WQ0028547_Residual Annual Report 2019_20200227 (3)

Initial Review
INITIAL REVIEW
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application r Annual Report
what is the submittal r Residual Annual Report
type?* r Additional Information
r Other
Annual Report 2019
Year*
Date Paper Copy 2/27/2020
Received:*
Project Number* WQ0028547
Email Notifications
Does this need review by the hydrogeologist?*
r Yes r No
Regional Office
CO Reviewer
Admin Reviewer [e-mail]

Submitted Form
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic subnittal, confirmation of receipt, and other issues.
..........................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
.......................................................................................
Submittal Type* r New Permit Application
r Renewal
r Annual Report
r Other
Permit Type * r Wastewater Irrigation
r Other Wastewater
r Closed -Loop Recycle
r Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?
r Yes r Nor N/A
Permit Number* WQ0028547
Applicant\Permittee * Town of Yanceyville
Facility Name * Town of Yanceyville
Phone Number*
336-751-1441
r Modification (Major or Minor)
r Additional Information
r Residual Annual Report
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2019 Yanceyville Annual Report - WQ0028547.pdf 6.71 MB
Upload only 1 R7F document. NL@iple documents must be combined into one R7F file.

For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required,
be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments {talcs, soils report, specs, etc.]
o One full-size engineering plan set
o One 11x17" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailine address:
Division of Water Resources ! Division of Water Resources
Non -Discharge Branch I Non -Discharge Branch
1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W
- =
Raleigh, NC 27699-1617 S12 N.5alisburySt.
For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560.
* rJ By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
Submission Date 2/24/2020

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0028547 County:
Facility Name (as shown on permit):
Land Application Operator:
Caswell County Year: 2019
Town ofYanceyville
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number ofapplication fields in the pennit:
17
Total number of fields utilized for land application during the year:
4
Total amount of dn- tons applied during the year for all application sites:
1 5,.71
Total number of acres utilizes for land application during the year:
31.1 5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
l) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was perforated in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in I5A NCAC 02T .l 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities),
8) All monitoring and reporting requirements in 15A NCAC 02T .1 11 I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Brian Collie - Town Manager
Permittee Name and Title (type or print)
t fir' en
-2`1- 2
Signature of Permittee Date
1 /7/2020
V
Signature of Preparer* Date Signature of land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DEN FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0028547
Facility Name: Town of Yanceyville
Residual Source WQ # or
NPDES #:
NCO04001I
WWTP Name: Yanceyville W WTP
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Colic.
Limit
a
m Ik
Sam le or Composite Date
818119
Percent Solids (%}
NA
11.3
Arsenic
75
3.96
Cadmium
85
0.758
Copper
4,300
205
Chromium
NA
22.2
Lead
840
35.4
Mercury
57
0.0982
Molybdenum
75
3.07
Nickel
420
16.1
Selenium
100
4.8
Zinc
7,500
398
Total Phosphorus
NA
6890
TKN
NA
15000
Ammonia -Nitrogen
NA
3100
Nitrate and Nitrite
NA-4
41.7
' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties foj ubmitting false ipfo rmation, including the possibility of fines and imprisonment for knowing violations."
Signature of P
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .11 02 (26)
1-13—Z0
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0028547 Laboratory: 1) Waypoint Analytical
Facility Name: Town of Yanceyviile 2)
Residual Source
NPDES # or WQ#:
NCO04001 I
WWTP Name: Yanceyville W WTP
Residual Analvsis Data
3)
4)
5)
Parameter
Sample or Composite Date
MagneSiLlin
1
-----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
rri 7i
G �
Z 3 -- ry 0
Signature of Preparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T A 102 (26)
DENR FORM RSSF - 6 (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to he analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0028547 Laboratory: 1) Waypoint Analytical
Facility Name: Town of Yanceyville 2)
Residual Source WQ # or 02-17-010 3)
1VPDES #: 4)
WWTP Name: Yanceyville WTP 5)
Residual Analysis Data
Parameter
+
Limit
ple or CompositeDate
I lilt
_-_--------
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the inrormation submitted. I am aware that there are significant
pen Itie& for submitting false infor including the possibility of fines and imprisonment for knowing violations."
r
1-z3-- 2.
Signature
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
W Q0028547
Facility Name: Town ofYanceyviile
Residual Source NCO04001 1
NPDES # or WQ#:
WWTP Name: Yanceyviile WWTP
RPcidual Analvgk Bata
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
Sam le or Composite Dal
``I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant peAplties for submitting Aformation, including the possibility of fines and imprisonment for knowing violations."
S
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26)
!-1?3— 20
Date
DENR FORM RSSF - B (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Yanceyville
WQ0028547
Operator: Jon Crispin Owner:
Acres Used: 4.75 Acres Permitted:
Total Dry Tons Applied (Annual): 25.45
Cation Exchange Capacity (non 503 only):
Bonnie Crispin Predominant Soil Series:
4.75 Site #: CS82 Field #:
FbB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
WWTP
8/8/19
21
3
1 41
5
61
7
81
9
10
11
1121
% Solids
11.3
Arsenic
3.96
Cadmium
0.758
Copper
205
Chromiurri
22.2
Lead
35.4
Mercury
0.0982
Molyb-
denum
3.07
Nickel
16.1
Selenium
4.8
Zinc
398
Total
Phos-
horus
6890
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
©
©
•
D
-
• ••
Event
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
•
••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
'.
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
�1, M�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
•�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� •�
Total
' .
'
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl;fz 1/7/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Yanceyville WQ Permit #: WQ0028547 Field #: 1 Acres Utilized: 4.75
Land Owner: Bonnie Crispin Annual Dry Tons Applied: 25.45 Site #: CS82 Acres Permitted: 4.75
Operator: Jon Crispin Predominant Soil Series: FbB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN:
QLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.y
Past 24
Hrs.
inches
co 'a
0
* �°n
o
*
4
7y CD
D
o'
TKN
mg/kg
Z
o
m.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN App lied
lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/5
13500
11.3
1.339
Yanceyville WWTP
D
<.5"
S
0.5
0.3
15000
3100
41.7
13.825
NA
Fescue
12/6
40500
11.3
4.018
Yanceyville WWTP
D
<.5"
S
0.5
0.3
15000
3100
41.7
41.476
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM
FSF supp ( attach FORM
FSF supp
to this form):
0.000
0.000
TOTALS:
01
54000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
ZnJ0141
0.00o
Lime A lied
Annuallbs/acre
0.042
0.008
2.196
0.238
0.379
0.001
0.033
0.172
0.051
4.264
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.042
0.008
2.196
0.238
0.379
0.001
0.033
0.172
0.051
4.264
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/7/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Yanceyville
WQ0028547
Operator: Jon Crispin Owner:
Acres Used: 7 Acres Permitted:
Total Dry Tons Applied (Annual): 36.05
Cation Exchange Capacity (non 503 only):
Bonnie Crispin Predominant Soil Series:
7 Site #: CS82 Field #:
FbB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
WWTP
8/8/19
21
3
1 41
5
61
7
81
9
10
11
1121
% Solids
11.3
Arsenic
3.96
Cadmium
0.758
Copper
205
Chromiurn
22.2
Lead
35.4
Mercury
0.0982
Molyb-
denum
3.07
Nickel
16.1
Selenium
4.8
Zinc
398
Total
Phos-
horus
6890
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
©
©
•
D
-
• ••
Event
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
•
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 ••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ••
1 1�•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�.
®
1••
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 1..
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl;fz 1/7/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Yanceyville WQ Permit #: WQ0028547 Field #: 2 Acres Utilized:
Bonnie Crispin Annual Dry Tons Applied: 36.05 Site #: CS82 Acres Permitted:
Jon Crispin Predominant Soil Series: FbB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN:
7
7
I
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.y
Past 24
Hrs.
inches
co 'a
0
* �°n
o
*
7y C
?: 't
* w
o
TKN
mg/kg
Z
o
M o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/6
49500
11.3
3.332
Yanceyville WWTP
D
<.5"
S
0.5
0.3
15000
3100
41.7
34.399
NA
Fescue
12/7
27000
11.3
1.818
Yanceyville WWTP
D
<.5"
S
0.5
0.3
15000
3100
41.7
18.763
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM
FSF supp ( attach FORM
FSF supp
to this form):
0.000
0.000
TOTALS:
01
76500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
53.162
0.00o
Lime A lied
Annuallbs/acre
0.041
0.008
2.112
0.229
0.365
0.001
0.032
0.166
0.049
4.099 70.967
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
2000
Current Cumulative lbs/ac
0.041
0.008
2.112
0.229
0.365
0.001
0.032
0.166
0.049
4.099
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/7/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Yanceyville
WQ0028547
Operator: Jon Crispin Owner:
Acres Used: 8.5 Acres Permitted:
Total Dry Tons Applied (Annual): 6.36
Cation Exchange Capacity (non 503 only):
Bonnie Crispin Predominant Soil Series:
8.5 Site #: CS82 Field #:
FbB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
WWTP
8/8/19
21
3
1 41
5
61
7
81
9
10
11
1121
% Solids
11.3
Arsenic
3.96
Cadmium
0.758
Copper
205
Chromiurri
22.2
Lead
35.4
Mercury
0.0982
Molyb-
denum
3.07
Nickel
16.1
Selenium
4.8
Zinc
398
Total
Phos-
horus
6890
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
©
©
•
D
-
• ••
Event
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• •
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl;fz 1/7/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Yanceyville WQ Permit #: WQ0028547 Field #: 3 Acres Utilized: 8.5
Land Owner: Bonnie Crispin Annual Dry Tons Applied: 6.36 Site #: CS82 Acres Permitted: 8.5
Operator: Jon Crispin Predominant Soil Series: FbB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN:
QLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
�y
co
c
*
o
*
Z
4
7y CD
?D
*
o'
TKN
mg/kg
Z
o
ac o
m.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN A lied
pp
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/7
13500
11.3
0.748
Yanceyville WWTF
D
<.5"
S
0.5
0.3
15000
3100
41.7
7.726
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM
FSF supp ( attach FORM
FSF supp
to this form):
0.000
0.000
TOTALS:
0
13500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
7.726
0.00o
Lime Applied
Annuallbs/acre
0.006
0.001
0.307
0.033
0.053
0.000
0.005
0.024
0.007
0.595 10.307
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
2000
Current Cumulative lbs/ac
0.006
0.001
0.307
0.033
0.053
0.000
0.005
0.024
0.007
0.595
Permitted C. P. L. R.****
1 36
1 34
1 1338
1
1 267
1 15
1
1 374
89
2498
Permit PAN Limit 1 st/2nd Crop
141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/7/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Yanceyville
WQ0028547
Operator: Jon Crispin Owner:
Acres Used: 10.9 Acres Permitted:
Total Dry Tons Applied (Annual): 67.85
Cation Exchange Capacity (non 503 only):
Bonnie Crispin Predominant Soil Series:
10.9 Site #: CS82 Field #:
FbB2
0
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
11
WWTP
8/8/19
21
3
1 41
5
61
7
81
9
10
11
1121
% Solids
11.3
Arsenic
3.96
Cadmium
0.758
Copper
205
Chromiurri
22.2
Lead
35.4
Mercury
0.0982
Molyb-
denum
3.07
Nickel
16.1
Selenium
4.8
Zinc
398
Total
Phos-
horus
6890
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
©
©
•
D
-
• ••
Event
1 1� •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�.
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11'
•
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 ..
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 ..
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1.1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1.1
®
•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
. .
Total
Phos-
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zl;fz 1/7/2020
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Yanceyville WQ Permit #: WQ0028547 Field #: 4 Acres Utilized: 10.9
Land Owner: Bonnie Crispin Annual Dry Tons Applied: 67.85 Site #: CS82 Acres Permitted: 10.9
Operator: Jon Crispin Predominant Soil Series: FbB2 Cation Exchange Capacity (non 503): 0
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 188 Crop 2 Name: Crop 2 Max. PAN:
QLiquid
Volume applied
(enter one) Solids/
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>
co 'a
0
* Z°n
o
CD N'
7y C
?: 't
D
o'
TKN
mg/kg
Z.
o
M o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
12/4
58500
11.3
2.529
Yanceyville WWTF
D
<.5"
S
0.5
0.3
15000
3100
41.7
26.108
NA
Fescue
12/5
85500
11.3
3.696
Yanceyville WWTF
D
<.5"
S
0.5
0.3
15000
3100
41.7
38.157
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM
FSF supp ( attach FORM
FSF supp
to this form):
0.000
0.000
TOTALS:
0
14400o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
64.265
0.000
Lime Applied
Annuallbs/acre
0.049
0.009
2.552
0.276
0.441
0.001
0.038
0.200
0.060
4.955 85.781
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.049
0.009
2.552
0.276
0.441
0.001
0.038
0.200
0.060
4.955
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/7/2020 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
8/20/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-221-0036
Client Project Description: Yonceyville WWTP
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www,way po inta n a lyti ca 1. co m
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/9/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Z� l
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Yonceyville WWTP
Lab Report Number: 19-221-0036
Date: 8/20/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 6

0 2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Yonceyville WWTP Report Date : 08/20/2019
755 Yadkinville Rd Information : Received : 08/09/2019
Mocksville , NC 27028
Report Number : 19-221-0036 REPOR T OF A NA L YSIS Danyale Love
Project Manager
Lab No : 89567
Matrix: Solids
Sample ID: Yonceyville WWTP
Sampled:
8/8/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
88.7
%
0.010
1
08/12/19 15:34
ADM
SW-DRYWT
Ammonia Nitrogen
3100
mg/Kg - dry
221
1
08/20/19 15:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<41.7
mg/Kg - dry
41.7
41.7
1
08/20/19 14:37
ZBD
4500NO3F-2011
Organic N
11900
mg/Kg - dry
9.20
461
1
08/16/19 16:40
CALCULATION -
pH
6.4
S.U.
1
08/20/19 07:13
JSL
9045D
Total Solids
11.3
%
0.010
0.010
1
08/12/19 15:34
ADM
2540G-2011
Total Volatile Solids
22.2
%
0.010
0.010
1
08/12/19 15:34
ADM
2540G-2011
Total Kjeldahl Nitrogen
15000
mg/Kg - dry
461
1
08/16/19 16:40
CLP 4500NORGD-2011
Phosphorus
6890
mg/Kg - dry
22.7
44.2
1
08/16/19 20:33
JTR
6010D
Aluminum
13200
mg/Kg - dry
18.0
44.2
1
08/16/19 20:33
BKN
6010D
Arsenic
3.963
mg/Kg - dry
3.71
4.42
1
08/16/19 20:33
JTR
6010D
Cadmium
0.7583
mg/Kg - dry
0.438
0.885
1
08/16/19 20:33
JTR
6010D
Calcium
9820
mg/Kg - dry
149
221
1
08/16/19 20:33
JTR
6010D
Chromium
22.2
mg/Kg - dry
1.68
2.21
1
08/16/19 20:33
JTR
6010D
Copper
205
mg/Kg - dry
1.28
2.21
1
08/16/19 20:33
JTR
6010D
Iron
16600
mg/Kg - dry
37.5
44.2
1
08/16/19 20:33
BKN
6010D
Lead
35.4
mg/Kg - dry
1.32
2.65
1
08/16/19 20:33
JTR
6010D
Magnesium
2840
mg/Kg - dry
19.6
44.2
1
08/16/19 20:33
JTR
6010D
Manganese
281
mg/Kg - dry
1.62
4.42
1
08/16/19 20:33
KKM
6010D
Mercury
0.09823
mg/Kg - dry
0.0305
0.138
1
08/16/19 13:42
TJS
7471A
Molybdenum
3.07
mg/Kg - dry
1.15
2.21
1
08/16/19 20:33
JTR
6010D
Nickel
16.1
mg/Kg - dry
1.46
2.21
1
08/16/19 20:33
JTR
6010D
Potassium
1420
mg/Kg - dry
26.4
44.2
1
08/16/19 20:33
KKM
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-221-0036
Lab No : 89567
Sample ID: Yonceyville WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Yonceyville WWTP
Information :
REPORT OF ANAL YSIS
Report Date : 08/20/2019
Received : 08/09/2019
C0"4Q� C)J�
Danyale Love
Project Manager
Matrix: Solids
Sampled: 8/8/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
4.80
mg/Kg - dry
4.34
4.42
1
08/16/19 20:33
JTR
6010D
Sodium
450
mg/Kg - dry
68.3
221
1
08/16/19 20:33
JTR
6010D
Zinc
398
mg/Kg - dry
9.56
11.1
1
08/16/19 20:33
JTR
6010D
Sulfur
6550
mg/Kg - dry
43.3
44.2
1
08/16/19 20:33
JTR
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
08/16/19 20:33
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

WayPAoint.
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-221-0036
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: #45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Kristina A. McAdams Date & Time: 08/09/2019 10:02:22
Page 5 of 6

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Page 6 of 6

Waypointo
ANALYTICAL
8/20/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-221-0037
Client Project Description: Yonceyville WTP
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www,way po inta n a lyti ca 1. co m
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 8/9/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Z� l
Page 1 of 6

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Yonceyville WTP
Lab Report Number: 19-221-0037
Date: 8/20/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Analyte: Aluminum
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L450146
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 2 of 6

0 2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Yonceyville WTP Report Date : 08/20/2019
755 Yadkinville Rd Information : Received : 08/09/2019
Mocksville , NC 27028
Report Number : 19-221-0037 REPOR T OF A NA L YSIS Danyale Love
Project Manager
Lab No : 89568
Matrix: Solids
Sample ID: Yonceyville WTP
Sampled:
8/8/2019 8:45
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
% Moisture
95.5
%
0.010
1
08/12/19 15:34
ADM
SW-DRYWT
Ammonia Nitrogen
3330
mg/Kg - dry
556
1
08/20/19 15:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<106
mg/Kg - dry
106
106
1
08/20/19 14:39
ZBD
4500NO3F-2011
Organic N
311
mg/Kg - dry
22.2
1110
1
08/16/19 16:41
CALCULATION -
pH
5.9
S.U.
1
08/20/19 07:13
JSL
9045D
Total Solids
4.48
%
0.010
0.010
1
08/12/19 15:34
ADM
2540G-2011
Total Volatile Solids
24.2
%
0.010
0.010
1
08/12/19 15:34
ADM
2540G-2011
Total Kjeldahl Nitrogen
3640
mg/Kg - dry
1110
1
08/16/19 16:41
CLP 4500NORGD-2011
Phosphorus
1640
mg/Kg - dry
57.1
111
1
08/16/19 20:38
JTR
6010D
Aluminum
140000
mg/Kg - dry
45.1
111
1
08/16/19 20:38
BKN
6010D
Arsenic
9.563
mg/Kg - dry
9.31
11.1
1
08/16/19 20:38
JTR
6010D
Cadmium
<1.10
mg/Kg - dry
1.10
2.22
1
08/16/19 20:38
JTR
6010D
Calcium
1880
mg/Kg - dry
373
556
1
08/16/19 20:38
JTR
6010D
Chromium
44.9
mg/Kg - dry
4.22
5.56
1
08/16/19 20:38
JTR
6010D
Copper
52.2
mg/Kg - dry
3.22
5.56
1
08/16/19 20:38
JTR
6010D
Iron
40700
mg/Kg - dry
94.2
111
1
08/16/19 20:38
BKN
6010D
Lead
21.5
mg/Kg - dry
3.31
6.67
1
08/16/19 20:38
JTR
6010D
Magnesium
1720
mg/Kg - dry
49.3
111
1
08/16/19 20:38
JTR
6010D
Manganese
1270
mg/Kg - dry
4.07
11.1
1
08/16/19 20:38
KKM
6010D
Mercury
<0.0716
mg/Kg - dry
0.0716
0.324
1
08/16/19 13:43
TJS
7471A
Molybdenum
<2.89
mg/Kg - dry
2.89
5.56
1
08/16/19 20:38
JTR
6010D
Nickel
19.7
mg/Kg - dry
3.67
5.56
1
08/16/19 20:38
JTR
6010D
Potassium
871
mg/Kg - dry
66.2
111
1
08/17/19 13:52
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 3 of 6

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 19-221-0037
Lab No : 89568
Sample ID: Yonceyville WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Yonceyville WTP
Information :
REPORT OF ANAL YSIS
Report Date : 08/20/2019
Received : 08/09/2019
C0 ,' &C)J�
Danyale Love
Project Manager
Matrix: Solids
Sampled: 8/8/2019 8:45
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<10.9
mg/Kg - dry
10.9
11.1
1
08/16/19 20:38
JTR
6010D
Sodium
3273
mg/Kg - dry
172
556
1
08/16/19 20:38
JTR
6010D
Zinc
89.1
mg/Kg - dry
24.0
27.8
1
08/16/19 20:38
JTR
6010D
Sulfur
2510
mg/Kg - dry
109
111
1
08/16/19 20:38
JTR
6010D
Sodium Absorption Ratio
<2.22
Ratio
2.22
5.00
1
08/16/19 20:38
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 4 of 6

WayPAoint.
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-221-0037
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: #45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Kristina A. McAdams Date & Time: 08/09/2019 10:04:18
Page 5 of 6

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Page 6 of 6

aceAnalytical o ANALYTICAL REPORT
National Center for Testing & Innovation August 21, 2019
• #r
EMA Resources
Sample Delivery Group: L1127514
Samples Received: 08/09/2019
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: ak-
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
16
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 1 of 21

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
YONCEYVILLE L1127514-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
2
3
4
5
5
7
7
8
9
10
11
12
13
15
16
17
19
20
21
CID
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 2 of 21

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
YONCEYVILLE L1127514-01 Waste Brent Collins 08/08/1908:30 08/09/1908:45 , C
P
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1328392
1 08/14/1912:00
08/14/1912:00
TM
Mt. Juliet, TN
Preparation by Method 1311
WG1329134
1 08/15/1910:14
08/15/1910:14
RT
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1331094
1 08/19/1913:48
08/19/1917:22
JER
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1324663
1 08/12/1916:35
08/12/1916:35
BAM
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1329770
1 08/16/1911:38
08/16/1914:15
ANP
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1328160
1 08/19/1915:00
08/19/1915:00
BAM
Mt. Juliet, TN
Mercury by Method 7470A
WG1329769
1 08/16/19 08:04
08/16/1913:03
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1329850
1 08/16/19 09:51
08/16/1912:11
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1329075
1 08/15/1916:59
08/15/1916:59
BMB
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1329756
1 08/16/19 08:29
08/17/19 09:52
LEL
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1330623
1 08/18/19 07:56
08/20/1910:44
LEL
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1330616
1 08/18/1914:38
08/19/19 03:03
AO
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1127514
08/21/1910:22
3 of 21
FTC
M
[Cn]
FSr
RC
F,
FAI
FSC

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
FSr
FC-1
�GI
Justin Carr rAl
Project Manager
FSC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 4 of 21

YONCEYVILLE
Collected date/time: 08/08/19 08:30
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 6.99
Final pH 4.98
Wet Chemistry by Method 9012 B
SAMPLE RESULTS - 01
L1127514
Qualifier Prep
Batch
date / time
8/15/201910:14:37 AM
WG1329134
8/14/201912:00:11 PM
WG1328392
8/15/201910:14:37 AM
WG1329134
8/15/201910:14:37 AM
WG1329134
8/15/201910:14:37 AM
WG1329134
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide 110
25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/19/201917:22 WG1331094
Dilution Analysis Batch
date / time
1 08/12/201916:35 WG1324663
Result Qualifier
Dilution Analysis
Analyte su
date / time
Corrosivity by pH 7.04 T8
1 08/16/201914:15
Sample Narrative:
L1127514-01 WG1329770: 7.04 at 22AC
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Analyte Deg. F
date / time
Batch
WG1329770
Batch
Ignitability DNI at 170 1 08/19/201915:00 WG1328160
Mercury by Method 7470A
Result
Analyte mg/I
Mercury ND
Metals (ICP) by Method 6010D
Qualifier RDL Limit
mg/I mg/I
0.0100 0.20
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.258
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Benzene
Carbon tetrachloride
Chlorobenzene
Result
Qualifier RDL
Limit
mg/I
mg/I
mg/I
ND
0.0500
0.50
ND
0.0500
0.50
ND
0.0500
100
ND
0.250
6
ACCOUNT: PROJECT
EMA Resources
Dilution Analysis Batch
date / time
1 08/16/201913:03 WG1329769
Dilution Analysis Batch
date / time
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
1 08/16/201912:11
WG1329850
ONE LAB. NATIONWIDE.
Cp
FTc
FSS
4
Cn
Fc
7G1
FAI
FSC
Dilution Analysis
Batch
date / time
1 08/15/201916:59
WG1329075
1 08/15/201916:59
WG1329075
1 08/15/201916:59
WG1329075
1 08/15/201916:59
WG1329075
SDG:
DATE/TIME: PAGE:
L1127514
08/21/1910:22 5 of 21

ONE LAB. NATIONWIDE.
YONCEYVILLE SAMPLE RESULTS - 01
Collected date/time: 08/08/19 08:30 L1127514
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1 08/15/201916:59
WG1329075
1,1-Dichloroethene
ND
0.0500
0.70
1 08/15/201916:59
WG1329075
2-Butanone (MEK)
ND
0.500
200
1 08/15/201916:59
WG1329075
Tetrachloroethene
ND
0.0500
0.70
1 08/15/201916:59
WG1329075
Trichloroethene
ND
0.0500
0.50
1 08/15/201916:59
WG1329075
Vinyl chloride
ND
0.0500
0.20
1 08/15/201916:59
WG1329075
(S) Toluene-d8
97.1
80.0-120
081151201916.59
WG1329075
(S) 4-Bromof/uorobenzene
90.7
77.0-126
081151201916.59
WG1329075
(S)1,2-Dichloroethane-d4
107
70.0-130
081151201916.59
WG1329075
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5-TP (Silvex)
ND
0.00200
1
1 08/17/2019 09:52
WG1329756
2,4-D
ND
0.00200
10
1 08/17/2019 09:52
WG1329756
(S)2,4-Dich/oropheny/Acetic Acid
65.8
14.0-158
081171201909:52
WG1329756
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1 08/20/201910:44
Endrin
ND
0.00500
0.02
1 08/20/201910:44
Heptachlor
ND
0.00500
0.0080
1 08/20/201910:44
Lindane
ND
0.00500
0.40
1 08/20/201910:44
Methoxychlor
ND
0.00500
10
1 08/20/201910:44
Toxaphene
ND
0.0100
0.50
1 08/20/201910:44
(S) Decachlorobipheny/
77.9
10.0-128
081201201910:44
(S) Tetrach/oro-m-xylene
54.8
10.0-127
081201201910.44
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Batch
WG1330623
WG1330623
WG1330623
WG1330623
WG1330623
WG1330623
WG1330623
WG1330623
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 08/19/2019 03:03
WG1330616
2,4-Dinitrotoluene
ND
0.100
0.13
1 08/19/2019 03:03
WG1330616
Hexachlorobenzene
ND
0.100
0.13
1 08/19/2019 03:03
WG1330616
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 08/19/2019 03:03
WG1330616
Hexachloroethane
ND
0.100
3
1 08/19/2019 03:03
WG1330616
Nitrobenzene
ND
0.100
2
1 08/19/2019 03:03
WG1330616
Pyridine
ND
0.100
5
1 08/19/2019 03:03
WG1330616
3&4-Methyl Phenol
ND
J4 0.100
400
1 08/19/2019 03:03
WG1330616
2-Methylphenol
ND
0.100
200
1 08/19/2019 03:03
WG1330616
Pentachlorophenol
ND
0.100
100
1 08/19/2019 03:03
WG1330616
2,4,5-Trichlorophenol
ND
0.100
400
1 08/19/2019 03:03
WG1330616
2,4,6-Trichlorophenol
ND
0.100
2
1 08/19/2019 03:03
WG1330616
(S) 2-Fluorophenol
23.4
10.0-120
0811912019 03:03
WG1330616
(S) Phenol-d5
14.5
10.0-120
0811912019 03:03
WG1330616
(S) Nitrobenzene-d5
39.1
10.0-127
0811912019 03:03
WG1330616
(S) 2-F/uorobipheny/
46.6
10.0-130
0811912019 03:03
WG1330616
(S) 2,4,6- Tribromophenol
48.7
10.0-155
0811912019 03:03
WG1330616
(S) p-Terphenyl-d14
64.1
10.0-128
0811912019 03:03
WG1330616
Fp
FTc
FS
Fn
Fc
F ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 6 of 21

WG1331094
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3441944-1 08/19/1917:07
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1127463-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1127463-08 08/19/19 17:20 • (DUP) R3441944-5 08/19/1917:21
Original Result DUP Result Dilution DUP RPD
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.000 1 0.000
L1128327-02 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1127514-01
DUP Qualifier DUP RPD
Limits
20
(OS) L1128327-02 08/19/1917:33 • (DUP) R3441944-6 08/19/1917:34
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide 0.788 0.781 1 0.828 20
Laboratory Control Sample (LCS)
(LCS) R3441944-2 08/19/1917:08
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.60 104 50.0-150
L1127463-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127463-06 08/19/1917:15 • (MS) R3441944-3 08/19/1917:16 • (MSD) R3441944-4 08/19/1917:19
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg % %
Reactive Cyanide 1.67 ND 1.48 1.50 89.1 90.1
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 1.11
L1128327-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1128327-04 08/19/1917:35 • (MS) R3441944-7 08/19/1917:36 • (MSD) R3441944-8 08/19/1917:37
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg % %
Reactive Cyanide 1.67 0.598 1.07 0.924 28.2 19.5
ACCOUNT: PROJECT:
EMA Resources
ONE LAB. NATIONWIDE.
RPD Limits
20
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 75.0-125 J6 J6 14.4 20
SDG: DATE/TIME: PAGE:
L1127514 08/21/1910:22 7 of 21
- I
Cp
FTc
FSS
4
— Cn
FSr
— 7G1
FAI
FSC

WG1324663
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3439694-1 08/12/19 16:35
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 7.63
L1126032-01 Original Sample (OS) • Duplicate (DUP)
MB RDL
mg/kg
25.0
(OS) L1126032-01 08/12/1916:35 • (DUP) R3439694-3 08/12/1916:35
Original Result DUP Result Dilution DUP RPD
Analyte mg/kg mg/kg %
Reactive Sulfide 97.0 95.6 1 1.49
Laboratory Control Sample (LCS)
(LCS) R3439694-2 08/12/1916:35
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg %
Reactive Sulfide 100 89.8 89.8
QUALITY CONTROL SUMMARY
L1127514-01
DUP Qualifier DUP RPD
Limits
o�
20
Rec. Limits LCS Qualifier
70.0-130
ONE LAB. NATIONWIDE.
— I
Cp
FTc
FSS
4
— Cn
FSr
— 7G1
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 8 of 21

WG1329770
Wet Chemistry by Method 9045D
Laboratory Control Sample (LCS)
(LCS) R3441236-1 08/16/1914:15
Spike Amount LCS Result
Analyte su su
Corrosivity by pH 10.0 9.93
Sample Narrative:
LCS: 9.93 at 21.2C
QUALITY CONTROL SUMMARY
L1127514-01
LCS Rec. Rec. Limits LCS Qualifier
99.3 99.0-101
ONE LAB. NATIONWIDE.
FP1
FTC
FSS
4
Cn
FSr
7G1
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 9 of 21

WG1328160 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1127514-01
L1127463-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1127463-03 08/19/1915:00 • (DUP) R3441865-2 08/19/1915:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F % %
Ignitability DNIat170 DNIat170 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3441865-1 08/19/1915:00
Spike Amount LCS Result LCS Rec.
Analyte Deg. F Deg. F %
Ignitability 82.0 81.9 99.9
Rec. Limits LCS Qualifier
96.0-104
ONE LAB. NATIONWIDE.
- I
Cp
FTC
FSS
4
Cn
FSr
7G1
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 10 of 21

WG1329769
Mercury by Method 7470A
Method Blank (MB)
(MB) R3441197-1 08/16/1912:36
MB Result
Analyte mg/1
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00330 0.0100
QUALITY CONTROL SUMMARY
L1127514-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3441197-2 08/16/1912:38 • (LCSD) R3441197-3 08/16/1912:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
Mercury 0.0300 0.0316 0.0301 105 100 80.0-120 4.87 20
L1127452-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127452-02 08/16/1912:42 • (MS) R3441197-4 08/16/1912:44 • (MSD) R3441197-5 08/16/1912:46
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I mg/I mg/I mg/I % % % %
Mercury 0.0300 ND 0.0311 0.0315 104 105 1 75.0-125 1.13
ONE LAB. NATIONWIDE.
RPD Limits
20
- I
Cp
FTc
FSS
4
— Cn
FSr
— 7G1
— $AI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 11 of 21

WG1329850
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3441179-1 08/16/1912:03
MB Result
Analyte mg/I
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
U
U
U
U
U
0.0366
U
MB Qualifier MB MDL
mg/I
0.0330
0.0330
0.0330
0.0330
0.0330
J 0.0330
0.0330
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
QUALITY CONTROL SUMMARY
L1127514-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3441179-2 08/16/1912:06 • (LCSD) R3441179-3 08/16/1912:08
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Arsenic
10.0
10.1
10.0
101
100
80.0-120
0.713
20
Barium
10.0
10.4
10.3
104
103
80.0-120
0.769
20
Cadmium
10.0
10.1
9.98
101
99.8
80.0-120
0.817
20
Chromium
10.0
9.85
9.79
98.5
97.9
80.0-120
0.569
20
Lead
10.0
10.0
9.98
100
99.8
80.0-120
0.443
20
Selenium
10.0
10.3
10.3
103
103
80.0-120
0.0531
20
Silver
2.00
1.94
1.93
97.2
96.5
80.0-120
0.781
20
L1127514-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127514-01 08/16/1912:11 • (MS) R3441179-5 08/16/1912:16 • (MSD) R3441179-6 08/16/1912:19
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
9.96
9.94
99.6
99.4
Barium
10.0
0.258
10.5
10.3
102
101
Cadmium
10.0
ND
9.93
9.85
99.3
98.5
Chromium
10.0
ND
9.66
9.58
96.6
95.8
Lead
10.0
ND
9.96
9.85
99.6
98.5
Selenium
10.0
ND
10.2
10.2
102
102
Silver
2.00
ND
1.92
1.92
96.1
95.9
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 75.0-125
0.248
1 75.0-125
1.07
1 75.0-125
0.852
1 75.0-125
0.865
1 75.0-125
1.12
1 75.0-125
0.110
1 75.0-125
0.241
ONE LAB. NATIONWIDE.
RPD Limits
20
20
20
20
20
20
20
FP1
FTc
FSS
4
Cn
FSr
7G1
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 12 of 21

WG1329075
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3440824-3 08/15/1912:29
QUALITY CONTROL SUMMARY
L1127514-01
ONE LAB. NATIONWIDE.
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Benzene U
0.0165
0.0500
Carbon tetrachloride U
0.0165
0.0500
Chlorobenzene U
0.0165
0.0500
Chloroform U
0.0825
0.250
1,2-Dichloroethane U
0.0165
0.0500
1,1-Dichloroethene U
0.0165
0.0500
2-Butanone (MEK) U
0.165
0.500
Tetrachloroethene U
0.0165
0.0500
Trichloroethene U
0.0165
0.0500
Vinyl chloride U
0.0165
0.0500
(S) Toluene-d8 102
80.0-120
(S) 4-Bromof/uorobenzene 94.3
77.0-126
(S)1,2-Dichloroethane-d4 106
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3440824-1 08/15/19 07:06
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Benzene 0.0250
0.0257
103
70.0-123
Carbon tetrachloride 0.0250
0.0239
95.7
68.0-126
Chlorobenzene 0.0250
0.0221
88.2
80.0-121
Chloroform 0.0250
0.0258
103
73.0-120
1,2-Dichloroethane 0.0250
0.0294
118
70.0-128
1,1-Dichloroethene 0.0250
0.0237
94.6
71.0-124
2-Butanone (MEK) 0.125
0.154
123
44.0-160
Tetrachloroethene 0.0250
0.0213
85.0
72.0-132
Trichloroethene 0.0250
0.0265
106
78.0-124
Vinyl chloride 0.0250
0.0271
108
67.0-131
(S) Toluene-d8
86.1
80.0-120
(S) 4-Bromofluorobenzene
90.7
77.0-126
(S)1,2-Dichloroethane-d4
121
70.0-130
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1127514 08/21/1910:22 13 of 21
FP1
FTC
FSS
4
Cn
FSr
7G1
FAI
FSC

WG1329075
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D
L1127514-01
L1127514-01 Original Sample (OS) • Matrix Spike (MS)
• Matrix
Spike Duplicate (MSD)
FP1
(OS) L1127514-01 08/15/1916:59 • (MS) R3440824-4 08/15/1917:19 • (MSD) R3440824-5 08/15/1917:39
Spike Amount Original Result MS Result
MSD Result MS Rec.
MSD Rec. Dilution
Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte mg/I mg/I mg/I
mg/I
%
%
%
%
%
FTc
Benzene 1.25 ND 1.03
1.06
82.5
84.3 1
17.0-158
2.19
27
Carbon tetrachloride 1.25 ND 1.04
0.991
82.9
79.2 1
23.0-159
4.54
28
FSS
Chlorobenzene 1.25 ND 0.935
0.975
74.8
78.0 1
33.0-152
4.24
27
Chloroform 1.25 ND 1.02
1.05
81.9
84.2 1
29.0-154
2.78
28
1,2-Dichloroethane 1.25 ND 1.27
1.29
102
103 1
29.0-151
1.77
27
rCn
1,1-Dichloroethene 1.25 ND 0.965
0.924
77.2
74.0 1
11.0-160
4.28
29
2-Butanone (MEK) 6.25 ND 6.74
6.89
108
110 1
10.0-160
2.14
32
FSr
Tetrachloroethene 1.25 ND 0.869
0.904
69.5
72.3 1
10.0-160
3.92
27
Trichloroethene 1.25 ND 0.971
1.02
77.6
81.6 1
10.0-160
4.96
25
Vinyl chloride 1.25 ND 1.05
1.07
83.9
85.2 1
10.0-160
1.58
27
(S) Toluene-d8
90.2
92.3
80.0-120
(S) 4-Bromof/uorobenzene
91.4
94.5
77.0-126
7 G
(S)1,2-Dichloroethane-d4
115
117
70.0-130
rAl
L1127493-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1127493-01 08/15/1916:40 • (MS) R3440824-6 08/15/1917:59
[ScSpike
Amount Original Result MS Result
MS Rec.
Dilution
Rec. Limits MS Qualifier
Analyte mg/I mg/I mg/I
%
%
Benzene 1.25 ND 1.18
94.4
1
17.0-158
Carbon tetrachloride 1.25 ND 1.12
89.6
1
23.0-159
Chlorobenzene 1.25 ND 0.995
79.6
1
33.0-152
Chloroform 1.25 ND 1.18
94.7
1
29.0-154
1,2-Dichloroethane 1.25 ND 1.38
110
1
29.0-151
1,1-Dichloroethene 1.25 ND 1.09
87.2
1
11.0-160
2-Butanone (MEK) 6.25 ND 7.39
118
1
10.0-160
Tetrachloroethene 1.25 ND 0.939
75.1
1
10.0-160
Trichloroethene 1.25 ND 1.11
88.9
1
10.0-160
Vinyl chloride 1.25 ND 1.24
98.8
1
10.0-160
(S) Toluene-d8
86.7
80.0-120
(S) 4-Bromofluorobenzene
88.7
77.0-126
(S)1,2-Dichloroethane-d4
120
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1127514
08/21/1910:22
14 of 21

WG1329756
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3441502-1 08/17/19 07:39
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S)2,4-Dichloropheny/Acetic 68.4
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
■
QUALITY CONTROL SUMMARY
L1127514-01
MB RDL
mg/I
0.00200
0.00200
14.0-158
(LCS) R3441502-2 08/17/19 08:09
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
2,4-D 0.0500
0.0409
81.8
50.0-120 P
2,4,5-TP (Silvex) 0.0500
0.0407
81.4
50.0-125 P
(S) 2,4-Dichloropheny/Acetic
75.6
14.0-158
Acid
L1127267-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127267-01 08/17/19 08:23 • (MS) R3441502-3 08/17/19 08:38 • (MSD) R3441502-4 08/17/19 08:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
2,4-D
0.0500
U
0.0415
0.0380
83.0
76.0
2,4,5-TP (Silvex)
0.0500
U
0.0406
0.0379
81.2
75.8
(S)2,4-Dichloropheny/Acetic
71.6
70.8
Acid
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 50.0-120 P P 8.81
1 50.0-125 P P 6.88
14.0-158
ONE LAB. NATIONWIDE.
RPD Limits
o�
20
20
FP1
FTc
3
SS
4
Cn
FSr
7G1
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 15 of 21

WG1330623
Pesticides (GC) by Method 8081B
Method Blank (MB)
(MB) R3442248-2 08/20/19 09:30
MB Result
Analyte
mg/I
Gamma BHC
U
Endrin
U
Heptachlor
U
Methoxychlor
U
Chlordane
U
Toxaphene
U
(S) Decachlorobipheny/ 81.6
(S) Tetrach/oro-m-xy/ene 51.2
MB Qualifier MB MDL MB RDL
mg/I mg/I
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1127514-01
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00333
0.0100
10.0-128
10.0-127
(LCS) R3442248-1 08/20/19 09:16
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
%
%
Gamma BHC
0.0100
0.00711
71.1
55.0-129
Endrin
0.0100
0.00808
80.8
57.0-134
Heptachlor
0.0100
0.00692
69.2
27.0-132
Methoxychlor
0.0100
0.00824
82.4
54.0-155
(S) Decachlorobiphenyl
66.5
10.0-128
(S) Tetroch/oro-m-xy/ene
43.0
10.0-127
L1126991-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1126991-01 08/20/1910:00 • (MS) R3442248-3 08/20/1910:15 • (MSD) R3442248-4 08/20/1910:29
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Gamma BHC
0.0100
ND
0.00737
0.00938
73.7
93.8
Endrin
0.0100
ND
0.00809
0.0103
80.9
103
Heptachlor
0.0100
ND
0.00719
0.00914
71.9
91.4
Methoxychlor
0.0100
ND
0.00842
0.0105
84.2
105
(S) Decachlorobipheny/
72.8
91.4
(S) Tetrach/oro-m-xylene
44.3
62.2
Dilution Rec. Limits
14.0-141
10.0-160
16.0-136
10.0-160
10.0-128
10.0-127
MS Qualifier MSD Qualifier RPD
24.0
24.0
23.9
22.0
ONE LAB. NATIONWIDE.
RPD Limits
39
40
34
FP1
FTc
FSS
4
Cn
FSr
7G1
FAI
[Sc
ACCOUNT: PROJECT:
EMA Resources
SDG:
L1127514
DATE/TIME:
08/21/1910:22
PAGE:
16 of 21

WG1330616 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1127514-01
Method Blank (MB)
(MB) R3441858-2 08/19/1910:55
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
27.5
10.0-127
(S) 2-F/uorobipheny/
29.1
10.0-130
(S) p-Terphenyl-d14
73.4
10.0-128
(S) Phenol-d5
7.20
J2
10.0-120
(S) 2-Fluorophenol
12.9
10.0-120
(S)2,4,6-Tribromopheno/
29.2
10.0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE.
(LCS) R3441858-1 08/19/1910:33
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.136
27.2
18.0-120
2,4-Dinitrotoluene 0.500
0.309
61.8
49.0-124
Hexachlorobenzene 0.500
0.287
57.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.124
24.8
19.0-120
Hexachloroethane 0.500
0.110
22.0
15.0-120
Nitrobenzene 0.500
0.197
39.4
27.0-120
Pyridine 0.500
0.149
29.8
10.0-120
2-Methylphenol 0.500
0.141
28.2
28.0-120
3&4-Methyl Phenol 0.500
0.146
29.2
31.0-120 J4
Pentachlorophenol 0.500
0.280
56.0
23.0-120
2,4,5-Trichlorophenol 0.500
0.286
57.2
44.0-120
2,4,6-Trichlorophenol 0.500
0.259
51.8
42.0-120
(S) Nitrobenzene-d5
42.9
10.0-127
(S) 2-F/uorobipheny/
4t 3
10.0-130
(S) p-Terphenyl-d14
65.1
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1127514 08/21/1910:22 17 of 21
FP1
FTC
FSS
4
Cn
FSr
7G1
FAI
FSC

WG1330616 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1127514-01
Laboratory Control Sample (LCS)
(LCS) R3441858-1 08/19/1910:33
Spike Amount LCS Result
Analyte mg/I mg/I
(S) Phenol-d5
(S) 2-Fluorophenol
(S) 2,4,6-Tribromophenol
LCS Rec. Rec. Limits LCS Qualifier
10.3 10.0-120
18.1 10.0-120
56.5 10.0-155
L1127514-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127514-01 08/19/19 03:03 • (MS) R3441867-1 08/19/19 03:24 • (MSD) R3441867-2 08/19/19 03:45
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.185
0.141
37.0
28.2
1 17.0-120
2,4-Dinitrotoluene
0.500
ND
0.365
0.365
73.0
73.0
1 39.0-125
Hexachlorobenzene
0.500
ND
0.346
0.342
69.2
68.4
1 35.0-122
Hexachloro-1,3-butadiene
0.500
ND
0.174
0.125
34.8
25.0
1 12.0-120
Hexachloroethane
0.500
ND
0.155
0.110
31.0
22.0
1 10.0-120
Nitrobenzene
0.500
ND
0.244
0.205
48.8
41.0
1 12.0-120
Pyridine
0.500
ND
0.128
0.119
25.6
23.8
1 10.0-120
2-Methylphenol
0.500
ND
0.195
0.184
39.0
36.8
1 10.0-120
3&4-Methyl Phenol
0.500
ND
0.203
0.195
40.6
39.0
1 10.0-120
Pentachlorophenol
0.500
ND
0.325
0.318
65.0
63.6
1 10.0-128
2,4,5-Trichlorophenol
0.500
ND
0.371
0.341
74.2
68.2
1 33.0-120
2,4,6-Trichlorophenol
0.500
ND
0.313
0.288
62.6
57.6
1 26.0-120
(S) Nitrobenzene-d5
52.9
42.3
10.0-127
(S) 2-F/uorobipheny/
55.6
477
10.0-130
(S) p-Terphenyl-d14
72.1
70.0
10.0-128
(S) Phenol-d5
16.5
14.1
10.0-120
(S) 2-F/uorophenol
24.5
20.7
10.0-120
(S)2,4,6-Tribromophenol
68.5
66.0
10.0-155
MS Qualifier MSD Qualifier RPD
27.0
0.000
1.16
32.8
34.0
17.4
7.29
5.80
4.02
2.18
8.43
8.32
ONE LAB. NATIONWIDE.
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
FP1
FTc
FSS
[Cn]
FSr
7G1
FAI
[Sc
ACCOUNT: PROJECT:
EMA Resources
SDG:
L1127514
DATE/TIME:
08/21/1910:22
PAGE:
18 of 21

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
CP
IP
FTC
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
[Cn]
RDL
Reported Detection Limit.
Rec.
Recovery.
FSr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
6
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
J2
Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4
The associated batch QC was outside the established quality control range for accuracy.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P
RPD between the primary and confirmatory analysis exceeded 40%.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1127514 08/21/1910:22 19 of 21

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
ME
MT NO
OR MN
T ID t WI NY
SD
WY MI
NV
t NE IA OH PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
N
NM O� AR SC
T MS AL`7GA
T TX * LA
T
AK
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1127514 08/21/1910:22 20 of 21

Billing Information:
Analysis/Container/Preservative
Chain of Custody Fag, o!_
EMA Resources
Mr. Brent Collins Pres
755 Yadkinville Road Chk
; '
755 Yadkinville Road
Mocksville, INC 27028
�aceAnajfyfical Nm..we.,e�arannroam,�.,'mn
Mocksville, NC 27028
12055 Lebanon Rd
Report to:
Email To: brentcollins@emaresourcesinccam
Mr. Brent Collins
Mount lul¢t, TN 37122 W. G5
Rvan 615 ]585858 �i�
RNon<: Btp-06L5859 O
615 ]58d859
Project
Cltlie Idle
Collected: .IIraa:
Description:
gnC[yv;
I'
L # (1 -? W
Phone: [phone]
Client Project #
Lab Project #
Fax: [phone]
J244
v
Collected by (print):
Site/Facility to
P.O.#
pr�n+/allhs
o
Acctnum: EMARES
CJ Co
an
`
?
G
Te
P68963
Collectedb
Rush] (Lab MUST Be Notified) Quote p
Same Day Day
a
O
u
�
Prelo in: P689635
login:
6
_Five
_ Next Day _ 5 Day (Rad Only) Date Results Needed
Z
TSR: 702 - C/ass ndra Foster
Immediately /
✓
Two Day _10 Day Iliad Only) No.
Day
U
a
I/l, /�!
PB: `�(
Packed on Ice N Y
_Three Of
J
"
a
Shipped via: Fed EX Ground
Sample lD
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
Re:—s:
Sample alrbo.dyl
Y'ona
C
SS
5
frh//9
8'3Db
2
X
X
-611
ey:)fit
I
---
--
—,,
' Matrix:Remarks:
— — —
.1 e` k
CDC Seal Present/Intact: _NE _t _N
SS - Soil AIR - Air F- Filter
pH Temp
GW-GlOUndWafe! B- Bloa$$ay
CDC Signed/Accurate: L _NY
^
WW - Waste Water
Flow Other
Bottles arrive intact: N
Correct bottles used: 2y _N
DW-DrinkingI at
OT Other -S a4e—
Samples returned via: `,t
l,l
Sufficient volume sent: /'Y _N
if able
-
_UPS _FedEx _Courier Tracking# (SoQ2J v15
l� lJ
VCA Zero Headspace: Y N
ace:
Preservation Ccrrect/checked: Y _N
Relinquished by: )Signature)
Date-
Time.
Received by: (Signature)
Trip Blank Received: Yes
r,18.119
3.Ognn
H MeoH
MD SCREEN: <0.5 mWh-
TBR
Relinquished by: (Signature)
Date.
time.
Received by: (Signaoire)
Temp: oC Bottles Received:
If preservation required by Login: Date/Time
Relinquished by (Signature)
Date:
Time.
Received for la y: ;Signature)
Date: Time:
Hold:
Conditio
V` I^ 9 , tF
NCF / OK
FA

aceAnalytical o
National Center for Testing & Innovation
• #r
ANALYTICAL REPORT
December 19. 2019
EMA Resources
Sample Delivery Group:
Samples Received:
Project Number:
Description:
L1169199
12/06/2019
Yanceyville WTP
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: ak-
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
16
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 1 of 23

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
YANCEYVILL WTP L1169199-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
8
9
10
11
12
13
15
16
17
19
20
21
Fn
FS
[Cn]
Fr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1169199 12/19/19 14:05
PAGE:
2 of 23

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
YANCEYVILL WTP L1169199-01 Waste Brent Collins 12/05/1908:30 12/06/1908:30 , C
P
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Batch
Dilution Preparation
date/time
Analysis
date/time
Analyst
Location
WG1395242
1 12/12/19 08:26
12/12/19 08:26
BAA
Mt. Juliet, TN
WG1396147
1 12/13/1912:51
12/13/1912:51
CGD
Mt. Juliet, TN
WG1396907
1 12/15/19 08:00
12/18/1919:37
SDL
Mt. Juliet, TN
WG1395273
1 12/13/19 01:00
12/13/19 01:00
LDT
Mt. Juliet, TN
WG1395945
1 12/13/1915:23
12/13/1916:10
JIC
Mt. Juliet, TN
WG1395517
1 12/16/1915:00
12/16/1915:00
SL
Mt. Juliet, TN
WG1396177
1 12/14/1918:08
12/16/1913:08
ABL
Mt. Juliet, TN
WG1396694
1 12/14/1916:53
12/16/19 03:46
CCE
Mt. Juliet, TN
WG1396052
1 12/13/19 20:53
12/13/19 20:53
ADM
Mt. Juliet, TN
WG1397171
1 12/16/19 09:17
12/17/19 03:01
LEL
Mt. Juliet, TN
WG1396828
1 12/15/19 07:29
12/15/1919:05
HMH
Mt. Juliet, TN
WG1397451
1 12/18/19 05:51
12/18/1917:20
LEA
Mt. Juliet, TN
FTC
M
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 3 of 23

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
FSr
FC-1
�GI
Justin Carr rAl
Project Manager
FSC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 4 of 23

YANCEYVILL WTP
Collected date/time: 12/05/19 08:30
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 7.04
Final pH 4.96
Wet Chemistry by Method 9012 B
SAMPLE RESULTS - 01
11169199
Qualifier Prep
Batch
date / time
12/13/201912:51:32 PM
WG1396147
12/12/2019 8:26:16 AM
WG1395242
12/13/201912:51:32 PM
WG1396147
12/13/201912:51:32 PM
WG1396147
12/13/201912:51:32 PM
WG1396147
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND J3 J6
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 12/18/201919:37 WG1396907
Dilution Analysis Batch
date / time
1 12/13/2019 01:00 WG1395273
Result Qualifier
Dilution Analysis
Analyte su
date / time
Corrosivity by pH 7.46 T8
1 12/13/201916:10
Sample Narrative:
L1169199-01 WG1395945: 7.46 at 20.5C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Analyte Deg. F
date / time
Batch
WG1395945
Batch
Ignitability DNI at 170 1 12/16/201915:00 WG1395517
Mercury by Method 7470A
Result
Analyte mg/I
Mercury ND
Metals (ICP) by Method 6010D
Qualifier RDL Limit
mg/I mg/I
0.0100 0.20
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
0.142
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Benzene
Carbon tetrachloride
Chlorobenzene
Result
Qualifier RDL
Limit
mg/I
mg/I
mg/I
ND
0.0500
0.50
ND
0.0500
0.50
ND
0.0500
100
ND
0.250
6
ACCOUNT: PROJECT
EMA Resources
Dilution Analysis Batch
date / time
1 12/16/201913:08 WG1396177
Dilution Analysis
Batch
date / time
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
1 12/16/2019 03:46
WG1396694
ONE LAB. NATIONWIDE.
FP1
FTc
FSS
4
Cn
Fc
R,
FAI
FSC
Dilution Analysis
date / time
Batch
1 12/13/2019 20:53
WG1396052
1 12/13/2019 20:53
WG1396052
1 12/13/2019 20:53
WG1396052
1 12/13/2019 20:53
WG1396052
SDG:
DATE/TIME: PAGE:
L1169199
12/19/19 14:05 5 of 23

ONE LAB. NATIONWIDE.
YANCEYVILL WTP SAMPLE RESULTS - 01
Collected date/time: 12/05/19 08:30 L1169199
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1 12/13/2019 20:53
WG1396052
1,1-Dichloroethene
ND
0.0500
0.70
1 12/13/2019 20:53
WG1396052
2-Butanone (MEK)
ND
0.500
200
1 12/13/2019 20:53
WG1396052
Tetrachloroethene
ND
0.0500
0.70
1 12/13/2019 20:53
WG1396052
Trichloroethene
ND
0.0500
0.50
1 12/13/2019 20:53
WG1396052
Vinyl chloride
ND
0.0500
0.20
1 12/13/2019 20:53
WG1396052
(S) Toluene-d8
92.4
80.0-120
1211312019 20:53
WG1396052
(S) 4-Bromof/uorobenzene
105
77.0-126
1211312019 20:53
WG1396052
(S)1,2-Dichloroethane-d4
116
70.0-130
1211312019 20:53
WG1396052
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5-TP (Silvex)
ND
0.00200
1
1 12/17/2019 03:01
WG1397171
2,4-D
ND
0.00200
10
1 12/17/2019 03:01
WG1397171
(S)2,4-Dich/oropheny/Acetic Acid
18.7
14.0-158
121171201903.01
WG1397171
Pesticides (GC) by Method 8081B
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Chlordane
ND
0.00500
0.03
Endrin
ND
0.00500
0.02
Heptachlor
ND
0.00500
0.0080
Lindane
ND
0.00500
0.40
Methoxychlor
ND
0.00500
10
Toxaphene
ND
0.0100
0.50
(S) Decachlorobipheny/
108
10.0-128
(S) Tetrach/oro-m-xylene
70.6
10.0-127
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
ND
0.100
7.50
2,4-Dinitrotoluene
ND
0.100
0.13
Hexachlorobenzene
ND
0.100
0.13
Hexachloro-1,3-butadiene
ND
0.100
0.50
Hexachloroethane
ND
0.100
3
Nitrobenzene
ND
0.100
2
Pyridine
ND
0.100
5
3&4-Methyl Phenol
ND
0.100
400
2-Methylphenol
ND
0.100
200
Pentachlorophenol
ND
0.100
100
2,4,5-Trichlorophenol
ND
0.100
400
2,4,6-Trichlorophenol
ND
0.100
2
(S) 2-Fluorophenol
45.1
10.0-120
(S) Phenol-d5
27.4
10.0-120
(S) Nitrobenzene-d5
65.1
10.0-127
(S) 2-F/uorobipheny/
75.1
10.0-130
(S) 2,4,6-Tribromophenol
80.0
10.0-155
(S) p-Terphenyl-d14
87.3
10.0-128
Dilution Analysis Batch
date / time
1 12/15/201919:05
1 12/15/201919:05
1 12/15/201919:05
1 12/15/201919:05
1 12/15/201919:05
1 12/15/201919:05
121151201919.05
121151201919.05
Dilution Analysis
date / time
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
1 12/18/201917:20
12118120191720
121181201917.20
12118120191720
121181201917.20
12118120191720
121181201917.20
WG1396828
WG1396828
WG1396828
WG1396828
WG1396828
WG1396828
WG1396828
WG1396828
Batch
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
WG1397451
Fp
FTc
FS
Fn
N
FC]
F
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 6 of 23

WG1396907
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3483840-1 12/18/19 19:20
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1169101-08 Original Sample (OS) • Duplicate (DUP)
(OS) L1169101-08 12/18/1919:28 • (DUP) R3483840-3 12/18/1919:29
Original Result DUP Result Dilution DUP RPD
Analyte mg/kg mg/kg %
Reactive Cyanide ND 0.202 1 200
L1169654-10 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1169199-01
DUP Qualifier DUP RPD
Limits
J P1 20
(OS) L1169654-10 12/18/19 20:45 • (DUP) R3483840-8 12/18/19 20:46
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3483840-2 12/18/1919:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.67 107 50.0-150
L11691O5-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1169105-01 12/18/1919:34 • (MS) R3483840-4 12/18/1919:35 • (MSD) R3483840-5 12/18/1919:36
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg % %
Reactive Cyanide 1.67 ND 1.31 1.57 72.2 88.1
L1169199-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1169199-01 12/18/1919:37 • (MS) R3483840-6 12/18/1919:38 • (MSD) R3483840-7 12/18/1919:39
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg % %
Reactive Cyanide 1.67 ND 0.783 0.994 47.0 59.7
ACCOUNT: PROJECT:
EMA Resources
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 J6 18.3
ONE LAB. NATIONWIDE.
RPD Limits
20
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 75.0-125 J6 J3 J6 23.7 20
SDG: DATE/TIME: PAGE:
L1169199 12/19/19 14:05 7 of 23

WG1395273
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3481968-1 12/13/19 01:00
MB Result MB Qualifier MB MDL
Analyte mg/kg mg/kg
Reactive Sulfide U 7.63
L1169199-01 Original Sample (OS) • Duplicate (DUP)
MB RDL
mg/kg
25.0
(OS) L1169199-01 12/13/19 01:00 • (DUP) R3481968-3 12/13/19 01:00
Original Result DUP Result Dilution DUP RPD
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000
Laboratory Control Sample (LCS)
(LCS) R3481968-2 12/13/19 01:00
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Sulfide 100 88.1 88.1
QUALITY CONTROL SUMMARY
L1169199-01
DUP Qualifier DUP RPD
Limits
o�
20
Rec. Limits LCS Qualifier
70.0-130
ONE LAB. NATIONWIDE.
— I
Cp
FTc
FSS
4
— Cn
FSr
— �GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 8 of 23

WG1395945 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1169199-01
Laboratory Control Sample (LCS)
(LCS) R3482256-1 12/13/1916:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
Corrosivity by pH 10.0 10.0 100 99.0-101
Sample Narrative:
LCS:10 at18.7C
ONE LAB. NATIONWIDE.
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 9 of 23

WG1395517 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1169199-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE.
(LCS) R3482850-1 12/16/19 15:00 • (LCSD) R3482850-2 12/16/1915:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F % % %
Ignitability 82.0 83.9 83.9 102 102 97.0-103 0.000 10
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 10 of 23
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG1396177
Mercury by Method 7470A
Method Blank (MB)
(MB) R3482771-1 12/16/19 12:07
MB Result
Analyte mg/1
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00330 0.0100
QUALITY CONTROL SUMMARY
L1169199-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3482771-2 12/16/1912:09 • (LCSD) R3482771-3 12/16/1912:11
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
Mercury 0.0300 0.0311 0.0311 104 104 80.0-120 0.00321 20
L1168389-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1168389-01 12/16/1912:13 • (MS) R3482771-4 12/16/1912:15 • (MSD) R3482771-5 12/16/1912:17
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/I mg/I mg/I mg/I % % % %
Mercury 0.0300 ND 0.0306 0.0296 102 98.7 1 75.0-125 3.26
L1168411-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1168411-03 12/16/1912:19 • (MS) R3482771-6 12/16/1912:21 • (MSD) R3482771-7 12/16/1912:23
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/I mg/I mg/I mg/1 % %
Mercury 0.0300 ND 0.0315 0.0310 105 103
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 1.67
ONE LAB. NATIONWIDE.
RPD Limits
20
RPD Limits
20
— I
Cp
FTc
FSS
4
— Cn
FSr
— �GI
— $AI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 11 of 23

WG1396694 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1169199-01
Method Blank (MB)
(MB) R3482576-1 12/16/19 03:54
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0330
0.100
Barium U
0.0330
0.100
Cadmium U
0.0330
0.100
Chromium U
0.0330
0.100
Lead U
0.0330
0.100
Selenium U
0.0330
0.100
Silver U
0.0330
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3482576-2 12/16/19 03:56 • (LCSD) R3482576-3 12/16/19 03:59
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Arsenic
10.0
9.70
9.86
97.0
98.6
80.0-120
1.65
20
Barium
10.0
9.77
9.84
97.7
98.4
80.0-120
0.690
20
Cadmium
10.0
9.77
9.86
97.7
98.6
80.0-120
0.941
20
Chromium
10.0
9.28
9.32
92.8
93.2
80.0-120
0.501
20
Lead
10.0
9.59
9.67
95.9
96.7
80.0-120
0.913
20
Selenium
10.0
10.2
10.2
102
102
80.0-120
0.480
20
Silver
2.00
1.77
1.76
88.3
88.1
80.0-120
0.199
20
L1168554-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1168554-01 12/16/19 04:02 • (MS) R3482576-5 12/16/19 04:07 • (MSD) R3482576-6 12/16/19 04:09
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
0.131
10.0
9.99
98.7
98.6
Barium
10.0
84.1
84.5
86.8
4.49
27.8
Cadmium
10.0
ND
9.91
9.92
99.1
99.2
Chromium
10.0
ND
9.19
9.09
91.9
90.9
Lead
10.0
2800
2520
2600
0.000
0.000
Selenium
10.0
ND
10.2
10.2
102
102
Silver
2.00
ND
1.73
1.74
86.6
87.1
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier MSD Qualifier RPD
0.0918
V V 2.72
0.121
1.14
E V E V 2.85
0.301
0.558
ONE LAB. NATIONWIDE.
RPD Limits
20
20
20
20
20
20
20
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG:
EMA Resources L1169199
DATE/TIME: PAGE:
12/19/19 14:05 12 of 23

WG1396052
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3482382-2 12/13/1914:35
MB Result
A I /I
na yte
mg
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
89.2
(S) 4-Bromof/uorobenzene
107
(S)1,2-Dichloroethane-d4
110
MB Qualifier
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
QUALITY CONTROL SUMMARY
L1169199-01
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3482382-1 12/13/1910:43 • (LCSD) R3482382-3 12/13/19 13:46
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Benzene
0.250
0.211
0.236
84.4
94.4
70.0-123
11.2
20
Carbon tetrachloride
0.250
0.273
0.289
109
116
68.0-126
5.69
20
Chlorobenzene
0.250
0.222
0.215
88.8
86.0
80.0-121
3.20
20
Chloroform
0.250
0.245
0.241
98.0
96.4
73.0-120
1.65
20
1,2-Dichloroethane
0.250
0.250
0.251
100
100
70.0-128
0.399
20
1,1-Dichloroethene
0.250
0.241
0.262
96.4
105
71.0-124
8.35
20
2-Butanone (MEK)
1.25
0.842
0.808
67.4
64.6
44.0-160
4.12
20
Tetrachloroethene
0.250
0.261
0.233
104
93.2
72.0-132
11.3
20
Trichloroethene
0.250
0.260
0.269
104
108
78.0-124
3.40
20
Vinyl chloride
0.250
0.185
0.191
74.0
76.4
67.0-131
3.19
20
(S) Toluene-d8
90.0
87.6
80.0-120
(S) 4-Bromofluorobenzene
105
104
77.0-126
(S)1,2-Dichloroethane-d4
108
106
70.0-130
ONE LAB. NATIONWIDE.
FP1
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4
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 13 of 23

WG1396052 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1169199-01
L1169101-15 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1169101-15 12/13/1918:33 • (MS) R3482382-5 12/13/19 21:53 • (MSD) R3482382-6 12/13/19 22:13
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Benzene
0.250
ND
0.258
0.252
103
101
Carbon tetrachloride
0.250
ND
0.392
0.374
157
150
Chlorobenzene
0.250
ND
0.244
0.246
97.6
98.4
Chloroform
0.250
ND
0.308
0.309
123
124
1,2-Dichloroethane
0.250
ND
0.299
0.307
120
123
1,1-Dichloroethene
0.250
ND
0.327
0.334
131
134
2-Butanone (MEK)
1.25
ND
1.02
1.03
81.6
82.4
Tetrachloroethene
0.250
ND
0.296
0.285
118
114
Trichloroethene
0.250
ND
0.272
0.282
109
113
Vinyl chloride
0.250
ND
0.249
0.230
99.6
92.0
(S) Toluene-d8
91.0
87.0
(S) 4-Bromof/uorobenzene
107
104
(S)1,2-Dichloroethane-d4
117
115
ONE LAB. NATIONWIDE.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
2.35
27
1 23.0-159
4.70
28
1 33.0-152
0.816
27
1 29.0-154
0.324
28
1 29.0-151
2.64
27
1 11.0-160
2.12
29
1 10.0-160
0.976
32
1 10.0-160
3.79
27
1 10.0-160
3.61
25
1 10.0-160
7.93
27
80.0-120
77.0-126
70.0-130
FP1
FTc
FSS
4
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FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 14 of 23

WG1397171
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3483001-1 12/17/19 00:44
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S)2,4-Dichloropheny/Acetic 172
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
(LCS) R3483001-2 12/17/19 00:58
Spike Amount
LCS Result
LCS Rec.
Analyte
mg/I
mg/I
%
2,4-D
0.0500
0.0365
73.0
2,4,5-TP (Silvex)
0.0500
0.0370
74.0
(S) 2,4-Dichloropheny/Acetic
272
Acid
QUALITY CONTROL SUMMARY
L1169199-01
MB RDL
mg/I
0.00200
0.00200
14.0-158
Rec. Limits LCS Qualifier
50.0-120
50.0-125
14.0-158
L1169193-46 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1169193-46 12/17/19 01:26 • (MS) R3483001-3 12/17/19 01:39 • (MSD) R3483001-4 12/17/19 01:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
2,4-D
0.0500
ND
0.0308
0.0356
61.6
71.2
2,4,5-TP (Silvex)
0.0500
ND
0.0310
0.0368
62.0
73.6
(S) 2,4-Dichloropheny/Acetic
22.8
270
Acid
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 50.0-120 14.5
1 50.0-125 17.1
14.0-158
ONE LAB. NATIONWIDE.
RPD Limits
o�
20
20
FP1
FTc
3
SS
4
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 15 of 23

WG1396828 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method 8081B L1169199-01
Method Blank (MB)
(MB) R3483610-1 12/15/1917:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobipheny/
58.9
10.0-128
(S) Tetrach/oro-m-xy/ene
40.0
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3483610-2 12/15/1918:03
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
%
%
Gamma BHC
0.0100
0.00887
88.7
55.0-129
Endrin
0.0100
0.00920
92.0
57.0-134
Heptachlor
0.0100
0.00846
84.6
27.0-132
Methoxychlor
0.0100
0.0104
104
54.0-155
(S) Decachlorobiphenyl
77.2
10.0-128
(S) Tetroch/oro-m-xy/ene
61.9
10.0-127
L1169825-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1169825-01 12/15/1919:17 • (MS) R3483610-3 12/15/1919:30 • (MSD) R3483610-4 12/15/1919:42
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Gamma BHC
0.0100
ND
0.00902
0.00985
90.2
98.5
Endrin
0.0100
ND
0.00942
0.0102
94.2
102
Heptachlor
0.0100
ND
0.0192
0.00925
192
92.5
Methoxychlor
0.0100
ND
0.0114
0.0122
114
122
(S) Decachlorobipheny/
81.1
86.8
(S) Tetrach/oro-m-xylene
59.7
64.4
ONE LAB. NATIONWIDE.
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 14.0-141 8.80 40
1 10.0-160 7.95 39
1 16.0-136 J5 P J3 69.9 40
1 10.0-160 6.78 34
10.0-128
10.0-127
FP1
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FSS
4
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 16 of 23

WG1397451 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1169199-01
Method Blank (MB)
(MB) R3483725-2 12/18/1912:58
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
51.7
10.0-127
(S) 2-F/uorobipheny/
58.7
10.0-130
(S) p-Terphenyl-d14
65.2
10.0-128
(S) Phenol-d5
16.7
10.0-120
(S) 2-Fluorophenol
30.2
10.0-120
(S)2,4,6-Tribromopheno/
64.5
10.0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE.
(LCS) R3483725-1 12/18/1912:38
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.288
57.6
18.0-120
2,4-Dinitrotoluene 0.500
0.414
82.8
49.0-124
Hexachlorobenzene 0.500
0.407
81.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.307
61.4
19.0-120
Hexachloroethane 0.500
0.282
56.4
15.0-120
Nitrobenzene 0.500
0.292
58.4
27.0-120
Pyridine 0.500
0.0738
14.8
10.0-120
2-Methylphenol 0.500
0.248
49.6
28.0-120
3&4-Methyl Phenol 0.500
0.254
50.8
31.0-120
Pentachlorophenol 0.500
0.462
92.4
23.0-120
2,4,5-Trichlorophenol 0.500
0.413
82.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.358
71.6
42.0-120
(S) Nitrobenzene-d5
52.2
10.0-127
(S) 2-F/uorobipheny/
73.5
10.0-130
(S) p-Terphenyl-d14
79.2
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1169199 12/19/19 14:05 17 of 23
FP1
FTC
FSS
4
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WG1397451 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1169199-01
Laboratory Control Sample (LCS)
(LCS) R3483725-1 12/18/1912:38
Spike Amount LCS Result
na yte
(S) Phenol-d5
(S) 2-Fluorophenol
(S) 2,4,6-Tribromophenol
LCS Rec.
Rec. Limits LCS Qualifier
19.3
10.0-120
32.3
10.0-120
85.5
10.0-155
L1167043-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1167043-02 12/18/1913:18 • (MS) R3483725-3 12/18/19 13:38 • (MSD) R3483725-4 12/18/1913:59
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.245
0.301
49.0
60.2
1 17.0-120
20.5
40
2,4-Dinitrotoluene
0.500
ND
0.432
0.436
86.4
87.2
1 39.0-125
0.922
25
Hexachlorobenzene
0.500
ND
0.415
0.416
83.0
83.2
1 35.0-122
0.241
24
Hexachloro-1,3-butadiene
0.500
ND
0.276
0.309
55.2
61.8
1 12.0-120
11.3
34
Hexachloroethane
0.500
ND
0.259
0.313
51.8
62.6
1 10.0-120
18.9
40
Nitrobenzene
0.500
ND
0.266
0.297
53.2
59.4
1 12.0-120
11.0
30
Pyridine
0.500
ND
0.0450
0.0774
9.00
15.5
1 10.0-120
J6 J3 52.9
37
2-Methylphenol
0.500
ND
0.237
0.269
47.4
53.8
1 10.0-120
12.6
30
3&4-Methyl Phenol
0.500
ND
0.242
0.278
48.4
55.6
1 10.0-120
13.8
36
Pentachlorophenol
0.500
ND
0.473
0.484
94.6
96.8
1 10.0-128
2.30
37
2,4,5-Trichlorophenol
0.500
ND
0.417
0.431
83.4
86.2
1 33.0-120
3.30
31
2,4,6-Trichlorophenol
0.500
ND
0.369
0.379
73.8
75.8
1 26.0-120
2.67
31
(S) Nitrobenzene-d5
48.9
47.8
10.0-127
(S) 2-F/uorobipheny/
76.9
78.1
10.0-130
(S)p-Terphenyl-d14
9t3
872
10.0-128
(S) Phenol-d5
18.1
2t2
10.0-120
(S) 2-F/uorophenol
28.4
35.5
10.0-120
(S)2,4,6-Tribromophenol
90.5
87.5
10.0-155
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA
Resources
L1169199
12/19/19 14:05
18 of 23
FP1
FTc
FSS
[Cn]
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[Sc

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
CP
IP
FTC
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
[Cn]
RDL
Reported Detection Limit.
Rec.
Recovery.
FSr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
6
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P
RPD between the primary and confirmatory analysis exceeded 40%.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1169199 12/19/19 14:05 19 of 23

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
ME
MT NO
OR MN
T ID t WI NY
SD
WY MI
NV
t NE IA OH PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
N
NM O� AR SC
T MS AL`7GA
T TX * LA
T
AK
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1169199 12/19/19 14:05 20 of 23

EMA Resource
755 Yadkinville Rd
Mocksville, NC 27028
Yanceyville WTP
I Client Project #:
"'- 336-751-1441
x 336-492-6394
ilected by:/i�y
Ilected by (signature):
- 0
Sample ID
Yanceyville WTP
Yancewille WTP
Alternate billing information:
Brent Collins
Yanceyville, NC
ESC Key:
Site/Facility ID#:
Rush1 ( Lab MUST Be Nesults
Needed:No.Same
Day......Next
Yes
Day.......il?
_No
orTwo
Day .......?
aResults
No YescmComp/Grab
Matrix'
te
TimeComp
8:30am 1119
[1dy119
8:30am 1
'Matrix: SS-S0iVS0Iid GW-Groundwater WW-WasteWater DW- Drinking OT-
Remarks: Y 1-i C
by:l,Sign e) Date: Time: Received by: (Signature)
iilsl (4 3.7°f""
by: (Si attire) Date: Time: Received by: (Signature)
by: (Signature) Date: Time: Rrved for lab by: (S
T to n/1.
Chain of Cudy
Page -L oft I
Prepared by:
ENVIRONMENTAL
SCIENCE CORP.
12065 Lebanon Road
Mt Juliet, TN 37122
Phone [phone]
Phone [phone]
FAX [phone]
CoCode EMARES (lab use only)
Template/Prelogin
Shipped Via:
a _
U U Remarks/Contaminant Sample # (lab only)
f- i Al9-er
3 p\
3' C049
PH --- Tenor
f� (� 8 Flow. Other
i r ( ❑ UPS Condition: (lab use only)
Samp es returned via: /�
❑FedEx ❑Courier ❑ _
Bottles Received: RAD SCREEN: <O b ,.
Temp: yl
2.0
Date: Time: pH Checked: NCF:

NationalPace Analytical • • : Innovation
Cooler Receipt F•
Client: MAVE 9 1., 11 &111
Cooler Received/Opened On: 12 / /19 Temperature:
Received By: Michael Pappas
Si nature:
Receipt Check List NP
Yes
No
COC Seal Present / Intact?
COC Signed / Accurate?
Bottles arrive intact?
Correct bottles used?
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?

Jeremy W. Watkins
ceAnalytical
National Center for Testing & Innovation
login #: L1169199 I Client: EMARES I Date: 12/6/19 1 Evaluated by: Jeremy
Non -Conformance check a licable items
Sample Integrity
Chain of Custody Clarification
Parameter(s) past holding
time
Login Clarification Needed
If Broken Container:
Temperature not in
range
Chain of custody is incomplete
Insufficient packing material around container
Improper container
type
Please specify Metals requested.
Insufficient packing material inside
cooler
H not in range.
x
Please specify TCLP requested.
Improper handling by carrier FedEx UPS Coon
Insufficient sample volume.
Received additional samples not listed on coc.
Sample was
frozen
Sample is biphasic.
Sample ids on containers do not match ids on
coc
Container lid not intact
Vials received with headspace.
Trip Blank not received.
If no Chain of Custody:
Broken container
x
Client did not "X" analysis.
Received by:
Broken container:
Chain of Custody is missing
Date Time:
Sufficient sample remains
Temp./Cont. Rec./pH:
Carrier:
Trackin #
Lein Comments:
1. Analysis not marked
2. WhatTCLP?
I Client informed by: I I Call I x I Email I I Voice Mail I I Date: 12/10/19 1 Time: 1:16PM
TSR Initials: IGC I Client Contact: Brent Collins
Full TCLP and RCI on -01. Samples are duplicates.

ANN IJAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Yanceyviile WQ Permit Number: WQ0028547
WWTP Name: Yanceyville WWTP NPDES Number: NCO040011
Monitoring Period: From II112019 TO 12/31/2019
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment)❑ 1 Alt_ C (Prior Testing)❑
Alt.D (No Prior Test) ❑ 1
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A on indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Rav ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Densl!j E7d
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Com sting ❑ lAcrobic
Digestion ❑
Anaerobic Di estion ❑
If applicable to alternative performed Class A or Class 13) complete the followin
monitorin
data:
Parameter
Allowable Level
in Sludge
$
Pathogen Density
Number of
Excee-
Frequency,
afAnal sus
y
Sample
yp
Type
Analytical
Tech-ni ue
q
inimu
Gen. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
bth Power
per gram of
total solids
MPN
CFU
1635
2440
3105
call g
0
Annual y
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliforrn
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt, 3 (30-day bench) 21
lAlt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 1SA NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
_ Charles Overby - Project Manager Brent Collins; Director of Technical Services
Prep r ame and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
L ;
-�o 1/7/2020
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF D2T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 1
Report Date: 8/16/2019
Project: Yanceyville WWTP
Date Sample Rcvd: 8/7/2019
Meritech Worlc Order #
080719161
Sample:
Yanceyville S-1 Grab
8/7/19
Parameters
Result
Analysis Date Reporting Limit
Method
%Total Solids
8.49
%
8/8/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
3105
col/g dry wt
8/7/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
080719162
Sample:
Yanceyville S-2 Grab
7/30/19
Parameters
Result
Analysis Date
Renorti� Limit
Method
% Total Solids
8.47 %
8/8/19
0-100 %
SM 254013
Fecal Coliform (Sludge)
3005 col/g dry wt
8/7/19
130 col/g dry wt
SM 9222D
Meritech Work Order #
080719163 Sample:
Yanceyville S-3 Grab
7/30/19
Parameters
Result
Analysis Date
Reporting Limit
Method
%Total Solids
7.91
%
8/8/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
2873
col/g dry wt
8/7/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
080719164
Sample:
Yanceyville S-4 Grab
7/30/19
Parameters Result Analysis Date Reporting Limit Method
%Total Solids
8.76
%
8/8/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
2179
col/g dry wt
8/7/19 130 col/g dry wt
SM 9222D
Meritech Work Order #
080719165
Sample:
Yanceyville S-5 Grab
7/30/19
Parameters Result Analysis Date Reporting Limit Method
Total Solids 13.9 % 8/8/19 0-100 % SM 254.O13
Fecal Coliform (Sludge) 1635 col/g dry wt 8/7/19 130 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 2
Report Date: 8/16/2019
Project: Yanceyville WWTP
Date Sample Rcvd: 7/30/2019
Meritech or Order # 080719166 Sample: Yanceyville S-6 Grab 7/30/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 9.12 % 8/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 1994 col/g dry wt 8/7/19 130 col/g dry wt SM 9222D
Meritech Work Order # 080719167 Sample: Yanceyville S-7 Grab 7/30/19
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 9.42 % . 8/8/19 0-100 % SM 2540B
Fecal Coliform (Sludge) 2702 col/g dry wt 8/7/19 130 col/g dry wt SM 9222D
I hereby certify thatl have reviewed and approve these data. v
t
—Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report [)ate: 9/18/2019
Project: Yanceyville WWTP
Date Sample Rcvd: 8/7/2019
Vectpr Attraction Reduction /Aerobically Digested SludC2 (30 Day Test
Meritech Work Order # 080719160 Sample: Yanceyville WWTP Grab 8/7/19
Total Solids Volatile Solids % Volatile Solids
Week 1 0.250 0.160 0.632
Weelc 2 0.270 0.160 0.587
Week 3 0.310 0.180 0.585
Week4 0.260 0.150 0.556
Week 5 0.300 0.180 0.618
Van Kleek Reduction (%): 5.61
Pass or Fail
Pass
I hereby certify that I have reviewed and approve these data. If 110 jncx / -
Lab oratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Yanceyville WQ Permit Number:
WWTP Name: Yanceyville WTP NPDES Number:
Monitoring Period: From 1/1/2019 To 12/31/2019
WQ0028547
02-17-010
Pathogen Reduction (I5A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
I Alt. A (timeltem) ❑ I
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogen s ❑
if $ plicable to alternative performed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
)=teat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ra 01
Gamma RaX ❑
Pasteu iaation ❑
Class B:
JAIt. (1) Fecal Density 21
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed jChss B on Indicate "Process to Significantly Reduce Pathogens",
Lime Stabilization ❑
Air Drying ❑
1 Composting ©
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed Class A or Class B complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th lower
per gram of
total solids
MPN
CFU
193
196
198
collg
0Annualy
G
SM9222D
1000 mpn per gram
of total solid (dry
Weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 M1PN per 4 grams
total solid (dry
I
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (incorporation) ❑
No vector attraction reduction alternatives were performed 21
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
reauirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Overby - Project Manager
Pre arer N d Titl type or 'nt)
Signature of Freparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
P-73-20 1/7/2020
Date Signature of Land Applier (if applicable)
*Freparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
❑ENR FORM PVRF 02T (12l2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech Worlc Order # 080719168 Sample: Yanceyville WTP-1 Grab
Page 1
Report Date: 8/16/2019
Project: Yanceyville WTP
Date Sample Rcvd: 8/7/2019
8/7/19
Parameters Result Analysis Date Reporting Limit Method
%Total Solids
4.71
%
8/8/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<193
col/g dry wt
8/7/19 193 col/g dry wt
SM 9222D
Meritech Work Order #
080719169
Sample:
Yanceyville WTP-2 Grab
8/7/19
Parameters Result Analysis Date Reporting Limit Method
%Total Solids
4.63
%
8/8/19 0-100 %
SM 254OB
Fecal Coliform (Sludge)
<196
col/g dry wt
8/7/19 196 col/g dry wt
SM 9222D
Meritech Work Order #
080719170
Sample:
Yanceyville WTP-3 Grab
8/7/19
Parameters Result Analysis Date Reporting Limit Method
%Total Solids
4.64
%
8/8/19 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<196
col/g dry wt
8/7/19 196 col/g dry wt
SM 9222D
Meritech Work Order #
080719171
Sample:
Yanceyville WTP-4 Grab
8/7/19
Parameters
Result
Analysis Date
Reporting Limit
Method
%Total Solids
4.60
%
8/8/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
<198
col/g dry wt
8/7/19
198
col/g dry wt
SM 9222D
Meritech Work Order #
080719172
Sample:
Yanceyville WTP-5
Grab
8/7/19
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
4.65
%
8/8/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
<195
col/g dry wt
8/7/19
195
col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 2
Report Date: 8/16/2019
Project: Yanceyville WTP
Date Sample Rcvd: 8/7/2019
Meritech Worlc Order # 080719173 Sample: Yanceyville WTP-6 Grab
Parameters Result Analysis Date Reporting Limit
% Total Solids 4.62 % 8/8/19 0-100 %
Fecal Coliform (Sludge) <197 col/g dry wt 8/7/19 197 col/g dry wt
Meritech Worlc Order # 080719174 Sample: Yanceyville WTP-7 Grab
Parameters Result Analysis Date Reporting Limit
% Total Solids 4.62 % 8/8/19 0-100 %
Fecal Coliform (Sludge) <197 col/g dry wt 8/7/19 197 col/g dry wt
1 hereby certify that I have reviewed and approve these data.
8/7/19
Method
SM 2540B
SM 9222D
8/7/19
Method
SM 2540B
SM 9222D
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Page 1 of 1
Report No: 19-353-9561
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypoint'.(D
ANALYTICAL
Client: Jon Crispin
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: CS-82
Date Received: 12/19/2019
Date of Report: 01/08/2020
Lab No Field ID
Sample ID
Soil Class HM% WN pH
Ac
P-1
K-1
S-1
Mn-1
Zn-I
Zn-AI
Cu-1
CEC
BS%
Ca%
Mg%
ESP Na
SS-1 NO3 N
08240
01
MIN 1.4
6.6
0.4
25
135
17
788
168
168
80
6.0
94
51
30
1.3 0.1
14
Crop Recommendations:
1- Lawn
Rec Uom
Ib/1000 sf
Lime (Vacre)
0.0
N
4.0
P205
1.0
K20
0
S
0.63
Mn
0
Mn-AI
481
Zn
0
Cu
0.10
B
0
Mg
0
Last Crop
08241
02
MIN 1.2
5.7
1.0
5
19
15
406
65
65
60
4.6
79
53
22
1.7 0.1
7
Crop Recommendations:
1- Lawn
Rec Uom
Ib/1000 sf
Lime (Vacre)
0.0
N
4.0
P205
2.0
K20
4.0
S
0.66
Mn
0.10
Mn-Al
265
Zn
0
Cu
0.10
B
0.02
Mg
0
Last Crop
08242
03
MIN 1.3
5.7
1.8
12
28
19
819
65
65
55
8.6
80
45
32
1.4 0.1
6
Crop Recommendations:
1- Lawn
Rec Uom
Ib/1000 sf
Lime (Vacre)
0.0
N
4.0
P205
2.0
K20
4.0
S
0.61
Mn
0
Mn-AI
513
Zn
0
Cu
0.10
B
0.02
Mg
0
Last Crop
08243
04
MIN 1.2
6.2
0.6
4
13
12
888
43
43
35
4.8
88
57
27
1.9 0.1
6
Crop Recommendations:
1- Lawn
Rec Uom
Ib/1000 sf
Lime (Vacre)
0.0
N
4.0
P205
2.0
K20
4.0
S
0.69
Mn
0
Mn-Al
547
Zn
0.10
Cu
0.10
B
0.02
Mg
0
Last Crop
Comment
Test result units = CEC and Na in meq/100cm3; NO: N in mg/dm3; WN in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Page 1 of 2
Report Number: 19-353-0561
Account Number:46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
•
Waypoi ntrM
ANALYTICAL
"Every acre... Every year. "TM
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Jon Crispin
Farm: CS-82
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 12/19/2019 Date Of Analysis: 12/20/2019 Date Of Report: 12/23/2019 NC = North Carolina Fertility Index Value
OM
w/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
°
/0
Rate
Soil Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
01
08240
3.4
M
109
30 L
NC = 25
264 VH
NC = 135
216 VH
616 M
18
VL
6.6
0.4
6.0
MIN
02
08241
2.9
M
101
6 VL
NC = 5
37 VL
NC = 19
120 H
491 M
18
VL
5.7
6.83
1.0
4.6
MIN
03
08242
3.2
M
102
14 L
NC = 12
54 VL
NC = 28
326 VH
772 L
28
VL
5.7
6.75
1.8
8.6
MIN
04
08243
2.9
M
101
5 VL
NC = 4
25 VL
NC = 13
158 VH
548 M
21
VL
6.2
6.87
0.6
4.8
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NO, N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm
Rate
SS
ms/cm Rate
01
11.3
30.0
51.3
1.3
6.7
8 VL
NC=17
6.7 H
NC=167.5
126 VH
NC=788
196 VH
1.6 H
NC=80.0
0.6
M
0.14
VL
02
2.1
21.7
53.4
1.7
21.7
7 VL
NC=15
2.6 M
NC=65.0
65 VH
NC=406
153 VH
1.2 M
NC=60.0
0.3
VL
0.07
VL
03
1.6
31.6
44.9
1.4
20.9
9 VL
NC=19
2.6 M
NC=65.0
131 VH
NC=819
224 VH
1.1 M
NC=55.0
0.4
L
0.06
VL
04
1.3
27.4
57.1
1.9
12.5
6 VL
NC=12
1.7 L
NC=42.5
142 VH
NC=888
98 VH
0.7 L
NC=35.0
0.3
VL
0.06
VL
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: POt�ic m� G�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 2 of 2
Report Number: 19-353-0561
Account Number:46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville INC 27028
Date Received: 12/19/2019
Date Of Report: 12/23/2019
•
Waypoi ntrM
ANALYTICAL
"Every acre... Every year. "TM
Farm: CS-82
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Grower: Jon Crispin
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
01
Lawn
0
0.0
4.0
1.0
0
0
0.63
0
0
0
0.10
0
02
Lawn
0
0.0
4.0
2.0
4.0
0
0.66
0
0.10
0
0.10
0.02
03
Lawn
0
0.0
4.0
2.0
4.0
0
0.61
0
0
0
0.10
0.02
04
Lawn
0
0.0
4.0
2.0
4.0
0
0.69
0.10
0
0
0.10
0.02
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Pori.M6 60w
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary