website: htW:Ilwww.settek.com
01-Oct-19
Client:
Synagro
Project:
Eden
BatchID: RI03470
Sample ID MB-R103470
SampType: MBLK
TestCode:
Sulfide,React Units: mg1L
Prep Date:
RunNo: 103470
Client ID; PBW
Batch ID: R103470
TestNoi
SW9034
Analysis Date: 9118/2019
SegNo: 2352149
Analyte
Result
PQL
SPK value SPK Ref Val
%REC LowLimit HighLimit . RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
ND 25.0
Sample ID LCS-R103470
SampType: LCS
TestCode: Sulfide,React Units: mg1L
Prep Date:
RunNo: 103470
Client ID: LCSW
Batch ID: R103470
TestNo: SW9034
Analysis Date: 9118/2019
SegNo: 2352150
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4830 25.0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
48CO 0 101 85
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
115
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 30 of 39

fflsumm3310
mi
`summit Environmental Technologies, Inc.
Win Si.
QC SUMMARY REPORT
ENylnOt4P P-NTAL rr-CitNoLi G4f-:S, iN.-
Cuyahoga Falls, Ohio 44223
WO#: 19090845
Anaiyflcal Labaratcries
TEL: [phone] FIX.- [phone]
Website: hLW:Ilwww.settek.com
01-Oct-19
Client:
Synagro
Project:
Eden
BatebID: R103470
Sample ID 19090844-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 103470
Client ID: Batch=
Batch ID: R103470
TestNo: SW9034
Analysis Date: 911812019
SegNoi 2352161
Analyte
Result
PQL SPK value SPK Ref Vai
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4890 25.0 4800 0 1C2 80 120
Sample ID 19090844-001AMSD
SampType: MSD
TestCode:
Sulfide,React Units: mg1Kg
Prep Date:
RunNo: 103470
Client ID: BatchQC
Batch ID: R103470
TestNo:
SW9034
Analysis Date: 9/18/2019
SegNo: 2352162
Analyte
Result
PQL
SPK value SPK Ref Val
%RFC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4820 25.0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
4800 0 100 80
B Value above quantization range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
120 4890 1.44 30
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 31 of 39

rnsumlir Summit Environmental Technologies, Inc. QC SUMMARY REPORT
m3310 Win St.
Ef VillQ:NMENTALTr—[:H Of-DCIES, lhtC Cuyahoga Falls, Ohio 44223 WO#: 19090845
A natyrleaf Laborat.anes TEL: [phone] FAX..- [phone]
Website: htty:llwww.settek.com 01-Oct-19
Client: Synagro
Project: Eden
BatchID: R1.03732
Sample ID LCS-R103732
SampType: LCS
TestCode:
pH_NPW(450 Units: s.u.@20.9C
Prep Date:
RunNo: 103732
Client ID: LCSW
Batch ID: R103732
TestNo:
SW9045D
Analysis Date: 912612019
SegNo: 2365556
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101 A
Sample ID 19091702-001ADUP
SampType: DUP
TestCode:
pH_NPW(450 Units: s.u.@20.4C
Prep Date:
RunNo: 103732
Client ID: BatchQC
Batch ID: R103732
TestNo:
SW9045D
Analysis Date: 912612019
SegNo: 2365558
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH
Qualifiers:
62
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
6.2 0.3
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
5 H
Original
Page 32 of 39

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
frSUMMIT 3310 Win St.
ENV] C4O.NMENTAL TECHNOLOG �, JHt' Cuyahoga Falls, Ohio 44223
AgaV Oca:l Laboratories TEL: [phone] FAX: [phone] WO#: 19090845
Website: htto:llwww.settel�. com 01-Oct-19
Client: Synagro
Project: Eden BatchID: R103732
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_OIL(9045 Units: s.u.@19.9C
Prep Date:
RunNo: 103732
Client ID: LCSW
Batch ID: R103732
TestNo:
SW9045D
Analysis Date: 9/2612019
SegNo: 2365569
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 '[10
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_OlL(9045 Units: s.u.@19.7C
Prep Date:
RunNo: 103732
Client ID: LCSW
Batch ID: R103732
TestNo:
SW9045D
Analysis Date: 912612019
SegNo: 2365574
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Sample ID CHECK 7
SampType: LCS
TestCode:
PH_OIL(9045 Units: s.u.@19.4C
Prep Date:
RunNo: 103732
Client ID: LCSW
Batch ID: R103732
TestNo:
SW9045D
Analysis Date: 9/26/2019
SegNo: 2366527
Analyte
Result
PQL
SPK value SPK Ref Val %REC
Lowt-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery hits
0 101 90 110
L Value above quantitation range H Holding tines for preparation or anal,
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
Rl, Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 33 of 39

fn
SUMMINt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
t=RkVInOt1661E14TAL tr-CkINGLOGi<-Sa, :Ptk.
Cuyahoga Falls, Ohio 44223
tiV0#: 19{190845
Analyrl ? Laboraloe s
TEL: [phone] FAX.- [phone]
Website: htt42:1Avww.settek.coin
01-Oct-19
Client:
Synagro
Project:
Eden
BatchID: R103732
Sample ID 19090844-001ADUP
SampType: DUP
TestCcde: PH_S(9045D) Units: sm.@19.8C
Prep Date:
RunNo: 103732
client ID: Batch=
Batch ID: R103732
TestNo: SW9045D
Analysis Date: 9126/2019
SegNo: 2365571
knalyte
Result
PQL SPK value SPK Ref Val %RDC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.8
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0 0 0
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
0 7.6 0.4 10
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted recc
Original
Page 34 of 39

Summit Environmental Technologies, Inc, QC SUMMARY REPORT
91summilt 3310 Win St.
EI4��lit.C}fPubFkiTALi=�tktlf]LCyCic Cuyahoga Falls, Ohio44223
Ar*vOoat Laboralonec TEL: [phone] FAX..- [phone] WO#: 19090845
Website: htt2:llwww.settek.com 01-Oct-19
Client: Synagro
Project: Eden BatchID: R1.03755
Sample ID MB
SampType: MBLK
TestCode: TCLP-SVOC- Units: mglL
Prep Date:
RunNo: 103755
Client ID: PBS
Batch ID: R103755
TestNo: SW8321A
Analysis Date: 912512019
SegNo: 2366793
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100 0 0
2,4,5-TP ND 0.0100 0 0
Surr: 2,4-Dichlorophenylacetic acid 0.0720 0.05000 144 70 130 S
Sample ID LCS
SampType: LCS
TestCode: TCLPSVOC- Units: mglL
Prep Date:
RunNo: 103755
Client ID: LCSS
Batch ID: R103755
TestNo: SW8321A
Analysis Date: 9125/2019
SegNo: 2366794
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Vai
%RPD RPDLimit Qual
2,4-D
0.342
0.0100 0.3000
0 114
60.5
141
2,4,5-TP
0.0700
0.0100 0.07500
0 93.3
68.3
144
Surr: 2,4-Dichlorophenylacetic acid
0.259
0.3000
86.3
70
130
Sample ID 19091306-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mglL
Prep Date:
RunNo: 103755
Client ID: MOW
Batch ID: R103755
TestNo: SW8321A
Analysis Date: 9/2512019
SegNo: 2366795
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D 0.185 0.0100 0.3000
2,4,5-TP 0.0430 0.0100 0.07500
Surr. 2,4-Dichlorophenylacetic acid 0.175 0.3000
0 61.7 37 105
0 57.3 38 106
47.0 70 130
S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal.
7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 35 of 39

rnsumm
ilt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENWRO'N &I ENTAL TECHNOLOGlJF C
Cuyahoga Falls, Ohio 44223
Anatyacal Laboratcrje� TEL: [phone] FAX: [phone]
WO#: 19090845
Wehsite: htW:Ilwww.settek.com
01-Oct-19
Client:
Synagro
Project:
Eden
BatchID: R103755
Sample ID 19091306-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mglL
Prep Date:
RunNo: 103755
client ID: BatchQC
Batch ID: R103755
TestNo: SW8321A
Analysis Date: 9125/2019
SegNo: 2366796
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.196
0.0100 0.3000
0 65.3
10
150 0.1850
5.77
30
2,4,5-TP
0.0460
0.0100 0.07500
0 61.3
10
150 0.04300
6.74
30
Sum 2,4-DichlorophenyIacetic acid
0.188
0.3000
51.3
70
130
0
0 S
vuauriers
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 36 of 39

mmi
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
fn 3310 Win St.
ENVIIIW41iENTAL tfr-CHNOE.OME'_S,.INC Cuyahoga Falls, Ohio 44223
Analy.ticaf Laiyora£one!rt TEL: [phone] FAX.- [phone] WO#: 19090845
Website: ho://www.settelc.com 01-Oc£-19
Client: Synagro
Project: Eden
BatchID: R103796
Sample ID LCS-R103796
SampType: LCS
TestCode: FlashPt S00 Units: OF
Prep Date:
RunNo: 103796
Client ID: LCSS
Batch ID: R103796
TestNo: SW1010
Analysis Date: 9/2712019
SegNo: 2368919
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Dual
Flashpoint (1407)
133
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
135.4 0 98.2 98
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
102
H Holding times for preparation or anal,
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 37 of 39

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SUMMITunSertt Envb•avraental Techrzolagres, Inc.
3310 I,Vhi St.
ENVIt0MMENTALTECHNOLOGIES, �NC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Analyflcaf taboralcoos %'Fs'I: [phone] TAX: [phone]
Website: http://mww,.settek.com
Client Name: SYN-NC-27028
Logged by: John A.Semenik
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Lop In
3. Coolers are present?
Work Order Number: 19090845
9/12/2019 10,10.00 AM
911212019 9:47:58 PM
9/1312019 10:28:32 AM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5 Was an attempt made to cool the samples?
RcptNo: 1
l,,.t+o.u•d•�e
Yes No ❑ Not Present ❑
UPS
Yes ❑ No ❑ NA ❑
Yes �/❑ No ❑
Yes ❑ No ❑ Not Present J.'/1
Signed By:
Yes LVOJ No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes V No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes V No ❑
$• Sufficient sample volume for indicated test(s)? Yes No ❑
9. Are samples (except VOA and ONG) properly preserved? Yes No ❑
10. Was preservative added to bottles? Yes ❑ No ] NA ❑
1 1 . Is the headspace in the VOA vials less than 114 inch or 6 mm? Yes ❑ No ❑ No VOA Vials ❑�
12, Were any sample containers received broken? Yes ❑ No �/❑
13. Does paperwork match bottle labels? Yes ❑ No ❑
(Note discrepancies on chain of custody)
14• Are matrices correctly identified on Chain of Custody? Yes 0 No ❑
15. Is it clear what analyses were requested? Yes n No ❑
16. Were all holding times able to be met? Yes 0 No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑�
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
--- -- --- - - - -- --
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed By
1 S.5 Goad Not Present
Page 39 of 39

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP
WWTP Name: Mebane Bridge WWTP NPDES Number:
Monitoring Period: from 01/01/19 To 03/31/19
WQ Permit Number:
WQ 0003035
NC 0025071
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost I leat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B.
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahle fn alternative nerfnrmerl Wlass A nr Clac.c Rl emmniefe the. fnllnwino mnnitnrinu dafs-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
'Technique
Minimum Geo, Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6"
MPN
MPN/g
CoIiform
power per gram
of total solids
16043
27865
59459
CFU/g
0
4/yr
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 NUN per 4 grams total
bacteria (in
solids (diy weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Aft. 2
Option/Alt, 3
Option/Alt, 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
111 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met, I am aware that there are significant penalties for false certification including fine and imprisonment."
Melinda Ward, WWTP Superintendent
Pr parer N me and Title ( type or print)
Signature ofPreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: plate Roth Report Date: 1/22/2019
Client: Synagro
284 Boger ]toad Project: Eden
Mocksville, NC 27028 Date Sample Rcv'd: 1/10/2019
Meritech Work Order # 01101937 Sample: Eden 1 of 4 Grab 1/10/19
Parameters Results Analysis Date Repprting Limit Method
Total Solids
18.7 %
1/11/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
16,043 col/g dry wt
1/10/19
258 cal/g dry wt
SM 9222D
Meritecb Work Order # 01101938 Sample: Eden 1 of 4 Grab
1/10/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 17.7 %u 1/11/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 28,249 col/g drywt 1/10/19 258 col/g drywt SM 9222D
Meritech Work Order # 01101939 Sample: Eden 1 of 4 Grab 1/10/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 18.2 % 1/11/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 16,484 col/g drywt 1/10/19 258 col/g drywt SM 9222D
Meritech Work Order # 01101940 Sample: Eden 1 of 4 Grab 1/10/19
Parameters Results Analysis Date Reporting Limit Method
Total Solids 18.6 % 1/11/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 26,882 col/g drywt 1/10/19 258 col/gdrywt SM 9222D
Meritech Work Order # 01101941 Sample: Eden 1 of 4 Grab 1/10/19
Parameters Results Analysis Date Reno�rting Limit Metho
%© TotaI Solids
18.5 %
1/11/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
59,459 col/g drywt
1/10/19
258 col/gdrywt
SM 9222D
642 Tamco Road, Reidsville, forth Carolina 27320
tel.[phone] fax.(336)342w1522

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date; 1/22/2019
Project, laden
Date Sample Rcvd: 1/7/2019
Meritech Work Order # 01101942 Sample: Eden 1 of 4 Grab 1/10/19
parameters Results Analyses Date Reporting Limit Limit Metro
%Total Solids 17,8 % 1/11/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 56,180 col/g dry wt 1/10/19 252 col/g dry wt SM 9222D
Meritech Work Order # 01101943 Sample: Eden 1 of 4 Grab 1/10/19
Parameters Results Analysis Date Re ti Limit Met o
°/o Total Solids
18.0 %
1/11/19
0-100 % SM 2540E
Fecal Coliform (Sludge)
19,444 col/g dry wt
1/10/19
228 col/g dry wt SM 9222D
Y hereby certify that I have reviewed and approve these data. Lab� entoH -
oratoryRepresentative
642 Tarnco Road, Reidsville, North Carolina 27320
tel,[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#:
MHERITECINC'
Client: A- Ivo Phone:
,
Address z Fax,
ENVIRONMENTAL LABORATORIES
Email:_
642 Tamco Rd. Phone: [phone]
Project:., fdik-n
Reidsville N C 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: 1\:)CS-'C I Turn Around Time*
'RUSH work needs prior approval,
How would you like your report sent? Charges Ao[31v
www.meritechlabs.com
"efz Stcl 10 da s) 3-5 Da 24 - 48 i4m
Circle all that apply,- � �mil (0eferred), Fax, Mail
Sampling Dates & Times
Pe n/Prirl ,.,rson Ta Vng Sample (Sig
(
Lab Use Only
Sample Location arid/or ID #
I
Start
End
Camp?'
1� #'of
fe'--s-i"(s)
Rlq61red
an Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont-
Y,', No
Cl OK?
Temperature Upon
Receipt:
DechloCination {<G.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation."*
Method of
Comments:
Compositor #
Shipment:
UPS
JJUg#
Fed Ex
Are these results for,egulatory , oses?._, Yes No
IP
Report results in: mg/L mg/kgug/L
ZHand Delivery
Relinquished by:
Received by: Date; Time;
Other
Time: Relinquished by: Date 3'
0
Received by: Date: Time:
1 i
Relinquished by. Date: Time:
M

FECAL DATA SHEET
Lab result
Log
16043
421
Min 16043
28249
4.45
Max 59459
16484
4.22
Geometric Mean 27865
26,882
4.43
59459
4.77
56180
4.75
19444
4.29
Average
4.45

Meritech, Inc.
: Environmental Laboratory
w Laboratory Certification No.1.65
Contact; Clay liisackerly Report Date: 2/21/2019
Client: Synagro
284 Boger Road Project; Eden
Mocksville, NC 27028 Date Sample Rcvd: 1/10/2019
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 01101936 Sample: Eden Grab 1/10/19
Total Solids Valg-.0 a Solids % Volatile Solids
Week 1 0.650 0.330 0,S07
Week 2 0.710 0.360 0.514
Week 3 0.740 0.360 0.484
Week 4 0.620 0.300 0.489
Weep 5 0.450
Van Kleeck Reduction (%): -11.00
0.240
0,533
1 hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tarnca Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COO
NPDES##:
� c�,_c, �;i.} Phone:
Address: `fit _� �`� Fax:
�c [��s�� l_e Q� � � Email:.l:fJ
Project:
P.O.##: _
Attention: � Turn AroundTirne*
��.
BRUSH work needs prior approval,
How would you like your report sent? C arves AmAy
std 1Q a s) 3-5 Qa 24-48Hrs
Circle all that apply: Email referred), Fax, Mail
�SI L�l
INC.RAERient:
#! I T �j 1� 'do
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
—
Sample Location and/or 1D #
Sampling Dates & Tunes
P I;
Person Taking sample (Sign/Print}:
Lab Use Only
Start
End
Camp?
drab?
#o#
Cont.
Test(s) Required
es Ice?
Yes Na
py OK,
7
C1 OK?
Date
Time
Date
Time
fz ri r i PR
1-1Q-- -
I i I D
Dom.
If -, �.� oen-
1-16
Temperature upon
Receipt
Method of
Shipment:
** Dachlorination (<o,s pm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in thEfield priorto preservation.
Comments:
Compositor #
. UPS
Jug #
IJ' Fed Ex
Are these rewu is for reg latory p rposes? Yes '. No
Report results in: mg/L mg/kg ug/L Q,
��"Hand Delivery
Relinquished by: Date: Time:
�� �z , ._�
Received by: pate: Time:
�Other
Rellnqujs}ted by: Date: Time:
Received b Date: Time:
Y�
Relinquished by; Date: Time:
Rece by 1- p e• p 1

%VS R
(older, more conservative method)
%VS In 0.5070 Enter in
%VS out 1 0.5330 . decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in X %VS out))
%VSR=
(method from p.132 of WH manual)
%VSR_ (%VS in - %VS out)
%VS in
%VSR=
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP
WWTP Name: Mebane Bridge WWTP
Monitoring Period: From 4/01/19
To 06/30/19
WQ Permit Number: WQ 0003035
NPDES Number: NC 0025071
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt, 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if nnnlirnhle to alternative nerfnrmed Wiens A or C'la.cs M comnlete the following, monitoring data. -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6"'
MPN
CFU/g
Coliform
power per gram
of total solids
15000
18724
24876
CFU/g
0
4/yr
Grab
9222 D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt, 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
OptionfMt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met.'"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CPR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements,)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisomnent."
Melinda Ward, WWTP Superintendent
Preparer Name And Title type or mt)
-y��3"_� ?- W- A
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 IO2 (26)

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report bate: 4/29/2019
Project: Eden
Date Sample Rcvd, 4/15/2019
Meritech Work Order #
041.51919
Sample: Eden 2 of 4 Cl) Grab
4/15/19
ParaMeters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.98 %
4/17/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
20,101 cal/g drywt 4/15/19
258 col/g drywt
SM 9222D
Meritech Work Order #
04151920
Sample, Eden 2 of 4 (2) Grab
4/15/19
Parameters
Ro t
Analysis Date
Reporting Limit
M 9tho
% Total Solids
4.00 %
4/17/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
15,000 col/g dry wt 4/15/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
04151921
Sample: Eden 2 of 4 (3) Grab
4/15/19
Parameters
Results
Analysis Date
Reporting Limi
Method
% Total Solids
4.08 %
4/17/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
19,608 col/g dry wt 4/15/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
04151922
Sample: Eden 2 of 4 (4) Grab
4/15/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
4.15 %
4/17/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
16,867 col/g dry wt 4/15/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
04191923
Sample: Eden 2 of (5) Grab
4/15/19
Parameters
Results
Anal sis Date
Reporting -Lim!
Metho
% Total Solids
4,22 %
4/17/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
16,588 col/g dry wt
4/15/19
258 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel,[phone] fax.[phone]

Page 2
Contact: Ryan Copeland Report Date: 4/29/2019
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd: 4/15/2019
Meritech Work Order # 04151924 Sample: Eden 2 of 4 (6) Grab 4/15/19
Parameters
Results
Analysis Date
Reporting Limi
Methpd
% Total Solids
4.08 %
4/17/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
19,608 col/g dry wt
4/15/19
252 cal/g dry wt
SM 9222D
Meritech Work Order #
0415192S Sample: Eden 2 of (7) Grab
4/15/19
Parameters
Results
Analysis. Date
Reporting Li
Method
% Total Solids
4.02 %
4/17/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
24,876 col/gdry wt
4/15/19
228 col/gdry wt
SM 9222D
I hereby certify thotI have reviewed and approve these data. Yda
La oracotyRepresentative
642 Tameo Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

8/9/18
Chain of Custody Record (COC)
NPDES#-
Client: �AJWO Phone:
'21,
MERITECH, INC.
Address: Fax:
ENVIRONMENTAL LABORATORIES
Mo"K�VLu5 NL Email.
Pa wn
Lv_,
642 Tarnco Rd. Phone: [phone]
Project:
LnEf
yc
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: info@ meritechiabs.com
Attention. (KJ% cepww'�)
7
Turn Around Time*
*RUSH work needs prior approval,
How would you like our report sent?
char esA iW
wwm w.meritechlabs.co
Std JIGAgys)
3_5 D I 24-48Hrs
Circle all that apply: Lnt 1) preferred), Fax, Mail
Sampling Dates &Times
Person Taking Sample (Sign/Print):
Lab Use Only
Sample Location and/or ID #
start
End
comp?
# of,
Test(s) Required
On Ice?
pH OK?
Date
Time
Date
Time
GTab?
CC)nt
CI OK?
L
L:
")A
44-
IS
Temperature Upon
Receipt- C�
I)X
Dechlorination
Method of
(<0.5APm)_of Ammonia, Cyanide,
Phenol and TKN samplesmust be done in the field prior to preservation.
Comments:
Compositor#
Shipment:
ups
Fed Ex
Are these results for regulatory purposes? Yes
4�5 No IZI
Report results in: mg/L
_LJu9#_
mg/kg E.� ug/L
MHand Delivery
Relinquished br. KY 8L) C Date: •
Time:
Received by:
Date:
Time:
Other
Relinquished by: Date:
Time:
Received by:
Date-,
Time:
Relinquished by: Date-
'rime:
Reel Lab � I
Ir 4 A.,
Dte,

FECAL DATA SHEET
Lab result
Log
20101
4.30
Min 15000
15000
4.18
Max 24876
19608
4.29
Geometric Mean 18724
16,867
4.23
16588
4.22
19608
4.29
24876
4.40
Average
4.27

M erite ch, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland Report Date: 5/20/2019
Client: Synagro
284 Boger Road Project: Eden
Mocksville, NC 27028 Date Sample Rcvd; 4/15/2019
Vector Attraction Reduction / Aerobically Digested Sludge (3 a Day Test)
Meritech Work Order # 04151918 Sample: Eden Grab 4/15/19
Total Solids Volatile Solids % Volatile Solids
Week 1 1.27 0,670 0526
Week 2 1.02 0.550 0.539
Week 3 1.12 0,590 0,523
Week 4 1.16 0,590 0.507
Week 5 1,37
Van lfleeck Reduction (%): -9.30
14YEAUIl
0.539
I hereby certify that I have reviewed and approve these data. /U't?
Labor yRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel,[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#; -- _
Client: s .' Phone:
Address: F,,,)GSTL FI—WM Fax:
Email:
Project:
Attention: ��}'dm_�I��t,r1 Turn Around Time*
How Would you like our report sent? RLlSEi work'needs prior approval,
� v � C araesADalv
Std soda s) 3-S Da s 24-48Hrs
Circle all that apply: Email l referred) , Fax, Mail
`�""MERI�"O
p 1 �4r INC'
ENVIRONMENTAL LABORATORIES
642 Tarnco Rd. Phone: [phone]
- Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates �e Times
t} Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Comp. ,
Grab?
#nt
Cont.
Test(s) -(s) Require
ce?
Yes No
pH OK?
Cl OK?
Date
Time
Date
Time
Temperature upon
Receipt: &1---
Method of
Shipment:
*** Dechlorination ([0.5 ppm) of Ammenia, Cyanide, phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor#
UPS
Jug#
Fed Ex
Are these results for regulatory purposes? Yes 7. No
Report results in: mg/i_ mg/kg � ug/L Ea
Hand Delivery
Relinquished by: K.VWDate' `is-jq Time: ��
�;z•��
Received by: Date: Time:
Other
Relinquished by: Date: Time:
Received by: Date: Time;
Relinquished by. Date: rime:

%VS R
(older, more conservative method)
%VS in F 1.270Q Enter in
%VS out 1.3700 -4 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 21.28
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR=
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number
WWTP Name: Mebane Bride WWTP NPDES Number:
Monitoring Period: From 07/01/19 To 09/30/19
WQ 0003035
NC 0025071
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A;
All. I/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if onnl —M. 4n olfwrn 9l ivw —f--A WT... A nr Clace Rl rum nlwtw thw Winwintr mnnitnrinu [Iota -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl0 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
421
543
883
CFU/g
0
4/yr
Grab
9222 D
CFU
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
colifonn)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt, 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Att. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt, 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
_Melinda Ward, WWTP Superintendent
Preparer name And Title (print or typ1A
��i e, -0Z
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Page 1
Contact: Mate Roth
Report Date:
8/2/2019
Client: Synagro
284 Boger Road
Project:
Eden
Mocksville, NC 27028
Date Sample Rcvd:
7/24/2019
Meritech Work Order H.
07241984
Sample: Eden Fecals Fecal 1 Grab
7/24/19
Parameters
Results
Analysis Date
Reporting limit
Method
% Total Solids
21.6 %
7/25/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
421 col/g dry wt 7/24/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
07241985
Sample: Eden Fecals Fecal 2 Grab
7/24/19
Parameters
Results
Analysis Date
Reporting Limit
Metho
% Total Solids
20.7 %
7/25/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
878 col/g drywt 7/24/19
258 col/g dry wt
SM 9222D
Meritech Work Order #
07241986
Sample: Eden Fecals Fecal 3 Grab
7/24/19
Parameters
Results
Analysis Date
Reporting limit
Method
% Total Solids
19.9 %
7/25/19
0-100 %
SM 254-0B
Fecal Coliform (Sludge)
<457 col/g dry wt 7/24/19
457 col/g dry wt
SM 9222D
Meritech Work Order #
07241987
Sample: Eden Fecals Fecal 4 Grab
7/24/19
Parameters
Results
Analvsis DateDat
Reporting Limit
Method
% Total Solids
20.5 %
7/25/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
443 col/g drywt
7/24/19
258 col/g drywt
SM 9222D
Meritech Work Order # 07241988 Sample: Eden Fecals Fecal 5 Grab 7/24/19
Parameters Results Analysis Date Re o tin Limit et o
% Total Solids 20.6 % 7/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) 883 col/g drywt 7/24/19 258 col/g drywt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 8/2/2019
Project. Eden
Date Sample RcVd: 7/24/2019
Meritech Work Order # 07241989 Sample: Eden Petals Fecal 6 Grab 7/24/19
Parameters Results Analysis Date Reporting Li it Method
Total Solids 20.4 % 7/25/19 0-100 % SM 2540E
Fecal Coliform (Sludge) <446 col/g dry wt 7/24/19 446 col/g dry wt SM 9222D
Meritech Work Order # 07241990 Sample: Eden Fecals Fecal 7 Crab 7/24/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
19.1 %
7/25/19
0-100 %
SM 2S40B
Fecal Coliform (Sludge)
<476 col/g dry wt
7/24/19
476 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. oha it.abaratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#:
Client: Phone:
Address: '7 9A � Z Fax:
to ip LLf Vi L" NIL Email. e ie,). CXA
Project: db2 rq
P-O-#-
Attention: Tum ArGund Time*
*RUSH work needs prior approval,
How would you like your report sent? arkps AnDIv
Std 10 JKs) 3-5 Da sI 24-481-Irs
Circle all that apply - Email I referred), Fax, Mail ---
L--J I
41 MERITECH, INC
-J) ,
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 2732G Fax-. 336-342-1522
Email: irifu@meritechiabs-com
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Vgn/Pff3fF-
Lab Use Only
Start
End
Comp?
Grab?
#of
Cant.
Test(s)
Required
On Ice?
Yes No
pH OK?
Cl OK?
Date
Time
Date
Time
q7LS
M4L LoLi FqZly� <
Vz
7
Temperature Upon
r.
Receipt; i-.-
ii.
Method of
Shipment:
Dechlorination (<0.5 ppm) of'Amonla, Cyanide, Phenol and TKN samples
must be done in the field priorto preservation,
Comments:
Compositor#
Jug#�
U'. UPS
Fed Ex
U'Hand Delivery
Are these results for regulatory purposes? Yes No
-
Relinquished by; Date�j Tim e:
Report results in: mgiL mg/kg 1� ug/i- El,
Received by., Date: Time:
Other
Relinquished by: Date: Time:
Rdceived by: Date: Time:
Relinquished by; Date: Time:
,6'- L' I
Id"

Lab result
421
878
457
443
883
443
476
Average
Log
2.62
2.94
2.66
2.65
2.95
2.65
2.68
2.73
FECAL DATA SHEET
Min 421
Max 883
Geometric Mean 543

Mearltech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland Report Date: 8/29/2019
Client: Synagro
284 Boger Road Project; Eden
Mocksville, NC 27028 Date Sample Revd: 7/24/2019
Vector Attraction Reduction Aerobically Digested Sludge 30 Da Test
Meritech Work Order # 07241991 Sample: Eden Composite 7/24/19
Total Solids
Volatile Solids
Week
0.570
0.290
Week 22
0.71.0
0.390
Week 3
0.650
0.320
Week
0.440
0.220
Week 5 0.530 0.260
Van Kleeck Reduction (%): 8.13
Me Volatile Solids
0.508
0.547
0.497
0.505
0.487
I hereby certify that I have reviewed and approve these data. - ff ".. ..
,Lab ratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
teL[phone] fax.[phone]

8;9/15 Chain of Custody Record (COC)
NPDES#:
Client: 'SY J WZ�2 Phone:
Address:- `ZTlq rpCC-i9L Fax:
Email. C4,
Project: rf)RJ
P.O.#:
Attention- 9"(AAJ g&Q Turn Around Time*
*RUSH work heads prior approval,
How would you like —your report sent? Std (10 Char esA [— rs
LO d ,6s) 3 .5 0 s 1 24-48 H
Circle all that apply: erred}, Fax, Will ff 'J' mail
p(pr = . J
MERITECH, INC,
N
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: info@ meritechlabs.corn
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Camp?
Grab?
#of
Cont.:
Test(s) Required
an Ice?
!Yes I NO
pH OK?
Cl OK?
Date
Time
Date
Time
LO&i -SE)DAY
-712,ij
4-
G)trr-LA&�
7foj I q
15f 03
Temperature Upon
Receipt
Method of
Shipment:
Dechlorlin2tion (<0.5 PPm) of Ammonia, Cyanide, Phvnol and TKN samples must be done linthe field prior to presprvatinn-
Comments:
:Compositor#
UPS
Jug#
Fed Ex
z
Are these results for regulatory purposes? rposes? Yes No
Report results in; rng/L mglkg ug/L
Z'Hand Delivery
Relinquished by: Date---711Time_'-
"Pz,,,j 1!5:- AXI 5
Received by: Date. Time:
Other
Relinquished by: Date: Time:
Received by: Date: Time;
Relinquished by; Date: Time:
Re y Da
7 134

%VSR
(older, more conservative method)
%VS in 0.5080 Enter in
%VS out 0.4870 ' decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 8.a6
(method from p. 132 of WH manual)
%VSR-_ (%VS in - %VS out)
%VS in
%VSR= 4.13
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035
WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071
Monitoring Period: From I0/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1 /A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt, 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlioahia fn alfarnafive nnrfnrmPrl (f lace A nr Cincc li) emmnfefe the fnlinwina mnnifnrino riatac
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl 0 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
73684
96221
135135
CFU/g
0
4/yr
Grab
9222D
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107)
- Please indicate optionlalternative performed:
0ption/Alt, I
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying --- Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"T certify, under penalty of law, that the pathogen requirements in 40 CPR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
_Melinda Ward, WWTP Superintendent
Prep rer Name and Title
, ( t� J-
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503,9(r) and 15A NCAC 2T.1102 (26)

Page 1
Contact: Nate Roth
Report Date:
11/21/2019
Client: Synagro
284 Boger Road
Project:
Eden
MocksviIle, NC 27028
Date Sample Rcvd:
11/12/2019
Meritech Work Order # 11121918 Sample: Eden 1 Grab
11/12/19
Parameters Results Analysis Date
Reporting Limit
Method
% Total Solids 18.7 % 11/15/19
0-100 %
SM 2S40B
Fecal Coliform (Sludge) 96,257 coI/g dry wt 11/12/19
508 col/gdrywt
SM 9222D
Meritech Work Order # 11121919 Sample: Eden 2 Grab 11/12/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.2 % 11/1S/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 93,750 col/g dry wt 11/12/19 SO col/g dry wt SM 9222D
Meritech Work Order # 11121920 Sample: Eden 3 Grab 11/12/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 18.6 % 11/1S/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 91,398 col/g dry wt 11/12/19 S08 col/g dry wt SM 9222D
Meritech Work Order #
11121921
Sample: Eden 4 Grab
11/12/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
18.2 %
11/15/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
120,879 col/g dry wt 11/12/19
508 cal/g dry wt
SM 9222D
Meritech Work Order #
11121922
Sample: Eden 5 Grab
11/12/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
19.0 %
11/15/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
73,684 col/g dry wt 11/12/19
508 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Nate Roth
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Report Date: 11/21/2019
Project: Eden
Date Sample Rcvd: 11/12/2019
Meritech Work Order # 11121923 Sample: Eden 6 Grab 11/12/19
Parameters Remits Analysis Date Reporting Limit Method
% Total Solids
18.5 %
11/15/19
0-100 %
SM 2540E
Fecal Coliform (Sludge)
135,135 col/g dry wt
11/12/19
508 col/g dry wt
SM 9222D
Meritech Work Order # 11121924 Sample: Eden 7 Grab
11/12/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
19.5 %
11/15/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
76,923 col/g drywt
11/12/19
494 col/g drywt
SM 9222D
I hereby certify thatf have reviewed and approve these data. L'�' -"?�
L boratoTyRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] faxz.[phone]

Chain of Custody Record (COC) NPDES#:
MERITECH INC.Client:`?N�CsYiU Phone:(,�Lb7
Address:iB 6pr,Gr--1 �"so Fax:
ENVIRONMENTAL LABORATORIES ' ul AJL Email: 6tz maLUY) CoS ")U4 42').
6 642 Tamco Rd. Phone: [phone] Project: 66e'i
Reidsville NC 27320 Fax: 336-342-IS22
P.O.#:
Email: [e-mail] Attention: Z'[ `) -
Turn Around Time*
How would you like your report sent? *Rusin work needs prior approval.
WWW.meritechlabs.Cam Circle all that apply: mail preferred), Fax, Mail std io a s} 3 5 DavS zfas
Sampling Dates & Times Person Taking Sample (Sign/Prin p� I Lab IUse Only
r
Sample Location and/or ID # Start End
Comp? q u i red On lc Ye pH OiC?
Date Time Date Time Crab? Cont.nt Test(s) Required
/ No Cl Oi<?
Z
4 a'
Temperature upon Receipt:
Method of *** i7echlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
I� ***
Shi ment: Comments: Compositor#
❑ UPS Jug #
❑ Fed EX Are these results for regulatory purposes? Yes No ❑ Report results In: mg/L ❑ mg/kg ❑ ug/L ❑
Relinquished by: Date: Time:
Hand Delivery � r! lZ�� L '7!0 Received by; pate: Time:
❑ Other Relinquished by: Date: Time: Received by: Date: Time:
Relinquished by: Date: Time: Re y b: Cite~ Ti 1.

FECAL DATA SHEET
Lab result
Log
96,257
4.98
Min
93,750
4.97
Max
91,398
4.96
Geometric Mean
120,879
5.08
73,684
4.87
135,135
5.13
76,923
4.89
Average
4.98
73684
135135
96221

Contact: Ryan Copeland Report Date: 12/17/2019
Client: Synagro
284 Roger Road Project: Eden
MocksvilIe, NC 27028 Date Sample Rcvd: 11/12/2019
Vector Attraction Reduction /Aerobically Digested Sludge 30 Day Test
Meritech Work Order## 11121917 Sample: Eden Grab 11/12/19
Total Solids Volatile Solids Yo Volatile Solids
Week 1 0.910 0.500 0.544
Week 2
0.840
0.460
0.542
Week 3
0.440
0.240
0.554
Week 4
0.530
0.300
0.567
Week 5
0.700
0.360
0.512
Van Kleeck Reduction (%): 12.01
I hereby certify that I have reviewed and approve these data. CipALVarIt#RhepreiZntatve
642 Tamco Road, Reidsville, North. Carolina 27320
tel.[phone] fax.[phone]

5.9.�06
Chain of Custody Record (CDC)
NPDES#:
M ERITEH,
Client: i11dla } -.i,� Phone:dxL �� ]�
��,,�
f r
Address: �-�iW �Z,:�-��1�; Fax.
ENVIRONMENTAL LABORATORIES
Email:._ra+��'E
LC �VJ
642 Tamco Rd. Phone: [phone]
Project: 0GN
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: L.�'[ IV - �LL��1'
Turn Around Time*
How would you like your report sent? *RUSH
work needs prior approval.
www.meritechlabs.corn
Circle all that apply;(Em�lpreferred], Fax, Mail Std 10
s] �_s_n�,�s 24�as�Hrs
Sampling Dates &Times
Person Taking Sample (Sign/Printl: ��r, _ ti
�I �
Lab Use Only
Sample Location
and/or ID #
Start End
Date
Comp? #of YeS
! Required
on ceps pH OK?
Time Date Time
Grab? Cont. L4S}
LCl
OK?
ll / 1 1�!
c�4 �i ! u�i '� J !�� 1
�. 1 f5` / I
�L.,. 1 Vf %�W14•. 1�� �C's r� I.j����i1�frS.�i
Temperature Upon Receipt:
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
1 �
L . 7
Shipment:
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
No ❑ Report results in: mg/L ❑ mg/kg
❑ ug/L ❑
Hand Delivery
Relinquished by: Date: Time:
r . ? Received b y. Date:
Timp;
❑ Other
Relinquished by: Date: Tirne:
Received by: Date:
Time:
Relinquished by: Date: Time:
R� by L

%VS R
(older, more conservative method)
%VS In 0.5440 Enter in
%VS out 0.5120 " * decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 12A5
(method from p.132 of WH manual)
%VSR= (%VS In - %VS out)
%VS in
%VSR= 5.88
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project:
EDEN
Fi led
Soil
Lime Requirement
Tons/Acre
Date Applied
(state -county -site -field)
pH
(from soil analysis)
Applied
NC-RC-11-01
6.0
0.0 tonslac.
NC-RC-11-02
6.7
0.0 tonslac.
NC-RC-11-06
6.6
0.0 tonslac.
NC-RC-26-1 B
6.4
0.0 tonslac.
NC-RC-26-2A
5.0
1.2 tons/ ac.
1.5TIAcre
Ordered*
NC-RC-26-03
5.9
0.0 tonslac.
NC-RC-26-05
5.6
0.5 tonslac.
1TIAcre
Ordered*
NC-RC-26-06
6.7
0.0 tonslac.
NC-RC-105-03
5.9
0.6 tonslac.
NC-RC-105-04
6.6
0.5 tonslac.
1TIAcre
12/10/19
NC-RC-117-01
1 6.0
0.0 tonslac.
* Ag lime will be applied once field and crop conditions are suitable

SECTION 7

Page 1 of 1
Report No: 19-347-0513
Account No: 07216
Advisor: Synagro Central LLC/ Durham
Mary Brewer
284 Boger Road
Mocksvhle NC 27028
Waypoint(D
ANALYTICAL
Client: Gray Tuttle
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointana lytica l.com
Farm: RC-11
Submitted By: Synagro Central LLCI Durham
Date Received: 12/1312019
Date of Report: 12/1612019
Lab No
Field Ib
Sample ID
Soil Class
HM% WIV
pH
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO N
21344
Ed 126
RC-11-1
MIN
0.7
6.0
70.0
174
30
50
206
375
375
125
74.2
6
4
1
CA
0.1
21345
FId 126
RC-11-2
ORG
7.9
6.7
70.0
97
30
29
163
155
257
95
74.3
6
5
1
0.1
0.1
21346
FId 126
RC-11-6
M-0
4.8
6.6
70.0
128
36
23
169
198
247
115
74.4
6
5
1
0.1
0.1
Comment:
Test result units = CEC and Na in meq/100cm3; ND3 N in mgldm3; WIV in glom3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY19-SL033836
Predictive
Client:
Aumen French
Advisor:
Hunter Copeland
C11,
°G
1612 Crutchfield Rd 1 1944
502 US 13 N
`
So Report
Mehlich-3 Extraction
Wentworth St
Windsor, NC 27983
wP
Reidsville, NC 27320
,c
Links to Helpful Information
Sampled.
Not Provided
Sampled County: Rockingham
Received:
06117/2019
Farm: RC-26
Completed:
06/20/2019
Client [D: 214285
Advisor ID: 493394
Sample ]D: RC261 B
Recommendations:
lime
Nutrients (Iblacre)
More
Crop
(tonslacre)
N P2O5
K7O Mg S
Mn Zn
Cu B
Information
Lime History:
1- FescuelOGrassiTim, M
0.0
120-200 0
30 0 0
0 0
0 0
Note: 12
2 -
0.0
Test Results [units - WN in glcrrr ; CEC and Na in megll00 cO; NO3-N in mgldaj:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1 Mn-1 Mn-All Mn-Al2
Zn-I Zn-AI
Cu-1 Na ESP
SS4 NO3-N
0.81 0.89
10.4 90 1.0 6.4
182 56
61 27
69 612 378
377 377
1357 0.2 2
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a qrant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.govlagronornil
Report No. FY19-SLO33836
Aumen French
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
AG
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or lb11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib11000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CFC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-1
M-O
manganese index
mineral -organic soil class
notations appear on the soil report, refer to Mote: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm,
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib11000 sq ft . If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmt###ind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 JP -I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/a gronomi/uyrst.htm

Page 1 of 1
Report No: 19-347-0523
Account No: 07216
Advisor: Synagro Central Ll.Cl Durham
Mary Brewer
284 Boger Road
Mocksville NC 27028
Waypoel t-..
ANALYTICAL
Client: Auman French
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: RC-26
Submitted By: Synagro Central LLCI Durham
Date Received: 12/13/2019
Date of Report: 12/16/2019
Lab No
Field ID
Sample ID
Soil Class
MM% WN
p14
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 NO3 N
21367
Fld 2-6
RC-26-2A
MIN
2.3
5.0
70.0
100
37
62
56
173
173
820
72.6
4
2
1
0.1
0
21368
Fld 2-6
RC-26-3
MIN
0.8
5.9
70.0
170
51
23
75
130
130
795
73.0
4
3
1
0.1
0.1
21369
Fld 2-6
RC-26-5
MIN
0.9
5.6
70.0
110
39
31
175
163
163
590
73A
5
3
1
0.1
0.1
21370
Fld 2-6
RC-26-6
MIN
0.7
6.7
70.0
22
50
21
256
143
143
60
73.6
5
3
2
0.1
0.1
Comment
Test result units = CEC and Na in meg/100cm3; NO3 N In mgldm3; WN in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: VVaypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-347-0528
Account No: 07216
Advisor: Synagro Central LLC! Durham
Mary Brewer
284 Boger Road
Mocicsville NC 27028
Waypoeinto
ANALYTICAL
Client: Barry Knight
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: RC-105
Submitted By: Synagro Central LLC/ Durham
Date Received: 12/13/2019
Date of Report: 12116/2019
ab No
Field ID
Sample 1D
Soil Class
HM% WN
pH
Ac
P-1
K-1
S-1
Mn-1
Zn-1
Zn-Al
Cu-1
CEC
BS%
Ca%
Mg%
ESP
Na SS-1 ND3 N
11384
Rd 3-4
RC-105-3
MIN
1.6
5.9
70.0
151
32
37
644
34C
340
1230
76.4
8
5
3
0.1
01
11386
Fld 3-4
RC-105-4
MIN
2.0
5.6
70.0
182
43
46
306
515
515
2040
75.8
8
5
2
0.1
0.1
Comment:
Test result units = CEC and Na in meg1100cm3; NO3 N in mgldm3; WN in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomil
Report No. FY19-SL033837
Predictive Client:
Charles Obryant
Advisor:
Hunter Copeland
456 Waynick Road
502 US 13 N
Mehlich-3 Extraction
Soil Rep®rt
Reidsville, NC 27320
Windsor, NC 27983
Sampled County: Rockingham
m Links to He Information Sampled: Not Provided
ohi�
Received: 06/17/2019
Farm: RC-17 Completed: 06/20/2019
Client ID. 499521
Advisor ID: 493394
Sample ID: RC17-1
Recommendations: Lime
Nutrients (Iblacre)
More
Crop (tonslacre) N P205
K2O Mg S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrasslTim, M 0.0 120-200 0
70 0 0
0 0
0 0
Note: 12
2 - 0.0
Test Results ]units - WIV in glcm3; CEC and Na in meg11OO crrr3; NO3-N in mg1drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
0.60 0,86 11.0 86 1.6 6.0 327 32 62 22
53 134 97
821 821
1579 0.1 1
North Carolina
r-.
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
beinq funded throuqh a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCCA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomil
Deport No. FY19-SL033837
Charles Obryant
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib11000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib11000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. if MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. if Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-0
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of IbI1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm #sFind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WIV
weight per volume
The first seven values [soil class, HM%, WIV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 JP -I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-!
zinc index
available)] indicate levels of plant nutrients or other fertility measurement_ Visit www.ncagr.Qov/acpronomi/uvrst.htm