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HomeMy WebLinkAboutWQ0005809_Residual Annual Report 2019_20200218Initial Review INITIAL REVIEW Reviewer Williams, Kendall Is this submital an application?* r Yes r No Annual Report 2019 Year* Date Paper Copy 2/17/2020 Received:* Project Number* WQ0005809 Email Notifications ................................................................................................... Does this need O Yes review by the a No hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Kendall.Williams@ncdenr.gov Submitted Form Project Contact Information Rease provide information on the person to be contacted by NJB Staff regarding electronic submittal, confirmation of receipt, and other issues. .................................................................................................................................................................................................................................................................................................................................................................................................... Name * Faron D. Leigh Email Address* Heigh@colpipe.com Project Information Submittal Type* f New Permit Application r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0005809 Applicant\Permittee * Colonial Pipeline Company Facility Name * Colonial Pipeline Company Phone Number* 336-669-7903 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) Land _Application_Annual_Report_2019.pdf 9.38MB upload only 1 RJF document. Multiple documents rust be combined into one RJF file. For new and modification permit applications, a paper copy may be required. If you have any questions about what is required, please contact the reviewer or Tessa Monday. If a paper application is required, be advised, applications accepted for pre -review until both the paper and electronic copies have been received. The paper copy shall include the following: o Application Form o All relevant attachments (caIcs, soils report, specs, etc. 0 one full-size engineering plan set 0 one 11x17" engineering plan set 0 0ne extra set of specifications o Fee (if required} Mailine address: Division of Water Resources Division of Water Resources Non -Discharge Branch I Non -Discharge Branch ---- --- - --- - --- ------------ ------------------------------------i---------------------------------------------------------------------------- 1617 Mail -service Center Att: Nathaniel Thornburg, 9"' Floor, Office #942W ---- -NC �-- - -------------------------------------------- ------------------------------------------------ Raleih, 7699-1617 512 N. SaVisbury St For questions or problems contact Tessa Monday at tessa.monday@ncdenr.Qov or 919.707.3660. * W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 2/13/2020 ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0005809 County: Facility Name (as shown on permit): Land Application Operator: Guilford Year: 2019 Colonial Pipeline Company Faron D. Leigh Phone: 336-669-7903 Land application of residual solids as allowed by the permit occurred during the past calendar year? ❑ Yes 0 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 1-Site, 4-Fields Total number of fields land application occurred during the year: 0 Total amount of dry tons applied during the year for all application sites: Total number of acres land application occurred during the year: Part B: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Resources.0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." nor Brian L. Smith z Pennittee Name and Title (type or print) Signature of Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) DENR FORM ACF (5/2003) Ale � 14 �%1(G4le- ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: WQ0005809 FACILITY NAME: PHONE:336-669-7903 COUNTY: FACILITY TYPE (please check one): ❑ El Colonial Pipeline Company Guilford OPERATOR: Faron D,. Leigh Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? ❑ Yes ❑Ko No If No skip parts A, B, C and certify form below - Part A*: Part B*• Month Sources(s) s) (include NPDES # if in applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons} Intended use(s) January February March April May June July August September October November December Totals: Annual d tons ; 0 0 0 0 Amendments used: I Bulking Agent(s) used: * If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Resources. ❑ Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (11/2005) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0005809 Laboratory: 1) AES, Inc. Facility Name: Colonial Pipeline Company 2) NPDES # or NIA 3) W Q#: WWTP Name: NIA Rvcirinal Analvek nntn 4) 5) Sample or CompositeDate Molybdenum Total Phosphorus ------------ Nitrate and Nitrite "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Colonial Pipeline Company Total Dry Tons Applied (Annual): WQ0005809 Cation Exchange Capacity (non 503 only): 14 Owner: Acres Permitted: 1.55 Site #: Field #: IA Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 1 L2]3 4 5 6 7 8 9 LDJ 11 12 % Solids Arsenic C admimn Chromium Copper Lead Mercury Molyb- denurn Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbslacre): �000000�0�00©0 ®0000000000©00 000�000�0000© .. - 0000000©0000© �0000000000000 �0©©00�0000000 enurn dao�000000 ®�©oo©oo�000�o ®0000000000000 h l EN phorus "i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land App iel r Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied (Annual): Permit #: WQ0005809 Cation Exchange Capacity (non 503 only): Operator: Owner: Acres Used: 0 Acres Permitted: 1.32 Site #: 0 9.93 Field #: 1B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 L3J L 4 5 J _6j 7 _Sj L 9 10 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �000000000�000 ! 000000000000 0�000000©0000 . - 0000�00000000 ©0000®00��000 ®00000�0000000 ®0©00000000000 �000000000�000 ®�0000©0000000 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Colonial Pipeline Company Total Dry Tons Applied (Annual): 0 WQ0005809 Cation Exchange Capacity (non 503 only): Owner: 0 Acres Permitted: 1.8 Site #: 11.5 Field #: IC Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 L 5 6 7 8 9 10 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- horus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): a o© o 0 0 0In .o �0©0000�000000 ®00000000�0000 ' 00000©00�00©� .. - 000000©�00000 �00©000�0000 r 0 �0©00000000��0 �000©0©0000®00 �00000©�0�0�0© ®0©000�000000© Total Phos- r r r r r r r r .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" �lP2 10:1a a Signature of Land App ier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Colonial Pipeline Company Total Dry Tons Applied (Annual): Permit #: WQ0005809 Cation Exchange Capacity (non 503 only): Operator: Acres Used: Owner: Acres Permitted: 0.97 Site #: 11.83 Field #: 1D Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Llj 2 3 j 4 5 6 7 8j 9j 10 11 j 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbslacre): a a W ion �0_0''__00000000 ! 00 �0�0000©o00i000 0�000000�0000 �0�000�0000000 �000�000000000 ����00000000000 ®0000��0©0©000 ®00��000©0©000 ®0��00000©00000 Total ' 1 1 1 1 1 1 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Appliel,7 Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE, Facility Name: Colonial Pipeline Company Permit #: WQ0005809 Annual Dry Tons Applied: Owner: Colonial Pipeline Company Operator: Site #: I Field #: 1 A #DIV/O! Faron D. Leigh Cation Exchange Capacity (non 503): 14 Acres Utilized: 0 Acres Permitted: 1.55 a Q S ecif Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) ite Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- nation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 * Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 1 #DN/O! #DIV/O! #DIV/O! #DIV/O! 2 #DIV/0! #DIV/O! #DIV/O! #DIV/O! 3 #DIV/0! #DIV/O! #DIV/O! #DIV/O! 4 #DIV/O! #DIV/O! #DIV/O! 4DIV/0! 5 #DIV/O! #DIV/0? #DIV/O! #DIV/O! 6 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 7 #DIV/O! #DIV/O! #DIV/O! #DIV/01 8 #DIV/O? #DIV/O! #DIV/O! #DIV/O! 9 #DIV/O! #DIV/O! #DIV/O! #DIV/O? 110 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 11 #DN/O! #DIV/O! #DIV/O! #DIV/O! 12 TOTALS: ##### :::::.:::::.:: As Cd Cr Cu Pb H­ Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 1 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113.351 0 0 42.1497 0 311.572:::::: `:: >::=`::=`:::-: 4.072 143.32 113.351 42.1497 311.572:::::::::::::::::>:::.....:::.. . 9 250 1000 250 500 - Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit I st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit #: WQ0005809 Annual Dry Tons Applied: Owner: Colonial Pipeline Company Operator: Site #: Field #: 1B Faron D. Leigh #DIV/O! Cation Exchange Capacity (non 503): 9.93 Acres Utilized: 0 Acres Permitted: 1.32 o °�' a � Q S ecif Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) ite Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 1 #DIV/O! #DIV/O! #DIV/O! #D1V/O! 2 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 3 #DIV/0! #DIV/O! #DIV/O! #DIV/O! 4 #DfV/O! #DIV/O! #DIV/01 #DIV/O! 5 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 6 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 7 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 8 #DIV/0! #DIV/O! #DIV/O! #DN/O! 9 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 10 #DrV/O! #DIV/O! #DIV/O! #DIV/O! 11 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 12 TOTALS: As Cd Cr Cu Pb Ro Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113.351 0 0 42,1497 0 311.572:::::::::::::::::::::::::::::::::::::::::::: 4.072 143.32 113.351 42.1497 311,572::::::::::::::::::::::::::.............. 9 250 1000 250 500 VA Prior Years Cumulative lbs/ac Permitted C. P. L. R.* * * Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." D�- *Application Method: S - Surface, IN - Injection, INC at -Incorporation Signature o Lan Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Permit #: WQ0005809 Annual Dry Tons Applied: #DIV/O! Owner: Colonial Pipeline Company Site #: Field #: Operator: Faron D. Leigh Cation Exchange Capacity (non 503): 11.5 1 C Acres Utilized: 0 Acres Permitted: 1.80 o o cC Q Specify Totals per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Inches Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- nation Rate** Miner- ali- zation Rate I Aninio nia- Ni- trogen Ni- trace and Nitrite PAN 1 PAN 2 Select Crop 1 or Crop 2 Gal. CuNd. Report Totals in Gal. Crop 1 Crop 2 #DIV/O! #DIV/O! #DN/O! #DN/O! 1 #DIV/O! #DN/O! #DN/01 #DN/O! #DIV/O! #DN/O! #DIV/O! #D1V/01 3 #DIV/O! #DIV/O! #DN/O! #DN/O! 4 #DN/0! #DN/O! #DN/O! #DN/O! 5 #DN/O! #DN/O! #DIV/O! #DN/O! 6 #DIVIO! #DN/O! #DN/0! #DN/O! 7 #DN/O! #DN/O! #DN/O! #DN/O! 8 #DIV/O! #DN/O! #DN/O! #DN/O! 9 #DIV/O! #DN/O! #DN/O! #DiV/O! 10 #DN/O! #DN/O! #DIV/O! #DN/01 11 #DIV/O! #DN/O! #DN/O! #DIV/O! 12 TOTALS: ##### ::=:::.::: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 4.072 0 143.32 113,351 0 0 42.1497 0 311.572 :: >>:.::=:.::: 4.072 143.32 113.351 142,1497 9 250 1000 250 500 ................... ­ Prior Years Cumulative lbs/ac Permitted C. P. L. R. * * * El Permit PAN Limit I st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,� *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land pplier Date **Volatilization Rate: Surface - 0.5. In i ection/Incorp oration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Colonial Pipeline Company Owner: Colonial Pipeline Company Operator Site #: 1 Field #: ID Permit #: WQ0005809 Annual Dry Tons Applied: #DIV/0! Faron D. Leigh Cation Exchange Capacity (non 503): 11.83 Acres Utilized: 0 Acres Permitted: 0.97 o a m o Q Specify Totals per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) ite Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trace and Nitrite PAN I PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd• Report in Gal, Crop 1 Crop 2 #DIV/O! #D1V/O! #DIV/O! #DIV/O! 1 #DIV/O! #DIV/O! #DIV/O! #D1V/O! 2 #D1V/O! #DIV/O! #DIV/O! #DIV/O! 3 4D1V/0! #DIV/O! #DIV/01 #DIV/O! 4 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 5 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 6 #DIV/O! #DIV/O! #DIV/O! #DIV/0! 7 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 8 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 9 #DIV/O! #DIV/O! #DIV/O! #DIV/O! 10 #DIV/O! #DIV/O! #DIV/O! #DN/O! III #DIV/O! #DIV/O! #D1V/O! #DN/O! 12 TOTALS: ##### :::::: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbslac 0 4.072 0 143.32 113.3511 0 1 0 142.1497 1 0 1 31I.572 4.072 143.32 113.3511 1 142.14971:::::::::::::::: 9 250 1000 250 500 Prior Years Cumulative lbslac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ..._ .0 Z-= .Z rJ/ Z—, *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Xpplier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorooration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: A411717-4,0 / / Permit Number: VV WTP Name: ��� NPDES Number: Monitoring Period: From To Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B:I Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Di estion❑ .............. If applicable to alternative performed (Class A or Class B) complete the followin monito -ing data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- deuces requency of Analysis Sample p yp Type Analytical Tech - ni ue Minimluir Geo. Mean Maximurd Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per grain of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction were options performed ❑ P CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) GNP'-59A COMPLIANCE REPORT FORM Perm► ��' O—g{Lc)w (Suhmit one each motriffiring period with GL6.i9 forrny.) Enter date monitoring results were due. ( l ,3//9 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES N IF the answer to question I or 2 is "YES", list in the space provided below the well identification numbers) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maiutenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: /}// ,,9 / /t w r It cvc-r e 6 e /o V c,, S 3% v - 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO" skip to section 8, If the answer to question 5 is "YES'; list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). r /pvPlf rv-rt `jP�o� �- 5• rn ft1OW171 ����7 a'/7 , /—Al Pi+?d�r �76/ /e+r/i Wtrt �3t%O1� �.S r�+l tra�'r G�h�''�JPf• ot�f'% st/6 ./r re 6 Are the monitoring wells listed in section located at or beyond the review boundary? YES N If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO'; monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", h v ! reauired to determine the im act the Waste disposal system is having of the review and compliance boundaries surrounding_thi.7„facillty. FaRure f o do so may_Sr bject the permittea to a Ngtice of Violation_ fines, and/or penalties, 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. )zh71 Signature of Permitted -(or Authorized Agen Date G3 k-59 k 12/8/2003 SUBMIT. FORM ON YELLOW PAPER ONLY - - - �tY/1K IMtnrgur cnvnsa. , • - , IIDlstvolNxOMATERr�ALIT' INFORMA7IONYPRO EsslNc u( rr �; ( GROUNDWATER QUALITY MONITORING: 6r1,7,Rh1A1�5E Y,JCL,CENTEri„R6�LNG(4t NO#69&1 175 ,Phonea(@79)73}3221 ,pf. I;OMPLIANCE'REPORT 'E(JRM 06-30-2022 Please Print Clearly aType PERMIT Number Expiration Date: Eg,GILITY INFORMATION Name: Colonial Pipeline Company Non -Discharge WQ0005809 UIC Facility NPDES Other Permit Name (if different): TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address: 411 Gallimore Dairy Road (Steep 27409 County Guilford ❑ Lagoon ❑ Remediation: infiltration Gallery Greensboro NC (Zlg), ❑ Spray Field ❑ Remediation: Iri4c (wale) ,. Telephone#: 336 669-7903 ElRotary Distributor 50 Land Application of Sludge Faron D. Leigh Contact Person: 9 No. to be sampled: 5 ElWater Source Heat Pump ❑ Other: Well Location/Site Name: Downgradient _ of wells ` from Pe<ma If WELL SAMPLING INFORMATION - WAS. MW-1 {MW-1 B) Date samplecollected: �� �� �� FIELD ANALYSES: WELL ID'NUMBER'(from Permit): DRY at H z- , units Temp. G • 3 C ✓� �� - Well Depth: 21.20. ft. Well Diameter: _2 in. P time of µ Mhos .Depth to Water Level: ft. below measuring point Screened Interval' 5 ft. to 20 ft. Spec. Cond. sampling,.. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor check here: Volume of water pumped/bailed: before sampling: ti, 01 gallons Appearance ❑ Samples for metals were collected unfiltered: RIYES ❑ NO and field acidified: ®YES ❑ NO t ABORATORY INFORMATION //-O II 13 Laboratory Name: Analytical Environmental SeMces Certification No. 562 Date sample analyzed; j-%1,v PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. - Lead <O• mg/I tom%/&% COD mg/I Nitrite (NO2) as N mg/I Pb- Nitrate (NO3) as N /, a' mgA Zn -Zinc67, Ad3 m9A Coliform: MF'Fecal /100ml Coliform: MFTotal - /100ml Phosphorus:: Total as P _ mg/I (Note; Use MPN method for highly wmid samples).. Orthophosphate _ mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids:: Total oU/ mg/I AI -Aluminum mgA pH. (when analyzed) units Be - Barium mg/I TOG mg/I Ca=Calcium mgA Chloride %//• 9 mg/I Cd- Cadmium <f-f. 17/1 s mg/I mgA Total a% d /±t mg/I Arsenic. -Chromium: Grease and Oils mg/I Cu- Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method#. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercurymg/I Report Attached? 5a Yes (1) ❑ No (0): Specific Conductance µMhos K Potassium mg/I VOC , method # 8260 Total Ammonia C G , „•( /i mg/I lMg - Magnesium mg/I ; method # (nmmonla Nitrogen; Wass N; Ammonia Nio-osen..:ota Mn - Manganese _ mg/I , method # TKN as N mgA Ni - Nickel mg/I ; method # - . VOC Removal%. For Remadhafflon Systems i I. certiF/that, to the best of my knowledge and belief, the information submitted in this report fs true; accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysts by a DWC-certifed laborato I am aware that there are si nifcant enalties for submien false information, indudin the bssibilit of foes arirl tm risonment for knowwiolatiens. ••- _ •- Pennittea, (or Auth.d�d Agent) Name and Title - Please Drintor Wive gnalt�m�of Permittes, (or AuthOrized j�aent) 00 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample mo MW-1 Project Name: Greensboro Collection Date: 1116/201910:00:00 AM Lab ID: 1911610-001 Matrix: Aqueous Reoortimi Dilutian .vnagses Aanan Limit YURI units uatcnw Factor Lime Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0,50 ug/L 288036 1 11/12/2019 W45 JE 2,2-Dichloropropane BRL 0.50 ug/L 288036 1 11/12201918:45 JE 2-Chlorotoluene BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE n-Butylbenzene BRL 0.50 ag/L 298036 1 11/121201918:45 JE n-Propylbenzene BRL 0.50 ag/L 289036 1 11/12/2019 18:45 JE Dichlorodifluoromethane BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE Chloromethane BRL 0.50 ug)L 298036 1 11/12/2019 18:45 JE Vinyl chloride BRL 0.50 ug/L 288036 t 11/12/2019 18:45 JE Bromomethane BRL MG ug/L 288036 t 11112/201918:45 JE Chloroethane BRL 1.0 ag/L 288036 1 11/12/2019 18:45 JE Trichlorofluoromethane BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE 1,1-Dichloroethene BRL 0.50 ag/L 288036 t 11/12/2019 18:45 JE Methylene chloride BRL 5.0 ug/L 288036 1 11/12/2019 18:45 JE trans-1,2-Dichloroethene BRL 0.50 ug/L 288036 t 11/12/2019 18:45 JE 1,1-Dichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE cis-1,2-Dichloroethene BRL 0.50 ug/L 288036 1 11/12/201919:45 JE Bromochloromethane BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE Chlorofonn BRL 0.50 ug/L 288036 1 11/12201918.45 JE 1,2-Dichloroethane BRL 0.50 ug/L 288036 t 11/12/2019 18:45 JE 1, 1, 1-Trichlor0ethane BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE 1,1-Dichloropropene BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE Carbon tetrachloride BRL 0.50 ug/L 288036 1 11/12201918:45 JE Benzene BRL 0.50 ag/L 288036 1 IM2201918:45 JE Dibromomethane BRL 0.50 ng/L 288036 1 11/12/2019 18:45 IF Tichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE Bromodichloromethme BRL 0.50 ag/L 289036 1 11112/201918:45 JE 1,1,2-Trichloroethane BRL 0.50 ug/L 288036 t 11/12201918:45 JE Toluene BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE 1,3-Dichloropropane BRL 0.50 og/L 288036 1 11/12201918:45 JE Dibromochloromethme BRL 0.50 ug/L 288036 I 11112201918:45 JE 1,2-Dibromoethme BRL 0.50 ug/L 288036 t ll/12201918:45 JE Tetrachloroethene BRL 0.50 ug/6 288036 1 11/12/2019 18:45 JE 1,1,1,2-Tetrachloroetlrane BRL 0.50 ag/L 288036 1 11/12/2019 18:45 JE Chlorobenzene BRL 0.50 ug/L 288036 1 11112201918:45 JE Ethylbenzene BRL 0.50 ug/L 288036 1 11/12201918.45 JE Bromoform BRL LO ug/L 288036 1 11/12201918A5 JE Styrene BRL 0.50 ug/L 288036 1 11/12/2019 18:45 JE 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 288036 l 11/12/2019 18:45 JE 1,2,3-Trichloropropane BRL 0.50 ug/L 288036 l 11/122019 18:45 JE Isopropylbenzene BRL 0.50 ug/L 288036 1 1t/l22019 18:45 JE Bromobenzene BRL 0,50 ug/L 288036 1 11/12/2019 18:45 JE Qualifiers: s Value exceeds maximum comminant level E Estimated(valne above goantitation more) BRL Below reporting limit S Spike Revewty outside limits due to matrix H Holding times far pmpamtioo or analysis exceeded Nan Seecaseomrative N Analyto not NELAC eatined NC Netconnrmed B Analyze detected in tho essecinted methoJ blank < Less than Result vahte > Gtenterthan Resnitvelue I Estimated value detected below Reporting Limit Page 10 of 52 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 1116/201910:00:00 AM Lab ID: 1911610-001 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Diclrlorobemene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobomene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzeoe BRL Xylenes, Total BRL Surr: Dibromofluoromethane 98.8 Surr: Toluene-d8 99.1 Surr: 4-Bromofluorobenzene 99.6 Total Phosphorus E365.1 Phosphorus, Total (As P) 3.00 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 221 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 10.9 Nitrogen, Nitrate (As N) 1.83 Hydrogen Ion (pH) by SM4500 H+ B pl-I 623 Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) 30 METALS, TOTAL SW6010D Cadmium BRL Qunliaers: ` value exceeds maximum eantaminent level BRL Below reportinglimit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than aesnh value (SW5030B) 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 u9/1- 288036 1 11/12201918:45 JE 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 ug/L 288036 1 111121201918:45 JE 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 ug/L 288036 1 11/12201918'45 JE 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 ug/L 288036 1 11/121201918:45 JE 1.0 ug/L 288036 1 11/12201919:45 IL 0.50 ug/L 288036 1 11/12/2019 18:45 JE In ug/L 288036 I 11/12/2019 18:45 JE 0.50 ug/L 288036 1 11/12/2019 18:45 JE 0.50 ug/L 288036 1 11/12201918:45 JE 2.0 ugll, 289036 1 11112201918:45 JE 76.4-125 %REC 288036 1 11/12/2019 18:45 JE 78.3-116 %REC 289036 1 11/12/2019 18:45 JE 64-125 %REC 288036 1 11/12/2019 18:45 JE (E365.1) 0.500 mg/L 287844 10 11/11201917:29 GO to mg/L 287951 1 II/13/2CI917:30 At (E350.1) 0.200 mg/L 287780 1 1 1/0M019 12:44 TL 1.00 mglL R411268 1 11/07/201916:27 BC 0.250 m9/1- R411268 1 11107/201916:27 BC 0.0100 H pH Units R411455 20 H Colonies/100 R411233 ml (SW3010A) 0.0050 mg1L 287829 1 11/12/201914:01 CS 10 11/071201913:42 MH 1 11/13/2019 10:47 KB E Estimated (vaue above quentimtion range) S Spike Recovery outside limits due to matrix Nmr Seecesenermtive NC Not cautioned < Less. than Being value J Estimated value detected below Reporting Limit Page 11 of 52 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: I l/6/2019 10:00:00 AM Lab ID: 1911610-001 Matrix: Aqueous Reporting Dilution Analyses Result Quad Units BatchlD Date Analyzed Analyst Limit Factor METALS,TOTAL SW6010D (SW3010A) Chromium 0.0144 0.0100 n,g/L 287829 1 11/13/201910:47 KB Lead BRL 0,0100 mg/L 287829 t 11/13/201910:47 KB Zinc 0203. 0.0200 nag/L 287829 1 11113/201910:47 KB Qualifiers: " Value c<ceeds maximum aiummuiwnt level BRL Below reporting limit H Holding times For preparation m analysis exceeded N Acolyte not NELAC certified E Acolyte deloo" in the associated method blank > Grater than Result value H Estimated (value above quontitation mnge) S Spike Recovery outside limits due to matrix No, See case narrative NC Not coufimmd < Less tlwn Result value 1 Estimated vale detected below Reporting Limit Page 12 of 52 SUBMIT FORM ON YEI I QW PAPER�ONLY > . DEPARTMENTOFENVI[., .MENTSNATURALRESOURCES" _ OCEsslNorumT ; ,+ w�sloNorwArEa4�aLIr1I10ZS e"I'T" GROUNDWATER QUALITY MONITORING: ,, 61TgMAILlSERVi65CENTER�RAL'EIGH;NC,27.699=1617 FPhone:(e19)7333221 ,., COMPCIANCE`REPORT FORM PERMIT Number: Expiration Date: 06-30-2022 Please Print Clearly Of Type FACILITY INFORMATION Colonial Pipeline Company Non -Discharge WQ0005809 UIC Facility Name. NPDES - Other Permit Name (if different): 411 Gallimore Dairy Road - TYPE OF PERMITTED OPERATION BEING MONITORED _ Facility Address: (sues`) NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro. p Y :❑Remediation. ❑ S ra Field ( aiaie) (zip) _ (cry( Faron D. Leigh Telephone#: 336-669-7903 _ ❑ Rotary Distributor ® Land Application of Sludge Contact Person: Well Location/Site Name: Downgradient No, of wells to be sampled: 5 ❑ Water Source Heat Pump ❑ Other. from permit) If WELL ' SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-2 Date sample collected: �/ —(L� /� FIELD ANALYSES: q WAS DRY at Well Depth: 25.20 ft. _2 Well Diameter., in. f�.� C pH 5�units Temp. ' time. of Depth to Water Level. % rt �. ft. below measuring point Screened .Interval: 18 ft. to 23fL S µMhos per. Cond. sampling, Measuring Point is 1.75 ft. above land surface : Relative M.P.Elevation: ft. Odor check here:❑ Volume. of water pumped/bailed before sampling: 'p, O gallons Appearance Samples for metals: were collected 'unfiltered: ®YES ONO and field acidified: ®YES El NO ARORATORY INFORMATION. Date: sample analyzed:_ // %3 Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. N Pb -Lead G ®, dle� mg/I COD mg/I Nitrite (NOZ) as mg/I 'Coliform: MF Fecal /100ml Nitrate (NO3) as N ;,�,; fjo mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mgA (Note. Use MPN method for highly turbid samples) < Orthophosphate !rig/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 621-1 ham_° mg/I AI -Aluminum m9A pH (when analyzed) units Ba- Barium mg/1 TOC mg/I Ca- Calcium 'mg/I Chloride �43. 3 mg/I Cd - Cadmium 40. OOS mg/I -Arsenic mg/I Chromium: Total '44.8/0�r mgA Grease and Oils mg/I Cu Copper mgA ORGANICS: (by GC, GC/MS, HPLC). Phenol mg/I Fe -iron mg/I (Specify test and method:#. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? 5a Yes (1). ❑ No (0) Specific Conductance µMhos K- Potassium mgA VOC , method# 8260 Total Ammonia S 6• ® mg/I.- Mg - Magnesium m9/1 .;method#.... (Ammonia Mtroaen; NH3 as N: Ammonia Nitrogen. Total). Mn Manganese mg/I ,..method# TKN as N mg/I Ni - Nickel mg/I ,.method #.. For Remediation Systems Only. (Attach Lab. Reports): best knowledge and belief. the information submitted Influent Total VOCS:: mg/L Effluent Total VOCs: mg/L VOC Removal% in this report is true. accurate, and complete, and thatthe laboratoryanalyficai data was produced using approved methods ofanalysis by a I certify that, to the of my V. I am aware that there anasignificant penalties for - submittin false information, including the possibility of fines and i , Z If 2/ i Brian L:..Smith - :Operations Manager - (Date) Permittee.(or Authorized Agent) Name and Title Please Pdntor Noe Sign of Permittee(or Authorrzed Agent) GW-59 Rev. 1/2007 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: I1/6/201910:30:00AM Lab ID: 1911610.002 Matrix: Aqueous Analyses Result Reporting Limit Qua[ Dilution Units BatchlD Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE 2,2-Dichloropropane BRL 0.50 Rg/L 288036 1 11/12/2019 19.10 JE 2-Chlorotoluene BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE n-Butylbenzene BRL 0,50 ug/L 288036 1 11/12/2019 19:10 JE n-Propylbenzene BRL 0,50 ug/L 288036 1 11/12/2019 19:10 JE Diehlorodifluorometlrane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE Chloromethane BRL 0.50 ng/L 288036 1 11/12/2019 19:10 JE Vinyl chloride BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE Bromomethane BRL 0.50 ug[L 288036 1 11/12/2019 19:10 JE Chloroethane BRL 1.0 ug/L 288036 1 11/12/2019 19:10 JE Trieblorotluoromethane BRL 0.50 ug/L 288036 1 11AM01919:10 JE 1,1-Dichloroethene BRL 0.50 ug/L 288036 1 t l/12/201919:10 JE Methylene chloride BRL 5.0 ug/L 288036 1 11/12/2019 19:10 JE trans-1,2-Dichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 19.10 JE 1,1-Dichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE cis-1,2-Dichloroethene BRI. 0.50 ug/L 288036 1 11112201919:10 JE Bromochloromethane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE Chloroform BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE 1,2-Dichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE 1, 1, 1-Trichloroethane BRL 0.50 ug/L 288036 1 11/122019 19:10 JE I,l-Dichloropropcne BRL 0,50 ngn. 288036 1 11/12/2019 19:10 JE Carbon tetrachloride BRL 0.50 ug/L 288036 1 11/12/201919:10 JE Benzene BRL 0.50 ng/L 288036 1 11112/201919:10 JE Dibromomethane BRL 0.50 ug/L 288036 I I1/12/201919:10 JE Trichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE Bromodichloromethane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE 1,1,2-Trichloroethane BRL 0.50 ug/L 288036 1 U/12201919:10 JE Toluene BRL 0.50 ug/l, 298036 1 11/12/201919:10 JE 1,3-Dichloropropane BRL 0.50 ug/L 288036 1 11/12/201919:10 JE Dibromochloromethime BRL 0.50 ug/L 288036 1 11/12/201919:10 JE 1,2-Dibromoethane, BRL 0.50 og/L 288036 1 11/12/2019 19:10 JE Tetrachloroethene BRL 0.50 ug/L 288036 1 11/12201919:10 JE 1, 1, 1,2-Tetrachloroethane BRL 0.50 uglL 288036 1 I1/122019 19.10 JE Chlorobenzene BRL 0.50 ug/6 288036 1 11/12/2019 19:10 JE Ethylbenzene BRL 0.50 ug/L 288036 I WIM01919:10 1E Bromoform BRL L0 uA 288036 1 11/12201919:10 JE Styrene BRL 0.50 ug/L 288036 1 11/12201919:10 JE 1, 1,2,2-Tetrachloroethane BRL 0,50 ug/L 299036 1 11/12/2019 19:10 JE 1,2,3-Trichloropropane BRL 0.50 ug/L 288036 1 11/12/2019 19:10 JE Isopropylbenzeue BRL 0.50 ug/L 298036 I 11/12/2019 19:10 JE Bromobenzene BRL 0.50 .91 288036 1 11/12201919:10 JE Qualifiers: r Value exceeds maximum conmminant level E Estimated (valna above quuntitation mnge) BRL Belowreporting limit S Spike Recovery outside limirs due to mevix hI Bolding times far prepemtion or analysis exceeded Narr, See case oumtive N Analyte not NELAC certified NC Notconfinned B Analyto detected in the associated method blink < Less than Result vain > Grentertban Resultvalne 1 Bstimat,1 value detected below Reporting Limit Page 13 of 52 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: I t/6/2019 10:30:00 AM Lab ID: 1911610-002 Matrix: Aqueous Reporting Dilution Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbemcne BRL 1,2,4-Trimethylbenzene BRL sec-Butylbeazene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobemene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibronro-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surf: Dibromotluoromethane 98.2 Sum Toluene-d8 99.2 Sort: 4-Bromotluorobenzene 98.3 Total Phosphorus E365.1 Phosphorus, Total (As P) 0.132 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 220 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 43.3 Nitrogen, Nitrate (As N) 2.80 Hydrogen Ion (pH) by SM4500 II+ B pH 7.15 Fecal Coliform (MP) SM9222D Fecal Coliform, (Mr) BRL METALS, TOTAL SW6010D Cadmium BRL Qunliners: a Ylue exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or modysis exceeded N Anobts not NELAC certified B Analyte denetted in the associated medmd blank > Greater than Result value (SW5030B) 0.50 ug/L 288036 1 11/12/2019 19:10 JE 0,50 ug/L 288036 1 11/12/2019 19:10 JE 0.50 ug/L 288036 1 11/12/2019 19:10 JE 0.50 ug/L 288036 1 11/12/2019 19:10 JE 0.50 ug/L 298036 l ll/12201919:10 JE 0.50 ug/L 288036 1 11/12/2019 19:10 JE 0.50 ug/6 288036 1 11/12/2019 19:10 JE 0.50 ug/L 288036 1 11/12/2019 19:10 JE 0.50 u9/L 288036 t 11/12/2019 19:10 JE 1.0 41, 288036 1 11/12/2019 19:10 JE 0.50 ug/L 288036 1 11/12201919:10 JE LO ug/L 288036 1 11/12/2019 19:10 JE 0.50 gall, 288036 1 11/12/2019 19:10 JE 0.50 g911, 288036 1 11/12m1919:10 JE 2.0 ug/L 288036 1 11/12201919:10 JE 76.4-125 %REC 288036 1 111IM01919:10 JE 78.3-116 %REC 288036 1 IMM01919:10 JE 64-125 %RLC 288036 1 ll/D201919:10 JE (E365.1) 0.050 mg/L 287844 1 11/111201915:52 GO l0 nag/l. 287951 1 IM3/201917:30 AJ (E350.1) 0200. ing/L 287780 1 11/08/201912:46 TL 10.0 mg/L R411268 10 1110001900:13 BC 0.250 mg/L R411268 l 11/07201916:43 BC 00100 H pH Unit. R411568 1 11113/201914:40 CS 20 H Colonies/l0o R411233 10 11/07201913:42 MH ml (SW3010A) 0.0050 mgfL 287829 l 11/13201910:50 ICB E Estimated (value above quanritatice range) S Spike Recovery outside limits due to matrix Nair Screaserhmmtive NC Not conamred c Less time Result value J Estimated value detected below Reporting Limit Page 14 of 52 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: 11/6/201910:30:00 AM Lab ID: 1911610-002 Matrix: Aqueous Reporting Reporting Dilution Analyses Result Qual Units BatchID Date Analyzed Analyst Factor METALS, TOTAL SW6010D (SW3010A) Chromium BRL 0.0100 mWL 287829 1 11/13/201910:50 KB Lead BRL 0.0100 mg/L 287829 t 11113/201910:50 KB Zinc 0.0602 0.0200 mg/L 287829 1 11/13/201910:50 KB Qnaliners: " Yolue exceeds maximum..mainnnt level Bat, Below reporting limit FI Bolding times for prepamtimi oranalysis exceeded N Anelyie not NELAC studied e Amlyte detected in Flue ...ended meWad blank > Grater flan Rasaltvalue E Estimated (value above quantualu n range) S Spike Recovery outside limits due to matrix Neu Seenusenavmive NC Notmnfimted < Less thus Raub valve I Estimated value detected below Reporting Limit Page 15 of 52 a EA Fat Per Fac Gr Cor We enr SUBMIT FORM ONYELLOW PAPER ONLY - • . DEPARMEN74OFEyVIRONMEN}Ts8°NATUR/1L RESOURCES OUNDWATER QUALITY MONITORING; �usloN!oEwATEr3ouu nv mogniATlou PRocEsslrlGtrNxm MPLIANCEREPORT FORM • 617SNIAISERYiCE4(lTER,RALEIaN,NC2Z699.16�7TPh01114.'491917333221,4.z' 06-30-2022 Please Print Clearly or Type PERMIT Number Expiration Date. :ILITY INFORMATION Colonial Pipeline Company Non -Discharge W00005809 : U ility Name: NPDES Other nit Name (if different): '' TYPE OF PERMITTED OPERATION BEINGMONITORED lity Address- 411 Gallimore Dairy Road ❑ ❑ Remediation: Infiltration Gallery :ensboro ?St.t) NC 27409 I'll, County Guilford Lagoon ❑ Spray Field '. ❑ Remediation: lclry) (smote) Telephone#. 336-669-7903 ❑ Rotary Distributor Land Application of Sludge tact Person: Faron D. Leigh Location/Site Name: Downgradient No. of wellsto be sampled: 5 ❑ Water Source Heat Pump ❑ Other: n°m Permit If WELL IPLING INFORMATION NUMBER (from Permit): MW-3 ae samp.c/�li� Date sample FIELD ANALYSES oC y WAS DRY at Depth: - 39.80 fL Well Diameter: 2 in. pH �,'°�i` units Temp. time of .hto Water Level �$. `jt �'ft. below measuring point Screened Interval: 38.5 ft. to 43.5 ft. Spec. Cond. . µ sMho sampling suring. Point is 1.73 ft. above land surface Relative M.P. Elevation:.' ft. Odor check here: r d/b !led before sam ling: � gallons Appearance - w vome of water pumps al @ - p Samples for metals were collected unfiltered: ®YES ❑ NO and field acidfed: ® YES ❑ NO I LABORATORY INFORMATION : //-O� a 1J� y Laboratory Name: Analytical Environmental Services Certification No. 562 Date sample analyzed: d-�i ski PARAMETERS NOTE: Values should reflect dissolvedand colloidal concentrations Lead 4&4. f1d mgA COD mg/I Nitrite (NO2) as N mgA Pb - Coldorm: MF Fecal ' /100ml Nitrate (NO,) as N ..J f - mg/I Zn -Zinc mg/I -Coliform: MF Total /100m1 Phosphorus: Total as P mg/I - - (Note. use MPN method for hiiiNy turbid samples) Orthophosphate mgA other (Specify Compounds and Concentration Units):: Dissolved Solids: Total mg/I AI -Aluminum mg/I pH (when analyzed) units Ba Barium mg/I TOC mgA Ca - Calcium mgA Chloride mg/I Cd Cadmium Fi- ®i/ mg/I Arsenic mg/I Chromium:, Total r.. or mg/I Grease and Oils - mg/I Cu- Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe -.Iron mgll (Specify test and method.#. ATTACH. LAB REPORT.) Sulfate mg/I Hg - Mercury mgll Report Attached? 5a Yes (1) ❑ No (0) Specific Conductance - µMhos K - Potassium mg/I VOC , method # 8260 Total. Ammonia: mg/I Mg - Magnesium _ mg/I - , method #. (A moni. Nitrogen: NHsas N: Artvnonia Nrtmgen: Tots) :Mn - Manganese mgA method #. . TKN as N mgA Ni - Nickel mg/I , method # Few RemediationSvstems Oniv.(Attach Lab Reports): Influent. Total VOCs; mg/L ,Effluent Total. VOCS: mg/L VOC Removal % - I eemryina; is"m, ueswu..n uw 'r,v '.—.............................. DWO-certified laborate, I am aware that there are si nificant enaItIq for subptt,mrg false Information, includins thepossibllit o(fnes antl im risonmentf r!,nwin violations. OperationsBrian L� Smith - •- Pennittee (or Authorized Aaern Name and Title - Please print or Was anarrare of P."ittee, (or Authrmtzed AQ.0t) GW-59 Rev. 00 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW3 Project Name: Greensboro Collection Date: 11/6/2019 1:00:00 PM Lab ID: 1911610-003 Matrix: Aqueous Analyses Result Reporting Limit Quad Dilution Units BatchID PflCfor Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW503013) 1,2-Dichloropropane BRL 0,50 ug/L 288036 1 11/12/2019 19:34 JE 2,2-Dichloropropane BILL 0,50 ug1L 288036 1 11/12/2019 19:34 JE 2-Chlorotoluene BILL. 0.50 ug/L 288036 1 11/12/2019 19:34 JE n-Butylbenzene BILL 0.50 ug/L 288036 ( 11/12/2019 19:34 JE n-Propylbenzene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Dichlorodifluoromethane BRL 0.50 ug/L 288036 1 11/12/201919:34 JE Chloromethane BRL 0.50 .tg/L 288036 1 11/12/2019 19:34 M Vinyl chloride BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Bromometham BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Chloroethane BRL 1.0 ug/L 288036 1 11/12/2019 19:34 JE Trichlorofluoromethane BRL 0,50 uglL 289036 1 11/12/2019 19:34 JE l,l-Dichloroethene BRL 0,50 ug/L 288036 1 11/12/2019 19.34 JE Methylene chloride BRL 5.0 ug/L 288036 1 11/12/2019 19:34 JE trans-1,2-1)ichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE I,l-Dichloroethane BRL 0.50 ug/L 288036 1 ll/I2201919:34 JE cis-1,2-Dichloroethene BRL 0.50 ug/L 289036 1 11/12/2019 19:34 JE Bromoc6loromethaue BRL 0,50 ug/L 288036 1 11/12/2019 19:34 JE Chloroform BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE 1,2-Dichloroethane BRL 0.50 ugIL 288036 1 11/12/2019 19 34 JE l,l,l-Trichloroethane BRL 0.50 ug/L 288036 1 11/12/20191934 JE 1,1-Dichoropropane BRL 0.50 ug/L 288036 I 11/12/2019 19:34 JE Carbon tetrachloride BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Benzene BRL 0.50 ug/L 289036 I 11/12201919:34 JE Dibromomethane BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Trichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Bromodichloromethane BRL 0.50 ug/L 288036 1 11/12201919.34 JE 1, 1,2-Trichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Toluene BRL 0.50 ug/L 288036 1 IIA2/201919:34 JE 1,3-Dichloropropane BRL 0.50 1191L 288036 1 11/12/2019 19:34 JE Dibromochloromethane BILL 0,50 eg/L 288036 1 11/12/2019 19:34 JE 1,2-Dibromoethane BRL 0.50 ug/L 288036 1 11/12201919:34 JE Tetrachloroethane BRI, 0.50 ug/L 288036 1 11/12201919:34 JE 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 288036 1 11112201919.34 JE Chlorobenzene BRL 0.50 ug/L 288036 1 11/12/20191934 JE Ethylbenzene BILL 0.50 ug/L 288036 1 11/12/201919:34 JE Bromoform BRL 1.0 ug/L 288036 1 111121201919:34 JE Styrene BRL 0.50 ug/6 288036 1 11/12/2019 19:34 JE 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 298036 1 11/12/2019 19:34 JE 1,2,3-Trichloropropane BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Isopropylbenzene BRL 0.50 ug/L 288036 1 11/1220191934 JE Bromobenzene BRL 0.50 ug/L 288036 1 11112/201919:34 JE Qualifiers: " Value exceeds maximum containment level E Estimated(valuo above quantimtion mnge) BRL Below reportin6 hunt S Spike Recovery outside limits due to matrix n Holding tinses for prepaation.,analysis exceeded N." See case namtive N Analyte not MLAC certified NC N.,e..finnad B Analyte detected in 11. associated metlmd blank < Less thaa Result vain > oeater than Result value J Eauamted value detected below Reporting Limit Page 16 of 52 Analytical Environmental Services, Inc Date: t9-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-3 Project Name: Greensboro Collection Date: 11/6/2019 1:00:00 PM Lab ID: 1911610-003 Matrix: Aqueous Analyses Result xepornng Qua[ Units BatchlD uuunon Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 4-Chlorotoluene BRL 0.50 ng/L 288036 1 11112/201919:34 JE 1,3,5-Trimethylbemene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE teat-Butylbenzene BRL 0.50 49/1. 288036 1 11/12/2019 19:34 JE 1,2,4-Trimethylbemene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE sec-Butylbenzene BRL 0.50 ug/L 298036 t 11/12/2019 19:34 JE 1,3-Dichlorobenzene BRL 0.50 pelt, 288036 1 11/12/2019 19:34 JE 1,4-Diclorobenzene, BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE 4-Isopropyltoluene BRL 0.50 vg/L 288036 1 11/12/2019 19:34 JE 1,2-Dichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE 1,2-Dibromo-3-chloropropane BRL LO ug/L 289036 1 11/12/2019 19:34 JE 1,2,4-Trichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Naphthalene BRL 1.0 ng/L 288036 1 U/12/201919:34 JE Hexachlorobutadiene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE 1,2,3-Trichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 19:34 JE Xylenes, Total BRL 2.0 ug/L 288036 1 11/12/2019 19:34 JE Surr: Dibromofluoromethane 106 76.4-125 %REC 288036 1 11/12/2019 19:34 JE Surr: Toluene-d8 100 78.3-116 soREC 288036 1 11/122019 19:34 JE Surr: 4-Bromofluorobenzene 101 64-125 iREC 288036 I 11/12/2019 19:34 JE Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 14 10 mgfL 287951 1 11/13/2019 17:30 AJ Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) 0.541 0.250 gfL R411228 1 11/072019 15:28 BC Hydrogen Ion (pH) by SM4500 H+ B pH 7.05 0.0100 H pH Units R411568 1 11/131201914:44 CS METALS, TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 ntg/L 287829 1 11/13/201910:57 KB Chromium 0.0216 0.0100 rng/L 287829 1 11/13/201910:57 KB Lead BRL 0.0100 tag/1, 287829 1 11/131201910:57 KB Zinc 0.0269 0.0200 tng/L 287829 1 11/13/2019 M57 KB Qualifiers: ' Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Audyte not NELAC certified B Anelym detected in the associated meamd blank > Greater than Result valve E Estimated (value above numeration range) S Spike Recovery outside limits due to matrix Naar See as nantive NC Not confimaed < Less than Result value 1 Estimated value detected below Reporting Limit Page 17 of 52 SUBMIT FORM ON YEI I OW PAPER ONLY �, DEP/1RfMEN7t,O,F}ENVIfZ914 S NATURAL RESOURCES t I�SIONFIV17PRrfUt 1INFORMATIONtPROGESSINGrUNR GROUNDWATER QUALITY MONITORING: SRO-OMUNANCE Erar�R, RuEIc Nc 7sss'P3rai Pho a;(yts)Tsy3ut .r -;` REPORT FORMsERutcE Please Print Clearly or Type PERMIT Number: : Expiration ate: 06-30-2022 D FACILITY INFORMATION olonial Pipeline CompanyNon-Discharge Cp WG20005809 UIC FaciliryName: NPDES Other Permit Name (If different): TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address. 411 Ga!limore Dairy Road (s"GeO) NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro (State) (ZIP) ❑ Spray Field ❑ Remediation: lat/1 Telephone#:336-669-7903 ❑ Rotary Distributor ® Land Application of Sludge Contact Person. Faron D. Leigh Well Location/Site Name: Downgradient No. of wells to be sampled: 5 ❑ Water SourceHeat Pump Other. som aemie., If WELL SAMPLING INFORMATION Date collected: �� �6 �/ FIELD ANALYSES: AS. WELL ID NUMBER (from Permit): MW-4 (MW-135) sample units Temp. 3 oC. DRY at Well Depth: 29.5 ft. _2 Well Diameter: in. Screened Interval: 13 ft. to 28 pH ,St time of ft. Spec. Cond. µMhos sampling, ^�,; Depth. to Water Level: ��ft. below measuring point Measuring Point is 2 ft. above land surface Relative M.P. Elevation: fL Odor check here: qqq/� 7`gallons Volume of water pumped/bailed before sampling: �(]l] YT�g11 Appearance Samples; for metals were collected unfiltered: ®YES ❑ NO and field acidified: DYES ❑ NO 1 CBORATORY INFORMATION �� � o Laboratory Name: Analytical Environmental) Services Certification No: 562 Date sample analyzed:. //�6% 7th,q PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. - ,� ��. 01t� mg/I Lead COD '. mg/I Nitrite (NOz)as N mg/I Pb - Coliform. MF-Fecal /100ml Nitrate (NOs),as N OZ 5 1 Zn - Zino Coliform: MF Total /100m1 Phosphorus: Totalas P mg/I (Nate. use MFN method for highly tumid samples) Orthophosphate n10 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total %, mg/I Al -Aluminum mg/I pH.(when analyzed) units Be - Barium. m9/I TOO mg/I Ca - Calcium mgA 'Chloride mg/I Cd - Cadmium <0- d0 S - mg/I _ Arsenic mg/I Chromium: Tpmg/I - Grease and Oils I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/l :(Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? 1 Yes (1) ❑ No (0) Specific Conductance µMhos K- Potassium mg/I VOC ,method # 8260 Total Ammonia mg/I Mg - Magnesium _ mg/I , method # (Ammonia Nlvosehk RHyas N; Ammonia Nitrogen Total) Mn- Manganese mg/I ,.method# TKN as mg/I Ni- Nickel mg/I -,method# /L YOC Removalq For Remediation Systems Only (Attach Lab Reports): Influent: Total VOCs:. ni -Effluent Total VOCS mg Brian L. Smith - Operations. Manager Permittee (or Authorized Agent) Name and Tiffe - Please print or Noe Signature of Pennittee (orAutmsnoded Agent} fDatel GW-59 Rev. 1/2007 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW-4) Project Name: Greensboro Collection Date: 11/6/2019 2:00:00 PM Lab ID: 1911610-008 Matrix: Aqueous . �_.... Reporting .,_:._ .,_1_1.,., Dilution nua.yace .._.,.... �..... �....- .._._.._.. Limit Factor Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE 2,2-Dichloropropane BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE 2-Chlorotoluene BRL 0.50 chit. 288036 1 1IIIMO1921:35 JE n-Butylbenzene BRL 0.50 ug/L 288036 1 111121201921:35 JE n-Propylbenzene BRL 0,50 ug/L 288036 1 11/12/2019 21:35 JE Dichlorodifluoromethane BRL 0.50 ug/L 298036 1 11/121201921:35 JE Chloromethane BRL 0.50 ug/L 288036 1 11/12201921:35 JE Vinyl chloride BRL 0.50 ug/L 288036 1 11/12/20192135 JE Bromomethane BRL 0.50 ug/L 288036 1 11112/201921:35 JE Chloroethane BRL LO ug/L 288036 1 11/121201921:35 JE Trichlorofluermnethane BRL 0.50 ug/L 289036 1 tl/12201921:35 JE 1,1-Dichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE Methylene chloride BRL 5.0 ug/L 288036 1 11112/201921:35 JE trans-1,2-Dichloroethene BRL 0.50 quit, 288036 1 11/12/2019 21:35 JE l,l-Dichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE cis-1,2-Dichloroethene BRL 0,50 ug/L 288036 1 11/12201921:35 JE Bromochlorometharne BRL 0.50 ug/L 288036 1 11112/20192135 JE Chloroform BRL 0.50 ng/L 288036 1 11/12/2019 21:35 JE 1,2-Dichloroethane BRL 0.50 ug/L 298036 1 11/12/2019 21:35 JE l,l,l-Trichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE 1,1-Dichloropropene BRL 0,50 ug/L 288036 1 11/12/2019 21:35 JE Carbon tetrachloride BRL 0.50 ug/L 288036 1 11112/201921:35 JE Benzene BRL 0.50 ug/L 288036 1 11/121201921:35 JE Dibromomethane BRL 0.50 ugfL 288036 1 11/12201921:35 JE Trichloroethene BRL 0.50 uWL 288036 t 11/12/20192135 JE Bromodichloromethane BRL 0.50 ng/L 288036 1 11112/201921.35 JE 1, 1,2-Trichloroethane BRL 0.50 ug/L 288036 1 11/122019 21:35 JE Toluene BRL 0.50 ug/L 288036 1 11/121201921:35 JE 1,3-Dichloropropane BRL 0.50 ug/L 288036 1 11/122019 21:35 JE Dibromochloromethme BRL O50 ug/L 288036 1 11/12/20192135 JE 1,2-Dibromoethane BRL 0.50 ng/L 288036 1 11/12/2019 21:35 JE Tetrachloroethene BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE 1, 1, 1,2-Tetrachloroethane BRL 0.50 qg/l. 288036 l 11/12201921:35 JE Chlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 21:35 JE Ethylbenzene BRL 0.50 ug/L 288036 l 11/121201921:35 JE Bromoform BRL 1.0 ug/L 288036 1 11/12/2019 21:35 JE Styrene BRL 0.50 ug/L 288036 t 11/12/2019 21:35 JE 1, 1,2,2-Tetrachloroethane BRL 0.50 uWL 288036 1 11/12/201921:35 JE 1,2,3-Trichloropropane BRL 0.50 atilt, 288036 1 11/12/2019 21 :35 JE Isopropylbenzene BRL 050 qg/L 288036 1 11/12201921:35 JE Bromobenzene BRL 0.50 ug/L 289036 1 11/122019 21:35 JE Quali0ers: * Value exceeds maximum contaminant level E Enimared(vulueabave quactitalm. mnpa) BRL Below reporting limit S Spike Recovery outside limits due to matrix a Holding times fra,urpamtion or analysis exceeded Nair See case aarmtive N Andyte not NELAC certified NC Notcanfimred e Analyte detected in the associated method blank < Lesstlam Rosrdtvalue > Greater than Result value 1 Estimated value detected below Reporting Limit Page 26 of 62 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW-4) Project Name: Greensboro Collection Date: 11/6/2019 2:00:00 PM Lab ID: 1911610-008 Matrix: Aqueous Reporting Dilution Analyses Result Qual Units BatcbID r` Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibmmo-3-chioropropanc BRL 1,2,4-Trichlombenzenc BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surr: Dibromotluoromethane 109 Surr: Toluene-d8 101 Surr: 4-Bromofluorobenzene 102 Residue, Dissolver) (TDS) by SM2540C Residue, Dissolved (TDS) 76 Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) BRL Hydrogen Imt (pH) by SM4500 H+ B pH 6,42 METALS,TOTAL SW6010D Cadmium BRL Chromium 0.0187 Lead BRL Zinc 0.0654 Qualifiers. . Value exceeds maximum contaminant level BRL Move reporting limit H holding times for preparation or analysis exceeded N Anulyte not NELAC certified B Analyte detected is the associmed method blank > (Later than Result value (SW5030B) 0.50 u9/1, 288036 1 11/12/201921:35 JE 0.50 ug/L 288036 1 11/12201921:35 JE 0.50 use 288036 1 11/12/201921:35 JE 0.50 ug/L 288036 1 11/12/2019 21:35 JE 050 ug/L 288036 1 11/121201921:35 JE MO ug/L 288036 1 11/12/20192135 JE 0.50 ug/L 288036 1 11/12/201921:35 JE 0.50 u9/L 288036 1 11/12201921:35 JE 0.50 ug/L 288036 1 11/12/201921:35 JE 1.0 ug/L 288036 1 11/12201921:35 JE 0.50 ug/L 289036 1 11/12/201921:35 JE LO ug/L 288036 1 11/12/2019 2135 JE 0.50 ug/L 288036 1 11/12/201921:35 JE 0.50 ug(L 288036 1 11112/201921:35 JE 2.0 ug/L 288036 1 11/12/2019 21:35 JE 76.4-125 %REC 288036 1 11/12/201921:35 JE 78.3-116 %REC 288036 1 11/12/201921:35 JE 64-125 %REC 288036 1 11/12/20192135 JE 10 mg/L 287951 1 11/13/2019 17:30 AJ 0.250 mg/L R411228 1 11/07201915,44 BC 0.0100 H pH Units R4H568 1 11/13201914:53 CS (S W 3010A) 0.0050 mg/L 287829 1 11/13/201910,59 KB 0.0too me, 287829 1 11/131201910:59 KB 0.0100 mg/L 287829 1 11/13201910:59 KB 0.0200 mg/L 287829 1 11/13201910:59 KB E Estimated (value above nuantivelion range) S Spike Recovery outside limits due to matrix Narr See case narrative NC Not confirmed < Less thus Result valve 1 Estimated value detected below Reporting Limit Page 27 of 52 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENTOFEP{yIR�ONMENII&NATURAL RESOURCES�11" GROUNDWATER QUALITY MONITORING: revlslON-Ofwa�Err4unukmlNF�oRlrya ON PROCESSING UNIT' p f RALEIGHrN�7699%16U7 }Phooe,i1919jaT33J221"r , COMPLIANCE REPORT FORM 61jrMAlESERNICE��NTER PERMITNumber Expiration` Date: 06-30-2022 Please Print Clearly a Type FACILITY INFORMATION Colonial Pipeline Company Non -Discharge W00005809 U IC Facility Name: NPDES Other Permit Name (if different): _ TYPE OF PERMITTED OPERATION BEING': MONITORED Facility Address: 411 Gallimore Dairy Road cs`ree`) NC 27409 County Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery GreenSbOro ❑ Spray Field ❑ Remediation: (sr«) PP) (c,ml Telephone#: 336-669-7903 ❑ Rotary Distributor `® Land Application of Sludge Contact Person: Faron D. Leigh Well Location/Site Name: Downgradient No. of wells to be sampled: 5 ❑ Water Source Heat Pump ❑ Other: from Perrot) - If WELL ' SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-6(MW-183) Date sample collected: 6: FIELD ANALYSES: oC 5�units Temp �_ AS DRY. at. Well Depth: 27.00 ft. Well. Diameter: _2 In. PH µMhos time of Depth to Water Level. ji�Y&4 ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. sampling, Measuring Point is 1.5 ft. above land: surface Relative M.P. Elevation: fL Odor check here: Volume of water pumped/bailed before sampling: ,gallons Appearance El Samples for metals: were collected unfiltered: ®YES ❑ NO and field acidified: ®YES ❑ NO. Date sample analyzed: / -117 ^4ry 11:ZKLaboratory Name: Analytical Environmental Services Certification No.:562 PARAMETERS NOTE: Values should reflect dissolved: and colloidal concentrations. Nitrite N Pb- Lead 40 Qf�_mgll COD mg/I (NO2) as mgA Coliform: MF Fecal A 00MIL Nitrate (NO3) as N 55 mgA Zn - Zinc <4424 /f mg/I Coliform: MF'Total /100m1 Phosphorus: Total as P ` Mg/I ,(Note. Use MPN method for highly wrbld Samplas) Orthophosphate mg/I Other (Specify Compounds: and Concentration Units): .Dissolved Solids: Total A®S mgA AI Aluminum mgA PH (when analyzed) units.. Bat -Barium - mgA TOC mg/I Ca -.Calcium: mg/I Chloride mg/I Cd Cadmium <a?`. 070 ] mg/I .Arsenic mg/I Chromium: Total ­4,1. 6FId mg/I -. Grease and Oils mg/I Cu Copper mgA ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe -Iron ' mgA (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg- Mercurymg/I ReportAttached? ® Yes(1). ,❑ No.(0). Specific Conductance µMhos K- Potassium mg/I - VOC , method # 8260 Total Ammonia mg/I Mg - Magnesium mg/I method #- (Ammonia Ntrogsm Woe N;Ammonla Nitrogen, Total) `Mn- Manganese mgA :method#. TKN as mgA Ni Nickel mgA , method# For Remediation Systems Only (Attach Lab. Reports): to the best my onmiedge and belief, the inferination submitted Influent Total VOCs: '. mg/L Effluent Total .VOCs: mg/L -VOC Removal% _ in this report is true, accurate, and complete, and that the laboratory analytical data vvas produced using approved methods ofanalysis by a I certify that, of 'jifir'�Tt Wjalt 2,, for subrnibt�nq false pformgfion, inclucjng the possibility of lines and imprisonment for knomno violations. Brian L. Smith - Operations Manager, (Date) Permittee (or Authorized Anent) Name and Title Please print or type 514ngiupe of Penniman (or Authonzed Agent) ' GW-59 Rev..112007 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-183 (MW-6) Project Name: Greensboro Collection Date: 11/6/2019 1:30:00 PM Lab ID: 1911610-009 Matrix: Aqueous Reporting DJlunon Analyses Result Limit Qual Units BatchID Factor DateAnalyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 299036 1 11112/201921:59 JE 2,2-Dichloropropane BRL 0.50 Batt. 288036 I 11/12201921:59 JE 2-Chlorotoluene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE n-Butylbenzene BRL 0.50 ug/L 288036 1 11/12201921:59 JE n-Propylbenzene BRL 0.50 ug/L 288036 1 11112/201921:59 JE Dichlorodifluoromethmic BRL 0,50 ug/L 288036 1 11/12/2019 21:59 JE Chloromethane BRL 0.50 ugtL 288036 1 11/12/2019 21:59 JE Vinyl chloride BRL 0.50 ug/L 288036 1 11/12201921:59 JE Bromomethane BRL 0.50 ta/L 288036 1 11/122019 21:59 JE Chloroethane BRL 1.0 ug/L 288036 1 11/122019 21:59 JE Trichlorofluoromethane BRL 0.50 tg/L 288036 1 II/12201921:59 JE 1,1-Dichloroethene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE Methylene chloride BRL 5.0 Bait 288036 1 11/12/2019 21:59 JE trans-1,2-Dichloroethene BRL 0.50 ug/L 298036 1 11/12201921:59 JE l,l-Dichloroethane BRL 0.50 tart. 288036 1 11/12/2019 21:59 JE cis-1,2-Dichloroethene BRL 0.50 up/L 288036 1 11/12/2019 21:59 JE Bromochloromethane BRL 0.50 talk, 288036 1 11/12/2019 21:59 JE Chloroform BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1,2-Diehloroethane BRL 0.50 Batt, 288036 1 11/12/2019 21:59 JE l,l,l-Trichloroethane BRL 0.50 ug/L 298036 1 11/121201921:59 JE l,l-Dichloropropene BRL 0.50 ua/L 288036 1 11/12/2019 21:59 JE Carbon tetrachloride BRL 0.50 ug/L 288036 1 11/122019 2L59 JE Benzene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE Dibromomethane BRL 0.50 ug/L 288036 1 11/12/201921:59 JE Trichloroethene BRL 0.50 BE& 288036 1 11/121201921:59 JE Bromodichloromethane BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1, 1,2-Trichloroethane BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE Toluene BRL 0.50 Bg/L 288036 1 11/12201921:59 JE 1,3-Dichloropropane BRL 0.50 ug/L 288036 I 11/12/2019 21:59 JE Dibromochloromethane BRL 0.50 tg/1. 288036 1 11/12/2019 21:59 JE 1,2-Dibromoethane BRL 0.50 ug/L 288036 1 11/12201921:59 JE Tetrachloroethene BRL 0.50 ug/L 288036 1 11/1220192L59 JE 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 289036 t 11/12201921:59 JE Chlorobenzene BRL 0.50 ug/L 288036 1 1U12201921:59 JE Ethylbenzene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE Bromaform BRL 1.0 ua/L 288036 1 11/12/2019 21:59 JE Styrene BRL 0.50 ug/L 298036 1 11/1220192L59 JE 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 288036 1 11/12201921:59 JE 1,2,3-Trichloropropane BRL 0.50 ug/L 288036 1 11/12201921:59 JE Isopropylbenzene BRL 0.50 matt, 289036 1 11/12201921:59 JE Bromobenzene BRL 0.50 ug/l, 288036 1 11/12/2019 21:59 JE Qualifiers. ' Value exceeds maximum contaminant level E Estimated (value above mactitation range) BRL Below mporting limit S spike Recovery onnide limits In, to matrix n kfolding times for preparation or analysis excaeded Barr Seauna..nsoya N Atulyte not NE -LAC certified NC Not confuvsed B Analyte detected in the associated method blank < Less it,. Result value > Greeter than Result .I. r Estimated value detected below Reporting Limit Page 28 of 52 Analytical Environmental Services, Inc Date: 19-Nov-19 Client: Colonial Pipeline Client Sample ID: MW-183(MW-6) Project Name: Greensboro Collection Date: 11/6/2019 1:30:00 PM Lab ID: 1911610.009 Matrix: Aqueous --- Reporting .._,._ .. Dilution Limit -_--------- Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 4-Chlorotoluene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1,3,5-Trimethylbenzene BRL O50 uea. 288036 I 11/12/2019 21:59 JE tert-Butylbenzene BRL 050 ttg/L 289036 1 11/122019 21:59 JE 1,2,4-Trimethylbenzene BRL 0.50 us/L 288036 1 11/12/2019 21:59 JE sec-Butylbenzene BRL 0.50 nail, 289036 1 Il/12201921,59 JE 1,3-Dichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1,4-Dichlorobenzene BRL 0.50 ug/L 288036 1 11112/201921:59 JE 4-Isopropyholuene BRL 0.50 calk, 288036 1 11112201921:59 JE 1,2-Dichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1,2-Dibromo-3-chloropropme, BRL 1.0 ug/L 288036 1 11/12201921:59 JE 1,2,4-Trichlorobenzene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE Naphthalene BRL 1.0 ug/L 288036 1 11/12/201921,59 JE Flexachlorobutudiene BRL 0.50 ug/L 288036 1 11/12/2019 21:59 JE 1,2,3-Trichlorobenzene BRL 0,50 ug/L 288036 1 11/12/2019 21:59 JE Xylenes, Total BRL 2.0 ug/L 288036 1 11/1220192159 JE Surr: Dibromoflumomethane 111 76,4-125 %REC 288036 1 11/122019 21:59 JE Surr: Toluene-d8 102 78.3-116 %REC 288036 1 11/12201921:59 JE Surr: 4-Bromotluorobenzene 102 64-125 %REC 288036 1 11/12MI921:59 JE Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 101 10 mg/L 287951 1 11/132019 17:30 At Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) 0.330 0.250 mg/L R411228 1 11/07/2019 16:40 BC Hydrogen Ion (pH) by SM4500 H+ B pit 5.86 0.0100 It pH Units R411568 1 11/13/2019 14:55 CS METALS, TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 mg/L 287829 1 11/1320191101 KB Chromium BRL 0.0100 mg/L 287829 1 11/13201911,01 KB Lead BRL 0.0100 mg/L 287829 1 I1/1320191101 KB Zino BRL 0.0200 mg/L 287829 1 11113/20191101 KB Qualifiers: . value exceeds maximum curator nant level BRL Belowreportinglimit H Holding times for preparation or analysis exceeded N Acolyte not NELAC certified a Anelyto detected in die associated method blank > Greeter than Result value E Estimated (value above quarmitition range) S Spike Recovery outside limits due to matrix Nart See case nemetive NC Not compared < Less than Result value r Estimated value detected below actuating Limit Page 29 of 52 GW-59F1 COMPLIANCE REPORT FORM Pernut (Sabrrrit one euch rrruniforing peruul )%,ith Gbe -59 forrrr.s.) A Enter date monitoring results were due. ~ - ) Will this monitoring report (GW-59 and GW-59A) YES No be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for g:idance. 4 Are any monitored constituents equal to or above the established standards? 1'NO if the answer to question 4 is 'NO', skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: /llI)/ /C-Ye/s WC,FF A!'/®w 6. S 5*•tr- 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO', skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, reported, and sample collection date for each occurrence (for the last two years). jconcentration(s) 1411�19° /P•'P�S =VCrr 9Prt3dJ �r� 1'. (�- �'' ��irC� p�ai/r• ,411 All, Ir�r /s w�rP hrlac� fv ,�V�vr,�: dam^ -¢ `} y- Af/w-j /3%! �� %r9 -w� [6 � Are the monitoring wells listed in section 5 ocated at or beyond the review boundary? YES NO v If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELYFOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly �7— located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division Involving this YES NO groundwater quality problem? If the answer to question 7 is "YES'; describe those actions in the space provided below. If the answer to question 7 is "NO', contact the Regional Office within 90 daysLanjvuatfonluav recut ed to determine the im act thp Uste disposal gystpm is having at the review and comoliango bszundaries surrounding fhL,� facility. Failure to do so may ar l _r� -t the Aermittee to a Notice of fines. and/or aenaltles. g this The person completing this portion (GW-59A) of the monitoring report should sign below an:1n form with GW-59 forms for required wells to the address provided at the top of the current Gm. I hereby acknowledge that the above information was evaluated and the information submitts report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Signature of Pormittee (or Authorized Agent) Date G%,� -54 \ 12l812043 SUBMIT FORMONY IOW PAPER ONLY OEP)ligrlyl INGU RArf w S Sla. GROUNDWATER QUALITY MONITORING: ..• ONMkON�WAlTEEN'RUALI 1 �r�4!�, F4V"„AguNareP`cROCES L('xri + # F �. A €alccr�T,EpyE14B/Ncsse.+7aQhona,(?ne) COMPLIANCE REPORT FORM PERMIT Number:. Expiration: Date: 06-302022 Please Print Clearly or Type FACILITY INFORMATION Colonial Pipeline Company Non -Discharge WQ0005809 UIC Facility Name: NPDES Other Permit Name (if different): TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address: 411 Gallimore Dai Road + "' eep 'NC 27409 ❑ Lagoon ❑ Remediation: Infiltration Gallery County: Guilford Greensboro '. ❑Spray Field ❑Remediation: - Isu re) (_n) icu„ Telephone#: 336-669-7903 ❑ Rotary Distributor ® Land Application of Sludge Faron D. Leigh Contact Person: 9 Well Location/Site Name:-DOWngradient No. of wells be sampled: 5 El Water Source Heat Pump El Other rrom Peq.m If WELL SAMPLING INFORMATION - WELL ID NUMBER (from Permit): MW-1 (MW-1 B) Date sample collected: G7% //^/9 FIELD ANALYSES: �� Q g/. J,�units Temp. �` WAS DRY at Well Depth: - 21.20 ft. Well Diameter: _2 in. pH µMhos time of: ' Depth to: Water Level:. 7 50 ft. below measuring point ` Screened IntervaC _ 5 ft. to 20 ft. Spec. Cond. �' sampling, Measuring Point is - 3 ft. above land: surface Relative M.P. Elevation: ft. Odor check here: Volume of water pumped/baled before sampling: ? /7.. gallons ' , Appearance Samplesffor metals were collected .unfiltered: ,.®YES I El NO and field acidified: ®YES ONO I ABORATORY INFORMATION Date sample analyzed: OT/a 6AC - �,%��7 Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolvedand colloidal concentrations. N - Pb - Lead 4a9.'. Q, mg/I COD. - mg/I Nitrite (NOS) as mg/I /100ml Nitrate(NOS)as A -.mg/I Zn - Zinc Coliform: MFFecal Coliform: MFTotal /100ml Phosphorus: Total as P mg/I (Nate. Use MPN method for highly Nrbid samples) ' Ortho hos hate : mg/I p p (Specify Concentration Units): OtherCompounds and Dissolved Solids:70 l T9 mg/I - AI -Aluminum mg/I _' la pH (when analyzed) units Be - Barium . mg/I iTOC mg/I Ca - Calcium - mg/I Chloride /7-7—mg/I Cd - Cadmium -ea, Oe-5 mg/I Arsenic mg/I 'Chromium: Total 6 Img/I Grease and Oils mg/I Cu -Copper mg1l ORGANICS: (by GC, GC/MS, HPLC). Phenol `'. mg/I Fe - Iron mg/I (Specify test: and method #. ATTACH :LAB REPORT.) Sulfate. mg/I Hg - Mercury mg/I ,Report Attached? ® Yes (1) ❑ No (0).'. Specific Conductance µMhos K Potassium mg/I VOC , method # 8260 1 rP Total Ammonia ?G . oc V mg/I Mg - Magnesium 'mg/I , method # (Ammonia Nitrogen; )NH, as N Ammonia Nitrogen Teal) IMn Manganese mg/I :, method # TKN as N mg/I Ni - Nickel mgA ,..method # - For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L ".Effluent Total VOCS: mg/L VOC Removal% th knowledge end belief. the information submitted in this report is true, accurate, and completei and that the laboratory analytical data was produced using approved me ads ofana]ySiS by a I cerl that, to the best of my luilgicant iie;ijl�iesfprsubr�!lfinqfal.. information, including the possibility of fines and ent for knowing violat, ns.. I ) _ Brian L'i Smtih - ' Operations Manager Signature of Permittee (or Authorized Aqent) (Date) Pepmttee for Authorized Aoent) Name and. Title 7 Please onnt or type GW-59 Rev. 1/2007 Analytical Environmental Services, Inc Date: 24-Ju1-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 7/11/2019 2:00:00 PM Lab ID: 1907B38-001 Matrix: Aqueous Reporting T Dilution Date Analyzed Analyst Factor ,.,.. Limit �,.,.. .,...., Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 a91L 282074 1 07/16/2019 12:39 JB 2,2-Dichloropropane BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB 2-Chlorotoluene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB n-Butylbenzene BRL 0.50 ug/L 282074 1 07/16201912:39 JB n-Propylbenzene BRL 0.50 ug/L 282074 1 07/161201912:39 JB Dichlorodifluoromethane BRL 0.50 uglL 282074 I 07/16/2019 12:39 JB Chloromethane BRL 0.50 ug/L 282074 1 07116/201912:39 JB Vinyl chloride BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB Bromomethane BRL 0.50 ug/L 282074 1 07116201912:39 JB Chloroethane BRL 0.50 ug/L 282074 1 07/161201912:39 JB Trichlorofluoromethane BRL 0.50 ug/L 282074 I 07116201912:39 JB 1,1-Dichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 B Methylene chloride BRL 5.0 ug/L 282074 1 07/162019 12:39 JB trans-1,2-Dichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB 1,1-Dichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB cis-1,2-Dichloroethene BRL 0.50 ug/L 282074 I 07116201912:39 JB Bromochloromethane BRL 0,50 ug/L 282074 1 07/16/2019 12:39 JB Chloroform BRL 0.50 ug/l. 282074 1 07/16201912:39 JB 1,2-Dichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB 1, 1, I-Trichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB 1,1-Dichloropropee BRL 0.50 ug/L 282074 1 07116/201912:39 JB Carbon tetrachloride BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB Benzene BRL 0.50 ug/L 282074 1 07/16201912:39 .IB Dibromomethane BRL 0.50 ug/L 282074 1 07116/201912:39 JB Trichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB Bromodichloromethane BRL 0.50 ug/L 282074 1 07116/201912:39 JB 1, 1,2-Trichloroethane BRL 0.50 ug1L 282074 1 07/16/2019 12:39 JB Toluene BRL 0.50 ug/l 282074 1 07/161201912:39 JB 1,3-Dichloropropane BRL 0.50 ug1L 282074 1 07/16/201912:39 JB Dibromochloromethane BRL 0.56 aglL 282074 1 07/161201912:39 JB 1,2-Dibromoethane BRL 0.50 ug/L 282074 - 1 07116/201912:39 JB Tetrachloroethene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB 1,1,1,2-Tenaebloroethane BRL 0.50 uglL 282074 1 07/16201912:39 JB Chlorobenzene BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB Ethylbenzene BRL 0.50 ug/L 282074 I 07/16201912:39 JB Bromoform BRL U0 ug/L 282074 1 07/161201912:39 JB Styrene BRL 0.50 ug/L 282074 1 07/16/201912:39 JB 1, 1,2,2-Tetrachloroethane BRL 0.50 eg/L 282074 1 07/16/2019 12:39 JB 1,2,3-Trichloroptopane BRL 0.50 ug/L 282074 1 07/16/2019 12:39 JB Isopropylbenzene BRL 0.50 ug/L 282074 1 07/161201912:39 JB Bromobertzene BRL 0.50 ug/L 282074 1 07116/201912:39 JB Qualifiers: a Value exceeds maximum contaminant level E Estimated (value above ventilation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Eolding loses fix prepazntion or analysis exceeded No. See once nmrative N Analyte net NELAC caddied NC Notconfi.d B Acolyte detected in the associated method blank < Less than Result vale > Greater than Result value I Estimated value detected below Reporting Limit Page 10of50 0 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 7/11/2019 2:00:00 PM Lab ID: 1907B38-001 Matrix: Aqueous Reporting _ _ . _ . Dilution _ nuusyscs ..00urr Volatile Organic Compounds by GUMS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobemene BRL Xylenes, Total BRL Son: Dibromofluoromethane 98.6 Surf: Toluene-d8 101 Surr:4-Bromofluorobenzene 98 Total Phosphorus E365.1 Phosphorus, Total (As P) 0.337 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved ('IDS) 289 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride - - - -I1.9 Nitrogen, Nitrate (As N) 2.66 Hydrogen Ion (pH) by SM4500 H+B pH 5.94 Fecal Coliform (AN) SM9222D Fecal Coliform, (MP) BRL METALS,TOTAL SW6010D Cadmium BRL Qualifiers. r Value exceeds maximum contaminant level BRL aelowreperting limit H Holding times for preparation or analysis exceeded N Acolyte not bMLAC certified B Analyte detected in the associated method blank > Greater than Result value Factor (SW5030B) 0.50 u9/L 282074 1 07/16/2019 12:39 JB 0.50 119/L 282074 1 07/161201912:39 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB 0.50 119/L 282074 1 07/16/2019 12:39 JB 0.50 119/L 282074 1 07/16/2019 12:39 JB 0.50 ug/L 282074 1 07116/201912:39 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB o50 ug/L 282074 1 07/16M1912:39 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB 0.50 ug/L 282074 1 07/16MI91239 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB 0.50 ug/L 282074 1 07116/201912:39 JB 0.50 ug/L 282074 1 07/16/2019 12:39 JB 2.0 119/1, 282074 1 07116201912:39 JB 76.4-125 %REC 282074 1 07116/201912:39 JB 78.3-116 %REC 282074 1 07/16/2019 12:39 JB 64-125 %REC 282074 1 07116120191239 JB (E365.1) 0,050 mg/L 281964 l 07115201915:32 GO 10 m9/L 281956 1 07/16/201910:00 DIN (E350.1) 0.200 mg/L 282026 1 07/15201914:34 TL 1.1.00 -mg/L R402550 l 07/122019.14:01 BC 0.250 1119/L R402550 1 07/12/201914:01 BC 0.0100 H PH units R402944 1 07/17201915:51 CG 4 H Colonies/100 R402782 2 07115201914:00 'TG ad (SW3010A) 0.0050 mg/L 28t987 I 07/16201914:57 DG E Estimated (value above cluentitation range) S Spike Recovery outside limits due to matrix N., See case nanetive NC NotconOrmed < Less than Result value I Estimated value donated below Reporting Limit Page 11 of 50 0 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Collection Date: 7/11/20192:00:00PM Lab ID: 1907B38-001 Matrix: Aqueous __,_. _ -__- Reporting _ . , T Dilution _ Limit - Factor ---" - "'"""'" METALS, TOTAL SW6010D (SW3010A) Chromium 0.0160 0.0I00 mt/L 281987 I 071161201914:57 DG Lead BRL 0.0100 mg/L 281987 1 07/161201914:57 DG Zinc 0.175 0.0200 mg/L 281987 1 07116/201914:57 DG Qualifiers: a Yalu. exceeds maximum contaminant level BM eelovereportinghnit • Holding times for preparation or analysis exceeded N Analyte not NELAC certified 6 Analyze detected in the associated method blank > Greater then Result value E Estimated (value above quantiention cause) S Spike Recovery outside limits due to matrix Narr See case narrative NC Not confirmed < Less than Result value I Estimated value detected below Reporting Limit Page 12 of 50 ' SUBMIT FORM ON YFt. I nW PAPER ONLY l� �„ OEPARLMENTaOFENVIRONMEN.,T NATORAL,'RESOyRCE5 4 IrPNKtlRM^IQNIPRo(cEsslNcuNlr GROUNDWATER QUALITY MONITORING: xJ�ulsloNomv�aTel?tc!i^I sa(z�MN�as rsutcEgErdr RftA� qH Ncx7es�aiet� ,Phone,(e�slTa3a2s+:. ; COMPLIANCEREPORT' FORM PERMIT Number:. Expiration. Date: 06-30-2022 Please Print Clearly or Type FACILITY INFORMATION Colonial Pipeline Company Non -Discharge WQ0005809 UIC Facility Name: NPDES Other P ermit Name (if different): TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address: 411 Gallimore Dairy Road -. (st,eeo ^NC 27409 ❑Lagoon ❑Remediation: Infiltration Gallery County ,Guilford Greensboro ❑ Spray Field ❑ Remediation: (;late) (Zip) Icay) Telephone#: 336-669-7903 ElRotary Distributor ® Land Application of Sludge contact Person: Faron D. Leigh Well Location/Site Name: DOwngradient `' No, of wells to be sampled: 5 ❑Water Source Heat Pump' ❑ Other. rrom Pe,mu f WELL SAMPLING INFORMATION r MW-2 Date sample collected: r�i /i/2 FIELD ANALYSES: WAS WELL ID NUMBER (from Permit): _ 2 in. /v:. j oC pH (?1Qumts Temp.i/� DRY at Well Depth: 2520 ft. Depth to Water Level: �, 3/%.ft. below measuring point Well. Diameter: _. Screened Interval: _18 ft. to 23 ft. Spec. Cord. µMhos time of, sampling, Measuring Point is 1.75 ft. above land surface Relative M.P. Elevation: ft. Odor -Appearance check here:❑ Volume of water pumped/bailed before sampling: 954 g aligns Sam lessfor.metalswere collected unfiltered:'.®YES - ❑ NO and field acidified: ®YES ❑NO - I ABORATORY INFORMATION Date. sample analyzed: ®%%oZ f%(Tq ri%�% Laboratory Name: Analytical Environmental Services Certification No, 562 PARAMETERS NOTE: Valuesshould reflect dissolved and colloidal concentrations. N Pb - Lead 'fie%s i� )mgll COD mg/I Nitrite (NO2)as mg/I 'Coliform: MF Fecal /100ml :Nitrate (NO3) as N 1,16 mg/I Zn - Zinc ®, /// mgA Coliform: MF Total /100ml Phosphorus: Total, as P mg/I (Nate: use MPN method for highly tumid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 17� / 3 mg/I AI -Aluminum TV pH (when analyzed) units Ba - Barium mg/I -TOC mg/I Ca - Calcium - mg/I Chloride 34, mg/I Cd Cadmium 'C 0.&YJ5 mg/I :Arsenic - mg/I 'Chromium: Total CL/05 mgA Grease and Oils mg/I Cu - Copper mg/I ORGANICS:: (by GC, GC/MS, HPLC) '. Phenol mg/I Fe --Iron " mgll -(Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mgll Report Attached? ® Yes (1)` ` ❑ No (0)' Specific Conductance µMhos K Potassium mgll VOC ,.method # 8260 Total Ammonia < mg/I :Mg - Magnesium mg/I ; method # (Ammonia N tm9eryNH,s N;Arn.niz Nitrogen Total) Mn - Manganese mg/I ;method # ,.. TKN;asN mg/I Ni- Nickel mgA ,'.method#.' For Remediation Systems Only. (Attach Lab Reports): Influent Total VOCs: `, mg/L •Effluent Total VOCS: mg/L VOC Removal% best knowledge and berref, the information submitted in this reportis truei accurate, and complete, and that the laboratory anail data was produced using approved methods of analysis by a I certify that. to the of my L bmitting false information, including the ossibilit% of fines and imprisonment for knowing violations. 2;j) t Brian L. Smith - Operations Manager' [Date) Pevnildee (or Authorized Agent) Name and Title - Please P.nt or Npe Signature of Papal (or Autho,i.d Agent) GW-59 Rev. 1/2007 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: 7/11/2019 2:20:00 PM Lab ID: 1907B38-002 Matrix: Aqueous Reportine Dilution Analyses Resmt - Limit - t2wil units BatchLU RACfOY Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 uglL 282074 1 07/161201913:04 JB 2,2-Dichloropropane BRL 0.50 ug/L 282074 1 07/16/2019 I3:04 JB 2-Chlorotoluene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB n-Butylbenzene BRL 0.50 ug/L 282074 1 07116/201913:04 JB n-Propylbenzene BRL 0.50 ug/L 282074 1 071161201913:04 JB Dichlorodifluoromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Chloromethane BRL 0.50 u9/6 282074 1 07116/201913:04 JB Vinyl chloride BRL 0.50 ug/L 282074 l 07/16/2019 13:04 JB Bromomethane BRL 0.50 itg/L 282074 1 07/16/2019 13:04 JB Chloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Trichlorofluoromethane BRL 0.50 ug/L 282074 1 07/161201913:04 JB 1,1-Dichloroethene BRL 0.50 ugJL 282074 1 07/16201913:04 JB Methylene chloride BRL 5.0 ug/L 282074 1 07/162019 13:04 JB trans-1,2-Dichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1,1-Dichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB cis-1,2-Dichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 .1B Bromochloromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Chloroform BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1,2-Dichloroethane BRL 0.50 ug/L 282074 1 07116201913:04 .03 1,1,1-Tricliloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB I,1-Dichloropropene BRL 0.50 ug/L 282074 1 07/16201913:04 JB Carbon tetrachloride BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Benzene BRL 0.50 ag/L 282074 1 07/16/2019 13:04 JB Dibromomethane BRL 0.50 ug/L 282074 1 07116/201913:04 JB Trichloroethene BRL 0.50 ug/L 282074 1 07116201913:04 JB Bromodichloromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1, 1,2-Trichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Toluene BRL 0.50 ug/L 282074 t 07/16/2019 13:04 JB 1,3-Dichloropropane BRL 0.50 ug/L 292074 1 07/16/2019 13:04 JB Dibrom0chi oromethane BRL 0.50 ug/L 282074 1 07/16/2019I3:04 JB 1,2-Dibromoethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Tetrachloroethene BRL 0.50 ug/L 282074 1 07116201913:04 JB 1,1,1,2-Tetrachloroethane BRL 0.50 ng/1. 282074 1 07/16/2019 13:04 JB Chlorobenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Ethylbenzene BRL 0.50 ug/L 282074 1 07/161201913:04 JB Bromoform BRL 0.50 ug/L 282074 I 07116/201913:04 JB Styrene BRL 0.50 uglL 282074 1 07/16/2019 13:04 JB 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1,2,3-Trichloropropane BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Isopropylbenzene BRL 0.50 ug/L 282074 1 07116/201913:04 JB Bromobenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Qualifiers: z Value exceeds maximum contaminant level E Estimated (value above Wmatitation range) BRL Belesvrep,dinglimit S Spike Recovery outside limits due to matrix H Holding times Par preparation or analysis exceeded Nmr See case nertative N Analyte not NELAC certified NC Noteonfinned B Analyte detected in the sesceiated method blank < Less then Result value > Greater tlson Result value I Estimated value detected below Reporting Limit Page 13 of 50 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Collection Date: 7/11/2019 2:20:00 PM Lab ID: 1907B38-002 Matrix: Aqueous Analyses Result nepurung Dnutlon Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 4-Chlorotoluene BRL 0.50 ug(L 282074 1 07/16/2019 13:04 JB 1,3,5-Trimethylbenzene BRL 0.50 ug/L 282074 1 07116201913:04 JB tert-Butylbenzene BRL 0.50 ug(L 282074 1 07/16/2019 13:04 JB 1,2,4-Trimethylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB sec-Butylbenzene BRL 0,50 ug/L 282074 1 07/16/2019 13:04 JB 1,3-Dichlorobenzene BRL 0.50 ug/L 282074 1 07/162019 13:04 JB 1,4-Dichlorobenzene BRL 0.50 ug/L 282074 1 07/16201913:04 JB 4-Isopropyltoluene BRL 0.50 ug/L 282074 1 07/162019 13:04 JB 1,2-Dichlorobenzene BRL 0.50 ug/L 282074 1 07116201913:04 JB 1,2-Dibromo-3-chloropropme BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1,2,4-Trichlorobenzene BRL 0.50 ug/L 282074 1 07/16201913:04 JB Naphthalene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB Hexachlorobutadiene BRL 0.50 ug/L 282074 1 07/16/2019 13:04 JB 1,2,3-Trichlorobenzene BRL 0.50 ug/L 282074 1 07/162019 13:04 JB Xylenes, Total BRL 2.0 ug(L 282074 1 07/16/2019 13:04 JB Surr: Dibromofluoromethme 101 76A-125 %REC 282074 1 07/162019 13:04 JB Surr: Toluene-d8 99.5 78.3-116 %REC 282074 1 07/16/2019 13:04 JB Surr: 4-Bromofluorobenzene 98.7 64-125 %REC 282074 1 07/16/2019 13:04 J3 Total Phosphorus E365.1 (E365.1) Phosphorus, Total (As P) 0.165 0.050 mg/L 281964 1 07/15/2019 15:34 GO Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 213 10 mg/L 281956 1 07/16/2019 10:00 NN Nitrogen, Ammonia (as N) E350.1 (E350.1) Nitrogen, Ammonia (As N) BRL 0.200 mg/L 282026 1 07/15/2019 14:36 TL Inorganic Anions by IC EPA 300.0 Chloride 36.1 1.60 mgd. R402550 1 07/12201914:17 BC Nitrogen, Nitrate (As N) 3.26 0.250 mg/1. R402550 1 07/122019 14a7 BC Ilydrogen Ion (pH) by SM4500 II+ B pH 6.30 0.0100 H pH Units R402844 1 07117201915:51 CG Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) 140 20 H Colonies/100 R402782 10 07/152019 14:00 TG m1 METALS, TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 mgiL 281987 1 07/16201915:00 DG Qualifiers; • Value exceeds maximrun contaminant 1ave1 BRL Belowmporting limit H Haldmgtimes for preparation ..analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value R Estimated (value above quantitation range) 8 spike Recovery outride limits due to matrix Nary See ease narrative NC Not confirmed < Less than Result value J Estimated value detected below Reporting Limit Page 14 of 50 Analytical Environmental Services, Inc Date: 24-7ul-19 Client: Colonial Pipeline Client Sample ID: NW-2 Project Name: Greensboro Collection Date: 7/11/2019 2:20:00 PM Lab ID: 19071338-002 Matrix: Aqueous _ _,_ Reporting Dilution rxrlaiye. nesuu Limit ttum units satcnw Factor Date Analyzed Analyst METALS, TOTAL SW6010D (SW3010A) Chromium 0.0105 0.0100 m911, 281987 1 07/16/201915:00 DG Lead BRL 0.0100 mg/L 281987 1 07/16/201915:00 DG Zinc 0.111 0.0200 mg/L 281987 1 07/16/201915:00 DG Qualifiers: a Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Anelyte not NELAC certified B Aoalyte detected in tbo associated method blank > Greater than Result value E Eatimated(value above quantitation range) S Spike Recovery outside limits due to matrix Narr See case narrative NC Not confirmed < Less then Result value 1 Estimated value detected below Reporting Limit Page 15 of 50 SUBMIT FORM ON Y IY£_I OW PAPER ONLY • DEPARTME+NT QF",tENWIR'qU�OrNMENj.$'NATURAL,lRESOURCES N` 1` , GROUNDWATER QUALITY MONITORING: .+ s M d+r h f t iT?0AIt�aSE.RyIC,E,t„L 4j1'F KALE GMpNC'� 00414}61,7' Phone4. (914) 733 221' COMPLIANCE REPORT FORM r bate: 06-30-2D22 Please Print Clearly or Type PERMIT Number: Expiration FnCILITY INFORMATION Colonial Pipeline Company Non -Discharge WO0005809 OIC Facility Name: NYDES Other Permit Name (if different): TYPE OF PERMITTED OPERATION VIONITOREio Facility Address: 411 Gallimore Dairy Road _ "2e`I 27409 County Guilford emediaBEING ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro NC (Zip) ❑ Spray Field ❑ Remediation. (aryl (soato) Telephone#: 336-669-7903 El Rotary Distributor ® Land Application of Sludge Faron D. Lei h Contact Person: 9 5 ❑ Water source Heat Pump ❑ Other: Well Location/Site Name: Dominoradient No. of wells:. to be sampled: tmm P..10 If WELL SAMPLING; INFORMATION MW-3 Date sampler collected: e" & —17 FIELD WAS WELL ID NUMBER (from Permit): in. /ANALYSES: oC pH 42,�units Temp. 2Z 5- DRY at Well Depth: 39.80 ft. Well Diameter: _2 Screened Interval: 38.5 ft. to 43.5 ft. Spec. Cond, µMhos time of sampling, - Depth to Water Level: /3, 40 ft. below measuring point Measuring Point is 1.73 ft. above land surface Relative M.P. Elevation: ft_ Odor '. check- here: Volume of water pumped/bailed A?.ed before sampling: �, oZ .5 gallons Appearance ❑ Samples for metals were collected unfiltered: :.RIYES ❑ NO and field acidified: ®YES ❑.NO' I ABORATORY INFORMATION ZXeel , Laboratory Name: Analytical Environmental Services Certification No. 562 Date sample analyzed: Z PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. N mg/I Pb-Lead t , ®fD mg/I mg/I Nitrite (NO2):as .COD Nitrate N G�mg/I Zn - Zinc ©, /j$ � mg4 ,Collform: MF Fecal /100ml (NO3)ias Coliform: MF:Total /100ml Phosphorus: Total as P mg/I .(Note: use MPN method for highly turbid samples) . -Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 814 mg/I AI -Aluminum mg/I pH (when analyzed) units Ba.-Barium -.mg/I _ TOC mg/I Ca' Calcium -mg/I Chloride mg/I Cd- Cadmium <,&,GO5mg/I Arsenic ril -. Chromium: Total m, 0aZ/ mg/I Grease and Oils mg/I Cu , Copper - ".mg/I ORGANICS: (by GC, GC/MS, HPLC) - Phenol mg/I Fe - Iron mg/I .(Specify test and method #. ATTACH LAB REPORT.) :Sulfate mg/I Hg- Mercurymg/I Report Attached? ® Yes(1)'. ❑ No(0)y Specific Conductance µMhos K - Potassium mg/I VOC - , method #'8260 Total Ammonia mg/I `:Mg - Magnesium mg/I , method # (Ammonia Nitrogen(NHi,as N; Ammonia Nitrogen Total). Mn - Manganese mg/I ",; method # .. - TKN as N mg/I Ni - Nickel mg/I ,: method # For Remediation Systems Only (Attach Lab Reports): - best knowledge and belief, the information submitted Influent Total VOCS: mg/L Effluent Total'.VOCs: mg/L ;VOC Removal% in this report is truei accurateand complete, and that the laboratory analytical data -as pnoduced using approved methods of analysis by a I certify that, to the ofi my • - ...... -- nvt aere. - - the possibility es -olations. I �`� 1• Brian L. Smith - 'Operations Manager (Date) Pennittee (or Authorized Aslant) Name and Title Please punt or type Signa Pertnittee (or AUNonzed Agent) GW-59 Re,.:112007 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-3 Project Name: Greensboro Collection Date: 7/11/201910:00:00AM Lab ID: 1907B38-003 Matrix: Aqueous Analyses Result Reporting Limit Qua] Units BatchlD Dilution Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 282074 I 07/16/2019 13:29 JB 2,2-Dichloropropane BRL 0.50 ug/L 282074 l 07/16/2019 13:29 JB 2-Chlorotoluene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB n-Buhylbenzene BRL 0.50 ug/L 282074 1 07/161201913:29 JB n-Propylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Dichlorodifluoromethane BRL 0.50 ug[L 282074 I 07116201913:29 JB Chloromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Vinyl chloride BRL 0.50 ug/L 282074 1 07/162019 13:29 JB Bromomethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Chloroethane BRL 0.50 ug/L 282074 I 07/16/2019 13:29 JB Trichlorofluoromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB 1,1-Dichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Methylene chloride BRL 5.0 ug/L 282074 1 07/162019 13:29 JB trans-1,2-Dichloroethene BRL 0.50 ug/L 282074 1 07116/201913:29 JB 1,1-Dichloroethane BRL 0.50 ug/L 282074 I 07/16/2019 13:29 JB cis-1,2-Dichloroethene BRL 0.50 ugyl, 282074 l 07/16/2019 13:29 JB Bromochloromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Chloroform BRL 0.50 ug(L 282074 1 07/16/2019 13:29 JB 1,2-Dichloroethme BRL 0.50 ug/L 282074 I 07/16/2019 13:29 JB 1,1,1-Trichloroethane BRL 0.50 u9/1, 282074 1 07/16/2019 13:29 JB 1,1-Dichloropropene BRL 0.50 ugfL 282074 t 07/16/2019 13:29 JB Carbon tetrachloride BRL 0.50 ug/L 282074 1 07/162019 13:29 JB Benzene BRL 0.50 119/1. 282074 1 07/16201913:29 JB Dibromomethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Tichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Bromodichloromethane BRL 0.50 ug/L 282074 1 07/161201913:29 JB 1, 1,2-Trichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Toluene BRL 0.50 Wit, 282074 1 07/16/2019 13:29 JB 1,3-Dichloropropane BRL 0.50 ug/L 282074 I 07/16/2019 13:29 JB Dibromochloromethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB 1,2-Dibromoethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Tetrachloroethene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB 1, 1, 1,2-Tetrachloroethme BRL 0.50 118/6 282074 1 07/16/2019 13:29 JB Chlorobenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Fthylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Bromoform BRL 0.50 u911. 282074 1 07116201913:29 JB Styrene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB 1,2,3-Trichloropropane BRL 0.50 119/1, 282074 1 07/16/2019 13:29 JB lsopropylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Bromobenzene BRL 0.50 ug/L 282074 1 07/16/2019 13:29 JB Qunliflers: ' Value exceeds maximum contaminant level E Estimated (value above gnantitntion range) BRL Below reporting limit S Spike Recovery outside limits due to matrix n Holding times far preparation or analysis excelled Narr Seecase narrative N Analyte not NELAC certified NC Not confiamed B Arulyte detected in the me.e ated method blank < Less then Result value > Greater than Result value 1 Betimated value detected below Reporting Limit Page 16 of 50 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-3 Project Name: Greensboro Collection Date: 7/11/2019 10:00:00 AM Lab ID: 19071338-003 Matrix: Aqueous rceporung Dilution Analyses Result Qual Units BatchD) Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyholuene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surr: Dibromofluoromethane 102 Surr: Toluene-d8 99.6 Surr: 4-13romofluorobenzene 99 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 86 Inorganic Anions by IC EPA300.0 Nitrogen, Nitrate (As N) 0.504 Hydrogen Ion (pH) by SM4500 H+B pH 6.83 METALS, TOTAL SW6010D Cadmium BRL Chromium 0.0214 Lead BRL Zinc 0.0513 Qualifiers: * Valuo exceeds maximum contaminant level BEL Below reporting limit H Holding times for preparation or analysis exceeded N Asmlyte not PIELAC certified B Analyle detected in the associated method blank > Greater than Result value (SW5030B) 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug(L 282074 1 07/16/2019 13:29 JB 0.50 119/1, 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ugJL 282074 1 07116/201913:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 ug/L 282074 1 07/16/2019 13:29 JB 0.50 u9/L 282074 1 07/16/2019 13:29 JB 0.50 119/1, 282074 1 07/16/2019 13:29 JB 2.0 ug/L 282074 1 07/16/2019 13:29 JB 76.4-125 %REC 282074 1 07/16/2019 13:29 JB 78.3-116 %REC 282074 1 07/16/2019 13:29 JB 64-125 95REC 282074 1 07/16/2019 13:29 JB 10 mg/L 281956 I 07/16/201910:00 NN 0.250 mg/L R402550 1 07/121201914:33 BC 0.0I00 H pH Units R402844 1 07/17/201915:51 CG (SW3010A) 0.0050 mg/L 281987 1 07/16/201915:02 DO 0.0100 1119/L 281987 I 07/16/201915:02 DO 0.01.00 mg/L 281987 1 07116/201915:02 DO 0.0200 mg/L 281987 1 07/161201915:02 DO E Estimated (value above quarentaticin range) S Spike Recovery outside limits due to matrix Nair Seeca mintative NC Notconfrmed < Less than Result value J Estimated value detected below Reporting Limit Page 17 of 50 SUBMIT FORM ON YELLQW PAPER ONLY DEPARTMENVClF{Eyr. q,y'RESOURCE t GROUNDWATER QUALITY MONITORING: I�xAR��RAl2fiffIwm"ji7c'99goA§"sl,'.r33227r*a' 401, COMPLIANCE REPORT FORM PER MIT Number: Expiration Date: 06-30,2022 ` Please Print Clearly a Type FACILITY INFORMATION Nonate: -Discharge W00005809 U IC Facility Name: Colonial Pipeline Company ` Other NPDES Permit Name (if different): TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address: 411 Gallimoref Dairy Road (Su.0 NC 27409 County Guilford ❑ Lagoon ElRemediation- Infiltration Gallery, Greensboro Q Spray Field ❑Remediation: (stare/ c��P) lctyl Telephone#: 336-669-7903 0; Rotary Distributor ® Land Application of Sludge Contact Person: Faron D. Leigh - No. wells to be sampled: 5 ❑. Water Source: Heat Pump El Other: Well Location/Site Name: Downgr'adient of from Permu If WELL SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-4 (MW-135) Date sample: collected: O% // Ir% FIELD AANLALLYSES: oC Temp. A7 WAS DRY at Well Depth: 29.5 ft. Well Diameter. 2 in. pH 7.�units 0 µMhos time of: Depth to Water Level:: .00ft. below measuring point Screened Interval 13 ft. to : 28 ft. :Spec. Cord. sampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft.:' Odor check here: Volume of water pumped/bailed before sampling: _ S 75_gallons , Appearance Sam lest:for.:metals were collected unfiltered:'®YES ❑ NO and field acidified: ®YES ❑ NO 1 4BORATORY INFORMATION. Date sample analyzed: 0%/aZ 7fAl2 d7 I% Laboratory Name: Analytical Environmental Services Certification No. 562 PARAMETERS NOTE: Values should reflect dissolvedand colloidal concentrations. Lead olQ mg/I COD mg/I Nitrite (NO2)`as N mg/I Pb ' Nitrate (1,103):.as N C,/ rng/I Zn - Zinc /l / mgil Coliform: MF Fecal /100ml Coliform: MF Total ` /100ml Phosphorus: Total as p mg/I Other (Specify Compounds and Concentration Units): (Note use MPN method for h�ghty turbrtlsamFlee) Orthophosphate mg/I Dissolved Solids: Total mg/I - AI -Aluminum ' mg/1 pH (when analyzed) units Ba - Barium " mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd Cadmium 4:0, 00-5 mg/I Arsenic mg/I Chromium. Total . mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC)' Phenol mg/I Fe,- Iron rig/I (Specify test and method#. ATTACH LAB REPORT.) - "Sulfate mgA Hg- Mercury �'mg/I Report Attached? IR Yes(1): ❑ No(0) Specific Conductance µMhos K- Potassium mgA VOC ;method # 8260 - Total Ammonia mg/I ;Mg - Magnesium ` _mgA .;.method# ,(Ammonia N tmyed(:NH,ss N; Ammonia Nitrogen Total). Mn - Manganese mg/I ,. method # TKN as N mg/I Ni -Nickel `-m9/1 ',: method #-... ,.. For Remediation Systems Only (Attach Lab; Reports): Influent Total VOCS: mg/L 'Effluent Total: VOCS: mg/L 'VOC Ramovat% Brian L. Smith - Operations Manager (Date) " Permittee (or Authorized Aqent) Name and Title Please print or we Sipnature of Penmttee (or Authorized A harm GW-59 Rev.1/2007 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW-4) Project Name: Greensboro Collection Date: 7/11/2019 10:50:00 AM Lab ID: 1907B38-008 Matrix: Aqueous Analyses Result y Reporting Limit Dilution Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 118/1. 282074 1 07116/201916:23 JB 2,2-Dichloropropane BRL 0.50 ug/L 282074 1 07/16201916:23 JB 2-Chlorotoluene BRL 0.50 ug/L 282074 1 07/16201916:23 JB n-Butylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB n-Propylbenzene BRL 0.50 ug/L 282074 I 07/16/2019 16:23 JB Dichlorodifluoromethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Chloromethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Vinyl chloride BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Bromomethane BRL 0.50 119/1, 282074 1 07116201916:23 JB Chloroethane BRL 0.50 ug(L 282074 t 07/16/2019 16:23 JB Trichlorofluoromethane BRL 0.50 ug/L 282074 1 07116201916:23 JB 1,1-Dichloroethene BRL 0.50 ug/L 282074 I 07/16/2019 16:23 JB Methylene chloride BRL 5.0 ug/L 282074 1 07/162019 16:23 JB trans-1,2-Dichloroethene BRL 0.50 ugJL 282074 1 07/16/2019 16:23 JB 1,1-Dichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB cis-1,2-Dichloroethene BRL 0.50 ug/L 282074 I 07116/201916:23 JB Bromochloromethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Chloroform BRL 0.50 ug/L 282074 1 07/16201916:23 JB 1,2-Dichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1, 1, 1-Trichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1,1-Dichloropropene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Carbon tetrachloride BRL 0.50 ug/L 282074 1 07/162019 16:23 JB Benzene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Dibromomethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Trichloroethene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Brorrodichloromethane BRL 0.50 ug/L 282074 1 07116201916:23 JB 1, 1,2-Trichloroethane BRL 0.50 ug/L 282074 I 07/16/2019 16:23 JB Toluene BRL 0.50 ug/L 282074 1 07/16201916:23 JB 1,3-Dichloropropane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Dibromochloromethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1,2-Dibromoethane BRL 0.50 ug/L 282074 t 07/16/2019 16:23 JB Tetrachloroethene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Chlorobenzene BRL 0.50 ue/L 282074 1 07/16/2019 16:23 JB Ethylbenzene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Bromoform BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Styrene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1, 1,2,2-Tetrachloroethane BRL 0.50 ug./L 282074 1 07/162019 16:23 JB 1,2,3-Trichloropropane BRL 0.50 ig/L 282074 1 07/1WW916:23 JB Isopropylbenzene BRL 0.50 ug/L 282074 1 07116201916:23 JB Bromobenzene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Qunlifiers: ' Value exceeds maximum contaminant level E Estimated (value above quantization range) BRL nelowreportioglimit 8 Spike Recovery outside limits duo to matrix H Holding limes for preparation or analysis exceeded Narr See case narrative N Ardelyte not PELAC certified NC Not confirmed o Arealyto detected in the associated method blank < Less than Result value > Greeter than Result valnc J Estimated value detected below Reporting Limit Page 26 of 50 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW-4) Project Name: Greensboro Collection Date: 7/11/201910:50:00AM Lab ID: 19071338-008 Matrix: Aqueous Analyses Result Reporting Limit Qual Units Dilution BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 4-Chlorotoluene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1,3,5-Trimethylbenzene BRL 0.50 1194. 282074 I 07116201916:23 JB tert-Butylbenzene BRL 0.50 ug/L 282074 1 07116201916:23 JB 1,2,4-Tr'imethylbenzene BRL 0.50 ago, 282074 1 07116201916:23 JB sec-Butylbenzene BRL 0.50 1194. 282074 1 07/16/2019 16:23 JB 1,3-Dichlorobenzene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1,4-Dichlorobenzene BRL 0.50 ug/L 282074 1 07116201916:23 JB 4-Isopropyltoluene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB 1,2-Dichlorobenzene BRL 0.50 ug/L 282074 t 07/16/2019 16:23 JB 1,2-Dibromo-3-chloropropme BRL 0.50 1194, 282074 1 07/16/2019 16:23 JB 1,2,4-Trichlorobenzene BRL 0.50 1184, 282074 1 07/162019 16:23 JB Naphthalene BRL 0.50 ug/L 282074 1 07/16/2019 16:23 JB Hexachlorobutadiene BRL 0.50 ug/L 282074 t 07/16/2019 16:23 JB 1,2,3-Trichlorobenzene BRL 0.50 uglL 282074 1 07116201916:23 JB Xylenes, Total BRL 2.0 ug/L 282074 1 07/16/2019 16:23 JB Sun: Dibromofluoromethano 100 76.4-125 %REC 282074 1 07/16/2019 16:23 JB Surr: Toluene-d8 101 78.3-116 %REC 282074 1 07/16/2019 16:23 JB Sun: 4-Bromofluorobenzene 96 64-125 /Rm 282074 I 07/16/2019 16:23 JB Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 105 to mg/L 281956 1 07/162019 10:00 NN Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) BRL 0.250 mg/L R402550 1 07/122019 15:53 BC Hydrogen Ion (pH) by SM4500 H+ B PH 6.23 0.0100 H PEI units R402844 1 07/17201915:51 CG METALS, TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 pnWL 281997 1 07/16201915:04 DO Chromium 0.0412 0.0100 m9/L 281987 1 07/16/201915:04 DG Lead BRL 0.0100 mg(L 281987 1 07/16/201915:04 DO Zinc 0.147 0.0200 m9/L 281987 1 07/16201915:04 DO Qualifi.ou • Value exceed. maximum contaminant level BRL Bclowrepoang limit H Holding times for preparation or analysis exceeded N Analyte not NELAC retitled e Analyte detected in the associated method blank > emater than Result value B Estimated (value above ipantitation range) S Spike Recovery outside limits due to matrix N. See case narrative NC Not confirmed < Less than Result value J Estimated value detected below Reporting Limit Page 27 of 50 SUBMIT FORM ON YFI LOW PAPER ONLY rx,QTER'QU9ALKE UI O PROCE SOUIRS �ITii' �W��� OTOF INFOI�M�AT NG UNIT, y, QUALITY MONITORING: . •' , r"5� " e Fhoge?i(aA)��azzt^ GROUNDWATER �d�7fI�uesR�tictr xel�„i�yN,tnz���fiis�a COM'PLIANCEREPORT_FORM ' Expiration Date: 06-30-2022 Please Print Cleariyor Type PERMIT Number: FACILITY INFORMATION Non -Discharge WQ0005809 UIC Facility Name: ,Colonial Pipeline Company :. NPDES Other. Permit Name (if different): TYPE OF PERMITTED OPERATION BEING: MONITORED Facility Address: 411 Gallimore Dairy Road 27409 County. Guilford ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro NC ` El Spray Field ❑Remediation Ic„ I (Slp,ia) (_np) Telephone#: 336-669-7903 El Rotary Distributor RI Land Application of Sludge Faron D. Lei h Contact Person: 9 l ❑ `. . ': No, of wells to be sampled: 5 Water Source Heat Pump El Other: Well Location/Site Name: DoWngradient tram Permit If WELL SAMPLING INFORMATION AS WELL ID NUMBER (from Permit): MW-6 (MW-183) Date sample collected: O%l` �9 FIELD ANALYSES: oC DRY: at Well Depth: 27.00 ft. WOO _2 in. pH .�•�units Temp. .%.�s time of Screened Interval 10 ft. to 25 ft. Spec. Cond. µMhos sampling, Depth to"Water Level �ft. below measuring point check 1.5 ft. above land surface Relative M.P. Elevation: ft. Odor Measuring Point is - hares❑ ater pumped/balled before sampling: <gallons Appearance - Volume of w//�n Sam les: foranetals were collected,unfiltered::®YES ❑ NO and field acidified: ®YES ❑ NO I ARORAT DRY INFORMATION O% /� �/ Laboratory Name: Analytical Environmental Services Certification No. 562 Date sample analyzed: irru PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.Pb -Lead mg/I as N mg/I L , '.COD mg/I Nitrite (NO2) Nitrate(NO3); as N�mg/l Zn - Zinc Go. tM&5 mgfl Coliform: MF Fecal /100ml Coliform: MF Total ' : 1100ml Phosphorus: Total as P rng/I Other (Specify Compounds and Concentration Units). - - (Note. use MPN method for highly turbid samples) Orthophosphate _ mg/1 Dissolved Solids: Total '1V,6 mg/I Al Aluminum mg/I pH (when analyzed) units Be Barium mg/I TOC mg/I Ca - Calcium mg/I mg/l Cd Cadmium Gd. 6a5 ' mg/I - Chloride Arsenic mg/I Chromium: Total <O, 6114 mg/I - Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) mg/I Fe. -:Iron `mg/I .(Specify test and method#. ATTACH LAB REPORT.) Phenol Sulfate mg/1 Hg - Mercurymg/I Report Attached? ba Yes (1) ❑ No (0) Specific Conductance µMhos ' K Potassium rng/1 VOC method #'8260 Total Ammonia mg/I Mg - Magnesium 117194 ;'method# (A moms wtrogeniNH,as ry Ammpma wrmsen, Torap Mn Manganese ' 171719/1 ,. method.# TKN.asN mg/I Ni Nickel -mg/I -,.method # For Remediation Systems Only (Attach Lab: Reports): Influent Total VOCs I mg/L -Effluent Total.VOCs; mg/L <VOG Removal'/ OEM - Brian L. Smith - Operations Manage[ signature of Permittee (or Authonzed Agent) !Date) Permittee (or Authorized Agent) Name and Title Please print or Noe GW-59 Rev. 172007 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-183 (MW-6) Project Name: Greensboro Collection Date: 7/11/201910:20:00AM Lab ID: 1907B38-009 Matrix: Aqueous Reoortina Dilution _ Analyses Ieesult Limit ttual Units 15MC1110 Factor Bate Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 282074 1 07/16/201916:47 JB 2,2-Dichloropropane BRL 0.50 ug/L 282074 1 07/16201916:47 JB 2-Chlorotoluene BRL 0.50 ug/L 282074 I 07/16/201916:47 JB n-Buhylbenzene BRL 0.50 ug/L 282074 1 07/16/201916:47 JB n-Propylbenzene BRL 0.50 ug/L 282074 1 07116201916:47 JB Dichlorodifluoromethane BRL 0.50 ug/L 282074 1 07/16/201916:47 JB Chloromethane BRL 0.50 ug/L 282074 1 07/16201916:47 JB Vinyl chloride BRL 0.50 ug/L 282074 1 07/16/2019 16:47 JB Bromomethane BRL 0.50 ug/L 282074 1 07/16/201916:47 JB Chloroethane BRL 0.50 ug/L 282074 1 07/161201916:47 JB Trichlorofluoromethane BRL 0.50 119/1. 282074 1 07116201916:47 JB 1,1-Dichloroethene BRL 0.50 ug/L 282074 1 07116201916:47 JB Methylene chloride BRL 5.0 ug/L 282074 1 07/162019 16:47 JB trans-1,2-Dichloroethene BRL 0.50 ug/L 282074 1 07/16201916:47 JB 1,1-Dichloroethane BRL 0.50 ug/L 282074 1 07/161201916:47 JB cis-1,2-Dichloroethene BRL 0.50 119/1, 282074 I 07116201916:47 JB Bromochloromethane BRL 0.50 ug/L 282074 1 07/16201916:47 JB Chloroform BRL 0.50 ug/L 282074 1 07/16/201916:47 JB 1,2-Dichloroethane BRL 0.50 ug/L. 282074 1 07/16201916:47 JB 1, 1, 1-Trichloroethane BRL 0.50 ug/L 282074 1 07/16201916:47 JB 1,1-Dichloropropene BRL 0.50 ug/L 282074 1 07116/201916:47 JB Carbon tetrachloride BRL 0.50 ug/L 282074 1 07/162019 16:47 JB Benzene BRL 0.50 ug/L 282074 1 07/16/201916:47 JB Dibromomethane BRL 0.50 ug/L 282074 I 07/16201916:47 JB Trichloroethene BRL 0.50 ug/L 282074 1 07/16201916:47 JB Bromodichloromethane BRL 0.50 ug/L 282074 1 07116201916:47 JB 1, 1,2-Trichloroethane BRL 0.50 ug/L 282074 1 07/16/2019 16:47 JB Toluene BRL 0.50 ug/L 282074 1 07116201916:47 JB 1,3-Dichloropropane BRL 0.50 ug/L 282074 1 07116201916:47 JB Dibromochloromethane BRL 0.50 ug/L 282074 1 07/16201916:47 JB 1,2-Dibromoethane BRL 0.50 ug/L 282074 1 07116/201916;47 JB Tetrachloroethene BRL 0.50 ug/L 282074 1 07/16/201916:47 JB 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 282074 1 07/16201916:47 JB Chlorobenzene BRL 0.50 ug/L. 282074 1 07/161201916:47 JB Ethylbenzene BRL 0.50 ug/L 282074 1 07/16201916:47 JB Bromoform BRL 0.50 ug/L 282074 1 07/16/201916:47 JB Styrene BRL 0.50 ug/L 282074 1 07/16201916:47 JB 1, 1,2,2-Tetmchloroethane BRL 0.50 ugfL 282074 1 07/16201916:47 JB 1,2,3-Trichloropropane BRL 0.50 ug/L 282074 1 07/16/2019 16:47 JB Isopropylbenzene BRL 0.50 ug/L 282074 1 07/16/201916:47 JB Bromobenzene BRL 0.50 ug/L 282074 1 07/16201916:47 JB Qualifiers: • Value exceeds maximum contaminant level E Estimated (value above quantization range) BRL Belowreportinglimit S Spike R.., outside limits due to matrix H Holding times for preparation or mabns s exceeded Nan See case narrative N Analyte not NELAC certified NC Not confirmed e Analyte detected in the associalcd method blank < Less than Result value > Greater than Result value / Estimated value detected below Reporting Limit Page 28 of 60 Analytical Environmental Services, Inc Date: 24-Jul-19 Client: Colonial Pipeline Client Sample ID: MW-183 (MW-6) Project Name: Greensboro Collection Date: 7/11/201910:20:00AM Lab ID: 1907B38-009 Matrix: Aqueous Reporting _ _... _ . _ Dilution _ Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobeozene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropme BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Surr: Dibromofluoromethane l00 Surr: Toluene-d8 99.8 Surr: 4-Bromofluorobenzene 96.5 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 106 Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) BRL Hydrogen Ion (pH) by SM4500 H+ B PH 5.57 METALS, TOTAL SW6010D Cadmium BRI Chromium BRI Lead BRI Zinc BRI Qualifiers: a Value exceeds maximum contaminant level BRL Below reporting limit It Holding times to, preparation or analysis exceeded N Analyte not NELAC certified B Anslyte detected in the associated method blank > Greater than Result value Factor --._--_, __ ._..„.,,,,. (SW5030B) 0.50 ug/L 282074 1 07116/201916:47 JB 0.50 ug/L 282074 1 07/16/201916:47 JB 0.50 ug/L 282074 1 07/16/201916:47 JB 0.50 AWL 282074 1 07/16201916:47 JB 0.50 119rt. 282074 1 07/16/2019 16:47 JB 0.50 ug/L. 282074 I 07/16/201916:47 JB 0.50 ug/L 282074 1 07/16/201916:47 JB 0.50 ug/L 282074 1 07/16201916:47 JB 0.50 ug/L 282074 1 07/16201916:47 JB 0.50 ug/L 282074 1 07/16201916:47 JB 0.50 u9/L 282074 1 01/16/201916:47 JB 0.50 ug/L 282074 1 07/16/201916:47 JB 0.50 ug/L 282074 1 07/16/2019 1647 JB 0.50 ug/L 282074 1 07/161201916:47 JB 2.0 ug/L 282074 1 07/16201916:47 JB 76.4-125 %REC 282074 1 07/16201916:47 JB 78.3-116 %REC 282074 I 07/16/201916:47 JB 64-125 %REC 282074 I 07116/201916:47 JB l0 mg/L 281956 1 07/161201910:00 NN 0.250 mg/L R402550 1 07112/201916:09 BC 0.0100 H pH Units R402844 1 07/17201915:51 CG (SW3010A) 0.0050 mg/L 281987 1 07/161201915:11 DO 0.0100 mg/L 281987 1 07/16201915 a1 DO 0.0100 mg/L 281987 1 07/16/201915:11 DO 0.0200 mg/L 281997 1 07/16201915:11 DO E Estimated(value above quantitamn range) S Spike Recovery outside limits due to matrix Nam See case narrstive NC Not confirmed < Less than Result value J Estimated value detected below Reporting Limit Page 29 of 50 GW-59A COMPLIANCE REPORT FORM Permit # (Submit one each tnonituring period �t!ith G4-i7 firms,} P Enter date monitoring results were due. (� 3G -ZF) Will this monitoring report (GW-59 and G111i_59A) YES NO be submitted after the established due date? X Z Was any required information missing on the GW-59 report forms? YES N F the answer to question 1 or 2 is "YES", list in the space provided below the well identification numbers) and xplain the problems encountered in obtaining the required information. q3Areany of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing}(ES NO dentification plate, area overgrown, etc,)? If the answer is "Yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? Y5 Np Y) if the answer to question 4 is `NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and conceritration(s) exceeding standards in the space provided below; -4// �f' A- veIs w r/oty 6, 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is NO , skip to section S. if the answer to question 5 is "YES"' list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). �eA 4, 6e%("//W . 5 5 u / ," dr 3 f �` �� '� pf/ 6.,ag /'0 7-,/fir aai S- cv-6 Pit 6./f dd/g, M r r N r7 :ed c% f 6 Are the monito ing wells listed in section 5 located at or beyond the review boundary? YES if the answer is "YES', a groundwater qualify problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answeris "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO'; v required to determine the impact the waste rllcposa! 2WQM L�2 having at the review and comoflanre boundaries surrounding th_i_s facility_ . Failure to do s.Q Inay subject permittee to a Notice pf Vl,t�r;,,., Fines. and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Signature of Permittee (or Authorized Agent) Date G4V-59A l2i$12003 GROUNDWATER QUALITY MONITORID COMPLIANCE REPORT FORM FAf ILITY'-INFORMATION Fa11 cility Name: Colonial Pipeline Company Permit Name (if different): FaciUty Address; 411Gallimore Dairy Road Greensboro s' ee9 NC (City) Contact Person: Faron D. Leigh`.. Well Location/Site Name: Downgradient SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-1 MV Well Depth. 21.20 g, Depth to Water Level 5, %a ft. below measuril Measuring; Point is 3 ft. above land sur Volume of water pumped/bailed before sampling:: - Samples for metals were coil acted -unfiltered:.®` Date sample analyzed:�t. 15' PARAMETERS NOTE: Values should reflecYd COD r Coliform: MF Fecal / Coliform: MFTotal (Note- Use MPN method for highly turbidsamples) Dissolved Solids: Total r pH'. (when analyzed) " t TOC T Chloride 11,7 r Arsenic r Grease and Oils r Phenol r Sulfate r Specific Conductance ` t Total Ammonia Z O • ' r (Ammonia Nitrogen; Niipae N, Ammonia Nitrogen Total) TKN as N r For Rem_ ediation Systems Only (Attach Lab Rep. Brian L. Smtih - Operations Manager m PeritteAu e{or thorized Ao Name and Title Please Dnnto GW-59- Rev. 1/2007 SUBMIT FORM.ON YYELLL..QAPAPER ONLY DE`fypJwi,TpNMErIIT'OErzE,[�U�1 MEN�TB. Tt1RAL�yRESOURCESxrye♦R IIp3�n�.0 I FORM O PhIOCES INGIt'lh'"ruy ". N++' 6,1j7�MWII�S,�RirtC��ER,jC./y'�J..GH�fytCfi99,.y1Te4�PtlhoOe dt9M,914`733-�3Y2'1 , vse Printaeady or,rype,, PERMIT?Number: '':Expiration Date: 06-30-2022 Non -Discharge WQ0005809 UIC NPDES Other ` TYPE OF, PERMITTED OPERATION BEING MONITORED El -Lagoon ❑Remediation: Infiltration Gallery 27409 County Guilford (zip) ❑ Spray Field ElRemediation: Telephone#: 336-669-7903 ❑ Rotary,Distributor 5dLand Application of Sludge No. of wellsao be sampled: 5 El Water, Source Heat Pump Other: tram Penn` If WELL ple colr i /a % B)_ Date samacted: 9 - FIELD ANALYSES: C o WAS DRY at { Well Diameter: 2 in. . pH 3- units Temp. v— Mhos time of ioint screened Interval 5ft. to 20 ft. Spec, Cond., sampling, Relative M.P. Elevation: ft. Odor check j here: 2 s gallons - Appearance El NO� and field acidified: ® YES: ❑ NO t7,1 Laboratory Name:, Analytical Environmental Services Certification No. 562 Dlved and colloidal concentrations. Nitrite (NO2) asN mg/I Pb -:Lead G'G. �/O mg/1 iml Nitrate (NO3) as N Mgt] Zn-Zinc Q, Q,&2Z mg/I iml Phosphorus: Total as P mg/I mg/I Other (Specify Compounds and Concentration Units): Orthophosphate iAl- Aluminum mg/I Ba Barium mg/I Ca Calcium mg/I Cd-Cadmium 005 mg/I Chromium: Total </J. /I / f% mg/I Cu - Copper -mg/I: ORGANICS: (by GC, GC/MS, HPLC) Fe --Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Hg -Mercury `• mg/I . Report Attached? ® Yes (1) , El No (0) os K -Potassium mg/I VOC , method # 8260 Mg - Magnesium mg/I ,method # Mn Manganese mg/1 ,method # Ni -.Nickel mg/I „method # Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 12:00:00 PM Lab ID: 1903C14-001 Matrix: Aqueous Analyses Y Result -jpai it Qua] Units BatchID unction Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0,50 ug/L 276110 1 03/19/2019 13:47 NP 2,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 2-Chlorotoluene BRL 0.50 ugR, 276110 1 03/19/2019 13:47 NP n-Butylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP n-Propylbenzene BRL 0.50 ug/L 276110 1 03/19201913:47 NP Dichlorodifluoromethane BRL 0.50 uglL 276110 1 03119201913:47 NP Chloromethane BRL 0.50 ug/L 276110 I 03/191201913:47 NP Vinyl chloride BRL 0.50 1191L 276110 1 03/192019 13:47 NP Bromomethane BRL 0.50 ug/L 276110 1 03/191201913:47 NP Chloroethane BRL 0.50 ug/L 276110 1 03119201913:47 NP Trichlorofluoromethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1,1-Dichloroethee BRL 0.50 ug/L 276110 1 03/1912019 13:47 DIP Methylene chloride BRL 0.50 ug/L 276110 1 03/192019 13:47 NP trans-1,2-Dichloroethee BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1,1-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP cis-1,2-Dichloroethee BRL 0.50 ug1L 276110 1 03119/201913:47 NP Bromochloromethane BRL 0.50 ng/L 276110 1 03/191201913:47 NP Chloroform BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1,2-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1,1,1-Trichloroethane BRL 0.50 491L 276110 1 03/191201913:47 NP 1,1-Dichloropropane BRL 0.50 ug/L 276110 1 03119201913:47 NP Carbon tetrachloride BRL 0.50 ug/L 276110 1 03/191201913:47 NP Benzene BRL 0.50 ug/L 276110 1 03119/201913:47 NP Dibromomethane BRL 0.50 ug/L 276110 1 03/191201913:47 NP Trichloroethene BRL 0.50 u91L 276110 1 03/19/2019 13:47 NP Bromodichloromethane BRL 0.50 ug/L 276110 1 03/19/201913:47 NP 1, 1,2-Trichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP Toluene BRL 0.50 ug/L 276110 1 03119201913:47 NP 1,3-Dichloropropane BRL 0.50 ug/L 276110 1 03/19201913:47 NP Dibromochloromethane BRL 0.50 ug/L 276110 1 03119/201913:47 NP 1,2-Dibronroethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP Tetrachloroethee BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP Chlorobenzene BRL 0.50 us/L 276110 1 03/19/2019 13:47 NP Ethylbenzene BRL 0.50 ug(L 276110 1 03119201913:47 NP Bromoform BRL 0.50 ug1L 276110 1 03/19/2019 13:47 NP Styrene _ BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP 1,1,2,2-Tetrachloroethane BRL 0.50 1191L 276110 1 03119201913:47 NP 1,2,3-Trichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 13:47 NP Isopropylbenzene BRL 0.50 ug1L 276110 1 03/19/2019 13:47 NP Bromobenzene BRL 0.50 U91L 276110 1 03119/201913:47 NP Qualifiers: * Value exceeds maximum contaminant level L Estimated (value above gantitation range) BEL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times For preparation or analysis exceeded Norr Seecasensoative N Acolyte not NELAC certified NC Net ... proud E Analyze detected in the associated method blank < Less than Result value > Greater than Result value 7 Estimated value detected below Reporting Limit Page 10 of 48 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-1 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 12:00:00 PM Lab ID: 1903C14-001 Matrix: Aqueous Analyses Result s"V,asL s'p; Quill Units BatchID uuunm' Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL test-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BILL Xylenes, Total BRL Surr: Dibromofluoromethane 95.7 Surr: Toluene-d8 99.9 Surr: 4-Bromofluorobenzene 91.9 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 130 Nitrogen, Ammonia (as N) E350.1 Nitrogen, Ammonia (As N) BRL Inorganic Anions by IC EPA 300.0 Chloride 11.7 Nitrogen, Nitrate (As N) 4.18 Hydrogen Ion (pH) by SM4500 H+ B pH 5.64 Fecal Coliform (MY) SM9222D Fecal Coliform, (NU) BRL METALS, TOTAL SW6010D Cadmium BRL Chromium BRL Lead BRL Zinc 0.0291 Qualifiers: • Value exceeds maximum contaminant level Bar, Below reporting limit H neldul, times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greatertlmn Result value (SW5030B) 0.50 ug/L 276110 I 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03119/201913:47 NP 0.50 ug/L 276110 I 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 u91L 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 0.50 U9fL 276110 1 03/19/2019 13:47 NP 0.50 ug/L 276110 1 03/19/2019 13:47 NP 2.0 ug/L 276110 I 03/19/2019 13:47 NP 76.4.125 %REC 276110 1 03/19/2019 13:47 NP 78.3-116 /REC 276110 1 031191201913A7 NP 64.125 %RFC 276110 1 03/19/201913;47 NP l0 mg(L 275159 1 03/14/201913:20 AT (E350.1) 0.200 mg/L 275816 1 03114/201910:33 3M 1.00 mg/L R393136 1 03113/201915:10 GO 0.250 mg(L R393136 1 03/131201915:10 GO 0.0100 H pH Units R393166 1 03/141201910:47 BK 4 H Calaniesllo0 R393463 2 03/13/201916:28 TG 1111 (SW3010A) 0.0050 mg/L 275948 1 03/18/201912:49 AI 0.0t00 mglL 275948 1 03/18/201912:49 AJ 0.0100 m9/L 275948 1 03/18/201912:49 Al 0.0200 mg(L 275948 1 03/18/20D 12:49 Alf E Estimated(value above Wanitalion range) S Spike Recovery outside limits due to matrix Nmr, See case narrative NC Not confirmed < Less Chun Result value 1 Estimated value detected below Reporting Limit Page 11 of 48 F ATER(QUALITY MONITORII NCE REPORT FORMFORMATION: Colonial Pipeline Company (if different):ss: 411'Gallimore Dairy Road Greensboro `$1fBe1) N( .Icily) (Slate} Conte Person: Faron D. Leigh ` Well Location/Site Name: Downgradient SAMPLINr' INFORMATION WELL ID: NUMBER(from Permit): MW-2 Well Depth: 25.20 ft. Depth to Water Level: -S, W ft..below measur Measuring: Point is 1.75 ft.:above land su Volume of water pumped/bailed before sampling;A i Samples for metals were collected, unfiltered: "R1 Date sample analyzed:-` •` PARAMETERS .NOTE: Values should reflect„i COD Coliform: MF Fecal Coliform: MF Total (Nate: Use MPN method for hlghlyturbid samples) Dissolved Solids: Total 3 pH (when analyzed) TOC O Chloride S• 7 Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia S �• '(Ammonia Nitrogen; NHsas N; Pmmonia.Nitrogen Total) TKN. as N i For Remediation Systems Only (Attach Lab Rel Brian L. Smith Operations Manager Permittee:(orAuthonzed Aaeit) Name and -Title Please pnnt GW-59 Rev. 1/2007 2 in. pH J'..�units temp. LL-.Z time of 1B ft. to 23 ft. Speer Cond. ! µMhos sampling, ft. Odor check Appearance here: 'ES° ❑ NO /tical Environmental Services Certification No 562 mg/I Pb - Lead <©� mg/I �mg/l - Zn-Zinc mg/I mg/I mg/I 'Other (Specify Compounds'and Concentration Units):.'. mg/I mg/I mg/I • (f; mg/I mgA mg/I ORGANICS: (by GC, GC/MS, HPLC) mg/I, ,(Specify test and method A ATTACH LAB REPORT.) mg/I "'Report Attachetl? IR Yes (1) ,❑ No (0) mg/I VOC ,.method# 8260 mg/I , method # mg/l , method # mg/I �;,method # Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 12:30:00 PM Lab ID: 1903C14-002 Matrix: Aqueous neporung Dilution Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 276110 l 03/19/2019 14:12 NP 2,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/191201914:12 NP 2-Chlorotoluene BRL 0.50 u91L 276110 1 03/19/2o19 14:12 NP n-Butylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP n-Propylbenzene BRL 0.50 ug(L 276110 1 03119/201914:12 NP Dichlorodifluoromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Chloromethane BRL 0.50 ug/L 276110 1 03119/201914:12 NP Vinyl chloride BRL 0.50 ug(L 276110 1 03/19/2019 14:12 NP Bromomethane BRL 0.50 ug/L 276110 1 03/151/201914:12 NP Chloroethane BRL 0.50 ug/L 276110 1 03/191201914:12 NP Trichlorofluoromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP I,l-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Methylene chloride BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP trans-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP I,I-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP cis-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Bromochloromethane BRL 0.50 ug/L 276110 1 03119/201914:12 NP Chloroform BRL 0.50 ug/L 276110 1 03/19201914:12 NP 1,2-Dichloroethane BRL 0.50 uglL 276110 1 03/19/2019 14:12 NP 1, 1, 1-Trichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,1-Dichloropropene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Carbon tetrachloride BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Benzene BRL 0.50 ugH. 276110 1 031191201914:12 NP Dibromomethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Trichloroethee BRL 0.50 uglL 276110 1 03119201914:12 NP Bromodichloromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,1,2-Trichloroethane BRL 0.50 u97L 276110 1 03/19201914:12 NP Toluene BRL 0.50 ug/L 276110 1 03/19201914:12 NP 1,3-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Dibromochloromethane BRL 0.50 ng/L 276110 1 03/19/2019 14:12 NP 1,2-Dibromoethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Tetrachloroethene BRL 0.50 UFA 276110 1 03/19/2019 14:12 NP 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 276110 t 03/19/2019 14:12 NP Chlorobenzene BRL 0.50 ug/L 276110 1 03/19201914:12 NP Ethylbenzene BRL 0.50 u9(L 276110 1 03/19/2019 14:12 NP Bromoform BRL 0.50 ugfL 2761t0 1 03/19/2019 14:12 NP Styrene BRL 0.50 ug/L 276110 l 03/19201914:12 NP 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,2,3-Trichloropropane BRL 0.50 ug/L 276110 1 03/19201914:12 NP Isopropylbenzene BRL 0.50 ng/L 276110 1 03/19/2019 14:12 NP Bromobenzene BRL 0.50 ug/L 276110 1 03119201914:12 NP Qualifiers: a Value exceeds maximum contaminant level ➢RL Babov.portinglimit 11 Holding times for preparation or analysis exceeded N Analyto not NELAC certified B Analyze detected in the associated method blank > Caeater than Result Value B Estimated (value above purnitatlon range) S Spike Recovery outside limits due to ms Fix Nam See case narrative NC Not confirmed c Less than Result Value J Estimated value detected below Reporting Limit Page 12 of 48 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-2 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 12:30:00 PM Lab ID: 1903C14.002 Matrix: Aqueous Reporting _ , , m Dilution _ Limit c-'»••'••�� Factor aiaaG llLL4rd'GCU HRmy" Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 4-Chlormoluene BRL 0.50 u27L 276110 1 03/19/201914:12 NP 1,3,5-Trimethylbenzene BRL 0.50 ug/L 276110 1 03/191201914:12 NP tent-Butylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,2,4-Trimethylbenzene BRL 0.50 ug[L 276110 1 03/19/2019 14:12 NP sec-Butylbenzene BRL 0.50 ug/L 276110 1 03119/201914:12 NP 1,3-Dichlorobenzene BRL 0.50 U9/1, 276110 1 03/19/2019 14:12 NP 1,4-Dichlorobenzene BRL 0.50 uglL 276110 1 03/191201914:12 NP 4-Isopropyltoluene BRL 0.50 ug/L 276110 I 03/19/2019 14:12 NP 1,2-Dichlorobenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,2-Dibromo-3-chloropropane BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,2,4-Trichlorobenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Naphthalene BRL 0.50 U91L 276110 1 03/19/2019 14:12 NP Hexachlorobutadiene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP 1,2,3-Tiichlorobenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:12 NP Xylenes, Total BRL 2.0 ug/L 276110 1 03/19/2019 14:12 NP Surr: Dibromofluoromethane 97.4 76.4-125 %REC 276110 1 03/19/2019 14:12 NP Surr: Toluene-0 99.9 78.3-116 %REC 276110 1 03/19/2019 14:12 NP Surr: 4-Bromofluorobenzene 91.4 64.125 %REC 276110 1 03119/201914:12 NP Residue, Dissolved (TDS) by SM2540C Residue, Dissolved(TDS) 163 10 mg/L 275159 I 03/14/2019 13:20 AT Nitrogen, Ammonia (as N) E350.1 (El350.1) Nitrogen, Ammonia (As N) BRL 0.200 mg(L 275816 1 03/14/2019 10:34 JM Inorganic Anions by IC EPA 300.0 Chloride 35.9 1.00 mg/L R393186 1 03/131201916:10 GO Nitrogen, Nitrate (As N) 3.06 0.250 mg/L R393186 1 03/1312019 16:10 GO Hydrogen Ion (pH) by SM4500 H+ B pH 6.07 0.0100 H pH units R393166 1 03114/201910:47 BK Fecal Coliform (MF) SM9222D Fecal Coliform, (MF) BRL 4 H Colonies/too R393463 2 03/13/2019 16:28 TG red METALS,TOTAL SW6010D (SW3010A) Cadmium BRL 0.0050 mgiL 275948 1 03/18/201912:51 AJ Chromium 0.0176 0.0100 mg/L 275948 1 03/18201912:51 AJ Lead BRL 0.0100 mg/L 275948 1 03/19201912:51 AJ Z41C 0.0743 0.0200 m9/1- 275948 1 03118201912:51 AJ Qualifiers: s Value exceeds maximum contaminant level an Belowrepm6s, limit H Holding times for preparation or analysis exceeded N Anelyte net NELAC certified ➢ Analyte detected in the associated method blade > Greater f nn Result value e Estimated (value above quamitation range) S Spike Recovery outride limits due to matrix Na.. Seecoseuaomfive NC Notconfirmed < Leaathaa Resultvalue J Estimated value detected below Reporting Limit Page 13 of 48 SUBMIT FORM ONYELLQWL' PER ONLY . pEPa,AAy R�TM�t�np�E,NY�I�ON,-MEN�,�ByN�AL°RESO,I�RCEB�}k da�t� �yi a'�'� �.I�ti�. ATERQUALITYMONITORING:CE REPORT FORM '- ExpirationDate. 06-30-2022 ,at:'06-U-2UFORMPlease Prnt Fac Clearlyor Types PERMITNumber' Non Discharge WQ0005809 UIC Colonial Pi eline Compan : P Y NPDES '`Other (if different): TYPE OF PERMITTED OPERATION BEING MONITORED; ,ss 411 Gallimore Dai Road. '! (st eep 21409 r County Guilford " ❑ Lagoon ❑ Remediation: Infiltration Gallery Greensboro NO ❑Spray Feld ❑ Remediation: Sae) Telephone#: 336-669-7903 ❑ Rotary Distributor ® Land Application of Sludge Contact Person: Faron D. Leigh NO. wells to be sampled: 5 ❑Water Source Heat Pump ❑Other: Well Location/Site Name: Downgradient of ,, from P.,mR ,. If WELL SAMPLING INFORMATION MW-3� Date sample collected: i%� �.Z '/ i FIELD ANALYSES: �.a WAS DRY at WELL ID NUMBER (from Permit): Well Diameter: 2 in. pHl' ,S„� `units Temp.L C time of ' Well Depth: ; 39.50 ft. Depth to Water Level. 14 .�R.below measuring point Screened Interval: 38:5 ft. to 43.5 ft, Spec. 'COnd. µMhos - sampling, '. Measuring Point is •73 ft. above land surface - Relative M.P. Elevation: ft. Odor check here: Volume ofwater pumpetl/bailed before sampling::. .3 gallons"' Appearance El Samples for metals were collected unfiltered: RIYES ❑ NO and field acidifitd: ®YES: ❑ NO A60RATORV INFORMATION Date gLaboratoryName: Analytical Environmental Services Certification No. 562 °. Date.sample analyzed:' PARAMETERS NOTE: Values should reflect; dissolved and colloidal'_ concentrations. 'Pb - Lead mg/I 'e(Oz)asN mg/I mg/I NiNiCOD N m94 Zn-Zinc O mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as // , r/,j%.6 Coliform: MF Total I /1 o0m1 Phosphorus: Total as',P mg/I `- mg4 Other(Speci fy Compounds and Concentration Units):. (Note: Use MPN method for highly WrbidSamples) ,;}Orthophosphate Dissolved Solids: Total 7cmg/l-.AI -Aluminum m9/l , pH l(when analyzed) = units Ba - Barium mg/1 TOC mg/I Ca - Calcium ` mg/I Chloride�mg(I Cd- Cadmium Arsenic mg/1 ---Ling/I Chromium: Total mg/1 Grease and Oils mg4 ' Cu -Copper mg/I ORGANICS: (by.: GC, GC%MS,; HPLC) (Specify test and method #: ATTACH LAB REPORT.) Phenol mg4 ` mg/I Fe -Iron mg/1 Hg -Mercury mg/I ReportAttached? ' '® Yes (1) ❑ No (0) Sulfate Specific Conductance : µMhos 'K -Potassium mg4 VOC ,method # 5260 Total Ammonia ` mg/I Mg - Magnesium mg77 ,method # 777 (Ammonia Nitrogen; NHyas N; Ammonia Nitrogen, Total)_ ' mg 4 Mn -Manganese 9 , method # TKN as N ` mg4 Ni - Nickel mg/I ` ` , method # For Remediation Systems Only (AttachL Lab Reports):` Influent Total VOCS: %mg/L EffluentTOtal VOCs. + mg/L VOC Removal% . - • oil Brian L. Smith - Operations Manager SlAnaturs of Pennittee (or Authonzed Aaent) IDatel � " Name and TMe - Please punt or type Pertnittee (or Authorized ApenO Na GW-59`. Rev. 1/2007 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-3 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 9:00:00 AM Lab ID: 1903C14-003 Matrix: Aqueous Analyses Result lceporting Limit Qual Units Dilution BatchB) Factor Date Analyzed Analyst Volatile Organic Compounds by GUMS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug(L 276110 1 03/19/2019 14:41 NP 2,2-Dichloropropane BRL 0.50 ug/L 276110 I 03/19/2019 14:41 NP 2-Chlorotoluene BRL 0.50 ug/L 276110 I 03/19/2019 14:41 NP n-Butylbenzene BRL 0.50 ug/L 2761I0 1 03/19/2019 14:41 NP n-Propylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Dichlorodifluoromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Chloromethane BRL 0.50 ug/L 276110 1 03119/201914:41 NP Vinyl chloride BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Bromomethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Chloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Trichlorofluoromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP 1,I-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Methylene chloride BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP trans-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03119/201914:41 NP 1,1-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP cis-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03119/2019 14:41 NP Bromochloromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Chloroform BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP 1,2-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP 1,1,1-Trichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP 1,1-Dichloropropee BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Carbon tetrachloride BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Benzene BRL 0.50 ug/L 276110 1 03/19201914:41 NP Dibromomethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Trichloroethene BRL 0.50 u9/6 276110 1 03/19201914:41 NP Bromodichloromethane BRL 0.50 u9/1, 276110 1 03/19/2019 14:41 NP 1, 1,2-Trichloroethane BRL 0.50 ug/I, 276110 1 03/19/2019 14:41 NP Toluene BRL 0.50 ug/L 276110 1 03119/201914:41 NP 1,3-Dichloropropane BRL 0.50 ug/L 276110 1 03119201914:41 NP Dibromochloromethane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP 1,2-Dibromoethane BRL. 0.50 ug/L 276110 1 03/19/2019 14:41 NP Tetruchloroethene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP I, 1, 1,2-Tetrachloroethane BRL 0.50 119/1, 276110 1 03/19/2019 14:41 NP Chlorobenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Ethylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Bromoform BRL 0.50 ng/L 276110 1 03/191201914:41 NP Styrene BRL 0.50 ug(L 276110 1 03/19/2019 14:41 NP 1, 1,2,2-Tetrachloroethone BRL 0.50 ug/L 276110 1 03/192019 14:41 NP 1,2,3-Trichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Isopropylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Bromobenzene BRL 0.50 ug/L 276110 1 03/19/2019 14:41 NP Qualifiers: * Value exceeds maximum contaminant level E Estimated (value above Vantitation mange) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Holding times for preparation or analysis exceeded Nan Seecasenanetive N Analyze not NELAC certified NC Not ornamented B Analyte detected in the associated method blank < Less than Result value > Greater than Result value J Estimated value detected below Reporting Limit Page 14 of 48 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: NM-3 Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 9:00:00 AM Lab ID: 1903C14-003 Matrix: Aqueous xepornng Damara Analyses Result Qual Units BatchID Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GUMS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexacblorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Sort: Dibromofluoromethme 96.7 Sort: Toluene-d8 99.3 Surr: 4-Bromofluorobenzene 92.2 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 72 Inorganic Anions by IC EPA300.0 Nitrogen, Nitrate (As N) 0.376 Hydrogen Ion (pH) by SM4500 H+ B pH 6.58 Fecal Coliform (M 1) SM9222D Fecal Coliform, (W) BRL METALS, TOTAL SW6010D (SW5030B) 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 1441 NP 0.50 119/L 276110 l 03/19/2.01914:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 u9/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ng/L 276110 1 03/191201914:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 0.50 ug/L 276110 1 03/19/2019 14:41 NP 2.0 119/L 276110 I 03/19/2019 14:41 NP 76.4-125 %REC 276110 1 03/19/2019 14:41 NP 78.3-116 u/,REC 276110 1 03119/201914:41 NP 64-125 %REC 276110 1 03/19/2019 14:41 NP 10 mg/L 275159 1 03/141201913:20 AT 0.250 m8/1, R393136 1 03/13/201913:39 GO 0.0100 H PH units R393166 I 03/14/2019 10:47 BK 4 Cadmium BRL 0.0050 Chromium 0.0263 0.0100 Lead BRL 0.0100 Zinc 0.0203 0.0200 Qualifiers: a Value exceeds maximum contumiuent level BRL Belcvreporting limit H Holding times far preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value H Colonies/100 R393463 2 03/131201916:28 TG w (SW3010A) mg/[. 275948 I 03/181201912:53 AJ mg/L 275948 1 03/18/201912:53 AJ mg(L 275948 1 03/181201912:53 At mg/L 275948 1 03/18/201912:53 AJ E Estimated (value above gaamitnticn range) S Spike Recovery outside limits due to matrix Narr Sec case nmrative NC Notconflrmed < Less than Result value J Estimated value detected below Reporting Limit Page 15 of 48 GROUNDWATER.QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Cleadyo Facility Name: Colonial Pipeline Company Permit Name (if. different): ` Facility Address: 411 Gallimore Dairy Road Greensboro $"a�) NC 27409 (aty) (Stela) (=V) Contact Person: Faron D. Leigh Well Location/Site Name: Downgradient �AMPLIN INFORMATION WELL ID NUMBER (from Permit): MW-4 (MW-135) Well Depth' 29.5 fL Depth to Water Level;. /5`..i Oft. below measuring point Massuring "Point is 2 ft. above land surface volume of water pumped/bailed before sampling:l, X'Si2 gallc Samples for metals werecollected unfiltered: ®YES ONO'; 1 4BORATORY INFORMATION Datesample analyzed:` O��/� 1''ii/'u 6.� /q PARAMETERS NOTE: Values should reflectdis11 solved and coil COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml Phi (Note:. Use MPN method for highly turbid samp//les) Dissolved Solids: Total h mg/I pH (when analyzed)>' units TOC mg/1 Chloride mg/I Arsenic mg/I Grease and Oils ' mgfl Phenol mg/I Sulfate mgfl Specific Conductance µMhos Total Ammonia ` rng/I (M monla Nitrogen; NHaas N, AmmonisNitrogen Total) TKN as N mg/I For Remediation Systems, Only (Attach Lab Reports): Influet Brian LSmith - Operations Manager Permitteia (or Authonied Agent) Name and Title - Please Print or tube GW-59'. Rev. 112007 iBMIT FORM ONYFIIOW PAPER ONLY I� •", p�E�pil}1yigOFEN, Y1lo� MEN,ApRAL'�,RESO,/R ah YISIO ERrQU ;�a,�rW' �"' �i �L,'EjCH G ��99 1 w, one979 r 33322 PERMIT:�Number: I " Expiration Date: 'UU-30-2022 Non -Discharge W00005809 UIC NPDES ' Other I TYKE OFPERMITT,ED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery :ounty Guilford 0 Spray Field ❑ Remediation:. Dne#:336-669-7903 0 Rotary Distributor ® Land Application of Sludge )f wells to be sampled: 51 El WateriSource Heat Pump Other: If WELL ample collected: �a3 /a FIELD ANALYSES: ° WAS DRY at �. DRY WeILDiameter: in. pH', (units Temp. /„9 C time of _.2 ;reened Interval: 13 ft, to 28 LMhos ft. Spec. Cond. sampling, M.P. Elevation: ft. Odor Appearance check ' here: dacidified: ®YES ❑NO ,ry Name: Analytical Environmental Services Certification No. 562 tcentrations. (NO2) as; N m9/1 - mg/I Pb - Lead : t9, r7/�'' (NOs) as'N < 4, y . mg/1 �^t Zn - Zinc I �. (r/ �i �!/ mg/1 Total as'P mgn phosphate rig/I Other (Specify Compounds and Concentration Units):. Aluminum mg/1 la - Barium mg/I I -,Calcium mgA Cadmium �0•".�G mg/I niumi Total mg/l u = Copper mg/I i ORGANICS: (by GC, GC/MS, HPLC) Fe -Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) 1 Mercury mg/l Report Attached? ®; Yes (1) El No (0) Potassium mg/I VOC , method # 8260 4agnesium mg/I ,method # 4anganese mg/l , method # Ni - Nickel mg/I , method # CCs: )'mg/L EffluenTT.otal VOCs: '' mg/L VOG Removal% accurate, and complete, and that the laboratory analytical data was produced using app roved methods of analysis by a Imprisonment for knowing violations. .Signature of Penmttee (orAuthonzed'Agent) (Date) Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW4) Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 11:00:00 AM Lab ID: 1903C14-008 Matrix: Aqueous Reporting _ Dilution n.ngaca ouu Limit aguar �nua aanu:uFactor a" "ace AnmyzeU Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 2,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 2-Chlorotoluene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP n-Butylbenzene BRL 0,50 ug/L 276110 1 03/19/2019 18:25 NP n-Propylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Dichlorodifluoromethane BRL 0.50 ug/L 2761I0 1 03119/201918:25 NP Chloromethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Vinyl chloride BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Bromomethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Chloroethane BRL 0.50 ug/L 276110 1 03/1W201918:25 NP Trichlorofluoromethane BRL 0.50 1191L 276110 1 03/19/2019 18:25 NP 1,1-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Methylene chloride BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP trans-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 1,1-Dichloroethane BRL 0.50 u91L 276110 1 03/19/2019 18:25 NP cis-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Bromochloromethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Chloroform BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 1,2-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 1, 1, 1-Trichloroethane BRL 0.50 ag/L 276110 1 03119/201918:25 NP 1,1-Dichloropropene BRL 0.50 ug/L 276110 1 03/191201918:25 NP Carbon tetrachloride BRL 0.50 ug/L 276110 1 03/19/2019 M25 NP Benzene BRL 0.50 1191L 276110 1 03/191201918:25 NP Dibromomethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Trichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Bromodichloromethane BRL 0.50 4L 276110 1 03/19/2019 18:25 NP 1,1,2-Trichloroethane BRL 0.50 1191L 276110 1 03119201918:25 NP Toluene BRL 0.50 ug/L 276110 1 03/19/201918:25 NP 1,3-Dichloropropane BRL 0.50 ug/L 276I10 1 03/19/2019 18:25 NP Dibromochloromethane BRL 0.50 ug/L 276110 1 03/19201918:25 NP 1,2-Dibromoethane BRL 0.50 ug/L 276110 1 03119/201918:25 NP Tetrachloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Chlorobenzene BRL 0.50 ug/L 276110 1 03/19201918:25 NP Ethylbenzene BRL 0.50 USIL 276110 1 03/19/2019 18:25 NP Bromoform BRL 0.50 ng/L 276110 1 03119201918:25 NP Styrene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 276110 1 03119201918:25 NP 1,2,3-Trichloropropane BRL 0.50 ug/L 276110 1 03119/201918:25 NP Isopropylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 18:25 NP Bromobenzene BRL 0.50 ug2 276110 1 03/19/2019 18:25 NP Qualifiers: ' Value exceeds maximum contaminant level E Estimated (value ebovo cluantitation range) BRL Below reporting limit S Spike Recovery outside limits due to matrix H Bolding times for preparation or analysis exceeded Narr See case narrative N Atelyte not NELAC certified NC Notconfirmed B Analyze detected in the emaciated method blank < Less than Result value > Cheater than Result value I estimated value detected below Reporting Limit Page 24 of 48 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-135 (MW-4) Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 11:00:00AM Lab ID: 1903CA-008 Matrix: Aqueous nepertmg I/llutlon Analyses Result Qual Units BatchID Date Analyzed Analyst _ Limit Factor Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropme BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Sort: Dibromofluoromethme 95.8 Star: Toluene-d8 98.9 Surr: 4-Bromofluorobenzene 92.5 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 66 Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) BRL Hydrogen Ion (pH) by SM4500 H+B pH 5.72 Fecal Coliform (NIF) SM9222D Fecal Coliform, (MF) BRI METALS, TOTAL SW6010D Cadmium BRL Chromium 0.0268 Lead BRL Zinc 0.0620 Qualifiers: • Value exceeds maximum contaminant level BRL Belowceportinglimit * Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyle detected in the associated method blank > Greater than Result value (SW5030B) 0.50 ug/L 276110 1 03119/201918:25 NP 0.50 ug/L 276110 1 03119/201918:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 118/1, 276110 I 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/191201918:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 1191L 276110 1 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/19/2019 1825 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 ug/L 276110 1 03/19/2019 18:25 NP 0.50 u91L 276110 1 03/19/2019 18:25 NP 2.0 ug/L 276110 1 03/19/2019 18:25 NP 76.4.125 %REC 276110 1 03/19/2019 18:25 NP 78.3-116 %REC 276110 1 03/19/2019 18:25 NP 64-125 %REC 276110 1 03/19/2019 18:25 NP 10 0.250 mg/L 275159 1 03/14/201913:20 AT mg/L R393136 1 03/13201914:39 0.0100 H pH Units R393166 1 03/14201910:47 14101 W. 4 I-1 Colonies/too R393463 2 03/13201916:28 TG m1 (SW3010A) 0.0050 mg/L 275948 1 03118201912:55 AJ 0.0100 mg/L 275948 1 03/18/201912:55 At 0.0100 m9/L 275948 I 03/18/201912:55 AJ 0.0200 mg/L 275948 1 03118201912:55 AJ E Estimated (value above quantitation caused S Spike Recovery outside limits due to matrix Neu See case narrative NC Not wnarmed < Less than Result at. J Estimated value detected below Reporting Limit Page 25 of 48 GROUNDWATER QUALITYMONITORING: COMPLIANCE REPORT FORM FACIITY'INFORMATION Please Print Facility Name: Colonial Pipeline Company Permit Name (if different): Facility Address: 411 Gallimore Dairy Road Greensboro (sire.) NC - 214U (City) (stave) MIN Contact Person: Faron D. Leigh' Well Location/Site Name: DoWnoradient SAMPLING INFORMATION WELL IDINUMBER(from Permit): MW-6(MW-1 83)' Well Depth: 1 27.00 % Depth to Water Level:: 85 ft. below measuring point Measuring ,Point is " 1.5 ft. above land surface Volume of water pumped/bailedbeforesamplmg;s //4 'i. Sam lesfor metalswere collected unfiltered: ®YES -E Date sample analyzed; 0 X� thrrt 03 /5 PARAMETERS NOTE: Values should reflect dissolved ar :COD - mg/I Coliform: MF Fecal 1100m1 Coliform: MF Total /100ml (Note: t eWNmathodtorlNglly Wrbid Samples) Dissolved Solids: Total_ mg/I pH {when analyzed) ` units TOC mg/I Chloride " mgn Arsenic mg/I .'Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance f' µMhos Total Ammonia mg/I (Ammonia Nitrogen;.NHyas N; Ammonia:Nitrogen, Total) TKN as N mgA For Remediation Systems Only (Attach LabReports): i. Brian L. Smith - Operations Manager Permittee.forAuthorized AQent)Name and: Title Pleasepdntor Npe GW-59 Rev. 1/2007 unty Guilford -1 Spray Field ❑ Remediation: Rotary Distributor ® Land Application of Sludge :],,Water Source Heat Pump Other: If WELL, FIELD ANALYSES: WAS PH, J+_Z4-units Temp- L3 oC DRY ttime ft,. Spec. Cord. µMhos = sampling; Odor check ? Appearence here: Services Certification No. 562 Pb - Lead S®• mg/I Zn - Zinc mg/I Other (Specify, Compound=s—and=Connccentration Units): Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-183 (MW-6) Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 10:00:00AM Lab ID: 1903C14-009 Matrix: Aqueous uepornng utlutlon Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst Volatile Organic Compounds by GC/MS SW8260D (SW5030B) 1,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP 2,2-Dichloropropane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP 2-Chlorotoluene BRL 0.50 ug/L 276110 1 03119/201918:50 NP n-Butylbenzene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP n-Propylbenzene BRL 0.50 ug/L 276110 1 03/191201918:50 NP Dichlorodifluoromethme BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Chloromethane BRL 0.50 ugWL 276I10 1 03/19/2019 18:50 NP Vinyl chloride BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Bromomethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Chloroethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Trichlorofluoromethane BRL 0.50 ug/L 276110 I 03119/201918:50 NP 1,1-Dichloreethene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Methylene chloride BRL 0.50 ❑g/L 276110 1 03/19/2019 18:50 NP trans-1,2-Dichloroethene .BRL 0.50 ug/L 276110 1 03/192019 18:50 NP I,1-Dichloroethane BRL 0.50 rWL 276110 1 03/19/2019 18:50 NP cis-1,2-Dichloroethene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Bromochloromethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Chloroform BRL 0.50 ug/L 276110 1 03119/201918:50 NP 1,2-Dichloroethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP 1, 1, 1-Triclrloroethane BILL 0.50 ug/L 2761t0 1 03/19201918:50 NP I,1-Dichloropropene BRL 0.50 ugll 276110 1 03/19/2019 18:50 NP Carbon tetrachloride BRL 0.50 ug/L 276110 I 03/19/2019 18:50 NP Benzene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Dibromomethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Trichloroethene BRL 0.50 ug/I. 276110 1 03119201918:50 NP Bromodichloromethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP 1,1,2-Trichloroethme BRL 0.50 ug/L 276110 1 03/19201918:50 NP Toluene BRL 0.50 ug/L 276110 1 03/19201918:50 NP 1,3-Dichloropropane BRL 0.50 ug/L 276110 1 03119201918:50 NP Dibromochloromethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP 1,2-Dibromoethane BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Tetrachloroethene BRL 0.50 ug/L 2761L0 1 03/19201918:50 NP 1, 1, 1,2-Tetrachloroethane BRL 0.50 ug/L 276110 I 03/19/2019 18:50 NP Chlorobenzene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Ethylbenzone BILL 0.50 ug/L 276110 1 03/19201918:50 NP Bromofonn BRL 0.50 ug/L 276110 I 03/19/2019 18:50 NP Styrene BRL 0.50 ug1L 276110 1 03/19/2019 18:50 NP 1, 1,2,2-Tetrachloroethane BRL 0.50 ug/L 276I10 1 03/19/2019 18:50 NP 1,2,3-Trichloropropane BRL 0.50 ugJL 276110 1 03/19/2019 18:50 NP Isopropylbenzene BRL 0.50 ug/L 276110 1 03/191201918:50 NP Bromobenzene BRL 0.50 ug/L 276110 1 03/19/2019 18:50 NP Qualifiers: ' Value exceeds maximnmcantanamontlevel BRL Below reporting limit H Holding times For preparation or analysis exceeded N Analyte not NELAC assured B Analyte detected in the associated method blank > Greater than Result value E Estimated (value above quontitation range) S Spike Recovery outside limits due to matrix Non See case..five NC Not con armed < Less than Result veto. I Estimated value detested holow Reporting Limit Page 26 of 48 Analytical Environmental Services, Inc Date: 21-Mar-19 Client: Colonial Pipeline Client Sample ID: MW-183 (MW-6) Project Name: Greensboro Quarterly Sampling Collection Date: 3/12/2019 10:00:00 AM Lab ID: 1903C14-009 Matrix: Aqueous ueportang Dilution Analyses Result Quill Units BatcbH) Date Analyzed Analyst Limit Factor Volatile Organic Compounds by GC/MS SW8260D 4-Chlorotoluene BRL 1,3,5-Trimethylbenzene BRL tert-Butylbenzene BRL 1,2,4-Trimethylbenzene BRL sec-Butylbenzene BRL 1,3-Dichlorobenzene BRL 1,4-Dichlorobenzene BRL 4-Isopropyltoluene BRL 1,2-Dichlorobenzene BRL 1,2-Dibromo-3-chloropropane BRL 1,2,4-Trichlorobenzene BRL Naphthalene BRL Hexachlorobutadiene BRL 1,2,3-Trichlorobenzene BRL Xylenes, Total BRL Sort: Dibromofluoromethane 97.6 Surr: Toluene-d8 100 Surr:4-Brornofluorobenzene 92.4 Residue, Dissolved (TDS) by SM2540C Residue, Dissolved (TDS) 94 Inorganic Anions by IC EPA 300.0 Nitrogen, Nitrate (As N) BRL Hydrogen Ion (pH) by SM4500 H+B pH 5.32 Fecal Coliform (MIT) SM9222D Fecal Coliform, (MF) BRL METALS, TOTAL SW6010D (SW5030B) 0.50 ug/L 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 1 03/191201918:50 NP 0.50 ug/L 276110 1 03/19/201918:50 NP 0,50 ug/L 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 I 03/19/201918:50 NP 0.50 118/1, 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 1 03/19/201918:50 NP 0.50 ug/L 2761I0 1 03/19/201918:50 NP 0.50 119/L 276110 1 03/19/2019 18:50 NP 0.50 119/1, 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 1 03/19/201918:50 NP 0.50 ug/L 276110 l 03119/201918:50 NP 0.50 ug/L 276110 1 03/19/201918:So NP 2.0 u9/1, 276110 1 03/19/201918:50 NP 76.4-125 %REC 276110 1 03/19/201918:50 NP 78.3-116 %aREC 276110 1 03/191201918:50 NP 64-125 %REC 276110 1 03/19/201918:50 NP 10 mg/L 275159 1 03/14/2019 13:20 AT 0.250 mg/L R393136 1 03/13/2019 14:09 GO 0.0100 H pH Units R393166 1 03/14/201910:47 BK 4 Cadmium BRL 0.0050 Chromium BRL 0.0100 Lead BRL 0.0100 Zinc BRL 0.0200 Qualifiers: ' valueexceeds maximmnconmmmeat level BRL Belowreportmg limit H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value I -I Colonies/100 R393463 ml (SW3010A) mg/L 275948 mg/L 275948 mg/L 275948 mg/6 275948 2 03113/201916:28 TG 1 03/18/2019 1158 AJ 1 03/18/2019 I2:58 At 1 03/18/2019 12:58 AJ 1 03/19/2019 I2:58 AJ E Estimated (value above quamitaimn range) 8 Spike Recovery outside limit due to main. Non See case narrative NC Not confirmed < Less than Result value 1 Estimated value detected below Reporting Limit Page 270t 48