WQ0005568_Residual Annual Report 2019_20200228

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/28/2020
Received:*
Project Number* WQ0005568
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0005568
ApplicantTermittee * City of Rocky Mount
Facility Name * City of Rocky Mount RLAP
Phone Number*
2528839301
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Rocky Mount Annual Report.pdf 10.74MB
upload only 1 RDF document. NL@iple documents must be combined into one RDF file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/28/2020

CITY OF ROCKY MOUNT
2019 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0005568
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
February 20, 2020
SOIL PLUS

SOIL PLUS
February 20, 2020
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2019 LAND APPLICATION ANNUAL REPORT
City of Rocky Mount "Class B" Program
NC Permit No.: WQ0005568
Soil Plus Project No. 200703.Al2
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the City of Rocky Mount on behalf of
Granville Farms, Inc. Soil Plus compiled this report using data gathered during the
compliance year. This data includes (1) certification form, (2) residual sampling, (3) field
loading calculations, (4) pathogen and vector attraction reduction documentation, (5)
standard soil fertility nutrient analysis.
The City of Rocky Mount conducted application events on permitted fields in Nash and
Edgecombe counties during 2019. A total of 1,747.82 dry tons or 14,620,500 gallons of
permitted residual biosolids were land applied to the City of Rocky Mount's permitted
fields (including Tar River Regional WWTP, Sunset WTP, and Tar River WTP). A total of
814.53 dry tons or 7,120,500 gallons of permitted residual biosolids were land applied to
Granville Farms permitted fields in Edgecombe, Franklin, Halifax, Johnston, Martin, Nash,
and Wake counties under permit numbers WQ0000838 and WQ0035595. An additional
469,000 gallons from Tar River WTP was taken to drying beds at Tar River Regional
WWTP for further processing.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the City of Rocky Mount (252-972-1401) for further
assistance.
Respectfully,
Drew Matthews, Soil Plus
PO Box 1396
Oxford, NC 27565
Brenton Bent, City of Rocky Mount
[phone]
Jason Smith, Granville Farms
dmatthewsgsoilplus.ne t
www.soilplus.net

City of Rocky Mount
2019 Annual Land
Application of
Residual Biosolids
Report
WQ0005568
Rocky Mount, NC
Annual Land Application
Certification Form
Annual Residual Sampling
Summary Forms
Field Loading
Summary Forms
Pathogen & Vector Attraction
Reduction Forms
2019 Soil Samples

City of Rocky Mount
2019 Class B Annual Report
WQ Permit# WQ0005568
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
WQ0005568 City of Rocky Mount Granville Farms, Inc. Edgecombe [phone]
Year: 2019
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. also, If residuals were generated but not land applied, please attach an explanation on how the
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 139
Total number of fields utilized for land application during the year: 22
Total amount of dry tons applied during the year for all application sites: 1747.82
Total number of acres utilized for land application during the year: 521.85
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below issued by the Division of Water Quality ❑d A
I f no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
facilities) .
8. All monitoring and reporting requirements in 15.E NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated
facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified by the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Brenton Bent, Public Works Director
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Wednesday, FebrMtry 19, 2020
2 2CD ?rJ2 0
Sign ure of Permittee �te
11-1 ZX02vm
Signature of Land Applier Date
(if different from Permittee)

Source Summary Report
WWTP
Sunset Ave WTP
Tar River Regional WWTP
Tar River WTP
Total
VolumeApplied , �Total�
1,288,000 246.98
8,495,500 976.53
4,837,000 673.79
14,620,500 1897.29
Friday, February 21, 2020 Page 1 of 1

Site# 1
Site# 22
Site# 25
YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
1 36.07
466,500
69.59
41.93
Fescue Pasture
141
29.7%
2 27.07
247,000
28.84
48.24
Fescue Pasture
141
34.2%
1 19.24
392,500
40.50
81.64
Fescue Pasture
198
41.2%
2 32.91
638,500
72.60
94.10
Fescue Pasture
211
44.6%
1A
17.77
232,000
23.39
51.65
Fescue Pasture
172
30.0%
1B
22.95
2,573,000
458.70
58.76
Pine
75
78.3%
1C
9.46
1,101,000
208.60
46.94
Pine
75
62.6%
1D
7.11
189,500
14.45
65.18
Fescue Pasture
172
37.9%
1E
12.59
218,000
15.36
34.70
Fescue Pasture
172
20.2%
1F
5.44
97,500
11.82
96.01
Fescue Pasture
148
64.9%
Friday, February 21, 2020 Page 1 of 3

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED
PERMITTED
CROPS AND
LOADING RATES
Acres
Volume
Crop 1 PAN
Crop 2 PAN
Crop 1 PAN 1
Crop 2
PAN 2
Field
Used
Applied
Total DT
lbs/Ac.
lbs/Ac.
Crop 1 Name
PAN
Used
Crop 2 Name
PAN
Used
2
22.74
624,500
68.24
134.53
Fescue Hay
158
85.1%
3
18.28
398,500
32.54
111.86
Fescue Pasture
151
74.1%
4
42.99
1,489,000
160.52
158.31
5.79
Common
192
82.5%
Annual Ryegrass -
50
11.6%
Bermudagrass Hay
Hay
5
69.68
1,251,500
146.89
56.11
Fescue Pasture
158
35.5%
6
33.89
1,706,000
176.15
185.67
13.39
Common
225
82.5%
Annual Ryegrass -
50
26.8%
Bermudagrass Hay
Hay
7
23.9
926,500
103.20
189.11
4.27
Common
225
84.0%
Annual Ryegrass -
50
8.5%
Bermudagrass Hay
Hay
8
4.38
28,000
1.12
0.65
Pine
75
0.9%
9A
4.38
42,000
1.68
0.98
Pine
75
1.3%
9B
13.83
344,500
42.53
131.38
Fescue Hay
194
67.7%
Site# 41
1
56.7
1,099,500
141.86
81.74
Wheat, Grain
125
65.4%
2
28.62
438,000
64.56
60.93
Wheat, Grain
125
48.7%
3B
11.85
117,000
14.15
68.70
Wheat, Grain
91
75.5%
Friday, February 21, 2020
Page 2 of 3

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
Total 14, 620,500 1,897.29
Friday, February 21, 2020 Page 3 of 3

City of Rocky Mount
2019 Class B Annual Report
WQ Permit# WQ0005568
Residual Sampling Summary Forms
Tar River Regional WWTP
Sunset WTP
Tar River WTP
Field Loading Calculations
2019 Analytical
2019 TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0005568 Facility Name City of Rocky Mount Source Permit No. NC0030317 Source Name Tar River Regional W WTP
Laboratory 1
Laboratory 2
Sample or CompositeDate
Parameter (mg/Kg) Class A Class B
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
City of Rocky
Mount
Meritech, Inc.
City of Rocky
Mount
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analytical
Pace Analyuca
1/10/2019
1/3/2019
4/12/2019
5/16/2019
6/4/2019
6/7/2019
7/2/2019
7/10/2019
8/30/2019
12/19/2019
12/31/2019
Aluminum
N/A
N/A
13,700
24,000
17,000
18,020
3,300
17,500
17,100
13,500
14,500
9,580
10,813
Ammonia Nitrogen
N/A
N/A
34,690.00
45,125.00
26,464.00
29,142.00
39,200.00
38,667.00
33,656.00
23,733.00
23,103.00
6,080.00
14,655.00
Arsenic
41
75
23.3
44.8
23.5
22.97
30.9
28
30.1
28.3
26
1.63
4
Cadmium
39
85
23
4.5
23
2.28
3.1
2.8
>
2.8
2.6
1.27
1.2
Calcium
N/A
N/A
14,100
3,401)
11,400
18,416
15,600
13,400
14,100
10,900
12,300
12800
15,889
Copper
1,500
4,3W
709
1170
544
562
748
680
713
507
619
611
672
Lead
300
840
49.2
97.6
405
50.7
63.2
54.8
55.4
40.1
51.6
44.8
50
Magnesium
N/A
N/A
4,310.00
6,320.00
3,550.00
3,881.00
3,380.00
3,030.00
3,510.00
4,410.00
4,820.00
3,840.00
4,560.00
Mercury
17
57
0.62
1.8
0.34
0.446
0.6
0.71
0.48
0.63
0.78
0.065
0.39
Molybdenum
N/A
75
15.8
28.1
16
13.9
19.7
18.9
19.7
14.2
132
10.3
12
Nickel
420
420
48.4
90.3
46
51
57.7
50.1
54.4
45.7
51.8
45.8
51
Nitrate -Nitrite Nitrogen
N/A
N/A
105.00
156.00
129.O0
142.00
249.00
196.00
180.00
87.00
185.00
327.00
267.00
Percent Solids
N/A
N/A
2.90
1.60
2.80
3.03
3.00
3.00
3.20
3.00
290
3.06
275
pH (no units)
N/A
N/A
7.45
7.45
7.44
7.22
7.79
7.66
7.50
7.09
7.20
6.60
7.43
Phosphorus
N/A
N/A
29 345.00
36,188.00
28,643.00
27,492.00
27,900.00
29,600.00
29,28L00
30,433.00
30,448.00
25,300.00
34,727.00
Potassium
N/A
N/A
11,600.00
22,400.00
11,700.00
11,485.00
15,500.00
14,000.00
15,000.00
14,200.00
13,000.00
5,850.00
6,966.00
PAN (Inj./Inc.)
N/A
N/A
46,112
58,444
35,872
37,809
46,479
44,953
39,274
33,520
37,378
17,43
22951
PAN (Surface)
N/A
N/A
28,767
35,881
- 640
3,38
26,879
25,620
22,446
21,654
25,826
14,383
15,63
Selenium
100
100
3.3
44.8
3.5
22.97
30.9
28
30.1
28.3
26
1.63
5.3
Sodium
N/A
N/A
11,600.00
222,400.00
11,700.00
11,485.00
15,500.00
14,000.00
15,000.00
14,200.00
13,000.00
2 850.00
3,859.00
SAR
N/A
N/A
3.72
4.3
4.09
3.48
5.07
4.91
5.22
5.01
4.27
0.99
1.15
TKN
N/A
N/A
72,414
89,000
57,393
57,558
62,633
58,967
51,781
56,067
70,069
42,800
41,418
Zinc
2,800
7,500
585
1150
554
578
733
712
G3G
5G0
G3
G.4
GGS
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
subnyitt ng false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer 67 Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 1/10/2019
Solids 2.9
Mineralization Rate 0.30
Gallons per DT 8,269.25
pH 7.45
Sodium Absorpotion 3.72 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 72,414 lbs./1,000 gal 17.51
Ammonia Nitrogen (mg/Kg) 34,690.00 lbs./1,000 gal 8.39
Nitrate -Nitrite (mg/Kg) 105.00 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 28,767 lbs./1,000 gal 6.96
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 46,112 lbs./1,000 gal 11.15
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.81
Phosphorus lbs./1,000 gal 7.10
Calcium lbs./1,000 gal 3.41
Magnesium lbs./1,000 gal 1.04
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
23.30
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
709.00
Copper lbs./1,000 gal
0.17
Lead (mg/Kg)
49.20
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.62
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
48.40
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
23.30
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
585.00
Zinc lbs./1,000 gal
0.14
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
72,414
28,767
57.53
43,647
72,414
46,112 92.22
26,302
43,647
6,547
13.09
37,100
26,302
3,945 7.89
22,357
37,100
2,782
5.56
34,317
22,357
1,677 3.35
20,680
34,317
1,287
2.57
33,030
20,680
775 1.55
19,904
33,030
619
1.24
32,411
19,904
373 0.75
19,531
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 40,003 80.01
Total 52,883 105.77

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 1/23/2019
Solids 1.6
Mineralization Rate 0.30
Gallons per DT 14,988.01
pH 7.45
Sodium Absorpotion 4.23 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 89,000 lbs./1,000 gal 11.88
Ammonia Nitrogen (mg/Kg) 45,125.00 lbs./1,000 gal 6.02
Nitrate -Nitrite (mg/Kg) 156.00 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 35,881 lbs./1,000 gal 4.79
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 58,444 lbs./1,000 gal 7.80
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.99
Phosphorus lbs./1,000 gal 4.83
Calcium lbs./1,000 gal 3.12
Magnesium lbs./1,000 gal 0.84
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
44.80
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
4.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
1170.00
Copper lbs./1,000 gal
0.16
Lead (mg/Kg)
97.60
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
1.80
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
90.30
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
44.80
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
1150.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
89,000
35,881 71.76
53,119
89,000
58,444 116.89
30,557
53,119
7,968 15.94
45,151
30,557
4,583 9.17
25,973
45,151
3,386 6.77
41,765
25,973
1,948 3.90
24,025
41,765
1,566 3.13
40,199
24,025
901 1.80
23,124
40,199
754 1.51
39,445
23,124
434 0.87
22,691
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 49,555 99.11
Total 66,309 132.62

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 4/12/2019
Solids 2.8
Mineralization Rate 0.30
Gallons per DT 8,564.58
pH 7.44
Sodium Absorpotion 4.09 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 57,393 lbs./1,000 gal 13.40
Ammonia Nitrogen (mg/Kg) 26,464.00 lbs./1,000 gal 6.18
Nitrate -Nitrite (mg/Kg) 129.00 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 22,640 lbs./1,000 gal 5.29
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 35,872 lbs./1,000 gal 8.38
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.73
Phosphorus lbs./1,000 gal 6.69
Calcium lbs./1,000 gal 2.66
Magnesium lbs./1,000 gal 0.83
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
23.50
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
544.00
Copper lbs./1,000 gal
0.13
Lead (mg/Kg)
40.50
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.34
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
46.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
23.50
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
554.00
Zinc lbs./1,000 gal
0.13
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
57,393
22,640 45.28
34,753
57,393
35,872 71.74
21,521
34,753
5,213 10.43
29,540
21,521
3,228 6.46
18,293
29,540
2,216 4.43
27,325
18,293
1,372 2.74
16,921
27,325
1,025 2.05
26,300
16,921
635 1.27
16,287
26,300
493 0.99
25,807
16,287
305 0.61
15,981
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 31,586 63.17
Total 41,412 82.82

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 5/16/2019
Solids 3.03
Mineralization Rate 0.30
Gallons per DT 7,914.46
pH 7.22
Sodium Absorpotion 3.48 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 57,558 lbs./1,000 gal 14.55
Ammonia Nitrogen (mg/Kg) 29,142.00 lbs./1,000 gal 7.36
Nitrate -Nitrite (mg/Kg) 142.00 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 23,238 lbs./1,000 gal 5.87
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 37,809 lbs./1,000 gal 9.55
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.90
Phosphorus lbs./1,000 gal 6.95
Calcium lbs./1,000 gal 4.65
Magnesium lbs./1,000 gal 0.98
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
22.97
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.28
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
562.00
Copper lbs./1,000 gal
0.14
Lead (mg/Kg)
50.70
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.45
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
51.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
22.97
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
578.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
57,558
23,238 46.48
34,320
57,558
37,809 75.62
19,749
34,320
5,148 10.30
29,172
19,749
2,962 5.92
16,787
29,172
2,188 4.38
26,984
16,787
1,259 2.52
15,528
26,984
1,012 2.02
25,972
15,528
582 1.16
14,946
25,972
487 0.97
25,485
14,946
280 0.56
14,665
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 32,073 64.15
Total 42,893 85.79

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 6/4/2019
Solids 3
Mineralization Rate 0.30
Gallons per DT 7,993.61
pH 7.79
Sodium Absorpotion 5.07 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 62,633 lbs./1,000 gal 15.67
Ammonia Nitrogen (mg/Kg) 39,200.00 lbs./1,000 gal 9.81
Nitrate -Nitrite (mg/Kg) 249.00 lbs./1,000 gal 0.06
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 26,879 lbs./1,000 gal 6.73
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 46,479 lbs./1,000 gal 11.63
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.88
Phosphorus lbs./1,000 gal 6.98
Calcium lbs./1,000 gal 3.90
Magnesium lbs./1,000 gal 0.85
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
30.90
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
3.10
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
748.00
Copper lbs./1,000 gal
0.19
Lead (mg/Kg)
63.20
Lead lbs./1,000 gal
0.02
Mercury (mg/Kg)
0.60
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
57.70
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
30.90
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
733.00
Zinc lbs./1,000 gal
0.18
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
62,633
26,879 53.76
35,754
62,633
46,479 92.96
16,154
35,754
5,363 10.73
30,391
16,154
2,423 4.85
13,731
30,391
2,279 4.56
28,112
13,731
1,030 2.06
12,701
28,112
1,054 2.11
27,057
12,701
476 0.95
12,225
27,057
507 1.01
26,550
12,225
229 0.46
11,996
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 36,083 72.17
Total 50,637 101.27

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 6/7/2019
Solids 3
Mineralization Rate 0.30
Gallons per DT 7,993.61
pH 7.66
Sodium Absorpotion 4.91 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 58,967 lbs./1,000 gal 14.75
Ammonia Nitrogen (mg/Kg) 38,667.00 lbs./1,000 gal 9.67
Nitrate -Nitrite (mg/Kg) 196.00 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 25,620 lbs./1,000 gal 6.41
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 44,953 lbs./1,000 gal 11.25
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.50
Phosphorus lbs./1,000 gal 7.41
Calcium lbs./1,000 gal 3.35
Magnesium lbs./1,000 gal 0.76
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
28.00
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.80
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
680.00
Copper lbs./1,000 gal
0.17
Lead (mg/Kg)
54.80
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.71
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
50.10
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
28.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
712.00
Zinc lbs./1,000 gal
0.18
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
58,967
25,620
51.24
33,348
58,967
44,953 89.91
14,014
33,348
5,002
10.00
28,345
14,014
2,102 4.20
11,912
28,345
2,126
4.25
26,219
11,912
893 1.79
11,019
26,219
983
1.97
25,236
11,019
413 0.83
10,605
25,236
473
0.95
24,763
10,605
199 0.40
10,406
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 34,204 68.41
Total 48,561 97.12

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 7/2/2019
Solids 3.2
Mineralization Rate 0.30
Gallons per DT 7,494.00
pH 7.5
Sodium Absorpotion 5.22 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 51,781 lbs./1,000 gal 13.82
Ammonia Nitrogen (mg/Kg) 33,656.00 lbs./1,000 gal 8.98
Nitrate -Nitrite (mg/Kg) 180.00 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 22,446 lbs./1,000 gal 5.99
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 39,274 lbs./1,000 gal 10.48
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 4.00
Phosphorus lbs./1,000 gal 7.81
Calcium lbs./1,000 gal 3.76
Magnesium lbs./1,000 gal 0.94
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
30.10
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
3.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
713.00
Copper lbs./1,000 gal
0.19
Lead (mg/Kg)
55.40
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.48
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
54.40
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
30.10
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
636.00
Zinc lbs./1,000 gal
0.17
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
51,781
22,446 44.89
29,336
51,781
39,274 78.55
12,508
29,336
4,400 8.80
24,935
12,508
1,876 3.75
10,631
24,935
1,870 3.74
23,065
10,631
797 1.59
9,834
23,065
865 1.73
22,200
9,834
369 0.74
9,465
22,200
416 0.83
21,784
9,465
177 0.35
9,288
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 29,997 59.99
Total 42,493 84.99

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 7/10/2019
Solids 3
Mineralization Rate 0.30
Gallons per DT 7,993.61
pH 7.09
Sodium Absorpotion 5.01 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 56,067 lbs./1,000 gal 14.03
Ammonia Nitrogen (mg/Kg) 23,733.00 lbs./1,000 gal 5.94
Nitrate -Nitrite (mg/Kg) 87.00 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 21,654 lbs./1,000 gal 5.42
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 33,520 lbs./1,000 gal 8.39
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.55
Phosphorus lbs./1,000 gal 7.61
Calcium lbs./1,000 gal 2.73
Magnesium lbs./1,000 gal 1.10
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
28.30
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.80
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
507.00
Copper lbs./1,000 gal
0.13
Lead (mg/Kg)
40.10
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.63
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
45.70
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
28.30
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
560.00
Zinc lbs./1,000 gal
0.14
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
56,067
21,654 43.31
34,413
56,067
33,520 67.04
22,547
34,413
5,162 10.32
29,251
22,547
3,382 6.76
19,165
29,251
2,194 4.39
27,057
19,165
1,437 2.87
17,727
27,057
1,015 2.03
26,043
17,727
665 1.33
17,063
26,043
488 0.98
25,554
17,063
320 0.64
16,743
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 30,513 61.03
Total 39,324 78.65

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 8/30/2019
Solids 2.9
Mineralization Rate 0.30
Gallons per DT 8,269.25
pH 7.2
Sodium Absorpotion 4.27 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 70,069 lbs./1,000 gal 16.95
Ammonia Nitrogen (mg/Kg) 23,103.00 lbs./1,000 gal 5.59
Nitrate -Nitrite (mg/Kg) 185.00 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 25,826 lbs./1,000 gal 6.25
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 37,378 lbs./1,000 gal 9.04
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.14
Phosphorus lbs./1,000 gal 7.36
Calcium lbs./1,000 gal 2.97
Magnesium lbs./1,000 gal 1.17
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
26.00
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.60
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
619.00
Copper lbs./1,000 gal
0.15
Lead (mg/Kg)
51.60
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.78
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
51.80
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
26.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
623.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
70,069
25,826 51.65
44,243
70,069
37,378 74.76
32,691
44,243
6,636 13.27
37,606
32,691
4,904 9.81
27,788
37,606
2,820 5.64
34,786
27,788
2,084 4.17
25,703
34,786
1,304 2.61
33,481
25,703
964 1.93
24,740
33,481
628 1.26
32,854
24,740
464 0.93
24,276
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 37,215 74.43
Total 45,793 91.59

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 12/19/2019
Solids 3.06
Mineralization Rate 0.30
Gallons per DT 7,836.87
pH 6.6
Sodium Absorpotion 0.99 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 42,800 lbs./1,000 gal 10.92
Ammonia Nitrogen (mg/Kg) 6,080.00 lbs./1,000 gal 1.55
Nitrate -Nitrite (mg/Kg) 327.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 14,383 lbs./1,000 gal 3.67
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 17,423 lbs./1,000 gal 4.45
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.49
Phosphorus lbs./1,000 gal 6.46
Calcium lbs./1,000 gal 3.27
Magnesium lbs./1,000 gal 0.98
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
1.63
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.27
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
611.00
Copper lbs./1,000 gal
0.16
Lead (mg/Kg)
44.80
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.07
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
45.80
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
1.63
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
6.40
Zinc lbs./1,000 gal
0.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
42,800
14,383 28.77
28,417
42,800
17,423 34.85
25,377
28,417
4,263 8.53
24,154
25,377
3,807 7.61
21,570
24,154
1,812 3.62
22,343
21,570
1,618 3.24
19,953
22,343
838 1.68
21,505
19,953
748 1.50
19,204
21,505
403 0.81
21,102
19,204
360 0.72
18,844
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 21,698 43.40
Total 23,956 47.91

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River Regional WWTP
Sampling Date 12/31/2019
Solids 2.75
Mineralization Rate 0.30
Gallons per DT 8,720.30
pH 7.43
Sodium Absorpotion 1.15 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 41,418 lbs./1,000 gal 9.50
Ammonia Nitrogen (mg/Kg) 14,655.00 lbs./1,000 gal 3.36
Nitrate -Nitrite (mg/Kg) 267.00 lbs./1,000 gal 0.06
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 15,623 lbs./1,000 gal 3.58
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 22,951 lbs./1,000 gal 5.26
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.60
Phosphorus lbs./1,000 gal 7.96
Calcium lbs./1,000 gal 3.64
Magnesium lbs./1,000 gal 1.05
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.20
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
672.00
Copper lbs./1,000 gal
0.15
Lead (mg/Kg)
50.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.39
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
51.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.30
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
661.00
Zinc lbs./1,000 gal
0.15
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
41,418
15,623 31.25
25,795
41,418
22,951 45.90
18,467
25,795
3,869 7.74
21,925
18,467
2,770 5.54
15,697
21,925
1,644 3.29
20,281
15,697
1,177 2.35
14,520
20,281
761 1.52
19,520
14,520
544 1.09
13,975
19,520
366 0.73
19,154
13,975
262 0.52
13,713
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 22,264 44.53
Total 27,705 55.41

2019 City of Rocky Mount Analytical Report
Technical Services Laboratory
WQ Permit Number: WQ0005568 Laborator 1) City of Rocky Mount
Sample Identification : City of Rocky Mount Biosolids performing 2) Pace Analytical
Residual Source WQ # or NPDES #: NC 0030317 analyses: 3) Environment-1
Facility Name: Tar River Regional W WTP
Residual Analysis Data
Parameter (mg/kg)
Ceiling Conc.
Limit
(mg/kg)
Sample or Composite
Date
1/10/19
1/23/19
4/12/19
5/16/19
6/4/19
6/7/19
7/2/19
7/10/19
8/30/19
12/31/19
Digester ID that is being Land
Applied (hauled from):
Digester #:
4
1
1
3
2
2
4
1
2
1
Temperature °C (1)
28.4
22.2
25.0
28.1
30.3
33.4
33.5
32.6
33.7
23.0
Percent Solids (1)
NA
2.90%
1.60%
2.80% 1
3.03%
3.00%
3.00%
3.20%
1 3.00%
2.90%
2.75%
Percent Volatile Solids (1)
NA
65.0
55.3
67.2
62.1
62.5
63.6
62.8
63.6
63.5
68.8
pH (1)
7.45
7.45
7.44
7.22
7.79
7.66
7.50
7.09
7.2
7.43
Arsenic (2)
75
23.300
44.80
23.50
22.97
30.90
28.00
30.10
28.30
26.00
4.00
Cadmium (2)
85
2.300
4.50
2.30
2.28
3.10
2.80
3.00
2.80
2.60
1.20
Copper (2)
4,300
709
1170
544
562
748
680
713
507
619
672.0
Lead (2)
840
49.20
97.6
40.5
50.7
63.2
54.8
55.4
40.1
51.6
50.0
Mercury (2)
57
0.620
1.800
0.340
0.446
0.600
0.710
0.480
0.630
0.780
0.390
Molybdenum (2)
75
15.80
28.1
16.0
13.9
19.70
18.90
19.70
14.2
13.2
12.0
Nickel (2)
420
48.40
90.3
46.0
51.0
57.7
50.1
54.4
45.7
51.8
51.0
Selenium (2)
100
23.300
44.80
2350
22.97
30.90.
28.00
30.10
28.30
26.00
5.30
Zinc (2)
7,500
585
1150
554
578
733
712
636
560
623
661
Total Phosphorus (1)
NA
29345
36188
28643
27492
27900
29600
29281
30433
30448
34727
TKN (1)
NA
72414
89000
57393
57558
62633
58967
51781
56067
70069
41418
Ammonia -Nitrogen (1)
NA
34690
45125
26464
29142
39200
38667
33656
23733
23103
14655
Nitrate and Nitrite (1)
NA
105
156
129
142
249
196
180
87
185
267
Potassium (
11600
22400
11700
11485
15500
14000
15000
14200
13000
6966
Sodium (2)
NA
11600
22400
11700
11485
15500
14000
15000
14200
13000
3859
Magnesium (2)
NA
4310
6320
3550
3881
3380
3030
3510
4410
4820
4560
Calcium (2)
NA
14100
23400
11400
18416
15600
13400
14100
10900
12300
15889
Silver (2)
NA
11.600
22.40
11.70
11.49
15.50
14.00
15.00
14.20
13.00
4.00
Aluminum (2)
NA
13700
24000
17000
18020
23300
17500
17100
13500
14500
10813
PAN
NA
1 28767
35881
22640
23238
26879
25619
22446
1 21654
1 25826
15624
SAR (wet)
NA
1 3.72
1 4.23
4.09
3.48
5.07
4.91
522
5.01
1 4.27
1.15
Loa ( 6500 gal)
NA
1 45.2
1 31.1
34.4
38.2
43.7
41.7
38.9
1 35.2
1 40.6
23.3
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false iuJormation, including the possibility of fines and imprisonment for knowing violations."
Lin
aZ a2 �Za b
Lab Supervisor/Manager Date
(1) Analyses performed by City of Rocky Mount Laboratory
(2) Analyses performed by Pace Analytical

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Work Order # 12191950
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite, Nitrogen
Aluminum, total
Arsenic, total
Cadmium, total
Calcium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorus, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
pH
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: RM 121919 Grab
Results
3.06 %
6,080 mg/kg
42,800 mg/kg
<327 mg/kg
9,580 mg/kg
<1.63 mg/kg
1.27 mg/kg
12,800 mg/kg
611 mg/kg
44.8 mg/kg
3,840 mg/kg
0.065 mg/kg
10.3 mg/kg
45.8 mg/kg
25,300 mg/kg
5,850 mg/kg
<1.63 mg/kg
2,850 mg/kg
6.40 mg/kg
6.6 S.U.
Analysis Date
12/20/19
12/26/19
12/26/19
12/24/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/24/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/31/19
12/20/19
Report Date: 1/6/2020
Project: Rocky Mount WWTP
Date Sample Rcvd: 12/19/2019
Reporting Limit
0-100 %
10 mg/kg
20 mg/kg
327 mg/kg
2.50 mg/kg
1.63 mg/kg
0.200 mg/kg
10.0 mg/kg
1.00 mg/kg
0.500 mg/kg
10.0 mg/kg
0.02 mg/kg
0.500 mg/kg
2.0 mg/kg
2.00 mg/kg
20.0 mg/kg
1.63 mg/kg
20.0 mg/kg
0.500 mg/kg
1.0 - 14.0 S.U.
12/19/19
Method
SM 2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500-HB
I hereby certify that I have reviewed and approve these data. '"Mo, - DQZW --
Laboratory Re resentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3202013
Chain of Custody Record (COC)
NPDES#:
Client: SOII Plus Phone: [phone]
Address: PO Box 1396 Fax: [phone]
Oxford, NC 27565 Email: [e-mail]
Project: Rocky Mount WWTP
P.O.#:
Attention: Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that a I Email(preferred), Fax, Mail Std(Os) 3-5 Days )a�S
apply:
M E RITECH, INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): Drew Matthews } !t� v iL .
Lab Use Only
Start
End
Comp.
Grab?
#of
cont,
Test(s)
Required
On Ice?
Yes / No
pH OK?
CI OK?
Date
Time
Date
Time
RM 121919
12/19/19
��` '. ', 4,a,1,
G
2
Residual Analysis (Al, Ammonia-N, As, Cd, Ca, Cu, Pb,
Mg, Hg, MID, Ni, Nitrate -Nitrite N, %TS, pH, P, K, Se,
Na, TKN, Zn)
Temperature Upon
Receipt:
Method Of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Comments: Please report Residual Analysis results in mg/kg
Please email results to [e-mail]
Compositor #
Jug #
O UPS
Fed Ex
Are these results for regulatory purposes? Yes
n No 0,
Report results in: mg/L Q mg/kg Q`= ug/L
Q Hand Delivery
Relinquished by:- ; Date:,
jime:
I t
Received by: Dat C Time: _
Other
Relinquished by Dat :
Z.— _12
Time:
�j.�
Received by: bate: Time:
Relinquished by: Date:
Time:
Received by Lab' A j 1 `D�; I Time:
1 J `J

_ ;a'ne A nalytica(
www.paco;abs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
October 18, 2019
Amanda James
City of Rocky Mount
3031 Treatment Plant Road
Rocky Mount, NC 27801
RE: Project: Full TCLP
Pace Project No.: 92443736
Dear Amanda James:
Enclosed are the analytical results for sample(s) received by the laboratory on August 30, 2019. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring for
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Amanda James, City of Rocky Mount
REPORT OF LABORATORY ANALYSIS
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Pace Project No.: 92443736
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Missouri Certification #: 235
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South Dakota Certification
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Texas/TNI Certification #: T104704188-17-3
Utah/TNI Certification #: PA014572017-9
USDA Soil Permit #: P330-17-00091
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
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New Mexico DW Certification
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REPORT OF LABORATORY ANALYSIS
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[phone]
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Project: Full TCLP
Pace Project No.: 92443736
Pace Analytical National Certification IDs
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LABO152
USDA Soil Permit #: P330-15-00234
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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SAMPLE ANALYTE COUNT
Project: Full TCLP
Pace Project No.: 92443736
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92443736001 BF0830 EPA 8081 B
SEM
9
PASI-C
EPA 8151A
LEL
3
PAN
EPA 601OD
SH1
14
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 8270E
PKS
18
PASI-C
EPA 8260D
SAS
14
PASI-C
ASTM D2974-87
VAK
1
PASI-PA
ASTM D2974-87
KDF
1
PASI-C
EPA 1010A
SMK
1
PASI-A
EPA 160.4 / SM254OB-2011
JP1
1
PASI-A
EPA 9040C
ECH
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM 4500S2F-2011
PAS
1
PASI-PA
92443736002 BF0830 EPA 601OD
IDS
14
PASI-A
EPA 7471 B
SOO
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
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ANALYTICAL RESULTS
Project: Full TCLP
Pace Project No.: 92443736
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: BF0830 Lab ID: 92443736001 Collected: 08/30/19 08:39 Received: 08/30/19 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Chlorinated Herb. (GC) 8151A
2,4,5-TP (Silvex)
2,4-D
Surrogates
2,4-DCAA (S)
6010 MET ICP, TCLP
Aluminum
Arsenic
Barium
Cadmium
Calcium
Chromium
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Silver
Zinc
7470 Mercury, TCLP
Mercury
8270E MSSV TCLP Sep Funnel
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 09/03/19 13:59 Initial pH: ; Final pH: 5
ND
ug/L
0.50
1
09/05/1911:50
09/09/1916:06
58-89-9
ND
ug/L
3.0
1
09/05/1911:50
09/09/1916:06
57-74-9
ND
ug/L
0.50
1
09/05/1911:50
09/09/1916:06
72-20-8
ND
ug/L
0.50
1
09/05/1911:50
09/09/1916:06
76-44-8
ND
ug/L
0.50
1
09/05/1911:50
09/09/1916:06
1024-57-3
ND
ug/L
1000
1
09/05/1911:50
09/09/1916:06
72-43-5
ND
ug/L
3.0
1
09/05/1911:50
09/09/1916:06
8001-35-2
106
%
10-138
1
09/05/1911:50
09/09/1916:06
2051-24-3
70
%
10-110
1
09/05/1911:50
09/09/1916:06
877-09-8
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 09/09/19 13:50 Initial pH: 8.62; Final pH: 4.91
ND mg/L 0.00200 1 09/10/1911:02 09/10/1917:53 93-72-1
ND mg/L 0.00200 1 09/10/1911:02 09/10/1917:53 94-75-7
!.'i�ly��C��ai6'fi��>✓7fG1f�Iifi1NY��1✓7fG1f�Ii�/F.'ic�i�ff�b�:�]
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 09/06/19 20:55 Initial pH: 7.49; Final pH: 4.5
ND
mg/L
0.50
1
09/11/19 20:51
09/12/19 20:13
7429-90-5
ND
mg/L
0.050
1
09/11/19 20:51
09/12/19 20:13
7440-38-2
ND
mg/L
0.25
1
09/11/19 20:51
09/12/19 20:13
7440-39-3
ND
mg/L
0.0050
1
09/11/19 20:51
09/12/19 20:13
7440-43-9
36.4
mg/L
1.0
1
09/11/19 20:51
09/12/19 20:13
7440-70-2
ND
mg/L
0.050
1
09/11/19 20:51
09/12/19 20:13
7440-47-3
ND
mg/L
0.025
1
09/11/19 20:51
09/12/19 20:13
7439-92-1
19.9
mg/L
0.50
1
09/11/19 20:51
09/12/19 20:13
7439-95-4
ND
mg/L
0.025
1
09/11/19 20:51
09/12/19 20:13
7439-98-7
0.053
mg/L
0.050
1
09/11/19 20:51
09/12/19 20:13
7440-02-0
31.3
mg/L
25.0
1
09/11/19 20:51
09/12/19 20:13
7440-09-7
ND
mg/L
0.10
1
09/11/19 20:51
09/12/19 20:13
7782-49-2
ND
mg/L
0.025
1
09/11/19 20:51
09/12/19 20:13
7440-22-4
0.62
mg/L
0.50
1
09/11/19 20:51
09/12/19 20:13
7440-66-6
Analytical Method:
EPA 7470A
Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 09/06/19 20:55
Initial
pH: 7.49; Final
pH: 4.5
ND mg/L 0.00020 1 09/09/1912:20 09/11/1910:00 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
1,4-Dichlorobenzene
ND ug/L 500 1 09/04/19 11:03
09/04/19 20:28
106-46-7
2,4-Dinitrotoluene
ND ug/L 500 1 09/04/19 11:03
09/04/19 20:28
121-14-2
Hexachloro-1,3-butadiene
ND ug/L 500 1 09/04/19 11:03
09/04/19 20:28
87-68-3
Hexachlorobenzene
ND ug/L 500 1 09/04/19 11:03
09/04/19 20:28
118-74-1
Hexachloroethane
ND ug/L 500 1 09/04/19 11:03
09/04/19 20:28
67-72-1
REPORT OF LABORATORY ANALYSIS
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Date: 10/18/2019 11:27 AM
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ANALYTICAL RESULTS
Project: Full TCLP
Pace Project No.: 92443736
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: BF0830 Lab ID: 92443736001 Collected: 08/30/19 08:39 Received: 08/30/19 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV TCLP Sep Funnel
2-Methyl phenol(o-Cresol)
3&4-MethyIphenol (m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260D MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Percent Solids
Total Solids
1010 Flashpoint,Closed Cup
Flashpoint
160.4 TVS and 2540B TS
Total Volatile Solids
9040 pH
pH at 25 Degrees C
Date: 10/18/2019 11:27 AM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
95-48-7
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
15831-10-4
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
98-95-3
ND ug/L
1000
1
09/04/19 11:03
09/04/19 20:28
87-86-5
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
110-86-1
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
95-95-4
ND ug/L
500
1
09/04/19 11:03
09/04/19 20:28
88-06-2
38 %
12-102
1
09/04/19 11:03
09/04/19 20:28
4165-60-0
47 %
13-107
1
09/04/19 11:03
09/04/19 20:28
321-60-8
78 %
21-132
1
09/04/19 11:03
09/04/19 20:28
1718-51-0
19 %
10-110
1
09/04/19 11:03
09/04/19 20:28
13127-88-3
27 %
10-110
1
09/04/19 11:03
09/04/19 20:28
367-12-4
80 %
27-108
1
09/04/19 11:03
09/04/19 20:28
118-79-6
Analytical Method: EPA 8260D
ND ug/L
100
20
09/11/1915:46
71-43-2
362 ug/L
200
20
09/11/1915:46
78-93-3
ND ug/L
100
20
09/11/1915:46
56-23-5
ND ug/L
100
20
09/11/1915:46
108-90-7
ND ug/L
100
20
09/11/1915:46
67-66-3
ND ug/L
100
20
09/11/1915:46
106-46-7
ND ug/L
100
20
09/11/1915:46
107-06-2
ND ug/L
100
20
09/11/1915:46
75-35-4
ND ug/L
100
20
09/11/1915:46
127-18-4
ND ug/L
100
20
09/11/1915:46
79-01-6
ND ug/L
100
20
09/11/1915:46
75-01-4
106 %
70-130
20
09/11/1915:46
17060-07-0
99 %
67-135
20
09/11/1915:46
2037-26-5
101 %
70-130
20
09/11/1915:46
460-00-4
Analytical Method: ASTM D2974-87
97.0 %
0.10
1
09/15/1915:54
Analytical Method: ASTM D2974-87
2.9 %
0.10
1
09/05/1914:53
Analytical Method: EPA 1010A
>190 deg F
70.0
1
09/10/19 14:12
Analytical Method: EPA 160.4 / SM2540B-2011
19500 mg/L
500
1
09/04/19 01:12
Analytical Method: EPA 9040C
7.3 Std. Units
0.10
1
09/15/19 15:40
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
Sample: BF0830 Lab ID: 92443736001 Collected: 08/30/19 08:39 Received: 08/30/19 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 33.4 1 09/05/19 20:14 09/05/19 20:44
734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 334 1 09/05/19 20:14 09/05/19 20:18
Sample: BF0830 Lab ID: 92443736002 Collected: 08/30/19 08:39 Received: 08/30/19 14:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Aluminum
14500
mg/kg
260
1
09/29/19 13:04
09/30/19 02:39
7429-90-5 M1
Arsenic
ND
mg/kg
26.0
1
09/29/19 13:04
09/30/19 02:39
7440-38-2
Cadmium
ND
mg/kg
2.6
1
09/29/19 13:04
09/30/19 02:39
7440-43-9
Calcium
12300
mg/kg
260
1
09/29/19 13:04
09/30/19 02:39
7440-70-2
Copper
619
mg/kg
13.0
1
09/29/19 13:04
09/30/19 02:39
7440-50-8
Lead
51.6
mg/kg
13.0
1
09/29/19 13:04
09/30/19 02:39
7439-92-1
Magnesium
4820
mg/kg
260
1
09/29/19 13:04
09/30/19 02:39
7439-95-4
Molybdenum
13.2
mg/kg
13.0
1
09/29/19 13:04
09/30/19 02:39
7439-98-7
Nickel
51.8
mg/kg
13.0
1
09/29/19 13:04
09/30/19 02:39
7440-02-0
Potassium
ND
mg/kg
13000
1
09/29/19 13:04
09/30/19 02:39
7440-09-7
Selenium
ND
mg/kg
26.0
1
09/29/19 13:04
09/30/19 02:39
7782-49-2
Silver
ND
mg/kg
13.0
1
09/29/19 13:04
09/30/19 02:39
7440-22-4
Sodium
ND
mg/kg
13000
1
09/29/19 13:04
09/30/19 02:39
7440-23-5
Zinc
623
mg/kg
26.0
1
09/29/19 13:04
09/30/19 02:39
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
B Preparation Method:
EPA 7471 B
Mercury
0.78
mg/kg
0.15
1
09/30/1917:13
09/30/1920:47
7439-97-6 H1,H2
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
97.1
%
0.10
1
09/05/19 14:54
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 1342665
Analysis Method: EPA 8151A
QC Batch Method: 8151A
Analysis Description: Chlorinated
Herb. (GC) 8151A
Associated Lab Samples: 92443736001
METHOD BLANK: R3449408-1
Matrix: Solid
Associated Lab Samples: 92443736001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4-D
mg/L
ND 0.00200
09/10/19 16:42
2,4,5-TP (Silvex)
mg/L
ND 0.00200
09/10/19 16:42
2,4-DCAA (S)
%
67.4 14.0-158
09/10/19 16:42
LABORATORY CONTROL SAMPLE: R3449408-2
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
2,4-D
mg/L
0.0500 0.0408
81.6 50.0-120
2,4,5-TP (Silvex)
mg/L
0.0500 0.0464
92.8 50.0-125
2,4-DCAA (S)
%
72.4 14.0-158
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: R3449408-3 R3449408-4
MS MSD
92443736001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units
Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qual
2,4-D mg/L
ND
0.0500 0.0500 0.0398
0.0399 79.6 79.8 50.0-120 0.251
2,4,5-TP (Silvex) mg/L
ND
0.0500 0.0500 0.0448
0.0456 89.6 91.2 50.0-125 1.77
2,4-DCAA (S) %
62.4 64.0 14.0-158
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 496621
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92443736001
METHOD BLANK: 2673843
Matrix: Water
Associated Lab Samples: 92443736001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
09/11/19 09:41
METHOD BLANK: 2673844
Matrix: Water
Associated Lab Samples: 92443736001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
09/11/19 09:46
LABORATORY CONTROL SAMPLE: 2674617
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0022
88 80-120
LABORATORY CONTROL SAMPLE: 2674618
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0024
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2674619 2674620
MS MSD
92443678001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units
Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/L
ND
0.0025 0.0025 0.0030
0.0027 120 108 75-125 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 500736
Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92443736002
METHOD BLANK: 2693879
Matrix: Solid
Associated Lab Samples: 92443736002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060
09/30/19 20:42
LABORATORY CONTROL SAMPLE: 2693880
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.083 0.098
118 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2693881 2693882
MS MSD
92443736002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.78
1.9 2 2.2
2.5 77 85 75-125 11 H1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/18/2019 11:27 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 500558 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92443736002
METHOD BLANK: 2693073
Associated Lab Samples: 92443736002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
09/30/19 02:33
Arsenic
mg/kg
ND
1.0
09/30/19 02:33
Cadmium
mg/kg
ND
0.10
09/30/19 02:33
Calcium
mg/kg
ND
10.0
09/30/19 02:33
Copper
mg/kg
ND
0.50
09/30/19 02:33
Lead
mg/kg
ND
0.50
09/30/19 02:33
Magnesium
mg/kg
ND
10.0
09/30/19 02:33
Molybdenum
mg/kg
ND
0.50
09/30/19 02:33
Nickel
mg/kg
ND
0.50
09/30/19 02:33
Potassium
mg/kg
ND
500
09/30/19 02:33
Selenium
mg/kg
ND
1.0
09/30/19 02:33
Silver
mg/kg
ND
0.50
09/30/19 02:33
Sodium
mg/kg
ND
500
09/30/19 02:33
Zinc
mg/kg
ND
1.0
09/30/19 02:33
LABORATORY CONTROL SAMPLE:
2693074
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Qualifiers
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
500
474
95
80-120
50
43.0
86
80-120
50
44.8
90
80-120
500
478
96
80-120
50
47.1
94
80-120
50
45.2
90
80-120
500
455
91
80-120
50
44.8
90
80-120
50
46.0
92
80-120
500
ND
96
80-120
50
41.2
82
80-120
25
22.6
91
80-120
500
480J
96
80-120
50
43.7
87
80-120
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2693075 2693076
MS MSD
92443736002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Aluminum mg/kg 14500 12400 12400 34700 30400 163 128 75-125 13 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/18/2019 11:27 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2693075
2693076
MS
MSD
92443736002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
1240
1240
1100
1090
89
88
75-125
1
Cadmium
mg/kg
ND
1240
1240
1130
1110
91
89
75-125
2
Calcium
mg/kg
12300
12400
12400
26500
23600
114
90
75-125
12
Copper
mg/kg
619
1240
1240
1930
1740
105
90
75-125
10
Lead
mg/kg
51.6
1240
1240
1190
1160
91
89
75-125
2
Magnesium
mg/kg
4820
12400
12400
16900
16200
97
91
75-125
4
Molybdenum
mg/kg
13.2
1240
1240
1140
1120
91
89
75-125
2
Nickel
mg/kg
51.8
1240
1240
1220
1190
94
92
75-125
2
Potassium
mg/kg
ND
12400
12400
19900
19100
100
94
75-125
4
Selenium
mg/kg
ND
1240
1240
1020
1000
82
80
75-125
2
Silver
mg/kg
ND
621
621
573
561
92
90
75-125
2
Sodium
mg/kg
ND
12400
12400
15700
15400
98
96
75-125
2
Zinc
mg/kg
623
1240
1240
1790
1630
94
81
75-125
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 497361 Analysis Method: EPA6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92443736001
METHOD BLANK: 2676110
Associated Lab Samples: 92443736001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Aluminum
mg/L
ND
0.50
09/12/1919:37
Arsenic
mg/L
ND
0.050
09/12/1919:37
Barium
mg/L
ND
0.25
09/12/1919:37
Cadmium
mg/L
ND
0.0050
09/12/1919:37
Calcium
mg/L
ND
1.0
09/12/1919:37
Chromium
mg/L
ND
0.050
09/12/1919:37
Lead
mg/L
ND
0.025
09/12/1919:37
Magnesium
mg/L
ND
0.50
09/12/1919:37
Molybdenum
mg/L
ND
0.025
09/12/1919:37
Nickel
mg/L
ND
0.050
09/12/1919:37
Potassium
mg/L
ND
25.0
09/12/1919:37
Selenium
mg/L
ND
0.10
09/12/1919:37
Silver
mg/L
ND
0.025
09/12/1919:37
Zinc
mg/L
ND
0.50
09/12/1919:37
METHOD BLANK: 2676111
Associated Lab Samples: 92443736001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Aluminum
mg/L
ND
0.50
09/12/1919:46
Arsenic
mg/L
ND
0.050
09/12/1919:46
Barium
mg/L
ND
0.25
09/12/1919:46
Cadmium
mg/L
ND
0.0050
09/12/1919:46
Calcium
mg/L
ND
1.0
09/12/1919:46
Chromium
mg/L
ND
0.050
09/12/1919:46
Lead
mg/L
ND
0.025
09/12/1919:46
Magnesium
mg/L
ND
0.50
09/12/1919:46
Molybdenum
mg/L
ND
0.025
09/12/1919:46
Nickel
mg/L
ND
0.050
09/12/1919:46
Potassium
mg/L
ND
25.0
09/12/1919:46
Selenium
mg/L
ND
0.10
09/12/1919:46
Silver
mg/L
ND
0.025
09/12/1919:46
Zinc
mg/L
ND
0.50
09/12/1919:46
LABORATORY CONTROL SAMPLE: 2678221
Qualifiers
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Aluminum mg/L 25 25.2 101 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/18/2019 11:27 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2678221
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.4
98
80-120
Barium
mg/L
2.5
2.5
101
80-120
Cadmium
mg/L
2.5
2.4
98
80-120
Calcium
mg/L
25
25.1
100
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.4
98
80-120
Magnesium
mg/L
25
25.5
102
80-120
Molybdenum
mg/L
2.5
2.3
94
80-120
Nickel
mg/L
2.5
2.4
98
80-120
Potassium
mg/L
25
29.9
120
80-120
Selenium
mg/L
2.5
2.6
104
80-120
Silver
mg/L
1.2
1.3
101
80-120
Zinc
mg/L
2.5
2.5
101
80-120
LABORATORY CONTROL SAMPLE:
Parameter
2678222
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/L
25
25.1
101
80-120
Arsenic
mg/L
2.5
2.4
98
80-120
Barium
mg/L
2.5
2.5
101
80-120
Cadmium
mg/L
2.5
2.4
98
80-120
Calcium
mg/L
25
25.0
100
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.4
97
80-120
Magnesium
mg/L
25
25.4
102
80-120
Molybdenum
mg/L
2.5
2.3
94
80-120
Nickel
mg/L
2.5
2.4
97
80-120
Potassium
mg/L
25
30.0
120
80-120
Selenium
mg/L
2.5
2.6
104
80-120
Silver
mg/L
1.2
1.3
101
80-120
Zinc
mg/L
2.5
2.5
101
80-120
LABORATORY CONTROL SAMPLE:
Parameter
2678223
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/L
25
24.1
96
80-120
Arsenic
mg/L
2.5
2.4
95
80-120
Barium
mg/L
2.5
2.5
101
80-120
Cadmium
mg/L
2.5
2.4
98
80-120
Calcium
mg/L
25
24.7
99
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.4
97
80-120
Magnesium
mg/L
25
24.2
97
80-120
Molybdenum
mg/L
2.5
2.3
93
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
LABORATORY CONTROL SAMPLE:
2678223
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Nickel
mg/L
2.5
2.4
98
80-120
Potassium
mg/L
25
24J
96
80-120
Selenium
mg/L
2.5
2.5
102
80-120
Silver
mg/L
1.2
1.2
98
80-120
Zinc
mg/L
2.5
2.5
100
80-120
LABORATORY CONTROL SAMPLE:
2678224
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Aluminum
mg/L
25
24.7
99
80-120
Arsenic
mg/L
2.5
2.4
98
80-120
Barium
mg/L
2.5
2.6
102
80-120
Cadmium
mg/L
2.5
2.5
100
80-120
Calcium
mg/L
25
25.3
101
80-120
Chromium
mg/L
2.5
2.5
101
80-120
Lead
mg/L
2.5
2.5
100
80-120
Magnesium
mg/L
25
24.7
99
80-120
Molybdenum
mg/L
2.5
2.4
95
80-120
Nickel
mg/L
2.5
2.5
99
80-120
Potassium
mg/L
25
24AJ
98
80-120
Selenium
mg/L
2.5
2.6
104
80-120
Silver
mg/L
1.2
1.3
100
80-120
Zinc
mg/L
2.5
2.5
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2678225
2678226
MS
MSD
92440275003
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Aluminum
mg/L
0.74
25
25
26.0
25.5
101
99
75-125
2
Arsenic
mg/L
ND
2.5
2.5
2.5
2.4
98
96
75-125
2
Barium
mg/L
2.3
2.5
2.5
4.9
4.8
102
97
75-125
2
Cadmium
mg/L
0.0068
2.5
2.5
2.4
2.4
97
95
75-125
2
Calcium
mg/L
60.0
25
25
88.4
86.5
113
106
75-125
2
Chromium
mg/L
0.89
2.5
2.5
3.4
3.3
101
98
75-125
2
Lead
mg/L
2.0
2.5
2.5
4.5
4.4
101
97
75-125
2
Magnesium
mg/L
1.4
25
25
26.9
26.4
102
100
75-125
2
Molybdenum
mg/L
ND
2.5
2.5
2.3
2.3
94
92
75-125
2
Nickel
mg/L
ND
2.5
2.5
2.4
2.4
97
94
75-125
2
Potassium
mg/L
ND
25
25
31.4
30.9
118
116
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.6
2.5
104
101
75-125
2
Silver
mg/L
ND
1.2
1.2
1.3
1.2
101
99
75-125
2
Zinc
mg/L
15.2
2.5
2.5
18.1
17.8
118
105
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 497203 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV TCLP
Associated Lab Samples: 92443736001
METHOD BLANK: 2677161
Associated Lab Samples: 92443736001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1-Dichloroethene
ug/L
ND
5.0
09/11/19 13:59
1,2-Dichloroethane
ug/L
ND
5.0
09/11/19 13:59
1,4-Dichlorobenzene
ug/L
ND
5.0
09/11/19 13:59
2-Butanone (MEK)
ug/L
ND
10.0
09/11/19 13:59
Benzene
ug/L
ND
5.0
09/11/19 13:59
Carbon tetrachloride
ug/L
ND
5.0
09/11/19 13:59
Chlorobenzene
ug/L
25.8
5.0
09/11/19 13:59
Chloroform
ug/L
ND
5.0
09/11/19 13:59
Tetrachloroethene
ug/L
ND
5.0
09/11/19 13:59
Trichloroethene
ug/L
ND
5.0
09/11/19 13:59
Vinyl chloride
ug/L
ND
5.0
09/11/19 13:59
1,2-Dichloroethane-d4 (S)
%
111
70-130
09/11/19 13:59
4-Bromofluorobenzene (S)
%
104
70-130
09/11/19 13:59
Toluene-d8 (S)
%
99
67-135
09/11/19 13:59
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2677160
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1-Dichloroethene
ug/L
50
54.5
109
70-130
1,2-Dichloroethane
ug/L
50
48.4
97
70-130
1,4-Dichlorobenzene
ug/L
50
45.9
92
70-130
2-Butanone (MEK)
ug/L
100
99.9
100
64-135
Benzene
ug/L
50
49.5
99
70-130
Carbon tetrachloride
ug/L
50
50.8
102
70-130
Chlorobenzene
ug/L
50
47.6
95
70-130
Chloroform
ug/L
50
50.8
102
70-130
Tetrachloroethene
ug/L
50
47.7
95
69-130
Trichloroethene
ug/L
50
46.1
92
70-130
Vinyl chloride
ug/L
50
54.6
109
70-131
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
99
67-135
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2677162 2677163
MS MSD
92443623006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
1,1-Dichloroethene ug/L ND 400 400 490 507 123 127 70-154 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/18/2019 11:27 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2677162
2677163
MS
MSD
92443623006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,2-Dichloroethane
ug/L
ND
400
400
415
412
104
103
70-137
1
1,4-Dichlorobenzene
ug/L
ND
400
400
387
375
97
94
70-133
3
2-Butanone (MEK)
ug/L
ND
800
800
815
821
89
90
60-139
1
Benzene
ug/L
ND
400
400
453
442
113
110
70-151
2
Carbon tetrachloride
ug/L
ND
400
400
455
457
114
114
70-143
0
Chlorobenzene
ug/L
ND
400
400
434
429
109
107
70-138
1
Chloroform
ug/L
ND
400
400
413
430
103
108
70-139
4
Tetrachloroethene
ug/L
ND
400
400
411
418
103
104
59-143
2
Trichloroethene
ug/L
ND
400
400
422
415
105
104
70-147
1
Vinyl chloride
ug/L
ND
400
400
485
483
121
121
70-156
0
1,2-Dichloroethane-d4 (S)
%
96
100
70-130
4-Bromofluorobenzene (S)
%
101
100
70-130
Toluene-d8(S)
%
99
99
67-135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 496097 Analysis Method: EPA 8081 B
QC Batch Method: EPA 3510C Analysis Description: 8081 TCLP Pesticides RV
Associated Lab Samples: 92443736001
METHOD BLANK: 2670517
Associated Lab Samples: 92443736001
Parameter
Chlordane (Technical)
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed
ug/L
ND
3.0
09/09/1916:50
ug/L
ND
0.50
09/09/1916:50
ug/L
ND
0.50
09/09/1916:50
ug/L
ND
0.50
09/09/1916:50
ug/L
ND
0.50
09/09/1916:50
ug/L
ND
1000
09/09/1916:50
ug/L
ND
3.0
09/09/1916:50
%
116
10-138
09/09/1916:50
%
10
10-110
09/09/1916:50
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
2672170
2672171
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Endrin
ug/L
1.2
1.3
1.1
103
90
20-134
13
30
gamma-BHC (Lindane)
ug/L
1.2
1.3
1.1
103
87
20-118
17
30
Heptachlor
ug/L
1.2
1.1
0.93
86
75
20-142
14
30
Heptachlor epoxide
ug/L
1.2
1.2
1.0
92
81
22-133
14
30
Methoxychlor
ug/L
3.8
4.5J
4.2J
119
111
44-150
30
Decachlorobiphenyl (S)
%
151
111
10-138
SO
Tetrachloro-m-xylene (S)
%
96
72
10-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 495848 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E TCLP MSSV
Associated Lab Samples: 92443736001
METHOD BLANK: 2670517
Associated Lab Samples: 92443736001
Parameter Units
1,4-Dichlorobenzene
ug/L
2,4,5-Trichlorophenol
ug/L
2,4,6-Trichlorophenol
ug/L
2,4-Dinitrotoluene
ug/L
2-Methyl phenol(o-Cresol)
ug/L
3&4-Methylphenol (m&p Cresol)
ug/L
Hexachloro-1,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachloroethane
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Pyridine
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
50.0
09/04/1913:58
ND
100
09/04/1913:58
ND
50.0
09/04/1913:58
69
27-108
09/04/1913:58
50
13-107
09/04/1913:58
34
10-110
09/04/1913:58
54
12-102
09/04/1913:58
21
10-110
09/04/1913:58
71
21-132
09/04/1913:58
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2671054
Units
Spike
Conc.
2671055
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,4-Dichlorobenzene
ug/L
500
199
187
40
37
10-110
6
30
2,4,5-Trichlorophenol
ug/L
500
287
286
57
57
39-108
0
30
2,4,6-Trichlorophenol
ug/L
500
302
301
60
60
40-104
0
30
2,4-Dinitrotoluene
ug/L
500
302
302
60
60
42-109
0
30
2-Methyl phenol(o-Cresol)
ug/L
500
247
253
49
51
31-110
2
30
3&4-MethyIphenol (m&p Cresol)
ug/L
500
225
228
45
46
30-110
2
30
Hexachloro-1,3-butadiene
ug/L
500
150
136
30
27
10-110
10
30
Hexachlorobenzene
ug/L
500
306
302
61
60
39-121
1
30
Hexachloroethane
ug/L
500
183
164
37
33
10-110
11
30
Nitrobenzene
ug/L
500
270
280
54
56
32-101
4
30
Pentachlorophenol
ug/L
1000
667
664
67
66
18-108
0
30
Pyridine
ug/L
500
158
145
32
29
10-110
8
30
2,4,6-Tribromophenol (S)
%
68
68
27-108
2-Fluorobiphenyl (S)
%
56
55
13-107
2-Fluorophenol(S)
%
36
34
10-110
Nitrobenzene-d5 (S)
%
59
55
12-102
Phenol-d6 (S)
%
22
22
10-110
Terphenyl-d14 (S)
%
69
66
21-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 361374 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92443736001
SAMPLE DUPLICATE: 1754213
92443736001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 97.0 97.0 0
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 496216 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Percent Solids
Associated Lab Samples: 92443736001
SAMPLE DUPLICATE: 2672737
92443736001 Dup
Parameter Units Result Result
Total Solids % 2.9 2.9
RPD Qualifiers
1
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 496909 Analysis Method: EPA 1010A
QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92443736001
SAMPLE DUPLICATE: 2675733
92442885001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 495828 Analysis Method: EPA 160.4 / SM2540B-2011
QC Batch Method: EPA 160.4 / SM2540B-2011 Analysis Description: 160.4 TVS and 2540B TS
Associated Lab Samples: 92443736001
SAMPLE DUPLICATE: 2671024
92443544001 Dup
Parameter Units Result Result
Total Volatile Solids mg/L 52000 47600
RPD Qualifiers
9
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 497903 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92443736001
SAMPLE DUPLICATE: 2680923
Parameter
pH at 25 Degrees C
92443843001 Dup
Units Result Result RPD Qualifiers
Std. Units 0.36 0.35 3 E,H3
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 360082
Analysis Method:
EPA 9014
QC Batch Method: SW-846 7.3.3.2
Analysis Description:
733C Reactive Cyanide
Associated Lab Samples: 92443736001
METHOD BLANK: 1747856
Matrix: Solid
Associated Lab Samples: 92443736001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cyanide, Reactive
mg/kg
ND
0.99 09/05/19 20:35
LABORATORY CONTROL SAMPLE: 1747857
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Cyanide, Reactive
mg/kg
99.3 ND
0 0-8
SAMPLE DUPLICATE: 1747858
30323041005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Cyanide, Reactive
mg/kg
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Full TCLP
Pace Project No.: 92443736
QC Batch: 360081
Analysis Method:
SM 4500S2F-2011
QC Batch Method: SW-846 7.3.4.2
Analysis Description:
734S Reactive Sulfide
Associated Lab Samples: 92443736001
METHOD BLANK: 1747852
Matrix: Solid
Associated Lab Samples: 92443736001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfide, Reactive
mg/kg
ND
9.9 09/05/19 20:18
LABORATORY CONTROL SAMPLE: 1747853
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Sulfide, Reactive
mg/kg
199 39.8
20 0-52
SAMPLE DUPLICATE: 1747854
30323041005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Sulfide, Reactive
mg/kg
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: Full TCLP
Pace Project No.: 92443736
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Wet-ii]:fAIce] NI*:
PAN
Pace Analytical National
PASI-A
Pace Analytical Services - Asheville
PASI-C
Pace Analytical Services - Charlotte
PASI-PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
1g Sample boiled over before 200 degrees
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H1 Analysis conducted outside the EPA method holding time.
H2 Extraction or preparation conducted outside EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Pace Project No.:
Full TCLP
92443736
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92443736001
BF0830
EPA 3510C
496097
EPA 8081B
496410
92443736001
BF0830
8151A
1342665
EPA 8151A
1342665
92443736002
BF0830
EPA 3050B
500558
EPA 6010D
500605
92443736001
BF0830
EPA 3010A
497361
EPA 6010D
497366
92443736001
BF0830
EPA 7470A
496621
EPA 7470A
496747
92443736002
BF0830
EPA 7471B
500736
EPA 7471B
500801
92443736001
BF0830
EPA 3510C
495848
EPA 8270E
495997
92443736001
BF0830
EPA 8260D
497203
92443736001
BF0830
ASTM D2974-87
361374
92443736002
BF0830
ASTM D2974-87
500420
92443736001
BF0830
ASTM D2974-87
496216
92443736001
BF0830
EPA1010A
496909
92443736001
BF0830
EPA 160.4/S M254013-
495828
2011
92443736001
BF0830
EPA 9040C
497903
92443736001
BF0830
SW-846 7.3.3.2
360082
EPA 9014
360102
92443736001
BF0830
SW-846 7.3.4.2
360081
SM 4500S2F-2011
360103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 10/18/2019 11:27 AM
without the written consent of Pace Analytical
Services, LLC.
Page 28 of 31

Document lyame: Document Revised: February 7, 2019
sample Condition Ulan Race{ SCUP Pa e 2 of 2
Document No.: [ssuing Authority:
Pace Grofinac Quality Office
Laboratory receiving samples:
Asheville Q Eden❑ Greenwood ❑ Huntersville ❑ Aa(elgh[ll"' MechankwMe❑ �
Client Name:
WO# : 92443736
project h
,oLdermercral QF d []UPS U5P5 o�Bent
1111111111111111111111111111
o 'er--
92443735
Custody Seal Present? []Yes No Seals fntact? []Yes []No
L101 l E
ersc urq en
PacWng N14terlal: []Bubble Wrap - []Hubble Reaps None ❑ Other
Bfoloecal Tissue F Zen?
Thermometer:
0 � Type of Ire Vlet []Blue
Oyes ❑NI) N/A
(]None
Gun ;
Cooler Temp ('C�: - q
Correctfon Factor. Add/5ubtracC('CJ -�' `!
�
Cooler Temp Corrected ('L}: �
Temp should be shore freeing to 6'C
[]Samples cut of temp criteria. _ampler as b, wotfng process
USDA ffegulated 5off ( N/A, watecsarapte)
has begun
Old samples ortglnate in a quarantine zone tiKrthfn the UrUd States: CA, NY, or SC (check maps)?
[]Yes No
old mmp4es odenam from a fMrefgn seurca ({ntematbna9y,
includ4Haaalt and PMW Rica)? []Yes QNa
CommentsjMcr ancy:
Chain ofCushrdy Present?
E�Y'as
QNo
❑N/A
L
Samples AnrtvedwithinHold Ttme?
FfYg .
11.
NIA
z,
Sham Hold Time Analysis ([72 hr,)?
[]Yes
2K.
[jN/A
3.
Rush Tum Around Time Requested?
r1Y,
a
©N/A
4.
5uffldentVo4ume?
es
No
ON/A
5.
Correct Containers Used?
Was
[]Na
❑N/A
6.
-Pace Containers Used?
es
ON.
NIA
Conaalmrs Intact?
es
OMo
EINIA
7.
Oisscived analysis: Samples Feld Filtered?
FlYes
UN.
LKIA
S. i
Sample Labers NI.Itch CDC?
ej&
[]Mo
ON/A
9,
-Includes0atejr1me/iD/Analysis iMaU-bL
iieadspace n VDA vats (>5-6mm)7 OYes QNa /A 10. j
Trip Blank Present? ©Yes ©Me (A IS.
Trip Blank Custody Seals Present? Yes No /A �
COMMENT515AMPtE 015C.REPANCY Field oata ftaquired? []Yes QNo
Lot ID of spliteentainers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date time:
Project Martager SCURF Review: IVI
Oats:
Page 29 of 31

pocumerrt No.:
*Check marls top half of box if pH and[or dechlorination is
verNied and within the acceptance range for preservation
samptes.
Exrepva= VOA, c0form, TOC, Oil and Grnasse, OR0(8O15 (water) DCr [iHR
**Bottam half of box is to list number of bottle
Document Ravlsed: February 7, 2MS
�t(#CEJA] e 1 of 2
issafngAuthorlty:
Pace Carnifnas Quatiy OfRce
Pr*cts. WQ# : 92443736
PM: TIH Due Date: 09/16/19
CLIENT: 91—Rocky Mt
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adjusted added
Vnta. snrhnn aver ifiero f, a.finrrnr.q nnr aria.-rinn trnnM r-.rnitn��nm nli.rvu ;amnfae . rnn� n(rhi� lnrm will �B lCPC fa:he iVofth GrOM. DEH R Certlnratlan office i1.e. #
Page 30 of 31

�P3G1 AnalyGc31
Section A
Required Client Information:
Company, Cily of Rocky Mount 1AMrT
Address3130 Treatment Plant Roa,
Rocky Mount, NC 27802
Emari
" rm*�rint!Cilrockymcunlnc.pov
Phone- Far
Requested Due Dale:
SAMPLE ID
One Character per box.
(A-2, o-9 1, .)
Sample Ids must be unique
In
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1 F0$3 U
2
3
4
5
L97
11
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -Of -Custody is a LEGAL DOCUMENT. All relevant fiel is must be completed accurately.
Section B
Required Project Information: Section C
Invoice Information:
Report To: more r74A
Copy To, L e- Auentiorr Pa e
Company Name.
Purchase Order#, Address
aroled Name, Pace Quote: Re ulata A enc
FuB TCLP Pace Pro ect M
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NC
ADDITIONAL COMMENTS RELINgUIS,RED By 1 AFFILIATION
GATE TIME ACC BYfAFPILU17M
V68blj�
TIME SAMPLE CONU710N5
3 i S
i�G . y N
SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER
-U l r� o
SIGNATURE of SAMPLER; c
fv -
� m
m DATE Sign d: � `Zu i_ m o z E z
H
O_
W

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
\VQ Permit No. WQ0(A1556A Facility Name Gq of Rocky Mount Source. Pectim N. NOX172133 Sn— Name Sunset Ave WIT
labomton
Labommry
Sampk or CompostmDat.
Parameter (mg/Kg) Cl.. A Class 0
Aluminum
N/A
N/A
Ammonia Nitrogen
N/A
N/A
Arsenic
41
75
Cadmium
39
95.
Caldron
N/A
N/A
Copper.
1,500
4,300
Lead,
300
840
Magnesium
N/A
N/A
Mercury
17
57
75
Nimus-Nmim Nitrogen
N/A
N/A
Pemem Solids.
N/A
N/A
pH (no units)
N/A
N/A
phosphorus
N/A
N/A
Potassium
N/A
N/A
PAN (inj./ttic)
N/A
N/A
PAN (Surfice)
N/A
N/A
Seknium
too
100
Sodium
N/A
NIA
SAR
TKN
N/A
N/A
Zinc 2;800 7$00
i 6p of Rocln'
Mcwel
a.Rockf
Mnant
Gry ofAocky
Mcwnt
(atynFRncky
Moan,
1 Pacx..Anilnad
•, 3J 12j 31117
ikce .4nvlme
Pace Aea1-
A/7I/bf9
Pare A.4 ca
Af'1:=K'l19
itfZb/]1J19
6,6Go
67,1W1
M1?Irl
3�.55
4.7
i 5
I15
21
"_i
2A3
1,75n
130,
I.Wo
1.125
25
I3.6
tail
921
14.7
10.5
5
7.6
361.W
3,1M.11l.tltl
375.INI
11 a.I.X1
11.19
1144
1111
0.115
4.9
44:3
10.5.
5
1ai
%1.50
M
015
A
913.95:
'IMCKI
5 51I
0.43
370
231
6.7I
6.50
6G+
520
896A
J930.11n
23,753.tk1
62.91111a1
1,3nS.1A1
Iri,irx.,ixi
7A?1Y,1
350J10
'99
435
1,1126
1,97n
11152
579
IM_
52
91
l9Alul
65f,
629
21
5
Ij5f (li
1.M
31.5f AX)
4.13
10.5(AI.M
11.67
193
1G1i
21
21.
"1 certify, under peualn- of law, that this document was prepared under my direction or supervision in accordance with a system designed m
assure that qualified personnel pmperly gathered and evaluated the information submitted. 1 am aware that titre are significant penalties for
submitting false information, including the possibility uffines and imprisonment for knowing viobdous.^
S' of Preparers Date
*Preparer is defined in 40 CFR art 5039(r) and 15A NCAC ZT .1102 (26)

&,,AGMAN FIELD LOADING ESTIMATES
Facility Sunset Ave W'IP
Sampling Date 3/12/2019
Solids 5.5
Mineralization Rate 0
Gallons per DT 4,360.15
pH 6.76
Sodium Absorpotion 6.56 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 5,273 lbs./1,000 gal 2.42
Ammonia Nitrogen (mg/Kg) 727.00 lbs./1,000 gal 0.33
Nitrate -Nitrite (mg/Kg) 71.50 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 435 lbs./1,000 gal 0.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 799 lbs./1,000 gal 0.37
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.26
Phosphorus lbs./1,000 gal 0.41
Calcium lbs./1,000 gal 0.80
Magnesium lbs./1,000 gal 0.17
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
9.90
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
4.70
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
25.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
13.60
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.19
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
18.30
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
9.90
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
19.30
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
51273
435 0.87
4,838
5,273
799 1.60
4,475
4,838
0 0.00
4,838
4,475
0 0.00
4,475
4,838
0 0.00
4,838
4,475
0 0.00
4,475
4,838
0 0.00
4,838
4,475
0 0.00
4,475
4,838
0 0.00
4,838
4,475
0 0.00
4,475
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 435 0.87
Total 799 1.60

&,,AGMAN FIELD LOADING ESTIMATES
Facility Sunset Ave W'IP
Sampling Date 4/9/2019
Solids 0.43
Mineralization Rate 0
Gallons per DT 55,769.34
pH 6.5
Sodium Absorpotion 4.15 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 36,977 lbs./1,000 gal 1.33
Ammonia Nitrogen (mg/Kg) 2,112.00 lbs./1,000 gal 0.08
Nitrate -Nitrite (mg/Kg) 913.95 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 1,970 lbs./1,000 gal 0.07
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 3,026 lbs./1,000 gal 0.11
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.26
Phosphorus lbs./1,000 gal 0.86
Calcium lbs./1,000 gal 0.49
Magnesium lbs./1,000 gal 0.11
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
62.90
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
28.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
160.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
92.10
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.44
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
122.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
62.90
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
160.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
36,977
1,970 3.94
35,007
36,977
3,026 6.05
33,951
35,007
0 0.00
35,007
33,951
0 0.00
33,951
35,007
0 0.00
35,007
33,951
0 0.00
33,951
35,007
0 0.00
35,007
33,951
0 0.00
33,951
35,007
0 0.00
35,007
33,951
0 0.00
33,951
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 1,970 3.94
Total 3,026 6.05

&,,AGMAN FIELD LOADING ESTIMATES
Facility Sunset Ave W'IP
Sampling Date 8/14/2019
Solids 3.7
Mineralization Rate 0
Gallons per DT 6,481.30
pH 6.64
Sodium Absorpotion 11.67 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 5,784 lbs./1,000 gal 1.78
Ammonia Nitrogen (mg/Kg) 946.00 lbs./1,000 gal 0.29
Nitrate -Nitrite (mg/Kg) 106.00 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 579 lbs./1,000 gal 0.18
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 1,052 lbs./1,000 gal 0.32
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.24
Phosphorus lbs./1,000 gal 0.40
Calcium lbs./1,000 gal 0.51
Magnesium lbs./1,000 gal 0.12
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
21.00
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.10
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
14.70
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
10.50
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.11
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.50
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
21.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
21.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
51784
579 1.16
5,205
5,784
1,052 2.10
4,732
5,205
0 0.00
5,205
4,732
0 0.00
4,732
5,205
0 0.00
5,205
4,732
0 0.00
4,732
5,205
0 0.00
5,205
4,732
0 0.00
4,732
5,205
0 0.00
5,205
4,732
0 0.00
4,732
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 579 1.16
Total 1,052 2.10

&,,AGMAN FIELD LOADING ESTIMATES
Facility Sunset Ave W'IP
Sampling Date 11/26/2019
Solids 2.31
Mineralization Rate 0
Gallons per DT 10,381.31
pH 5.2
Sodium Absorpotion 1.23 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 4,762 lbs./1,000 gal 0.92
Ammonia Nitrogen (mg/Kg) 100.00 lbs./1,000 gal 0.02
Nitrate -Nitrite (mg/Kg) 2.25 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 52 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 102 lbs./1,000 gal 0.02
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.05
Phosphorus lbs./1,000 gal 0.15
Calcium lbs./1,000 gal 0.22
Magnesium lbs./1,000 gal 0.08
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
7.60
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.05
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
8.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
26.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
41762
52 0.10
4,710
4,762
102 0.20
4,660
4,710
0 0.00
4,710
4,660
0 0.00
4,660
4,710
0 0.00
4,710
4,660
0 0.00
4,660
4,710
0 0.00
4,710
4,660
0 0.00
4,660
4,710
0 0.00
4,710
4,660
0 0.00
4,660
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 52 0.10
Total 102 0.20

2019 City of Rocky Mount Analytical Report
WQ Permit Number: WQ0005568
Sample Identification: City of Rocky Mount _
Residual Source WQ # or NPDES #:
Residual Anah sis Data
NC 0072133
Facility Name: Sunset Avenue Water Treatment Plant
Laboratories_ 1) City of Rocky Mount
performing 2) Pace Analytical
analyses: 3) Environmentl
Parameter m kc)
Ceiling Cone.
Limit
(m 1 )
Sample or Composite
Date
3/12/19
4/9/19
8/14/19
11/26/19
Percent Solids s (1)
NA
5.50%
0.43%
3.70%
2.31%
pH (1)
6.76
6.50
6.64
5.20
Arsenic (2)
75
9.90
62.90
21.00
2.500
Cadmium (2)
85
4.700
28.300
2.100
0.500
Copper (2)
4,300
'5.00
160.0
14.70
5.00
Lead (2)
840
13.60
92.10
10.5
7.60
Mercury (2)
57
0.190
0.440
0.110
0.050
Molybdenum (2)
75
4.900
44.300
10.50
5.000
Nickel (2)
420
18.3
122.0
10.5
8.00
Selenium (2)
100
9.90
62.90
21.00
5.000
Zinc (2)
7,5U0
19.3
160.0
21.0
26.0
Total Phosphorus (1)
NA
896
23953
1308
762
TKN (1)
NA
5273
36977
5784
4762
Ammonia -Nitrogen (1)
NA
727
2112
946
100
Nitrate and Nitrite (1)
NA
71.5
913.95
106.0
2.25
Potassium (2}
NA
4930
62900
10500
250
Sodium (2)
NA
4930
31500
10500
1250
Magnesium (2)
NA
361
3090
375
414
Calcium (2)
NA
1750
13600
1640
1125
Silver (2)
NA
4.900
31.500
10.50
2.500
Aluminum (2)
NA
6660
67100
6510
3255
PAN
NA
2253
15916
2514
1917
SAR (wet)
NA
6.56
4.15
11.67
1.23
PAN/Load 5 gal)
NA
6.72
3.71
5.04
2.40
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
informaRon, including the possibility of fines and imprisonment for knowing violations."
Lab
(1) Analyses performed by City of Rocky Mount Laboratory
(2) Analyses performed by Meritech, Inc
-A7�o:�a
Date

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Pemul No. W NI(1)5568 pacih%y Name fairy of pocky Afowrt Scarce P-1 No. NOX172125 Suutce Namr Tar {fiver IXrfP
Laboratory)
laboratory 2
Sample or CompoaireDale
Paramemr (mg/%g) Class A Class B
City ofRoeky
hi—
C.ityof RrxkS-
Mront
(BynfRoA,
Ataant
,,y ofRarkr
M—
Pace Malytid
Arc Aadytical
Pm .4nalgtid
Ikee A W,
If/M13119
3/I2/2nU
-!/912G1'J
9(31Z'19
Ah-inami N/A N/A
15,5(xr
05g)
4,971,
3,158
Ammonia Ni—gen N/A
N/A
� � 75
85
48Jai
T5
243reJ
24.3
1,74RW
(126
6.1
V07.I9)
4
ar5 —
Arsenic 41
Cadmium 39
2(1s
Calciom N/A
N/A� I,nAI
AM
-2 n)
IZ7
Copper 1500
Lead 360
4,300
21.7
14.9
107
31t
31 i
0.9
6.11
$40
7.13
Magnesium. N/A
N/A
3911x�
2,90RIN,
6440r
529r1r
Mcrcury 17
57
n.m8
n*).
(13
1102
Molybdenum N/A
75
3.7
32.1
31.3
5
Nickel 420
NiwtrNinite NitmRen N/A
420
N/A
29-2
i955
185
3W7,
92.4
28
8.tx,
490.1A)
Percent Solids N/A
N/A
,,. a
IIU
Q%
u.._
pH (mr units) N/A
PhosphomsN/A
Potassium N/A
N/A
5.01
7.211
(ou
5.79
I,u5G;J11
N/A
N/A
701A)
1.731101
6,10.rnl
24MxUn
1,8961x1
3J,3(ltl.(M3
PAN (]nj./Inc.) N/A
PAN (Surface) N/A
N/A
❑.
84
i44
422
2,149
1.279
5,kr5
1557
_ N/A
Selenium IOD
Sndium N/A
SAR N/A
100
N/A
N/A
75
3,73u.11�1
5.12
24.3
62.6
31 kM)rMl
13.90
5
4,459.rx1
-�04
12,1011.1M1
IA3
TKN N/A - N/A
1,687
19d54
19;(Ml
13M1,
Zinc 7,800 7,500
14.3
]fi7
fi2a
"1 cc.rtif -, order penalty of law, that this document was prepamd under my direction or supereiaion in accordance with a system designed to
assure that quaRficd personnel properly gathered and evaluamd the information submitted- I am aware that there am significant penalties for
submitting false iofomation, including the bidit, ffine, and imprisonment/f,, knowing vtolatinvs ^
Signau of Prepare,* Date
*Pmparer is defined in 40 CFR P 03.9(,) and 15A NCAC Zr .1102 (26)

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River VAP
Sampling Date 3/12/2019
Solids 6.7
Mineralization Rate 0
Gallons per DT 3,579.23
pH 5
Sodium Absorpotion 5.92 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 3,687 lbs./1,000 gal 2.06
Ammonia Nitrogen (mg/Kg) 48.00 lbs./1,000 gal 0.03
Nitrate -Nitrite (mg/Kg) 59.55 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 84 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 108 lbs./1,000 gal 0.06
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.08
Phosphorus lbs./1,000 gal 0.39
Calcium lbs./1,000 gal 0.57
Magnesium lbs./1,000 gal 0.33
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
7.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
3.20
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
20.70
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
14.90
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.08
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
29.20
Nickel lbs./1,000 gal
0.02
Selenium (mg/Kg)
7.50
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
34.30
Zinc lbs./1,000 gal
0.02
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
3,687
84 0.17
3,603
3,687
108 0.22
3,579
3,603
0 0.00
3,603
3,579
0 0.00
3,579
3,603
0 0.00
3,603
3,579
0 0.00
3,579
3,603
0 0.00
3,603
3,579
0 0.00
3,579
3,603
0 0.00
3,603
3,579
0 0.00
3,579
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 84 0.17
Total 108 0.22

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River VAP
Sampling Date 4/9/2019
Solids 1.3
Mineralization Rate 0
Gallons per DT 18,446.78
pH 7.2
Sodium Absorpotion 1.93 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 19,154 lbs./1,000 gal 2.08
Ammonia Nitrogen (mg/Kg) 243.00 lbs./1,000 gal 0.03
Nitrate -Nitrite (mg/Kg) 300.77 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 422 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 544 lbs./1,000 gal 0.06
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.63
Phosphorus lbs./1,000 gal 0.67
Calcium lbs./1,000 gal 3.65
Magnesium lbs./1,000 gal 0.31
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
24.30
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
20.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
107.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
73.30
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.29
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
185.00
Nickel lbs./1,000 gal
0.02
Selenium (mg/Kg)
24.30
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
167.00
Zinc lbs./1,000 gal
0.02
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
19,154
422 0.84
18,732
19,154
544 1.09
18,610
18,732
0 0.00
18,732
18,610
0 0.00
18,610
18,732
0 0.00
18,732
18,610
0 0.00
18,610
18,732
0 0.00
18,732
18,610
0 0.00
18,610
18,732
0 0.00
18,732
18,610
0 0.00
18,610
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 422 0.84
Total 544 1.09

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River VAP
Sampling Date 9/3/2019
Solids 0.96
Mineralization Rate 0
Gallons per DT 24,980.02
pH 6.3
Sodium Absorpotion 13.50 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 19,063 lbs./1,000 gal 1.53
Ammonia Nitrogen (mg/Kg) 1,740.00 lbs./1,000 gal 0.14
Nitrate -Nitrite (mg/Kg) 409.00 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 1,279 lbs./1,000 gal 0.10
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 2,149 lbs./1,000 gal 0.17
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.51
Phosphorus lbs./1,000 gal 0.15
Calcium lbs./1,000 gal 0.23
Magnesium lbs./1,000 gal 0.05
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
62.60
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
6.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
31.30
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
31.30
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.23
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
92.40
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
62.60
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
62.60
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
19,063
1,279 2.56
17,784
19,063
2,149 4.30
16,914
17,784
0 0.00
17,784
16,914
0 0.00
16,914
17,784
0 0.00
17,784
16,914
0 0.00
16,914
17,784
0 0.00
17,784
16,914
0 0.00
16,914
17,784
0 0.00
17,784
16,914
0 0.00
16,914
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 1,279 2.56
Total 2,149 4.30

&,,AGMAN FIELD LOADING ESTIMATES
Facility Tar River W'IP
Sampling Date 11/26/2019
Solids 0.72
Mineralization Rate 0
Gallons per DT 33,306.69
pH 5.7
Sodium Absorpotion 0.74 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 13,875 lbs./1,000 gal 0.83
Ammonia Nitrogen (mg/Kg) 3,097.00 lbs./1,000 gal 0.19
Nitrate -Nitrite (mg/Kg) 8.06 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 1,557 lbs./1,000 gal 0.09
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 3,105 lbs./1,000 gal 0.19
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.03
Phosphorus lbs./1,000 gal 0.06
Calcium lbs./1,000 gal 0.07
Magnesium lbs./1,000 gal 0.03
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
4.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
0.90
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
6.11
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
28.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
22.00
Zinc lbs./1,000 gal
0.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
13,875
1,557 3.11
12,318
13,875
3,105 6.21
10,770
12,318
0 0.00
12,318
10,770
0 0.00
10,770
12,318
0 0.00
12,318
10,770
0 0.00
10,770
12,318
0 0.00
12,318
10,770
0 0.00
10,770
12,318
0 0.00
12,318
10,770
0 0.00
10,770
Equations
1 st Yr. PAN (mg/Kg)-(MR
x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)-
2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)-
3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)-
4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)-
5th Yr. TKN x (MR/16)
Total 1,557 3.11
Total 3,105 6.21

2019 City of Rocky Mount Analytical Report
WQ Permit Number: WQ0005568
Sample Identification: City of Rocky Mount Biosolids
Residual Source WQ # or NPDES #: NC 0072125
Facility Name: Tar River Reservoir Water Treatment Plant
Residual Analysis Data
Laboratories 1) City of Rocky Mount
performing 2) Pace Analytical
analyses: 3) Environmentl
Parameter (mg/kg)
cs mg Uonc.
Limit
(mg/kg)
SaLtnple or Composite Date
3/12/19
4/9/19
9/3/19
11/26/19
Percent So i s (1)
1`A
6.70%
1.30%
0.96%
0.72%
pH (1)
5.0
7.2
6.3
5.7
Arsenic (2)
75
7.50
24.300
62.600
4.000
Cadmium (2)
85
3.200
1 20.300
6.300
1 0.50
Copper (2)
4,300
20.70
107.00
31.30
0.9
Lead (2)
840
14.90
73.30
31.30
6.11
Mercury (2)
57
0.078
0.290
0.230
0.020
Molybdenum (2)
75
3.700
12.100
31.30
5.000
Nickel (2)
420
29.2
185.0
92.4
28.0
Selenium (2)
100
7.50
24.30
62.60
5.000
Zinc (2)
7,500
34.3
167.0
62.6
22.0
Total Phosphorus (1)
NA
701
6169
1896
1056.9
TKN (1)
NA
3687
19154
19063
13875
Ammonia -Nitrogen (1)
NA
48
243
1740
3097
Nitrate and Nitrite (1)
NA
59.55
300.77
409.00
8.06
Potassium (2)
NA
3730
24300
1 31300
529
Sodium (2)
NA
3730
12100
31300
1459
Magnesium (2)
NA
593
2900
644
529
Calcium (2)
NA
1020
33700
2830
1237
Silver (2)
NA
3.700
12.100
31.30 1
2.500
Aluminum (2)
NA
15500
63500
4870
3158
PAN
NA
1539
7987
8208
5868
SAR (wet)
NA
5.92
1.93
13.50
0.74
VAN/Load( /6500 gal)
NA 1
5.59
5.63
4.27
2.29
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Lab S
(1) Analyses performed by City of Rocky Mount Laboratory
(2) Analyses performed by Meritech, Inc
Date

City of Rocky Mount
2019 Class B Annual Report
WQ Permit# WQ0005568
Land Application Field Summary Forms

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 1 County Nash Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1 SoilSeries Nason Crop 1 Pan 141
LandOwner Barbara Taylor Jones Acres Permited 36.07 Soil Abbrevation: NnB Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
02/02/2019 Gallons
32,500
1.60
36.07
0.06
2.17
Tar River Regional WWTP
Moist
0 Surface
4.35
0.50
0.30
89,000
45,125.00 156.00
4.31
Crop 1
02/04/2019 Gallons
84,500
1.60
36.07
0.16
5.64
Tar River Regional WWTP
Moist
0 Surface
11.31
0.50
0.30
89,000
45,125.00 156.00
11.22
Crop 1
02/05/2019 Gallons
52,000
1.60
36.07
0.10
3.47
Tar River Regional WWTP
Moist
0 Surface
6.96
0.50
0.30
89,000
45,125.00 156.00
6.90
Crop 1
02/06/2019 Gallons
52,000
1.60
36.07
0.10
3.47
Tar River Regional WWTP
Moist
0 Surface
6.96
0.50
0.30
89,000
45,125.00 156.00
6.90
Crop 1
03/05/2019 Gallons
42,000
6.70
36.07
0.33
11.73
Tar River WTP
Moist
0 Surface
0.46
0.50
0
3,687
48.00 59.55
0.05
Crop 1
03/11/2019 Gallons
35,000
6.70
36.07
0.27
9.78
Tar River WTP
Moist
0 Surface
0.38
0.50
0
3,687
48.00 59.55
0.05
Crop 1
03/12/2019 Gallons
35,000
6.70
36.07
0.27
9.78
Tar River WTP
Moist
0 Surface
0.38
0.50
0
3,687
48.00 59.55
0.05
Crop 1
03/14/2019 Gallons
28,000
6.70
36.07
0.22
7.82
Tar River WTP
Moist
0 Surface
0.30
0.50
0
3,687
48.00 59.55
0.04
Crop 1
03/15/2019 Gallons
26,000
2.80
36.07
0.08
3.04
Tar River Regional WWTP
Moist
0 Surface
4.82
0.50
0.30
57,393
26,464.00 129.00
3.81
Crop 1
03/18/2019 Gallons
58,500
2.80
36.07
0.19
6.83
Tar River Regional WWTP
Moist
0 Surface
10.85
0.50
0.30
57,393
26,464.00 129.00
8.57
Crop 1
03/19/2019 Gallons
21,000
6.70
36.07
0.16
5.87
Tar River WTP
Moist
0 Surface
0.23
0.50
0
3,687
48.00 59.55
0.03
Crop 1
Total Volume Applied
466,500
Total Dry Tons
69.59
Sum Total P
47.00
Total
41.93
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.068
0.013
1.306
0.139 0.002
0.041
0.172
0.068
1.329
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.089
0.979
51.408
30.994 0.027
0.861
0.624
0.117
89.546
Cumulative Total
0.157
0.992
52.714
31.133 0.029
0.902
0.796
0.185
90.875
N/A
Permitted CPLR
36
34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��p y *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 1 County Nash Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 2 SoilSeries Nason Crop 1 Pan 141
LandOwner Barbara Taylor Jones Acres Permuted 27.07 Soil Abbrevation: NnB Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
03/12/2019
Gallons
65,000
2.80
27.07
0.28
7.59
Tar River Regional WWTP
Moist
0
Surface
16.06
0.50
0.30
57,393
26,464.00 129.00
12.69
Crop 1
03/13/2019
Gallons
65,000
2.80
27.07
0.28
7.59
Tar River Regional WWTP
Moist
0
Surface
16.06
0.50
0.30
57,393
26,464.00 129.00
12.69
Crop 1
03/14/2019
Gallons
26,000
2.80
27.07
0.11
3.04
Tar River Regional WWTP
Moist
0
Surface
6.42
0.50
0.30
57,393
26,464.00 129.00
5.08
Crop 1
03/19/2019
Gallons
91,000
2.80
27.07
0.39
10.63
Tar River Regional WWTP
Moist
0
Surface
22.49
0.50
0.30
57,393
26,464.00 129.00
17.77
Crop 1
Total Volume Applied
247,000
Total Dry Tons 28.84
Sum Total P 61.03
Total 48.24
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.050
0.005
1.159
0.086
0.001
0.034
0.098
0.050
1.180
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.100
0.741
41.106
24.929
0.019
0.466
11.902
0.068
81.077
Cumulative Total
0.150
0.745
42.265
25.016
0.020
0.500
12.000
0.118
82.257
N/A
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
���y *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
\rtT' X �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 22 County Nash Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1 SoilSeries Georgeville Crop 1 Pan 198
LandOwner Linda E. Fisher Acres Permuted 19.24 Soil Abbrevation: GeC Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
05/01/2019
Gallons
110,500
3.03
19.24
0.73
13.96 Tar River Regional WWTP
Dry
0
Surface
39.90
0.50
0.30
57,558
29,142.00 142.00
33.73
Crop 1
05/01/2019
Gallons
35,000
1.30
19.24
0.10
1.90 Tar River WTP
Dry
0
Surface
1.22
0.50
0
19,154
243.00 300.77
0.08
Crop 1
05/03/2019
Gallons
42,000
1.30
19.24
0.12
2.28 Tar River WTP
Dry
0
Surface
1.46
0.50
0
19,154
243.00 300.77
0.10
Crop 1
05/07/2019
Gallons
65,000
3.03
19.24
0.43
8.21 Tar River Regional WWTP
Dry
0
Surface
23.47
0.50
0.30
57,558
29,142.00 142.00
19.84
Crop 1
05/08/2019
Gallons
91,000
3.03
19.24
0.60
11.50 Tar River Regional WWTP
Dry
0
Surface
32.86
0.50
0.30
57,558
29,142.00 142.00
27.77
Crop 1
05/28/2019
Gallons
49,000
1.30
19.24
0.14
2.66 Tar River WTP
Dry
0
Surface
1.70
0.50
0
19,154
243.00 300.77
0.12
Crop 1
Total Volume Applied
392,500
Reported in Gallons
Arsenic Cadmium
Current Year
0.098
0.022
Prior Year
0.468
0.238
Cumulative Total
0.565
0.261
Permitted CPLR
36
34
Total Dry Tons 40.50
Copper Chromium
Lead
2.043
0.230
39.980
3.961
42.023
4.190
1338
267
Mercury Molybdenum
0.002 0.057
0.049 1.158
0.050 1.215
15
Sum Total P 100.61
Nickel
Selenium
Zinc
0.310
0.098
2.142
4.851
0.379
43.326
5.161
0.476
45.468
374
89
2498
Total 81.64
Total
Crop 1
Crop 2
PAN
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
(lbs./Ac.)
11W II WAMKE0101`K
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��py *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
_ WII �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 22 County Nash Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 2 SoilSeries Georgeville Crop 1 Pan 211
LandOwner Linda E. Fisher Acres Permuted 32.91 Soil Abbrevation: GeB Crop 2
Operator Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
05/02/2019
Gallons
123,500
3.03
32.91
0.47
15.60 Tar River Regional WWTP
Dry
0
Surface
26.07
0.50
0.30
57,558
29,142.00 142.00
22.04
Crop 1
05/02/2019
Gallons
35,000
1.30
32.91
0.06
1.90 Tar River WTP
Dry
0
Surface
0.71
0.50
0
19,154
243.00 300.77
0.05
Crop 1
05/03/2019
Gallons
97,500
3.03
32.91
0.37
12.32 Tar River Regional WWTP
Dry
0
Surface
20.58
0.50
0.30
57,558
29,142.00 142.00
17.40
Crop 1
05/09/2019
Gallons
117,000
3.03
32.91
0.45
14.78 Tar River Regional WWTP
Dry
0
Surface
24.70
0.50
0.30
57,558
29,142.00 142.00
20.88
Crop 1
05/13/2019
Gallons
6,500
3.03
32.91
0.02
0.82 Tar River Regional WWTP
Dry
0
Surface
1.37
0.50
0.30
57,558
29,142.00 142.00
1.16
Crop 1
05/15/2019
Gallons
182,000
3.03
32.91
0.70
23.00 Tar River Regional WWTP
Dry
0
Surface
38.42
0.50
0.30
57,558
29,142.00 142.00
32.47
Crop 1
05/22/2019
Gallons
35,000
1.30
32.91
0.06
1.90 Tar River WTP
Dry
0
Surface
0.71
0.50
0
19,154
243.00 300.77
0.05
Crop 1
05/24/2019
Gallons
42,000
1.30
32.91
0.07
2.28 Tar River WTP
Dry
0
Surface
0.85
0.50
0
19,154
243.00 300.77
0.06
Crop 1
Total Volume Applied
638,500
Total Dry Tons 72.60
Sum Total P 113.42
Total 94.10
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.102
0.017
2.312
0.232
0.002
0.061
0.274
0.102
2.398
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.393
0.182
31.862
3.218
0.038
0.954
4.226
0.330
38.213
Cumulative Total
0.495
0.198
34.173
3.450
0.040
1.015
4.500
0.431
40.611
1.0 T/Ac. 11 /20/19
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��py *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
�WX �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1A SoilSeries Aycock Crop 1 Pan 172
LandOwner City of Rocky Mount Acres Permuted 17.77 Soil Abbrevation: AyB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia
-Nitrite
PAN
PAN Crop
03/01/2019
Gallons
32,500
2.80
17.77
0.21
3.79
Tar River Regional WWTP
Moist
0
Surface
12.23
0.50
0.30
57,393
26,464.00
129.00
9.67
Crop 1
08/01/2019
Gallons
45,500
3.00
17.77
0.32
5.69
Tar River Regional WWTP
Dry
0
Surface
19.50
0.50
0.30
56,067
23,733.00
87.00
13.87
Crop 1
08/01 /2019
Gallons
35,000
0.96
17.77
0.08
1.40
Tar River WTP
Dry
0
Surface
0.30
0.50
0
19,063
1,740.00
409.00
0.20
Crop 1
08/02/2019
Gallons
65,000
3.00
17.77
0.46
8.13
Tar River Regional WWTP
Dry
0
Surface
27.85
0.50
0.30
56,067
23,733.00
87.00
19.82
Crop 1
08/02/2019
Gallons
28,000
0.96
17.77
0.06
1.12
Tar River WTP
Dry
0
Surface
0.24
0.50
0
19,063
1,740.00
409.00
0.16
Crop 1
08/07/2019
Gallons
26,000
3.00
17.77
0.18
3.25
Tar River Regional WWTP
Dry
0
Surface
11.14
0.50
0.30
56,067
23,733.00
87.00
7.93
Crop 1
Total Volume Applied
232,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.082
0.008
Prior Year
0.467
0.199
Cumulative Total
0.549
0.207
Permitted CPLR
36
34
Total Dry Tons 23.39
Copper Chromium
Lead
1.216
0.103
37.628
3.845
38.844
3.948
1338
267
Mercury Molybdenum
0.001 0.043
0.063 1.425
0.064 1.468
15
Sum Total P 71.26
Nickel
Selenium
Zinc
0.134
0.082
1.331
4.880
0.418
47.251
5.014
0.500
48.582
374
89
2498
Total 51.65
Total
Crop 1
Crop 2
PAN
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
(lbs./Ac.)
Wori_MrIacr`K
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��py *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
_ WII �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Pine
Facility Name City of Rocky Mount Field Name 1B SoilSeries Aycock Crop 1 Pan 75
LandOwner City of Rocky Mount Acres Permited 22.95 Soil Abbrevation: AyB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia
-Nitrite
PAN
PAN Crop
01 /02/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
01/07/2019
Gallons
42,000
6.70
22.95
0.51
11.73
Tar River WTP
Moist
0
Surface
0.72
0.50
0
3,687
48.00
59.55
0.09
Crop 1
01/08/2019
Gallons
42,000
6.70
22.95
0.51
11.73
Tar River WTP
Moist
0
Surface
0.72
0.50
0
3,687
48.00
59.55
0.09
Crop 1
01/09/2019
Gallons
49,000
6.70
22.95
0.60
13.69
Tar River WTP
Moist
0
Surface
0.84
0.50
0
3,687
48.00
59.55
0.10
Crop 1
01/10/2019
Gallons
49,000
6.70
22.95
0.60
13.69
Tar River WTP
Moist
0
Surface
0.84
0.50
0
3,687
48.00
59.55
0.10
Crop 1
01/11/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
01/19/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
01 /24/2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Moist
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
01/25/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
01/29/2019
Gallons
42,000
6.70
22.95
0.51
11.73
Tar River WTP
Moist
0
Surface
0.72
0.50
0
3,687
48.00
59.55
0.09
Crop 1
01 /30/2019
Gallons
63,000
6.70
22.95
0.77
17.60
Tar River WTP
Moist
0
Surface
1.08
0.50
0
3,687
48.00
59.55
0.13
Crop 1
01/31/2019
Gallons
49,000
6.70
22.95
0.60
13.69
Tar River WTP
Moist
0
Surface
0.84
0.50
0
3,687
48.00
59.55
0.10
Crop 1
02/01 /2019
Gallons
42,000
6.70
22.95
0.51
11.73
Tar River WTP
Moist
0
Surface
0.72
0.50
0
3,687
48.00
59.55
0.09
Crop 1
02/04/2019
Gallons
91,000
6.70
22.95
1.11
25.42
Tar River WTP
Moist
0
Surface
1.55
0.50
0
3,687
48.00
59.55
0.19
Crop 1
02/07/2019
Gallons
98,000
6.70
22.95
1.19
27.38
Tar River WTP
Moist
0
Surface
1.67
0.50
0
3,687
48.00
59.55
0.20
Crop 1
02/08/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
02/15/2019
Gallons
35,000
6.70
22.95
0.43
9.78
Tar River WTP
Moist
0
Surface
0.60
0.50
0
3,687
48.00
59.55
0.07
Crop 1
02/25/2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Moist
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
03/04/2019
Gallons
56,000
6.70
22.95
0.68
15.65
Tar River WTP
Moist
0
Surface
0.96
0.50
0
3,687
48.00
59.55
0.11
Crop 1
03/05/2019
Gallons
26,000
2.80
22.95
0.13
3.04
Tar River Regional WWTP
Moist
0
Surface
7.58
0.50
0.30
57,393
26,464.00 129.00
5.99
Crop 1
03/06/2019
Gallons
65,000
2.80
22.95
0.33
7.59
Tar River Regional WWTP
Moist
0
Surface
18.94
0.50
0.30
57,393
26,464.00 129.00
14.97
Crop 1
03/08/2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Moist
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
03/13/2019
Gallons
42,000
6.70
22.95
0.51
11.73
Tar River WTP
Moist
0
Surface
0.72
0.50
0
3,687
48.00
59.55
0.09
Crop 1
03/14/2019
Gallons
14,000
6.70
22.95
0.17
3.91
Tar River WTP
Moist
0
Surface
0.24
0.50
0
3,687
48.00
59.55
0.03
Crop 1
03/15/2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Moist
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
03/18/2019
Gallons
21,000
5.50
22.95
0.21
4.82
Sunset Ave WTP
Moist
0
Surface
0.38
0.50
0
5,273
727.00
71.50
0.18
Crop 1
03/18/2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Moist
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
03/19/2019
Gallons
14,000
6.70
22.95
0.17
3.91
Tar River WTP
Moist
0
Surface
0.24
0.50
0
3,687
48.00
59.55
0.03
Crop 1
03/29/2019
Gallons
49,000
6.70
22.95
0.60
13.69
Tar River WTP
Moist
0
Surface
0.84
0.50
0
3,687
48.00
59.55
0.10
Crop 1
03/29/2019
Gallons
14,000
5.50
22.95
0.14
3.21
Sunset Ave WTP
Moist
0
Surface
0.25
0.50
0
5,273
727.00
71.50
0.12
Crop 1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
04/01 /2019
Gallons
28,000
6.70
22.95
0.34
7.82
Tar River WTP
Dry
0
Surface
0.48
0.50
0
3,687
48.00
59.55
0.06
Crop 1
04/02/2019
Gallons
7,000
0.43
22.95
0.01
0.13
Sunset Ave WTP
Dry
0
Surface
0.26
0.50
0
36,977
2,112.00
913.95
0.02
Crop 1
04/02/2019
Gallons
42,000
1.30
22.95
0.10
2.28
Tar River WTP
Dry
0
Surface
1.22
0.50
0
19,154
243.00
300.77
0.08
Crop 1
04/05/2019
Gallons
28,000
0.43
22.95
0.02
0.50
Sunset Ave WTP
Dry
0
Surface
1.05
0.50
0
36,977
2,112.00
913.95
0.09
Crop 1
04/09/2019
Gallons
49,000
0.43
22.95
0.04
0.88
Sunset Ave WTP
Dry
0
Surface
1.83
0.50
0
36,977
2,112.00
913.95
0.15
Crop 1
04/10/2019
Gallons
42,000
0.43
22.95
0.03
0.75
Sunset Ave WTP
Dry
0
Surface
1.57
0.50
0
36,977
2,112.00
913.95
0.13
Crop 1
04/11/2019
Gallons
28,000
0.43
22.95
0.02
0.50
Sunset Ave WTP
Dry
0
Surface
1.05
0.50
0
36,977
2,112.00
913.95
0.09
Crop 1
04/16/2019
Gallons
28,000
0.43
22.95
0.02
0.50
Sunset Ave WTP
Dry
0
Surface
1.05
0.50
0
36,977
2,112.00
913.95
0.09
Crop 1
04/17/2019
Gallons
45,500
2.80
22.95
0.23
5.31
Tar River Regional WWTP
Dry
0
Surface
13.26
0.50
0.30
57,393
26,464.00
129.00
10.48
Crop 1
04/18/2019
Gallons
28,000
0.43
22.95
0.02
0.50
Sunset Ave WTP
Dry
0
Surface
1.05
0.50
0
36,977
2,112.00
913.95
0.09
Crop 1
04/18/2019
Gallons
39,000
2.80
22.95
0.20
4.55
Tar River Regional WWTP
Dry
0
Surface
11.37
0.50
0.30
57,393
26,464.00
129.00
8.98
Crop 1
04/25/2019
Gallons
35,000
0.43
22.95
0.03
0.63
Sunset Ave WTP
Dry
0
Surface
1.31
0.50
0
36,977
2,112.00
913.95
0.11
Crop 1
04/29/2019
Gallons
28,000
0.43
22.95
0.02
0.50
Sunset Ave WTP
Dry
0
Surface
1.05
0.50
0
36,977
2,112.00
913.95
0.09
Crop 1
06/03/2019
Gallons
7,000
1.30
22.95
0.02
0.38
Tar River WTP
Dry
0
Surface
0.20
0.50
0
19,154
243.00
300.77
0.01
Crop 1
06/17/2019
Gallons
28,000
1.30
22.95
0.07
1.52
Tar River WTP
Dry
0
Surface
0.82
0.50
0
19,154
243.00
300.77
0.06
Crop 1
06/18/2019
Gallons
42,000
1.30
22.95
0.10
2.28
Tar River WTP
Dry
0
Surface
1.22
0.50
0
19,154
243.00
300.77
0.08
Crop 1
06/19/2019
Gallons
21,000
1.30
22.95
0.05
1.14
Tar River WTP
Dry
0
Surface
0.61
0.50
0
19,154
243.00
300.77
0.04
Crop 1
06/24/2019
Gallons
21,000
1.30
22.95
0.05
1.14
Tar River WTP
Dry
0
Surface
0.61
0.50
0
19,154
243.00
300.77
0.04
Crop 1
06/25/2019
Gallons
21,000
1.30
22.95
0.05
1.14
Tar River WTP
Dry
0
Surface
0.61
0.50
0
19,154
243.00
300.77
0.04
Crop 1
06/26/2019
Gallons
35,000
1.30
22.95
0.08
1.90
Tar River WTP
Dry
0
Surface
1.02
0.50
0
19,154
243.00
300.77
0.07
Crop 1
06/27/2019
Gallons
14,000
1.30
22.95
0.03
0.76
Tar River WTP
Dry
0
Surface
0.41
0.50
0
19,154
243.00
300.77
0.03
Crop 1
06/28/2019
Gallons
28,000
1.30
22.95
0.07
1.52
Tar River WTP
Dry
0
Surface
0.82
0.50
0
19,154
243.00
300.77
0.06
Crop 1
06/30/2019
Gallons
42,000
1.30
22.95
0.10
2.28
Tar River WTP
Dry
0
Surface
1.22
0.50
0
19,154
243.00
300.77
0.08
Crop 1
O8/07/2019
Gallons
28,000
0.96
22.95
0.05
1.12
Tar River WTP
Dry
0
Surface
0.19
0.50
0
19,063
1,740.00
409.00
0.12
Crop 1
08/07/2019
Gallons
45,500
3.00
22.95
0.25
5.69
Tar River Regional WWTP
Dry
0
Surface
15.10
0.50
0.30
56,067
23,733.00
87.00
10.74
Crop 1
08/09/2019
Gallons
42,000
0.96
22.95
0.07
1.68
Tar River WTP
Dry
0
Surface
0.28
0.50
0
19,063
1,740.00
409.00
0.19
Crop 1
O8/12/2019
Gallons
49,000
0.96
22.95
0.09
1.96
Tar River WTP
Dry
0
Surface
0.32
0.50
0
19,063
1,740.00
409.00
0.22
Crop 1
08/27/2019
Gallons
56,000
0.96
22.95
0.10
2.24
Tar River WTP
Dry
0
Surface
0.37
0.50
0
19,063
1,740.00
409.00
0.25
Crop 1
08/28/2019
Gallons
49,000
0.96
22.95
0.09
1.96
Tar River WTP
Dry
0
Surface
0.32
0.50
0
19,063
1,740.00
409.00
0.22
Crop 1
O8/30/2019
Gallons
28,000
0.96
22.95
0.05
1.12
Tar River WTP
Dry
0
Surface
0.19
0.50
0
19,063
1,740.00
409.00
0.12
Crop 1
09/11/2019
Gallons
28,000
0.96
22.95
0.05
1.12
Tar River WTP
Dry
0
Surface
0.19
0.50
0
19,063
1,740.00
409.00
0.12
Crop 1
10/22/2019
Gallons
28,000
2.31
22.95
0.12
2.70
Sunset Ave WTP
Dry
0
Surface
0.18
0.50
0
4,762
100.00
2.25
0.01
Crop 1
10/23/2019
Gallons
21,000
2.31
22.95
0.09
2.02
Sunset Ave WTP
Dry
0
Surface
0.13
0.50
0
4,762
100.00
2.25
0.01
Crop 1
11/20/2019
Gallons
7,000
2.31
22.95
0.03
0.67
Sunset Ave WTP
Moist
0
Surface
0.04
0.50
0
4,762
100.00
2.25
0.00
Crop 1
11/21/2019
Gallons
56,000
2.31
22.95
0.24
5.39
Sunset Ave WTP
Moist
0
Surface
0.36
0.50
0
4,762
100.00
2.25
0.02
Crop 1
11/26/2019
Gallons
35,000
2.31
22.95
0.15
3.37
Sunset Ave WTP
Moist
0
Surface
0.22
0.50
0
4,762
100.00
2.25
0.02
Crop 1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
11/27/2019 Gallons
21,000 2.31
22.95
0.09
2.02
Sunset Ave WTP
Moist
0 Surface
0.13
0.50
0
4,762
100.00
2.25
0.01
Crop 1
12/04/2019 Gallons
35,000 0.72
22.95
0.05
1.05
Tar River WTP
Moist
0 Surface
0.10
0.50
0
13,875
3,097.00
8.06
0.14
Crop 1
12/05/2019 Gallons
35,000 0.72
22.95
0.05
1.05
Tar River WTP
Moist
0 Surface
0.10
0.50
0
13,875
3,097.00
8.06
0.14
Crop 1
12/16/2019 Gallons
28,000 0.72
22.95
0.04
0.84
Tar River WTP
Moist
0 Surface
0.08
0.50
0
13,875
3,097.00
8.06
0.11
Crop 1
12/19/2019 Gallons
21,000 0.72
22.95
0.03
0.63
Tar River WTP
Moist
0 Surface
0.06
0.50
0
13,875
3,097.00
8.06
0.09
Crop 1
12/31 /2019 Gallons
56,000 0.72
22.95
0.07
1.68
Tar River WTP
Moist
0 Surface
0.15
0.50
0
13,875
3,097.00
8.06
0.23
Crop 1
Total Volume Applied
2,573,000
Total Dry Tons
400.99
Sum Total P
108.39
Total
57.23
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.395 0.144
2.063
0.696 0.004
0.216
1.343
0.399
2.630
Lime (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
0.672 0.340
28.321
4.524 0.070
1.370
7.858
0.445
27.946
Cumulative Total
1.067 0.485
30.385
5.220 0.075
1.586
9.201
0.845
30.575
1.0 T/Ac.
12/13/19
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Pine
Facility Name City of Rocky Mount Field Name 1C SoilSeries Norfolk Crop 1 Pan 75
LandOwner City of Rocky Mount Acres Permited 9.46 Soil Abbrevation: NoB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia
-Nitrite
PAN
PAN Crop
01/15/2019
Gallons
21,000
6.70
9.46
0.62
5.87
Tar River WTP
Moist
0
Surface
0.87
0.50
0
3,687
48.00
59.55
0.10
Crop 1
01/16/2019
Gallons
35,000
6.70
9.46
1.03
9.78
Tar River WTP
Moist
0
Surface
1.45
0.50
0
3,687
48.00
59.55
0.17
Crop 1
01/17/2019
Gallons
35,000
6.70
9.46
1.03
9.78
Tar River WTP
Moist
0
Surface
1.45
0.50
0
3,687
48.00
59.55
0.17
Crop 1
01/18/2019
Gallons
84,000
6.70
9.46
2.48
23.47
Tar River WTP
Moist
0
Surface
3.48
0.50
0
3,687
48.00
59.55
0.41
Crop 1
01/28/2019
Gallons
70,000
6.70
9.46
2.07
19.56
Tar River WTP
Moist
0
Surface
2.90
0.50
0
3,687
48.00
59.55
0.35
Crop 1
02/22/2019
Gallons
35,000
6.70
9.46
1.03
9.78
Tar River WTP
Moist
0
Surface
1.45
0.50
0
3,687
48.00
59.55
0.17
Crop 1
03/19/2019
Gallons
21,000
5.50
9.46
0.51
4.82
Sunset Ave WTP
Moist
0
Surface
0.91
0.50
0
5,273
727.00
71.50
0.44
Crop 1
03/20/2019
Gallons
21,000
5.50
9.46
0.51
4.82
Sunset Ave WTP
Moist
0
Surface
0.91
0.50
0
5,273
727.00
71.50
0.44
Crop 1
03/20/2019
Gallons
28,000
6.70
9.46
0.83
7.82
Tar River WTP
Moist
0
Surface
1.16
0.50
0
3,687
48.00
59.55
0.14
Crop 1
03/25/2019
Gallons
21,000
6.70
9.46
0.62
5.87
Tar River WTP
Moist
0
Surface
0.87
0.50
0
3,687
48.00
59.55
0.10
Crop 1
03/25/2019
Gallons
28,000
5.50
9.46
0.68
6.42
Sunset Ave WTP
Moist
0
Surface
1.22
0.50
0
5,273
727.00
71.50
0.59
Crop 1
03/27/2019
Gallons
35,000
6.70
9.46
1.03
9.78
Tar River WTP
Moist
0
Surface
1.45
0.50
0
3,687
48.00
59.55
0.17
Crop 1
03/27/2019
Gallons
35,000
5.50
9.46
0.85
8.03
Sunset Ave WTP
Moist
0
Surface
1.52
0.50
0
5,273
727.00
71.50
0.74
Crop 1
03/28/2019
Gallons
28,000
5.50
9.46
0.68
6.42
Sunset Ave WTP
Moist
0
Surface
1.22
0.50
0
5,273
727.00
71.50
0.59
Crop 1
03/28/2019
Gallons
49,000
6.70
9.46
1.45
13.69
Tar River WTP
Moist
0
Surface
2.03
0.50
0
3,687
48.00
59.55
0.24
Crop 1
04/04/2019
Gallons
35,000
0.43
9.46
0.07
0.63
Sunset Ave WTP
Dry
0
Surface
3.18
0.50
0
36,977
2,112.00
913.95
0.26
Crop 1
04/08/2019
Gallons
42,000
0.43
9.46
0.08
0.75
Sunset Ave WTP
Dry
0
Surface
3.81
0.50
0
36,977
2,112.00
913.95
0.31
Crop 1
04/12/2019
Gallons
28,000
0.43
9.46
0.05
0.50
Sunset Ave WTP
Dry
0
Surface
2.54
0.50
0
36,977
2,112.00
913.95
0.21
Crop 1
04/17/2019
Gallons
21,000
0.43
9.46
0.04
0.38
Sunset Ave WTP
Dry
0
Surface
1.91
0.50
0
36,977
2,112.00
913.95
0.16
Crop 1
04/22/2019
Gallons
39,000
2.80
9.46
0.48
4.55
Tar River Regional WWTP
Dry
0
Surface
27.58
0.50
0.30
57,393
26,464.00
129.00
21.80
Crop 1
04/26/2019
Gallons
21,000
0.43
9.46
0.04
0.38
Sunset Ave WTP
Dry
0
Surface
1.91
0.50
0
36,977
2,112.00
913.95
0.16
Crop 1
07/17/2019
Gallons
14,000
0.96
9.46
0.06
0.56
Tar River WTP
Dry
0
Surface
0.22
0.50
0
19,063
1,740.00
409.00
0.15
Crop 1
07/18/2019
Gallons
28,000
0.96
9.46
0.12
1.12
Tar River WTP
Dry
0
Surface
0.45
0.50
0
19,063
1,740.00
409.00
0.30
Crop 1
08/09/2019
Gallons
26,000
3.00
9.46
0.34
3.25
Tar River Regional WWTP
Dry
0
Surface
20.93
0.50
0.30
56,067
23,733.00
87.00
14.89
Crop 1
08/13/2019
Gallons
49,000
0.96
9.46
0.21
1.96
Tar River WTP
Dry
0
Surface
0.79
0.50
0
19,063
1,740.00
409.00
0.53
Crop 1
08/15/2019
Gallons
35,000
0.96
9.46
0.15
1.40
Tar River WTP
Dry
0
Surface
0.56
0.50
0
19,063
1,740.00
409.00
0.38
Crop 1
08/16/2019
Gallons
14,000
0.96
9.46
0.06
0.56
Tar River WTP
Dry
0
Surface
0.22
0.50
0
19,063
1,740.00
409.00
0.15
Crop 1
08/19/2019
Gallons
21,000
0.96
9.46
0.09
0.84
Tar River WTP
Dry
0
Surface
0.34
0.50
0
19,063
1,740.00
409.00
0.23
Crop 1
10/24/2019
Gallons
21,000
2.31
9.46
0.21
2.02
Sunset Ave WTP
Dry
0
Surface
0.33
0.50
0
4,762
100.00
2.25
0.02
Crop 1
10/25/2019
Gallons
28,000
2.31
9.46
0.29
2.70
Sunset Ave WTP
Dry
0
Surface
0.43
0.50
0
4,762
100.00
2.25
0.03
Crop 1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
10/28/2019 Gallons
14,000 2.31
9.46
0.14
1.35
Sunset Ave WTP
Dry
0 Surface
0.22
0.50
0
4,762
100.00
2.25
0.01
Crop 1
11/22/2019 Gallons
42,000 2.31
9.46
0.43
4.05
Sunset Ave WTP
Moist
0 Surface
0.65
0.50
0
4,762
100.00
2.25
0.04
Crop 1
11/25/2019 Gallons
35,000 2.31
9.46
0.36
3.37
Sunset Ave WTP
Moist
0 Surface
0.54
0.50
0
4,762
100.00
2.25
0.04
Crop 1
12/17/2019 Gallons
21,000 0.72
9.46
0.07
0.63
Tar River WTP
Moist
0 Surface
0.14
0.50
0
13,875
3,097.00
8.06
0.21
Crop 1
12/18/2019 Gallons
21,000 0.72
9.46
0.07
0.63
Tar River WTP
Moist
0 Surface
0.14
0.50
0
13,875
3,097.00
8.06
0.21
Crop 1
Total Volume Applied
1,101,000
Total Dry Tons
177.53
Sum Total P
89.77
Total
44.93
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.417 0.138
1.685
0.635 0.005
0.230
1.130
0.425
2.134
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.531 0.145
10.726
1.869 0.058
0.607
2.878
0.369
16.519
Cumulative Total
0.948 0.283
12.411
2.504 0.063
0.837
4.008
0.793
18.653
1.0 T/Ac.
12/4/19
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
uvR u+�d 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1D SoilSeries Aycock Crop 1 Pan 172
LandOwner City of Rocky Mount Acres Permuted 7.11 Soil Abbrevation: AyB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
03/07/2019
Gallons
39,000
2.80
7.11
0.64
4.55
Tar River Regional WWTP
Moist
0
Surface
36.69
0.50
0.30
57,393
26,464.00 129.00
29.00
Crop 1
08/09/2019
Gallons
45,500
3.00
7.11
0.80
5.69
Tar River Regional WWTP
Dry
0
Surface
48.73
0.50
0.30
56,067
23,733.00 87.00
34.67
Crop 1
08/20/2019
Gallons
42,000
0.96
7.11
0.24
1.68
Tar River WTP
Dry
0
Surface
0.90
0.50
0
19,063
1,740.00 409.00
0.60
Crop 1
08/21 /2019
Gallons
63,000
0.96
7.11
0.35
2.52
Tar River WTP
Dry
0
Surface
1.35
0.50
0
19,063
1,740.00 409.00
0.91
Crop 1
Total Volume Applied
189,500
Total Dry Tons 14.45
Sum Total P 87.66
Total 65.18
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.149
0.015
1.546
0.153
0.002
0.080
0.241
0.149
1.680
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.358
0.158
25.695
2.473
0.060
0.865
3.331
0.254
31.195
Cumulative Total
0.507
0.173
27.240
2.626
0.062
0.945
3.572
0.404
32.875
2.0 T/Ac. 12/4/19
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
���y *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
\rtT' X �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1E SoilSeries Aycock Crop 1 Pan 172
LandOwner City of Rocky Mount Acres Permuted 12.59 Soil Abbrevation: AyB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN Ammonia
-Nitrite
PAN
PAN Crop
08/09/2019 Gallons
26,000 3.00
12.59
0.26
3.25
Tar River Regional WWTP
Dry
0 Surface
15.72
0.50
0.30
56,067
23,733.00
87.00
11.19
Crop 1
08/12/2019 Gallons
52,000 3.00
12.59
0.52
6.51
Tar River Regional WWTP
Dry
0 Surface
31.45
0.50
0.30
56,067
23,733.00
87.00
22.38
Crop 1
08/22/2019 Gallons
56,000 0.96
12.59
0.18
2.24
Tar River WTP
Dry
0 Surface
0.68
0.50
0
19,063
1,740.00
409.00
0.46
Crop 1
08/23/2019 Gallons
35,000 0.96
12.59
0.11
1.40
Tar River WTP
Dry
0 Surface
0.42
0.50
0
19,063
1,740.00
409.00
0.28
Crop 1
08/29/2019 Gallons
49,000 0.96
12.59
0.16
1.96
Tar River WTP
Dry
0 Surface
0.59
0.50
0
19,063
1,740.00
409.00
0.40
Crop 1
Total Volume Applied
218,000
Total Dry Tons
15.36
Sum Total P
48.86
Total
34.70
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.100 0.010
0.814
0.090 0.001
0.050
0.153
0.100
0.924
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.490 0.236
40.134
4.210 0.049
1.167
5.567
0.359
37.604
Cumulative Total
0.590 0.246
40.948
4.300 0.050
1.217
5.720
0.458
38.528
1.0 T/Ac.
12/4/19
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
j� *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
T4 i 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 1F SoilSeries Norfolk Crop 1 Pan 148
LandOwner City of Rocky Mount Acres Permuted 5.44 Soil Abbrevation: NoC Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied
% Solids Used DT/Ac. Tons Source
Condition Precip
Method
P Volatilization Mineralization
TKN Ammonia -Nitrite PAN
PAN Crop
03/14/2019 Gallons 45,500
2.80 5.44 0.98 5.31 Tar River Regional WWTP
Moist 0
Surface
55.94 0.50 0.30
57,393 26,464.00 129.00 44.22
Crop 1
08/13/2019 Gallons 52,000
3.00 5.44 1.20 6.51 Tar River Regional WWTP
Dry 0
Surface
72.78 0.50 0.30
56,067 23,733.00 87.00 51.79
Crop 1
Total Volume Applied
97,500
Total Dry Tons 11.82
Sum Total P 128.73
Total 96.01
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.114
0.011
2.275
0.175
0.002
0.065
0.199
0.114
2.421
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.434
0.195
33.636
3.620
0.039
0.887
5.258
0.323
31.537
Cumulative Total
0.548
0.206
35.911
3.795
0.041
0.952
5.457
0.437
33.958
1.5 T/Ac. 12/4/19
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Hay
Facility Name City of Rocky Mount Field Name 2 SoilSeries Norfolk Crop 1 Pan 158
LandOwner City of Rocky Mount Acres Permuted 22.74 Soil Abbrevation: NoB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
03/12/2019
Gallons
71,500
2.80
22.74
0.37
8.35
Tar River Regional WWTP
Moist
0
03/15/2019
Gallons
39,000
2.80
22.74
0.20
4.55
Tar River Regional WWTP
Moist
0
03/18/2019
Gallons
32,500
2.80
22.74
0.17
3.79
Tar River Regional WWTP
Moist
0
03/20/2019
Gallons
13,000
2.80
22.74
0.07
1.52
Tar River Regional WWTP
Moist
0
05/29/2019
Gallons
52,000
3.03
22.74
0.29
6.57
Tar River Regional WWTP
Dry
0
05/31/2019
Gallons
78,000
3.03
22.74
0.43
9.86
Tar River Regional WWTP
Dry
0
06/26/2019
Gallons
78,000
3.00
22.74
0.43
9.76
Tar River Regional WWTP
Dry
0
07/11/2019
Gallons
42,000
0.96
22.74
0.07
1.68
Tar River WTP
Dry
0
07/26/2019
Gallons
28,000
0.96
22.74
0.05
1.12
Tar River WTP
Dry
0
07/30/2019
Gallons
28,000
0.96
22.74
0.05
1.12
Tar River WTP
Dry
0
08/15/2019
Gallons
45,500
3.00
22.74
0.25
5.69
Tar River Regional WWTP
Dry
0
08/16/2019
Gallons
19,500
3.00
22.74
0.11
2.44
Tar River Regional WWTP
Dry
0
09/03/2019
Gallons
45,500
2.90
22.74
0.24
5.50
Tar River Regional WWTP
Dry
0
09/04/2019
Gallons
52,000
2.90
22.74
0.28
6.29
Tar River Regional WWTP
Dry
0
Total Volume Applied
624,500
Reported in Gallons
Arsenic Cadmium
Current Year
0.164
0.016
Prior Year
0.597
0.328
Cumulative Total
0.761
0.344
Permitted CPLR
36
34
Total Dry Tons 68.24
Copper Chromium
Lead
3.282
0.278
43.187
4.660
46.470
4.938
1338
267
Mercury Molybdenum
0.003 0.097
0.106 1.571
0.109 1.668
15
Application
Total
Method
P
Volatilization
Mineralization
Surface
21.03
0.50
0.30
Surface
11.47
0.50
0.30
Surface
9.56
0.50
0.30
Surface
3.82
0.50
0.30
Surface
15.89
0.50
0.30
Surface
23.83
0.50
0.30
Surface
25.40
0.50
0.30
Surface
0.28
0.50
0
Surface
0.19
0.50
0
Surface
0.19
0.50
0
Surface
15.24
0.50
0.30
Surface
6.53
0.50
0.30
Surface
14.73
0.50
0.30
Surface
16.84
0.50
0.30
Sum Total P 165.00
Nickel
Selenium
Zinc
0.309
0.164
3.402
5.826
0.460
51.454
6.135
0.624
54.856
374
89
2498
Nitrate Crop 1
Crop 2
TKN
Ammonia -Nitrite
PAN
PAN Crop
57,393
26,464.00 129.00
16.62
Crop 1
57,393
26,464.00 129.00
9.07
Crop 1
57,393
26,464.00 129.00
7.56
Crop 1
57,393
26,464.00 129.00
3.02
Crop 1
57,558
29,142.00 142.00
13.43
Crop 1
57,558
29,142.00 142.00
20.14
Crop 1
58,967
38,667.00 196.00
21.99
Crop 1
19,063
1,740.00 409.00
0.19
Crop 1
19,063
1,740.00 409.00
0.13
Crop 1
19,063
1,740.00 409.00
0.13
Crop 1
56,067
23,733.00 87.00
10.84
Crop 1
56,067
23,733.00 87.00
4.65
Crop 1
70,069
23,103.00 185.00
12.50
Crop 1
70,069
23,103.00 185.00
14.28
Crop 1
Total 134.53
Total
Crop 1
Crop 2
PAN
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
(lbs./Ac.)
2.5 T/Ac. 12/5/19
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 3 SoilSeries Roanoke Crop 1 Pan 151
LandOwner City of Rocky Mount Acres Permuted 18.28 Soil Abbrevation: Ro Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
01/11/2019
Gallons
39,000
2.90
18.28
0.26
4.72
Tar RiverRegionalWWTP
Moist
0
Surface
15.14
0.50
0.30
72,414
34,690.00 105.00
14.84
Crop
01/18/2019
Gallons
32,500
2.90
18.28
0.22
3.93
Tar River Regional WWTP
Moist
0
Surface
12.62
0.50
0.30
72,414
34,690.00 105.00
12.37
Crop 1
01/19/2019
Gallons
52,000
2.90
18.28
0.34
6.29
Tar River Regional WWTP
Moist
0
Surface
20.19
0.50
0.30
72,414
34,690.00 105.00
19.79
Crop 1
01/23/2019
Gallons
32,500
1.60
18.28
0.12
2.17
Tar River Regional WWTP
Moist
0
Surface
8.59
0.50
0.30
89,000
45,125.00 156.00
8.51
Crop 1
01/29/2019
Gallons
39,000
1.60
18.28
0.14
2.60
Tar River Regional WWTP
Moist
0
Surface
10.30
0.50
0.30
89,000
45,125.00 156.00
10.22
Crop 1
02/07/2019
Gallons
45,500
1.60
18.28
0.17
3.04
Tar River Regional WWTP
Moist
0
Surface
12.02
0.50
0.30
89,000
45,125.00 156.00
11.92
Crop 1
02/09/2019
Gallons
130,000
1.60
18.28
0.47
8.67
Tar River Regional WWTP
Moist
0
Surface
34.34
0.50
0.30
89,000
45,125.00 156.00
34.05
Crop 1
07/12/2019
Gallons
28,000
0.96
18.28
0.06
1.12
Tar River WTP
Dry
0
Surface
0.23
0.50
0
19,063
1,740.00 409.00
0.16
Crop 1
Total Volume Applied
398,500
Total Dry Tons 32.54
Sum Total P 113.43
Total 111.86
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.127
0.013
3.272
0.260
0.004
0.080
0.253
0.127
3.037
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.392
0.194
33.350
3.122
0.059
0.867
4.772
0.330
37.452
Cumulative Total
0.519
0.207
36.622
3.382
0.064
0.947
5.025
0.457
40.490
N/A
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
��py *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
�WX �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Common Bermudagrass Hay
Facility Name City of Rocky Mount Field Name 4 SoilSeries Wagram Crop 1 Pan 192
LandOwner City of Rocky Mount Acres Permited 42.99 Soil Abbrevation: WaB Crop 2 Annual Ryegrass - Hay
Operator Joel Boseman Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
02/02/2019
Gallons
52,000
1.60
42.99
0.08
3.47
Tar River Regional WWTP
Moist
0
Surface
5.84
0.50
0.30
89,000
45,125.00 156.00
5.79 Crop 2
04/17/2019
Gallons
6,500
2.80
42.99
0.02
0.76
Tar River Regional WWTP
Dry
0
Surface
1.01
0.50
0.30
57,393
26,464.00 129.00
0.80
Crop 1
04/18/2019
Gallons
6,500
2.80
42.99
0.02
0.76
Tar River Regional WWTP
Dry
0
Surface
1.01
0.50
0.30
57,393
26,464.00 129.00
0.80
Crop 1
04/22/2019
Gallons
6,500
2.80
42.99
0.02
0.76
Tar River Regional WWTP
Dry
0
Surface
1.01
0.50
0.30
57,393
26,464.00 129.00
0.80
Crop 1
04/23/2019
Gallons
6,500
2.80
42.99
0.02
0.76
Tar River Regional WWTP
Dry
0
Surface
1.01
0.50
0.30
57,393
26,464.00 129.00
0.80
Crop 1
05/18/2019
Gallons
58,500
3.03
42.99
0.17
7.39
Tar River Regional WWTP
Dry
0
Surface
9.45
0.50
0.30
57,558
29,142.00 142.00
7.99
Crop 1
05/20/2019
Gallons
65,000
3.03
42.99
0.19
8.21
Tar River Regional WWTP
Dry
0
Surface
10.50
0.50
0.30
57,558
29,142.00 142.00
8.88
Crop 1
05/21/2019
Gallons
39,000
3.03
42.99
0.11
4.93
Tar River Regional WWTP
Dry
0
Surface
6.30
0.50
0.30
57,558
29,142.00 142.00
5.33
Crop
05/22/2019
Gallons
39,000
3.03
42.99
0.11
4.93
Tar River Regional WWTP
Dry
0
Surface
6.30
0.50
0.30
57,558
29,142.00 142.00
5.33
Crop 1
05/23/2019
Gallons
58,500
3.03
42.99
0.17
7.39
Tar River Regional WWTP
Dry
0
Surface
9.45
0.50
0.30
57,558
29,142.00 142.00
7.99
Crop 1
05/24/2019
Gallons
39,000
3.03
42.99
0.11
4.93
Tar River Regional WWTP
Dry
0
Surface
6.30
0.50
0.30
57,558
29,142.00 142.00
5.33
Crop 1
05/28/2019
Gallons
58,500
3.03
42.99
0.17
7.39
Tar River Regional WWTP
Dry
0
Surface
9.45
0.50
0.30
57,558
29,142.00 142.00
7.99
Crop 1
06/27/2019
Gallons
91,000
3.00
42.99
0.26
11.38
Tar River Regional WWTP
Dry
0
Surface
15.68
0.50
0.30
58,967
38,667.00 196.00
13.57
Crop 1
06/28/2019
Gallons
84,500
3.00
42.99
0.25
10.57
Tar River Regional WWTP
Dry
0
Surface
14.56
0.50
0.30
58,967
38,667.00 196.00
12.60
Crop 1
07/01/2019
Gallons
19,500
3.20
42.99
0.06
2.60
Tar River Regional WWTP
Dry
0
Surface
3.54
0.50
0.30
51,781
33,656.00 180.00
2.72
Crop 1
07/02/2019
Gallons
32,500
3.20
42.99
0.10
4.34
Tar River Regional WWTP
Dry
0
Surface
5.91
0.50
0.30
51,781
33,656.00 180.00
4.53
Crop 1
07/02/2019
Gallons
21,000
0.96
42.99
0.02
0.84
Tar River WTP
Dry
0
Surface
0.07
0.50
0
19,063
1,740.00 409.00
0.05
Crop 1
07/03/2019
Gallons
35,000
0.96
42.99
0.03
1.40
Tar River WTP
Dry
0
Surface
0.12
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
07/03/2019
Gallons
32,500
3.20
42.99
0.10
4.34
Tar River Regional WWTP
Dry
0
Surface
5.91
0.50
0.30
51,781
33,656.00 180.00
4.53
Crop 1
07/04/2019
Gallons
32,500
3.20
42.99
0.10
4.34
Tar River Regional WWTP
Dry
0
Surface
5.91
0.50
0.30
51,781
33,656.00 180.00
4.53
Crop 1
07/05/2019
Gallons
35,000
0.96
42.99
0.03
1.40
Tar River WTP
Dry
0
Surface
0.12
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
07/08/2019
Gallons
32,500
3.20
42.99
0.10
4.34
Tar River Regional WWTP
Dry
0
Surface
5.91
0.50
0.30
51,781
33,656.00 180.00
4.53
Crop 1
07/09/2019
Gallons
6,500
3.20
42.99
0.02
0.87
Tar River Regional WWTP
Dry
0
Surface
1.18
0.50
0.30
51,781
33,656.00 180.00
0.91
Crop 1
07/11/2019
Gallons
65,000
3.00
42.99
0.19
8.13
Tar River Regional WWTP
Dry
0
Surface
11.51
0.50
0.30
56,067
23,733.00 87.00
8.19
Crop 1
07/16/2019
Gallons
32,500
3.00
42.99
0.09
4.07
Tar River Regional WWTP
Dry
0
Surface
5.76
0.50
0.30
56,067
23,733.00 87.00
4.10
Crop 1
07/17/2019
Gallons
162,500
3.00
42.99
0.47
20.33
Tar River Regional WWTP
Dry
0
Surface
28.78
0.50
0.30
56,067
23,733.00 87.00
20.48
Crop 1
07/29/2019
Gallons
42,000
0.96
42.99
0.04
1.68
Tar River WTP
Dry
0
Surface
0.15
0.50
0
19,063
1,740.00 409.00
0.10
Crop 1
08/28/2019
Gallons
45,500
3.00
42.99
0.13
5.69
Tar River Regional WWTP
Dry
0
Surface
8.06
0.50
0.30
56,067
23,733.00 87.00
5.73
Crop 1
08/29/2019
Gallons
32,500
3.00
42.99
0.09
4.07
Tar River Regional WWTP
Dry
0
Surface
5.76
0.50
0.30
56,067
23,733.00 87.00
4.10
Crop 1
09/19/2019
Gallons
35,000
0.96
42.99
0.03
1.40
Tar River WTP
Dry
0
Surface
0.12
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
09/20/2019 Gallons
28,000 0.96
42.99
0.03
1.12
Tar River WTP
Dry
0 Surface
0.10
0.50
0
19,063
1,740.00 409.00
0.07
Crop 1
09/23/2019 Gallons
28,000 0.96
42.99
0.03
1.12
Tar River WTP
Dry
0 Surface
0.10
0.50
0
19,063
1,740.00 409.00
0.07
Crop 1
09/24/2019 Gallons
104,000 2.90
42.99
0.29
12.58 Tar River Regional WWTP
Dry
0 Surface
17.82
0.50
0.30
70,069
23,103.00 185.00
15.11
Crop 1
09/24/2019 Gallons
28,000 0.96
42.99
0.03
1.12
Tar River WTP
Dry
0 Surface
0.10
0.50
0
19,063
1,740.00 409.00
0.07
Crop 1
09/26/2019 Gallons
28,000 0.96
42.99
0.03
1.12
Tar River WTP
Dry
0 Surface
0.10
0.50
0
19,063
1,740.00 409.00
0.07
Crop 1
Total Volume Applied
1,489,000
Total Dry Tons
160.52
Sum Total P
204.92
Total
158.31
5.79 Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.220 0.022
4.208
0.363 0.004
0.126
0.400
0.220
4.320
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.481 0.291
43.251
4.507 0.071
1.290
6.241
0.355
39.823
Cumulative Total
0.701 0.313
47.458
4.870 0.075
1.416
6.642
0.575
44.144
1.5 T/Ac.
12/5/19
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
uvR u+�d 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Pasture
Facility Name City of Rocky Mount Field Name 5 SoilSeries Norfolk Crop 1 Pan 158
LandOwner City of Rocky Mount Acres Permited 69.68 Soil Abbrevation: NoB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
01/07/2019
Gallons
32,500
2.90
69.68
0.06
3.93
Tar River Regional WWTP
Moist
0
Surface
3.31
0.50
0.30
72,414
34,690.00 105.00
3.25
Crop 1
01/08/2019
Gallons
39,000
2.90
69.68
0.07
4.72
Tar River Regional WWTP
Moist
0
Surface
3.97
0.50
0.30
72,414
34,690.00 105.00
3.89
Crop 1
01/09/2019
Gallons
52,000
2.90
69.68
0.09
6.29
Tar River Regional WWTP
Moist
0
Surface
5.30
0.50
0.30
72,414
34,690.00 105.00
5.19
Crop 1
01/10/2019
Gallons
45,500
2.90
69.68
0.08
5.50
Tar River Regional WWTP
Moist
0
Surface
4.63
0.50
0.30
72,414
34,690.00 105.00
4.54
Crop 1
01/17/2019
Gallons
52,000
2.90
69.68
0.09
6.29
Tar River Regional WWTP
Moist
0
Surface
5.30
0.50
0.30
72,414
34,690.00 105.00
5.19
Crop 1
01/28/2019
Gallons
26,000
1.60
69.68
0.02
1.73
Tar River Regional WWTP
Moist
0
Surface
1.80
0.50
0.30
89,000
45,125.00 156.00
1.79
Crop 1
02/01/2019
Gallons
32,500
1.60
69.68
0.03
2.17
Tar River Regional WWTP
Moist
0
Surface
2.25
0.50
0.30
89,000
45,125.00 156.00
2.23
Crop 1
02/06/2019
Gallons
39,000
1.60
69.68
0.04
2.60
Tar River Regional WWTP
Moist
0
Surface
2.70
0.50
0.30
89,000
45,125.00 156.00
2.68
Crop 1
02/26/2019
Gallons
91,000
1.60
69.68
0.09
6.07
Tar River Regional WWTP
Moist
0
Surface
6.31
0.50
0.30
89,000
45,125.00 156.00
6.25
Crop 1
02/28/2019
Gallons
26,000
1.60
69.68
0.02
1.73
Tar River Regional WWTP
Moist
0
Surface
1.80
0.50
0.30
89,000
45,125.00 156.00
1.79
Crop 1
04/23/2019
Gallons
32,500
2.80
69.68
0.05
3.79
Tar River Regional WWTP
Dry
0
Surface
3.12
0.50
0.30
57,393
26,464.00 129.00
2.47
Crop 1
04/24/2019
Gallons
45,500
2.80
69.68
0.08
5.31
Tar River Regional WWTP
Dry
0
Surface
4.37
0.50
0.30
57,393
26,464.00 129.00
3.45
Crop 1
04/25/2019
Gallons
45,500
2.80
69.68
0.08
5.31
Tar River Regional WWTP
Dry
0
Surface
4.37
0.50
0.30
57,393
26,464.00 129.00
3.45
Crop 1
05/13/2019
Gallons
42,000
0.43
69.68
0.01
0.75
Sunset Ave WTP
Dry
0
Surface
0.52
0.50
0
36,977
2,112.00 913.95
0.04
Crop 1
05/15/2019
Gallons
63,000
0.43
69.68
0.02
1.13
Sunset Ave WTP
Dry
0
Surface
0.78
0.50
0
36,977
2,112.00 913.95
0.06
Crop 1
05/16/2019
Gallons
63,000
0.43
69.68
0.02
1.13
Sunset Ave WTP
Dry
0
Surface
0.78
0.50
0
36,977
2,112.00 913.95
0.06
Crop 1
05/17/2019
Gallons
49,000
0.43
69.68
0.01
0.88
Sunset Ave WTP
Dry
0
Surface
0.60
0.50
0
36,977
2,112.00 913.95
0.05
Crop 1
05/18/2019
Gallons
70,000
0.43
69.68
0.02
1.26
Sunset Ave WTP
Dry
0
Surface
0.86
0.50
0
36,977
2,112.00 913.95
0.07
Crop 1
05/20/2019
Gallons
42,000
1.30
69.68
0.03
2.28
Tar River WTP
Dry
0
Surface
0.40
0.50
0
19,154
243.00 300.77
0.03
Crop 1
05/21/2019
Gallons
35,000
1.30
69.68
0.03
1.90
Tar River WTP
Dry
0
Surface
0.34
0.50
0
19,154
243.00 300.77
0.02
Crop 1
05/23/2019
Gallons
28,000
1.30
69.68
0.02
1.52
Tar River WTP
Dry
0
Surface
0.27
0.50
0
19,154
243.00 300.77
0.02
Crop 1
07/08/2019
Gallons
56,000
0.96
69.68
0.03
2.24
Tar River WTP
Dry
0
Surface
0.12
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
07/09/2019
Gallons
56,000
0.96
69.68
0.03
2.24
Tar River WTP
Dry
0
Surface
0.12
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
07/31/2019
Gallons
28,000
0.96
69.68
0.02
1.12
Tar River WTP
Dry
0
Surface
0.06
0.50
0
19,063
1,740.00 409.00
0.04
Crop 1
09/11/2019
Gallons
45,500
2.90
69.68
0.08
5.50
Tar River Regional WWTP
Dry
0
Surface
4.81
0.50
0.30
70,069
23,103.00 185.00
4.08
Crop 1
09/12/2019
Gallons
52,000
2.90
69.68
0.09
6.29
Tar River Regional WWTP
Dry
0
Surface
5.50
0.50
0.30
70,069
23,103.00 185.00
4.66
Crop 1
09/27/2019
Gallons
28,000
0.96
69.68
0.02
1.12
Tar River WTP
Dry
0
Surface
0.06
0.50
0
19,063
1,740.00 409.00
0.04
Crop 1
09/30/2019
Gallons
35,000
0.96
69.68
0.02
1.40
Tar River WTP
Dry
0
Surface
0.08
0.50
0
19,063
1,740.00 409.00
0.05
Crop 1

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Total Volume Applied
1,251,500
Total Dry Tons 86.21
Sum Total P 64.52
Total 55.58
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.083 0.014
1.508
0.145
0.002
0.051
0.181
0.083
1.427
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.559 0.360
55.866
5.769
0.116
1.501
8.725
0.416
47.622
Cumulative Total
0.641 0.375
57.373
5.913
0.118
1.552
8.905
0.499
49.048
N/A
Permitted CPLR
36 34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
t_- *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
�.iCYt 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Common Bermudagrass Hay
Facility Name City of Rocky Mount Field Name 6 SoilSeries Norfolk Crop 1 Pan 225
LandOwner City of Rocky Mount Acres Permited 33.89 Soil Abbrevation: NoB Crop 2 Annual Ryegrass - Hay
Operator Joel Boseman Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN
Crop
04/29/2019
Gallons
45,500
2.80
33.89
0.16
5.31
Tar River Regional WWTP
Dry
0
Surface
8.98
0.50
0.30
57,393
26,464.00 129.00
7.10
Crop 1
04/30/2019
Gallons
45,500
2.80
33.89
0.16
5.31
Tar River Regional WWTP
Dry
0
Surface
8.98
0.50
0.30
57,393
26,464.00 129.00
7.10
Crop 1
05/03/2019
Gallons
45,500
3.03
33.89
0.17
5.75
Tar River Regional WWTP
Dry
0
Surface
9.33
0.50
0.30
57,558
29,142.00 142.00
7.88
Crop 1
05/07/2019
Gallons
52,000
3.03
33.89
0.19
6.57
Tar River Regional WWTP
Dry
0
Surface
10.66
0.50
0.30
57,558
29,142.00 142.00
9.01
Crop 1
05/07/2019
Gallons
56,000
1.30
33.89
0.09
3.04
Tar River WTP
Dry
0
Surface
1.11
0.50
0
19,154
243.00 300.77
0.08
Crop 1
05/08/2019
Gallons
56,000
1.30
33.89
0.09
3.04
Tar River WTP
Dry
0
Surface
1.11
0.50
0
19,154
243.00 300.77
0.08
Crop 1
05/08/2019
Gallons
52,000
3.03
33.89
0.19
6.57
Tar River Regional WWTP
Dry
0
Surface
10.66
0.50
0.30
57,558
29,142.00 142.00
9.01
Crop 1
05/09/2019
Gallons
56,000
1.30
33.89
0.09
3.04
Tar River WTP
Dry
0
Surface
1.11
0.50
0
19,154
243.00 300.77
0.08
Crop 1
05/09/2019
Gallons
52,000
3.03
33.89
0.19
6.57
Tar River Regional WWTP
Dry
0
Surface
10.66
0.50
0.30
57,558
29,142.00 142.00
9.01
Crop 1
05/10/2019
Gallons
49,000
1.30
33.89
0.08
2.66
Tar River WTP
Dry
0
Surface
0.97
0.50
0
19,154
243.00 300.77
0.07
Crop 1
05/10/2019
Gallons
71,500
3.03
33.89
0.27
9.03
Tar River Regional WWTP
Dry
0
Surface
14.66
0.50
0.30
57,558
29,142.00 142.00
12.39
Crop 1
05/15/2019
Gallons
6,500
3.03
33.89
0.02
0.82
Tar River Regional WWTP
Dry
0
Surface
1.33
0.50
0.30
57,558
29,142.00 142.00
1.13
Crop 1
05/16/2019
Gallons
32,500
3.03
33.89
0.12
4.11
Tar River Regional WWTP
Dry
0
Surface
6.66
0.50
0.30
57,558
29,142.00 142.00
5.63
Crop 1
05/17/2019
Gallons
26,000
3.03
33.89
0.10
3.29
Tar River Regional WWTP
Dry
0
Surface
5.33
0.50
0.30
57,558
29,142.00 142.00
4.51
Crop 1
07/10/2019
Gallons
56,000
0.96
33.89
0.07
2.24
Tar River WTP
Dry
0
Surface
0.25
0.50
0
19,063
1,740.00 409.00
0.17
Crop 1
07/18/2019
Gallons
325,000
3.00
33.89
1.20
40.66
Tar River Regional WWTP
Dry
0
Surface
73.02
0.50
0.30
56,067
23,733.00 87.00
51.96
Crop 1
07/22/2019
Gallons
45,500
3.00
33.89
0.17
5.69
Tar River Regional WWTP
Dry
0
Surface
10.22
0.50
0.30
56,067
23,733.00 87.00
7.27
Crop 1
08/30/2019
Gallons
97,500
2.90
33.89
0.35
11.79
Tar River Regional WWTP
Dry
0
Surface
21.19
0.50
0.30
70,069
23,103.00 185.00
17.97
Crop 1
09/12/2019
Gallons
28,000
0.96
33.89
0.03
1.12
Tar River WTP
Dry
0
Surface
0.13
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
09/13/2019
Gallons
28,000
0.96
33.89
0.03
1.12
Tar River WTP
Dry
0
Surface
0.13
0.50
0
19,063
1,740.00 409.00
0.08
Crop 1
09/13/2019
Gallons
52,000
2.90
33.89
0.19
6.29
Tar River Regional WWTP
Dry
0
Surface
11.30
0.50
0.30
70,069
23,103.00 185.00
9.58
Crop 1
09/16/2019
Gallons
35,000
0.96
33.89
0.04
1.40
Tar River WTP
Dry
0
Surface
0.16
0.50
0
19,063
1,740.00 409.00
0.11
Crop 1
09/16/2019
Gallons
45,500
2.90
33.89
0.16
5.50
Tar River Regional WWTP
Dry
0
Surface
9.89
0.50
0.30
70,069
23,103.00 185.00
8.39
Crop 1
09/17/2019
Gallons
35,000
0.96
33.89
0.04
1.40
Tar River WTP
Dry
0
Surface
0.16
0.50
0
19,063
1,740.00 409.00
0.11
Crop 1
09/17/2019
Gallons
52,000
2.90
33.89
0.19
6.29
Tar River Regional WWTP
Dry
0
Surface
11.30
0.50
0.30
70,069
23,103.00 185.00
9.58
Crop 1
09/18/2019
Gallons
42,000
0.96
33.89
0.05
1.68
Tar River WTP
Dry
0
Surface
0.19
0.50
0
19,063
1,740.00 409.00
0.13
Crop 1
09/18/2019
Gallons
39,000
2.90
33.89
0.14
4.72
Tar River Regional WWTP
Dry
0
Surface
8.47
0.50
0.30
70,069
23,103.00 185.00
7.19
Crop 1
10/22/2019
Gallons
123,500
3.06
33.89
0.46
15.76
Tar River Regional WWTP
Dry
0
Surface
23.53
0.50
0.30
42,800
6,080.00 327.00
13.38
Crop 2
10/29/2019
Gallons
28,000
2.31
33.89
0.08
2.70
Sunset Ave WTP
Dry
0
Surface
0.12
0.50
0
4,762
100.00 2.25
0.01
Crop 2
10/30/2019
Gallons
28,000
2.31
33.89
0.08
2.70
Sunset Ave WTP
Dry
0
Surface
0.12
0.50
0
4,762
100.00 2.25
0.01
Crop 2

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Total Volume Applied
1,706,000
Total Dry Tons 176.15
Sum Total P 261.70
Total 185.67
13.39 Total
Reported in Gallons
Arsenic
Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.255
0.039
5.068
0.480
0.005
0.147
0.611
0.256
4.771
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.420
0.201
38.587
3.752
0.054
1.113
4.858
0.372
46.550
Cumulative Total
0.676
0.240
43.656
4.232
0.059
1.260
5.469
0.628
51.321
2.5 T/Ac. 12/16/19
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
t_- *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
�.iCYt 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Common Bermudagrass Hay
Facility Name City of Rocky Mount Field Name 7 SoilSeries Norfolk Crop 1 Pan 225
LandOwner City of Rocky Mount Acres Permited 23.90 Soil Abbrevation: NoB Crop 2 Annual Ryegrass - Hay
Operator Joel Boseman Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN
Crop
06/04/2019
Gallons
39,000
3.00
23.90
0.20
4.88
Tar River Regional WWTP
Dry
0 Surface
11.39
0.50
0.30
62,633
39,200.00 249.00
10.97
Crop 1
06/05/2019
Gallons
39,000
3.00
23.90
0.20
4.88
Tar River Regional WWTP
Dry
0 Surface
11.39
0.50
0.30
62,633
39,200.00 249.00
10.97
Crop 1
06/17/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.10
0.50
0.30
58,967
38,667.00 196.00
12.20
Crop 1
06/18/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.10
0.50
0.30
58,967
38,667.00 196.00
12.20
Crop 1
06/19/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.10
0.50
0.30
58,967
38,667.00 196.00
12.20
Crop 1
06/24/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.10
0.50
0.30
58,967
38,667.00 196.00
12.20
Crop 1
06/25/2019
Gallons
78,000
3.00
23.90
0.41
9.76
Tar River Regional WWTP
Dry
0 Surface
24.17
0.50
0.30
58,967
38,667.00 196.00
20.92
Crop 1
07/22/2019
Gallons
28,000
0.96
23.90
0.05
1.12
Tar River WTP
Dry
0 Surface
0.18
0.50
0
19,063
1,740.00 409.00
0.12
Crop 1
07/25/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.50
0.50
0.30
56,067
23,733.00 87.00
10.31
Crop 1
07/25/2019
Gallons
42,000
0.96
23.90
0.07
1.68
Tar River WTP
Dry
0 Surface
0.27
0.50
0
19,063
1,740.00 409.00
0.18
Crop 1
07/26/2019
Gallons
32,500
3.00
23.90
0.17
4.07
Tar River Regional WWTP
Dry
0 Surface
10.35
0.50
0.30
56,067
23,733.00 87.00
7.37
Crop 1
07/30/2019
Gallons
32,500
3.00
23.90
0.17
4.07
Tar River Regional WWTP
Dry
0 Surface
10.35
0.50
0.30
56,067
23,733.00 87.00
7.37
Crop 1
07/31/2019
Gallons
32,500
3.00
23.90
0.17
4.07
Tar River Regional WWTP
Dry
0 Surface
10.35
0.50
0.30
56,067
23,733.00 87.00
7.37
Crop 1
08/19/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.50
0.50
0.30
56,067
23,733.00 87.00
10.31
Crop 1
08/20/2019
Gallons
52,000
3.00
23.90
0.27
6.51
Tar River Regional WWTP
Dry
0 Surface
16.57
0.50
0.30
56,067
23,733.00 87.00
11.79
Crop 1
08/21/2019
Gallons
71,500
3.00
23.90
0.37
8.94
Tar River Regional WWTP
Dry
0 Surface
22.78
0.50
0.30
56,067
23,733.00 87.00
16.21
Crop 1
08/23/2019
Gallons
45,500
3.00
23.90
0.24
5.69
Tar River Regional WWTP
Dry
0 Surface
14.50
0.50
0.30
56,067
23,733.00 87.00
10.31
Crop 1
08/29/2019
Gallons
26,000
3.00
23.90
0.14
3.25
Tar River Regional WWTP
Dry
0 Surface
8.28
0.50
0.30
56,067
23,733.00 87.00
5.89
Crop 1
09/25/2019
Gallons
39,000
2.90
23.90
0.20
4.72
Tar River Regional WWTP
Dry
0 Surface
12.02
0.50
0.30
70,069
23,103.00 185.00
10.19
Crop 1
10/29/2019
Gallons
26,000
3.06
23.90
0.14
3.32
Tar River Regional WWTP
Dry
0 Surface
7.02
0.50
0.30
42,800
6,080.00 327.00
3.99
Crop 2
12/30/2019
Gallons
70,000
0.72
23.90
0.09
2.10
Tar River WTP
Moist
0 Surface
0.19
0.50
0
13,875
3,097.00 8.06
0.27
Crop 2
Total Volume Applied
926,500
Total Dry Tons
103.20
Sum Total P
245.20
Total
189.11
4.27
Total
Reported in
Gallons Arsenic
Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current
Year
0.241
0.024
4.919
0.403 0.005
0.141
0.427
0.241
5.051
Lime (T/Ac.) Date
Obs./Ac.)
Obs./Ac.)
Prior Year
0.228
0.172
27.552
2.807 0.048
0.780
3.666
0.265
33.824
Cumulative
Total
0.469
0.197
32.471
3.210 0.054
0.921
4.093
0.507
38.874
3.0 T/Ac.
12/13/19
Permitted CPLR
36
34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
`'� *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
'
'+6R �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
C:._-.....__..._CT --A A --I.'-- Tl..... ****/ n T D n-11..f....f T D..f,.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Perm itNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Pine
Facility Name City of Rocky Mount Field Name 8 SoilSeries Norfolk Crop 1 Pan 75
LandOwner City of Rocky Mount Acres Permuted 4.38 Soil Abbrevation: NoC Crop 2
Operator Joel Boseman Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate Crop 1 Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia -Nitrite PAN PAN Crop
07/15/2019 Gallons 28,000 0.96 4.38 0.26 1.12 Tar River WTP Dry 0 Surface 0.97 0.50 0 19,063 1,740.00 409.00 0.65 Crop 1
Total Volume Applied
28,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.032
0.003
Prior Year
0.163
0.093
Cumulative Total
0.195
0.096
Permitted CPLR
36
34
Total Dry Tons 1.12
Copper Chromium
Lead
0.016
0.016
6.081
0.944
6.097
0.960
1338
267
Mercury Molybdenum
0.000 0.016
0.036 0.411
0.036 0.427
15
Sum Total P 0.97
Nickel
Selenium
Zinc
0.047
0.032
0.032
1.403
0.092
9.048
1.451
0.124
9.080
374
89
2498
Total 0.65 Total
Crop 1 Crop 2
PAN PAN
(lbs./Ac.) (lbs./Ac.)
Lime (T/Ac.) Date
2.5 T/Ac. 12/16/19
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
6R u l 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Perm itNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Pine
Facility Name City of Rocky Mount Field Name 9A SoilSeries Dogue-P Crop 1 Pan 75
LandOwner City of Rocky Mount Acres Permuted 4.38 Soil Abbrevation: DgA Crop 2
Operator Joel Boseman Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate Crop 1 Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia -Nitrite PAN PAN Crop
07/16/2019 Gallons 42,000 0.96 4.38 0.38 1.68 Tar River WTP Dry 0 Surface 1.46 0.50 0 19,063 1,740.00 409.00 0.98 Crop 1
Total Volume Applied
42,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.048
0.005
Prior Year
0.073
0.035
Cumulative Total
0.122
0.040
Permitted CPLR
36
34
Total Dry Tons 1.68
Copper Chromium
Lead
0.024
0.024
9.145
0.771
9.169
0.795
1338
267
Mercury Molybdenum
0.000 0.024
0.002 0.539
0.002 0.563
15
Sum Total P 1.46
Nickel
Selenium
Zinc
0.071
0.048
0.048
1.212
0.064
8.653
1.283
0.113
8.701
374
89
2498
Total 0.98 Total
Crop 1 Crop 2
PAN PAN
(lbs./Ac.) (lbs./Ac.)
Lime (T/Ac.) Date
2.0 T/Ac. 12/17/19
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
6R ul 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0005568 Site# 25 County Edgecombe Crop 1 Fescue Hay
Facility Name City of Rocky Mount Field Name 9B SoilSeries Dogue-CP Crop 1 Pan 194
LandOwner City of Rocky Mount Acres Permuted 13.83 Soil Abbrevation: DgA Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement Applied
% Solids
Used DT/Ac. Tons Source
Condition Precip
Method
P
Volatilization Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
09/26/2019
Gallons 136,500
2.90
13.83 1.19
16.51 Tar River Regional WWTP
Dry 0
Surface
72.68
0.50 0.30
70,069
23,103.00 185.00
61.65
Crop 1
09/27/2019
Gallons 78,000
2.90
13.83 0.68
9.43 Tar River Regional WWTP
Dry 0
Surface
41.53
0.50 0.30
70,069
23,103.00 185.00
35.23
Crop 1
10/23/2019
Gallons 130,000
3.06
13.83 1.20
16.59 Tar River Regional WWTP
Dry 0
Surface
60.69
0.50 0.30
42,800
6,080.00 327.00
34.50
Crop 1
Total Volume Applied
344,500
Reported in Gallons
Arsenic Cadmium
Current Year
0.101
0.013
Prior Year
0.213
0.096
Cumulative Total
0.314
0.109
Permitted CPLR
36
34
Total Dry Tons 42.53
Copper Chromium
Lead
3.788
0.301
22.022
2.092
25.810
2.393
1338
267
Mercury Molybdenum
0.003 0.074
0.024 0.684
0.027 0.758
15
Sum Total P 174.91
Nickel
Selenium
Zinc
0.304
0.101
2.352
1.883
0.215
27.699
2.187
0.316
30.051
374
89
2498
Total 131.38
Total
Crop 1
Crop 2
PAN
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
(lbs./Ac.)
1.0 T/Ac. 12/17/19
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
6R ul 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 41 County Edgecombe Crop 1 Wheat, Grain
Facility Name City of Rocky Mount Field Name 1 SoilSeries Norfolk Crop 1 Pan 125
LandOwner Creekside Properties Acres Permuted 56.70 Soil Abbrevation: NoA Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
02/04/2019
Gallons
65,000
1.60
56.70
0.08
4.34
Tar River Regional WW I?
Moist
0 Surface
5.54
0.50
0.30
89,000
45,125.00 156.00
5.49
Crop 1
02/05/2019
Gallons
91,000
1.60
56.70
0.11
6.07
Tar River Regional WWTP
Moist
0 Surface
7.75
0.50
0.30
89,000
45,125.00 156.00
7.68
Crop 1
02/05/2019
Gallons
56,000
6.70
56.70
0.28
15.65
Tar River WTP
Moist
0 Surface
0.39
0.50
0
3,687
48.00 59.55
0.05
Crop 1
02/06/2019
Gallons
45,500
1.60
56.70
0.05
3.04
Tar River Regional WWTP
Moist
0 Surface
3.88
0.50
0.30
89,000
45,125.00 156.00
3.84
Crop 1
02/07/2019
Gallons
58,500
1.60
56.70
0.07
3.90
Tar River Regional WWTP
Moist
0 Surface
4.98
0.50
0.30
89,000
45,125.00 156.00
4.94
Crop 1
02/15/2019
Gallons
21,000
5.50
56.70
0.08
4.82
Sunset Ave WTP
Moist
0 Surface
0.15
0.50
0
5,273
727.00 71.50
0.07
Crop 1
02/22/2019
Gallons
28,000
5.50
56.70
0.11
6.42
Sunset Ave WTP
Moist
0 Surface
0.20
0.50
0
5,273
727.00 71.50
0.10
Crop 1
02/28/2019
Gallons
35,000
6.70
56.70
0.17
9.78
Tar River WTP
Moist
0 Surface
0.24
0.50
0
3,687
48.00 59.55
0.03
Crop 1
02/28/2019
Gallons
58,500
1.60
56.70
0.07
3.90
Tar River Regional WWTP
Moist
0 Surface
4.98
0.50
0.30
89,000
45,125.00 156.00
4.94
Crop 1
03/01/2019
Gallons
13,000
2.80
56.70
0.03
1.52
Tar River Regional WWTP
Moist
0 Surface
1.53
0.50
0.30
57,393
26,464.00 129.00
1.21
Crop 1
03/01/2019
Gallons
56,000
6.70
56.70
0.28
15.65
Tar River WTP
Moist
0 Surface
0.39
0.50
0
3,687
48.00 59.55
0.05
Crop 1
03/05/2019
Gallons
58,500
2.80
56.70
0.12
6.83
Tar River Regional WWTP
Moist
0 Surface
6.90
0.50
0.30
57,393
26,464.00 129.00
5.45
Crop 1
03/06/2019
Gallons
58,500
2.80
56.70
0.12
6.83
Tar River Regional WWTP
Moist
0 Surface
6.90
0.50
0.30
57,393
26,464.00 129.00
5.45
Crop 1
03/07/2019
Gallons
71,500
2.80
56.70
0.15
8.35
Tar River Regional WWTP
Moist
0 Surface
8.43
0.50
0.30
57,393
26,464.00 129.00
6.67
Crop 1
03/08/2019
Gallons
104,000
2.80
56.70
0.21
12.14
Tar River Regional WWTP
Moist
0 Surface
12.27
0.50
0.30
57,393
26,464.00 129.00
9.70
Crop 1
03/11/2019
Gallons
97,500
2.80
56.70
0.20
11.38
Tar River Regional WWTP
Moist
0 Surface
11.50
0.50
0.30
57,393
26,464.00 129.00
9.09
Crop 1
03/13/2019
Gallons
104,000
2.80
56.70
0.21
12.14
Tar River Regional WWTP
Moist
0 Surface
12.27
0.50
0.30
57,393
26,464.00 129.00
9.70
Crop 1
03/14/2019
Gallons
78,000
2.80
56.70
0.16
9.11
Tar River Regional WWTP
Moist
0 Surface
9.20
0.50
0.30
57,393
26,464.00 129.00
7.27
Crop 1
Total Volume Applied
1,099,500
Total Dry Tons
141.86
Sum Total P
97.51
Total
81.74
Total
Reported in
Gallons Arsenic
Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current
Year
0.105 0.015
2.228
0.198 0.002
0.067
0.228
0.105
2.254
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.077 0.041
11.769
0.822 0.011
0.245
0.893
0.075
13.284
Cumulative
Total
0.182 0.056
13.996
1.020 0.013
0.312
1.121
0.180
15.538
1.0 T/Ac.
1 /8/20
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
+"R u 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 41 County Edgecombe Crop 1 Wheat, Grain
Facility Name City of Rocky Mount Field Name 2 SoilSeries Norfolk Crop 1 Pan 125
LandOwner Creekside Properties Acres Permuted 28.62 Soil Abbrevation: NoA Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
01/18/2019 Gallons
26,000
2.90
28.62
0.11
3.14
Tar RiverRegionalWWI?
Moist
0 Surface
6.45
0.50
0.30
72,414
34,690.00 105.00
6.32
Crop
01/19/2019 Gallons
71,500
2.90
28.62
0.30
8.65
Tar River Regional WWTP
Moist
0 Surface
17.73
0.50
0.30
72,414
34,690.00 105.00
17.38
Crop 1
01/23/2019 Gallons
19,500
1.60
28.62
0.05
1.30
Tar River Regional WWTP
Moist
0 Surface
3.29
0.50
0.30
89,000
45,125.00 156.00
3.26
Crop 1
01/29/2019 Gallons
19,500
1.60
28.62
0.05
1.30
Tar River Regional WWTP
Moist
0 Surface
3.29
0.50
0.30
89,000
45,125.00 156.00
3.26
Crop 1
02/06/2019 Gallons
63,000
6.70
28.62
0.62
17.60
Tar River WTP
Moist
0 Surface
0.86
0.50
0
3,687
48.00 59.55
0.10
Crop 1
02/25/2019 Gallons
45,500
1.60
28.62
0.11
3.04
Tar River Regional WWTP
Moist
0 Surface
7.68
0.50
0.30
89,000
45,125.00 156.00
7.61
Crop 1
02/26/2019 Gallons
65,000
1.60
28.62
0.15
4.34
Tar River Regional WWTP
Moist
0 Surface
10.97
0.50
0.30
89,000
45,125.00 156.00
10.87
Crop 1
02/26/2019 Gallons
35,000
6.70
28.62
0.34
9.78
Tar River WTP
Moist
0 Surface
0.48
0.50
0
3,687
48.00 59.55
0.06
Crop 1
02/27/2019 Gallons
28,000
6.70
28.62
0.27
7.82
Tar River WTP
Moist
0 Surface
0.38
0.50
0
3,687
48.00 59.55
0.05
Crop 1
03/15/2019 Gallons
65,000
2.80
28.62
0.27
7.59
Tar River Regional WWTP
Moist
0 Surface
15.19
0.50
0.30
57,393
26,464.00 129.00
12.01
Crop 1
Total Volume Applied
438,000
Total Dry Tons
64.56
Sum Total P
66.32
Total
60.93
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.081
0.014
1.739
0.167 0.002
0.050
0.199
0.081
1.662
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.106
0.049
12.388
0.982 0.011
0.277
1.217
0.099
14.102
Cumulative Total
0.187
0.063
14.127
1.148 0.013
0.327
1.416
0.180
15.764
1.5 T/Ac.
1 /9/20
Permitted CPLR
36
34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
IA�� �y *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
WII �4L 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Appfier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermutNumber WQ0005568 Site# 41 County Edgecombe Crop 1 Wheat, Grain
Facility Name City of Rocky Mount Field Name 3B SoilSeries Wagram Crop 1 Pan 91
LandOwner Creekside Properties Acres Permuted 11.85 Soil Abbrevation: WaB Crop 2
Operator Joel Boseman Crop 2 Pan
Volume
Acres
Dry
Soil
Application
Total
Nitrate Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN
Ammonia -Nitrite
PAN
PAN Crop
01/07/2019 Gallons
19,500 2.90
11.85
0.20
2.36
Tar River Regional WWTP
Moist
0 Surface
11.68
0.50
0.30
72,414
34,690.00 105.00
11.45
Crop 1
01/08/2019 Gallons
32,500 2.90
11.85
0.33
3.93
Tar River Regional WWTP
Moist
0 Surface
19.47
0.50
0.30
72,414
34,690.00 105.00
19.08
Crop 1
01/09/2019 Gallons
26,000 2.90
11.85
0.27
3.14
Tar River Regional WWTP
Moist
0 Surface
15.57
0.50
0.30
72,414
34,690.00 105.00
15.27
Crop 1
01/10/2019 Gallons
26,000 2.90
11.85
0.27
3.14
Tar River Regional WWTP
Moist
0 Surface
15.57
0.50
0.30
72,414
34,690.00 105.00
15.27
Crop 1
01/17/2019 Gallons
13,000 2.90
11.85
0.13
1.57
Tar River Regional WWTP
Moist
0 Surface
7.79
0.50
0.30
72,414
34,690.00 105.00
7.63
Crop 1
Total Volume Applied
117,000
Total Dry Tons
14.15
Sum Total P
70.08
Total
68.70
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.056 0.005
1.693
0.117 0.001
0.038
0.116
0.056
1.397
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.027 0.008
4.085
0.193 0.001
0.042
0.251
0.015
3.178
Cumulative Total
0.083 0.014
5.778
0.311 0.002
0.079
0.366
0.070
4.575
1.5 T/Ac.
1 /9/20
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
j� *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
T4 i 2-13-2020 aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

City of Rocky Mount
2019 Class B Annual Report
WQ Permit# WQ0005568
Pathogen & Vector Attraction Reduction Form
Tar River Regional WWTP
38% Volatile Solids Reduction
Aerobic Digestion

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Rocky Mount WQ Permit Number: WQ0005568
WWTP Name: Tar River Regional WWI'P NPEDS Number: NCO030317
Monitoring Period: 01/01/2019 to 03/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not .Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Aerobic Digestion
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T .1107): ,Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Darrell Highsmith, Chief Operator
Preparer Name and Title (type or print)
Signature of Preparer* Date
Jason smith V1'
Land Applier Name and Title (if applicable)(type or print)
-,� 2i20i2020
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 17, 2020

Volatile Reduction
(503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
18-Feb-20
Average Temperatures
Test date
Age #1
Age #2
Age #3
Age #4
VR #1
VR #2
VR #3 VR #4
Di . #1
DI . #2
Dig. #3
Dig. #4
1/1/2019
125.85
83.37
278.39
101.10
25.70
25.60
22.75
22.83
40.45
40.45
25.46
25.45
1/2/2019 126.85 84.37 279.39 102.10 48.08 15.22 26.91
1 /3/2019
127.85
79.72
280.39
103.10
25.51
22.91
40.45
25.49
1 /4/2019
128.85
74.17
281.39
104.10
49.88
11.39
30.77
25.34
22.88
40.45
25.48
25.14
`24.97
22.88
40.43
25.31
1 /5/2019 129.85 65.07 282.39 105.10
1 /6/2019
130.85
66.07
283.39
106.10
22.88
40.50
25.13
1/7/2019
131.85
67.07
284.39
107.10
46.87
11.13
30.43
24.61
22.80
40.00
25.05
1 /8/2019
132.85
68.07
285.39
108.10
24.29
22.78
24.98
1 /9/2019
133.85
69.07
286.39
109.10
50.21
14.88
35.76
23.93
22.70
24.90
1/10/2019
134.85
70.07
287.39
110.10
35.67
23.70
22.58
24.78
1 /11 /2019
135.85
71.07
288.39
111.10
49.11
12.73
23.66
22.62
24.78
1/12/2019
136.85
72.07
289.39
112.10
23.52
22.62
24.80
1/13/2019
137.85
73.07
290.39
113.10
23.42
22.62
24.86
23.24
22.64
24.93
1/14/2019
138.85
74.07
251.54
114.10
48.95
13.66
23.13
22.68
25.09
1 /15/2019
139.85
75.07
219.54
115.10
22.97
22.69
25.20
1/16/2019
140.85
76.07
201.40
116.10
51.54
15.80
22.85
22.56
25.20
1 /17/2019
141.85
77.07
169.37
117.10
22.77
22.54
25.20
1 /18/2019 142.85 78.07 156.21 118.10 50.82 14.48
1 /19/2019
143.85
79.07
147.42
119.10
22.60
22.54
25.21
1 /20/2019
144.85
80.07
148.42
120.10
22.47
22.54
25.23
1 /21 /2019
145.85
81.07
149.42
121.10
22.43
22.54
25.36
1 /22/2019
146.85
82.07
150.42
122.10
22.20
22.41
25.36
1 /23/2019
147.85
83.07
151.42
123.10
54.21
18.73
49.00
22.00
22.40
25.35
1 /24/2019
148.85
84.07
152.42
124.10
22.00
22.42
25.47
1 /25/2019
149.85
85.07
153.42
125.10
19.29
50.02
22.00
22.37
25.49
1 /26/2019
150.85
86.07
154.42
126.10
_
21.95
22.44
25.60
21.88
22.53
25.73
1 /27/2019
151.85
87.07
155.42
127.10
21.71
22.41
25.66
1 /28/2019 152.85 88.07 147.31 128.10 17.23 49.44
1 /29/2019
153.85
89.07
140.16
129.10
1 /30/2019
154.85
90.07
137.38
130.10
1 /31 /2019
155.85
91.07
138.38
131.10
Average 140.9 78.37 213.6 116.1
Minimum 125.8 65.07 137.4 101.1
49.96 15.37
46.87 11.13
21.58 22.32
25.60
50.85
21.43
22.21
25.48
21.43
22.15
25.48
39.87
23.227
22.588
40.39 25.262
26.91
21.430
22.15
40 24.780
I

Volatile Reduction
(503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
18-Feb-20
Test date
Age #1
Age #2
Age #3
Age #4 VR #1
VR #2
VR #3
VR #4
Dig. #1
Average Temperatures
DI . #2 Dig. #3 Dig. #4
2/1 /2019
2/2/2019
2/3/2019
2/4/2019
156.85
157.85
158.85
159.85
92.07
93.07
94.07
95.07
139.38
140.38
141.38
142.38
132.10
133.10
134.10
135.10
20.42
21.01
18.87
13.59
51.73
54.64
21.43
21.43
21.43
22.10
22.10
22.10
21.50
21.50
21.50
25.58
25.58
25.58
21.43 22.08 21.80
25.61
2/5/2019
2/6/2019
2/7/2019
2/8/2019
2/9/2019
2/10/2019
2/11/2019
2/12/2019
2/13/2019
2/14/2019
2/15/2019
2/16/2019
2/17/2019
2/18/2019
2/19/2019
2/20/2019
2/21 /2019
2/22/2019
2/23/2019
2/24/2019
2/25/2019
2/26/2019
2/27/2019
2/28/2019
160.85
161.85
162.85
163.85
164.85
165.85
166.85
167.85
168.85
169.85
170.85
138.19
119.99
100.91
93.56
75.22
70.95
66.77
60.51
61.51
62.51
63.51
64.51
65.51
96.07
97.07
98.07
99.07
100.07
101.07
102.07
103.07
104.07
105.07
106.07
107.07
108.07
109.07
110.07
111.07
112.07
113.07
114.07
115.07
116.07
117.07
118.07
119.07
143.38
144.38
145.38
146.38
147.38
148.38
149.38
150.38
151.38
152.38
153.38
154.38
155.38
156.38
157.38
158.38
159.38
160.38
161.38
162.38
163.38
164.38
165.38
166.38
136.10
137.10
138.10 _
139.10
140.10
141.10
142.10
143.10
144.10
146.52
147.52
148.52
149.52
150.52
151.52
152.52
153.52
154.52
155.52
156.52
157.52
158.52
159.52
160.52
20.97
21.03
22.58
22.96
22.41
23.71
22.28
24.94
24.92
25.28
12.35
10.93
13.29
9.10
8.21
9.03
8.09
9.82
10.96
13.53
55.60
55.76
61.69
58.46
57.24
59.12
60.69
62.46
61.26
62.16
21.42
21.28
22.03
21.92
21.73
22.03
25.71
25.81
21.28 21.96 22.36
25.98
21.28 22.00 22.65
26.06
21.13 21.90 22.65
26.02
21.13 21.90 22.65
26.02
20.99 21.80 22.74
26.03
20.80 21.75 22.73
25.93
20.78 21.74 22.76
26.00
20.78 21.74 22.80
26.01
20.78 21.78 22.93
26.22
20.83 21.78 22.93
26.28
20.82 21.75 22.93
26.34
20.93 21.75 22.88
21.28 21.77 22.88
21.06 21.68 22.87
26.38
26.62
26.59
21.06 21.72 22.95
26.79
21.06 21.76 23.04
26.97
20.90 21.71 23.04
26.97
20.68 _21.65 23.04
20.35 21.66 _23.13
20.50 21.73 23.20
20.40 21.70 23.16
20.40 21.70 23.15
26.97
27.14
27.32
27.27
27.25
Average
125.1
105.6
152.9
146.4
22.71
11.48
58.40
20.987
21.831
22.626
26.323
Minimum
60.51
92.07
139.4
132.1
20.42
8.090
51.73
20.350
21.65
21.5
25.58
1

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees Q 18-Feb-20
Test date
3/1 /2019
3/3/2019
3/6/2019
3/7/2019
3/8/2019
3/9/2019
3/10/2019
3/11 /2019
3/12/2019
3/13/2019
3/14/2019
3/15/2019
3/16/2019
3/17/2019
3/18/2019
3/19/2019
3/20/2019
3/21 /2019
3/24/2019
3/25/2019
3/26/2019
3/27/2019
3/28/2019
3/29/2019
3/30/2019
3/31 /2019
Average Temperatures
Age #1
Age #2
Age #3
Age #4
VR #1
VR #2
VR #3
VR #4
Dig. #1
Dig. #2
Dig. #3
Dig. #4
66.51
120.07
167.38
161.52
25.96
16.13
61.99
20.40
21.71
23.12
27.25
67.51
121.07
168.38
162.52
20.40
21.71
23.12
27.25
68.51
122.07
169.38
158.24
21.00
21.78
23.12
27.25
69.51
123.07
170.38
159.24
40.67
27.59
18.11
21.10
21.75
23.09
27.31
70.51
129.87
171.38
160.24
20.40
21.70
23.03
27.30
71.51
130.87
172.38
161.24
36.90
27.55
22.77
20.33
21.69
23.03
27.36
72.51
131.87
173.38
162.24
20.13
21.69
23.02
27.36
73.51
132.87
174.38
163.24
35.01
27.20
25.26
20.20
21.71
23.06
27.36
74.51
133.87
175.38
164.24
20.20
21.73
23.06
27.39
75.51
134.87
176.38
165.24
76.51
135.87
177.38
166.24
32.91
29.16
31.06
77.51
136.87
178.38
167.24
78.51
137.87
179.38
168.24
36.30
24.44
34.95
79.51
138.87
180.38
169.24
80.51
139.87
181.38
170.24
33.53
26.40
40.03
81.51
140.87
182.38
171.24
_
82.51
141.87
183.38
172.24
83.51
142.87
184.38
173.24
36.03
27.66
48.51
84.51
14 3.8 7
185.38
174.24
85.51
144.87
186.38
175.24
33.69
27.99
16.48
86.51
145.87
187.38
176.24
16.48
79.75
146.87
188.38
177.24
35.13
28.53
21.67
78.75
147.87
189.38
178.24
77.37
148.87
190.38
179.24
78.37
149.87
191.38
180.24
30.85
26.55
16.55
79.37
150.87
192.38
181.24
80.37
151.87
193.38
182.24
33.67
27.42
22.09
81.37
152.87
194.38
183.24
_
82.37
153.87
195.38
184.24
34.39
29.65
20.65
83.37
154.87
196.38
185.24
_
84.37
155.87
197.38
186.24
Average 77.81 140.1
Minimum 66.51 120.1
182.4 171.6 34.92 27.39
167.4 158.2 30.85 24.44
20.20
20.27
20.29
21.75
21.81
21.86
23.06
23.13
23.18
27.45
27.55
27.65
20.30
21.90
23.34
27.68
20.34
21.91
23.44
27.68
20.48
21.96
23.56
27.68
20.48
21.98
23.61
27.75
20.48
22.02
23.68
27.83
20.50
22.05
23.82
27.80
20.54
22.01
23.83
27.71
20.59
21.99 _
23.82
27.71
20.72
22.07
23.93
27.71
20.77
22.13
24.02
27.71
20.77
22.17
24.05
27.87
20.77
22.16
24.10
28.13
20.81
22.21
24.20
28.26
20.85
22.31
24.32
28.44
20.82
22.33
24.30
28.22
20.78 22.34 24.26 28.22
20.77 _
22.35
24.25
28.22
20.77
22.39
24.33
28.60
20.77
22.43
24.38
28.84
25.05 61.99 20.556 21.987 23.621 27.759
16.13 61.99 20.13 21.690 23.020 27.25
1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Rocky Mount WQ Permit Number: WQ0005568
WWTP Name: Tar River Regional WWTP NPEDS Number: NCO030317
Monitoring Period: 04/01/2019 to 06/30/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Aerobic Digestion
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
IAnalytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
�] requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Darrell Highsmith, Chief Operator
Preparer Name and Title (type or print)
a "Ll - I Q�*- - a
Signature of Preparer* I Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
11-1� &4L 2i2oi2o2o
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 17, 2020

Volatile Reduction
(503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
18-Feb-20
Average Temperatures
Test date
Age #1
Age #2
Age #3
Age #4
VR #1
VR #2
VR #3
VR #4
Dig. #1
Dig. #2
Di . #3
Dig. #4
4/1 /2019
85.37
156.87
198.38
187.24
34.22
28.92
21.08
20.85
22.59
24.58
29.26
4/2/2019
86.37
157.87
199.38
188.24
20.92
20.95
22.68
22.76
24.71
24.82
28.97
28.54
4/3/2019 87.37 158.87 187.05 189.24 36.33 30.21 21.85
4/4/2019
88.37
159.87
176.33
190.24
21.02
22.83
24.90
28.54
4/5/2019
89.37
160.87
166.93
191.24
51.99
19.00
21.57
21.10
22.93
24.96
28.54
4/6/2019
90.37
161.87
167.93
192.24
21.10
22.93
24.98
27.93
4/7/2019
91.37
162.87
168.93
193.24
21.10
22.96
25.00
26.70
4/8/2019
92.37
163.87
165.09
144.80
36.57
30.19
26.79
21.21
23.15
25.20
27.05
4/9/2019
93.37
164.87
166.09
145.80
21.31
23.34
25.38
27.40
4/10/2019
94.37
165.87
167.09
134.14
40.11
32.46
29.30
21.36
23.44
25.45
4/11/2019
95.37
166.87
168.09
117.18
41.71
21.40
23.49
25.44
4/12/2019
96.37
167.87
169.09
113.48
40.51
32.54
27.42
1.39
21.45
23.53
25.47
24.90
4/13/2019
97.37
168.87
170.09
102.27
21.47
23.64
25.58
24.90
4/14/2019
98.37
169.87
171.09
96.41
21.53
23.71
25.73
24.90
4/15/2019
99.37
170.87
172.09
88.60
33.57
31.26
8.93
21.58
23.82
25.82
23.30
4/16/2019
100.37
171.87
173.09
89.60
21.66
23.94
25.96
23.63
4/17/2019
101.37
172.87
174.09
90.60
33.39
35.86
8.27
21.70
24.08
26.46
25.18
4/18/2019
102.37
173.94
175.09
91.60
21.70
24.17
26.50
25.36
4/19/2019
103.37
174.94
176.09
87.43
21.70
24.17
26.50
25.36
4/20/2019
104.37
175.94
173.74
88.43
21.75
24.23
26.56
25.36
4/21 /2019
4/22/2019
4/23/2019
4/24/2019
4/25/2019
4/26/2019
4/27/2019
4/28/2019
4/29/2019
4/30/2019
105.37 176.94 162.89 89.43
106.37
177.94
163.89
90.43 `
107.37
178.94
164.89
91.43
108.37
179.94
165.89
92.43
109.37
180.94
166.89
93.43
110.37
181.94
167.89
94.43
111.37
182.94
168.89
95.43
112.37
183.94
169.89
96.43
113.37
184.94
170.89
97.43
114.37
185.94
171.89
98.43
Average 99.87 171.4
Minimum 85.37 156.9
172 122.0 40.21
162.9 87.43 34.22
34.62
29.70
34.00
37.09
32.57
35.67
35.86
40.41
31.82
19
29.46
21.08
21.81
24.30
26.64
25.36
14.41
21.87
24.29
26.51
25.52
20.68
21.93
21.94
21.94
24.40
24.40
24.45
26.46
26.33
26.31
25.46
25.35
25.39
17.53
21.94
22.01
22.06
22.11
22.09
24.57
24.63
24.73
24.94
25.08
26.36
26.35
26.35
26.42
26.47
25.64
25.64
25.64
25.89
26.07
19.40
12.94 21.552 23.806 25.807 26.135
1.39 20.850 22.590 24.58 23.3
1

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C) 18-Feb-20
Average Temperatures
Test date
Age #1
Age #2
Age #3
Age #4 VR #1
VR #2
VR #3
VR #4
Dig. #1
DI . #2
Dig. #3
Dig. #4
5/1/2019
115.37
186.94
172.89
99.43
35.97
42.63
21.00
22.14
25.23
26.54
26.22
5/2/2019
116.37
187.94
173.89
100.43
22.14
25.35
26.60
26.39
5/3/2019
117.37
188.94
174.89
101.43
36.68
36.22
21.18
22.14
25.47
26.68
26.50
5/4/2019
118.37
189.94
175.89
102.43
22.19
25.52
26.72
26.50
5/5/2019
119.37
190.94
176.89
103.43
22.24
25.57
26.74
26.50
5/6/2019
120.37
191.94
177.89
104.43
38.72
36.70
24.74
22.41
25.70
26.88
26.55
5/7/2019
121.37
192.94
178.89
105.43
22.61
25.86
27.04
26.59
5/8/2019
122.37
193.94
179.89
106.43
35.96
35.15
23.46
22.82
26.05
27.20
26.67
5/9/2019
155.54
194.94
180.89
107.43
22.82
26.16
27.29
26.79
5/10/2019
156.54
195.94
181.89
108.43
35.86
37.90
26.94
22.82
26.20
27.30
26.82
5/11/2019
157.54
194.26
182.89
109.43
22.87
26.23
27.28
26.82
5/12/2019
158.54
195.26
183.89
110.43
22.93
26.26
27.27
_
26.82
5/13/2019
159.54
196.26
184.89
111.43
36.81
39.24
27.05
23.11
26.46
27.34
26.92
5/14/2019
160.54
197.26
180.27
112.43
37.12
40.24
25.39
23.20
26.62
27.37
_
26.98
5/15/2019
161.54
198.26
175.96
113.43
37.33
40.23
27.18
23.24
26.76
27.41
27.02
5/16/2019
162.54
199.26
176.96
114.43
41.01
41.01
23.24
26.87
27.45
27.10
5/17/2019
163.54
200.26
177.96
115.43
36.31
26.93
23.24
27.02
27.49
27.20
5/18/2019
164.54
201.26
178.96
116.43
23.05
27.04
27.48
27.20
5/19/2019
165.54
202.26
179.96
117.43
22.73
27.05
27.48
27.20
5/20/2019
166.54
203.26
180.96
118.43
37.12
27.18
22.75
27.34
27.60
27.30
5/21 /2019
167.54
204.26
181.96
119.43
23.00
27.61
27.70
27.36
5/22/2019
168.54
205.26
182.96
120.43
38.02
27.96
27.73
27.75
27.51
5/23/2019
169.54
206.26
183.96
121.43
27.76
27.75
27.56
5/24/2019
170.54
207.26
184.96
122.43
34.71
25.49
27.90
27.75
27.64
5/25/2019
171.54
208.26
185.96
123.43
28.05
27.87
27.85
5/26/2019
172.54
209.26
186.96
124.43
28.16
27.92
27.99
5/27/2019
173.54
210.26
187.96
125.43
28.23
27.49
27.92
5/28/2019
174.54
211.26
188.96
135.81
28.44
27.49
28.12
_5/29/2019
175.54
212.26
189.96
136.81
37.57
26.22
28.54
27.49
28.22
5/30/2019
176.54
213.26
190.96
137.81
28.62
27.49
28.32
5/31 /2019
177.54
214.26
191.96
138.81
37.56
26.62
28.73
27.49
28.42
Average
154.2
200.1
181.7
115.6
37.12
Minimum
115.4
186.9
172.9
99.43
34.71
38.81 25.52 1 22.747 26.920 27.334 27.194
35.15 21 22.14 25.23 26.540 26.22
I

Volatile Reduction
(503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees Q
Average Temperatures
Test date
Age #1
Age #2
Age #3
Age #4 VR #1 VR #2
VR #3 VR #4
Dig. #1 Dig. #2 Dig. #3 Dig. #4
6/1 /2019
179.94
215.26
192.96
139.81
28.99 27.74 28.49
6/2/2019
180.94
216.26
193.96
140.81
29.14 27.89 28.62
6/3/2019
181.94
217.26
194.96
141.81 38.97
30.06
29.41 28.14 28.84
6/4/2019
6/5/2019
6/6/2019
6/7/2019
6/8/2019
6/9/2019
6/10/2019
6/11 /2019
6/12/2019
6/13/2019
6/14/2019
6/15/2019
6/16/2019
6/17/2019
6/18/2019
6/19/2019
6/20/2019
6/21 /2019
6/22/2019
6/23/2019
6/24/2019
6/25/2019
6/26/2019
6/27/2019
6/28/2019
6/29/2019
6/30/2019
182.94
218.26
195.96
142.81
183.94
219.26
196.96
143.81
184.94
210.44
197.96
144.81
185.94
211.44
198.96
137.03
186.94
212.44
199.96
138.03
39.97
40.57
30.62
31.80
29.60
28.28
29.00
29.67
28.31
29.10
29.67
28.31
29.17
29.67
28.31
29.21
29.74 28.31 29.24
18-Feb-20
167.94
213.44
200.96
139.03
29.80
28.30
29.29
152.71
214.44
201.96
140.03
32.39
29.89
28.31
29.40
127.66
107.30
89.72
87.71
215.44
216.44
217.44
218.44
202.96
203.96
204.96
205.96
141.03
142.03
143.03
144.03
35.29
_
29.94
30.00
30.00
30.00
30.16
30.31
28.33
28.26
28.26
28.26
28.34
28.44
29.44
29.59
29.68
29.76
29.85
29.94
85.86 219.44 206.96 145.03
79.24
80.24
220.44
221.44
207.96
208.96
146.03
147.03
25.42
36.25
28.20
28.70
28.60
28.95
29.04
29.04
29.04
29.15
29.29
29.40
29.50
29.62
30.45
30.54
30.73
30.73
30.73
30.76
30.86
30.96
31.07
31.04
31.04
31.04
28.44
28.23
28.36
28.36
28.36
28.20
28.27
28.60
28.60
30.06
30.13
30.26
30.31
30.35
30.40
30.48
30.63
30.75
30.85
30.85
30.85
81.24 222.44 209.96 148.03
82.24 223.44 _ 210.96 149.03 27.63 37.58
83.24 224.44 211.96 150.03
84.24 225.44 212.96 151.03 39.03
85.24 226.44 213.96 152.03
86.24 227.44 214.96 153.03
87.24 228.44 215.96 154.03 32.01 38.24
88.24 229.44 216.96 155.03
89.24 230.44 217.96 156.03 32.23 36.54
90.24
91.24
92.24
93.24
231.44
232.44
233.44
234.44
218.96
219.96
220.96
221.96
_ 157.03
158.03
159.03
160.03
34.90
37.55
29.62
30.88
30.89
29.62 30.74
30.97
Average 119.3 221.6
Minimum 79.24 210.4
207.5 147.3 30.44
193 137.0 25.42
39.84
38.97
35.03 29.126 30.252 28.288 29.88
30.06 28.200 28.99 27.74 28.49
1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Rocky Mount WQ Permit Number: WQ0005568
WWTP Name: 'Tar River Regional WWTP NPEDS Number: NCO030317
Monitoring Period: 07/01/2019 to 09/30/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Aerobic Digestion
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Darrell Highsmith, Chief Operator
Preparer Name and Title (type or print)
Signature of Preparer Date
Jason Smitli VP
Land Applier Name and Title (if applicable)(type or print)
&A-0 2/20/2020
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 17, 2020

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
Average Temperatures
Test date Age #1 Age #2 Age #3 Age #4 VR #1 VR #2 VR #3 VR #4 1 Dig. #1 Dig. #2 Dig. #3 Dig. #4
7/1/2019
94.24
235.44
222.96
161.03
37.52
7/2/2019
95.24
236.44
223.96
162.03
7/3/2019
96.24
237.44
224.96
163.03
7/4/2019
97.24
238.44
225.96
164.03
7/5/2019
98.24
239.44
226.96
165.03
39.02
7/6/2019
99.24
240.44
227.96
166.03
7/7/2019
100.24
241.44
228.96
167.03
7/8/2019
101.24
242.44
229.96
168.03
39.42
7/9/2019
102.24
243.44
230.96
169.03
7/10/2019
103.24
244.44
231.96
170.03
39.82
7/11/2019
104.24
245.44
232.96
171.03
7/12/2019
105.24
246.44
233.96
172.03
7/13/2019
106.24
247.44
234.96
173.03
7/14/2019
107.24
248.44
235.96
174.03
7/15/2019
108.24
249.44
236.96
175.03
7/16/2019
109.24
250.44
237.96
176.03
7/17/2019
110.24
251.44
238.96
177.03
7/18/2019
111.24
252.44
239.96
178.03
7/19/2019
112.24
253.44
240.96
161.79
7/20/2019
113.24
254.44
241.96
162.79
7/21 /2019
114.24
255.44
242.96
177.37
7/22/2019
115.24
256.44
243.96
178.37
7/23/2019
116.24
257.44
244.96
179.37
7/24/2019
105.17
258.44
245.96
180.37
7/25/2019
99.35
259.44
0.00
181.37
7/26/2019
97.23
260.44
0.00
182.37
7/27/2019
98.23
224.16
0.00
183.37
7/28/2019
99.23
175.24
0.00
184.37
7/29/2019
100.23
158.66
_ 0.00
185.37
7/30/2019
101.23
127.83
0.00
186.37
7/31 /2019
102.23
119.32
0.00
187.37
24.31
Average 104 233.9 181.5 173.6 38.95 24.31
Minimum 94.24 119.3 0 161.0 37.52 24.31
29.56
31.05 _
31.05
38.16
29.63
31.43
31.15
29.62
31.33
31.26
29.62
31.33
31.26
29.74
31.33
31.26
29.74
31.33
31.26
29.74
31.18
31.25
29.87
31.15
31.27
29.98
31.33
31.29
_
29.98
31.00
31.29
30.04
31.00
31.29
30.04
31.00
31.29
30.04
31.00
31.33
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.04
30.16
30.22
30.35
30.38
30.46 31.00
38.16 29.99 31.176
38.16 29.56 31
31.41
31.46
31.49
31.56
31.56
31.56
31.60
31.74
31.72
31.69
31.66
31.66
31.66
31.74
31.84
32.02
32.06
32.23
31.513
18-Feb-20
31.05
1

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees Q 18-Feb-20
Test date
Age #1
Age #2
Age #3
Age #4 VR #1
VR #2 VR #3 VR #4
Average Temperatures
Dig. #1
Dig. #2 Di . #3 Dig. #4
8/1/2019
103.23
116.04
0.00
188.37
30.46
30.60 32.23
8/2/2019
104.23
117.04
0.00
189.37
23.00
30.46
30.57 32.23
8/3/2019
105.23
110.21
0.00
190.37
30.53
30.57 32.30
8/4/2019
106.23
111.21
0.00
191.37
30.57
30.57 32.35
8/5/2019
8/6/2019
8/7/2019
8/8/2019
8/9/2019
107.23
108.23
109.23
110.23
111.23
' 112.21
113.21
114.21
115.21
116.21
0.00
0.00
0.00
0.00
0.00
192.37
193.37
194.37
195.37
196.37
21.63 21.63
28.23
30.61
30.65
30.64
30.64
30.64
29.58
29.98
30.22
30.26
30.29
32.50
32.50
32.50
32.50
32.50
8/10/2019
112.23
117.21
0.00
197.37
30.92
30.29
32.50
8/11/2019
113.23
118.21
0.00
198.37
31.04
30.29
32.50
8/12/2019
114.23
119.21
0.00
199.37
31.43
30.37
_
8/13/2019
115.23
120.21
0.00
200.37
31.43
30.41
8/14/2019
116.23
121.21
0.00
201.37
31.43
31.43
31.43
30.51
30.59
30.77
8/15/2019 117.23 122.21 0.00 202.37
8/16/2019 118.23 123.21 0.00 203.37 34.07
8/17/2019
8/18/2019
8/19/2019
8/20/2019
8/21 /2019
8/22/2019
8/23/2019
8/24/2019
8/25/2019
8/26/2019
8/27/2019
8/28/2019
8/29/2019
8/30/2019
8/31 /2019
119.23
120.23
121.23
122.23
123.23
124.23
125.23
126.23
137.55
138.55
139.55
140.55
141.55
142.55
143.55
124.21
125.21
126.21
127.21
128.21
129.21
130.21
131.21
132.21
133.21
134.21
135.21
136.21
137.21
138.21
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
204.37
205.37
206.37
207.37
208.37
209.37
210.37
211.37
212.37
213.37
214.37
215.37
216.37
120.98
109.83
37.67
37.87
38.55
44.16
42.18
42.49
31.30
30.77
31.00 30.77
31.00 30.97
31.13
31.26
31.39
31.50
31.50
31.50
31.47
31.48
31.52
_
31.49
32.70 31.49
32.70 31.49
Average
Minimum
120.6
103.2
123.7
110.2
0
0
196.8
109.8
34.99 21.63
21.63 21.63
31.096
30.826
32.419
30.46 29.58
32.23

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
Average Temperatures
Test date Age #1 Age #2 Age #3 Age #4 VR #1 VR #2 VR #3 VR #4 Dig. #1 Dig. #2 Dig. #3 Dig. #4
9/1/2019 144.55 139.21 0.00 92.45 32.70 31.49
9/2/2019 145.55 140.21 0.00 80.17 32.70 31.49
9/3/2019
146.55
141.21
0.00
71.08
9/4/2019
147.55
142.21
0.00
67.87
9/5/2019
148.55
143.21
0.00
58.62
9/6/2019
149.55
144.21
0.00
59.62
9/7/2019
150.55
145.21
0.00
60.62
9/8/2019
_151.55
146.21
0.00
61.62
9/9/2019
152.55
147.21
0.00
62.62
9/10/2019
153.55
148.21
0.00
63.62
9/11 /2019 154.55 149.21 0.00 64.62
9/12/2019 155.55 150.21 0.00 54.76
9/13/2019 156.55 151.21 0.00 55.76
9/14/2019
157.55
152.21
0.00
56.76
9/15/2019
158.55
153.21
0.00
57.76
9/16/2019
159.55
154.21
0.00
58.76
9/17/2019
160.55
155.21
0.00
59.76
9/18/2019
161.55
156.21
0.00
60.76
9/19/2019
162.55
157.21
0.00
61.76
9/20/2019
163.55
158.21
0.00
62.76
9/21 /2019
164.55
159.21
0.00
63.76
9/22/2019
165.55
160.21
0.00
64.76
9/23/2019
166.55
162.66
0.00
65.76
9/24/2019
167.55
163.66
0.00
66.76
9/25/2019
168.55
164.66
0.00
67.76
9/26/2019
169.55
165.66
0.00
68.76 _
9/27/2019
170.55
166.66
0.00
69.76 25.10
9/28/2019
171.55
167.66
0.00
70.76
9/29/2019
172.55
168.66
0.00
71.76
9/30/2019
173.55
169.66
0.00
72.76 35.69
Average 159.1 154.1 0 65.15 30.4
Minimum 144.6 139.2 0 54.76 25.10
10.36 1 32.70 31.49
32.70 31.49
11.57
32.70 31.49
32.70 31.49
32.70 31.49
14.74
32.70 31.51
32.70 31.58
15.83
32.70 31.64
32.70 31.64
26.10
27.55
27.93
27.93
27.93
28.03
28.06
28.43
18-Feb-20
18.32
32.70
32.70
32.70
32.70
31.64
31.92
31.94
31.97
28.43
28.43
28.43
28.76
17.24
32.70
32.70
32.70
32.70
32.70
32.70
32.70
32.07
32.18
32.18
32.18
32.27
32.39
32.47
29.02
29.07
29.09
28.79
28.79
28.79
28.90
21.19
26.39
32.70
32.57
28.94
23.33
32.70
32.53
28.75
32.70
32.53
28.82
32.70
32.53
28.91
32.70
32.40
28.91
32.70
32.27
28.91
32.70
32.10
29.05
17.66 1 32.7 31.948
10.36 32.700 31.49
28.488
26.100
1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Rocky Mount WQ Permit Number: WQ0005568
WWTP Name: Tar River Regional WWTP NPEDS Number: NCO030317
Monitoring Period: 10/01/2019 to 12/31/2019
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Aerobic Digestion
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T .1107): Alt. 1 (VS reduction)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
0 requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
❑ requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Darrell Highsmith, Chief Operator
Preparer Name and Title (type or print)
1
el
Signature of Prepare Date
Jason Smith VP
Land Applier Name and Title (if applicable)(type or print)
-,1W &A-0 2/20/2020
Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 17, 2020

Volatile Reduction
(503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C)
18-Feb-20
Test date
Age #1
Age #2
Age #3
Age #4
VR #1
VR #2
VR #3 VR #4
Dig. #1
Average Temperatures
Dig. #2 Dig. #3 Dig. #4
10/1 /2019
10/2/2019
10/3/2019
10/4/2019
10/5/2019
10/6/2019
174.55
175.55
176.55
177.55
178.55
179.55
170.66
171.66
172.66
173.66
174.66
175.66
0.00
0.00
0.00
0.00
0.00
0.00
73.76
74.76
75.76
76.76
77.76
78.76
26.53
27.56
32.70
32.70
31.84
31.45
28.74
28.81
32.70 31.45
28.87
32.70 31.45
28.97
32.70 31.60
28.97
32.70 31.65
28.97
10/7/2019
10/8/2019
10/9/2019
10/10/2019
180.55
181.55
182.55
183.55
112.06
113.06
114.06
115.06
0.00
0.00
0.00
0.00
79.76
80.76
81.76
82.76
34.11
33.75
34.11
32.70
30.90
28.94
32.70
29.10
30.40
28.97
28.97
28.97
10/11/2019
184.55
116.06
0.00
83.76
28.45
28.45
30.70
28.97
10/12/2019
185.55
117.06
0.00
84.76
30.70
28.97
10/13/2019
186.55
118.06
0.00
85.76
30.70
28.97
10/14/2019
10/15/2019
10/16/2019
10/17/2019
10/18/2019
10/19/2019
10/20/2019
10/21 /2019
10/22/2019
187.55
141.54
116.45
115.11
85.51
73.61
66.37
67.37
68.37
119.06
120.06
121.06
122.06
123.06
124.06
125.06
126.06
127.06
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
86.76
87.76
88.76
89.76
90.76
91.76
92.76
93.76
94.76
29.30
30.68
31.19
29.86
29.30
_
30.45
29.64
29.85
28.94
29.09
29.10
29.11
29.11
29.13
29.11
29.13
29.15
29.13
29.20
29.27
29.14
24.00 29.42
29.18
10/23/2019
10/24/2019
10/25/2019
10/26/2019
10/27/2019
10/28/2019
10/29/2019
10/30/2019
10/31 /2019
69.37
70.37
71.37
72.37
73.37
74.37
75.37
76.37
77.37
128.06
129.06
130.06
131.06
132.06
133.06
134.06
135.06
136.06
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
95.76
96.76
97.76
98.76
99.76
100.76
0.00
0.00
0.00
15.24
11.47
28.70
17.60
30.72
30.06
32.18
30.86
23.65
23.43
29.19
29.12
29.23
29.23
22.93 29.01
29.23
22.93 29.01
29.09
22.93 29.01
28.94
23.26 28.96
28.89
23.55 28.95
23.81 28.94
24.16 29.02
Average
Minimum
126.8
66.37
133.6
112.1
0
0
78.82
0
18.25
11.47
30.74
28.45
29.95
26.53
27.569
1 22.930
29.937
28.940
29.032
28.74
1

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C} 18-Feb-20
Test date Age #1 Age #2 Age #3 Age #4 VR #1 VR #2 VR #3 VR #4
11 /1 /2019
78.37
137.06
0.00
0.00
23.59
26.64
11 /2/2019
79.37
138.06
0.00
0.00
11 /3/2019
80.37
139.06
`
0.00
0.00
11 /4/2019
81.37
140.06
0.00
0.00
21.51
29.93
11 /5/2019
82.37
141.06
0.00
0.00
11 /6/2019
83.37
142.06
0.00
0.00
21.78
30.81
11 /7/2019
84.37
143.06
0.00
0.00
11 /8/2019
77.66
144.06
0.00
0.00
22.06
30.00
11 /9/2019
72.75
145.06
0.00
0.00
11 /10/2019
70.23
146.06
0.00
0.00
11 /11 /2019
65.99
147.06
0.00
0.00
19.81
30.46
11 /12/2019
58.41
148.06
0.00
0.00
28.85
11 /13/2019
59.41
149.06
0.00
0.00
11 /14/2019
60.41
150.06
0.00
0.00
32.46
11 /15/2019
61.41
151.06
0.00
0.00
22.37
29.45
11/16/2019
62.41
152.06
0.00
0.00
11 /17/2019
63.41
153.06
0.00
0.00
11 /18/2019
64.41
154.06
0.00
0.00
24.21
31.86
11 /19/2019
65.41
155.06
0.00
0.00
11 /20/2019
66.41
156.06
0.00
0.00
24.55
31.68
11 /21 /2019
67.41
157.06
0.00
0.00
11 /22/2019
68.41
158.06
0.00
0.00
26.01
31.09
11 /23/2019
69.41
159.06
0.00
0.00
_
11 /24/2019
70.41
160.06
0.00
0.00
11 /25/2019
71.41
161.06
0.00
0.00
28.70
33.19
11 /26/2019
72.41
162.06
36.71
0.00
11 /27/2019
73.41
163.06
37.71
0.00
27.93
33.23
11 /28/2019
74.41
164.06
35.23
0.00
11 /29/2019
75.41
165.06
28.58
0.00
11 /30/2019
76.41
166.06
29.58
0.00
Average 71.23 151.6 5.594
Minimum 58.41 137.1 0
0 23.87 30.74
0 19.81 26.64
Average Temperatures
)i4. #1 Diu. #2 Dig. #3 Dig. #4
24.61
28.84
24.61
28.84
24.61
28.84
24.65
28.81
24.78
28.78
25.00
28.80
25.05
28.55
25.04 28.45
25.04
28.45
25.04
28.45
24.96
28.32
24.78
28.23
24.70
28.12
_ 24.53
27.97
24.36
27.81
24.36
27.81
24.36
27.81
24.18
27.,62
24.13
27.22
24.07
26.96
24.03
26.85
24.02
26.71
24.02
26.60
24.02
26.61
24.04
26.43
24.13
26.45
24.14
26.28
24.14 26.28
24.14 26.28
24.14 26.13
24.456 27.643
24.020 26.13
1

Volatile Reduction (503.32 (b) Requirements (8/99): >38% VR, >40 days @ >20 degrees C) 18-,web-20
Average Temperatures
Test date
Age #1
Age #2
Age #3
Age #4
VR #1
VR #2
VR #3
VR #4
DIG. #1
Dig. #2
Di . #3 Dig. #4
12/1/2019
77.41
167.06
23.89
0.00
24.15
25.95
12/2/2019
78.41
168.06
24.89
0.00
31.13
32.63
18.67
24.22
25.86
19.60
12/3/2019
79.41
169.06
25.89
0.00
24.26
25.75
19.55
12/4/2019
80.41
170.06
26.89
0.00
33.63
35.07
19.35
24.34
25.64
19.57
24.35
25.64
20.15
12/5/2019
81.41
171.06
27.89
0.00
32.51
34.16
17.90
24.28
25.57
20.48
12/6/2019
82.41
172.06
28.89
0.00
34.75
34.99
18.79
24.26
25.46
20.48
12/7/2019 83.41 173.06 29.89 0.00
12/8/2019
84.41
174.06
30.89
0.00
24.23
25.33
20.48
12/9/2019
85.41
175.06
31.89
0.00
34.42
34.68
19.59
24.27
25.27
20.78
12/10/2019
86.41
176.06
32.89
0.00
24.12
25.13
21.53
24.00
25.16
21.73
12/11 /2019
87.41
177.06
33.89
0.00
34.40
34.87
19.65
23.99
25.19
21.79
12/12/2019
88.41
178.06
34.89
0.00
33.42
34.87
20.93
24.02
25.22
21.90
12/13/2019 89.41 179.06 35.89 0.00 33.55 35.41 9.79
12/14/2019
90.41
180.06
34.27
0.00
23.99
25.11
21.90
12/15/2019
91.41
181.06
31.16
0.00
23.90
24.99
21.90
23.67
24.77
22.03
12/16/2019
92.41
182.06
29.52
0.00
36.18
36.33
18.46
23.60
24.83
22.27
12/17/2019
93.41
183.06
28.21
0.00
23.57
24.71
22.31
12/18/2019
94.41
184.06
27.16
0.00
37.01
36.84
18.49
23.52
24.70
22.36
12/19/2019
95.41
185.06
27.21
0.00
23.43
24.61
22.27
12/20/2019
96.41
186.06
28.21
0.00
37.62
38.08
19.17
23.41
24.59
22.27
12/21 /2019 97.41 187.06 29.21 0.00
12/22/2019
98.41
188.06
30.21
0.00
23.46
24.53
22.27
12/23/2019
99.41
189.06
31.21
0.00
36.86
36.53
52.52
23.30
24.36
22.28
12/24/2019
100.41
190.06
32.21
0.00
23.36
24.38
22.28
12/25/2019
101.41
191.06
33.21
0.00
23.45
24.41
22.28
12/26/2019
102.41
192.06
34.21
0.00
23.45
24.41
22.28
12/27/2019
103.41
193.06
35.21
0.00
39.36
23.32
24.30
22.30
23.43
24.31
22.30
12/28/2019
104.41
194.06
36.21
0.00
23.43
24.48
22.30
12/29/2019 105.41 195.06 37.21 0.00
12/30/2019
106.41
196.06
38.21
0.00
37.54
37.16
26.89
23.46
24.50
22.38
12/31 /2019
107.41
197.06
39.21
0.00
39.26
39.74
20.99
23.43
24.50
22.41
Average
92.41
182.1
31.31
0
35.44
35.81
21.51
23.796
24.957
21.614
Minimum
77.41
167.1
23.89
0
31.13
32.63
9.79
23.3
24.3
19.55
f

Page 1
Contact: Drew Matthews Report Date: 12/30/2019
Client: Soil Plus
P.O. Box 1396 Project: Rocky Mount WWTP
Oxford, NC 27565 Date Sample Rcvd: 12/19/2019
Meritech Work Order # 12191951 Sample: RM121919 (001) Grab 12/19/19
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 3.11 % 12/20/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 5,262 col/g dry wt 12/19/19 130 col/g dry wt SM 9222D
Meritech Work Order #
12191952
Sample: RM121919 (002) Grab
12/19/19
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
3.08 %
12/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
4,132 col/g dry wt 12/19/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
12191953
Sample: RM121919 (003) Grab
12/19/19
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
3.09 %
12/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
6,472 col/g dry wt 12/19/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
12191954
Sample: RM121919 (004) Grab
12/19/19
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
3.10 %
12/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,279 col/g dry wt 12/19/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
12191955
Sample: RM121919 (005) Grab
12/19/19
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
3.07 %
12/20/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,626 col/g dry wt 12/19/19 130 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Page 2
Report Date: 12/30/2019
Project: Rocky Mount WWTP
Date Sample Rcvd: 12/19/2019
Meritech Work Order # 12191956
Sample: RM121919 (006) Grab
12/19/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.08 %
12/20/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
5,608 col/g dry wt 12/19/19
130 col/g dry wt
SM 9222D
Meritech Work Order # 12191957
Sample: RM121919 (007) Grab
12/19/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.11 %
12/20/19
0-100 %
SM 2540B
Fecal Coliform (Sludge)
4,969 col/g dry wt 12/19/19
130 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. HWQ,, 0
At
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-7013
Chain of Custody Record (COC)
NPDES#:
client:
Client: SOH PIUS Phone: [phone]
PO Box 1396 Fax: [phone]
Oxford NC 27565 Email: [e-mail]
Project: Rocky Mount W WTP
P.O.#:
Attention: Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emai (preferred), Fax, Mail
Std(10days) 3�s ,ems
X
MERITECH, INC,
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates &Times
i P S Ta
king aking ample (Sign/Print):
Drew Matthews i �'.,4J �(�- L' `° �_
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
•
Test(s) Required
On Ice?
Yes / No
pH01<?
Cl OK?
Date
Time
Date
Time
RM 121919
(001)
12/19/19
G
1
Fecal Coliform / % Total Solids
RM 121919
(002)
12/19/19
`):r'" r.,1,
G
1
Fecal Coliform / % Total Solids
RM 121919
(003)
12/19/19
`l , � S ,,
G
1
Fecal Coliform / % Total Solids
RM 121919
(004)
12/19/19
`1; I'1 r�,
G
1
Fecal Coliform / % Total Solids
RM 121919
(005)
12/19/19
G
1
Fecal Coliform / % Total Solids
RM 121919
(006)
12/19/19
`1 • PAn
G
1
Fecal Coliform / % Total Solids C
RM 121919 (007)
12/19/19
11: 1
G
1
Fecal Coliform / % Total Solids
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field prior to preservation. ***
Comments:
Please email results to [e-mail]
Compositor #
[J' UPS
Jug #
QFed Ex
Are these results for regulatory purposes? Yes
No [
Report results in: mg/L mg/kg Q- ug/L 0
Hand Delivery
Relinquished by: 1 �, - Date: Time:
{ >✓ �, 1 tI �ri�1 i
5
Received by: D Time:
Other
Relinquished b : `
Relin q y l 2-�� Time:
`
3-J -
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab:
.� 1 2DatRA Time:

Meritech, Inc.
Environmental Laboratory
m`4-—Laboratory Certification No. 165
Contact: Drew Matthews Report Date: 1/24/2020
Client: Soil Plus
P.O. Box 1396 Project: Rocky Mount WWTP
Oxford, NC 27565 Date Sample Rcvd: 12/19/2019
Vector Attraction Reduction / Aerobically Digested Sludge 30 Day Test)
Meritech Work Order # 12191949 Sample: RM 121919 Grab 12/19/19
Total Solids Volatile Solids % Volatile Solids
Week 1 0.540 0.350 0.650
Week 2
0.450
0.290
0.642
Week 3
0.400
0.260
0.650
Week 4
0.400
0.260
0.653
Week 5
0.330
0.210
0.643
Mass Balance Equation = 1.16% Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
I hereby certify that I have reviewed and approve these data,
La oratory Represe tat tative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-202013 Chain of Custody Record (COC)
NPDES#:
Client: SOO PIUS Phone: [phone]
Address: PO Box 1396 Fax: [phone]
Oxford, NC 27565 Email: [e-mail]
Project: Rocky Mount WWTP
P.O.#:
Attention: Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
Std (10 days) 3 - 5 Da s �4 - dR Hrc
Circle all that apply: Email(preferred), Fax, Mail , =
X
MERITECH, INC.
- ENVIRONMENTAL LABORATORIES
la sy ' x
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
�•y
www.meritech—la s.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): Drew Matthews I1 t �` ( �:1
Lab Use Only
Start
End
Comp.
Grab?
#of
Cont.
Test(s) Required
on Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
RM 121919
12/1.9/19
G
1
30 Day Bench Scale Test
Temperature Upon
Receipt:
Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments: Compositor #
Shipment: Please email results to [e-mail]
UPS Jug #
Q Fed Ex Are these results for regulatory purposes? Yes W No C '. Report results in: mg/L mg/kg ED. ug/L
Q Hand Delivery
Relinquished by: • (� j 4, ];,, •, Date:, .1l i Time:
Received by: `�Dat :/ Time:
Other
Relinquished by: I/
Date /� Time:
V '�' , "
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab:), n
DaM —I1 Time: a

City of Rocky Mount
2019 Class B Annual Report
WQ Permit# WQ0005568
Soil Samples

Page 1 of 1
Report No: 19-288-0553
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms Inc
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Site 1
Date Received: 10/15/2019
Date of Report: 10/16/2019
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
19627
1
MIN 0.2
1.0 6.1
1.6
248
75
33
94
530
530
335
11.4
86
68
14
0.5 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
10
S
0
Mn
0
Mn-AI
72
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19628
2
MIN 0.2
0.8 6.1
1.8
241
130
31
100
575
575
340
12.7
86
63
17
0.5 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
0
S
0
Mn
0
Mn-AI
75
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19629
3
MIN 0.3
0.8 6.1
1.7
296
147
31
88
588
588
430
13.3
87
70
12
0.5 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
0
S
0
Mn
0
Mn-AI
68
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-288-0555
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Site 22
Date Received: 10/15/2019
Date of Report: 10/16/2019
Lab No Field ID Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS% Ca%
Mg% ESP Na SS-1 NO3 N
19635 1
MIN 0.2
0.8 5.9
1.7
570
329
92
169
1060
1060
1140
18.8
91 72
9 1.2 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
0
S
0
Mn
0
Mn-AI
120
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19636 2
MIN 0.3
0.7 5.7
1.8
472
284
81
313
925
925
890
15.2
88 66
11 1.2 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.6
N
150
P205
0
K20
0
S
0
Mn
0
Mn-AI
209
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 1 of 2
Report No: 19-310-0519
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms INC
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Site 25
Submitted By: Drew Matthews/Soil Plus
Date Received: 11/06/2019
Date of Report: 11 /07/2019
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
03264
1A
MIN
0.3
4.8
3.8
427
59
85
238
1195
1195
1315
12.5
70
60
6
1.3 0.2
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
2.5
N
200
P205
0
K20
30
S
0
Mn
0
Mn-AI
178
Zn
0
Cu
0
B
Mg
0
Last Crop
03265
1B
MIN
0.4
5.4
1.7
94
35
40
75
160
160
365
5.9
71
59
8
1.2 0.1
Crop Recommendations:
1- Loblolly Pine
Rec Uom
lb/acre
Lime (Vacre)
0.9
N
100
P205
0
K20
80
S
0
Mn
4
Mn-AI
71
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03266
1 C
MIN
0.4
5.5
2.4
81
47
35
94
190
190
520
9.6
75
65
7
0.8 0.1
Crop Recommendations:
1- Loblolly Pine
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
100
P205
0
K20
80
S
0
Mn
4
Mn-AI
81
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03267
1D
MIN
0.8
4.7
2.5
267
52
119
150
553
553
665
9.1
72
61
7
1.9 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
1.7
N
150
P205
0
K20
40
S
0
Mn
0
Mn-AI
127
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03269
1E
MIN
1.1
5.5
2.0
122
59
104
244
295
295
475
10.8
81
70
7
1.4 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.9
N
150
P205
0
K20
30
S
0
Mn
0
Mn-AI
171
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03270
1F
MIN
0.5
5.2
2.6
178
59
108
231
403
403
650
11.0
77
66
6
1.8 0.2
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
1.5
N
150
P205
0
K20
30
S
0
Mn
0
Mn-AI
168
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03271
2
MIN
0.7
4.7
3.7
424
83
100
200
725
725
1265
10.0
63
52
6
1.3 0.1
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
2.5
N
200
P205
0
K20
10
S
0
Mn
0
Mn-AI
157
Zn
0
Cu
0
B
Mg
0
Last Crop
03272
3
MIN
0.4
6.8
0.5
197
27
64
94
315
315
465
15.5
97
91
5
0.6 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.0
N
150
P205
0
K20
84
S
0
Mn
0
Mn-AI
61
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 2 of 2
Report No: 19-310-0519
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms INC
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Site 25
Submitted By: Drew Matthews/Soil Plus
Date Received: 11/06/2019
Date of Report: 11 /07/2019
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
103273
4
MIN
0.8
5.5
2.8
286
89
121
288
750
750
705
16.8
83
70
10
1.4 0.2 I
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
1.3
N
200
P205
0
K20
10
S
0
Mn
0
Mn-AI
197
Zn
0
Cu
0
B
Mg
0
Last Crop
03274
5
MIN
0.3
6.0
1.8
290
88
116
156
578
578
660
21.2
92
84
5
0.7 0.1
Crop Recommendations:
1- Fescue Hay
Rec Uom
lb/acre
Lime (Vacre)
0.5
N
150
P205
0
K20
0
S
0
Mn
0
Mn-AI
111
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03275
6
MIN
1.0
4.6
3.4
353
76
125
250
648
648
570
10.0
66
52
9
1.8 0.2
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
2.4
N
200
P205
0
K20
10
S
0
Mn
0
Mn-AI
188
Zn
0
Cu
0
B
Mg
0
Last Crop
03276
7
MIN
0.4
4.4
4.0
222
92
100
300
510
510
445
9.4
57
43
8
1.7 0.2
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
2.9
N
200
P205
0
K20
10
S
0
Mn
0
Mn-AI
221
Zn
0
Cu
0
B
Mg
0
Last Crop
03277
8
MIN
0.7
4.8
3.8
506
34
89
100
570
570
1620
7.9
53
43
6
1.5 0.1
Crop Recommendations:
1- Loblolly Pine
Rec Uom
lb/acre
Lime (Vacre)
2.5
N
100
P205
0
K20
80
S
0
Mn
4
Mn-AI
95
Zn
0
Cu
0
B
0
Mg
0
Last Crop
03278
9A
MIN
0.5
4.7
2.5
77
44
52
38
118
118
180
6.1
59
45
9
1.6 0.1
Crop Recommendations:
1- Loblolly Pine
Rec Uom
lb/acre
Lime (Vacre)
1.7
N
100
P205
0
K20
80
S
0
Mn
4
Mn-AI
59
Zn
0
Cu
0
B
0.5
Mg
0
Last Crop
03280
9B
MIN
0.4
5.5
2.1
62
35
23
63
90
90
130
7.4
71
60
8
0.8 0.1
Crop Recommendations:
1- Bermudagrass Hay
Rec Uom
lb/acre
Lime (Vacre)
1.0
N
200
P205
10
K20
149
S
20
Mn
0
Mn-AI
62
Zn
0
Cu
0
B
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.

Page 1 of 1
Report No: 19-288-0557
Account No: 04596
Advisor: Soil Plus, LLC
Joyce Barrette
P.O. Box 1396
Oxford NC 27565
Waypoint"'o
ANALYTICAL
Client: Granville Farms Inc
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Farm: Site 41
Date Received: 10/15/2019
Date of Report: 10/16/2019
Lab No Field ID
Sample ID
Soil Class HM%
W/V pH
Ac
P-1
K-1
S-1
Mn-I
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na SS-1 NO3 N
19638
1
MIN
0.3
1.2 5.0
1.6
269
21
50
56
228
228
280
4.0
59
46
8
2.0 0.1
Crop Recommendations:
1- Corn
Rec Uom
lb/acre
Lime (Vacre)
1.0
N
160
P205
0
K20
97
S
0
Mn
0
Mn-AI
66
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19639
2
MIN
0.4
1.2 4.9
1.7
191
21
31
69
158
158
215
3.8
55
43
8
1.5 0.1
Crop Recommendations:
1- Corn
Rec Uom
lb/acre
Lime (Vacre)
1.1
N
160
P205
0
K20
97
S
0
Mn
0
Mn-AI
75
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19640
3A
MIN
0.2
1.3 5.1
1.7
118
15
23
50
88
88
135
2.9
42
29
8
2.1 0.1
Crop Recommendations:
1- Corn
Rec Uom
lb/acre
Lime (Vacre)
1.0
N
160
P205
0
K20
111
S
20
Mn
0
Mn-AI
61
Zn
0
Cu
0
B
0
Mg
0
Last Crop
19641
3B
MIN
0.1
1.3 4.4
1.8
140
5
33
13
38
38
115
2.6
29
20
7
1.5 0
Crop Recommendations:
1- Corn
Rec Uom
lb/acre
Lime (Vacre)
1.3
N
160
P205
0
K20
137
S
0
Mn
0
Mn-AI
49
Zn
0
Cu
0
B
0
Mg
0
Last Crop
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc.