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HomeMy WebLinkAboutWQ0004825_Residual Annual Report 2019_20200225Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application r Annual Report what is the submittal r Residual Annual Report type?* r Additional Information r Other Annual Report 2019 Year* Date Paper Copy 2/25/2020 Received:* Project Number* WQ0004825 Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electronic subnittal, confirmation of receipt, and other issues. .......................................................................................................................................................................................................................................................................................................................................................................... Name * Lysa Finnerty Email Address* Ifinnerty@synagro.com Project Information Submittal Type* r New Permit Application r Renewal r Annual Report r Other Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted? r Yes r Nor N/A Permit Number* WQ0004825 Applicant\Permittee * Synagro Facility Name * City of Randleman Phone Number* 4434899026 r Modification (Major or Minor) r Additional Information r Residual Annual Report r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Randleman 2019 Annual Report Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) RANDLEMAN NC 2019 Annual FINAL.pdf 9.62MB Upload only 1 RDF document. Maniple documents must be combined into one RDF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contactthe reviewer or Tessa Monday. If a paper 2-pol cation is required, be advised, applications accepted for pre -review until both the paper and elect-c-ii.- --ol:ies have been received. The paper copy shall include the following: o Application Form o All relevant attachments {talcs, soils report, specs, etc.] o One full-size engineering plan set o One 11x17" engineering plan set o One extra set of specifications o Fee (if required) Mailine address: Division of Water Resources ! Division of Water Resources Non -Discharge Branch I Non -Discharge Branch 1617 Mail Service Center I Att: Nathaniel Thornburg, P Floor, Office #942W - = Raleigh, NC 27699-1617 S12 N.5alisburySt. For questions or problems contact Tessa Monday attessa.monday@)ncdenr.Qov or 919.707.3560. * rJ By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/21/2020 435 Williams Court, Suite 100 Baltimore, T\-1D 21220 wwwsynagroxom FEBRUARY 21, 2020 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2019 Annual Report for Permit No. WQ0004825 Dear NCDEQ: SYNA-11G.JR0 Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the City of Randleman, NC. If you have any questions or need additional information, please do not hesitate to contact Nick Holcomb at (336) 495-7500 or Ryan Copeland at (336) 607-4494. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Nick Hokomb, City of Randleman Ryan Copeland, Synagro YOUR PARTNER FORA CLEANER, GREENER WORLD CITY OF RANDLEMANI NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0004825 2019 ANNUAL REPORT City of Randleman, NC Residuals Land Application Program 2019 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms & Il�letals Field Loading Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH &Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00004825 County Randolph Year 2019 Facility Name (as shown on permit) City of Randleman WWTP NPDES No. NC0025445 .and Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A. and Part Band proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A —Residuals Application Summary: Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 2 Total amount of dry tons applied during the year for all application sites: 64.8 Total number of acres utilized for land application during the year: 44.5 Part B —Annual Compliance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 143 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C —Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Michael Glass, Plant Superintendent Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) (if different from Pennittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T 01102 (26) DENR FORM ACF (12/2006) 2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC RANDLEMAN, NC RANDLEMAN, NC RANDLEMAN WWTP LIQUID MONTH/YEAR AMOUNT UNIT DRY TONS UNIT May 2019 266,600.00 G 33.57 D August 2019 248,000.00 G 31.23 D YEARLY TOTAL 514,600.00 G 64.80 D DRY METRIC 30.45 28.32 58.77 1/30/2020 Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004825 Facility Name: RANDLEMAN, NC NPDES# : NCO025445 or WQ# (residual only) WWTP Name: RANDLEMAN WWTP Residuals Analysis Data Product Type L=4 L1Q Date Sampled (grab) or 05/29/19 08/13/19 Date Composited Percent Solids 3 . 02 3 . 60 PARAMETERS (mg/kg dry weight) Arsenic <5 <5 Cadmium <1 <1 Mercury 0.198 0.2 Chromium 63.4 41.8 Copper 172 158 Lead 29.8 30.5 Molybdenum 8.3 5.13 Nickel 17.3 13.7 Selenium <5 <5 Zinc 140 127 Total Phosphorus 8570 7150 TKN 102000 44700 Ammonia -Nitrogen 13700 11400 Nitrate and Nitrite 310 <4. 89 Laboratory Waypoint Analytical Virginia Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." DENR FORM RSSF (5/2003) Printed: Thursday - February 6 2020 at 10:53:47 for: 2027 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Report Please note that your permit may contain additional parameters to be analyzed than those required to be summerized on this form Permit Number Facility Name NPDES# or WQ# (residual only) WWTP Name Residual Analysis Data Product Type Date Sampled Date Composited Percent Soilds WQ0004825 RANDLEMAN, NC N30025445 RANDLEMAN WWTP LIQ 05/29/19 3.02 LIQ 08/13/19 3.60 PARAMETERS (mg/kg dry weight)' Aluminium 9270 16200 Calcium 87800 121000 Magnesium 5450 6080 pH 10.70 11.80 Potasium 2230 1460 Sodium 1660 797 PAN 33650 15695 SAR 0.2549 0.1148 Laboratory Waypoint Analytical Virginia Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (SIGNATURE OF PREPARER) NR -Data Not Reported or Data Not Required Report Run Date:- 2/6/2020 10:54:51 AM Waypoint.. ANALYTICAL 6/7/2019 Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Repon` Number: 19-151-0208 Project Description: Randleman WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received samples) on 5/31/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory`s liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Virginia 460014 Page 1 of 7 �� � �- � � i � Client: Synagro Central LLC/ Randleman Project: Randleman 1/WVfP Lab Report Number: 19-151-0208 Date: 6/7/2019 7fi21 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax $04-271-6446 www.waypointanaiyticai.com CASE NARRATIVE Metals Analysis Method 6010D Sample 66658 (Randleman VWVfP) Analyte: Aluminum �C Batch No: L439168/L438971 The matrix spike and/or the matrix spike duplicate was outside QC acceptance ranges. A dilution test was performed and passed QC acceptance ranges. No matrix interference is suspected. Page 2 of 7 Wa Dint,. vp ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 8Q4-743-9401 °Fax 804-271-6446 www.waypointanalyfical.com Sample Summary Table Report Number: 19-151-0208 Client Project Description: Randleman WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/2019 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/2019 SM-2540G WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/2019 SW-7471B WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/2019 SM-4500-NH3C-TKN WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/Z019 4500NO3F-2011 WTN 66658 Randleman WWTP Solids 05/Z9/2019 11:45 05/31/2019 6010D WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/Z019 SM-4500-NH3C WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/2019 9045D WTN 66658 Randleman WWTP Solids 05/29/2019 11:45 05/31/Z019 AOAC 955.01 WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 3 of 7 Report Number: 19-151-0208 Account Number: 46483 Send To: Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville , NC 27028 �����, ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94Q1 °Fax 804-271-6446 www.waypointanalytical.com Project :Randleman WWTP REPORT OFANALYS/S Date Sampled: 5/29/2019 11:45:00 Lab Number : 66658 Date Received: 05/31/2019 00:00 Sample Id :Randleman WWTP Date Reported: 06/07/2019 Total Solids * 3.02 ADM 06/04/2019 15:05 Moisture * 97.00 ADM 06/04/2019 15:05 Total Kjeldahl Nitrogen 10.20 102000 250 JPJ 06/05/2019 09:30 Phosphorus 0.86 8570 50.0 BKN 06/05/2019 20:26 Potassium 0.22 2230 50.0 BKN 06/05/2019 20:26 Sulfur 0.94 9370 50.0 KKM 06/06/201911:18 Calcium 8.78 87800 250 BKN 06/05/2019 20:26 Magnesium 0.55 5450 50.0 BKN 06/05/2019 20:26 Sodium 0.17 1660 250 BKN 06/05/2019 20:26 Iron 8210 50.0 BKN 06/05/2019 20:26 Aluminum 9270 50.0 BKN 06/05/2019 20:26 Manganese 208 5.00 BKN 06/05/2019 20:26 Copper 172 2.50 BKN 06/05/2019 20:26 Zinc 140 12.5 BKN 06/05/2019 20:26 Ammonia Nitrogen 1.37 13700 100 JPJ 06/05/2019 13:30 Organic N 8.83 88300 250 06/05/2019 09:30 Nitrate+Nitrite-N 310 4.82 ZBD 06/07/201912:36 All values are on a dry weight basis except as noted by asterisk. Detection limit on a01 N series is on a wet basis. B - Analyte detected in blank H -Beyond Holding Time I ��G Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. SM-2540G SM-2540G SM-4500-NH3C-TKN 6010D 6010D 6010D [:1<i7�[�1�1 6010D 6010D [:1<iy[�1�� 6010D 6010D 6010D 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 m` ��,"�' Pauric McGroary Agronomist Page 4 of 7 Report Number: 19-151-0208 Account Number: 46483 Send To: Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville , NC 27028 11Va Dint-.. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax SQ4-271-6446 www.waypointanalytical.cam Project :Randleman WWTP REPORT OF ANALYSIS Date Sampled: 5/29/2019 11:45:00 Lab Number : 66658 Date Received: 05/31/2019 00:00 Sample Id :Randleman WWTP Date Reported: 06/07/2019 [�Fi:Gi11R�i1 Chromium Nickel Lead Arsenic Mercury Selenium p H '" Calcium Carbonate Equivalent Molybdenum Comments: <1.00 1.00 BKN 06/05/2019 20:26 6010D 63.4 2.50 BKN 06/05/2019 20:26 6010D 17.3 2.50 BKN 06/05/2019 20:26 6010D 29.8 3.00 BKN 06/05/2019 20:26 6010D <5.00 5.00 BKN 06/05/2019 20:26 6010D 0.198 0.0153 TJS 06/05/2019 11:39 SW-7471 B <5.00 5.00 BKN 06/05/2019 20:26 6010D 10.7 JSL 06/05/2019 07:32 9045D 21.80 218000 1000 DXT 06/05/2019 10:11 AOAC 955.01 8.30 2.50 BKN 06/05/2019 20:26 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H -Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page 5 of 7 �' '� a � 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.way p o i nta n a l y ti ca I. co m Cooler Receipt Form Customer Number: 46483 Customer Name: Synagro Central LLC/ Randleman Report Number: 19-151-0208 Shipping Method 0 Fed Ex � US Postal � Lab � Other UPS � Client � Courier Thermometer ID: Shipping container/cooler uncompromised? � Yes � No Number of coolers received � 1 Custody seals intact on shipping container/cooler? � Yes � No � Not Required Custody seals intact on sample bottles? � Yes � No ®Not Required Chain of Custody (COC) present? � Yes � No COC agrees with sample label(s)? � Yes � No COC properly completed � Yes � No Samples in proper containers? � Yes � No Sample containers intact? � Yes � No Sufficient sample volume for indicated test(s)? � Yes � No All samples received within holding time? � Yes � No Cooler temperature in compliance? � Yes � No Cooler/Samples arrived at the laboratory on ice. ®Yes � No Samples were considered acceptable as cooling process had begun. Water -Sample containers properly preserved � Yes 0 No ®N/A Water -VOA vials free of headspace � Yes � No � N/A Trip Blanks received with VOAs � Yes 0 No � N/A Soil VOA method 5035 —compliance criteria met � Yes � No � N/A High concentration container (48 hr) � Low concentration Encore samplers (48 hr) High concentration pre -weighed (methanol -14 d) (— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? � Yes � No Comments: Signature: Brandi Watson Date &Time: 05/31/2019 12:41:39 Page 6 of 7 SAMPLING LOG # CUSTOMER: ZDYNALtHU I PROJECT MANAGER:---? 1 � l OP LI 1 Phone: A & L CUSTOMER LAB # SAMPLE I.D. Relinquished by Sampler: ��� Relinquished by: Relinquished by: �IIII�IIIUII���llll�l�l�1l� 46483 ; F�D�IWD ��F �USYL'®®1f' �i0_r�®lftD d�B�A1LYSDS Svnaare Central LLC1 Ran 12:04:20 CORD Randleman WWTP ,roper field sampling procedures were uses ourmg the collection of these samples. SAMP!ING SAMPLE LOCATION TYPE S L %Comp ��,,��,pp Date Time 5/5DI101 ISOu ote I Time �n 6 t Time # OF CONTAINERS 1 Recieved by: Recieved by: SAMPLER SAMPLING DATE TIME 5/Zgrj Z Ills METHOD PRESERVED REMARKS: SPECIAL INSTRUCTIONS: '� j� For monitoring purposes. (STATE} PO#: SAMPLE ANALYSIS REQUEST "®' SL-I SL2 NHQ N NOS N Organic Cd Cr Ni Pb As Hg Se PH CaG03 Volatile Mo equity Solids WijiP ��1`����A�P����/ p� SLG:Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc METHOD SHIPPED UPS Product Code Product Name Sample Date Report Range Ratio 2027-01-LIQ-NC RANDLEMAN, NC RANDLEMAN WWTP 5/29/2019 1/1/2019-8/31/2019 0.2549 LIQUID Na mg/I = (Na mg/kg x %Solids) = 100 = (1660 x 3.0200) _ 100 = 50.132 Ca mg/I = (Ca mg/kg x %Solids) = 100 = (87800 x 3.0200) _ 100 = 2651.56 Mg mg/I = (mg mg/kg x %Solids) = 100 = (5450 x 3.0200) _ 100 = 164.59 Na meq = Na mg/I _ Molec.Wgt.Na = 50.132 + 23 = 2.17965 Ca meq = Ca mg/I = Molec.Wgt.Ca = 2651.56 + 20 = 132.578 Mg meq = Mg mg/I = Molec.Wgt.Mg = 164.59 _ 12 = 13.7158 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.17965 = SgrRoot[0.5(132.578+13.7158)] = 0.254853 Printed: 2/5/2020 Page 1 10:39 Waypoi nt ,. ANALYTICAL 8/23/2019 Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-227-0010 Project Description: Randleman WWTP 7621 Whitepine Road, Richmond, VA 23237 Main $04-743-9401 °Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received samples) on 8/15/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Virginia 460014 Page 1 of 6 �, # �, � � ► 7621 Whitepine Raad, Richmond, VA 23237 Main $t)4-743-94p1 °Fax $Q4-271-6446 www.waypainta nalyfical.cam Sample Summary Table Report Number: 19-227-0010 Client Project Description: Randleman WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 67839 Randleman WWTP Solids 08/13/2019 10:15 O8/15/2019 67839 Randleman WWTP Solids 08/13/2019 10:15 08/15/2019 SM-2540G WTN 67839 Randleman WWTP Solids 08/13/2019 10:15 08/15/2019 SW-74716 WTN 67839 Randleman WWTP Solids 08/13/2019 10:15 08/15/2019 SM-4500-NH3C-TKN WTN 67839 Randleman WWTP Solids O8/13/2019 10:15 08/15/2019 4500NO3F-2011 WTN 67839 Randleman WWTP Solids 08/13/2019 10:15 08/15/2019 6010D WTN 67839 Randleman WWTP Solids OS/13/2019 10:15 08/15/Z019 SM-4500-NH3C WTN 67839 Randleman WWTP Solids 08/13/2019 10:15 08/15/2019 9045D WTN 67839 Randleman WWTP Solids 08/13/2019 10:15 OS/15/2019 AOAC 955.01 WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 Report Number: 19-227-0010 Account Number: 46483 Send To: Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville , NC 27028 �' �� �,: �� ANP�LYTICaL 7621 Whitepine Road, Richmond, VA 23237 Main SD4-743-94D1 °Fax 8D4-271-6446 www.waypointanalytical.cam Project :Randleman WWTP REPORT OFANALYS/S Date Sampled: 8/13/2019 10:15:00 Lab Number : 67839 Date Received: 08/15/2019 00:00 Sample Id :Randleman WWTP Date Reported: 08/23/2019 Total Solids * 3.60 ADM 08/19/2019 16:04 SM-2540G Moisture * 96.40 ADM 08/19/2019 16:04 SM-2540G Total Kjeldahl Nitrogen 4.47 44700 250 JPJ 08/22/2019 11:00 SM-4500-NH3C-TKN Phosphorus 0.72 7150 50.0 BKN 08/21/201919:19 6010D Potassium 0.15 1460 50.0 BKN 08/21/201919:19 6010D Sulfur 0.79 7900 50.0 BKN 08/21/201919:19 6010D Calcium 12.10 121000 2500 BKN 08/22/201910:03 6010D Magnesium 0.61 6080 50.0 BKN 08/21/201919:19 6010D Sodium 0.08 797 250 BKN 08/21/201919:19 6010D Iron 7020 50.0 BKN 08/21/201919:19 6010D Aluminum 16200 50.0 BKN 08/21/201919:19 6010D Manganese 236 5.00 BKN 08/21/201919:19 6010D Copper 158 2.50 BKN 08/21/201919:19 6010D Zinc 127 12.5 BKN 08/21/201919:19 6010D Ammonia Nitrogen 1.14 11400 100 JPJ 08/22/2019 11:15 SM-4500-NH3C Organic N 3.33 33300 250 08/22/2019 11:00 CALCULATION Nitrate+Nitrite-N <4.89 4.89 ZBD 08/22/201914:28 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H -Beyond holding time I �tG �� ��4N� Our reports and letters are for the exclusive and confidential use of ourclients, and may not be reproduced in whole or part. nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other pub/ic announcements without obtaining ourprior written authorization. AgfOnOn'IISt Page 3 of 6 Report Number: 19-227-0010 Account Number: 46483 Send To: Synagro Central LLC/ Randleman Mary Brewer 284 Boger Road Mocksville , NC 27028 '�IVa aint..: �� ANALYTICAL 7621 Whitepine Read, Richm©nd, V�4 2323? Main $U4-743-94U1 °Fax 804-271-6446 www.waypointanalytical.com Project :Randleman WWTP REPORT OF ANALYSIS Date Sampled: 8/13/2019 10:15:00 Lab Number : 67839 Date Received: 08/15/2019 00:00 Sample Id :Randleman WWTP Date Reported: 08/23/2019 Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH Calcium Carbonate Equivalent Molybdenum Comments: <1.00 1.00 BKN 08/21/201919:19 6010D 41.8 2.50 BKN 08/21/201919:19 6010D 13.7 2.50 BKN 08/21/201919:19 6010D 30.5 3.00 BKN 08/21/201919:19 6010D <5.00 5.00 BKN 08/21/201919:19 6010D 0.200 0.0157 TJS 08/20/2019 12:59 SW-7471 B <5.00 5.00 BKN 08/21/201919:19 6010D 11.8 JSL 08/21/2019 07:06 9045D 27.80 278000 1000 DXT 08/22/2019 06:38 AOAC 955.01 5.13 2.50 BKN 08/21/201919:19 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H -Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, fhe results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. 1 G�r<G 1"'� ���� Pauric McGroary Agronomist Page 4 of 6 u �� ' • • ► � � 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9441 °Fax 804-271-5446 www.waypo i nta n a i yti ca I. co m Cooler Receipt Form Customer Number: 46483 Customer Name: Synagro Central LLC/ Randleman Report Number: 19-227-0010 Shipping Method Fed Ex � US Postal 0 Lab � Other UPS 0 Client � Courier Thermometer ID: Shipping container/cooler uncompromised? ®Yes � No Number of coolers received 1 Custody seals intact on shipping container/cooler? � Yes � No ®Not Required Custody seals intact on sample bottles? � Yes � No ®Not Required Chain of Custody (COC) present? � Yes 0 No COC agrees with sample label(s)? � Yes 0 No COC properly completed � Yes � No Samples in proper containers? � Yes 0 No Sample containers intact? � Yes � No Sufficient sample volume for indicated test(s)? � Yes � No All samples received within holding time? � Yes 0 No Cooler temperature in compliance? � Yes � No Cooler/Samples arrived at the laboratory on ice. � Yes ®No Samples were considered acceptable as cooling process had begun. Water -Sample containers properly preserved 0 Yes � No ®N/A Water -VOA vials free of headspace � Yes 0 No � N/A Trip Blanks received with VOAs � Yes � No � N/A Soil VOA method 5035 —compliance criteria met 0 Yes � No � N/A � High concentration container (48 hr) � Low concentration Encore samplers (48 hr) High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? � Yes � No Comments: Signature: Brandi Watson Date &Time: 08/15/2019 14:00:06 Page 5 of 6 PROJECT MANAGER: Phone: (a)b C4JST®MEfl SAMPLE I.G. wftv)i Relinquished by Sampler: , r `�� Relinquished by: Relinquished by: SAMPLING LOCATION vy�c.n Date � y/ A&L 7621 1 Richm __4� Omf Time E -00 Time Recieved by: by: 19�227-0010 OF464M ID & ANALYSIS 0&15�2019 RECORD dit .procedures were usea aunng tne collection of these samples. SAMPLER SAMPLlN% ®ATE TIME w REMARKS: PS SP'ECkAL 1NSTRUCTiONS: � � JL ' / „„� r ,� For co monitoring purposes% PO#: (STATE) ANALYSIS REQUEST SAMPLE SL2 NH4-N NO3-N Organic N Cd Cr iyi Pb As Hg Se PH cacti a uiv Volatile Solids MQ Cl NC► N z' SL�I SL�i: Total Solids (Moisture), Total ICeidahi Nitrogen, Phosphorus, and Potassium aL2: Basic Test SLi pins Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Page 6 of 6 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2027-01-1.IQ-NC RANDLEMAN, NC RANDLEMAN WWTP 8/13/2019 9/1/2019=12/31/2019 0.1148 LIQUID Na mg/I = (Na mg/kg x % Solids) - 100 = (797 x 3.6000) = 100 = 28.692 Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (121000 x 3.6000) = 100 = 4356 Mg mg/I = (mg mglkg x %Solids) _ 100 = (6080 x 3.6000) _ 100 = 218.88 Na meq = Na mg/I _ Molec.Wgt.Na = 28.692 _ 23 = 1.24748 Ca meq = Ca mg/I - Molec.Wgt.Ca = 4356 _ 20 = 217.8 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 218.88 + 12 = 18.24 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.24748 = SgrRoot[0.5(217.8+18.24)] = 0.11483 Printed: 2/5/2020 Page 1 18:12 •_. • ! •[rpm • Product Code Product Name Sample Date Report Range Ratio 2027-01-LIQ-NC RANDLEMAN, NC RANDLEMAN WWTP 8/13/2019 9/1/2019=12131/2019 0.1148 LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (797 x 3.6000) + 100 = 28.692 Ca mg/I = (Ca mg/kg x %Solids) + 100 = (121000 x 3.6000) + 100 = 4356 Mg mg/I = (mg mg/kg x %Solids) = 100 = (6080 x 3.6000) _ 100 = 218.88 Na meq = Na mg/I _ Molec.Wgt.Na = 28.692 + 23 = 1.24748 Ca meq = Ca mg/I = Molec.Wgt.Ca = 4356 = 20 = 217.8 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 218.88 + 12 = 18.24 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.24748 = SgrRoot[0.5(217.8+18.24)] = 0.11483 Printed: 2/5/2020 Page 1 10:39 FACILITY NAME: RANDLEMAN,NC OWNER: W. HOWARD FIELDS SITE #: NC RD 00018 FIELD# : RD 00018 0003 RESIDUAL SOURCE(S): See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES : CORONICA PERMIT #: W00004825 OPERATOR: W. HOWARD FIELDS A7VNUAL DRY TONS APPLIED : 31.23 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 16.00 ACRES PERMITTED: 16.00 rage: 1 Lime Applied *** Date Lbs/Ac DATE or Gallons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids Acre Source Moist Hours * Rate** Rate Nitrite 8/13/19 552800,00 (G) 3487,500 3.02 0.439 RAL DRY 0-<I/2" SUR 0.5 0.30 1020(p 13,700.00 p 310.00 p 33650 FESCUE HAY 8/15/19 93,000.00 (G) 5812,500 3.02 0.732 RAL DRY 0-<I/2" SUR 0.5 0.30 1020(p 13,700.00 p 310.00 p 33650 FESCUE HAY 8/16/19 99,200.00 (G) 6200,0001 3.02 0.781 RAL DRY 0-<1/2" SUR 0.5 0.30 102,00(p 13,700.00 p 310.00 p 33650 FESCUE HAY Aug49 248,000.00 (G) 15,500.000 Total Gallons/Ac: 15,500.00 Total Wet Tons/Ac: I m� c,ub,u I umtiL0. v.vv As Cu Cr Cu Pb Hg Iwo Ni Se Zn P PAN TOTALS: Annual lbs/acre 131 0.020 0.004 0.248 0.671 0.116 <.001 0.032 0.068 0.020 0.547 33.46 Cumulative lbs/acre 0.131 0.071 4.364 8.559 4.983 0.023 0.241 0.614 0.189 13.976 I7\iB 7\►1�71f�1T/_\�■i`[�i 7\�i�7N�ITI_\��i.�5�]IY��(�1�11� x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL METALS FIELD LOADING SUIVIIVIARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Randleman, NC Total Dry Tons Applied (Annual): 31.23 Permit #: Operator: Acres Used: WQ0004825 W. Howard Fields Cation Exchange Capacity (non 503 only): Owner: W. Howard Fields Predominant Soil Series: Coronica 16 Acres Permitted: 16 Site #: NC RD 00018 Field #: RD 00018 0003 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 5/29/19 2 3 4 5 6 7 8 9 10 11 12 %Solids 3.02 Arsenic 5 Cadmium 1 Copper 172 Chromi 63.4 Lead 29.8 Mercury 0.198 Molyb- denum 8 3 Nickel 17.3 Selenium 5 Zinc 140 Total Phos- horns 8570 Annual Heaw Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ App Event 1.95 �� Arsenic 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.671 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.671 Chromiui 0.248 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.248 Lead 0.116 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 denum Nickel 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.068 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 0.547 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.547 Total Phos- 33.457 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 33.457 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Z /� Z'ZC3 Date DENR FORM MFLSF (12/2006) FACILITY NAME: RANDLEMAN, NC OWNER: ROY HOLDER SITE #: NC RD 00019 FIELD# : RD 00019 0001 RESIDUAL SOURCE(S): See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES : CECIL PERMIT #: WQ0004825 OPERATOR: ROY HOLDER ANNUAL DRY TONS APPLIED : 33.57 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 28.50 ACRES PERMITTED: 28.50 rage: 1 Lime Applied *** Date Lbs/Ac DATE or Gallons (G) or Cubic Yards (CY) or Wet Tons WT (specify) ( ) (p fy) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total ( Per Acre Solids Acre Source Moist Hours k Rate** Rate Nitrite 5/29/19 9000.00 (G) 3157.895 3.02 0.398 RAL DRY 0-<l/2" SUR 0.5 0.30 102,00(p 13,700.00 p 310.00 p 33650 FESCUE PASTURE 5/30/19 144,000.00 (G) 5052,632 3.02 0.636 RAL DRY 0-<1/2" SUR 0.5 0.30 102,00(p 13,700.00 p 310.00 p 33650 FESCUE PASTURE 5/31/19 325600,00 (G) 1143,860 3.02 0.144 RAL MOIST 0-<1/2" SUR 0.5 0.30 102200(p 13,700.00 p 310.00 p 33650 FESCUE PASTURE May-19 266,600.00 (G) 9,354.387 Total Gallons/Ac: Total Wet Tons/Ac: 9,354.39 1 L/L6l \.UVlli 1LLJl AV. U.VV As Cd Cr Cu Pb rigMo Ni Se Zn I- PAN TOTALS Annual lbs/acre 79 0.012 0.002 0.149 0.405 0.070 <.001 0.020 0.041 0.012 0.330 20.19 Cumulative lbs/acre 0.082 0.061 3.476 5.965 3.165 0.020 0.162 0.413 0.100 15.894 1:7_\rB:7•\�1�711�1�/_\r•Ar•[�17\�1�7if u : ►�1dYY�lC�Iillit7 zazo (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR -Surface, INJ -Injection, SURIN -Incorporation *** See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Randleman, NC WQ0004825 Roy Holder Total Dry Tons Applied (Annual): 33.57 Cation Exchange Capacity (non 503 only): Owner: Roy Holder Predominant Soil Series 28.5 Acres Permitted: Cecil 28.5 Site #: NC RD 00019 Field #: RD 00019 0001 Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 5/29/19 2 3 4 5 6 7 8 9 10 11 12 %Solids 3.02 Arsenic 5 Cadmium 1 Copper 172 Chromi 63.4 Lead 29.8 Mercury 0.198 Molyb- denum 8 3 Nickel 17.3 Selenium 5 Zinc 140 Total Phos- horus 8570 Annual Heave Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ App Event 1.18 Arsenic 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.405 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.405 Chromiu 0.149 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.149 Lead 0.070 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.070 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Nickel 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.041 Selenium 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Zinc 0.330 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.330 Total Phos- 20.191 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 20.191 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowj►g violations". of Land Applier � �� zoZo Date DENR FORM MFLSF (12/2006) SHEALY ENVIRONMENTAL SER!/ICES, INC. Repor# of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Ryan Copeland Project Name: Randleman Lot Number:UB13010 Date Completed:02/19/2019 02/19/2019 1:43 PM Approved and released by: Lab Director -Greenville: Lucas Odom A C C R E D I T E D —�— DooDav The electronic signature above is the equivalent of a handwritten signature. This report shall not b.e reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Paint Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 10 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot (dumber: UB13010 This Report of Analysis contains the analytical results) for the samples) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the samples) in this report was/were performed after the method recommended 15 minute holding time. . TCLP VOCs The container received for sample -001 did not contain a teflon lined lid. TCLP Herbicides The continuing calibration verification (CCV) associated with sample UB13010-001 recovered 2,4 D above the upper control limit. The samples associated with this CCV were non -detect for the affected analytes; therefore, the data has been reported. TCLP Pesticides The continuing calibration verification (CCV) associated with sample UB13010-001 recovered Methoxychlor above the upper control limit. The sample associated with this CCV was non -detect for the affected analytes; therefore, the data has been reported. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 10 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Synagra Lot Number: UB13010 Sample Number Sample ID Matrix Date Sampled Date Received 001 Randleman VWVTP Solid 02/12/2019 1330 02/13/2019 (1 sample) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 10 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary Synagro Lot Number: UB13010 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 Randleman WWTP Solid Ignitability (Pensky-Martens 1010A >140 ° F 5 001 Randleman WWTP Solid Reactive Sulfide 7.3.4 60 mg/kg 5 (2 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vdww.shealylab.com Page 4 of 10 Client: Synagro Description: Randleman WWTP Laboratory ID: UB13010-001 Matrix: Solid Date Sampled:02/12/2019 1330 Date Received:02/13/2019 noraanic non-metals Solids: 1.63 02/14/2019 0139 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 02/14/2019 1145 PJK 97581 1 (pH) 9045D 1 02/14/2019 1404 PJK 97582 1 (Reactive Cya) 7.3.3 1 02/19/2019 1201 MSG 02/18/2019 0835 1 (Reactive Sul) 7.3.4 1 02/18/2019 1716 HET 02/18/2019 0835 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 pH @ 20.1 ° C 9045D . 6.4 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 60 50 mg/kg 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/50306 8260B 10 02/15/2019 0514 KGT 97624 02/13/2019 0022 CAS Analytical Parameter Number Method Result Q LOQ Units Run Benzene 71-43-2 8260B ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260E ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 82608 ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260B ND 0.050 mg/L 1 Chloroform 67-66-3 8260B ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260B ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 82606 ND 0.050 mg/L 1 Trichloroethene 79-01-6 82608 ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260E ND 0.010 mg/L 1 Run 1 Accepfance Surrogate Q %Recovery Limits 1,2-Dichloroethane-d4 86 70-130 Bromofluorobenzene 100 70-130 Toluene-d8 96 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 02/17/2019 1404 CMP2 02/14/2019 1819 97588 02/13l2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270D ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270D ND 0.080 mg/L 1 Hexachlorobenzene 118-74-1 8270D ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270D ND 0.040 mg/L 1 LOQ = Limit of Quantitation B =Detected in the method blank E =Quantitation of compound exceeded the calibration range ND =Not detected at or above the LOQ N =Recovery is out of criteria P =The RPD between iwo GC columns exceeds 40 H =Out of holding time W =Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page5of10 Client: Synagro Description: Randleman WWTP Laboratory ID:UB13010-001 Matrix: Solid Date Sampled:02/12/2019 1330 Date Received:02/13/2019 Solids: 1.63 02/14/2019 0139 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 02/17/2019 1404 CMP2 02/14/2019 1819 97588 02/13/2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run Hexachloroethane 67-72-1 8270D ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270D ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270D ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270D ND 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270D ND 0.20 mg/L 1 Pyridine 110-86-1 8270D ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270D ND 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270D ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q %Recovery Limits 2-Fluorobiphenyl 72 37-129 2-Fluorophenol 32 24-127 Nitrobenzene-d5 64 38-127 Phenol-d5 41 28-128 Terphenyl-d14 112 10-148 2,4,6-Tribromophenol 83 41-144 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 02/16/2019 0029 DAL1 02/14/2019 1949 97590 02/13/2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q %Recovery Limits DCAA 76 62-117 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081E 1 02/19/2019 0019 CHG 02/14/2019 1819 97587 02/13/2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run gamma-BHC (Lindane) 58-89-9 8081E ND 0.00040 mg/L 1 Chlordane 57-74-9 80816 ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081E ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081B ND 0.00040 mg/L 1 LOQ = Limit of Quantitation B =Detected in the method blank E =Quantitation of compound exceeded the calibration range ND =Not detected at or above the LOO N =Recovery is out of criteria P =The RPD between two GC columns exceeds 40 H =Out of holding time W =Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 10 Client:Synagro Laboratory ID: UB13010-001 Description: Randleman WWTP Matrix: Solid Date Sampled:02/1212019 1330 %Solids: 1.63 02/14/2019 0139 Date Received:02/13/2019 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 02/19/2019 0019 CHG 02/14/2019 1819 97587 02/13/2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run Methoxychlor 72-43-5 8081 B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 80816 ND 0.0080 mg/L 1 Surro ate Run 1 Acceptance g Q %Recovery Limits Decachlorobiphenyl 88 20-131 Tetrachloro-m-xylene 71 26-132 TCLP Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 6010D 1 02l15/2019 1807 CJZ 02/15/2019 0842 97635 02/13/2019 2300 1 1311/7470A 7470A 1 02/17/2019 2025 JMH 02/17/2019 1313 97780 02/13/2019 2300 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.15 mg/L 1 Barium 7440-39-3 6010D ND 0.25 mg/L 1 Cadmium 7440-43-9 6010D ND 0.050 mg/L 1 Chromium 7440-47-3 6010D ND 0.10 mg/L 1 Lead 7439-92-1 6010D ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 6010D ND 0.20 mg/L 1 Silver 7440-22-4 6010D ND 0.10 mg/L 1 LOQ =Limit of Quantitation B =Detected in the method blank E =Quantitation of compound exceeded the calibration range ND =Not detected at or above the LOQ N =Recovery is out of criteria P =The RPD between two GC columns exceeds 40 H =Out of holding time W =Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 10 Chain of Custody �:J Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page8of10 CD 0 0 Q 0 Sheeny Environment f Services. Inc- `' 1 oe Ventage @girl, Drsva �� Chan of Custody Record Writ Columbia, Scuth Carollne 29172 Number Ta1Bph na Na. ( 3,, 7'91•arGD Fax No. (803) 7919111 ',Ferno.sheEI&b.cufn C,I eset Report to Oxytact Simpler 'P' in(ed Nanw) %Duote No. VA14 Ca Peia" .Aldrass Tebfthone No ax No* Ernai: �, . � � •V�e'Uill �Jr , �a�e Gc fi• r- r _ 1 4f C;+x �itE B zip C= k� rese~,�ati�re Number Containers 7J 1. ems. A. ;AN03 7, NoGH 3aMe Proled Mamie 2. N&C,42rtA 5. HCL hre5eereta,E _.- _ i F'L . J 12. 4 So Na "hka. 1V ''H11Lot N:=* Prajed t 7tsnCar ta.47 Number � C4i81rskt , ,tea - Sample ID;DasuiAon `w t5 a U8'1301 (Cant rr sfor.:s�hsampicrwy':4c Cana Trno GO M �s ctrtnbioed ex) rim Irne; owl x n n tz � 1 1 ;4 TJrtt. 'h'raurrJ'rm Re;shot eRi° til:^ iui Ipsv re xl [y kd Jo• iu:Lr.Qea Tn. T} Simple DisptNal OC Rzqulrerlerrs ?PIoaw OpCCfYi Nsa (ve 4f t nd V(i�r5iif { AIiMM � 1 �Nzm-F#azar,9 �h"Jamm_ gr3kin Irritant IJSlardwd Lush Prim Sot a4y:+ a a. J Rr brut lu Gllerrt I rsposat Lar �, f@ :yakson untnomin '1- +eltnquisied ry1 &ampler, Dalr� �Yre k h. d hp C ^fr iyne 2- Relinquis,r d bye Date Tsne 2. Peai'.•ad by Da le Tanu $. a IinglaeJterJ Ixy tJBt 7snd 3• ',i4 d by Ddu I®rrt r4. %inqulshed u4V ate, #. Laburator� R27 e- rw-d t> D e Tsans Note: All samples are retained for six Weeks from mcelpat tJJ1lother LAB USE ONLY p 1ptT p.. ItMp. q!jpp etnent3 are made Pe• ru tl off+ ILe QGt!?Ck i F ' 01 t� r'+co Pm;c � ' , a c ❑ Y td E^fauctiv* EWa t 06&27r2C 12 �W Z n SIY�Ix' t_lIi'Ifr�Iltler.l�kt Srrr!ICC3. t'YL'. Laru�nesu tdJiblb'r:1tiLQ41"fit-1.1 Fa�� I ai I C:lien7; _ � t.nc�l�r ers ectcrl 6�}rrafate: ; ��• � ,� `� L+at ,�: - ❑ } prakt,a:nt, ttn the rt+�lera Yes ❑ hro I`�A '�. �I� 4u5tdaf;^ seals ti}'ere. }treat�tt; krrea� tltet� ittt�uc antE canl�r[aken? , pll trig Ili. _ C'hlarirtr� �tt'ip li7° _ _� "I'�stcd lr�-- _- Ctri�insE tcrrtperatntre unit eceipt.�r l�ea'iveti tCarreectrxt6 tcrrlperairare uluats reccilat: �"ia5aa}i�l Snapei:up .[DO�^�{�� � fc9�thrtd: ❑'Teinpera[7ii�e lxnk 'first �c�ttla��; 11{ '�'rtrt ID: t€t,rttn Ccyn•Wc:licat Facr�r; °C: TvtetFiarti uf'i:.�alairt: r 't�,`r~t Ise (`1 Ice d'a�:�.� ❑ 13t � Lee �"-1 1wlnne r ,Yes ,� �ry L I•;��, '- I.f temp��ruitarc: of ate} s:aoler e�crc:d..d fi3O"C, t1�as 13rrrjr'o! itrlarlaar• Tt�ut%fia:c}7 Rhi! kaas l�ntilietl dry: pliainrr ?• errr�it .•' f��-tc�-I`ace: fcircte �xttc}. !_ Yes ❑ Rio ❑ N�a. 4. is the ciir7tnrerc:i;a1 ccturit�t's 13ac4,in� slip ai��elter� to this fcin7Y? - _ - r es =l No 5. i'��ere �+rr�ptrrcustrM,`ly' grocei7ktres (rcJat�ttishc.dr'receiva�lj tarllat�rd? es ! I�lo _.. fi, ��rere sffmisli< leis lister on tlie f:t7tJ:r +� [z., blar 7, 'Mlr`cre sasrrplc tl�s tilted on al] fir3n�[e �:olttttiraers'r' �'"e� s� 1Va S. 1�`as collection date � �>rte listicd aptt t17e t�t9C.7 ❑ es �+Pa �. Vt+as ealleet}ott date � tiat7e Gfited' oit all .,�ranl�ie r�rrEslincri? - - � s ❑ Nr� 16t, laid atI asintainer loll inf�rert�iicrn fl Lt. +'ialr:. tithe) rr�rcc kk�itl7 thct C{�rr? _ "es � Nc7 l I , '�r'cre tests ltt be perfaaatte�I Jistetl pan the C't�C? �"� e~5 ❑ �a I �, tl�iai all sxirrlprlrs arri'k�c ilt tJta praipvr cnittrtir�ers fc+r r�ar:h test �rtcl?ar ir7 �a��r:i i.a�rsciiti,�tt ho (du3t.tlaru�cii, Is rfn; etc. tiatfL,sn7pYle} NVIwine a4ailably? Yes ❑ : 14 Nt,`vrc all samPh s recei'�cd within 'I 61te. holding, Time or 8 hvuts, wlt 4.lteter conics first? Yl ! No 15. Wur4 any samples colitaine,•.s arsrssiiWV% s (eir: Iti. oitel sample{ Not listed Lill COC? Yes I ] I�Io If. Far VOA and RSK"I 'S samples, were bubh1c.3 preseatt`�Jre,-sites" ('.%a°'garftttsrr in ciia a7et�r] in I My of the' OIA vials? ❑ Ves l�io 17. Were. all DR0Anetals?matt• tent sata Ple,":1"Mcived. at a PI-1 ct9`t: 2`? ❑ IF ❑ No N 18. � ellie ajl r ; ullido samples rizamly d sal a pf l > 12 and sulJida sanit*les rcc�hed at a pt 1 "= 9? 11. Wifffe All applicable NI l,r'1'I�.�I, eyant eipha ilol,161 (•. E1;3rr rL 1 Barn rJes fi r►fresidu. l C Yes ❑ No YwNA chlnrrrlc:? yes 2l1_ Were. climircmarlcs?railim (Le, r_cqutisteal difuVons, )IIS,rJat�l�7 signaliorul, etc...} correctly lr7ar�scrilted ft'a n� the C7 nrtxr rh¢ zom merit %l ction in f MS4,) _ _ yes No 2l.'Alas the qL i� number Ii,ted art; ttMe umtmner label? If 5'e*> Quote S, Mple. Presurvat nn (h�itrst be Lomplevul ft,r awry sairaple(s) inc�,m,.ctly Bice ertirard or with l7ea4spacc,) al7tlplr(sj Wen: ret:eived ina tail ll preserved anti were 2(1jtr5te41a;xordingly in sample ru` Liviii with mt_. of circle tlrtc r l 12SO 1, l•1NO3,1.1CI, Na014 using SR # 1 imp of presmervatioll If more titan one preurk' anve is heeded, plcusc nare in the ec)r¢rrI-i below. ,ii, pim(sj y eta aec eialld kk� th bubblcs 6 rzanr in dia`rtr;i<r. S'Arraples(s) _ _ _ receivicd viith TRI' > 10 tt'tp?,,r3J (If t+t9 is III ) and were a.djIlstt'cl raccorlty lit sm-aptlr rcccivilte with sodium thiosul}:ate l;?�a,+�',{a,) with Shealy ID_ft _ R bttr code 17boJs apfrJied bv: '_ Date: G - d_ r}tui n cnts: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 10 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: Town of Randleman WWTP Town of Randleman WWTP Monitoring Period: WQ Permit Number: WQ 0004825 NPIDES Number: NC 0025445 From 01/01/19 To 12/31/2019 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion If anulicable to alternative performed (Class A or Class Bl comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6" MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) Option/Alt. 9 (Injection) (40-day bench) Option/Alt. 10 (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) (30-day bench) (Spec. were performed No vector attraction reduction alternatives "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael Glass, Plant Superintendent Prepar r Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Using a pH Meter with Two -Point Standardization and .A,ui omatic Temperatare Compensation (ATC) Probe Analysis Method: SW"846Method 9045D,.Soil And Waste pH Initial pH > 110 S.Ur 2 ]noun p]l > 12.0 S.U. 24 Hour pH >11.5 S.U. � o cp m F Initial Adjusted y ° 2 �Cr */su p Adjusted o �* 244-Ir pH/su Adjusted r piI/su, o Initial rt a '` 2 (� ,� a Temp/°C 24-Hi' x a 9 Temp/ C i* )�I' /su 0 Temp/ C 0 3 r� pE['�lsu co 0 EL .ia co 1,.I m W pIEI*!su ° P e wd h ..� /i2 Z 12.N/LI �Z �JO G 1�/zl°` jz.3� Xj �C! i�3`�f �? f30�' 152i •�I2 13Z3 ,b t2 3 0 /�� ti` Zb iz 1230 �Jl� jz�3 JS i1"� z o t� cab ry�{7 S I2•3�z�r� � t ��I Xd r .� �r 3 ;z,�� f �3 ,,� ,1 l� 1���� H rbs 1 3v le 30012 �3� 1• I % ! / ''r � /,:+ 1246! f!F^ I IS4�1 Zsa 13 1 3o°L ��= �� ►Sy1e —JL, \\%6 3� nL 1 � IZ' � t3IiSr ./ �� �i��o� �.�s IS53.�g �35 EquivalentpIl value at25°C; Con;ectionPaator (CR) = 0.03 pkIuuits x.(°CTemp exatutexneasuremenl:-25°C); Equivalentpll=Measured pk.-ri--coe ter. comments* -23- q � , I I i� . � , I�� ,�� � ; ,���, ,p µ �,, �� �'Tsing a p3C� Meter wi'�Ix'�'wo �'oiztt �1:andardizaizon and �.vttamatic �'ezu�perature Compensatio�a (A.'.�� 'robe aszatysis Method: E'EN-��6 Method 9045ID, Salt Azad i7Vaste p�' � � � y N '"' .�.$�.� g9�>' �.�L.� ���, .� z amour ]�l�> �.�.�Q ���� .-� �� �0ur ]pm[>��,�3 �.�� w a"` o � C~3 �° � '� � � � � .Y .. '3 � � � ., N '° c �: � � � m � � � M � �. ' �,1�}�{{ N W �uitiat p��lsu• "�"em / C iz � Adjusted �zziiial p]fj[*!su "� � � � y '� �* � �' � � yy G p � ti � �. � . n �: ��{( f% t+y � Z ]C�r ;� !su p 7Cemp/°C �.d'usted 1 2_� plf�*/s€z d is ti. � @ � � � "' � � o y � rt ' ,o y �* � y � ^�- � � � p w � g � � � K � ��µ( N i'K 2�-�r 3�/sa P A 7Cezzz / C p adjusted �� �• p�-r/su ' •Jr^' l� f�dB� ��� iz•�3 � 11����d�� lZ''(�lj fg `�'� {1��6�1 3G� �Z-.6`Z. eF'ry3 d r y3 i�w� f2� /23�y DgZS� �� "°� j Z=���1$°G %Z ,aD II'2� '� -.3� 1Z.�,cS f 15" l�Z• 3 0 i2 %z�l%a o�t55 �" z7 �2 `� ��1�, iZ� 1 % �1c��1 og3s' ►i35 * Ec�.iivalezaipI3 value at25�C; Cai�eet9.on:t'actor �tlti) = u.u3 pklutnts x, � u z.empez'atute ineasureanenti—L�-��; �CJ,ulYalt'.11CIJ11"ivlG4Jutcu,Nla -+r- �u� a+i�. Comvzents: Ci :, 5 -zs- • Agricultural Lime Application Log Year: 2019 Project: Randleman Field (state -county -site -field code) Soil pH (from Lime Requirement soil analysis) Tons/Acre Applied Date Applied NC-RD-19-01 5.7 0.3 tons/ac. Liquid Lime NC-RD-18-03 6.9 0.0 tons/ac. Page 1 of 1 Report No: 19-347-0519 Account No: 07216 Advisor: Synagro Central LLC/ Durham Mary Brewer 284 Boger Road Mocksville NC 27028 V1/a oint.�, vp ANALYTICAL Client: Howard Fields 2850 Daisy Lane, Wilson, NC 27896 Main 252-206-1721 °Fax 252-206-9973 www.waypointanalytical.com Farm: RD-18 Submitted By: Synagro Central LLC/ Durham Date Received: 12/13/2019 Date of Report: 12/16/2019 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-1 S-1 Mn-1 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na SS -I NO3 N 21355 Fld 3 RD-18-3 MIN 0.5 6.9 70.0 141 19 50 531 315 315 240 82.6 15 14 1 0.1 0.1 Comment: Test result units =CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are pertormed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Carolina, Inc. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033841 Predictive Client: Roy /Chris Holder Advisor: SYNAG RO �G�GULTUR@moo _ oo2N 4283 Holder Farm Rd. 284 Boger Road _,�°`` � I � � S o a i I Report Mehlich-3 Extraction Liberty, NC 27298 Mocksville, NC 27028 �°�, � �- ��``� Sampled County :Randolph Links to Helpful Information Sampled: Not Provided Received: 06/17/2019 Farm: RD-19 / rdx47 Completed: 06/20/2019 Client ID: 129187 Advisor ID: 499503 Sample ID: RDX471 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N PzOs Kz0 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 _ 0.0 Test Results [units - WN in g/crr>3; CEC and Na in meq/100 crrr3; NOs-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NOs-N 0.32 1.04 12.9 91 1.2 6.3 272 240 63 19 57 695 429 611 611 307 0.1 1 Sample ID: RD19-1 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2O5 Kz0 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.5 120-200 70 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crrr3; NOs-N in mg/drrr�]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NOs-N 0.41 0.83 8.1 81 1.5 5.7 30 89 56 20 42 719 448 195 195 239 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Tobacco Trust Fund Commission Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL033841 Roy /Chris Holder Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crops) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on time, even if the report recommends more. You can apply the rest in similar increments every six months until the full ratE is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient 'to be added (in units of Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 Ib per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pu bs.htm. Report Abbreviations Ac exchangeable acidity B boron BS% %CEC occupied by basic cations Ca% %CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-I potassium index Kz0 potash Mg% %CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-AI1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-1 manganese index M-O mineral -organic soil class N nitrogen Na sodium NOs-N ORG Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH the exact fertilizer grade recommended on the report, visit www.ncapr.crov/agronomi/ob,oart4.htrrrY�sfind information that P-I may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. Pzos S-I Test Results � SS -I WN Zn-AI The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrgov/agronomi/uyrst.htm nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index