WQ0034688_Residual Annual Report 2019_20200302

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 3/2/2020
Received:*
Project Number* WQ0034688
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Lysa Finnerty
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0034688
ApplicantTermittee * SYNAGRO
Phone Number*
4434899026
Facility Name * Neuse Regional Water and Sewer Authority
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2019 Annual Report for Neuse Regional Water and Sewer Authority
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
NEUSE NC 2019 Annual Report FINAL.pdf 10.83MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/27/2020

435 1Villiams Court, Suite 100
Baltimore, iv117 21220
www. synagro.com
FEBRUARY 27, 2020
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2019 Annual Report for Permit No. WQ0034688
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the alcove referenced report on
behalf of Neuse Regional Water and Sewer Authority, NC.
If you have any questions or need additional information, please do not hesitate to contact
Charlie Colic at [phone] or Melinda Boyd at 336-909-8627.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Charlie Colie, Neuse Regional Water and Sewer Authoriy
Melinda Boyd, Synagro
YOUR PARTNER FORA CLEANER, GREENER WORLD

NEUSE REGIONAL WATER AND SEWER
AUTHORITY
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0034688
2019 ANNUAL REPORT

Neuse Regional Water and Sewer Authority, NC
Residuals Land Application Program
2019 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: M0034688 County Lenoir Year 2019
Facility Name (asshown on permit) Neuse Regional Water Treatment Plant NPDES No. NCO0881 I l
Land Application Operator Synanro _ Phone# [phone]
Land application of residuals as allowed by the above pennit occurred during the past calendar year?
X YES NO. If NO, skip Pat A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how tlhe residuals were handled.
Part A — Residuals_Annlic-ation Stlmnjw Y:
Total number of application fields in die permit: N/A
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 291,56
'Dotal number of acres utilized for land application during die year: 159.6
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 201919 with all conditions of the land application pennit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YF,S NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this pennit were applied to due permitted sites.
2. Soil plI was adjusted as specified in the pennit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residwils during; the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the pennit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part: 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T . 1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the pennit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations arc
attached to include appropriate actions and renhediations.
11. Vegetative cover was maintained and proper crop management was perforned on each site receiving residuals, as specified
in tie pennit.
12. No nmoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C -T Certification:
'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that Here are significant penalties for subiidtting false infonuation, including the possibility of fines and imprisonment for
knowing violations."
Harold Herring, Executive Director
Pennittee Name and "fitle (type or print)
yaL ot-5 Fre-R e.(-
Signature of Preparer* VDate
(if different from Pennittoe)
f
z�
ignatare of Pennittee Date
A&6LE4 o
Signature of Land Applier Date
(if different from Pennittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2019 ANNUAL OPERATIONS SUMMARY -LAND APPLICATION IN NC
NEUSE REGIONAL WASA, NC
NEUSE REGIONAL WASA, NC WTP LIQUID
MONTHNEAR
January 2019
October 2019
YEARLY TOTAL
AMOUNT UNIT
3,849,300.00 G
2,759,400,00 G
6,608,700.00 G
DRY TONS UNIT
260.04 D
31.52 D
291.56 D
DRY METRIC
TONS
235.85
28.61
264.46
1 /30/2020

SECTION 2

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0034688
Facility Name. NEUSE REGIONAL WASA, NC
NPDES# : NCO088111
or WQ# (residua! only)
WWTP Name: NEUSE REGIONAL WASA WTP
Residuals Analysis Data
Product Type
WPL
WFL
WPL
Date Sampled (grab) or 08/16/16
04/26/19
10/15/19
Date Composited
Percent Solids
62
0.50
0.274
PARAMETERS (mglkg dry weight)
Arsenic
11.9
<8.38
<30
Cadmium
<1
<1.68
<7.6
Mercury 0.0749
0.0752
<7
Chromium
66.1
25.9
27
Copper
827
363
270
Lead
15
17.1
<27
Molybdenum
<2.5
<4.19
<60
Nickel
16.5
13.3
<63
Selenium
<5
<8.3 8
<4 9
Zinc
83.8
75
140
Total Phosphorus
2820
2170
2900
TKN
58600
<250
15000
Ammonia -Nitrogen
3790
<100
170C
Nitrate and Nitrite
414
<4. 92
21C
Laboratory
Waypoint Analytical Virginia Inc.
SHEALY ENVIRONMENTAL SERVICES INC.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
M
(SIGNATURE OF PREP
Date__.
DENR FORM RSSF (512003) Printed: Wednesday - February 72 2020 at 10:10:51 for. 1703 01

ANNUALS RESIDUALS SAMPLING SUMMITRY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0034688
Facility Name: NEUSE REGIONAL WASA, NC
NPDES# : NCO088111
or WQ# (residual only)
WWTP Name: NEUSE REGIONAL WASA WTP
Residuals Analysis Data
Product Type yip;,
WPL
WPL
Date Sampled (grab) or 08/16/? 8
04/26/19
10/15/19
Date Composited
Percent Solids 1.62
0.50
0.274
PARAMETERS (d glkg dry weight)
Aluminum 134000
112000
1.90000
Calcium 3560
2970
<3700
Magnesium 1170
1280
<3700
pH 7.40
6.30
6.20
Potassium 757
1.020
<3700
Sodium 748
1380
<3700
Laboratory
WaypointAnalytica[ Virgin [a Inc.
SHEALY ENVIRONMENTAL SERVICES INC,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penaities for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Ki
NR - Data Not Reported or Data Not Required
Date �zo
DENR FORM RSSF-B (712002) Printed: Wednesday - February 12 2020 at 10:11.09 for. 1703 01

JA
Waypoinc,
iUALYTIUL
9/4/2018
Synagro Central LLC/ Neuse Reg WASA
Marshall Puryear
284 Boger Road
Suite 204
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-234-0204
Project Description: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-940 O Fax [phone]
www.waypointanalytical.com
Dear Marshall Puryear:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/22/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P. P, u-7-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratorys option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007

ANALYTICAL
Waypointo
Report Number: 18-234-0204
Client Project Description: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
62374
NRWASA
Solids
08/161201813:15
08/22/2018
62374
NRWASA
Solids
081161201813:15
08/22/2018
SM-4500-NH3C
WTN
62374
NRWASA
Solids
081161201813:15
08/22/2018
9045D
WTN
62374
NRWASA
Solids
08/16/201813:15
08/22/2018
4500NO3F-2011
WTN
62374
NRWASA
Solids
08/16/201813:15
08/2212018
6010D
WTN
62374
NRWASA
Solids
08/16/201813:15
08/22/2018
SW-7471B
WTN
62374
NRWASA
Solids
08/16/201813:15
08/22/2018
SM-4500-NH3C-TKN
WTN
62374
NRWASA
Solids
08/16/201813:15
08/22/2018
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
P�no') '-�fR

Report Number: 18-234-0204
Account Number: 00454
Submitted By: Melinda Boyd
Send To. Synagro Central LLC/ Neuse Reg WASA
Marshall Puryear
284 Boger Road
Suite 204
Mocksville , NC 27028
Lab Number: 62374
Sample Id : NRWASA
Project: NRWASA
REPORT OFANALYSIS
7621 Whitepine Roars, Richmond, VA 23237
Main 804-743-94€1 ° Fax [phone]
www.waypointarvalytical.com
Date Sampled: 8/16/2018 13:15:00
Date Received: 08/22/2018 00:00
Date Reported: 09/04/2018
Total Solids
1.62
16200
1000
CJH
08/24/2018 18:52
SM-2540G
Moisture *
98.40
1000
CJH
08/24/2018 18:52
SM-254OG
Total Kjeldahl Nitrogen
58600
472
CLP
08/29/2018 13:00
SM-4500-NH3C-TKN
Phosphorus
0.28
2820
50.0
JTR
08/31/2018 04:44
601OD
Potassium
0.08
757
50.0
JTR
08/31/2018 04:44
6010D
Sulfur
0.77
7720
50.0
JTR
08/31/2018 04:44
6010D
Calcium
0.36
3560
100
JTR
08/31/2018 04:44
6010D
Magnesium
0.12
1170
50.0
JTR
08/31/2018 04:44
601OD
Sodium
0.07
748
250
JTR
08/31/2018 04:44
601OD
Iron
27400
50.0
JTR
08131/2018 04:44
601OD
Aluminum
134000
500
BKN
08/31/201812:41
6010D
Manganese
3650
5.00
JTR
08131/201804:44
6010D
Copper
827
2.50
JTR
08/31/2018 04:44
6010D
Zinc
83.8
5.00
JTR
08/31/2018 04:44
6010D
Ammonia Nitrogen
3790
25.0
ZBD
08/29/2018 09:30
SM-4500-NH3C
Organic N
54810
472
08/29/2018 09:30
CALCULATION
Nitrate+Nitrite-N
414
4.94
ZBD
08/28/201814:46
4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
owr
Our reoor is a,^r; !efr2rs are, for rt - amn;usrv? ,.I,! cnn;ide,
ria! usF Of uur c?i0; 7rs.
and gray roi be ranroauced !n
hoM- or part. ,-?Or may any
reiererce 6,- made
to tha work, i/ a rssu!rs, er fl-e con pang in any e;cv jSirag'
.^,evvs ie+ease. o: oPh
riqu�frC-nonovrx.& rmenrs ✓:,
out obfain.;r � our prior L, rifien aurnorizaLan.
Pauric McGroary
Agronomist
0ars a :t r,f w

Report Number: 18-234-0204
Account Number: 00454
Submitted By- Melinda Boyd
Send To: Synagro Central LLC/ Neuse Reg WASA
Marshall Puryear
284 Boger Road
Suite 204
MocksWle , NC 27028
Lab Number; 62374
Sample Id : NRWASA
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Molybdenum
Comments:
Project. NRWASA
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Date Sampled: 8/16/2018 13:15:00
Date Received: 08/22/2018 00:00
Date Reported: 09/04/2018
<1.00
1.00
JTR
08/31/2018 04:44
6010D
66.1
2.50
JTR
08/31/2018 04:44
601 OD
16.5
2.50
JTR
08/31/2018 04:44
601 OD
15.0
3.00
JTR
08131/2018 04:44
601 OD
11.9
5.00
JTR
08/31/2018 04.44
601 OD
0.0749
0.0157
KKM
08/27/2018 12:30
SW-7471 B
<5.00
5.00
JTR
08131 /2018 04:44
601 OD
7.4
JSL
08/30/2018 08:09
9045D
<2.50
2.50
JTR
08/31/2018 04:44
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Ljur rpo,7s a,,^d fatiars are for the exciuswe at d Cn_ n`ic'sntial usa G" ao ' eGenis. end mar✓ not be reps c+ced ?n whole or part. nor may � 3 reiare Ce e s adc
to the war , the results, nr the coy -'pa lV if-,an}�� >e �slnri, r!Eu s rr lease. or olherpublic announcemems r,itt:out obt mina our par or Written authoezation.
Pauric McGroary
Agronomist
�� A r,f

Cooler Receipt Form
Customer Number: 00454
Customer Name: Synagro Central LLC/ Neuse Reg WASA
Report Number: 18-234-0204
Shipping Method
(� Fed Ex US Postal 0 Lab 0 Other
UPS (J Client (-) Courier Thermometer ID: I
Shipping container/cooler uncompromised? Yes (_) No
Number of coolers received F1
Custody seals intact on shipping contain erlcooler? 0 Yes 0 No ® Not Required
Custody seals intact on sample bottles? 0 Yes (] No Not Required
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
(,) No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
p g
Y . "--
� es
0 No
Cooler temperature in compliance?
0 Yes
(D No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
L Yes
C) No
0 N/A
Water - VOA vials free of headspace
0 Yes
C) No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
C) Yes
(-) No
0 N/A
High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson -------- Date & Time: 8/22/2018 12:59:32
P nri' Py rif A

Phone: i
A & L CUSTOMER
LAS # SAMPLE I.D.
Relinquished by Sampler:
noto
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTf ONS:
For— C
SAMPLING
SAMPLE
LOCA' ION
TYPE
� a nloo,
!L
monitoring purposes.
IN I HE111111111(�� -0204AIN OF CUSTODY
Svnaa2018 perro Central LLC! Neuse Pea WASA �8 ��-+ �, I
NRWASA 12:58:37 E
CORD
-------------
were used during the collection of o se sampjes.
SAPvIP LER
# OF SAMPLING METHOD METHOD
CONTAINERS DATE TIME PRESERVED SHIPPED
4P f a (00Ler
4
Date Time Recieved by:
REMARKS:
D e Time R y.o
Ddte J Time Red ed by: a
SAMPLE
9,1r9. SLR SL2 NN NI Cr$II ANi
OS
ANALYSIS REQuEsT
orm-E-Svi
SLI, Total Solids (Wstu?e), TOtal Kieldahi nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Maricga.nese, Copper and Zinc
PR ] CaC0,1 Volatile]
J equly, Solids I Nip C9 ND2 iV

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample pate ReportRange Ratio
1703-01-WPI_-NC NEUSE REGIONAL WASA, NC WI'P LIQUID 8116=18 10111201B-1/3112019 0-3527
Na mg/1 = (Na mglkg x % Solids) ,.100 ~ (748 x 1,6200) + 100 = 12.1176
Ca rng/l = (Ca mglkg x % Solids) + 100 = (3560 x 1.6200) + 100 = 57,672
Mg mgli = (mg mglkg x % Solids) + 100 = (1170 x 1,6200) + 100=18.954
Na meq = Ne mg/1 + Molec,Wgt,Na = 12.1176 + 23 = 0,526852
Ca meq = Ca M911 + Molec.Wgt.Ca = 57.672 + 20 = 2.8836
Mg meq = Mg mg/1 + Molec.Wgt.Mg = 18.954 + 12 = 1.6796
SAR = Na meq + SgrRoct[0.5 x (Ca meq + Mg maq)] = 0.526852 + SgrRoot[0.5(2.8836+1.6795)] = 0.352684
Printed: 2/12/2020
Page 1
10:11

Waypoint,o
ANALYTICAL
5/9/2019
Synagro-ADM
Jeff: Spencer
1730 East Moore Street SE
SouthPort, NC, 28461
Ref: Analytical Testing
Report Number: 19-121-1027
Project Description: NR2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax [phone]
www.waypointanalytical.com
Dear Jeff Spencer:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/1/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. .
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
4ewa X,Gar
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Page 1 of 6

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-121-1027
Client Project Description: N1112
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
66127
NR2
Solids
04/26/201911:35
05/01/2019
66127
NR2
Solids
04/26/201911:35
05/01/2019
SM-4500-NH3C
WTN
66127
NR2
Solids
04/26/201911:35
05/01/2019
9045D
WTN
66127
NR2
Solids
04/26/201911:35
05/01/2019
4500NO3F-2011
WTN
66127
NR2
Solids
04/26/201911:35
05/01/2019
6010D
WTN
66127
NR2
Solids
04/26/201911:35
05/01/2019
SW-74718
WTN
66127
NR2
Solids
04/26/2019 11:35
05/01/2019
SM-4500-NH3C-TKN
WTN
66127
NR2
Solids
04/26/201911:35
05/01/2019
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

Report Number: 19-121-1027
Account Number: 45637
Send To: Synagro-ADM
Jeff Spencer
1730 East Moore Street SE
SouthPort , NC 28461
Lab Number: 66127
Sample Id : NR2
Waypoit
ANALYTICAL
Project: NR2
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 4/26/2019 11:35:00
Date Received: 0510112019 00:00
Date Reported: 05/09/2019
Total Solids
0.50
5000
100.0
ADM
05/02/2019 15:52
Moisture *
99.50
100.0
ADM
05/02/2019 15:52
Total Kjeldahl Nitrogen
<0.03
<250
250
JPJ
05/08/2019 14:30
Phosphorus
0.22
2170
83.8
BKN
05/06/201918:41
Potassium
0.10
1020
83.8
BKN
05/06/201918:41
Sulfur
0.52
5210
83.8
BKN
05/06/201918:41
Calcium
0.30
2970
419
BKN
05/06/201918A1
Magnesium
0.13
1280
83.8
BKN
05/06/201918:41
Sodium
0.14
1380
419
BKN
05/06/201918:41
Iron
26100
83.8
BKN
05/06/201918:41
Aluminum
112000
83.8
BKN
05/06/201918:41
Manganese
1550
8.38
BKN
05/06/201918:41
Copper
363
4.19
BKN
05/06/201918:41
Zinc
75.0
20.9
BKN
05/061201918:41
Ammonia Nitrogen
<0.01
<100
100
JPJ
05/08/2019 10:30
Organic N
0.00
0
250
05/08/2019 10:30
Nitrate+Nitrite-N
<4.92
4.92
ZBD
0510712019 13:27
SM-2540 G
SM-2540 G
SM-4500-NH3C-TKN
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
6010D
SM-4500-NH3C
CALCULATION
4500NO3F-2011
All Values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond Holding Time
porir-
Ac
60wr
Our reports and letters are for the exclusive and confidential use of cur clmnts, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6

Report Number: 19-121-1027
Account Number: 45637
Send To: Synagro-ADM
Jeff Spencer
1730 East Moore Street SE
SouthPort, NC 28461
Lab Number: 66127
Sample Id : NR2
e
Waypoi t
ANALYTICAL
Project . NR2
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticai.com
Date Sampled: 4/26/2019 11:35:00
Date Received: 05/01/2019 00:00
Date Reported: 05/09/2019
Cadmium
<1.68
1.68
BKN
05/06/201918:41
6010D
Chromium
25.9
4.19
BKN
05/06/201913:41
6010D
Nickel
13.3
4.19
BKN
05/06/201918:41
6010D
Lead
17.1
5.03
BKN
05/06/201918:41
6010D
Arsenic
<8.38
8.38
BKN
05/06/201918:41
6010D
Mercury
0.0752
0,0157
TJS
05/06/2019 12:20
SW-7471 B
Selenium
<8.38
8.38
BKN
05/06/201918:41
6010D
pH *
6.3
JSL
05/07/2019 07:08
9045D
Molybdenum
<4.19
4.19
BKN
05/06/201918:41
6010D
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B - Analyte detected in blank
H - Beyond Holding Time
pwir-
m,C 6ew
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary
to the work; the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization,
Agronomist
Page 4 of 6

WayPAoint.,
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 O Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 45637
Customer Name: Synagro-ADM
Report Number: 19-121-1027
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
— 1f
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
0 Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
C) No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: .Brandi Watson I Date & Time: 05101I2019 14:38:37
Page 5 of 6

SAMPLING LOG #
CUSTOMER: SYNAGRO
IIIIIIIIlI11IQlll�llllllllllllllllllllllllllllllllllllllflllllll 19-121_'o27
Mat
3
Synaaro-ADM 05-01-2019 14:
NR2 14:35:03
PROJECTMANAGER:
U �i
Phone: 7
A & L CUSTOMER
SAMPLING
SAMPLE
LAB # SI.D.
LOCATION
TYP E
/��AMPLE
x _
WG1
L
Relinquished by Sampler:
bate Time
Relinquished by: U05
Relinquished by:
SPECIAL INSTRUCTIONS:
For
SAMPLE
e Time
4lA
Time
DMAIN OF CUSTODY
IECORD & ANALY.SUS
RECORD
l attest that the proper field sampling procedures
were usedduringthe collection of these samples.
SAMPLER
# OF SAMPLING METHOD METHOD
CONTAINERS DATE TIME PRESERVED SHIPPED
Wa L II
Redeved by: REMARKS:
by:
-1( i)Q,I 0�� kn c T4-\-ca#zvca
�-- 'A'TEj monitoring purposes. PO#:
ANALYSIS REQUEST
I.O. Organic
5Ly SL2 I NH,-N NO3-N N Cd Cr Ni Pb As Hg Se pH CaCO3 Volatile Mo . CI NO -N
equiv. Solids a
�\ J000 Poe ',or PO
r¢yI i�
vl✓I�x I i-/l-Y/lL'��
SLII: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
✓ 1 1 1--�

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
1703-01-WPL-NC NEUSE REGIONAL WASA, NC WTP LIQUID 4/26/2019 21112019-4/3012019 0.3756
Na mgll = (Na mglkg x % Solids) + 100 = (1380 x 0.5000) � 100 = 6.9
Ca mg/1 = (Ca mglkg x % Solids) + 100 = (2970 x 0.5000) + 100 = 14.85
Mg mgll = (mg mglkg x % Solids) 100 = (1280 x 0.5000) _ 100 = 6.4
Na meq = Na mg/1 Molec.Wgt.Na = 6.9 + 23 = 0.3
Ca meq = Ca mgll - Molec.Wgt.Ca = 14.85 + 20 = 0.7425
Mg meq = Mg mgli + Molec.Wgt.Mg = 6.4 + 12 = 0,533333
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.3 + SgrRoot[0.5(0.7425+0.533333)] = 0.375612
Printed: 2/7/2020
Page 1 12:42

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Melinda Boyd
Project Name: NRWASA
Lot Number:UJ17033
Date Completed:10/25/2019
WqM X -0-M r, ' ' W.-Ow N
10/25/2019 12:04 PM
Approved and released by:
Lab Director - Greenville: Lucas Odom
AM
e
�J
WDUM
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 9

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: UJ17033
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure: UJ17033-00. Due to low % solids, the initial amount of these samples were 3 times the
standard procedure amount. The LOQ has been adjusted accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 8

Client:Synagro Laboratory ID:UJ17033-001
Description: NRWASA Matrix: Solid
Date Sampled:10/15/2019 1500 % Solids: 0.274 1011912019 0021
Gate Received: 10/1712019
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 254OG
1 10/18/2019 0021 MOM
32440
1 350.1
(Ammonia - N) 350.1
1 10/18/2019 1549 DMA
32376
1
(Nitrate - N ) 9056A
1 10/18/2019 1005 SLU
32501
1
(Nitrite - N ) 9056A
1 10/18/2019 1005 SLU
32502
1
(Phosphorus) 365.1
1 10/24/2019 1010 DMA
10/23/2019
1429 32936
1
(Soil pH meas) 9045D
1 10/21/2019 2034 HET
32774
1 351.4
(TKN) 351.2
1 10/18/2019 1551 DMA
10/18/2019
1057 32485
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
0.274
%
1
Ammonia - N (gas diffusion)
350.1
1700
370
190
mglkg
1
Nitrate - N (soluble)
9056A
210 B
180
8.9
mglkg
1
Nitrite - N (soluble)
9056A
23 J
73
7,0
mglkg
1
Phosphorus
7723-14-0 365.1
2900
1800
370
mglkg
1
Soil pH measured in water @ 20.3 ° C
9045D
6.2
su
1
TKN
351.2
15000
9100
9100
mglkg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 10/19/2019 0731 KSH2
10/18/2019 1422 32494
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 74718
ND
29
TO
mglkg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050E
6010D
1 10/21/2019 0742 LLL
10/18/2019 1115 32478
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
190000
2400
900
mglkg
1
Arsenic
7440-38-2 6010D
ND
90
30
mglkg
1
Cadmium
7440-43-9 6010D
ND
30
7.6
mglkg
1
Calcium
7440-70-2 6010D
ND
30000
3700
mglkg
1
Chromium
7440-47-3 6010D
27 J
60
15
mglkg
1
Copper
7440-50-8 6010D
270
60
27
mglkg
1
Iron
7439-89-6 6010D
32000
600
270
mglkg
1
Lead
7439-92-1 6010D
ND
60
27
mg/kg
1
Magnesium
7439-95-4 6010D
ND
30000
3700
mg/kg
1
Manganese
7439-96-5 6010D
2300
90
36
mglkg
1
Molybdenum
7439-98-7 6010D
ND
240
60
mglkg
1
Nickel
7440-02-0 6010D
ND
240
63
mg/kg
1
LOQ = Limit of Quartitation
13 = Detected in the method blank
E = Quantltation of compound exceeded the calibration range
DL = Detection Limit
ND = Not detected at or above the DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds
40%
J = Estimated result < LOQ and a DL
ti = Out of holding time
W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 8

Client:5ynagro Laboratory ID:UJ17033-001
Description: NRWASA Matrix: Solid
Date Sampled:1011512019 1500 % Solids: 0.274 10/1812019 0021
Date Received:1011712019
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 601OD 1 10/21/2019 0742 LLL 10/18/2019 1115 32478
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7
601OD
ND
30000
3700
mglkg
1
Selenium
7782-49-2
601OD
NO
120
49
mglkg
1
Sodium
7440-23-5
6010D
ND
30000
3700
mglkg
1
Zinc
7440-66-6
6010D
140 J
300
75
mglkg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitaticn of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between Me GC columns exceeds 40% J = Estimated result < LOQ and > DL
H - Out of holding lime W = Reported on wet weight basis
Shealy Environmental Services, Inc.
105 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 8

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0
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0
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SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 8

SHEALY ENVIRONMENTAL SERVICES INC.
L
�3y
7F
ti�u
LIE..
...
Shealy Environmental Services, Inc.
106 Vantage Pofnt Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 8

SHEALY ENVIRONMENTAL SERVICES, INC.
5lionl� rnwirmTrznl.:l 5orvit ", Iran` I of €
l7�xcmenl t`iurwt�r ti GC(r! �C- I i LIT�4i� f��r4. 8 :+241
Sample Receipt Checklist I( RQ
Client_ SYNt1GKO Coolcr Inslaected by daty: RMG r IUMU19 Jzt ti L'J 17{13
------------- ................
I cdEx Oiler,
Mealas of leceipt: �_ ❑ Client. ® UPS ® �
Ely,--ql
®NorON101
11. Were cu.stndp seals prie.%int on the roofer?
eK . Nki 21 N 2,. lFG€ 0ndl gcAI3 were aresent, tvere t1Y4'+? I[LLkfSsl uns3 UItl79"571:{,`777__._y
H Strip ID: NA Chlorine Strip ID: NA, J Icy: NA
Ori-heal temperadwv upon mevipt t Derivcd (Corrcrmd) leniperarure upon recaipt %Solid Snap -Cup ID; NA
4.4 f 4.4 le NA INN u{; NA r NA 'L1C' NA /NA ne
lrlelllrrt.l: rrmprladtrru Startle [, A ainst BL�tlles 1R GUH ID: ` IR (Am Correction rKtrri: U °C
M ethod of coolant: V1 Wet Ice 11 Ice P=ke , ❑ Dry lc(: © Moue —
Yes
❑ No
O NA
1 If kraperatvre akfi stay cooler exceeded 6,0T, was Project Manager �Ivti re[l4
PN4 was l+loAW lryt phone 1'email 1 face-trr-race (Circlda �nej,
® 'Yes
❑ No
❑ Nil
4. Is the commercial coa ie3's pacicl[Ig slip atfarhrd to t is tbrm?
0 Ves
-ffYes
❑ No
5. Were proper custody pmcedures (r0inquidiede'ruclaved) followed?
9 No
_
6. Wm- sample JUs Ilsted on i.he COC?
® Yes
Q No
+. were salltpale IDS lislnd un all saniple containers?
r�.w�
iy Yes
0 No
8. Was coLlection daLZ & 1irnG [iSWd oil the COC?
® YD3
❑ NO
9. Was collection date & time Iiswd on all sam pie cont€tinuni?
0 Yes
0 No
T6, Did a][ container [abel if.,formution (11), datc, time) agree wlih th CCOC?
0 Y �:S
❑ No
[ 1. Vert+ ta:sts to he aerthrined I[sted on the COC?
'
❑ No
12, Old all samples atTivre in the proper containers for each test nnellor i,n good condition
(unhunkcn. lids on, etc.):`
—QfYes
❑ No
..
13. Wus atda?LpLElatir salaaplc volume available?
yea
❑ No
�ZNo
14" Were o11 urnples received williin i 11€u Mcli.ng time or48 hoam, whichce ronr:onaas first?
Yes
M Were any 9ulllyles tannininvum naiSSIFT;'excess fcimle o0c) samples 1 &)L liuuJ rrrr CO("
❑ l'es
-ffYes
No
®I�iA
16. ror VOA and RSK-1 +5 samples, were bubbles presc[a€'t"'pe�i�sirc°r {;�"or Nnni ill dlaltteter)
in uny ot'tllr V0A vials?
No
NK
I - Wcal; tall DZiC+.+rnewIs.+nutrient sample—reeeiVM at a pli of <2?
4'es
:gip
NA
18, Were all cyarflde sain le.s revived at a pF[> 12 a€ad ,ulllglc! swrnpks weived at a E 14 > p?
Yes�
Nu
10 NA
I . �rl+er6 A1,1p(} lca a NF[v''I'K ;'cvar€%dlrrrhenr>1,16?5 (U.5tn�:L) saiinples reed residualEl
13 ' es
ElN
.................
"�
20, %'4ome client r�emar[Wregwmt; (I.c, rulucslcd di[:€tlons, K4'1vE 1ND diesignzdio�as, etc...j
cotroctltr transcribed tram VA;00C intsa 10 eonamen€rectinn In LTMS^
❑ V s
No
21- Was the qluow nurrzbrr listrd on the co►ataiiia label? tf ves. 9,1LIOle 3r NA
Sample i?resei-vatif[n {Must be completer) tN, any sample(s) incorrectly preserwd or with lwadsppoe.)
1mlrin(sj 1Vrl Were roe-eived incorrectly preuerved End Were; ndju.sted aocordingly
insamplCNA inL,ofcir€:Iconc:H2ZiU4,FJNMeHCl, MiOlinsing5R# NA
7inae tri pq seCua4lUn NA If more thAri Ogle pmservatiLe is ncr:ded, plcrasc note in the comrni nts below.
Saillp°1e.(3E NA 4Vedt reccivud wRh bubb[es'•'6 min to diarrocter-
Salllples(s) *Irk _ _ _ were received with TRC.- 0.5 tnVL (lr'i# 19 is no) and were
adjusted aculYtlirrrily in 8amplc raceiving i4'lttt !,Odiltril 11i0.5Lrli8CC ( £€y�til }t),Vlt i he3lW" HLk; '114A
--
Sk Imircnde lads applied by: ANIG
C401rumcnts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 8

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1703-01-WPL-NC NEUSE REGIONAL WASH, NC WTP LIQUID 10/15/2019 101112019-1213112019 0.5362
Na rng11 = (Na mg/kg x % Solids) + 100 = (3700 x 0.2740) 100 = 10.138
Ca rng11 = (Ca mg/kg x % Solids) r 100 = (3700 x 0.2740) + 100 = 10.138
Mg mgll = (mg mgtkg x % Solids) + 100 = (3700 x 0.2740) + 100 = 10.138
Na rneq = Na mgll + Molec.Wgt.Na = 10.138 + 23 = 0.440783
Ca rneq = Ca mgll + Molec,Wgt.Ca = 10.138 _ 20 = 0.5069
Mg rneq = Mg mgll + Molec.Wgt.Mg = 10.138 + 12 = 0.844833
SAR = Na rneq + SgrRoot[0.5 x (Ca meq + Mg rneq)] = 0.440783 + SgrRoot[0.5(0.5069+0.844833)] = 0.536159
Printed: 2121 /2020
Page 1 13:34

SECTION 3

FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: NEUSE REGIONAL
SITE #: NC LN 000X5 FIELD# : LN 000X5 0001
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES : KALMLA
PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 74.92
OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.70 ACRES PERMITTED: 31.70
Page: 1
Lime Applied ***
Date Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
{ppm)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1/8/19
1,020,600.0( (G)
32195.5841
1,62
2.175
NRWASA
SUR
0.5
0.40
58,600. p
3,790.00 p
414,00 p
24233
BERMUDAGRASS
Jan-19
1,020,600.00 (G)
32,195.584
1
10/17/19
434,700.00 (G)
13712.934
0,27
1 0.157
NRWASA
SUR
0.5
0.40
15,000, p
1,700.00 p
210,00 p
6380
BERMUDAGRASS
10/18/19
88,200.00 (G)
2782.334
0.27
0.032
1 NRWASA
SUR
0.5
0A0
15,000. p
1,700,00 p
210.00 p
6380
BERMUDAGRASS
Oct-19
522,900.00 (G)
16,495.268
iotal uallons/Ac: 4N,49U.85
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.063 0.007 0.298 3.699 0.075 0,003 0,033 0,096 0.040 0.417 13.36 108
Cumulative lbs/acre 0.475 0.063 3.655 41.747 0.507 0.017 0.208 0.852 0.173 3.194
Permit PAN Limit (lbs/acre) Ist Cropl2nd Crop
230
l\
Y
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
„
375.0
89.0
2500.0
v
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR —Not Reported or Not Required % = percent p = ppm or mgikg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 - Injection, SURIN - Incorporation *** See Site PH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITYNAME: NEUSE REGIONAL WASA, NC
OWNER: NEUSE REGIONAL
SITE #: NC LN 00OX5 FIELD# : LN 00OX5 0002
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: KALMIA
PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 33,25
OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 12.40 ACRES PERMITTED: 12.40
Page: 1
Lime Applied ***
Date
Lbs/Ac
Gallons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
nation
TKN
Nitrogen
and
(ppm}
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1/8/19
474,100,00 (G)
382318711
1.62
2.583
NRWASA
SUR
0.5
0.40
59,600. p
3,790.00 p
414.00 p
24233
FESCUE
Jan-19
474,100.00 (G)
38,233.871
10/17/19
107,100.00 (G)
8637.0971
0.27
0.099
NRWASA
SUR
0.5
0.40
15,000.p
1,700.00 p
210.00 p
6380
FESCUE
Oct-19
107,100.00 (G)
8,637,097
1
1
.t omi uanonsiAc: 4u,a /u.y r
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0,00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.067 0.007 0.347 4.325 0.083 0.002 0.025 0.098 0.036 0.461 15.14 126
Cumulative lbs/acre 0.380 0.042 2.884 42.704 0AI I 0.011 0.146 0.636 0.126 2.500
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
E
? "
»
161
UMMM
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
Jnlw,�
X g
— .
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A— Not Applicable NR = Not Reported or Not Required %=percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURiN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: NEUSE REGIONAL
SITE #: NC LN 000X5 FIELD# : LN 000X5 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: KALMIA
PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 3.24
OPERATOR: NEUSE REGIONAL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.40 ACRES PERMITTED: 9.40
Page: 1
Lime Applied asa
Date
LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons CWT) (specify)
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TI{N
Nitrogen
and
(pp-)
Crop
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/17/19
283,500.00 (G)
30159.5741
0.27
0.345
NRWA,SA
SUR
0.5
0.40
15,000. p
1,700.00 p
210.00 p
6380
FESCUE
Oct-19
283,500.00 (G)
30,159.574
1
1
1
Total Gallons/Ac: 30,159.57
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0,021 0.005 0.019 0.186 0.019 0.005 0.041 0.043 0.034 0.096 2.00 4
Cumulative lbs/acre 0.424 0.043 3,204 49.689 0.425 0,016 0.186 0.585 0.129 2.535
Permit PAN Limit (lbs/acre) 1st Cropl2nd Crop
"
2
.. .. ....
2 30
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
NRWASAWPL — NEUSE REGIONAL WASA, NC WTP LIQUID
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility o£fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, tN7 - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: NEUSE REGIONAL WASA, NC PREDOMINANT SOIL SERIES: JOHNS
OWNER: SOVEREIGN REAL ESTATE PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 35.00
SITE #: NC LN OOOX6 FIELD# : LN 00OX6 0001 OPERATOR: MICHAEL GINN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 13.60 ACRES PERMITTED: 13.60
Page
Lime Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
I Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Fast 24
Method
nation
zation
TKN
Nitrogen
and
(ppm)
Crop
111
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1/8/19
488,250.00 (G)
35900.7351
1.62
2.425
NRWASA
SUR
0.5
0.40
58,600. p
3,790.00 p
414.00 p
24233
CORN
Jan-19
488,250.00 (G)
35,900.735
1
10/16/19
138,600.00 (G)
10191.176I
0.27
0.116
NRWASA
SUR
0.5
0.40
15,000. p
1,700.00 p
210.00 p
6380
I WI -MAT
10/17/19
37,800.00 (G)
2779.412
0.27
0.032
NRWASA
SUR
0.5
0.40
15,000. p
1,700.00 p
210.00 p
6111
WHEAT
Oct-19
176,400.00 (G)
12,970.588
Total UallonslAc:
Total Wet Tons/Ac:
Total Cubic Yds/Ac:
48,871.32
Permit PAN Limit (lbs/acre) 1 st Crop/2nd Crop
130
50
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
X —
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incarporation LO
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: SOVEREIGN REAL ESTATE
SITE #: NC LN 00OX6 FIELD# : LN 00OX6 0002
RESIDUAL SOURCE(S): See list at bottom of report
[=AL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: KALMIA
PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 12.50
OPERATOR: MICHAEL GINN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.50 ACRES PERMITTED: 7.50
time Applied * �*
Date
LbsAc
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Day
site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip,
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
[
[ Per Acre
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
t
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
1/8/19
170,100.00 (G)
22680.0001
1.62
1.532
NRWASA
SUR
0.5
0.40
58,600. p
3,790.00 p
414.00 p
24233
WHEAT
Jan-19
1 170,100.00 (G)
22,680.000
1
10/16/19
69,300.00 (G)
9240.000
0.27
0.106
NRWASA
SUR
0.5
0.40
15,000.p
1,700.00 p
210.00 p
6380
WHEAT
10/17/19
18,900.00 (G)
2520.000
0.27
0.029
NRWASA
SUR
0.5
0.40
15,000.p
1,700.00 p
210.00 p
6380
WHEAT
Oct-19
88,200.00 (G)
11,760.000
I ULM l7MIURS11A :: m'44V.VV
Total Wet Tons/Ac:
Total Cubic YdsfAc: 0.00
TOTALS
As Cd Cr Cu Ph Hg Mo Ni Se Zn P PAN
Annuallbs/acre 0.045 0.005 0,210 2.607 0.053 0.002 0.024 0.067 0.028 0.294 9A2 74
2
Cumulative lbs/acre 0.418 0.059 3.094 41.472 0.451 0.015 0.183 0.741 0.161 2.809
Permit PAN Limit lbs/acre 1st Cro 2nd Crop
z
50
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
IS 0
375.0
89.0
2500.0 i
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
x �4Q4' �__ ,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
NIA=Not Applicable NR —Not Reported or Not Required %= percent p —ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, IN7 - Injection, SUR1N - Incorporation ** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: SOVEREIGN REAL ESTATE
SITE #: NC LN 000X6 FIELD# : IN 000X6 0003
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LUMl3EE
PERMIT #: WQ0034688 ANNUAL DRY TONS APPLIED: 8.78
OPERATOR: MICHAEL GINN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 26.30 ACRES PERMITTED: 26.30
Page : I
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
till-
nation
Miner -
ali-
zaticn
TKN
Ammonia
Nitrogen
Nitrate
and
I
PAN
(PP-)
Crop
Total
j
I Per Acre
f
Acre
Source
Moist
Hours
*
Rate**
Rate
Nitrite
10/14/19
340,200.00 (G)
12935.361
0.27
0.148
NRWASA
SUR
0.5
0.40
15,000. p
1,700,00 p
210M p
6380
WHEAT
10/15/19
428,400.00 (G)
16288.973
0.27
0.186
NRWASA
SUR
0.40
15,000.p
1,700.00 p
210.00 p
6380
WHEAT
Oct-19
768,600.00 (G)
29,224.334
L
total Nations/.A,c: 29,2Z4.33
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbslacra 0.020 0.005 0.018 0.180 0.018 0.005 0.040 0.042 0.033 0.093 L94 4
Cumulative lbs/acre 0.174 0.022 1.192 25.062 0.187 0.009 0.099 0.222 0.076 1.071
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
Z
i `
``
;
106
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15,0
375.0
89.0
2500 0
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
x �-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fries and imprisonment for knowing violations."
NIA = Not Applicable NR = Not Reported or Not Required % — percent p = ppm or mglkg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

FACILITY NAME: NEUSE REGIONAL WASA, NC
OWNER: SOVEREIGN REAL ESTATE
SITE #: NC LN 000X6 FIELD# : LN 000X6 0004
RESIDUAL SOURCE(S): See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: JOHNS
PERMIT #: W00034688 ANNUAL DRY TONS APPLIED: 123.87
OPERATOR: MICHAEL GINN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 58.70 ACRES PERMITTED: 58.70
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ah-
Ammonia
Nitrate
PAN
Total
I Per Acre
➢ATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past24
Method
zation
nation
TKN
Nitrogen
and
m
(Pp )
Cro p
Acre
Source
Moist
Hours
*
Rate"
Rate
Nitrite
1/8/19
1,696,250.0( (G)
28896.9341
1.62
1.952
NRWASA
SUR
0.5
0A0
58,600. p
3,790.00 p
414.00 p
24233
CORN
Jan-19
1,696,250.00 (G)
28,896.934
10/15/19
189,000.00 (G)
3219.761
0.27
0.037
NRWASA
SUR
0.5
0A0
15,000.p
1,700M p
210.00 p
6380
I WHEAT
10/16/19
554,400.00 (G)
9444.634
0.27
0.108
NRWASA
SUR
0.5
0.40
15,000.p
1,700.00 p
210.00 p
6380
I WHEAT
10/17/19
69,300.00 (G)
1180.579
0.27
0.013
NRWASA
SUR
0.5
0.40
15,000.p
1,700.00 p
210.00 p
6380
WHEAT
Oct-19
812,700.00 (G)
13,844.974
ibtal UallonslAc: 42,741.91
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 0.00
TOTALS:
As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN
Annuallbs/acre 95
0.056 0.006 0.267 3.3I4 0.067 0,003 0.029 0.084 0.035 0,371 11.93
2
Cumulative lbs/acre 0.238 0.040 L951 28.643 0.253 0.009 M12 0.255 0.118 1.441
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
' 130
50
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted.1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A —Not Applicable NR= Not Reported or Not Required %= percent p — ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020

SECTION 4

summill
,
AnafyNcal Laboralarlaa
January 21, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Neuse Regional WASA
Dear Melinda Boyd:
Summit Envif•onnaental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX- [phone]
Wehsite: h1tp:1Avwiy.settekcom
Order No.: 19010533
Summit Environmental Technologies, Inc. received I sample(s) on 1/10/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho 01100923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank)3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
0112O0001, Rhode Island LA00031 ?,South Carolina 92016001, Texas T104704466-11-5, Utalr OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 30

Summit Environmental Technologies, Inc.
SUMMIT3310 Win St. �dSe Narrative
ENVIRONMENTAL TECHIM01 ti1;if-S, NC Cuyahoga Falls, Ohio 44223 WO#: 1901.0533
Analytical Lab oratanes TEL: [phone] FAX., [phone]
Website: hth�:,(/�yimsettehconz Date: 1�21/2019
CLIENT: Synagro
Project: Neuse Regional WASA
WorkOrder Narrative:
19010533: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19010533-001A SVOC-BNA TCLP(8270d): Possible low bias for Pyridine due to low recovery in
CCV; Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
19010533-001A SVOC-BNA_TCLP(8270d): Sample exhibited low recovery of Surrogates: 2-
Fluorophenol, Phenol-d6 possibly due to matrix effect.
Analytical Sequence QC Notes:
CCV 40ng 14287 SVOC-MSTR_S(8270): The CCV (Batch R93442) exhibited high recovery for
Hexachlorobutadiene and Pentachlorophenol. The associated samples are ND for the analytes with high
recoveries.
Original
Page 2 of 30

UMMIT
'�ummitL'nvir�onmentalTechnologies, Inc. Vase Narrative
S3310 Win St.
ENVIRONMENTAL TECt1HOLOrF 1E5, INC Cuyahoga Falls, Ohio 44223 WO#; 19010533
Analytical t abaralonev TEL: [phone] F,4X.• [phone]
Website: http•1/wwrv.seliek.com Date: 1/21/2019
CLIENT: Synagro
Project: Neuse Regional WASA
CCV 40ng 14287 SVOC-MSTRS(8270): The CCV (Batch R93442) exhibited low recovery for
Pyridine. Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Check shows
adequate instrument sensitivity for reporting purposes.
MB-35513 SVOC-BNA TCLP(8270): MB-35513 exhibited low recovery of Surrogate: 2-Fluorophenol.
MB-35513 SVOC-BNA TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
LCS-35513 SVOC-BNA_TCLP(8270): LCS-35513 exhibited low recovery of Surrogate: 2
Fluorophenol.
LCS-35513 SVOC-BNA TCLP(8270): Possible low bias for Pyridine due to low recovery in CCV;
Reporting Limit Check shows adequate instrument sensitivity for reporting purposes.
Original
Page 3 of 30

UMMIEF Summit in Technologies, InQualifiers andAcronyms
3310 Win
EHVI110N?A5UTAL TECHNO INS' Cuyahoga Falls, Ohio 442; WO##: 19010533
Am?r yticaf Labo,raloH'es TEL: [phone]I FAX.- (330) 253-44
Website: http://www.settek.co Date: 1/2112019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit,
H The hold time for sample preparation and/or analysis was exceeded. Not Clean Water Act compliant.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response,
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GCIMS.
X The result was not confirmed when GUMS Analysis was performed.
BINVM+ The analyte was detected in the associated blank.
G The 1CB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
RIQDR The RPD was outside of accepted recovery limits,
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-1+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
W Samples were received outside temperature limits (0' -- 6° C). Not Clean Water Act compliant.
ZZ Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RI.
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvI
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 30

Suntnrit Enviz•onmental Technologies, Inc. Workorder
SUMMIEF 3310 Win St.
€Pd' IRONNILNTAL TECH UOI OSIr!;, WC Cuyahoga Falls, Ohio 44223 Sample Summary
Analyfdcal Laboraferle.. TEL: [phone] FAX.- [phone] WO#: 19010533
Website- httn://www.settek.com 21-Jan-19
CLIENT: Synagro
Project: Neuse Regional WASA
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
19010533-001 NRWASA TCLP 1/8/2019 12:30:00 PM 1/10/2019 10,15:00 AM Solid
Page 5 of 30

Summit Environmental Technologies, Inc.
SUMMIT33I0 Win St.
IE=fLifliii?NNIENTAL ICJ-1NQ 0G11�S, :NC Cuyahoga Falls, Ohio 44223
A,rWy0C2± Lab raloneg TEL: (330) .253-8211 FAX.- [phone]
Website: hht :/lwww.settekcom
DATES REPORT
WO#: 19010533
21-Jan-19
Client: Synagro
Project: Neuse Regional WASA
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
19010533-00IA NRWASA TCLP 1/8/2019 12:30:00 PM Solid Ignitability of Solids (SW-846: 1030) 1/11/2019 11:00.00 AM
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
1/I7/2019 3:09:04 PM
1/14/2019 11:38:00 AM
1/14/2019 11:08:00 AM
TCLP Herbicides Analysis (SW1311/81/I0/2019 5:44:59 PM 1/11/2019 5:00:00 PM 1/18/2019 6:58:00 PM
TCLP Mercury Analysis (SW131117471/10/2019 5:44:59 PM 1/16/2019 11:30:00 A 1/16/2019 4:44:00 PM
�7
TCLP Metals Analysis (SW1311/6010.1/10/2019 5:44:59 PM 1/14/2019 8:25:00 AM 1/14/2019 4:32:16 PM
TCLP Pesticides Analysis (SW1311/8(1/10/2019 5:44:59 PM 1/15/20192:45:00 PM 1/18/2019 12:22:00 AM
TCLP Semi-Volatiles Analysis 1/10/2019 5:44:59 PM 1/14/2019 10:45:00 A 1/16/2019 4:23:00 AM
(S W1311 /8270) * R
TCLP Volatiles Analysis 1/10/2019 5:46:19 PM 1/14/2019 4:08:00 PM
Original
Page 6 of 30

SUMM17-
SinnnaitEnvironmental Technologies, Inc.
33.10 ff7in St.
Analytical Report
EhAr?QNNIENTAL i,EG]%WC]OrlirS, INC
Cuyahoga
Fails, Ohio 44223
(base report)
Labo:ralorl&s
TEL: (330)
253-8211 FAX: [phone]
WO#: 19010533
W'ebsite: httn://ivww.settek.cona
Date Reported: 1/21/2019
CLIENT: Synagro
Tag Number:
Matrix: SOLID
Collection Date:
I/8/2019 12:30:00 PM
Lab ID: 19010533-OOIA
Project: Neuse Regional WASA
Client Sample ID NRWASA TCLP
Analyses Result
RL
Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00200
mg/L
1 1/16/2019 4:44:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW601OD
SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As)
ND
0.500
mg/L
1 1/14/2019 4:32:16 PM
TCLP Barium(Ba)
ND
5.00
mglL
1 1/14/2019 4:32:16 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1 1/14/2019 4:32:16 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1 1/14120194:32:16 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1 1/14/2019 4:32:16 PM
TCLP Selenium(Se)
N❑
0.0500
mg/L
1 1/14/2019 4:32:16 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1 1/14/2019 4:32:16 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
1,4-Dichlorobenzene
ND
0.0800
mg/L
2 1/16/2019 4:23:00 AM
2,4,5-Trichlorophenol
ND
0.200
mg/1-
2 1/16/2019 4:23:00 AM
2,4,6-Trichlorophenoi
ND
0.200
mg/L
2 1/16/2019 4:23:00 AM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2 1/16/2019 4:23:00 AM
c-Cresol
ND
0.200
mg/L
2 1/16/2019 4:23:00 AM
mlp-Cresol(s)
ND
0.200
mglL
2 1/16/2019 4:23:00 AM
Cresols, Total
ND
4.00
mg/L
2 1/16/2019 4:23:00 AM
Hexachloro-1,3-butadiene
ND
0.0160
QC+ mglL
2 1/16/2019 4:23:00 AM
Hexachlorobenzene
ND
0.0400
mg/L
2 1/16/2019 4:23:00 AM
Hexachloroethane
ND
0.0800
mg/L
2 1/16/2019 4:23:00 AM
Nitrobenzene
ND
0.0800
mg/L
2 1/16/2019 4:23:00 AM
Pentachloropheno!
ND
0.200
QC+ mg/L
2 1/16/2019 4:23:CO AM
Pyridine
ND
0.200
QC- mglL
2 1/16/2019 4:23:00 AM
Surr: 2-Fluorophenol
6.76
10 - 109
S %Rec
2 1/16/2019 4:23:00 AM
Surr: Phenol-d6
8.28
10 - 109
S %Rec
2 1/16/2019 4:23:00 AM
Surr: Nitrobenzene-d5
63.5
19 - 120
%Rec
2 1/16/2019 4:23:00 AM
Surr. 2,4,6-Tribromophenol
15.0
10 - 120
%Rec
2 1/16/2019 4:23:00 AM
Surr: 2-Fluorobiphenyl
63.3
22 - 117
%Rec
2 1/16/2019 4:23:00 AM
Qualifiers. * Value exceeds Maximum Contaminant
E Value above quantitation
range
Level.
H Holding times for preparation or analysis
exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound
Limit.
N Tentatively identified compounds
ND Not Detected
0 RSD is greater than
RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R IUD outside accepted recovery limits
RL Reporting Detection
Limit
Page 7 of 30

IT Summit Environmental Technologies, hoc. Analytical Report
SUMM3310 Win St.
ENVInONKIENTAL t G9�HtlLcy lS,"r, tNr. Cuyahoga Falls, Ohio 44223 (base report)
Anaiyrlcal Labmalafies TEL: [phone] FAX.- [phone] WO#: 19010533
Website: htto://iviviv.settek.con? Date Reported: 1/21/2019
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/8/2019 12:30:00 PM
Lab ID: 19010533-OOIA
Project: Neuse Regional WASA
Client Sample ID NRWASA TCLP
Analyses Result
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
RL Qual Units
DF
Date Analyzed
SW8270D SW3510C Analyst: IBJH
Surr: p-Terphenyl-dl4 100 34 - 116 %Rec 2 1/16/2019 4:23:00 AM
NOTES:
Possible low bias for Pyridine due to low recovery in CCV; Reporting Limit Cheer shows adequate instrument sensitivity for reporting
purposes.
Sample exhibited low recovery of Surrogates: 2-Fluorophenol, Phenol-d6 possibly due to matrix effect.
TCLP METALS, VOC, BNA, PEST, HERS -SOLID
SW8081
SW351OC Analyst: MES
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND
0.0250
mg/L
10 1/18/2019 12:22:00 AM
Toxaphene ND
0.0500
mg/L
10 1/18/2019 12:22:00 AM
Endrin ND
0.00500
mg/L
10 1/18/2019 12:22:00 AM
gamma-BHC ND
0.00500
mg/L
10 1/18/2019 12:22:00 AM
Heptachlor ND
0.00500
d mg/L
10 1/18/2019 12:22:00 AM
Heptachlor epoxide ND
0.00500
mg/L
10 1/18/2019 12:22:00 AM
Methoxychlor ND
0.00500
d mg1L
10 1/18/2019 12:22:00 AM
Surr: TCMX 23.7
10 - 119
%Rec
10 1/18/2019 12:22:00 AM
Surr: DCB 31.9
10 - 119
%Rec
10 1/18/2019 12:22:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW131118151)
2,4-D ND
1.00
mg/L
1 1/18/2019 6:58:00 PM
2,4,5-TP ND
0.500
mg/L
1 1/18/2019 6:58:00 PM
Surr: DCAA 56.7
20- 140
%Rec
1 Ill8/2019 6:58"00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichlorcethene ND
0.125
mg/L
25 1/14/2019 4:08:00 PM
1,2-Dichloroethane ND
0.125
mg/L
25 1/14/2019 4:08:00 PM
MEK ND
0.625
mg/L
25 1/14/2019 4:08:00 PM
Benzene ND
0.125
mg1L
25 1/14/2019 4:08:00 PM
Carbon tetrachloride ND
0.125
mg/L
25 1/14/2019 4:08:00 PM
Chlorobenzene ND
0.125
mg/L
25 1/14/2019 4:08:00 PM
E Value above quantitation range
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified compounds
ND Not Detected
O RSD is greater than
RSDlimit
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 8 of 30

SUMM17-
SummitEnvironmental"1'ec177aologies, Inc.
3310 ffin St.
Analytical Report
EPIVIRONNI NTAL IFECI EVAt(tG1F.5,. 9Nr`
Cuyahoga Falls, Ohio 44223
(base report)
Am*yt;C: 11 ; nboralorJ610
TEL: [phone] FAX: [phone]
WO#: 19010533
Website: htt7j:11wiviv.settelc co7n
Date Reported: 1/21/2019
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
1/8/2019 12:30:00 PM
Lab ID:
19010533-OOIA
Project:
Neuse Regional WASA
Client Sample
ID NRWASA TCLP
Analyses
Result RL Qua] Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
98.0
Surr: Dibromofluorom ethane
103
Surr: Toluene-d8
103
RCI-SOLID-WI IGNITABILITY1030
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND
RCI-SOLID-WI IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-WI IGNITABILITY1030
PH (SW9045D)
pH 5.8
RCI-SOLID-W1 IGNITABILITY1030
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND
SW8260B SW1311 M Analyst: CTB
0.125
mg/L
25
1/14/2019 4:08:00 PM
0.125
mg/L
25
1/14/2019 4:08:00 PM
0.125
mg/L
25
1/14/2019 4:08:00 PM
0.0500
mg/L
25
1/14/2019 4:08:00 PM
70 - 130
%Rec
25
1/14/2019 4:08:00 PM
70 - 130
%Rec
25
1/14/2019 4:08:00 PM
70 - 130
%Rec
25
1/14/2019 4:08:00 PM
SW9014
Analyst: MS
0.496
mg/Kg
1
1/14/2019 11:38:00 AM
SW1030
Analyst: AJT
1
1/11/2019 11:00:00 AM
SW9045D
Analyst: VVK
s.u.@20.00
1
1/17/2019 3:09:04 PM
SW9034
Analyst: MS
25.0
mg/Kg
1
1/14/2019 11:08:00 AM
Qualifiers:
* Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N "Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 30

UMMIEF
Summit Environmental Technologies, Inc.
3310 Win St.
Accreditation Program
Analytes Report
ErNWIIIONNIEWTQL rEC8tAQC LQCIiZ S, INC
Cuyahoga Falls, Ohio 44223
Anaiyr; cai isabw-atordas TEL: [phone] FAX: [phone]
WO#: 19010533
Website: h#2.-Ilww)g.settelc.coni
21-Jan-19
Client:
Synagro
State: NW
Project:
Neuse Regional WASA
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte Status
19010533-001A Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides Analysis (SW 131 1/8151)
2,4,5-TP
A
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Solid
TCLP Herbicides Analysis (SW 1311/8151)
DCAA
A
Solid
TCLP Mercury Analysis (SW131I/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW 1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW131118 081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphcnyl
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SWI31I/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW131118081)
Methoxycblor
A
Solid
TCLP Pesticides Analysis (SWI311/808I)
Tetrachloro-m-xylene
A
Solid
TCLP Pesticides Analysis (SW1311/808I)
Toxaphene
A
Solid
TCLP Serni-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Senu-VolatilesAnalysis. (SWI311/8270)
2,4,6-TribromophenoI
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SWI31118270)
2,4-Dinitrotoluenc
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorophenol
A
Version #2
Page 10 of 30

Summit l;avironmentacTechnologies, Inc.
Accreditation
Program
frS
3310 win. st.
UMMIT
Analytes Report
ENWIIION661r:t4TAL T-CHNOl fF.^,ff5,
:Nr. Cuyahoga Falls Ohio 44223
Ajp aeyOaai L abr yatarle6
TEL: [phone] FAX.- [phone]
WO#:
19010533
Website: http://Wivw.Eettek.conz
21-Tan-I9
Client: Synagro
State: NW
Project: Neuse Regional WASA
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
19010533-OOIA Solid
TCLP Semi-Volatiles Analysis (SW1311/9270)
2-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/9270)
3,4-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW131I/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene-d5
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
PhenoW6
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
p-Terphenyl-d14
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-13ntanane
A
Solid
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Dibromofluoromethane
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Toluene-d8
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Version #2
Page 11 of 30

IT Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
EM111 Mhih1ENTA.L TE�Ikz`lC7LL7G1�_ , : ^ Cuyahoga Falls, Ohio 44223
Aryatydcal La�boriloroes TEL: [phone] FAX.- [phone] WO#: 190] 0533
Website: hL .-Il vww.settetc.com 21-Jan-14
Client: Synagro
Project: Neuse Regional WASA
SatchED: 35 472
Sample ID MB-35472
SampType: MBLK
TestCode: tclp-goo-mstr Units: mg1L
Prep Date: 1/1012019
RunNo: 93332
Client ID: PBS
Batch ID: 35472
TestNo: SW8260B SW1311M
Analysis Date: 1/11/2019
SegNoi 1903835
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua!
1,1-Dichloroethene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
0.250
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.0500
Chloroform
ND
0.0500
TetrachIoroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
464
Surr: Dibromofluoromethane
602
Surr. Toluene-d8
496
500.0 92.8 70 130
500.0 120 70 130
500.0 99.2 70 130
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
1-1 Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum. Compound Limit. ND Not Detected
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 12 of 30

SUMMINt
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVI-,zON 61ENTAL'd=CPNOLOG S, hCC
A.njry.rlcal Laharatorjart
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX., [phone]
WO#: 19010533
Website: hW:Ilwww.settek.com
21-Jan-19
Client:
Synagro
Project:
Neuse Regional WASA
BatchID: 35513
Sampie ID MB-35513
SampType: MBLK
TestCode: SVOC-BNA T Units: %Rec
Prep Date: 111412019
RunNo: 93442
Client 0: PBS
Batch ID: 35513
TestNo: E625 SW3510C
Analysis Date: 1/1512019
SegNo: 1908302
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: 2-Fluorophenol
0.0980
1.000
9.80
10
109 S
Surr: Phenol-d6
0.100
1.000
10.0
10
109
Surr: Nitrobenzene-d5
0.665
1.000
66.5
19
120
Surr; 2,4,6-Tribromophenol
0.146
1.000
14.6
10
120
Surr:2-Fluorobiphenyl
0.654
1.000
65.4
22
117
Surr: p-Terphenyl-d14
0.893
1.000
89.3
34
116
Sample ID LCS-35513
SampType: LCS
TestCode: SVOC-BNA_T Units: %Rec
Prep Date: 1114/2019
RunNo: 93442
Client ID: LCSS
Batch ID: 35513
TestNo: E625 SW3510C
Analysis Date: 1115/2019
SegNo: 1908303
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: 2-Fluorophenol 0.110
1.000 11.0
17.1
130
S
Surr: Phenol-d6 0.108
1.000 10.8
10
130
Surr: Nitrobenzene-d5 0.721
1.000 72.1
32.6
130
Surr:2,4,6-Tribromophenol 0.179
1.000 17.9
4,43
130
Surr:2-Fluorobiphenyl 0.734
1.000 73.4
41.8
130
Surr: p-Terphenyl-d14 1.05
1.000 105
36.4
130
Qualifiers: * Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 13 of 30

Summit Environmental Technologies,.lnc. QC SUMMARY REPORT
summill 3310 Win St.
Efk4(Ir 0WMEmT,a.L Tr-OHNO[,M311ES„ JKC Cuyahoga Falls, Ohio 44223
WO#: 19010533
Arweyt�=i Laboraiorlas TEL: [phone] FAX.- [phone]
Website: hQ.-Ilwww.settek.cam .21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID: 35513
Sample ID 19010307-001AMS
SampType: MS
TestCode: SVOC-BNA_T Units: %Rec
Prep Date: 111412019
RunNo: 93442
Client ID: BatchQC
Batch ID; 35513
TestNo: E625 SW3510C
Analysis Date: 1115/2019
SegNo: 1908304
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr:2-Fluorophenol
0.107
1.000
10.7
3.39
89.9
W
Surr: Phenol-d6
0.107
1.000
10.7
-2.08
55
W
Surr: Nitrobenzene-d5
0.683
1.000
68.3
14.5
154
W
Surr:2,4,6-Tribromophenol
0.175
1.000
17.5
19.5
93.2
SW
Surr:2-Fluorobiphenyl
0.753
1.000
75.3
34.4
121
W
Surr. p-TerphenylA14
1.01
1.000
101
8.86
156
W
Sample lD 19010307-001AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: %Rec
Prep Date: 1/14/2019
RunNo: 93442
3lient ID: Batch=
Batch ID: 35513
TestNo: E625 SW3510C
Analysis Date: 1/1512019
SegNo: 1908305
5,nalyte
Result
PQL. SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr 2-Fluorophenol 0.0844
1.000 8.44
3.39
89.9
0
W
Surr: Phenol-d6 0.0900
1.000 9.00
-2.08
55
0
W
Surr: Nitrobenzene-d5 0.586
1.000 58.6
14.5
154
0
W
Sum 2,4,6-Tribromophenol 0.152
1.000 15.2
19.5
93.2
0
SW
Sum 2-Fluorobiphenyl 0.677
1.000 67.7
34.4
121
0
W
Surr: p-Terphenyl-d14 0.965
1.000 96.5
8.86
156
0
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Bolding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Original
MC Value is below Minimum Compound Limit.
ND
Not Detected
O
RSD is greater than RSD]imit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 14 of 30

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
Summ 3310 Win St.
EKE flrLONMENTAL TECHNCE Cn .: Cuyahoga Falls, Ohio 44223
WOO: 19010533
ArWytlecal Laborworoes TEL: [phone] FAX.- [phone]
Website: htW:Ilwww.settek.com 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchXD: 35523
Sample ID Ics-35523
SampType: LCS
TestCode:
tclp-svoc-her Units: mglL
Prep Date: 1111/2019
RunNo: 93601
Client ID: LCSS
Batch ID: 35523
TestNo:
SW8151A SW8151A
Analysis Date: 1/1812019
SegNo: 1914631
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 78.4
43.8
130
2,4,5-TP
N❑
0,500 0.500
0 62.9
51.5
1l1
Surr: DCAA
357
500.0
71.4
34.2
150
Sample ID mb-35523
SampType: MBLK
TestCode:
tclp-svoc-her Units: mglL
Prep Date: 1/11/2019
RunNo: 93601
Client ID: PBS
Batch ID: 35523
TestNo:
SW8151A SW8151A
Analysis Date: 1/1812019
SegNo: 1914632
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 1.00 0 0 d
2,4,5-TP ND 0.500 0 0
Surr: DCAA 320 500.0 64.0 20 140
Sample ID 19010307-001ams
SampType: MS
TestCode: tclp-svoc-her Units: mglL
Prep Date: 1/11/2019
RunNo: 93601
Client ID: BatchQC
Batch ID: 35523
TestNo: SW8151A SW8151A
Analysis Date: 1118/2019
SegNo: 1914634
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 100
37
105
W
2,4,5-TP
ND
0.500 0.500
0 89.8
38
106
W
Surr: DCAA
567
500.0
113
20
140
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 15 of 30
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

MIT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUM3310 Win St.
EMYliL0WP.1EMTAL T2C1 N0L-0G1r$, JKC Cuyahoga Falls, Ohio 44223 WO#: 19010533
Ar7atytk.-. Lgberratories TEL: [phone]I FAX.- [phone]
Website: httnJ/www.setfeic.com 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID: 35523
Sample ID 19010307-001amsd
SampType: MSD
TestCode:
tclp-srroc-her Units: mglL
Prep Date: 1/1112019
RunNo: 93601
3lient ID: Batch=
Batch ID: 35523
TestNo:
SW8151A SW8151A
Analysis Date: 1/18/2019
SegNo: 1914646
4nalyte
Result
PQL
SPK value SPK Ref Val
%RFC Lowl-imit Hightimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
1.00 0.500
0 83.7
37
105
0 0
30 W
2,4,5-TP
ND
0,500 0.500
0 71.5
38
106
0 0
30 W
Surr: DCAA
453
500.0
90.6
20
140
0
W
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding tines for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 16 of 30
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

111 Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMM3310 Win St.
EN4rli'OWMEWALI-ECHNOLtbM5F OiC Cuyahoga Falls, Ohio44223
WO#: 19010533
d.rPatyGCaP Labbrwaraes TEL: [phone]I FAX: [phone]
Website: httn:Ilwww.settek.corn 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA SatchID: 35549
TCLP Mercury ND 0.00200
TCLP Mercury ND 0.00500
TCLP Mercury 0.00401 0.00200 0.00400 0 100 80 120
Sample 1D 19010659-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 111612019
RunNo: 93469
Client ID; Batch=
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 111612019
SegNo: 1909440
Analyte
Result
PQL SPK value SPK Ref Val
%RFC LowUmit HignLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00468 0.00200
0.00400 0.000380 108 75
125
Qualifiers: Value exceeds Maximum Contaminant Level.
B Analyte detected iri the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
J Analyte detected below quantitation limits
ND Not Detected
M
0
Manual Integration used to determine
RSD is greater than RSDlimit Original
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 17 of 30

SUM3310
MIT
Summit Environmental Technologies, Inc.
Win St.
QC SUMMARY REPORT
EA?4�IiC}.Nh1Ei�TlIL crt2Vp�Ckdai,, Ft�
Cuyahoga Falls, Ohio 44223
WO#: 19010533
A rnalyt�caY Laboraloneas TEL:
[phone] F.4X.• [phone]
Website: hQ://www.settek.com
21-.Tart-19
Client:
Synagro
Project:
Neuse Regional WASA
SatchID: 35549
Sample ID 19010659-002AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/1612019
RunNo: 93469
Client ID: Batcl =
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909440
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID 19010659-002AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1116/2019
RunNo: 93469
Client ID: BatchQC
Batch ID: 35549
TestNo: SW7470A SW7470A
Analysis Date: 1/16/2019
SegNo: 1909441
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00462 0.00200 0,00400 0.000380 106 75 125 0.00468 1.29 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H HoIding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 18 of 30
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

I
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SUMMA3310 Win St.
i=MIMONIMEMTAL Cuyahoga Falls, Ohio 44223
�:.rratytl ! Labcrarone�t TEL: [phone] FAX: [phone] WO#: 19010533
Website: http:llwww.settek.com 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID: R93297
lgnitability 8.08 7.240 0 112 70 130
lgnitability non-flammable 0 0 20
lgnitability non-flammable 0 0 20
lgnitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 19 of 30
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

MMIT
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENY1110N1-1ENTAL ECU MOLOG;NEZ, NC Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone] WO#: 19010533
Website: httn://www.settek.com 2I--Jan-I9
Client: Synagro
Project: Neuse Regional WASA
BatehlD: R93297
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Ignitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 20 of 30
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

SUMMISummit
Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
EK;4rHI014MENTAL I-ECHNOLOGIr_ ,
Cuyahoga Falls, Ohio 44223
hn�iyt�a P Laboratories TEL: [phone] FAX- [phone]
WO#: 19010533
Website: hQ:Ilivww.settek.com,
21-Jan-19
Client:
Synagro
Project:
Neuse Regional WASA
BatchID: R93297
Sample ID 19010534-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
;lient ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 1111/2019
SegNo: 1902705
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Quai
lgnitability non-flammable 0 0 20
Sample lD 19010535-001ADUP
SampType: DUP
TestCode: Ignitability_S Units:
Prep Date:
RunNo: 93297
Client ID: BatchQC
Batch ID: R93297
TestNo: SW1030
Analysis Date: 111112019
SegNo: 1902707
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
lgnitability non-flammable 0 0 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H IdoIding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 21 of 30
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDtimit
R RPD outside accepted recovery limits
Original

ummiSummit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
EKA'11'$0P,IAIEi, TAL 3ECHNL1LGGI-r$, WO Cuyahoga Falls, Ohio 44223
- 4..r?s1yd=i Lab6eA10r00s TEL: [phone] FAV..- [phone] WO#: 19010533
Website: hilp:llwww.settek.com 21-.Ian-19
Client: Synagro
Project: Neuse Regional WASA BatchID: R93390
Sample ID 19010535-01AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
,lient 1D: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/14/2019
SegNo: 1906045
analyte
Resuit
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
3yanide, Reactive 8.98 0.490 10.00 0 89.8 81.6 122
Sample ID 19010535-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 93390
client ID: BatchQC
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/1412019
SegNo: 1906046
analyte
Result
PQL SPK value SPK Ref Val
%REC LcwUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
cyanide, Reactive 9.09 0.495 10,00 0 90.9 81.6 122
Qualifiers: * Value exceeds Maximum Contaminant Level.
lq Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 22 of 30
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

summlir
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVI4t4NMENTAL Cit�NGiCCb IES,.
Cuyahoga Falls, Ohio44223
WO#: 19010533
tin&f�[ cal Laboraloaes TEL: [phone] FAX.- [phone]
Website: http://Www.settek.com
21-Tan-19
CIient:
Synagro
Project:
Neuse Regional WASA
BatchID: R93390
Sample I❑ LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mglL
Prep Date:
RunNo: 93390
'lient ID: LCSW
Batch ID: R93390
TestNo: SW9014
Analysis Date: 1/1412019
SegNo: 1906029
Malyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
9.57 0.490
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
10.00 0 95.7
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 23 of 30
85 115
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

UMMISummit Environmental Technologies, Inc. 3310 Win St, QC SUMMARY REPORT
ENVJi` ONMENTAL TECHNOf-OGIL Itt(I Cuyahoga Falls, Ohio 44223
Arr$(ytical Laboratories TEL: [phone] Ff1X.- [phone]
WQ#: 19010533
Website: htt :Ilwww.settek.com 21-Jan-19
CIient: Synagro
Project: Neuse Regional WASA BatchID: R93465
Sample ID 19010535-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
CIient ID: BatchQC
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/14/2019
SegNo: 1908916
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4210 25.0 4800 0 87.7 80 120
Sample ID
19010535-OOIAMSD SampType: MSD
TestCode:
Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 93465
Client ID:
BatchQC Batch ID: R93465
TestNo:
SW9034
Analysis Date: 1/1412019
SegNo: 1908917
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4320 25.0 4800 0 90.0 80 120 4210 2.58 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 24 of 30
E Value above quantitation range
M Manual integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

UMMITSummit
Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
�Ati�lit41Jh1hITAL ��r�a[ , : _ =
Cuyahoga Falls, Ohio 44223
Auaf Ucat Labanjlor€tts
TEL: [phone] FAX.- [phone]
WO#: 19010533
Website: http:llwivw.setteli.com
21-Tan-19
Client:
Synagro
Project:
Neuse Regional WASA
BatchID: R93465
Sample ID MB-R93465
SampType: MBLK
TestCode: Sulfide,React Units: mglL
Prep Date:
RunNo: 93465
Client ID: PBW
Batch ID: R93465
TestNo: SW9034
Analysis Date: 1/1412019
SegNo: 1908902
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowUmit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
ND 25.0
Sample ID LCS-R93465
SampType: LCS
TestCode:
Sulfide,React Units: mg1L
Prep Date:
RunNo: 93465
Client ID: LCSW
Batch ID: R93465
TestNo:
SW9034
Analysis Date: 111412019
SegNo: 1908903
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
4620 25.0 4800 0 96.2 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 25 of 30
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

umml
3310 Win StSummit Environmental Technologies, St. QC SUMMARY REPORT
frsmr .
iEWIRONNIeNTAL =EMINQLOGIFS, INC,' Cuyahoga Falls, Ohio 44223
AnIaly6ca1 TEL: [phone] FOX: [phone] WO#: 19010533
Website: htto:llwww.setteic com 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID• R93510
Sample ID CHECK 7 SampType: LCS
Client ID: LCSS Batch ID: R93510
Analyte Result
pH 7.0
Sample ID CHECK 7 SampType: LCS
Client ID: LCSS Batch ID: R93510
Analyte Result
pH 7.0
TestCode: pH S(9045D) Units: s.u.@21.6C Prep Date;
TestNo: SW9045D Analysis Date: 111712019
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
7.0 0 101 90 110
TestCode: pH_S(9045D) Units: s.u.@21.00 Prep Date:
TestNo: SW9045D Analysis Date: 1/1712019
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
7.0 0 101 90 110
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 26 of 30
RunNo: 93510
SegNo: 1911700
%RPD RPDLimit Qual
RunNo: 93510
SegNo: 1911706
%RPD RPDLimit Qual
B Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

UMMITSummit Environmental Technologies, Inc. 3310 Wan St. QC SUMMARY REPORT
EWli'OANIENTAL17ECHNOF0Gi_33,]N,P. Cuyahoga Falls, Ohio44223
ArpafyNcal Labc=ones TEL: [phone] FAX.- [phone] WO#: 19010533
Website: http:41www.settek.com 21-Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID: R93510
Sample ID LCS-R93510
SampType: LCS
TestCode:
pH_Oil(9045 Units: sm,@21.6C
Prep Date:
RunNo: 93510
Client ID: LCSW
Batch ID: R93510
TestNo:
SW9045D
Analysis Date: 1/17/2019
SegNo 1911010
Analyte
Result
PQL
SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDI-imit Qual
M
7.0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
7.0 0 101 90 110
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation Iimits
ND Not Detected
PL Permit Limit
Page 27 of 30
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ffISUMMIT
, lhk Cuyahoga Falls, Ohio 44223
AJ75eyticza Laboraiorj&+ TEE: (330) 253-82JJ FAY..- [phone] WO#: 19010533
Website: hft :11www.setteLcom 21_Jan-19
Client: Synagro
Project: Neuse Regional WASA BatchID• R93510
Sample ID 19010626-004ADUP SampType: DUP TestCode: pH_NPW{450 Units: sm.@20AC Prep Date:
CIient 1D: Batch4C Batch ID: R93510 TestNo: SW9045D Analysis Date: 1/17/2019
Analyte
pH
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
7.5 7.6
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
Page 28 of 30
RunNo: 93510
SegNo: 1911018
%RPD RPDLimit Qual
1.1 5 W
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original

Summit Environmental Technologies, Inc.
3310 Win Street
Cuyahoga Falls, Ohio 44223 Tel: [phone] Fax: 330.253.448
Analysis Request/Chain of Custody
For Summit Environmental Technologies, Ins use only
Pap -of- I sE:r No. I ql)M�
Company Name (Please Print)
Project Na=
wa.. M Me&Ws
,Pww
porn any ess �
Project Address
Id
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Client Phone N
ri
Report to
►t4c�� i,
Client Fax No. PMpase Fax 12MIIs J
Q
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"a 4
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Email Please "I Resssrlts J �
Quote No.
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4..[aiCt Ferjo�
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Salnplc tl by t
Check if 01do VAP samples ./
mnpleYde>�ifiesllvn
l7xfR
Ca
the
CuiiecGed
C?
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NoteslCommettts:
wmic anu yellow pages somia accompany sate r— to the laooratory. am cltent
k-, n lv
the pink page
oaeo�tr
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7 tOR of Sampk OtiVartc�
T�+�r� � ,MRTtFI�CATION REQU ED G h0
�+f t1:PORTTdSTATC(UWONLY) VVS- NO
if ycg, pknsc Provide PWS, M, & MP
•'if.is camlp&Ie s1T. 1rn sxsu s kb .. is nrd
Will rut moat 11W wsulo 4, xm.
12145�agjof1
Page 29 of 30

summilr
SannnzitEnvirazvrer�rat TechsTo(ogies, Inc.
3310 Win St.
l=i46VMONMENTAL TECHnaMO IF3. Wi-, Cuyahoga Falls, Ohio 44223 Sample Log -in Check List
Ayfaly0ca,l Car.boralorfes TEL: [phone] FAX.- [phone]
Websile: htiv:11mviv.seitek.com
Client Name: SYN-NC-27028
Logged by: Rachel Thomas
Completed By: Christopher Livengood
Reviewed By: Jennifer Woolf
Chain of CusfodV
1. Is Chain of Custody complete?
2. How was the sample delivered?
Log In
3. Coolers are present?
Work Order Number: 19010533
1/10/2019 10:15:00 AM
1/10/2019 2:52:12 PM
1/11/2019 9:50:31 AM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping containerlcooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >4° C to 6.0'C
7, Sample(s) in proper container(s)?
g• Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 114 inch or 6 mm?
12. Were any sample containers received broken?
13. does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14• Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16, Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handlin_q (if applicable)
Yes 0
UPS
Yes❑
Yes ❑�
Yes ❑
Signed By:
Yes W
Yes W
Yes ❑�
Yes ❑�
Yes❑
Yes ❑
Yes ❑
Yes ❑
Yes 0
Yes ❑�
Yes
Yes U
RcptNo: 1
No ❑ Not Present 1 1
No ❑ NA ❑
No ❑
No ❑ Not Present
No ❑ NA ❑
No ❑ NA ❑
No ❑
No ❑
No ❑
No S?]
No ❑
No 0
No ❑
No ❑
No ❑
No ❑
NA ❑
No VOA Vials 0
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: l Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed By
�1 2,1 Good Not Present
Page 30 of 30

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Neuse Regional Water and Sewer Authority WQ Permit Number: WQ0034688
WWTP Name: Neuse Regional Water Treatment Plant NPDES Number: NCO088111
Monitoring Period: From
01/01/19 To 12/31/19
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
It. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying bleat Treatment Thermopbilic
Beta Ray Gamma Ray Pasteurization
Class A:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens".
Lime Stabilization Air Drying
Anaerobic Digestion
Composting Aerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
<240
<240
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying -- Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CPR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32I15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CPR 503.33/15A NCAC 02T.1107 have not been met." (PIease note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certilicat' including fine and imprisonment."
Harold Herring, Executive Director NRWASA U'
Preparer NanyAd Title ( or ^ Land Applier Name and if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
190437 01 NR1
02 NR2
NC DENR #664
NC PHHS #37799
US EPA #NC01918
190437
Yes
J. Zubeck 03/07/19
3tudgE Gr Fee. Collform-S <287 MPNlg 10 03108/19 ERP 9223 - MPN
TS (%) 0.627% % 0.01 03/08/19 ERP 2540 G -TS
3109E Gr Fec. Coliform-S <240 MPN/g 10 03/08/19 ERP 9223 - MPN
TS (%) 0.749% % 0.01 03/08/19 ERP 2540 G -TS
Report '
Review LIP
Protect Manager date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 chris(a camerontesting,com

219S. Steele Str. Cameron Testing Services, Inc. chain of Custo
Sanford, NC 27330 '
Phone: , NC 27330 NC WWIGW Cert. #654 NC PHHS Cert# 37799 US EPA NC01918 Page
Company:
Contact:
Address Ci
State, Zip)
Project:
V1I1 � �
�--
J � 1/�S
r J
Email:
i Phane:
Fax:
Notes:
— --
CTS lab use only
Sample } emp ;'� / Pro!. --
Arrive:
j Due: I
Regulatory - Rush
(YIN) (YfN)
Collected:
!Name:
� i �
Signature:
Sample Information
Number of bottles
Requested Analysis
Sample ID
m a x
o
8V
?
}
L
ca % m
ua, m o [7 a o
a r r rn
O
Preservatives: (U)npreserved, H(C)I,
H2(5)O4, H(OtOher(X},)Indicateate, Na(0)H,
CTS LabQy
l�
- — -
nn
Ocss
4Fcec,Relinquished:
Received:
Dateffime
C/7 4y-
Rush work will require prior approval. Additional charges will apply

SECTION 6

Agricultural Lime Application Log
Year: 2019
Project. Neuse Regional,WASA
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(tonstacre)
Tons/Acre
Applied
Date Applied
NC-LN-X6-1
5.4
1.3
NC-LN-X6-2
5.4
1.3
NC-LN-X6-3
5.6
0.9
NC-LN-X6-4
5.6
1.0
NC-LN-X5-1
5.9
0.5
NC-LN-X5-2
5.8
0.5
N C-LN-X5-3
6
0
'crop In the field, Will be applied after harvest.

SECTION 7

Page 1 of 1
Report No: 20-045-0768
Account No: 46463
Advisor: Synagro Central i Kinston
Marshall Puryear
284 Boger Road
Suite 204
Mocksville NC 27028
Comment:
Waypoeint(!D
ANALYTICAL
Client: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Form: Li
Date Received: 02/14/2020
Date of Report: 02/1712020
Test result units = CEC and Na in meg1100cm3; NQ3 N in mgldm3; W1V in glcm3
North Carolina Division of Water Quality Certifoatior #257, Analysis and fertility recommendations shown on this report are performed In accordance within NCOA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 1
Report No; 19-029-0541
Account No: 46485
Advisor: Synagro Central LLCI Roanoke Rapids
Marshall Puryear
284 Boger Road
Suite 204
Mocksville NC 27889
Lab No
Field ID
Sample ID
06884
NR-1
06885
NR-2
06386
NR-3
06887
NR-4
Comment:
Waypoint,.(D
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Client: Mike Ginn
Farm: NR
NRVVASA
Date Received: 01/29/2019
Date of Report: 01/30/2019
Soil Class
HM%
WN pH Ac P-1
K 1
S-1
Mn-1
Zn-1
Zn-Al Cu-1 CEC SS% Ca% Mg%
ESP
Na SS-1 NO3-N
MIN
0.9
5.4 1.4 158
53
58
44
150
150 320 4.8 71 52 13
1.4
0.1
MIN
1A
5.4 1.0 129
48
54
44
88
88 290 3.6 71 52 11
1.8
0.1
MIN
0.9
5.6 0.9 136
57
73
44
90
90 285 3.7 77 53 14
2.1
0.1
MIN
1.1
5.5 0.8 67
47
94
38
75
75 475 3.0 74 53 11
2.0
0.1
Test result units = CEC and Na in meg1100cm3; NO3 N in mgldrn3; W/V in glcm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analvsis oreoared bv: Wavooint Ana[vtical Viroinia. Ina