NCG020354_COMPLETE FILE - HISTORICAL_20180221

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
1V C& Da Q 3�5V
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ CAI O () as
YYYYMMDD

Green Meadow, LLC
February 14, 2018
North Carolina Department of Environmental Quality
Division of Water Resources
ATTN: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2017 Wastewater Monitoring Results!
Brickhaven Mine No. 2 Tract "A":
Permit No. NCG020354
Chatham County, North Carolina
To Whom It May Concern:
D
Please accept two copies of the 2017 annual documentation submittal for wastewater permit
compliance for the Brickhaven Mine No. 2, Tract "A" (Brickhaven) site in Chatham County, North
Carolina, governed by NPDES Permit No. NCG020354.
Included with this submittal you will find the annual DMR report form for the analytical data. "No Flow"
conditions were observed for the first quarter while wastewater discharge occurred during the second,
third and fourth quarters of 2017 at Mine Pit Outfall 1 (MP01). No constituents were detected above
their respective benchmark levels during any of the quarterly monitoring periods of 2017. Analytical
reports from each quarterly monitoring event have also been included in this submittal package in
addition to the daily dewatering logs.
Based on the analytical results received from the second, third and fourth quarterly monitoring periods
of 2017, Brickhaven will continue analytical monitoring on a quarterly basis at MPOI.
Please feel free to contact me at [phone] or [e-mail] with any questions or concerns
you may have.
Sincerely,
N4rnn E.Divers, III
Director of Engineering, Environmental and Quality
Attachments: Annual Summary Discharge Monitoring Report (DMR) - Wastewater
2017 Quarterly Analytical Data
2017 Daily Dewatering Logs
Cc: Brickhaven Mine No. 2 Tract "A"
File
Green Meadow, LLC • 12601 Plantside Drive • Louisville, Kentucky 40299
0: 502-245-1353 • F: 502-245-7398

RESEARCh & ANA[YACA1
`L UbORATORIES, INC.
Analytical/Process Consultations
07 July 2017
Mr. Kyle Hoover, P.E., P.G., PMP
Environmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Mine Lake discharge analysis for the sample collected at the
Brickhaven site identified as MPOI on 29 June 2017. If you should require any additional information or
have any further questions concerning the information contained in this report please feel free to contact me
at 336,996.2841 or inI'onrandalabs.com,
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short Street • Kernersville, North Garalina 27284 • 336.996-2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANAiyTICA[
LAbORATORIES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
7/7/2017
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in NC 9t34 z. t11
NC937701
Client Sample 10: Mine Lake Discharge MP01 Lab Sample ID: 36582-01
Site: Brickhaven Collection date: 6129/2017 10:40
Parameter Method Result Units Rep Limit An,alyst Analysis 0atelTime
pH SM 4500 H+B-2000 6.64 Std, Units 6/29/2017
Settleable Matter SM 2540 F-1997 <0.1 m111 0.1 AA 6/30/2017 1445
Total Suspended Solids (fSS) SM 2540 0-1997
Turbidity
EPA 180.1
16.1 mg/L 2.5 AA 715/2017
30.8 SITU 1 AA 6/30/2017 1517
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www,randalabs.com Page 1

RESEARCh & ANA[yTICA[
r.� LAWRATORIES, INC.
Analytical J Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
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RESEARCh & ANA[yTICA1
LABORATORIES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (1) water samples were received in good condition on 30 June 2017.
The sample was analyzed without difficulties unless noted below.
Sidney L. Champion
Director of Laboratory Services
Date
P.Q. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 • 336.996-2841 • Fax [phone]
www.randslabs.com

RESEARCh & ANA[yTICA[
LABORATORIES, INC.
AnalyticallProcess Consultations
01 September 2017
Mr. Kyle Hoover, P.E., P.(j., PMP
Environmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Mine Lake discharge analysis for the sample collected at the
13rickhaven site identified as MP01 on 24 August 2017. 11'you should require an), additional information or
have any further questions concerning the information contained in this report please f-ecl free to contact me
at 336.996.2841 or info a,randalabs.com.
Best Regards,
Sidney L. Champion
EXCClrtiVe Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P 0. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANA[Y-riC 1
LAORATORiES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
9/1/2017
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NCU37701
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Client Sample ID: MP01 Lab Sample ID: 39206-01
Site: Brickhaven Collection Date: 8/24/2017 15:29
Parameter Method Result Units Rep -Limit Analyst Analysis Date/Time
pH SM 4500 H+13-2000 6.39 Std. Units 8/24/2017
Settleable Matter
SM 2540 F-1997
<0.1
ml/I
0.1
AA
8/25/2017 1400
Total Suspended Solids (TSS)
SM 2540 D-1997
3.5
mg/L
2,5
AA
8/30/2017
Turbidity
EPA 180,1
5.41
NITU
1
AA
8/25/2017 1530
NA = not analyzed
�O. Box 473 1 66 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com _ v Page 1
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- -• RESEARCh & ANA1yTICA1
h LAbORATORIE5 INC.
AnaWcal / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
I few
MM�m-
MEN
IMEMIN

RESEARCh & ANAyTiCAI
LAbQRATWES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (1) water sample was received in good condition on 25 August 2017. The
sample was analyzed without difficulties unless noted below.
Sidney L. Champion
Director of Laboratory Services
01- I-1-,�
Da to
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-995-2641 • Fax [phone]
www.randalabs.com

IRESEARCh & ANA1yTICA[
LAbORATORIES, INC.
Analytical/Process Consultations
12 October 2017
Mr. Kyle Hoover, P.E., P.G., PMP
Environmental Protection Specialist III
Charah, LLC;
435 South 'Tryon Street
Suite 180
Charlotte- NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy of the Mine Lake discharge analysis for the sample collected at the
Brickhaven site identified as M1101 on 05 October 2017. 11'you should require any additional information or
have any further questions conccrilintg the information contained in this report please fecl free to contact me
at 336.996.2841 or info (c randalabs.com.
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Sox 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996.2841 • Fax [phone]
www,randalabs.com

9(ESEARCh & ANA1yTiCA[
LAbORAT®RiES? INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
10/12/2017
�psuuiiiy
NCtl34
NCH37701
..........
!*`ED AN1`1V
Client Sample 10: MP01 Lab Sample 10: 41107-01
Site: Brickhaven Collection Date: 10/5/2017 10:04
Parameter Method Result Units Rep Limit Analyst Analysis Dateliime
pH SM 4500 H+13-2000 6,01 Std. Units 10/5/2017
Settleable Matter SM 2540 F-1997 <0.1 ml/I 0.1 AA 10/6/2017 1500
Total Suspended Solids (i'SS) SM 2540 D-1997
Turbidity
EPA 180.1
3.5 mg/L
9,48 NTU
2.5 AA 10111 /2017
1 AA 10/6/2017 1600
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www,randalabs.com Page 1
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RESEARCh & ANAIyTiCAI
UbowoRiES, INC.
Analytical / Prooess Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
water/ Wastewater
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RESEARCh & ANAtyTICAt
LABORATORIES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (1) wvater sample was received in good condition on 06 October 2017.
The sample was analyzed without difficulties unless noted below.
Sidncy L. Champion
Director of Laboratory Services
10-12-tl
Date
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336.996-2841 • Fax [phone]'
wmv.randalabs.com

Part A Continued: Wastewater Monitoring Requirements
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MAll L ORIGINAL ANI) ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO _DISCHARGE" & I-INIIT
VIOLATIONS! BY MARCH 1 OF EACH YEAR TO:
Division of Water QualitN'
Attu: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
(91R)S07-6379
YOU A1t/4T SIGN THIS CF_RTIFIC4TION FOR ANY INFORMATION REPORTED:
"I certify, tinder penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquire of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief. true. accurate, and complete.
I am aware that there fwp ciunirrnant pep I�es for submitting false information, including the possibility of fines and imprisonment for knuwing violations."
attire
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Permit fate: I/P?010-1?/31/2014 Last Kevised 07-02-1 1
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Part A Condt-tued: Wastewater Monitoring Requirements
Outfall No..
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VIOLATIONS) BY MARCH I OF EACH YEAR TO:
[division of Water Qualitv
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
( A 19) 907-6371)
YOU AI U U SI GA' TH IS CERTI FI CA TION.FOR ,AN f' IIVFURALMON REPORTED:
"i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knuwledge and belief', true, accurate, and complete.
t am aware that thnrr %rr civnifoant neo tar es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Si aturc of crmittee�
'a- n,
(Date)
Permit Datc; 1 /1 /2010-12/31 /2014
Last Kevised 02-02-1 1

Part A Conii7nued. Wastewater Monitoring Requirements
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iJMAIL ORIGINAL AND ONE COPY OF THIS ANNUA-L SUMMARY (INCLUDING ALL "NO FLOW","NO DISCHARGE " & LLNUT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Atin: DWQ Central Files
1 61 7 ,Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST SIGN THIS CERTI FIC4 TION FOR ANY INFORMATION REPORTED:
"I certify, under penaity of iaw, that -this document and all attachments were prepared under my direction or supervision in accordance ,vith a �,ystert designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons .Oho manage the system, or
those persons directly responsible for gather
ing the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there ssre ciuniftioant rjev Sies for submitting false information, including the possibility of fines and imprisonment for knowing violations."
_ )
(Sig azure of P mitteet (Date)
Permit Date: 1/1/2010-12/31/2014 Last Revised 02-02-1 1

Part A Continued: Wastewater Monitoring Requirements
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VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water QualitN
Attu: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 2-7699-1617
[phone]
YO U Al U.4T SIGN THIS CER TI FIC4 TION FOR .4 iV I' IrVFORAbI TIVN REPORTED:
"i certify, under penalty of law. that this document and all attachments were prepared under my direction or supervision in accordance .rich a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry, of the person or persons who manage the systern, or
those persons directly responsible for gathering the information, the infortnution submitted is, to the best of my knowledge and belief, true. accurate, and complete.
I am aware rhat ihPrn swp cinniAwnt peoi 'tyres for submitting false information, including the possibility of Fines and imprisonment for kno►ving violalions."
1�1 -iul
(Signa re of Permittee) (Date)
Pennit Date: 111!?010-13/3I/'014 Last Kevised 021-02-1 1
V�,r 3 ut-_'

Part A Continued: Wastewater Monitoring Requirements
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VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Qualit}'
Attn: DWQ Central Files
1617 klail Service Center
Raleigh. North Carolina 27699-1617
(919) 807-6 79
YOU AIUVT SIGN THIS CERTIFICATION FOR AIV I' IIVFORAMT1ON REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Bused on my inquiry of the person or persons who manage the system. or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true.. accurate. and complete.
I am aware ihar ,hare+ swp cipnif4wnt DCV911 es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Sig ture of Permittee) (Date)
Permit fate: 1/1/2010-12/31l2014 Last Ke�ised 021-02-1 I
P:n,r , $If"

Part A Continued: Wastewater Monitoring Requirements
Outfall No::
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Division of Water Quality
Attu: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
Y (INCLUDING ALI, "NO FLOW". "NO DISCHARGE— S. LltMIT
V0tJ;11U.4TSIGtV THIS CERTIFICATION FOR : tN)' IrVFURtt1-tTPU.N REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who tnanage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of m}v knowledge and belief. true. accurate, and complete.
at
I am aware ththere arr civnifmnt peo fetes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(, gnature oVPermittee) (Date)
Permit Date: i/1/_'010-12/31/?Old Last Ke,,ised 02-U•'-1

Part A Continued: Wastewater Monitoring Requirements
Outfall No.
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VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Qualit,
Attn: DWQ Central Files
1617 !Hail Service Center
Raleigh, North Carolina 27699-1617
(()19) 807-6379
l'Of! ,11111 .SIGN THIS CERTIFICATION FOR ANY INFORAIA'1'LON REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system. or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that therr :wp cinnirtwnt pev6Wl s for submitting false information, including the possibility' of tines and imprisonment for knowing violations."
S 1-
(Si nature o ermittee) (hate)
Permit hate: 1/1/3010-12131/2014 Lass Revisvd 02-02- 1 1

Part A Continued: Wastewater IVlonitoring Requirements
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VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Atut: DWQ Central Files
1617 i1ail Service Center
Raleigh. North Carolina 27699-1617
t9}9}507-6379
YOU MU.VT SIGN TIIIS CERTI FICATION FOR ANY INFORAi.-1 TION REPORTED.
"I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance with ,t system designed to
assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry ofthe person or persons -*.ho manage the system. or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and cornpicle.
I am aware tha+ thorP %;we iiani*wnt petlat�es for submitting false information, including the possibility of tines and imprisonment for knowing violations."
(S nature rmitreej
�; - //---! 7
(Date)
Perm it Date: 1 / 1120 10- 1213 1 /2014
1-List Krvised 021-02-1 1
piwr , fit"

Part A Confinued: Wastewater Monitorinp Reauirements
Outfall yin,,
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH.].OF EACH YEAR TO:
Division of Water Quality
.Attu: DWQ Central Files
1617 (Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU r1IU.ST SIGN THIS CERTIFICATION FOR ANY INFORA?A71ON REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance %sith a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquire of the person or persons tivho manage the system. or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that th,-rn —P civniftoant pevgOes for submitting false information, including the possibility- of fines and imprisonment for knots-ing violations."
Y-
tSign ture of Permittee)
<;-I)-r
(Da te)
Permit fate: 1/1/2010-12/31/2014
Last Revised 02-02-1 !

Part A Can iuued: Wastewater Monitoring Requirements �t0i
Oatfall No.
• �f"�
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" K LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR _TO -
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
YOU i1.1UST,SIGN THIS CERTIFIC4TION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance ti►ith a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons .rltu manage the system. of
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true. accurate, and complete.
I am aware thAt rh— swP Of niAwnt neu6@es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Si n lure oflermwee) (Date)
1;
Permit Date: l/l/2010-1-2/3112014 Last Kraised 02-02-11

Part A Continued: Wastewater Monitoring Requirements -�SNr< -zoF7
Outfall No.
rDat12 Satn It:,r'� 'r
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY INCLUDING ALL "NO FLOW","NO DISCHARGE" & LIINIIT
VIOLATIONS) BY MARCH I OF EACH YEA1_2 T. ):
Division of Water Quality
Aun: DWQ Central Files
1617 Mail Service Center
ltaleiQh, North Carolina 27699-1617
[phone]
YOU AILISTSIGA' THISCERTIFICATIOA' FORAJVYINFORAI.9TIOAV REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance ►vith a system designed iv
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief', true, accurate, and complete.
I am aware that thrry tiro, civnLAwnt netTa'l� for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Sign titre of ermittee) (Date)
Permit 17ate: 111/22010-12/31-?014 Last Revised 02-0-1-1 1
pHo ; nt' 1

Part A Continued: Wastewater Monitoring Requirements -::�JV ',Zc? 17
Outfall No.-
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MAFL ORIGINAL AND ONE, COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" K LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO;
Division of \kater QualitIv
Atin: DWQ Central Files
1617 Mail Semite Center
Raleigh- North Carolina 27699-1617
{919) S07-6379
YOU ,t'IUV T SIGN THIS CERTI FICATION FOR A'NY INFOR,1a 9 TION REPORTED. -
"I certify, tinder penalty of law, that this document and all attachments were prepared under my direction or supervision in accurdance with a systctn designed to
assure that qualified personnel properly gather and evaluate the information submitted. based on my inquiry of the person or persons %vhv inanage the systein, ,ir
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and helief', true, accurate, and complete.
i am sw3re.. that tharr %rr 6vnifioant ne altyeS for submitting false information, including the possibility of fines and imprisonment for kno-tving Violations."
(Signs urc of P�ittee) (Date)
Permit Date: 1111?010-12'1311201 } Last Kvvised 02-02-1 1
P ,v i of-2

Part A Continued: Wastewater Monitoring Requirements l-„(y 2Q 1-7
Outfatl No.
r�
Date Semple,x
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MAFL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
V E(ILATIONS) BY MARCH 1 OF EACH YEAR TO:
Division of Water Quality
Attu: DWQ Central Files
1617 \lail Service Center
IlaleiQh, North Carolina 27699-1617
[phone]
}'OU ,11UST SIGN THIS CERTIFICATION POR.41V )' INFORAI.4TION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons ,rho manage the system, ur
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief'. true, accurate, and complete.
I am aware. that thorP uri ciuniftmint pea6l '`oes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signatu c of Permittee) (Date)
Permit hate: 1/l/2010-12/3112014 Last Kevised 0-1-02-1 1
I>;m r i of "

Part A Conlinued: Wastewater Monitoring Reauirements
Outfall No.,
*Date'Satnpie ,'�TtalSEl�w�,'
�> C4ffe'cied13:���ri�I�hiSoilds
K
,���'O ns ndedr '
.
'Tiit•bidity3
r
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Standard'
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—
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G `;' 117
�-
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE!' & LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
Ann: DWQ Central Files
1617 Mail Service Center
Raleigh. North Carolina 27699-1617
[phone]
YOU AI AU SI GN THIS C'ERTI FICA TION FOR ANY INFORAM T ION REPORTED:
"I certify, under penalty of law, that this document and all attach ments.were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and.evaluate the information submitted. Based on my inquiry of the person or persons who utanage the system. or
those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware. ttiat tharo are cipni&asnt pe altws for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Si nature �ferfllilleC)
g
ia9..l 7--
(Date)
Permit Date: I / 12010-1 /3 112014
L�tsl Revised 02-02-1 1

Part A Continued: Wastewater Monitoring Reuuirements
Outfeli No.,
DateISample t
- 't
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-
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" b_: LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
i)ivision of Water Qualitti,
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh. North Carolina 27699-1617
[phone]
YOL;AIUSTSIGNTHIS CERTIFICAT1OiVFOR: iVYINFORh1.9TJOVREPORTED:
"I certify, under penalty of law, that this document and all.attachments were prepared under my direction or supervision in accordance ►+ ith a system designed to
assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system. or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true. accurate, and complete.
I am aware. t", %-P aianikoant pet4'taes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Si naturje fPermittee)
(Date)'/„t�
Permit Date: 1/112010-1213112014
Lest Revised
Pare ; of

Part A Continued: Wastewater Monitoring Requirements
Outfall l,Ia.;
;Date 5s�ieY ��
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_09-12N
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH YEAR TO:
1?ivision of Water Quality•
Attn: DWQ Central files
1617 NIail Service Center
Raleialz- North Carolina 27699-1617
(919) o' -6379
YOU MUST SIGN THIS CERTIFICATION FOR ANY LNFORA1A77UN REPORTED. -
"I certify, under penalty of law, that this document -arid all attachments were prepared under my direction or supervision in accordance ►with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted- Based on my inquiry of the person or persons who manage the S)•stem, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true. accurate, and complete.
I am aware that thPrr :wp rdt nifi ant ye s for submitting false information, including the possibilih• of fines and imprisonment for knosving violations."
(Sign tore of Permittee) (Date)
Permit Date: 1!1l2010-12/31/201d Last Kevised 02-02-1 1
Paae = of

Part A Continued: Wastewater Yionitoring Requirements e0e, , 10r
Outfall No.
ADttte"NBMpie
-:-Colftedts�x��=ail-1�'g�
zTtttellkliiw
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-
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C<< 7
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" 8; LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quaiit-'
Aun: DWQ Central Files
1617 Mail Servicc Center
Raleigh. North Carolina 1-7699-1617
[phone]
YOU AI LWT SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance vo ith a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons -who manage the system, ur-
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, tr•ur, accurate. and complete_
am aware that thPrd, %we 6pniflwnt pe slues for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(S nature oCermiltee)
( Date)
Permit fate: 1/]/-2010-1-'/3112014
1-asl Revised 03-0'--1 1
i'�„�, 3 ol•,

Part A Cowhiued: Wastewater Monitoring Requirements ` c tc e- 4,,) -7
Outfall No.,'
nDIIi S1� IC it
t . �3
G011ected �
4'�6
r .:ems r�
Tial'low�
- r ����
��
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r
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2
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co!/ml"'
HI t
/ e / 7
—
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW", "NO DISCHARGE" � LIMIT
VIOLATIONS) BY AIARCH I OF EACH YEAR TO:
Divislon of Water Quality
Attn: DWQ Central Files
1617 \•lail Service Center
KaleiQb. North Carolina 27690-1617
[phone]
V011 AIU.ST SIGN THIS CERTIFICATION FOR AN}• INFORAIATION REPORTED: _
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a swstern designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons whu manage the system• or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that thorn sire csnnifroant pepDees for submitting false information, including the possibility of fines and imprisonment for knv►wing violations."
(Sign titre of Permittee) (Date)
Permit mate: 1/1/2010-1?hlr'2014 Last Kevised 02-02- 1 1

Part A Cants sued: Wasteivater Monitoring Requirements 9, .- a i 7
Outfall NO.
� �•
'�...���rd
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MAIL ORIGINAL AND ONE COPY OF •fHIS ANNUAL SUMMARY (INCLUDING ALI., "NO FLOW". "NO DISCHARW— &- LfNTIT
VIOLATIONS ICY A-1ARCII 1 OF EACH YEAR TO:
Division of Water Quality
Atin: DWQ Central Files
1617 Mail Service Center
Raleigh. North Carohna 27699-1617
(`) l 91 407-6379
YOU rtIUST SIGN TIIIS CERTI FICATION FOR ANY INFORAIr1 TION REPORTED:
"I certify, under penalty of lacy, that this document and all attachments were prepared under my direction or supervision in accordance ►vitlh it system designed to
assure that qualified personnel properhgather and evaluate the information submitted. Based on in}' inquiry of the person or persons v-ho nnanare the s}•stein, Of
those persons directly responsible for gathering the information. the information submitted is, to the best of my knowledge and belief, true. occuratc, and cornplcti•-
I am aware. That th—I —P rinniGQant nepatlies for submitting false information, including the possibility of lines and imprisonment for knowing violations."
-r
(Sign lure 6�rfar—mittee) (Date1
Permit Date: 1l1/2010-I2/3Ii3014 Las[ Kevised0-1-U-1-11
U...,,., - ..f'-�

Part A Continued: Wastewater Monitorine Reuuirements 2D/-7
Outi811 No.
Uati?'Satt►ple r
Colkt
• --++;t.Y.. :?ir�r-FM,f
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// I 17
61
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7
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11117117
MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY i1NCLUDING ALL "NO FLOW", ---NO DISCHARGE" & LIMIT
VIOLATIONS) BV MARCH_ I OF EACH_YEAR.TO:
Division of Water Quality
Attn: DWQ Central Fiies
1617 Mail Service Center
Raleigh, North Carolina 2-7699-1617
[phone]
YOU AMUSIGN THIS CERTIFICATIOiV FOR ANY LNFORAIATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my.knowledge and belief'. trur, accurate, and complete.
I am aware that thi-rp swe 6ontlaoant pep E�es for submitting false information, including the possibility of fines and imprisonment for knuNving violations."
(Si9 ature of Permittee)
/1.- 1 Z-/
(Date)
Permit flare: 1/1/?010-1?/31/201-t
Last Krvised 0_'-02-1 1

Part A Continued: Wastewater illonitoring Requirements A1vyr h,.,_ �ej-7
Outfall No..
•
•Date Sam le :
�- ,., x,t
-s^-s.Ci3llected��R•Solids
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW". "NO DISCHARGE" & LIMIT
VIOLATIONS) BY MARCH 1 OF EACH H YEAR TO:
Division of Water Quality
,Nun: DWQ Central Files
1617 Mail Service Certler
Raleigh, North Carolina 27699-1617
[phone]
YOU MUST MGt`' THIS CERTIFICATION FOR ANY INFORA7.471ON REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under ms direction or supervision in accordance with a systrm deigned to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the systcm. ur
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief. true, accurate, and complctc.
I am aware tl.at thorn arr ci�niftoant pet al�ftes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(SiNntuneofZoemittee)
L� -1
(Date)
Permit Date: I/1/'_010-1 131/2014
Last Kc% iced 0-1-U2- I I

Part A Conlinued: Wastewater Monitoring; Requirements /eCr,..l1z, 2017
Qutfall No.
,
,•
DsteySstnple, � .r
-Coflctetl _,
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY (INCLUDING ALL "NO FLOW-, "NO DISCHARGE" &- LIMIT
VIOLATIONS) BY AIARCll I OF EACH YEAR TO:
Division of Water Quality
Attn: DWQ Central Files
1617 Mad Service Center
Raleigh, North Caroiina 27699-1617
[phone]
YOU MUSTSIGN THIS CERTIFICATION 1"OR ANf' INFORMATION REPORTED:
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons vvho manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete_
I am aware that cionifinant neuQues for submitting false information, including the possibility of fines and imprisonment for knu%ving violations."
(Si nature o rermittee)
(Date)
Permit Dace! I / 1 /2010-12/31 /201 a
Last Revised 02-02.1 1
13--, . - -

Part A Continued: Wastewater Monitoring Requirements bece';, P-01-7
outfalt No.
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MAIL ORIGINAL AND ONE COPY OF THIS ANNUAL SUMMARY JINCLUDING ALL "NO FLOW"',—NO'DISCHA.R(:E'' S- LIMIT
VIOLATIONS) BY MARCH I OF EACH YEAR TO:
Division of Water Quality
,tun: D Q Central Files
1617 klail service Center
Raleigh, North Carolina 27699-1617
0 101 807-Fi_3 79
YOV AI U.ST SIGN THIS CF. RTI FICA TION FOR AN Y I.NFURAL4 TION REPORTED:
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance %001 a vslcrn dc,igned to
assure that qualified personnel properly gather and evaluate the information submitted.. Based on my inquiry of the person or persons vi lio utanage the System, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief: true, aCCur-ate, and coruplete.
I am aware tlwr fhnro iwr ciunirinant neo��eS for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(, gnature of Permittee}
(Date)
Permit mate: 1/I/2010-12/31/2014

11 ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — WASTEWATER
SUBMIT TO CENTRAL OFFICE*
General Permit No. NCG020000
Calendar Year - 2017
"Report ALL WASTEWATER monitoring data on this form (include "No Flow"1"No Discharge" and Limit Violations) from
the previous calendar year to the DEQ by MARCH 1 of each year.
Certificate of Coverage No. NCG02 ®0 5❑®
Facility Name: Brickhaven No. 2 Mine Tract "A"
County: Chatham
Phone Number: ( 704 ) 731-2300 Total no. of outfalls monitored 1
Certified Laboratory Research 8i Analytical Laboratories, Inc. Lab # 34
Lab #
Wastewater (WW) Discharge Outfall No. MP01
Is this an industrial sand mine (See 40 CFR §436 Subpart D)?
Yes ❑
No
Does this outfall discharge WW to SA waters?
Yes ❑
No ❑X
Does this outfall discharge WW to SB or PNA waters?
Yes ❑
No X❑
Does this outfall discharge WW to HQW or ORW waters?
Yes ❑
No ❑X
If so, what is the 7Q10 flow rate? or Tidally influenced
waters,
7Q10 not available ❑
Does this outfall discharge WW to Trout (Tr) designated waters?
Yes ❑
No ❑X
Were there any limit violations in the calendar year?
Yes ❑
No E]
Outfall No:
MP 1
Daly Flow
Rate, cfs
-.'. ..<.:..�:,.
pH,'
SlJ
.:
TSS,°
mg11
.. fi::: ' .
�SSr
mill
lfapplicabl¢
Discharge x
,,� :
Turbidity, ,
NTU "
' Upstream
3��R �ti ,
(U) fTurbidity,r
n. -
..,'NTU `.
D:ownStream .
w , , 1..
(D) Turbidity,;
NTU I
Fecal '.
Coliform 7.
co11.100. no
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Effluent
Limitations
Mo. Ave ! Doily Max.
HOW or ORW
50% of
7Q10
Indicate NO FLOW
If applfca6le
freshwater
6.0-9.0
saltwater
6.8-$.5
v
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25145
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20130
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and Tr or PNA
10115
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SA, 513, PNA,
or any Trout
U.110.2
No Limit
Circle Water
Quality Standard
appliesA
5U 25110
NIA
Water Quality
Standard applies
,
NIA
Water Quality l
Standard applies
,
NIA
Date ,Sample
Collected,
mo4dlyr
Period 1
No Flow
NIA
NIA
NIA
NIA
NIA
NIA
NIA
06/29/2017
0.557
6.64
16.1
<0.1
30.8
NIA
NIA
NIA
08/24/2017
0.557
6.39
3.5
<0.1
5.41
N/A
NIA
NIA
10/05/2017
0.668
6.01
3.5
<0.1
9.48
NIA
NIA
NIA
Permit Date 101112015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 q 3❑ S❑®
CERTIFICATION
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Required by 40 CFR §122.221
Signature
Date 02114/2018
� � o,gnsursiy�edwNo,m.�nOrves
y/hry o=cnsca—, L u-uaerneil=ndwe,:�ha�.h,ca�„_=us
OaSe. 2019 03.1 a 03 32, 36-05'00'
Mail Annual Summary Wastewater DMR to the NCDEQ Central Office:
Note the address is correct — Central Files is housed in DWR (not DEMLR)
N.C. Department of Environmental Quality (DEQ)
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files Telephone [phone]
Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at:
[phone]
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

reen Meadow,_LLC
� February 14, 2018
North Carolina Department of Environmental Quality
Division of Water Resources
ATTN: DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2017 Stormwater Monitoring Results
Brickhaven Mine No. 2 Tract "A"
NPDES Permit No. NCG0203S4
Chatham County
To Whom It May Concern:
FEB 21 2018
CEWRAL FILES
OWF? SECTION
ON
Please accept two copies of the 2017 annual documentation submittal required for stormwater permit
compliance for the Brickhaven Mine No. 2 Tract "A" (Brickhaven) site in Chatham County, North
Carolina, governed by NPDES Permit No. NCG020354.
Included with this submittal you will find the annual DMR report form for the analytical data. Outfalls for
Sediment Basins 1, 2, 3, 4, 6 and 7 were sampled during the first and second semiannual monitoring
periods. Due to site conditions and accessibility during qualifying rain events, the outfalls were sampled
on different dates rather than all at one time. Analytical reports from each sampling event have also
been included in this submittal package.
During our review of the laboratory data received on February 21, 2017, a turbidity level of 50.7 NTU
was detected at the Sediment Basin 6 outfall during the first semiannual monitoring period. The North
Carolina Department of Environmental Quality was notified on March 15, 2017, within 30 days of receipt
of the data package, and the appropriate Tier 1 response was recorded in the facility record. No
downstream impacts were observed. A follow-up sampling event was completed on May 1, 2017 for
turbidity, with a compliant result of 5.53 NTU. No other constituents were detected above their
respective benchmark levels during the first or second semiannual monitoring periods of 2017 for any of
the sediment basin outfalls.
Based on the analytical results received from the first and second semiannual monitoring periods of
2017, Brickhaven will continue with a semiannual monitoring frequency for all sediment basin outfalls.
Green Meadow, LLC e 12601 Plantside Drive a Louisville, Kentucky 40299
0: 502-245-1353 a F: 502-245-7398
Page 1 of 2

green Meodow LLC
V
Please feel free to contact me at [phone] or ndiyers2charah.com with any questions or concerns
you may have.
Sincefn
No . Divers, III
Director of Engineering, Environmental and Quality
Attachments: Annual Summary Discharge Monitoring Report (DMR)— Stormwater
2017 Semiannual Analytical Data
Cc: Brickhaven Mine No. 2 Tract "A"
File
Green Meadow, LLC • 12601 Plantside Drive + Louisville, Kentucky 40299
0: 502-245-1353 • F: 502-245-7398
Page 2 of 2

Georgoulias, Bethany
From: Georgoulias, Bethany
Sent: Monday, March 13, 2017 11:31 AM
To: 'Kyle Hoover, P.E., P.G., PMP'; Adams, Diane
Cc: Norman Divers; Valentine, Thad; Vinson, Toby
Subject: RE: Follow -Up on Call f Brickhaven Drying Bed Design
Kyle,
Thank you for your follow up call. As we discussed this morning, the modification the company is proposing would
require monitoring be modified to comply with wastewater monitoring and effluent limit conditions. In other words,
the discharge from the stormwater ponds where this effluent flows would no longer be considered stormwater
only. The company should also modify its Stormwater Pollution Prevention Plan, site overview maps, bnd related
documents to show the new wastewater outfall(s). Keep in mind that effluent limit exceedances are violations of permit
conditions, unlike benchmark exceedances that receive the appropriate tiered responses under the permit. These
discharges would flow to the same receiving waters as the mining operation was permitted under its original COC (which
authorizes both stormwater and wastewater discharges). Also remember that the permittee must adhere to all
conditions of Part II of General Permit NCGO20000 (Operation of a Treatment Facility).
We also understand that the beneficial reuse of CCR in structural fill being employed at this site has leachate that is
collected and contained elsewhere, and that leachate would not be routed through the ponds in the modifications you
are describing here. You explained that the drying beds will be for clays being removed from the mine lake only.
Our Program would appreciate a letter describing the finalized treatment configuration and revised site map that
includes all new wastewater outfalls for the Central Office permit file, so that future permit reviewers and inspectors
have these modification details for reference.
I understand Diane Adams will be out at the site later this month for a site visit. If you have any other questions, please
let her or me know.
Regards,
Bethany Georgoulias
Environmentai Engineer
Stormwater Program, Division of Energy, Mineral, and Land Resources
N.C. Department of Erivironmental Quality
919 807 6372 office
bet hany. geor og ulias a ncdenr.gov
1612 Mail Service Center, Raleigh, NC 27699-1612 (mailing)
512 N. Salisbury Street, Raleigh, NC 27604 (location)
Websitc: littp://deq.nc.7oL v/about/divisions/energy-mineral-land-resources/stormwater
t - C�-
Nothing Compares-.%,
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Kyle Hoover, P.E., P.G., PMP [mailto:[e-mail]]
Sent: Friday, March 10, 2017 3:47 PM
To: Adams, Diane <[e-mail]>
Cc: Georgouhas, Bethany<[e-mail]>; Norman Divers <[e-mail]>
Subject: Follow -Up on Call I Brickhaven Drying Bed Design
Diane,
Thank you for your follow-up call this afternoon concerning the proposed drying bed design at Brickhaven. As you
requested, I have put together a flow diagram of the proposed means of conveying the treated effluent from the drying
bed.
I hope this figure clarifies any questions about how treated effluent would be directed. As we are looking to elect to use
the drying bed as our means of treating the mine lake water before off -site discharge, we would monitor for permit
compliance at the conveyance pump intake and convey all compliant, treated effluent to the approved NPDES Discharge
Point for mine wastewaters at the Brickhaven site. We would do so using a mechanical pump and convey all compliant
flows collected in a ditch at the outfall of the drying bed through a closed pipe to the approved off -site discharge point
as shown by the blue line in the flow diagram. We understand that we could begin this process under the current
permit program if we convey treated flows for discharge under the monitoring and testing program already in place per
our permit Section IV(D).
We have also considered what options we have to discharge treated flows to one of the existing stormwater basins
onsite — potentially basin #4 or basin #7. These options are shown as the green dashed lines. From our understanding
of our NPDES permit, the comingling of treated wastewater and stormwater would fall under NPDES NCG020354 Permit
Section IV (D)(3) (co -mingling of wastewater and stormwater)which is a permitted method. I understand that this
option would require additional monitoring in accordance with the requirements in Section IV (D) Tables 7 and S in the
selected stormwater basin.
Thank you Diane. I have copied Bethany on this email as well so I can follow-up with her via phone this afternoon.
Please feel free to give me a call with any further questions or concerns.
Kyle Hoover, P.E., P.G., PMP
Engineering Manager J Charah, LLC
Mobile: [phone] Office: 502-245-1353 J
khoover charah.com http://www.chgrah.com
<Cc* Charah- Service Above All

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Charah' DRAFT - NOT FOR CONSTRUCTION BRiCKHAVEN STRUCTURAL FILL T
MONCURE, CHATHAM COUNTY, NORTH CAROLIMAROLINA
FIGURE 31 MINE SPOILS DRYING BED DESIGN FLOW DIAGRA

117 RESEARCh & ANA yTICAt
`,- LAbORATORIES, INC.
1 qq y
Analytical/Process Consultations
08 February 2017
Mr. Kyle Hoover, P.E., P.G.. PMP
Environmental Protection Specialist HI
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear IMr. Hoover:
Enclosed is one (1) copy of the storniwater analysis for the sample collected at the Brickhaven site
identified as S130 41 on 01 February 2017. If you should require any additional information or have an),
further questions concerning; the information contained in this report please feel free to contact me at
336.996.2841 or [e-mail].
Best Reaurds,
Sidney L. Champion
}executive Vice President
Director of Laboratory Services
J
Research & Analytical Laboratories. Inc.
P,0, Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336-996.2641 • Fax [phone]
www.randalabs.corn

I ', F i :,Al ;A A 1 I A!
UboRATORiES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/9/2017
v) NC 434 Z.Cn
N
NC1137701
r �
Client Sample ID: Stormwater SBO t,1 Lab Sample ID: 30342.01
Site: Brickhaven Collection Date: 2/1/2017 11:03
Parameter MethodY� _ — _ —Result Units -Rep Limit Analyst Analysis Date/Time
Settleable Matter SPA} 2540 F-1997 <0.1 mW 0.1 AW 2/1/2017 1415
Total Suspended Solids (TSS) SM 2540 D-1997 4.0 mg/L 2.5 JB 2/6/2017
Turbidity EPA 1BO.1 12.4 NTU 1 AW 2/1/2017 1547
1?;=no onci, eci
P.Q. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1

RESEARCh & ANA1yT1CA[
LABORATORIES, INC.
Analytical / Process Consultations
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RESEARCh & ANAlyTiCAL
LAbORATOMES, INC.
r
Analytical/Process Consultations
2 i ALIOUSt 2017
N,Ir. Kyle Hoover, 11.13.- P.G.- PIMP
EnaironMeMat Protection Specialist ill
charah, LLC
435 South "l IT011 Street
Suite 180
Charlotte, NC; 28202
Deal. lNir. Hoover:
l,nclosed is one (1) copy of'the stormwater analysis for the sample collected at the 13rickhaverl site
identified as S130 tt 1 on 17 All"-ust 2017. 11 N'011 S1101.11d r'eCllllre ant- l(Cht1011al Inf01-Miltiml or have ally
further questions coilcerl1iilQ the infornlatioll contained in this report please feel free to contact me at
)36.996.2841 or iniorihi- ndalabs.com.
Best Re,,:ards,
Sidney L.. CL1,lmpion
Executive Vice President
Director of' L.aboratory Services
Research &Analytical Laboratories. Inc.
PC. Box 473 • 106 Short Street • Kernersvilte. North Carolina 27284 • 336-996-2841 • Fax [phone]
www,randalabs.com

I(ESEARCh & ANAIyTICAI
LA ORATORIES BNCI
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
8/22/2017
,$I%It It t lIfff
14
: va K 434 z
r K 1137701
' r
r�`EDMA� ,
Client Sample ID: SB0#1 Lab Sample ID: 38950-01
Site: Brickhaven Collection Date: 8/17/2017 12:17
Parameter Method Result �UnitsT Rep Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 mUl 0.1 AA 8/18/2017 1600
Total Suspended Solids (TSS) SM 2540 D-1997 13.0 mg/L 2.5 AA 8/21/2017
Turbidity EPA 180.1 21 A NTU 1 AW 8/18/2017 1610
PM = no! 0nc;IyzeG'
P.O. Box 473 106 Short Street Kernersvi€le, North Carolina 27284 Tel: [phone] Fax: [phone] wµ v,randalabs.com Page 1

RESEARCh & ANA[yTICA1
R LAbORATORIES, INC.
Analytical / Process Consultations
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RESEARCh & ANA[yTICA[
` LAhORATORIES, INC.
Anaiybcal/Process Consultations
CASE- NARRATIVE
Oue (1) water sample was received in good condition can 18 August 2017. The
sample was in.alyzed without difr]CUliles unless noted helOW.
SidIieY L. Champion
Director of Laboratory Seer -ices
or L3/)-
Date
P.O. Box 473 • 106 Short Street • Kernersville. North Carolina 27284 * 336-996.2841 • Fax [phone]
mvw.randalabszom

RESEARCh & ANAlyTiCAI
LABORATORIES, INC.
5
'Analytical/Process Consultations
17 ,Nlarch 2017
Mr. Kyle Hoover, f'.1�., P.G., 11M1'
E'nvironmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear liMr. Hoover:
Inclosed is one ( I ) copy of the stormwater analysis for the sample collected at the Brickhaven site
identified as S130 rf# 2 on 13 March 2017. If you should require any additional information or have any
fur€her questions concerning the information contained in this report please: feel free to contact me at
336.996.2841 or info(ebrandalabs.com.
Best Rcaards,
Sidney L. Champion
I XeCUtiVe Vice President
Director of Laboratory Services
Research & Analytical Laboratories. Inc.
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336.096-2841 • Fax [phone]
www.randalabs.com

7
UbORATORiES, hC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Client Sample ID: S80 #f2
Site: Brickhaven
i Parameter Method
Settleable Matter SM 2,940 F-1997
Total Suspended Solids (TSS) SM 2540 0-1997
Turbidity EPA 180.1
Result
<0.1
10.6
15.6
Report of Analysis
3/23/2017
IIIF$III
ru;q 'O•
Nc "377t31
t?`A`y��� ++��
Lab Sample ID: 32012-01
Collection Date: 3/13/2017 10:32
Units R 2 Limit Analyst Analysis Date/Time
mi/i 0.1 AVV 3/14/2017 1450
mg1L 2.5 AW 3/14/2017
NTU 1 AW 3/14/2017 1640
PJA. = not orlc;iy-7ed
P.O, Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] vv ".randaiabs.corn Page 1

RESEARCh & ANA[yTiCAL
UbowoRks, INC.
Analytical / Prooass Consultations
Phono [phone]
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Water / Wastewater
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RESEARCh & ANA1yTICAL
LAbORATORiES, INC.
' My
Analytical/Process Consultations
CAST: NARRATIVE'
One (1) water sample was received in good condition on 14 March 2017.
The sample was analyzed without difficulties unless noted below.
Sidney L. Champion
Director of Laboratory Semites
Date
P.O. Box 473 • 106 short Street • Kernersville, North Carolina 272B4 • 336-996.2841 • Fax [phone]
www,randalabs.com

>, RESEARCh & ANA yT1CAL
i; LAbORATORiES, INC.
Analytical/Process Consultations
23 V1av 2017
Xlr. Kyle Hoover. P.l .. P.G.. 1'N91'
Environmental Protection Specialist Ill
Charah.
435 South Ti-von Street
Suite 180
Charlotte. NC 28202
Dear [Mr. Hoover:
Enclosed is tine (E ) copy of the for the sample collected at the Bi-ickhaven site
identified as 5130 rT3 on 19 May 2017, 11'ynu should require any additional inirn•nlation or have ally further
questiarls collcerrlin`.� 111c lllfm.matlorl C:olllalned in this report please feel free to contact me at 116.996.2941
or infion.randalahs.cclnl.
Best Re"ards.
Sidney 1.. Champion
Fxecutivc Vice President
Director of Laboratory Services
Research K Analytical L.ahoratol-les. Inc.
R O. Box 473 • 106 Short Street • Kernersvilte, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

RESEARCH & ANA[ylroCA[
� LAbORA•TORIES, INC.
:.: Q_ . J
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
5/23/2017
a �
�cn NC 434 Z N
NC 1937701
Client Sample ID: SBO #3 Lab Sample ID: 34905-01
Site: Brickhaven Collection Date: 5/1912017 8:39
Parameter Method Result knits Rep Limit Analyst Analysis DatelTime
Settleable Matter SM 2540 F-1997 <0.1 mill 0.1 AA 5/19/2017 1325
Total Suspended Solids (TSS) SM 2540 D-1997 36.0 mg/L 5 AA 5/22/2017
Turbidity EPA 180.1 29.9 NTU 1 AA 5/19/2017 1645
,',IA = not analyzed
P.O. Box 473 106 Short Street Kernersviile, North Carolina 27284 Tei: 336-996-2841 Fax: [phone] a ").randalabs.com Page 1
'al r;C•� t7E45r' �Cf

RESEARCh & ANA1yTiCA1
_.Jc I-AbORATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
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RESEARch & ANAlyTiCAI
LAbORATORiES, INC.
Analytical/Process Consultations
CASs: NA1ZR,\ 'IV1:
One (1) ►eater sample was received in good condition on 19 tblay 2017, The
Sample was analyzed without difficulties unless noted below.
Sidney L. Champion
Director of Laboratory Services
Date
RO, Box -173 • 906 Short Street • Kernersville, North Carolina 27264 • 336-996-2841 • Fax [phone]
www.randafabs,com

RESEARCh & ANAlyTICAI
LABORATORIES, INC.
Analytical/Process Consultations
12 December 2017
Mr. Kyle Hoover, P.E:., P.C., 1 N,111
l nvironmental Protection Specialist Ill
Charah, LLC
435 Sottth I ryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one (1) copy oC the shwnn 'awr analysis Or the samples collected at the I3rickhavcn site
identified as 5130 42 and SBO 43 on 04 lVenlher 2017. If you should require any additional information or
have any Further questions concerning the information contained in this report please feel 1rce to contact me
m 33&996.2941 or inlor(Oandalabs.com.
Best Regards.
Sidney 1.. Champion
EXM16ve Vice PreSident
Director ol- Laboratory Services
Research & Analgical Lahoratorres. Inc.
RCY Box 473 • 106 Short Street • Kemwsvi h North Cara N 27284 • 336-996-2841 • Fax [phone]
mvw. randa tabs. com

PICESEARCh & ANAtyTiCAI
L.1abORATORiES PNC,
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Client Sample ID: SBO #2
Site: 6rickhaven
Report of Analysis
12/12/2017
.%'G�&iYr� `rl''.
<
Juj
tr) NC 434 x;
NC037701
A0. 00
Lab Sample ID: 43633-01
Collection Date: 12/4/2017 11:16
'aram eter Method Result Units Remit Analyst Analysis DatefTirne
Settleable Flatter
SM 2540 F-1997
<0.1
1110
0.1
AA
12/5/2017 1500
Total Suspended Solids (TSS)
SM 2540 D-1997
2.7
mg/L
2.5
AA
12/6/2017
Turbidity
EPA 180.1
4.99
NTU
1
AA
12/5/2017 1545
NA = nor analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel, 336-996-2841 Fax: [phone] wmmandalabs.com Page 1
r31 ,t ;, 1:.. 1

arm IIEESEARCh & ANAlyTiCAI
LAORATORiES, NC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
12/12/2017
4$116Mir+1i
� ' y M
"t:cn NCtt34 z:N
NC;t37701
h ti
/PIED At1 s�
►at11atkI10%
Client Sample ID: SBO #3 Lab Sample ID: 43633-02
Site: Brickhaven Collection Date: 12/4/2017 11:03
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
SettleaNe Matter — -- - SPA 2540 F-1997 -� — — _<0.1 -- -mill --- -- 0.1---AA 12/5/2017 1500
Total Suspended Solids (TSS) SNI 2540 0-1997 8.2 mglL 2.5 AA 12/6/2017
Turbidity EPA 180.1 15.0 NTU 1 AA 12/5/2017 1548
;•JA = nor onalyzecl
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel; 336-996-2841 1=av 336-996-0326 vrrny.randalabs.corn Page 1

RESEARCh & ANA1yi1CAL
LABORATORIES INC.
Analytical / Process consultations
Phone [phone]
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RESEARCh & ANA[yTICA1
LAbORATORiES, INC.
Analytical/Process Consultations
CAST: Naltl2ATIV V
Bvo (2) water samples were 1-cceived in good condition on 05 December
2017. The samples wei-c analyzed without difficulties 11111less noted below.
Sidney L. Champion
Director of Laboratmw Sc1-vices
Date
P.O. Sox 473 • 106 Snort Street • Kernersville. North Carolina 27284 • 336-996-2841 • Fax [phone]
ww.v.randalabs.com

RESEARCh & ANAlyTICAI
;
bboRATWES, INC.
171 .1.
Analytical/Process Consultations
08 February 2017
Mr. Kyle Hoover, P.1s., P.G.. P1t-11'
Environmental Protection Specialist lit
Charah. LLC
435 South Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
Enclosed is one ( 1) copy of the stormwater analysis for the sample collected at the 13rickhaven site
identified as S130 # 4 on 31 January 2017. If you should require any additional information or have any
further questions concerning the information contained in this report please feel free to contact me at
336.996.2841 or infona randalabs.com.
Best Regards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories; Inc.
P.O. Box 473 • 106 Short Street • Kernersville, Forth Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs corn

AbORAT®RiES ONC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/9/2017
li%II aIl11jf
pp
G� C,'�r
M NC 434 z:Ln
NC93770.1
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rirr... `� `�e� �y 0-
Client Sample ID: Storrnwater S130#4 Lab Sample ID: 30341-01
Site: Brickhaven Collection Date: 1/31/2017 14:10
Parameter — --- _-- Method Result _Units— Rep Limit Analyst Analysis DateMme
Settleable Flatter SM 2540 F-1097 <0.1 mm 0.1 AW 2/1/2017 1415
Total SUSpended Solids (TSS) SM 2540 D-1997
Turbidity
EPA 180.1
6.0 mg/L 2.5 JB 2/6/2017
13.0 NTU 1 AW 2/1/2017 1545
✓`iF, = no! anafyzed
P,Q. Box 472 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
ml +]u bis!e 1,d

RESEARCh & ANA1yTICA1
LABORATORIES, INC.
analytical / Proem Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
Water / Wastewater
Misc.
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© RESEARCh & ANAlyTiCAI
LAhORATORIES, INC.
Analytical/Process Consultations
07 November 2017
N]r. Kyle Hoover. P.F., P.G. 1'MP
l;nviranmental Protection Specialist III
Charah, L LC
4335 South 'Tryon Street
Suite 180
Charlotte, 14C. 2H2O7
Dear NO Hoover:
I;nelosed is one (1) copy t)1 the marmwater analysis for the satin }le collected m the lAckhavmi site
identiHed as TH) 04 on'_7 Cktober 2017, iryo a should require any additional information or have any
further questions concerning the in1-ormation contained in this report please feel tree to contact me at
336.996.2841 of inli��r�randalahs.c«m.
Best Regards,
Sidney L. Champion
laccuRe Vice President
Director of Laboratory Services
Research A; Analytical I..abnratories. Inc.
P. ❑. Box 473 • 108 Short Street • Kernersui w AM Carolina 27284 • 336.996-2841 • Fax [phone]
www.rondalabs.com

�. �1 `, i i 1
RESEARC
_ Ii INC.
♦ 4 I �-
ti
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
111712017
►'k;1181rtei14
♦�' 1#I
w. LU
NC r-34:
w NC t137701
r
Client Sample ID: S80#4 Lab Sample ID: 42055-01
Site: Brickhaven Collection Date: 10/27/2017 11:32
Parameter Method _ Result N Units Rep Limit Analyst Analysis Date[Time Y
Settleable Matter SM 2540 T:-1997 <0.1 mlll 0.1 AA ^10127/2017 1600
Total Suspended Solids (TSS) SM 2540 0-1997 4.3 mg/L 2.5 AA 1013012017
Turbidity EPA 180.1 9.74 NTU 1 AA 1012712017 1600
P.O. Box 473 106 Short Street Ke€nersville, North Carolina 27284 Tel: [phone] Fax' 336-996.0326 mAy.randalabs.com Page 1

RE5EARCh & ANA1yTICA[
I-AbORATORiE5, INC.
Analytical / Process Consultations
Phone [phone]
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RESEARCh & QANA1YTICA[
LABORATORIES, INC.
Analytical/Process Consultations
GAS'U] N:11zlt.= TIN'F
()ne (1) ►►;;ter san►ple ►Vas IWeived in good condition on 27 October 2017.
The Sample was an.tlN,Zed withutat difficulties ut►less noted 1>elu►►'.
/'GEr-
Sidney L. Champion
Director- of Lahoratot-►' Services
� --� 'J 11
Date
P0. Box 473 • 106 Short Street • Kernersville, (`forth Carolina 27284 • 336-996-2841 • Fax [phone]
www.randatabs.coni

RESEARCh & ANA1yTICA[
�t `l LABORATORIES, INC.
Analytical/Process Consultations
21 February 2017
rNdr. Kyle Hoover, P.1r,, P.G.; I)MI)
Environmental Protection Specialist III
Charah. LLC
435 South 'Tryon Street
Suite 180
Charlotte, NC 28202
Dear 1,Ir. Hoover:
Inclosed is one (1) copy of the stormwater analysis for the sample collected at the I3rickhaven site
idcntified as SBO ;' 6 on 09 February 2017. If you should require any additional information or have any
further questions concerning; the information contained in this report please feel free to contact me at
336.996.2841 or info a randalabs.com.
Best Re<izards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short Street • Kernersviile, North Carolina 27284 • 336-996.2841 • Fax [phone]
www.randalabs.com

RESEARCW & ANA1yTiCA1
►` LAbORATORl ESQ INC.
y,
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/21 /2017
���u�rririr�
NC ti34 . U1 r
r NC t:37701 z
w
00
�� ��ED1A11�'�;`�y
Client Sample ID: SB046 Lab Sample ID: 30826-01
Site: Brickhaven Collection Date: 2/9/2017 '12:07
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
Settleable Matter SM 2540 F-1997 <0.1 ml/I 0.1 AW 2/10/2017 1230
Total Suspended Solids (TSS) SM 2540 D-1997 19A mg/L 2.5 JB 2/13/2017
Turbidity EPA 180.1 50.7 NTU 1 AW 2/10/2017 1420
0.41 = not cmdy�eci
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 _ Tel: [phone] Fax: [phone] tiv M.randalabs.corn Page 1
furl L::ii L`a SIC 'J iU

RESEARCh & ANAIyTiCAI
LAWRATORIESIF INC.
Analylleal / Prooass Consultutlona
Phone [phone]
CHAIN OF CUSTODY RECORD
Water / Wastewater
isa
Company
CA6.lt LLC
Job No.
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T; RESEARCh & ANAlyTiCAI
a
LABORATORIES, INC.
Analytical/Process Consultations
CASE NA11RATI V
One (1) water sample was received in good condition on 10 February 2017.
Fhe sample was analyzed without difficulties unless noted below.
Sidney L. Cliampion
Director of Lahorntory Services
Date
P.0. Box 473 • 108 Short Street • Kernersville, North Carolina 27284 . 336.996-2641 • Fax [phone]
vrww.randalabs.com

RESEARCh & ANA[yTICA[
t� LABORATORIES, INC.
Analytical/Process Consultations
I I May 2017
Mr. Kyle Hoover, P.E., P.G.- PMP
Environmental Protection Specialist Ill
Charah, L,L,C
435 South 'Tryon Street
Suite 180
Charlotte, NC 28202
Dear Mr. Hoover:
1lnclosed is one (1) copy of'the stormwater analysis for the saunple collected at the BrIckhaven site
identified as SBO 116 on 01 May 2017. IFyou should require any additional information or have any Further
questions concerning the information contained in this report Please feel Free; to contact me at 336,996.2841
or int« a,randaiabs. coin.
Best Regards,
Sidney L. Champion
Eaxecutive: Vice President
Director of Laboratory Services
Research & Analytical Laboratories, Inc.
P.O. Box 473 • 106 Short Street • Kernersvi9e, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randelabs.com

RESEARCh & ANA[yTiCAI
oo LA ORAT®RiESINC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
5/10/2017
Cd
r w
NC 434 z:
4
NC tt37701
i ,► r
r •
��rrru tts���
Client Sample ID: SBO#6 Lab Sample ID: 34120-01
Site: Brickhaven Collection Date: 5/1/2017 10:57
Parameter Method Result Units Rep Limit Analyst Arlalysis Dateffime
Turbidity EPA 180.1 5.53 NTU 1 AA 5/2/2017 1553
NA = no, orlalyzeci
P.O. Box 473 106 Short Street Kerrersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 1
ra{ Gnn b:isic vlo

RESEARA & ANALyTiCAL
bboltATORiES, INC.
Analytical / Proems Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
Sampler Sfgilatunc-7
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RESEARCh & ANAlyTICAI
LABORATORIES, INC.
Analytical/Process Consultations
CASE NARRATIVE
One (l) water sample was received in good condition on 02 May 2017. The
sample was analyzed without difficulties unless noted below.
/� A,-- os-hN )r�
Sidney L. Champion
Director of Laboratory Services
Date
P.D. Box 473 • 106 Shart Street •Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalahs.com

RESEARCh & ANA[yT1CAL
LABORATORIES, INC.
Analytical/Process Cansult,abons
13 September 2017
Mr. Kyle Hoover. P.L. P.G. PIMP
Finvironmental Protection Specialist ill
Charah. 1_.LC.
435- South Tryon Street
Suite 190
Charlotte, NC; 28202
Dear Mr. Hoover:
1 i1closed is one (I ) copy of the stor1mviller analysis for the Sample collected aE the 1.31-ickhaven site
identified its SBO 46 can 06 September 2017. if }Ou should require any additional inl'ormation car have any
lurther questions Mlcerrlinil tilt MfOrrllation contained In this report please feel free to contact me at
3 6.996,2841 or inli?fir}rarl�ial�tbs.ci�m.
Best Regards,
Sidney L. ChampWil
hsccutive Vicc President
Director of' Laboratory Services
Research K. Analytical Laboratories. Inc.
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 272B4 • 336-996-2641 • Fax [phone]
%vmv.randalabs.com

RESEARCh & ANALyTICA1
LA ORAT®RBES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
9/12/2017
r ��tt�� a rrittt
c
:rq NC43,1 Z. w
w NCh37701
+ ttfiri�:crvtir+��
'lient Sample ID: SBO m6 Lab Sample ID: 39563-01
Site: Brickhaven Collection Date: 91612017 9:37
Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
Settleable ,fatter SM 2540 F-1997 <0.1 mlll 0'1 AA 9/6/2017 1600
Total Suspended Solids USS7 SM 2540 D-1997 6.5 mg/L 2.5 AA 9/7/2017
Turbidity EPA 180.1 12.2 NTU 1 AA 916120/7 1550
rIA = not ariolvzea
D. Box 473 1D3 Short Street Kernersville. North Carolina 27284 Tel [phone] Fax: [phone] vfivmrandalabs.com Page t

RESEARCh & ANA1yTiCA[
LABORATORIES, INC.
i
Analytical/Process Consultations
CAST; \ARRATIVI;
One (1) water sample was received in good condition on UG September 2017.
The sample was analyzed without difficulties unless note(] below.
z � G/�.
�' d�1�31a�
Sidney L. champion
Director of Laboratory Services
Date
P.O. Sax 473 • 106 Short Street • Kernersviile, North Carolina 27284 • 336-996.2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANA[yiricAl
UbORmortkS, INC.
Analytical / Process. Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
Water/Wastewater
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Co mpany
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f RESEARCh & ANA[yTICA1
LAbORATORiES, INC.
" ` J Analytical/Process Consultations
08 February 2017
Mr. Kyle Hoover, Y.E.; P.G., PIMP
Environmental Protection Specialist III
Charah, LLC
435 South Tryon Street
Suite 180
Charlotte, \C 28202
Dcar Mr. Hoover:
Enclosed is one (1) copy of the stormwater analysis for the sample collected at the Brickhaven situ
identil-led as SBO 47 on 03 February 2017. If you should require any additional information or have any
further questions concerning the information contained in this report please feel free to contact me at
336.996.2841 or infoRrandaiabs.com.
Best 1tegards,
Sidney L. Champion
Executive Vice President
Director of Laboratory Services
Research cR Analytical Laboratories, Inc.
Ro. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336.996-2841 • Fax [phone]
www.randalabs.com

RESEARCh & ANA[yiricAi
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
2/9/2017
`%jIaaIIIIII
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:a
NC 1;34 Z-
NC 437701
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Client Sample ID: S60 #7 Lab Sample ID: 30441-01
Site: Bric�,haverl Collection Date: 2/3/2017 10:19
�Parameter Method..-_ -- w_-- — Result Units 4Rep Limit Analyst Analysis Dateffime
— _-...----------- -- - — - _
Settleable Matter Sfv12540 F-1997 <0.1 mlll �0.1 AW 2/3/2017 1400
Total Suspended Solids (TSS) SM 2540 D-1997
Turbidity
EPA 180.1
15.3 mglL 2.5 JB 2/6/2017
18.1 NTU 1 AW 2/312017 1538
hl,•.= not onolyzed
P.O. BOX 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] m v.randalabs.com Page t

RESFARCb & ANALyTlCAL
Ub4RATOR1ESi INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
Water / Wastewater
Misc.
Company
Job No.
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RESEARCh & ANAlyTiCAI
LABORATORIES, INC.
Analytical/Process Consultations
08 November 2017
N,Ir. Kyle Hoover. 1'.I... P.G.. NMI'
t"livironmental Protection Specialist [il
C11a1-ah. LLC
433 South Tryon Street
SUitC 190
Charlotte, NC 28202
Dear N,Ir. Hoover:
l.;nclosed is one (€) Copy oi,the s101-111water analysis for the Sample collected at the Brickhaven site
identified as SBO �f7 on 02 November 2017. [('voir should require any additional information or have any
1`ilrther questions concerning the information Coniamcd In this report please feel free to contact 111e at
6.996.28=41 or ink) Qq randaiahsxom.
Best Reimrds.
Sidnev 1..- Champion
EXCCLI ive Vice: President
Director of' Laboratory Services
Research & Analytical I..aboratories, Inc.
R D. Box 473 • 106 Short Street • Kernersville, North Carolina 27284 • 336.996-2841 • Fax 336�996-0326
wvnv.randalabszom

RESEARCh & ANA[yTICAI
( - LA ORMORIES, INC.
For: Charah, LLC
435 South Tryon Street Suite 180
Charlotte, NC 28202
Attn: Kyle Hoover
Report of Analysis
11/8/2017
Is11$111f1
� A•:Y r
i. Lu;Q i•. WWW r
rn NC 434 i; N Z
' NC #37701
Client Sample ID: SBO ##7 Lab Sample ID: 42312-01
Site: Bric'r.haven Collection Date: 11/2/2017 12:11
Parameter Method — —�� Result Units Rep Limit An_ aiysf Analysis DatelTime J
Settleable Matter SM 2540 F-1997 <0.1 M111 0.1 AA 11/3/2017 1400
Total Suspended Solids (TSS) SPv1 2540 D-1997
Turbidity
EPA 180.1
M74111
30.7
rng/L 2.5 AA 11/6/2017
NTU 1 AA 1 ' 13/2017 1600
t`!A = not onolyzed
P,O. Box 473 106 Short Street Kernersville,'Nodh Carolina 27284 Tel: [phone] Fax: [phone] mvw.randalabs.com Page 1
I :11 _ EI;C 'iLJ

R ESEARCh & ANA1yT[CA1
LABORATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
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RESEARCh & ANA[yTiCAI
LABORATORIES, INC.
Analytical/Process COnsultationr
CASF NARRATIVE
One (1) ►vater sample was received in good condition on 03 NOvernber 2017.
The sample Nvas analyzed without difficulties unless note'(! below.
I;d,7 // gr— i) Lk )1-7
Sidney L. Champion
Director of L.ahoratoi-v Seri ices
Dale
P.O. Box 473 • 106 Short Street - Kernersville, North Carolina 27284 • 336-996-2841 • Fax [phone]
www.randalabs.com

ANNUAL SUMMARY DISCHARGE MONITORING
REPORT (DMR) — STORMWATER
II SUBMIT TO CENTRAL OFFICE* II
General Permit No. NCG020000
Calendar Year - 2017
'Report ALL STORMWATER monitoring data on this form (include "No Flow"1"No Discharge" and Benchmark
Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year, I
Certificate of Coverage No. N0002 ®00 `1❑
Facility Name: Brickhaven No._2 Mitre Tract "A"
County: Chatham
Phone Number: ( ) Total no. of SDOs monitored 6
Certified Laboratory Research & Analytical Laboratories, Inc. Lab # 34
Lab #
Stormwater Discharge Outfall (SDO) No. 1 VMA Outfall? Yes ❑ No ❑h'
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No X
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
Outfall No.
1
Total
Rainfall,
inches
TSS,
mgll
SS,
mill
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turgidity,
NTU
Non -polar
O&G, mg/I
(VMA) !
New
Motor Oil
Usage
al/mo.
Stormwater
Benchmarks
fndlcata NO
FLOW i!
a !lca6fa
circle
Benchmark
h
00 50
n
0.1
Benchmark
Benchmark
�,���y�,�]r!
025 1 0
NIA
Water Quality
Standard applies
NIA
Water Quality
Standard applies
1 5
�55 a requires
average requires
TSS and Non•polar
Non-rin
SS aO&G monitoring
Date Sample
Collected,
•� x�
's,
^
f
1 h• e w Y
Exr�ti
a"n 7
'taF�,
iQ
�"h
u°�
R�
02/01 /2017
1.43
4.0
<0.1
12.4
NIA
NIA
NIA
N/A
08/ 17/2017
0.47
13.0
<0.1
21.4
N/A
NIA
NIA
NIA
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. N0002 [ ❑J F-;�F41
Additional Outfall Attachment (make copies as needed for additional outfalls)
St.ormwater Discharge Outfall (SDO) No. 2 VMA Outfall? Yes ❑ No
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMt_R to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
2 Outfall No.
2
Total
Rainfall,
inches
TSS,
mgll
SS,
mlll
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mg'/1
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
lndicale N0
FLOW!(
applicable
Circle
Benchmark
t�11 0I1
UL
0'�
Circle
enchmark
�02519 0
NIA
Water Duality
Standard applies
NIA
Waller Quality
Standard applies
�
5gereq
ave>rs a wires
TSS and Non -polar
O&G monitorin
Date Sample
Collected,
I
-
-
r
03/13/2017
0.85
10.6
<0.1
15.6
NIA
NIA
NIA
NIA
12/04/2017
0.85
2.7
<0.1
4.99
NIA
NIA
NIA
N/A
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 ®❑3 ��
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 3 VMA Outfall? Yes ❑ No ❑X
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
Outfall No.
3
Total
Rainfall,
inches
TSS,
mgll
SS,
m1/1
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mgh
(VMA)
New
Motor Oil
Usage
gallmo.
Sformwafer
Benchmarks
indicaleNO
F`ow''
a !!cable
Circle
mark
100 0
0.1
Circle
nclm3rk
50 25110
NIA
"later°nali,y
Standard applies
NIA
waterOuality
Standard applies
15
>55 gallmo.
avoragaraqulres
TSS and Non -polar
O&G mortRorin
Date Sample
Collected,
molddlyr
_
_
05/19/2017
0.34
36.0
<0.1
29.9
NIA
NIA
NIA
NIA
12/04/2017
0.85
8.2
<0.1
15.0
NIA
NIA
NIA
NIA
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 0❑MF41
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 4 VMA Outfall? Yes ❑ No
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples beiow benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring
Other
a
4 Outfall Na.
4
Total
Rainfall,
inches
TSS,
mgll
SS,
mill
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mg/I
(VMA)
New
Motor Oil
Usage
allmo.
Stormwater
Benchmarks
lndica[aN0
W FLOi€
applicable
Circle
ark
! n
�Q1 v
�'�
Circle
nchmarR
!
5V 25r 0
NA
f!
!
Water Quality
Standard applies
NA
!
Water Quatity
Standard applles
5
?55gaIfmo.
average requires
TSS andNon•polar
O&G monitoring
Date Sample
Collected,
mo/dd/yr
01/31/2017
1.43
6.0
<0.1
13,0
NIA
NIA
NIA
NIA
10/27/2017
1.92
4.3
<0.1
9.74
NIA
NIA
NIA
N/A
Permit Date 1011/2015 — 9/30/2020
Last Revised 10-2-2015

Certificate of Coverage No. NCG02 ❑❑F5_]❑4
Additional Outfall Attachment (make copies as needed for additional outfalls)
Stormwater Discharge Outfall (SDO) No. 6 VMA Outfall? Yes ❑ No
Is this outfall currently in Tier 2 for any parameter? Yes ❑ No [�
Was this outfall ever in Tier 2 during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, was monthly monitoring discontinued?
Yes, enough consecutive samples below benchmarks to decrease frequency ❑
Yes, received approval from DEMLR to reduce monitoring frequency ❑
No, turbidity benchmark exceedances did not require monthly monitoring ❑
Other ❑
Outfall No.
6
Total
Rainfall,
inches
TSS,
mg/1
SS,
ml/l
Turbidity,
NTU
Upstream
(U) Turbidity,
NTU
Downstream
(D) Turbidity,
NTU
Non -polar
O&G, mgll
(VMA) '(gal/Mo.)
New
Motor Oil
Usage
Stormwater
Benchmarks
fndicatoNO
FLOW ff
a ,fcahle
Circle
Benchmark
100 50
0.1
Circle_
Benchmark
50 25110
NIA
Water Quality
Standard applies
NIA
Water Quality
Standard applies
15
>55gaurno,
average requires
TSS and Non polar
48G monitoring
Date Sample
Collected,
mo/dd/yr
i
I
L°
02/09/2017
0.59
19.4
<0.1
50.7
NIA
NIA
NIA
NIA
05/01/2017
5.81
NIA
NIA
5.53
NIA
NIA
NIA
NIA
09/06/2017
2.15
6.5
<0.1
12.2
NIA
NIA
N/A
N/A
Permit Date 10/1/2015 — 9/30/2020
Last Revised 10-2-2015

aceAnalytical
wwpacslabs.wn
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
October 06, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Mine Lake 9/30
Pace Project No.: 92314419
�,�Uo�o3sy
RECEIVED
CENTRAL FILES
DWR SECTION
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on September 30, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 17

r
r ,
aceAnalytical
www.pamfabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Mine Lake 9130
Pace Project No.: 92314419
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Urginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 17

r
aceAnalytica!
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Mine Lake 9130
Pace Project No.: 92314419
Lab ID Sample ID
92314419001 MINE LAKE OUTLET
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 180.1
AES2
1
PASI-A
SM 2540D
MJS
1
PASI-A
SM 254OF
EWS
t
PASI-A
EPA9040
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 17

i f '
6
aceAnalytical
wsvwpecelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828 )254-7176
SUMMARY OF DETECTION
Project: Mine Lake 9/30
Pace Project No.: 92314419
Lab Sample ID Client Sample ID
Method Parameters Result Units
92314419001 MINE LAKE OUTLET
EPA 180.1 Turbidity 7.2 NTU
EPA 9040 pH 4.2 Std. Units
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Report Limit Analyzed
1.0 101011161313
0,10 10/03/1615:41 H6
Qualifiers
Page 4 of 17

aceAnalXical
www.paceJabs.com
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville. NC 28804
[phone]
PROJECT NARRATIVE
Project: Mine Lake 9130
Pace Project No.: 92314419
Method: EPA 180.1
Description: 180.1 Turbidity
Client: Charah
Date: October 06, 2016
General Information:
1 sample was analyzed for EPA 180.1. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 17

aceAnalyticai*
wwwpacelahs.cnm
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Mine Lake 9/30
Pace Project No.: 92314419
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: October 06, 2016
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 17

aceAnalyfical
www.p,cetabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Mine Lake 9130
Pace Project No.: 92314419
Method: SM 254OF
Description: 254OF Total Settleable Solids
Client: Charah
Date: October 06, 2016
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 17

aceAnalytical
wwwpacelabs.wm
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Mine Lake 9130
Pace Project No.: 92314419
Method: EPA 9040
Description: 9040 pH
Client: Charah
Date: October 06, 2016
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA required holding time.
• MINE LAKE OUTLET (Lab ID: 92314419001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 17

aceAnalytical
~-Pacelabs.ciom
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828 )254-7176
ANALYTICAL RESULTS
Project: Mine Lake 9130
Pace Project No.: 92314419
Sample: MINE LAKE OUTLET
Lab ID: 92314419001 Collected: 09/30/16 09:00
Received: 09/30/16 13:45 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
7.2 NTU
1.0
1
10/0111613:13
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
5.1
1
10/04/16 23:49
2540F Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mL/Uhr
0.10
1
10/01/16 13:15
9040 pH
Analytical Method: EPA 9040
pH
4.2 Std. Units
0.10
1
10/03/16 15:41 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 17

r j
aceAnalyitical
www.paceiabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Ashevilfe, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Mine Lake 9130
Pace Project No.: 92314419
QC Batch: 331409 Analysis Method: EPA 1 80. 1
OC Batch Method: EPA 180.1 Analysis Description: 180.1 Turbidity
Associated Lab Samples: 92314419001
METHOD BLANK: 1836223 Matrix: Water
Associated Lab Samples: 92314419001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 1.0 10/0111613:13
LABORATORY CONTROL SAMPLE: 1836224
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Turbidity NTU 10 9.7 97 90-110
SAMPLE DUPLICATE: 1836225
92314419001 Oup
Parameter Units Result Result RPD Qualifiers
Turbidity NTU 7.2 7.8 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 17

I y
aceAnalytrcal
www pacetabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Mine Lake 9130
Pace Project No.: 92314419
QC Batch: 331785
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92314419001
METHOD BLANK: 1838357
Matrix: Water
Associated Lab Samples: 92314419001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 10/04/16 23:48
LABORATORY CONTROL SAMPLE: 1838358
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 250
100 90-110
SAMPLE DUPLICATE: 1838359
92314419001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
SAMPLE DUPLICATE: 1838361
92314466003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Rosults presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 17

aceAnalXical.
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Mine Lake 9130
Pace Project No.: 92314419
QC Batch: 331411 Analysis Method: SM 254OF
QC Batch Method: SM 254OF Analysis Description: 2540F Total Settable Solids
Associated Lab Samples: 92314419001
METHOD BLANK: 1836229
Associated Lab Samples: 92314419001
Parameter Units
Total Settleable Solids mULlhr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 10101/16 13:15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 17

I
aceAnalXical
www,paceiabsxorn
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Mine Lake 9130
Pace Project No.: 92314419
QC Batch: 331485
QC Batch Method: EPA 9040
Associated Lab Samples: 92314419001
SAMPLE DUPLICATE: 1836532
Parameter Units
pH Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
92313329001 Dup
Result Result RPD Qualifiers
6.7 6.9 2 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without she written consent of Pace Analytical Services, LLC. Page 13 of 17

aceAnalytical•
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
(828 )254-7176
QUALIFIERS
Project: Mine Lake 9130
Pace Project No.: 92314419
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/06/2016 10:11 AM without the written consent of Pace Analytical Services, L.I.C. Page 14 of 17

•
aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Mine Lake 9130
Pace Project No.: 92314419
Lab ID
Sample ID
QC Batch Method
QC Batch
92314419001
MINE LAKE OUTLET
EPA 180.1
331409
92314419001
MINE LAKE OUTLET
SM 2540D
331785
92314419001
MINE LAKE OUTLET
SM 254OF
331411
92314419001
MINE LAKE OUTLET
EPA 9040
331485
Date: 10/06/2016 10:11 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 15 of 17

aceAnady ka1
Document Name:
Condition Upon Recei:
Document No.:
F-RAL•CS•001-Rev.04
[pent dame:
Project A
Courier: [:]Fe ❑UPS UUSPS Client
❑ Commercial ❑Pace ❑Other:
Document Revised: May 24, 2016
Pale 1 of 2
Issuing Authority:
Pace Raleilth Quality Office
^-_ , +:�• IeFarml use nNI v
WQ:92314419
92314419
Custody Seal Present? Des 0No Seals Intact? ❑Yes �ZNo Ann„ n,l„ a r�
Date/tnitlah Pelson Examining Contents
Packing Material: ❑Bubble Wrap [:]Bubble Bags None []Other:
Thermometer: T1505 Type of I owet []Blue QNone ❑Samples on ice, cooling process ha begun
Correction Factor:0,0'C Cooler Temp Corrected ('C): ,;10 Biological Tissue Frozen? [:]Yes[]NO3/A
Temp should be above !f zing to 61C r
USDA Regulated Soil ( L6 N/A, water sample)
Did sampleVWginate In a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (Inter tna finally,
❑Yes 1ANo Including Hawaii and Puerto Rico)? ❑Yes o
eomments/Discre a _
Chain of Custod Present?
I&S
No
[]MIA
1,
Samples Arrived within Hold Time?
Yes
No
❑N/A
2.
Short Hold Time Mal sis <72 hr.)7
6fY.,
No
N/A
3,
a VA S
Rush Turn Around Time Requested?
byei
16No
N/A
4,
Sufficient Volume?
wfyes
No
❑N/A
S.
Correct Containers Used?
I/"
❑Na
[]N/A
6.
-Pace Contalners Used?
b4s
ONo
❑N A
Containers Intact?
os
ON,
N/A
7.
Samples Field Filtered?
❑Yes
QNO
PINIA
B. Note If sediment is visible in the dissolved container
Sample tabels Match COC7
Yes
[]NO
❑N/A
9.
-Includes Date me/ID/Analysis Matrix:
Ali containers needing arld/base preservation have been
10.
checked?
Is
❑No
❑N/A
All containers needing preservation are found to be in
compliance with EPA recommendation?
,_,(
KU04 dM7
(HN , HIS0a, Kle2; NaOH >9 Sulfide, N20H>12 Cyanide)
O,s
bd Te.S
❑No
❑N/A
Kbm"u
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,UH
es
No
N A
Samples checked for dechlorination?
Yes
No
N/A
11.
Head space in VOA Vials >S-6mm 7
Des
JJNa
/A
12.
Trip Blank Present?
❑Yes
❑No
/A
13.
Trip Blank Custody Seals Present?
[]Yes
❑No
N/A
Pace Trip Blank Lot If (1f purchased):
CLIENT NDTIFICATION/AESOU TION
Person Contacted: Date/lime:
Comments/Sample
Discrepancy:
Field Data Requlredt ❑Yes []NO
Project Manager SCURF Review: (� T Date:
Project Manager SRF Review: Date: /D
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the Nooh rolina DEHNR Certification Office (I.e.
Out of hold, Incorrect preservative, out of lemp, incorrect containers) .
Page 16 of 17

2aceAnaIX cal"
-- wrw.paeatabt.cum
r
6701 Contererioe drive, Haleigh, NO 27607
ph: [phone], tax: [phone]
NCWW Ced#67, NCDW CerW37731
Report Result To:
Company: AArA
Address:
Attn:
Phone:
Pax:
Sampled by (signature):
Chain ®f Custody W.o.#
BiH To:
Project Reterence:
Project Number:
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
—Rush pro)ects are sublect to prEor approval by
the raboratory
Requested Due Date:
Ref ]shed (skin re)
)
R wpm
c��
t
�b
Time
3
Ralhgt by (sk nature)
ecelved by (signature)
Date
Tore
Aelinqull rs by (signature)
Received by (sl9miure)
Data
Time
Receipt Conditions (Lab Via Only)
❑ 4t2°C ❑ Tem °C
Res. chlorine:
❑ Absent ❑ Present ❑ rVa
Acid preserv. <27
❑ Yes ❑ No ❑ rVa
Base preserv. >i 24
❑ Yes ❑ No ❑ We.
Page 17 of 17

i-
1
e
aceAnalytica!
www pxere6xcan
June 03, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
() D-v 3--Sy
RECEIVE®
JAN 3 1 2017
CENTRAL FILES
DWR SECTION
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on May 31, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
cc: Cotlin lalummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced. except in full,
without the written consent of Pace Analytical Serv(ces, Inc.,
Page 1 of 19

tr
ace Ahalytrcal
www pamiab's cam
Project: 5/31 VWV Discharge 5131
Pace Project No.: 92299554
Raleigh Certification IDS
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #; E8764B
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37736
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 990300D1
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
Page 2 of 19

aceAnalytical
f
SAMPLE ANALYTE COUNT
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Pace Analytical Services, Inc.
2225 Riverside I)r
Asheville, NC 28804
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92299554001 5131 WW GRAB SM 2540D
KCE
1
PASI-E
SM 254OF
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 9222D
RC
1
PASI-R
EPA 180.1
DMN
1
PASi-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 3 of 19

� - 1
•
aceAnalytical
SUMMARY OF DETECTION
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Pace Analytical Services, Inc,
2225 Riverside Or
Asheville, NC 2aaR4
[phone]
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92299554001
5131 WW GRAB
SM 2540D
Total Suspended Solids
6.6
mg1L
2.5
06/01/16 14:24
EPA9040
pH
6.4
Std. Units
0.10
06/01/16 17A0 H1.H6
SM 92220
Fecal Colifofms
164
CFU7100 mL
1.0
05/31/16 16:07
EPA 180.1
Turbidity
8.5
NTU
1.0
06/01/16 22:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Artalytical Services, Inc.. Page 4 of 19

c
aceAnalyti{cal
wrrwpacelabs.wmm
PROJECT NARRATIVE
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: June 03, 2016
Pace Analytical Sorvicas, Inc.
2225 Riverside Dr
Asheville, NC 28864
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below,
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within CC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDENl22981
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1746097)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc., Page 5 of 19

r ,
a
aceAnalytical
wwwpetefableom
PROJECT NARRATIVE
Project: 5/31 VWV Discharge 5131
Pace Project No.: 92299554
Method:
SM 2540F
Description:
2540E Total Settleable Solids
Client:
Charah
Date:
June 03, 2016
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2B804
t828)254-7176
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report,
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below,
Matrix Spikes:
All percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
7h!s report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 19

aceAnalytical
wwwpacawabs corn
PROJECT NARRATIVE
Proje& 5131 WW Discharge 5131
Pace Project No.: 92299554
Method: EPA 9040
Description: 9040 pH
Client: Charah
Date: June 03, 2015
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 2aB04
[phone]
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below,
1­11: Analysis conducted outside the EPA method holding time.
5131 WW GRAB (tab ID: 92299554001)
1­16: Analysis initiated outside of the 15 minute EPA required holding time.
• 5131 WW GRAB (Lab ID: 92299554001)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 19

/!2eAnalytical"
Wwwpaaela6scom
PROJECT NARRATIVE
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Method: 5M 92220
Description: MW 9222D Fecal Coliform RAL
Client: Charah
Date: June 03. 2016
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NO 28804
[phone]
General Information:
1 sample was analyzed for SM 9222D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations jincluding MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
Ali internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: RBIOI6172
D& The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1745707)
• Fecal Coliforms
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 8 of 19

Pace Analytical Services, Inc.
s 2225 Riverside Dr
aceAnalX cal Asheville. NC 28804
rwwpecelabs rxun
[phone]
PROJECT" NARRATIVE
Projecl: 5131 WW Discharge 5l31
Pace Project No.: 92299554
Method: EPA 180.1
Description: 180.1 Turbidity
Client: Charah
Date: June 03, 2016
General Information:
1 sample was analyzed for EPA 180.1. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andlor the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spike$:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wilhouI the written consent of Pace Anatytical Services, Inc.. Page 9 of 19

aceAnalytrcal
W"Pecafebsc=
r
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 28804
[phone]
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Sample: 5131 WW GRAB
Lab ID: 92299554001 Collected: 05/31/16 11:00
Received: 05131/16 15:110 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No, Qua[
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.6 mg1L
25
1
06/01116 14:24
254OF Total Settleable Solids
Analytical Method: SM 254OF
Tots! Settleable Solids
ND mIJUhr
0.10
1
06/01/16 17:10
9040 pH
Analytical Method: EPA 9040
pH
6.4 Std. Units
0.10
1
06/01/16 17:40 H1,1-16
MBIO 9222D Fecal Colitorm RAL
Analytical Method: SM 9222D
Fecal Coliforms
164 CFU1100 mL
1.0
1
05/31/16 16:07
180.1 Turbidity
Analytical Method: EPA 180.1
Turbidity
8.5 NTU
1.0
1
06/01/16 22:30
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM without the written consent of Pace Analytical Services, Inc. Page 10 of 19

F
aceAnalytical
*W;X mradtavrt
QUALITY CONTROL DATA
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
QC Batch: EDEN122981 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92299554001
METHOD BLANK: 1746094 Matrix: Water
Associated Lab Samples: 92299554001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 06101116 14:20
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 1746095
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 264 106 90-110
SAMPLE DUPLICATE: 1746096
92299480001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 174 159 3
SAMPLE DUPLICATE: 1746097
92299527003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/1- 75.3 83.0 10 D6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM w4houl the written consent of Pace Analytical Services, Inc. Page 11 of 19

acMnalAtul
eMwpeadabaoam
QUALITY CONTROL DATA
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
QC Batch: EDEN122992 Analysis Method: SM 254OF
QC Batch Method: SM 254OF Analysis Description: 2540F Total Sellable Solids
Associated Lab Samples: 92299554001
METHOD BLANK: 1746505
Associated Lab Samples: 92299554001
Parameter Units
Total Settleable Solids mUUhr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 06101/1617:10
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Results presentee on this page are In the units indicated by the "Units" column except where an attemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06103/2016 08:56 AM without the written consent of Pace Analytical Services, Inc.,
Page 12 of 19

aceAnalytical
*W..pscafaDa.aom
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
QC Batch: EDEN122995
QC Batch Method: EPA9040
Associated Lab Samples: 92299554001
SAMPLE DUPLICATE: 1746763
Parameter Units
pH Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH EDEN
92299554001 Dup
Result Result RPD Qualifiers
6.4 6.4 0 H1,H6
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Results presented on thls page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the rtght of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM without the written consent of Pace Analytical Service$. Inc . Page 13 of 19

e
ace Analytical
w viopacerabs mm
QUALITY CONTROL DATA
Project: 5131 WW Discharge 5/31
Pace Project No.: 92299554
QC Batch: RBIO16172 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL
Associated Lab Samples: 92299554001
METHOD BLANK: 1745706 Matrix: Water
Associated Lab Samples: 92299554001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU1100 mL ND 1.0 05/31/16 16:07
SAMPLE DUPLICATE: 1745707
Parameter
Fecal Coliforms
92299554D01 Dup
Units Result Result
CFUI100 mL 164 109
RPD Qualifiers
40 D6
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
Results presented an this page are fn the units indicated by the "Units" column except where an aRernatc unli Is presented to the right of the resull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM without the written consent of Pace Analytical Services, Inc.
Page 14 of 19

s
aceAnapical
r"Pscm h. corn
QUALITY CONTROL DATA
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville. NC 288U4
(828}254-7176
QC Batch: WET145278
Analysis Method:
EPA 180.1
QC Batch Method: EPA 180.1
Analysis Description:
180.1 Turbidity
Associated Lab Samples: 92299554001
METHOD BLANK: 1746596
Matrix: Water
Associated Lab Samples: 92299554001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Quatifiers
Turbidity
NTU
ND
1.0 06101/16 22:30
LABORATORY CONTROL SAMPLE: 1746597
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Turbidity
NTU
10 10
100 90-110
SAMPLE DUPLICATE: 1740598
92299534001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Turbidity
NTU
ND
ND
Results presented on this page are in the units Indicated by the "Units" column except where an ahemate unit Is presented to the fight or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 19

r
aceAnalytical"
www.pnceleb&WM
QUALIFIERS
Project: 5131 WW Discharge 5131
Pace Project No.: 92299554
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot,
ND - Not Detected at or above adjusted reporting limit,
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Dipheny[hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyi ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
06 The precision between the sample and sample duplicate exceeded laboratory control limits.
Fit Analysis conducted outside the EPA method holding time.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 08:56 AM without the written consent of Pace Analytical Services, Inc . Page 15 of 19

4 '
ace Analytical
wwwpacMabscam
DUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Servlces. Inc.
2225 Riverside Or
Asheville, NC 26804
[phone]
Project: 5131 WW Discharge 5131
Pace Project No,: 92299554
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92299554001
5131 WW GRAB
SM 2540D
EDEN122981
92299554001
$131 WW GRAB
SM 2540F
EDEN122992
92299554001
5131 WW GRAB
EPA9040
EDEN122995
92299554001
5131 WW GRAB
SM 9222D
R131016172
92299554001
5131 WW GRAB
EPA 180.1
WET145278
Date: 06/03/2016 08:56 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ,
Page 17 of 19

�PacaAnalytical n
'���+++'C+'. fYG111C. V`VVVUC IH \c•aavcVi �ur.u+�
Sample Condition Upon Rocelpt(SCUfi Page 1 of 2
Document No.: Issuing Authority:
F-RAL-CS-001'rev.05 Pace Raleigh Quality Office
Client Name: WQ# 92299554
Project
Courier. qFEdpEH ❑UPS ❑USPS CIlent �I �I' III �� I �EI
ElCommercial ❑ ce ❑Other: 92299554
Custody Seal Present? ❑Yes No Seals Intact? []Yes VrNo 2 l
4atc/Initiats Parson Examining Contents: � U�,i
Packing Material: []Bubble Wrap [)Bubble Bags PNone ❑Other:
Thermometer: IR SN:1220653g7 ❑IR SN:122065371 Typp of Ice: �Wer ❑Blue []None ❑Samples on Ice, cooling process has begun
Correction Factor: OIC Cooler Temp Corrected ('C): !!! Blotogfcal Tissue Frozen? Dyes Clio,L_,/,tj`+,/A
Temp should be above rf eling to 6*C
USDA Regulated Soli ( N/A, water sample)
Dld sampl4�s� orlglnate in a quarantine :one wlthln the United States: CA, NY, or SC (check maps)? Did samples afiginate from a foreign source {Int�ern) tiona:lY,
l�Yra ANa Ineludina Hawaii and Puerto Rica I? nYes 74-11
COMMENTS:
Chain of Custody Present?
illeS
NO
N A
1.
Chain of Custody FI lied Out?
es
No
N A
2.
Chain of Custody Relintlulshed?
es
ON6
(.:INIA
3.
Sampler Name and/or Signature on CDC?
Yes
No
H A
4
Sam piesArrived within Hold Tim e?
ulyes
ONo
N A
S.
Short Hold Time Mai sts 472 hr ?
Yes
ONO'
_ ti A
Rush Turn Around Time Re uadad7
Yes
264,
QNA
r
7.
Sufficient Volume?
14Yes
QNo
nNIA
.8.
Correct Containers Used?
{[Yes
ONO
QN/A
9.
-Pace Containers Used?
Ye,
JJN0
QNJA
Containers Intact?
Yes
ON.
❑N A
10.
Flltered Volume Received for Dissclved Tests?
Yes
No
NIA
11, Note If sedlment 1s visible In the dUsalved container
Sample labels Match COC?
Yes
ONO
❑N/A
12.
-Includes DatefFime D Ana sis Matrix:
All containers needing acid/base preservation have beery
• -'
13
checked?
E! iYes
[]NO
❑N/A
All containers needing preservation are found to be in
complianoe with EPA recommendation?
(MNO,, HrSO., HCk2; NaOH >9 Sulfide, NaOH>32 Cyanide)
Yes
[]No
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
Ws
ORO/8015 water 130C,I1H
No
EINIA
Samples checked for dechlorination
Ye,
J3N0.
❑N A
14.
Heads ace to VOA Vials >5-5mml?
Yes
No
N A
15.
Trlp Blank Present?
Oyes
ONO
N/A
15.
Trip Blank Custody Seals Present?
❑Yes
❑No
N/A
Pace Trip Blank tot p It purchased):
CLIENT NOTIPCATION/RESOLUTION
Person Contacted: Date/Tlme:
Comments/Resolutlon:
!r'
Project Manager SCURF Review: Date:
Project Manager SRF Review: J Dater
Note: whenever there Is a discrepancy affecting North Carolina compilance samples, a copy of this form will be sent to the
out of hold, lnconect preservative, out of temp, Incorrect containers)
Field Data Required? ❑Yes ❑Na
tl Carolina DEHNR Certification Office (I.e.
Page 18 of 19

aceAnalyti5 6
r � wti«w.pasalabs.com
r
6701 Conterenoe Dr1ve. Raleigh, NC 2760T
ph: (919) 93"984, fax: (919) 834-M7
NCWW Cert#67, NCDW CeA47731
Report Results To:
Chain of Custody W.O.#
Company: -! .4.
Address: IL71 —41�a�.J 2!.
Phone:
Fax:1�µNcC-� wort
Sampled by (sfgnature):
Bill To:
Project Reference: V3i W MI
Project dumber.
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (wlsufchargo)
"Flush projects aro au*6 to Prior apptaval by
the laboratory'
Requested Due Date:
7 sc►t1Cr.(S1C SoJlJs� rSS� '�/�JJi j'J
ReJir►qu: by (sfgnatare)
ate 3� ``}}
t u
Time
R by {signature)
Received by (slgnarire)
D to
Time
Relinquished by (signaiurs)
Romtved by (elgnahrs)
Data
Time
Racoipt ConclMons { U Only)
❑ 4 kVC ❑ TCmp. °C
Res, Chlorine:
❑ Absent ❑ Present ❑ n!a
Acid presay. <27
❑ Yes ❑ No ❑ r11a
Base preserv. >12?
❑ Yes ❑ No ❑ rva
9
Page 19 of 19

T.- , _.
aceAnalytical"
w"pacetsDs com
March 31, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Wastewater Discharge -march
Pace Project No.: 92291594
Pace Analytical Services. Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
N & &- 0 a- 0 3 sy
9,GvE-NED
3�,t4 31 ZV
GENTR ION
pWR S_
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on March 28, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
christopher,[e-mail]
Project Manager
Enclosures
cc: Collin Mummert, Charah Inc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 1 of 19

a
aceAnalytical
www.peoWM&cam
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Raleigh Certification iDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 633
VirginialVELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Pace Analytical Services, Ina.
2225 Riverside Dr
Asheville, NO 28804
t828j254-7176
Page 2 of 19

1
acmnaiytlCai *
wwwpacefaba mm
SAMPLE ANALYTE COUNT
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
Lab ID Sample ID Method
Analysts
Analytas
Reported Laboratory
92291594001 WW Discharge SM 2130B
CHM
11 PASI-E
SM 2540D
KCE
1 PASI-E
SM 254OF
CHM
1 PASI-E
EPA 9040
DWJ
1 PASI-E
SM 9222D
RC
1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. Page 3 of 19

ace Analytical
wMwpecelebSoom
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Lab Sample ID Client Sample ID
Method Parameters
92291594001 WW Discharge
SM 2130B Turbidity
SM 2540D Total Suspended Solids
EPA 9040 pH
Pate Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY Of DETECTION
Result Units Report Limit Analyzed Qualifiers
33.3 NTU 0.50 031291% 10:50
23.9 mglL 2.5 03/291161114
6.5 Std. Units 0.10 03/29/16 11:00 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 4 of 19

aceAnalytical
( wwwpacelabscom
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville. NC 28804
[phone]
PROJECT NARRATIVE
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Method: SM 2130B
Description: 2130B Turbidity EDN
Client: Charah
Date: March 31. 2016
General Information:
1 sample was analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noled below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank,
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 19

aceAnalXical
wrrw.pacelabacam
PROJECT NARRATIVE
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Date: March 31, 2016
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below,
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits wilh any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN122282
D6: The precision between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1696856)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„ Page 6 of 19

laceAnalytical
www.pesdsbs m+n
PROJECT NARRATIVE
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Method: SM 2540F
Description: 2540E Total Settleable Solids
Client: Charah
Date: March 31. 2016
Pace Analytical Sorvices, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or an the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of ttlis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analyles were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„ Page 7 of 19

acmnalytical
www.pec91abs oom
PROJECT NARRATIVE
Project: Wastewater Discharge -march
Pace Project No.' 92291594
Method: EPA 9040
Description: 9040 pH
Client: Charah
Date: March 31. 2016
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H6: Analysis initiated outside of the 15 minute EPA required holding time.
• WW Discharge (Lab ID: 92291594001)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below,
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below,
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,. Page 8 of 19

e
acmnalydical
www.pacafabs com
PROJECT NARRATIVE
Project: Wastewater Discharge -march
Pace Project No,: 92291594
Method: SM 9222D
Description: MBIO 92220 Fecal Coliform RAL
Client: Charah
Date: March 31, 2016
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
General Information:
1 sample was analyzed for SM 9222D- All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below,
Initial Calibrations (Including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below,
Surrogates:
All surrogates were within QC limits with any exceptions noted below,
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below,
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below,
DuplicateSample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc . Page 9 of 19

aceAnalyfical•
»rw.p&0VW&mm
I
ANALYTICAL RESULTS
Project: Wastewater Discharge -march
Pace Project No.: 92291594
Pace Analytical Services, Ini.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
Sample: WW Discharge
Lab ID: 92291594001 Collected: 03/28116 12:00
Received: 03128/16 16:05 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qua1
2130B Turbidity EDN
Analytical Method: SM 2130B
Turbidity
33.3 NTU
0.50
1
03/29/1610750
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
23.9 mg1L
2.5
1
03129/16 11:14
254OF Total Settleable Solids
Analytical Method: SM 254OF
Total Settleable Solids
NO MUUhr
0.10
1
03/29/16 09:30
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units
0.10
1
03/29/16 11:00 H6
IIIICilO 92220 Fecal Coliform RAL
Analytical Method: SM 9222D
Fecal Coliforms
NO CFU1100 mL
1,0
t
03128/16 16:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/31/2016 03:00 PM without the written consent of Pace Analytical Services. Inc.
Page 10 of 19

r
lacieAnalytical
.pacelatucom
QUALITY CONTROL DATA
Project: Wastewater Discharge -march
Pace Project No.. 92291594
QC Batch: EDEN122283 Analysis Method: SM 2130B
QC Balch Method: SM 2130B Analysis Description: 2130E Turbidity EDN
Associated Lab Samples: 92291594001
METHOD BLANK: 1696876 Matrix: Water
Associated Lab Samples: 92291594001
Parameter
Turbidity
SAMPLE DUPLICATE: 1696877
Parameter
Turbidity
Blank Reporting
Units Result Limit Analyzed Qualifiers
NTU ND 0.50 03129/1610:50
92291594001 Dup
Units Resuit Result RPD Qualifiers
NTU 33,3 32.3 3
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
{B28}254-7176
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03131 /2016 03:00 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 19

� r
a
aceAnalytical
www.poewabscom
QUALITY CONTROL DATA
Project: Wastewater Discharge -march
Pace Project No.'. 92291594
QC Batch: EDEN122282 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92291594001
METHOD BLANK: 1696854 Matrix: Water
Associated Lab Samples: 92291594001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 03I29/16 11:08
Pace Analytical Services, Inc.
2225 Riverside Or
Asheville. NC 28804
(B28)254-7176
LABORATORY CONTROL SAMPLE: 1696855
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 226 90 90-110
SAMPLE DUPLICATE: 1696856
92291547001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 28.6 31.2 9 D6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03l3112016 03:00 PM wilhout the written consent of Pace Analytical Services, Inc. Page 12 of 19

a
aceAnalytical
www.pacelabEoam
QUALITY CONTROL DATA
Project: Wastewater Discharge -march
Pace Project No.: 92291594
QC Batch: EDEN122280 Analysis Method: SM 254OF
QC Batch Method: SM 2540F Analysis Description: 254OF Total Settable Solids
Associated Lab Samples: 92291594001
METHOD BLANK: 1696736
Associated Lab Samples: 92291594001
Parameter Units
Total Settleable Solids mUUhr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.10 03129l16 09:30
SAMPLE DUPLICATE: 1696737
92291594001 DUp
Parameter Units Result Result
Total Settleable Solids mUUhr NO NO
RPD Qualifiers
Pace Analytical Services. Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
Results presented on this page are In the units Indlcated by the "Units" column except where an etlemate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03131/2016 03:00 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 19

aceAnalytical
wwwpacdabs can
Project: Wastewater Discharge -march
Pace Project No.: 92291594
QC Batch: EDF-N122284
QC Batch Method: EPA 9040
Associated Lab Samples: 92291594001
SAMPLE DUPLICATE: 1696945
Parameter Units
pH
Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH EDEN
92291594001 Dup
Result Result RPD Qualifiers
6.5 6.5 0 H6
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/31/2016 03:00 PM without the written consent of Pace Analytical Services, Inc_
Page 14 of 19

aceAnalytical.
wwwpacNabs tam
Project: Wastewater Discharge -march
Pace Project No.: 92291594
QC Batch: RBI016053
QC Batch Method: SM 9222D
Associated Lab Samples: 92291594001
METHOD BLANK: 1696802
Associated Lab Samples: 92291594001
Parameter Units
Fecal Coliforms CFU1100 mL
SAMPLE DUPLICATE: 1696803
Parameter
Fecal Cotiforms
QUALITY CONTROL DATA
Analysis Method: SM 9222D
Analysis Description. 9222D MBIO Fecal Coliform - RAL
Malrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 03/281161626
92291597001 Dup
Units Result Result RPD Qualifiers
CFUI100 mL 82.0 82.0 0
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28864
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/3112016 03:00 PM without the written consent of Pace Analytical Services, inc_,
Page 15 of 19

e
aceAnalytical
www pscwhbi cam
QUALIFIERS
Project: Wastewater Discharge -march
Pace Project No,: 92291594
DEFINITIONS
Pare Analytical Services, Inc:
2225 Riverside pr
Asheville, NC 28804
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit,
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RP❑ values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vnyt chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a Combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
>ET%T:7_1111ite]:fN&I
PASI-E Pace Analytical Services - Eden
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 03131 /2016 03:00 PM without the wrinen Consent of Pace Analytical Services, Inc . Page 16 of 19

ace Analytical*
*" Paceiab&m"
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
(B28)254.7176
Pr6;ectT Wastewater Discharge -march
Pace Project No,: 92291594
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92291594001
WW Discharge
SM 2130B
EDEN122283
92291594001
WW Discharge
SM 2540D
EDEN122282
92291594001
WW Discharge
SM 254OF
EDEN122280
92291594001
WW Discharge
EPA 9040
EDEN122284
92291594001
WW Discharge
SM 9222D
13131016053
Date: 03131/2016 03:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, tnc.,
Page 17 of 19

DRCUment Name: Uocurnent iievrsea: [brtU2U1O
__ Sa_mpin Condition Upon Receipi(SCUR)�— Page 1 of 2
�lCt f{f1ciICa�• Document No.,. F� Issuing Authority:
F-RAL-CS-001-rev.05 I Pace Raleloh Quality Office E
Parr. 2 of 2 for Intemal Use ONLY
• Client Name: Project ri WO# : 92291594
p
Courier: []Fed Ex ❑UPS ❑LISPS Client 11111111111111
Commercial ❑Pace ❑Other:
92291594
Custody Seal Present? []Yes 0No Seals Intact? Dyes No
[)ate/rnitlals Person Examining Contents'J-0 1 f
Packing Material: ❑Bubhle wrap ❑t3utr61e Bags [�Nnne❑Other. t
Thermometer: iRSN:1220GS387 ❑in so%12206S371 7 eofIce: tlI%Vet ❑81ue ❑None❑Sampies onice, coolingprrsetshas begun
Correction FactorAT Cooler Temp Corrected (.Cl
Bialagical Tissue Frozen? []Yes ❑No [I/A
Temp should be above fr ezing to 6'C
USDA Regulated Soil ( N/A, water sample)
Did sarnple originate Ina quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples 069ihate From a foreign source linteerr)abona€ly,
nYes No Indudlnv Hawaii and Puertn Rlcol? rlws I 6
COMMENTS:
Chain Of Custody Present?
Yes
QNo
OPIA
1.
Chain of Custody Filled Out?
es
❑rao
N!A
2.
Chain of Custcdy Relinquished?
Yes
❑No
❑N/A
3.
Sam Eer Name and/or S1 nature on COC7
Yes
QNo
N/A
4.
Samples Arrived within Hold Time?
Yes
Na
❑N/A
S.
Short Hold Time Anal is (472 hr ?
yes
ONG
❑N/A
b. WYJV- V Y✓ .
Rush Turn Around Time Requested?
Yes
hNo
N/A
7.
Sufficient Volume?
QlYes
No
N/A
B.
Correct Containers Used?
-Pace Containers Used?
Yes
ONO
QNo
❑N/A
QNjA
9.
Containers Intact?
Yes
Ohio
N/A
10.
Filtered Volume Received for Dissolved Tests?
❑Yes.
No
N A
11. Nate if sediment is visible In the dissolved container
Sample Labels Match COC?
-includes Date/Time rD/Analysis Matrb:
0Yes
❑No
❑N/A
12.
All containers needing acid/base preservation have been
checked?
Ali containers needing preservatioh are found to be to
compliance with EPA recommendation?
(HNO1, H2504, HCIc2; Na0H s9 Sulfide, NaOH>12 Cyanide)
Exceptions. VOA, Conform, TOC, Oil and Grease,
DRO/8015 water)DOC,LLHg
r-k.
T
Yes
�es
ONO
ONO
ONO
❑N/A
❑N/A
CHIA
13
Samples checked for dechlorinatlon
0yes
Utto
NIA
14.
Heads ceInVOAVials >5•6mm?
QY.
❑No
N/A
15.
Tiip Blank Present?
Trip Blank Custody Seals Present?
Pace Trip Blank Lot tl If purchasedy
❑Yes
❑Yes
ONO
❑No
N/A
NIIN
16.
CLIENT NOTIFICAPON/RESOLUTION
Person Contacted:
Como cents/Re silutloe:
Project Manager SLJRF Review: W
Projed Manager SRF Review: ell_
Note: Whenever there Is a discrepancy affeeting North c�arcliina compllar,
Out of hold, Incorrect preservative,(out of temp, Inrorn.ct cuntatnen)
Field data Raquired? []Yes ❑No
y of :is form ent to the rW=1/ "EkNR C - it ladon Office {I
Page 18 of 19

e
ace Arrafytical
�' urair.paeal0he.aom
6701 Conlerem a Drive, Raleigh, NC 27607
pig: (9 i.9) ON AW4, fait'. ,•i F (919) SM67
NCWW Cert#67, NCDW CertAr Ml
Chaim of Custody
Report Results To:
Company: _o>�-h+ -►I�.
Address:.f.Z71 ir�ZGtlr"L -h��t'Wlr�1
Phone: !r04-`os- 5z jD
Fax: K�JA rt�r�—�-�lAc �r iti_. curt
Sampled by (signature):
Bill To:
Project Relorenae:
�,54)14f I �G-r�11
Project Number:
Purchase Order #:
❑ Standard Report Delivery
❑ Rush Report Delivery (w/surcharge)
"Rush pr*05 aro .ubjw to phoi approval by
the UtWatory
Requested Due Date:
Reltnqui by (slgnaitae)
kR:aowo&K,,od(E'l&re)
yatel
ate
Time
Time
Rel by (signature)
Received by (eignatu )
Flelinqulahed by (slgnaaxe)
Received by (signature)
Date
lime
Fieceipt GonMons (L9 Vnly)
❑ 4t2C ❑Temp: °C
Res. Chlorine:
❑ Absent ❑ Present ❑ rVa
Add preserv. c2?
❑ Yes ❑ No ❑ rVa
Base preserv. >127
❑ Yes ❑ No ❑ nla
Page 19 of 19

.f'
aceAnalyiical.
wwwp"abs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
January 14, 2016
Glenn Amey
Charrah
330 S Tryon St
Suite 510
Charlotte, NC 28202
RE: Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Pccr- <5 ---) 3's- -//
RECEIVED
JAN 3 1 2017
CENTRAL FILES
DWR SECTION
Dear Glenn Amey:
Enclosed are the analytical results for sample(s) received by the laboratory on January 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Enclosures
=��Q pCCRfQ��FG
9g RAT9�r
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 19

laceAnalyfical.
wwwpacelabs.cam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevifle, NC 28804
[phone]
Project: Sed Basin 7 1/7
Pace Project No.: 92282272
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Eden Certification lDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2of19

t
Pace Analytical Services, Inc.
aceAnalXical
2225 Riverside
04
AsheviAe, NC 28804
www.pacelabs.com
[phone]
SAMPLE ANALYTE COUNT
Project: Sed Basin 7 117
Pace Project No.: 92282272
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92282272001 SED 7
SM 2130B
DWJ
1 PASI-E
SM 2540D
CHM
1 PASI-E
SM 2540F
DWJ
1 PASI-E
EPA 9040
KCE
1 PASI-E
SM 9222D
RC
1 PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 19

l
ace Analytical
wwwpacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SUMMARY OF DETECTION
Project: Sed Basin 7 117
Pace Project No.: 92282272
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92282272001
SED 7
SM 2130B
Turbidity
9.6
NTU
0.50
01/08/16 11:10
SM 25401)
Total Suspended Solids
7.9
mg/L
2.5
01/08/16 11:27
EPA9040
pH
4,2
Std. Units
0.10
01/0811611:47 H6
SM 9222D
Fecal Coliforms
4.0
CFU1100 mL
1.0
01/07/16 16:20 1g
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 19

aceAnalytical
www.pacebhs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashe0le, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 117
Pace Project No.: 92282272
Method: SM 2130B
Description: 2130E Turbidity EDN
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 2130B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andlor the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
AA analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 19

aceAnaiytical
www.pacefabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 117
Pace Project No.: 92282272
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Charah
Dale: January 14, 2016
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC Limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: EDEN121359
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1643609)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 19

acmnalXical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 117
Pace Project No.: 92282272
Method: SM 2540F
Description: 2540E Total Settleable Solids
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 2540F. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below,
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 19

aceAnalj&al
www.pacolabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 117
Pace Project No.: 92282272
Method: EPA 9040
Description: 9040 pH
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1-16: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SED 7 (Lab ID: 92282272001)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 19

aceAnalytical
wwwpasefabs.c=
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Project: Sed Basin 7 117
Pace Project No.: 92282272
Method: SM 9222D
Description: MB10 9222D Fecal Coliform RAL
Client: Charah
Date: January 14, 2016
General Information:
1 sample was analyzed for SM 9222D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody andlor the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
Alt internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank.
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: RB1016848
19: This is a less than value
• SED 7 (Lab ID: 92282272001)
• Fecal Coliforms
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 19

1
Pace
Analytical Services, Inc.
aceAnalytical"
2225 Riverside Dr.
Asheville, NC 2880404
www.pacelabs.com
(828 )254-7176
ANALYTICAL RESULTS
Project: Sed Basin 7 117
Pace Project No.: 92282272
Sample: SED 7
Lab ID: 92282272001 Collected: 01/07/16 12:00
Received: 01/07/16 16:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
2130B Turbidity EDN
Analytical Method: SM 2130B
Turbidity
9.6 NTU
0.50
1
01108/1611:10
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7.9 mg/L
2.5
1
01/08/16 11:27
254OF Total Settleable Solids
Analytical Method: SM 2540F
Total Settleable Solids
ND mL/L/hr
0.10
1
01/08/16 11:10
9040 pH
Analytical Method: EPA 9040
pH
4.2 Std. Units
0.10
1
01/08/16 11:47
H6
MBIO 9222D Fecal Coliform RAL
Analytical Method: SM 9222D
Fecal Coliforms
4.0 CFU/100 mL
1.0
1
01/07/16 16:20
1g
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 19

aceAnalXical
wwwpacelabs.cam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 117
Pace Project No.: 92282272
QC Batch: EDEN121357 Analysis Method: SM 2130B
QC Batch Method: SM 2130B Analysis Description: 2130E Turbidity EDN
Associated Lab Samples: 92282272001
METHOD BLANK: 1643578 Matrix: Water
Associated Lab Samples: 92282272001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Turbidity NTU ND 0.50 01108/1611:10
SAMPLE DUPLICATE- 1643579
92282272001 Dup
Parameter Units Result Result
Turbidity NTU 9.6 9.6
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 19

t9
aceAnalytical
www.pacelabs.00m
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 117
Pace Project No.: 92282272
QC Batch: EDEN121359 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92282272001
METHOD BLANK: 1643607 Matrix: Water
Associated Lab Samples: 92282272001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 01/08/16 11:26
LABORATORY CONTROL SAMPLE: 1643608
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 242 97 90-110
SAMPLE DUPLICATE: 1643609
92282233001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 72.0 67.2 7 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 19

ace Analytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 117
Pace Project No.: 92282272
QC Batch: EDENI21356 Analysis Method: SM 254OF
QC Batch Method: SM 254OF Analysis Description: 254OF Total Settable Solids
Associated Lab Samples: 92282272001
METHOD BLANK: 1643576
Associated Lab Samples: 92282272001
Parameter Units
Total Settleable Solids mL/Llhr
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 01/081161110
Results presented on this page are in the units indicated by the "units" column except whore an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc..
Page 13 of 19

aceAnalytical
www pacefabs, tern
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 117
Pace Project No.: 92282272
OC Batch: EDEN121361 Analysis Method: EPA 9040
OC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92282272001
SAMPLE DUPLICATE: 1643679
Parameter
pH
92282272001 Dup
Units Result Result RPD Qualifiers
Std. Units 4.2 4.2 0 H6
Results presented on this page are in the units indicated by the "Units" column except where an alternato unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 19

aceAnaiXical.
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Sed Basin 7 117
Pace Project No.: 92282272
QC Batch: RBIO15848 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - RAL
Associated Lab Samples: 92282272001
METHOD BLANK: 1643328 Matrix: Water
Associated Lab Samples: 92282272001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU1100 mL ND 1 A 01/07/16 15:35
SAMPLE DUPLICATE: 1643329
92282231001 Dup
Parameter Units Result Result RPD Qualifiers
Fecal Coliforms CFU1100 mL 6.0 17.0 96
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc..
Page 15 of 19

aceAnalytical
www.pacelabs.=
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALIFIERS
Project: Sed Basin 7 117
Pace Project No.: 92282272
DEFINITIONS
DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit,
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
1g This is a less than value
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /14/2016 10:33 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19

w
aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Sed Basin 7 117
Pace Project No,: 92282272
Lab ID
Sample ID
QC Batch Method
QC Batch
92282272001
SED 7
SM 2130B
EDEN121357
92282272001
SED 7
SM 2540D
EDEN121359
92282272001
SED 7
SM 254OF
EDEN121356
92282272001
SED 7
EPA 9040
EDEN/21361
92282272001
SED 7
SM 9222D
RB1015848
Date: 01/14/2016 10:33 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical Method
Analytical
Batch
Page 17 of 19

4
aoAnalytt{cal a
r
www.pacelaba.cam
6701 Conferenoe Ddve, Raleigh, NC 27607
ph: [phone],1w [phone]
NCWW CerW67, NCDW Certk37731
Report Results To:
Company:
Chain ®f Custody W.O.#
Address: 17-71
Attn: -6 11 ice .y egAj-e-k
Phone: SL-1S9-- „--6r1
Fax: CFNy srCr h k e-0
Sampled by (signature):
Bill To:
Protect Reference: 542 "; n :7 _
rn�
Project Number:
Purchase Order#:
O Standard Report Delivery
❑ Rush Report Delivery (wlsurcharge)
"Rush proloc is are subject to prior approval by
the laboratory
Requested Due Date:
Paae 18 of 19

It
Document Name: r Document Revised: 26OCT2015
aceAnaical Sample Condition Upon Receipt(SOUR) Page 1 of 2
Document No.: Issuing Authority:
r F-RAL-CS-001-rev.03 Pace Huntersville Quality Office .
amClient Name: Project if: i W® • 92282272
Courier: ❑Fed Ex . ❑UPS ❑USPS VCllent I 111111
IIHIII I�I� III
❑Commercial ❑Pace ❑Other. i 92282272
Custody Seal on Cooler/Box Present? ❑Yes EIo Seals Intact? ❑Yes PKo l
Packing Material. El Bubble Wrap []Bubble Bags None ❑other:
h AIRGunSN:122065387
T ermometer
Used: ❑ IR Gun SN:122065371 Type of ice: [ivet ❑Blue [3NOne []Samples on Ice, cooling process has begun
Cooler Temp Corrected ('C): k � TTTT Blologlcal Tissue Frozen? ❑Yes []NO NfA
Temp should be above fre zing to 6'C Correction Factor: 0.0 •C Date and Initials of Person Examining Contents 1
USDA Regulated Soll ( " N/A, water sample)
Did sampies �onBInate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (internationally,
❑Yc5 LdNo including Hawall and Puerto Rico)? ❑Yes �No
If Yes to either question, fill out a Regulated $oil Checklist and Include with $CUR/COC paperwork,
COMMENTS:
Chain of Custody Present?
yes
ONO
Q NIA
1.
Chain of Custody Filled Out?
Yes
ONo
QNLA
2.
Chalri of Custody Relinquished?
es
QNo
ONIA
3.
Sampler Name and/or Signature on COCT
Yes
Ono
N A
4.
Samples Arrived within Hold Time?
Yes
No
N A
S.
Short Hold Time Analysis <72 hr)7
Yes
ONO
JatNA..
6,
Rush Turn Around Time Requested?
0yes
No
QNIA
7.
Sufficient Volume?
CAYes
No
N A
8.
Correct Containers Used?
-Pace Containers Used?
t
ONO
No
[:]N/A
N A
9.
Containers Intact?
Yes
❑No
❑N/A
10.
Filtered Volume Received for Dissolved Tests?
Yes
No
N A
11. Note If sediment is vlslble In the dissolved container
Sample labels Match COC?
-Includes Date/Time/1D Anai sis Matrlx:
(Yes
I
ONO
(:]N/A
12.
All containers needing acld/base preservation have been
checked?
All containers needing preservation are found to be In
compliance with EPA recommendation?
(HNO,, HiSO4, HCl<2; NaCIH >9 Sulflde, NaOH>12 Cyanide)
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLH
IiYes
T
Yes
Yes
❑No
❑No
No
❑N/A
❑NIA
[]N/A
13
Samples checked for dechlorizatlon
19yes
No
A
14.
Headspace In VOA Vials (>5.6mm)?
byes ,
ONO
N/A
1S.
Trip Blank Present?
Trip Blank Custody Seals Present?
Pace Trip Blank Lot #i (ifpurchased):
Oyes
©Yes
ONO
❑No
NIA
gN/A
16.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Resolutlon:
Date/Time;
Field Data Required? Dyes ❑No
Project Manager SCURF Review: Date:
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form wtil be sent to the tf rth,rotlna UEHNR Certtflcattan Office (Le. out of
hold, Incorrect preservative, out of temp, Incorrect containers). /

Energy, Mineral
and Land Resources
ENVInd NMENTAL QUALITY
November 15, 2016
Green Meadow LLC
Attw Charles Price
12601 Plantside Drive
Louisville, Kentucky 40299
Subject: COMPLIANCE EVALUATION INSPECTION
NPDES Stormwater General Permit NCG020000
Company
Brickhaven 2A, Certificate of Coverage NCG020354
Chatham County
Dear Mr. Price:
PAT' MCCRORY
Governor
DONALD R, VAN DER VAART
Secretary
TRACY DAVIS
U7reclor
On November 10, 2016, a site inspection was conducted for the Brickhaven No 2 Mine Tract "A" facility located at 1149
Flatwood Road, Moncure, Chatham County, North Carolina. A copy of the Compliance Inspection Report is enclosed for
your review. Glenn Amey as well as other staff were also present during the inspection and their time and assistance is
greatly appreciated. The site visit and file review revealed that the subject facility is covered by NPDES Stormwater
General Permit NCG020000, Certificate of Coverage NCG020354. Permit coverage authorizes the discharge of
stormwater from the facility to receiving waters designated as an unnamed tributary to Gulf Creek in the Cape Fear River
Basin.
As a result of the inspection, the facility was found to be in compliance with the conditions of the NCG020000 permit.
Please refer to the enclosed Compliance inspection Report for additional comments and observations made during the
inspection.
Please be advised that violations of the NPDES Stormwater General Permit are subject to a civil penalty
assessment of up to $25,000 per day for each violation. if you or your staff has any questions, comments, or needs
assistance with understanding any aspect of your permit, please contact me at [phone] or by e-mail at
[e-mail].
Sincerely,
CS144.- k"---
C. Diane Adams
Sr. Environmental Specialist
Enclosure
cc: Jeremey J. Kerly, P.G., Environmental Protection Specialist 11 `Charah, Inc (email)
Glenn Amey, PG, Engineering Manager JCharah, Inc (email)
(_RR MLR—Sto mmwate—CFi]6s-NCG0200 0
RRO- Land -Quality -files
State of North Carolina I Environmental Quality I Energy, Mineral and Land Resources
Raleigh Regional 0fricel628 Mail Service Center, Raleigh, North Carolina 27699-1628
Phone: [phone] / PAX: 919-571-47181 Internet: http:l/portal,ncdenr.org/"ch/ir/
An Equal Opportunity 1 Affirmative Action Employer— 50% Recycled 1 10% Post Consumer Paper

Permit: NCG020354
SOC:
County: Chatham
Region: Raleigh
Contact Person: Steve Wyse
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
Compliance Inspection Report
Effective: 10/01/15 Expiration: 09/30/20 owner: Green Meadow LLC
Effective: Expiration: Facility: Brickhaven No. 2 Mine Tract "A"
1149 Flatwood Rd
Moncure NC 27559
Title: Phone: [phone]
Certification:
Phone:
FA
On -Site Representative(s):
Related Permits:
Inspection Date: 11/10/2016
Primary Inspector Carolyn D Adams
Secondary Inspector(s):
Entry Time: 10:OOAM Exit Time: 11:00AM
Phone:
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Mining Activities Stormwater Discharge COC
Facility Status: Compliant Not Compliant
Question Areas:
■ Storm Water
(See attachment summary}
Page: 1

W
0
Permit: NCGO20354 owner -Facility: Green Meadow LLC
Inspectlon Date: 11110/2016 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
Brickhaven appears to be utilizing the pollution prevention plan and making appropriate updates. Analytical and qualitative
monitoring reports were readily available and being conducted per the permit requirements, No violations were observed
during this inspection and all outfalls were inspected/observed.
Page: 2

Permit: NCG020354 Owner - Facility: Green Meadow kLC
Inspection Date: 11110/2016 Inspection Type; Compliance Evaluation Reason for Visit -Routine
I
Analytical Monitoring Yes No NA NE
Has the facility conducted its Analytical monitoring? ®❑ ❑ ❑
# Has the facility conducted Its Analytical monitoring from Vehicle Maintenance areas? ❑ ❑ ® ❑
Comment: Analytical records were available.
Permit and Outfalls Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? E ❑ ❑ ❑
# Were all outfalls observed during the inspectlon? ■ ❑ ❑ ❑
# If the facility has representative outfall status, Is it property documented by the Division? Cl ❑ ® ❑
# Has the facility evaluated all illicit (non stormwater) discharges? ■ ❑ ❑ ❑
Comment: Outfalls were observed and no violations noted.
Qualitative Monitorinct Yea No NE
Has the facility conducted Its Qualltative Monitoring semi-annually? ®❑ ❑ ❑
Comment: Qualitative monitoring records were available.
Stormwater Pollution Prevention Plan
Yes No NA HE
Does the site have a Stormwater Pollutlon Prevention Plan?
®❑ ❑ ❑
# Does the Plan Include a General Location (USGS) map?
®❑ ❑ ❑
# Does the Plan include a "Narrative Description of Practices"?
❑ ❑ ❑
# Does the Plan include a detailed site map Including outfall locations and drainage areas?
®❑ ❑ ❑
# Does the Plan Include a list of significant spills occurring during the past 3 years?
®[] ❑ El
# Has the facility evaluated feasible alternatives to current practices?
®❑ ❑ ❑
# Does the facility provide all necessary secondary containment?
®❑ ❑
# Does the Plan include a BMP summary?
®❑ ❑ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
®❑ ❑ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
®❑ ❑ ❑
# Does the facility provide and document Employee Training?
®❑ ❑ ❑
# Does the Plan include a list of Responsible Party(s)?
®❑ ❑ ❑
# Is the Plan reviewed and updated annually?
®❑ ❑ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
®❑ ❑ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
®❑ ❑ ❑
Page 3

permit. NCGO20354 owner -Facility: Green Meadow LLC
Inspection Date: 11/10/2018 Inspection Type. Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan Yes No NA NE
Comment: The facility had on site a stormwater pollution prevention plan. The plan has been appropriately
implemented and is routinely being updated. Appropriate training has been provided.
Page: 4

1H
9 pa_;V�
.11A
MCDENR
North Carolina Department of Environment and Natural Resources
Pal McCrory
Governor
June 5, 2015
Mr. Charles Price
Green Meadow, LLC
12601 Plantside Drive
Louisville, Kentucky 40299
RE: Mining Permit No. 19-25
Brickhaven No. 2 Mine Tract "A"
Chatham County
Cape Fear River Basin
Dear Mr. Price:
Donald R. van der Vaart
Secretary
Your application for renewal and modification of the above referenced mining permit has
been approved. The modification is to redesign the erosion and sedimentation control
measures throughout the site and reduce the affected acreage to 267 acres as indicated on
the Mine Maps last revised December 31, 2014. The modification also includes changing the
method for reclaiming the mine by constructing structural fill using Coal Combustion
Byproducts (GCBs) in accordance with the provisions of the Coal Ash Management Act of
2014 and the terms and conditions of Permit to Construct and Operate Brickhaven No. 2 Mine
Tract "A° Mine Structural Fill Permit No. 1910-STRUC-2015 issued by the Division of Waste
Management on ,tune 5, 2015. A copy of the renewed and modified mining permit is enclosed.
The new expiration date is June 5, 2025.
The conditions in the renewed and modified permit were based primarily upon the initial
application. Modifications were made as indicated by the renewal and modification requests
and as required to insure compliance with The Mining Act of 1971. f would like to draw your
particular attention to the following conditions where minor additions or changes were made:
Operating Condition Nos. 1 B, 1 C, 3C, 3D, 4B, 4C, 5, 10B, and 12A and Reclamation Condition
Nos. 1, 2A, 2E, 3, 4A and 4B.
G.S. 74-65 states that any actions taken under the Mining Act of 1971, such as the
issuance of mining permits, shall not be construed to supersede or otherwise affect or prevent
the enforcement of any zoning regulation or ordinance duly adopted by an incorporated city or
county or by any agency or department of the State of North Carolina, except insofar as a
provision of said regulation or ordinance is in direct conflict with the Mining Act of 1971. Thus,
the responsibility of compliance with any applicable zoning regulations lies with you.
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
512 North Salisbury Street, Raleigh, North Carolina 27604 - lnternet: htt :11 ortal.ncdecv.oralvlebllrl
Mailing Address: 1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707.92001 FAX [phone]
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled l 10% Post Consumer Paper

9
Mr. Price
Page Two
As a reminder, your permitted acreage at this site is 301 acres and the amount of land
you are allowed to disturb is 267 acres.
Please review the renewed and modified mining permit and contact Ms. Judy Wehner,
Assistant State Mining Specialist, at [phone] should you have any questions
concerning this matter.
Siyfcerely,
Mavis, PE, CPM
Dir to
Division of nergy, inera , a
TE D/jw
Enclosures
cc: Mr. John Holley, PE, DEMLR Raleigh Regional Office Supervisor
Mr. Bradley Bennett, DEMLR Stormwater Permitting Supervisor
Ms. Janet Boyer, PE, DEMLR State Mining Specialist
Mr. Ed Mussler, PE, Division of Waste Management Permitting Supervisor
Mr. Jay Zimmerman, Director, Division of Water Resources
Mr. William Gerringer-Mine and Quarry Bureau, w/o enclosures

DEPARTMENT OF ENVIRONMENT
AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL AND LAND RESOURCES
LAND QUALITY SECTION
PERMIT
for the operation of a mining activity
In accordance with the provisions of G.S. 74-46 through 68, "The Mining
Act of 1971," Mining Permit Rule 15A NCAC 5 B, and other applicable
laws, rules and regulations
Permission is hereby granted to:
Green Meadow, LLC
Brickhaven No. 2 Mine Tract "A°
Chatham County - Permit No. 19-25
for the operation of a
Clay Mine
which shall provide that the usefulness, productivity and scenic values of
all lands and waters affected by this mining operation will receive the
greatest practical degree of protection and restoration_
MINING PERMIT EXPIRATION DATE: .tune 5, 2025

Page 2
In accordance with the application for this mining permit, which is hereby approved by the
Department of Environment and Natural Resources, hereinafter referred to as the Department,
and in conformity with the approved Reclamation Plan attached to and incorporated as part of
this permit, provisions must be made for the protection of the surrounding environment and for
reclamation of the land and water affected by the permitted mining operation. This permit is
expressly conditioned upon compliance with -all the requirements of the approved Reclamation
Plan. However, completed performance of the approved Reclamation Plan is a separable
obligation, secured by the bond or other security on file with the Department, and may survive
the expiration, revocation or suspension of this permit.
This permit is not transferable by the permittee with the following exception: If another
operator succeeds to the interest of the permittee in the permitted mining operation, by virtue
of a sale, lease, assignment or otherwise, the Department may release the permittee from the
duties imposed upon him by the conditions of his permit.and by the Mining Act with reference
to the permitted operation, and transfer the permit to the successor operator, provided that
-.---both.operators have complied with the requirements of the Mining Act and that the successor
operator agrees o assume h— du ies of -the permittee with-reference-tcFrmlamatio[t of th
affected land and posts a suitable bond or other security.
In the event that the Department determines that the permittee or permittee's successor is not
complying with the Reclamation Plan or other terms and conditions of this permit, or is failing
to achieve the purposes and requirements of the Mining Act, the Department may give the
operator written notice of its intent to modify, revoke or suspend the permit, or its intent to
modify the Reclamation Plan as incorporated in the permit. The operator shall have right to a
hearing at a designated time and place on any proposed modification, revocation or
suspension by the Department. Alternatively and in addition to the above, the Department
may institute other enforcement procedures authorized by law.
Definitions
Wherever used or referred to in this permit, unless the context clearly indicates otherwise,
terms shall have the same meaning as supplied by the Mining Act, N.C.G.S. 74-49.
Modifications
October 5, 1995: This permit has been modified to increase the affected acreage from 17
acres to 83.5 acres, approve the pit expansion and the upgrading of the associated sediment
and erosion control measures as per the Mine Site Map dated August 27, 1995, and allow
modification to the spray irrigation system as approved by the Division of Water Quality.
August 2 1996: This permit has been modified to change the corporate name from Cherokee
Sanford Group, Inc. to Cherokee�Sanford Group, LLC.
September 24 1998: This permit has been modified to allow the temporary use (two year
approval) of Photafloc polymer for enhanced sediment control experimentation purposes, with
stipulations as outlined in the approval letter.

Page 3
November 4, 1999: This permit has been modified to increase the affected acreage at the site
to 337 acres as indicated on the mine map dated September 9, 1999. This modification also
includes the revised erosion and sediment control plan dated September 22, 1999 and allows
the use of Calgon Catr-Floc DL for flocculation of fine particles in the basins onsite.
April 6, 2005: This permit has been modified to change the corporate name from Cherokee
Sanford Group, LLC to General Shale Brick, Inc.
October 10, 2007: This permit has been modified to increase the permitted acreage to 648.65
acres and the affected acreage at this site to 590.89 acres as indicated on the Mine Details
Map last revised April 23, 2007, The modification includes the addition of several tracts to the
east and south of the existing permit boundaries. In addition, the modification includes
expansion of the mine excavation area into said tracts and installation and includes the
maintenance of all associated erosion and sediment control measures.
October 20, 2014:-.This permit has been modified to establish thepermitted. acreage as 301
acres and the affected acreage at thi—s—s—ife—a—s 2TO716 acres as m icated on the I ract-w
Overall Site Topography Map dated September 3, 2014. Mining Permit No. 19-08 has been
split into two separate mining permits, Brickhaven No.2 Mine Tract "A" (mining permit No. 19-
25) and Brickhaven No. 2 Mine Tract "B" (Mining Permit No. 19-08).
January 23, 2015: This permit has been transferred in its entirety from General Shale Brick,
Inc. to Green Meadow, LLC.
April 23, 2015: This permit has been modified to replace the flocculant currently permitted with
FLOC-UL8 and GT Clear, manufactured by Green Technologies, to improve settling efficiency
of suspended solids in the mine discharge water at this site provided these products are used
in accordance with the manufacturer's instructions as outlined in the letter and supplemental
information received by the Land Quality Section on April 10, 2015.
June 5, 2015: This permit has been modified to redesign the erosion and sedimentation
control measures throughout the site and reduce.the affected acreage to 267 acres as
indicated on the Mine Maps last revised December 31, 2014. The modification also includes
changing the method for reclaiming the mine by constructing structural fill using Coal
Combustion Byproducts (GCBs) in accordance with the provisions of the Coal Ash
Management Act of 2014 and the terms and conditions of Permit to Construct and Operate
Brickhaven No. 2 Mine Tract "A" Mine Structural Fill Permit No. 1910-STRUC-2015 issued by
the Division of Waste Management on June 5, 2015,
Expiration Date
This permit shall be effective from the date of its issuance until June 5, 2025.

Page 4
Conditions
This permit shall be subject to the provisions of the Mining Act, N.C.G.S. 74-46, et. seq.. and to
the following conditions and limitations:
OPERATING CONDITIONS;
A. Any wastewater processing or mine dewatering shall be in accordance with the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission. GS 74-51 (d) (3)
B. Any approvals or permits required to collect, handle, and properly dispose of any
water contacting Coal Combustion Byproducts (CCBs) shall be obtained prior to
any placement of CCBs within the mining permit boundary. GS 74-51 (d) (3)
- -- - --- - C.-- - Any stormwater runoff from the affected areas'at the site=shall be managed in
accordance with any applicaole permit requirements and regulations
promulgated by the Environmental Management Commission. It shall be the
permittee's responsibility to contact the Stormwater Program to secure any
necessary stormwater permits, permit modifications, or other approval
documents. The terms and conditions of NPDES General Permit No.
NCG020354 last revised December 16, 2014 shall be followed. GS .74-51 (d) (3)
2. A. Any mining process producing air contamination emissions shall be subject to the
permitting requirements and rules promulgated by the N.C. Environmental
Management Commission and enforced by the Division of Air Quality. GS 74-51
(d) (3)
B. During mining operations, water trucks or other means that may be necessary
shall be utilized to prevent dust from leaving the permitted area. GS 74-51 (d) (3)
3. A- Sufficient buffer shall be maintained between any affected land and any adjoining
waterway or wetland to prevent sedimentation of that waterway or wetland from
erosion of the affected land and to preserve the integrity of the natural
watercourse or wetland. GS 74-51 (d) (2)
B. Any mining activity affecting waters of the State; waters of the U. S., or wetlands
shall be in accordance with the requirements and regulations promulgated and
enforced by the N. C. Environmental Management Commission. GS 74-51 (d) (2)
C. Buffers shall be maintained as indicated on the Mine Maps last revised
December 31, 2014. GS 74-51 (d) (2)

Page 5
D. No land disturbing activities shall be allowed within 50 feet of any wetland or
waterway until proof has been submitted to the Land Quality Section that all
necessary permits/certifications have been obtained from the US Army Corps of
Engineers and the Division of Water Resources. GS 74-51 (d) (2)
4, A. Adequate mechanical barriers including but not limited to diversions, earthen
dikes, check dams, sediment retarding structures, rip rap pits, or ditches shall be
provided in the initial stages of any land disturbance and maintained to prevent
sediment from discharging onto adjacent surface areas or into any lake, wetland
or natural watercourse in proximity to the affected land. GS 74-51 (d) (6)
B. In order to improve settling efficiency of suspended solids in the mine discharge
water at this site, the operator shall use the flocculants FLOC-UL8 and GT Clear,
manufactured by Green Technologies, provided these products are used in
accordance with the manufacturer's instructions as outlined in the letter and
supplemental information received by the Land Quality Section on April 10, 2015.
- GS 74-51 (d) 6
C. All mining activities and any land disturbing activities conducted within the mining
permit boundary associated with the construction of the Coal Combustion
Byproducts (CCBs) structural fill, including the installation and maintenance of all
associated erosion and sediment control. measures, shall be conducted as
indicated on the Mine Maps last revised December 31, 2014 and the
supplemental information received by the Land Quality Section on November 21,
2014, January 6, 2015 and March 17, 2015. GS 74-51 (d) (1-7)
5. Groundwater monitoring and sampling prior to, during and post -disposal of Coal
Combustion Byproducts (CCBs) into the mined pits shall be implemented as outlined in
the Coal Ash Management Act and per the plan prepared for and approved by the
Division of Waste Management through Permit to Construct and Operate Brickhaven
No, 2 Mine Tract "A" Mine Structural Fill Permit No. 1910-STRUC-2015 issued on June
5, 2015, GS 74-51 (d) (2 and 3)
6. All affected area boundaries (267 acres) shall be permanently marked at the site on
100-foot intervals unless the line of sight allows for larger spacing intervals. GS 74-51
(d) (4)
The angle for graded slopes and fills shall be no greater than the angle that can be
retained by vegetative cover or other adequate erosion control measure, structure, or
device In any event, exposed slopes or any excavated channels, the erosion of which
may cause off -site damage because of siltation, shall be planted or otherwise provided
with ground cover, devices or structures sufficient to restrain such erosion. GS 74-51 (d)
(4)

Page 6
The affected land shall be graded so as to prevent collection of pools of water that are,
or likely to become, noxious or foul. Necessary structures such as drainage ditches or
conduits shall be constructed or installed when required to prevent such conditions. GS
74-51 (d) (2)
9. Existing vegetation or vegetated earthen berms shall be maintained between the mine
and public thoroughfares whenever practical to screen the operation from the public. GS
74-51 (d) (4)
10. A. Sufficient buffer shall be maintained between any excavation and any mining
permit boundary to protect adjacent property_ GS 74-51 (d) (4)
B. Buffers shall be maintained as indicated on the Mine Maps last revised
December 31, 2014. GS 74-51 (d) (4)
--11:----A physical barrier -consisting of a fence or earthen berm, etc., shall be maintained
around the perimeter of any highwall. GS 74-51 (d) (4)
12, A_ The on -site disposal of Coal Combustion Byproducts (CCBs) as structural fill
within the reining permit boundary shall be conducted in accordance with the
Coal Ash Management Act and Permit to Construct and Operate Brickhaven No.
2 Mine Tract "A" Mine Structural Fill Permit No. 1910-STRUC-2015 issued by the
Division of Waste Management on June 5, 2015, GS 74-51 (d) (7)
B. Notwithstanding the above condition, no on -site disposal of refuse or other solid
waste that is generated outside of the mining permit area shall be allowed within
the boundaries of the mining permit area unless authorization to conduct said
disposal has first been obtained from both the Division of Waste Management
and the Land Quality Section, Department of Environment and Natural
Resources. The method of disposal shall be consistent with the approved
reclamation plan. GS 74-51 (d) (7)
C. Mining refuse as defined by G.S. 74-49 (14) of The Mining Act of 1971 generated
on -site and directly associated with the mining activity may be disposed of in a
designated refuse area. All other waste products must be disposed of in a
disposal facility approved by the Division of Waste Management. No petroleum
products, acids, solvents or their storage containers or any other material that
may be considered hazardous shall be disposed of within the permitted area. GS
74-51 (d) (7)
D. For the purposes of this permit, the Division of Energy, Mineral and Land
Resources considers the following materials to be "mining refuse" (in addition to
those specifically listed under G.S. 74-49 (14) of the N.C. Mining Act of 1971):
GS 74-51 (d) (7)

Page 7
1, on -site generated land clearing debris
2. conveyor belts
3. wire cables
4. v-belts
5, steel reinforced air hoses
6. drill steel
E. If mining refuse is to be permanently disposed within the mining permit boundary,
the following information must be provided to and approved by the Division of
Energy, Mineral, and Land Resources prior to commencement of such disposal:
GS 74-51 (d) (7)
1, the approximate boundaries and size of the refuse disposal area;
2. a list of refuse items to be disposed;
3, verification that a minimum of 4 feet of cover will be provided over the
refuse;
4. verification that the refuse will be disposed at least 4 feet above the
seasonally high water table; and,
5. verification that a permanent vegetative groundcover will be established,
13, An Annual Reciamation Report shall be submitted on a form supplied by the
Department by February 1 of each year until reclamation is completed and approved.
GS 74-55
14. The operator shall notify the Department in writing of the desire to delete, modify or
otherwise change any part of the mining, reclamation, or erosion/sediment control plan
contained in the approved application for a mining permit or any approved revision to it.
Approval to implement such changes must be obtained from the Department prior to on -
site implementation of the revisions. GS 74-52 (a)
15. The security, which was posted pursuant to N.C,.G.S. 74-54 in the form of a
$500,000.00 blanket bond, is sufficient to cover the operation as indicated in the
approved application. This security must remain in force for this permit to be valid. The
total affected land shall not exceed the bonded acreage. GS 74-54
16, A. Authorized representatives of the Division of Archives and History shall be
granted access to the site to determine the presence of significant archaeological
resources. GS-74-50 (b3) (7)
B. Pursuant to N. C. G. S. 70 Article 3, "The Unmarked Human Burial and Human
Skeletal Remains Protection Act," should the operator or any person in his
employ encounter human skeletal remains, immediate notification shall be
provided to the county medical examiner and the chief archaeologist, North
Carolina Division of Archives and History. GS-70-3

Page 8
APPROVED RECLAMATION PLAN
The Mining Permit incorporates this Reclamation Plan, the performance of which is a condition
on the continuing validity of that Mining Permit. Additionally, the Reclamation Plan is a
separable obligation of the permittee, which continues beyond the terms of the Mining Permit.
The approved plan provides:
Minimum Standards As Provided By G.S. 74-53
The final slopes in all excavations in soil, sand, gravel and other unconsolidated
materials shall be at such an angle as to minimize the possibility of slides and be
consistent with the future use of the land.
2. Provisions for safety to persons and to adjoining property must be provided in all
- --- - -excavations-in-rock:
3. All overburden and spoil shall be left in a configuration which is in accordance with
accepted conservation practices and which is suitable for the proposed subsequent use
of the land.
4. No small pools of water shall be allowed to collect or remain on the mined area that are,
or are likely to become noxious, odious or foul.
The revegetation plan shall conform to accepted and recommended agronomic and
reforestation practices as established by the North Carolina Agricultural Experiment
Station and the North Carolina Forest Service,
6. Permittee shall conduct reclamation activities pursuant to the Reclamation Plan herein
incorporated. These activities shall be conducted according to the time schedule
included in the plan, which shall to the extent'feasible provide reclamation simultaneous
with mining operations and in any event, provide reclamation at the earliest practicable
time after completion or termination of mining on any segment of the permit area and
shall be completed within two years after completion or termination of mining.
RECLAMATION CONDITIONS:
Provided further, and subject to the reclamation schedule, the planned reclamation shall
be to backfiil the mine.excavation with Coal Combustion Byproducts (GCBs) in
accordance with the Coal Ash Management Act and Permit to Construct and Operate
Brickhaven No. 2 Mine Tract "A" Mine Structural Fill Permit No. 1910-STRUC-2015
issued by the Division of Waste Management on June 5, 2015. In addition, any
disturbed areas shall be regraded and revegetated as indicated on the Reclamation
Plan, Sheet 03C-02, dated November 2014. GS 74-53
The specifications for surface gradient restoration to a surface suitable for the planned
future use are as follows: GS 74-53

Page 9
A. All the final perimeter side slopes shall be graded to a 3 horizontal to 1 vertical or
flatter slope.
B. Any settling ponds or sediment basins shall be backfilled and stabilized.
C. The processing, stockpile, and other disturbed areas neighboring the mine
excavation shall be leveled and smoothed.
D. Compacted surfaces shall be disced, subsoiled or otherwise prepared before
revegetation.
E. Materials not specifically approved within this mining permit shall not be
permanently disposed of at the mine site. On -site disposal of Coal Combustion
Byproducts (GCBs) and mining refuse shall be conducted in accordance with
Operating Condition Nos. 11A through 11 E.-
F. The affected land shall be graded to prevent the collection of noxious or foul
water.
3. Revegetation Plan:
After site preparation, all disturbed land areas shall be revegetated as per the Seeding
Plan submitted on the Erosion and Sedimentation Control Details, Sheet 3 of 3, last
revised December 31, 2014. GS 74-53
Whenever possible, disturbed areas should be vegetated with native warm season
grasses such as switch grass, Indian grass, bluestem and gamma grass. GS 74-51 (d)
(2)
In addition, the permittee shall.consult with a professional wildlife biologist with the N.C.
Wildlife Resources Commission to enhance post -project wildlife habitat at the site. GS
74-51 (d) (2)
4. Reclamation Plan -
A. Reclamation shall be conducted simultaneously with mining to the extent
feasible. In any event, reclamation shall be initiated as soon as feasible after
completion or termination of mining of any mine segment under permit. GS 74-53

Page 10
B. Specific reclamation phases and schedules shall be followed as described in the
Reclamation Timeline, Section C, submitted with the supplemental information
received by the Land Quality Section on January 6, 2015 as follows: GS 74-53
Acres
Estimated Completion
Phase 1 (Cellsl and 2) 62,5
December 2019
Phase 2 (Cells 3 and 4) 47.5
July 2021
Phase 3 (Cell 5) 34.8
August 2022
This permit, issued to Cherokee Brick Company on August 30, 1985, transferred to
Cherokee Sanford Group on November 4, 1988, simultaneously renewed and modified
_October..5,_1995, modified August.2, 1996, September 24, 1998, November 4,.1999, -
__ and pri 2-0�5, renewed- eptember 15, 20D5, modified Octo ear 1672007 and
October 20, 2014, transferred to Green Meadow LLC January 23, 2015, and modified
April 23, 2015, is hereby simultaneously renewed and modified this 51h day of June,
2015 pursuant to G.S. 74-52.
Tracy E. Davis, PE, CPM, Director
Division of Energy, Mineral, and Land Resources
By Authority of the Secretary
Of the Department of Environment and Natural Resources

f LAND & WATER RESOURCES DIVISION
/ \ Envimnmentai Quality Department
CHATHAM COLIIVTY P.O. Box 548
NORTH CAROLINA Pittsboro, NC 27312
PHONE: [phone]
Fax: [phone] . E-mail: [e-mail] . Website: www.chathamnc.org
Soil Erosion and Sedimentation Control
NOTICE OF VIOLATION OF THE CHATHAM COUNTY SOIL EROSION AND SEDIMENTATION
CONTROL ORDINANCE
May 26, 2015
CIERTIFIED MAIL
RETURN RECEIPT REQUESTED
Green Meadow, LLC
12601 Plantside Drive
Louisville, KY 40299
Attn: Charles Price
Green Meadow, LLC
C/O Corporate Service Company
327 Hillsborough Street
Raleigh, NC 27603
And
Moncure Holdings, LLC
2717 New Hill Olive Chapel Rd,
New Hill, NC 27562
Attn: Jason Kaplan
Moncure Holdings, LLC
C/O Loretta Young
PO Box 71
New Hill, NC 27562
RE: Charah Rail Spur
To the Above Named Persons and Entities:
On May 20, 2015, personnel of this office inspected the above referenced project. This inspection was
performed to determine compliance with the Chatham County Soil Erosion and Sedimentation Control
Ordinance.
It is our understanding that you and/or your firm are responsible for this land -disturbing activity. The.
purpose of this letter is to inform you that this activity was found to be in violation of the Chatham
County Soil Erosion and Sedimentation Control Ordinance. If you feel you are not responsible for the
following violations, please notify this office immediately.

L r {
f LAND & WATER RESOURCES DIVISION
\ Environmental Quality Department
CHATHAM COUNTY P.O. sox 548
NORTH CAROLINA
Pittsboro, NC 27312
PHONE: [phone]
Fax: [phone] • E-mail: [e-mail] • Website: vvww.chathamnc.org
The violations that were found are:
1. No approved plan, Section 164.05(G): No person shall initiate any land -disturbing activity on a
tract if more than 20, 000 square feet is to be uncovered unless, a plan for the activity is filed with the
county 30 or more days prior to initiating the activity, and the plan is approved and a land -disturbing
pennit is granted by the county in accordance with Section 164.12 of this chapter.
Land -disturbing activity is being conducted on the proposed Charah Rail Spur project without prior plan
approval or permit issuance.
2. Failure to take all reasonable measures, Section 164.05(A): Protection ofprqperty. Persons
conducting land- disturbing activity shall take all reasonable measures to protect all public and private
property from damage caused by the activity.
No erosion control measures were provided for the initial clearing phase of the project to prevent impacts
from sedimentation.
3. Inadequate buffer zone, Section 164.05(13): Riparian buffers Land -disturbing activity conducted
in proximity to any surface water is also subject to, and must provide a riparian buffer in accordance with
the riparian buffer requirements set forth in the County Watershed Protection Ordinance. Under no
circumstance shall a riparian buffer be less than 30 feet.
Riparian buffers were not provided in accordance Section 304 of the Watershed Protection Ordinance.
To correct these violations, you must:
1. Submit a plan to this office for approval. Once a Land -Disturbance permit is issued,
proceed with installation of erosion control measures per the construction sequence
on the approved plan.
2. Take immediate action to stabilize the disturbed stream banks and protect the
channel. At a minimum, this should include silt fence along the bank of the tributary
to prevent disturbed soils from entering the stream and leaving the site.
3. Buffers must be restored and re -vegetated. All riparian buffers must be shown on the
plan and any crossings must be designed to minimize the amount of intrusion into the
buffer.
Please be advised that if these violations are not corrected within 10 days after receipt of this notice,
Chatham County may take the appropriate legal action against you. That action could be the assessment
of a civil penalty, and the amount may be up to $5000 per day for each violation. The penalty may be
assessed from the date of the violation. If the violations are corrected within the time period specified
for compliance, no further legal action will be pursued.
Please be advised that no activity associated with this project, other than that related to achieving
compliance, should be conducted until the site is brought into compliance. When corrective actions are
complete, you should notify this office so that work can be inspected. You should not assume that the
property is in compliance with the Ordinance until we have notified you. After installation, all erosion
control measures must be maintained in proper working order until the site is completely stabilized.
We solicit your cooperation, and would like to avoid taking further enforcement action. At the same time,
it is your responsibility to understand and comply with the requirements of the Ordinance.
j.*

J LAND & WATER RESOURCES DIVISION
/ Environmental Quality Department
CHATHAM COUNTY P.O. Box 548
NORTH CAROLINA
Pittsboro, NC 27312
PHONE: (919} 545-8343
Fax: [phone] • E-mail: [e-mail] • Website: www.chathamnc.org
We also recommend you contact Danny Smith of NC Division of Water Resources at [phone] and
Andrew Williams with US Army Corps of Engineers at [phone] regarding any potential compliance
issues with State and Federal standards with on site streams and wetlands.
Should you have questions concerning this notice or the requirements of the Ordinance please contact
me at your earliest convenience. My office phone number Is [phone].
Sincerely,
Rachael Thorn, CPESC
Lead Erosion & Sedimentation Control Officer
Chatham County
Enclosures: Sedimentation Inspection Report
cc: Charlie Horne, Chatham County Manager
Jason Sullivan, Chatham County Director of Planning
Dan LaMontagne, Chatham County Director of Environmental Quality
Danny Smith, Division of Water Resources, Water Quality Regional Operations
John Holley, Regional Engineer, NC DEMLR
Andrew Williams, US Army Corps of Engineers, Raleigh Regulatory Field Office
Steve Stroud, NAI Carolantic

. Nx
1. 7.
K2

11''`k,
CHArHAMCOUN Y
MO�lll C OLI},,
Project:
Project 4:
Person Financially Responsible:
Address:
River Basin:
Date of Inspection:
Inspector:
1. Project Location:
ID Pictures
Erosion and Sedimentation Control Inspection Report
Charah Rail Spur
2015-021
Green Meadow LLC
12601 Plantside Drive, Louisville, KY 40299
Ca a Fear River Basin
S/20/2015
Rachael Thorn
l ,
LAND WATER RESOUR02S Plk'!S�ON
Environmental Quality Department.
P.O. Box 548
Pittsboro, NC 27312
PHONE: [phone]
Fax: [phone] Website: www.chathamnc.org
Proposed Rail Spur into Brickhaven No. 2 Mine Tract A
2. Weather and soil conditions: Sunny and clear. Workable soils
3. Initial Inspection: Yes
4. Is site in compliance with the ordinance? No
5. Is the site being placed under a Notice of Violation? Yes
6. Is the site currently under a Notice of Violation? No
7. Is site in compliance with SPCA and rules? No
2 No approved plan, Section 164,05(G)
❑ Failure to follow approved plan, Section 164.10(0)
❑ Failure to submit revised plan, Section 164.10(M)
❑ Failure to provide adequate groundcover, Section 164.05(I)
❑ Failure to self Inspect, G.S. 113A-54.1(e) and 15A NCAC 413.0131
❑ Insufficient measures to retain sediment on site, Section 164.05(3)
Failure to take all reasonable measures, Section 164,05(A)
Inadequate buffer zone, Section 164.05(B)
❑ Graded slopes and fills too steep, Section 164.05(C)
❑ Unprotected exposed slopes, Section 164.05(C)
❑ Failure to maintain measures, Section 164.18 and 15 NCAC 4B .0113
S. Potential NPDES Permit Violation; Yes Describe: No approved plan for greater than 1 acre of disturbance
9. Has sediment damage occurred since last inspection? No Where?
Description of sediment damage:
Degree of damage:
10. Contact made with (name): Erik West
How was Inspection Report was provided to responsible arty? sent
Date 5 26 2015
11. Corrective actions needed
QSubmit an adequate sedimentation and erosion control plan for approval, covering all areas disturbed or to be disturbed.
2 Provide adequate stream buffers
7Other: Provide minimum temporary measures, such as silt fence, to protect the tributary stream until a plan Is approved and can be fully implemented.
Comments: An erosion control plan for the Charah Rail Spur was submitted to this office on May 8th. The plan was
under review on May 19th when it was reported that site clearing had been conducted. Charah was contacted via
telephone and it was confirmed that clearing activity had occurred. An inspection was scheduled for the following
day. On May 20th, county staff visited the Brickhaven Mine and Charah Rail Spur sites. The inspection of the
proposed Rail Spur site revealed the following: 1) Clear cutting of the Rail and Utility Easement between Old US I
and Brickhaven Tract A was complete, 2) Activities underway during inspection included geotechnical boring for
bridge abutments at STA 16+00 as well as removal of remaining downed trees, 3) No erosion control measures were
provided, 4) The clearing limits spanned approximately 150 feet and encompassed the easement and project limits
from Old US 1 to the Brickhaven Mine, 5) Disturbance was also documented at the tributary to Shaddock Creek,
including the channel banks, 6) No buffer remained for the tributary and 7) Channel banks were in an unstable
condition. A Notice of Violation (NOV) will be issued for this project. Please refer to the NOV for more
information. Contact Rachael Thorn at [phone] with any questions or concerns.

,AK41'
� h
NC®ENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Govemor
June 1, 2015
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Green Meadow, LLC
ATTN: Charles Price
12601 Plantside Dr.
Louisville, Kentucky 40299
Moncure Holdings, LLC
ATTN: Jason Kaplan
2717 New Hill Olive Chapel Rd.
New Hill, NC 27562
Moncure Holdings, LLC
c/o Loretta Young
PO Box 71
New Hill, NC 27562
Donald R. van der Vaart
Secretary
RE: Notice of Violation and Notice of Intent to Enforce Illegal Discharge
Failure to Secure Stormwater General Permit NCG010000
Charah Rail Spur
Chatham County
Dear Sirs and Madam:
On May 29, 2015, I (from the Raleigh Regional Office of the Division of Energy, Mineral, and Land
Resources (DEMLR)) visited the subject site and observed potential impacts from land -disturbing
activities to surface waters. Specifically, concentrated stormwater flow had entered watercourses where
clearing operations had encroached on the banks to create an equipment crossing. This site visit and a
subsequent DEMLR file review confirmed that Sedimentation and Erosion Control plan approval had
not been secured for the land -disturbing activity. Therefore, coverage under the NPDES General
Permit (NCG010000) to discharge stormwater from land- disturbing activities has not been secured in
accordance with the provisions of the applicable North Carolina General Statute.
Division of Energy, Mineral, and Land Resources
Energy Section - Geological Survey Section • Land Quality Section
1628 Mail Service Center Raleigh, NC 27699-PHONE: [phone] FAX: [phone]
Internet http:/lnortal.ncdenr.org/w_eb/ir/
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Notice of Violation
Charah Rail Spur
June 1, 2015
Page 2 of 3
This General Permit is applicable to point source discharges from construction activities disturbing one
or more acres of land. The submission of a proposed Erosion and Sedimentation Control Plan to
DEMLR or the appropriate delegated local program shall be considered to take the place of a Notice of
Intent for coverage under this General Permit for those projects requiring this Permit coverage.
Coverage under this General Permit shall become effective upon issuance of an approval for the Erosion
and Sedimentation Control Plan by the Land Quality Section of DEMLR or the delegated local program.
Prior to the commencement of construction and land disturbing activities approval of the Erosion and
Sedimentation Control Plan shall be obtained.
Please note that the above referenced discharge to the waters of the State constitutes a violation of
North Carolina General Statue (NCGS) 143-215.1 (a) (1) and (11) which states:
"No person shall do any of the following things or carry out any of the following activities until or
unless that person has received a permit from the Commission and has complied with all conditions set
forth in the permit:
(1) Make any outlets into waters of the State.
(I I)Cause or permit discharges regulated under G.S. 143-214.7 that result in water
pollution. "
This,Office is developing a potential enforcement action regarding these matters. The violations cited
above are subject to civil penalties of up to $ 25,000.00 per day. Please respond to this Notice in writing
within ten (10) days of your receipt of this letter. Your written response to this notice should minimally
include the following:
1. Please provide records of when the land -disturbance began.
2. Explain in. your response how you have complied with the conditions outlined in the Notice of
Violation from Chatham County dated May 26, 2015.
3. Please provide a written account explaining what measures you have taken to correct these issues
(permanently eliminate) potential sedimentation impacts to waters.
0 12

Notice of Violation
Charah Rail Spur
June 1, 2015
Page 3 of 3
Thank you for your attention to this matter. Please understand, this office is developing an enforcement
action recommendation regarding this matter. Your response to this letter will be considered as a part of
this process. If you have questions regarding this matter you may contact me at [phone].
ly,
DL. Holley, Jr., PE, CPESC
gional Engineer
Land Quality Section
Attachment: Stormwater Inspection Report
cc: Ms. Ashley Rodgers, PE, State Sedimentation Specialist
Mr. Matt Winfree, Charah, Inc.
Ms. Rachael Thorn, CPESC, Chatham County
Mr. Danny Smith, Regional Water Quality Supervisor, DWR
Ms. Karen Higgins, DWR 401 /Wetlands Unit

vironment and Natural Resources
Land Quality Section: 3800 Barrell Drive, Raleigh, NC 27609, Phone: [phone]
County:
Chatham Project: r Charah Rail Spur River basin: Cape Fear
Cireen Meadow LLC and Mon cure Holdings, LLC T'H-20i5-80x.
Person financially responsible. Project
12601 Address: Plantside Dr, Louisville Kentucky and 2717 New Hill Olive Chapel Rd, New Hill NC Case NA
1. Project location: Woodland Rd.
Pictures: No: r Yes: +/ Video: r Digital: P
Clear, hot and Workable
2. Weather and sail conditions:
First inspection: Yes: r14 No: r
3.
Is site currently under notice of violation? Yes: r*—' No: r by Chatham Co.
4.
Is the site in compliance with S.P.C.A. and rules? Yes: r No: Wo
If no, check violations below:
5.
Violations:
P—"
a. No approved plan, G.S. 113A-57 (4) and 15A NCAC 4B.0107(c)
r
g. Inadequate buffer zone, G.S. I I3A-57(1)
r
b. Failure to follow approved plan, G.S. 113A-57(5)
r
h. Graded slopes and fills too steep,
r
c. Failure to submit revised plan, G.S. 113A-54.1(b) and
G.S. 113A-57(2) or 15A NCAC 4B.0124(d)
15A NCAC 413.011 S(a)
r
i. Unprotected exposed slopes, G.S. 1 13A-57(2)
r
d. Failure to provide adequate groundcover, G.S. 113A-57(3);
r J.
Failure to maintain measures, 15A NCAC 413.0113
15A NCAC 4B.0107(b) or 15A NCAC 4B.0124(e)
r k. Failure to sell -inspect G.S. 1 I3A-54.1(e) and
r
e. Insufficient measures to retain sediment on site, G.S. I I3A-57(3)
15A NCAC 4B.0131
r
f, Failure to take all reasonable measures, 15A NCAC 48.0105
r
1. Other describe
6.
Is the site in compliance with NPDES Permit NCG 010000? Yes: r
No: (✓
Not Applicable: r If no, check violations below:
r
in. Failure to manage construction site pollutants, NCG 010000 Sec. 11,
B.1 r
r. Failure to have approved plan and NPDES
r
n. Failure to provide ground stabilization, NCG 010000 Sec, 11, B.2
permit on site, NCG 010000 Sec. III, 3(d)
r
o. Failure to maintain rain gauge or record daily rainfall,
r s.
Failure to install and maintain BMP's,
NCG 010000 Sec. 11, B.3(a,b)
NCG 010000 Sec. I11, 4
r
p. Failure to meet self -inspection and reporting requirements,
r
t. Failure to operate and maintain control
NCG 010000 Sec. II, 8,3(c-i)
measures, NCG 010000 Sec. IV, I
r
q, Failure to dewater sediment basin from surface,
r
u. Bypass of stormwater control facilities,
NCG 010000 Sec. 11, BA
NCG 010000, Sec. IV, 3
� v. Other (describe) 5.l(a) & 15A NCAC 211.0126
`
7. Has sedimentation damage occurred r since last inspection at 10 inspection? Yes: r If yes, where? (check all chat apply) No: F00
Lake/natural watercourse on the tract: r Lake/natural watercourse off the tract: r Other property: r
Description: I
Stormwater Discharge Outfall with high turbidity or sediment loss:
Degree of damage: slight: r moderate : r severe: r
Matt Winfree Charah Site Manager
8. Contact made with (name): Title:
Inspection report given: r or sent: FO to person financially responsible. Date given/sent: I With Stonnwater NOV
9. Corrective actions needed: Secure approval of an adequate S&EC plan through Chatham County covering all areas disturbed
or to be disturbed. Install all applicable erosion and sediment control devices required by that plan.
Report by:
rOthers present: John L, Hollcy, Jr., PE CPESC Matt Winfree' Charah
5-29-2015 about 5 PM about 7:30PM
Date of inspection: Time arriving on site: Time leaving site:
Rcvision Date 09042013 Pagel O172

tna
Land Quality Section: 3800 Barrett Drive, Raleigh, NC 27609, Phone: [phone]
See Stormwater NOV
cc:
Corrective actions needed (continued) NA
10. Comments: This inspection was performed specifically to address the NC Wneral NPDES permit required.
Work had stopped when I inspected this site, and stop -gap silt fencing and temporary cleanup work had been performed at watercourse
crossings.
Revision Date 09092013 Page 2 of

NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Mr. Charles E. Price
Green Meadow, LLC
12601 Plantside Drive
Louisville, KY 40299
Dear Mr. Price:
December 16, 2014
John E. Skvarla, III
Secretary
RECEIVED
DEC 22 20f4
CENTRAL FILES
DWR SECTfOni
Subject: NPDES General Permit NCG020354
Green Meadow, LLC
Formerly General Shale Brick, Inc.
Certificate of Coverage NCG020354
Chatham County
Division personnel received your request to revise your stormwater permit Certificate of
Coverage to accurately reflect your new company and/or facility name.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in
the General Permit remain unchanged and in full effect. This revised Certificate of Coverage is
issued under the requirements of North Carolina General Statutes 143-215.1 and the
Memorandum of Agreement between North Carolina and the U.S. Environmental Protection
Agency.
If you have any questions or need further information, please contact the Stormwater Permitting
Program at [phone].
4Siincerely,
for Tracy E. is, P.E., CPM, Director
Division of Energy, Mineral and Land Resources
cc: Raleigh Regional Office
ormwater Permitting Program Files
Central Files
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-9200 / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 - Internet: httpj//portal.ncdenr.orglwebllr1
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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCG020354
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Green Meadow, LLC
is hereby authorized to operate treatment systems and to discharge stormwater and mine
dewatering wastewater and process wastewater, from a facility located at:
Brickhaven No.2 Mine Tract "A"
1149 Moncure Flatwood Road
Moncure
Chatham County
to receiving waters designated as unnamed tributary to Gulf Creek, a class WS-IV stream, in the
Cape Fear River Basin, in accordance with the effluent limitations, monitoring requirements, and
other conditions set forth in Parts 1, I1, II1, and IV of General Permit No. NCG020354 as
attached.
This certificate of coverage shall become effective December 16, 2014.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day December 16, 2014
for Tracy E. Davis,4PfE., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

Division of Energy, Mineral & Land Resources
4mj's
Land Section/Stormwater Permitting
Quality
NcorrM
National Pollutant Discharge Elimination System
twM-Mown
PERMIT NAMEIOWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
pate Received
Year Nlonlh
D
I. Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
1 2 161 01 01 0 N I d I V 0 2 0 3 5 4
II. Permit status ,prior to requested change.
a. Permit issued to (company name): General Shale Brick, Inc.
b. Person legally responsible for permit: Gregory A Bowles
First Ml Last
Director of Real EqqS Environment & Geology
Title
RECEIVED 3015 Bristol Highway
DEC 1 201Permit Holder Mailing Address
0.
Johnson CityTN. 37601
DENR-LAND QUALITY � City State zip
STORMWATER FERW iTNG [phone] ( )
Phone Fax
c. Facility name (discharge): Brickhaven No. 2,Mine Tract "A"
d. Facility address: 1149 Moncure Flatwood Road
Address
Moncure NC 27559
City State ' Zip
e. Facility contact person: [phone] ext.
Larry Cockerill _ 243
First / MI / Last Phone
III. Please provide the following for the requested change (revised permit).
a: Request for change is a result of: ® Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain-
b. Permit issued to (company name):
c. Person legally responsible for permit:
d. Facility name (discharge):
e. Facility address:
f. Facility contact person:
Green Meadow. LLC
Charles
E Price
First
MI Last
Managing Member
—
Tick
12601 PIantside Drive
Permit Holder Msilirig Address
Louisville
KY 40299
Ciry
State Zip
502 245-1353
charah.coai
Phone
E-mail Address
Brickhaven No. 2 Mine Tract "A"
1149 Moncure Flatwood Road
Address �:
Moncure
NC 27559
City
State zip
Charles
E Price
. First
MI Last
[phone]
[e-mail] �
Phone E-mail Address

NPD.ES.PERMIT NAMEIOWNERSFiIP CHANGE FORM
Page'2 of 2
IV. Permit contact information (if different from the person legally responsible for the, permit)
Permit contact: Charles E Price
First MI East
Manaaints.Member
Title
12601 P•lantsiderDrive
Mailing Address'
Louisville KY 40299
City State Zip
(M)_24571353 [e-mail]
Phone E-mail Address
V Will the permitted facility continue to conduct the -some industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
VI. Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE -INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill •ofsale) 4s repuered'for an ownership change request: Articles of incorporation are
notsufficientfor an ownership change.
.....................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request,.the signed
Applicant's Certification is sufficient. `'
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, Gregory A. Bowles, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of rhy-'khowledge. I understand that ifall required parts of this
application are nokompleted and that if all -required supporting information is not included, this application
r
package will be returned as incomplete.
�2-Ai 1
` Signature Date
APPLICANT CERTIFICATION
1, Charles.E. Price, attest that•this application for a name/ownership change has been reviewed and is
accurate and complete to•the.best,of my knowledge. I understand that if all required parts of this
application are, ot,completed and that if all required supporting information is not included, this application
package will returried as incom e
/Y
Signature. Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources .
Stormwater Permitting Program
1612 Mail Service Center
Raleigh; North Carolina 27699.1612

FILED
)Q OA
1770 * - -� ��
ooss
n �
BOOK 177 0 PAOE00 9 9
CHATHAM COUNTY NC
TREVA B. SEAGROVES
REGISTER OF DEEDS
FILED Nov 13, 2014
AT 01:04:38 pm
BOOK 01770
START PAGE 0099
END PAGE
0108
INSTRUMENT #
11093
EXCISE TAX
$23,700.00
NORTH CAROLINA SPECIAL WARRANTY DEED
Excise Tax: $23,700.00
Parcel Identifier No. 0005361, 0005362, 0071836, 0085332 (portion) and 0061577 (portion) Verified by County on
the day of 2014 By:
Mail[Box to: Moore & Van Allen PLLC (MPM, 100 N. Tryon 5treet. Suite 4700 Charlotte NC 28202
This instrument was prepared by:Bradshaw & Robinson, LLP, P.O. Box 607, Pittsboro. NC 27312 (without title examination)
Brief description for the Index: 333.55 acres more or less Cape Fear Township,Chatham Count
THIS DEED made this 13th day of November, 2014 (the "Effective Date"), by and between
GRANTOR
GENERAL SHALE BRICK, INC.,
a Delaware corporation
3015 Bristol Highway
Johnson City, Tennessee 37601
GRANTEE
GREEN MEADOW, LLC,
a North Carolina limited liability company
12601 Plantside Drive
Louisville, Kentucky 40299
Enter in appropriate block for each Grantor and Grantee: name, mailing address, and, if appropriate, character of entity, e.g.
corporation or partnership.
The designation Grantor and Grantee as used herein shall include said parties, their heirs, successors, and assigns, and shall include
singular, plural, masculine, feminine or neuter as required by context.
W ITNESSETH, that the Grantor, for a valuable consideration paid by the Grantee, the receipt of which is hereby acknowledged, has and
by these presents does grant, bargain, sell and convey unto the Grantee in fee simple, all that certain lot, parcel of land or condominium
unit situated in Capp Fear Township, Chatham County, North Carolina and more particularly described as follows (the "Property"):
Being all of that certain parcel or tract of land identified as "Tract A 333.55 Acres" and shown on map or plat
entitled, "Recombination Survey of General Shale Brick, Inc." prepared by WNC Professional Engineers &
Surveyors recorded in Plat Slide 2014-263, Chatham County Public Registry, reference to which is hereby
made for a more particular description.
Page 1 of 3

1770
0100
80UX 1770Pl E0100
The Property was acquired by Grantor by instruments recorded in Book 696, Page 894, in Book 1326, Page 940, and in Book 1326,
Page 950, Chatham County Registry. Grantor is the successor -by -merger to Cherokee Sanford Group, LLC, a Delaware limited
liability company.
All or a portion of the Property does not include the primary residence of the Grantor.
Grantor hereby expressly conveys the Property subject to, and G ranter hereby expressly reserves from this conveyance, the Use
Restriction, and all other terms and conditions, and rights of the Grantor, pursuant to Exhibit A attached hereto and
incorporated herein by reference.
TO HAVE AND TO HOLD the aforesaid lot or parcel of land and all privileges and appurtenances thereto belonging to the Grantee in
fee simple.
And the Grantor covenants with the Grantee, that Grantor has done nothing to impair such title as Grantor received, and Grantor will
warrant and defend the title against the lawful claims of all persons claiming by, under or through Grantor, other than the following
exceptions:
1. Any defects in, interests in, objections to, exceptions to, or conditions, liens, encumbrances or other matters of record
relating to the title to the Property, whether evidenced by written instrument, or, if not evidenced by written
instrument, then any such matters that would be revealed by an accurate survey of the Property completed on the
Effective Date in accordance with exception #7, below.
2. Any encroachments upon or by the Property, any boundary disputes or conflicts regarding the boundaries of the
Property, any claims, rights -of -way, easements, restrictions and restrictive covenants upon or relating to the Property,
any encumbrances or other title defect(s), and the terms, provisions and conditions set forth in any instruments
evidencing or referring to any such defects, exceptions, conditions, liens, encumbrances, overlaps, encroachments or
boundary disputes or other matters.
3. All matters listed in Schedule B — Section 11 of the ALTA Commitment Form Commitment for Title Insurance issued
by Chicago Title Insurance Company as Commitment Number 14-12874CH (Revision 7, dated November 7, 2014),-
which matters are incorporated herein by reference, including, but not limited to that certain Timber Deed and
Easement by and between Cherokee Sanford Group, LLC and Cherokee Land Company, LLC recorded in Book817,
Page 632, Chatham County Registry.
4. The lien of non -delinquent real property taxes and assessments, and any other non -delinquent impositions or exactions
of any governmental or quasi -governmental authority or body politic, or political subdivision, agency or department
thereof.
5. Any service, installation, connection, maintenance or construction charges due subsequent to the Effective Date.
6. The effect of any federal, state or municipal laws, rules, regulations or ordinances having applicability to the Property,
or any portion thereof, or the use or enjoyment of the same, whether now or hereafter in effect, including, but not
limited to, zoning, building, health, safety and environmental laws, rules and regulations, and notices of record relating
thereto.
7. Any defects in, interests in, objection to, exceptions to, or conditions, liens, encumbrances or other matters that would
have been disclosed on a current ALTA/AGSM Land Title Survey of the Property prepared as of the Effective Date in
accordance with the 2011 Minimum Standard Detail Requirements for ALTAIACSM Land Title Surveys jointly
established and adopted by ALTA, ACSM and NSPS.
8. Any discrepancies, shortages in area, or state of facts which an inspection of the Property would disclose and which are
not shown by the public records.
9. Any creditors' rights exceptions customarily taken by title insurance companies.
[The remainder of this page is intentionally left blank; Grantor's signature is on the following page.]
Page 2 of 3

1*770
oloa
Bon 17 7 0 ME 0 01
IN WITNESS WHEREOF, the Grantor has duly executed the foregoing as of the day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By:
Kevin H. Ham, Vice President
State of Tennessee - County of f� a&_n
1, the undersigned Notary Public of the County of 6G2LahyznQj2n and State aforesaid, certify that Kevin H. Ham
personally came before me this day and acknowledged that he is the V11ce President of General Shale Brick, Inc., a Delaware
corporation, and that by authority duly given and as the act of such entity, he signed the foregoing instrument in its name on its behalf
as its act and deed. Witness my hand and Notarial stamp or seal, this -SE- day of November, 2014.
My Commission Expires: 6 -d9 -.2D/(
(Affix Seal)
QTA •'y
� f �
• OF
. r
�ft
TENNE88EE
s NOTARY w
N,S,ti• ptisuC . r -
11,-11,Q+ON tG```��
Page 3 of 3
4L-� cag7,—
Ta-►nrr74z 7f60/L Notary Public
Notary's Panted or Typed Name

1'770
0102
WOK 17 70 PAGE 0102
EXHIBIT A TO
NORTH CAROLINA SPECIAL WARRANTY DEED
THIS EXHIBIT A TO NORTH CAROLINA SPECIAL WARRANTY DEED (this "Agreement") is
entered into as of November 13, 2014 (the "Effective Date") by and between GENERAL SHALE BRICK, INC.,
a Delaware corporation (the "Grantor") and GREEN MEADOW, LLC, a North Carolina limited liability company
(the "Grantee"). Grantor and Grantee are sometimes referred to herein individually as a "Party" and collectively
as the "Parties."
WITNESSETH:
THAT, WHEREAS, the Parties entered into that certain Agreement for Purchase and Sale of Property dated
November 12, 2014 (the "Contract"); and
WHEREAS, the Parties wish to provide record notice of certain terms of the Contract including, but not
limited to, matters regarding the Use Restriction.
NOW, THEREFORE, in consideration of ten dollars ($10.00), and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged, Grantor and Grantee hereby agree as
follows:
SECTION 1. Declaration of Covenants. Grantor, with the joinder and the consent of the Grantee, hereby
declares that the Property shall be held, conveyed, encumbered, used, occupied and improved subject to the
following covenants, which shall encumber the title to the Property and shall be binding upon all persons now
having or hereafter acquiring any right, title, or interest in the Property, and their respective heirs, successors, and
assigns, and which shall inure to the benefit of the Grantor, its successors and assigns (the "Use Restriction"):
(a) Use Restriction. Prior to October 31, 2049, the Property shall not be used for the production,
manufacturing, storage, transportation or distribution of bricks, ceramic clay products or concrete masonry units.
This restriction on use shall run with the title to the Property and shall be enforceable by Grantee, its successors and
assigns. The Use Restriction shall expire and be null and void without further action of any Party on October 31,
2049 at 11:59 p.m. (local time).
SECTION 2. Environmental Release. Grantee, on behalf of itself and its members, managers and affiliates
and each of their respective successors and assigns (collectively, the "Releasors"), as of the Effective Date, hereby
waives, releases, and absolutely and forever discharges Grantor and its officers, directors, shareholders, subsidiaries,
affiliates, employees, agents and representatives, and their respective heirs, successors and assigns (collectively, the
"Releasees"), from any and all present or future rights, claims, actions, causes of action, demands, damages, liabilities,
attorneys' fees, costs, fines, penalties and expenses of every kind and nature whatsoever, now known or unknown, direct
or indirect, which any of the Releasors may have with respect to any of the Releasees, directly or indirectly arising from
or relating to (x) the presence or alleged presence of Hazardous Materials in, on, under, about, originating from or
relating to the Property if such Hazardous Materials were present at the Property on or prior to the Effective Date
including, without limitation, any such claims under or on account of any Environmental Law or this Agreement, (y)
any violation or alleged violation of any Environmental Law in connection with the Property that occurred or is alleged
to have occurred on or prior to the Effective Date, and (z) the ownership, use, occupancy or operation of the Property
by Releasees on and prior to the Effective Date, including the use and/or operation of the Property for the mining of
clay or other mineral substances, and the conduct of any activities affecting the air, soil and/or water of the Property,
and activities related to the foregoing.

1'770
0103 B00% 17 7 0 ME 010 3
SECTION 3. Environmental Indemnity. From and after the Effective Date, Grantee shall indemnify,
defend and hold harmless Grantor and the other Releasees (individually, a "Grantor Indemnitee" and collectively,
"Grantor Indemnitees") from and against, and pay for (a) any and all actions, allegations, appeals, causes of action
(including removal and remedial actions), claims, demands, investigations, and lawsuits, of any kind, brought by
Grantee, a third party or any government entity against any Grantor Indemnitees based on, or arising or resulting from
(1) the actual or alleged presence of Hazardous Materials at, on, under or adjacent to the Property, to the extent such
Hazardous Material was first present or first alleged to be present at, on, under or adjacent to the Property on or after
the Effective Date, (2) any activity by Grantee, or any Person affiliated with Grantee, in connection with any actual,
proposed or threatened use, treatment, storage, holding, existence, disposition or other Release, generation, production,
manufacturing, processing, refining, control, management, abatement, removal, arrangement for disposal, handling,
transfer or transportation to or from the Property of any Hazardous Materials at any time located in, under, on or above
the Property, (3) the imposition, recording or filing or the threatened imposition, recording or filing of any
Environmental Lien encumbering the Property relating in any way to the activities conducted on, or operation or use
of, the Property on or after the Effective Date; (4) any actual or threatened injury to, destruction of, or loss of natural
resources in any way connected with the Property arising on or after the Effective Date, including, but not limited to,
costs to investigate and assess such injury, destruction or loss relating in any way to the activities conducted on, or
operation or use of, the Property on or after the Effective Date; (5) any personal injury, wrongful death, or property or
other damage arising on or after the Effective Date under any statutory or common law or tort law theory, related to
environmental hazards on the Property, including, but not limited to, damages assessed for private or public nuisance
or for the conducting of an abnormally dangerous activity on the Property relating in any way to the activities conducted
on, or operation or use of, the Property on or after the Effective Date; and (6) any Environmental Claim relating in any
way to the Grantee's operation or use of the Property on or after the Effective Date (individually, a "Claim" and
collectively, "Claims'); and (b) any and all assessments, civil penalties, out-of-pocket costs and expenses (including
court costs and reasonable attorneys' fees) actually incurred by a Grantor Indemnitee (but excluding costs and expenses
of defending any Claim incurred by any such Grantor Indemnitee after Grantee has accepted and is diligently pursuing
defense of such Claim, unless such costs and expenses of defending such Claim are incurred with Grantee's prior written
consent), damages (including consequential and punitive damages awarded to any third -party), decrees, fines,
judgments, liabilities (including for strict liability), losses, obligations, orders and penalties (whether compensatory or
punitive) which may be assessed against or suffered or incurred by any Grantor Indemnitee based upon, or arising or
resulting from (i) any Claim that is (y) owed to Grantee, a third -party or any governmental entity, or (z) related to any
remedial actions to the Property required of Grantor under any applicable Environmental Law; or (ii) to the extent
arising out of, relating to or resulting from the Release or Threatened Release of Hazardous Materials from the Property
to, on, under, adjacent to, or otherwise affecting the real property owned by Grantor (including as successor in interest
to Cherokee Sanford Group, LLC, a Delaware limited liability company), or General Shale, Inc., on the date hereof (the
"Subiect Property"), any remedial actions reasonably appropriate to enable clay to be mined from the Subject Property
or required to comply with applicable Environmental Law, including, without limitation, action to (x) test, identify,
investigate and monitor such Hazardous Materials or Release, and (y) clean-up, contain and remove such Hazardous
Materials (all of the foregoing, collectively, "Losses"}.
In the event that any Grantor Indemnitee receives written notice of the assertion of any Claim by any third -party or any
governmental entity with respect to which the Grantee is required to provide indemnification under this Agreement, the
Grantor Indemnitee shall provide Grantee with prompt written notice (a "Claim Notice") of any Claim for which
indemnity is sought, which Claim Notice shall set forth in reasonable detail a statement of the pertinent facts known to
the Grantor Indemnitee concerning the Claim(s) that are the subject of the Claim Notice; provide d, however, that any
failure by a Grantor Indemnitee to give a timely, complete or accurate Claim Notice shall not affect the rights or
obligations of any party hereunder except and only to the extent that, as a result of such failure, Grantee's defense of
any such Claim was materially and adversely prejudiced. Grantee shall have the right, upon delivering written notice
(the "Defense Notice") to the Grantor Indemnitee within six (6) months after receipt from a Grantor Indemnitee of a
Claim Notice, to assume and conduct, at Grantee's sole cost and expense, the defense against those Claims identified
PAGE 2
CHARM 636741 v2

0104 9oox 17 7 0 PAGE 010 4
in the Claim Notice that are identified in the Defense Notice; provided, however, that (i) delivery by Grantee of a
Defense Notice shall constitute Grantee's irrevocable agreement that the Grantor Indemnitee(s) are entitled to
indemnification under this Agreement with respect to the Claims set forth in the Defense Notice, and (ii) Grantor shall
have the right to approve the defense counsel engaged by Grantee, such approval not to be unreasonably withheld,
conditioned or delayed (provided that Grantor hereby approves Moore & Van Allen PLLC). In the event that Grantee
shall fail to give a Defense Notice for any Claims identified in the Claims Notice within six (6) months after receipt
from a Grantor Indemnitee of such Claim Notice, then in any such event the Grantor Indemnitees shall have the right
to conduct the defense of the Claims identified in the Claim Notice in good faith, provided that Grantor Indemnitees
shall be prohibited from compromising or settling any such Claims without the prior written consent of Grantee, which
consent shall not be unreasonably withheld, conditioned or delayed. In order to seek Grantee's consent, a Grantor
Indemnitee must provide to Grantee written notice detailing all of the terms, conditions and obligations of any proposed
settlement or compromise, including providing a copy of any proposed settlement agreement or other contractual
arrangement to be executed by parties to the proposed settlement or compromise (a "Grantor Indemnitee Settlement
Notice"). If Grantee does not provide to the respective Grantor Indemnitee(s) a written response to a Grantor
Indemnitee Settlement Notice within twenty (20) -Business Days of Grantee's receipt of the Grantor Indemnitee
Settlement Notice (as provided in Section 18(b) herein), then Grantee's consent will be deemed given to the respective
Grantor Indemnitee. In the event the Grantee does timely deliver a Defense Notice and thereby elects to conduct the
defense of the Claims identified in the Defense Notice, the Grantor Indemnitees will cooperate with and make available
to the Grantee such assistance and materials as Grantee may reasonably request, all at the sole cost and expense of
Grantee. Regardless of which party defends such Claims, the other party hereto shall have the right at its own cost and
expense to participate in the defense assisted by counsel of its own choosing. Without the prior written consent of the
Grantor Indemnitees, which shall not be unreasonably withheld, conditioned or delayed, Grantee shall not approve the
entry of any judgment or enter into any settlement or compromise of any such Claims if (a) pursuant to or as a result of
such judgment, settlement or compromise, such judgment, settlement or compromise would lead to liability or create
any financial or other obligation on the part of any Grantor Indemnitee for which the Grantor Indemnitee is not fully
indemnified and made whole hereunder, (b) the terms of such judgment, settlement or compromise do not provide for
a full and complete release of all such Claims in favor of each Grantor Indemnitee that is the subject of the Claim, and
(c) injunctive or other equitable relief will be imposed against any Grantor Indemnitee. In order to seek a Grantor
Indemnitee's consent, Grantee must provide to the Grantor Indemnitee written notice detailing all of the terms,
conditions and obligations of any proposed judgment, settlement or compromise, including providing a copy of any
proposed settlement agreement or other contractual arrangement to be executed by parties to the proposed settlement
or compromise (a "Grantee Settlement Notice"). If a Grantor Indemnitee does not provide to Grantee a written
response to a Grantee Settlement Notice, within twenty (20) Business Days of the Grantor Indemnitee's receipt of the
Grantee Settlement Notice (as provided under Section 4 herein), then the Grantor Indemnitee's consent shall be deemed
given to the Grantee. Any judgment entered or settlement or compromise agreed upon as set forth in a Grantor
Indemnitee Settlement Notice that is consented to by Grantee or a Grantee Settlement Notice that is consented to by
Grantor, in the manner provided herein, shall be binding upon Grantee, and shall be conclusively deemed to be an
obligation with respect to which the Grantor Indemnitees are entitled to prompt indemnification hereunder; subject to
Grantee's right to appeal an appealable judgment or order.
For purposes of this Agreement, the term "Hazardous Materials" means chemicals, pollutants, contaminants, wastes,
toxic substances, hazardous substances, radioactive materials or genetically modified organisms, which are, have been
or become regulated by any federal, state or local government authority including, without limitation, (w) petroleum or
any fraction thereof, (x) asbestos, (y) any substance or material defined as a "hazardous substance" pursuant to § 101
of the Comprehensive Environmental Response, Compensation, and Liability Act (42 U.S.C. § 9601), or (z) any
substance or material defined as a "hazardous chemical" pursuant to the federal Hazard Communication Standard (29
C.F.R. § 1910.1200); the term "Environmental Claim" means any claim, action, cause of action, investigation, or
notice (written or oral) by any person or entity alleging potential liability (including, without limitation, potential
liability for investigatory costs, cleanup costs, governmental response costs, natural resource damages, property
damages, personal injuries, or civil or criminal penalties) arising out of or resulting from (yy) the actual or alleged
PAGE 3
CHAR211638741 Q

1-770 900x 177 o PAGEo10,5'
0105
presence or release into the environment of any Hazardous Materials at any location, whether or n It owned or operated
by the Grantor, or (zz) circumstances forming the basis of any actual or alleged violation of any Environmental Law;
and the term "Environmental Lary" means all federal, state, local, and foreign laws and regulations relating to pollution
or protection of human health or the environment (including, without limitation, ambient air, surface water, ground
water, wetlands, land surface, subsurface strata, and indoor and outdoor workplace), including, withiout,limitation, (yyy)
laws and regulations relating to emissions, discharges, releases, or threatened releases of Hazardous Materials, and (zzz)
common law principles of tort liability. The terms "Release" and "Threatened Release" shaill have the meanings
defined under Environmental Law. The term "Environmental Lien" means any mortgage, pledge, hypothecation,
assignment, deposit arrangement, encumbrance, lien (statutory or other), charge, or preference, priority,or other security
interest or preferential arrangement arising pursuant to any Environmental Law or as a result of the presence, Release
or threatened Release or disposal of any Hazardous Materials. Grantee and Grantor agree that, in the event of any
Release or Threatened Release of Hazardous Materials in, at, on, under, about, originating from or relating to the
Property, or any Claims or Losses relating thereto, then (i) there shall be a presumption that such Hazardous Materials
were first introduced and first present in, at, on, under or about the Property after the Effective Date, -and (ii) Grantee
shall bear the burden of proof if Grantee claims or asserts that such Hazardous Materials were present in, at, on, under
or about the Property on or prior to the Effective Date.
Grantee agrees that it shall not sell, assign or otherwise transfer any of the Property unless the ptirch'aser, assignee or
transferee thereof, at or prior to such sale, assignment or transfer, agrees in writing (x) to be bound by and comply with
the terms of this Section 3 as if it were the Grantee hereunder, and (y) that Grantor is an intended beneficiary of such
writing. The immediately preceding sentence shall expire and be of no further force and effect at such time as none of
the following owns any portion of the Subject Property: (i) Grantor, (ii) Grantor's affiliates, (iii) any successor to all or
substantially all of the business of Grantor or its affiliates, and (iv) any direct or indirect subsidiary of Wienerberger AG.
SECTION 4. Notice, Any notice required or permitted to be given under this Agreement shall be in writing
and shall be deemed to have been given when deposited in Federal Express (or any other reputable national "next day"
delivery service) or in the United States mail via registered or certified mail, postage prepaid, return rreceipt requested,
and addressed as follows:
GRANTOR: General Shale Brick, Inc.
3015 Bristol Highway
Johnson City, Tennessee 37601
Attn: Real Estate Department
Phone: [phone]
and a copy (which shall
not constitute notice)
to: John A. Flaherty, Esq.
Dickstein Shapiro LLP
One Stamford Plaza
263 Tresser Blvd
Stamford, CT 06902
Phone: [phone]
GRANTEE: Green Meadows, LLC
12601 Plantside Drive
Louisville, KY 40299
Phone: [phone]
PAGE 4
CHARZ163874I v2

1770
0106
BOOK 17 7 0 PAGE 010 6
and a copy (which shall
not constitute notice)
to: Moore & Van Allen PLLC
100 N. Tryon Street, Suite 4700
Charlotte, North Carolina 28202-4003
Attention: Henry B. Ward, III
Phone: [phone]
Either Party may, from time to time, by notice as herein provided, designate a different address to which notices shall
be sent. Rejection or other refusal to accept or inability to deliver a notice required hereunder because of a changed
address of which no notice was given shall be deemed to be receipt of the notice. Grantee and Grantor agree that the
counsel for the Parties may deliver notice on behalf of the Parties.
SECTION 5. General Provisions.
(a) Applicable Law. This Agreement shall be governed by and construed in accordance with the
substantive laws of the State of North Carolina, without giving effect to its conflict of laws provisions.
(b) Entire Agreement. This Agreement and the Contract contain the entire understanding and
agreement by and between the Parties with respect to the Use Restriction, and all prior or contemporaneous oral or
written agreements regarding the Use Restriction, except for the Contract, are merged herein.
(c) Binding Effect. This Agreement shall be binding upon and shall inure to the benefit of the Parties,
and their respective heirs, successors and assigns.
(d) Severability. If any term or provision, or any portion thereof, of this Agreement, or the application
thereof to any person or circumstances shall, to any extent, be determined by a court of competent jurisdiction to
be invalid or unenforceable, then the remainder of this Agreement, or the application of such term or provision to
persons or circumstances, other than those as to which it is held invalid or unenforceable, shall not be affected
thereby, and each term and provision of this Agreement shall be valid and be enforced to the fullest extent permitted
by law.
(e) Captions and Headings. The captions and headings throughout this Agreement are for convenience
and reference only and the words set forth therein shall in no way be held to define or add to the interpretation,
construction or meaning of any provision of this Agreement.
(f) No Waiver. Failure of any Party to insist upon compliance of any provision of this Agreement .
shall not constitute a waiver of the rights of such Party to subsequently insist upon compliance with that provision
or any other provision of this Agreement, nor in any way to affect the validity of all or any part of this Agreement.
(g) Amendment. No amendment to this Agreement shall be effective unless made in a writing signed
by the Parties, or their respective successors and assigns, and recorded on the Chatham County Registry.
[The remainder of this page is intentionally left blank; signatures begin on the following page.]
CHAR211638741 v2
PAGE S

1770 '
0107 eou 17 7 0 pha 010 7
IN WITNESS WHEREOF, Grantor and Grantee have duly executed this Agreement as of the
day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By;
Kevin H. Ham, Vice President
State of Tennessee - County of
I, the undersigned Notary Public of the County of and State aforesaid,
certify that Kevin H. Ham personally came before me this day and ac cnowledged that he is the Vice
President of General Shale Brick, Inc., a Delaware corporation, and that by authority duly given and
as the act of such entity, he signed the foregoing instrument in its name on its behalf as its act and deed.
Witness my hand and Notarial stamp or seal, this -T' day of November, 2014.
My Commission Expires:
6 -a9 - .zorto
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9.
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[The remainder of this page is intentionally left blank; Grantee's signature is on the following page.]
EASEMENT AGREEMENT PAGE 6
AND DECLARATION OF COVENANTS

1770
0108
gooK 1770ME0108
GREEN MEADOW, LLC,
a North Carolina Whited liability company
By: Charah nc., its Member/M ger
By:
Print Name: Charles E. Price
Title: President & CEO
State of - County of .•�
I, the undersigned Notary Public of the County of and State aforesaid, certify that
Charles E. Price personally came before me this day and a0gowfedged. that he is the President & CEO of Charah,
Inc., the Member/Manager of Green Meadow, LLC, a North Carolina limited liability company, and that by
authority duly given and as the act of such entity, he signed the foregging instrument in its name on its behalf as its
act and deed. Witness my hand and Notarial stamp or seal, this =day of November, 2014.
My C�Expires: I—) A- ✓U Notary Public
Notary's Printed or Typed Name
(Affix Seal)
tlrrrryry�,
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7
PAGE 7

Transmittal
RECEIVED
DEC 15 2014
DFNR-LAND QUALITY
STORMWATER PFRi I i'TING
Date: Friday, December 12, 2014
Project: Brickhaven $ Colon Mine Sites
To: Bradley Bennett — NCDENR Division of Energy, Mineral and Land Resources — Stormwater
Permitting Program
From: Mike Plummer
Subject: Brickhaven & Colon Mine Sites Ownership Change
We are sending you: ® Attached ❑ Under separate cover via the following items:
❑ Shop drawings ❑ Prints ❑ Plans
❑ Samples ❑ Specifications ❑ Copy of letter
❑ Change Order ❑ Other:
Copies Date No. Description
1 12/12/2014 Colon Mine Site Permit Name/Ownership Change
Form
1 11/13/2014 Colon Mine Recorded Deed
1 11/21/2013 Colon Mine NPDES Permit COC NCG020854
1 12/12/2014 Brickhaven Permit Name/Ownership Change Form
1 11/13/2014 Brickhaven Mine Record Deed
1 2/11/2010 Brickhaven NPDES Permit COC NCG020354
These are transmitted as checked below:
® For your approval ❑ Approved as submitted
❑ For your use ❑ Approved as noted
❑ As requested ❑ Returned for corrections
❑ For review/comment ❑ Other:
❑ For bids due
Remarks:
Copy to:
❑ Resubmit
❑ Submit
❑ Return
❑ Prints returned after loan to us
Signed: gmiRummer

Division of Energy, Mineral & Land Resources FOR AGENCY USE ONLY
Data Roce[ved
Land Quality Section/Stormwater Permitting Year Month o
National Pollutant Discharge Elimination System
NCDENR
PERMIT NAME/OWNERSHIP CHANGE FORM
1. Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
G 1 $101 2 10 10 0 7T I N I C I G 0 2 0 3 5 4
11. Permit status prior to requested change.
a. Permit issued to (company name): General Shale Brick, Inc.
b. Person legally responsible for permit: Gregory A Bowles
First MI Last
Director of Real Estate, Environment & Geology
Title
RECEIVED 3015 Bristol Hi wa
DEC 15 2014 Permit Holder Mailing Address
Johnson City TN 37601
GEAIR-I.AN!0 QUALITY � City State Zip
STORMWATER PERMITTING [phone] _(_ )
Phone ..... Fax
c. Facility name (discharge): Brickhaven No. 2 Mine Tract "A"
d. Facility address: 1149 Moncure Flatwood Road
Address
Moncure NC 27559
City State Zip
e. FaciIity contact person: [phone] ext.
_ Larry Cockerill _ _ 243
First / MI / Last Phone
11I. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ® Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain:
b. Permit issued to (company name):
c. Person legally responsible for permit:
Green Meadow, LLC
Charles E Price
First MI Last
Managing Member
Title
12601 Plantside Drive
Permit Holder Mailing Address
Louisville KY 40299
City State Zip
(502)_245-1353 __cprice [e-mail]
Phone E-mail Address
d. Facility name (discharge):
Brickhaven No. 2 Mine Tract "A"
e. Facility address:
H49 Moncure Flatwood Road
Address
Moncure NC 27559
City State Zip
f. Facility contact person:
Charles E Price
First MI Last
[phone] _ [e-mail] -
Phone E-mail Address

NPDES PERMIT_ NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
IV. Permit contact information (if different from the person legally responsible for the permit)
Permii contact: Charles E Price
First MI Last
_ Managing, Member
Title
12601 Plantside Drive
Mailing Address
Louisville KY 40299
city state zip
[phone] [e-mail]
Phone E-mail Address
V. Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
VI Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE;OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
.....................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
I, Gregory A. Bowles, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will be returned as incomplete.
(z A%Ak
Signature T T Date
APPLICANT CERTIFICATION
1. Charles.E. Price, attest that this application for a name/ownership change has been reviewed and is
accurate and complete to the best of in), knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information is not included, this application
package will returned as incom e
Signature,
Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy. Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612

FILED
T770 -
0099 n
oou 17 7 0 PAGE 0 0 9 9
Excise Tax: $23,700.00
CHATHAM COUNTY NC
TREVA B. SEAGROVES
REGISTER OF DEEDS
FILED Nov 13, 2014
AT 01:04:38 pm
BOOK 01770
START PAGE 0099
END PAGE
0108
INSTRUMENT #
11093
EXCISE TAX
$23,700.00
NORTH CAROLINA SPECIAL WARRANTY DEED
Parcel Identifier No. 0005361, 0005362, 0071836, 0085332 (portion) and 0061577 (portion) Verified by County on
the day of , 2014 By: T
Mail/Box to: Moore & Van Allen PLLC (MPH), 100 N. Tryon Street. Suite 4700, Charlotte, NC 28202
This instrument was prepared by:Bradshaw & Robinson, LLP, P.O. Box 607, Pittsboro, NC 27312 (without title examination)
Brief description for the Index: 333.55 acres, more or less, Cage Fear Township, Chatham County
THIS DEED made this 13th day of November, 2014 (the "Effective Date"), by and between
GRANTOR
GENERAL SHALE BRICK, INC.,
a Delaware corporation
3015 Bristol Highway
Johnson City, Tennessee 37601
GRANTEE
GREEN MEADOW, LLC,
a North Carolina limited liability company
12601 Plantside Drive
Louisville, Kentucky 40299
Enter in appropriate block for each Grantor and Grantee: name, mailing address, and, if appropriate, character of entity, e.g.
corporation or partnership.
The designation Grantor and Grantee as used herein shall include said parties, their heirs, successors, and assigns, and shall include
singular, plural, masculine, feminine or neuter as required by context.
WITNESSETI-i, that the Grantor, for a valuable consideration paid by the Grantee, the receipt ofwhich is hereby acknowledged, has and
by these presents does grant, bargain, sell and convey unto the Grantee in fee simple, all that certain lot, parcel of land or condominium
unit situated in Cape Fear Township, Chatham County, North Carolina and more particularly described as follows (the "Property"):
Being all of that certain parcel or tract of land identified as "Tract A 333.55 Acres" and shown on map or plat
entitled, "Recombination Survey of General Shale Brick, Inc." prepared by WNC Professional Engineers &
Surveyors recorded in Plat Slide 2014-263, Chatham County Public Registry, reference to which is hereby
made for a more particular description.
Page 1 of 3

1'770
0100
an 17 7 0 PAGE 010 O
The Property was acquired by Grantor by instruments recorded in Book 696, Page 894, in Book 1326, Page 940, and in Book 1326,
Page 950, Chatham County Registry. Grantor is the successor -by -merger to Cherokee Sanford Group, LLC, a Delaware limited
liability company.
All or a portion of the Property does not include the primary residence of the Grantor.
Grantor hereby expressly conveys the Property subject to, and Grantor hereby expressly reserves from this conveyance, the Use
Restriction, and all other terms and conditions, and rights of the Crantor, pursuant to Exhibit A attached hereto and
incorporated herein by reference.
TO HAVE AND TO HOLD the aforesaid lot or parcel of land and all privileges and appurtenances thereto belonging to the Grantee in
fee simple.
And the Grantor covenants with the Grantee, that Grantor has done nothing to impair such title as Grantor received, and Grantor will
warrant and defend the title against the lawful claims of all persons claiming by, under or through Grantor, other than the following
exceptions:
1. Any defects in, interests in, objections to, exceptions to, or conditions, liens, encumbrances or other matters of record
relating to the title to the Property, whether evidenced by written instrument, or, if not evidenced by written
instrument, then any such matters that would be revealed by an accurate survey of the Property completed on the
Effective Date in accordance with exception #7, below.
2. Any encroachments upon or by the Property, any boundary disputes or conflicts regarding the boundaries of the
Property, any claims, rights -of -way, easements, restrictions and restrictive covenants upon or relating to the Property,
any encumbrances or other title defect(s), and the terms, provisions and conditions set forth in any instruments
evidencing or referring to any such defects, exceptions, conditions, liens, encumbrances, overlaps, encroachments or
boundary disputes or other matters.
3. All matters listed in Schedule B — Section 11 of the ALTA Commitment Form Commitment for Title Insurance issued
by Chicago Title Insurance Company as Commitment Number 14-12874CH (Revision 7, dated November 7, 2014),
which matters are incorporated herein by reference, including, but not limited to that certain Timber Deed and
Easement by and between Cherokee Sanford Group, LLC and Cherokee Land Company, LLC recorded in Book 817,
Page 632, Chatham County Registry.
4. The lien of non -delinquent real property taxes and assessments, and any other non -delinquent impositions orexactions
of any governmental or quasi -governmental authority or body politic, or political subdivision, agency or department
thereof.
5. Any service, installation, connection, maintenance or construction charges due subsequent to the Effective Date.
6. The effect of any federal, state or municipal laws, rules, regulations or ordinances having applicability to the Property,
or any portion thereof, or the use or enjoyment of the same, whether now or hereafter in effect, including, but not
limited to, zoning, building, health, safety and environmental laws, rules and regulations, and notices of record relating
thereto.
7. Any defects in, interests in, objection to, exceptions to, or conditions, liens, encumbrances or other matters that would
have been disclosed on a current ALTAIACSM Land Title Survey of the Property prepared as of the Effective Date in
accordance with the 2011 Minimum Standard Detail Requirements for ALTAIACSM Land Title Surveys jointly
established and adopted by ALTA, ACSM and NSPS.
8. Any discrepancies, shortages in area, or state of facts which an inspection of the Property would disclose and which are
not shown by the public records.
9. Any creditors' rights exceptions customarily taken by title insurance companies.
[The remainder of this page is intentionally left blank; Grantor's signature is on the following page.]
Page 2 of 3

T770
0101
Bog 17 7 o PUE 0 o
IN WITNESS WHEREOF, the Grantor has duly executed the foregoing as of the day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By:
Kevin H. Ham, Vice President
State of Tennessee - County of L iyn
I, the undersigned Notary Public of the County of and State aforesaid, certify that Kevin II. Ham
personally came before me this day and acknowledged that he is the ice President of General Shale Brick, Inc., a Delaware
corporation, and that by authority duly given and as the act of such entity, he signed the foregoing instrument in its name on its behalf
as its act and deed. Witness my hand and Notarial stamp or seal, this S day of November, 2014.
My Commission Expires: '07�
(Affix Seal)
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i TENNESSEE ,
. NOTARY r
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Page 3 of 3
Notary Public
Notary's Printed or Typed Name

1'770
0102
BOOK 1 7 7 O ME O 102
EXHIBIT A TO
NORTH CAROLINA SPECIAL WARRANTY DEED
THIS EXHIBIT A TO NORTH CAROLINA SPECIAL WARRANTY DEED (this "Agreement") is
entered into as of November 13, 2014 (the "Effective Date") by and between GENERAL SHALE BRICK, INC.,
a Delaware corporation (the "Grantor") and GREEN MEADOW, LLC, a North Carolina limited liability company
(the "Grantee"). Grantor and Grantee are sometimes referred to herein individually as a "Party" and collectively
as the "Parties."
WITNESSETH:
THAT, WHEREAS, the Parties entered into that certain Agreement for Purchase and Sale of Property dated
November 12, 2014 (the "Contract"); and
WHEREAS, the Parties wish to provide record notice of certain terms of the Contract including, but not
limited to, matters regarding the Use Restriction.
NOW, THEREFORE, in consideration of ten dollars ($10.00), and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged, Grantor and Grantee hereby agree as
follows:
SECTION 1. Declaration of Covenants. Grantor, with the joinder and the consent of the Grantee, hereby
declares that the Property shall be held, conveyed, encumbered, used, occupied and improved subject to the
following covenants, which shall encumber the title to the Property and shall be binding upon all persons now
having or hereafter acquiring any right, title, or interest in the Property, and their respective heirs, successors, and
assigns, and which shall inure to the benefit of the Grantor, its successors and assigns (the "Use Restriction"):
(a) Use Restriction. Prior to October 31, 2049, the Property shall not be used for the production,
manufacturing, storage, transportation or distribution of bricks, ceramic clay products or concrete masonry units.
This restriction on use shall run with the title to the Property and shall be enforceable by Grantee, its successors and
assigns. The Use Restriction shall expire and be null and void without further action of any Party on October 31,
2049 at 11:59 p.m. (local time).
SECTION 2. Environmental Release. Grantee, on behalf of itself and its members, managers and affiliates
and each of their respective successors and assigns (collectively, the "Releasors"), as of the Effective Date, hereby
waives, releases, and absolutely and forever discharges Grantor and its officers, directors, shareholders, subsidiaries,
affiliates, employees, agents and representatives, and their respective heirs, successors and assigns (collectively, the
"Releasees"), from any and all present or future rights, claims, actions, causes of action, demands, damages, liabilities,
attomeys' fees, costs, fines, penalties and expenses of every kind and nature whatsoever, now known or unknown, direct
or indirect, which any of the Releasors may have with respect to any of the Releasees, directly or indirectly arising from
or relating to (x) the presence or alleged presence of Hazardous Materials in, on, under, about, originating from or
relating to the Property if such Hazardous Materials were present at the Property on or prior to the Effective Date
including, without limitation, any such claims under or on account of any Environmental Law or this Agreement, (y)
any violation or alleged violation of any Environmental Law in connection with the Property that occurred or is alleged
to have occurred on or prior to the Effective Date, and (z) the ownership, use, occupancy or operation of the Property
by Releasees on and prior to the Effective Date, including the use and/or operation of the Property for the mining of
clay or other mineral substances, and the conduct of any activities affecting the air, soil and/or water of the Property,
and activities related to the foregoing.

1'770
0103
Boox 17 7 0 ME 010 3
SECTION 3. Environmental Indemnity. From and after the Effective Date, Grantee shall indemnify,
defend and hold harmless Grantor and the other Iteleasees (individually, a "Grantor Indemnitee" and collectively,
"Grantor Indemnitees") from and against, and pay for (a) any and all actions, allegations, appeals, causes of action
(including removal and remedial actions), claims, demands, investigations, and lawsuits, of any kind, brought by
Grantee, a third party or any government entity against any Grantor Indemnitees based on, or arising or resulting from
(1) the actual or alleged presence of Hazardous Materials at, on, under or adjacent to the Property, to the extent such
Hazardous Material was first present or first alleged to be present at, on, under or adjacent to the Property on or after
the Effective Date, (2) any activity by Grantee, or any Person affiliated with Grantee, in connection with any actual,
proposed or threatened use, treatment, storage, holding, existence, disposition or other Release, generation, production,
manufacturing, processing, refining, control, management, abatement, removal, arrangement for disposal, handling,
transfer or transportation to or from the Property of any Hazardous Materials at any time located in, under, on or above
the Property, (3) the imposition, recording or filing or the threatened imposition, recording or filing of any
Environmental Lien encumbering the Property relating in any way to the activities conducted on, or operation or use
of, the Property on or after the Effective Date; (4) any actual or threatened injury to, destruction of, or loss of natural
resources in any way connected with the Property arising on or after the Effective Date, including, but not limited to,
costs to investigate and assess such injury, destruction or loss relating in any way to the activities conducted on, or
operation or use of, the Property on or after the Effective Date; (5) any personal injury, wrongful death, or property or
other damage arising on or after the Effective Date under any statutory or common law or tort law theory, related to
environmental hazards on the Property, including, but not limited to, damages assessed for private or public nuisance
or for the conducting of an abnormally dangerous activity on the Property relating in any way to the activities conducted
on, or operation or use of, the Property on or after the Effective Date; and (6) any Environmental Claim relating in any
way to the Grantee's operation or use of the Property on or after the Effective Date (individually, a "Claim" and
collectively, "Claims"); and (b) any and all assessments, civil penalties, out-of-pocket costs and expenses (including
court costs and reasonable attorneys' fees) actually incurred by a Grantor Indemnitee (but excluding costs and expenses
of defending any Claim incurred by any such Grantor Indemnitee after Grantee has accepted and is diligently pursuing
defense of such Claim, unless such costs and expenses of defending such Claim are incurred with Grantee's prior written
consent), damages (including consequential and punitive damages awarded to any third -party), decrees, fines,
judgments, liabilities (including for strict liability), losses, obligations, orders and penalties (whether compensatory or
punitive) which may be assessed against or suffered or incurred by any Grantor Indemnitee based upon, or arising or
resulting from (i) any Claim that is (y) owed to Grantee, a third -party or any governmental entity, or (z) related to any
remedial actions to the Property required of Grantor under any applicable Environmental Law; or (ii) to the extent
arising out of, relating to or resulting from the Release or Threatened Release of Hazardous Materials from the Property
to, on, under, adjacent to, or otherwise affecting the real property owned by Grantor (including as successor in interest
to Cherokee Sanford Group, LLC, a Delaware limited liability company), or General Shale, Inc., on the date hereof (the
"Subject Property"), any remedial actions reasonably appropriate to enable clay to be mined from the Subject Property
or required to comply with applicable Environmental Law, including, without limitation, action to (x) test, identify,
investigate and monitor such Hazardous Materials or Release, and (y) clean-up, contain and remove such Hazardous
Materials (all of the foregoing, collectively,
In the event that any Grantor Indemnitee receives written notice of the assertion of any Claim by any third -party or any
governmental entity with respect to which the Grantee is required to provide indemnification under this Agreement, the
Grantor Indemnitee shall provide Grantee with prompt written notice (a "Claim Notice") of any Claim for which
indemnity is sought, which Claim Notice shall set forth in reasonable detail a statement of the pertinent facts known to
the Grantor Indemnitee concerning the Claim(s) that are the subject of the Claim Notice; provided, however, that any
failure by a Grantor Indemnitee to give a timely, complete or accurate Claim Notice shall not affect the rights or
obligations of any party hereunder except and only to the extent that, as a result of such failure, Grantee's defense of
any such Claim was materially and adversely prejudiced. Grantee shall have the right, upon delivering written notice
(the "Defense Notice") to the Grantor Indemnitee within six (6) months after receipt from a Grantor Indemnitee of a
Claim Notice, to assume and conduct, at Grantee's sole cost and expense, the defense against those Claims identified
PAGE 2
CHAR2\163874I Q

0104 coax 17 7 0 PAGE 010 4
in the Claim Notice that are identified in the Defense Notice; provide d, however, that (i) delivery by Grantee of a
Defense Notice shall constitute Grantee's irrevocable agreement that the Grantor Indemnitee(s) are entitled to
indemnification under this Agreement with respect to the Claims set forth in the Defense Notice, and (ii) Grantor shall
have the right to approve the defense counsel engaged by Grantee, such approval not to be unreasonably withheld,
conditioned or delayed (provided that Grantor hereby approves Moore & Van Allen PLLC). In the event that Grantee
shall fail to give a Defense Notice for any Claims identified in the Claims Notice within six (6) months after receipt
from a Grantor Indemnitee of such Claim Notice, then in any such event the Grantor Indemnitees shall have the right
to conduct the defense of the Claims identified in the Claim Notice in good faith, provided that Grantor Indemnitees
shall be prohibited from compromising or settling any such Claims without the prior written consent of Grantee, which
consent shall not be unreasonably withheld, conditioned or delayed. In order to seek Grantee's consent, a Grantor
Indemnitee must provide to Grantee written notice detailing all of the terms, conditions and obligations of any proposed
settlement or compromise, including providing a copy of any proposed settlement agreement or other contractual
arrangement to be executed by parties to the proposed settlement or compromise (a "Grantor Indemnitee Settlement
Notice"). If Grantee does not provide to the respective Grantor Indemnitee(s) a written response to a Grantor
Indemnitee Settlement Notice within twenty (20) Business Days of Grantee's receipt of the Grantor Indemnitee
Settlement Notice (as provided in Section 18(b) herein), then Grantee's consent will be deemed given to the respective
Grantor Indemnitee. In the event the Grantee does timely deliver a Defense Notice and thereby elects to conduct the
defense of the Claims identified in the Defense Notice, the Grantor Indemnitees will cooperate with and make available
to the Grantee such assistance and materials as Grantee may reasonably request, all at the sole cost and expense of
Grantee. Regardless of which party defends such Claims, the other party hereto shall have the right at its own cost and
expense to participate in the defense assisted by counsel of its own choosing. Without the prior written consent of the
Grantor Indemnitees, which shall not be unreasonably withheld, conditioned or delayed, Grantee shall not approve the
entry of any judgment or enter into any settlement or compromise of any such Claims if (a) pursuant to or as a result of
such judgment, settlement or compromise, such judgment, settlement or compromise would lead to liability or create
any financial or other obligation on the part of any Grantor Indemnitee for which the Grantor Indemnitee is not fully
indemnified and made whole hereunder, (b) the terms of such judgment, settlement or compromise do not provide for
a full and complete release of all such Claims in favor of each Grantor Indemnitee that is the subject of the Claim, and
(c) injunctive or other equitable relief will be imposed against any Grantor Indemnitee. In order to seek a Grantor
Indemnitee's consent, Grantee must provide to the Grantor Indenmitee written notice detailing all of the terms,
conditions and obligations of any proposed judgment, settlement or compromise, including providing a copy of any
proposed settlement agreement or other contractual arrangement to be executed by parties to the proposed settlement
or compromise (a "Grantee Settlement Notice"). If a Grantor Indemnitee does not provide to Grantee a written
response to a Grantee Settlement Notice, within twenty (20) Business Days of the Grantor Indemnitee's receipt of the
Grantee Settlement Notice (as provided under Section 4 herein), then the Grantor Indemnitee's consent shall be deemed
given to the Grantee. Any judgment entered or settlement or compromise agreed upon as set forth in a Grantor
Indemnitee Settlement Notice that is consented to by Grantee or a Grantee Settlement Notice that is consented to by
Grantor, in the manner provided herein, shall be binding upon Grantee, and shall be conclusively deemed to be an
obligation with respect to which the Grantor Indemnitees are entitled to prompt indemnification hereunder, -subject to
Grantee's right to appeal an appealable judgment or order.
For purposes of this Agreement, the term "Hazardous Materials" means chemicals, pollutants, contaminants, wastes,
toxic substances, hazardous substances, radioactive materials or genetically modified organisms, which are, have been
or become regulated by any federal, state or local government authority including, without limitation, (w) petroleum or
any fraction thereof, (x) asbestos, (y) any substance or material defined as a "hazardous substance" pursuant to § 101
of the Comprehensive Environmental Response, Compensation, and liability Act (42 U.S.C. § 9601), or (z) any
substance or material defined as a "hazardous chemical" pursuant to the federal Hazard Communication Standard (29
C.F.R. § 1910.1200); the term "Environmental Claim" means any claim, action, cause of action, investigation, or
notice (written or oral) by any person or entity alleging potential liability (including, without limitation, potential
liability for investigatory costs, cleanup costs, governmental response costs, natural resource damages, property
damages, personal injuries, or civil or criminal penalties) arising out of or resulting from (yy) the actual or alleged
PAGE 3
CHAR2%1638741 v2

1-770 94�K 1 (! 0 pnE 010 5
0105
presence or release into the environment of any Hazardous Materials at any location, whether or not owned or operated
by the Grantor, or (zz) circumstances forming the basis of any actual or alleged violation of any Environmental Law;
and the term "Environmental Law" means all federal, state, local, and foreign laws and regulations relating to pollution
or protection of human health or the environment (including, without limitation, ambient air, surface water, ground
water, wetlands, land surface, subsurface strata, and indoor and outdoor workplace), including, without limitation, (yyy)
laws and regulations relating to emissions, discharges, releases, or threatened releases of Hazardous Materials, and (v_z)
common law principles of tort liability. The terms "Release" and "Threatened Release" shall have the meanings
defined under Environmental Law. The term "Environmental Lien" means any mortgage, pledge, hypothecation,
assignment, deposit arrangement, encumbrance, lien (statutory or other), charge, or preference, priority or other security
interest or preferential arrangement arising pursuant to any Environmental Law or as a result of the presence, Release
or threatened Release or disposal of any Hazardous Materials. Grantee and Grantor agree that, in the event of any
Release or Threatened Release of Hazardous Materials in, at, on, under, about, originating from or relating to the
Property, or any Claims or Losses relating thereto, then (i) there shall be a presumption that such Hazardous Materials
were first introduced and first present in, at, on, under or about the Property after the Effective Date, and (ii) Grantee
shall bear the burden of proof if Grantee claims or asserts that such Hazardous Materials were present in, at, on, under
or about the Property on or prior to the Effective Date.
Grantee agrees that it shall not sell, assign or otherwise transfer any of the Property unless the purchaser, assignee or
transferee thereof, at or prior to such sale, assignment or transfer, agrees in writing (x) to be bound by and comply with
the terms of this Section 3 as if it were the Grantee hereunder, and (y) that Grantor is an intended beneficiary of such
writing. The immediately preceding sentence shall expire and be of no further force and effect at such time as none of
the following owns any portion of the Subject Property: (i) Grantor, (ii) Grantor's affiliates, (iii) any successor to all or
substantially all of the business of Grantor or its affiliates, and (iv) any direct or indirect subsidiary of Wienerberger AG.
SECTION 4. Notice. Any notice required or permitted to be given under this Agreement shall be in writing
and shall be deemed to have been given when deposited in Federal Express (or any other reputable national "next day"
delivery service) or in the United States mail via registered or certified mail, postage prepaid, return receipt requested,
and addressed as follows:
GRANTOR: General Shale Brick, Inc.
3015 Bristol Highway
Johnson City, Tennessee 37601
Attn: Real Estate Department
Phone: [phone]
and a copy (which shall
not constitute notice)
to: John A. Flaherty, Esq.
Dickstein Shapiro LLP
One Stamford Plaza
263 'Presser Blvd
Stamford, CT 06902
Phone: [phone]
GRANTEE: Green Meadows, LLC
12601 Plantside Drive
Louisville, KY 40299
Phone: [phone]
PAGE 4
CHAR2U 638741 v2

1770
0106
Bou 177 0 ?ADE 010 S
and a copy (which shall
not constitute notice)
to: Moore & Van Allen PLLC
100 N. Tryon Street, Suite 4700
Charlotte, North Carolina 28202-4003
Attention: Henry B. Ward, Ill
Phone: [phone]
Either Party may, from time to time, by notice as herein provided, designate a different address to which notices shall
be sent. Rejection or other refusal to accept or inability to deliver a notice required hereunder because of a changed
address of which no notice was given shall be deemed to be receipt of the notice. Grantee and Grantor agree that the
counsel for the Parties may deliver notice on behalf of the Parties.
SECTION 5. General Provisions.
(a) Applicable Law. This Agreement shall be govcrncd by and construed in accordance with the
substantive laws of the State of North Carolina, without giving effect to its conflict of laws provisions.
(b) Entire Agreement. This Agreement and the Contract contain the entire understanding and
agreement by and between the Parties with respect to the Use Restriction, and all prior or contemporaneous oral or
written agreements regarding the Use Restriction, except for the Contract, are merged herein.
(c) Binding Effect. This Agreement shall be binding upon and shall inure to the benefit of the Parties,
and their respective heirs, successors and assigns.
(d) Severability. If any term or provision, or any portion thereof, of this Agreement, or the application
thereof to any person or circumstances shall, to any extent, be determined by a court of competent jurisdiction to
be invalid or unenforceable, then the remainder of this Agreement, or the application of such term or provision to
persons or circumstances, other than those as to which it is held invalid or unenforceable, shall not be affected
thereby, and each term and provision of this Agreement shall be valid and be enforced to the fullest extent permitted
by law,
(e) Captions and Headings. The captions and headings throughout this Agreement are for convenience
and reference only and the words set forth therein shall in no way be held to define or add to the interpretation,
construction or meaning of any provision of this Agreement.
(f) No Waiver. Failure of any Party to insist upon compliance of any provision of this Agreement
shall not constitute a waiver of the rights of such Party to subsequently insist upon compliance with that provision
or any other provision of this Agreement, nor in any way to affect the validity of all or any part of this Agreement.
(g) Amendment. No amendment to this Agreement shall be effective unless made in a writing signed
by the Parties, or their respective successors and assigns, and recorded on the Chatham County Registry.
[The remainder of this page is intentionally left blank; signatures begin on the following page.]
PAGE 5
CHAR211638741 v2

1770
0107 sao 17 7 0 phi Q 10 7
IN WITNESS WHEREOF, Grantor and Grantee have duly executed this Agreement as of the
day and year first above written.
GENERAL SHALE BRICK, INC.,
a Delaware corporation
By: �� z
Kevin H. Ham, Vice President
State of Tennessee - County of
I, the undersigned Notary Public of the County of and State aforesaid,
certify that Kevin H. Ham personally came before me this day and ac cnowledged that he is the Vice
President of General Shale Brick, Inc., a Delaware corporation, and that by authority duly given and
as the act of such entity, he signed the foregoing instrument in its name on its behalf as its act and deed.
Witness my hand and Notarial stamp or seal, this -5- day of November, 2014.
My Commission Expires:
- .20!
�CggT0�0�
STATE ••~ 9
r
. - .1 NOTARV
Notary Public
Notary's Printed or Typed Name
[The remainder of this page is intentionally left blank; Grantee's signature is on the following page.]
EASEMENT AGREEMENT PAGE 6
AND DECLARATION OF COVENANTS

1770
0108
B04K 1 7 7 d PAGE O 1 0 8
GREEN MEADOW, LLC,
a North Carolina limited liability company
By: CharCah nc., its Member/M ger
By:Ze
Print Name: Charles E. Price
Title: President & CEO
State of - County of
I. the undersigned Notary Public of the County of and State aforesaid, certify that
Charles E. Price personally came before me this day and aclgowfeJged that he is the President & CEO of Charah,
Inc., the Member/Manager of Green Meadow, LLC, a North Carolina limited liability company, and that by
authority duly given and as the act of such entity, he signed the fore#2ing instrument in its name on its behalf as its
act and deed. Witness my hand and Notarial stamp or seal, this ZLday of November, 2014.
My Cf�mmission Expires: r� ✓� , Notary Public
11 �L �d_� Z Notary's Printed or Typed Name
(Affix Seal)
�F,..�,sfrl{�Frry
c r�
� __
C3
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PAGE 7

Alexander, Laura
From: Georgoulias, Bethany ;•.
Sent: Friday, June 27, 2014 12A2 PM
To- Alexander, Laura
Subject: FW: Permit -Facility Contact Updates
142
Be+lkiny G or's,roidius, E-Divironniewa11;nginuer
NCf7ENR / Division ofE?nergy, Mineral, and Lind Resources
Storrmyater Periniiting Progr tm
1612 Mail Service Center, Raleigh, NC-2709-1 G 12
512 N. Sttiisbivy Street, Raleigh, NC 27604
919 / 807-6372 (phone); 919 1807-6494 (fah)
Wcbsito: fittn;//portal.ncder; r �ti� /lr/4tnrm rFit
I -rnoh' cot•respuridarrca to and fi•mis this yddress uacp• be sldyucl u, tha North Carolina l'uhhe Records ,rnr and nxrn he disaGrsel to third parries,
From: [e-mail] fma_ho• [e-mail]]
Sent; Thursday, May 29, 2014 10:33 AM
To: SVC DENR.stormwater
Subject: Permit -Facility Contact Updates
PI ase Update contacts as follows:
NCGO20533
VOwner Affiliation - Parmit Narne/Ownership Change Form to be submitted
Contact Name -- Steve Wyse, PO Box 3547, Johnson City, TN 37602, 423/952-42811
[e-mail]
FacilityContact - Warren Paschal, 300 Brick Plant road Moncurre NC 919/744-6533 x-
�
221, [e-mail]
JPermit Contact -- Steve Wyse, PO Box 3547, Johnson City, TN 37602, 423/952-4281,
steve [e-mail]
CG020354
Owner Affiliation - Permit Name/Ownership Change Form to be submitted
✓Contact Name - Steve Wyse, PO Box 3547, Johnson City, TN 37602, 423/952-4281,
steve.wyse2generalshalt✓:ggm
Facility Contact - Warren Paschal, 300. Brick
221., warren. ascha enerals ale.com
Permit Contact - Steve Wyse, PO Box 3547,
steve.wyse Aener'alshale�rQm
Steve Wyse
General Shale
42.31952-4281
Plant road, Moncure, NC 91.9/744-653.3 x-
Johnson City, TN 37602, 423/952-4281,

ti
1#
',�A1 Is Division of Energy, Mineral & Land Resources
! Land Quality SectfonlStormwater Permitting
National Pollutant Discharge Elimination System
NC®ENR
N m.GrnuxOavnwtwrrr br
PERMIT NAMEIOWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
Month
bay
I. Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
N I O j S 1 O N I G 1 ,3 1 0 12 1 0 13 5 4
IL Permit status prior to requested change.
a. Permit issued to (company name): General Shale Brick, Inc.
b. Person legally responsible for permit: Gregory Bowles
First Ml Last
Director of Environment
�11 CP Title
! 'r� PO Box 3547
JU� o T ! Permit Holder Mailing Address
j Johnson City TN 37602
D NR - WA QUALITy
� city State Zip
StOrttiW�
tN --raran'N:s' [phone] ( )
a --
__ Phone Fax
c. Facility name (discharge): Moncure II Mine
d. Facility address: Flatwoods Road
Address
Moncure NC 27559
City State Zip
e. Facility contact person: Warren Paschal (919) 774 - 653 3
First / MI / Last Phone
III. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ❑ Change in ownership of the facility
* *No ownership change occurred" ❑ Name change of the facility or owner
Ifother please explain: Name listed on Contacts Summary is incorrect
b. Permit issued to (company name): General Shale Brick, Inc.
c. Person legally responsible for permit: Gregory Bowles
First MI Last
Director of Environment
Title
PO Box 3547
Permit Holder Mailing Address
Johnson City TN 37602
City State Zip
423 282-4661
Phone E-mail Address
d. Facility name (discharge): Moncure II Mine
c. Facility address: Flatwood Road
Address
Moncure NC 27559
City State Zip
f. Facility contact person: Warren Paschal
First MI Last
(919 7Z74-6533 x-221
Phone E-mail Address
warren . p schal@ger eralshale . com
IV. Permit contact information (if different from the person lega y responsible for the permit)
Revised Jan. 27.2014

I
'
e
.
i
„
J

ti
NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
Permit contact: Steve Wyse
First MI Last
Environmental Engineer
Title
PO Box 3547
Mailing Address
Johnson City TN 37602
City State Zip
[phone] [e-mail]
Phone E-mail Address
V Will the permitted facility continue to conduct the same industrial activities conducted prior
to this ownership or name change?
© Yes
❑ No (please explain)
VI. Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is required for an ow e 1. &1 i o ation are
not sufficient for an ownership change **No ownership change occurred*
...................................................................................................................
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as inoom te. ignature Gregory Bowles Date
APPLICANT CERTIFICATION
I, , attest that this application for a name/ownership change has been reviewed and is accurate and
complete to the best of my knowledge. I understand that if all required parts of this application are not
completed and that if all required supporting information is not included, this application package will be
returned as into lete.
ignaturc Gregory Bowles Date
Revised Jan. 27.2014
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612

�Y 1jl i. '.r•
1
_I �,�! tr�•G. 1,- ,..�i' I__4 a ;,.. :r, ,. .- � � }:• 1•r
.t .Si'�;-•�Cu_r'f'1<' :1' •l1:fr' �: `i. r .,. ,'j ',j3;ti. ,li.: l:,r:i; Si'�,: _��

A�)
RCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue
Governor
Warren Paschal
General Shale Brick, Inc.
1600 Colon Rd
Sanford, NG 27330
Dear Permittee:
Coleen H. Sullins
Director
February 11, 2010
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
General Shale Brick, Inc.
COC Number NCG020354
Chatham County
In response to your renewal application for continued coverage under stormwater General Permit NCG020000
the Division of Water Quality (DWQ) is forwarding herewith the reissued stormwater General Permit. This permit
is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October 15,
2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage
• A copy of stormwater General Permit NCG020000
• A copy o1 a Technical Bulletin for the General Permit
• Two copies of the Tier 2 / Exceedence Discharge Monitoring Report (DMR) Form for Stormwater
• One copy each of the Annual Summary DMR Forms for Stormwater and Wastewater
• Two copies of the Limit Violation DMR Form for Wastewater
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater and wastewater, and it specifies your obligations with
respect to discharge controls, management, monitoring, and record keeping. Please review the new permit to
familiarize yourself with all the changes in the reissued permit. If your Certificate of Coverage (COC) restricts
authorization to discharge stormwater only (or other limited terms) based on your original application, or
subsequent modifications to your COC, you must continue to meet these requirements or contact the Stormwater
Permitting Unit to request a modification of this renewal COC.
The more significant changes in the General Permit since your last Certificate of Coverage include the following:
Part II:
• Section B — Language referencing PAMS has been changed. Flocculants may now be used if evaluated
by the Division and administered in accordance with maximum application doses and other requirements.
PPaart III:
• Section A — The permit now requires a Stormwater Pollution and Prevention Plan (SPPP) tailored to the
mining industry, in lieu of a Stormwater BMP Plan.
• Section A - Inactive mines may be inspected on a reduced schedule: at least once per month and after
0.5" (or more) of rain. To qualify, inactive mines must possess an "Inactive Renewal" from DLR or certify
to DWQ the site has been stabilized. The permittee must notify the DWQ Regional Office of inactive
status. Discharges from inactive mines must still be monitored on the same schedule as active mines.
Wetlands and stormwater Branch
1617 MaH Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury SL Raleigh, North Carolina 27604 �TOne
Phone: 919-807-i3M% FAX: 919407-r4941CustamerService: l$77-623-6748 NO Carolina
Internet www.nwaterquality.org Naturally
An Equal oppomrMy 1 Affi mk" Action Employer

Permit Reissuance — Permit Number NCG020354
February 11, 2010
Page 2
• Section B — Revised provisions require that stormwater discharges be sampled twice per year (instead of
annually), and that the sampling results be compared to new benchmark values. (The previous cut-off
concentrations have been removed.)
• Section B — Revised provisions require the permittee to execute Tier One, Tier Two & Tier Three
response actions, based on the first benchmark exceedence (Tier One) and the second consecutive
benchmark exceedence (Tier Two). Tier Two requires that the permittee institute monthly monitoring
(reported to the appropriate Regional Offices) instead of twice -per -year monitoring. Monthly monitoring
shall be done until three consecutive monitoring events show no benchmark exceedences.
• Section B — This part contains a new provision that four exceedences of any benchmark will trigger
increased DWQ involvement in the permittee's stormwater management and control actions. DWQ may
direct the permittee to apply for an individual permit, institute specific monitoring, or may direct the
implementation or installation of specific stormwater control measures.
• Section B — The definition of "Representative Storm Event" (RSE) now allows 48 hours (instead of 72
hours) of little or no precipitation to precede an RSE.
• Section B — Stormwater discharges from a basin designed to contain the 10-year storm must now be
monitored.
• Sections B & C — Failure to monitor according to permit terms triggers monthly monitoring for the
remainder of the permit.
• Section C — Analytical monitoring for Total Petroleum Hydrocarbons (TPH) has replaced the Oil & Grease
parameter in the previous permit.
• Section D — Qualitative monitoring must now be conducted during the same representative storm event
.as the analytical monitoring.
• Section D — The permittee is required to keep a written record of his response to problems identified by
his qualitative monitoring observations..
• Section D — If the permittee fails to respond effectively to problems identified by qualitative monitoring, the
permittee maybe required by DWQ to perform corrective action.
e Section D — Qualitative ROS: Representative Outfali Status may be granted for qualitative monitoring for
some Stormwater Discharge Ouffalls (SDOs).
• Section D — If mines do not respond to problems seen in visual monitoring, DWQ may now require that
mines change the monitoring frequency, apply for an individual permit, implement in -stream monitoring,
install or modify structural stormwater controls, or implement other controls.
• Sections B, C, & D — Inability to sample due to adverse weather must be reported in the SPPP and
recorded in the Annual Summary DMR.
• Section E — A lower TSS Wastewater limit for PNA waters is included in the permit-
• Section E — All mining operations are now required to monitor TSS in wastewater effluent discharges (not
only industrial sand mines). However, TSS limits only apply to industrial sand mining operations.
• Section E — Turbidity limits on effluent discharges have been removed; however, turbidity standards still
apply in the receiving waters.
• Section E — Approval of a Pumping O&M Plan may be required prior to coverage (for sites with
dewatering activities that have the potential to drain wetlands or other surface waters).
• Section E — ATC Requirements have been changed for clarity_ These requirements are now outlined for
Mine Dewatering Wastewater, Process Wastewater, Overflow From Non -Closed -Loop Process Recycle
Wastewater Systems, and Overflow From A Closed -Loop Process Recycle (CLPR).
• Section E— Monitoring for Fecal coliforms in discharges to SA waters has been clarified. Fecal coliform
monitoring is now required for all process and mine dewatering wastewater discharges to SA waters.
• Part IV:
• Section E — Items 1. and 2. require submittal of a new reporting form: the Annual Summary DMR. This
annual summary of the analytica! monitoring results should be submitted to the DWO Central Office by
March 1 of each year.
• Section E -- Exceedences and violations must be sent to the appropriate DWQ Regional Office within 30
days of receipt from the lab.
• Section E — Results of "No Flow" or "No Discharge" must be recorded within 30 days from the sampling
period in the SPPP. "No flow" or "No Discharge" must also be reported on the Annual Summary DMR
form.

Permit Reissuance — Permit Number NCG020354
February 11, 2010
Page 3
Your coverage under the General Permit is transferable only through the specific action of DWQ.
This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor
does it relieve the permittee from responsibility for compliance with any other applicable federal, state, or local
law, rule, standard, ordinance, order, judgment, or decree.
If you have any questions regarding this permit package please contact these members of the Stormwater
Permitting Unit: Jennifer Jones at [phone] or Bethany Georgoulias at [phone].
Sincerely,
for Coleen H. Sullins
cc: DWQ Central Files
Stormwater Permitting Unit Files
Raleigh Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCG020354
STORMWATER, MINE DEWATERING WATER AND/OR PROCESS WASTEWATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
General Shale Brick, Inc.
is hereby authorized to operate approved wastewater treatment system(s) and discharge stormwater
and/or wastewater, as approved in the original permit/application or subsequent permit modification,
from a facility located at:
General Shale Brick, Inc.
Flatwoods Rd
Moncure
Chatham County
to receiving waters designated as a UT of Gulf Creek, a class WS-IV waterbody in the Cape Fear River
Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth
in Parts I, 11, 111, IV, V, and VI of General Permit No. NCG020000 as attached.
This certificate of coverage shall become effective February 11, 2010.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 111h day of February, 2010.
for Coleen H. Sullins, Director
Division of Water Quality
By Authority of the Environmental Management Commission

STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND
NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG020000
TO DISCHARGE STORMWATER, MINE DEWATERING, AND PROCESS WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission and the Federal Water Pollution Control Act, as amended, this permit is
hereby issued to all owners or operators, hereafter permittees, which are covered by this permit as
evidenced by receipt of a Certificate of Coverage by the Environmental Management Commission to
allow the discharge of stormwater, mine dewatering wastewater, and process wastewater to
the surface waters of North Carolina or to a separate storm sewer system conveying discharges
to surface waters, from active and inactive mining sites, in accordance with the terms and
conditions set forth herein.
Coverage under this General Permit is applicable to:
♦ Stormwater point source discharges associated with mining and quarrying of non-
metallic minerals (except fuels), mine excavation, processing, and vehicle maintenance;
♦ Mine dewatering wastewater discharges;
♦ Wastewater discharges from sand and/or gravel operations;
♦ Operation of non -discharging closed -loop recycle systems (and infrequent overflows);
♦ Process wastewater discharges from non -closed -loop recycle systems.
The following activities and associated discharges are excluded from coverage under this permit:
♦ Borrow Pits covered by the DOT statewide stormwater permit,
♦ Peat Mining,
♦ Coal Mining,
♦ Metal Mining,
♦ Oil and Gas Extraction Operations, and
♦ Combined Mining/Asphalt Operations (where asphalt operation is not covered by a separate
permit).
The Generai Permit shall become effective on January 1, 2010.
The General Permit shall expire at midnight on December 31, 2014.
Signed this day December 29, 2009.
Original Signed by Chuck Wakild
for Coleen H. Sullins, Director
Division of Water Quality
By the Authority of the Environmental Management Commission

Permit No. NCG020000
TABLE OF CONTENTS
PART I INTRODUCTION
Section A: General Permit Coverage
Section B: Permitted Activities
PART II AUTHORIZATION TO CONSTRUCT AND OPERATE A TREATMENT FACILITY
Section A: Requirements to Construct New or Expanded Treatment Facilities
Section B: Requirements For Operation of a Treatment Facility
PART 11] MONITORING, CONTROLS AND LIMITATIONS FOR PERMITTED DISCHARGES
Section A: Stormwater Pollution Prevention Plan (SPPP)
Section B: Stormwater Discharges: Analytical Monitoring Requirements
Section C: Stormwater Discharges: On -Site Vehicle Maintenance
Section D: Stormwater Discharges: Qualitative Monitoring Requirements
Section E: Wastewater Discharges: Effluent Limitations and Monitoring Requirements for Mine
Dewatering Wastewater and Process Wastewater
PART IV STANDARD CONDITIONS
Section A: Compliance and Liability
1.
Compliance Schedule
2.
Duty to Comply
3.
Duty to Mitigate
4.
Civil and Criminal Liability
5.
Oil and Hazardous Substance Liability
6.
Property Rights
7.
Severability
8.
Duty to Provide Information
9.
Penalties for Tampering
10.
Penalties for Falsification of Reports
Section B: General Conditions
1. General Permit Expiration
2. Transfers
3. When an Individual Permit May be Required
4. When an Individual Permit Maybe Requested
i

i; I� ii i i 7 �► [.>! ► [KK1y�lIlI1Ir I]
S. Signatory Requirements
6. General Permit Modification, Revocation and Reissuance, or
Termination
7. Certificate of Coverage Actions
Section C: Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Hait or Reduce not a Defense
3. Bypassing of Wastewater or Stormwater Control Facilities
Section D: Monitoring and Records
1.
Representative Sampling
2.
Recording Results
3.
Flow Measurements
4.
Test Procedures
5.
Non-Stormwater Discharges
6.
Representative Outfall
7.
Records Retention
8.
Inspection and Entry
Section E: Reporting
Requirements
1.
Discharge Monitoring Reports
2.
Submitting Reports
3.
Availability of Reports
4.
Non-Stormwater Discharges
5.
Planned Changes
6.
Anticipated Noncompliance
7.
Bypass
8.
Twenty-four Hour Reporting
9.
Other Noncompliance
10.
Other Information
PART V LIMITATIONS REOPENER
PART V1 ADMINISTERING AND COMPLIANCE MONITORING FEE REQUIREMENTS
it

Permit No. NCG020000
PART I — INTRODUCTION
SECTION A: GENERAL PERMIT COVERAGE
All persons desiring to have facilities covered by this General Permit must register with the Division
of Water Quality (DWQ) by the filing of a Notice of Intent (NOI) and applicable fees. The NOI shall be
submitted and a certificate of coverage issued prior to any discharge of stormwater associated with
industrial activity, mine dewatering wastewater, or process wastewater that has a point source
discharge to the surface waters of the state.
This General Permit covers mining and quarrying of nonmetallic minerals (except fuels) including
borrow pits (that would not be covered under the statewide DOT stormwater permit) and active or
inactive mines that discharge stormwater contaminated with, or that has come in contact with,
any overburden, raw material, intermediate products, finished products, byproducts or waste
products located at the site of such operations and stormwater runoff from vehicle maintenance
areas. This General Permit also covers discharge of wastewater from processing mined materials
and mine dewatering wastewater from the groundwater and/or stormwater that accumulates in
the mine pit.
Any owner or operator not wishing to be covered or limited by this General Permit may make
application for an individual NPDES permit in accordance with NPDES procedures in 15A NCAC 2H
.0100, stating the reasons supporting the request. Any application for an individual permit should
be made at least 180 days prior to commencement of discharge.
This General Permit does not cover activities or discharges covered by an individual NPDES permit
until the individual permit has expired or has been revoked. Any person conducting an activity
covered by an individual permit but which could be covered by this General Permit may request
that the individual permit be revoked and coverage under this General Permit be provided.
Any facility may apply for new or continued coverage under this permit until a Total Maximum
Daily Load (TMDL) for pollutants for stormwater or wastewater discharges is established. A TMDL
sets a pollutant -loading limit that affects a watershed, or portion of a watershed, draining to an
impaired water. For discharges to watersheds affected by a TMDL, coverage under this
permit may depend on the facility demonstrating it does not have reasonable potential to
violate applicable water quality standards for those pollutants as a result of discharges. If
the Division determines that discharges have reasonable potential to cause water quality standard
violations, the facility shall apply for an individual permit 180 days prior to the expiration date of
this general permit. Once that individual permit is effective, the facility will no longer have
coverage under this general permit. [Note the permittee must identify impaired waters (scheduled
for TMDL development) and waters already subject to a TMDL in the Site Plan, as outlined in the
Stormwater Pollution Prevention Plan (SPPP), Part III, Section A.
Parts 1-II Page 1 of

Permit No. NCG020000
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge
stormwater, mine dewatering, and/or process wastewater to the surface waters of North Carolina
or a separate storm sewer system which has been adequately treated and managed in accordance
with the terms and conditions of this General Permit. Types of approved discharges are
dependent upon approval and are detailed in the permittee's individual Certificate of
Coverage (COC). All discharges shall be in accordance with the conditions of this permit
Any other point source discharge to surface waters of the state is prohibited unless it is an
allowable non-stormwater discharge or is covered by another permit, authorization, or approval. If
mining activities will expand or change such that the types of discharges are affected, the permittee
is to contact DWQ to determine if modifications to the COC are necessary first. The permittee is also
responsible for contacting the Division of Land Resources (DLR) if modifications to the Mining
Permit are necessary, as compliance with the Mining Permit is a stipulation of this permit.
The discharges allowed by this General Permit shall not cause or contribute to violations of
Water Quality Standards. Discharges allowed by this permit must meet applicable wetland
standards as outlined in 15A NCAC 2B .0230 and .0231 and water quality certification requirements
as outlined in 15A NCAC 2}f .0500. This permit does not relieve the permittee's responsibility for
compliance with any other applicable federal, state or local law, rule, standard, ordinance, order or
decree.
PART II — AUTHORIZATION TO CONSTRUCT AND OPERATE A TREATMENT FACILITY
Mining operations involving construction and operation of wastewater treatment facilities for
mine dewatering or process wastewater (such as saw water, wash water, etc,) are subject to
construction and operation requirements for treatment facilities as outlined in Sections A and B
below.
SECTION A: REQUIREMENTS FOR CONSTRUCTING NEW OR EXPANDING
WASTEWATER TREATMENT FACILITIES
All new or expanding wastewater treatment facilities must receive an Authorization to
Construct (AtC) from DWQ, unless specificully excluded in Part III, Section E in this permit.
Treatment facility arrangements excluded from the AtC requirement are as follows:
♦ Dewatering wastewater directly pumped from the pit through erosion and
sedimentation control facilities and that does not require additional treatment other
than those structures to meet effluent limits prior to discharge.
♦ Water conveyed from mined sand and/or gravel through erosion and
sedimentation control facilities and that does not require additional treatment other
than those structures to meet effluent limits prior to discharge.
♦ Closed -loop process recycle wastewater systems that are designed to operate with
a minimum of two feet (2') of freeboard and that limit the water entering the system to
makeup water and/or precipitation that falls directly into the system (i.e., exclude
stormwater runoff from draining into the system).
e Facilities designed to administer polyacrylamides (DAMS) or other chemical
flocculant materials, as long as administered in accordance with Division requirements
and that do not require additional treatment other than those structures to meet
effluent limits prior to discharge.
Parts I -II Page 2 of 4

Permit No. NCG020000
Treatment facility arrangements that are subject to AtC requirement include, but are
not limited to:
♦ Dewatering wastewater treatment facilities for discharges that do not meet effluent
limits and do not protect water quality standards.
♦ Process recycle wastewater systems that are not designed to operate with a
minimum of two feet (2') of freeboard and/or do not otherwise meet criteria to be
considered closed -loop recycle system (i.e„ Non -closed -loop recycle systems).
2. Application for the AtC requires that plans and specifications be submitted to the Division of
Water Quality, Stormwater Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-
1617 for approval.
3. Upon approval of the plans and specifications by the Division, a set of approved plans and
specifications for the subject project will be returned to the permittee. These plans must be
retained by the permittee for the life of the treatment facility.
4. Upon receipt of an approved AtC, approved treatment facilities shall be constructed and
implemented in accordance with the conditions of this permit, approved plans and
specifications, and other supporting data. Treatment facilities shall be constructed to meet
the effluent limitations in Part 111, Section E of this General Permit. All such inspections
must be documented with printed name, date, and signature of individual performing the
inspection(s).
Upon completion of construction and prior to operation of a permitted facility, a
certification of plans and specifications must be received from a professional engineer in
accordance with G.S. 89-25 certifying that the permitted facility has been installed in
accordance with this permit, the approved plans and specifications, and other supporting
materials. Mail the Certification of plans and specifications to the Division of Water Quality,
Stormwater Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
6. The permittee shall notify the DWQ Regional Office at least seventy-two (72) hours in
advance of operation of the installed facilities so that an in -place inspection can be made if
the Regional Office so desires. Such notification to the Regional Supervisor shall be made
during normal business hours from 8:00 a.m, until 5:00 p.m. on Monday through Friday,
excluding State Holidays.
Parts I-I1 Page 3 of 4

Permit No. NCGO20000
SECTION B: REQUIREMENTS FOR OPERATION OF A WASTEWATER TREATMENT
FACILITY
Existing, new and expanding wastewater treatment facilities shall be subject to the following
operational requirements.
Operation and maintenance of treatment facilities must be in accordance with the
requirements in this General Permit. For the purposes of this permit no documentation
other than a signed Certificate of Coverage is required to operate an existing treatment
facility. New treatment facilities must also have an Authorization to Construct (AtC) permit,
with the exceptions noted in Section A above.
2. Diversion or bypass of untreated wastewater from a treatment facility is prohibited except
under provisions of this permit in Part IV, Section C.3 and Part IV, Section E.7
In the event that a facility fails to perform satisfactorily, including the creation of nuisance
conditions, the permittee shall take immediate corrective action, including those actions
that may be required by this Division, such as the construction of additional or replacement
treatment or disposal facilities.
4. The issuance of this permit shall not relieve the permittee of the responsibility for damages
to surface waters of the State resulting from the operation of a treatment facility.
S. Any discharge from a treatment system to groundwater must protect the groundwater
standards specified in 15A NCAC 2L, Groundwater Classification and Standards.
Any groundwater quality monitoring, as deemed reasonably necessary by the Division, shall
be provided.
Flocculants evaluated by the Division may be used if administered in accordance with
maximum application doses and any other current requirements. No other chemical
flocculants shall be used in the treatment facility without written authorization from the
Division. Evaluated Polyacrylamide (PAMS) information can be found via the Stormwater
Permitting Unit website.
8. All discharges of mine dewatering wastewater and process wastewater will be monitored in
accordance with Part 111, Section E of this permit.
Parts I-11 Page 4 of 4

Permit No. NCG020000
PART III — MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
SECTION A: STORMWATER POLLUTION AND PREVENTION PLAN (SPPP)
All permittees shall develop and implement a Stormwater Pollution Prevention Plan (SPPP),
herein after referred to as the Plan. This Plan shall be considered public information in accordance
with Part IV, Standard Conditions, Section E, Paragraph 3 of this General Permit. The Plan shall
include, at a minimum, the following items:
1. Site Plan. The site plan shall provide a description of the physical facility and the potential
pollutant sources that may be expected to contribute to contamination of stormwater
discharges. The site plan shall contain the following:
(a) A general location map (USGS quadrangle map or appropriately drafted equivalent
map), showing the facility's location in relation to transportation routes and surface
waters, the name of the receivingwater(s) to which the stormwater outfall(s)
discharges, or if the discharge is to a municipal separate storm sewer system, the
name of the municipality and the ultimate receiving waters, and accurate latitude
and longitude of the point(s) of discharge. The general location map (or
alternatively the site map) shall identify whether each receiving water is impaired
(on the state's 303(d) list of impaired waters) or is located in a watershed for
which a TMDL has been established, and what the parameter(s) of concern are.
(b) A narrative description of storage practices, loading and unloading activities,
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices. A narrative description of the potential pollutants that
could be expected to be present in the stormwater discharge from each outfall.
(c) A site map drawn at a scale sufficient to clearly depict: the site property boundary,
the stormwater discharge outfalls, all on -site and adjacent surface waters and
wetlands, industrial activity areas (including storage of materials, disposal areas,
process areas, loading and unloading areas, and haul roads), site topography, all
drainage features and structures, drainage areas for each outfall, direction of flow in
each drainage area, industrial activities occurring in each drainage area, buildings,
existing BMPs (with design capacities), and permanent impervious surfaces, such as
roads or process areas that are unlikely to change frequently. The site map shall
include a distance legend. In addition, the following industrial activity areas must
also be identified on the site map: fueling, engine maintenance and repair, vessel
maintenance and repair, washing, painting, sanding, blasting, welding, and metal
fabrication.
(d) A list of significant spills or leaks of pollutants that have occurred during the
previous three (3) years and any corrective actions taken to mitigate spill impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part IV, Standard Conditions, Section B,
Paragraph S. The permittee shall re -certify annually that the stormwater
outfalls have been evaluated for the presence of non-stormwater discharges.
Part III Page 1 of 16 Pages

l�iii[i►G�►IKKIy�IIIIIIII
2. Erosion and Sedimentation Control. The permittee shall implement the management
practices and the erosion and sedimentation control measures that are included in the
mining permitor erosion and sedimentation control permit issued by the Division of Land
Resources (DLR). Compliance with the DLR issued permit is considered a requirement
of this general permit. Any deviation from the DLR issued permit, or amendments to the
issued permit, that impacts water quality shall constitute a violation of the terms and
conditions of this general permit. All erosion and sediment controls shall be inspected, and
a respective written record of repairs and maintenance shall be available to DWQ
inspectors. A signed copy of the issued permit including the approved erosion and
sedimentation control measures and the reclamation plan shall be maintained on the
site at all times. Once an area is released by the Division of Land Resources in accordance
with NC G.S. Chapter 74, Article 7, it shall no longer be subject to this general permit.
3. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed which control or
minimize the exposure of significant materials to stormwater, including structural and
nonstructural measures. The stormwater management plan, at a minimum, shall
incorporate the following:
(a) Management of Stormwater Runoff and Runon. The permittee shall maintain
stormwater BMPs for mine excavation and disturbance areas, process areas, and
any other areas associated with mining or vehicle maintenance activities. In
addition, controls should be used to limit or isolate selected land disturbance and
process areas and limit the amount of off site stormwater runon to those areas.
Appropriate Best Management Practices (BMPs) should be used to divert, infiltrate,
reuse or otherwise manage stormwater runoff and runon in a manner that reduces
pollutants in stormwater discharges leaving the site. Appropriate BMPs may
include but are not limited to: vegetative swales, berms, use of reclaimed mine
areas, and reuse of collected stormwater (such as for an industrial process or as an
irrigation source).
(b) BMP Controls Inspection and Maintenance. All stormwater controls shall be
inspected. All inspections are to be documented with a written record of repairs.
BMPs shall be inspected by or under the direction of the permittee at least once
every seven calendar days and within 24 hours after any storm event that results in
a discharge, unless the site is inactive.
Reduced Inspections for inactive mines: For inactive mines that have obtained an
"Inactive Renewal" Mining Permit from DLR, BMPs must be inspected at least
once every month, and within 24 hours of any storm event of 0.5 inches or more.
For mines where active mining has suspended temporarily, but the mine maintains
an active Mining Permit from DLR, the permittee must certify to DWQ that all
portions of the site where clearing, grading, and/or excavation activities have
temporarily ceased have been stabilized with vegetation, and may then conduct
BMP inspections within 24 hours of any storm event that results in a discharge (no
weekly minimum). The permittee must send certification to the DWQ Regional
Office of "inactive" status and may be subject to an inspection for verification. The
permittee must also notify the Regional Office upon resuming mining activities.
A rain gauge and monitoring records are to be kept on site. BMPs shall be operated
and maintained. BMPs must be cleaned out when sediment storage capacity is at
50% permitted volume. If visible sedimentation is leaving the property, corrective
Part III Page 2 of 16 Pages

Permit No. NCG020000
action shall be taken to reduce the discharge of sediments. Visible sedimentation
shall be recorded with a brief explanation of measures taken to prevent future
releases, as well as any measures taken to remove the sediment that has left the site.
Visible sedimentation records shall be kept onsite. All other stormwater specific
controls (e.g. oil/water separators) shall be inspected and qualitatively monitored
(as per Part Ill. D) on a semi-annual schedule. A log of all sampling data, including
activities taken to implement BMPs associated with vehicle maintenance activities,
shall be maintained and incorporated into the SPPP and kept onsite and available
for inspection purposes. These items shall be available for the duration of the
permit term and made available to the Director upon request. These data shall be
sent to the Regional Office upon request.
(c) Secondary Containment Requirements and Records. Secondary containment is
required for: bulk storage of liquid materials; storage in any amount of Section 313
of Title III of the Superfund Amendments and Reauthorization Act (SARA) water
priority chemicals; and storage in any amount of hazardous substances, in order to
prevent leaks and spills from contaminating stormwater runoff. A table or summary
of all such tanks and stored materials and their associated secondary containment
areas shall be maintained. If the secondary containment devices are connected to
stormwater conveyance systems, the connection shall be controlled by manually
activated valves or other similar devices (which shall be secured closed with a
locking mechanism), and any stormwater that accumulates in the containment area
shall be at a minimum visually observed for color, foam, outfall staining, visible
sheens and dry weather flow, prior to release of the accumulated stormwater.
Accumulated stormwater shall be released if found to be uncontaminated by any
material. Records documenting the individual making the observation, the
description of the accumulated stormwater, and the date and time of the release
shall be kept for a period of five (S) years.
4. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or the team) responsible for implementing the
SPRP shall be identified in a written list incorporated into the SPRP and signed and dated by
each individual acknowledging their responsibilities for the plan. A responsible person
shall be on -site at all times during facility operations that have the potential to contaminate
stormwater runoff through spills or exposure of materials associated with the facility
operations. The SPRP must be site stormwater specific. Therefore, an oil Spill Prevention
Control and Countermeasure plan (SPCC) may be a component of the SPRP, but may not he
sufficient to completely address the stormwater aspects of the SPRP. The common
elements of the SPCC with the SPRP may be incorporated by reference into the SPRP.
5. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance and good housekeeping program shall be developed and implemented. The
program shall ensure equipment used during mining activity on a site must be operated and
maintained to prevent potential pollution of the surface water or groundwaters of the state.
Fuels, lubricants, coolants, hydraulic fluids, or any other petroleum products shall not be
discharged on the ground or into surface waters. Spent lubricants and fuels shall be
disposed of properly and in accordance with applicable federal disposal regulations. Spilled
fluids shall be cleaned up to the maximum extent practicable and properly disposed of to
prevent entry to surface waters or groundwaters of the state. The program shall establish
schedules of inspections, maintenance, and housekeeping measures for vehicle
maintenance and industrial activity areas (including material storage and handling areas,
Part Ill Page 3 of 16 Pages

Permit No. NCG020000
disposal areas, process areas, loading and unloading areas, and haul roads), where not
already addressed under another element of this Plan. Schedules for inspections,
maintenance, and housekeeping, and documentation that these program elements are being
implemented, shall be recorded and maintained in the SPPP.
6. Employee Training. Training programs shall be developed and training provided at a
minimum on an annual basis for facility personnel with responsibilities for: spill response
and cleanup, preventative maintenance activities, and for any of the facility's operations
that have the potential to contaminate stormwater runoff. Facility personnel (or team)
responsible for implementing the training shall be identified, and their annual training shall
be documented by the signature of each employee trained. Additional required training
items include: used oil management, spent solvent management, disposal of spent
abrasives, disposal of vessel wastewaters, fueling procedures, sanding, painting and blasting
procedures, and used battery management.
7. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position assignments provided.
8. Plan Amendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance that has a significant effect on the potential
for the discharge of pollutants to surface waters. All aspects of the Stormwater Pollution
Prevention Plan shall be reviewed and updated on an annual basis. The annual update
shall include an updated list of significant spills or leaks of pollutants for the previous three
(3) years, or the notation that no spills have occurred. The annual update shall include
written re -certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. Each annual update shall include a documented re-evaluation
of the effectiveness of the BMPs listed in the BMP Summary of the Stormwater Management
Plan. The Director may notify the permittee when the Plan does not meet one or more of
the minimum requirements of the permit. Within 30 days of such notice, the permittee shall
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with Part
VI, Standard Conditions, Section B, Paragraph 5) to the Director that the changes have been
made.
Plan Implementation. The permittee shall implement the Plan and all appropriate BMPs
to ensure that contaminants do not enter surface waters via stormwater that comes in
contact with any unstabilized overburden, raw materials, intermediate products, finished
products, byproducts or waste products located on the site covered by this permit.
Implementation of the Plan shall include documentation of all monitoring, measurements,
inspections, maintenance activities, and training provided to employees, including the log of
the sampling data and of actions taken to implement BMPs associated with the industrial
activities, including vehicle maintenance activities. Such documentation shall be kept on -
site for a period of five years and made available to the Director or the Director's authorized
representative immediately upon request.
SECTION B: STORMWATER DISCHARGES: ANALYTICAL MONITORING REQUIREMENTS
Stormwater discharges are defined as stormwater from mining activity areas, including (but not
limited to) areas of mine excavation, other land disturbance, process areas, and vehicle
maintenance. This section does not apply to wastewater discharges from mine dewatering
Part III Page 4 of 16 Pages

Permit No. NCG020000
and process areas. Analytical monitoring for stormwater discharges shall be performed For
parameters as specified in Tables 1 through 3. All analytical monitoring shall be performed
during a representative storm event as defined below.
Monitoring Exemption
Analytical monitoring is not required for any basin or pond designed to contain the 25-year, 24-
hour storm (see Part VI1, Definitions) without discharging, and that can regain capacity to hold such
an event within five (5] days' time through means other than discharge to surface waters. A basin
or pond that meets this provision is considered a non -discharging stormwater control.
Table 1. Analytical Monitoring Requirements for Stormwater Discharges from Mining
Activities
Discharge
Characteristics
Units
Measurement
Fre uenc 1
Sample
Type2
Sample
Location3
Settleable Solids
MI/1
Semi-annual
Grab
SDO
Total Suspended Solids
m I
Semi-annual
Grab
SDO
Turbid4 4
NTU
Semi-annual
Grab
SDO, or U,D4
Total Rainfalls
inches
Semi-annual
--
--
Event Durations
minutes
Semi-annual
Estimate
--
Total Flow6
MG
Semi-annual
Estimate
SDO
Footnotes:
1. Measurement Frequency: Twice per year during a representative storm event, as defined for this permit.
Failure to comply with semi-annual monitoring in accordance with permit terms for any six-month
monitoring -period immediately triggers monthly monitoring for the remaining permit term.
2. Grab samples shall be collected within the first 30 minutes of discharge. For sites where multiple outfalls
are separated by distances that preclude collection within 30 minutes of each discharge event is not
feasible, begin collection procedures within 30 minutes and continue until all outfalls with discharges are
sampled. Documentation explaining why it was not possible to take samples within the first 30 minutes
must be kept in the SPPP.
3. Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless
representative outfall status (ROS) has been granted and documented by the Division of Water Quality. A
copy of the letter granting ROS shall be kept on site.
4. Turbidity may be monitored at the Stormwater Discharge Outfall. Alternatively, the permittee may
choose to monitor turbidity in the receiving water, directly upstream and downstream of the stormwater
discharge outfall(s).
S. For each sampled representative storm event the total precipitation must be recorded. An on -site rain
gauge or local rain gauge reading must be recorded.
6. Total flow shall be: (a) measured continuously, or (b) calculated based on the amount of area draining to
the outfall, the amount of impervious area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event. Total rainfall precipitation and
duration of the rainfall event refers to the representative storm event sampled.
All analytical monitoring shall be performed during a representative storm event at each
stormwater discharge outfall (SDO). The permit allows the permittee to monitor turbidity at the
SDO or up- and downstream of the SDO; however, the permittee should consider regular turbidity
sampling up- and downstream of the discharge(s) when feasible to ensure compliance with water
quality standards.
Part III Page 5 of 16 Pages

Permit No. NCG020000
A representative storm event for the purposes of this General Permit is a storm event that
measures greater than 0.1 inches of rainfall. The time between this storm event and the previous
storm event measuring greater than 0.1 inches must be at least 48 hours. One storm event may
have a time period within it that has no precipitation. This time period may last up to 10 hours. For
example, if it rains but stops before producing any collectable discharge, a sample may be collected if
the next rain producing a discharge begins within 10 hours.
The permittee shall complete the analytical samplings in accordance with the schedule specified in
Table 2. A minimum of 60 days must separate each sample event unless monthly monitoring
has been instituted under a Tier 2 response. Failure to comply with semi-annual monitoring in
accordance with permit terms for any six-month monitoring period immediately triggers monthly
monitoring for the remainingpermit termunless adverse weather conditions prevent sample
collection during the sample collection period. Inability to sample due to adverse weather
conditions must be documented in the SPPP with date, time and written narrative (see Adverse
Weather in Definitions) and reported on the Annual Summary DMR.
Table 2. Monitoring Schedule
Semi-annual
Monitoring Events1,2
Start Date
(All Years),,
End Date
(All Years) 3
1
January 1
June 30
2
July 1
December 31
Footnotes:
1. Maintain semi-annual monitoring during permit renewal process (unless tiers prompt monthly). If at the
expiration of the General Permit, the permittee has submitted an application for renewal of coverage
before the submittal deadline, the permittee will be considered for renewed coverage. The applicant
must continue monitoring until the renewed Certificate of Coverage is issued.
2. If no discharge occurs during the sampling period, the permittee must record "No Flow" or "No
Discharge" within 30 days of the end of the six-month sampling period in the SPPP. "No Flow" or "No
Discharge" shall be reported on the Annual Summary Discharge Monitoring Reports (DMR). This DMR is
to be submitted to the Division's Central Office by March 1 of each year.
3. Monitoring periods remain constant throughout the five-year permit term (from January 1, 2010 to
December 31, 201.4).
In all cases, the permittee shall report (as required in Part IV, Section E.) the analytical results fi•om
each sample within the monitoring period. The permittee shall compare those results to the
benchmark values in Table 3. Exceedences of benchmark values require the permittee to increase
monitoring, increase management actions, increase record keeping, send the monthly monitoring
results to the appropriate Regional Office, and/or install stormwater Best Management Practices
(BMPs) in a tiered program. See below the descriptions of tiered response actions.
Table 3. Benchmark Values for Stormwater Discharges
Discharge Characteristics
Benchmark Values
Settleable Solids
0.1 ml
Total Suspended Solids (TSS)
100 1-nall
TSS ORW, H W, trout, and PNA waters
50 mg/1
Turbidity
N/A See below
Part III Page 6 of 16 Pages

Permit No. NC6020000
The discharge shall not cause the turbidity of the receiving water to exceed Water Quality
Standards:
10 NTU freshwater streams, lakes, and reservoirs designated as trout waters
25 NTU all lakes and reservoirs, and all salt waters
50 NTU all other streams and surface waters
If turbidity of the receiving stream exceeds these levels due to natural background conditions, the
existing turbidity level shall not be increased. If the turbidity exceeds these levels as a result of
stormwater discharges, the permittee must immediately institute Tier 2 response actions,
including monthly monitoring of all stormwater discharge outfalls to the receiving waters. The
permit allows the permittee to monitor turbidity in the effluent or up- and downstream of the
discharge point; however, the permittee should consider regular turbidity sampling up- and
downstream of the discharge(s) when feasible to ensure compliance with water quality standards.
Tier One
If: The first valid sampling results are above a benchmark value, or outside of the benchmark
range, for any parameter at any outfall;
Then: The permittee shall
1. Conduct a stormwater management inspection of the facility within two weeks of
receiving sampling results.
2. Identify and evaluate possible causes of the benchmark value exceedence.
3. Identify potential and select the specific: source controls, operational controls, or
physical improvements to reduce concentrations of the parameters of concern, or to
bring concentrations within the benchmark range.
4. Implement the selected actions within two months of the inspection.
5. Record each instance of a Tier One response in the stormwater Pollution Prevention
Plan. Include the date and value of the benchmark exceedence, the inspection date, the
personnel conducting the inspection, the selected actions, and the date the selected
actions were implemented.
6. Send all monitoring results for that sample period to the appropriate DWQ Regional
Office.
Part III Page 7 of 16 Pages

Permit No. NCG020000
Tier Two
If: During the term of this permit, the first valid sampling results from two (2) consecutive
monitoring periods are above the benchmark values, or outside of the benchmark range, for
any specific parameter at a specific discharge outfall;
Then: The permittee shall
1. Repeat all the required actions outlined above in Tier One.
2. Immediately institute monthly monitoring for all parameters at every outfall where a
sampling result exceeded the benchmark value for two (2) consecutive samples.
Monthly (analytical and qualitative) monitoring shall continue until three (3)
consecutive samples are below the benchmark values or within the benchmark range.
3. Send all monthly monitoring to the appropriate DWQ Regional Office.
4. If no discharge occurs during the sampling period, the permittee is required to record
"No Flow" or "No Discharge" in the SPPP for the sampling the period to comply with
monthly monitoring requirements and mustsubmit reports in accordance with this
permit.
5. Maintain a record of Tier Two responses in the Stormwater Pollution Prevention Plan,
Tier Three
During the term of this permit, if the valid sampling results required for the permit monitoring
periods exceed the benchmark value, or are outside the benchmark range, for any specific
parameter at any specific outfall on four (4) occasions, the permittee shall notify the DWQ
Regional Office Supervisor in writing within 30 days of receipt of the fourth analytical
results. DWQ may but is not limited to:
• Require that the permittee revise, increase, or decrease the monitoring frequency for the
remainder of the permit;
• Rescind coverage under the General Permit, and require that the permittee to apply for
an individual stormwater discharge permit;
• Require the permittee to implement in -stream Turbidity Monitoring (U,D)
• Require the permittee to install or modify structural stormwater controls; or
• Require the permittee to implement other stormwater control measures
SECTION C: ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
(STORMWATER DISCHARGES)
Facilities which have any on -site vehicle maintenance activity that uses more than 55 gallons of
new motor oil per month when averaged over the calendar year shall perform analytical
monitoring as specified below in Table 4. This monitoring shall be performed at all outfalIs
discharging stormwater runoff from vehicle maintenance areas, and in accordance with the
Part III Page 8 of 16 Pages

Permit No. NCGO20000
schedule presented in below. All analytical monitoring shall be performed during a representative
storm event as defined for this General Permit, unless adverse weather conditions prevent sample
collection during the sample collection period. Inability to sample due to adverse weather
conditions must be documented in the SPPP with date, time and written narrative (see Adverse
Weather in Definitions) and reported on the Annual Summary DMR.
Table 4. Analytical MonitoringRe uirements from On -Site Vehicle Maintenance Areas
Discharge Characteristics
Units
Measurement
Fre uenc 1
Sample
Type2
Sample
Location3
H
standard
Semi-annual
Grab
SDO
Total Petroleum Hydrocarbons (TPH)
EPA Method 1664 SGT-HEM .
mg/I
Semi-annual
Grab
SDO
Total Suspended Solids (TSS)
m I
Semi-annual
Grab
SDO
Total Rainfall4
inches
Semi-annual
Grab
--
Event Duration4
minutes
Semi-annual
Estimate
--
Total Flows
MG
Semi-annual
Estimate
SDO
New Motor Oil Usage
gallons month
Semi-annual
Estimate
--
Footnotes:
1. Measurement Frequency: Twice per year during a representative storm event (See Table 2). A
minimum of 60 days must separate each event. Failure to comply with semi-annual monitoring in
accordance with permit terms for any six-month monitoring period immediately triggers monthly
Monitoring for the remaining_pgrmit term.
2. Grab samples shall be collected within the first 30 minutes of discharge.
3. Sample location: Samples shall be collected at each stormwater discharge outfall (SDO) that
discharges stormwater runoff from area(s) where vehicle maintenance activities occur.
4. For each sampled representative storm event the total precipitation must be recorded. An on -site or
local rain gauge reading must be recorded.
5. Total flow shall be: (a) measured continuously, or (b) calculated based on the amount of area
draining to the outfall, the amount of impervious area, and the total amount of rainfall, or (c)
estimated by the measurement of flow at 20 minute intervals during the rainfall event. Total rainfall
precipitation and duration of the rainfall event refers to the representative storm event sampled.
In all cases, the permittee shall report (as required in Part IV, Section E.) the analytical results from
each sample within the monitoring period. The permittee shall compare those results to the
benchmark values in Table 5. Exceedences of benchmark values require the permittee to increase
monitoring, increase management actions, increase record keeping, send the monthly monitoring
results to the appropriate Regional Office, and/or install stormwater Best Management Practices
(BMPs) in a tiered program. The permittee shall comply with the required tiered response actions
identified above.
Table 5. Benchmark Values for On -Site Vehicle Maintenance Activities
Discharge Characteristics
Benchmark Values
H
within range the 6.0 — 9.0
Total Petroleum Hydrocarbons (TPH)
15 m l
Total Suspended Solids (TSS)
100 m l
TS5 ORW, H W, trout, and PNA waters
50 m l
Part III Page 9 of 16 Pages

Permit No. NCG020000
SECTION D: QUALITATIVE MONITORING REQUIREMENTS (STORMWATER
DISCHARGES)
Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified below in Table 6. Qualitative
monitoring is for the purpose of evaluating the effectiveness of the Stormwater Pollution
Prevention Plan (SPPP) and assessing new sources of stormwater pollution.
Qualitative monitoring of stormwater outfalls must be performed during a representative storm
event as defined for this General Permit, unless adverse weather conditions prevent sample
collection during the sample collection period. Inability to sample due to adverse weather
conditions must be documented in the SPPP with date, time and written narrative (see Adverse
Weather in Definitions). Qualitative monitoring will be performed twice per year, in accordance
with the schedule in Table 2. A minimum of 60 days must separate monitoring dates.
Table 6. Qualitative Monitoring Requirements
Discharge Characteristics
Frequency2
torin
ninit min g
MoLoonl-
Color
Semi-annual
SDO
Odor
Semi-annual
SDO
Clarity
Seri -annual
SDO
Floating Solids
Semi-annual
SDO
Suspended Solids
Semi-annual
SDO
Foam
Semi-annual
SDO
Oil Sheen
Semi-annual
SDO
Deposition at or immediately below the outfall
Semi-annual
SDO
Erosion at or immediately below the outfall
Semi-annual
SDO
Other obvious indicators of stormwater pollution
Semi-annual
SDO
Footnotes:
1. Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall
(00) regardless of representative outfall status (ROS), unless ROS is granted specifically for
qualitative monitoring. A copy of any letter granting ROS shall be kept on site.
2. For any outfalls represented by SDOs with representative status for qualitative monitoring,
qualitative monitoring is only required annually instead of semi-annually.
Representative outfall status (ROS) specifically for qualitative monitoring may be granted for some
stormwater outfalls and must be documented by the Division of Water Quality. Qualitative
monitoring for all outfalls represented must still be performed annually at a minimum.
Qualitative monitoring records shall not be turned into the Division except when requested.
Qualitative monitoring records shall be maintained on site as part of the SPPP.
Part Ill Page 10 of 16 Pages

Permit No. NCG020000
Qualitative monitoring is for the purposes of evaluating the effectiveness of the Stormwater
Pollution Prevention Plan (SPPP), assessing new sources of stormwater pollution, and prompting
the permittee's response actions to pollution. If the permittee repeatedly fails to respond
effectively to correct problems identified by qualitative monitoring, or if the discharge causes or
contributes to a water quality standard violation, DWQ may but is not limited to:
• Require that the permittee revise, increase, or decrease the monitoring frequency for the
remainder of the permit;
• Rescind coverage under the General Permit, and require that the permittee to apply for an
individual stormwater discharge permit;
• Require the permittee to implement in -stream Turbidity Monitoring (U,D)
• Require the permittee to install or modify structural stormwater controls; or
• Require the permittee to implement other stormwater control measures
SECTION E: WASTEWATER DISCHARGES: EFFLUENT LIMITATIONS AND MONITORING
REQUIREMENTS FOR MINE DEWATERING WASTEWATER & PROCESS
WASTEWATER
1. MINE DEWATERING WASTEWATER
Mine dewatering requirements apply to all mines that dewater from pits including quarries, clay
brick, sand & gravel, borrow pits, and refractory mining, as well as mines with similar discharges.
Note that for Construction Sand and Gravel or Industrial Sand mines, "mine dewatering"
wastewater includes wet pit overflows caused solely by direct rainfall and groundwater seepage.
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge mine dewatering wastewater controlled in accordance with
the conditions of this permit. Mine dewatering activities that have the potential to drain wetlands
or other surface waters must have secured and implemented a Pumping Operation and
Monitoring (0&M) Plan approved by the Division. Pumping 0&M Plans shall include, but are not
limited to:
• Groundwater monitoring strategies to demonstrate the effect of pumping.
• Detailed plans to maintain the surrounding hydrology that protects the affected streams and
wetlands and the respective monitoring to demonstrate compliance.
• The pumping regime deemed necessary to protect affected streams and wetlands.
Alternative site specific pumping and monitoring regimes may be approved by the Division on a
case -by -case basis. At the Division's discretion, approval of the Pumping O&M Plan may be
required prior to coverage under this general permit.
Analytical monitoring of mine dewatering wastewater shall be performed as specified below in
Table 7. For each parameter, an effluent limitation is contained in Table 8. An exceedence of any
of these limitations is a violation of the permit conditions and may be subject to enforcement action
as specified in Part IV, Section A.2 of this permit.
Part Ili Page 11 of 16 Pages

Permit No. NCG020000
Mine Dewatering Treatment System ATC Requirement:
Engineered erosion and sedimentation control (E&SC) structures that sufficiently treat mine
dewatering wastewater so that permit effluent limits are met and water quality is protected, do not
require an Authorization to Construct (AtC) and may operate in accordance with Part 11, Sections A
and B. Any additional treatment devices (other than erosion and sediment control
structures) needed to meet permit limits and conditions are subject to Authorization to
Construct (AtC) requirements.
2. PROCESS WASTEWATER
Process wastewater includes, but may not be limited to, the water involved in the slurry transport,
washing, sawing of mined material, air emissions control or processing exclusive of mining of sand,
gravel and stone washing operations, dimension stone cutting operations, and air scrubbing and
dust control operations.
A) Overflow From Non -Closed Loop Recycle Systems
A "closed -loop" system is a wastewater recycle system where the only other water that may be
added is either make-up water or precipitation that fails directly into the system. "Closed -loop"
systems must operate at or below two feet of freeboard and must be designed to exclude
stormwater runoff from draining into it. Nan -closed -loop recycle systems may recycle water,
but do not meet the above design criteria.
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge overflow from the process recycle wastewater systems that are
not designed as closed -loop recycle systems.
Analytical monitoring of overflow from process recycle wastewater systems that are not designed as
closed -loop recycle systems shall be performed as specified below in Table 7. For each parameter,
an effluent limitation is contained in Table 8. For the purposes of this permit, overflow refers to a
discharge of process wastewater as a result of a precipitation event.
Non -Closed -Loop Recycle System ATC Requirement:
Non -closed loop recycle systems do not meet the requirements for closed -loop recycle systems and
are not designed and operated with two feet of freeboard. Authorization to construct and operate
requirements (Part 11, Sections A and B) are applicable to non -closed -loop recycle systems.
B) Other Treated Process Wastewater Discharges
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge treated process wastewater from mining operations.
Treatment may involve conveyance through erosion and sedimentation control (E&SC) structures
and/or other engineered treatment systems.
Analytical monitoring of process wastewater shall be performed as specified below in Table 7. For
each parameter, an effluent limitation is contained in Table 8. An exceedence of any of these
limitations will result in a violation of the permit conditions and may be subject to enforcement
action as specified in Part IV, Section A.2 of this permit.
Part III Page 12 of 16 Pages

Permit No. NCGO2000O
Process Wastewater Treatment System ATC Requirement:
Engineered Erosion and Sedimentation control (E&SC) structures that sufficiently treat process
wastewater so that permit effluent limits are met and water quality is protected, do not require an
authorization to construct (AtC) and may operate in accordance with Part 11, Sections A and B.
Any additional treatment devices (other than erosion and sediment control structures)
needed to meet permit limits and conditions are subject to Authorization to Construct (AtC)
requirements.
Table 7. Monitoring Requirements for Wastewater Discharges in Section D -1., 2., and 3.
Discharge
Characteristics
Units
Measurement
Fre uenc 1
Sample
T e2
Sample
Location3
Type
H2
Standard
Quarterly
Grab
E
All
Settleable Solids2
m] 1
Quarterly
Grab
E
All
Total Suspended Solids2 4
mg/l
Quarterly
Grab
E
All
Turbidity2
NTU
Quarterly
Grab
E or U,D
All
Fecal Coliform2 5
co] ml
I Quarterly
Grab
I E
I All to SA waters
Total Flow6
MG
Quarterly
-
E
All
Footnotes:
1. The monitoring frequency is quarterly (see Table 4) unless the effluent limitation in Table 8 is exceeded,
at which time monthly monitoring will be required for that parameter for the remaining permit term.
Failure to comply with quarteriy monitoring in accordance -with -permit terms for any one calendar
quarter immediately triggers monthly monitoring for all parameters for the remaining permit term.
2. A grab sample is not required for pH, settleable solids, TSS, turbidity, or fecal coliform from a
basin/pond designed to contain or treat mine dewatering wastewater and that results from rainfall in
excess of 10-yr, 24-hr storm (except this exemption is not available for mine dewatering of clay pits).
3. Sample Location: E - Effluent, or combined (U - Upstream, D - Downstream)
4. All facilities that are mining Industrial Sand are required to monitor TSS and are subject to the TSS
limits in Table 8. All other types of mines covered by this permit are also required to monitor TSS, but
are not subject to the limits in Table 8.
S. Only facilities discharging to waters classified as SA waters are required to monitor for this parameter
6. Total Flow volume shall be recorded by a continuous flow measurement instrument. Alternatively, pump
curves and pump logs may be used as a means to calculate flow volume.
Part III Page 13 of 16 Pages

l; �"? [7 � [il! r, [KK1y.IlI1I1I17
Table 8. EFFLUENT LIMITATIONS FOR PROCESS WASTEWATER AND MINE DEWATERING
WASTEWATER
Discharge Characteristics
Effluent Limitations
Monthl Avera a
Dail Maximum .
Settleable Solids
0.1 ml I
0.2 ml
Total Suspended Solidsl
25 m 1
45 m 1
Total Suspended Solidsl HQW
20 m 1
45 mg/1
Total Suspended Solidsl Trout waters & PNA waters
10 mg/1
45 m 1
H Ran e2 freshwaters
--------
6.0 - 9.0
H Ran e2 saltwaters
--------
6.8 - 8.5
Turbidit 3
--------
--------
Total Volume of Wastewater Discharged (HQW)4
--------
50% of 7Q10 flow4
Footnotes:
1.. Applicable to Industrial Sand mining. Monthly Average Limit for discharges to waters designated as HQW
waters is 20 mg/l and 10 mg/l for trout waters and Primary Nursery Areas (PNAs)
2. Designated swamp waters can have a pH as low as 4.3 if due to natural conditions.
3. No limit in the effluent discharge applies, but turbidity in the receiving.waters shall not exceed levels
described below as a result of wastewater discharges.
4. The total volume of treated wastewater for all discharges combined shall not exceed 50 percent of the
total in -stream flow of the receiving waters under 7Q10 conditions in HQW waters, including trout and
PNA waters.
The discharge shall not cause the turbidity of the receiving water to exceed Water Quality
Standards:
10 NTU freshwater streams, lakes, and reservoirs designated as trout waters
25 NTU all lakes and reservoirs, and all salt waters
50 NTU all other streams and surface waters
If turbidity of the receiving stream exceeds these levels due to natural background conditions, the
existing turbidity level shall not be increased. If the turbidity exceeds these levels as a result of
wastewater discharges, the permittee must immediately institute monthly monitoring for all
parameters. The permit allows the permittee to monitor turbidity in the effluent or up- and
downstream of the discharge point; however, the permittee should consider regular turbidity
sampling up- and downstream of the discharge(s) when feasible to ensure compliance with water
quality standards.
The permittee shall complete the analytical samplings of wastewater discharges in accordance with
the schedule specified in Table 9. Failure tocomply _with quarterly monitoring in accordance with
permit terms for any one calendar- quarter- immediately triggers monthly monitoring for all
parameters for the remaining permit term.
Part III Page 14 of 16 Pages

�iiil<7►[i�►LKKiy.IlIlIlI1]
Table 9. Monitoring Schedule
Quarterly
Monitoring Eventsl•z
Start Date
(All Years)I
End Date
(All Years) 3
1
January 1
March 31
2
Aril 1
June 30
3
July 1
September 30
4
October 1
December 31
Footnotes:
1. Maintain quarterly monitoring during permit renewal process (unless an exceedence or failure to
monitor prompts monthly monitoring). If at the expiration of the General Permit, the permittee has
submitted an application for renewal of coverage before the submittal deadline, the permittee will be
considered for renewed coverage. The applicant must continue monitoring until the renewed Certificate
of Coverage is issued.
2. If no discharge occurs during the sampling period, the permittee must record "No Flow" or "No
Discharge" within 30 days of the end of the three-month sampling period in their SPPP. No Flow" or "No
Discharge" shall be reported on the Annual Summary Discharge Monitoring Reports (DMR). This DMR is
to be submitted to the Division's Central Office by March 1 of each year.
3. Monitoring periods remain constant throughout the five-year permit term (from January 1, 2010 to
December 31, 2014).
3. OVERFLOW FROM A CLOSED -LOOP PROCESS RECYCLE CLPR WASTEWATER SYSTEM
DESIGNED TO OPERATE WITH MINIMUM OF TWO _FEET (2') OF FREEBOARD
A "closed -loop" system is a system where the only water that can be added must be either make-
up water or precipitation that falls directly into the system. The system must operate at or below
two feet of freeboard. The system must be designed to exclude stormwater runoff from draining
into it.
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge overflow from closed -loop process wastewater recycle
systems designed and operated with two feet of freeboard during normal operation. For the
purposes of this permit, overflow refers to a discharge that occurs as a result of a precipitation
event that over -tops the two feet of freeboard and is associated with any of the following:
a) Sand, Gravel, and Stone Washing Operations
b) Dimension Stone Cutting operations
c) Crusher Dust Control Operations
No analytical monitoring is required for overflow from closed -loop process recycle (CLPR)
wastewater systems designed to operate with two feet of freeboard.
Closed -Loop Process Recycle Wastewater System ATC Requirement:
Authorization to construct and operate requirements (Part 11, Sections A and B) are not
applicable to a closed -loop process recycle wastewater systems that satisfy these design
criteria.
Part Ill Page 15 of 16 Pages

Permit No. NCG020000
4. BMP Conditions
a) The permittee shall utilize best management practices (BMPs) to ensure that contaminants
do not enter the surface waters as a result of blasting at the site.
b) Flocculants evaluated by the Division maybe used if administered in accordance with
maximum application doses and any other current requirements.
S. Residual Management
The residuals generated from treatment facilities used to meet the effluent limitations must be
disposed of in accordance with applicable standards and in a manner such as to prevent any
pollutants from such materials from entering waters of the state or navigable waters of the United
States.
Part III Page 16 of 16 Pages

Permit No. NCG020000
PART IV — STANDARD CONDITIONS FOR NPDES STORMWATER GENERAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedul
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing facilities already operating, but applying for coverage under this General Permit for the first
time: The Stormwater Pollution Prevention Plan shall be developed and implemented within 12
months of the effective date of the initial Certificate of Coverage issued pursuant to this General
Permit and updated thereafter on an annual basis. Secondary containment, as specified in Part 111,
Section A, Paragraph 3(c) of this permit, shall be accomplished within 1.2 months of the effective date
of the initial Certificate of Coverage.
New facilities applying for permit coverage for the first time and existing facilities previously
permitted and applying for renewal under this General Permit: All requirements, conditions,
limitations, and controls contained in this permit become effective immediately upon issuance of the
Certificate of Coverage. The Stormwater Pollution Prevention Plan shall be developed and
implemented prior to the beginning of discharges from the operation of the industrial activity and be
updated thereafter on an annual basis. Secondary containment, as specified in Part 111, Section A,
Paragraph 3(c) of this permit shall be accomplished prior to the beginning of discharges from the
operation of the industrial activity.
2. Duty —to -Comply
The permittee must comply with all conditions of this General Permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for certificate of
coverage termination, revocation and reissuance, or modification; or denial of a certificate of
coverage upon renewal application.
a. The permittee shall comply with standards or prohibitions established under section 307(a)
of the Clean Water Act for toxic pollutants within the time provided in the regulations that
establish these standards or prohibitions, even if the permit has not yet been modified to
incorporate the requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $25,000 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than 1 year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment
for not more than 3 years, or both. Also, any person who violates a permit condition may be assessed
an administrative penalty not to exceed $10,000 per violation with the maximum amount not to
exceed $1.25,000, [Ref: Section 309 of the Federal Act 33 USC 1319 and 40 CFR 122.41(a).]
c. Under state law, a daily civil penalty of not more than ten thousand dollars ($10,000) per violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General Statutes 143-215.6A]
d. Any person may be assessed an administrative penalty by the Director for violating section
301, 302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing
any of such sections in a permit issued under section 402 of the Act. Administrative penalties for
Class 1 violations are not to exceed $10,000 per violation, with the maximum amount of any Class l
penalty assessed not to exceed $25,000. Penalties for Class 11 violations are not to exceed $10,000
Parts IV, V, and VI Page 1 of 9 Pages

Permit No. NCG020000
per day For each day during which the violation continues, with the maximum amount of any Class li
penalty not to exceed $125,000.
3. Duty to Miti_gatf,
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
General Permit which has a reasonable likelihood of adversely affecting human health or the
environment.
4. Civil and Criminal Liability
Except as provided in Section D of this permit regarding bypassing of stormwater control facilities,
nothing in this General Permit shall be construed to relieve the permittee From any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3,143-215.6A, 1.43-215.6B, 143-
21.5.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may
be temporarily suspended.
5. Qil and_Hazard!2u5_Subatan.ce Liability
Nothing in this General Permit shall be construed to preclude the institution of any legal action or
relieve the permittee from any responsibilities, liabilities, or penalties to which the permittee is or
may be subject to under NCGS 143-215.75 et seq. or Section 311. of the Federal Act, 33 USC 1321.
6. ProeM Rights
The issuance of this General Permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any
invasion of personal rights, nor any infringement of federal, state or local laws or regulations.
7. Severability
The provisions of this General Permit are severable, and if any provision of this General Permit, or
the application of any provision of this General Permit to any circumstances, is held invalid, the
application of such provision to other circumstances, and the remainder of this General Permit, shall
not be affected thereby.
8. Duty to Provide Information
The permittee shall furnish to th'e Director, within a reasonable time, any information which the
Director may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating the certificate of coverage issued pursuant to this General Permit or to determine
compliance with this General Permit. The permittee shall also furnish to the Director upon request,
copies of records required to be kept by this General Permit.
9. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this General Permit
shall, upon conviction, be punished by a fine of not more than $10,000 per violation, or by
imprisonment for not more than two years per violation, or by both. If a conviction of a person is for
a violation committed after a first conviction of such person under this paragraph, punishment is a
fine of not more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or
both.
10. Penalties for Falsification of Rem
Parts IV, V, and VI Page 2 of 9 Pages

Permit No. NCGO20000
The Clean Water Act provides that any person who knowingly makes any false statement,
representation, or certification in any record or other document submitted or required to be
maintained under this General Permit, including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per violation,
or by imprisonment for not more than two years per violation, or by both.
SECTION B: GENERAL CONDITIONS
1. General Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to discharge beyond
the expiration date, the permittee shall submit forms and fees as are required by the agency
authorized to issue permits no later than 180 days prior to the expiration date. Any permittee that
has not requested renewal at least 180 days prior to expiration, or any permittee that does not have a
permit after the expiration and has not requested renewal at least 180 days prior to expiration, will
be subjected to enforcement procedures as provided in NCGS §143-2153.6 and 33 USC 1251 et. seq.
2. Transfers
The certificate of coverage issued pursuant to this General Permit is not transferable to any person
except after notice to and approval by the Director. The Director may require modification or
revocation and reissuance of the certificate of coverage to change the name and incorporate such
other requirements as may be necessary under the Clean Water Act. Permittee is required to
notify the Division within 90 days in the event the permitted facility is sold or closed.
3. When an Individual Permit May be Required
The Director may require any owner/operator authorized to discharge under a certificate of
coverage issued pursuant to this General Permit to apply for and obtain an individual permit or an
alternative General Permit. Any interested person may petition the Director to take action under this
paragraph. Cases where an individual permit may be required include, but are not limited to, the
following:
a. The discharger is a significant contributor of pollutants;
b. Conditions at the permitted site change, altering the constituents and/or characteristics of
the discharge such that the discharge no longer qualifies for a General Permit;
C. The discharge violates the terms or conditions of this General Permit;
d. A change has occurred in the availability of demonstrated technology or practices for the
control or abatement of pollutants applicable to the point source;
C. Effluent limitations are promulgated for the point sources covered by this General Permit;
f. A water quality management plan containing requirements applicable to such point sources
is approved after the issuance of this General Permit.
g. The Director determines at his or her own discretion that an individual permit is required.
4. When an Individual Permit Maybe Requested
Any permittee operating under this General Permit may request to be excluded from the coverage of
this General Permit by applying for an individual permit. When an individual permit is issued to an
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Permit No. NCG020000
owner/operator the applicability of this General Permit is automatically terminated on the effective
date of the individual permit.
Signatory Requirements
All applications, reports, or information submitted to the Director shall be signed and certified.
All notices of intent to be covered under this General Permit shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this
Section, a responsible corporate officer means: (a) a president, secretary, treasurer
or vice president of the corporation in charge of a principal business function, or any
other pet -son who performs similar policy or decision making functions for the
corporation, or (b) the manager of one or more manufacturing production or
operating facilities employing more than 250 persons or having gross annual sales
or expenditures exceeding 25 million (in second quarter 1.980 dollars), if authority
to sign documents has been assigned or delegated to the manager in accordance
with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, state, federal, or other public agency: by either a principal
executive officer or ranking elected official.
b. All reports required by the General Permit and other information requested by the Director
shall be signed by a person described above or by a duly authorized representative of that
person. A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility
for the overall operation of the regulated facility or activity, such as the position of
plant manager, operator of a well or well field, superintendent, a position of
equivalent responsibility, or an individual or position having overall responsibility
for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.);
and
(3) The written authorization is submitted to the Director.
C. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification; which shall not be modified in any way:
"I certify, under penalty of law, that this document and all attachments were prepared under
my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on illy inquiry of
the person or persons who manage the system, or those pet -sons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for
knowing violations."
6. QenCEal Permit Modification. Revocation and Reissuance. or Termination
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Permit No. NCG020000
The issuance of this General Permit does not prohibit the Director from reopening and modifying the
General Permit, revoking and reissuing the General Permit, or terminating the General Permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts
122 and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North
Carolina General Statute 143-215.1 et. al.
After public notice and opportunity for a hearing, the General Permit may be terminated for cause.
The filing of a request for a General Permit modification, revocation and reissuance, or termination
does not stay any General Permit condition. The certificate of coverage shall expire when the General
Permit is terminated.
Certificate of Coverage Actions
The certificate of coverage issued in accordance with this General Permit may be modified, revoked
and reissued, or terminated for cause. The notification of planned changes or anticipated
noncompliance does not stay any General Permit condition.
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment
and control (and related appurtenances) which are installed or used by the permittee to achieve
compliance with this General Permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the
operation of back-up or auxiliary facilities or similar systems which are installed by a permittee only
when the operation is necessary to achieve compliance with the General Permit.
Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity in order to maintain compliance with the condition of this
General Permit.
3. Bypassing of Stormwater Control Facilities
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass
unless:
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage;
and
There were no feasible alternatives to the bypass, such as the use of auxiliary control
facilities, retention of stormwater or maintenance during normal periods of equipment
downtime or dry weather. This condition is not satisfied if adequate backup controls should
have been installed in the exercise of reasonable engineering judgment to prevent a bypass
which occurred during normal periods of equipment downtime or preventive maintenance;
and
C. The permittee submitted notices as required under Section E of this Part.
If the Director determines that it will meet the three conditions listed above, the Director may
approve an anticipated bypass after considering its adverse effects.
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Permit No. NCG020000
SECTION D: MONITORING AND RECORDS
Representative SaInDlin
Samples collected and measurements taken, as required herein, shall be characteristic of the volume
and nature of the permitted discharge. Analytical sampling shall be performed during a
representative storm event. Samples shall be taken on a day and time that is characteristic of the
discharge. All samples shall be taken before the discharge joins or is diluted by any other waste
stream, body of water, or substance.
Recording Results
For each measurement, sample, inspection or maintenance activity performed or collected pursuant
to the requirements of this General Permit, the permittee shall record the following information:
a. The date, exact place, and time of sampling, measurements, inspection or maintenance
activity;
b. The individual(s) who performed the sampling, measurements, inspection or maintenance
activity;
C. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted
scientific practices shall be selected and used to ensure the accuracy and reliability of measurements
of the volume of monitored discharges.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published
pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations
published pursuant to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as
Amended, and Regulation 40 CFR 136.
To meet the intent of the monitoring required by this General Permit, all test procedures must
produce minimum detection and reporting levels and all data generated must be reported down to
the minimum detection or lower reporting level of the procedure.
5. Representative Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that
are required to be sampled, the permittee may petition the Director for representative outfail status.
If it is established that the stormwater discharges are substantially identical and the permittee is
granted representative outfail status, then analytical sampling requirements may be performed at a
reduced number of outfalls.
6. Records Retention
Qualitative monitoring shall be documented and records maintained at the facility along with the
Stormwater Pollution Prevention Plan. Copies of analytical monitoring results shall also be
maintained on -site. The permittee shall retain records of all monitoring information, including all
calibration and maintenance records and all original strip chart recordings for continuous
monitoring instrumentation, and copies of all reports required by this General Permit for a period of
Parts IV, V, and VI Page 6 of 9 Pages

Permit No. NCG020000
at least 5 years from the date of the sample, measurement, report or application. This period may be
extended by request of the Director at any time. If this volume of records cannot be maintained on -
site, the documents must be made available to an inspector upon request as immediately as possible.
Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized
contractor acting as a representative of the Director), or in the case of a facility which discharges
through a municipal separate storm sewer system, an authorized representative of a municipal
operator or the separate storm sewer system receiving the discharge, upon the presentation of
credentials and other documents as may be required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this General Permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the
conditions of this General Permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this General Permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring General Permit
compliance or as otherwise authorized by the Clean Water Act, any substances or
parameters at any location.
SECTION E: REPORTING REQUIREMENTS
Discharge Monitoring Reports
Samples analyzed in accordance with the terms of this permit shall be recorded on Discharge
Monitoring Report (DMR) forms provided by the Director, Annual Summary DMRs shall be delivered
to the Division (Central Office) no later than March 1 of each year (See 2. of this Section). In
addition, any samples analyzed in accordance with the terms of this permit that violate a
wastewater effluent limit or exceed a stormwater benchmark value shall be submitted to the
Division Regional Office on a DMR form and delivered to Division Central Files no later than 30
days from the date the facility receives the sampling results from the laboratory.
When no discharge has occurred from one or more outfalls during the report period, the permittee is
required to record "NO FLOW" or "NO DISCHARGE" in the SPPP within 30 days of the end of the
sampling period."No Flow" or "No Discharge" information shall be reported on the Annual Report
DMR.
The permittee shall record the required qualitative monitoring observations on the SDO Qualitative
Monitoring Report form provided by the Division, and shall retain the completed forms on site.
Qualitative monitoring results should not be submitted to the Division, except upon DWQ's specific
direction to do so.
The permittee shall include the signed certification statement described in Part 1V, Section B.S.c.
Submitting Reports (3 copies)
Two signed copies of an Annual Summary Discharge Monitoring Report (DMR) shall be submitted to
DWQ no later than March 1 of each year. They shall be submitted to:
Central Files
Division of Water Quality
1617 Mail Service Centel -
Raleigh, North Carolina 27699-1617
Parts IV, V, and VI Page 7 of 9 Pages

Permit No. NCG020000
One signed DMR form with wastewater effluent limit violations or benchmark value exceedences
shall be sent to the appropriate DWQ Regional Office no later than 30 days from the date the
facility receives the sampling results from the laboratory.
One copy of all tiered (stor'rnwater) response forms shall also be sent to the appropriate DWQ
Regional Office no later than 30 days from the date the facility receives the sampling results
from the laboratory. All stormwater outfall parameters shall be monitored and recorded during
that monitoring period.
Addresses for each RO and the counties covered by each RO can be found here:
httl2://www.enr.state.nc.us/html/regionaloffiices.htmi. The permittee shall retain the completed
originals on site. Qualitative monitoring results should not be submitted to the Regional Offices or
Central Files unless specifically requested by DWQ.
3. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the
Federal Act, 33 USC 131.8, all reports prepared in accordance with the terms shall be available for
public inspection at the offices of the Division of Water Quality. As required by the Act, analytical
data shall not be considered confidential. Knowingly making any false statement on any such report
may result in the imposition of criminal penalties as provided for in NCGS 143-215.613 or in Section
309 of the Federal Act,
4. Non-Stormwater Discharges
If the storm event monitored in accordance with this General Permit coincides with a non-
stormwater discharge, the permittee shall separately monitor all parameters as required under the
non-stormwater discharge permit and provide this information with the stormwater discharge
monitoring report.
Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned changes at the
permitted facility which could significantly alter the nature or quantity of pollutants discharged. This
notification requirement includes pollutants which are not specifically listed in the General Permit or
subject to notification requirements under 40 CFR Part 122.42 (a).
Anticipated Noncom h!� .ance
The permittee shall give notice to the Director as soon as possible of any planned changes at the
permitted facility which may result in noncompliance with the General Permit requirements.
Bypass
a. Anticipated bypass. If the permittee knows in advance of the need fora bypass, it shall
submit prior notice, if possible at least ten days before the date of the bypass; including an
evaluation of the anticipated quality and affect of the bypass.
b. Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware
of an unanticipated bypass.
Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance
which may endanger health or the environment. Any information shall be provided orally within 24
Parts IV, V, and VI Page 8 of 9 Pages

Permit No. NCG020000
hours from the time the permittee became aware of the circumstances. A written submission shall
also be provided within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period
of noncompliance, including exact dates and times, and if the noncompliance has not been corrected,
the anticipated time compliance is expected to continue; and steps taken or planned to reduce,
eliminate, and prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been
received within 24 hours.
9. Spills
The permittee shall report to the local DWQ Regional Office, within 24 hours, all significant spills as
defined in Part VII of this permit. Additionally, the permittee shall report spills including: any oil spill
of 25 gallons or more, any spill regardless of amount that causes a sheen on surface waters, any oil
spill regardless of amount occurring within 100 feet of surface waters, and any oil spill less than 25
gallons that cannot be cleaned up within 24 hours.
1.0. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under 24 hour reporting at
the time monitoring reports are submitted.
11.. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in a Notice of Intent to
be covered under this General Permit or in any report to the Director, it shall promptly submit such
facts or information.
PART V - LIMITATIONS REOPENER
This General Permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) Cc), and (d), 304(b)
(2) and 307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or
approved:
a. Contains different conditions or is otherwise more stringent than any effluent limitation in the
General Permit; or
b. Controls any pollutant not limited in the General Permit.
The General Permit as modified or reissued under this paragraph shall also contain any other requirements in
the Act then applicable.
PART VI - ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being
billed by the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4)
may cause this Division to initiate action to revoke the Certificate of Coverage.
Parts IV, V, and VI Page 9 of 9 Pages

Permit No. NCG020000 '
PART Vll - DEFINITIONS
1. Act
See Clean Water Act.
2. Adverse Weather
Adverse conditions are those that are dangerous or create inaccessibility for personnel, such as local
flooding, high winds, or electrical storms, or situations that otherwise make sampling impractical.
When adverse weather conditions prevent the collection of samples during the sample period, the
permittee must take a substitute sample or perform a visual assessment during the next qualifying
storm event. Documentation of an adverse event and the rationale must be included with your SPPP
records. Adverse weather does not exempt the permittee from having to file a monitoring report in
accordance with the sampling schedule. Adverse events and failures to monitor must be explained on
the Annual Summary DMR Report and recorded and explained in the SPPP records.
3. Arithmetic Mean
The arithmetic mean of any set of values is the summation of the individual values divided by the
number of individual values.
4. Allowable Non-Stormwater Discharges
a. This permit regulates stormwater discharges. Non-stormwater discharges which shall be
allowed in the stormwater conveyance system are:
(a) All other discharges that arc authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner cond ensate
without added chemicals, springs, discharges of uncontaminated potable
water, waterline and fire hydrant flushings, water From footing drains, flows
from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -Fighting training.
5. Be5t Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may
take the form of process, activity, or physical structure. More information on BMPs can be found at:
http://cfpub.epa.gov/npdcs/stormwater/iiienuofbnnps/index.cfm.
6. Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility
including the collection system, which is not a designed or established operating mode for the facility.
7. Bulk Storage of liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above
ground storage container having a capacity of greater than 660 gallons or with multiple above
ground storage containers located in close proximity to each other having a total combined storage
capacity of greater than 1,320 gallons.
8. Certificate of Coverage
Part VII Page 1 of 6

Permit No. NCGO2O000
The Certificate of Coverage (COC) is the cover sheet which accompanies the General Permit upon
issuance and lists the facility name, location, receiving stream, river basin, effective date of coverage
under the permit and is signed by the Director.
9. Clean Water Act
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, ct. seq.
10. Division or DWO
The Division of Water Quality, Department of Environment and Natural Resources.
11. Director
The Director of the Division of Water Quality, the permit issuing authority.
12, EMC
The North Carolina Environmental Management Commission.
13. Grab Sample
An individual sample collected instantaneously. Grab samples that will be analyzed (quantitatively
or qualitatively) must be taken within the first 30 minutes of discharge.
14. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
15. Inactive-MiningInactive-Mining 0 eration
Mining Sites that are not being actively mined, but which have an identifiable owner/operator;
inactive mining sites do not include sites where mining claims are being maintained prior to
disturbances associated with the extraction, benefaction, or processing of mined materials, nor sites
where minimal activities are undertaken for the sole purpose of maintaining a mining claim.
16. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a
land treatment facility, a surface impoundment, an injection well, a hazardous waste long-term
storage facility or a surface storage facility.
17. Mine Dewatering Wastewater
Mine Dewatering Wastewater includes any water that is impounded in, or that collects in, the mine
and is pumped, drained or otherwise removed from the mine through the efforts of the mine
operation. In Construction Sand and Gravel or Industrial Sand mines, "mine dewatering"
wastewater also includes wet pit overflows caused solely by direct rainfall and groundwater seepage.
Discharges of commingled process wastewater and mine dewatering wastewater from the facilities
shall be deemed discharges of process wastewater.
Part VII Page 2 of 6

Permit No. NCG020000
18. Municipal Separate Storm Sewer System
A stormwater collection system within an incorporated area of local self-government such as a city or
town.
19. No Exposure
A condition of no exposure means that all industrial materials and activities are protected by a storm
resistant shelter or acceptable storage containers to prevent exposure to rain, snow, snowmelt, or
runoff. Industrial materials or activities include, but are not limited to, material handling equipment
or activities, industrial machinery, raw materials, intermediate products, by-products, final products,
or waste products. DWQ may grant a No Exposure Exclusion from NPDES Stornnvater Permitting
requirements only if a facility complies with the terms and conditions described in 40 CFR
§122.26(g)
20. Notice -of Intent
The state application form which, when submitted to the Division, officially indicates the Facility's
notice of intent to seek coverage under a General Permit.
21. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsoil or similar naturally -occurring surface materials that are not disturbed by mining operations
22. Permittee
The owner or operator issued a certificate of coverage pursuant to this General Permit.
23. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe,
ditch, channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be
discharged to waters of the state.
24. Process Wastewater
Process Wastewater includes any wastewater used in the slurry transport, washing, sawing of mined
material, air emissions control or processing exclusive of mining. This water shall also include any
other water which becomes commingled with such wastewater in a pit, pond, lagoon, mine or other
treatment facility for such wastewater.
25. Representative Storm Event
A representative storm event for the purposes of this general permit is a storm event that measures
greater than 0.1 inches of rainfall. The time between this storm event and the previous storm event
measuring greater than 0.1 inches must be at least 48 hours. One storm event may have a time period
with no precipitation. This time period may last up to 10 hours. For example, if it rains but stops
before producing any collectable discharge, a sample may be collected if the next rain producing a
discharge begins within 10 hours.
26. Representative Outfall Status
When it is established that the discharge of stormwater runoff from a single outfall is representative
of the discharges at multiple outfalls, the DWQ may grant representative outfall status.
Part Vli Page 3 of 6

Permit No. NCG020000
Representative outfall status allows the permittee to perform analytical monitoring (and in some
cases qualitative monitoring) at a reduced number of outfalls.
27, Rinse Water Discharge
The discharge of rinse water from equipment cleaning areas associated with industrial activity.
Rinse waters from vehicle and equipment cleaning areas are process wastewaters and do not include
washwaters utilizing any type of detergent or cleaning agent.
28. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus
sufficient freeboard to allow for the 25-year, 24-hour storm event.
29. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. is listed in 40 CFR 372.6S pursuant to Section 313 of Title 1]1 of the Superfund Amendments
and Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community
Right -to -Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title 111, Section 313
reporting requirements; and
Meets at least one of the following criteria:
(1) Is listed in appendix D of 40 CFR Part 122 on Table 11 (organic priority pollutants),
Table III (certain metals, cyanides, and phenols) or Table 1V (certain toxic pollutants
and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40
CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
30. Severe Property Damage
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production.
31. Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or
production; hazardous substances designated under section 101(14) of CERCLA; any chemical the
facility is required to report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and
waste products such as ashes, slag and sludge that have the potential to be released with stormwater
discharges.
32. Significant SSnills
Part VII Page 4 of 6

Permit No. NCGO20OOO
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable
quantities under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117,21) or section
102 of CERCLA (Ref: 40 CFR 302.4).
33. Stormwater Discharge Outfall (SDO).
The point of departure of Stormwater from a discernible, confined, or discrete conveyance, including
but not limited to, storm sewer pipes, drainage ditches, channels, spillways, or channelized collection
areas, from which stormwater flows directly or indirectly into waters of the State of North Carolina.
34. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall
or as a result of snowmelt.
35. Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and
which is directly related to manufacturing, processing or rate material storage areas at an industrial
site. Facilities considered to be engaged in "industrial activities" include those activities defined in
40 CFR 122.26(b)(14). The term does not include discharges from facilities or activities excluded
from the NPDES program.
36. Stormwater Pollution Prevention Plan
A comprehensive site -specific plan which details measures and practices to reduce stormwater
pollution and is based on an evaluation of the pollution potential of the site.
37. Total Flow
The flow corresponding to the time period over which the entire storm event occurs. Total flow shall
be either; (a) measured continuously, (b) calculated based on the amount of area draining to the
outfall, the amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated
by the measurement of flow at 20-minute intervals during the rainfall event.
38. Total Maximum Daily Load (TMDL).
TMDLs are written plans for attaining and maintaining water quality standards, in all seasons, for a
specific water body and pollutant. (A list of approved TMDLs for the state of North Carolina can be
found at http://hZo.enr.state.nc.us/tmdl/)
39. Toxic Pollutant
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
40. Treatment Facilities
Treatment facilities include any pit, pond, lagoon, basin, mine or containment structure used to treat
or contain process wastewater generated on mine sites. They must be used to meet Effluent
Limitations and are not Stormwater Best Management Practices (BMPs).
41. Vehicle Maintenance Activity
Part VII Page 5 of 6

Permit No. NCG020000
Vehicle or vessel rehabilitation, mechanical repairs, painting, fueling, lubrication, cleaning
operations, or airport deicing operations.
42. Visibie Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water,
air, gravity, or ice from its site of origin which can be seen with the unaided eye.
43. 225--year. 24 hourstorm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once
in 25 years.
Part VII Page 6 of 6

GF WA rFR Michael F. Easley, Governor
�C� QG William G. Ross Jr., Secretary
r North Carolina Departmeni of Environment and Natural Resources
❑ Alan W. Klimek, P.l;, Director
Division of Water Quality
March 11, 2005
Mr. Warren Paschal
General Shale Brick, Inc.
1600 Colon Road
Sanford, NC 27330
Dear 14tr: Paschal:
Subject: NPDES General Permit NCG020000
Certificate of Coverage NCG020354
General Shale Brick, Inc.
Formerly Cherokee Sanford Group, L.LC
Chatham County
Division personnel have reviewed and approved your request to change your name under the General Permit,
received on March 7, 2005.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the General
Permit remain unchanged and in full effect. 11is revised Certificate of Coverage is issued under the requirements of
North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S.
Environmental Protection Agency.
If you have any questions, please contact the Stormwater Permitting Unit at [phone], extension 502.
Sincerely,
ORIGINAL SIGNED BY
BRADI-Ev n—ENNIBTT
,Alan W. Klimek P. E. -
cc: DWQ Central Files
Raleigh Regional Office, Water Quality Section
Stormwater Permitting Unit
NUrih Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617
Internet: h2o.enr.sfate nc.us 5I2 N. Salishury St. Raleigh, NC 27604
N� thCarolina
,A7at1rr1711!1
Phone [phone] Customer Service
FAX [phone]
An Equal OpportunityfAffirmative Action Employer — 50% Recycled110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG020000
CERTIFICATE OF COVERAGE No. NCG020354
STOR-MWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Conunission, and the
Federal Water Pollution Control Act, as amended,
GENERAL SHALE BRICK, INC
is hereby authorized to discharge stormwater from a facility located at
GENERAL SHALE BRICK, INC
FLATWOODS ROAD
MONCURE
CHATHAM COUNTY
to receiving waters designated as an unnamed tributary to Gulf Creek, a class WS-IV stream, in the Cape rear River
Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1,
I1, III, 1V, V, and VI of General Permit No. NCG020000 as attached.
This certificate of coverage shall become effective March 11, 2005.
This Certificate of Coverage shall remain in'effect for the duration of the General Permit.
Signed this day March 11, 2005. ORIGINAL SIGNED BY
BRADLEY BENNETT
E
Alan W. Klimek, Director
Division of Water Quality
By Authority of the Environmental Management Commission

Michael F. Easley, Governor
William G, Ross Jr., Secretary
North Carolina Department ol' Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
February 7, 2005
J Warren Paschal
Cherokee Sanford Group LLC
1600 Colon Rd
Sanford, NC 27330
Subject: NPDES Stormwater Permit Coverage Renewal
Cherokee Sanford Group LLC
COC Number NCG020354
Chatham County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG020000 the Division of Water
Quality (DWQ) is forwarding herewith the reissued stormwater general permit. Please review the new permit to familiarize
yourself with the changes in the reissued permit. The general permit authorizes discharges of stormwater and some types of
wastewater. You must meet the provisions of the permit for the types of discharges present at your facility. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1963.
The following information is included with your permit package:
• A new Certificate of Coverage
• A copy of General Stormwater Permit NCG020000
• A copy of a Technical Bulletin for the general permit
• Five copies of Discharge Monitoring Report (DMR) Forms - wastewater and stormwater
Five copies of Qualitative Monitoring Report Form
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require modification
or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other
permits which may be required by DENR or relieve the permittee from responsibility for compliance with any other applicable
federal, state, or local law, rule, standard, ordinance, order, judgment, or decree.
If you have any questions regarding this permit package please contact Ken Pickle of the Central Office Stormwater Permitting
Unit at [phone], ext.584.
Sincerely./
/l�t �{ SI�,�' G9
Jor Alan W. Klimek, P.E.
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
One
NorthCarolina
✓1117111 A11f
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phonc [phone] Customer Service
Internet: h2o.enr.state.nc.uslsulstormwater.html 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone].623.6748
An Equal Opportunity/Affirmative Action Employer— 50% Recycledl10% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO, NCG020000
CERTIFICATE OF COVERAGE No. NCG020354
STORMWATER AND PROCESS WASTEWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and
the Federal Water Pollution Control Act, as amended,
Cherokee Sanford Group LLC
is hereby authorized to discharge stormwater and to operate treatment systems and discharges associated
with mine dewatering wastewater and process wastewater from a facility located at
Cherokee Sanford Group LLC
Flatwoods Rd
Moncure
Chatham County
to receiving waters designated as a UT of Gulf Creek, a class WS-IV stream in the Cape Fear River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
II, III, IV, V, and VI of General Permit No. NCG020000 as attached.
This certificate of coverage shall become effective February 7, 2005.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day February 7, 2005
,3f _
for Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

Cherokee Sanford. -Brick
Certified Mail #Z347941570
March 7, 2000
Mr. Kerr Stevens, Director
Division of Water Quality
NCDENR
P. O. Box 27867
Raleigh, NC 27611-7686
Re: Cherokee Sanford Group, LLC
Permit No. WQ0007589, Brickhaven No. 2 Wastewater Spray Irrigation, Chatham County
Storm Water Permit No. NCG070091, Moncure Facility & Mine, Chatham County - -0,1
Storm Water Permit No. NCG020354, Brickhaven No. 2 Mine, Chatham County -
Storm Water Permit No. NCG070154, Sanford Facility & Mine, Lee County -a��n
Storm Water Permit No. NCG070089, Lee County Facility & Mine, Lee County e
Dear Mr. Stevens:
The purpose of this letter is to advise the North Carolina Department of Environment and Natural
Resources of change in the ownership of Cherokee Sanford Group, LLC ("CSG") which holds the
above referenced water quality permits. On or about February 10, 2000, CSG, a Delaware Limited
Liability Company, was sold to General Shale Products, LLC, a Delaware Limited Liability Company.
A name change will not occur as a result of the change in ownership.
The new officers of CSG are as follows:
President and CEO - Richard L. Green
Vice President of Finance - Richard F. Ray
Vice President - Kenneth A. Parham
Vice President - Walter Banyas
Secretary - James C. Widener
Treasurer - J. Edward Knight
Assistant Treasurer -Mike McCreary
Assistant Secretary - J. Edward Knight
The address for each of these officers is:
P.O. Box 3547 ;
Johnson City, TN 37602
1600 Colon Road • Sanford, North Carolina 27330 • [phone] - 800-277-2700 • Sales Fax,
(9r19j-77'd'6634
Our concern for the environment ... ��J ... means using recycled paper!

The new directors of CSG are as follows:
Richard L. Green - Chairman
Walter Banyas
Kenneth A. Parham
Richard F. Ray
Please feel free to contact me at 919.774.5306 should you have any questions or wish to discuss the
information provided.
Sincerely,
wo�� RLI-a�
Warren Paschal, Director of Environmental Compliance
Cherokee Sanford Group, LLC
cc: Walt Banyas, General Shale Products, LLC

State of North Carolina
Department of'Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
October 4, 1996
Mr. J. Warren Paschal
Cherokee Sanford Group, LLC
1600 Colon Road
Sanford, NC 27330
4••
F:
Subject: General Permit No. NCG020000
Brickhaven Mine #2
COC NCG020354
Chatham County
Dear Mr. Mr. Paschal:
In accordance with your application for discharge permit received on July 15, 1996, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you. you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Water Quality. The Division of Water Quality may require modification or revocation and reissuanee of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Miinagement
Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Steve Ulmer at telephone number 919/733-
5083, extension 545.
Sincerely,
OFMNAL S1GNM BY
BRAMEY BENNETT
A. Preston How,,frd, Jr., P. E.
cc: Raleigh Regional Office
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

It
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG020000
CI R'duCATE OF COVERAGE NO. NCGO20354
STORNIWATER, MINTS: DEWATERING. AND/OR OVERFLOW FROM
PROCESS WATER RECYCLES SYSTEMS DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELINTINA'I'ION SYSTEM
III compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promrlgatcd and adopted by the North Carolina Environmental Commission, and the
Federal Water pollution Control Act, as amended.
Cherokee Sanford Group, El_C
is hereby authorized to operate or continue ol)Lration of a treatment system for mine de+v;rtering and storrnwatcr front
a facility located at
13rickImven 1y1ine4'2
Flatwoods Road
rN1ortcurc
Chatham County
to receiving waters designated .rs an unnamed tributary to Gulf Creek in the Cape fear River Basin
in accordance with the of fluent limitations, nlonitorinb rcyuiremcnts, and other conditions set forth in farts 1, If, 111
and IV of General Permit No. NCG020000 as attached.
This Certificate of Cover�rge shall become effectivc October 4, I996.
This Certificate of Coveragc shall remain in effect I -or the duration of ike General Permit.
Sh,NlU i this day Octol,<r 4, I996.
13RAMEY BENNETT
A. Preston Howard, Jr- P.1 ., Director
Divislon of Water (Inapt.
By Awhority ul the Managc;nront Commission

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NPDES FACILITY AND PERMIT DATA 09/04/96 17:21:37
UPDATE OPTION TRXID 5NU KEY NCG020354
PERSONAL DATA FACILITY APPLYING FOR PERMIT REGION
FACILITY NAME) CHEROKEE SANFORD GRP-BRICKH 2 COUNTY> CHATHAM 05
ADDRESS: MAILING (REQUIRED) LOCATION CREQUIRED)
STREET: 1600 COLON ROAD STREET: FLATWOODS ROAD
CITY: SANFORD ST NC ZIP 27330 CITY: MONCURE ST NC ZIP 27330
TELEPHONE [phone] DATE FEE PAID: 07/15/96 AMOUNT: 400.00
STATE CONTACT> ULMER PERSON IN CHARGE J WARREN PASCHAL
1=PROPOSED,2=EXIST,3=CLOSED 1 1=MAJOR,2=MINOR 2 1=MUN,2=NON-MUN 2
LAT: 3535200 LONG: 07901000 N=NEW,M=MODIFICATION,R=REISSUE> N
DATE APP RCVD 07/15/96 WASTELOAD REQS
DATE STAFF REP REQS 08/01/96 WRSTELOAD RCVD
DATE STAFF REP RCVD 08/30/96 SCH TO ISSUE
DATE TO P NOTICE / / DATE DRAFT PREPARED 09/01/96
DATE OT AG COM REQS / / DATE DENIED
DATE OT AG COM RCVD / / DATE RETURNED /
DATE TO EPA / / DATE ISSUED !a /D/ -?(ASSIGN/CHANGE PERMIT
DATE FROM EPA / / EXPIRATION DATE ae/3J/9 ix
FEE CODE C 0 ) 1=(>10MGD),2=(>1MGD),3=(>0,1MGD),4=(<O,1MGD),5=SF,6=CGP25,64,79),
7=(GP49,73)8=(GP76)9=(GP13,34,30,52)0=(NOFEE) DIS/C 73 CONBILL C
COMMENTS:
MESSAGE:* ENTER DATA FOR UPDATE*

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